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MO-28442_47696_CA_IAR_20210115_Initial Abatement Action Report
TERRAut ENVIRONMENTAL CONSULTANTS, P.C. INITIAL ABATEMENT ACTION REPORT Details the November 2020 UST Closure and Soil Excavation BARBARA LINKER ET AL PROPERTY 1238 UNION ST. S CONCORD, NC 27217 Latitude: 35.378049' N Longitude:-80.551330' W Release Information Date Discovered: November 20, 2020 (Lab Confirmed) Estimated Release Quantity: Unknown Release Cause/Source: Non-commercial UST System Registered UST Capacities: (1) 550-gallon heating oil Facility ID: Not Applicable NCDWM-UST Incident No.: Pending NCDWM-UST Risk Ranking: Pending Responsible Party & Property Owner Barbara Linker 100 Krimminger Ave. SE Concord, NC 28025 Terraquest Project No. 16820 January 15, 2021 100 East Ruffin Street • Mebane, North Carolina 27302 Telephone (919) 563-9091 - Facsimile (919) 563-9095 www.terraquestpc.com CERTIFICATION FOR THE SUBMITTAL OF AN ENVIRONMENTAL / GEOLOGICAL ASSESSMENT Attached is the Initial Abatement Action Report for: Responsible Party: Barbara Linker et al Address: 100 Kimminger Ave. SE City: Concord State: NC Zip Code: 28025 Site Name: Barbara Linker et al Property Address: 1238 Union St. S City: Concord State: NC Zip Code: 28025 I, Jonathan R. Grubbs, a Licensed Geologist in the State of North Carolina for TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. do hereby certify that I am familiar with and have reviewed all material including figures within this report and that to the best of my knowledge the data, site assessment, figures, and other associated materials are correct and accurate. All work was performed under my direct supervision. My seal and signature are affixed below. Terraquest Environmental Consultants, P.C. is licensed to practice geology and engineering in North Carolina. The geology certification number of the corporation is C-291. The engineering certification number of the corporation is C-4634. Engineering is practiced out of the Cary, NC office. TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. , 2-:> -4- Ryan D. Kerins Project Manager sm z =o ; lip RE _ •#,•,glotN,%%%� Jonathan R. Grubbs, P.G. Vice President Initial Abatement Action Report Prepared by: Terraquest Environmental Consultants, P.C. Prepared on: January 15, 2021 i Barbara Linker et al Property 1238 Union St. S Concord, Cabarrus County, NC TABLE OF CONTENTS 1.0 INTRODUCTION................................................................................................................... 1 2.0 UST REMOVAL & RELEASE DISCOVERY............................................................................... 1 3.0 REMEDIAL EXCAVATION..................................................................................................... 2 4.0 GROUNDWATER INVESTIGATION....................................................................................... 3 5.0 FREE PRODUCT CHECK........................................................................................................ 3 6.0 POTENTIAL SOURCES OF PETROLEUM HYDROCARBONS................................................... 4 7.0 NATURE AND ESTIMATED QUANTITY OF RELEASE............................................................. 4 8.0 SITE AND VICINITY DESCRIPTION........................................................................................ 4 9.0 CONCLUSIONS/RECOMENDATIONS....................................................................................5 10.0 LIMITATIONS.......................................................................................................................5 REFERENCES.................................................................................................................................... 7 TABLES: 1. Summary of Soil Sampling Results FIGURES: 1. Site Location Map 2. Site Layout and Closure Soil Sample Map APPENDICES: A. Environmental Acronyms and Technical Methods / Standard Procedures B. Analytical Report C. Residual Liquid, UST Disposal, and Soil Disposal Manifests D. UST-61 24-Hour Release and UST Leak Reporting Form Initial Abatement Action Report Barbara Linker et al Property Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S Prepared on: January 15, 2021 ii Concord, Cabarrus County, NC 1.0 INTRODUCTION On behalf of the responsible party, Barbara Linker et al, Terraquest Environmental Consultants, P.C. has prepared this Initial Abatement Action Report for the Barbara Linker et al property located at 1238 Union St. S in Concord, Cabarrus County, North Carolina. This report documents the closure of a 550-gallon heating oil UST and subsequent excavation of contaminated soil in November 2020. The site's location and layout are depicted in Figures 1 and 2. Environmental acronyms used in this report are detailed in Appendix A along with Terraquest's technical methods and standard procedures. 2.0 UST REMOVAL & RELEASE DISCOVERY The UST was installed off the southwest side of the residence during its construction in 1965 and was replaced with an aboveground storage tank (AST) in the 1990's. On November 18, 2020 prior to excavating the tank, Terraquest supervised the removal of 425 gallons of residual liquid composed mostly of water from the UST by CCI of Salisbury, NC. The 550-gallon heating oil tank was buried approximately 20 inches below ground level (BGL) and was excavated and taken offsite for environmentally -sound disposal by CCI on November 18, 2020. The dimensions of the UST were 46 inches wide by 74 inches long. The tank's former location is shown on Figure 2. Following UST removal, Terraquest inspected the UST and noted holes up to 1.4-inch in size along the sides and seams. Terraquest collected a soil sample CS1 from beneath the UST at a depth of 5.5 feet BGL. The soil sample was screened using a photoionization detector (PID) and revealed the presence of heating -oil type contaminants with a detected measurement of 397.1 parts per million (ppm). This screening measurement coupled with the stained soil and noted holes in the UST indicated a release of heating oil had occurred from the UST. The CS1 soil sample collected for analysis was placed in the proper laboratory -prepared sampling containers, labeled with the Initial Abatement Action Report Barbara Linker et al Property Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S Prepared on: January 15, 2021 1 Concord, Cabarrus County, NC project name, project number, sample identification, required analysis, and date and time of collection. The sample was immediately placed on ice and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation was maintained for the soil sample prior to an analysis using a UVF Trilogy unit for TPH Diesel -Range Organics (DRO) and Gasoline -Range Organics (GRO). Analytical results of the CS1 soil sample revealed contaminant concentrations above the North Carolina Department of Environmental Quality Division of Waste Management UST Section (NCDEQ DWM-UST) Actions Limits for both the TPH GRO and DRO methods. Table 1 summarizes the sample depth and detected concentrations of the CS1 soil sample. The locations of the soil sample is identified in Figure 2. The complete analytical report is included in Appendix B. 3.0 REMEDIAL EXCAVATION With the PID screening measurement, stained soil, and noted holes, Michael Linker, a representative of the property owner, directed Terraquest to supervise the excavation of contaminated soil beneath and surrounding the former heating oil UST. The impacted soil was excavated using a mini excavator to a depth of seven feet BGL where bedrock was encountered. All of the contaminated soil above the bedrock and from the sidewalls was removed. Soil samples SW1 through SW4 were collected at the sidewall limits and sample BE1 was collected at the base of the excavation from soils immediately above the bedrock prior to their removal. The SW1 through SW4 and BE1 soil samples collected for analysis were placed in the proper laboratory - prepared sampling containers, labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples were immediately placed on ice and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation was maintained for the soil samples. The SW1 through SW4 soil samples were analyzed using a UVF Trilogy unit for TPH DRO and GRO. The BE1 soil sample was submitted to a NC -certified laboratory for analysis per EPA Method 8260 + MTBE + IPE (volatile organics), EPA Method 8270 Base Neutral and Acid Extractable (semi -volatile Initial Abatement Action Report Prepared by: Terraquest Environmental Consultants, P.C. Prepared on: January 15, 2021 2 Barbara Linker et al Property 1238 Union St. S Concord, Cabarrus County, NC organics), Massachusetts Department of Environmental Protection (MADEP) methods for volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH). The four sidewall samples SW1 through SW4 results were either below the NCDEQ DWM-UST Actions Limits or the laboratory's sample method detection limits. The BE1 base of excavation sample was above the TPH Action Limits and had detected concentrations above the Soil -to - Groundwater Maximum Soil Contaminant Concentrations (S-t-G MSCCs) and Residential MSCCs. Soil contamination was excavated down to the bedrock surface and all of the excavatable contaminated soil was removed in the base and sidewalls of the former UST basin. The limits of the final excavation measured nine feet wide by sixteen feet long. Table 1 summarizes the sample depth, PID measurements, and detected concentrations of the soil samples. The locations of the soil samples are identified in Figure 2. The complete analytical reports are included in Appendix B. Fill dirt obtained from Keller Dirt and Gravel of Kannapolis, NC was used to backfill the excavation. Two loads of contaminated soil totaling 32.65 tons were removed and taken offsite for disposal at Alternative Energy Solutions of NC, LLC in Thomasville, NC. The weight -certified soil disposal manifests are provided in Appendix C. 4.0 GROUNDWATER INVESTIGATION Groundwater was not encountered or investigated as part of this phase of field work. 5.0 FREE PRODUCT CHECK Free product was not encountered during site activities. Initial Abatement Action Report Barbara Linker et al Property Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S Prepared on: January 15, 2021 3 Concord, Cabarrus County, NC 6.0 POTENTIAL SOURCES OF PETROLEUM HYDROCARBONS The primary source of petroleum hydrocarbons for this release incident was the former heating oil UST. A heating oil AST was noted immediately adjacent to the former heating oil UST and is currently supplying the residence's furnace. An inspection of the AST and surrounding surface soils do not indicate that a release incident from the AST has occurred and is contributing to the UST release. 7.0 NATURE AND ESTIMATED QUANTITY OF RELEASE The nature of the release is petroleum as heating oil from the former non-commercial UST. The amount of the release is unknown. A UST-61 24-Hour Release and UST Leak Reporting Form is provided in Appendix D. 8.0 SITE AND VICINITY DESCRIPTION The site is located in a residential and commercial area located south of Concord, NC. The subject and surrounding properties to the north, east, and west have a residential zoning classification. The surrounding properties to the south have a commercial zoning classification. The New Grace Baptist Church is located approximately 1,100 feet to the northwest. The site and the surrounding properties derive their drinking water from the City of Concord municipal water supply system. The subject property residence is connected to a septic system located south of the residence. A water supply well that formerly supplied the subject property residence was noted within 30 feet of the former UST location. The well is currently not in use, but not abandoned. No additional water supply wells were noted within a 150-foot radius from the former UST location. The location of the water supply well is depicted in Figure 2. According to the Geologic Map of North Carolina, the site lies in the Charlotte Belt of the Piedmont Physiographic Province (Brown, et al., 1985) and has been mapped as having a Initial Abatement Action Report Barbara Linker et al Property Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S Prepared on: January 15, 2021 4 Concord, Cabarrus County, NC metamorphosed quartz diorite bedrock lithology. On a regional scale, the Piedmont is characterized by gently rolling, well rounded hills and long low ridges with a few hundred feet of elevation difference between the hills and valleys. The closest surface water body features are intermittent streams located approximately 1,200 feet to the northeast and approximately 1,400 feet to the west. The eastern stream feeds into Cold Water Creek located approximately 4,450 feet to the east and into Irish Buffalo Creek located approximately 4,900 feet to the west. Surface water features are displayed with topography on Figure 1. 9.0 CONCLUSIONS/RECOMENDATIONS Terraquest personnel supervised the removal of one heating oil UST in November 2020 at the Barbara Linker et al property located at 1238 Union St. S in Concord, NC. Initial abatement activities included the removal of that tank and the excavation and offsite disposal of 32.65 tons of contaminated soil. Excavation was conducted to the limits possible given the presence of the onsite structures and features horizontally and bedrock vertically. Given the removal of the UST, the removal of the excavatable contaminated soil, the non- commercial status of the UST, and the presence of municipal water, the release incident is a "LOW" risk eligible for a "No Further Action" Letter and closure of the release incident. 10.0 LIMITATIONS This report is limited to the investigation of petroleum hydrocarbons in soil and does not imply that other unforeseen adverse impacts to the environment are not present at or around the subject facility. In addition, subsurface heterogeneities not identified during the current study may influence the migration of groundwater or contaminants in unpredicted ways. The limited amount of sampling and testing conducted during this study cannot practically reveal all subsurface heterogeneities. Furthermore, the subsurface conditions, particularly groundwater flow elevations, and water quality may very through time. The opinions and conclusions Initial Abatement Action Report Barbara Linker et al Property Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S Prepared on: January 15, 2021 5 Concord, Cabarrus County, NC determined in this report are in accordance with industry -accepted geologic and hydrogeologic practices at this time and location. No warranty is implied or intended. Initial Abatement Action Report Prepared by: Terraquest Environmental Consultants, P.C. Prepared on: January 15, 2021 6 Barbara Linker et al Property 1238 Union St. S Concord, Cabarrus County, NC REFERENCES Brown, et al., 1985. Geologic Map of North Carolina, North Carolina. Department of Natural Resources and Community Development, 1:500,000 scale. Initial Abatement Action Report Barbara Linker et al Property Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S Prepared on: January 15, 2021 7 Concord, Cabarrus County, NC TABLES Table 1 SUMMARY OF SOIL SAMPLING RESULTS Date: 121420 Incident Name: Barbara Linker etal- 1238 Union St. SE Concord NC Incident No.: P11,i19 Facility IM NA Analytical Method a Contaminant of Concern 15 Sample ID CODllected Sam le Depth PID d - A CS1 1111:121 5.5 397.1 5.905 875 - - - - - - - - - - - - - - - - - - - - - - SWI I3/I/20 6-7 0 <0.2 2.56 - - - - - - - - - - - - - - - - - - - - - - - SW2 11/18/20 6-7 0 0.24 1.08 - - - - - - - - - - - - - - - - - - - - - - - SW3 I3/IB/20 5-6 3.2 <0.2 2.2 - - - - - - - - - - - - - - - - - - - - - - - SW4 11/18/20 6-7 1.2 0.69 <1 - - - - - - - - - - - - - - - - - - - - - - BEI 1l/IB/20 7.0 342.1 2,420 736 0.0126 0.279 0.156 0.814 1.45 12.9/<0.333 0.805 3.52 0.39 6.11 1.64 2.1 0.319 0.633 3.09 7.11 1.2 IS 23 <12.5 2,354 414 TPH Action Limit 100 So Soil -to -groundwater MSCC 0.0056 4.3 4.9 4.6 0.12 0.16 1.7 4.3 1.7 1.5 1.3 3.3 16 940 47 56 270 0.004 3.6 68 540 8 31 18 1,200 1,560 3,129 300 313 626 626 1.564 782 782 626 9,385 4,600 620 469 469 20 63 939 1,500 31,000 469 Residential Soil Cleanup Level Industrial/Commercial Soil CIeanu Level 164 32,000 40,000 81,760 1 4000 8,176 16,350 16,350 40,880 20,440 20,"0 16,350 245,280 122,000 16,400 12,264 12,264 100 1.635 24,528 40,000 BI0,000 12,264 Notes: 1. All results in me/U. 2. Bold denotes a compound detection. 