7401_PittCounty_SouthernUnit_MSWLF_Jan21GW_FID1606191_20210826

ENR USE ONLY —]Paper Report []Electronic Data -Email CD (data loaded: Yes / No Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Groundwater Management Associates, Inc.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Emma H. Shiolev. P.G.
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006)
Southern Unit of the Pitt County 3025 Landfill Road 74-01 .1600 January 13-14, 2021
Municipal Solid Waste Landfill Greenville, NC 27834
Environmental Status: (Check all that apply)
Initial/Background Monitoring 1] Detection Monitoring �X Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells Methane gas monitoring data
Groundwater monitoring data from private water supply wells Corrective action data (specify)
Leachate monitoring data
Surface water monitoring data Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard. NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Emma H. Shipley, P.G. Project Hydrogeologist 252-758-3310
Facility Representative Name (Print) -- Title (Area Code) Telephone Number
8/26/2021 Affix NC Geologist Seal
Signature I ` Date
4300 Sapphire Court, Suite 100, Greenville, NC 27834
Facility Representative Address
C-121 (PG Flrm License Number)
NC PE Firm License Number (if applicable effective May 1, 2009)
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Compounds Detected At or Above Groundwater or Surface Water Standards during the January 2021 Sampling
Event (1/13-1/14/2021) - Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well ID
Date
Parameter
Results
(Ng/L)
MDL
(Ng/L)
NC 2L or
13 �d*
IMAC
(Ng/L)
MCL
(Ng/L)
Groundwater Samples
MW611
1/14/2020
1,4-Dioxane
6.5
0.8
3
-
-
1/14/2021
Barium Total
2120
1.1
700
-
2000
P1111
1/14/2021
Cobalt Total
2.383
1.4
-
1
-
1/14/2021
Vanadium Total
4.673
1.4
-
0.3
-
P16R
1/13/2021
1/14/2021
1,4-Dioxane
78 D
1.6
3
-
-
Barium Total
1100
1 1.1
700
-
2000
P17
1/13/2021
1,4-Dioxane
5
0.8
3
-
-
1/13/2021
1,4-Dioxane
160 D
2
3
-
-
1/14/2021
Barium Total
1870
1.10
700
-
2000
1/13/2021
Benzene
4
0.15
1
-
5
P19
1/14/2021
Beryllium Total
15.3
0.16
-
4
4
1/14/2021
Cobalt Total
19.3
1.40
-
1
-
1/14/2021
Vanadium Total
1.463
1.4
-
0.3
-
1/13/2021
Vinyl Chloride
0.573
0.32
0.03
-
2
P2OR
1/14/2021
Vanadium Total
2.443
1.4
-
0.3
-
1/14/2021
Beryllium Total
8.87
0.16
-
4
4
P2OD
1/14/2021
Chromium Total
12.9
1.4
10
-
100
1/14/2021
Vanadium Total
12.6
1.4
-
0.3
-
P28
1/14/2021
Vanadium Total
1.533
1.4
-
0.3
-
1/14/2021
1,4-Dioxane
140 D
4
3
-
-
1/14/2021
Barium Total
1290
1.1
700
-
2000
1/14/2021
Benzene Total
1.6
0.15
1
-
5
P29
1/14/2021
Cobalt Total
4.663
1.4
-
1
-
1/14/2021
Lead
18
3.1
15
-
15
1/14/2021
Thallium Total
0.2523
0.22
-
0.2
2
1/14/2021
Vanadium Total
36.1
1.4
-
0.3
-
1/14/2021
Arsenic
100
7.6
10
-
10
PZ1
1/14/2021
Cobalt Total
2.213
1.4
-
1
-
1/14/2021
Vanadium Total
12.4
1.4
-
0.3
-
PZ2
1/14/2021
1,4-Dioxane
3.6
0.8
3
-
-
Surface Water Samples
1/14/2021
jCobalt Total
8.023
1 1.4
1 4
1-
-
SW1
1/ 14/20211
Lead
3.543
1 3.1
1 0.54-
1
-
MDL = Method Detection Limit MCL = Federal Maximum Contaminant Level
IMAC = Interim Maximum Allowable Concentration
I = The analyte was positively identified, but the value is estimated below the reporting limit.
*15A NCAC 2L groundwater standards are listed for all groundwater sampling locations. 15A NCAC 2B standards are
listed for surface water sampling locations (SW1 and SW2).
Value represents an EPA action level.
*Value represents an EPA secondary Maximum Contaminant Level
+NC Protective Value for Surface Waters
Concentrations highlighted i yellow v were detected above the 2L (or 2B) standards.
Concentrations highlighted i orange a were detected above the IMAC.
Page 1 of 2

Compounds Detected At or Above Groundwater or Surface Water Standards during the January 2021 Sampling
Event (1/13-1/14/2021) - Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Preliminary analysis of cause and significance of concentrations detected at or above
groundwater or surface water standards:
1,4-Dioxane, barium, benezene, chromium, lead, and arsenic were detected at concentrations exceeding the
15A NCAC 02L groundwater standards in monitoring wells for the Southern Unit. Of these constituents, only
1,4-dioxane and arsenic were detected at concentrations above state standards in groundwater samples
collected from just below the southern property ditch (which generally acts as a local groundwater discharge
feature). This is the first occurrence of 1,4-dioxane above the 15A NCAC 02L standard below the southern
ditch. Arsenic was also detected in temporary groundwater piezometer PZ1, but this sample was highly
turbid (NTU = 297), and GMA suspects that a large portion of the arsenic detected in this sample is
associated with suspended particulates and is not representative of true dissolved concentrations. None of
the constituents were detected at concentrations exceeding state regulatory standards in downgradient
surface -water samples. The recently completed cap and stormwater upgrades are expected to reduce the
concentrations of all contaminants in groundwater downgradient of the Southern Unit. Thus, all detected
parameters are currently being addressed through the planned actions and pilot study.
The detection of 1,4-dioxane and other contaminants in well P29, which is located between the Northern and
Southern Landfill Units, indicates that the Northern Unit is also a source for these contaminants. Pitt County
has recently completed substantial cap and stormwater repairs and upgrades intended to limit the infiltration
of rainwater into the Southern Landfill Unit and reduce leachate volume and concentrations. If the cap and
stormwater upgrades are successful at the Southern Unit, the County may make similar improvements to the
Northern Unit, if needed, at at future date.
Page 2 of 2

JANUARY 2021 SEMI-ANNUAL WATER
QUALITY MONITORING EVENT AND
PILOT STUDY UPDATE
SOUTHERN PORTION OF THE
PITT COUNTY SOLID WASTE
MUNICIPAL LANDFILL
(FACILITY PERMIT # 74-01)
GREENVILLE, PITT COUNTY
PREPARED FOR
MR. TIM CORLEY, PE
ENGINEERING DEPARTMENT
PITT COUNTY
1717 WEST 5T" STREET
GREENVILLE, NC 27834
PREPARED BY
GROUNDWATER MANAGEMENT
ASSOCIATES, INC. (GMA)
4300 SAPPHIRE CT., SUITE 100
GREENVILLE, NORTH CAROLINA 27834
TELEPHONE: [phone]
AUGUST 26, 2021
GMA is a professional corporation licensed to practice geology (C-121) and engineering (C-0854) in North Carolina.

TABLE OF CONTENTS
1.0 INTRODUCTION........................................................................................... 1
1.1 Site Background......................................................................................... 2
1.2 Physical Setting and Hydrogeology............................................................... 2
1.3 Contaminants of Concern and Site Regulatory Status ..................................... 3
1.3.1 1, 4-Dioxane Assessment and Pilot Study Update ........................... 5
2.0 JANUARY 2021 SEMI-ANNUAL MONITORING EVENT........................................6
2.1 Groundwater Hydrology.............................................................................7
2.2 Sample Collection and Analyses.................................................................. 8
2.3 Analytical Results and Discussion................................................................ 8
3.0 WELL REHABILITATION AND MAINTENANCE .................................................. 9
4.0 CONCLUSIONS AND FUTURE WORK............................................................. 10
5.0 REPORT CERTIFICATION............................................................................. 11
6.0 REFERENCES.............................................................................................. 11
FIGURES
1. Site Layout and Existing Monitoring Network
2. Groundwater and Surface Water Sampling Locations - Southern Unit
3. Equipotential Map, January 13, 2021
TABLES
1. Monitoring Well Construction and Elevations
2. Monitoring Well Water Levels and Sample Purge Volumes
3. Staff Gauge Elevations and Water Levels
4. Calculations of Groundwater Velocity
5. Field -Water Quality Parameters
6. Appendix I Target Parameters
7. List of Compounds Detected during the January 2021 Sampling Event
APPENDICES
A. Correspondence from the NC Division of Waste Management
B. Sampling Records
C. Laboratory Report and Chain -of -Custody Forms for Water Samples
D. Well Rehabilitation Field Sheets
E. As -Built Drawings for the Southern Unit Cap Repair and Stormwater Upgrade

1.0 INTRODUCTION
Pitt County (the County) is currently assessing corrective action measures for 1,4-dioxane and
benzene groundwater contamination at the Southern Unit of the inactive Pitt County Solid
Waste Municipal Landfill (Facility Permit #74-01, Figure 1). In 2017, the County confirmed a
slight exceedance of the NC Groundwater Quality Standard (NCAC 02L) for benzene in
groundwater samples collected from the landfill's monitoring well network. Exceedances of the
NCAC 02L groundwater standard for 1,4-dioxane were confirmed in January 2019. Testing for
1,4-dioxane began in response to a May 2018 directive from the North Carolina Department of
Environmental Quality (NCDEQ), Division of Waste Management (DWM), Solid Waste Section
(SWS) that required all North Carolina landfills to begin testing for the constituent as part of
their routine groundwater monitoring (Appendix A).
Following approval from the SWS, the County has collected groundwater samples from just
beneath the southern ditch to monitor the extent of benzene contamination at the facility. This
ditch serves as a groundwater discharge location for the Southern Unit. To date, benzene has
not been detected in exceedance of the NCAC 02L standard in these samples, which suggests
that benzene contamination above the NCAC 02L groundwater standard does not extend off the
facility property.
In response to the confirmation of concentrations of 1,4-dioxane above the NCAC 02L standard
in groundwater at the site, Groundwater Management Associates, Inc. (GMA), on behalf of the
County, submitted a proposal to the SWS on June 21, 2019 to further assess and address 1,4-
dioxane contamination at the landfill. Specifically, GMA proposed to: 1) fully delineate the
vertical and horizontal extents of 1,4-dioxane, and 2) initiate a pilot study to establish the
effectiveness of cap and stormwater system upgrades and repairs at reducing groundwater
contaminant concentrations and preventing further degradation of groundwater quality.
Following approval of the pilot study by the SWS on June 26, 2019 (Appendix A), a geophysical
evaluation was performed to evaluate the integrity of the Southern Landfill Unit cap and to
provide a baseline from which to evaluate hydrologic improvements following cap upgrades and
repairs. The results of this evaluation were provided in the in the "July 2019 Semi -Annual
Water Quality Monitoring Event and Pilot Study Update" report (GMA, 2019).
After completion of the geophysical survey, the County contracted with an engineering firm
(The Wooten Company) to design cap repairs and stormwater upgrades that will eliminate or
greatly reduce the infiltration of precipitation into the Southern Unit and protect the
groundwater from further contamination via leaching from landfill waste. The Wooten
Company's (Wooten's) design included repairing the cap on the western end of the Southern
Landfill, regrading multiple areas to eliminate ponding on the mound, restoring the stormwater
conveyance system to operate as originally designed, and adding new drainage pipes to the
southwest corner of the mound at a total cost of over $1 million. The design plans were
finalized in June of 2020, and construction began on November 4, 2020. Although the

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 2 of 12
construction was originally scheduled to be completed within 120 days, the project experienced
significant weather -related delays due to long periods of high rainfall. Construction was finally
completed in June of 2021.
The County continued to monitor groundwater at the Southern Unit on a semi-annual schedule
during the planning and construction period. The remainder of this report presents the results
of the January 2021 semi-annual monitoring event that occurred during active construction at
the Southern Unit.
1.1 Site Background
The Pitt County Landfill occupies approximately 156 acres along Allen Road west of the city of
Greenville, NC (Figure 1). The landfill is comprised of a Northern Unit that closed in 1990 and a
Southern Unit that reached capacity in 1995. An east -west trending railroad (Norfolk Southern
Railroad) separates the Northern and Southern Units. The Pitt County landfill is unlined, and
leachate is not collected. The Northern Unit received waste from 1974 until 1990, and the
Southern Unit received waste from 1991 until 1995. Due to the closure dates, only the
Southern Unit is subject to the September 1993 rules for municipal solid waste landfills (15A
NCAC 13B .1600). Pitt County monitors the Northern Unit in accordance with the conditions of
the solid waste permit and 15A NCAC 13B .0510.
1.2 Physical Setting and Hydrogeology
The Pitt County Landfill lies in the central portion of the Coastal Plain Physiographic Province of
North Carolina where Cretaceous to Recent age Coastal Plain sedimentary formations overlie
Mesozoic and older basement bedrock (Horton and Zullo, 1991). Coastal Plain sediments and
sedimentary rocks have significant variations in permeability and water -producing capabilities.
High -permeability strata that readily produce usable quantities of water are aquifers, and low -
permeability sediments that restrict the movement of groundwater, either into or out of
aquifers, are confining beds. Coastal Plain aquifers typically use the predominant geologic
formation name that is associated with the aquifer. The two uppermost aquifers at the Pitt
County Landfill are: the unconfined Surficial/Yorktown aquifer and the confined Peedee Aquifer.
The Surficial/Yorktown Aquifer is locally composed of fossiliferous clays and sands. The clays
within the unit tend to serve as confining layers and restrict recharge to underlying aquifers
(GMA and McGill, 2001). The Peedee Aquifer consists of unconsolidated sands and sandstones
of the of Late Cretaceous age Peedee Formation (Winner & Coble, 1996). In the western half
of Pitt County, the Peedee Aquifer lies directly beneath the Surficial/Yorktown Aquifer, and the
elevation of the top of the Peedee Aquifer is above sea level (GMA and McGill, 2001).
A detailed description of the local site hydrogeology is provided in the Water Quality Monitoring
Plan for the Southern Unit (GMA, 1994). In general, a sandy clay extends from the original land
surface beneath the landfill to varying depths of 6 to 13 feet. A portion of this clay may have

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 3 of 12
been excavated from adjacent to the Southern Unit mound and used as part of the clay cap for
the mound. Coarser, more permeable sediments (silty fine sand, clayey sand, and very clayey
sand) typically exist at depths of 10 to 16 feet. Underlying these more permeable sediments, at
a depth of approximately 16 feet below the original land surface, is a thin, discontinuous, dark
gray clay that ranges from 0.5 to 3.0 feet in thickness, with an average thickness of 1 foot.
This clay layer exists at an elevation of approximately 66 feet above mean sea level and has
previously been referred to as the "66-foot clay" (GMA, 1994). Below this clay layer lie silty,
fine sands. During the installation of deep monitoring well P20D, GMA observed a silty, clay
layer from approximately 45 to 48 feet below the land surface. Below this clay layer, GMA
observed a fine, phosphatic sand. GMA believes the deepest on -site monitoring wells (e.g.
MW1R, MW3, and P20D) may penetrate the top of the Peedee Aquifer, which is estimated to be
about 25 feet thick at the location of the landfill (GMA and McGill, 2001). We provide a general
summary of the stratigraphy below.
Average depth of strata relative
to original land surface (feet)
Lithology
0 — 9.5
sandy clay
9.5 — 16
silty fine sand, clayey sand, and very clayey sand
16 — 17
dark gray clay
17 — 45
silty, fine sand
45 — 48
silty, clay
48 — 60+
fine, phosphatic sand
1.3 Contaminants of Concern and Site Regulatory Status
As described in the introduction, the Southern Unit of the Pitt County Landfill is currently under
assessment for low-level exceedances of the NC Groundwater Quality Standard (NCAC 02L) for
benzene. The County first confirmed a slight exceedance of the NCAC 02L groundwater
standard for benzene in groundwater samples collected from the landfill's monitoring well
network in 2017. Since that time and following approval from the NCDEQ, DWM, SWS, the
County has collected groundwater samples from just beneath the southern ditch to monitor the
extent of benzene contamination at the facility. This ditch serves as the groundwater discharge
location for the Surficial Aquifer at Southern Unit. To date, the County has not detected
benzene in exceedance of the NCAC 02L standard in these samples, which suggests that
benzene contamination above the NCAC 02L groundwater standard does not extend off the
facility property.
Pitt County is also currently assessing the Southern Landfill Unit for exceedances of the NCAC
02L standard for 1,4-dioxane. In May 2018, the NCDEQ DWM SWS directed all North Carolina
landfills to begin testing for 1,4-dioxane as part of their routine groundwater monitoring. 1,4-
Dioxane is used primarily as a chlorinated solvent stabilizer, but it can also be found in paint

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 4 of 12
strippers, varnishes, waxes, and a variety of consumer products (US EPA, 2014). 1,4-Dioxane is
fully miscible in water, and it migrates readily with groundwater. This compound is short-lived
in the atmosphere, but it does not volatilize rapidly from water.
1,4-Dioxane was detected at the landfill in July 2019, and the County immediately and
voluntarily chose to perform an updated potential receptor investigation to determine if any
water -supply wells might be at risk. Pitt County opted to conduct the potential receptor survey
as a proactive measure in the interest of public health. The updated potential receptor survey,
conducted by GMA in September 2018, did not identify any well being used as a drinking water
source within 2,000 feet of the facility (GMA, 2018).
Exceedances of the NCAC 02L groundwater standard for 1,4-dioxane were confirmed at the
Southern Unit of the Pitt County Landfill in January 2019. GMA suspects that the detection of
1,4-dioxane in monitoring wells adjacent to the Southern Landfill Unit relates to degradation of
the integrity of one or both landfill caps and the stormwater drainage systems designed to
quickly shunt surface water off the landfill mounds. Pitt County emplaced the clay caps above
the Landfill in the mid-1990s. Over time, erosion of the cap, as well as cracking due to
heating/cooling, desiccation, and/or subsidence due to decomposition of fill material, can
increase the permeability of this type of barrier. Cap degradation may allow infiltration of water
that can leach contaminants downward into the underlying groundwater. Eliminating infiltration
of water through the cap, and ensuring that the stormwater conveyance system operates as
designed, are primary goals for reducing, or eliminating, the release of additional contaminants
into the groundwater.
GMA, on behalf of the County, submitted a proposal to the SWS on June 21, 2019 to further
assess and address 1,4-dioxane contamination at the landfill. Specifically, we proposed to:
1) Delineate the vertical and horizontal extents of 1,4-dioxane by installing two additional
groundwater monitoring wells (one Type II monitoring well located between the two landfill
units and one double -cased, deep Type III monitoring well south of the Southern Mound)
and six surface water staff gauges.
2) Conduct a pilot study to document, and establish the effectiveness of, cap upgrades and
repairs to limit the infiltration of rainwater into the soil cap, and to evaluate if the repairs
have reduced leachate volumes and contaminant concentrations. During the pilot study,
the County proposed to:
a) conduct geophysical testing of the Southern Unit to evaluate landfill cap integrity,
b) repair any areas of concern identified by the geophysical testing,
c) inspect surface water drainage structures on the mound to ensure that they are
operating as designed, and then

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 5 of 12
d) repeat geophysical testing after cap repairs are made to document the results of the
cap repairs.
3) Install two in -stream piezometers approximately 1.5 feet below the ditch bottom at the
locations of the currently collected porewater samples. The in -stream piezometers will be
used to collect representative groundwater samples, measure groundwater levels, and
determine any discharge relationships at repeatable locations just below the stream bed.
The NCDEQ-SWS approved the proposed activities on June 26, 2019 (Appendix A), and the
County immediately began to implement the pilot study. We provide an update regarding the
status of the approved activities in Section 1.3.1 below.
1.3.1 1,4-Dioxane Assessment and Pilot Study Update
North Carolina Administrative Code 15A NCAC 13B .1634 requires the County to characterize
the nature and extent of any release. The County began assessing the horizontal extent of 1,4-
dioxane during the January 2019 monitoring event by voluntarily sampling additional wells that
were no longer part of the groundwater monitoring program.
In June of 2019, the County installed the two monitoring wells and the six surface water staff
gauges described in GMA's Pilot Study proposal in June of 2019. A single -cased (Type -II)
monitoring well was installed between the Northern and Southern mounds, just north of well
P16R (Figure 1). This well, designated as well P29, is hydrologically separated from well P16R
by two drainage ditches along the railroad, and the well is screened from 7 to 12 feet below the
land surface. A 60-foot-deep, double -cased (telescoping, Type -III) groundwater monitoring
well was installed on the south side of the Southern Unit, just off the toe of the slope of the
Southern Mound (Figure 1). This well, designated as well P20D, allowed the County to further
assess the vertical extent of 1,4-dioxane at the Southern Unit. The outer casing of P20D
extends to 45 feet below land surface, and the well is screened from 50 to 60 feet below land
surface.
In accordance with the June 26, 2019 Pilot Plan approval from the NCDEQ-SWS, in August
2019, GMA also installed two shallow, in -stream piezometers (PZ1 and PZ2) below the ditch
bottom along the southern property boundary near the locations of the historically collected
porewater samples (Figure 1). Each piezometer has a 9-inch long screen set 21 inches below
the ditch bottom. The County uses the instream piezometers to collect representative
groundwater samples to monitor benzene migration and to evaluate groundwater discharge
relationships to the ditch.
To evaluate the integrity of the Southern Landfill Unit cap, and to provide a baseline from which
to evaluate hydrologic improvements following cap upgrades and repairs, Geo Solutions
Limited, Inc. completed electromagnetic (EM) and ground -penetrating radar (GPR) surveys of

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 6 of 12
the Southern Landfill Unit on June 2611, July ist and July 2"d 2019 (GMA, 2019). The EM survey
identified a couple of areas of elevated apparent conductivity that may correspond to leachate
moving away from the landfill. Additionally, the EM survey indicated that solid waste appears to
extend beyond the toe of the slope to the edge of the gravel road in the proximity of monitoring
wells MW6R, P16R, and P20R. This finding was consistent with GMA's observations of trash
during the installation of well P20D. The GPR survey identified several areas that have only a
thin landfill cap that was completely eroded away in some locations. The identified areas
include the northwestern upper slope of the mound, the western narrow berm, and the
southern toe north of monitoring wells P28 and P19. The GPR results indicate that the current
impermeable cap thickness at the Southern Landfill is, on average, 10 inches and ranges from 0
to 30 inches. Full details of the geophysical evaluation can be found in Geo Solutions' report,
which was provided as Appendix F of the July 2019 monitoring report from GMA (GMA, 2019).
After completion of the geophysical survey, the County contracted with an engineering firm
(The Wooten Company) to design cap repairs and stormwater upgrades that will eliminate or
greatly reduce the infiltration of precipitation into the Southern Unit. The County provided the
geophysical report to Wooten to aid their design of cap repairs and stormwater upgrades for
the facility. Wooten resurveyed the Southern Landfill Unit in early 2020, and in June 2020,
Wooten submitted a final design to the County. This design included repairing the cap on the
western end of the Southern Landfill, regrading multiple areas to eliminate ponding on the
mound, restoring the stormwater conveyance system to operate as originally designed, and
adding new drainage pipes to the southwest corner of the mound. The County chose to make
these substantial upgrades to protect the groundwater from further contamination via leaching
from landfill waste.
Construction activities commenced at the site on November 4, 2020. The County's contractor
originally anticipated completing the work by March 2021, but the project experienced
significant weather -related delays due to long periods of high rainfall from December 2020
through February 2021 (NCSCO, 2021). Construction was completed in June of 2021. As -built
drawings for the Southern Unit cap repair and stormwater upgrades are provided in Appendix A.
The County continues to monitor both the Northern and Southern Landfill Units on their
approved schedules (semi-annually for the Southern and annually for the Northern). The
January 2021 monitoring event occurred during active construction at the Southern Unit.
2.0 JANUARY 2021 SEMI-ANNUAL MONITORING EVENT
GMA performed the semi-annual monitoring event at the Southern Unit on January 13 to 14,
2021. Sampling procedures and analytical methods complied with the approved Water Quality

