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HomeMy WebLinkAboutMO-28442_47696_CA_IAR_20210115_Initial Abatement Action ReportTERRAut
ENVIRONMENTAL CONSULTANTS, P.C.
INITIAL ABATEMENT ACTION REPORT
Details the November 2020 UST Closure and Soil Excavation
BARBARA LINKER ET AL PROPERTY
1238 UNION ST. S
CONCORD, NC 27217
Latitude: 35.378049' N Longitude:-80.551330' W
Release Information
Date Discovered: November 20, 2020 (Lab Confirmed)
Estimated Release Quantity: Unknown
Release Cause/Source: Non-commercial UST System
Registered UST Capacities: (1) 550-gallon heating oil
Facility ID: Not Applicable
NCDWM-UST Incident No.: Pending
NCDWM-UST Risk Ranking: Pending
Responsible Party & Property Owner
Barbara Linker
100 Krimminger Ave. SE
Concord, NC 28025
Terraquest Project No. 16820
January 15, 2021
100 East Ruffin Street • Mebane, North Carolina 27302
Telephone (919) 563-9091 - Facsimile (919) 563-9095
www.terraquestpc.com
CERTIFICATION FOR THE SUBMITTAL
OF AN ENVIRONMENTAL / GEOLOGICAL ASSESSMENT
Attached is the Initial Abatement Action Report for:
Responsible Party: Barbara Linker et al
Address: 100 Kimminger Ave. SE
City: Concord State: NC Zip Code: 28025
Site Name: Barbara Linker et al Property
Address: 1238 Union St. S
City: Concord State: NC Zip Code: 28025
I, Jonathan R. Grubbs, a Licensed Geologist in the State of North Carolina for TERRAQUEST
ENVIRONMENTAL CONSULTANTS, P.C. do hereby certify that I am familiar with and have
reviewed all material including figures within this report and that to the best of my knowledge
the data, site assessment, figures, and other associated materials are correct and accurate. All
work was performed under my direct supervision. My seal and signature are affixed below.
Terraquest Environmental Consultants, P.C. is licensed to practice geology and engineering in
North Carolina. The geology certification number of the corporation is C-291. The engineering
certification number of the corporation is C-4634. Engineering is practiced out of the Cary, NC
office.
TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C.
, 2-:> -4-
Ryan D. Kerins
Project Manager
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Jonathan R. Grubbs, P.G.
Vice President
Initial Abatement Action Report
Prepared by: Terraquest Environmental Consultants, P.C.
Prepared on: January 15, 2021 i
Barbara Linker et al Property
1238 Union St. S
Concord, Cabarrus County, NC
TABLE OF CONTENTS
1.0
INTRODUCTION................................................................................................................... 1
2.0
UST REMOVAL & RELEASE DISCOVERY............................................................................... 1
3.0
REMEDIAL EXCAVATION..................................................................................................... 2
4.0
GROUNDWATER INVESTIGATION....................................................................................... 3
5.0
FREE PRODUCT CHECK........................................................................................................ 3
6.0
POTENTIAL SOURCES OF PETROLEUM HYDROCARBONS................................................... 4
7.0
NATURE AND ESTIMATED QUANTITY OF RELEASE............................................................. 4
8.0
SITE AND VICINITY DESCRIPTION........................................................................................ 4
9.0
CONCLUSIONS/RECOMENDATIONS....................................................................................5
10.0
LIMITATIONS.......................................................................................................................5
REFERENCES.................................................................................................................................... 7
TABLES:
1. Summary of Soil Sampling Results
FIGURES:
1. Site Location Map
2. Site Layout and Closure Soil Sample Map
APPENDICES:
A. Environmental Acronyms and Technical Methods / Standard Procedures
B. Analytical Report
C. Residual Liquid, UST Disposal, and Soil Disposal Manifests
D. UST-61 24-Hour Release and UST Leak Reporting Form
Initial Abatement Action Report Barbara Linker et al Property
Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S
Prepared on: January 15, 2021 ii Concord, Cabarrus County, NC
1.0 INTRODUCTION
On behalf of the responsible party, Barbara Linker et al, Terraquest Environmental Consultants,
P.C. has prepared this Initial Abatement Action Report for the Barbara Linker et al property
located at 1238 Union St. S in Concord, Cabarrus County, North Carolina. This report documents
the closure of a 550-gallon heating oil UST and subsequent excavation of contaminated soil in
November 2020.
The site's location and layout are depicted in Figures 1 and 2. Environmental acronyms used in
this report are detailed in Appendix A along with Terraquest's technical methods and standard
procedures.
2.0 UST REMOVAL & RELEASE DISCOVERY
The UST was installed off the southwest side of the residence during its construction in 1965 and
was replaced with an aboveground storage tank (AST) in the 1990's. On November 18, 2020 prior
to excavating the tank, Terraquest supervised the removal of 425 gallons of residual liquid
composed mostly of water from the UST by CCI of Salisbury, NC. The 550-gallon heating oil tank
was buried approximately 20 inches below ground level (BGL) and was excavated and taken
offsite for environmentally -sound disposal by CCI on November 18, 2020. The dimensions of the
UST were 46 inches wide by 74 inches long. The tank's former location is shown on Figure 2.
Following UST removal, Terraquest inspected the UST and noted holes up to 1.4-inch in size along
the sides and seams. Terraquest collected a soil sample CS1 from beneath the UST at a depth of
5.5 feet BGL. The soil sample was screened using a photoionization detector (PID) and revealed
the presence of heating -oil type contaminants with a detected measurement of 397.1 parts per
million (ppm). This screening measurement coupled with the stained soil and noted holes in the
UST indicated a release of heating oil had occurred from the UST. The CS1 soil sample collected
for analysis was placed in the proper laboratory -prepared sampling containers, labeled with the
Initial Abatement Action Report Barbara Linker et al Property
Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S
Prepared on: January 15, 2021 1 Concord, Cabarrus County, NC
project name, project number, sample identification, required analysis, and date and time of
collection. The sample was immediately placed on ice and analyzed before the expiration of an
analytical method's prescribed holding time. Chain -of -custody documentation was maintained
for the soil sample prior to an analysis using a UVF Trilogy unit for TPH Diesel -Range Organics
(DRO) and Gasoline -Range Organics (GRO). Analytical results of the CS1 soil sample revealed
contaminant concentrations above the North Carolina Department of Environmental Quality
Division of Waste Management UST Section (NCDEQ DWM-UST) Actions Limits for both the TPH
GRO and DRO methods. Table 1 summarizes the sample depth and detected concentrations of
the CS1 soil sample. The locations of the soil sample is identified in Figure 2. The complete
analytical report is included in Appendix B.
3.0 REMEDIAL EXCAVATION
With the PID screening measurement, stained soil, and noted holes, Michael Linker, a
representative of the property owner, directed Terraquest to supervise the excavation of
contaminated soil beneath and surrounding the former heating oil UST. The impacted soil was
excavated using a mini excavator to a depth of seven feet BGL where bedrock was encountered.
All of the contaminated soil above the bedrock and from the sidewalls was removed. Soil samples
SW1 through SW4 were collected at the sidewall limits and sample BE1 was collected at the base
of the excavation from soils immediately above the bedrock prior to their removal. The SW1
through SW4 and BE1 soil samples collected for analysis were placed in the proper laboratory -
prepared sampling containers, labeled with the project name, project number, sample
identification, required analysis, and date and time of collection. The samples were immediately
placed on ice and analyzed before the expiration of an analytical method's prescribed holding
time. Chain -of -custody documentation was maintained for the soil samples. The SW1 through
SW4 soil samples were analyzed using a UVF Trilogy unit for TPH DRO and GRO. The BE1 soil
sample was submitted to a NC -certified laboratory for analysis per EPA Method 8260 + MTBE +
IPE (volatile organics), EPA Method 8270 Base Neutral and Acid Extractable (semi -volatile
Initial Abatement Action Report
Prepared by: Terraquest Environmental Consultants, P.C.
Prepared on: January 15, 2021 2
Barbara Linker et al Property
1238 Union St. S
Concord, Cabarrus County, NC
organics), Massachusetts Department of Environmental Protection (MADEP) methods for volatile
petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH).
The four sidewall samples SW1 through SW4 results were either below the NCDEQ DWM-UST
Actions Limits or the laboratory's sample method detection limits. The BE1 base of excavation
sample was above the TPH Action Limits and had detected concentrations above the Soil -to -
Groundwater Maximum Soil Contaminant Concentrations (S-t-G MSCCs) and Residential MSCCs.
Soil contamination was excavated down to the bedrock surface and all of the excavatable
contaminated soil was removed in the base and sidewalls of the former UST basin. The limits of
the final excavation measured nine feet wide by sixteen feet long. Table 1 summarizes the
sample depth, PID measurements, and detected concentrations of the soil samples. The
locations of the soil samples are identified in Figure 2. The complete analytical reports are
included in Appendix B.
Fill dirt obtained from Keller Dirt and Gravel of Kannapolis, NC was used to backfill the excavation.
Two loads of contaminated soil totaling 32.65 tons were removed and taken offsite for disposal
at Alternative Energy Solutions of NC, LLC in Thomasville, NC. The weight -certified soil disposal
manifests are provided in Appendix C.
4.0 GROUNDWATER INVESTIGATION
Groundwater was not encountered or investigated as part of this phase of field work.
5.0 FREE PRODUCT CHECK
Free product was not encountered during site activities.
Initial Abatement Action Report Barbara Linker et al Property
Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S
Prepared on: January 15, 2021 3 Concord, Cabarrus County, NC
6.0 POTENTIAL SOURCES OF PETROLEUM HYDROCARBONS
The primary source of petroleum hydrocarbons for this release incident was the former heating
oil UST. A heating oil AST was noted immediately adjacent to the former heating oil UST and is
currently supplying the residence's furnace. An inspection of the AST and surrounding surface
soils do not indicate that a release incident from the AST has occurred and is contributing to the
UST release.
7.0 NATURE AND ESTIMATED QUANTITY OF RELEASE
The nature of the release is petroleum as heating oil from the former non-commercial UST. The
amount of the release is unknown. A UST-61 24-Hour Release and UST Leak Reporting Form is
provided in Appendix D.
8.0 SITE AND VICINITY DESCRIPTION
The site is located in a residential and commercial area located south of Concord, NC. The subject
and surrounding properties to the north, east, and west have a residential zoning classification.
The surrounding properties to the south have a commercial zoning classification. The New Grace
Baptist Church is located approximately 1,100 feet to the northwest. The site and the
surrounding properties derive their drinking water from the City of Concord municipal water
supply system. The subject property residence is connected to a septic system located south of
the residence. A water supply well that formerly supplied the subject property residence was
noted within 30 feet of the former UST location. The well is currently not in use, but not
abandoned. No additional water supply wells were noted within a 150-foot radius from the
former UST location. The location of the water supply well is depicted in Figure 2.
According to the Geologic Map of North Carolina, the site lies in the Charlotte Belt of the
Piedmont Physiographic Province (Brown, et al., 1985) and has been mapped as having a
Initial Abatement Action Report Barbara Linker et al Property
Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S
Prepared on: January 15, 2021 4 Concord, Cabarrus County, NC
metamorphosed quartz diorite bedrock lithology. On a regional scale, the Piedmont is
characterized by gently rolling, well rounded hills and long low ridges with a few hundred feet of
elevation difference between the hills and valleys. The closest surface water body features are
intermittent streams located approximately 1,200 feet to the northeast and approximately 1,400
feet to the west. The eastern stream feeds into Cold Water Creek located approximately 4,450
feet to the east and into Irish Buffalo Creek located approximately 4,900 feet to the west. Surface
water features are displayed with topography on Figure 1.
9.0 CONCLUSIONS/RECOMENDATIONS
Terraquest personnel supervised the removal of one heating oil UST in November 2020 at the
Barbara Linker et al property located at 1238 Union St. S in Concord, NC. Initial abatement
activities included the removal of that tank and the excavation and offsite disposal of 32.65 tons
of contaminated soil. Excavation was conducted to the limits possible given the presence of the
onsite structures and features horizontally and bedrock vertically.
Given the removal of the UST, the removal of the excavatable contaminated soil, the non-
commercial status of the UST, and the presence of municipal water, the release incident is a
"LOW" risk eligible for a "No Further Action" Letter and closure of the release incident.
10.0 LIMITATIONS
This report is limited to the investigation of petroleum hydrocarbons in soil and does not imply
that other unforeseen adverse impacts to the environment are not present at or around the
subject facility. In addition, subsurface heterogeneities not identified during the current study
may influence the migration of groundwater or contaminants in unpredicted ways. The limited
amount of sampling and testing conducted during this study cannot practically reveal all
subsurface heterogeneities. Furthermore, the subsurface conditions, particularly groundwater
flow elevations, and water quality may very through time. The opinions and conclusions
Initial Abatement Action Report Barbara Linker et al Property
Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S
Prepared on: January 15, 2021 5 Concord, Cabarrus County, NC
determined in this report are in accordance with industry -accepted geologic and hydrogeologic
practices at this time and location. No warranty is implied or intended.
Initial Abatement Action Report
Prepared by: Terraquest Environmental Consultants, P.C.
Prepared on: January 15, 2021 6
Barbara Linker et al Property
1238 Union St. S
Concord, Cabarrus County, NC
REFERENCES
Brown, et al., 1985. Geologic Map of North Carolina, North Carolina. Department of Natural
Resources and Community Development, 1:500,000 scale.
Initial Abatement Action Report Barbara Linker et al Property
Prepared by: Terraquest Environmental Consultants, P.C. 1238 Union St. S
Prepared on: January 15, 2021 7 Concord, Cabarrus County, NC
TABLES
Table 1 SUMMARY OF SOIL SAMPLING RESULTS
Date: 121420 Incident Name: Barbara Linker etal- 1238 Union St. SE Concord NC Incident No.: P11,i19 Facility IM NA
Analytical Method
a
Contaminant
of Concern
15
Sample ID
CODllected
Sam le Depth
PID
d
-
A
CS1
1111:121
5.5
397.1
5.905
875
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
SWI
I3/I/20
6-7
0
<0.2
2.56
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
SW2
11/18/20
6-7
0
0.24
1.08
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
SW3
I3/IB/20
5-6
3.2
<0.2
2.2
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
SW4
11/18/20
6-7
1.2
0.69
<1
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
BEI
1l/IB/20
7.0
342.1
2,420
736
0.0126
0.279
0.156
0.814
1.45
12.9/<0.333
0.805
3.52
0.39
6.11
1.64
2.1
0.319
0.633
3.09
7.11
1.2
IS
23
<12.5
2,354
414
TPH
Action Limit
100
So
Soil -to -groundwater MSCC
0.0056
4.3
4.9
4.6
0.12
0.16
1.7
4.3
1.7
1.5
1.3
3.3
16
940
47
56
270
0.004
3.6
68
540
8
31
18
1,200
1,560
3,129
300
313
626
626
1.564
782
782
626
9,385
4,600
620
469
469
20
63
939
1,500
31,000
469
Residential Soil Cleanup Level
Industrial/Commercial Soil CIeanu Level
164
32,000
40,000
81,760
1 4000
8,176
16,350
16,350
40,880
20,440
20,"0
16,350
245,280
122,000
16,400
12,264
12,264
100
1.635
24,528
40,000
BI0,000
12,264
Notes:
1. All results in me/U.
2. Bold denotes a compound detection.
3. Shading denotes a Soil-to-aroundwater MSCC violation. Red italics indicates a Residential MSCC violation
4. "<' = less than sample deteRion IimiU Naphthalene Results: 8260/8270
5. Sample depths are in feet below ground level.
6. "MSCC" = Maximum Soil Contaminant Concentration: #- considered immobile: "1" --Ret analYte was identified between reportine limit and method detection limit; W' -value failed to meet OA/QC, estimated value
FIGURES
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MAP SOURCE:
USGS 7.5 MINUTE TOPOGRAPHIC MAP OF CONCORD & CONCORD SE, NC
GRAPHIC SCALE
0' 2,000' 4,000'
n nam
J
SITE LOCATION MAP
BARBARA LINKER ET AL
I
®"
-
-����
1238
CONCORD, CABARRUS
BARBARA LINKER ET AL
UN ON ST SE
COUNTY, NC
CONCORD, NC
PROJECT NO. 16820
DRAWN BY:
JRG
DATE: 11 20 20
ENVIRONMENTAL CONSULTANTS, P.C.
SCALE: 1" = 2,000'
CHECKED BY:
MJB
FIGURE NO. 1
LEGEND
SOIL SAMPLE LOCATION (SAMPLE DEPTH IN FEET BELOW GROUND LEVEL)
SW AND BE SOIL SAMPLES ANALYZED BY EPA 8260, 8270 DNA, & MADEP VPH/EPH.
B1 SOIL SAMPLE ANALYZED BY UVF TRILOGY TPH 3550 (DRO) & 5030 (GRO).
<S-T-G - NO DETECTIONS ABOVE ACTION LIMITS OR S-T-G MSCCS
ALL RESULTS IN MILLIGRAMS PER KILOGRAM (MG/KG).
B: BENZENE 4-I: 4-ISOPROPYLTOLUENE NAPH: NAPHTHALENE 1-M: 1-METHYLNAPHTHALENE
2-M: 2-METHYLNAPHTHLANE C9-C18: C9-C18 ALIPHATICS C9-C22: C9-C22 AROMATICS
ONLY COMPOUNDS DETECTED AT CONCENTRATIONS GREATER THAN THE S-T-G MSCCS LISTED.
RED UNDERLINED CONCENTRATIONS ARE GREATER THAN RESIDENTIAL MSCCS.
SEE TABLE 1 FOR A COMPLETE LISTING OF DETECTED COMPOUNDS.