3. Shading denotes a Soil-to-aroundwater MSCC violation. Red italics indicates a Residential MSCC violation 4. "<' = less than sample deteRion IimiU Naphthalene Results: 8260/8270 5. Sample depths are in feet below ground level. 6. "MSCC" = Maximum Soil Contaminant Concentration: #- considered immobile: "1" --Ret analYte was identified between reportine limit and method detection limit; W' -value failed to meet OA/QC, estimated value FIGURES � A o vQ EP D NSF y� x "o� p4 o o l�D v O TWINFIELD 0o e < NNE SF RO t �Sr< OLD AIRPORT O['D.FARM ✓oG9ti OJ�O ' _ \ � SE 3 �Q SETTER LN`SE �j, J� �S� Q p Q � b � / O n b �P�QQ• 601 PQ\�� Q 1 `� cUM BERLAND CT 5 r r �7 O ARRO{yNEAD 0�^� z 650 z - A ^� ' ER AVE-SE 6 ^� o c - 1 _ J / 49 y/ A 0 WOODLAND DR SW /I 0 0 O 0 G<650 FN� 49 AQ 600 hh cpo MORNING DEW DR 0 O Crf rl 0 Z cy yBERRY_LN o� lrl s o CN RD E 601 o h .ENO cc C3 �� Po 1\/ NTRY HO fNSGP��o V - CQOUSE DR _ o �^ bye �p0 (�'n0 o p b c MAP SOURCE: USGS 7.5 MINUTE TOPOGRAPHIC MAP OF CONCORD & CONCORD SE, NC GRAPHIC SCALE 0' 2,000' 4,000' n nam J SITE LOCATION MAP BARBARA LINKER ET AL I ®" - -���� 1238 CONCORD, CABARRUS BARBARA LINKER ET AL UN ON ST SE COUNTY, NC CONCORD, NC PROJECT NO. 16820 DRAWN BY: JRG DATE: 11 20 20 ENVIRONMENTAL CONSULTANTS, P.C. SCALE: 1" = 2,000' CHECKED BY: MJB FIGURE NO. 1 LEGEND SOIL SAMPLE LOCATION (SAMPLE DEPTH IN FEET BELOW GROUND LEVEL) SW AND BE SOIL SAMPLES ANALYZED BY EPA 8260, 8270 DNA, & MADEP VPH/EPH. B1 SOIL SAMPLE ANALYZED BY UVF TRILOGY TPH 3550 (DRO) & 5030 (GRO). <S-T-G - NO DETECTIONS ABOVE ACTION LIMITS OR S-T-G MSCCS ALL RESULTS IN MILLIGRAMS PER KILOGRAM (MG/KG). B: BENZENE 4-I: 4-ISOPROPYLTOLUENE NAPH: NAPHTHALENE 1-M: 1-METHYLNAPHTHALENE 2-M: 2-METHYLNAPHTHLANE C9-C18: C9-C18 ALIPHATICS C9-C22: C9-C22 AROMATICS ONLY COMPOUNDS DETECTED AT CONCENTRATIONS GREATER THAN THE S-T-G MSCCS LISTED. RED UNDERLINED CONCENTRATIONS ARE GREATER THAN RESIDENTIAL MSCCS. SEE TABLE 1 FOR A COMPLETE LISTING OF DETECTED COMPOUNDS. RESIDENCE FORMER SW4(6-7 GRASS HEATING 3550: 0.68 OIL UST 5030: <1 SW1 (6-7): 3550: <0.2 SW3(5-6): r _ 5030: 2.56 3550: <0.2 5030: 2.2 1 ® 1 LIMITS OF BE 7.O L * / EXCAVATION /3550: 2,420 5030: 736 CS1 (5.5): B: 0.0126 3550: 51905 4-I: 1.45 5030: 875 NAPH: 12.9 SW2 (6-7): 1 -M: 15 3550: 0.24 2-M: 23 5030: 1.08 C9-Cl8: 2,354 C9-C22: 1,263 GRASS FENCE SCALE: 1 "- 211 SITE LAYOUT & CLOSURE SOIL SAMPLE MAP PROJECT N0. 16820 DATE: 1/15/21 BARBARA LINKER ET AL PROPERTY a — — CHECKED BY: MJB SCALE: VARIES 1298 UNION ST. SE ® ®� ffil CONCORD, CABARRUS COUNTY, NC ®�®® ■ ®��� BARBARA LINKER ET AL CONCORD, NC I ENVIRONMENTAL CONSULTANTS, P.c. DRAWN BY: JRG FIGURE NO. 2 APPENDIX A ENVIRONMENTAL ACRONYMS 2L Standard Groundwater Standards in Title 15A NCAC 2L 0.0202(g) 2B Standard Surface Water Standards under Title 15A NCAC 2B AFVR Aggressive Fluid -Vapor Recovery AST Aboveground Storage Tank BGL Below Ground Level BTEX Benzene, toluene, ethylbenzene, xylenes C&D Construction and Demolition CAP Corrective Action Plan CSA Comprehensive Site Assessment DPE Dual -phase Extraction EPA Environmental Protection Agency ePATA Electronic Pre -Approval Task Authorization EPH Extractable Petroleum Hydrocarbons ESA Environmental Site Assessment GCL Gross Contamination Level LEL Lower Explosive Limit LSA Limited Site Assessment IPE di -Isopropyl Ether ISCO In -situ Chemical Oxidation MADEP Massachusetts Department of Environmental Protection MDL Method Detection Limit MNA Monitored Natural Attenuation MMPE Mobile Multi Phase Extraction MSCC Maximum Soil Contaminant Concentration MSL Mean Sea Level MSW Municipal Solid Waste MTBE Methyl tertiary -Butyl Ether NC North Carolina NCAC NC Administrative Code NCDENR NC Department of Environment and Natural Resources NCDEQ NC Department of Environmental Quality NCDOT NC Department of Transportation NCDWM-SW NC Division of Waste Management's Solid Waste Section NCDWM-UST NC Division of Waste Management's UST Section NCDWQ NC Division of Water Quality NORR Notice of Regulatory Requirements NORP Notice of Residual Petroleum NOV Notice of Violation NPDES National Pollutant Discharge Elimination System OVM Organic Vapor Meter PID Photoionization Detector PLC Programmable Logic Controller POE Point of Entry (water treatment system) POTW Publicly Owned Treatment Works RBCA Risk Based Corrective Action RL Reporting Limit RP Responsible Party SCFM Standard Cubic Feet per Minute SVE Soil Vapor Extraction STG Soil to Groundwater TA Task Authorization TCC Target Cleanup Concentrations Terraquest Terraquest Environmental Consultants, P.C. TPH Total Petroleum Hydrocarbon UST Underground Storage Tank VOA Volatile Organic Analysis VOC Volatile Organic Compound VPH Volatile Petroleum Hydrocarbons XP Explosion Proof Terraquest Environmental Consultants, P.C. 100 E Ruffin St, Mebane, NC 27302 P (919) 563-9091 F(919) 563-9095 TECHNICAL METHODS/STANDARD PROCEDURES Equipment Decontamination All soil sampling equipment utilized during site assessment activities is decontaminated according to standard and accepted protocol. Cleaning solutions range from clean potable water to acidic solutions or organic solvents depending on the contaminants present at the site. Equipment utilized at sites, such as hand augers, contaminated with petroleum hydrocarbons, is generally decontaminated with a low-sudsing detergent such as Luiquinox° and triple rinsed with distilled water. Larger equipment, such as drill rigs and associated tools, is steam cleaned. All decontamination procedures are completed within an established decontamination area which is located away from the active study area. Frequency of equipment decontamination depends on the nature of work being performed, but in no case is decontamination performed less frequently than once per test (i.e., soil boring, well installation, sample collection, etc.). Equipment blanks are collected as a quality control measure when required by job specifications. Soil Boring Installation Soil borings are completed using hand -operated sampling tools, truck -mounted drills, or Geoprobe° drilling rigs depending on the depth of sample collection and other site -specific conditions. Hand operated stainless -steel bucket augers are utilized to collect soil samples at regular intervals to determine site stratigraphy and to test for the presence of volatile organic compounds. Samples retrieved from the hand auger are necessarily disturbed during the augering process, but can provide accurate information on soil type and contaminant concentrations when properly interpreted. Soil samples from hand augered borings are generally retrieved at one to two foot intervals. Truck -mounted or Geoprobe° drilling equipment is often utilized when sample retrieval depths exceed twenty feet or subsurface conditions prevent utilization of hand augers (i.e., buried rocks, wood, bricks or other materials occur in the subsurface). Truck -mounted drilling rigs usually retrieve soil via a hollow -stem auger/split spoon collection method. Geoprobe° rigs usually employ a Macro -Core° tube retrieval system. Hollow stem augers provide relatively undisturbed 2-foot cores of soil samples. Soil samples are generally collected at five foot intervals utilizing standard penetration test procedures as defined by the American Society for Testing and Materials (ASTM) or are pushed to the desired depth using the head of the drill rig. The standard penetration test involves driving a 2" outside diameter by 1- 3/8" inside diameter split -spoon sampler a minimum distance of one foot with a 340-lb. slide hammer falling a distance of 30 inches. A Geoprobe° rig is a hydraulically -powered soil probing machine. The probe utilizes static force and percussion to advance a small diameter sampling device into the subsurface. The sampling apparatus provides relatively undisturbed 5-foot cores of soil samples. Soil samples are collected continuously. The Macro -Core° tube contains an inserted poly -vinyl chloride (PVC) liner which retains the soil sample as the tube is driven into the ground. The Macro -Core° tube is decontaminated between each 5-foot sample interval in a soil boring using a Liquinox and tap - water mixture. A new PVC liner is used to collect soil from each sample interval in a soil boring. Soil samples retrieved from the hollow -stem augers or Geoprobe are then carefully described according to the Unified Soil Classification System. Soil descriptions are recorded on a soil boring log. Soil Sampling Soils to be analyzed by a North Carolina -certified laboratory are prepared according to the specified analytical method. Initially, soil samples are removed from the ground using either a hand auger, backhoe bucket, spilt spoon auger, or a Macro -Core° sampling tube. During the removal, care is taken to keep the disturbance of the soil structure to a minimum to reduce the loss of contaminants. Once removed, the samples are placed in the proper sample container for the specified analytical method. For samples collected for the MADEP VPH and EPA Method 8260, a TerraCore° sampler is used to collect one 5-gram allotment of soil. The allotment is placed in methanol -preserved 40 mL vials. Also, one 5-gram allotment of soil is placed into sodium bisulfate - preserved 40 mL vials (one 5-gram allotment per vial, 2 vials per sample) for the 8260 low concentration method. A 250-mL glass jar of the sampled soil is also collected to provide moisture content information. Soils sampled for MADEP EPH, EPA Method 8270 and TPH 5030 and 3550 are placed in a 250-mLglass jar (for MADEP EPH analysis an amber jar is required). TPH 5030 samples are preserved in methanol similar to the 8260 analysis. Field personnel wear new, disposable nitrile gloves during the collection of each sample. The soil samples are labeled with the sample location, sample identification, date and time of collection, and the analytical method. The samples are placed on ice, sent to a laboratory, and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is maintained for each sample collected in the field. If the soil is being sampled for volatile or semi -volatile compounds, a portion of the collected soil is placed in a sealable bag and screened for volatile organic vapors. Head screening procedures are described in the following paragraph. Headspace Screening Collected soil samples are routinely tested for the presence of volatile organic compounds (VOCs). After retrieval from the ground, a portion of a soil sample is placed in a sealable plastic bag. The soil samples are then set aside for approximately five minutes so that volatile constituents present in the sample can reach equilibrium concentrations with headspace gases in the bag. Once a suitable time period has passed, the probe of the sampling instrument, typically an Organic Vapor Monitor (OVM) or a Photo Ionization Detector (PID), is inserted into the bag and the relative concentration of total VOCs is measured and permanently recorded in a field note book. VOC concentrations are measured using either a Thermo Electron Corp. Innova Series catalytic OVM or an Ion Science PhoCheck PID. Both the OVM and PID instrumentation are periodically calibrated according to the manufacturer's recommended procedures. The OVM and PID are qualitative tools employed to detect and estimate the concentration of organic or hydrocarbon vapors. A thin probe is inserted through a small break in the seal of a bagged soil sample. For the OVM, an air sample from the headspace of the bag is drawn through the probe into an internal chamber where the vapors are catalyzed. The concentration of the VOCs is registered on a digital scale in parts per million (ppm). For the PID, an air sample from the headspace of the bag is drawn across the face of a lamp causing the sample to emit photons, the presence of which are converted into a VOC ppm reading that is displayed. Oxygen levels are field calibrated prior to each use. VOC calibration occurs periodically depending upon use by using a span gas of known concentration in a process recommended by the manufacturer. Well Installation/Construction Monitoring wells are installed using hand -operated sampling tools, a truck -mounted drill rig, or a Geoprobe drilling rig depending on the depth of well and other site -specific conditions. All monitoring wells are installed according to the requirements of 15A NCAC 2C-Well Construction Standards. Specifically, individual monitoring wells are constructed of 2-inch diameter, schedule 40 PVC casing riser and screen. The screen interval is generally 10 to 15 feet of machine slotted PVC with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above the top of the screen. A one to two foot -thick bentonite pellet seal is then placed above the filter pack. The remainder of the well annulus is completely filled with a Portland (Type 1/11) cement grout mixture. A protective outer steel manhole, locking cap, and concrete pad is installed for each well. Type II Monitoring Well Construction Single -cased monitoring wells are generally used in delineation of groundwater quality within the surficial aquifer. The wells are constructed of 2-inch diameter, schedule 40 PVC casing and screen. The screen interval is generally 10 to 15 feet of machine slotted PVC with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above the top of the screen. A one to two foot -thick bentonite pellet seal is then placed above the filter pack. The remainder of the well annulus is completely filled with a Portland (Type 1/II) cement grout mixture. A protective outer steel manhole, locking cap, and concrete pad are installed for each well. Type III Monitoring Well Construction Double -cased monitoring wells are used in the delineation of groundwater quality within a deeper portion of the surficial aquifer or an additional aquifer (e.g. aquitard, bedrock). A four to six-inch outer casing is installed through the surficial aquifer until a sufficient depth or until the deeper aquifer is encountered. The casing is secured with a Portland -grout collar that is tremmied into the annular spaced from the bottom of the bore hole to the surface. Once the grout has sufficiently cured, the bore hole is continued through the bottom of the outer casing to a depth approximately 15 - 20 feet beneath the outer casing. The inner casing is constructed of 2-inch diameter, schedule 40 PVC casing riser and screen. The screen interval is generally 5 to 10 feet of machine slotted PVC with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above the top of the screen. A one to two foot -thick bentonite pellet seal is then placed above the filter pack. The remainder of the well annulus is completely filled with the same Portland grout mixture used in the outer casing. A protective outer steel manhole, locking cap, and concrete pad are installed for each well. Well Development Following installation of each well, surging and pumping or bailing techniques will be used to remove fines from the screened interval. Groundwater is removed from each well until clear water is retrieved or a noticeable reduction in the amount of silt is achieved. Purged groundwater is disposed of in an environmentally safe