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 7 of 12
Monitoring Plan dated September 8, 1994, and subsequent groundwater policy memos issued
by the NCDEQ-SWS (Appendix A).
Twenty-six groundwater -monitoring wells and two temporary groundwater piezometers
comprise the groundwater -monitoring network for the entire landfill facility (Figure 1, Table 1).
The water -quality monitoring network used for the January 2021 semi-annual monitoring of the
Southern Unit consisted of two background monitoring wells (P4 and MW1R), five shallow'
wells located around the Southern Mound (P12, P16R, P20R, P28, and MW6R), a 'deep' well
located south of the Southern mound (P20D), a well located between the Northern and
Southern Landfill Unit (P29), a hydraulically-upgradient surface water sample location (SW1),
and a hydraulically-downgradient surface water sample location (SW2) (Figure 2).
2.1 Groundwater Hydrology
GMA measured static water levels in all monitoring wells and temporary piezometers (Table 2)
and at all 13 staff gauges (Table 3) on January 13, 2021. Depth to groundwater in monitoring
wells at the site ranged from approximately 0.47 to 12.13 feet below the land surface.
Estimates of groundwater velocity (Table 4) ranged from approximately 0.001 to 0.024
feet/day, or 0.38 to 8.78 feet/year. These represent relatively slow groundwater velocities.
An equipotential map prepared using these water -level measurements (Figure 3) shows that the
horizontal component of groundwater flow at the Southern Unit was generally directed to the
south and southeast. A portion of the Northern Landfill Unit lies hydraulically upgradient of the
Southern Unit, but the highest groundwater levels at the facility are located offsite, just
northwest of the landfill boundary near the Pitt County Solid Waste and Recycling site on
Stantonsburg Road. Groundwater samples collected and analyzed from wells in this offsite area
represent background groundwater chemistry.
The groundwater elevation at instream piezometer PZ1 was slightly higher than the surface
water elevation during the January 2021 monitoring event (Tables 2 and 3). The groundwater
elevation at instream piezometer PZ2, however, was slightly lower than the surface water
elevation. During the January 2021 event, GMA observed a beaver dam just upstream of PZ2
that was partially breached, and impounded water from behind the dam was flowing into the
southern property boundary ditch (Figure 3). The influx of water from the beaver
impoundment caused a higher head in the ditch than in the groundwater beneath the ditch
immediately downstream of the breach. As a result, the ditch was losing water to the
groundwater system (i.e., acting as a groundwater recharge feature) in this area. The water
level measurements collected further downstream, at PZ1, indicate that in this area
groundwater was discharging to the southern boundary ditch, consistent with historic
observations of groundwater and surface water interactions at this location.

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 8 of 12
2.2 Sample Collection and Analyses
For monitoring of the Southern Unit, GMA analyzed water samples collected from twelve
monitoring wells, two temporary piezometers, and two surface water sampling locations as
shown on Figure 2. During sampling, GMA collected field water -quality parameters to
document adequate purging prior to sample collection and to aid in evaluating groundwater
chemistry at the site (Table 5). We provide a copy of the well sampling record in Appendix C.
Sampling procedures and analytical methods complied with the approved Water Quality
Monitoring Plan dated September 8, 1994, and subsequent directives issued by the SWS
(Appendix A).
GMA transferred all samples to Environmental Conservation Laboratories, Inc. (ENCO) in ice -
filled coolers under chain -of -custody protocol for analysis of Appendix I parameters and 1,4-
dioxane (Table 6). Copies of the chain -of -custody forms and analytical reports are provided in
Appendix C. Consistent with the May 29, 2018 NCDEQ-SWS memo, ENCO analyzed the
samples using EPA -approved analytical methods sufficiently sensitive to detect the presence of
regulated constituents at or below the applicable standard (unless no such method currently
exists, e.g. for vinyl chloride analysis).
2.3 Analytical Results and Discussion
Twenty-seven parameters (acetone, arsenic, barium, benzene, beryllium, cadmium, carbon
disulfide, chlorobenzene, chromium, cis-1,2-dichloroethene, cobalt, copper, 1,4-
dichlorobenzene, 1,1-dichloroethene, 1,4-dioxane, ethylbenzene, 2-hexanone, lead, m,p-
xylenes, nickel, o-xylene, selenium, thallium, vanadium, vinyl chloride, xylene, and zinc) were
detected at concentrations above their method detection limits during the January 2021
sampling event (Table 7). Seven of those constituents (arsenic, barium, benzene, chromium,
1,4-dioxane, lead, and vinyl chloride) were detected at concentrations exceeding the NCAC 02L
standard, and four parameters (beryllium, cobalt, thallium, and vanadium) were detected at
concentrations above their Interim Maximum Allowable Concentration (IMAC) during this
monitoring event (Table 7).
Zinc, carbon disulfide, and 2-hexanone were detected in the equipment blank. GMA believes
that zinc concentrations are related to residual powder from the manufacturing process used to
produce the powder -free' nitrile gloves that we used during sampling. Nitrile gloves are also
the likely source of the carbon disulfide detected in the equipment blank (USGS, 2012). GMA is
unsure of the source of 2-hexanone in the equipment blank. The lab did not detect 2-hexanone
in any other sample from the January 2021 event.
Samples from wells P19 and P29 contained benzene (4.0 µg/L and 1.6 µg/L, respectively) above
the 1.0 µg/L NCAC 02L groundwater standard. Importantly, benzene was not detected in either

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 9 of 12
in -stream piezometer samples (PZ1 and PZ2). Therefore, there continues to be no evidence
that benzene is migrating off of the landfill property at this time.
1,4-Dioxane was detected in wells MW6R, P16R, P17, P19, P29 and PZ2 (6.5 µg/L, 78 µg/L, 5.0
µg/L, 160 µg/L, 140 µg/L, and 3.6 µg/L, respectively) at concentrations exceeding the NCAC
02L groundwater standard of 3 µg/L. The detection of 1,4-dioxane in well P29 located between
the two landfill units indicates that 1,4-dioxane may be leaching from both the Southern and
Northern mounds. 1,4-Dioxane was also detected in the down -gradient surface water sample,
SW2, but the concentration was below the NCAC 02B and NCAC 02L standards. Importantly,
the lab did not detect 1,4-dioxane in the sample collected from the "deep" down -gradient
monitoring well, P20D.
Samples from wells MW6R, P16R, P19, and P29 contained concentrations of barium (2120 µg/L,
1100 µg/L, 1870 µg/L, and 1290 µg/L respectively) above the NCAC 02L standard of 700 µg/L.
Barium occurs naturally in the native soils at the Pitt County Landfill as evidenced by the
ubiquitous occurrence of this alkaline metal in all samples collected at the site, including those
located in up -gradient off -site areas. GMA has previously demonstrated that barium is often a
constituent of the particulate matter in many of the groundwater samples collected at the Pitt
County Landfill and that dissolved barium concentrations do not exceed the NCAC 02L standard
in some locations (GMA, 2011 and 2015). Despite the apparent natural occurrence of barium at
this site, the concentrations of barium detected in wells MW6R and P19 are unlikely to be solely
attributable to natural sources.
Upgradient surface water sample SW1 contained a concentration of only cobalt above the 15A
NCAC 02B surface -water standards. In recent years, multiple metals have exceeded the
standards at this location (e.g. 7 parameters above the 2B standards in July 2019, GMA 2020).
Metal exceedances at this upgradient surface -water sample location corresponded with highway
construction on the adjoining parcel directly next to the SW1 sampling location. Per the NC
DOT website, construction on the bypass started in August 2016 and was completed in
November of 2019 (NC DOT, 2019). The lab did not detect any of the target parameters above
the 2B surface -water standards in the down -gradient samples for the Southern Unit (SW2).
3.0 WELL REHABILITATION AND MAINTENANCE
Over recent years GMA has noticed an increased frequency of monitoring wells bailing dry (i.e.
water is removed from the well during the purging process faster than water from the formation
can enter the well). Additionally, many of the wells at the Pitt County Landfill remain turbid
after purging, which increases the concentrations of metals in the samples. GMA believes that
many of these monitoring wells, which were installed in the 1990s, are likely affected by a

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 10 of 12
combination of scale and biological plugging. To extend the life of these monitoring wells, and
to provide representative groundwater samples, Pitt County opted to perform physical well
rehabilitation via surging and pumping all monitoring wells at the facility.
On June 16 and 17, 2021, GMA redeveloped all shallow monitoring wells using a high flow
Waterra° brand inertial foot valve. The foot valve was attached to HDPE tubing, inserted into
the well, and oscillated (pulled up and pushed down) over a short vertical distance. This action
pumps water out of the well while simultaneously surging the well. During the procedure, GMA
monitored for temperature, pH, specific conductance, and turbidity (Appendix Q. GMA also
measured the total well depth before and after the well redevelopment procedure. GMA
removed as much as 0.33 feet of sediment from the bottom of the wells. The effect of these
well redevelopment procedures will be determined after the next monitoring event.
4.0 CONCLUSIONS AND FUTURE WORK
1,4-Dioxane, barium, and benzene were detected at concentrations exceeding the NCAC 02L
groundwater standards at multiple locations during the January 2021 monitoring event.
However, these constituents were not detected at concentrations above state standards in
groundwater samples collected from just below the southern property ditch, which acts as a
local groundwater discharge feature, or in downgradient surface -water samples. These results
suggest that these 1,4-dioxane, benzene, and concentrations in excess of naturally occurring
barium are not migrating off -site at this time. Further, neither 1,4-dioxane nor benzene were
detected in the sample collected from the deep monitoring well located down -gradient of the
Southern Landfill Unit (P20D). Barium was detected in this well, but the concentration (112
ug/L) was well below the NCAC 02L standard and below concentrations detected in upgradient,
off -site monitoring wells. The absence of these target compounds indicates that 1,4-dioxane,
benzene, and non-native barium have not migrated out of the Surficial/Yorktown Aquifer at the
site.
To protect the groundwater from further contamination via leaching from landfill waste, Pitt
County has made extensive landfill cap repairs and stormwater upgrades that will eliminate or
greatly reduce the infiltration of precipitation into the Southern Landfill Unit. Repairs at the
Southern Unit were recently completed in June of 2021. Final as -built drawings of the facility
following repairs are provided in Appendix E. The upgrades to the facility included repairing the
cap on the western end of the Southern Landfill, regrading multiple areas to eliminate ponding
on the mound, restoring the stormwater conveyance system to operate as originally designed,
and adding new drainage pipes around the mound.

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 11 of 12
The County continues to monitor groundwater at the Southern Unit on a semi-annual schedule.
The results of a semi-annual monitoring conducted in July of 2021 will be presented in a
subsequent report. The next semi-annual monitoring event at the Pitt County Solid Waste
Municipal Landfill is scheduled for January of 2022. The sampling network will continue to
include wells P19, P20D, and P29 and the two in -stream piezometers. GMA will also continue to
document water levels at all staff gauges that were installed during July of 2019.
Now that construction at the Southern Unit is complete, the County will initiate a pilot study to
establish the effectiveness of cap and stormwater system upgrades and repairs at reducing
groundwater contaminant concentrations and preventing further degradation of groundwater
quality. As part of this assessment, the County will repeat the geophysical surveying completed
in 2019 to evaluate hydrologic improvements following the repairs.
5.0 REPORT CERTIFICATION
This report was prepared by Groundwater Management Associates, Inc. (GMA), a professional
corporation licensed to practice geology (#C-121) and engineering (#C-0854) in North Carolina.
I, Emma H. Shipley, a North Carolina Licensed Geologist for GMA, do certify that the
information contained in this repo,r�:is correct and accurate to the best of my knowledge.
'1 M�
y
Emma H. Shipley, P.G.
Project Hydrogeologist
6.0 REFERENCES
.IQO;'y.,
O/
z e ;' SEAL ,: r
m =eta 23690 W
� .'CFQLOC���, 40
Groundwater Management Associates, Inc., 1994, Water Quality Monitoring Plan for the Active
Southern Unit of the Pitt County Landfill, 71 pages.
Groundwater Management Associates, Inc., 2011, Alternative Source Demonstration Report, Pitt
County Solid Waste Municipal Landfill, Greenville, Pitt County, 8 pages.
Groundwater Management Associates, Inc., 2015, January 2015 Semi -Annual Water Quality
Monitoring Event, Greenville, Pitt County, 147 pages.
Groundwater Management Associates, Inc., 2018, Potential Receptor Survey: Northern and
Southern Units of the Pitt County Landfill, Greenville, Pitt County, 14 pages.

January 2021 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
August 26, 2021
Page 12 of 12
Groundwater Management Associates, Inc., 2019, January 2019 Semi -Annual Water Quality
Monitoring Event and Pilot Study Update, Greenville, Pitt County, 201 pages.
Groundwater Management Associates, Inc. and McGill and Associates, 2001, Water Resources
Management Plan, Pitt County, North Carolina.
Horton, J.W. and V.A. Zullo, 1991, The Geology of the Carolinas: Carolina Geological Society
Fiftieth Anniversary Volume, 406 pp.
NC DOT, 2019, Southwest Bypass Opens to Traffic ahead of Schedule,
https://www. ncdot.gov/news/press-releases/Pages/2019/2019-11-21-pitt-count
southwest-bypass-opens.aspx, accessed December 4, 2019.
NCSCO, 2021, North Carolina State Climate Office, Winter Recap 2020-21: La Nina Lays Low in
a Persistent Wet Winter, https://climate.ncsu.edu/blog/2021/03/winter-recap-2020-21-la-
nina-lays-low-in-a-persistent-wet-winter/, accessed July, 20, 2021.
USEPA, 2014, Technical Fact Sheet — 1,4-Dioxane, Office of Solid Waste and Emergency
Response, EPA 505-F-14-011, 8 pages.
USGS, 2012, Program Evaluation of Volatile Organic Compound (VOC) Blank Data and
Application of Study Reporting Levels to Groundwater Data Collected for the California
GAMA Priority Basin Project, May 2004 through September 2010. Scientific
Investigations Report 2012-5139, 106 pages.
Winner, M.D. and R.W. Coble, 1996, Hydrogeologic Framework of the North Carolina Coastal
Plain, USGS Professional Paper 1404-I, 119 pages.

FIGURES

y� r
_m: r'
r
i
ga P21
P16R
P11R''
.;� SOUTHERN UNIT
P19 MW6R`� .. .
ry .I P1r7 P28
4.
`e t SG6 o..
P12
SG8 P20R PZ1
P8
SG7 PZ2
SG2
THIS A NOT INTENDED
IS FOR GENERAL REFERENCEONURPoG P ONIFY RPOSESD SHOULD NOT BE USED, f
AND Is NOT INTENOEO FOR, SURVEYOR ENGINEERING PURPOSES. LOCATIONS ARE APPROXIMATE. �~
GIs sOURGE DATA:
ORTHOIMAGERYOBTAINED FROM NG ONEMAP, IMAGE DATE: FEBRUARY 2020
PARCEL BOUNDARIES FROM PITT COUNTY GIS, http, l/map-pittcc. pp-d.ta.arcgis.wm
LEGEND
G SURFACE WATER SAMPLE TEMPORARY PIEZOMETER DITCHES SCALE IN FEET GMA
STAFF GAUGE )K ABANDONED / LOST WELL 0 00'
`
MONITORING WELL APPROXIMATE PARCEL BOUNDARIES GNOUN DINATE A MANAGEM F NIT A SSO[IAT ES, INC_
File: DRAWINGS/25101 SITE LAYOUTAND EXISTING MONITORING NETWORK DATE: 3/17/2021
FIG 1
PROJECT 25101 PITT COUNTY LANDFILL, GREENVILLE, PITT CO., NC FIGURE 1

_
r'
r
4.
r
'SW1•
MW1R
NORTHERN UNIT
ZIA
_
-
IF 0
1� q
q P11R
SOUTHERN UNIT
"�
�
r
P19 MW6R
4 ,
P1r7 P28
P12
P20R
�.m
PZ1
-
PZ2
SW2
THIS PRODUCT IS FOR GENERAL REFERENCE PURPOSES ONLY AND SHOULD NOT BE USED,
AND IS NOT INTENDED FOR, SURVEYOR ENGINEERING PURPOSES. LOCATIONSAREAPPROXIMATE.
GIS SOUDATA:
SOURCE
GORCEERV OBTAINED FROM NO ONE MAP, IMAGE DATE'. FEB RUARV 2020
PARCEL BOUNDARIES F ROM PITT COUNTY GIS, hFp1 f map-pihnc
F;
SIG2
-
LEGEND-® SURFACE WATER SAMPLE
TEMPORARY PIEZOMETER
DITCHES
SCALE IN FEET
MONITORING WELL
APPROXIMATE PARCEL BOUNDARIES
0 `00'
-
GIIOII .TEE MANAGEMENT ASSOCIATES, INC-
File: DRAWINGS/25101
GROUNDWATER AND SURFACE WATER SAMPLING
LOCATIONS - SOUTHERN UNIT
DATE: 7/9/2021
FIG 1
PROJECT 25101
PITT COUNTY LANDFILL, GREENVILLE, PITT CO., NC
FIGURE 2

THIS PRODUCT IS FOR GENERAL REFERENCE PURPOSES ONLY AND SHOULD NOT BE USED,
AND IS NOT INTENDED FOR, SURVEY OR ENGINEERING PURPOSES. LOCATIONS ARE APPROXIMATE.
GIS SOURCE DATA:
TOPOGRAPHIC CONTOURS OBTAINED FROM NC ONEMAP,
PARCEL BOUNDARIES FROM PITT COUNTY GIS, https://map-pittnc.opendata.arcgis.com
SG10
80.58
:c
I
D
Jco
—
81< F.
R1
P11R
79.29 .s�
79.E
80 �.
u
" �81
P
_ _
!1 19,�
P11 "� $��77.81 '
--� 76.62
78 1'/ 8� �,� P20D1
=MUNN(75.43) o
�P20R,
P1275.'89
77.29' 1.100' SG8
7776 SG7--- ^ ` 72.80 �'PZ2 '
73.33 73 72.45 Z�
75 74 (surface water)
Approximate
location of
beaver dam
(water elevation >2 ft higher)
"r
I .oSG5'
75.540401 P21
`80 �
1
W� 7�1
-8�0_
MW7M�779,8
P26 —
79257
8�p�7W6
. I
74.95
75
J .���♦ 76
'MW3�kZ7
M 4 (76.58)* 78
SG9 '
(75.32) '� p07
X P09� �80; 7,7.03
1
• . ` 76.04
o P23 80�
76.02 �.
MW6R II ` . MW5
■ 7,5:25 SG 3 Ns,' cow
19
�P24` 0SO# ;PO %
71
PZ1 `X 74
72 71.95 P08 Q,
CID
(surface water) 73.09
73
CO SG2 7172
70.47
GENERAL NOTES:
' �P-020W77
78. 33
1
1. TOPOGRAPHIC CONTOUR INTERVAL = 2.0 FEET
2. GROUNDWATER CONTOUR INTERVAL = 1.0 FOOT
3. ARROW INDICATES DIRECTION OF GROUNDWATER FLOW
4. WATER LEVEL ELEVATIONS ARE POSTED BY EACH WELL
5. ( ) INDICATES DATA NOT USED FOR CONTOURING
- LEGEND -
MONITORING WELL
UNMEASURED MONITORING WELL
ABANDONED MONITORING WELL
PROPERTY LINE
�--��
RAILROAD TRACKS
TOPOGRAPHIC CONTOUR
—
POND
GROUNDWATER ELEVATION
CONTOUR
INDICATES DIRECTION OF
GROUNDWATER FLOW
77.31
WATER LEVEL
(FEET ABOVE SEA LEVEL)
----
DITCH
L
STAFF GAUGE
FIGURE 3
DATE 6/3/2021 PROJECT: 25101
DRW BY: AWC CHK BY: EHS
SCALE IN FEET
0 350 700'
1" = 350'
EQUIPOTENTIAL MAP
JAN UARY 13, 2021
A
GMA
= =�-
GROUNDWATER MANAGEMENT ASSOCIATES, INC.