RESIDENCE
FORMER SW4(6-7
GRASS HEATING 3550: 0.68
OIL UST 5030: <1
SW1 (6-7):
3550: <0.2
SW3(5-6): r _ 5030: 2.56
3550: <0.2
5030: 2.2 1
® 1 LIMITS OF
BE 7.O
L * / EXCAVATION
/3550: 2,420
5030: 736 CS1 (5.5):
B: 0.0126 3550: 51905
4-I: 1.45 5030: 875
NAPH: 12.9 SW2 (6-7):
1 -M: 15 3550: 0.24
2-M: 23 5030: 1.08
C9-Cl8: 2,354
C9-C22: 1,263
GRASS
FENCE
SCALE: 1 "- 211
SITE LAYOUT
& CLOSURE SOIL SAMPLE MAP PROJECT N0. 16820 DATE: 1/15/21
BARBARA LINKER ET AL PROPERTY a — — CHECKED BY: MJB SCALE: VARIES
1298 UNION ST. SE ® ®� ffil
CONCORD, CABARRUS COUNTY, NC ®�®® ■ ®���
BARBARA LINKER ET AL CONCORD, NC I ENVIRONMENTAL CONSULTANTS, P.c. DRAWN BY: JRG FIGURE NO. 2
APPENDIX A
ENVIRONMENTAL ACRONYMS
2L Standard Groundwater Standards in Title 15A NCAC
2L 0.0202(g)
2B Standard
Surface Water Standards under Title 15A
NCAC 2B
AFVR
Aggressive Fluid -Vapor Recovery
AST
Aboveground Storage Tank
BGL
Below Ground Level
BTEX
Benzene, toluene, ethylbenzene, xylenes
C&D
Construction and Demolition
CAP
Corrective Action Plan
CSA
Comprehensive Site Assessment
DPE
Dual -phase Extraction
EPA
Environmental Protection Agency
ePATA
Electronic Pre -Approval Task Authorization
EPH
Extractable Petroleum Hydrocarbons
ESA
Environmental Site Assessment
GCL
Gross Contamination Level
LEL
Lower Explosive Limit
LSA
Limited Site Assessment
IPE
di -Isopropyl Ether
ISCO
In -situ Chemical Oxidation
MADEP
Massachusetts Department of
Environmental Protection
MDL
Method Detection Limit
MNA
Monitored Natural Attenuation
MMPE
Mobile Multi Phase Extraction
MSCC
Maximum Soil Contaminant
Concentration
MSL
Mean Sea Level
MSW
Municipal Solid Waste
MTBE
Methyl tertiary -Butyl Ether
NC
North Carolina
NCAC
NC Administrative Code
NCDENR
NC Department of Environment and
Natural Resources
NCDEQ
NC Department of Environmental
Quality
NCDOT
NC Department of Transportation
NCDWM-SW
NC Division of Waste Management's Solid
Waste Section
NCDWM-UST
NC Division of Waste Management's UST
Section
NCDWQ
NC Division of Water Quality
NORR
Notice of Regulatory Requirements
NORP
Notice of Residual Petroleum
NOV
Notice of Violation
NPDES
National Pollutant Discharge
Elimination System
OVM
Organic Vapor Meter
PID
Photoionization Detector
PLC
Programmable Logic Controller
POE
Point of Entry (water treatment system)
POTW
Publicly Owned Treatment Works
RBCA
Risk Based Corrective Action
RL
Reporting Limit
RP
Responsible Party
SCFM
Standard Cubic Feet per Minute
SVE
Soil Vapor Extraction
STG
Soil to Groundwater
TA
Task Authorization
TCC
Target Cleanup Concentrations
Terraquest
Terraquest Environmental Consultants,
P.C.
TPH
Total Petroleum Hydrocarbon
UST
Underground Storage Tank
VOA
Volatile Organic Analysis
VOC
Volatile Organic Compound
VPH
Volatile Petroleum Hydrocarbons
XP
Explosion Proof
Terraquest Environmental Consultants, P.C.
100 E Ruffin St, Mebane, NC 27302
P (919) 563-9091 F(919) 563-9095
TECHNICAL METHODS/STANDARD PROCEDURES
Equipment Decontamination
All soil sampling equipment utilized during site assessment activities is decontaminated according
to standard and accepted protocol. Cleaning solutions range from clean potable water to acidic
solutions or organic solvents depending on the contaminants present at the site. Equipment
utilized at sites, such as hand augers, contaminated with petroleum hydrocarbons, is generally
decontaminated with a low-sudsing detergent such as Luiquinox° and triple rinsed with distilled
water. Larger equipment, such as drill rigs and associated tools, is steam cleaned. All
decontamination procedures are completed within an established decontamination area which is
located away from the active study area. Frequency of equipment decontamination depends on
the nature of work being performed, but in no case is decontamination performed less frequently
than once per test (i.e., soil boring, well installation, sample collection, etc.). Equipment blanks are
collected as a quality control measure when required by job specifications.
Soil Boring Installation
Soil borings are completed using hand -operated sampling tools, truck -mounted drills, or
Geoprobe° drilling rigs depending on the depth of sample collection and other site -specific
conditions. Hand operated stainless -steel bucket augers are utilized to collect soil samples at
regular intervals to determine site stratigraphy and to test for the presence of volatile organic
compounds. Samples retrieved from the hand auger are necessarily disturbed during the augering
process, but can provide accurate information on soil type and contaminant concentrations when
properly interpreted. Soil samples from hand augered borings are generally retrieved at one to
two foot intervals.
Truck -mounted or Geoprobe° drilling equipment is often utilized when sample retrieval depths
exceed twenty feet or subsurface conditions prevent utilization of hand augers (i.e., buried rocks,
wood, bricks or other materials occur in the subsurface). Truck -mounted drilling rigs usually
retrieve soil via a hollow -stem auger/split spoon collection method. Geoprobe° rigs usually employ
a Macro -Core° tube retrieval system.
Hollow stem augers provide relatively undisturbed 2-foot cores of soil samples. Soil samples are
generally collected at five foot intervals utilizing standard penetration test procedures as defined
by the American Society for Testing and Materials (ASTM) or are pushed to the desired depth using
the head of the drill rig. The standard penetration test involves driving a 2" outside diameter by 1-
3/8" inside diameter split -spoon sampler a minimum distance of one foot with a 340-lb. slide
hammer falling a distance of 30 inches.
A Geoprobe° rig is a hydraulically -powered soil probing machine. The probe utilizes static force
and percussion to advance a small diameter sampling device into the subsurface. The sampling
apparatus provides relatively undisturbed 5-foot cores of soil samples. Soil samples are collected
continuously. The Macro -Core° tube contains an inserted poly -vinyl chloride (PVC) liner which
retains the soil sample as the tube is driven into the ground. The Macro -Core° tube is
decontaminated between each 5-foot sample interval in a soil boring using a Liquinox and tap -
water mixture. A new PVC liner is used to collect soil from each sample interval in a soil boring.
Soil samples retrieved from the hollow -stem augers or Geoprobe are then carefully described
according to the Unified Soil Classification System. Soil descriptions are recorded on a soil
boring log.
Soil Sampling
Soils to be analyzed by a North Carolina -certified laboratory are prepared according to the specified
analytical method. Initially, soil samples are removed from the ground using either a hand auger,
backhoe bucket, spilt spoon auger, or a Macro -Core° sampling tube. During the removal, care is
taken to keep the disturbance of the soil structure to a minimum to reduce the loss of
contaminants. Once removed, the samples are placed in the proper sample container for the
specified analytical method. For samples collected for the MADEP VPH and EPA Method 8260, a
TerraCore° sampler is used to collect one 5-gram allotment of soil. The allotment is placed in
methanol -preserved 40 mL vials. Also, one 5-gram allotment of soil is placed into sodium bisulfate -
preserved 40 mL vials (one 5-gram allotment per vial, 2 vials per sample) for the 8260 low
concentration method. A 250-mL glass jar of the sampled soil is also collected to provide moisture
content information. Soils sampled for MADEP EPH, EPA Method 8270 and TPH 5030 and 3550 are
placed in a 250-mLglass jar (for MADEP EPH analysis an amber jar is required). TPH 5030 samples
are preserved in methanol similar to the 8260 analysis. Field personnel wear new, disposable
nitrile gloves during the collection of each sample.
The soil samples are labeled with the sample location, sample identification, date and time of
collection, and the analytical method. The samples are placed on ice, sent to a laboratory, and
analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody
documentation is maintained for each sample collected in the field.
If the soil is being sampled for volatile or semi -volatile compounds, a portion of the collected soil is
placed in a sealable bag and screened for volatile organic vapors. Head screening procedures are
described in the following paragraph.
Headspace Screening
Collected soil samples are routinely tested for the presence of volatile organic compounds (VOCs).
After retrieval from the ground, a portion of a soil sample is placed in a sealable plastic bag. The
soil samples are then set aside for approximately five minutes so that volatile constituents present
in the sample can reach equilibrium concentrations with headspace gases in the bag. Once a
suitable time period has passed, the probe of the sampling instrument, typically an Organic Vapor
Monitor (OVM) or a Photo Ionization Detector (PID), is inserted into the bag and the relative
concentration of total VOCs is measured and permanently recorded in a field note book. VOC
concentrations are measured using either a Thermo Electron Corp. Innova Series catalytic OVM or
an Ion Science PhoCheck PID. Both the OVM and PID instrumentation are periodically calibrated
according to the manufacturer's recommended procedures.
The OVM and PID are qualitative tools employed to detect and estimate the concentration of
organic or hydrocarbon vapors. A thin probe is inserted through a small break in the seal of a
bagged soil sample. For the OVM, an air sample from the headspace of the bag is drawn through
the probe into an internal chamber where the vapors are catalyzed. The concentration of the VOCs
is registered on a digital scale in parts per million (ppm). For the PID, an air sample from the
headspace of the bag is drawn across the face of a lamp causing the sample to emit photons, the
presence of which are converted into a VOC ppm reading that is displayed. Oxygen levels are field
calibrated prior to each use. VOC calibration occurs periodically depending upon use by using a
span gas of known concentration in a process recommended by the manufacturer.
Well Installation/Construction
Monitoring wells are installed using hand -operated sampling tools, a truck -mounted drill rig, or a
Geoprobe drilling rig depending on the depth of well and other site -specific conditions. All
monitoring wells are installed according to the requirements of 15A NCAC 2C-Well Construction
Standards. Specifically, individual monitoring wells are constructed of 2-inch diameter, schedule 40
PVC casing riser and screen. The screen interval is generally 10 to 15 feet of machine slotted PVC
with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the
screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above
the top of the screen. A one to two foot -thick bentonite pellet seal is then placed above the filter
pack. The remainder of the well annulus is completely filled with a Portland (Type 1/11) cement
grout mixture. A protective outer steel manhole, locking cap, and concrete pad is installed for each
well.
Type II Monitoring Well Construction
Single -cased monitoring wells are generally used in delineation of groundwater quality within the
surficial aquifer. The wells are constructed of 2-inch diameter, schedule 40 PVC casing and screen.
The screen interval is generally 10 to 15 feet of machine slotted PVC with a slot size of 0.010". Only
flush threaded joints are used. The annulus space around the screen is filled with washed filter
pack No. 2 sand. The filter pack extends one to two feet above the top of the screen. A one to two
foot -thick bentonite pellet seal is then placed above the filter pack. The remainder of the well
annulus is completely filled with a Portland (Type 1/II) cement grout mixture. A protective outer
steel manhole, locking cap, and concrete pad are installed for each well.
Type III Monitoring Well Construction
Double -cased monitoring wells are used in the delineation of groundwater quality within a deeper
portion of the surficial aquifer or an additional aquifer (e.g. aquitard, bedrock). A four to six-inch
outer casing is installed through the surficial aquifer until a sufficient depth or until the deeper
aquifer is encountered. The casing is secured with a Portland -grout collar that is tremmied into the
annular spaced from the bottom of the bore hole to the surface. Once the grout has sufficiently
cured, the bore hole is continued through the bottom of the outer casing to a depth approximately
15 - 20 feet beneath the outer casing. The inner casing is constructed of 2-inch diameter, schedule
40 PVC casing riser and screen. The screen interval is generally 5 to 10 feet of machine slotted PVC
with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the
screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above
the top of the screen. A one to two foot -thick bentonite pellet seal is then placed above the filter
pack. The remainder of the well annulus is completely filled with the same Portland grout mixture
used in the outer casing. A protective outer steel manhole, locking cap, and concrete pad are
installed for each well.
Well Development
Following installation of each well, surging and pumping or bailing techniques will be used to
remove fines from the screened interval. Groundwater is removed from each well until clear water
is retrieved or a noticeable reduction in the amount of silt is achieved. Purged groundwater is
disposed of in an environmentally safe manner.
Groundwater Sampling
Petroleum Sites
Groundwater samples are collected from temporary or permanent monitoring wells according to
established sampling protocol. When multiple monitoring wells or sampling points are sampled,
sampling is completed beginning with the least contaminated well to the most contaminated well,
if it is known. When permanent monitoring wells for petroleum sites are sampled, the well is
purged of a minimum of three well -bore volumes prior to sample collection in order to assure that
sampled water is representative of aquifer conditions. In temporary wells, the first water which
migrates into the open borehole is sampled. Samples from both temporary and permanent
monitoring wells are collected using individually wrapped disposable polyethylene bailers by field
personnel wearing disposable nitrile gloves. Only one well is sampled with a given bailer in order to
prevent sample cross -contamination. During both well purging and sampling, proper protective
clothing and equipment is used and is dependent upon the type and level of contaminants present.
Also, field personnel change gloves between different samples to reduce the chance of cross -
contamination. Water samples are transferred from the bailer to laboratory -prepared sampling
containers using slow emptying devices to reduce the chance of contamination loss through
volatilization. Preservatives, such as acids, are provided by the laboratory in pre -prepared
containers in which collected samples are placed if in -field preservation is necessary. The samples
are labeled with the project name, project number, sample identification, required analysis, and
date and time of collection. The samples are placed on ice, shipped to a certified laboratory, and
analyzed before the expiration of an analytical method's prescribed holding time. Chain -of -custody
documentation is maintained for each sample collected in the field.
Other Groundwater Sampling Protocols
When required by state or federal regulations, low -flow groundwater sampling procedures are
instituted. Groundwater samples collected in low -flow situations are collected using a peristaltic
pump. A peristaltic pump is a type of positive displacement pump. The fluid is contained within a
flexible tube fitted inside a circular pump casing. A rotor with a number of rollers attached to the
external circumference compresses the flexible tube. As the rotor turns, the part of tube under
compression closes thus forcing the fluid to be pumped to move through the tube. Groundwater
parameters such as water level drawdown, pH, conductivity, dissolved oxygen (DO) and turbidity.
Pumping rate, drawdown, and the time or volume required to obtain stabilization of parameter
readings can be used as a future guide to purge the well. Measurements are collected at a pre -
pumping established interval (typically five to ten minutes). Once all or a majority of the
parameters have stabilized forthree successive readings, stabilization has been achieved. In lieu of
measuring all five parameters, a minimum subset would include pH, conductivity, and turbidity or
DO. Three successive readings should be within ± 0.1 for pH, ± 3% for conductivity, and ± 10% for
turbidity and DO.
Upon parameter stabilization, sampling is initiated. Sampling flow rate is maintained at the estab-
lished purge rate or is adjusted slightly to minimize aeration, bubble formation, turbulent filling of
sample bottles, or loss of volatiles due to extended residence time in tubing. The same device used
for purging is used to collect the groundwater sample. Generally, volatile parameters are sampled
first. The sequence in which samples for inorganic parameters are collected is not determined
unless filtered (dissolved) samples are collected. Preservatives, such as acids, are provided by the
laboratory in pre -prepared containers in which collected samples are placed if in -field preservation
is necessary. The samples are labeled with the project name, project number, sample
identification, required analysis, and date and time of collection. The samples are placed on ice,
shipped to a certified laboratory, and analyzed before the expiration of an analytical method's
prescribed holding time. Chain -of -custody documentation is maintained for each sample collected
in the field.
During both well purging and sampling, proper protective clothing and equipment is used and is
dependent upon the type and level of contaminants present. Also, field personnel change gloves
between different monitoring wells or sampling points to reduce the chance of cross -
contamination. When multiple monitoring wells or sampling points are sampled, sampling is
completed beginning with the least contaminated well to the most contaminated well, if it is
known.
Stockpile Sampling
The number of composite samples collected from a stockpile or a total quantity of excavated soil is
based upon the cubic yardage. One composite sample is collected for every 100 cubic yards of
contaminated soil excavated. The volume of a stockpile or total quantity of excavated soil is
calculated by approximating the general geometry of a stockpile or estimating the capacity of the
dump trucks used for hauling. If a stockpile is sampled, a grid pattern is laid out on the stockpile,
dividing the stockpile into segments of approximately 200 cubic yards. Two soil borings are
advanced within a grid and three soil samples are collected from each soil boring at various depths.
The six soil samples are mixed into a composite sample by a trained TerraQuest technician. If truck
loads are sampled, an aliquot sample is collected from the hauling trucks at a frequency based
upon the capacity of the hauling trucks.
Aliquots are gently mixed into a composite sample by a trained TerraQuest technician. Every effort
is made to minimize the loss of contaminants through volatilization. The composited soil samples
are jarred in the appropriate laboratory -prepared containers, labeled with the sample location,
sample identification, date of collection, time of collection, the analytical method, and the
preservative. The samples are placed on ice, shipped to a laboratory, and analyzed before the
expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is
maintained for each sample collected in the field.
Surface Water Sampling
Surface water samples, specifically samples from creeks or streams, are collected from a
moving/flowing portion of the creek or stream to ensure that stagnant water is not collected. Field
personnel are careful to collect samples from flowing areas that are not so turbulent as to cause a
loss of volatile contaminants which might have been contained in the creek's/stream's water.