manner. Groundwater Sampling Petroleum Sites Groundwater samples are collected from temporary or permanent monitoring wells according to established sampling protocol. When multiple monitoring wells or sampling points are sampled, sampling is completed beginning with the least contaminated well to the most contaminated well, if it is known. When permanent monitoring wells for petroleum sites are sampled, the well is purged of a minimum of three well -bore volumes prior to sample collection in order to assure that sampled water is representative of aquifer conditions. In temporary wells, the first water which migrates into the open borehole is sampled. Samples from both temporary and permanent monitoring wells are collected using individually wrapped disposable polyethylene bailers by field personnel wearing disposable nitrile gloves. Only one well is sampled with a given bailer in order to prevent sample cross -contamination. During both well purging and sampling, proper protective clothing and equipment is used and is dependent upon the type and level of contaminants present. Also, field personnel change gloves between different samples to reduce the chance of cross - contamination. Water samples are transferred from the bailer to laboratory -prepared sampling containers using slow emptying devices to reduce the chance of contamination loss through volatilization. Preservatives, such as acids, are provided by the laboratory in pre -prepared containers in which collected samples are placed if in -field preservation is necessary. The samples are labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples are placed on ice, shipped to a certified laboratory, and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is maintained for each sample collected in the field. Other Groundwater Sampling Protocols When required by state or federal regulations, low -flow groundwater sampling procedures are instituted. Groundwater samples collected in low -flow situations are collected using a peristaltic pump. A peristaltic pump is a type of positive displacement pump. The fluid is contained within a flexible tube fitted inside a circular pump casing. A rotor with a number of rollers attached to the external circumference compresses the flexible tube. As the rotor turns, the part of tube under compression closes thus forcing the fluid to be pumped to move through the tube. Groundwater parameters such as water level drawdown, pH, conductivity, dissolved oxygen (DO) and turbidity. Pumping rate, drawdown, and the time or volume required to obtain stabilization of parameter readings can be used as a future guide to purge the well. Measurements are collected at a pre - pumping established interval (typically five to ten minutes). Once all or a majority of the parameters have stabilized forthree successive readings, stabilization has been achieved. In lieu of measuring all five parameters, a minimum subset would include pH, conductivity, and turbidity or DO. Three successive readings should be within ± 0.1 for pH, ± 3% for conductivity, and ± 10% for turbidity and DO. Upon parameter stabilization, sampling is initiated. Sampling flow rate is maintained at the estab- lished purge rate or is adjusted slightly to minimize aeration, bubble formation, turbulent filling of sample bottles, or loss of volatiles due to extended residence time in tubing. The same device used for purging is used to collect the groundwater sample. Generally, volatile parameters are sampled first. The sequence in which samples for inorganic parameters are collected is not determined unless filtered (dissolved) samples are collected. Preservatives, such as acids, are provided by the laboratory in pre -prepared containers in which collected samples are placed if in -field preservation is necessary. The samples are labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples are placed on ice, shipped to a certified laboratory, and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is maintained for each sample collected in the field. During both well purging and sampling, proper protective clothing and equipment is used and is dependent upon the type and level of contaminants present. Also, field personnel change gloves between different monitoring wells or sampling points to reduce the chance of cross - contamination. When multiple monitoring wells or sampling points are sampled, sampling is completed beginning with the least contaminated well to the most contaminated well, if it is known. Stockpile Sampling The number of composite samples collected from a stockpile or a total quantity of excavated soil is based upon the cubic yardage. One composite sample is collected for every 100 cubic yards of contaminated soil excavated. The volume of a stockpile or total quantity of excavated soil is calculated by approximating the general geometry of a stockpile or estimating the capacity of the dump trucks used for hauling. If a stockpile is sampled, a grid pattern is laid out on the stockpile, dividing the stockpile into segments of approximately 200 cubic yards. Two soil borings are advanced within a grid and three soil samples are collected from each soil boring at various depths. The six soil samples are mixed into a composite sample by a trained TerraQuest technician. If truck loads are sampled, an aliquot sample is collected from the hauling trucks at a frequency based upon the capacity of the hauling trucks. Aliquots are gently mixed into a composite sample by a trained TerraQuest technician. Every effort is made to minimize the loss of contaminants through volatilization. The composited soil samples are jarred in the appropriate laboratory -prepared containers, labeled with the sample location, sample identification, date of collection, time of collection, the analytical method, and the preservative. The samples are placed on ice, shipped to a laboratory, and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is maintained for each sample collected in the field. Surface Water Sampling Surface water samples, specifically samples from creeks or streams, are collected from a moving/flowing portion of the creek or stream to ensure that stagnant water is not collected. Field personnel are careful to collect samples from flowing areas that are not so turbulent as to cause a loss of volatile contaminants which might have been contained in the creek's/stream's water. Samples are collected by field personnel wearing disposable nitrile gloves. Field personnel change gloves between different locations to reduce the chance of cross -contamination. Samples are collected directly from the appropriate creek or stream location and placed into the appropriate laboratory -prepared containers. Preservatives, such as acids, are provided by the laboratory in pre - prepared containers in which collected samples are placed if in -field preservation is necessary. The samples are labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples are cooled on ice to approximately four degrees centigrade, shipped to a certified laboratory, and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is maintained for each sample collected in the field. Potable Well Sampling Groundwater samples from potable wells are collected from sampling points, typically spigots, located in the closest proximity to the potable well pump house as possible. Prior to sample collection, the water is run for a sufficient amount of time to purge the bladder tank and assure that sampled water is representative of aquifer conditions. Once purged, the flow rate is reduced and samples are placed in the appropriate laboratory prepared containers with the appropriate acid preservatives added if preservation of the sample is necessary. The samples are labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples are placed on ice, shipped to a laboratory, and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is maintained for each sample collected in the field. Public Water Supply Line Sampling Groundwater samples from public water supply lines are collected from sampling points, typically spigots. To sample the spigot, the flow rate is reduced and samples are placed in the appropriate laboratory prepared containers. The samples are labeled with the sample location, sample identification, date of collection, time of collection, and required analytical method. The samples are placed on ice, shipped to a laboratory, and analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is maintained for each sample collected in the field. Air Sampling Air samples are collected with the aide of a manually operated MityVac° pump manufactured by Pristech, Inc. The air sampling process begins by connecting a length of rubber hose from the MityVac° pump to the port to be sampled, or by hanging the hose inside of an emissions stack in such a manner as to ensure no outside air causes dilution. Another length of hose is fixed to the outlet port of the pump and is connected to a new Tedlar bag. Once the pump is hooked up, a valve on the Tedlar collection bag is opened and air is manually forced into the bag by the pumping action of sampling personnel. Field Measurements Field measurements taken to determine the pH, conductivity, temperature, and dissolved oxygen concentration of a particular groundwater sample are taken directly after a particular monitoring well has been adequately purged. This ensures that the groundwater parameter data collected is representative of the aquifer conditions at a given location. Once purging of the monitoring well is complete, the decontaminated probe head and cord of the appropriate unit is lowered into the required monitoring well. If the depth to water in a specific monitoring well is greater than the length of cord for a particular unit, a new, disposable bailer is slowly lowered into the appropriate monitoring well and a representative groundwater sample is retrieved. A slow pouring device is fitted onto the end of the disposable bailer and the sample is slowly poured into a new, disposable plastic cup. Groundwater parameter data are then collected from the groundwater in the cup using the required unit. For pH, conductivity, and temperature, a Hanna Instruments Model 991300 portable meter is utilized. This unit is periodically calibrated and maintained in accordance with the unit's operations manual by field personnel. Prior to data collection, the unit is properly decontaminated to prevent cross -contamination. The unit is decontaminated between each sample. The procedure used for sample measurement involves lowering the meter's probe into the new, disposable cup containing the groundwater sample to be measured and slowly stirring the probe to force groundwater across the probe's membrane. The measurements displayed by the meter are then recorded. For dissolved oxygen concentration measurements, a YSI° Model 55 Handheld Dissolved Oxygen System is utilized. This unit is periodically calibrated and maintained in accordance with the unit's operations manual by field personnel. Prior to data collection, the unit is properly decontaminated to prevent cross -contamination. The unit is decontaminated between each sample. The procedure used for sample measurement involves adjusting the unit for the correct altitude where the sampling will take place and adjusting the reported units desired. Once this is done, the unit's probe is inserted into the groundwater sample to be measured and the probe is slowly stirred to force the groundwater across the probe's membrane. The measurements displayed by the unit are then recorded. For turbidity measurements, a Hach 2100P Portable Turbidity meter or equal equivalent is utilized. The unit is calibrated prior to use in accordance with the unit's operations manual by field personnel. Groundwater samples are collected in glass containers for measurement by the instrument. The glass containers are washed with bottled -water between each measurement collection. Once the sample is collected and inserted into the instrument, the measurements displayed by the instrument are then recorded. APPENDIX B TERRA W.Owi ENVIRONMENTAL CONSULTANTS, uest P.C. UVF TRILOGY ANALYTICAL REPORT Project Name: 1238 Union St SE, Concord, NC Project Number: 16820 Date: 11/20/2020 Standard Technical Procedures The UVF TRILOGY instrument is a fixed -wavelength fluorometer but uses deep UV LEDS to detect monoaromatic and polyaromatic hydrocarbons. SITELAB's CAL-025 GRO Module is used to detect volatile petroleum hydrocarbons in the C6 to C10 range. This test matches well to EPA Methods for GRO, BTEX, BPH or VOC's using GC/FID instrumentation. SITELAB's CAL-042 EDRO Module is used to detect petroleum hydrocarbons in the C10 to C36 diesel and oil range. This test matches well to EPA methods for TPH, EPH, DRO, and others using GC-FID instrumentation. Prior to field usage, the UVF TRILOGY is calibrated with five calibration standard solutions per targeted analyte. Soil samples are weighed to the nearest gram (i.e. 5.0 g) and added to a 1-ounce HDPE Nalgene bottle with a measured amount of laboratory grade methanol to the nearest mL (i.e. 10 mL) to create a sample extract. After addition of both the soil and methanol, the bottle is agitated for several minutes. Next, the sample rests for several minutes allowing for the soil and methanol extract to separate. After ample resting time, the methanol extract is collected with a syringe. A filter is connected to the end of the syringe and dispensed into a clean sample test tube. The test tube is labeled with sample ID and extract dilution factor (i.e. 2X). Known amounts of extract are pipetted into a second test tube and diluted with methanol. The sample ID and dilution factor are labeled on the test tube (i.e. 100X). Samples are placed into a clean cuvette and carefully inserted into the selected UV Module. Prior to analyzing the sample, the stored calibration that matches the UV Module being used, is selected. The UVF TRILOGY produces a result that when multiplied to the dilution factor equals the true TPH value. Quenching occurs when the detector is swamped by too many or certain type of hydrocarbons, producing low or negative concentrations. The sample is tested at multiple dilutions to confirm the results are linear and accurate. Solvent blank samples are periodically analyzed to confirm the solvent is clean and the calibration of the machine is maintained. UVF Analytical Report TEIRMCiluest i�—w =1 ENYI RONMENTLL CONSULTANTS, P.C. sfteLAB f Project Name 1238 Union St SE, Concord, NC Sample Name BE1 (7.0) Project Number 16820 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units BE1 (7.0) 7.0 11/18/2020 DRO 500 2420 50 mg/kg BE1 (7.0) 7.0 11/18/2020 GRO 200 736 100 mg/kg Friday, November 20, 2020 Page 1 of 6 Project Name 1238 Union St SE, Concord, NC Sample Name CS-1 (5.5) Project Number 16820 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units CS-1 (5.5) 5.5 11/18/2020 DRO 500 5905 50 mg/kg CS-1 (5.5) 5.5 11/18/2020 GRO 500 875 250 mg/kg Friday, November 20, 2020 Page 2 of 6 Project Name 1238 Union St SE, Concord, NC Sample Name SW1 (6-7) Project Number 16820 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units SW1 (6-7) 6-7 11/18/2020 DRO 2 <0.2 0.2 mg/kg SW1 (6-7) 6-7 11/18/2020 GRO 2 2.56 1 mg/kg Friday, November 20, 2020 Page 3 of 6 Project Name 1238 Union St SE, Concord, NC Sample Name SW2 (6-7) Project Number 16820 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units SW2 (6-7) 6-7 11/18/2020 DRO 2 0.24 0.2 mg/kg SW2 (6-7) 6-7 11/18/2020 GRO 2 1.08 1 mg/kg Friday, November 20, 2020 Page 4 of 6 Project Name 1238 Union St SE, Concord, NC Sample Name SW3 (5-6) Project Number 16820 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units SW3 (5-6) 5-6 11/18/2020 DRO 2 <0.2 0.2 mg/kg SW3 (5-6) 5-6 11/18/2020 GRO 2 2.2 1 mg/kg Friday, November 20, 2020 Page 5 of 6 Project Name 1238 Union St SE, Concord, NC Sample Name SW4 (6-7) Project Number 16820 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units SW4 (6-7) 6-7 11/18/2020 DRO 2 0.68 0.2 mg/kg SW4 (6-7) 6-7 11/18/2020 GRO 2 <1 1 mg/kg Friday, November 20, 2020 Page 6 of 6 � o.