TABLES

Table 1. Monitoring Well Construction and Elevations
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Number,
Easting
(feet)*
Northing
=
fC = J=
U O V)
w a
Q>
o
W
U
�
J
7 O W
An a
>
- Ol
y=
3�a
o=
�
O U
+, V1 U)
wJ
a.
e
G o
O O
EJ
E
o o
a CO
= V J
O V) V)
'wa
aaWell
..
o
W
V1
e
= O J
O V)
++ Ea
0,2
W CO
MW1R
2463487.26
676793.08
85.48
82.5
52.98
40.0
50.0
42.5
32.5
MW3
2467253.81
676198.15
82.97
80.5
47.47
35.0
45.0
45.5
35.5
MW4
2466875.66
676066.89
83.58
81.9
21.68
10.0
20.0
71.9
61.9
MW6R
2465083.71
675392.21
80.94
78.15
19.79
7.0
17.0
71.15
61.15
MW8
2464639.20
676915.58
84.41
81.62
16.79
4.0
14.0
77.62
67.62
MW8D
2464553.05
676827.15
84.28
81.37
30.91
18.0
28.0
63.37
53.37
P02
2467254.11
676191.82
84.65
80.6
19.05
11.0
15.0
69.6
65.6
PO4
2463438.60
676616.81
85.02
81.5
21.52
8.0
18.0
73.5
63.5
POs
2463490.61
676797.65
85.94
82.3
17.14
8.5
13.5
73.8
68.8
P06
2463171.35
676568.01
84.72
81.5
17.72
8.5
14.5
73
67
P07
2466875.67
676056.22
85.41
81.9
19.51
11.0
16.0
70.9
65.9
P08
2466074.39
674918.18
85.22
81.4
20.3
9.0
17.0
72.4
64.4
P09
2466189.91
675932.77
84.08
80.1
18.48
9.5
14.5
70.6
65.6
P11R
2463141.14
675651.83
86.04
82.3
19.74
13.0
16.0
69.3
66.3
P12
2463126.32
675048.53
79.31
75.9
20.91
10.5
17.5
65.4
58.4
P13
2466105.04
676161.21
85.8
82
19.8
11.0
16.0
71
66
P13D
2466119.99
676174.03
84.67
81.2
54.97
47.5
51.5
33.7
29.7
Pis
2465472.37
676703.00
87.90
84.25
20.71
4.0
17.0
80.25
67.25
P16R
2464194.10
675837.67
87.44
84.3
17.14
11.0
14.0
73.3
70.3
P17
2463319.94
675286.12
80.38
76.3
15.08
8.0
11.0
68.3
65.3
P19
2463898.87
675403.02
83.9
78.5
18.4
9.0
13.0
69.5
65.5
P20R
2464435.49
675068.13
85.21
81.7
33.51
10.0
30.0
71.7
51.7
P20D
2464583.16
675103.79
84.52
81.5
63.02
50.0
60.0
31.5
21.5
P21
2465286.45
675904.93
82.07
77.8
15.27
8.0
11.0
69.8
66.8
P23
2465657.48
675745.22
82.93
79.4
19.53
11.0
16.0
68.4
63.4
P26
2466246.80
676940.21
84.59
82.2
16.39
9.0
14.0
73.2
68.2
P28
2463542.16
675278.55
77.74
74.8
10.94
3.5
8.0
71.3
66.8
P29
2464558.30
676041.26
85.36
82.4
14.96
7.0
12.0
75.4
70.4
PZ1
2464848.16
675165.00
72.44
70.8
3.39
1.0
1.8
69.8
69.1
PZ2
2464485.95
675009.74
72.89
71.2
3.44
1.0
1.8
70.2
69.5
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid
(NCGS) control based on ties to NCGS Monument 'RUTH' and NCGS Monuments 'MARY'. Horizontal data referenced
to NAD 83(2011). Vertical data referenced to NGVD 29.
BLS = below land surface ASL = above sea level LS = land surface

Table 2. Monitoring Well Water Levels and Sample Purge Volumes
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Date
Elevation
of Top of
Casing
(feet ASL)
Land
Surface
Elevation*
(feet ASL)
Total Well
Depth
below LS
(feet)
Depth to
Water
(feet)
Elevation
of Water
(feet ASL)
Height of
Water in
Well
(feet)
Three
Well
Volumes
(gallons)
Amount
Purged
(gallons)
Number of
Well
Volumes
Purged
Purged to
Dryness?
MW1R
1/13/21
85.48
82.50
50.0
6.54
78.94
46.4
22.6
22.6
3.0
no
MW3
1/13/21
82.97
80.50
45.0
6.39
76.58
41.1
20.0
20.0
3.0
no
MW4
1/13/21
83.58
81.90
20.0
6.34
77.24
not sampled
MW6R
1/13/21
80.94
78.15
17.0
5.69
75.25
14.1
7.1
7.1
3.0
no
MW8
1/13/21
84.41
81.62
14.0
4.83
79.58
12.0
5.8
5.8
3.0
no
MW8D
1/31/21
84.28
81.37
28.0
5.29
78.99
not sampled
P02
1/13/21
84.65
80.60
15.0
6.32
78.33
12.7
6.2
6.2
3.0
no
PO4
1/13/21
85.02
81.50
18.0
4.23
80.79
17.3
8.4
8.4
3.0
no
P05
1/13/21
85.94
82.30
13.5
4.51
81.43
12.6
6.1
5.4
2.7
yes
P06
1/13/21
84.72
81.50
14.5
3.93
1 80.79
13.8
6.7
5.7
2.6
yes
P07
1/13/21
85.41
81.90
16.0
8.38
77.03
11.1
5.4
1 4.1
1 2.3
1 yes
P08
1/13/21
85.22
81.40
17.0
12.13
73.09
not sampled
P09
1/13/21
84.08
80.10
14.5
6.70
77.38
11.8
5.7
4.9
2.6
yes
P11R
1/13/21
86.04
82.30
16.0
6.75
79.29
13.0
6.3
3.2
1.5
yes
P12
1/13/21
79.31
75.90
17.5
2.02
77.29
18.9
9.2
4.9
1.6
yes
P13
1/13/21
85.80
82.00
16.0
7.78
78.02
12.0
5.8
5.8
3.0
no
P13D
1/13/21
84.67
81.20
51.5
8.44
76.23
46.5
22.6
22.6
3.0
no
P15
1/13/21
87.90
84.25
17.0
8.82
79.08
not sampled
P16R
1/13/21
87.44
84.30
14.0
8.89
78.55
8.3
4.0
4.1
3.1
yes
P17
1/13/21
80.38
76.30
11.0
3.76
76.62
11.3
5.5
3.2
1.7
yes
P19
1/13/21
83.90
78.50
13.0
6.09
77.81
12.3
6.0
4.1
2.1
yes
P20R
1/13/21
85.21
81.70
30.0
9.32
75.89
24.2
11.3
11.3
3.0
no
P20D
1/13/21
84.52
81.50
60.0
9.09
75.43
53.9
1 26.2
26.2
1 3.0
no
P21
1/13/21
82.07
77.80
11.0
6.03
76.04
9.2
4.5
3.0
2.0
yes
P23
1/13/21
82.93
79.40
16.0
6.91
76.02
12.6
6.1
6.2
3.0
yes
P26
1/13/21
84.59
82.20
14.0
5.07
79.52
not sampled
P28
1/13/21
77.74
74.80
8.0
2.99
74.75
1 8.0
3.8
3.5
2.7
yes
P29
1/13/21
85.36
82.40
12.0
5.99
79.37
9.0
4.4
4.4
3.0
no
PZ1
1/13/21
72.44
70.80
1.8
0.47
71.97
a grab surface water sample was collected at this location
PZ2
1/13/21
72.89
71.20
1.8
0.47
72.42
a grab surface water sample was collected at this location
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid (NCGS) control based on ties to NCGS
MnniimPnf'RIITH' and NC(;S MnniimPntc'MARY'_ Hnri7nnfaI data rPfPrPnrPrl fn NAn R"i ?nii) VPrfiraI data rPfPrPnrPrl fn N(;Vr) ?9_
ASL = Above Sea Level LS = land surface

Table 3. Staff Gauge Elevations and Water Levels
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Staff
Gauge
Date
Easting
(feet)*
Northing
feet *
Reference
Point
Elevation of
Reference
Point
feet ASL
Staff Gauge
Reading or
Depth to Water
Measurement
(ft)
Elevation of
Water
(feet ASL
SG1
1/13/21
2464589.3
676053.46
4-foot mark
81.06
1.22
78.28
SG2
1/13/21
2466082.36
674856.14
4-foot mark
71.68
2.79
70.47
SG3
1/13/21
2464175.98
675874.46
4-foot mark
80.60
1.56
78.16
SG4
1/13/21
2467192.35
676705.36
4-foot mark
76.38
2.57
74.95
SGS
1/13/21
2465262.23
675928.45
3-foot mark
76.88
1.66
75.54
SG6
1/13/21
2465175.63
675356.1
4-foot mark
74.18
0.91
71.09
SG7
1/13/21
2463215.14
675010.08
3-foot mark
75.13
1.20
73.33
SG8
1/13/21
2463932.14
675059.19
3-foot mark
73.91
1.89
72.80
SG9
1/13/21
2466110.5
676143.36
3-foot mark
76.96
1.36
75.32
SG10
1/14/21
2463086.65
676845.47
3-foot mark
82.02
1.56
80.58
SG11
1/13/21
2463169.96
676528.73
3-foot mark
81.47
0.86
79.33
SG12
1/13/21
2463583.11
676511.02
3-foot mark
81.13
1.19
79.32
SG96
1/13/21
2466366.84
676889.34
3-foot mark
77.83
1.20
76.03
PZ1-SW+
1/13/21
2464848.16
675165.00
TOC
72.44
0.49
71.95
PZ2-SW+
1/13/21
2464485.95
675009.74
TOC
72.89
0.44
72.45
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid
(NCGS) control based on ties to NCGS Monument'RUTH' and NCGS Monuments'MARY. Horizontal data referenced
to NAD 83(2011). Vertical data referenced to NGVD 29.
+ Surface water elevations determined by measurinq depth to surface water from top of casinq
ASL = Above Sea Level
TOC = top of casing

Table 4. Calculations of Groundwater Velocity
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Date
Horizontal
Hydraulic
Gradient
(ft/ft)
Hydraulic
Conductivity
(ft/day)
Effective
Porosity
Horizontal
Groundwater
Velocity
(ft/day)
Horizontal
Groundwater
Velocity
(ft/year)
MW6R
1/13/21
0.003
0.50
0.29
0.005
2.00
PO4
1/13/21
0.009
0.50
0.19
0.022
8.21
P12
1/13/21
0.009
0.20
0.43
0.004
1.48
P20R
1/13/21
0.003
0.10
0.32
0.001
0.38
P28
1/13/21
0.014
0.30
0.17
0.024
8.78

Table S. Field -Water Quality Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Sample
Date
pH
Temp-
erature
(degrees
Celsius)
Specific
Conductance
(µS)
Dissolved
oxygen
(mg/L)
Turbidity during
collection of
organic samples
(ntu)
Turbidity during
collection of
metals samples
(ntu)
MW1R
1/14/2021
5.50
15.2
68
1.9
3.0
3.0
MW3
1/14/2021
4.19
18.4
96
15.1
2.8
2.8
1/14/2021
6.75
15.5
2019
0.8
29
--
MW6R
1/14/2021
--
--
--
--
--
14.2
MW8
1/13/2021
5.66
15.6
108
1.6
306
306
P02
1/14/2021
4.75
18.3
53
32.2
34
34
1/13/2021
5.07
15.6
85
4.6
20
20.2
PO4
1/14/2021
--
--
--
--
--
POS
1/14/2021
5.03
15.2
41
2.4
38
38
P06
1/14/2021
5.36
16.1
73
1.65
15
15
P07
1/14/2021
4.17
17.6
173
0.9
20
20
P09
1/14/2021
4.80
17.3
111
2.0
73
73
P1111
1/14/2021
6.10
15.2
79
1.2
364
364
P12
1/14/2021
5.86
14.8
62
3.70
45
44.7
P 13
1/14/2021
5.27
18.1
41
11
34
34.2
P13D
1/14/2021
5.74
18.4
96
0.9
26
26
1/13/2021
6.64
16.2
5205
1.5
115
--
P16R
1/14/2021
--
--
--
--
--
15
P17
1/13/2021
5.88
16.5
228.3
1.8
31
31.10
P19
1/13/2021
3.84
16.3
1459.0
1.3
146
--
1/14/2021
--
--
--
--
--
6
P20R
1/13/2021
5.89
17.5
104
1.7
29
--
1/14/2021
--
--
--
--
--
100.0
P20D
1/14/2021
6.03
17.3
61.3
0.9
70.5
70.5
P21
1/14/2021
7.17
15.7
65
3.2
9
9
1/13/2021
5.72
19.6
59
26.9
59
--
P23
1/14/2021
--
--
--
--
--
9
P28
1/13/2021
5.72
15.0
70
3
269
--
1/14/2021
--
--
--
--
--
133
P29
1/14/2021
4.43
15.1
4732.00
3.4
152
152
SW1
1/14/2021
4.50
9.70
112.40
6.37
29.50
29.50
SW2
1/14/2021
5.79
9.30
169.40
8.22
67.00
67.00
SW4
1/13/2021
5.81
9.00
215.00
7.88
9.23
9.23
PZ1
1/14/2021
5.48
9.80
146.00
16.80
297
297
PZ2
1/14/2021
1 6.30
8.40
676.30
36.50
475
475

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standardsi
DEQ
CAS
2L
IMAC
MCL
Calculated
Number
Name
Other Names
Std.
(Ng�L)
GWP Std
67-64-1
Acetone
2-Propanone
6000
--
--
--
107-13-1
Acrylonitrile
Acrylonitrile
--
--
--
--
7440-36-0
Antimony
Antimony
--
1
6
--
7440-38-2
Arsenic
Arsenic
10
--
10
--
7440-39-3
Barium
Barium
700
--
2000
--
71-43-2
Benzene
Benzene
1
--
5
--
7440-41-7
Beryllium
Beryllium
--
4
4
--
Bromochloromethane;
Methane, bromochloro-
--
--
--
0.6
74-97-5
Chlorobromethane
Bromodichloromethane;
Methane, bromodichloro
0.6
--
80
--
75-27-4
Dichlorobromomethane
Bromoform;
75-25-2
Tribromomethane
Methane, tribromo-
4
--
80
--
7440-43-9
Cadmium
Cadmium
2
--
5
--
75-15-0
Carbon disulfide
Carbon disulfide
700
--
--
--
56-23-5
Carbon tetrachloride
Methane, tetrachloro-
0.3
--
5
--
108-90-7
Chlorobenzene
Benzene, chloro-
50
--
100
--
Chloroethane; Ethyl
Ethane, chloro-
3000
--
--
--
75-00-3
chloride
Chloroform;
67-66-3
Trichloromethane
Methane, trichloro-
70
--
80
--
7440-47-3
Chromium
Chromium
10
--
100
--
7440-48-4
Cobalt
Cobalt
--
1
--
--
7440-50-8
Copper
Copper
1000
--
1300
--
Dibromochloromethane;
124-48-1
Chlorodibromomethane
Methane, dibromochloro
0.4
--
80
--
1,2-Dibromo-3-
Propane, 1,2-dibromo-3-
96-12-8
chloro ro ane; DBCP
chloro-
0.04
--
0.2
--
1,2-Dibromoethane;
106-93-4
Ethylene dibromide; EDB
Ethane, 1,2-dibromo-
0.02
--
0.05
--
o-Dichlorobenzene; 1,2-
95-50-1
Dichlorobenzene
Benzene, 1,2-dichloro-
20
--
600
--
p-Dichlorobenzene; 1,4-
106-46-7
Dichlorobenzene
Benzene, 1,4-dichloro-
6
--
75
--
2-Butene,
110-57-6
trans-1,4-Dichloro-2-butene
E4-dichloro-,
1,1-Dichloroethane;
75-34-3
Eth Ididene chloride
Ethane, 1,1-dichloro-
6
--
--
--

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standardsi
IMAC
DEQ
CAS
2L
(Ng�L)
MCL
Calculated
Number
Name
Other Names
Std.
GWP Std
1,2-Dichloroethene;
Ethane, 1,2-dichloro-
0.4
--
5
--
107-06-2
Ethylene dichloride
1,1-Dichloroethylene; 1,1-
Ethene, 1,1-dichloro-
350
--
7
--
75-35-4
Dichloroethene;
cis-1,2-Dichloroethylene;
Ethene, 1,2-dichloro-,(Z)
70
--
70
--
156-59-2
cis-1,2-Dichloroethene
trans-1,2-Dichloroethylene;
Ethene, 1,2-dichloro-,(E)
100
--
100
--
156-60-5
trans-1,2-Dichloroethene
78-87-5
1,2-Dichloropropane
Propane, 1,2-dichloro-
0.6
--
5
--
cis-1 3-Dichloropropene
1-Propene, 1,3-dichloro-
0.4
--
--
--
10061-01-5
Z -
trans-1 3-Dichloropropene
1-Propene, 1,3-dichloro-
0.4
--
--
--
10061-02-6
E -
100-41-4
Ethylbenzene
Benzene, ethyl-
600
--
700
--
2-Hexanone; Methyl butyl
2-Hexanone
--
40
--
--
591-78-6
ketone
7439-92-1
Lead
Lead
15
--
15
--
Methyl bromide;
Methane, bromo-
--
10
--
--
74-83-9
Bromomethane
Methyl chloride;
Methane, chloro-
3
--
--
--
74-87-3
Chloromethane
Methylene bromide;
Methane, dibromo-
--
70
--
--
74-95-3
Dibromomethane
Methylene chloride;
Methane, dichloro-
5
--
5
--
75-09-2
Dichloromethane
Methyl ethyl ketone; MEK;
2-Butanone
4000
--
--
--
78-93-3
2-Butanone
Methyl iodide;
Methane, iodo-
--
--
--
--
74-88-4
Iodomethane
4-Methyl-2-pentanone;
2-pentanone, 4-methyl-
--
100
--
--
108-10-1
Methyl isobut I ketone
7440-02-0
Nickel
Nickel
100
--
--
--
7782-49-2
Selenium
Selenium
20
--
50
--
7440-22-4
Silver
Silver
20
--
--
--
100-42-5
Styrene
Benzene, ethenyl-
70
--
100
--
1,1,1,2-Tetrachloroethane
Ethane 1112-
_
1
__
630-20-6
tetrachloro�
1,1,2,2-Tetrachloroethane
Ethane 1 1 2 2-
0.2
__
79-34-5
tetrachloro�

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
CAS
2L
IMAC
MCL
Calculated
Number
Name
Other Names
Std.
(Ng�L)
GWP Std
Tetra chIoroethylene;
Tetra ch I oroethen e;
Ethene, tetrachloro-
0.7
--
5
--
127-18-4
Perch loroeth lene
7440-28-0
Thallium
Thallium
--
0.2
2
--
108-88-3
Toluene
Benzene, methyl-
600
--
1000
--
1,1,1-Trichloroethane;
71-55-6
Meth (chloroform
Ethane, 1,1,1-trichloro-
200
--
200
--
Trichloroethylene;
Ethene, trichloro-
3
--
5
--
79-01-6
Trichloroethene
79-00-5
1,1,2-Trichloroethane
Ethane, 1,1,2-trichloro-
--
0.6
5
--
Trichlorofluoromethane;
Methane,trichlorofluoro-
2000
--
--
--
75-69-4
CFC-11
96-18-4
1,2,3-Trichloropropane
Propane, 1,2,3-trichloro-
0.005
--
--
--
7440-62-2
Vanadium
Vanadium
--
3.5
--
--
108-05-4
Vinyl acetate
Acetic acid, ethenylester
--
88
--
--
75-01-4
VIIIYI ullulluu,Ethene,
chloro-
0.03
--
2
--
7440-66-6
Zinc
Zinc
1000
--
--
--
1330-20-7
Xylene (total)
Benzene, dimethyl-
500
--
--
All units are in micrograms per liter (pg/L)
2L STD = 15A NCAC 2L groundwater standard
'Applicable Groundwater Protection Standard is the lower of the listed standards.

Table 7. List of Compounds Detected during the January 2021 Sampling Event (1/13-1/14/2021)
Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well
ID
Date
I
Parameter
Results
(Ng/L)
MDL
(Ng/L)
NC 2L or 213
Std*(Ng/L)
IMAC
(Ng/L)
MCL
(Ng/L)
Groundwater Samples
1/13/2021
2-Hexanone
1.93
0.88
-
40
-
EB
1/13/2021
Carbon Disulfide
53.00
1.5
700
-
-
1/13/2021
Zinc Total
114.00
4.4
1000
-
5000#
FB
1/14/2021
Acetone
141
10
6000
-
-
TB
1/13/2021
Acetone
67
10
6000
-
-
TB
1/13/2021
Acetone
31
10
6000
-
-
1/14/2020
1,4-Dioxane
6.5
0.8
3
-
-
MW6R
1/14/2021
Barium Total
2120
1.1
700
-
2000
1/14/2021
Nickel Total
2.71 J
2.2
100
-
-
1/14/2021
Barium Total
111
1.1
700
-
2000
PO4
1/14/2021
Copper Total
15.6
1.6
1000
-
1300^
1/14/2021
Zinc Total
4.453
4.4
1000
-
5000#
1/14/2021
Barium Total
99.2
1.1
700
-
2000
1/14/2021
Beryllium Total
1.93
0.16
-
4
4
1/14/2021
Cobalt Total
2.383
1.4
-
1
-
P11R
1/14/2021
Copper Total
7.10 J
1.6
1000
-
1300^
1/14/2021
Nickel Total
3.28 J
2.2
100
-
-
1/14/2021
Vanadium Total
4.673
1.4
-
0.3
-
1/14/2021
Zinc Total
39.8
4.4
1000
-
5000#
P12
1/14/2021
Barium Total
34.9
1.1
700
-
2000
1/14/2021
Beryllium Total
0.5533
0.16
-
4
4
1/13/2021
1,4-Dioxane
78 D
1.6
3
-
-
1/13/2021
Acetone
123
10
6000
-
-
1/14/2021
Barium Total
1100
1.1
700
-
2000
P16R
1/13/2021
Benzene
0.863
0.15
1
-
5
1/14/2021
Chromium Total
2.883
1.4
10
-
100
1/14/2021
Nickel Total
16.6
2.2
100
-
-
1/13/2021
1 4-Dioxane
5
0.8
3
-
-
1/13/2021
Barium Total
147
1.10
700
-
2000
1/13/2021
Benzene
0.433
0.15
1
-
5
P17
1/13/2021
Beryllium Total
1.43
0.16
-
4
4
1/13/2021
Chlorobenzene
4.3
0.17
50
-
100
1/13/2021
Copper Total
1.893
1.6
1000
-
1300^
1/13/2021
Nickel Total
2.793
2.2
100
-
-
1/13/2021
1,1-Dichloroethane
4.2
0.13
6
-
7
1/13/2021
1 4-Dichlorobenzene
5.1
0.19
6
-
-
1/13/2021
1 4-Dioxane
160 D
2
3
-
-
1/14/2021
Barium Total
1870
1.10
700
-
2000
1/13/2021
Benzene
4
0.15
1
-
5
1/14/2021
Beryllium Total
15.3
0.16
-
4
4
1/13/2021
Chlorobenzene
7
0.17
50
-
100
1/13/2021
cis-l2-Dichloroethene
2.7
0.15
70
-
70
1/14/2021
Cobalt Total
19.3
1.40
-
1
-
P19
1/14/2021
Copper Total
1.723
1.6
1000
-
1300^
1/13/2021
Eth (benzene
1.8
0.13
600
-
700
1/14/2021
Lead
6.071
3.10
15
-
15
1/13/2021
m -X lenes
0.421
0.17
500
-
-
1/14/2021
Nickel Total
29.4
2.2
100
-
-
1/13/2021
o-X lene
0.563
0.065
500
-
-
1/14/2021
Selenium Total
2.08
1.82
20
-
50
1/14/2021
Vanadium Total
1.46 J
1.4
-
0.3
-
1/13/2021
Vinyl Chloride
0.57 J
0.32
0.03
-
2
1/13/2021
X lenes Total
0.983
0.45
500
-
-
1/14/2021
Zinc Total
120
4.4
1000
-
5000#
1/13/2021
1,4-Dioxane
2.1
0.8
3
-
-
1/14/2021
Barium Total
51.4
1.1
700
-
2000
P20R
1/14/2021
Beryllium Total
1.66
0.16
-
4
4
1/14/2021
Vanadium Total
2.441
1.4
-
0.3
-
1/14/2021
Zinc Total
12.1
4.4
1000
-
5000#