Samples are collected by field personnel wearing disposable nitrile gloves. Field personnel change
gloves between different locations to reduce the chance of cross -contamination. Samples are
collected directly from the appropriate creek or stream location and placed into the appropriate
laboratory -prepared containers. Preservatives, such as acids, are provided by the laboratory in pre -
prepared containers in which collected samples are placed if in -field preservation is necessary. The
samples are labeled with the project name, project number, sample identification, required
analysis, and date and time of collection. The samples are cooled on ice to approximately four
degrees centigrade, shipped to a certified laboratory, and analyzed before the expiration of an
analytical method's prescribed holding time. Chain -of -custody documentation is maintained for
each sample collected in the field.
Potable Well Sampling
Groundwater samples from potable wells are collected from sampling points, typically spigots,
located in the closest proximity to the potable well pump house as possible. Prior to sample
collection, the water is run for a sufficient amount of time to purge the bladder tank and assure
that sampled water is representative of aquifer conditions. Once purged, the flow rate is reduced
and samples are placed in the appropriate laboratory prepared containers with the appropriate
acid preservatives added if preservation of the sample is necessary. The samples are labeled with
the project name, project number, sample identification, required analysis, and date and time of
collection. The samples are placed on ice, shipped to a laboratory, and analyzed before the
expiration of an analytical method's prescribed holding time. Chain -of -custody documentation is
maintained for each sample collected in the field.
Public Water Supply Line Sampling
Groundwater samples from public water supply lines are collected from sampling points, typically
spigots. To sample the spigot, the flow rate is reduced and samples are placed in the appropriate
laboratory prepared containers. The samples are labeled with the sample location, sample
identification, date of collection, time of collection, and required analytical method. The samples
are placed on ice, shipped to a laboratory, and analyzed before the expiration of an analytical
method's prescribed holding time. Chain -of -custody documentation is maintained for each sample
collected in the field.
Air Sampling
Air samples are collected with the aide of a manually operated MityVac° pump manufactured by
Pristech, Inc. The air sampling process begins by connecting a length of rubber hose from the
MityVac° pump to the port to be sampled, or by hanging the hose inside of an emissions stack in
such a manner as to ensure no outside air causes dilution. Another length of hose is fixed to the
outlet port of the pump and is connected to a new Tedlar bag. Once the pump is hooked up, a
valve on the Tedlar collection bag is opened and air is manually forced into the bag by the pumping
action of sampling personnel.
Field Measurements
Field measurements taken to determine the pH, conductivity, temperature, and dissolved oxygen
concentration of a particular groundwater sample are taken directly after a particular monitoring
well has been adequately purged. This ensures that the groundwater parameter data collected is
representative of the aquifer conditions at a given location. Once purging of the monitoring well is
complete, the decontaminated probe head and cord of the appropriate unit is lowered into the
required monitoring well. If the depth to water in a specific monitoring well is greater than the
length of cord for a particular unit, a new, disposable bailer is slowly lowered into the appropriate
monitoring well and a representative groundwater sample is retrieved. A slow pouring device is
fitted onto the end of the disposable bailer and the sample is slowly poured into a new, disposable
plastic cup. Groundwater parameter data are then collected from the groundwater in the cup
using the required unit.
For pH, conductivity, and temperature, a Hanna Instruments Model 991300 portable meter is
utilized. This unit is periodically calibrated and maintained in accordance with the unit's operations
manual by field personnel. Prior to data collection, the unit is properly decontaminated to prevent
cross -contamination. The unit is decontaminated between each sample. The procedure used for
sample measurement involves lowering the meter's probe into the new, disposable cup containing
the groundwater sample to be measured and slowly stirring the probe to force groundwater across
the probe's membrane. The measurements displayed by the meter are then recorded.
For dissolved oxygen concentration measurements, a YSI° Model 55 Handheld Dissolved Oxygen
System is utilized. This unit is periodically calibrated and maintained in accordance with the unit's
operations manual by field personnel. Prior to data collection, the unit is properly decontaminated
to prevent cross -contamination. The unit is decontaminated between each sample. The procedure
used for sample measurement involves adjusting the unit for the correct altitude where the
sampling will take place and adjusting the reported units desired. Once this is done, the unit's
probe is inserted into the groundwater sample to be measured and the probe is slowly stirred to
force the groundwater across the probe's membrane. The measurements displayed by the unit are
then recorded.
For turbidity measurements, a Hach 2100P Portable Turbidity meter or equal equivalent is utilized.
The unit is calibrated prior to use in accordance with the unit's operations manual by field
personnel. Groundwater samples are collected in glass containers for measurement by the
instrument. The glass containers are washed with bottled -water between each measurement
collection. Once the sample is collected and inserted into the instrument, the measurements
displayed by the instrument are then recorded.
APPENDIX B
TERRA
W.Owi
ENVIRONMENTAL CONSULTANTS,
uest
P.C.
UVF TRILOGY ANALYTICAL REPORT
Project Name: 1238 Union St SE, Concord, NC
Project Number: 16820
Date: 11/20/2020
Standard Technical Procedures
The UVF TRILOGY instrument is a fixed -wavelength fluorometer but uses deep UV LEDS to detect
monoaromatic and polyaromatic hydrocarbons.
SITELAB's CAL-025 GRO Module is used to detect volatile petroleum hydrocarbons in the C6 to C10 range.
This test matches well to EPA Methods for GRO, BTEX, BPH or VOC's using GC/FID instrumentation.
SITELAB's CAL-042 EDRO Module is used to detect petroleum hydrocarbons in the C10 to C36 diesel and
oil range. This test matches well to EPA methods for TPH, EPH, DRO, and others using GC-FID
instrumentation.
Prior to field usage, the UVF TRILOGY is calibrated with five calibration standard solutions per targeted
analyte.
Soil samples are weighed to the nearest gram (i.e. 5.0 g) and added to a 1-ounce HDPE Nalgene bottle
with a measured amount of laboratory grade methanol to the nearest mL (i.e. 10 mL) to create a sample
extract. After addition of both the soil and methanol, the bottle is agitated for several minutes. Next, the
sample rests for several minutes allowing for the soil and methanol extract to separate.
After ample resting time, the methanol extract is collected with a syringe. A filter is connected to the end
of the syringe and dispensed into a clean sample test tube. The test tube is labeled with sample ID and
extract dilution factor (i.e. 2X).
Known amounts of extract are pipetted into a second test tube and diluted with methanol. The sample
ID and dilution factor are labeled on the test tube (i.e. 100X).
Samples are placed into a clean cuvette and carefully inserted into the selected UV Module. Prior to
analyzing the sample, the stored calibration that matches the UV Module being used, is selected. The
UVF TRILOGY produces a result that when multiplied to the dilution factor equals the true TPH value.
Quenching occurs when the detector is swamped by too many or certain type of hydrocarbons, producing
low or negative concentrations. The sample is tested at multiple dilutions to confirm the results are linear
and accurate.
Solvent blank samples are periodically analyzed to confirm the solvent is clean and the calibration of the
machine is maintained.
UVF Analytical Report
TEIRMCiluest
i�—w =1
ENYI RONMENTLL CONSULTANTS, P.C. sfteLAB
f
Project Name 1238 Union St SE, Concord, NC Sample Name BE1 (7.0)
Project Number 16820
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
BE1 (7.0) 7.0 11/18/2020 DRO 500 2420 50 mg/kg
BE1 (7.0) 7.0 11/18/2020 GRO 200 736 100 mg/kg
Friday, November 20, 2020 Page 1 of 6
Project Name 1238 Union St SE, Concord, NC
Sample Name CS-1 (5.5)
Project Number 16820
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
CS-1 (5.5) 5.5 11/18/2020 DRO 500 5905 50 mg/kg
CS-1 (5.5) 5.5 11/18/2020 GRO 500 875 250 mg/kg
Friday, November 20, 2020 Page 2 of 6
Project Name 1238 Union St SE, Concord, NC
Sample Name SW1 (6-7)
Project Number 16820
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
SW1 (6-7) 6-7 11/18/2020 DRO 2 <0.2 0.2 mg/kg
SW1 (6-7) 6-7 11/18/2020 GRO 2 2.56 1 mg/kg
Friday, November 20, 2020 Page 3 of 6
Project Name 1238 Union St SE, Concord, NC
Sample Name SW2 (6-7)
Project Number 16820
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
SW2 (6-7) 6-7 11/18/2020 DRO 2 0.24 0.2 mg/kg
SW2 (6-7) 6-7 11/18/2020 GRO 2 1.08 1 mg/kg
Friday, November 20, 2020 Page 4 of 6
Project Name 1238 Union St SE, Concord, NC
Sample Name SW3 (5-6)
Project Number 16820
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
SW3 (5-6) 5-6 11/18/2020 DRO 2 <0.2 0.2 mg/kg
SW3 (5-6) 5-6 11/18/2020 GRO 2 2.2 1 mg/kg
Friday, November 20, 2020 Page 5 of 6
Project Name 1238 Union St SE, Concord, NC
Sample Name SW4 (6-7)
Project Number 16820
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
SW4 (6-7) 6-7 11/18/2020 DRO 2 0.68 0.2 mg/kg
SW4 (6-7) 6-7 11/18/2020 GRO 2 <1 1 mg/kg
Friday, November 20, 2020 Page 6 of 6
� o.-..�
�:�R►A - Terraquest Environmental Consultants, P.C. Chain -Of -Custody Record 1 _I
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(Lab Use) (Field Identification) Depth Date Time Comp/Grab Matrix Sample Comments
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tiff eu rof ins Environment resting
Xenco
Analytical Report 679115
for
Terraquest Environmental Consultants, P.C.
Project Manager: Jonathan Grubbs
1238 Union St SE Concord
12.14.2020
pCCRF'0
TN !�
9e0 iO
RA ..
4147 Greenbriar Dr.
Stafford, TX 77477
Xenco-Houston (EPA Lab Code: TX00122):
Texas (T104704215-20-38), Arizona (AZ0765), Florida (E871002-33), Louisiana (03054)
Oklahoma (2020-014), North Carolina (681), Arkansas (20-035-0)
Xenco-Dallas (EPA Lab Code: TX01468):
Texas (T104704295-20-26), Arizona (AZ0809)
Xenco-El Paso (EPA Lab Code: TX00127): Texas (T104704221-20-18)
Xenco-Lubbock (EPA Lab Code: TX00139): Texas (T104704219-20-23)
Xenco-Midland (EPA Lab Code: TX00158): Texas (T104704400-19-21)
Xenco-Carlsbad (LELAP): Louisiana (05092)
Xenco-San Antonio (EPA Lab Code: TNI02385): Texas (T104704534-20-8)
Xenco-Tampa: Florida (E87429), North Carolina (483)
Page 1 of 27 Final 1.000
tiff eu rof ins Environment Testing
]lento
12.14.2020
Project Manager: Jonathan Grubbs
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302
Reference: Eurofins Xenco, LLC Report No(s): 679115
1238 Union St SE Concord
Project Address:
Jonathan Grubbs:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the Eurofins Xenco, LLC Report Number(s) 679115. All results being
reported under this Report Number apply to the samples analyzed and properly identified with a Laboratory ID
number. Subcontracted analyses are identified in this report with either the NELAC certification number of
the subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is available
upon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC Matrix
Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reported using all
other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by Eurofins Xenco, LLC. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 679115 will be filed for 45
days, and after that time they will be properly disposed without further notice, unless otherwise arranged with
you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting Eurofins Xenco, LLC to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
FOR 11 "FFl
*,
� � HMO,
Chad Bechtold
Project Manager
A Small Business and Minority Company
Houston - Dallas- Midland - Tampa - Phoenix- Lubbock- San Antonio - 8 Paso - Atlanta - New Mexico
Page 2 of 27 Final 1.000
tiff eu rof ins Environment Testing
Xenco
Sample Cross Reference 679115
Sample Id
BEI (T)
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Matrix Date Collected
S 11.18.2020 13:48
Sample Depth
Lab Sample Id
679115-001
Page 3 of 27
Final 1.000
tiff eurofins CASE NARRATIVE
Environment Testing
Xenco
Client Name: Terraquest Environmental Consultants, P.C.
Project Name: 1238 Union St SE Concord
Project ID: Report Date: 12.14.2020
Work Order Number(s): 679115 Date Received: 11.25.2020
Sample receipt non conformances and comments:
Sample receipt non conformances and comments per sample:
None
Analytical non conformances and comments:
Batch: LBA-3143789 SVOCs by SW846 8270E
The sample 679115-001 was analyzed at a dilution of 20 for Method 8270E - SVOCs due to the oily
sample matrix. Elevated reporting limits (RLs and MDLs) are provided.
Batch: LBA-3144206 EPH by MADEP Method
Lab Sample ID 679115-001 was randomly selected for Matrix Spike/Matrix Spike Duplicate (MS/MSD).
C 19 to C36Aliphatic Hydrocarbons, C9 to C 18 Aliphatic Hydrocarbons recovered below QC limits in the
Matrix Spike. CI I to C22 Aromatics, C19 to C36Aliphatic Hydrocarbons, C9 to C18 Aliphatic
Hydrocarbons recovered above QC limits in the Matrix Spike Duplicate. Outlier/s are due to possible
matrix interference. Samples in the analytical batch are: 679115-001.
The Laboratory Control Sample for C 19 to C36Aliphatic Hydrocarbons, C 11 to C22 Aromatics, C9 to C 18
Aliphatic Hydrocarbons is within laboratory Control Limits; therefore, the data was accepted.
Although C 11 to C22 Aromatics and C9 to C 18 Aliphatic Hydrocarbons were detected in the Method
Blank, the concentration for these targets in the associated sample 679115-001 were more than 10 times
the amount in the Method Blank.
Batch: LBA-3144346 VOCs by SW-846 8260D
Lab Sample ID 679115-001 was randomly selected for Matrix Spike/Matrix Spike Duplicate (MS/MSD).
1, 1 -Dichloropropene, 1,2,4-Trimethylbenzene, 2-Butanone, 2-Hexanone, Bromomethane, Chloroethane,
Methylene Chloride, Trichlorofluoromethane, trans-1,2-dichloroethene recovered below QC limits in the
Matrix Spike. Outlier/s are due to possible matrix interference. Samples in the analytical batch are:
679115-001.
The Laboratory Control Sample for Bromomethane, Methylene Chloride, 1,2,4-Trimethylbenzene, 2-
Hexanone, Trichlorofluoromethane, 2-Butanone, trans-1,2-dichloroethene, 1,1-Dichloropropene,
Chloroethane is within laboratory Control Limits; therefore, the data was accepted.
Page 4 of 27 Final 1.000
tiff eu rof ins Environment Testing
Xenco Hits Summary 679115
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Below is a summary of the analytes which were found to be present in the samples associated with this work order. This should only
be used in conjunction with the included analytical results.
Sample ID: BEI (71)
Sample ID: 679115-001
Date/Time Sampled: 11.18.2020 13:48
Matrix:
Solid
Analyte Name
Method
CAS No.
Dil.
Result
RL/PQL
MDL
Units
Qual
1,2,4-Trimethylbenzene
SW8260D
95-63-6
100
6.11
0.842
0.0429
mg/kg
DX
1,3,5-Trimethylbenzene
SW8260D
108-67-8
25
1.64
0.210
0.0122
mg/kg
2-Butanone
SW8260D
78-93-3
25
0.319
0.842
0.153
mg/kg
JX
Benzene
SW8260D
71-43-2
25
0.0126
0.0421
0.00871
mg/kg
J
Ethylbenzene
SW8260D
100-41-4
25
0.156
0.0421
0.0141
mg/kg
Naphthalene
SW8260D
91-20-3
100
12.9
1.68
0.337
mg/kg
D
Sec-Butylbenzene
SW8260D
135-98-8
25
2.10
0.210
0.0110
mg/kg
Toluene
SW8260D
108-88-3
25
0.279
0.210
0.0421
mg/kg
Total Xylenes
SW8260D
1330-20-7
100
0.814
0.0421
0.0337
mg/kg
isopropylbenzene
SW8260D
98-82-8
25
0.390
0.210
0.00732
mg/kg
m,p-Xylenes
SW8260D
179601-23-1
25
0.677
0.0842
0.0337
mg/kg
n-Butylbenzene
SW8260D
104-51-8
25
3.52
0.210
0.0115
mg/kg
n-Propylbenzene
SW8260D
103-65-1
25
0.805
0.210
0.0120
mg/kg
o-Xylene
SW8260D
95-47-6
25
0.137
0.0421
0.0414
mg/kg
p-Cymene (p-Isopropyltoluene)
SW8260D
99-87-6
25
1.45
0.210
0.0134
mg/kg
Sample ID: BEI (71) Sample ID: 679115-001 Date/Time Sampled: 11.18.2020 13:48 Matrix: Solid
Analyte Name
Method
CAS No.
Dil.
Result
RL/PQL
MDL
Units
Qual
1-Methylnaphthalene
SW8270E
90-12-0
20
15.0
3.56
0.570
mg/kg
2-Methylnaphthalene
SW8270E
91-57-6
20
23.0
3.56
0.964
mg/kg
Anthracene
SW8270E
120-12-7
20
0.633
3.56
0.295
mg/kg
J
Fluorene
SW8270E
86-73-7
20
3.09
3.56
0.295
mg/kg
J
Phenanthrene
SW8270E
85-01-8
20
7.11
3.56
0.354
mg/kg
Pyrene
SW8270E
129-00-0
20
1.20
3.56
0.312
mg/kg
J
Sample ID: BEI (T)
Sample ID: 679115-001
Date/Time Sampled: 11.18.2020 13:48
Matrix:
Solid
Analyte Name
Method
CAS No. Dil. Result RL/PQL MDL
Units Qual
C9-C10 Aromatic
VPH
HYDC9C10 1000 325 16.8 6.06
mg/kg
C9-C12 Aliphatic
VPH
ALHYDRC9C12 1000 604 50.5 22.5
mg/kg
Sample ID: BEI (T)
Sample ID: 679115-001
Date/Time Sampled: 11.18.2020 13:48
Matrix: Solid
Analyte Name
Method
CAS No. Dil. Result RL/PQL MDL
Units Qual
Percent Moisture
SM2540G
MOIST 1 6.29
%
Sample ID: BEI (T)
Sample ID: 679115-001
Date/Time Sampled: 11.18.2020 13:48
Matrix: Solid
Page 5 of 27 Final 1.000
tiff eu rof ins Environment resting
Xenco Hits Summary 679115
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Sample ID: 679115-001 Date/Time Sampled: 11.18.2020 13:48
Matrix: Solid
Analyte Name
Method
CAS No. Dil.