-..� �:�R►A - Terraquest Environmental Consultants, P.C. Chain -Of -Custody Record 1 _I �— =----- 100 E. Ruffin Street., Mebane, NC 27302 Page l of !lair.--- - EIMRONp[tt�ALCONtOLTANI9..�. �� 919 563-9091 ( ) client Name:Terraquest Environmental Project Number: Requested Analyses '�� �,= IC2�Z� Address:100 E. RUffin Street Project Name: 123`g ��btiS�s� ��r� UVFTrilogy city/sr/zip: Mebane, NC 27302 Reporting Contact: �i �Q� Te1:919-563-9091 Fax: 919-563-9095 Reporting contact Email: ` r � �. maces .c Samplers) Name: %% �� �� Sampler(s) Sign re: ��eF��� C7 p Imo- I�- Item # Sample ID Sample Collection Collection (Lab Use) (Field Identification) Depth Date Time Comp/Grab Matrix Sample Comments CS - s. S.5 � � ,� � ao, 0 5 0 � - � --� ' � � Z - h �-`� r. t 3! Oc. �-. 8 za i K �- �. ._ . ' . -. . .. - - • ,. ..- - o � r � • � - -. -.: i � - - ` ._ _ .. � tiff eu rof ins Environment resting Xenco Analytical Report 679115 for Terraquest Environmental Consultants, P.C. Project Manager: Jonathan Grubbs 1238 Union St SE Concord 12.14.2020 pCCRF'0 TN !� 9e0 iO RA .. 4147 Greenbriar Dr. Stafford, TX 77477 Xenco-Houston (EPA Lab Code: TX00122): Texas (T104704215-20-38), Arizona (AZ0765), Florida (E871002-33), Louisiana (03054) Oklahoma (2020-014), North Carolina (681), Arkansas (20-035-0) Xenco-Dallas (EPA Lab Code: TX01468): Texas (T104704295-20-26), Arizona (AZ0809) Xenco-El Paso (EPA Lab Code: TX00127): Texas (T104704221-20-18) Xenco-Lubbock (EPA Lab Code: TX00139): Texas (T104704219-20-23) Xenco-Midland (EPA Lab Code: TX00158): Texas (T104704400-19-21) Xenco-Carlsbad (LELAP): Louisiana (05092) Xenco-San Antonio (EPA Lab Code: TNI02385): Texas (T104704534-20-8) Xenco-Tampa: Florida (E87429), North Carolina (483) Page 1 of 27 Final 1.000 tiff eu rof ins Environment Testing ]lento 12.14.2020 Project Manager: Jonathan Grubbs Terraquest Environmental Consultants, P.C. 100 E. Ruffin Street Mebane, NC 27302 Reference: Eurofins Xenco, LLC Report No(s): 679115 1238 Union St SE Concord Project Address: Jonathan Grubbs: We are reporting to you the results of the analyses performed on the samples received under the project name referenced above and identified with the Eurofins Xenco, LLC Report Number(s) 679115. All results being reported under this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number. Subcontracted analyses are identified in this report with either the NELAC certification number of the subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report. Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with NELAC standards. The uncertainty of measurement associated with the results of analysis reported is available upon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reported using all other available quality control measures. The validity and integrity of this report will remain intact as long as it is accompanied by this letter and reproduced in full, unless written approval is granted by Eurofins Xenco, LLC. This report will be filed for at least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise arranged with you. The samples received, and described as recorded in Report No. 679115 will be filed for 45 days, and after that time they will be properly disposed without further notice, unless otherwise arranged with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard practices, controlled substances under regulated protocols, etc). We thank you for selecting Eurofins Xenco, LLC to serve your analytical needs. If you have any questions concerning this report, please feel free to contact us at any time. Respectfully, FOR 11 "FFl *, � � HMO, Chad Bechtold Project Manager A Small Business and Minority Company Houston - Dallas- Midland - Tampa - Phoenix- Lubbock- San Antonio - 8 Paso - Atlanta - New Mexico Page 2 of 27 Final 1.000 tiff eu rof ins Environment Testing Xenco Sample Cross Reference 679115 Sample Id BEI (T) Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Matrix Date Collected S 11.18.2020 13:48 Sample Depth Lab Sample Id 679115-001 Page 3 of 27 Final 1.000 tiff eurofins CASE NARRATIVE Environment Testing Xenco Client Name: Terraquest Environmental Consultants, P.C. Project Name: 1238 Union St SE Concord Project ID: Report Date: 12.14.2020 Work Order Number(s): 679115 Date Received: 11.25.2020 Sample receipt non conformances and comments: Sample receipt non conformances and comments per sample: None Analytical non conformances and comments: Batch: LBA-3143789 SVOCs by SW846 8270E The sample 679115-001 was analyzed at a dilution of 20 for Method 8270E - SVOCs due to the oily sample matrix. Elevated reporting limits (RLs and MDLs) are provided. Batch: LBA-3144206 EPH by MADEP Method Lab Sample ID 679115-001 was randomly selected for Matrix Spike/Matrix Spike Duplicate (MS/MSD). C 19 to C36Aliphatic Hydrocarbons, C9 to C 18 Aliphatic Hydrocarbons recovered below QC limits in the Matrix Spike. CI I to C22 Aromatics, C19 to C36Aliphatic Hydrocarbons, C9 to C18 Aliphatic Hydrocarbons recovered above QC limits in the Matrix Spike Duplicate. Outlier/s are due to possible matrix interference. Samples in the analytical batch are: 679115-001. The Laboratory Control Sample for C 19 to C36Aliphatic Hydrocarbons, C 11 to C22 Aromatics, C9 to C 18 Aliphatic Hydrocarbons is within laboratory Control Limits; therefore, the data was accepted. Although C 11 to C22 Aromatics and C9 to C 18 Aliphatic Hydrocarbons were detected in the Method Blank, the concentration for these targets in the associated sample 679115-001 were more than 10 times the amount in the Method Blank. Batch: LBA-3144346 VOCs by SW-846 8260D Lab Sample ID 679115-001 was randomly selected for Matrix Spike/Matrix Spike Duplicate (MS/MSD). 1, 1 -Dichloropropene, 1,2,4-Trimethylbenzene, 2-Butanone, 2-Hexanone, Bromomethane, Chloroethane, Methylene Chloride, Trichlorofluoromethane, trans-1,2-dichloroethene recovered below QC limits in the Matrix Spike. Outlier/s are due to possible matrix interference. Samples in the analytical batch are: 679115-001. The Laboratory Control Sample for Bromomethane, Methylene Chloride, 1,2,4-Trimethylbenzene, 2- Hexanone, Trichlorofluoromethane, 2-Butanone, trans-1,2-dichloroethene, 1,1-Dichloropropene, Chloroethane is within laboratory Control Limits; therefore, the data was accepted. Page 4 of 27 Final 1.000 tiff eu rof ins Environment Testing Xenco Hits Summary 679115 Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Below is a summary of the analytes which were found to be present in the samples associated with this work order. This should only be used in conjunction with the included analytical results. Sample ID: BEI (71) Sample ID: 679115-001 Date/Time Sampled: 11.18.2020 13:48 Matrix: Solid Analyte Name Method CAS No. Dil. Result RL/PQL MDL Units Qual 1,2,4-Trimethylbenzene SW8260D 95-63-6 100 6.11 0.842 0.0429 mg/kg DX 1,3,5-Trimethylbenzene SW8260D 108-67-8 25 1.64 0.210 0.0122 mg/kg 2-Butanone SW8260D 78-93-3 25 0.319 0.842 0.153 mg/kg JX Benzene SW8260D 71-43-2 25 0.0126 0.0421 0.00871 mg/kg J Ethylbenzene SW8260D 100-41-4 25 0.156 0.0421 0.0141 mg/kg Naphthalene SW8260D 91-20-3 100 12.9 1.68 0.337 mg/kg D Sec-Butylbenzene SW8260D 135-98-8 25 2.10 0.210 0.0110 mg/kg Toluene SW8260D 108-88-3 25 0.279 0.210 0.0421 mg/kg Total Xylenes SW8260D 1330-20-7 100 0.814 0.0421 0.0337 mg/kg isopropylbenzene SW8260D 98-82-8 25 0.390 0.210 0.00732 mg/kg m,p-Xylenes SW8260D 179601-23-1 25 0.677 0.0842 0.0337 mg/kg n-Butylbenzene SW8260D 104-51-8 25 3.52 0.210 0.0115 mg/kg n-Propylbenzene SW8260D 103-65-1 25 0.805 0.210 0.0120 mg/kg o-Xylene SW8260D 95-47-6 25 0.137 0.0421 0.0414 mg/kg p-Cymene (p-Isopropyltoluene) SW8260D 99-87-6 25 1.45 0.210 0.0134 mg/kg Sample ID: BEI (71) Sample ID: 679115-001 Date/Time Sampled: 11.18.2020 13:48 Matrix: Solid Analyte Name Method CAS No. Dil. Result RL/PQL MDL Units Qual 1-Methylnaphthalene SW8270E 90-12-0 20 15.0 3.56 0.570 mg/kg 2-Methylnaphthalene SW8270E 91-57-6 20 23.0 3.56 0.964 mg/kg Anthracene SW8270E 120-12-7 20 0.633 3.56 0.295 mg/kg J Fluorene SW8270E 86-73-7 20 3.09 3.56 0.295 mg/kg J Phenanthrene SW8270E 85-01-8 20 7.11 3.56 0.354 mg/kg Pyrene SW8270E 129-00-0 20 1.20 3.56 0.312 mg/kg J Sample ID: BEI (T) Sample ID: 679115-001 Date/Time Sampled: 11.18.2020 13:48 Matrix: Solid Analyte Name Method CAS No. Dil. Result RL/PQL MDL Units Qual C9-C10 Aromatic VPH HYDC9C10 1000 325 16.8 6.06 mg/kg C9-C12 Aliphatic VPH ALHYDRC9C12 1000 604 50.5 22.5 mg/kg Sample ID: BEI (T) Sample ID: 679115-001 Date/Time Sampled: 11.18.2020 13:48 Matrix: Solid Analyte Name Method CAS No. Dil. Result RL/PQL MDL Units Qual Percent Moisture SM2540G MOIST 1 6.29 % Sample ID: BEI (T) Sample ID: 679115-001 Date/Time Sampled: 11.18.2020 13:48 Matrix: Solid Page 5 of 27 Final 1.000 tiff eu rof ins Environment resting Xenco Hits Summary 679115 Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Sample ID: 679115-001 Date/Time Sampled: 11.18.2020 13:48 Matrix: Solid Analyte Name Method CAS No. Dil. Result RL/PQL MDL Units Qual C11 to C22 Aromatics MA EPH Cl lC22 10 938 90.7 45.4 mg/kg DX C19 to C36Aliphatic Hydrocarbons MA EPH ALHYDR090 50 414 427 213 mg/kg JD 6 X C9 to C18 Aliphatic Hydrocarbons MA EPH ALHYDRC9C18 50 1750 320 160 mg/kg DX Page 6 of 27 Final 1.000 tiff eurof ins Environment Testing Certificate of Analytical Results 679115 Xenco Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Sample Id: BEI (71) Matrix: Soil Date Received:11.25.2020 09:30 Lab Sample Id: 679115-001 Date Collected: 11.18.2020 13:48 Analytical Method: EPH by MADEP Method Prep Method: SW3550 Tech: JUN Analyst: VIC Date Prep: 12.02.2020 20:39 % Moisture: 6.29 Seq Number: 3144206 Basis: Dry Weight Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil C9 to C18 Aliphatic Hydrocarbons ALHYDRC9C11 1750 320 160 mg/kg 12.12.2020 13:27 DX 50 C19 to C36Aliphatic Hydrocarbons ALHYDRCI9C: 414 427 213 mg/kg 12.12.2020 13:27 JDX 50 C11 to C22 Aromatics C11C22 938 90.7 45.4 mg/kg 12.07.2020 19:53 DX 10 Surrogate Cas Number % Recovery Units Limits Analysis Date Flag 1-Chlorooctadecane 3386-33-2 52 % 40-140 12.07.2020 22:33 o-Terphenyl 84-15-1 91 % 40-140 12.07.202015:06 2-Fluorobiphenyl 321-60-8 100 % 40-140 12.07.202015:06 Page 7 of 27 Final 1.000 tiff eurof ins Environment Testing Certificate of Analytical Results 679115 Xenco Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Sample Id: BEI (71) Matrix: Soil Date Received:11.25.2020 09:30 Lab Sample Id: 679115-001 Date Collected: 11.18.2020 13:48 Analytical Method: SVOCs by SW846 8270E Prep Method: SW3550 Tech: JUN Analyst: EKL Date Prep: 12.02.2020 20:25 % Moisture: 6.29 Basis: Dry Weight Seq Number: 3143789 Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil 1,2,4-Trichlorobenzene 120-82-1 0.310 U 3.56 0.310 mg/kg 12.04.2020 17:34 U 20 1,2-Dichlorobenzene 95-50-1 0.328 U 3.56 0.328 mg/kg 12.04.2020 17:34 U 20 1,3-Dichlorobenzene 541-73-1 0.296 U 3.56 0.296 mg/kg 12.04.2020 17:34 U 20 1,4-Dichlorobenzene 106-46-7 0.320 U 3.56 0.320 mg/kg 12.04.2020 17:34 U 20 1-Methylnaphthalene 90-12-0 15.0 3.56 0.570 mg/kg 12.04.2020 17:34 20 2,4,5-Trichlorophenol 95-95-4 0.407 U 3.56 0.407 mg/kg 12.04.2020 17:34 U 20 2,4,6-Trichlorophenol 88-06-2 0.336 U 3.56 0.336 mg/kg 12.04.2020 17:34 U 20 2,4-Dichlorophenol 120-83-2 0.372 U 3.56 0.372 mg/kg 12.04.2020 17:34 U 20 2,4-Dimethylphenol 105-67-9 0.351 U 3.56 0.351 mg/kg 12.04.2020 17:34 U 20 2,4-Dinitrotoluene 121-14-2 0.272 U 3.56 0.272 mg/kg 12.04.2020 17:34 U 20 2,6-Dinitrotoluene 606-20-2 0.497 U 3.56 0.497 mg/kg 12.04.2020 17:34 U 20 2-Chloronaphthalene 91-58-7 0.620 U 3.56 0.620 mg/kg 12.04.2020 17:34 U 20 2-Chlorophenol 95-57-8 0.337 U 3.56 0.337 mg/kg 12.04.2020 17:34 U 20 2-Methylnaphthalene 91-57-6 23.0 3.56 0.964 mg/kg 12.04.2020 17:34 20 2-methylphenol 95-48-7 0.396 U 3.56 0.396 mg/kg 12.04.2020 17:34 U 20 2-Nitroaniline 88-74-4 0.333 U 7.11 0.333 mg/kg 12.04.2020 17:34 U 20 2-Nitrophenol 88-75-5 0.313 U 3.56 0.313 mg/kg 12.04.2020 17:34 U 20 3&4-Methylphenol 15831-10-4 0.329 U 3.56 0.329 mg/kg 12.04.2020 17:34 U 20 3-Nitroaniline 99-09-2 0.297 U 7.11 0.297 mg/kg 12.04.2020 17:34 U 20 4,6-dinitro-2-methyl phenol 534-52-1 0.271 U 7.11 0.271 mg/kg 12.04.2020 17:34 U 20 4-Bromophenyl-phenylether 101-55-3 0.283 U 3.56 0.283 mg/kg 12.04.2020 17:34 U 20 4-chloro-3-methylphenol 59-50-7 0.393 U 3.56 0.393 mg/kg 12.04.2020 17:34 U 20 4-Chloroaniline 106-47-8 0.270 U 7.11 0.270 mg/kg 12.04.2020 17:34 U 20 4-Chlorophenyl-phenyl ether 7005-72-3 0.345 U 3.56 0.345 mg/kg 12.04.2020 17:34 U 20 4-Nitroaniline 100-01-6 0.296 U 7.11 0.296 mg/kg 12.04.2020 17:34 U 20 4-Nitrophenol 100-02-7 0.552 U 7.11 0.552 mg/kg 12.04.2020 17:34 U 20 Acenaphthene 83-32-9 0.331 U 3.56 0.331 mg/kg 12.04.2020 17:34 U 20 Acenaphthylene 208-96-8 0.315 U 3.56 0.315 mg/kg 12.04.2020 17:34 U 20 Aniline (Phenylamine, Aminobenzene) 62-53-3 0.291 U 7.11 0.291 mg/kg 12.04.2020 17:34 U 20 Anthracene 120-12-7 0.633 3.56 0.295 mg/kg 12.04.2020 17:34 J 20 Benzo(a)anthracene 56-55-3 0.300 U 3.56 0.300 mg/kg 12.04.2020 17:34 U 20 Benzo(a)pyrene 50-32-8 0.367 U 3.56 0.367 mg/kg 12.04.2020 17:34 U 20 Benzo(b)fluoranthene 205-99-2 0.268 U 3.56 0.268 mg/kg 12.04.2020 17:34 U 20 Benzo(g,h,i)perylene 191-24-2 0.328 U 3.56 0.328 mg/kg 12.04.2020 17:34 U 20 Benzo(k)fluoranthene 207-08-9 0.413 U 3.56 0.413 mg/kg 12.04.2020 17:34 U 20 Benzoic Acid 65-85-0 0.747 U 21.3 0.747 mg/kg 12.04.2020 17:34 U 20 Benzyl Butyl Phthalate 85-68-7 0.387 U 3.56 0.387 mg/kg 12.04.2020 17:34 U 20 bis(2-chloroethoxy) methane 111-91-1 0.359 U 3.56 0.359 mg/kg 12.04.2020 17:34 U 20 bis(2-chloroethyl) ether 111-44-4 0.324 U 3.56 0.324 mg/kg 12.04.2020 17:34 U 20 Page 8 of 27 Final 1.000 tiff eurof ins Environment Testing Certificate of Analytical Results 679115 Xenco Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Sample Id: BEI (71) Matrix: Soil Date Received:11.25.2020 09:30 Lab Sample Id: 679115-001 Date Collected: 11.18.2020 13:48 Analytical Method: SVOCs by SW846 8270E Prep Method: SW3550 Tech: JUN % Moisture: 6.29 Analyst: EKL Date Prep: 12.02.2020 20:25 Basis: Dry Weight Seq Number: 3143789 Parameter Cas Number Result RL NIDL Units Analysis Date Flag Dil bis(2-chloroisopropyl) ether 39638-32-9 0.380 U 3.56 0.380 mg/kg 12.04.2020 17:34 U bis(2-ethylhexyl) phthalate 117-81-7 3.56 U 7.11 3.56 mg/kg 12.04.2020 17:34 U Chrysene 218-01-9 0.353 U 3.56 0.353 mg/kg 12.04.2020 17:34 U Dibenz(a,h)Anthracene 53-70-3 0.271 U 3.56 0.271 mg/kg 12.04.2020 17:34 U Dibenzofuran 132-64-9 0.330 U 3.56 0.330 mg/kg 12.04.2020 17:34 U Diethyl Phthalate 84-66-2 0.326 U 3.56 0.326 mg/kg 12.04.2020 17:34 U Dimethyl Phthalate 131-11-3 0.339 U 3.56 0.339 mg/kg 12.04.2020 17:34 U di-n-Butyl Phthalate 84-74-2 0.342 U 3.56 0.342 mg/kg 12.04.2020 17:34 U di-n-Octyl Phthalate 117-84-0 0.283 U 3.56 0.283 mg/kg 12.04.2020 17:34 U Fluoranthene 206-44-0 0.313 U 3.56 0.313 mg/kg 12.04.2020 17:34 U Fluorene 86-73-7 3.09 3.56 0.295 mg/kg 12.04.2020 17:34 J Hexachlorobenzene 118-74-1 0.346 U 3.56 0.346 mg/kg 12.04.2020 17:34 U Hexachlorobutadiene 87-68-3 0.295 U 3.56 0.295 mg/kg 12.04.2020 17:34 U Hexachlorocyclopentadiene 77-47-4 0.324 U 3.56 0.324 mg/kg 12.04.2020 17:34 U Hexachloroethane 67-72-1 0.369 U 3.56 0.369 mg/kg 12.04.2020 17:34 U Indeno(1,2,3-c,d)Pyrene 193-39-5 0.287 U 3.56 0.287 mg/kg 12.04.2020 17:34 U Isophorone 78-59-1 0.310 U 3.56 0.310 mg/kg 12.04.2020 17:34 U Naphthalene 91-20-3 0.333 U 3.56 0.333 mg/kg 12.04.2020 17:34 U Nitrobenzene 98-95-3 0.395 U 3.56 0.395 mg/kg 12.04.2020 17:34 U N-Nitrosodi-n-Propylamine 621-64-7 0.371 U 3.56 0.371 mg/kg 12.04.2020 17:34 U N-Nitrosodiphenylamine 86-30-6 0.397 U 3.56 0.397 mg/kg 12.04.2020 17:34 U Pentachlorophenol 87-86-5 0.259 U 