Table 7. List of Compounds Detected during the January 2021 Sampling Event (1/13-1/14/2021)
Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well
ID
Date
Parameter
Results
(Ng/L)
MDL
(Ng/L)
NC 2L or 213
Std*(Ng/L)
IMAC
(Ng/L)
MCL
(Ng/L)
1/14/2021
Barium Total
112
1.1
700
-
2000
1/14/2021
Beryllium Total
8.87
0.16
-
4
4
1/14/2021
Cadmium Total
0.7563
0.36
2
-
5
P20D
1/14/2021
Chromium Total
12.9
1.4
10
-
100
1/14/2021
Lead
5.433
3.10
15
-
15
1/14/2021
Nickel Total
4.31 J
2.2
100
-
-
1/14/2021
Vanadium Total
12.6
1.4
-
0.3
1/14/2021
Zinc Total
20.1
4.4
1000
-
5000#
1/14/2021
Barium Total
38.4
1.1
700
-
2000
1/14/2021
Beryllium Total
0.7413
0.16
-
4
4
P28
1/14/2021
Copper Total
2.491
1.6
1000
-
1300^
1/14/2021
Nickel Total
3.161
2.2
100
-
-
1/14/2021
Vanadium Total
1.53
1.4
-
0.3
-
1/14/2021
Zinc Total
14
4.4
1000
-
5000#
1/14/2021
1,4-Dichlorobenzene
0.89 J
0.19
6
-
-
1/14/2021
1,4-Dioxane
140 D
4
3
-
-
1/14/2021
Barium Total
1290
1.1
700
-
2000
1/14/2021
Benzene Total
1.6
0.15
1
-
5
1/14/2021
Beryllium Total
0.9803
0.16
-
4
4
1/14/2021
Chlorobenzene
5.1
0.17
50
-
100
1/14/2021
Cobalt Total
4.663
1.4
-
1
-
P29
1/14/2021
Ethylbenzene
0.48 J
0.13
600
-
700
1/14/2021
Lead
18
3.1
15
-
15
1/14/2021
Nickel Total
7.503
2.2
100
-
-
1/14/2021
Selenium Total
2.54
1.82
5
-
50
1/14/2021
Thallium Total
0.2523
0.22
-
0.2
2
1/14/2021
Vanadium Total
36.1
1.4
-
0.3
-
1/14/2021
Zinc Total
5.63 J
4.4
1000
-
5000#
1/14/2021
1,4-Dioxane
2.1
0.8
3
-
-
1/14/2021
Arsenic
100
7.6
10
-
10
1/14/2021
Barium Total
101
1.1
700
-
2000
1/14/2021
Cadmium Total
1.72
0.36
2
-
5
pZ1
1/14/2021
Cobalt Total
2.211
1.4
-
1
-
1/14/2021
opper ota
3.41 J
1000
1300
1/14/2021
Lead
-
15
1/14/2021
Nickel Total3.31
J
2.2
100
-
-
1/14/2021
Vanadium Total
12.4
1.4
-
0.3
-
1/14/2021
Zinc Total
26.4
4.4
1000
-
5000#
1/14/2021
1,4-Dioxane
NE3.6
0.8
3
-
-
PZ2
1/14/2021
Barium Total
190
1.1
700
-
2000
1/14/2021
Cadmium Total
0.3603
0.36
2
-
5
1/14/2021
Zinc Total
18.3
4.4
1000
-
5000#
Surface WaterSamp/es
1/14/2021
Barium Total
23.9
1.1
21,000
-
2000
1/14/2021
Beryllium Total
0.212 J
0.16
6.5
-
4
1/14/2021
Cobalt Total
8.023
1.4
4
-
-
SW3
1/14/2021
Lead
3.54 J
3.1
0.54"
-
-
1/14/2021
Nickel Total
3.41 J
2.2
16.10-
-
-
1/14/2021
Vanadium Total
2.153
1.4
-
-
-
1/14/2021
Zinc Total
15.3
4.4
36.5-
-
5000#
1/14/2021
Barium Total
40.3
1.1
21,000
-
2000
SW2
1/14/2021
Chromium Total
1.441
1.4
23.81-
-
-
1/14/2021
Zinc Total
18.8
4.4
36.5"
-
5000#
1/13/2021
1,4-Dioxane
3.5
0.8
80
-
-
SW4
1/13/2021
Barium Total
40
1.1
21,000
-
2000
1/13/2021
Zinc Total
5.971
4.4
365-
-
1 5000#
MDL = Metnoo Detection Limit MCL = reaerai Maximum contaminant Levei
IMAC = Interim Maximum Allowable Concentration
J = The analyte was positively identified, but the value is estimated below the reporting limit.
*15A NCAC 2L groundwater standards are listed for all groundwater sampling locations. 15A NCAC 213 standards are listed for
surface water sampling locations (SWi and SW2).
Value represents an EPA action level.
#Value represents an EPA secondary Maximum Contaminant Level
+NC In -Stream Taraet Value for Surface Waters
"Hardness -dependent metal standard calculated assumina an in -stream hardness of 25 ma/L of CaCO,
Concentrations highlighted in yellow were detected above the 2L (or 2B) standards.
Concentrations highlighted ink were detected above the IMAC.

APPENDIX A
CORRESPONDENCE FROM THE
NC DIVISION OF WASTE MANAGEMENT

NORTH (.4i2oL,TI` A DWI=AR3'MTzjgT Off'
taMMONTi ENT kNb NATURAL Pr--soUACt�S
'DMX'Qr[ on 'ArA�-$-YM M.AXI-1.7,M�ls
Sc:p;cmbar•lU, i��8
Mr. PI* G_ Dickerson
Pitt Co=y Etrfreer
Pitt County Office Bnildipa
1717 Wesst:'Pifth St -,et
G --xvi le, N.C. 27834 .
Re: Sbmiannml Water Quatty SamphgR-4quiremcnts for the YwLberrt
Pardon ofthr, Pbt:Couaty Landtll (PerMif #74-01).
]scar Mckerson,
A-acotding to vor telephone tonvtr4dCoa yesterday I have; atlachcd two
Ie[ters 4b Ri may help 01mil'y the s=ping re juirementa for. the narth=portion
of Ibd closed Pitt County landfla, The 17ecernber 277, 1994 letter- spocites the
sampling points and amiyses. This letter also axplains that the s--Imiarmual
sampg cvent5 for hlhc mort.�era portion of facility can be conduct d - lin
simultaneously with the southern Subtitle D oei to prey-,-nt-dupllcadon of
samples. Subsequent letw have modified the Sequ red an lyticar methods.
The- Apffl 8, 19 97 letter disCSss&s the hzi�W]4on of Eve new -wells to the
mouitari❑g Vs4m io 1) acquire data ot. Both the verb f,, I and horizonW ground.
water -flow, 2) to detzrmke the continuity of the "gray clay'! layer- benbath the
-.,site and 3) establish true upgra Rest monitor sL-Wons for hez northern portion
oft]: Iant1fIl- With the additions to Ih8 monitoring system yho Section did nfft
see 6e 4o t;ifjtiisetall ccring samples a rouLrsc basisftDihatr7u:ziosing
points P-14, P-15, F 25, P-25, MW-2A and MV213 become oftheirproxfmjty to
wasto. Afler the ffiftW da;a was colleoted on the abovo itcMs 1-3, the Section
did not T�qufie samples to be taken from tho two new decacr Qpgmdient wells.
Additionally, MW-2 was abandoned.
EU summary, thO fallowing monitoring pofAts.shauld be: Sbmpled on a
semlatmtral basis for -she northern portion of the I"dE (this is -not meant to
oxcit%.e prctiously app=ovedmonitoring requirerrztmLfor the smithern pordon):
M)V-1, M-W-3. P-1. P-2. P-C P-5, P-A P-7, P-9, F-13, F-I6, P-21, F-23, the -Mo
nevv upgtadient shallow woUs and the now downgradieeL well ncsted with P-I 3.
Prtt-aFproved swxaee waterloeataons should also be sampled. Poteraiometric
data sliaWd. N— collected our all wells at ilre site dur D mclh sampling episode and
-a p aUnflometric map submitted -with each serniaimusl data paa3ag--
401 o�cr.�n+ 79a.a5, ourrC i7t{1. fi rlL�laf71 .1C 3�4C7
A'!1C?!L Et10-7�3•+1ov6 FAX RSn 711-�IIIIS
M1hl E.'sLld L U pr��RiUH1l'1' t Ar^ 1f1 h. �571vc .Surf Pi`11f.�1ryyrrn- L-[}�};, nCCyu Lraf E O'� l.O �ti-La aLlsxiLh PAF•Cll

If to -County desires to tkop-or add moat Wring lioints to the semiaumual sampling -
routine; please submit piolacsals to the Solid Waste Section for "Oluation.and approval. If you
have auy questions or wmments, please call me at 919-733-0692, cAensiorr 261.
Sincercly,
Ivla- Poindexter, Hydrogeologist
droundwater Compliance Unit
Solid Wye Section
c: Philip Prete
'ferry Dover
Pobby Nelms
Centaal f 1e

Waste Management
ENVIRONMENTAL QUALITY
March 16, 2017
Sent Via Email — iohn.demary@pittcountync.�ov
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Proposal for Assessment of Benzene Contamination Migration
Pitt County MSW Landfill (Northern and Southern)
Pitt County
Solid Waste Permit Number 74-01
DIN 27529
Dear Mr. Demary:
ROY COOPER
MICHAEL S. REGAN
Sec retao
MICHAEL SCOTT
Director
The NC Solid Waste Section has completed a review of the Proposal for Assessment of Benzene
Contamination Migration dated March 15, 2017 (DIN 27528) submitted on your behalf by Groundwater
Management Associates, Inc. (GMA) for the closed Pitt County MSW Landfill, NC Solid Waste Permit
Number 7401. During the January 2017 semiannual water quality monitoring event benzene was
detected at concentrations exceeding the NC 2L Groundwater Standards in two groundwater monitoring
wells.
Based upon the groundwater exceedances, Pitt County is requesting to collect two pore water samples
from the beneath the southern boundary ditch and analyze for Appendix I constituents. The proposed
sampling locations are located downgradient of groundwater monitoring well P20R and will be sampled
during the July 2017 semiannual water quality monitoring event.
As a result, the Proposal for Assessment of Benzene Contamination Migration is approved as described. If
you have any questions, please feel free to contact me by email at [e-mail] or
by phone at 828.296.4706. Thank you for your continued cooperation with this matter.
Sincerely,
L)4—
Jaclynne Drummond
Compliance Hydrogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
State of North Carolina I Environmental Quality I Waste Management
Asheville Regional Office 1 2090 U.S. Highway 70 1 Swannanoa, NC 28778
828 296 4500

cc sent via email: Tim Corley, Pitt County Engineer
Jason Watkins, Field Operations Branch Head
Drew Hammonds, Eastern District Supervisor
Ray Williams, Environmental Senior Specialist
Elizabeth Werner, Permitting Hydrogeologist
Emma Shipley, GMA
Steve Campbell, GMA
Slaivul Nw1hCon}Ilea h k ivlrurunrntal+2ua11ty I WasteManagemenl
Ashevile I funal lftr 1 10%) U.'� I Itghwuy 10 1 5wannanoa, NC 28778
828 2% 4.500

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
NORTH CAROLINA
Environmental Quality
June 26, 2019
Sent Via Email - [e-mail]
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Proposal for 1,4-Dioxane Assessment and Pilot Study at the Pitt County Municipal Solid
Waste Landfill
Closed and Unlined Pitt County MSW Landfill Northern and Southern Units
Pitt County
Solid Waste Permit Numbers 7401-MSWLF- and 7401-MSWLF-1974
FID 1323161
Dear Mr. Demary,
The Solid Waste Section (Section) has completed a review of the Proposal for 1,4-Dioxane Assessment
and Pilot Study at the Pitt County Municipal Solid Waste Landfill dated June 21, 2019 (FID 1323159)
and submitted on your behalf by Groundwater Management Associates, Inc. for the closed and unlined
Pitt County Landfill, Solid Waste Permit Numbers 7401-MSWLF- and 7401-MSWLF-1974.
To address the 1,4-Dioxane being detected within the groundwater at the landfill, Pitt County is
proposing to:
1) Delineate the vertical and horizontal extent of 1,4-Dioxane by installing two additional groundwater
monitoring wells (Type II and Type III) and six surface water gauges;
2) Initiate a one-year pilot study to determine the effectiveness of cap upgrades and repairs to see if
they have limited the infiltration of rainwater into the soil cap, and if they have reduced leachate
volumes and concentrations. Geophysical testing of the Southern Unit only will also be conducted to
evaluate landfill cap integrity. The County will repair any areas identified by the geophysical testing
and will inspect surface water drainage structures on the mound to ensure that they are operating as
designed. Once repairs are made, geophysical testing will be repeated to document hydrologic
benefits from cap repairs and to determine if the repairs have significantly reduced rainfall infiltration;
and
3) Install two instream piezometers approximately 1.5 feet below the ditch bottom at the locations of
the currently collected porewater samples. The instream piezometers will be used to collect
representative groundwater samples, measure groundwater levels, and determine any discharge
relationships at repeatable locations just below the stream bed.
Based upon a review of the Proposal for 1,4-Dioxane Assessment and Pilot Study at the Pitt County
Municipal Solid Waste Landfill, the Section approves the activities as described. If you have any
questions or concerns regarding this letter, please feel free to contact me by phone at 828.296.4706
or by email at [e-mail]. Thank you for your continued cooperation with this
matter.
North Carolina Department of Environmental Quality 1 Division of Waste Management
Asheville Regional Office 1 2090 U& Highway 70 1 Swannanoa, North Carolina 28775
828.296.4500

Sincerely,
L;�4' rc�—�
Jaclynne Drummond
Hyd rogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
cc sent via email: Tim Corley, Pitt County Engineer
Ed Mussler, SWS Chief
Adam Ulishney, SWS Environmental Compliance Branch Head
Jason Watkins, SWS Field Operations Branch Head
Drew Hammonds, SWS Eastern District Supervisor
Ray Williams, SWS Environmental Senior Specialist
Sherri Stanley, SWS Permitting Branch Head
Ethan Caldwell, SWS Permitting Engineer
Emma Shipley, GMA
Dr. Richard Spruill, GMA
Jay Holley, GMA
North Carollno Department of Envhvnmental Reality I AivWan of Waste Management
Asheville Regional Office 12090 U.&HighwayM I Swannanoa, North Carolina 28775
828296A500

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
NORTH CAROLINA
Environmental Quality
July 2, 2020
Sent Via Email - [e-mail]
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Request for Reduced Sampling Frequency of Appendix 11 Constituents
Closed and Unlined Pitt County MSW Landfill Southern Unit
Pitt County
Solid Waste Permit Number 7401-MSWLF-1974
FID 1417776
Dear Mr. Demary,
The Solid Waste Section (Section) has completed a review of the Request for Reduced Sampling
Frequency of Appendix II Constituents dated July 1, 2020 (FID 1417773) and submitted on your behalf
by Groundwater Management Associates, Inc. for the closed and unlined Pitt County Landfill Southern
Unit, Solid Waste Permit Number 7401-MSWLF-1974.
In accordance with 15A NCAC 13B .1634 a request was provided to the Section to modify the
groundwater monitoring frequency for the full set of Appendix II constituents because no Appendix II
constituents have been detected since 2014. Pitt County is requesting to sample for Appendix II
constituents on a biennial basis with the next scheduled Appendix II sampling event occurring during
July 2022. The County will continue to sample for Appendix I parameters and for 1,4-dioxane on a
semi-annual basis.
Based upon a review of the Request for Reduced Sampling Frequency of Appendix 11 Constituents, the
Section approves the request as written at this time. If you have any questions or concerns regarding
this response letter, please feel free to contact me by phone at 828.296.4706 or by email at
[e-mail].
Sincerely,
1
Jaclynne Drummond
Hyd rogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
cc sent via email: Tim Corley, Pitt County
North Carolina Department of Environmental Quality 1 Division of Waste Management
Asheville Regional Office 1 2090 U& Highway 70 1 Swannanoa, North Carolina 28775
828.296.4500

Adam Ulishney, SWS Environmental Compliance Branch Head
Jason Watkins, SWS Field Operations Branch Head
Drew Hammonds, SWS Eastern District Supervisor
Ray Williams, SWS Environmental Senior Specialist
Ethan Caldwell, SWS Permitting Engineer
Emma Shipley, GMA
North Carolina Department of Environmental Quality I Divislon of Waste Manageme nl
Asheville Regional Office 12040 U.S. Highway 70 1 Swannanoa, North CAnnhna 28778
828.296.4500

APPENDIX B
SAMPLING RECORDS

GMA Project 25101: Pitt County Landfill Jan 292 field Sheet
Collected By: LS
M1'CU
v
Field Parameters
Date/Time
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v
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Water level
Volatiles
Metals
Notes (well/lock
Well
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F
p
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m Vo
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PH
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collected
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$V (in gallons) = 70.5 r'h = 0.4856745 * h
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
I = Appendix 1 II = Appendix II
GMA

GMA Project 25101: Pitt County Landfill Jan 2020 Field Sheet
Collected By: ( V S C. S
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Field Parameters
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°
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a
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m m
3
3
pH
(0Q
iv" (µ5)
(mg/L)
Turbidity
collected
Sampling
Sampling
condition, etc.)
P05
a
X
o
17.1
"1 S�
Ii CJI
I- 11
i
lst bail
IlJ
2nd
�f , Zl+
i
5
4 11..
1S
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p
l.�
LA
Z_
<.c
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II l�`�
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Q
3rd
-
-
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1st bail
1� 2nd
11� "j%
M5;0l
`�'L
•�
(�Z.610
=1_�7
Z , 30
35- 3
_��
_Ip�.
d
C
1
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3b
1
�3
5,
o
P07
19.5
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, �, �Z
�;y�
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107—
'jr lq
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t5,3
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��
2--(o5
i rl
o
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/
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�oa�y-1a1SS J
_
1
_
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ld'js
2 3rd
q!(
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(7�.)
r
�`I'r�
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-S 2-1
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Ij iy�zi
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18.5
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r
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7
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7
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2-1
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a o
1 ���
2nd
�;
(5 .5
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rs,, ��
l5• Z
1r1, q
P12
d
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20.9
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/
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� .��-
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� �r� _[�I,,l
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j�
.v
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[
L� .� 7
1
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lY`�t 1
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(often goes dry)
t42nd
1���
Ic
_
_
7`�
.7'z
a �
I
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�V
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1 :).U�
lq (a
5 Z�
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^�.Z
V (in gallons) = 70.5 r'h = 0.4856745 * h
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
GMA ;`'�
I = Appendix 1 II = Appendix II

GMA Project 25101: Pitt County Landfill Jan 2020 Field Sheet
Collected By: f-14S C S•
0
c
M1.
r
o 'a
;
,.
to
3
o c
E
>
m c
— a
N M
Field Parameters
o sP
Date/Time
Purging
completion/
E
,�
� m
a
ea
a
o a0
Temp C-errdoct- DO
Water level Volatiles Metals
Notes (well/lock
Well
y
o
N =
o $
_ �°,
m m
3
3 pH (°C) 6gty(µS) (mg/L) Turbidity
collected Sampling Sampling
condition, etc.)
w
1stbail
L
J�S�
Ili•()
I"1��5
(�.5 7
����
��1�12'1
i ( I
`z)
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5. ?
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1 5�
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/I
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(often goes dry)
(
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a
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l%��
15,13
-
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1st
to2,
1L.Z
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15
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X
18.4
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I Z: (G�
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d
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S.J
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I.7`�
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lrpi3s
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lstl`
-
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t 2. -
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\r (� I
t ((k�u
Often goes dry
—�.5
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c
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y• 5
0
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2nd
,��
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l'7 3rd
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a
`1 t
bCti.IS
�, (�
i S
'� 1 Ci
�.4�qj
C'j (�(g
V (in gallons) = 70.5 r'h = 0.4856745 * h
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
GMA
I = Appendix 1 II = Appendix II

GMA Project 25101: Pitt County Landfill Jan 2020 Field Sheet
Collected By: 1� LS
O
m
c
NN
°1
t
a
o c.
`0
3
o
3
s
o
°i
o
M1_
U
1
axi
y
Field Parameters
Date/Time
c
Sf `
Purging
completion/
E
.fO u m
a
W _
fO
o CO
a,
Temp
C-6i05ct-
DO
Water level
Volatiles
Metals
Notes (well/lock
Well
V)
C
H n .'�..
C .wy.,
x U
m m
f0
U• 3
3
pH
°
(C)
itliEy (µS)
(mg/L)
Turbidity
collected
Sampling
Sampling
condition, etc.)
P23
c
X
19.5
l�@S
1st
li
� 2nd
5, G0
`j -72
I (o�S
17, �
izu.3
p
5 1, 0
`i. G,.5
Zb ,�(
2,`i
59
� f 1-3 �Z�
�
i 1J/21
I Ilylll
l
(often goes dry)
1
a �
d3 3rd
1 v2j�(S
P28
c
2
X
10.9
qc
2, �
�-.01 1
�'
1st
-
�o
S, C
l- --
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l ,
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. `��J
. t 0
`t�i.
Zitl b
' 1'7� Z�
�—pQ
_i
) I7� �'2�
I I14 I ZI
r' D N
(sometimes goes dry)
a �
J-
l
end
_ _
G- ►
`J `IS
3� 1
1.�
0
�t`l 3rd
5 72
(r7.0
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2,51
%� 1
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X
14.96
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���
' 1st�q2�
2nd
L{
�, 1
5�'�Z
�.5_ Z
���
,+►qI
- ice; ir ���el
(;
_
.Z.��l
Q
lb 3rd
����
(S. I
yl3.2
13, 1U
Q'-10
CL
�'S
1 %
1(l'421
SWl
a °o
a
i1v3i21
((►`��
�+I`��ZI
-
C
-
� ,� �
�� . 3
, b��.�i
, ZZ
�� . ��
' 3.7
is
SW2
v
SW4
a —
��
�?j'',�j
+ 7i I O
1-7 . I V
a
=M
x
-
5.45�
cv. /.��
� ► ! )�
a
M
1, �(v.3
i
Lt ( lid
PZ2
rL x
a •.°-o
_
�y1�
V (in gallons) = 70.5 r'h = 0.4856745 * h
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
GMA
I = Appendix 1 II = Appendix II

GMA Project 25101: Pitt County Landfill Jan 2020 Field Sheet
Collected By: WS &',;
N
Field Parameters
Date/Time
-
E
3
°1
3
N
dC
G
tf
f°
X
M1.
2
C
Purging
OD
c
o
o V
o
>
�;
o
completion/
o
o n —
Y m
a
m E
—
a,
o
co
> Temp
Conduct-
DO
Water level
Volatiles
Metals
Notes (well/lock
Well
vf0i
o
^
o
i v°
m m
3
3 pH (°C)
ivity (µS)
(mg/L) Turbidity
collected
Sampling
Sampling
condition, etc.)
4 LH 4
Z( �O
FB
EB
(13Zl Iv.57
Collect surface water samples facing upstream. Collect from point of confluence for SW2
EB: Pour lab DI water into bailer and over gloves and rope into ss pitcher then into sample containers.
FB: Use lab DI water to fill sample containers directly. Collect on -site preferably near the dirt road within the landfill.
V (in gallons) = 70.5 r'h = 0.4856745 * h
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
I = Appendix 1 II = Appendix II

APPENDIX C
LABORATORY REPORT AND CHAIN -OF -CUSTODY
FORMS FOR WATER SAMPLES

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, February 10, 2021
Groundwater Management Associates, Inc. (GR022)
Attn: Emma Shipley
4300 Sapphire Court, Suite 100
Greenville, NC 27834
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Pitt County Landfill - App I
ENCO Workorder(s): CE00125
Dear Emma Shipley,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, January 15, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 99