Result
RL/PQL
MDL
Units
Qual
C11 to C22 Aromatics
MA EPH
Cl lC22 10
938
90.7
45.4
mg/kg
DX
C19 to C36Aliphatic Hydrocarbons
MA EPH
ALHYDR090 50
414
427
213
mg/kg
JD
6
X
C9 to C18 Aliphatic Hydrocarbons
MA EPH
ALHYDRC9C18 50
1750
320
160
mg/kg
DX
Page 6 of 27 Final 1.000
tiff eurof ins Environment Testing Certificate of Analytical Results 679115
Xenco
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Sample Id: BEI (71) Matrix: Soil Date Received:11.25.2020 09:30
Lab Sample Id: 679115-001 Date Collected: 11.18.2020 13:48
Analytical Method: EPH by MADEP Method Prep Method: SW3550
Tech: JUN
Analyst: VIC Date Prep: 12.02.2020 20:39 % Moisture: 6.29
Seq Number: 3144206 Basis: Dry Weight
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
C9 to C18 Aliphatic Hydrocarbons
ALHYDRC9C11 1750
320
160
mg/kg
12.12.2020 13:27
DX 50
C19 to C36Aliphatic Hydrocarbons
ALHYDRCI9C: 414
427
213
mg/kg
12.12.2020 13:27
JDX 50
C11 to C22 Aromatics
C11C22 938
90.7
45.4
mg/kg
12.07.2020 19:53
DX 10
Surrogate
Cas Number
% Recovery
Units
Limits
Analysis Date
Flag
1-Chlorooctadecane
3386-33-2
52
%
40-140
12.07.2020 22:33
o-Terphenyl
84-15-1
91
%
40-140
12.07.202015:06
2-Fluorobiphenyl
321-60-8
100
%
40-140
12.07.202015:06
Page 7 of 27 Final 1.000
tiff eurof ins Environment Testing Certificate of Analytical Results 679115
Xenco
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Sample Id: BEI (71)
Matrix:
Soil
Date Received:11.25.2020 09:30
Lab Sample Id: 679115-001
Date Collected: 11.18.2020 13:48
Analytical Method: SVOCs by SW846 8270E
Prep Method: SW3550
Tech: JUN
Analyst: EKL
Date Prep:
12.02.2020 20:25
% Moisture: 6.29
Basis: Dry
Weight
Seq Number: 3143789
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
1,2,4-Trichlorobenzene
120-82-1
0.310 U
3.56
0.310
mg/kg
12.04.2020 17:34
U
20
1,2-Dichlorobenzene
95-50-1
0.328 U
3.56
0.328
mg/kg
12.04.2020 17:34
U
20
1,3-Dichlorobenzene
541-73-1
0.296 U
3.56
0.296
mg/kg
12.04.2020 17:34
U
20
1,4-Dichlorobenzene
106-46-7
0.320 U
3.56
0.320
mg/kg
12.04.2020 17:34
U
20
1-Methylnaphthalene
90-12-0
15.0
3.56
0.570
mg/kg
12.04.2020 17:34
20
2,4,5-Trichlorophenol
95-95-4
0.407 U
3.56
0.407
mg/kg
12.04.2020 17:34
U
20
2,4,6-Trichlorophenol
88-06-2
0.336 U
3.56
0.336
mg/kg
12.04.2020 17:34
U
20
2,4-Dichlorophenol
120-83-2
0.372 U
3.56
0.372
mg/kg
12.04.2020 17:34
U
20
2,4-Dimethylphenol
105-67-9
0.351 U
3.56
0.351
mg/kg
12.04.2020 17:34
U
20
2,4-Dinitrotoluene
121-14-2
0.272 U
3.56
0.272
mg/kg
12.04.2020 17:34
U
20
2,6-Dinitrotoluene
606-20-2
0.497 U
3.56
0.497
mg/kg
12.04.2020 17:34
U
20
2-Chloronaphthalene
91-58-7
0.620 U
3.56
0.620
mg/kg
12.04.2020 17:34
U
20
2-Chlorophenol
95-57-8
0.337 U
3.56
0.337
mg/kg
12.04.2020 17:34
U
20
2-Methylnaphthalene
91-57-6
23.0
3.56
0.964
mg/kg
12.04.2020 17:34
20
2-methylphenol
95-48-7
0.396 U
3.56
0.396
mg/kg
12.04.2020 17:34
U
20
2-Nitroaniline
88-74-4
0.333 U
7.11
0.333
mg/kg
12.04.2020 17:34
U
20
2-Nitrophenol
88-75-5
0.313 U
3.56
0.313
mg/kg
12.04.2020 17:34
U
20
3&4-Methylphenol
15831-10-4
0.329 U
3.56
0.329
mg/kg
12.04.2020 17:34
U
20
3-Nitroaniline
99-09-2
0.297 U
7.11
0.297
mg/kg
12.04.2020 17:34
U
20
4,6-dinitro-2-methyl phenol
534-52-1
0.271 U
7.11
0.271
mg/kg
12.04.2020 17:34
U
20
4-Bromophenyl-phenylether
101-55-3
0.283 U
3.56
0.283
mg/kg
12.04.2020 17:34
U
20
4-chloro-3-methylphenol
59-50-7
0.393 U
3.56
0.393
mg/kg
12.04.2020 17:34
U
20
4-Chloroaniline
106-47-8
0.270 U
7.11
0.270
mg/kg
12.04.2020 17:34
U
20
4-Chlorophenyl-phenyl ether
7005-72-3
0.345 U
3.56
0.345
mg/kg
12.04.2020 17:34
U
20
4-Nitroaniline
100-01-6
0.296 U
7.11
0.296
mg/kg
12.04.2020 17:34
U
20
4-Nitrophenol
100-02-7
0.552 U
7.11
0.552
mg/kg
12.04.2020 17:34
U
20
Acenaphthene
83-32-9
0.331 U
3.56
0.331
mg/kg
12.04.2020 17:34
U
20
Acenaphthylene
208-96-8
0.315 U
3.56
0.315
mg/kg
12.04.2020 17:34
U
20
Aniline (Phenylamine, Aminobenzene)
62-53-3
0.291 U
7.11
0.291
mg/kg
12.04.2020 17:34
U
20
Anthracene
120-12-7
0.633
3.56
0.295
mg/kg
12.04.2020 17:34
J
20
Benzo(a)anthracene
56-55-3
0.300 U
3.56
0.300
mg/kg
12.04.2020 17:34
U
20
Benzo(a)pyrene
50-32-8
0.367 U
3.56
0.367
mg/kg
12.04.2020 17:34
U
20
Benzo(b)fluoranthene
205-99-2
0.268 U
3.56
0.268
mg/kg
12.04.2020 17:34
U
20
Benzo(g,h,i)perylene
191-24-2
0.328 U
3.56
0.328
mg/kg
12.04.2020 17:34
U
20
Benzo(k)fluoranthene
207-08-9
0.413 U
3.56
0.413
mg/kg
12.04.2020 17:34
U
20
Benzoic Acid
65-85-0
0.747 U
21.3
0.747
mg/kg
12.04.2020 17:34
U
20
Benzyl Butyl Phthalate
85-68-7
0.387 U
3.56
0.387
mg/kg
12.04.2020 17:34
U
20
bis(2-chloroethoxy) methane
111-91-1
0.359 U
3.56
0.359
mg/kg
12.04.2020 17:34
U
20
bis(2-chloroethyl) ether
111-44-4
0.324 U
3.56
0.324
mg/kg
12.04.2020 17:34
U
20
Page 8 of 27 Final 1.000
tiff eurof ins Environment Testing Certificate of Analytical Results 679115
Xenco
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Sample Id: BEI (71) Matrix: Soil Date Received:11.25.2020 09:30
Lab Sample Id: 679115-001 Date Collected: 11.18.2020 13:48
Analytical Method: SVOCs by SW846 8270E Prep Method: SW3550
Tech: JUN % Moisture: 6.29
Analyst: EKL Date Prep: 12.02.2020 20:25 Basis: Dry Weight
Seq Number: 3143789
Parameter Cas Number Result RL NIDL Units Analysis Date Flag Dil
bis(2-chloroisopropyl) ether
39638-32-9
0.380 U
3.56
0.380
mg/kg
12.04.2020 17:34
U
bis(2-ethylhexyl) phthalate
117-81-7
3.56 U
7.11
3.56
mg/kg
12.04.2020 17:34
U
Chrysene
218-01-9
0.353 U
3.56
0.353
mg/kg
12.04.2020 17:34
U
Dibenz(a,h)Anthracene
53-70-3
0.271 U
3.56
0.271
mg/kg
12.04.2020 17:34
U
Dibenzofuran
132-64-9
0.330 U
3.56
0.330
mg/kg
12.04.2020 17:34
U
Diethyl Phthalate
84-66-2
0.326 U
3.56
0.326
mg/kg
12.04.2020 17:34
U
Dimethyl Phthalate
131-11-3
0.339 U
3.56
0.339
mg/kg
12.04.2020 17:34
U
di-n-Butyl Phthalate
84-74-2
0.342 U
3.56
0.342
mg/kg
12.04.2020 17:34
U
di-n-Octyl Phthalate
117-84-0
0.283 U
3.56
0.283
mg/kg
12.04.2020 17:34
U
Fluoranthene
206-44-0
0.313 U
3.56
0.313
mg/kg
12.04.2020 17:34
U
Fluorene
86-73-7
3.09
3.56
0.295
mg/kg
12.04.2020 17:34
J
Hexachlorobenzene
118-74-1
0.346 U
3.56
0.346
mg/kg
12.04.2020 17:34
U
Hexachlorobutadiene
87-68-3
0.295 U
3.56
0.295
mg/kg
12.04.2020 17:34
U
Hexachlorocyclopentadiene
77-47-4
0.324 U
3.56
0.324
mg/kg
12.04.2020 17:34
U
Hexachloroethane
67-72-1
0.369 U
3.56
0.369
mg/kg
12.04.2020 17:34
U
Indeno(1,2,3-c,d)Pyrene
193-39-5
0.287 U
3.56
0.287
mg/kg
12.04.2020 17:34
U
Isophorone
78-59-1
0.310 U
3.56
0.310
mg/kg
12.04.2020 17:34
U
Naphthalene
91-20-3
0.333 U
3.56
0.333
mg/kg
12.04.2020 17:34
U
Nitrobenzene
98-95-3
0.395 U
3.56
0.395
mg/kg
12.04.2020 17:34
U
N-Nitrosodi-n-Propylamine
621-64-7
0.371 U
3.56
0.371
mg/kg
12.04.2020 17:34
U
N-Nitrosodiphenylamine
86-30-6
0.397 U
3.56
0.397
mg/kg
12.04.2020 17:34
U
Pentachlorophenol
87-86-5
0.259 U
7.11
0.259
mg/kg
12.04.2020 17:34
U
Phenanthrene
85-01-8
7.11
3.56
0.354
mg/kg
12.04.2020 17:34
Phenol
108-95-2
0.319 U
7.11
0.319
mg/kg
12.04.2020 17:34
U
Pyrene
129-00-0
1.20
3.56
0.312
mg/kg
12.04.2020 17:34
J
Pyridine
110-86-1
0.357 U
7.11
0.357
mg/kg
12.04.2020 17:34
U
Surrogate
Cas Number
% Recovery
Units
Limits
Analysis Date
Flag
2-Fluorophenol
367-12-4
62
%
25-121
12.04.2020 17:34
Phenol-d6
13127-88-3
63
%
24-113
12.04.2020 17:34
Nitrobenzene-d5
4165-60-0
78
%
23-120
12.04.2020 17:34
2-Fluorobiphenyl
321-60-8
83
%
30-115
12.04.2020 17:34
2,4,6-Tribromophenol
118-79-6
77
%
19-122
12.04.2020 17:34
Terphenyl-D14
1718-51-0
84
%
18-137
12.04.2020 17:34
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Page 9 of 27 Final 1.000
tiff eurof ins Environment Testing Certificate of Analytical Results 679115
Xenco
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Sample Id: BEI (71)
Matrix:
Soil
Date Received:11.25.2020 09:30
Lab Sample Id: 679115-001
Date Collected: 11.18.2020 13:48
Analytical Method: VOCs by SW-846 8260D
Prep Method: SW5035A
Tech: SAD
Analyst: SAD
Date Prep:
12.02.2020 12:30
% Moisture: 6.29
Basis: Dry
Weight
Seq Number: 3144346
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
Acetone
67-64-1
0.467 U
4.21
0.467
mg/kg
12.02.2020 14:17
U
25
Benzene
71-43-2
0.0126
0.0421
0.00871
mg/kg
12.02.2020 14:17
J
25
Bromobenzene
108-86-1
0.0146 U
0.210
0.0146
mg/kg
12.02.2020 14:17
U
25
Bromochloromethane
74-97-5
0.0221 U
0.210
0.0221
mg/kg
12.02.2020 14:17
U
25
Bromodichloromethane
75-27-4
0.0106 U
0.210
0.0106
mg/kg
12.02.2020 14:17
U
25
Bromofonn
75-25-2
0.0435 U
0.210
0.0435
mg/kg
12.02.2020 14:17
U
25
Bromomethane
74-83-9
0.0397 U
0.210
0.0397
mg/kg
12.02.2020 14:17
UX
25
2-Butanone
78-93-3
0.319
0.842
0.153
mg/kg
12.02.2020 14:17
JX
25
tert-Butylbenzene
98-06-6
0.0540 U
0.210
0.0540
mg/kg
12.02.2020 14:17
U
25
Sec-Butylbenzene
135-98-8
2.10
0.210
0.0110
mg/kg
12.02.2020 14:17
25
n-Butylbenzene
104-51-8
3.52
0.210
0.0115
mg/kg
12.02.2020 14:17
25
Carbon Tetrachloride
56-23-5
0.0691 U
0.210
0.0691
mg/kg
12.02.2020 14:17
U
25
Chlorobenzene
108-90-7
0.00996 U
0.210
0.00996
mg/kg
12.02.2020 14:17
U
25
Chloroethane
75-00-3
0.0187 U
0.421
0.0187
mg/kg
12.02.2020 14:17
UX
25
Chloroform
67-66-3
0.00727 U
0.210
0.00727
mg/kg
12.02.2020 14:17
U
25
Chloromethane
74-87-3
0.0181 U
0.210
0.0181
mg/kg
12.02.2020 14:17
U
25
2-Chlorotoluene
95-49-8
0.0144 U
0.210
0.0144
mg/kg
12.02.2020 14:17
U
25
4-Chlorotoluene
106-43-4
0.0111 U
0.210
0.0111
mg/kg
12.02.2020 14:17
U
25
p-Cymene (p-Isopropyltoluene)
99-87-6
1.45
0.210
0.0134
mg/kg
12.02.2020 14:17
25
Dibromochloromethane
124-48-1
0.0376 U
0.210
0.0376
mg/kg
12.02.2020 14:17
U
25
1,2-Dibromoethane
106-93-4
0.0439 U
0.210
0.0439
mg/kg
12.02.2020 14:17
U
25
1,2-Dichlorobenzene
95-50-1
0.0121 U
0.210
0.0121
mg/kg
12.02.2020 14:17
U
25
1,3-Dichlorobenzene
541-73-1
0.0115 U
0.210
0.0115
mg/kg
12.02.2020 14:17
U
25
1,4-Dichlorobenzene
106-46-7
0.00903 U
0.210
0.00903
mg/kg
12.02.2020 14:17
U
25
1,2-Dichloroethane
107-06-2
0.0128 U
0.210
0.0128
mg/kg
12.02.2020 14:17
U
25
1, 1 -Dichloroethane
75-34-3
0.0158 U
0.210
0.0158
mg/kg
12.02.2020 14:17
U
25
trans-1,2-dichloroethene
156-60-5
0.0183 U
0.210
0.0183
mg/kg
12.02.2020 14:17
UX
25
cis-1,2-Dichloroethene
156-59-2
0.0127 U
0.210
0.0127
mg/kg
12.02.2020 14:17
U
25
1, 1 -Dichloroethene
75-35-4
0.0117 U
0.210
0.0117
mg/kg
12.02.2020 14:17
U
25
2,2-Dichloropropane
594-20-7
0.0221 U
0.210
0.0221
mg/kg
12.02.2020 14:17
U
25
1,3-Dichloropropane
142-28-9
0.0172 U
0.210
0.0172
mg/kg
12.02.2020 14:17
U
25
1,2-Dichloropropane
78-87-5
0.00835 U
0.210
0.00835
mg/kg
12.02.2020 14:17
U
25
trans- l,3-dichloropropene
10061-02-6
0.0383 U
0.210
0.0383
mg/kg
12.02.2020 14:17
U
25
1, 1 -Dichloropropene
563-58-6
0.0189 U
0.210
0.0189
mg/kg
12.02.2020 14:17
UX
25
cis-1,3-Dichloropropene
10061-01-5
0.00966 U
0.210
0.00966
mg/kg
12.02.2020 14:17
U
25
Ethylbenzene
100-41-4
0.156
0.0421
0.0141
mg/kg
12.02.2020 14:17
25
2-Hexanone
591-78-6
0.0898 U
2.10
0.0898
mg/kg
12.02.2020 14:17
UX
25
isopropylbenzene
98-82-8
0.390
0.210
0.00732
mg/kg
12.02.2020 14:17
25
Methylene Chloride
75-09-2
0.178 U
0.842
0.178
mg/kg
12.02.2020 14:17
UX
25
Page 10 of 27 Final 1.000
tiff eurof ins Environment Testing Certificate of Analytical Results 679115
Xenco
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Sample Id: BEI (71) Matrix: Soil Date Received:11.25.2020 09:30
Lab Sample Id: 679115-001 Date Collected: 11.18.2020 13:48
Analytical Method: VOCs by SW-846 8260D Prep Method: SW5035A
Tech: SAD % Moisture: 6.29
Analyst: SAD Date Prep: 12.02.2020 12:30 Basis: Dry Weight
Seq Number: 3144346
Parameter Cas Number Result RL NIDL Units Analysis Date Flag Dil
4-Methyl-2-Pentanone
108-10-1
0.110 U
2.10
0.110
mg/kg
12.02.2020 14:17
U
MTBE
1634-04-4
0.0172 U
0.210
0.0172
mg/kg
12.02.2020 14:17
U
Naphthalene
91-20-3
12.9
1.68
0.337
mg/kg
12.02.202015:28
D
n-Propylbenzene
103-65-1
0.805
0.210
0.0120
mg/kg
12.02.2020 14:17
Styrene
100-42-5
0.00865 U
0.210
0.00865
mg/kg
12.02.2020 14:17
U
1,1,1,2-Tetrachloroethane
630-20-6
0.0112 U
0.210
0.0112
mg/kg
12.02.2020 14:17
U
1,1,2,2-Tetrachloroethane
79-34-5
0.0198 U
0.210