7.11 0.259 mg/kg 12.04.2020 17:34 U Phenanthrene 85-01-8 7.11 3.56 0.354 mg/kg 12.04.2020 17:34 Phenol 108-95-2 0.319 U 7.11 0.319 mg/kg 12.04.2020 17:34 U Pyrene 129-00-0 1.20 3.56 0.312 mg/kg 12.04.2020 17:34 J Pyridine 110-86-1 0.357 U 7.11 0.357 mg/kg 12.04.2020 17:34 U Surrogate Cas Number % Recovery Units Limits Analysis Date Flag 2-Fluorophenol 367-12-4 62 % 25-121 12.04.2020 17:34 Phenol-d6 13127-88-3 63 % 24-113 12.04.2020 17:34 Nitrobenzene-d5 4165-60-0 78 % 23-120 12.04.2020 17:34 2-Fluorobiphenyl 321-60-8 83 % 30-115 12.04.2020 17:34 2,4,6-Tribromophenol 118-79-6 77 % 19-122 12.04.2020 17:34 Terphenyl-D14 1718-51-0 84 % 18-137 12.04.2020 17:34 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Page 9 of 27 Final 1.000 tiff eurof ins Environment Testing Certificate of Analytical Results 679115 Xenco Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Sample Id: BEI (71) Matrix: Soil Date Received:11.25.2020 09:30 Lab Sample Id: 679115-001 Date Collected: 11.18.2020 13:48 Analytical Method: VOCs by SW-846 8260D Prep Method: SW5035A Tech: SAD Analyst: SAD Date Prep: 12.02.2020 12:30 % Moisture: 6.29 Basis: Dry Weight Seq Number: 3144346 Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil Acetone 67-64-1 0.467 U 4.21 0.467 mg/kg 12.02.2020 14:17 U 25 Benzene 71-43-2 0.0126 0.0421 0.00871 mg/kg 12.02.2020 14:17 J 25 Bromobenzene 108-86-1 0.0146 U 0.210 0.0146 mg/kg 12.02.2020 14:17 U 25 Bromochloromethane 74-97-5 0.0221 U 0.210 0.0221 mg/kg 12.02.2020 14:17 U 25 Bromodichloromethane 75-27-4 0.0106 U 0.210 0.0106 mg/kg 12.02.2020 14:17 U 25 Bromofonn 75-25-2 0.0435 U 0.210 0.0435 mg/kg 12.02.2020 14:17 U 25 Bromomethane 74-83-9 0.0397 U 0.210 0.0397 mg/kg 12.02.2020 14:17 UX 25 2-Butanone 78-93-3 0.319 0.842 0.153 mg/kg 12.02.2020 14:17 JX 25 tert-Butylbenzene 98-06-6 0.0540 U 0.210 0.0540 mg/kg 12.02.2020 14:17 U 25 Sec-Butylbenzene 135-98-8 2.10 0.210 0.0110 mg/kg 12.02.2020 14:17 25 n-Butylbenzene 104-51-8 3.52 0.210 0.0115 mg/kg 12.02.2020 14:17 25 Carbon Tetrachloride 56-23-5 0.0691 U 0.210 0.0691 mg/kg 12.02.2020 14:17 U 25 Chlorobenzene 108-90-7 0.00996 U 0.210 0.00996 mg/kg 12.02.2020 14:17 U 25 Chloroethane 75-00-3 0.0187 U 0.421 0.0187 mg/kg 12.02.2020 14:17 UX 25 Chloroform 67-66-3 0.00727 U 0.210 0.00727 mg/kg 12.02.2020 14:17 U 25 Chloromethane 74-87-3 0.0181 U 0.210 0.0181 mg/kg 12.02.2020 14:17 U 25 2-Chlorotoluene 95-49-8 0.0144 U 0.210 0.0144 mg/kg 12.02.2020 14:17 U 25 4-Chlorotoluene 106-43-4 0.0111 U 0.210 0.0111 mg/kg 12.02.2020 14:17 U 25 p-Cymene (p-Isopropyltoluene) 99-87-6 1.45 0.210 0.0134 mg/kg 12.02.2020 14:17 25 Dibromochloromethane 124-48-1 0.0376 U 0.210 0.0376 mg/kg 12.02.2020 14:17 U 25 1,2-Dibromoethane 106-93-4 0.0439 U 0.210 0.0439 mg/kg 12.02.2020 14:17 U 25 1,2-Dichlorobenzene 95-50-1 0.0121 U 0.210 0.0121 mg/kg 12.02.2020 14:17 U 25 1,3-Dichlorobenzene 541-73-1 0.0115 U 0.210 0.0115 mg/kg 12.02.2020 14:17 U 25 1,4-Dichlorobenzene 106-46-7 0.00903 U 0.210 0.00903 mg/kg 12.02.2020 14:17 U 25 1,2-Dichloroethane 107-06-2 0.0128 U 0.210 0.0128 mg/kg 12.02.2020 14:17 U 25 1, 1 -Dichloroethane 75-34-3 0.0158 U 0.210 0.0158 mg/kg 12.02.2020 14:17 U 25 trans-1,2-dichloroethene 156-60-5 0.0183 U 0.210 0.0183 mg/kg 12.02.2020 14:17 UX 25 cis-1,2-Dichloroethene 156-59-2 0.0127 U 0.210 0.0127 mg/kg 12.02.2020 14:17 U 25 1, 1 -Dichloroethene 75-35-4 0.0117 U 0.210 0.0117 mg/kg 12.02.2020 14:17 U 25 2,2-Dichloropropane 594-20-7 0.0221 U 0.210 0.0221 mg/kg 12.02.2020 14:17 U 25 1,3-Dichloropropane 142-28-9 0.0172 U 0.210 0.0172 mg/kg 12.02.2020 14:17 U 25 1,2-Dichloropropane 78-87-5 0.00835 U 0.210 0.00835 mg/kg 12.02.2020 14:17 U 25 trans- l,3-dichloropropene 10061-02-6 0.0383 U 0.210 0.0383 mg/kg 12.02.2020 14:17 U 25 1, 1 -Dichloropropene 563-58-6 0.0189 U 0.210 0.0189 mg/kg 12.02.2020 14:17 UX 25 cis-1,3-Dichloropropene 10061-01-5 0.00966 U 0.210 0.00966 mg/kg 12.02.2020 14:17 U 25 Ethylbenzene 100-41-4 0.156 0.0421 0.0141 mg/kg 12.02.2020 14:17 25 2-Hexanone 591-78-6 0.0898 U 2.10 0.0898 mg/kg 12.02.2020 14:17 UX 25 isopropylbenzene 98-82-8 0.390 0.210 0.00732 mg/kg 12.02.2020 14:17 25 Methylene Chloride 75-09-2 0.178 U 0.842 0.178 mg/kg 12.02.2020 14:17 UX 25 Page 10 of 27 Final 1.000 tiff eurof ins Environment Testing Certificate of Analytical Results 679115 Xenco Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Sample Id: BEI (71) Matrix: Soil Date Received:11.25.2020 09:30 Lab Sample Id: 679115-001 Date Collected: 11.18.2020 13:48 Analytical Method: VOCs by SW-846 8260D Prep Method: SW5035A Tech: SAD % Moisture: 6.29 Analyst: SAD Date Prep: 12.02.2020 12:30 Basis: Dry Weight Seq Number: 3144346 Parameter Cas Number Result RL NIDL Units Analysis Date Flag Dil 4-Methyl-2-Pentanone 108-10-1 0.110 U 2.10 0.110 mg/kg 12.02.2020 14:17 U MTBE 1634-04-4 0.0172 U 0.210 0.0172 mg/kg 12.02.2020 14:17 U Naphthalene 91-20-3 12.9 1.68 0.337 mg/kg 12.02.202015:28 D n-Propylbenzene 103-65-1 0.805 0.210 0.0120 mg/kg 12.02.2020 14:17 Styrene 100-42-5 0.00865 U 0.210 0.00865 mg/kg 12.02.2020 14:17 U 1,1,1,2-Tetrachloroethane 630-20-6 0.0112 U 0.210 0.0112 mg/kg 12.02.2020 14:17 U 1,1,2,2-Tetrachloroethane 79-34-5 0.0198 U 0.210 0.0198 mg/kg 12.02.2020 14:17 U Tetrachloroethylene 127-18-4 0.0156 U 0.210 0.0156 mg/kg 12.02.2020 14:17 U Toluene 108-88-3 0.279 0.210 0.0421 mg/kg 12.02.2020 14:17 1,2,3-Trichlorobenzene 87-61-6 0.0842 U 0.210 0.0842 mg/kg 12.02.2020 14:17 U 1,2,4-Trichlorobenzene 120-82-1 0.0842 U 0.210 0.0842 mg/kg 12.02.2020 14:17 U 1,1,2-Trichloroethane 79-00-5 0.0165 U 0.210 0.0165 mg/kg 12.02.2020 14:17 U 1, 1, 1 -Trichloroethane 71-55-6 0.0212 U 0.210 0.0212 mg/kg 12.02.2020 14:17 U Trichloroethene 79-01-6 0.0208 U 0.210 0.0208 mg/kg 12.02.2020 14:17 U Trichlorofluoromethane 75-69-4 0.0129 U 0.210 0.0129 mg/kg 12.02.2020 14:17 UX 1,2,3-Trichloropropane 96-18-4 0.0189 U 0.210 0.0189 mg/kg 12.02.2020 14:17 U 1,2,4-Trimethylbenzene 95-63-6 6.11 0.842 0.0429 mg/kg 12.02.202015:28 DX 1,3,5-Trimethylbenzene 108-67-8 1.64 0.210 0.0122 mg/kg 12.02.2020 14:17 Vinyl Acetate 108-05-4 0.108 U 0.421 0.108 mg/kg 12.02.2020 14:17 U Vinyl Chloride 75-01-4 0.0186 U 0.210 0.0186 mg/kg 12.02.2020 14:17 U o-Xylene 95-47-6 0.137 0.0421 0.0414 mg/kg 12.02.2020 14:17 m,p-Xylenes 179601-23-1 0.677 0.0842 0.0337 mg/kg 12.02.2020 14:17 Total Xylenes 1330-20-7 0.814 0.0421 0.0337 mg/kg 12.02.2020 14:17 Isopropyl Ether 108-20-3 0.0442 U 0.210 0.0442 mg/kg 12.02.2020 14:17 U Surrogate Cas Number % Recovery Units Limits Analysis Date Flag Dibromofluoromethane 1868-53-7 88 % 53-142 12.02.2020 14:17 1,2-Dichloroethane-D4 17060-07-0 99 % 56-150 12.02.2020 14:17 Toluene-D8 2037-26-5 104 % 70-130 12.02.2020 14:17 4-Bromofluorobenzene 460-00-4 106 % 68-152 12.02.2020 14:17 25 25 100 25 25 25 25 25 25 25 25 25 25 25 25 25 100 25 25 25 25 25 100 25 Page 11 of 27 Final 1.000 tiff eu rof ins Environment resting Xenco Sample Id: BEI (71) Lab Sample Id: 679115-001 Analytical Method: VPH Tech: NGA Analyst: NGA Seq Number: 3144596 Parameter C5-C8 Aliphatic C9-C12 Aliphatic C9-C10 Aromatic Surrogate 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) Certificate of Analytical Results 679115 Terraquest Environmental Consultants, P.C., Mebane, NC 1238 Union St SE Concord Matrix: Soil Date Received:11.25.2020 09:30 Date Collected: 11.18.2020 13:48 Date Prep: 12.10.2020 19:10 Cas Number Result RL MDL Prep Method: SW5035A % Moisture: 6.29 Basis: Dry Weight Units Analysis Date Flag Dil ALHYDRC5C8 12.5 U 50.5 12.5 mg/kg 12.11.2020 02:06 U 1000 ALHYDRCKE 604 50.5 22.5 mg/kg 12.11.2020 02:06 1000 HYDC9C10 325 16.8 6.06 mg/kg 12.11.2020 02:06 1000 Cas Number % Recovery Units Limits Analysis Date Flag 615-59-8 120 % 70-130 12.11.2020 02:06 615-59-8 117 % 70-130 12.11.2020 02:06 Page 12 of 27 Final 1.000 tiff eu rof ins Environment resting Xenco Flagging Criteria X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD. B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or laboratory contamination. D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference. Dilution factors are included in the final results. The result is from a diluted sample. E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated. F RPD exceeded lab control limits. J The target analyte was positively identified below the quantitation limit and above the detection limit. U Analyte was not detected. L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations. H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the Department Supervisor and QA Director. Data were determined to be valid for reporting. K Sample analyzed outside of recommended hold time. JN A combination of the "N" and the " Y qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated numerical value may not be consistent with the amount actually present in the environmental sample. ** Surrogate recovered outside laboratory control limit. BRL Below Reporting Limit. ND Not Detected. RL Reporting Limit MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation DL Method Detection Limit NC Non -Calculable SMP Client Sample BLK Method Blank BKS/LCS Blank Spike/Laboratory Control Sample BKSD/LCSD Blank Spike Duplicate/Laboratory Control Sample Duplicate MD/SD Method Duplicate/Sample Duplicate MS Matrix Spike + NELAC certification not offered for this compound. * (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation MSD: Matrix Spike Duplicate Page 13 of 27 Final 1.000 tiff eurof ins QC Summary 679115 Environment Testing 1lenco Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Analytical Method: Percent Moisture by SM2540G Seq Number: 3143638 Matrix: Solid MB Sample Id: 3143638-1-BLK MB Units Analysis Fla Parameter Result Date g Percent Moisture 0.0300 % 12.02.2020 08:00 Analytical Method: Percent Moisture by SM2540G Seq Number: 3143638 Matrix: Soil Parent Sample Id: 678371-013 MD Sample Id: 678371-013 D Parent MD %RPD RPD Units Analysis Fla Parameter Result Result Limit Date g Percent Moisture 25.6 25.7 0 10 % 12.02.2020 08:00 Analytical Method: Percent Moisture by SM2540G Seq Number: 3143638 Matrix: Solid Parent Sample Id: 679112-001 MD Sample Id: 679112-001 D Parent MD %RPD RPD Units Analysis Fla Parameter Result Result Limit Date g Percent Moisture 8.36 9.02 8 10 % 12.02.2020 08:00 Analytical Method: EPH by MADEP Method Seq Number: 3144206 MB Sample Id: 7716195-1-BLK MB Spike Parameter Result Amount C9 to C 18 Aliphatic Hydrocarbons 5.13 15.0 C 19 to C36Aliphatic Hydrocarbons <4.00 20.0 C11 to C22 Aromatics 4.84 42.5 Surrogate MB MB %Rec Flag 1-Chlorooctadecane 74 o-Terphenyl 85 2-Fluorobiphenyl 116 Prep Method: SW3550 Matrix: Solid Date Prep: 12.02.2020 LCS Sample Id: 7716195-1-BKS LCSD Sample Id: 7716195-1-BSD LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis Flag Result %Rec Result %Rec Limit Date 13.5 90 15.0 100 40-140 11 25 mg/kg 12.07.2020 21:39 17.0 85 14.8 74 40-140 14 25 mg/kg 12.07.2020 21:39 39.3 92 40.3 95 40-140 3 25 mg/kg 12.07.202014:14 LCS LCS LCSD LCSD Limits Units Analysis %Rec Flag °/oRec Flag Date 79 74 40-140 % 12.07.2020 21:39 86 90 40-140 % 12.07.202014:14 113 118 40-140 % 12.07.202014:14 MS/MSD Percent Recovery [D] = 100*(C-A) / B Relative Percent Difference RPD = 200* I (C-E) / (C+E) LCS/LCSD Recovery [D] = 100 * (C) / [B] Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) Page 14 of 27 LCS = Laboratory Control Sample A = Parent Result C = MS/LCS Result E = MSD/LCSD Result Final 1.000 MS = Matrix Spike B = Spike Added D = MSD/LCSD % Rec tiff etirof ins QC Summary 679115 Environment Testing 1lenco Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Analytical Method: EPH by MADEP Method Seq Number: 3144206 Parent Sample Id: 679115-001 Parent Spike Parameter Result Amount C9 to C18 Aliphatic Hydrocarbons 1950 16.0 C19 to C36Aliphatic Hydrocarbons 476 21.3 C11 to C22 Aromatics 921 45.3 Surrogate 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Prep Method: SW3550 Matrix: Soil Date Prep: 12.02.2020 MS Sample Id: 679115-001 S MSD Sample Id: 679115-001 SD MS MS MSD MSD Limits %RPD RPD Units Analysis Flag Result %Rec Result %Rec Limit Date 1840 0 2100 938 40-140 13 50 mg/kg 12.07.2020 23:00 X 446 0 517 192 40-140 15 50 mg/kg 12.07.2020 23:00 X 970 108 1050 285 40-140 8 50 mg/kg 12.07.202015:32 X MS MS MSD MSD Limits Units Analysis %Rec Flag %Rec Flag Date 50 42 40-140 % 12.07.2020 23:00 106 115 40-140 % 12.07.202015:32 110 100 40-140 % 12.07.202015:32 MS/MSD Percent Recovery [D] = 100*(C-A) / B Relative Percent Difference RPD = 200* I (C-E) / (C+E) LCS/LCSD Recovery [D] = 100 * (C) / [B] Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) Page 15 of 27 LCS = Laboratory Control Sample A = Parent Result C = MS/LCS Result E = MSD/LCSD Result Final 1.000 MS = Matrix Spike B = Spike Added D = MSD/LCSD % Rec tiff etirof ins Environment resting 1lenco Analytical Method: SVOCs by SW846 8270E Seq Number: 3143789 MB Sample Id: 7716193-1-BLK Parameter 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1-Methylnaphthalene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(k)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene QC Summary 679115 Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Matrix: Solid LCS Sample Id: 7716193-1-BKS MB Spike LCS LCS LCSD LCSD Result Amount Result %Rec Result %Rec <0.0145 1.67 1.43 86 1.34 80 <0.0154 1.67 1.42 85 1.35 81 <0.0139 1.67 1.41 84 1.33 80 <0.0150 1.67 1.41 84 1.34 80 <0.0267 1.67 1.43 86 1.36 81 <0.0191 1.67 1.54 92 1.48 89 <0.0158 1.67 1.56 93 1.47 88 <0.0174 1.67 1.60 96 1.52 91 <0.0165 1.67 1.54 92 1.45 87 <0.0127 1.67 1.49 89 1.43 86 <0.0233 1.67 1.54 92 1.46 87 <0.0290 1.67 1.52 91 1.33 80 <0.0158 1.67 1.57 94 1.49 89 <0.0452 1.67 1.44 86 1.38 83 <0.0185 1.67 1.60 96 1.53 92 <0.0156 1.67 1.47 88 1.42 85 <0.0146 1.67 1.52 91 1.45 87 <0.0154 1.67 1.59 95 1.53 92 <0.0139 1.67 1.52 91 1.47 88 <0.0127 1.67 1.34 80 1.30 78 <0.0133 1.67 1.43 86 1.37 82 <0.0184 1.67 1.57 94 1.51 90 <0.0126 1.67 1.46 87 1.39 83 <0.0162 1.67 1.42 85 1.35 81 <0.0139 1.67 1.40 84 1.36 81 <0.0258 1.67 1.54 92 1.49 89 <0.0155 1.67 1.42 85 1.35 81 <0.0148 1.67 1.44 86 1.37 82 <0.0136 1.67 1.45 87 1.40 84 <0.0138 1.67 1.46 87 1.42 85 <0.0141 1.67 1.41 84 1.37 82 <0.0172 1.67 1.47 88 1.43 86 <0.0126 1.67 1.44 86 1.39 83 <0.0154 1.67 1.47 88 1.42 85 <0.0194 1.67 1.48 89 1.45 87 <0.0350 5.00 3.90 78 3.02 60 <0.0182 1.67 1.51 90 1.47 88 <0.0168 1.67 1.44 86 1.36 81 <0.0152 1.67 1.41 84 1.33 80 <0.0178 1.67 1.43 86 1.35 81 <0.167 1.67 1.53 92 1.49 89 <0.0165 1.67 1.44 86 1.40 84 <0.0127 1.67 1.47 88 1.43 86 <0.0154 1.67 1.44 86 1.37 82 <0.0153 1.67 1.45 87 1.40 84 <0.0159 1.67 1.45 87 1.40 84 <0.0160 1.67 1.50 90 1.46 87 <0.0133 1.67 1.45 87 1.41 84 <0.0147 1.67 1.45 87 1.42 85 <0.0138 1.67 1.45 87 1.39 83 Prep Method: SW3550 Date Prep: 12.02.2020 LCSD Sample Id: 7716193-1-BSD Limits %RPD RPD Units Analysis Flag Limit Date 35-129 6 30 mg/kg 12.02.202019:07 38-122 5 30 mg/kg 12.02.202019:07 38-120 6 30 mg/kg 12.02.202019:07 37-121 5 30 mg/kg 12.02.202019:07 38-127 5 30 mg/kg 12.02.202019:07 40-135 4 30 mg/kg 12.02.202019:07 39-139 6 30 mg/kg 12.02.202019:07 36-135 5 30 mg/kg 12.02.202019:07 38-133 6 30 mg/kg 12.02.202019:07 48-131 4 30 mg/kg 12.02.202019:07 42-136 5 30 mg/kg 12.02.202019:07 32-138 13 30 mg/kg 12.02.202019:07 38-125 5 30 mg/kg 12.02.202019:07 36-126 4 30 mg/kg 12.02.202019:07 37-128 4 30 mg/kg 12.02.202019:07 30-133 3 40 mg/kg 12.02.202019:07 33-142 5 30 mg/kg 12.02.202019:07 38-126 4 30 mg/kg 12.02.202019:07 41-135 3 40 mg/kg 12.02.202019:07 30-146 3 40 mg/kg 12.02.202019:07 37-140 4 30 mg/kg 12.02.202019:07 40-134 4 30 mg/kg 12.02.202019:07 34-124 5 40 mg/kg 12.02.202019:07 41-131 5 30 mg/kg 12.02.202019:07 46-132 3 40 mg/kg 12.02.202019:07 21-152 3 40 mg/kg 12.02.202019:07 37-131 5 30 mg/kg 12.02.202019:07 39-129 5 30 mg/kg 12.02.202019:07 33-117 4 40 mg/kg 12.02.202019:07 39-139 3 30 mg/kg 12.02.202019:07 44-135 3 30 mg/kg 12.02.202019:07 43-153 3 30 mg/kg 12.02.202019:07 40-153 4 30 mg/kg 12.02.202019:07 40-153 3 30 mg/kg 12.02.202019:07 