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PROJECT NARRATIVE
Client: Groundwater Management Associates, Inc. (GR022)
Project: Pitt County Landfill - App I
Lab ID: CE00125
Overview
Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods
referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in
the QC Remarks section below.
Quality Control Samples
The associated LCS exhibited high bias; since the result is ND, there is no impact (QL-02).
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an acceptable
LCS recovery (QM-07).
Post -digestion spike did not meet method requirements due to confirmed matrix effects (QM-08).
Quality Control Remarks
This compound is a common laboratory contaminant (0-01).
The internal standard(s) for this sample were outside the acceptance limits due to sample matrix interference. The sample
was re -analyzed at a dilution (QI-03).
The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01).
Other Comments
The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any
exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of
the report.
Released By:
Environmental Conservation Laboratories, Inc.
Chuck Smith
Project Manager
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-MW1R
Lab ID: CE00125-01
Sampled: 01/14/21 16:59
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 09:42
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:22
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 17:27
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 11:24
Client ID: 7401-MWlR
Lab ID: CE00125-01RE1
Sampled: 01/14/21 16:59
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:10
Client ID: 7401-MW3
Lab ID: CE00125-02
Sampled: 01/14/21 15:20
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:08
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 10:48
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 17:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 11:50
Client ID: 7401-MW3
Lab ID: CE00125-02RE1
Sampled: 01/14/21 15:20
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:12
Client ID: 7401-MW6R
Lab ID: CE00125-03
Sampled: 01/14/21 08:31
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 18:27
EPA 8260D
EPA 5030B_MS
01/28/21
01/20/21 00:00
01/20/21 12:15
Client ID: 7401-MW6R
Lab ID: CE00125-04
Sampled: 01/14/21 16:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:11
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:26
Client ID: 7401-MW6R
Lab ID: CE00125-04RE1
Sampled: 01/14/21 16:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:14
Client ID: 7401-MW8
Lab ID: CE00125-05
Sampled: 01/13/21 11:09
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/12/21
01/18/21 09:22
01/20/21 10:13
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:43
01/26/21 11:31
EPA 8260D
EPA 5030B_MS
01/27/21
01/14/21 15:24
01/15/21 19:34
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 00:00
01/20/21 12:40
Client ID: 7401-MW8
Lab ID: CE00125-OSRE1
Sampled: 01/13/21 11:09
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/12/21
01/18/21 09:43
02/04/21 15:15
Client ID: 7401-122
Lab ID: CE00125-06
Sampled: 01/14/21 15:05
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:15
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:35
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 18:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 13:19
Client ID: 7401-132
Lab ID: CE00125-06RE1
Sampled: 01/14/21 15:05
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:17
FINAL
This report
relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 3 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-134
Lab ID: CE00125-07
Sampled: 01/13/21 12:15
Received: O1/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
01/27/21
01/14/21 15:24
01/15/21 20:04
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 00:00
01/20/21 13:45
Client ID: 7401-134
Lab ID: CE00125-08
Sampled: 01/14/21 12:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:07
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:39
Client ID: 7401-124
Lab ID: CE00125-08RE1
Sampled: 01/14/21 12:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:18
Client ID: 7401-P5
Lab ID: CE00125-09
Sampled: 01/14/21 17:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:20
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:43
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 19:27
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 14:10
Client ID: 7401-P6
Lab ID: CE00125-10
Sampled: 01/14/21 12:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:10
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:48
EPA 8260D
EPA 5030B_MS
01/28/21
01/19/21 12:39
01/19/21 19:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 14:35
Client ID: 7401-136
Lab ID: CE00125-30RE1
Sampled: 01/14/21 12:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:20
Client ID: 7401-P7
Lab ID: CE00125-11
Sampled: 01/14/21 11:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:25
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:52
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 20:27
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 15:00
Client ID: 7401-137
Lab ID: CE00125-11RE1
Sampled: 01/14/21 11:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:21
Client ID: 7401-139
Lab ID: CE00125-12
Sampled: 01/14/21 11:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:12
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:56
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 20:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 15:26
Client ID: 7401-139
Lab ID: CE00125-12RE1
Sampled: 01/14/21 11:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:23
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-P11R
Lab ID: CE00125-13
Sampled: 01/14/21 09:28
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:15
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:01
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 12:39
01/19/21 21:27
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 15:51
Client ID: 7401-P11R
Lab ID: CE00125-13RE1
Sampled: 01/14/21 09:28
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:24
Client ID: 7401-1312
Lab ID: CE00125-14
Sampled: 01/14/21 09:55
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:22
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:35
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 12:39
01/19/21 21:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 16:16
Client ID: 7401-1313
Lab ID: CE00125-15
Sampled: 01/14/21 14:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:13
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:39
EPA 8260D
EPA 503013_MS
O1/28/21
01/20/21 00:00
01/20/21 16:41
Client ID: 7401-1313
Lab ID: CE00125-15RE1
Sampled: 01/14/21 14:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:29
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 12:39
01/20/21 16:06
Client ID: 7401-131313
Lab ID: CE00125-16
Sampled: 01/14/21 14:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:35
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:43
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 12:39
01/19/21 22:57
EPA 8260D
EPA 5030B_MS
O1/28/21
01/20/21 00:00
01/20/21 17:07
Client ID: 7401-P13D
Lab ID: CE00125-16RE1
Sampled: 01/14/21 14:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:31
Client ID: 7401-P16R
Lab ID: CE00125-17
Sampled: 01/13/21 15:13
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
O1/27/21
01/14/21 15:24
01/15/21 20:34
EPA 8260D
EPA 503013_MS
O1/27/21
01/20/21 00:00
01/20/21 19:13
Client ID: 7401-P16R
Lab ID: CE00125-18
Sampled: 01/14/21 09:07
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:37
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:47
Client ID: 7401-131611
Lab ID: CE00125-18RE1
Sampled: 01/14/21 09:07
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:32
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1337
Lab ID: CE00125-19
Sampled: 01/13/21 15:35
Received: O1/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/12/21
01/18/21 09:33
01/21/21 11:40
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:43
01/26/21 12:52
EPA 8260D
EPA 503013_MS
O1/27/21
01/14/21 15:24
01/15/21 21:04
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 00:00
01/20/21 17:32
Client ID: 7401-1317
Lab ID: CE00125-19RE1
Sampled: 01/13/21 15:35
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:43
02/04/21 15:34
Client ID: 7401-1319
Lab ID: CE00125-20
Sampled: 01/13/21 16:11
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
O1/27/21
01/14/21 15:24
01/15/21 21:34
EPA 8260D
EPA 5030B_MIS
O1/27/21
01/20/21 00:00
01/20/21 19:38
Client ID: 7401-1319
Lab ID: CE00125-21
Sampled: 01/14/21 10:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:42
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:56
Client ID: 7401-1319
Lab ID: CE00125-21RE1
Sampled: 01/14/21 10:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:35
Client ID: 7401-1320R
Lab ID: CE00125-22
Sampled: 01/13/21 16:35
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
01/27/21
01/14/21 15:24
01/15/21 22:04
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 00:00
01/20/21 17:57
Client ID: 7401-1320R
Lab ID: CE00125-23
Sampled: 01/14/21 10:18
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:45
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 13:00
Client ID: 7401-1320R
Lab ID: CE00125-23RE1
Sampled: 01/14/21 10:18
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:37
Client ID: 7401-1320D
Lab ID: CE00125-24
Sampled: 01/14/21 16:20
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:47
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 08:29
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 08:33
EPA 8260D
EPA 5030B_MS
O1/28/21
01/20/21 00:00
01/20/21 18:23
EPA 8260D
EPA 503013_MS
O1/28/21
01/20/21 10:35
01/20/21 19:20
Client ID: 7401-13201)
Lab ID: CE00125-24RE1
Sampled: 01/14/21 16:20
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 08:56
Client ID: 7401-1321
Lab ID: CE00125-25
Sampled: 01/14/21 09:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:49
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:04
EPA 8260D
EPA 5030B_MS
O1/28/21
01/20/21 00:00
01/20/21 18:48
EPA 8260D
EPA 503013_MS
O1/28/21
01/20/21 10:35
01/20/21 19:48
FINAL
This report
relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 6 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1321
Lab ID: CE00125-25RE3
Sampled: 01/14/21 09:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:39
Client ID: 7401-1323
Lab ID: CE00125-26
Sampled: 01/13/21 14:55
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
O1/27/21
01/14/21 15:24
01/15/21 22:34
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 14:20
01/21/21 00:15
Client ID: 7401-1323
Lab ID: CE00125-27
Sampled: 01/14/21 08:45
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:52
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:09
Client ID: 7401-P28
Lab ID: CE00125-28
Sampled: 01/13/21 15:45
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
O1/27/21
01/19/21 11:22
01/19/21 18:30
EPA 8260D
EPA 503013_MS
O1/27/21
01/20/21 14:20
01/21/21 00:40
Client ID: 7401-1328
Lab ID: CE00125-29
Sampled: 01/14/21 10:05
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:54
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:39
Client ID: 7401-1328
Lab ID: CE00125-29RE1
Sampled: 01/14/21 10:05
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:40
Client ID: 7401-1329
Lab ID: CE00125-30
Sampled: 01/14/21 13:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:56
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:43
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 18:58
EPA 8260D
EPA 503013_MS
O1/28/21
01/22/21 00:00
01/22/21 18:06
Client ID: 7401-1229
Lab ID: CE00125-30RE1
Sampled: 01/14/21 13:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:42
Client ID: 7401-SW1
Lab ID: CE00125-31
Sampled: 01/14/21 17:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:42
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:48
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 19:25
EPA 8260D
EPA 5030B_MIS
O1/28/21
01/20/21 14:20
01/21/21 01:06
Client ID: 7401-SW1
Lab ID: CE00125-31RE1
Sampled: 01/14/21 17:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:43
Client ID: 7401-SW2
Lab ID: CE00125-32
Sampled: 01/14/21 15:37
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:44
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:52
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 19:53
EPA 8260D
EPA 5030B_MS
O1/28/21
01/20/21 14:20
01/21/21 01:31
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-SW2
Lab ID: CE00125-32RE3
Sampled: 01/14/21 15:37
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:48
Client ID: 7401-SW4
Lab ID: CE00125-33
Sampled: 01/13/21 17:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/12/21
01/18/21 09:33
01/21/21 12:46
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:46
01/26/21 09:56
EPA 8260D
EPA 503013_MS
O1/27/21
01/18/21 11:52
01/18/21 20:51
EPA 8260D
EPA 503013_MS
O1/27/21
01/20/21 14:20
01/21/21 01:56
Client ID: 7401-SW4
Lab ID: CE00125-33RE1
Sampled: 01/13/21 17:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:46
02/04/21 15:50
Client ID: 7401-PZ1
Lab ID: CE00125-34
Sampled: 01/14/21 10:55
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:48
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 10:01
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 20:20
EPA 8260D
EPA 503013_MS
01/28/21
01/22/21 00:00
01/22/21 17:40
Client ID: 7401-PZ3
Lab ID: CE00125-34RE1
Sampled: 01/14/21 10:55
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:51
Client ID: 7401-PZ2
Lab ID: CE00125-35
Sampled: 01/14/21 10:30
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:51
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 10:05
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 20:47
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 14:20
01/21/21 02:21
Client ID: 7401-PZ2
Lab ID: CE00125-35RE1
Sampled: 01/14/21 10:30
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:53
Client ID: 7401-EB
Lab ID: CE00125-36
Sampled: 01/13/21 16:57
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/12/21
01/18/21 09:33
01/21/21 12:53
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:46
01/26/21 10:09
EPA 8260D
EPA 503013_MS
O1/27/21
01/18/21 11:52
01/18/21 16:17
EPA 8260D
EPA 503013_MS
O1/27/21
01/20/21 14:20
01/21/21 02:47
Client ID: 7401-EB
Lab ID: CE00125-36RE1
Sampled: 01/13/21 16:57
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:46
02/04/21 15:54
Client ID: 7401-FB
Lab ID: CE00125-37
Sampled: 01/14/21 09:30
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:56
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 10:13
EPA 8260D
EPA 5030B_MS
O1/28/21
01/19/21 11:22
01/19/21 17:08
Client ID: 7401-FB
Lab ID: CE00125-37RE1
Sampled: 01/14/21 09:30
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
O1/28/21
01/22/21 00:00
01/22/21 11:21
FINAL
This report
relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-TripBlank
Lab ID: CE00125-38RE3
Sampled: 01/13/21 00:00
Received: O1/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
O1/27/21
01/25/21 16:38
01/25/21 19:44
Client ID: 7401-TripBlank
Lab ID: CE00125-39RE1
Sampled: 01/13/21 00:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Pren Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
O1/27/21
01/25/21 16:38
01/25/21 20:12
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 99

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SAMPLE DETECTION SUMMARY
Client ID: 7401-MW1R
Lab ID:
CE00125-01
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
54.6
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.348
J
0.160
1.00
ug/L
EPA 6010D
Client ID: 7401-MW3
Lab ID:
CE00125-02
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
190
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.221
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
5.97
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
5.82
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
3.29
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
26.7
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-MW6R
Lab ID:
CE00125-03
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
6.5
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-MW6R
Lab ID:
CE00125-04
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
2120
1.10
10.0
ug/L
EPA 6010D
Nickel - Total
2.71
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-MW8
Lab ID:
CE00125-05
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
11.8
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.375
J
0.160
1.00
ug/L
EPA 6010D
Copper - Total
1.98
J
1.60
10.0
ug/L
EPA 6010D
Vanadium - Total
2.88
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
7.24
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-132
Lab ID:
CE00125-06
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
4.16
J
1.10
10.0
ug/L
EPA 6010D
Client ID: 7401-134
Lab ID:
CE00125-08
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
111
1.10
10.0
ug/L
EPA 6010D
Copper - Total
15.6
1.60
10.0
ug/L
EPA 6010D
Zinc - Total
4.45
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-PS
Lab ID:
CE00125-09
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
12.9
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.179
1
0.160
1.00
ug/L
EPA 6010D
Copper - Total
1.91
1
1.60
10.0
ug/L
EPA 6010D
Client ID: 7401-136
Lab ID:
CE00125-10
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
58.8
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.337
J
0.160
1.00
ug/L
EPA 6010D
Zinc - Total
4.89
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-137
Lab ID:
CE00125-11
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
216
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.464
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.38
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
3.12
J
1.60
10.0
ug/L
EPA 6010D
Nickel- Total
4.14
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
2.31
J
1.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 99

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SAMPLE DETECTION SUMMARY
Client ID: 7401-P9
Lab ID:
CE00125-12
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
116
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.761
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.66
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
2.03
J
1.60
10.0
ug/L
EPA 6010D
Nickel- Total
3.10
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-P11R
Lab ID:
CE00125-13
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
99.2
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
1.93
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.38
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
7.10
J
1.60
10.0
ug/L
EPA 6010D
Nickel - Total
3.28
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
4.67
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
39.8
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1312
Lab ID:
CE00125-14
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
34.9
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.553
J
0.160
1.00
ug/L
EPA 6010D
Client ID: 7401-1313
Lab ID:
CE00125-15
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
54.2
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.204
J
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
1.73
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
2.16
J
1.60
10.0
ug/L
EPA 6010D
Vanadium - Total
1.69
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P13D
Lab ID:
CE00125-16
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
1.5
J
0.80
2.0
ug/L
EPA 8260D
Barium - Total
100
1.10
10.0
ug/L
EPA 6010D
Client ID: 7401-P16R
Lab ID:
CE00125-17
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
78
D
1.6
4.0
ug/L
EPA 8260D
Acetone
12
J
10
20
ug/L
EPA 8260D
Benzene
0.86
J
0.15
1.0
ug/L
EPA 8260D
Client ID: 7401-11316R
Lab ID:
CE00125-18
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
1100
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.88
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
16.6
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-1317
Lab ID:
CE00125-19
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
5.0
0.80
2.0
ug/L
EPA 8260D
Barium - Total
147
1.10
10.0
ug/L
EPA 6010D
Benzene
0.43
1
0.15
1.0
ug/L
EPA 8260D
Beryllium - Total
1.43
0.160
1.00
ug/L
EPA 6010D
Chlorobenzene
4.3
0.17
1.0
ug/L
EPA 8260D
Copper - Total
1.89
J
1.60
10.0
ug/L
EPA 6010D
Nickel - Total
2.79
J
2.20
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 99

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SAMPLE DETECTION SUMMARY
Client ID: 7401-1319
Lab ID:
CE00125-20
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,1-Dichloroethane
4.2
0.13
1.0
ug/L
EPA 8260D
1,4-Dichlorobenzene
5.1
0.19
1.0
ug/L
EPA 8260D
1,4-Dioxane
160
D
2.0
5.0
ug/L
EPA 8260D
Benzene
4.0
0.15
1.0
ug/L
EPA 8260D
Chlorobenzene
7.0
0.17
1.0
ug/L
EPA 8260D
cis-1,2-Dichloroethene
2.7
0.15
1.0
ug/L
EPA 8260D
Ethylbenzene
1.8
0.13
1.0
ug/L
EPA 8260D
m,p-Xylenes
0.42
J
0.17
2.0
ug/L
EPA 8260D
o-Xylene
0.56
J
0.065
1.0
ug/L
EPA 8260D
Vinyl chloride
0.57
J
0.32
1.0
ug/L
EPA 8260D
Xylenes (Total)
0.98
J
0.45
3.0
ug/L
EPA 8260D
Client ID: 7401-1319
Lab ID:
CE00125-21
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
1870
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
15.3
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
19.3
1.40
10.0
ug/L
EPA 6010D
Copper - Total
1.72
J
1.60
10.0
ug/L
EPA 6010D
Lead - Total
6.07
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
29.4
2.20
10.0
ug/L
EPA 6010D
Selenium - Total
2.08
1.82
2.00
ug/L
EPA 6020E
Vanadium - Total
1.46
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
120
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-132011
Lab ID:
CE00125-22
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,4-Dioxane
2.1
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-132011
Lab ID:
CE00125-23
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
51.4
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
1.66
0.160
1.00
ug/L
EPA 6010D
Vanadium - Total
2.44
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
12.1
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-132013
Lab ID:
CE00125-24
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
112
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
8.87
0.160
1.00
ug/L
EPA 6010D
Cadmium - Total
0.756
J
0.360
1.00
ug/L
EPA 6010D
Chromium - Total
12.9
1.40
10.0
ug/L
EPA 6010D
Lead - Total
5.43
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
4.31
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
12.6
1.40
10.0
ug/L
EPA 6010D
Zinc - Total 20.1 4.40 10.0 ug/L EPA 6010D
Client ID: 7401-1321 Lab ID: CE00125-25
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
58.0
1.10
10.0
ug/L
EPA 6010D
Nickel - Total
2.53
1
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-1323
Lab ID:
CE00125-27
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
19.6
1.10
10.0
ug/L
EPA 6010D
Zinc - Total
7.76
1
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 99

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SAMPLE DETECTION SUMMARY
Client ID: 7401-1328
Lab ID:
CE00125-29
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
38.4
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.741
3
0.160
1.00
ug/L
EPA 6010D
Copper - Total
2.49
3
1.60
10.0
ug/L
EPA 6010D
Nickel- Total
3.16
3
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
1.53
3
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
14.0
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P29
Lab ID:
CE00125-30
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,4-Dichlorobenzene
0.89
3
0.19
1.0
ug/L
EPA 8260D
1,4-Dioxane
140
D
4.0
10
ug/L
EPA 8260D
Barium - Total
1290
1.10
10.0
ug/L
EPA 6010D
Benzene
1.6
0.15
1.0
ug/L
EPA 8260D
Beryllium - Total
0.980
3
0.160
1.00
ug/L
EPA 6010D
Chlorobenzene
5.1
0.17
1.0
ug/L
EPA 8260D
Cobalt - Total
4.66
3
1.40
10.0
ug/L
EPA 6010D
Ethylbenzene
0.48
3
0.13
1.0
ug/L
EPA 8260D
Lead - Total
18.0
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
7.50
3
2.20
10.0
ug/L
EPA 6010D
Selenium - Total
2.54
1.82
2.00
ug/L
EPA 6020E
Vanadium - Total
36.1
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
5.63
3
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1329
Lab ID:
CE00125-30RE3
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Thallium - Total
0.252
3
0.220
2.00
ug/L
EPA 6020E
Client ID: 7401-SW3
Lab ID:
CE00125-31
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
23.9
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.212
3
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
8.02
3
1.40
10.0
ug/L
EPA 6010D
Lead - Total
3.54
3
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
3.41
3
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
2.15
3
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
15.3
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-SW2
Lab ID:
CE00125-32
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
40.3
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
1.44
3
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
18.8
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-SW4
Lab ID:
CE00125-33
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
3.5
0.80
2.0
ug/L
EPA 8260D
Barium - Total
40.0
1.10
10.0
ug/L
EPA 6010D
Zinc - Total
5.97
3
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-PZI
Lab ID:
CE00125-34
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
2.1
0.80
2.0
ug/L
EPA 8260D
Arsenic - Total
100
7.60
10.0
ug/L
EPA 6010D
Barium - Total
101
1.10
10.0
ug/L
EPA 6010D
Cadmium - Total
1.72
0.360
1.00
ug/L
EPA 6010D
Cobalt - Total
2.21
3
1.40
10.0
ug/L
EPA 6010D
Copper - Total
3.41
3
1.60
10.0
ug/L
EPA 6010D
Lead - Total
8.46
3
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
3.31
3
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
12.4
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
26.4
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 99

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SAMPLE DETECTION SUMMARY
Client ID: 7401-PZ2
Lab ID:
CE00125-35
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,4-Dioxane
3.6
0.80
2.0
ug/L
EPA 8260D
Barium - Total
190
1.10
10.0
ug/L
EPA 6010D
Cadmium - Total
0.360
J
0.360
1.00
ug/L
EPA 6010D
Zinc - Total
18.3
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-EB
Lab ID:
CE00125-36
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
2-Hexanone
1.9
J
0.88
5.0
ug/L
EPA 8260D
Carbon disulfide
53
1.5
5.0
ug/L
EPA 8260D
Zinc - Total
114
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-FB
Lab ID:
CE00125-37
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Acetone
14
J
10
20
ug/L
EPA 8260D
Client ID: 7401-TripBlank
Lab ID:
CE00125-38RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Acetone
67
10
20
ug/L
EPA 8260D
0-01
Client ID: 7401-TripBlank
Lab ID:
CE00125-39RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Acetone
31
10
20
ug/L
EPA 8260D
0-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MWlR Lab Sample ID:CE00125-01 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:59 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
17:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
17:27
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 15 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MWlR Lab Sample ID:CE00125-01 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:59 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 17:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 17:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
56
1
50.0
112 %
53-136
IA19023
EPA 6260D
01/19/21 17:27
REF
Dibromofluoromethane
50
1
50.0
99 %
67-129
IA19023
EPA 6260D
01119121 17:27
REF
Toluene-d8
49
1
50.0
98 %
59-134
IA19023
EPA 6260D
01119121 17:27
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:22
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Barium [7440-39-3]^
54.6
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 09:42
JDH
Beryllium [7440-41-7]A
0.348
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 09:42
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 09:42
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:22
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:10
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 11:24
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
108 %
75-125
1A20026
EPA 8260D
01120121 11:24
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW3 Lab Sample ID:CE00125-02 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 15:20 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
17:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
17:57
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 17 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW3 Lab Sample ID:CE00125-02 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 15:20 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 17:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 17:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
59
1
50.0
117 %
53-136
IA19023
EPA 6260D
01/19/21 17:57
REF
Dibromofluoromethane
54
1
50.0
109 %
67-129
IA19023
EPA 6260D
01119121 17:57
REF
Toluene-d8
55
1
50.0
109 %
59-134
IA19023
EPA 8260D
01119121 17:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 10:48
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Barium [7440-39-3]^
190
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Beryllium [7440-41-7]A
0.221
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 10:08
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:08
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Cobalt[7440-48-4]A
5.97
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Nickel[7440-02-O]^
5.82
J
ug/L
1
2.20
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 10:48
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:12
RLF
Vanadium [7440-62-2]^
3.29
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Zinc[7440-66-6]^
26.7
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 11:50
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
5.1
1
5.00
103 %
75-125
1A20026
EPA 8260D
01120121 11:50
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 99