0.0198
mg/kg
12.02.2020 14:17
U
Tetrachloroethylene
127-18-4
0.0156 U
0.210
0.0156
mg/kg
12.02.2020 14:17
U
Toluene
108-88-3
0.279
0.210
0.0421
mg/kg
12.02.2020 14:17
1,2,3-Trichlorobenzene
87-61-6
0.0842 U
0.210
0.0842
mg/kg
12.02.2020 14:17
U
1,2,4-Trichlorobenzene
120-82-1
0.0842 U
0.210
0.0842
mg/kg
12.02.2020 14:17
U
1,1,2-Trichloroethane
79-00-5
0.0165 U
0.210
0.0165
mg/kg
12.02.2020 14:17
U
1, 1, 1 -Trichloroethane
71-55-6
0.0212 U
0.210
0.0212
mg/kg
12.02.2020 14:17
U
Trichloroethene
79-01-6
0.0208 U
0.210
0.0208
mg/kg
12.02.2020 14:17
U
Trichlorofluoromethane
75-69-4
0.0129 U
0.210
0.0129
mg/kg
12.02.2020 14:17
UX
1,2,3-Trichloropropane
96-18-4
0.0189 U
0.210
0.0189
mg/kg
12.02.2020 14:17
U
1,2,4-Trimethylbenzene
95-63-6
6.11
0.842
0.0429
mg/kg
12.02.202015:28
DX
1,3,5-Trimethylbenzene
108-67-8
1.64
0.210
0.0122
mg/kg
12.02.2020 14:17
Vinyl Acetate
108-05-4
0.108 U
0.421
0.108
mg/kg
12.02.2020 14:17
U
Vinyl Chloride
75-01-4
0.0186 U
0.210
0.0186
mg/kg
12.02.2020 14:17
U
o-Xylene
95-47-6
0.137
0.0421
0.0414
mg/kg
12.02.2020 14:17
m,p-Xylenes
179601-23-1
0.677
0.0842
0.0337
mg/kg
12.02.2020 14:17
Total Xylenes
1330-20-7
0.814
0.0421
0.0337
mg/kg
12.02.2020 14:17
Isopropyl Ether
108-20-3
0.0442 U
0.210
0.0442
mg/kg
12.02.2020 14:17
U
Surrogate
Cas Number
% Recovery
Units
Limits
Analysis Date
Flag
Dibromofluoromethane
1868-53-7
88
%
53-142
12.02.2020 14:17
1,2-Dichloroethane-D4
17060-07-0
99
%
56-150
12.02.2020 14:17
Toluene-D8
2037-26-5
104
%
70-130
12.02.2020 14:17
4-Bromofluorobenzene
460-00-4
106
%
68-152
12.02.2020 14:17
25
25
100
25
25
25
25
25
25
25
25
25
25
25
25
25
100
25
25
25
25
25
100
25
Page 11 of 27 Final 1.000
tiff eu rof ins Environment resting
Xenco
Sample Id: BEI (71)
Lab Sample Id: 679115-001
Analytical Method: VPH
Tech: NGA
Analyst: NGA
Seq Number: 3144596
Parameter
C5-C8 Aliphatic
C9-C12 Aliphatic
C9-C10 Aromatic
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Certificate of Analytical Results 679115
Terraquest Environmental Consultants, P.C., Mebane, NC
1238 Union St SE Concord
Matrix: Soil Date Received:11.25.2020 09:30
Date Collected: 11.18.2020 13:48
Date Prep: 12.10.2020 19:10
Cas Number Result RL MDL
Prep Method: SW5035A
% Moisture: 6.29
Basis: Dry Weight
Units Analysis Date Flag Dil
ALHYDRC5C8 12.5 U
50.5
12.5
mg/kg
12.11.2020 02:06 U 1000
ALHYDRCKE 604
50.5
22.5
mg/kg
12.11.2020 02:06 1000
HYDC9C10 325
16.8
6.06
mg/kg
12.11.2020 02:06 1000
Cas Number
% Recovery
Units
Limits
Analysis Date Flag
615-59-8
120
%
70-130
12.11.2020 02:06
615-59-8
117
%
70-130
12.11.2020 02:06
Page 12 of 27 Final 1.000
tiff eu rof ins Environment resting
Xenco
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the " Y qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit. ND Not Detected.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non -Calculable
SMP Client Sample
BLK Method Blank
BKS/LCS Blank Spike/Laboratory Control Sample BKSD/LCSD Blank Spike Duplicate/Laboratory Control Sample Duplicate
MD/SD Method Duplicate/Sample Duplicate MS Matrix Spike
+ NELAC certification not offered for this compound.
* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
MSD: Matrix Spike Duplicate
Page 13 of 27 Final 1.000
tiff eurof ins QC Summary 679115
Environment Testing
1lenco
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Analytical Method: Percent Moisture by SM2540G
Seq Number: 3143638 Matrix: Solid
MB Sample Id: 3143638-1-BLK
MB Units Analysis Fla
Parameter Result Date g
Percent Moisture 0.0300 % 12.02.2020 08:00
Analytical Method: Percent Moisture by SM2540G
Seq Number: 3143638 Matrix: Soil
Parent Sample Id: 678371-013 MD Sample Id: 678371-013 D
Parent MD %RPD RPD Units Analysis Fla
Parameter Result Result Limit Date g
Percent Moisture 25.6 25.7 0 10 % 12.02.2020 08:00
Analytical Method: Percent Moisture by SM2540G
Seq Number: 3143638 Matrix: Solid
Parent Sample Id: 679112-001 MD Sample Id: 679112-001 D
Parent MD %RPD RPD Units Analysis Fla
Parameter Result Result Limit Date g
Percent Moisture 8.36 9.02 8 10 % 12.02.2020 08:00
Analytical Method: EPH by MADEP Method
Seq Number: 3144206
MB Sample Id: 7716195-1-BLK
MB Spike
Parameter Result Amount
C9 to C 18 Aliphatic Hydrocarbons 5.13 15.0
C 19 to C36Aliphatic Hydrocarbons <4.00 20.0
C11 to C22 Aromatics 4.84 42.5
Surrogate
MB MB
%Rec Flag
1-Chlorooctadecane
74
o-Terphenyl
85
2-Fluorobiphenyl
116
Prep Method: SW3550
Matrix:
Solid
Date Prep: 12.02.2020
LCS Sample Id:
7716195-1-BKS
LCSD Sample Id: 7716195-1-BSD
LCS LCS
LCSD
LCSD
Limits
%RPD RPD Units Analysis Flag
Result %Rec
Result
%Rec
Limit Date
13.5 90
15.0
100
40-140
11 25 mg/kg 12.07.2020 21:39
17.0 85
14.8
74
40-140
14 25 mg/kg 12.07.2020 21:39
39.3 92
40.3
95
40-140
3 25 mg/kg 12.07.202014:14
LCS
LCS
LCSD
LCSD
Limits Units Analysis
%Rec
Flag
°/oRec
Flag
Date
79
74
40-140 % 12.07.2020 21:39
86
90
40-140 % 12.07.202014:14
113
118
40-140 % 12.07.202014:14
MS/MSD Percent Recovery [D] = 100*(C-A) / B
Relative Percent Difference RPD = 200* I (C-E) / (C+E)
LCS/LCSD Recovery [D] = 100 * (C) / [B]
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample)
Page 14 of 27
LCS = Laboratory Control Sample
A = Parent Result
C = MS/LCS Result
E = MSD/LCSD Result
Final 1.000
MS = Matrix Spike
B = Spike Added
D = MSD/LCSD % Rec
tiff etirof ins QC Summary 679115
Environment Testing
1lenco
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Analytical Method: EPH by MADEP Method
Seq Number: 3144206
Parent Sample Id: 679115-001
Parent Spike
Parameter Result Amount
C9 to C18 Aliphatic Hydrocarbons 1950 16.0
C19 to C36Aliphatic Hydrocarbons 476 21.3
C11 to C22 Aromatics 921 45.3
Surrogate
1-Chlorooctadecane
o-Terphenyl
2-Fluorobiphenyl
Prep Method: SW3550
Matrix:
Soil
Date Prep: 12.02.2020
MS Sample Id:
679115-001 S
MSD Sample Id: 679115-001 SD
MS MS
MSD
MSD
Limits
%RPD RPD Units Analysis
Flag
Result %Rec
Result
%Rec
Limit Date
1840 0
2100
938
40-140
13 50 mg/kg 12.07.2020 23:00
X
446 0
517
192
40-140
15 50 mg/kg 12.07.2020 23:00
X
970 108
1050
285
40-140
8 50 mg/kg 12.07.202015:32
X
MS
MS
MSD
MSD
Limits Units Analysis
%Rec
Flag
%Rec
Flag
Date
50
42
40-140 % 12.07.2020 23:00
106
115
40-140 % 12.07.202015:32
110
100
40-140 % 12.07.202015:32
MS/MSD Percent Recovery [D] = 100*(C-A) / B
Relative Percent Difference RPD = 200* I (C-E) / (C+E)
LCS/LCSD Recovery [D] = 100 * (C) / [B]
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample)
Page 15 of 27
LCS = Laboratory Control Sample
A = Parent Result
C = MS/LCS Result
E = MSD/LCSD Result
Final 1.000
MS = Matrix Spike
B = Spike Added
D = MSD/LCSD % Rec
tiff etirof ins Environment resting
1lenco
Analytical Method: SVOCs by SW846 8270E
Seq Number: 3143789
MB Sample Id: 7716193-1-BLK
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-methylphenol
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol
3-Nitroaniline
4,6-dinitro-2-methyl phenol
4-Bromophenyl-phenylether
4-chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl-phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline (Phenylamine, Aminobenzene)
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Butyl Phthalate
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
QC Summary 679115
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Matrix: Solid
LCS Sample Id: 7716193-1-BKS
MB
Spike
LCS
LCS
LCSD
LCSD
Result
Amount
Result
%Rec
Result
%Rec
<0.0145
1.67
1.43
86
1.34
80
<0.0154
1.67
1.42
85
1.35
81
<0.0139
1.67
1.41
84
1.33
80
<0.0150
1.67
1.41
84
1.34
80
<0.0267
1.67
1.43
86
1.36
81
<0.0191
1.67
1.54
92
1.48
89
<0.0158
1.67
1.56
93
1.47
88
<0.0174
1.67
1.60
96
1.52
91
<0.0165
1.67
1.54
92
1.45
87
<0.0127
1.67
1.49
89
1.43
86
<0.0233
1.67
1.54
92
1.46
87
<0.0290
1.67
1.52
91
1.33
80
<0.0158
1.67
1.57
94
1.49
89
<0.0452
1.67
1.44
86
1.38
83
<0.0185
1.67
1.60
96
1.53
92
<0.0156
1.67
1.47
88
1.42
85
<0.0146
1.67
1.52
91
1.45
87
<0.0154
1.67
1.59
95
1.53
92
<0.0139
1.67
1.52
91
1.47
88
<0.0127
1.67
1.34
80
1.30
78
<0.0133
1.67
1.43
86
1.37
82
<0.0184
1.67
1.57
94
1.51
90
<0.0126
1.67
1.46
87
1.39
83
<0.0162
1.67
1.42
85
1.35
81
<0.0139
1.67
1.40
84
1.36
81
<0.0258
1.67
1.54
92
1.49
89
<0.0155
1.67
1.42
85
1.35
81
<0.0148
1.67
1.44
86
1.37
82
<0.0136
1.67
1.45
87
1.40
84
<0.0138
1.67
1.46
87
1.42
85
<0.0141
1.67
1.41
84
1.37
82
<0.0172
1.67
1.47
88
1.43
86
<0.0126
1.67
1.44
86
1.39
83
<0.0154
1.67
1.47
88
1.42
85
<0.0194
1.67
1.48
89
1.45
87
<0.0350
5.00
3.90
78
3.02
60
<0.0182
1.67
1.51
90
1.47
88
<0.0168
1.67
1.44
86
1.36
81
<0.0152
1.67
1.41
84
1.33
80
<0.0178
1.67
1.43
86
1.35
81
<0.167
1.67
1.53
92
1.49
89
<0.0165
1.67
1.44
86
1.40
84
<0.0127
1.67
1.47
88
1.43
86
<0.0154
1.67
1.44
86
1.37
82
<0.0153
1.67
1.45
87
1.40
84
<0.0159
1.67
1.45
87
1.40
84
<0.0160
1.67
1.50
90
1.46
87
<0.0133
1.67
1.45
87
1.41
84
<0.0147
1.67
1.45
87
1.42
85
<0.0138
1.67
1.45
87
1.39
83
Prep Method: SW3550
Date Prep:
12.02.2020
LCSD Sample Id: 7716193-1-BSD
Limits
%RPD
RPD
Units
Analysis Flag
Limit
Date
35-129
6
30
mg/kg
12.02.202019:07
38-122
5
30
mg/kg
12.02.202019:07
38-120
6
30
mg/kg
12.02.202019:07
37-121
5
30
mg/kg
12.02.202019:07
38-127
5
30
mg/kg
12.02.202019:07
40-135
4
30
mg/kg
12.02.202019:07
39-139
6
30
mg/kg
12.02.202019:07
36-135
5
30
mg/kg
12.02.202019:07
38-133
6
30
mg/kg
12.02.202019:07
48-131
4
30
mg/kg
12.02.202019:07
42-136
5
30
mg/kg
12.02.202019:07
32-138
13
30
mg/kg
12.02.202019:07
38-125
5
30
mg/kg
12.02.202019:07
36-126
4
30
mg/kg
12.02.202019:07
37-128
4
30
mg/kg
12.02.202019:07
30-133
3
40
mg/kg
12.02.202019:07
33-142
5
30
mg/kg
12.02.202019:07
38-126
4
30
mg/kg
12.02.202019:07
41-135
3
40
mg/kg
12.02.202019:07
30-146
3
40
mg/kg
12.02.202019:07
37-140
4
30
mg/kg
12.02.202019:07
40-134
4
30
mg/kg
12.02.202019:07
34-124
5
40
mg/kg
12.02.202019:07
41-131
5
30
mg/kg
12.02.202019:07
46-132
3
40
mg/kg
12.02.202019:07
21-152
3
40
mg/kg
12.02.202019:07
37-131
5
30
mg/kg
12.02.202019:07
39-129
5
30
mg/kg
12.02.202019:07
33-117
4
40
mg/kg
12.02.202019:07
39-139
3
30
mg/kg
12.02.202019:07
44-135
3
30
mg/kg
12.02.202019:07
43-153
3
30
mg/kg
12.02.202019:07
40-153
4
30
mg/kg
12.02.202019:07
40-153
3
30
mg/kg
12.02.202019:07
33-156
2
30
mg/kg
12.02.202019:07
31-135
25
50
mg/kg
12.02.202019:07
43-145
3
30
mg/kg
12.02.202019:07
30-129
6
30
mg/kg
12.02.202019:07
33-127
6
30
mg/kg
12.02.202019:07
25-124
6
30
mg/kg
12.02.202019:07
46-145
3
30
mg/kg
12.02.202019:07
42-135
3
30
mg/kg
12.02.202019:07
41-155
3
30
mg/kg
12.02.202019:07
39-132
5
30
mg/kg
12.02.202019:07
45-131
4
30
mg/kg
12.02.202019:07
43-132
4
30
mg/kg
12.02.202019:07
43-142
3
30
mg/kg
12.02.202019:07
34-166
3
30
mg/kg
12.02.202019:07
41-138
2
30
mg/kg
12.02.202019:07
41-131
4
30
mg/kg
12.02.202019:07
MS/MSD Percent Recovery [D] = 100*(C-A) / B LCS = Laboratory Control Sample MS = Matrix Spike
Relative Percent Difference RPD = 200* I (C-E) / (C+E) A = Parent Result B = Spike Added
LCS/LCSD Recovery [D] = 100 * (C) / [B] C = MS/LCS Result D = MSD/LCSD % Rec
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) E = MSD/LCSD Result
Page 16 of 27
Final 1.000
tiff etirof ins Environment resting
xenco
QC Summary 679115
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Analytical Method: SVOCs by SW846 8270E
Prep Method: SW3550
Seq Number: 3143789
Matrix:
Solid
Date Prep: 12.02.2020
MB Sample Id: 7716193-1-BLK
LCS Sample
Id:
7716193-1-BKS
LCSD Sample Id: 7716193-1-BSD
Parameter
NIB
Spike
LCS
LCS
LCSD
LCSD
Limits
%RPD RPD
Units
Analysis Fla S
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
Hexachlorobenzene
<0.0162
1.67
1.40
84
1.35
81
36-142
4
30
mg/kg
12.02.202019:07
Hexachlorobutadiene
<0.0138
1.67
1.41
84
1.33
80
35-129
6
30
mg/kg
12.02.202019:07
Hexachlorocyclopentadiene
<0.0152
1.67
1.23
74
1.16
69
16-106
6
30
mg/kg
12.02.202019:07
Hexachloroethane
<0.0173
1.67
1.40
84
1.34
80
36-121
4
30
mg/kg
12.02.202019:07
Indeno(1,2,3-c,d)Pyrene
<0.0134
1.67
1.48
89
1.42
85
39-154
4
30
mg/kg
12.02.202019:07
Isophorone
<0.0145
1.67
1.48
89
1.41
84