33-156 2 30 mg/kg 12.02.202019:07 31-135 25 50 mg/kg 12.02.202019:07 43-145 3 30 mg/kg 12.02.202019:07 30-129 6 30 mg/kg 12.02.202019:07 33-127 6 30 mg/kg 12.02.202019:07 25-124 6 30 mg/kg 12.02.202019:07 46-145 3 30 mg/kg 12.02.202019:07 42-135 3 30 mg/kg 12.02.202019:07 41-155 3 30 mg/kg 12.02.202019:07 39-132 5 30 mg/kg 12.02.202019:07 45-131 4 30 mg/kg 12.02.202019:07 43-132 4 30 mg/kg 12.02.202019:07 43-142 3 30 mg/kg 12.02.202019:07 34-166 3 30 mg/kg 12.02.202019:07 41-138 2 30 mg/kg 12.02.202019:07 41-131 4 30 mg/kg 12.02.202019:07 MS/MSD Percent Recovery [D] = 100*(C-A) / B LCS = Laboratory Control Sample MS = Matrix Spike Relative Percent Difference RPD = 200* I (C-E) / (C+E) A = Parent Result B = Spike Added LCS/LCSD Recovery [D] = 100 * (C) / [B] C = MS/LCS Result D = MSD/LCSD % Rec Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) E = MSD/LCSD Result Page 16 of 27 Final 1.000 tiff etirof ins Environment resting xenco QC Summary 679115 Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Analytical Method: SVOCs by SW846 8270E Prep Method: SW3550 Seq Number: 3143789 Matrix: Solid Date Prep: 12.02.2020 MB Sample Id: 7716193-1-BLK LCS Sample Id: 7716193-1-BKS LCSD Sample Id: 7716193-1-BSD Parameter NIB Spike LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis Fla S Result Amount Result %Rec Result %Rec Limit Date Hexachlorobenzene <0.0162 1.67 1.40 84 1.35 81 36-142 4 30 mg/kg 12.02.202019:07 Hexachlorobutadiene <0.0138 1.67 1.41 84 1.33 80 35-129 6 30 mg/kg 12.02.202019:07 Hexachlorocyclopentadiene <0.0152 1.67 1.23 74 1.16 69 16-106 6 30 mg/kg 12.02.202019:07 Hexachloroethane <0.0173 1.67 1.40 84 1.34 80 36-121 4 30 mg/kg 12.02.202019:07 Indeno(1,2,3-c,d)Pyrene <0.0134 1.67 1.48 89 1.42 85 39-154 4 30 mg/kg 12.02.202019:07 Isophorone <0.0145 1.67 1.48 89 1.41 84 36-128 5 30 mg/kg 12.02.202019:07 Naphthalene <0.0156 1.67 1.43 86 1.35 81 35-128 6 30 mg/kg 12.02.202019:07 Nitrobenzene <0.0185 1.67 1.47 88 1.39 83 32-129 6 30 mg/kg 12.02.202019:07 N-Nitrosodi-n-Propylamine <0.0174 1.67 1.47 88 1.41 84 34-129 4 30 mg/kg 12.02.202019:07 N-Nitrosodiphenylamine <0.0186 1.67 1.46 87 1.40 84 27-155 4 30 mg/kg 12.02.202019:07 Pentachlorophenol <0.0121 1.67 1.28 77 1.24 74 14-148 3 40 mg/kg 12.02.202019:07 Phenanthrene <0.0166 1.67 1.40 84 1.35 81 37-139 4 30 mg/kg 12.02.202019:07 Phenol <0.0150 1.67 1.57 94 1.47 88 34-127 7 40 mg/kg 12.02.202019:07 Pyrene <0.0146 1.67 1.45 87 1.41 84 42-138 3 30 mg/kg 12.02.202019:07 Pyridine <0.0167 1.67 1.07 64 1.01 60 30-113 6 40 mg/kg 12.02.202019:07 Surrogate NIB NIB LCS LCS LCSD LCSD Limits Units Analysis %Rec Fla g %Rec Flag u %Rec Flag Date 2-Fluorophenol 83 94 89 25-121 % 12.02.202019:07 Phenol-d6 80 96 92 24-113 % 12.02.202019:07 Nitrobenzene-d5 76 88 83 23-120 % 12.02.202019:07 2-Fluorobiphenyl 82 87 82 30-115 % 12.02.202019:07 2,4,6-Tribromophenol 75 90 87 19-122 % 12.02.202019:07 Terphenyl-D14 86 87 86 18-137 % 12.02.202019:07 MS/MSD Percent Recovery [D] = 100*(C-A) / B Relative Percent Difference RPD = 200* I (C-E) / (C+E) LCS/LCSD Recovery [D] = 100 * (C) / [B] Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) LCS = Laboratory Control Sample A = Parent Result C = MS/LCS Result E = MSD/LCSD Result MS = Matrix Spike B = Spike Added D = MSD/LCSD % Rec Page 17 of 27 Final 1.000 tiff etirof ins Environment resting 1lenco QC Summary 679115 Analytical Method: SVOCs by SW846 8270E Seq Number: 3143789 Parent Sample Id: 678938-001 Parameter 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1-Methylnaphthalene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(k)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Matrix: Soil MS Sample Id: 678938-001 S Parent Spike MS MS MSD MSD Result Amount Result %Rec Result %Rec <0.0175 2.00 1.52 76 1.60 80 <0.0185 2.00 1.52 76 1.61 81 <0.0167 2.00 1.50 75 1.58 79 <0.0180 2.00 1.50 75 1.59 80 <0.0321 2.00 1.56 78 1.66 83 <0.0229 2.00 1.66 83 1.79 90 <0.0189 2.00 1.66 83 1.78 89 <0.0210 2.00 1.70 85 1.82 91 <0.0198 2.00 1.65 83 1.75 88 <0.0153 2.00 1.57 79 1.71 86 <0.0280 2.00 1.65 83 1.75 88 <0.0349 2.00 1.51 76 1.61 81 <0.0190 2.00 1.68 84 1.77 89 <0.0543 2.00 1.55 78 1.68 84 <0.0223 2.00 1.71 86 1.83 92 <0.0187 2.00 1.57 79 1.68 84 <0.0176 2.00 1.63 82 1.74 87 <0.0185 2.00 1.70 85 1.80 90 <0.0167 2.00 1.65 83 1.77 89 <0.0153 2.00 1.46 73 1.62 81 <0.0159 2.00 1.54 77 1.64 82 <0.0221 2.00 1.70 85 1.84 92 <0.0152 2.00 1.49 75 1.61 81 <0.0195 2.00 1.52 76 1.63 82 <0.0167 2.00 1.57 79 1.70 85 <0.0311 2.00 1.63 82 1.79 90 <0.0186 2.00 1.53 77 1.61 81 <0.0178 2.00 1.55 78 1.65 83 <0.0164 2.00 1.45 73 1.60 80 <0.0166 2.00 1.57 79 1.69 85 <0.0169 2.00 1.53 77 1.67 84 <0.0207 2.00 1.59 80 1.73 87 <0.0151 2.00 1.58 79 1.72 86 <0.0185 2.00 1.59 80 1.71 86 <0.0233 2.00 1.59 80 1.74 87 <0.0421 6.01 7.18 119 7.84 130 <0.0218 2.00 1.62 81 1.78 89 <0.0202 2.00 1.54 77 1.62 81 <0.0183 2.00 1.48 74 1.56 78 <0.0214 2.00 1.53 77 1.63 82 <0.200 2.00 1.70 85 1.81 91 <0.0199 2.00 1.56 78 1.69 85 <0.0153 2.00 1.60 80 1.74 87 <0.0186 2.00 1.55 78 1.65 83 <0.0184 2.00 1.57 79 1.70 85 <0.0191 2.00 1.56 78 1.67 84 <0.0193 2.00 1.64 82 1.79 90 <0.0160 2.00 1.58 79 1.73 87 <0.0177 2.00 1.58 79 1.71 86 <0.0166 2.00 1.56 78 1.67 84 Prep Method: SW3550 Date Prep: 12.02.2020 MSD Sample Id: 678938-001 SD Limits %RPD RPD Units Analysis Flag Limit Date 35-129 5 30 mg/kg 12.02.2020 20:19 38-122 6 30 mg/kg 12.02.2020 20:19 38-120 5 30 mg/kg 12.02.2020 20:19 37-121 6 30 mg/kg 12.02.2020 20:19 38-127 6 30 mg/kg 12.02.2020 20:19 40-135 8 30 mg/kg 12.02.2020 20:19 39-139 7 30 mg/kg 12.02.2020 20:19 36-135 7 30 mg/kg 12.02.2020 20:19 38-133 6 30 mg/kg 12.02.2020 20:19 48-131 9 30 mg/kg 12.02.2020 20:19 42-136 6 30 mg/kg 12.02.2020 20:19 32-138 6 30 mg/kg 12.02.2020 20:19 38-125 5 30 mg/kg 12.02.2020 20:19 36-126 8 30 mg/kg 12.02.2020 20:19 37-128 7 30 mg/kg 12.02.2020 20:19 30-133 7 40 mg/kg 12.02.2020 20:19 33-142 7 30 mg/kg 12.02.2020 20:19 38-126 6 30 mg/kg 12.02.2020 20:19 41-135 7 40 mg/kg 12.02.2020 20:19 30-146 10 40 mg/kg 12.02.2020 20:19 37-140 6 30 mg/kg 12.02.2020 20:19 40-134 8 30 mg/kg 12.02.2020 20:19 34-124 8 40 mg/kg 12.02.2020 20:19 41-131 7 30 mg/kg 12.02.2020 20:19 46-132 8 40 mg/kg 12.02.2020 20:19 21-152 9 40 mg/kg 12.02.2020 20:19 37-131 5 30 mg/kg 12.02.2020 20:19 39-129 6 30 mg/kg 12.02.2020 20:19 33-117 10 40 mg/kg 12.02.2020 20:19 39-139 7 30 mg/kg 12.02.2020 20:19 44-135 9 30 mg/kg 12.02.2020 20:19 43-153 8 30 mg/kg 12.02.2020 20:19 40-153 8 30 mg/kg 12.02.2020 20:19 40-153 7 30 mg/kg 12.02.2020 20:19 33-156 9 30 mg/kg 12.02.2020 20:19 31-135 9 50 mg/kg 12.02.2020 20:19 43-145 9 30 mg/kg 12.02.2020 20:19 30-129 5 30 mg/kg 12.02.2020 20:19 33-127 5 30 mg/kg 12.02.2020 20:19 25-124 6 30 mg/kg 12.02.2020 20:19 46-145 6 30 mg/kg 12.02.2020 20:19 42-135 8 30 mg/kg 12.02.2020 20:19 41-155 8 30 mg/kg 12.02.2020 20:19 39-132 6 30 mg/kg 12.02.2020 20:19 45-131 8 30 mg/kg 12.02.2020 20:19 43-132 7 30 mg/kg 12.02.2020 20:19 43-142 9 30 mg/kg 12.02.2020 20:19 34-166 9 30 mg/kg 12.02.2020 20:19 41-138 8 30 mg/kg 12.02.2020 20:19 41-131 7 30 mg/kg 12.02.2020 20:19 MS/MSD Percent Recovery [D] = 100*(C-A) / B LCS = Laboratory Control Sample MS = Matrix Spike Relative Percent Difference RPD = 200* I (C-E) / (C+E) A = Parent Result B = Spike Added LCS/LCSD Recovery [D] = 100 * (C) / [B] C = MS/LCS Result D = MSD/LCSD % Rec Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) E = MSD/LCSD Result Page 18 of 27 Final 1.000 tiff etirof ins Environment resting xenco QC Summary 679115 Analytical Method: SVOCs by SW846 8270E Seq Number: 3143789 Parent Sample Id: 678938-001 Parameter Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Surrogate 2-Fluorophenol Phenol-& Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D 14 MS/MSD Percent Recovery Relative Percent Difference LCS/LCSD Recovery Log Difference Parent Result <0.0195 <0.0166 <0.0183 <0.0208 <0.0162 <0.0174 <0.0188 <0.0222 <0.0209 <0.0224 <0.0146 <0.0199 <0.0180 <0.0176 <0.0201 Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Spike Amount 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 Prep Method: SW3550 Matrix: Soil Date Prep: 12.02.2020 MS Sample Id: 678938-001 S MSD Sample Id: 678938-001 SD MS MS MSD MSD Limits %RPD RPD Units Analysis Flag Result %Rec Result %Rec Limit Date 1.53 77 1.65 83 36-142 8 30 mg/kg 12.02.2020 20:19 1.52 76 1.58 79 35-129 4 30 mg/kg 12.02.2020 20:19 1.35 68 1.45 73 16-106 7 30 mg/kg 12.02.2020 20:19 1.50 75 1.59 80 36-121 6 30 mg/kg 12.02.2020 20:19 1.60 80 1.73 87 39-154 8 30 mg/kg 12.02.2020 20:19 1.60 80 1.69 85 36-128 5 30 mg/kg 12.02.2020 20:19 1.53 77 1.61 81 35-128 5 30 mg/kg 12.02.2020 20:19 1.57 79 1.65 83 32-129 5 30 mg/kg 12.02.2020 20:19 1.60 80 1.68 84 34-129 5 30 mg/kg 12.02.2020 20:19 1.58 79 1.68 84 27-155 6 30 mg/kg 12.02.2020 20:19 1.42 71 1.51 76 14-148 6 40 mg/kg 12.02.2020 20:19 1.51 76 1.63 82 37-139 8 30 mg/kg 12.02.2020 20:19 1.64 82 1.75 88 34-127 6 40 mg/kg 12.02.2020 20:19 1.57 79 1.71 86 42-138 9 30 mg/kg 12.02.2020 20:19 0.693 35 0.947 47 30-113 31 40 mg/kg 12.02.2020 20:19 MS MS MSD MSD Limits Units Analysis '% Rec Flag %Rec Flag Date 83 88 25-121 % 12.02.2020 20:19 86 90 24-113 % 12.02.2020 20:19 78 83 23-120 % 12.02.2020 20:19 78 82 30-115 % 12.02.2020 20:19 82 87 19-122 % 12.02.2020 20:19 80 86 18-137 % 12.02.2020 20:19 [D] = 100*(GA) / B RPD = 200* I (C-E) / (C+E) [D] = 100 * (C) / [B] Log Diff. = Log(Sample Duplicate) - Log(Original Sample) LCS = Laboratory Control Sample A = Parent Result C = MS/LCS Result E = MSD/LCSD Result MS = Matrix Spike B = Spike Added D = MSD/LCSD % Rec Page 19 of 27 Final 1.000 tiff etirof ins Environment Testing 1lenco Analytical Method: VOCs by SW-846 8260D Seq Number: 3144346 MB Sample Id: 7716731-1-BLK Parameter Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone tert-Butylbenzene Sec-Butylbenzene n-Butylbenzene Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethane trans-1,2-dichloroethene cis-1,2-Dichloroethene 1, 1 -Dichloroethene 2,2-Dichloropropane 1,3-Dichloropropane 1,2-Dichloropropane trans-1,3-dichloropropene 1, 1 -Dichloropropene cis-1,3-Dichloropropene Ethylbenzene 2-Hexanone isopropylbenzene Methylene Chloride 4-Methyl-2-Pentanone MTBE Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene QC Summary 679115 Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Matrix: Solid LCS Sample Id: 7716731-1-BKS MB Spike LCS LCS LCSD LCSD Result Amount Result %Rec Result %Rec <0.0111 0.250 0.212 85 0.246 98 <0.000207 0.0500 0.0475 95 0.0468 94 <0.000346 0.0500 0.0492 98 0.0472 94 <0.000526 0.0500 0.0462 92 0.0466 93 <0.000251 0.0500 0.0452 90 0.0454 91 <0.00103 0.0500 0.0536 107 0.0541 108 <0.000943 0.0500 0.0386 77 0.0392 78 <0.00365 0.250 0.198 79 0.238 95 <0.00128 0.0500 0.0508 102 0.0479 96 <0.000261 0.0500 0.0518 104 0.0483 97 <0.000274 0.0500 0.0512 102 0.0475 95 <0.00164 0.0500 0.0491 98 0.0478 96 <0.000237 0.0500 0.0503 101 0.0496 99 <0.000444 0.0500 0.0456 91 0.0444 89 <0.000173 0.0500 0.0450 90 0.0445 89 <0.000431 0.0500 0.0393 79 0.0386 77 <0.000342 0.0500 0.0499 100 0.0479 96 <0.000264 0.0500 0.0479 96 0.0449 90 <0.000319 0.0500 0.0525 105 0.0490 98 <0.000895 0.0500 0.0494 99 0.0500 100 <0.00104 0.0500 0.0487 97 0.0507 101 <0.000288 0.0500 0.0502 100 0.0475 95 <0.000273 0.0500 0.0503 101 0.0479 96 <0.000214 0.0500 0.0491 98 0.0472 94 <0.000304 0.0500 0.0442 88 0.0452 90 <0.000376 0.0500 0.0453 91 0.0446 89 <0.000434 0.0500 0.0482 96 0.0471 94 <0.000301 0.0500 0.0458 92 0.0452 90 <0.000277 0.0500 0.0500 100 0.0488 98 <0.000524 0.0500 0.0461 92 0.0456 91 <0.000409 0.0500 0.0469 94 0.0468 94 <0.000198 0.0500 0.0462 92 0.0464 93 <0.000909 0.0500 0.0471 94 0.0478 96 <0.000448 0.0500 0.0481 96 0.0472 94 <0.000230 0.0500 0.0464 93 0.0462 92 <0.000336 0.0500 0.0506 101 0.0494 99 <0.00213 0.250 0.209 84 0.237 95 <0.000174 0.0500 0.0530 106 0.0515 103 <0.00422 0.0500 0.0431 86 0.0434 87 <0.00261 0.250 0.199 80 0.224 90 <0.000409 0.0500 0.0422 84 0.0433 87 <0.00200 0.0500 0.0506 101 0.0503 101 <0.000286 0.0500 0.0514 103 0.0482 96 <0.000205 0.0500 0.0506 101 0.0501 100 <0.000267 0.0500 0.0528 106 0.0526 105 <0.000470 0.0500 0.0463 93 0.0467 93 <0.000370 0.0500 0.0554 ill 0.0532 106 <0.00100 0.0500 0.0475 95 0.0460 92 <0.00200 0.0500 0.0557 ill 0.0536 107 <0.00200 0.0500 0.0561 112 0.0537 107 Prep Method: SW5035A Date Prep: 12.02.2020 LCSD Sample Id: 7716731-1-BSD Limits %RPD RPD Units Analysis Limit Date 50-150 15 25 mg/kg 12.02.202010:31 66-142 1 25 mg/kg 12.02.202010:31 75-125 4 25 mg/kg 12.02.202010:31 60-140 1 25 mg/kg 12.02.202010:31 75-125 0 25 mg/kg 12.02.202010:31 75-125 1 25 mg/kg 12.02.202010:31 60-140 2 25 mg/kg 12.02.202010:31 75-125 18 25 mg/kg 12.02.202010:31 75-125 6 25 mg/kg 12.02.202010:31 75-125 7 25 mg/kg 12.02.202010:31 75-125 7 25 mg/kg 12.02.202010:31 62-125 3 25 mg/kg 12.02.202010:31 60-133 1 25 mg/kg 12.02.202010:31 60-140 3 25 mg/kg 12.02.202010:31 74-125 1 25 mg/kg 12.02.202010:31 60-140 2 25 mg/kg 12.02.202010:31 73-125 4 25 mg/kg 12.02.202010:31 74-125 6 25 mg/kg 12.02.202010:31 75-125 7 25 mg/kg 12.02.202010:31 73-125 1 25 mg/kg 12.02.202010:31 73-125 4 25 mg/kg 12.02.202010:31 75-125 6 25 mg/kg 12.02.202010:31 75-125 5 25 mg/kg 12.02.202010:31 75-125 4 25 mg/kg 12.02.202010:31 68-127 2 25 mg/kg 12.02.202010:31 72-125 2 25 mg/kg 12.02.202010:31 75-125 2 25 mg/kg 12.02.202010:31 75-125 1 25 mg/kg 12.02.202010:31 59-172 2 25 mg/kg 12.02.202010:31 75-125 1 25 mg/kg 12.02.202010:31 75-125 0 25 mg/kg 12.02.202010:31 74-125 0 25 mg/kg 12.02.202010:31 66-125 1 25 mg/kg 12.02.202010:31 75-125 2 25 mg/kg 12.02.202010:31 74-125 0 25 mg/kg 12.02.202010:31 75-125 2 25 mg/kg 12.02.202010:31 75-125 13 25 mg/kg 12.02.202010:31 75-125 3 25 mg/kg 12.02.202010:31 75-125 1 25 mg/kg 12.02.202010:31 60-140 12 25 mg/kg 12.02.202010:31 60-140 3 25 mg/kg 12.02.202010:31 70-130 1 25 mg/kg 12.02.202010:31 75-125 6 25 mg/kg 12.02.202010:31 75-125 1 25 mg/kg 12.02.202010:31 72-125 0 25 mg/kg 12.02.202010:31 74-125 1 25 mg/kg 12.02.202010:31 71-125 4 25 mg/kg 12.02.202010:31 59-139 3 25 mg/kg 12.02.202010:31 75-137 4 25 mg/kg 12.02.202010:31 75-135 4 25 mg/kg 12.02.202010:31 MS/MSD Percent Recovery [D] = 100*(C-A) / B LCS = Laboratory Control Sample MS = Matrix Spike Relative Percent Difference RPD = 200* I (C-E) / (C+E) A = Parent Result B = Spike Added LCS/LCSD Recovery [D] = 100 * (C) / [B] C = MS/LCS Result D = MSD/LCSD % Rec Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) E = MSD/LCSD Result Flag Page 20 of 27 Final 1.000 tiff etirof ins Environment resting 1lenco QC Summary 679115 Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Analytical Method: VOCs by SW-846 8260D Prep Method: SW5035A Seq Number: 3144346 Matrix: Solid Date Prep: 12.02.2020 MB Sample Id: 7716731-1-BLK LCS Sample Id: 7716731-1-BKS LCSD Sample Id: 7716731-1-BSD Parameter NIB Spike LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis Result Amount Result %Rec Result %Rec Limit Date 1,1,2-Trichloroethane <0.000392 0.0500 0.0473 95 0.0485 97 75-127 3 25 mg/kg 12.02.2020 10:31 1, 1, 1 -Trichloroethane <0.000503 0.0500 0.0471 94 0.0467 93 75-125 1 25 mg/kg 12.02.2020 10:31 Trichloroethene <0.000494 0.0500 0.0489 98 0.0470 94 62-137 4 25 mg/kg 12.02.2020 10:31 Trichlorofluoromethane <0.000307 0.0500 0.0466 93 0.0457 91 67-125 2 25 mg/kg 12.02.2020 10:31 1,2,3-Trichloropropane <0.000450 0.0500 0.0454 91 0.0478 96 75-125 5 25 mg/kg 12.02.2020 10:31 1,2,4-Trimethylbenzene <0.000255 0.0500 0.0492 98 0.0464 93 75-125 6 25 mg/kg 12.02.2020 10:31 1,3,5-Trimethylbenzene <0.000289 0.0500 0.0498 100 0.0470 94 70-130 6 25 mg/kg 12.02.2020 10:31 Vinyl Acetate <0.00256 0.250 0.210 84 0.221 88 60-140 5 25 mg/kg 12.02.2020 10:31 Vinyl Chloride <0.000441 0.0500 0.0448 90 0.0436 87 60-140 3 25 mg/kg 12.02.2020 10:31 o-Xylene <0.000985 0.0500 0.0497 99 0.0494 99 75-125 1 25 mg/kg 12.02.2020 10:31 m,p-Xylenes <0.000800 0.100 0.101 101 0.0990 99 75-125 2 25 mg/kg 12.02.2020 10:31 Isopropyl Ether <0.00105 0.0500 0.0426 85 0.0430 86 60-140 1 