00�
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ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CE00125-03 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2108:31 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
18:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
18:27
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 19 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CE00125-03 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2108:31 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 18:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 18:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
59
1
50.0
119 %
53-136
IA19023
EPA 6260D
01119121 16:27
REF
Dibromofluoromethane
52
1
50.0
103 %
67-129
IA19023
EPA 6260D
01119121 16:27
REF
Toluene-d8
54
1
50.0
108 %
59-134
IA19023
EPA 8260D
01119121 16:27
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
6.5
ug/L
1
0.80 2.0
1A20026
EPA 8260D
01/20/21 12:15
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes
Toluene-d8 5.4 1 5.00 109 % 75-125 1A20026 EPA 8260D 01120121 12:15 KKW
Description: 7401-MW6R Lab Sample ID:CE00125-04 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 11:26
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Barium [7440-39-3]^
2120
ug/L
1
1.10
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18012
EPA 6010D
01/20/21 10:11
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:11
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Nickel[7440-02-O]^
2.71
J
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 11:26
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:14
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 99

00�
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ANALYTICAL RESULTS
Description: 7401-MW8 Lab Sample ID:CE00125-05 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 11:09 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
19:34
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
19:34
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 21 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW8 Lab Sample ID:CE00125-05 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 11:09 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 19:34 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 19:34 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
IA14039
EPA 6260D
01115121 19:34
REF
Dibromofluoromethane
47
1
50.0
93 %
67-129
IA14039
EPA 6260D
01115121 19:34
REF
Toluene-d8
48
1
50.0
97 %
59-134
IA14039
EPA 6260D
01115121 19:34
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:31
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Barium [7440-39-3]^
11.8
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:13
JDH
Beryllium [7440-41-7]A
0.375
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 10:13
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:13
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Copper[7440-50-8]A
1.98
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 10:13
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:31
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:15
RLF
Vanadium [7440-62-2]^
2.88
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:13
JDH
Zinc[7440-66-6]^
7.24
J
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 12:40
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-18
5.6
1
5.00
112 %
75-125
1A20026
EPA 8260D
01120121 12:40
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P2 Lab Sample ID:CE00125-06 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 15:05 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
18:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
18:57
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page
23 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P2 Lab Sample ID:CE00125-06 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 15:05 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 18:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 18:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
56
1
50.0
113 %
53-136
IA19023
EPA 6260D
01/19/21 18:57
REF
Dibromofluoromethane
48
1
50.0
97 %
67-129
IA19023
EPA 6260D
01119121 16:57
REF
Toluene-d8
51
1
50.0
103 %
59-134
IA19023
EPA 6260D
01119121 16:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:35
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Barium [7440-39-3]^
4.16
J
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:15
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
1A18012
EPA 6010D
01/20/21 10:15
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:15
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:35
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:17
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 13:19
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffK
Notes
Toluene-d8
5.6
1
5.00
112 %
75-125
1A20026
EPA 8260D
01120121 13:19
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P4 Lab Sample ID:CE00125-07 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 12:15 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
20:04
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
20:04
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 25 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P4 Lab Sample ID:CE00125-07 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 12:15 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 20:04 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 20:04 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA14039
EPA 6260D
01115121 20:04
REF
Dibromofluoromethane
47
1
50.0
95 %
67-129
IA14039
EPA 6260D
01115121 20:04
REF
Toluene-d8
46
1
50.0
91 %
59-134
IA14039
EPA 6260D
01115121 20:04
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
1A20026
EPA 8260D
01/20/21 13:45
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes
Toluene-d8 4.7 1 5.00 93 % 75-125 1A20026 EPA 8260D 01120121 13:45 KKW
Description: 7401-P4 Lab Sample ID:CE00125-08 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 12:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 11:39
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Barium [7440-39-3]^
111
ug/L
1
1.10
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18012
EPA 6010D
01/20/21 11:07
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:07
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Copper[7440-50-B]^
15.6
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 11:39
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:18
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Zinc[7440-66-6]^
4.45
J
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P5 Lab Sample ID:CE00125-09 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 17:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
19:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
19:27
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 27 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P5 Lab Sample ID:CE00125-09 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 17:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 19:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 19:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
56
1
50.0
111 %
53-136
IA19023
EPA 6260D
01119121 19:27
REF
Dibromofluoromethane
52
1
50.0
104 %
67-129
IA19023
EPA 6260D
01119121 19:27
REF
Toluene-d8
51
1
50.0
102 %
59-134
IA19023
EPA 8260D
01119121 19:27
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:43
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Barium [7440-39-3]^
12.9
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:20
JDH
Beryllium [7440-41-7]A
0.179
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 10:20
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:20
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Copper[7440-50-8]A
1.91
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 10:20
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:43
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
01/26/21 11:43
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 14:10
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffK
Notes
Toluene-d8
5.8
1
5.00
116 %
75-125
1A20026
EPA 8260D
01120121 14:10
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P6 Lab Sample ID:CE00125-10 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 12:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
19:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
19:57
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 29 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P6 Lab Sample ID:CE00125-10 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 12:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 19:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 19:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
59
1
50.0
119 %
53-136
IA19023
EPA 6260D
01/19/21 19:57
REF
Dibromofluoromethane
53
1
50.0
105 %
67-129
IA19023
EPA 6260D
01119121 19:57
REF
Toluene-d8
52
1
50.0
104 %
59-134
IA19023
EPA 8260D
01119121 19:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:48
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Barium [7440-39-3]^
58.8
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 11:10
JDH
Beryllium [7440-41-7]A
0.337
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 11:10
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:10
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:48
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:20
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Zinc[7440-66-6]^
4.89
J
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 14:35
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
4.8
1
5.00
95 %
75-125
1A20026
EPA 8260D
01120121 1425
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 30 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P7 Lab Sample ID:CE00125-11 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 11:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
20:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
20:27
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page
31 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P7 Lab Sample ID:CE00125-11 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 11:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 20:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 20:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
57
1
50.0
114 %
53-136
IA19023
EPA 6260D
01119121 20:27
REF
Dibromofluoromethane
51
1
50.0
101 %
67-129
IA19023
EPA 6260D
01119121 20:27
REF
Toluene-d8
52
1
50.0
105 %
59-134
IA19023
EPA 8260D
01119121 20:27
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:52
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Barium [7440-39-3]^
216
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Beryllium [7440-41-7]A
0.464
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 10:25
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:25
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Cobalt[7440-48-4]A
2.38
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Copper[7440-50-8]^
3.12
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Nickel[7440-02-O]^
4.14
J
ug/L
1
2.20
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:52
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:21
RLF
Vanadium [7440-62-2]^
2.31
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 15:00
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
5.1
1
5.00
101 %
75-125
1A20026
EPA 8260D
01120121 15:00
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 32 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P9 Lab Sample ID:CE00125-12 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 11:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
20:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
20:57
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page
33 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P9 Lab Sample ID:CE00125-12 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 11:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 20:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 20:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
53
1
50.0
107 %
53-136
IA19023
EPA 6260D
01119121 20:57
REF
Dibromofluoromethane
46
1
50.0
92 %
67-129
IA19023
EPA 6260D
01119121 20:57
REF
Toluene-d8
49
1
50.0
97 %
59-134
IA19023
EPA 6260D
01119121 20:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:56
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Barium [7440-39-3]^
116
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 11:12
JDH
Beryllium [7440-41-7]A
0.761
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 11:12
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:12
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Cobalt[7440-48-4]A
2.66
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 11:12
JDH
Copper[7440-50-8]^
2.03
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 11:12
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Nickel[7440-02-O]^
3.10
J
ug/L
1
2.20
10.0
lA18012
EPA 6010D
01/20/21 11:12
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:56
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:23
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 15:26
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
5.5
1
5.00
110 %
75-125
1A20026
EPA 8260D
01120121 15:26
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P11R Lab Sample ID:CE00125-13 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:28 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21 21:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21 21:27
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 35 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PllR Lab Sample ID:CE00125-13 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:28 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 21:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 21:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
58
1
50.0
115 %
53-136
IA19023
EPA 6260D
01119121 21:27
REF
Dibromofluoromethane
49
1
50.0
97 %
67-129
IA19023
EPA 6260D
01119121 21:27
REF
Toluene-d8
50
1
50.0
100 %
59-134
IA19023
EPA 6260D
01119121 21:27
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:01
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Barium [7440-39-3]^
99.2
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Beryllium [7440-41-7]A
1.93
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 11:15
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:15
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Cobalt[7440-48-4]A
2.38
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Copper[7440-50-8]^
7.10
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Nickel[7440-02-O]^
3.28
J
ug/L
1
2.20
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:01
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:24
RLF
Vanadium [7440-62-2]^
4.67
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Zinc[7440-66-6]^
39.8
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 15:51
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
5.5
1
5.00
110 %
75-125
1A20026
EPA 8260D
01120121 15:51
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 36 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CE00125-14 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21 21:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21 21:57
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 37 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CE00125-14 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 21:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 21:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
55
1
50.0
110 %
53-136
IA19023
EPA 6260D
01119121 21:57
REF
Dibromofluoromethane
50
1
50.0
101 %
67-129
IA19023
EPA 6260D
01119121 21:57
REF
Toluene-d8
50
1
50.0
100 %
59-134
IA19023
EPA 8260D
01119121 21:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:35
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Barium [7440-39-3]^
34.9
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 11:22
JDH
Beryllium [7440-41-7]A
0.553
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 11:22
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:22
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:35
RLF
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
01/26/21 12:35
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20026
EPA 8260D
01/20/21 16:16
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
5.0
1
5.00
99 %
75-125
1A20026
EPA 8260D
01120121 16:16
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 38 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13 Lab Sample ID:CE00125-15 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 14:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte FCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
QL-02,
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
1A20009
EPA 8260D
01/20/21
16:06
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
m,p-Xylenes [108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 39 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13 Lab Sample ID:CE00125-15 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 14:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A20009
EPA 8260D
01/20/21 16:06
RKY QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A20009
EPA 8260D
01/20/21 16:06
RKY
Xylenes (Total) [1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A20009
EPA 8260D
01/20/21 16:06
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
IA20009
EPA 6260D
01120121 16:06
RKY
Dibromofluoromethane
52
1
50.0
105 %
67-129
IA20009
EPA 6260D
01120121 16:06
RKY
Toluene-d8
61
1
50.0
122 %
59-134
IA20009
EPA 8260D
01120121 16:06
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:39
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Barium [7440-39-3]^
54.2
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:13
JDH
Beryllium [7440-41-7]^
0.204
J
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 11:13
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:13
JDH
Chromium [7440-47-3]^
1.73
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:13
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Copper[7440-50-8]^
2.16
J
ug/L
1
1.60
10.0
lA18015
EPA 6010D
01/21/21 11:13
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:39
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:29
RLF
Vanadium [7440-62-2]^
1.69
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:13
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 16:41
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
1A20026
EPA 8260D
01120121 16:41
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 40 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P131) Lab Sample ID:CE00125-16 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 14:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
22:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
22:57
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 41 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13D Lab Sample ID:CE00125-16 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 14:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 22:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 22:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
52
1
50.0
104 %
53-136
IA19023
EPA 6260D
01119121 22:57
REF
Dibromofluoromethane
45
1
50.0
90 %
67-129
IA19023
EPA 6260D
01119121 22:57
REF
Toluene-d8
47
1
50.0
94 %
59-134
IA19023
EPA 6260D
01119121 22:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:43
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Barium [7440-39-3]^
100
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:35
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:35
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:35
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:43
RLF
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:31
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Zinc [7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.5
J
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 17:07
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.6
1
5.00
92 %
75-125
1A20026
EPA 8260D
01120121 17:07
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 42 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P1611 Lab Sample ID:CE00125-17 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:13 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Acetone [67-64-1]A
12
J
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
20:34
REF
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
20:34
REF
Benzene [71-43-2]A
0.86
J
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 43 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CE00125-17 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:13 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 20:34 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 20:34 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
53
1
50.0
107 %
53-136
IA14039
EPA 6260D
01115121 20:34
REF
Dibromofluoromethane
48
1
50.0
95 %
67-129
IA14039
EPA 6260D
01115121 20:34
REF
Toluene-d8
49
1
50.0
98 %
59-134
IA14039
EPA 6260D
01115121 20:34
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
78
D
ug/L
2
1.6 4.0
1A20026
EPA 8260D
01/20/21 19:13
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes
Toluene-d8 5.4 1 5.00 108 % 75-125 1A20026 EPA 8260D 01120121 19:13 KKW
Description: 7401-P16R Lab Sample ID:CE00125-18 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:07 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 12:47
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Barium [7440-39-3]^
1100
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:37
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:37
]DH
Chromium [7440-47-3]^
2.88
J
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Nickel[7440-02-O]^
16.6
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 12:47
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:32
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 44 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CE00125-19 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:35 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21 21:04
REF
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21 21:04
REF
Benzene [71-43-2]A
0.43
J
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Chlorobenzene [108-90-7]A
4.3
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 45 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CE00125-19 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:35 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 21:04 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 21:04 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
52
1
50.0
103 %
53-136
IA14039
EPA 6260D
01115121 21:04
REF
Dibromofluoromethane
45
1
50.0
91 %
67-129
IA14039
EPA 6260D
01115121 21:04
REF
Toluene-d8
48
1
50.0
96 %
59-134
IA14039
EPA 6260D
01115121 21:04
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:52
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Barium [7440-39-3]^
147
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:40
JDH
Beryllium [7440-41-7]^
1.43
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 11:40
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:40
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Copper[7440-50-8]^
1.89
J
ug/L
1
1.60
10.0
lA18015
EPA 6010D
01/21/21 11:40
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Nickel[7440-02-O]^
2.79
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 11:40
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:52
RLF
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:34
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Zinc [7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
5.0
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 17:32
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
5.0
1
5.00
101 %
75-125
1A20026
EPA 8260D
01120121 1722
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 46 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CE00125-20 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 16:11 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
U
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
U
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
U
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,1-Dichloroethane [75-34-3]A
4.2
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,4-Dichlorobenzene [306-46-7]^
5.1
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
2-Butanone [78-93-3]^
1.3
U
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
2-Hexanone [591-78-6]^
0.88
U
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Acetone [67-64-1]^
10
U
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21 21:34
REF
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21 21:34
REF
Benzene [71-43-2]A
4.0
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Bromochloromethane [74-97-5]^
0.48
U
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Bromomethane [74-83-9]^
0.14
U
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
U
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Carbon tetrachloride [56-23-5]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Chlorobenzene [308-90-7]A
7.0
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Chloroethane [75-00-3]^
0.23
U
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Chloromethane [74-87-3]^
0.13
U
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
cis-1,2-Dichloroethene [156-59-2]A
2.7
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
U
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Dibromochloromethane [124-48-1]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Dibromomethane [74-95-3]^
0.27
U
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Ethylbenzene [100-41-4]A
1.8
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
m,p-Xylenes[108-38-3/306-42-3]A
0.42
J
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
o-Xylene [95-47-6]A
0.56
J
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 47 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CE00125-20 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 16:11 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.57 J ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 21:34 REF
Xylenes(Total)[1330-20-7]^ 0.98 J ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 21:34 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
51
1
50.0
101 %
53-136
IA14039
EPA 6260D
01115121 21:34
REF
Dibromofluoromethane
46
1
50.0
92 %
67-129
IA14039
EPA 6260D
01115121 21:34
REF
Toluene-d8
49
1
50.0
97 %
59-134
IA14039
EPA 6260D
01115121 21:34
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
160
D
ug/L
2.5
2.0 5.0
1A20026
EPA 8260D
01/20/21 19:38
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes
Toluene-d8 5.7 1 5.00 113 % 75-125 1A20026 EPA 8260D 01120121 19:38 KKW
Description: 7401-P19 Lab Sample ID:CE00125-21 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 12:56
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Barium [7440-39-3]^
1870
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Beryllium [7440-41-7]^
15.3
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:42
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:42
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Cobalt[7440-48-4]^
19.3
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Copper[7440-50-8]^
1.72
J
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Lead [7439-92-1]^
6.07
J
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Nickel[7440-02-O]^
29.4
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Selenium [7782-49-2]^
2.08
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 12:56
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:35
RLF
Vanadium [7440-62-2]^
1.46
J
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
Zinc[7440-66-6]^
120
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:42
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 48 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CE00125-22 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 16:35 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
22:04
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
22:04
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 49 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CE00125-22 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 16:35 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 22:04 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 22:04 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
52
1
50.0
105 %
53-136
IA14039
EPA 6260D
01115121 22:04
REF
Dibromofluoromethane
48
1
50.0
96 %
67-129
IA14039
EPA 6260D
01115121 22:04
REF
Toluene-d8
48
1
50.0
96 %
59-134
IA14039
EPA 6260D
01115121 22:04
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
2.1
ug/L
1
0.80 2.0
1A20026
EPA 8260D
01/20/21 17:57
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes
Toluene-d8 6.0 1 5.00 119 % 75-125 1A20026 EPA 8260D 01120121 17:57 KKW
Description: 7401-P20R Lab Sample ID:CE00125-23 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:18 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 13:00
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Barium [7440-39-3]^
51.4
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Beryllium [7440-41-7]^
1.66
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:45
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:45
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 13:00
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:37
RLF
Vanadium [7440-62-2]^
2.44
J
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Zinc[7440-66-6]^
12.1
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 50 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P201) Lab Sample ID:CE00125-24 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:20 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte FCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dichloroethane [507-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
QL-02,
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
1A20009
EPA 8260D
01/20/21
19:20
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
m,p-Xylenes [108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 51 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20D Lab Sample ID:CE00125-24 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:20 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A20009
EPA 8260D
01/20/21 19:20
RKY QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A20009
EPA 8260D
01/20/21 19:20
RKY
Xylenes (Total) [1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A20009
EPA 8260D
01/20/21 19:20
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
51
1
50.0
103 %
53-136
IA20009
EPA 6260D
01120121 19:20
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA20009
EPA 6260D
01120121 19:20
RKY
Toluene-d8
63
1
50.0
125 %
59-134
IA20009
EPA 8260D
01120121 19:20
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 08:29
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Barium [7440-39-3]^
112
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Beryllium [7440-41-7]^
8.87
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 11:47
JDH
Cadmium [7440-43-9]^
0.756
J
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:47
JDH
Chromium [7440-47-3]^
12.9
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Lead [7439-92-1]^
5.43
J
ug/L
1
3.10
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Nickel[7440-02-O]^
4.31
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 08:33
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Thallium [7440-28-0]^
1.10
UD
ug/L
10
1.10
10.0
1A18022
EPA 6020B
01/26/21 08:56
RLF
QI-03
Vanadium [7440-62-2]^
12.6
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Zinc[7440-66-6]^
20.1
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 18:23
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
108 %
75-125
1A20026
EPA 8260D
01120121 18:23
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 52 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P21 Lab Sample ID:CE00125-25 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte FCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dichloroethane [507-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
QL-02,
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
1A20009
EPA 8260D
01/20/21
19:48
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
m,p-Xylenes [108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 53 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P21 Lab Sample ID:CE00125-25 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A20009
EPA 8260D
01/20/21 19:48
RKY QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A20009
EPA 8260D
01/20/21 19:48
RKY
Xylenes (Total) [1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A20009
EPA 8260D
01/20/21 19:48
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
49
1
50.0
98 %
53-136
IA20009
EPA 6260D
01/20/21 19:48
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA20009
EPA 6260D
01120121 19:48
RKY
Toluene-d8
63
1
50.0
125 %
59-134
IA20009
EPA 6260D
01120121 19:48
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:04
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Barium [7440-39-3]^
58.0
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:49
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:49
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:49
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Nickel[7440-02-O]^
2.53
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 11:49
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 09:04
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:39
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 18:48
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.3
1
5.00
107 %
75-125
1A20026
EPA 8260D
01120121 18:48
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 54 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P23 Lab Sample ID:CE00125-26 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 14:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
22:34
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
22:34
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 55 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P23 Lab Sample ID:CE00125-26 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 14:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 22:34 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 22:34 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
IA14039
EPA 6260D
01115121 22:34
REF
Dibromofluoromethane
49
1
50.0
98 %
67-129
IA14039
EPA 6260D
01115121 22:34
REF
Toluene-d8
49
1
50.0
98 %
59-134
IA14039
EPA 6260D
01115121 22:34
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
IA20035
EPA 8260D
01/21/21 00:15
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes
Toluene-d8 5.7 1 5.00 113 % 75-125 1A20035 EPA 8260D 01121121 00:15 KKW
Description: 7401-P23 Lab Sample ID:CE00125-27 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2108:45 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020E
01/26/21 09:09
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Barium [7440-39-3]^
19.6
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:52
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:52
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020E
01/26/21 09:09
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020E
01/26/21 09:09
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Zinc[7440-66-6]^
7.76
J
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 56 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CE00125-28 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:45 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 18:30
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Benzene [71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 57 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CE00125-28 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:45 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 18:30 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 18:30 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
49
1
50.0
97 %
53-136
IA19015
EPA 6260D
01119121 18:30
REF
Dibromofluoromethane
53
1
50.0
105 %
67-129
IA19015
EPA 6260D
01119121 18:30
REF
Toluene-d8
61
1
50.0
123 %
59-134
IA19015
EPA 6260D
01119121 18:30
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
IA20035
EPA 8260D
01/21/21 00:40
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes
Toluene-d8 4.4 1 5.00 87 % 75-125 1A20035 EPA 8260D 01121121 00:40 KKW
Description: 7401-P28 Lab Sample ID:CE00125-29 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:05 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020E
01/26/21 09:39
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Barium [7440-39-3]^
38.4
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Beryllium [7440-41-7]^
0.741
J
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:54
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:54
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Copper[7440-50-8]^
2.49
J
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Nickel[7440-02-O]^
3.16
J
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020E
01/26/21 09:39
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020E
02/04/21 15:40
RLF
Vanadium [7440-62-2]^
1.53
J
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Zinc[7440-66-6]^
14.0
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 58 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CE00125-30 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 13:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,4-Dichlorobenzene [306-46-7]^
0.89
J
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 18:58
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Benzene [71-43-2]A
1.6
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Chlorobenzene [108-90-7]A
5.1
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Ethylbenzene [100-41-4]A
0.48
J
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 59 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CE00125-30 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 13:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 18:58 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 18:58 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA19015
EPA 6260D
01119121 18:58
REF
Dibromofluoromethane
51
1
50.0
101 %
67-129
IA19015
EPA 6260D
01119121 16:58
REF
Toluene-d8
62
1
50.0
123 %
59-134
IA19015
EPA 8260D
01119121 16:58
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:43
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:56
JDH
Barium [7440-39-3]^
1290
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Beryllium [7440-41-7]A
0.980
J
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 11:56
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:56
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:56
JDH
Cobalt[7440-48-4]A
4.66
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:56
JDH
Lead [7439-92-1]A
18.0
ug/L
1
3.10
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Nickel[7440-02-O]^
7.50
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Selenium [7782-49-2]^
2.54
ug/L
2
1.82
2.00
lAlS022
EPA 6020B
01/26/21 09:43
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:56
JDH
Thallium [7440-28-0]^
0.252
J
ug/L
2
0.220
2.00
lAlS022
EPA 6020B
02/04/21 15:42
RLF
Vanadium [7440-62-2]^
36.1
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Zinc[7440-66-6]^
5.63
J
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]A
140
D
ug/L
5
4.0
10
1A22042
EPA 8260D
01/22/21 18:06
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
5.4
1
5.00
109 %
75-125
1A22042
EPA 8260D
01122121 18:06
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 60 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CE00125-31 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/14/21 17:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte FCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 19:25
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Benzene [71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 61 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CE00125-31 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/14/21 17:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 19:25 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 19:25 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA19015
EPA 6260D
01/19/21 19:25
REF
Dibromofluoromethane
52
1
50.0
103 %
67-129
IA19015
EPA 6260D
01119121 19:25
REF
Toluene-c48
61
1
50.0
121 %
59-134
IA19015
EPA 8260D
01119121 19:25
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:48
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:42
JDH
Barium [7440-39-3]^
23.9
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Beryllium [7440-41-7]A
0.212
J
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 12:42
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:42
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:42
JDH
Cobalt[7440-48-4]A
8.02
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:42
JDH
Lead [7439-92-1]A
3.54
J
ug/L
1
3.10
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Nickel[7440-02-O]^
3.41
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 09:48
RLF
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:42
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:43
RLF
Vanadium [7440-62-2]^
2.15
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Zinc[7440-66-6]^
15.3
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20035
EPA 8260D
01/21/21 01:06
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
107 %
75-125
1A20035
EPA 8260D
01121121 01:06
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 62 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CE00125-32 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/14/21 15:37 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte FCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 19:53
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Benzene [71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 63 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CE00125-32 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/14/21 15:37 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 19:53 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 19:53 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
101 %
53-136
IA19015
EPA 6260D
01119121 19:53
REF
Dibromofluoromethane
52
1
50.0
104 %
67-129
IA19015
EPA 6260D
01119121 19:53
REF
Toluene-c48
62
1
50.0
124 %
59-134
IA19015
EPA 8260D
01119121 19:53
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:52
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Barium [7440-39-3]^
40.3
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:44
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:44
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:44
JDH
Chromium [7440-47-3]^
1.44
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:44
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 09:52
RLF
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:48
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Zinc[7440-66-6]^
18.8
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 12:44
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA20035
EPA 8260D
01/21/21 01:31
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
1A20035
EPA 8260D
01121121 01:31
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 64 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW4 Lab Sample ID:CE00125-33 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/13/21 17:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte FCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA18028
EPA 8260D
01/18/21
20:51
REF
QL-02,
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
1A18028
EPA 8260D
01/18/21
20:51
REF
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
1A18028
EPA 8260D
01/18/21
20:51
REF
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
1A18028
EPA 8260D
01/18/21
20:51
REF
m,p-Xylenes [108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 65 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW4 Lab Sample ID:CE00125-33 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/13/21 17:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A18028
EPA 8260D
01/18/21 20:51
REF QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A18028
EPA 8260D
01/18/21 20:51
REF
Xylenes (Total) [1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A18028
EPA 8260D
01/18/21 20:51
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
48
1
50.0
96 %
53-136
IA16028
EPA 6260D
01118121 20:51
REF
Dibromofluoromethane
53
1
50.0
107 %
67-129
IA16028
EPA 6260D
01116121 20:51
REF
Toluene-d8
61
1
50.0
121 %
59-134
IA16028
EPA 6260D
01116121 20:51
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:56
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Barium [7440-39-3]^
40.0
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:46
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:46
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:46
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 09:56
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:50
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Zinc[7440-66-6]^
5.97
J
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]A
3.5
ug/L
1
0.80
2.0
1A20035
EPA 8260D
01/21/21 01:56
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.3
1
5.00
105 %
75-125
1A20035
EPA 8260D
01121121 01:56
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 66 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ1 Lab Sample ID:CE00125-34 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 20:20
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 67 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ1 Lab Sample ID:CE00125-34 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 20:20 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 20:20 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
48
1
50.0
96 %
53-136
IA19015
EPA 6260D
01119121 20:20
REF
Dibromofluoromethane
51
1
50.0
102 %
67-129
IA19015
EPA 6260D
01119121 20:20
REF
Toluene-d8
61
1
50.0
122 %
59-134
IA19015
EPA 6260D
01119121 20:20
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 10:01
RLF
Arsenic[7440-38-2]^
100
ug/L
1
7.60
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Barium [7440-39-3]^
101
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:48
JDH
Cadmium [7440-43-9]^
1.72
ug/L
1
0.360
1.00
lA18015
EPA 6010D
01/21/21 12:48
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:48
JDH
Cobalt[7440-48-4]^
2.21
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Copper[7440-50-8]^
3.41
J
ug/L
1
1.60
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Lead [7439-92-1]^
8.46
J
ug/L
1
3.10
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Nickel[7440-02-O]^
3.31
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 10:01
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:48
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:51
RLF
Vanadium [7440-62-2]^
12.4
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Zinc[7440-66-6]^
26.4
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
2.1
ug/L
1
0.80
2.0
1A22042
EPA 8260D
01/22/21 17:40
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
108 %
75-125
1A22042
EPA 8260D
01122121 17:40
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 68 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ2 Lab Sample ID:CE00125-35 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:30 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 20:47
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 69 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ2 Lab Sample ID:CE00125-35 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:30 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 20:47 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 20:47 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
49
1
50.0
97 %
53-136
IA19015
EPA 6260D
01119121 20:47
REF
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA19015
EPA 6260D
01119121 20:47
REF
Toluene-d8
62
1
50.0
124 %
59-134
IA19015
EPA 6260D
01119121 20:47
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 10:05
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Barium [7440-39-3]^
190
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:51
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:51
JDH
Cadmium [7440-43-9]^
0.360
J
ug/L
1
0.360
1.00
lA18015
EPA 6010D
01/21/21 12:51
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 10:05
RLF
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:53
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Zinc[7440-66-6]^
18.3
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 12:51
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]A
3.6
ug/L
1
0.80
2.0
1A20035
EPA 8260D
01/21/21 02:21
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
104 %
75-125
1A20035
EPA 8260D
01121121 02:21
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 70 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CE00125-36 Received: 01/15/21 10:00
Matrix: Water Sampled:01/13/21 16:57 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte FCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA18028
EPA 8260D
01/18/21
16:17
REF
QL-02,
QV-01
2-Hexanone [591-78-6]^
1.9
1
ug/L
1
0.88
5.0
IA18028
EPA 8260D
01/18/21
16:17
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
Acetone [67-64-1]^
10
U
ug/L
1
10
20
1A18028
EPA 8260D
01/18/21
16:17
REF
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Bromomethane [74-83-9]^
0.14
U
ug/L
1
0.14
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Carbon disulfide [75-15-0]^
53
ug/L
1
1.5
5.0
IA18028
EPA 8260D
01/18/21
16:17
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
1A18028
EPA 8260D
01/18/21
16:17
REF
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 71 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CE00125-36 Received: 01/15/21 10:00
Matrix: Water Sampled:01/13/21 16:57 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A18028
EPA 8260D
01/18/21 16:17
REF QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A18028
EPA 8260D
01/18/21 16:17
REF
Xylenes (Total) [1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A18028
EPA 8260D
01/18/21 16:17
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA16028
EPA 6260D
01118121 16:17
REF
Dibromofluoromethane
54
1
50.0
108 %
67-129
IA16028
EPA 6260D
01116121 16:17
REF
Toluene-d8
61
1
50.0
122 %
59-134
IA16028
EPA 8260D
01116121 16:17
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 10:09
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Barium [7440-39-3]^
1.10
U
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:53
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:53
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 10:09
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:54
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Zinc[7440-66-6]^
114
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20035
EPA 8260D
01/21/21 02:47
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
104 %
75-125
1A20035
EPA 8260D
01121121 02:47
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 72 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CE00125-37 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/14/2109:30 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Acetone [67-64-1]A
14
J
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 17:08
REF
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Benzene [71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 73 of 99