36-128
5
30
mg/kg
12.02.202019:07
Naphthalene
<0.0156
1.67
1.43
86
1.35
81
35-128
6
30
mg/kg
12.02.202019:07
Nitrobenzene
<0.0185
1.67
1.47
88
1.39
83
32-129
6
30
mg/kg
12.02.202019:07
N-Nitrosodi-n-Propylamine
<0.0174
1.67
1.47
88
1.41
84
34-129
4
30
mg/kg
12.02.202019:07
N-Nitrosodiphenylamine
<0.0186
1.67
1.46
87
1.40
84
27-155
4
30
mg/kg
12.02.202019:07
Pentachlorophenol
<0.0121
1.67
1.28
77
1.24
74
14-148
3
40
mg/kg
12.02.202019:07
Phenanthrene
<0.0166
1.67
1.40
84
1.35
81
37-139
4
30
mg/kg
12.02.202019:07
Phenol
<0.0150
1.67
1.57
94
1.47
88
34-127
7
40
mg/kg
12.02.202019:07
Pyrene
<0.0146
1.67
1.45
87
1.41
84
42-138
3
30
mg/kg
12.02.202019:07
Pyridine
<0.0167
1.67
1.07
64
1.01
60
30-113
6
40
mg/kg
12.02.202019:07
Surrogate
NIB
NIB
LCS
LCS
LCSD
LCSD
Limits
Units
Analysis
%Rec
Fla g
%Rec
Flag
u
%Rec
Flag
Date
2-Fluorophenol
83
94
89
25-121
%
12.02.202019:07
Phenol-d6
80
96
92
24-113
%
12.02.202019:07
Nitrobenzene-d5
76
88
83
23-120
%
12.02.202019:07
2-Fluorobiphenyl
82
87
82
30-115
%
12.02.202019:07
2,4,6-Tribromophenol
75
90
87
19-122
%
12.02.202019:07
Terphenyl-D14
86
87
86
18-137
%
12.02.202019:07
MS/MSD Percent Recovery [D] = 100*(C-A) / B
Relative Percent Difference RPD = 200* I (C-E) / (C+E)
LCS/LCSD Recovery [D] = 100 * (C) / [B]
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample)
LCS = Laboratory Control Sample
A = Parent Result
C = MS/LCS Result
E = MSD/LCSD Result
MS = Matrix Spike
B = Spike Added
D = MSD/LCSD % Rec
Page 17 of 27 Final 1.000
tiff etirof ins Environment resting
1lenco
QC Summary 679115
Analytical Method: SVOCs by SW846 8270E
Seq Number: 3143789
Parent Sample Id: 678938-001
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-methylphenol
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol
3-Nitroaniline
4,6-dinitro-2-methyl phenol
4-Bromophenyl-phenylether
4-chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl-phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline (Phenylamine, Aminobenzene)
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl Butyl Phthalate
bis(2-chloroethoxy) methane
bis(2-chloroethyl) ether
bis(2-chloroisopropyl) ether
bis(2-ethylhexyl) phthalate
Chrysene
Dibenz(a,h)Anthracene
Dibenzofuran
Diethyl Phthalate
Dimethyl Phthalate
di-n-Butyl Phthalate
di-n-Octyl Phthalate
Fluoranthene
Fluorene
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Matrix: Soil
MS Sample Id: 678938-001 S
Parent
Spike
MS
MS
MSD
MSD
Result
Amount
Result
%Rec
Result
%Rec
<0.0175
2.00
1.52
76
1.60
80
<0.0185
2.00
1.52
76
1.61
81
<0.0167
2.00
1.50
75
1.58
79
<0.0180
2.00
1.50
75
1.59
80
<0.0321
2.00
1.56
78
1.66
83
<0.0229
2.00
1.66
83
1.79
90
<0.0189
2.00
1.66
83
1.78
89
<0.0210
2.00
1.70
85
1.82
91
<0.0198
2.00
1.65
83
1.75
88
<0.0153
2.00
1.57
79
1.71
86
<0.0280
2.00
1.65
83
1.75
88
<0.0349
2.00
1.51
76
1.61
81
<0.0190
2.00
1.68
84
1.77
89
<0.0543
2.00
1.55
78
1.68
84
<0.0223
2.00
1.71
86
1.83
92
<0.0187
2.00
1.57
79
1.68
84
<0.0176
2.00
1.63
82
1.74
87
<0.0185
2.00
1.70
85
1.80
90
<0.0167
2.00
1.65
83
1.77
89
<0.0153
2.00
1.46
73
1.62
81
<0.0159
2.00
1.54
77
1.64
82
<0.0221
2.00
1.70
85
1.84
92
<0.0152
2.00
1.49
75
1.61
81
<0.0195
2.00
1.52
76
1.63
82
<0.0167
2.00
1.57
79
1.70
85
<0.0311
2.00
1.63
82
1.79
90
<0.0186
2.00
1.53
77
1.61
81
<0.0178
2.00
1.55
78
1.65
83
<0.0164
2.00
1.45
73
1.60
80
<0.0166
2.00
1.57
79
1.69
85
<0.0169
2.00
1.53
77
1.67
84
<0.0207
2.00
1.59
80
1.73
87
<0.0151
2.00
1.58
79
1.72
86
<0.0185
2.00
1.59
80
1.71
86
<0.0233
2.00
1.59
80
1.74
87
<0.0421
6.01
7.18
119
7.84
130
<0.0218
2.00
1.62
81
1.78
89
<0.0202
2.00
1.54
77
1.62
81
<0.0183
2.00
1.48
74
1.56
78
<0.0214
2.00
1.53
77
1.63
82
<0.200
2.00
1.70
85
1.81
91
<0.0199
2.00
1.56
78
1.69
85
<0.0153
2.00
1.60
80
1.74
87
<0.0186
2.00
1.55
78
1.65
83
<0.0184
2.00
1.57
79
1.70
85
<0.0191
2.00
1.56
78
1.67
84
<0.0193
2.00
1.64
82
1.79
90
<0.0160
2.00
1.58
79
1.73
87
<0.0177
2.00
1.58
79
1.71
86
<0.0166
2.00
1.56
78
1.67
84
Prep Method: SW3550
Date Prep:
12.02.2020
MSD Sample Id: 678938-001 SD
Limits
%RPD
RPD
Units
Analysis Flag
Limit
Date
35-129
5
30
mg/kg
12.02.2020 20:19
38-122
6
30
mg/kg
12.02.2020 20:19
38-120
5
30
mg/kg
12.02.2020 20:19
37-121
6
30
mg/kg
12.02.2020 20:19
38-127
6
30
mg/kg
12.02.2020 20:19
40-135
8
30
mg/kg
12.02.2020 20:19
39-139
7
30
mg/kg
12.02.2020 20:19
36-135
7
30
mg/kg
12.02.2020 20:19
38-133
6
30
mg/kg
12.02.2020 20:19
48-131
9
30
mg/kg
12.02.2020 20:19
42-136
6
30
mg/kg
12.02.2020 20:19
32-138
6
30
mg/kg
12.02.2020 20:19
38-125
5
30
mg/kg
12.02.2020 20:19
36-126
8
30
mg/kg
12.02.2020 20:19
37-128
7
30
mg/kg
12.02.2020 20:19
30-133
7
40
mg/kg
12.02.2020 20:19
33-142
7
30
mg/kg
12.02.2020 20:19
38-126
6
30
mg/kg
12.02.2020 20:19
41-135
7
40
mg/kg
12.02.2020 20:19
30-146
10
40
mg/kg
12.02.2020 20:19
37-140
6
30
mg/kg
12.02.2020 20:19
40-134
8
30
mg/kg
12.02.2020 20:19
34-124
8
40
mg/kg
12.02.2020 20:19
41-131
7
30
mg/kg
12.02.2020 20:19
46-132
8
40
mg/kg
12.02.2020 20:19
21-152
9
40
mg/kg
12.02.2020 20:19
37-131
5
30
mg/kg
12.02.2020 20:19
39-129
6
30
mg/kg
12.02.2020 20:19
33-117
10
40
mg/kg
12.02.2020 20:19
39-139
7
30
mg/kg
12.02.2020 20:19
44-135
9
30
mg/kg
12.02.2020 20:19
43-153
8
30
mg/kg
12.02.2020 20:19
40-153
8
30
mg/kg
12.02.2020 20:19
40-153
7
30
mg/kg
12.02.2020 20:19
33-156
9
30
mg/kg
12.02.2020 20:19
31-135
9
50
mg/kg
12.02.2020 20:19
43-145
9
30
mg/kg
12.02.2020 20:19
30-129
5
30
mg/kg
12.02.2020 20:19
33-127
5
30
mg/kg
12.02.2020 20:19
25-124
6
30
mg/kg
12.02.2020 20:19
46-145
6
30
mg/kg
12.02.2020 20:19
42-135
8
30
mg/kg
12.02.2020 20:19
41-155
8
30
mg/kg
12.02.2020 20:19
39-132
6
30
mg/kg
12.02.2020 20:19
45-131
8
30
mg/kg
12.02.2020 20:19
43-132
7
30
mg/kg
12.02.2020 20:19
43-142
9
30
mg/kg
12.02.2020 20:19
34-166
9
30
mg/kg
12.02.2020 20:19
41-138
8
30
mg/kg
12.02.2020 20:19
41-131
7
30
mg/kg
12.02.2020 20:19
MS/MSD Percent Recovery [D] = 100*(C-A) / B LCS = Laboratory Control Sample MS = Matrix Spike
Relative Percent Difference RPD = 200* I (C-E) / (C+E) A = Parent Result B = Spike Added
LCS/LCSD Recovery [D] = 100 * (C) / [B] C = MS/LCS Result D = MSD/LCSD % Rec
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) E = MSD/LCSD Result
Page 18 of 27
Final 1.000
tiff etirof ins Environment resting
xenco
QC Summary 679115
Analytical Method: SVOCs by SW846 8270E
Seq Number: 3143789
Parent Sample Id: 678938-001
Parameter
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-c,d)Pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosodi-n-Propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Surrogate
2-Fluorophenol
Phenol-&
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-D 14
MS/MSD Percent Recovery
Relative Percent Difference
LCS/LCSD Recovery
Log Difference
Parent
Result
<0.0195
<0.0166
<0.0183
<0.0208
<0.0162
<0.0174
<0.0188
<0.0222
<0.0209
<0.0224
<0.0146
<0.0199
<0.0180
<0.0176
<0.0201
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Spike
Amount
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
2.00
Prep Method: SW3550
Matrix:
Soil
Date Prep: 12.02.2020
MS Sample Id:
678938-001 S
MSD Sample Id: 678938-001 SD
MS
MS
MSD
MSD
Limits
%RPD RPD
Units
Analysis Flag
Result
%Rec
Result
%Rec
Limit
Date
1.53
77
1.65
83
36-142
8
30
mg/kg
12.02.2020 20:19
1.52
76
1.58
79
35-129
4
30
mg/kg
12.02.2020 20:19
1.35
68
1.45
73
16-106
7
30
mg/kg
12.02.2020 20:19
1.50
75
1.59
80
36-121
6
30
mg/kg
12.02.2020 20:19
1.60
80
1.73
87
39-154
8
30
mg/kg
12.02.2020 20:19
1.60
80
1.69
85
36-128
5
30
mg/kg
12.02.2020 20:19
1.53
77
1.61
81
35-128
5
30
mg/kg
12.02.2020 20:19
1.57
79
1.65
83
32-129
5
30
mg/kg
12.02.2020 20:19
1.60
80
1.68
84
34-129
5
30
mg/kg
12.02.2020 20:19
1.58
79
1.68
84
27-155
6
30
mg/kg
12.02.2020 20:19
1.42
71
1.51
76
14-148
6
40
mg/kg
12.02.2020 20:19
1.51
76
1.63
82
37-139
8
30
mg/kg
12.02.2020 20:19
1.64
82
1.75
88
34-127
6
40
mg/kg
12.02.2020 20:19
1.57
79
1.71
86
42-138
9
30
mg/kg
12.02.2020 20:19
0.693
35
0.947
47
30-113
31
40
mg/kg
12.02.2020 20:19
MS
MS
MSD
MSD
Limits
Units
Analysis
'% Rec
Flag
%Rec
Flag
Date
83
88
25-121
%
12.02.2020 20:19
86
90
24-113
%
12.02.2020 20:19
78
83
23-120
%
12.02.2020 20:19
78
82
30-115
%
12.02.2020 20:19
82
87
19-122
%
12.02.2020 20:19
80
86
18-137
%
12.02.2020 20:19
[D] = 100*(GA) / B
RPD = 200* I (C-E) / (C+E)
[D] = 100 * (C) / [B]
Log Diff. = Log(Sample Duplicate) - Log(Original Sample)
LCS = Laboratory Control Sample
A = Parent Result
C = MS/LCS Result
E = MSD/LCSD Result
MS = Matrix Spike
B = Spike Added
D = MSD/LCSD % Rec
Page 19 of 27 Final 1.000
tiff etirof ins Environment Testing
1lenco
Analytical Method: VOCs by SW-846 8260D
Seq Number: 3144346
MB Sample Id: 7716731-1-BLK
Parameter
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
tert-Butylbenzene
Sec-Butylbenzene
n-Butylbenzene
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
p-Cymene (p-Isopropyltoluene)
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethane
trans-1,2-dichloroethene
cis-1,2-Dichloroethene
1, 1 -Dichloroethene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,3-dichloropropene
1, 1 -Dichloropropene
cis-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
isopropylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
MTBE
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethylene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
QC Summary 679115
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Matrix: Solid
LCS Sample Id: 7716731-1-BKS
MB
Spike
LCS
LCS
LCSD
LCSD
Result
Amount
Result
%Rec
Result
%Rec
<0.0111
0.250
0.212
85
0.246
98
<0.000207
0.0500
0.0475
95
0.0468
94
<0.000346
0.0500
0.0492
98
0.0472
94
<0.000526
0.0500
0.0462
92
0.0466
93
<0.000251
0.0500
0.0452
90
0.0454
91
<0.00103
0.0500
0.0536
107
0.0541
108
<0.000943
0.0500
0.0386
77
0.0392
78
<0.00365
0.250
0.198
79
0.238
95
<0.00128
0.0500
0.0508
102
0.0479
96
<0.000261
0.0500
0.0518
104
0.0483
97
<0.000274
0.0500
0.0512
102
0.0475
95
<0.00164
0.0500
0.0491
98
0.0478
96
<0.000237
0.0500
0.0503
101
0.0496
99
<0.000444
0.0500
0.0456
91
0.0444
89
<0.000173
0.0500
0.0450
90
0.0445
89
<0.000431
0.0500
0.0393
79
0.0386
77
<0.000342
0.0500
0.0499
100
0.0479
96
<0.000264
0.0500
0.0479
96
0.0449
90
<0.000319
0.0500
0.0525
105
0.0490
98
<0.000895
0.0500
0.0494
99
0.0500
100
<0.00104
0.0500
0.0487
97
0.0507
101
<0.000288
0.0500
0.0502
100
0.0475
95
<0.000273
0.0500
0.0503
101
0.0479
96
<0.000214
0.0500
0.0491
98
0.0472
94
<0.000304
0.0500
0.0442
88
0.0452
90
<0.000376
0.0500
0.0453
91
0.0446
89
<0.000434
0.0500
0.0482
96
0.0471
94
<0.000301
0.0500
0.0458
92
0.0452
90
<0.000277
0.0500
0.0500
100
0.0488
98
<0.000524
0.0500
0.0461
92
0.0456
91
<0.000409
0.0500
0.0469
94
0.0468
94
<0.000198
0.0500
0.0462
92
0.0464
93
<0.000909
0.0500
0.0471
94
0.0478
96
<0.000448
0.0500
0.0481
96
0.0472
94
<0.000230
0.0500
0.0464
93
0.0462
92
<0.000336
0.0500
0.0506
101
0.0494
99
<0.00213
0.250
0.209
84
0.237
95
<0.000174
0.0500
0.0530
106
0.0515
103
<0.00422
0.0500
0.0431
86
0.0434
87
<0.00261
0.250
0.199
80
0.224
90
<0.000409
0.0500
0.0422
84
0.0433
87
<0.00200
0.0500
0.0506
101
0.0503
101
<0.000286
0.0500
0.0514
103
0.0482
96
<0.000205
0.0500
0.0506
101
0.0501
100
<0.000267
0.0500
0.0528
106
0.0526
105
<0.000470
0.0500
0.0463
93
0.0467
93
<0.000370
0.0500
0.0554
ill
0.0532
106
<0.00100
0.0500
0.0475
95
0.0460
92
<0.00200
0.0500
0.0557
ill
0.0536
107
<0.00200
0.0500
0.0561
112
0.0537
107
Prep Method: SW5035A
Date Prep:
12.02.2020
LCSD Sample Id: 7716731-1-BSD
Limits
%RPD
RPD
Units
Analysis
Limit
Date
50-150
15
25
mg/kg
12.02.202010:31
66-142
1
25
mg/kg
12.02.202010:31
75-125
4
25
mg/kg
12.02.202010:31
60-140
1
25
mg/kg
12.02.202010:31
75-125
0
25
mg/kg
12.02.202010:31
75-125
1
25
mg/kg
12.02.202010:31
60-140
2
25
mg/kg
12.02.202010:31
75-125
18
25
mg/kg
12.02.202010:31
75-125
6
25
mg/kg
12.02.202010:31
75-125
7
25
mg/kg
12.02.202010:31
75-125
7
25
mg/kg
12.02.202010:31
62-125
3
25
mg/kg
12.02.202010:31
60-133
1
25
mg/kg
12.02.202010:31
60-140
3
25
mg/kg
12.02.202010:31