25 mg/kg 12.02.2020 10:31 Surrogate NIB NIB LCS LCS LCSD LCSD Limits Units Analysis %Rec Flag %Rec Flag %Rec Flag Date Dibromofluoromethane 92 94 95 53-142 % 12.02.2020 10:31 1,2-Dichloroethane-D4 98 98 100 56-150 % 12.02.2020 10:31 Toluene-138 99 101 101 70-130 % 12.02.2020 10:31 4-Bromofluorobenzene 96 96 93 68-152 % 12.02.2020 10:31 MS/MSD Percent Recovery [D] = 100*(C-A) / B Relative Percent Difference RPD = 200* I (C-E) / (C+E) LCS/LCSD Recovery [D] = 100 * (C) / [B] Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) LCS = Laboratory Control Sample A = Parent Result C = MS/LCS Result E = MSD/LCSD Result MS = Matrix Spike B = Spike Added D = MSD/LCSD % Rec Flag Page 21 of 27 Final 1.000 QC Summary 679115 tiff eurof ins Environment Testing 1lenco Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Analytical Method: VOCs by SW-846 8260D Prep Method: SW5035A Seq Number: 3144346 Matrix: Soil Date Prep: 12.02.2020 Parent Sample Id: 679115-001 MS Sample Id: 679115-001 S Parameter Parent Spike MS MS Limits Units Analysis Result Amount Result %Rec Date Acetone <0.467 10.5 8.50 81 50-150 mg/kg 12.02.2020 16:34 Benzene 0.0126 2.10 1.58 75 66-142 mg/kg 12.02.2020 16:34 Bromobenzene <0.0146 2.10 1.90 90 75-125 mg/kg 12.02.2020 16:34 Bromochloromethane <0.0221 2.10 1.53 73 60-140 mg/kg 12.02.2020 16:34 Bromodichloromethane <0.0106 2.10 1.57 75 75-125 mg/kg 12.02.2020 16:34 Bromoform <0.0435 2.10 1.63 78 75-125 mg/kg 12.02.2020 16:34 Bromomethane <0.0397 2.10 0.754 36 60-140 mg/kg 12.02.2020 1 6:34 2-Butanone 0.319 10.5 8.13 74 75-125 mg/kg 12.02.2020 16:34 tert-Butylbenzene <0.0540 2.10 1.93 92 75-125 mg/kg 12.02.2020 16:34 Sec-Butylbenzene 2.10 2.10 3.80 81 75-125 mg/kg 12.02.2020 16:34 n-Butylbenzene 3.52 2.10 5.11 76 75-125 mg/kg 12.02.2020 16:34 Carbon Tetrachloride <0.0691 2.10 1.59 76 62-125 mg/kg 12.02.2020 16:34 Chlorobenzene <0.00996 2.10 1.76 84 60-133 mg/kg 12.02.2020 16:34 Chloroethane <0.0187 2.10 0.789 38 60-140 mg/kg 12.02.2020 16:34 Chloroform <0.00727 2.10 1.63 78 74-125 mg/kg 12.02.2020 16:34 Chloromethane <0.0181 2.10 1.27 60 60-140 mg/kg 12.02.2020 16:34 2-Chlorotoluene <0.0144 2.10 1.90 90 73-125 mg/kg 12.02.2020 16:34 4-Chlorotoluene <0.0111 2.10 1.87 89 74-125 mg/kg 12.02.2020 16:34 p-Cymene (p-Isopropyltoluene) 1.45 2.10 3.21 84 75-125 mg/kg 12.02.2020 16:34 Dibromochloromethane <0.0376 2.10 1.69 80 73-125 mg/kg 12.02.2020 16:34 1,2-Dibromoethane <0.0439 2.10 1.75 83 73-125 mg/kg 12.02.2020 16:34 1,2-Dichlorobenzene <0.0121 2.10 1.78 85 75-125 mg/kg 12.02.2020 16:34 1,3-Dichlorobenzene <0.0115 2.10 1.78 85 75-125 mg/kg 12.02.2020 16:34 1,4-Dichlorobenzene <0.00903 2.10 1.73 82 75-125 mg/kg 12.02.2020 16:34 1,2-Dichloroethane <0.0128 2.10 1.57 75 68-127 mg/kg 12.02.2020 16:34 1,1-Dichloroethane <0.0158 2.10 1.59 76 72-125 mg/kg 12.02.2020 16:34 trans-1,2-dichloroethene <0.0183 2.10 1.47 70 75-125 mg/kg 12.02.2020 16:34 cis-1,2-Dichloroethene <0.0127 2.10 1.59 76 75-125 mg/kg 12.02.2020 16:34 1, 1 -Dichloroethene <0.0117 2.10 1.52 72 59-172 mg/kg 12.02.2020 16:34 2,2-Dichloropropane <0.0221 2.10 1.65 79 75-125 mg/kg 12.02.2020 16:34 1,3-Dichloropropane <0.0172 2.10 1.70 81 75-125 mg/kg 12.02.2020 16:34 1,2-Dichloropropane <0.00835 2.10 1.66 79 74-125 mg/kg 12.02.2020 16:34 trans-1,3-dichloropropene <0.0383 2.10 1.67 80 66-125 mg/kg 12.02.2020 16:34 1, 1 -Dichloropropene <0.0189 2.10 1.53 73 75-125 mg/kg 12.02.2020 16:34 cis-1,3-Dichloropropene <0.00966 2.10 1.60 76 74-125 mg/kg 12.02.2020 16:34 Ethylbenzene 0.156 2.10 1.89 83 75-125 mg/kg 12.02.2020 16:34 2-Hexanone <0.0898 10.5 6.99 67 75-125 mg/kg 12.02.2020 16:34 isopropylbenzene 0.390 2.10 2.20 86 75-125 mg/kg 12.02.2020 16:34 Methylene Chloride <0.178 2.10 1.40 67 75-125 mg/kg 12.02.2020 16:34 4-Methyl-2-Pentanone <0.110 10.5 7.60 72 60-140 mg/kg 12.02.2020 16:34 MTBE <0.0172 2.10 1.60 76 60-140 mg/kg 12.02.2020 16:34 Naphthalene 13.8 2.10 16.1 110 70-130 mg/kg 12.02.2020 16:34 n-Propylbenzene 0.805 2.10 2.69 90 75-125 mg/kg 12.02.2020 16:34 Styrene <0.00865 2.10 1.74 83 75-125 mg/kg 12.02.2020 16:34 1, 1, 1,2-Tetrachloroethane <0.0112 2.10 1.88 90 72-125 mg/kg 12.02.2020 16:34 1,1,2,2-Tetrachloroethane <0.0198 2.10 1.77 84 74-125 mg/kg 12.02.2020 16:34 Tetrachloroethylene <0.0156 2.10 1.77 84 71-125 mg/kg 12.02.2020 16:34 Toluene 0.279 2.10 1.84 74 59-139 mg/kg 12.02.2020 16:34 1,2,3-Trichlorobenzene <0.0842 2.10 1.91 91 75-137 mg/kg 12.02.2020 16:34 1,2,4-Trichlorobenzene <0.0842 2.10 1.90 90 75-135 mg/kg 12.02.2020 16:34 MS/MSD Percent Recovery [D] = 100*(C-A) / B LCS = Laboratory Control Sample MS = Matrix Spike Relative Percent Difference RPD = 200* I (C-E) / (C+E) A = Parent Result B = Spike Added LCS/LCSD Recovery [D] = 100 * (C) / [B] C = MS/LCS Result D = MSD/LCSD % Rec Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) E = MSD/LCSD Result Page 22 of 27 Final 1.000 Flag V X /1 /1 X tiff etirof ins QC Summary 679115 Environment Testing 1lenco Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Analytical Method: VOCs by SW-846 8260D Seq Number: 3144346 Parent Sample Id: 679115-001 Parameter Parent Spike Result Amount 1,1,2-Trichloroethane <0.0165 2.10 1, 1, 1 -Trichloroethane <0.0212 2.10 Trichloroethene <0.0208 2.10 Trichlorofluoromethane <0.0129 2.10 1,2,3-Trichloropropane <0.0189 2.10 1,2,4-Trimethylbenzene 6.32 2.10 1,3,5-Trimethylbenzene 1.64 2.10 Vinyl Acetate <0.108 10.5 Vinyl Chloride <0.0186 2.10 o-Xylene 0.137 2.10 m,p-Xylenes 0.677 4.21 Isopropyl Ether <0.0442 2.10 Surrogate Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene Analytical Method: VPH Seq Number: 3144596 MB Sample Id: 7716905-1-BLK Parameter MB Spike Result Amount C5-C8 Aliphatic <0.00745 0.150 C9-C12 Aliphatic <0.0134 0.150 C9-C10 Aromatic <0.00360 0.0500 Surrogate %Rec MB /oRec Flag 2,5-Dibromotoluene 118 2,5-Dibromotoluene (PID) 109 Matrix: Soil MS Sample Id: 679115-001 S MS MS Limits Result %Rec 1.90 90 75-127 1.64 78 75-125 1.60 76 62-137 1.38 66 67-125 1.69 80 75-125 7.73 67 75-125 3.37 82 70-130 7.51 72 60-140 1.35 64 60-140 1.85 82 75-125 4.06 80 75-125 1.56 74 60-140 MS MS %Rec Flag 93 103 102 103 Prep Method: SW5035A Date Prep: 12.02.2020 Units Analysis Flag Date mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 X mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 X mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 mg/kg 12.02.202016:34 Limits Units Analysis Date 53-142 % 12.02.202016:34 56-150 % 12.02.202016:34 70-130 % 12.02.202016:34 68-152 % 12.02.202016:34 Prep Method: SW5035A Matrix: Solid Date Prep: 12.10.2020 LCS Sample Id: 7716905-1-BKS LCSD Sample Id: 7716905-1-BSD LCS LCS LCSD LCSD Limits %RPD RPD Units Analysis Flag Result %Rec Result %Rec Limit Date 0.164 109 0.165 110 70-130 1 25 mg/kg 12.10.202015:25 0.147 98 0.154 103 70-130 5 25 mg/kg 12.10.202015:25 0.0507 101 0.0517 103 70-130 2 25 mg/kg 12.10.202015:25 LCS LCS LCSD LCSD Limits Units Analysis %Rec Flag %Rec Flag Date 108 113 70-130 % 12.10.202015:25 100 107 70-130 % 12.10.202015:25 MS/MSD Percent Recovery [D] = 100*(C-A) / B Relative Percent Difference RPD = 200* I (C-E) / (C+E) LCS/LCSD Recovery [D] = 100 * (C) / [B] Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) Page 23 of 27 LCS = Laboratory Control Sample A = Parent Result C = MS/LCS Result E = MSD/LCSD Result Final 1.000 MS = Matrix Spike B = Spike Added D = MSD/LCSD % Rec tiff etirof ins QC Summary 679115 Environment Testing 1lenco Terraquest Environmental Consultants, P.C. 1238 Union St SE Concord Analytical Method: VPH Seq Number: 3144596 Parent Sample Id: 679969-001 Parameter Parent Spike Result Amount C5-C8 Aliphatic <1.39 27.9 C9-C12 Aliphatic <2.48 27.9 C9-C10 Aromatic 2.81 9.29 Surrogate 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) Prep Method: SW5035A Matrix: Solid Date Prep: 12.10.2020 MS Sample Id: 679969-001 S MSD Sample Id: 679969-001 SD MS MS MSD MSD Limits %RPD RPD Units Analysis Flag Result %Rec Result %Rec Limit Date 44.8 161 44.6 160 70-130 0 25 mg/kg 12.10.202016:50 X 38.0 136 39.5 142 70-130 4 25 mg/kg 12.10.202016:50 X 11.6 95 11.9 98 70-130 3 25 mg/kg 12.10.202016:50 MS MS MSD MSD Limits Units Analysis %Rec Flag %Ree Flag Date 107 122 70-130 % 12.10.202016:50 101 117 70-130 % 12.10.202016:50 MS/MSD Percent Recovery [D] = 100*(C-A) / B Relative Percent Difference RPD = 200* I (C-E) / (C+E) LCS/LCSD Recovery [D] = 100 * (C) / [B] Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) Page 24 of 27 LCS = Laboratory Control Sample A = Parent Result C = MS/LCS Result E = MSD/LCSD Result Final 1.000 MS = Matrix Spike B = Spike Added D = MSD/LCSD % Rec 0 0 Z o � n N � � m nx a o _. m 0. ai 3 ° � n T w 3 [1-D CDo oo v_ u y o ea 7 3 3 .q a K w ` W m N a (n � m CD ^ ° G Fr T O w n T1 D � m D OII Q 6 C E5 s y rn c o o p3 v g M v M W CO (D CD CL N uQ x C) 3 II n CL w z v a ¢ m C) n 6 O o _�T n O FL a C m to ^ m m 0 3 La m — S m O a a a m o' A y fl n CQ � n g 0 o 3 % Z ¢ v A � A U a C r v� a D a, n -13 -0 n o 1 U' m M 3 /� '- N r 2 v n a c N c N o W a 0 M V o 0 y v NCL a w 0 o W t7 M O 41 m ^ a N tV M C 3 1 ,�„ CD cID UN sv '1 —i m _ m d i w m .. .. n �y o rn 3 ^ W fD CD fD 4 CO Z � � N W 1 n m O O W t O, O C IU 7 a v a' C) 1 � a o b co cCL o t � ® a 3 411 -0 E o ;a ; N � ¢1 C 7 m O QJ �( ID W O 0 JID Q �, n T 9l N E C Z Number of Containers g m N y ro a z n to M C III cn (D_ O Z- o N D? m m CD c0 O CDr C CD M ro O v 'tO � in 0 -D L g n' LET 0 a ? Cn C -* p N Z 2 2 2 Z � W n N z O D O r Cn O� CuEl Q fD 3 a Z < <D + vs r N z cn 0EF v'Yi <D m CD m 0 _m o D c 6 p n N '0 < O CD o C C r� 3 CD y C X C"! O 0 Page 25 of 27 Final 1.000 N � 497 QD 0 M IIV OD 0 rn � X [] c C Cf) rn EC O Z m e .29112A01E9Hue ZZ )C � o �2 �rrI�ZJ > "g00Pz on m - O m- nAa TI ~ " - CO) o -n o Ci? n _ O r a c> 0 X = m wx oT 3- CO ;Cl m m00 �� --I z -4 y00 o =250 �o y O L 4 r C rn 4 N O 56&J3fC6P&FE4A 1. Select the 'Print' button to print 1 copy of each label. 2. The Return Shipment instructions, which provide your recipient with information on the returns process, will be printed with the label(s). 3. After printing, select your next step by clicking one of the displayed buttons. Note:To review or print individual labels, select the Label button under each label image above. Use of this system constitutes your agreement to the service conditions in the current FedEx Service Guide, available on fedex.com.FedEx will not be responsible for any claim in excess of $100 per package, whether the result of loss, damage, delay, non-delivery,misdelivery,or misinformation, unless you declare a higher value, pay an additional charge, document your actual loss and file a timely claim.Limitations found in the current FedEx Service Guide apply. Your right to recover from FedEx for any loss, including intrinsic value of the package, loss of sales, income interest, profit, attorney's fees, costs, and other forms of damage whether direct, incidental,consequential, or special is limited to the greater of $100 or the authorized declared value. Recovery cannot exceed actual documented loss -Maximum for items of extraordinary value is $500, e.g. jewelry, precious metals, negotiable instruments and other items listed in our ServiceGuide. Written claims must be filed within strict time limits, see current FedEx Service Guide. l 5 7 Page 26 of 27 Final 1.000 Eurofins Xenco, LLC Prelogin/Nonconformance Report- Sample Log -In Client: Terraquest Environmental Consultants, F Acceptable Temperature Range: 0 - 6 degC Date/ Time Received: 11.25.2020 09.30.00 AM Air and Metal samples Acceptable Range: Ambient Work Order #: 679115 Temperature Measuring device used: HOU-188 Sample Receipt Checklist Comments #1 *Temperature of cooler(s)? 3.3 #2 *Shipping container in good condition? Yes #3 *Samples received on ice? Yes #4 *Custody Seals intact on shipping container/ cooler? N/A #5 Custody Seals intact on sample bottles? N/A #6*Custody Seals Signed and dated? N/A #7 *Chain of Custody present? Yes #8 Any missing/extra samples? No #9 Chain of Custody signed when relinquished/ received? Yes #10 Chain of Custody agrees with sample labels/matrix? Yes #11 Container label(s) legible and intact? Yes #12 Samples in proper container/ bottle? Yes #13 Samples properly preserved? Yes #14 Sample container(s) intact? Yes #15 Sufficient sample amount for indicated test(s)? Yes #16 All samples received within hold time? Yes #17 Subcontract of sample(s)? No #18 Water VOC samples have zero headspace? N/A * Must be completed for after-hours delivery of samples prior to placing in the refrigerator Analyst: TOL PH Device/Lot#: Checklist completed by: Lw�� Date: 11.25.2020 Lisandra Torres Checklist reviewed by: �f d .Q� b� Date: 11.29.2020 Chad Bechtold Page 27 of 27 Final 1.000 APPENDIX C NON=HAZARDOUS WASTE MANIFEST Please print or type (Form designed for use on elite (12 pitch) typewriter) W H Q O 0 X a N a x z O z qEOYC�D NON —HAZARDOUS 1. Generator's US EPA ID No. WASTE MANIFEST Manifest Document No. 2. Page of 3. Ganeta[gr'a Name and �Ilinp Address ,r N G JE (�JT(Vl J 4. Generator's Phone ) 5. Transporter 1 Comp try Name 6. US EPA ID Number A. State Transporters ID B. Transported Phone 7. Transporter 2 Company Name 8. US EPA ID Number C. Stale Transporter's ID D. Transporter 2 Phone 9. Des[ noted Facility Name Site Address �W I;bAlss (� 10, US EPA ID Number {••- 1� SR s lreLI y '" Se E. State Facility's ID F. Facility's Phone 11. WASTE DESCRIPTION Containers 13. 14. Total Unit No, Type Quantity Wt.IVoIa. 102 -6 50 ..Zi/f G b E N E R e A T O R d. G. Additional Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above 15. Special Handling Instructions and Additional Intom atlon 16. GENERATOR'S r rcondition for transporrttThe materials N I hereby describedat the ani manifest arehnot subject to fadement are full and on thiscontents I ho ra dous wastedescribed reg lations.n all respects Date Printed free Name Ill (^rk� ^Cl �t Si t r— Month �I Day 1 Year AO T 17. Transporter 1 Acknowledgement of Receipt of Materials Date R A P Printed/typed Name Signature Month ` Dpay Vear O 18. Transporter 2 Acknowledgement of Receipt of Materials Date R T E PrintedTyped Name Signature Month Day Year R F 19. Discrepancy Indication Space A C L20. Facility Owner or Operator: Certification of receipt of the waste materials covered by this manifest, except as noted In item 19. Data T Printed Typed Na Signature nth Day ,rear YON ✓\ CF14 ©2002 LABELMASTER® (800)621-6808 www.labelmaster.com� PHII PRINGIED U.zi.G,o.a�,.in..q L swixa"N�"a"I NON -HAZARDOUS WASTE MANIFEST Please print or type (Form designed for use on elite (12 pitch) typewriter) W H in a 0 a i Z 0 Z NON -HAZARDOUS 1. Generators US EPA ID No. Manifest 2. Page t WASTE MANIFEST Document No. of 3. Gen atoNrandfa&neasXJU�N .foi' y& CONCOri� all 4. Generators Phone ( ) 5. Transpoder 1Qnnistany Name 6, US EPA ID Number A. State Transporter's 10 GGCB Transporter 1 Phone ]. Transporter 2 Company Name 8. US EPA ID Number C. State Transporter's 10 D, Transporter 2 Phone 9. Designated Facility Name and Site Address 10. US EPA ID Number E. State Facility's ID F. Facility's Phone 11. WASTE DESCRIPTION Containers 13. 14. IN Total Unit No. Type Quantity WLNol. G b. E N E R o A T O R d. G. Additional Descriptions for Materiels Listed Above H. Handling Codes for Wastes Listed Above 15. Special Handling Instructions and Additional Information 16. GENERATOR'S CERTIFICATION: I heron certify that the contents of this shipment are fully and accurately described and are In all respects in proper condition for transport. The mate role described on this manifest are not subject to federal hazardous waste regulations. Date Printe llryped Name Li✓k Signature Month Day Year /yfecN�L F, z // /0? 