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ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CE00125-37 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/14/2109:30 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 17:08 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 17:08 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
IA19015
EPA 6260D
01/19/21 17:08
REF
Dibromofluoromethane
52
1
50.0
104 %
67-129
IA19015
EPA 6260D
01119121 17:08
REF
Toluene-d8
61
1
50.0
122 %
59-134
IA19015
EPA 8260D
01119121 17:08
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 10:13
RLF
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Barium [7440-39-3]^
1.10
u
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:56
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:56
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 10:13
RLF
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
1A18022
EPA 6020B
01/26/21 10:13
RLF
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
IA22042
EPA 8260D
01/22/21 11:21
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.0
1
5.00
101 %
75-125
1A22042
EPA 8260D
01122121 11:21
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 74 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CE00125-38 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/13/2100:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dichloroethane [507-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Acetone [67-64-1]A
67
ug/L
1
10
20
IA25038
EPA 8260D
01/25/21 19:44
RKY
0-01
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
IA25038
EPA 8260D
01/25/21 19:44
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Ethylbenzene[500-41-4]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Iodomethane[74-88-4]A
1.7
U
ug/L
1
1.7
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 75 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CE00125-38 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/13/2100:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL POLL
Batch
Method
Analyzed
AX Notes
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32 1.0
1A25038
EPA 8260D
01/25/21 19:44
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45 3.0
1A25038
EPA 8260D
01/25/21 19:44
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA25038
EPA 6260D
01125121 19:44
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA25038
EPA 6260D
01125121 19:44
RKY
Toluene-d8
62
1
50.0
124 %
59-134
IA25038
EPA 8260D
01125121 19:44
RKY
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 76 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CE00125-39 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/13/2100:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Acetone [67-64-1]A
31
ug/L
1
10
20
IA25038
EPA 8260D
01/25/21
20:12
RKY
0-01
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
IA25038
EPA 8260D
01/25/21
20:12
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Iodomethane[74-88-4]A
1.7
U
ug/L
1
1.7
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 77 of 99

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ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CE00125-39 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/13/2100:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL POLL
Batch
Method
Analyzed
Ay Notes
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32 1.0
1A25038
EPA 8260D
01/25/21 20:12
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45 3.0
1A25038
EPA 8260D
01/25/21 20:12
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
50
1
50.0
99 %
53-136
IA25038
EPA 6260D
01125121 20:12
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA25038
EPA 6260D
01125121 20:12
RKY
Toluene-d8
61
1
50.0
122 %
59-134
IA25038
EPA 6260D
01125121 20:12
RKY
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 78 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A14039 - EPA 5030E MS
Blank (1A14039-BLK1) Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 14:32
Analvte
Result
Flaq
POL
Units
1, 1, 1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 79 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IA14039 - EPA 5030E MS - Continued
Blank (SA34039-BLK1) Continued Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 14:32
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene
54
u91L
50.0 107 53-136
Dibromofluoromethane
49
u91L
50.0 98 67-129
Toluene-d8
49
u91L
50.0 98 59-134
LCS (1A14039-BS1)
Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 12:32
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
107
75-133
Benzene
18
1.0
ug/L
20.0
91
80-134
Chlorobenzene
18
1.0
ug/L
20.0
92
80-120
Toluene
19
1.0
ug/L
20.0
93
71-120
Trichloroethene
19
1.0
ug/L
20.0
93
74-120
4-Bromofluorobenzene
55
u91L
50.0
109
53-136
Dibromofluoromethane
50
u91L
50.0
99
67-129
Toluene-d8
52
u91L
50.0
105
59-134
Matrix Spike (3A14039-MS1)
Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 13:02
Source: CE00684-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
24
1.0
ug/L
20.0
0.21 U
118
75-133
Benzene
18
1.0
ug/L
20.0
0.15 U
92
80-134
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
92
80-120
Toluene
18
1.0
ug/L
20.0
0.14 U
92
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
97
74-120
4-Bromofluorobenzene
52
u91L
50.0
104
53-136
Dibromofluoromethane
48
u91L
50.0
97
67-129
Toluene-d8
49
u91L
50.0
98
59-134
Matrix Spike Dup (3A14039-MSD1)
Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 13:32
Source: CE00684-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
26
1.0
ug/L
20.0
0.21 U
128
75-133
8
20
Benzene
21
1.0
ug/L
20.0
0.15 U
103
80-134
11
17
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
103
80-120
11
16
Toluene
20
1.0
ug/L
20.0
0.14 U
102
71-120
10
17
Trichloroethene
23
1.0
ug/L
20.0
0.15 U
113
74-120
15
22
4-Bromofluorobenzene 57 u91L 50.0 115 53-136
Dibromofluoromethane 53 u91L 50.0 106 67-129
Toluene-d8 57 u91L 50.0 113 59-134
Batch IA18028 - EPA 5030E MS
Blank (3A38028-BLK3) Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 15:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L
1,1,1-Trichloroethane 0.12 U 1.0 ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 80 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IAIB02B - EPA 5030E MS - Continued
Blank (SA38028-BLK1) Continued Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 15:50
Analvte
Result
Flaq
POL
Units
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 50 u9/L 50.0 100 53-136
Dibromofluoromethane 53 u9/L 50.0 105 67-129
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 81 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IAIB02B - EPA 5030E MS - Continued
Blank (SA38028-BLK1) Continued Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 15:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 62 u91L 50.0 124 59-134
LCS (1A18028-BS1) Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 13:59
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
114
75-133
Benzene
22
1.0
ug/L
20.0
110
80-134
Chlorobenzene
22
1.0
ug/L
20.0
108
80-120
Toluene
22
1.0
ug/L
20.0
109
71-120
Trichloroethene
21
1.0
ug/L
20.0
107
74-120
4-Bromofluorobenzene
49
ug/L
50.0
99
53-136
Dibromofluoromethane
51
ug/L
50.0
103
67-129
Toluene-d8
62
ug/L
50.0
123
59-134
Matrix Spike (1A18028-MS1)
Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 14:27
Source: CE00929-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
114
75-133
Benzene
22
1.0
ug/L
20.0
0.15 U
109
80-134
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
108
80-120
Toluene
22
1.0
ug/L
20.0
0.14 U
109
71-120
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
105
74-120
4-Bromofluorobenzene
51
ug/L
50.0
101
53-136
Dibromofluoromethane
52
ug/L
50.0
104
67-129
Toluene-d8
62
u91L
50.0
125
59-134
Matrix Spike Dup (3A18028-MSD1)
Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 14:55
Source: CE00929-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
22
1.0
ug/L
20.0
0.21 U
112
75-133
2
20
Benzene
21
1.0
ug/L
20.0
0.15 U
104
80-134
5
17
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
106
80-120
2
16
Toluene
21
1.0
ug/L
20.0
0.14 U
104
71-120
5
17
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
100
74-120
4
22
4-Bromofluorobenzene 51 u91L 50.0 102 53-136
Dibromofluoromethane 53 u91L 50.0 106 67-129
Toluene-& 62 u91L 50.0 125 59-134
Batch IA19015 - EPA 5030E MS
Blank (lA19015-BLK3) Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 15:45
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
FINAL
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full. Page 82 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A19015 - EPA 5030E MS - Continued
Blank (SA3901S-BLK1) Continued Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 15:45
Analvte
Result
Flaq
POL
Units
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 51 u91L 50.0 102 53-136
Dibromofluoromethane 52 u91L 50.0 104 67-129
Toluene-d8 62 u91L 50.0 124 59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 83 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A19015 - EPA 5030E MS - Continued
LCS (1A19015-BS1) Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 13:55
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
24
1.0
ug/L
20.0
122
75-133
Benzene
23
1.0
ug/L
20.0
114
80-134
Chlorobenzene
23
1.0
ug/L
20.0
114
80-120
Toluene
23
1.0
ug/L
20.0
113
71-120
Trichloroethene
22
1.0
ug/L
20.0
111
74-120
4-Bromofluorobenzene
50
u91L
50.0
100
53-136
Dibromofluoromethane
51
u91L
50.0
102
67-129
Toluene-d8
61
u91L
50.0
121
59-134
Matrix Spike (3A19015-MS1)
Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 14:22
Source: CE00929-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
117
75-133
Benzene
22
1.0
ug/L
20.0
0.15 U
111
80-134
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
111
80-120
Toluene
22
1.0
ug/L
20.0
0.14 U
110
71-120
Trichloroethene
22
1.0
ug/L
20.0
0.15 U
109
74-120
4-Bromofluorobenzene
51
u91L
50.0
102
53-136
Dibromofluoromethane
51
u91L
50.0
103
67-129
Toluene-d8
62
u91L
50.0
124
59-134
Matrix Spike Dup (3A19015-MSD1)
Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 14:50
Source: CE00929-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
117
75-133
0.4
20
Benzene
22
1.0
ug/L
20.0
0.15 U
109
80-134
1
17
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
110
80-120
0.7
16
Toluene
22
1.0
ug/L
20.0
0.14 U
111
71-120
0.6
17
Trichloroethene
22
1.0
ug/L
20.0
0.15 U
108
74-120
2
22
4-Bromofluorobenzene
49
u91L
50.0
99
53-136
Dibromofluoromethane
50
u91L
50.0
101
67-129
Toluene-d8
60
u91L
50.0
121
59-134
Batch IA19023 - EPA 5030B MS
Blank (lA19023-BLK1) Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 16:27
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
FINAL
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full. Page 84 of 99

(� �Eo
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IA19023 - EPA 5030E MS - Continued
Blank (SA39023-BLK1) Continued Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 16:27
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit Notes
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
4-Bromofluorobenzene
57
ug/L
50.0
114
53-136
Dibromofluoromethane
51
ug/L
50.0
102
67-129
Toluene-d8
53
u91L
50.0
106
59-134
LCS (1A19023-BSI)
Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 14:13
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit Notes
1,1-Dichloroethene
22
1.0
ug/L
20.0
111
75-133
Benzene
18
1.0
ug/L
20.0
90
80-134
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be reproduced in
full.
Page 85 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A19023 - EPA 5030E MS - Continued
LCS (1A19023-BS1) Continued Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 14:13
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Chlorobenzene
18
1.0
ug/L
20.0 92 80-120
Toluene
19
1.0
ug/L
20.0 93 71-120
Trichloroethene
20
1.0
ug/L
20.0 98 74-120
4-Bromofluorobenzene
59
ug/L
50.0 117 53-136
Dibromofluoromethane
53
u91L
50.0 106 67-129
Toluene-d8
54
u91L
50.0 107 59-134
Matrix Spike (3A19023-MS1)
Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 14:56
Source: CE00929-10
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
115
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
93
80-134
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
94
80-120
Toluene
19
1.0
ug/L
20.0
0.14 U
93
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
94
74-120
4-Bromofluorobenzene
61
u91L
50.0
123
53-136
Dibromofluoromethane
55
ug/L
50.0
110
67-129
Toluene-d8
54
u91L
50.0
108
59-134
Matrix Spike Dup (3A19023-MSD1)
Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 15:26
Source: CE00929-10
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
105
75-133
9
20
Benzene
18
1.0
ug/L
20.0
0.15 U
88
80-134
6
17
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
89
80-120
5
16
Toluene
18
1.0
ug/L
20.0
0.14 U
90
71-120
4
17
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
96
74-120
1
22
4-Bromofluorobenzene 56 u91L 50.0 112 53-136
Dibromofluoromethane 51 u91L 50.0 102 67-129
Toluene-d8 52 u91L 50.0 104 59-134
Batch IA20009 - EPA 5030E MS
Blank (3A20009-BLK3) Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 15:10
Analvte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1, 2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dich loroethane
1,1-Dichloroethene
1, 2, 3-Trich I o rop ropa ne
1,2-Di bromo-3-ch loropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
FINAL
Spike Source %REC
Result
Flaq
POL
Units Level Result %REC Limits
0.17
U
1.0
ug/L
0.12
U
1.0
ug/L
0.28
U
1.0
ug/L
0.14
U
1.0
ug/L
0.13
U
1.0
ug/L
0.21
U
1.0
ug/L
0.23
U
1.0
ug/L
0.48
U
1.0
ug/L
0.66
U
1.0
ug/L
0.19
U
1.0
ug/L
0.21
U
1.0
ug/L
0.10
U
1.0
ug/L
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit Notes
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IA20009 - EPA 5030E MS - Continued
Blank (1A20009-BLK1) Continued Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 15:10
Analvte
Result
Flaq
POL
Units
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 50
u91L
50.0 100 53-136
Dibromofluoromethane 51
u91L
50.0 101 67-129
Toluene-d8 61
u91L
50.0 122 59-134
LCS (1A20009-BSI)
Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 13:18
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
113
75-133
Benzene
22
1.0
ug/L
20.0
109
80-134
Chlorobenzene
21
1.0
ug/L
20.0
105
80-120
Toluene
22
1.0
ug/L
20.0
108
71-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 87 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IA20009 - EPA 5030E MS - Continued
LCS (1A20009-BSI) Continued Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 13:18
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Trichloroethene
21
1.0
ug/L
20.0
104
74-120
4-Bromofluorobenzene
49
u91L
50.0
98
53-136
Dibromofluoromethane
50
u91L
50.0
100
67-129
Toluene-d8
62
u91L
50.0
123
59-134
Matrix Spike (1A20009-MS1)
Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 13:46
Source: CE01004-05
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
22
1.0
ug/L
20.0
0.21 U
110
75-133
Benzene
22
1.0
ug/L
20.0
0.15 U
109
80-134
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
108
80-120
Toluene
22
1.0
ug/L
20.0
0.14 U
108
71-120
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
105
74-120
4-Bromofluorobenzene
51
u91L
50.0
102
53-136
Dibromofluoromethane
49
u91L
50.0
96
67-129
Toluene-d8
62
u91L
50.0
124
59-134
Matrix Spike Dup (1A20009-MSD1)
Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 14:14
Source: CE01004-05
Spike
Source
%REC
RPD
Analvte
Result Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
106
75-133
4
20
Benzene
21
1.0
ug/L
20.0
0.15 U
107
80-134
2
17
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
107
80-120
2
16
Toluene
21
1.0
ug/L
20.0
0.14 U
106
71-120
1
17
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
102
74-120
3
22
4-Bromofluorobenzene 49 u91L 50.0 99 53-136
Dibromofluoromethane 49 u91L 50.0 98 67-129
Toluene-d8 61 u91L 50.0 123 59-134
Batch IA25038 - EPA 5030E MS
Blank (1A25038-BLK1) Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 18:50
Analvte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,3-Trichloropropane
1,2-Di bromo-3-ch loropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,4-Dichlorobenzene
2-Butanone
FINAL
Spike Source %REC
Result
Flaq
POL
Units Level Result %REC Limits
0.17
U
1.0
ug/L
0.12
U
1.0
ug/L
0.28
U
1.0
ug/L
0.14
U
1.0
ug/L
0.13
U
1.0
ug/L
0.21
U
1.0
ug/L
0.23
U
1.0
ug/L
0.48
U
1.0
ug/L
0.66
U
1.0
ug/L
0.19
U
1.0
ug/L
0.21
U
1.0
ug/L
0.10
U
1.0
ug/L
0.19
U
1.0
ug/L
1.3
U
5.0
ug/L
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit Notes
Page 88 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IA2503B - EPA 5030E MS - Continued
Blank (1A25038-BLK1) Continued Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 18:50
Analvte
Result
Flaq
POL
Units
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 51
u91L
50.0 102 53-136
Dibromofluoromethane 52
u91L
50.0 104 67-129
Toluene-d8 61
u91L
50.0 123 59-134
LCS (1A25038-BSI)
Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 17:00
Spike
Source
%REC RPD
Analvte
Result Flaq
Q
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
22
1.0
ug/L
20.0
108
75-133
Benzene
20
1.0
ug/L
20.0
101
80-134
Chlorobenzene
22
1.0
ug/L
20.0
109
80-120
Toluene
21
1.0
ug/L
20.0
104
71-120
Trichloroethene
22
1.0
ug/L
20.0
110
74-120
4-Bromofluorobenzene 49 u91L 50.0 97 53-136
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 89 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A2503B - EPA 5030E MS - Continued
LCS (1A25038-BS1) Continued Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 17:00
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Dibromofluoromethane 50 u91L 50.0 101 67-129
Toluene-& 61 u91L 50.0 122 59-134
Matrix Spike (3A25038-MS1) Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 17:27
Source: CE01183-03
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
25
1.0
ug/L
20.0
0.21 U
123
75-133
Benzene
21
1.0
ug/L
20.0
0.15 U
103
80-134
Chlorobenzene
23
1.0
ug/L
20.0
0.17 U
115
80-120
Toluene
21
1.0
ug/L
20.0
0.14 U
106
71-120
Trichloroethene
23
1.0
ug/L
20.0
0.15 U
114
74-120
4-Bromofluorobenzene
49
u91L
50.0
96
53-136
Dibromofluoromethane
52
u91L
50.0
103
67-129
Toluene-d8
60
u91L
50.0
120
59-134
Matrix Spike Dup (1A25038-MSDS)
Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 17:55
Source: CE01183-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
24
1.0
ug/L
20.0
0.21 U
118
75-133
4
20
Benzene
21
1.0
ug/L
20.0
0.15 U
107
80-134
4
17
Chlorobenzene
23
1.0
ug/L
20.0
0.17 U
113
80-120
2
16
Toluene
21
1.0
ug/L
20.0
0.14 U
105
71-120
0.4
17
Trichloroethene
22
1.0
ug/L
20.0
0.15 U
112
74-120
2
22
4-Bromofluorobenzene 50 u91L 50.0 99 53-136
Dibromofluoromethane 54 u91L 50.0 108 67-129
Toluene-d8 61 u91L 50.0 123 59-134
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch IA28012 - EPA 3005A
Blank (3A38012-BLK3) Prepared: 01/18/2021 09:22 Analyzed: 01/20/2021 09:36
Analvte
Result
Flaq
POL
Units
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 90 of 99