74-125
1
25
mg/kg
12.02.202010:31
60-140
2
25
mg/kg
12.02.202010:31
73-125
4
25
mg/kg
12.02.202010:31
74-125
6
25
mg/kg
12.02.202010:31
75-125
7
25
mg/kg
12.02.202010:31
73-125
1
25
mg/kg
12.02.202010:31
73-125
4
25
mg/kg
12.02.202010:31
75-125
6
25
mg/kg
12.02.202010:31
75-125
5
25
mg/kg
12.02.202010:31
75-125
4
25
mg/kg
12.02.202010:31
68-127
2
25
mg/kg
12.02.202010:31
72-125
2
25
mg/kg
12.02.202010:31
75-125
2
25
mg/kg
12.02.202010:31
75-125
1
25
mg/kg
12.02.202010:31
59-172
2
25
mg/kg
12.02.202010:31
75-125
1
25
mg/kg
12.02.202010:31
75-125
0
25
mg/kg
12.02.202010:31
74-125
0
25
mg/kg
12.02.202010:31
66-125
1
25
mg/kg
12.02.202010:31
75-125
2
25
mg/kg
12.02.202010:31
74-125
0
25
mg/kg
12.02.202010:31
75-125
2
25
mg/kg
12.02.202010:31
75-125
13
25
mg/kg
12.02.202010:31
75-125
3
25
mg/kg
12.02.202010:31
75-125
1
25
mg/kg
12.02.202010:31
60-140
12
25
mg/kg
12.02.202010:31
60-140
3
25
mg/kg
12.02.202010:31
70-130
1
25
mg/kg
12.02.202010:31
75-125
6
25
mg/kg
12.02.202010:31
75-125
1
25
mg/kg
12.02.202010:31
72-125
0
25
mg/kg
12.02.202010:31
74-125
1
25
mg/kg
12.02.202010:31
71-125
4
25
mg/kg
12.02.202010:31
59-139
3
25
mg/kg
12.02.202010:31
75-137
4
25
mg/kg
12.02.202010:31
75-135
4
25
mg/kg
12.02.202010:31
MS/MSD Percent Recovery [D] = 100*(C-A) / B LCS = Laboratory Control Sample MS = Matrix Spike
Relative Percent Difference RPD = 200* I (C-E) / (C+E) A = Parent Result B = Spike Added
LCS/LCSD Recovery [D] = 100 * (C) / [B] C = MS/LCS Result D = MSD/LCSD % Rec
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample) E = MSD/LCSD Result
Flag
Page 20 of 27
Final 1.000
tiff etirof ins Environment resting
1lenco
QC Summary 679115
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Analytical Method:
VOCs by SW-846 8260D
Prep Method: SW5035A
Seq Number:
3144346
Matrix:
Solid
Date Prep: 12.02.2020
MB Sample Id:
7716731-1-BLK
LCS Sample
Id:
7716731-1-BKS
LCSD Sample Id: 7716731-1-BSD
Parameter
NIB
Spike
LCS
LCS
LCSD
LCSD
Limits
%RPD RPD
Units
Analysis
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
1,1,2-Trichloroethane
<0.000392
0.0500
0.0473
95
0.0485
97
75-127
3
25
mg/kg
12.02.2020 10:31
1, 1, 1 -Trichloroethane
<0.000503
0.0500
0.0471
94
0.0467
93
75-125
1
25
mg/kg
12.02.2020 10:31
Trichloroethene
<0.000494
0.0500
0.0489
98
0.0470
94
62-137
4
25
mg/kg
12.02.2020 10:31
Trichlorofluoromethane
<0.000307
0.0500
0.0466
93
0.0457
91
67-125
2
25
mg/kg
12.02.2020 10:31
1,2,3-Trichloropropane
<0.000450
0.0500
0.0454
91
0.0478
96
75-125
5
25
mg/kg
12.02.2020 10:31
1,2,4-Trimethylbenzene
<0.000255
0.0500
0.0492
98
0.0464
93
75-125
6
25
mg/kg
12.02.2020 10:31
1,3,5-Trimethylbenzene
<0.000289
0.0500
0.0498
100
0.0470
94
70-130
6
25
mg/kg
12.02.2020 10:31
Vinyl Acetate
<0.00256
0.250
0.210
84
0.221
88
60-140
5
25
mg/kg
12.02.2020 10:31
Vinyl Chloride
<0.000441
0.0500
0.0448
90
0.0436
87
60-140
3
25
mg/kg
12.02.2020 10:31
o-Xylene
<0.000985
0.0500
0.0497
99
0.0494
99
75-125
1
25
mg/kg
12.02.2020 10:31
m,p-Xylenes
<0.000800
0.100
0.101
101
0.0990
99
75-125
2
25
mg/kg
12.02.2020 10:31
Isopropyl Ether
<0.00105
0.0500
0.0426
85
0.0430
86
60-140
1
25
mg/kg
12.02.2020 10:31
Surrogate
NIB
NIB
LCS
LCS
LCSD
LCSD
Limits
Units
Analysis
%Rec
Flag
%Rec
Flag
%Rec
Flag
Date
Dibromofluoromethane
92
94
95
53-142
%
12.02.2020 10:31
1,2-Dichloroethane-D4
98
98
100
56-150
%
12.02.2020 10:31
Toluene-138
99
101
101
70-130
%
12.02.2020 10:31
4-Bromofluorobenzene
96
96
93
68-152
%
12.02.2020 10:31
MS/MSD Percent Recovery [D] = 100*(C-A) / B
Relative Percent Difference RPD = 200* I (C-E) / (C+E)
LCS/LCSD Recovery [D] = 100 * (C) / [B]
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample)
LCS = Laboratory Control Sample
A = Parent Result
C = MS/LCS Result
E = MSD/LCSD Result
MS = Matrix Spike
B = Spike Added
D = MSD/LCSD % Rec
Flag
Page 21 of 27 Final 1.000
QC Summary
679115
tiff eurof ins
Environment Testing
1lenco
Terraquest
Environmental Consultants, P.C.
1238 Union St SE Concord
Analytical Method: VOCs by SW-846 8260D
Prep Method: SW5035A
Seq Number: 3144346
Matrix: Soil
Date Prep: 12.02.2020
Parent Sample Id: 679115-001
MS Sample Id: 679115-001 S
Parameter
Parent
Spike
MS
MS
Limits
Units
Analysis
Result
Amount
Result
%Rec
Date
Acetone
<0.467
10.5
8.50
81
50-150
mg/kg
12.02.2020 16:34
Benzene
0.0126
2.10
1.58
75
66-142
mg/kg
12.02.2020 16:34
Bromobenzene
<0.0146
2.10
1.90
90
75-125
mg/kg
12.02.2020 16:34
Bromochloromethane
<0.0221
2.10
1.53
73
60-140
mg/kg
12.02.2020 16:34
Bromodichloromethane
<0.0106
2.10
1.57
75
75-125
mg/kg
12.02.2020 16:34
Bromoform
<0.0435
2.10
1.63
78
75-125
mg/kg
12.02.2020 16:34
Bromomethane
<0.0397
2.10
0.754
36
60-140
mg/kg
12.02.2020 1 6:34
2-Butanone
0.319
10.5
8.13
74
75-125
mg/kg
12.02.2020 16:34
tert-Butylbenzene
<0.0540
2.10
1.93
92
75-125
mg/kg
12.02.2020 16:34
Sec-Butylbenzene
2.10
2.10
3.80
81
75-125
mg/kg
12.02.2020 16:34
n-Butylbenzene
3.52
2.10
5.11
76
75-125
mg/kg
12.02.2020 16:34
Carbon Tetrachloride
<0.0691
2.10
1.59
76
62-125
mg/kg
12.02.2020 16:34
Chlorobenzene
<0.00996
2.10
1.76
84
60-133
mg/kg
12.02.2020 16:34
Chloroethane
<0.0187
2.10
0.789
38
60-140
mg/kg
12.02.2020 16:34
Chloroform
<0.00727
2.10
1.63
78
74-125
mg/kg
12.02.2020 16:34
Chloromethane
<0.0181
2.10
1.27
60
60-140
mg/kg
12.02.2020 16:34
2-Chlorotoluene
<0.0144
2.10
1.90
90
73-125
mg/kg
12.02.2020 16:34
4-Chlorotoluene
<0.0111
2.10
1.87
89
74-125
mg/kg
12.02.2020 16:34
p-Cymene (p-Isopropyltoluene)
1.45
2.10
3.21
84
75-125
mg/kg
12.02.2020 16:34
Dibromochloromethane
<0.0376
2.10
1.69
80
73-125
mg/kg
12.02.2020 16:34
1,2-Dibromoethane
<0.0439
2.10
1.75
83
73-125
mg/kg
12.02.2020 16:34
1,2-Dichlorobenzene
<0.0121
2.10
1.78
85
75-125
mg/kg
12.02.2020 16:34
1,3-Dichlorobenzene
<0.0115
2.10
1.78
85
75-125
mg/kg
12.02.2020 16:34
1,4-Dichlorobenzene
<0.00903
2.10
1.73
82
75-125
mg/kg
12.02.2020 16:34
1,2-Dichloroethane
<0.0128
2.10
1.57
75
68-127
mg/kg
12.02.2020 16:34
1,1-Dichloroethane
<0.0158
2.10
1.59
76
72-125
mg/kg
12.02.2020 16:34
trans-1,2-dichloroethene
<0.0183
2.10
1.47
70
75-125
mg/kg
12.02.2020 16:34
cis-1,2-Dichloroethene
<0.0127
2.10
1.59
76
75-125
mg/kg
12.02.2020 16:34
1, 1 -Dichloroethene
<0.0117
2.10
1.52
72
59-172
mg/kg
12.02.2020 16:34
2,2-Dichloropropane
<0.0221
2.10
1.65
79
75-125
mg/kg
12.02.2020 16:34
1,3-Dichloropropane
<0.0172
2.10
1.70
81
75-125
mg/kg
12.02.2020 16:34
1,2-Dichloropropane
<0.00835
2.10
1.66
79
74-125
mg/kg
12.02.2020 16:34
trans-1,3-dichloropropene
<0.0383
2.10
1.67
80
66-125
mg/kg
12.02.2020 16:34
1, 1 -Dichloropropene
<0.0189
2.10
1.53
73
75-125
mg/kg
12.02.2020 16:34
cis-1,3-Dichloropropene
<0.00966
2.10
1.60
76
74-125
mg/kg
12.02.2020 16:34
Ethylbenzene
0.156
2.10
1.89
83
75-125
mg/kg
12.02.2020 16:34
2-Hexanone
<0.0898
10.5
6.99
67
75-125
mg/kg
12.02.2020 16:34
isopropylbenzene
0.390
2.10
2.20
86
75-125
mg/kg
12.02.2020 16:34
Methylene Chloride
<0.178
2.10
1.40
67
75-125
mg/kg
12.02.2020 16:34
4-Methyl-2-Pentanone
<0.110
10.5
7.60
72
60-140
mg/kg
12.02.2020 16:34
MTBE
<0.0172
2.10
1.60
76
60-140
mg/kg
12.02.2020 16:34
Naphthalene
13.8
2.10
16.1
110
70-130
mg/kg
12.02.2020 16:34
n-Propylbenzene
0.805
2.10
2.69
90
75-125
mg/kg
12.02.2020 16:34
Styrene
<0.00865
2.10
1.74
83
75-125
mg/kg
12.02.2020 16:34
1, 1, 1,2-Tetrachloroethane
<0.0112
2.10
1.88
90
72-125
mg/kg
12.02.2020 16:34
1,1,2,2-Tetrachloroethane
<0.0198
2.10
1.77
84
74-125
mg/kg
12.02.2020 16:34
Tetrachloroethylene
<0.0156
2.10
1.77
84
71-125
mg/kg
12.02.2020 16:34
Toluene
0.279
2.10
1.84
74
59-139
mg/kg
12.02.2020 16:34
1,2,3-Trichlorobenzene
<0.0842
2.10
1.91
91
75-137
mg/kg
12.02.2020 16:34
1,2,4-Trichlorobenzene
<0.0842
2.10
1.90
90
75-135
mg/kg
12.02.2020 16:34
MS/MSD Percent Recovery
[D] = 100*(C-A) / B
LCS = Laboratory Control Sample
MS =
Matrix Spike
Relative Percent Difference
RPD = 200*
I (C-E) / (C+E)
A = Parent Result
B = Spike Added
LCS/LCSD Recovery
[D] = 100 *
(C) / [B]
C = MS/LCS Result
D = MSD/LCSD % Rec
Log Difference
Log Diff. =
Log(Sample Duplicate)
- Log(Original Sample)
E = MSD/LCSD Result
Page 22 of 27
Final 1.000
Flag
V
X
/1
/1
X
tiff etirof ins QC Summary 679115
Environment Testing
1lenco
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Analytical Method: VOCs by SW-846 8260D
Seq Number:
3144346
Parent Sample Id:
679115-001
Parameter
Parent
Spike
Result
Amount
1,1,2-Trichloroethane
<0.0165
2.10
1, 1, 1 -Trichloroethane
<0.0212
2.10
Trichloroethene
<0.0208
2.10
Trichlorofluoromethane
<0.0129
2.10
1,2,3-Trichloropropane
<0.0189
2.10
1,2,4-Trimethylbenzene
6.32
2.10
1,3,5-Trimethylbenzene
1.64
2.10
Vinyl Acetate
<0.108
10.5
Vinyl Chloride
<0.0186
2.10
o-Xylene
0.137
2.10
m,p-Xylenes
0.677
4.21
Isopropyl Ether
<0.0442
2.10
Surrogate
Dibromofluoromethane
1,2-Dichloroethane-D4
Toluene-D8
4-Bromofluorobenzene
Analytical Method: VPH
Seq Number:
3144596
MB Sample Id:
7716905-1-BLK
Parameter
MB
Spike
Result
Amount
C5-C8 Aliphatic
<0.00745
0.150
C9-C12 Aliphatic
<0.0134
0.150
C9-C10 Aromatic
<0.00360
0.0500
Surrogate %Rec
MB
/oRec Flag
2,5-Dibromotoluene 118
2,5-Dibromotoluene (PID) 109
Matrix: Soil
MS Sample Id: 679115-001 S
MS
MS
Limits
Result
%Rec
1.90
90
75-127
1.64
78
75-125
1.60
76
62-137
1.38
66
67-125
1.69
80
75-125
7.73
67
75-125
3.37
82
70-130
7.51
72
60-140
1.35
64
60-140
1.85
82
75-125
4.06
80
75-125
1.56
74
60-140
MS MS
%Rec Flag
93
103
102
103
Prep Method: SW5035A
Date Prep: 12.02.2020
Units
Analysis Flag
Date
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34 X
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34 X
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34
mg/kg
12.02.202016:34
Limits
Units
Analysis
Date
53-142
%
12.02.202016:34
56-150
%
12.02.202016:34
70-130
%
12.02.202016:34
68-152
%
12.02.202016:34
Prep Method: SW5035A
Matrix:
Solid
Date Prep: 12.10.2020
LCS Sample Id:
7716905-1-BKS
LCSD Sample Id: 7716905-1-BSD
LCS LCS
LCSD
LCSD
Limits
%RPD RPD Units Analysis Flag
Result %Rec
Result
%Rec
Limit Date
0.164 109
0.165
110
70-130
1 25 mg/kg 12.10.202015:25
0.147 98
0.154
103
70-130
5 25 mg/kg 12.10.202015:25
0.0507 101
0.0517
103
70-130
2 25 mg/kg 12.10.202015:25
LCS
LCS
LCSD
LCSD
Limits Units Analysis
%Rec
Flag
%Rec
Flag
Date
108
113
70-130 % 12.10.202015:25
100
107
70-130 % 12.10.202015:25
MS/MSD Percent Recovery [D] = 100*(C-A) / B
Relative Percent Difference RPD = 200* I (C-E) / (C+E)
LCS/LCSD Recovery [D] = 100 * (C) / [B]
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample)
Page 23 of 27
LCS = Laboratory Control Sample
A = Parent Result
C = MS/LCS Result
E = MSD/LCSD Result
Final 1.000
MS = Matrix Spike
B = Spike Added
D = MSD/LCSD % Rec
tiff etirof ins QC Summary 679115
Environment Testing
1lenco
Terraquest Environmental Consultants, P.C.
1238 Union St SE Concord
Analytical Method: VPH
Seq Number:
3144596
Parent Sample Id:
679969-001
Parameter
Parent
Spike
Result
Amount
C5-C8 Aliphatic
<1.39
27.9
C9-C12 Aliphatic
<2.48
27.9
C9-C10 Aromatic
2.81
9.29
Surrogate
2,5-Dibromotoluene
2,5-Dibromotoluene (PID)
Prep Method: SW5035A
Matrix:
Solid
Date Prep: 12.10.2020
MS Sample Id:
679969-001 S
MSD Sample Id: 679969-001 SD
MS MS
MSD
MSD
Limits
%RPD RPD Units Analysis Flag
Result %Rec
Result
%Rec
Limit Date
44.8 161
44.6
160
70-130
0 25 mg/kg 12.10.202016:50 X
38.0 136
39.5
142
70-130
4 25 mg/kg 12.10.202016:50 X
11.6 95
11.9
98
70-130
3 25 mg/kg 12.10.202016:50
MS
MS
MSD
MSD
Limits Units Analysis
%Rec
Flag
%Ree
Flag
Date
107
122
70-130 % 12.10.202016:50
101
117
70-130 % 12.10.202016:50
MS/MSD Percent Recovery [D] = 100*(C-A) / B
Relative Percent Difference RPD = 200* I (C-E) / (C+E)
LCS/LCSD Recovery [D] = 100 * (C) / [B]
Log Difference Log Diff. = Log(Sample Duplicate) - Log(Original Sample)
Page 24 of 27
LCS = Laboratory Control Sample
A = Parent Result
C = MS/LCS Result
E = MSD/LCSD Result
Final 1.000
MS = Matrix Spike
B = Spike Added
D = MSD/LCSD % Rec
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1. Select the 'Print' button to print 1 copy of each label.