1240 T 17. Transporter i Acknowledgement of Receipt of Materials Date R A Printed/Typed Name Signature Month Day Year N 5 P O 1S. Transporter 2 Acknowledgement of Receipt of Materials Date R T PrintedlTyped Name Signature Month Day Year E R 19. Discrepancy Indication Space F A C 1 20. Facility Owner or Operator. Certification of receipt of the waste materials covered by this manifest, except as noted in item 19. j Date T Printedi Signal M nN� ar Y Pi; Jy CF14 02002 LABELMASTER® (800) 621-5806 www.labelmaster.corty ® ", umxoeoreEnx 6q'�NN Alternative Energy Solutions of NC, 1,1,(' Post office Box 310 Sanford, NC 27331 Phone#: 336-3024889 Fax #: 704-973-9573 Y Y A%A nt: • AES 3841 ('nnningham Road Thomasville, NC 27360 ription: i / _ a '* 26; NORTH CAROLINA PUBLIC WEIG14MASTER LICENSE E I S JUNE 30, 2020 JOHN GODF E 42673 INVALI SS SIGNED WAS'hE MANIFEST Phony. Ph Origination: (: r)ss Weight: — fare Weight: '—— a Vet Weight: Ll <oee'nerafor°s ('ertification: I ceu-ti fy that lne materials described above mt this unanfifest arc na:t subject to federal regnlatimts fm• reporting propeu' disposal of HAZARDOUS WASTE.. Genei ator /Agent Signature Title Ack:mwledgmeot of Receipt of Material: Date Drivers Si imtt:re I7euc Noted Discrepancies: Inspected &Accepted (except as oted •hove By: Earthtec Environmental, Inc) Accel,tteaY By: Date _//92D 4LL� NON=HAZARDOUS WASTE MANIFEST 2G 9 W H a N D 0 C Q N a x z 0 Z Pleaec}imrtOrlype (Form designed for use on elite (12 pitch) typewriter) NON'HAZARDOUS 1. Generator's US EPA 10 No. Manifest 2. Page 1 WASTE MANIFEST Document No. or 3. Generator's Na to Ming Ad re s M �Fa OaZ 01to v if So�fr4 Co,i.�or� rvc 4. Generator's Phone ( ) 5. Transporter 1 Company Name 6. US EPA ID Number A. State Transporters ID B. Transporter 1 Phone T. Transporter 2 Company Name 8, US EPA ID Number C. State Transporter's ID D. Transporter Phone 9. Dp5ign6{ytl Fd ility Name and Site Address:' HtS 10, US EPA ID Number E. State. Facility's ID F. Facility's Phone 38 �t i c�nn�Atin 11. WASTE DESCRIPTION Containers 13, 14. Total Unit No. Type Quantity WtNol. a fle ru cvn't CAN Itc 2CJ;1 DiT d, E NORSWFIGHt'IO effo Z JUKE 1 1S N PUBLIC IR q2 R ✓ LIC F LJ� JOE SIGNED r1l)0 T LESS 0 G. Additional Descriptions for Materials Listed Above H. Handling Codes for Wastes Usted Above 15. Special Handling Indications and Additional Information 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fully and accurately described and are in all respects In proper condition for transport. The materials described on this manifest are not subject to federal hazardous waste regulations. Date Printedrfyped Name Ski%nature, Month Day Year T iT. Transporter 1 Acknowledgement of Receipt of Materials Date R A Printed/Typed Name Sign Monte Month Day Year P� ZGl O IF Transpoder2Acknowledgementof Receiptof Materials Dale T Printed/fyped Name Signature Month Day Year E I R F 19. Discrepancy Indication Space A C L20. Facility Owner or Operator: Certification of receipt of the waste materials covered by this manifest, except as noted in item 19. 1 Dare T Y PrintecirTyped Name Sign�b J J1e r n p'nth Day - Year L CF14 ®2002 LABELN(ASTFA® (800)621-5806 www.labelmaster.com (D USING US,xosareaxINK 'SINK APPENDIX D UST-61 I 24-Hour Release and UST Leak Reporting Form. For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release (DWMUSEONLY) Suspected Contamination? (Y/N) N Facility ID Number NA Incident# Risk(H,I,L,U) Confirmed GW Contamination? (Y/N) N Date Leak Discovered 11/20/20 Received On Received By Confirmed Soil Contamination ?(Y/N) Y Comm/Non-Commercial? Non -Comm Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) Y Reg/Non-regulated? Non -regulated Region Free Product? (Y/N) N If Yes, State Greatest Thickness INCIDENT DESCRIPTION Incident Name: Barbara Linker el al Property Address: 1238 Union St. S County: Cabarrus Regional Office (circle one): Ash ville, Mooresville ayetteville, City/Town: Concord Zip Code: 28025 Raleigh, Washington, Wilmington, Wins o - a em Latitude (decimal degrees): 35.378049 Longitude (decimal degrees) :--80.551330 Obtained by: ❑ GPS Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors) OTopographic During the removal of a 550-gallon heating oil UST, stained soils exhibiting a heating oil were noted in the map ❑? vicinity of holes noted in the UST along its sides and seams. The UST was hauled offsite for disposal. GIS Address matching 7 • ther ❑? Unknown Describe location: Approximately 32.65 tons of contaminated oil were excavated from the UST basin and hauled offsite for disposal. No free product was noted in the UST basin. Google Earth HOW RELEASE WAS DISCOVERED (Release code) (Check one) ORelease Detection Equipment or Methods IZVisual/Odor OGroundwater Contamination *uring UST Closure/Removal OWater in Tank IdSurface Water Contamination IdProperty Transfer OWater Supply Well Contamination MOther (specify) SOURCE OF CONTAMINATION Source of Release Cause of Release Type of Release Product Type Released (Check primary source) (Check primary cause) (Check one) (Check primary product type released) -Tank oSpill -Petroleum❑? Gasoline/ Diesel/ M Diesel/Veg.Oil M Piping Overfill Non -Petroleum Kerosene Blend seating Oil M Vegetable Oil 100% Dispenser � Corrosion � Both Other Petroleum � E10 — E20 M Submersible Turbine Pump 0 Physical/Mechanical Location Products Damage ME21 — E84 M Delivery Problem (Check one) Metals Metals IN Install Problem DE85 — E99 M Spill Bucket �❑? Other Inorganics � N Facility ❑� Other Other Ethanol 100% \hUnknown - esidence Other Organics IZ E01 — E09 Unknown❑? Other Definitions presented on reverse Ownership 1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural Residentia 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining UST Form 61 (02/19) Page 1 of 2 IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3. UST SYSTEM OWNER UST Owner/Company Barbara Linker et al Property Point of Contact Address Michael Linker 100 Krimminger Ave. SE City State Zip Code Telephone Number Concord NC 28025 UST SYSTEM OPERATOR UST Operator/Company Address same as UST System Owner City State Zip Code Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address same as UST System Owner City State Zip Code Telephone Number Draw Sketch of Area (showing two major road intersections) or Attach Map See attached Map Person Reporting Incident: Jonathan Grubbs Company: Terraquest Environmental Consultants, P.C. Telephone Number: 919-563-9091 Title: Vice President Address: 100 E. Ruffin St., Mebane, NC 27302 Date: 11/20/2020 UST Form 61 (02/19) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) histallation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined � A o vQ EP D NSF y� x "o� p4 o o l�D v O TWINFIELD 0o e < NNE SF RO t �Sr< OLD AIRPORT O['D.FARM ✓oG9ti OJ�O ' _ \ � SE 3 �Q SETTER LN`SE �j, J� �S� Q p Q � b � / O n b �P�QQ• 601 PQ\�� Q 1 `� cUM BERLAND CT 5 r r �7 O ARRO{yNEAD 0�^� z 650 z - A ^� ' ER AVE-SE 6 ^� o c - 1 _ J / 49 y/ A 0 WOODLAND DR SW /I 0 0 O 0 G<650 FN� 49 AQ 600 hh cpo MORNING DEW DR 0 O Crf rl 0 Z cy yBERRY_LN o� lrl s o CN RD E 601 o h .ENO cc C3 �� Po 1\/ NTRY HO fNSGP��o V - CQOUSE DR _ o �^ bye �p0 (�'n0 o p b c MAP SOURCE: USGS 7.5 MINUTE TOPOGRAPHIC MAP OF CONCORD & CONCORD SE, NC GRAPHIC SCALE 0' 2,000' 4,000' n nam J SITE LOCATION MAP BARBARA LINKER ET AL I ®" - -���� 1238 CONCORD, CABARRUS BARBARA LINKER ET AL UN ON ST SE COUNTY, NC CONCORD, NC PROJECT NO. 16820 DRAWN BY: JRG DATE: 11 20 20 ENVIRONMENTAL CONSULTANTS, P.C. SCALE: 1" = 2,000' CHECKED BY: MJB FIGURE NO. 1 Beverly, Trudy From: jrgrubbs@terraquestpc.com Sent: Thursday, January 21, 2021 2:25 PM To: Beverly, Trudy Subject: RE: [External] 1238 Union St S Concord NC Heating Oil UST Release CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. No we did not, but we removed all the soil contamination up to bedrock. We collected one soil sample (BE1) of the soil immediately above the bedrock to document that the contamination extended to bedrock and then removed the impacted soil. Thanks! Jonathan R. Grubbs, P.G. TerraQuest Environmental Consultants, P.C. 100 East Ruffin Street Mebane, NC 27302 (P) 919-563-9091 (F) 919-563-9095 (C) 919-906-0707 jrgrubbs@terraquestpc.com From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Thursday, January 21, 2021 2:18 PM To: jrgrubbs@terraquestpc.com Subject: RE: [External] 1238 Union St S Concord NC Heating Oil UST Release Hey Jonathan, You encountered rock during excavation. Did you sample groundwater? Trudy Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality �E W Ue47r Imen � �. UST Section, Mooresville Regional Office 704.235.2182 (Office) 161 Trudy. B everlykncdenr. gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-proeram INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httDs:Hdeu.ne. aov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaaement-eis-mans File Review Procedures: https:Hdcq.nc. gov/about/divisions/waste-manaaement/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): httns://deo.nc. aov/about/divisions/waste-manaeement/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https:Hfiles.nc.gov/ncdeg[Waste%20Manatiement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.pdf https:Hfiles.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%20filc%20names%20for%2OLaserfiche.docx From: jr rubbs@terraquestpc.com[mailto:Irgrubbs@terraquestpc.com] Sent: Thursday, January 21, 2021 1:33 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: [External] 1238 Union St S Concord NC Heating Oil UST Release CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Hey Trudy! We supervised the removal and subsequent soil excavation for a residential non-commercial heating oil UST at 1238 Union St S in Concord NC. The UST-61 is included in the report. We excavated contaminated soil to achieve a clean closure. We have clean sidewall samples and removed all of the soil up to 7 feet BGL where we encountered bedrock. Could you please review the attached Initial Abatement Action Report and let me know if you have any questions! Thanks! Jonathan R. Grubbs, P.G. TerraQuest Environmental Consultants, P.C. 100 East Ruffin Street Mebane, NC 27302 (P) 919-563-9091 (F) 919-563-9095 (C) 919-906-0707 jrgrubbs@terraguestpc.com Beverly, Trudy From: Beverly, Trudy Sent: Monday, May 10, 2021 7:10 AM To: Jonathan Grubbs Subject: RE: [External] 1238 Union St S Concord NC Heating Oil UST Release Good Morning Jonathan, We spoke by phone on April 14th about this site. You were going to get a groundwater sample from the well on the parcel. Do you have that data for review? Thanks, Trudy Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management _ North Carolina Department of Environmental Quality EQ�� NR,vN7en[al �� �UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy.Beverlykncdenr. gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: hops://deq.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: hgps://deg.nc.gov/about/divisions/waste-management/ust/ast-prosram INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans File Review Procedures: https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): hi�2s://deg.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https://files.nc.aov/ncdep/Waste%2OManaeement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.adf htips://files.nc.,gov/ncdegiWaste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Jonathan Grubbs [mailto:jrgrubbs@terraquestpc.com] Sent: Friday, April 30, 2021 8:08 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: Re: [External] 1238 Union St S Concord NC Heating Oil UST Release CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Good morning Trudy! Any progress on the review of UST closure report for the 1238 Union St S Concord NC Heating Oil UST Release? Thanks! Jonathan R. Grubbs, P.G. TerraQuest Environmental Consultants, P.C. 100 East Ruffin Street Mebane, NC 27302 (P) 919-563-9091 (F) 919-563-9095 (C) 919-906-0707 %rgrubbs@terraguestpc.com On Apr 14, 2021, at 11:51 AM, Jonathan Grubbs <jrgrubbs@terraguestpc.com> wrote: Thanks Trudy Jonathan R. Grubbs, P.G. TerraQuest Environmental Consultants, P.C. 100 East Ruffin Street Mebane, NC 27302 (P) 919-563-9091 (F) 919-563-9095 (C) 919-906-0707 0rgrubbs@terraguestpc.com On Apr 14, 2021, at 11:04 AM, Beverly, Trudy <trudy.beverly@ncdenr.gov> wrote: Hey Jonathan, I'll try to get that done today and get back with you. Trudy <image001.jpg> Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy.Beverlykncdenn -gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: htl2s://deg.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: ht!ps:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-proeram INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans File Review Procedures: https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): hitps://deg.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: httos:Hfiles.nc.aov/nedea/Waste%2OMana¢ement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policy.odf https:Hfiles.nc.gov/ncdeq/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Jonathan Grubbs[mailto:irgrubbs@terraguestpc.com] Sent: Wednesday, April 14, 2021 10:59 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: Re: [External] 1238 Union St S Concord NC Heating Oil UST Release CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Good morning! Just checking in to see if you had had a chance to review that site check for 1238 Union St. S. Concord, NC. Thanks! Jonathan R. Grubbs, P.G. TerraQuest Environmental Consultants, P.C. 100 East Ruffin Street Mebane, NC 27302 (P) 919-563-9091 (F) 919-563-9095 (C) 919-906-0707 0rgrubbs@terraquestpc.com On Apr 13, 2021, at 3:05 PM, jrgrubbs@terraquestpc.com wrote: Hey Trudy! Hope you are well! Have you had a chance to make a determination on this site - 1238 Union St S Concord NC? The property owners are putting the property up for sale and want to know if it can be closed out or additional investigation is required. Thanks! Jonathan R. Grubbs, P.G. TerraQuest Environmental Consultants, P.C. 100 East Ruffin Street Mebane, NC 27302 (P) 919-563-9091 (F) 919-563-9095 (C) 919-906-0707 jrgrubbs@terraquestpc.com From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Thursday, January 21, 2021 2:18 PM To: jrgrubbs@terraquestpc.com Subject: RE: [External] 1238 Union St S Concord NC Heating Oil UST Release Hey Jonathan, You encountered rock during excavation. Did you sample groundwater? Trudy 9 <image001.jpg> Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy.Beverly(a ncdenr.gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: hops://deq.nc.gov/about/divisions/waste-manaaement/ust Branch's Above Ground Storage Tanks Website Address: hops://deg.nc.gov/about/divisions/waste-management/ust/ast-proeram INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httns://deo.nc. eov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaeement-eis-maps File Review Procedures: https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): hitps://deq.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: httys:Hfiles.nc.¢ov/ncdeci[W aste%2OMana2ement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policy.pdf https:Hfiles.nc. gov/ncdeq/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: jrrubbs@terraquestpc.com[mailto:Irgrubbs@terraquestpc.com] Sent: Thursday, January 21, 2021 1:33 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: [External] 1238 Union St S Concord NC Heating Oil UST Release CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Hey Trudy! We supervised the removal and subsequent soil excavation for a residential non-commercial heating oil UST at 1238 Union St S in Concord NC. The UST-61 is included in the report. We excavated contaminated soil to achieve a clean closure. We have clean sidewall samples and removed all of the soil up to 7 feet BGL where we encountered bedrock. Could you please review the attached Initial Abatement Action Report and let me know if you have any questions! Thanks! Jonathan R. Grubbs, P.G. TerraQuest Environmental Consultants, P.C. 100 East Ruffin Street Mebane, NC 27302 (P) 919-563-9091 (F) 919-563-9095 (C) 919-906-0707 irgrubbs@terraquestpc.com