2. The Return Shipment instructions, which provide your recipient with information on the returns process, will be printed with the
label(s).
3. After printing, select your next step by clicking one of the displayed buttons.
Note:To review or print individual labels, select the Label button under each label image above.
Use of this system constitutes your agreement to the service conditions in the current FedEx Service Guide, available on fedex.com.FedEx will not
be responsible for any claim in excess of $100 per package, whether the result of loss, damage, delay, non-delivery,misdelivery,or misinformation,
unless you declare a higher value, pay an additional charge, document your actual loss and file a timely claim.Limitations found in the current FedEx
Service Guide apply. Your right to recover from FedEx for any loss, including intrinsic value of the package, loss of sales, income interest, profit,
attorney's fees, costs, and other forms of damage whether direct, incidental,consequential, or special is limited to the greater of $100 or the
authorized declared value. Recovery cannot exceed actual documented loss -Maximum for items of extraordinary value is $500, e.g. jewelry,
precious metals, negotiable instruments and other items listed in our ServiceGuide. Written claims must be filed within strict time limits, see current
FedEx Service Guide.
l
5
7
Page 26 of 27 Final 1.000
Eurofins Xenco, LLC
Prelogin/Nonconformance Report- Sample Log -In
Client: Terraquest Environmental Consultants, F Acceptable Temperature Range: 0 - 6 degC
Date/ Time Received: 11.25.2020 09.30.00 AM Air and Metal samples Acceptable Range: Ambient
Work Order #: 679115 Temperature Measuring device used: HOU-188
Sample Receipt Checklist Comments
#1 *Temperature of cooler(s)?
3.3
#2 *Shipping container in good condition?
Yes
#3 *Samples received on ice?
Yes
#4 *Custody Seals intact on shipping container/ cooler?
N/A
#5 Custody Seals intact on sample bottles?
N/A
#6*Custody Seals Signed and dated?
N/A
#7 *Chain of Custody present?
Yes
#8 Any missing/extra samples?
No
#9 Chain of Custody signed when relinquished/ received?
Yes
#10 Chain of Custody agrees with sample labels/matrix?
Yes
#11 Container label(s) legible and intact?
Yes
#12 Samples in proper container/ bottle?
Yes
#13 Samples properly preserved?
Yes
#14 Sample container(s) intact?
Yes
#15 Sufficient sample amount for indicated test(s)?
Yes
#16 All samples received within hold time?
Yes
#17 Subcontract of sample(s)?
No
#18 Water VOC samples have zero headspace?
N/A
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: TOL PH Device/Lot#:
Checklist completed by: Lw�� Date: 11.25.2020
Lisandra Torres
Checklist reviewed by: �f d .Q�
b� Date: 11.29.2020
Chad Bechtold
Page 27 of 27 Final 1.000
APPENDIX C
NON=HAZARDOUS WASTE MANIFEST
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5. Transporter 1 Comp try Name 6. US EPA ID Number
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7. Transporter 2 Company Name
8. US EPA ID Number
C. Stale Transporter's ID
D. Transporter 2 Phone
9. Des[ noted Facility Name Site Address �W
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{••- 1� SR s lreLI y '" Se
E. State Facility's ID
F. Facility's Phone
11. WASTE DESCRIPTION
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Above
15. Special Handling Instructions and Additional Intom atlon
16. GENERATOR'S r rcondition for transporrttThe materials N I hereby describedat the
ani manifest arehnot subject to fadement are full and
on thiscontents
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Date
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Date
R
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PrintedTyped Name
Signature
Month
Day
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19. Discrepancy Indication Space
A
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Facility Owner or Operator: Certification of receipt of the waste materials covered by this manifest, except as noted In item 19.
Data
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CF14 ©2002 LABELMASTER® (800)621-6808 www.labelmaster.com�
PHII PRINGIED U.zi.G,o.a�,.in..q L swixa"N�"a"I
NON -HAZARDOUS WASTE MANIFEST
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5. Transpoder 1Qnnistany Name
6, US EPA ID Number
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Transporter 1 Phone
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8. US EPA ID Number
C. State Transporter's 10
D, Transporter 2 Phone
9. Designated Facility Name and Site Address
10. US EPA ID Number
E. State Facility's ID
F. Facility's Phone
11. WASTE DESCRIPTION
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13.
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IN
Total
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H. Handling Codes for Wastes Listed Above
15. Special Handling Instructions and Additional Information
16. GENERATOR'S CERTIFICATION: I heron certify that the contents of this shipment are fully and accurately described and are In
all respects
in proper condition for transport. The mate role described on this manifest
are not subject to federal hazardous waste regulations.
Date
Printe llryped Name
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Signature
Month
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Month
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Alternative Energy Solutions of NC, 1,1,('
Post office Box 310
Sanford, NC 27331
Phone#: 336-3024889
Fax #: 704-973-9573
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3841 ('nnningham Road
Thomasville, NC 27360
ription:
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NORTH CAROLINA
PUBLIC WEIG14MASTER
LICENSE E I S JUNE 30, 2020
JOHN GODF E 42673
INVALI SS SIGNED
WAS'hE MANIFEST
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Origination:
(: r)ss Weight: —
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<oee'nerafor°s ('ertification: I ceu-ti fy that lne materials described above mt this unanfifest arc na:t subject to federal regnlatimts fm• reporting propeu' disposal of HAZARDOUS WASTE..
Genei ator /Agent Signature Title
Ack:mwledgmeot of Receipt of Material: Date
Drivers Si imtt:re I7euc
Noted Discrepancies:
Inspected &Accepted (except as oted •hove By: Earthtec Environmental, Inc)
Accel,tteaY By: Date
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15. Special Handling Indications and Additional Information
16. GENERATOR'S CERTIFICATION: I hereby certify that the
contents of this shipment are fully and accurately described and are in
all respects
In proper condition for transport. The materials described on
this manifest are not subject to federal hazardous waste regulations.
Date
Printedrfyped Name
Ski%nature,
Month
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T
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APPENDIX D
UST-61
I 24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
in NC suspected release
(DWMUSEONLY)
Suspected Contamination? (Y/N) N
Facility ID Number NA
Incident# Risk(H,I,L,U)
Confirmed GW Contamination? (Y/N) N
Date Leak Discovered 11/20/20
Received On Received By
Confirmed Soil Contamination ?(Y/N) Y
Comm/Non-Commercial? Non -Comm
Reported by (circle one): Phone, Fax or Report
Samples Taken?(Y/N) Y
Reg/Non-regulated? Non -regulated
Region
Free Product? (Y/N) N If Yes, State Greatest
Thickness
INCIDENT DESCRIPTION
Incident Name: Barbara Linker el al Property
Address: 1238 Union St. S
County: Cabarrus
Regional Office (circle one): Ash ville, Mooresville ayetteville,
City/Town: Concord
Zip Code: 28025
Raleigh, Washington, Wilmington, Wins o - a em
Latitude (decimal degrees): 35.378049 Longitude (decimal degrees) :--80.551330
Obtained by:
❑ GPS
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)
OTopographic
During the removal of a 550-gallon heating oil UST, stained soils exhibiting a heating oil were noted in the
map
❑?
vicinity of holes noted in the UST along its sides and seams. The UST was hauled offsite for disposal.
GIS Address matching
7
• ther
❑? Unknown
Describe location:
Approximately 32.65 tons of contaminated oil were excavated from the UST basin and hauled offsite for
disposal. No free product was noted in the UST basin.
Google Earth
HOW RELEASE WAS DISCOVERED (Release code)
(Check one)
ORelease Detection Equipment or Methods IZVisual/Odor OGroundwater Contamination
*uring UST Closure/Removal OWater in Tank IdSurface Water Contamination
IdProperty Transfer OWater Supply Well Contamination MOther (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check primary source) (Check primary cause) (Check one) (Check primary product type released)
-Tank oSpill -Petroleum❑? Gasoline/ Diesel/ M Diesel/Veg.Oil
M Piping Overfill Non -Petroleum Kerosene Blend
seating Oil M Vegetable Oil 100%
Dispenser � Corrosion � Both
Other Petroleum � E10 — E20
M Submersible Turbine Pump 0 Physical/Mechanical
Location Products
Damage ME21 — E84
M Delivery Problem (Check one) Metals Metals
IN Install Problem DE85 — E99
M Spill Bucket �❑? Other Inorganics
�
N Facility
❑� Other Other Ethanol 100%
\hUnknown - esidence Other Organics
IZ E01 — E09
Unknown❑? Other
Definitions presented on reverse
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural Residentia 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes
2. No 3. Unknown
Number of Water Supply Wells Affected
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Barbara Linker et al Property
Point of Contact
Address
Michael Linker
100 Krimminger Ave. SE
City
State
Zip Code
Telephone Number
Concord
NC
28025
UST SYSTEM OPERATOR
UST Operator/Company
Address
same as UST System Owner
City
State
Zip Code
Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner
Address
same as UST System Owner
City
State
Zip Code
Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
See attached Map
Person Reporting Incident: Jonathan Grubbs
Company: Terraquest Environmental Consultants, P.C.
Telephone Number: 919-563-9091
Title: Vice President
Address: 100 E. Ruffin St., Mebane, NC 27302
Date: 11/20/2020
UST Form 61 (02/19)
Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
histallation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined
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MAP SOURCE:
USGS 7.5 MINUTE TOPOGRAPHIC MAP OF CONCORD & CONCORD SE, NC
GRAPHIC SCALE
0' 2,000' 4,000'
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SITE LOCATION MAP
BARBARA LINKER ET AL
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1238
CONCORD, CABARRUS
BARBARA LINKER ET AL
UN ON ST SE
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CONCORD, NC
PROJECT NO. 16820
DRAWN BY:
JRG
DATE: 11 20 20
ENVIRONMENTAL CONSULTANTS, P.C.
SCALE: 1" = 2,000'
CHECKED BY:
MJB
FIGURE NO. 1
Beverly, Trudy
From: jrgrubbs@terraquestpc.com
Sent: Thursday, January 21, 2021 2:25 PM
To: Beverly, Trudy
Subject: RE: [External] 1238 Union St S Concord NC Heating Oil UST Release
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
No we did not, but we removed all the soil contamination up to bedrock. We collected one soil sample (BE1) of the soil
immediately above the bedrock to document that the contamination extended to bedrock and then removed the
impacted soil.
Thanks!
Jonathan R. Grubbs, P.G.
TerraQuest Environmental Consultants, P.C.
100 East Ruffin Street
Mebane, NC 27302
(P) 919-563-9091
(F) 919-563-9095
(C) 919-906-0707
jrgrubbs@terraquestpc.com
From: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Sent: Thursday, January 21, 2021 2:18 PM
To: jrgrubbs@terraquestpc.com
Subject: RE: [External] 1238 Union St S Concord NC Heating Oil UST Release
Hey Jonathan,
You encountered rock during excavation. Did you sample groundwater?
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
�E W
Ue47r Imen � �. UST Section, Mooresville Regional Office
704.235.2182 (Office)
161
Trudy. B everlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httDs:Hdeu.ne. aov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaaement-eis-mans
File Review Procedures:
https:Hdcq.nc. gov/about/divisions/waste-manaaement/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
httns://deo.nc. aov/about/divisions/waste-manaeement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https:Hfiles.nc.gov/ncdeg[Waste%20Manatiement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.pdf
https:Hfiles.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%20filc%20names%20for%2OLaserfiche.docx
From: jr rubbs@terraquestpc.com[mailto:Irgrubbs@terraquestpc.com]
Sent: Thursday, January 21, 2021 1:33 PM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Subject: [External] 1238 Union St S Concord NC Heating Oil UST Release
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Hey Trudy!
We supervised the removal and subsequent soil excavation for a residential non-commercial heating oil UST at 1238
Union St S in Concord NC. The UST-61 is included in the report.
We excavated contaminated soil to achieve a clean closure. We have clean sidewall samples and removed all of the soil
up to 7 feet BGL where we encountered bedrock.
Could you please review the attached Initial Abatement Action Report and let me know if you have any questions!
Thanks!
Jonathan R. Grubbs, P.G.
TerraQuest Environmental Consultants, P.C.
100 East Ruffin Street
Mebane, NC 27302
(P) 919-563-9091
(F) 919-563-9095
(C) 919-906-0707
jrgrubbs@terraguestpc.com
Beverly, Trudy
From: Beverly, Trudy
Sent: Monday, May 10, 2021 7:10 AM
To: Jonathan Grubbs
Subject: RE: [External] 1238 Union St S Concord NC Heating Oil UST Release
Good Morning Jonathan,
We spoke by phone on April 14th about this site. You were going to get a groundwater sample from the well on the
parcel. Do you have that data for review?
Thanks,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
_ North Carolina Department of Environmental Quality
EQ�� NR,vN7en[al �� �UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: hops://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hgps://deg.nc.gov/about/divisions/waste-management/ust/ast-prosram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hi�2s://deg.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc.aov/ncdep/Waste%2OManaeement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.adf
htips://files.nc.,gov/ncdegiWaste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Jonathan Grubbs [mailto:jrgrubbs@terraquestpc.com]
Sent: Friday, April 30, 2021 8:08 AM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Subject: Re: [External] 1238 Union St S Concord NC Heating Oil UST Release
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Good morning Trudy!
Any progress on the review of UST closure report for the 1238 Union St S Concord NC Heating Oil UST Release?
Thanks!
Jonathan R. Grubbs, P.G.
TerraQuest Environmental Consultants, P.C.
100 East Ruffin Street
Mebane, NC 27302
(P) 919-563-9091
(F) 919-563-9095
(C) 919-906-0707
%rgrubbs@terraguestpc.com
On Apr 14, 2021, at 11:51 AM, Jonathan Grubbs <jrgrubbs@terraguestpc.com> wrote:
Thanks Trudy
Jonathan R. Grubbs, P.G.
TerraQuest Environmental Consultants, P.C.
100 East Ruffin Street
Mebane, NC 27302
(P) 919-563-9091
(F) 919-563-9095
(C) 919-906-0707
0rgrubbs@terraguestpc.com
On Apr 14, 2021, at 11:04 AM, Beverly, Trudy <trudy.beverly@ncdenr.gov> wrote:
Hey Jonathan,
I'll try to get that done today and get back with you.
Trudy
<image001.jpg> Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenn -gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: htl2s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: ht!ps:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hitps://deg.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httos:Hfiles.nc.aov/nedea/Waste%2OMana¢ement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc.gov/ncdeq/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Jonathan Grubbs[mailto:irgrubbs@terraguestpc.com]
Sent: Wednesday, April 14, 2021 10:59 AM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Subject: Re: [External] 1238 Union St S Concord NC Heating Oil UST Release
CAUTION: External email. Do not click links or open attachments unless you verify. Send all
suspicious email as an attachment to Report Spam.
Good morning! Just checking in to see if you had had a chance to review that site check
for 1238 Union St. S. Concord, NC. Thanks!
Jonathan R. Grubbs, P.G.
TerraQuest Environmental Consultants, P.C.
100 East Ruffin Street
Mebane, NC 27302
(P) 919-563-9091
(F) 919-563-9095
(C) 919-906-0707
0rgrubbs@terraquestpc.com
On Apr 13, 2021, at 3:05 PM, jrgrubbs@terraquestpc.com wrote:
Hey Trudy!
Hope you are well!
Have you had a chance to make a determination on this site - 1238
Union St S Concord NC? The property owners are putting the property
up for sale and want to know if it can be closed out or additional
investigation is required.
Thanks!
Jonathan R. Grubbs, P.G.
TerraQuest Environmental Consultants, P.C.
100 East Ruffin Street
Mebane, NC 27302
(P) 919-563-9091
(F) 919-563-9095
(C) 919-906-0707
jrgrubbs@terraquestpc.com
From: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Sent: Thursday, January 21, 2021 2:18 PM
To: jrgrubbs@terraquestpc.com
Subject: RE: [External] 1238 Union St S Concord NC Heating Oil UST
Release
Hey Jonathan,
You encountered rock during excavation. Did you sample groundwater?
Trudy
9
<image001.jpg> Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverly(a ncdenr.gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: hops://deq.nc.gov/about/divisions/waste-manaaement/ust
Branch's Above Ground Storage Tanks Website Address: hops://deg.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaeement-eis-maps
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hitps://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.¢ov/ncdeci[W aste%2OMana2ement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policy.pdf
https:Hfiles.nc. gov/ncdeq/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: jrrubbs@terraquestpc.com[mailto:Irgrubbs@terraquestpc.com]
Sent: Thursday, January 21, 2021 1:33 PM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Subject: [External] 1238 Union St S Concord NC Heating Oil UST Release
CAUTION: External email. Do not click links or open attachments unless you
verify. Send all suspicious email as an attachment to Report Spam.
Hey Trudy!
We supervised the removal and subsequent soil excavation for a
residential non-commercial heating oil UST at 1238 Union St S in
Concord NC. The UST-61 is included in the report.
We excavated contaminated soil to achieve a clean closure. We have
clean sidewall samples and removed all of the soil up to 7 feet BGL
where we encountered bedrock.
Could you please review the attached Initial Abatement Action Report
and let me know if you have any questions!
Thanks!
Jonathan R. Grubbs, P.G.
TerraQuest Environmental Consultants, P.C.
100 East Ruffin Street
Mebane, NC 27302
(P) 919-563-9091
(F) 919-563-9095
(C) 919-906-0707
irgrubbs@terraquestpc.com