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1A16012 - EPA 3005A - Continued
LCS (IA18012-BSI) Prepared: 01/18/2021 09:22 Analyzed: 01/20/2021 09:44
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limi
RPD
Limit
Notes
Arsenic
205
10.0
ug/L
200
102
80-120
Barium
219
10.0
ug/L
200
109
80-120
Beryllium
20.4
1.00
ug/L
20.0
102
80-120
Cadmium
20.8
1.00
ug/L
20.0
104
80-120
Chromium
208
10.0
ug/L
200
104
80-120
Cobalt
211
10.0
ug/L
200
105
80-120
Copper
205
10.0
ug/L
200
103
80-120
Lead
207
10.0
ug/L
200
104
80-120
Nickel
218
10.0
ug/L
200
109
80-120
Silver
214
10.0
ug/L
200
107
80-120
Vanadium
206
10.0
ug/L
200
103
80-120
Zinc
212
10.0
ug/L
200
106
80-120
Matrix Spike (1A18012-MS1)
Prepared: 01/18/2021
09:22 Analyzed: 01/20/2021 09:47
Source: CE00125-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limi
RPD
Limit
Notes
Arsenic
210
10.0
ug/L
200
7.60 U
105
75-125
Barium
276
10.0
ug/L
200
54.6
111
75-125
Beryllium
21.4
1.00
ug/L
20.0
0.348
105
75-125
Cadmium
21.0
1.00
ug/L
20.0
0.360 U
105
75-125
Chromium
212
10.0
ug/L
200
1.40 U
106
75-125
Cobalt
212
10.0
ug/L
200
1.40 U
106
75-125
Copper
208
10.0
ug/L
200
1.60 U
104
75-125
Lead
208
10.0
ug/L
200
3.10 U
104
75-125
Nickel
220
10.0
ug/L
200
2.20 U
110
75-125
Silver
215
10.0
ug/L
200
1.90 U
107
75-125
Vanadium
211
10.0
ug/L
200
1.40 U
105
75-125
Zinc
217
10.0
ug/L
200
4.40 U
109
75-125
Matrix Spike Dup (1AI8012-MSDI)
Prepared: 01/18/2021
09:22 Analyzed: 01/20/2021 09:49
Source: CE00125-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limi
RPD
Limit
Notes
Arsenic
212
10.0
ug/L
200
7.60 U
106
75-125
0.9
20
Barium
279
10.0
ug/L
200
54.6
112
75-125
0.8
20
Beryllium
21.6
1.00
ug/L
20.0
0.348
106
75-125
1
20
Cadmium
21.2
1.00
ug/L
20.0
0.360 U
106
75-125
0.6
20
Chromium
215
10.0
ug/L
200
1.40 U
108
75-125
1
20
Cobalt
214
10.0
ug/L
200
1.40 U
107
75-125
0.8
20
Copper
210
10.0
ug/L
200
1.60 U
105
75-125
1
20
Lead
210
10.0
ug/L
200
3.10 U
105
75-125
1
20
Nickel
223
10.0
ug/L
200
2.20 U
111
75-125
1
20
Silver
217
10.0
ug/L
200
1.90 U
109
75-125
1
20
Vanadium
213
10.0
ug/L
200
1.40 U
107
75-125
1
20
Zinc
218
10.0
ug/L
200
4.40 U
109
75-125
0.2
20
Post Spike (1A18012-PS1)
Prepared: 01/18/2021
09:22 Analyzed: 01/20/2021 09:52
Source: CE00125-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be reproduced in
full.
Page 91 of 99

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1AlB012 - EPA 3005A - Continued
Post Spike (SA38012-PS3) Continued
Prepared: 01/18/2021 09:22 Analyzed: 01/20/2021 09:52
Source: CE00125-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit
Notes
Arsenic
0.237
0.0100
mg/L
0.200
0.000328
118
80-120
Barium
0.298
0.0100
mg/L
0.200
0.0546
122
80-120
QM-08
Beryllium
0.0236
0.00100
mg/L
0.0200
0.000348
116
80-120
Cadmium
0.0235
0.00100
mg/L
0.0200
-0.000371
117
80-120
Chromium
0.235
0.0100
mg/L
0.200
-0.000303
118
80-120
Cobalt
0.235
0.0100
mg/L
0.200
0.000142
117
80-120
Copper
0.231
0.0100
mg/L
0.200
0.000378
115
80-120
Lead
0.232
0.0100
mg/L
0.200
-0.00127
116
80-120
Nickel
0.245
0.0100
mg/L
0.200
0.000137
122
80-120
QM-08
Silver
0.224
0.0100
mg/L
0.200
-0.000314
112
80-120
Vanadium
0.233
0.0100
mg/L
0.200
0.000410
116
80-120
Zinc
0.241
0.0100
mg/L
0.200
0.00199
120
80-120
Batch lAlB015 - EPA 3005A
Blank (3A38015-BLK1)
Prepared: 01/18/2021 09:33 Analyzed: 01/21/2021 11:09
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (1A18015-BSI)
Prepared: 01/18/2021 09:33 Analyzed: 01/21/2021 11:16
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
Arsenic
216
10.0
ug/L
200
108
80-120
Barium
223
10.0
ug/L
200
112
80-120
Beryllium
21.2
1.00
ug/L
20.0
106
80-120
Cadmium
21.8
1.00
ug/L
20.0
109
80-120
Chromium
214
10.0
ug/L
200
107
80-120
Cobalt
215
10.0
ug/L
200
107
80-120
Copper
211
10.0
ug/L
200
106
80-120
Lead
217
10.0
ug/L
200
109
80-120
Nickel
224
10.0
ug/L
200
112
80-120
Silver
218
10.0
ug/L
200
109
80-120
Vanadium
213
10.0
ug/L
200
106
80-120
Zinc
220
10.0
ug/L
200
110
80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 92 of 99

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www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1A18015 - EPA 3005A - Continued
Matrix Spike (1A18015-MS3)
Prepared:
01/18/2021
09:33 Analyzed: 01/21/2021 11:21
Source: CE00125-15
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
213
10.0
ug/L
200
7.60 U
107 75-125
Barium
261
10.0
ug/L
200
54.2
103 75-125
Beryllium
21.9
1.00
ug/L
20.0
0.204
108 75-125
Cadmium
21.7
1.00
ug/L
20.0
0.360 U
109 75-125
Chromium
217
10.0
ug/L
200
1.73
108 75-125
Cobalt
218
10.0
ug/L
200
1.40 U
109 75-125
Copper
212
10.0
ug/L
200
2.16
105 75-125
Lead
216
10.0
ug/L
200
3.10 U
108 75-125
Nickel
228
10.0
ug/L
200
2.20 U
114 75-125
Silver
219
10.0
ug/L
200
1.90 U
109 75-125
Vanadium
216
10.0
ug/L
200
1.69
107 75-125
Zinc
224
10.0
ug/L
200
4.40 U
112 75-125
Matrix Spike Dup (3A18015-MSD1)
Prepared:
01/18/2021
09:33 Analyzed: 01/21/2021 11:23
Source: CE00125-15
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
215
10.0
ug/L
200
7.60 U
107 75-125 0.8
20
Barium
267
10.0
ug/L
200
54.2
106 75-125 2
20
Beryllium
22.0
1.00
ug/L
20.0
0.204
109 75-125 0.9
20
Cadmium
22.0
1.00
ug/L
20.0
0.360 U
110 75-125 1
20
Chromium
220
10.0
ug/L
200
1.73
109 75-125 1
20
Cobalt
220
10.0
ug/L
200
1.40 U
110 75-125 1
20
Copper
215
10.0
ug/L
200
2.16
106 75-125 1
20
Lead
219
10.0
ug/L
200
3.10 U
109 75-125 1
20
Nickel
231
10.0
ug/L
200
2.20 U
116 75-125 1
20
Silver
222
10.0
ug/L
200
1.90 U
111 75-125 2
20
Vanadium
219
10.0
ug/L
200
1.69
108 75-125 1
20
Zinc
227
10.0
ug/L
200
4.40 U
113 75-125 1
20
Post Spike (SA18015-PS1)
Prepared:
01/18/2021
09:33 Analyzed: 01/21/2021 11:25
Source: CE00125-15
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.214
0.0100
mg/L
0.200
-0.00225
107
80-120
Barium
0.275
0.0100
mg/L
0.200
0.0542
111
80-120
Beryllium
0.0219
0.00100
mg/L
0.0200
0.000204
108
80-120
Cadmium
0.0218
0.00100
mg/L
0.0200
0.000124
108
80-120
Chromium
0.219
0.0100
mg/L
0.200
0.00173
109
80-120
Cobalt
0.216
0.0100
mg/L
0.200
8.44E-5
108
80-120
Copper
0.212
0.0100
mg/L
0.200
0.00216
105
80-120
Lead
0.215
0.0100
mg/L
0.200
0.000524
107
80-120
Nickel
0.226
0.0100
mg/L
0.200
0.00131
112
80-120
Silver
0.222
0.0100
mg/L
0.200
-0.000938
111
80-120
Vanadium
0.217
0.0100
mg/L
0.200
0.00169
108
80-120
Zinc
0.223
0.0100
mg/L
0.200
0.00273
110
80-120
Batch IA18021 - EPA 3005A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 93 of 99

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1AlBO21 - EPA 3005A - Continued
Blank (1A18021-BLK3) Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 10:44
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (1A18021-BSI)
Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 10:52
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
22.4
1.00
ug/L
20.0 112 80-120
Selenium
21.7
1.00
ug/L
20.0 109 80-120
Thallium
22.1
1.00
ug/L
20.0 111 80-120
Matrix Spike (1A18021-MS3)
Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 10:56
Source: CE00125-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
40.8
2.00
ug/L
40.0 0.740 U 102 75-125
Selenium
39.6
2.00
ug/L
40.0 1.82 U 99 75-125
Thallium
40.5
2.00
ug/L
40.0 0.570 100 75-125
Matrix Spike Dup (3A18021-MSDS)
Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 11:01
Source: CE00125-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
44.8
2.00
ug/L
40.0 0.740 U 112 75-125 9
20
Selenium
41.2
2.00
ug/L
40.0 1.82 U 103 75-125 4
20
Thallium
44.2
2.00
ug/L
40.0 0.570 109 75-125 9
20
Post Spike (SA38021-PS3)
Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 11:05
Source: CE00125-02
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
21.4
1.00
ug/L
20.0 0.0196 107 75-125
Selenium
20.1
1.00
ug/L
20.0 0.0374 100 75-125
Thallium
21.3
1.00
ug/L
20.0 0.285 105 75-125
Batch lAlBO22 - EPA 3005A
Blank (3A38022-BLK1)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:25
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (1A18022-BSI)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:38
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
Antimony
19.2
1.00
ug/L
20.0
96
80-120
Selenium
19.7
1.00
ug/L
20.0
99
80-120
Thallium
19.3
1.00
ug/L
20.0
96
80-120
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be reproduced in
full. Page 94 of 99

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1AlBO22 - EPA 3005A - Continued
Matrix Spike (1A18022-MS3)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:43
Source: CE00125-24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Antimony
40.0
2.00
ug/L
40.0 0.740 U 100 75-125
Selenium
36.5
2.00
ug/L
40.0 1.82 U 91 75-125
Thallium
28.2
2.00
ug/L
40.0 0.220 U 71 75-125
QM-07
Matrix Spike Dup (3A18022-MSDS)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:47
Source: CE00125-24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Antimony
40.3
2.00
ug/L
40.0 0.740 U 101 75-125 0.7
20
Selenium
40.7
2.00
ug/L
40.0 1.82 U 102 75-125 11
20
Thallium
28.2
2.00
ug/L
40.0 0.220 U 70 75-125 0.07
20
QM-07
Post Spike (SA18022-PS1)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:51
Source: CE00125-24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Antimony
20.5
1.00
ug/L
20.0 0.0648 102 75-125
Selenium
19.0
1.00
ug/L
20.0 -1.08 95 75-125
Thallium
14.6
1.00
ug/L
20.0 0.0727 73 75-125
QM-08
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch IA20026 - EPA 5030B MS
Blank (3A20026-BLK3)
Prepared: 01/20/2021 00:00 Analyzed: 01/20/2021 10:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
0.80
U
2.0
ug/L
Toluene-&
5.0
u91L
5.00 99 75-125
LCS (1A20026-BSI)
Prepared: 01/20/2021 00:00 Analyzed: 01/20/2021 10:29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
23
2.0
ug/L
25.0 94 80-133
Toluene-&
5.2
u91L
5.00 104 75-125
Matrix Spike (1A20026-MS1)
Prepared: 01/20/2021 00:00 Analyzed: 01/20/2021 20:03
Source: CE00125-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
24
2.0
ug/L
25.0 0.80 U 95 80-133
Toluene-&
5.7
u91L
5.00 114 75-125
Matrix Spike Dup (1A20026-MSDS)
Prepared: 01/20/2021 00:00 Analyzed: 01/20/2021 20:28
Source: CE00125-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
25
2.0
ug/L
25.0 0.80 U 98 80-133 3
19
Toluene-&
5.3
u91L
5.00 105 75-125
Batch IA20035 - EPA 5030E MS
FINAL This
report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 95 of 99

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch IA20035 - EPA 5030E MS - Continued
Blank (1A20035-BLKI)
Prepared: 01/20/2021 14:20 Analyzed: 01/20/2021 23:25
Spike Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
0.80 U
2.0
ug/L
Toluene-&
5.0
u91L
5.00
99 75-125
LCS (IA20035-BSI)
Prepared: 01/20/2021 14:20 Analyzed: 01/20/2021 21:44
Spike Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
24
2.0
ug/L
25.0
96 80-133
Toluene-&
5.8
u91L
5.00
115 75-125
Matrix Spike (3A20035-MSS)
Prepared: 01/20/2021 14:20 Analyzed: 01/20/2021 22:09
Source: CE00125-26
Spike Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
25
2.0
ug/L
25.0 0.80 U
101 80-133
Toluene-d8
5.2
u91L
5,00 103 75-125
Matrix Spike Dup (3A20035-MSD1)
Prepared: 01/20/2021 14:20 Analyzed: 01/20/2021 22:34
Source: CE00125-26
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
25
2.0
ug/L
25.0 0.80 U 100 80-133 0.6
19
Toluene-d8
4.6
u91L
5.00 92 75-125
Batch IA22042 - EPA 5030E MS
Blank (1A22042-BLKI)
Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 10:49
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Uni
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
0.80 U
2.0
ug/L
Toluene-&
5.4
u91L
5.00 108 75-125
LCS (1A22042-BS1)
Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 10:24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
26
2.0
ug/L
25.0 104 80-133
Toluene-&
5.4
u91L
5,00 108 75-125
Matrix Spike (3A22042-MS1)
Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 19:46
Source: CE00125-30
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Uni
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
280
10
ug/L
125 140 109 80-133
Toluene-d8 27 u9/L 25.0 108 75-125
Matrix Spike Dup (1A22042-MSD1) Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 20:11
Source: CE00125-30
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 270 10 ug/L 125 140 107 80-133 1 19
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 96 of 99

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch IA22042 - EPA 5030E MS - Continued
Matrix Spike Dup (1A22042-MSDS) Continued Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 20:11
Source: CE00125-30
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 27 ug/L 25.0 109 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 97 of 99

(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
0-01 This compound is a common laboratory contaminant.
QI-03 The internal standard(s) for this sample were outside the acceptance limits due to sample matrix
interference. The sample was reanalyzed at a dilution.
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 98 of 99

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
E NkCC-� 1DT75 Central Port Dr. 4810 Executive Paris Court, Suite 111 102-A Woodwinds Industrial C1.
Orlando, FL 32824 Jacksonville. FL 32216-8089 Cary, NC 275t1ce INE �Mw
[phone] [phone] Fax [phone] (919} 467-3090 Fax t919) 467-3515 Page _L Of J
Client Name
01101WKNOw t AnadebW kXL (GAM)
Projecl Number
11 e
Requested
Analyses
Requested Turnaround
Times
Note: Rush requests subject la
acceptance by the facility
zl_� Standard
Expedited
Due
! 0
S�
r
x
r
32
m
G
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m
x
U
rj Iq
Address
4300 IanrF"rr`9 C�+Q�te 100
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Project Narnstoesc
PHt=dkapLl I
City/STOp
Greenville, NC 27834
PO 11) Billing Info
1,5 It i
Tel
{2 )
52 7W3310
Fax
Reporting Contact
Emma Shi play
Sample((s) Name. Affiliation (Print)
Bating Contact
Emma Shipley
Sampler(s) Signature
Site Location I Time Zone
Lab Workorder
CE00125
Prettervatlon
(See
Codes)
(Combine
as necessary)
Item u
Sample ID (Feld Identification)
Collection Date
Collection
Time
Comp I Grab
Matrix
(see codes)
Total it of
Containers
Sample Comments
74014MIR
1-14.21
74014AW3
1- 1 y- 2
1 S: 'LJ
Gw
7
X
X
ak
,.'� �'.( "z'
'�` ;`��
Gw
7
X
X
�
�
Al401-MMR
7401-MW8
I -13 -2l
I l °- �
Gw
7
X
X
74014P2
I_ .2,1
5` p5
Gw
7
X
X
7401-P4
GW
7
X
X
7401-P5
I -Iy�ZI
t .'
Gw
7
X
X
7401-Pe
l- l'i - 21
12 ; 0
Gw
7
X
X
7401-P7
I- I _ -LI
Gw
7
X
X
7401-P9
- 1 -Zjl
I' ` o
Gw
7
X
X
7401-P11R
�1`I
C) r Zc•,
v
Gw
7
X
X
'1'7
<-- Total 1! Of Containers n
Sample Kit Prepared Byl
on tin
z
Relinquished By
Dalr�me
'j'`�� _I
Received
Dalamme
Comments!Speelal R rting Requirements
Relinquished By
DateMme
lived
Dalerriime
Relinquished By
Deterrime
Recei By
Datamme
Coder n's & Temps on
oon Rempl u
— �'l.V — \
Corldfion U Receipt
Acceptable Unacceptable
Matrix: f3W-Gmundwrater SO -Soil DWDrinking Water SE-Sedimerd SW -Surface Water WW-Wastewater A -Air er (detail in comments) Praaervatiom f-lce H-HCl WU 3 S•H2SO4 NO-NaOH O-Other (detal in comments)
Nola: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

14 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
�O 10776 Central Pert Dr 4810 Executive Park Court, Suite 111 102-A Woodwinds Indusrnal Cl.
Orlando, FL 32824 Jacksonville, FL 32216-8069 Cary, NG 27511
[phone] [phone] Fax [phone] [phone] Fax (919) a67-3515 Page -2
3—
of
Client Name
Project Number
Requested
Analyses
Requested Turnaround
p
�tr> IarA p�tllent AasooWftss, Inc. (GF4=
[nme
Times
Address - - - - ---
�
Note :Rush requests subtecl to
Pro*1 NNameMesc
4300 Sapphire Court, Suite 1 GO
PKt CoUnly LMM ^ AM I
�
acceptance by the facility
PO 01 Billing Info
City/STFGp
t'
x
Greertviae, NC 27834
5 i i5I
Reporting Contact
0
K Standard
Tel
i..x
[phone]
Emme Shipley
` Expedited
Due
Samplers) Name. Affiliation (Print)
Billing Conlacl
CM Sht l G,
Emma Shipley
po
.Sampler(s) Signature
Site Location / Time zone
Lab Work order
F>-
Preservation
(See
Codes)
(Combine
as necessary)
`tea_ `nne'F 1 }/� a��+
�+EVO ■ `�.+
-
Collection
Matrix
Total 1r of
Item d
Sample IV )Field Identification)
Collection Dale
Time
Comp ! Grab
(see codes)
Containers
Sample Comments
7401-P12
I-M-21
+SS
6r&b
7401-P13
i -j -2
' 0
GW
7
X
X
7401-P130
t- ry - r
! y' 0 0
Qw
7
X
X
7401-P18R
j • 0 !Z—V4•
>s'`3 :0-1
GW
7
X
X
7401-P17
1- 13 - ZI
I Si 3S
GW
7
X
X
7401-P19
Vs !' t,o'
�,�t ;i°
GW
T
X
X
7401-P20R
t t3`v7. 1W
GW
7
X
X
74014220D
, 1 W, LI
GW
7
X
X
7401-P21
, 7-1
91.00
GW
7
X
X
7401-P23
l ,. .L
Ss 5
GW
7
X
X
7401-P20
t, r�
>~5 s
OW
7
X
X
7401-P29
} i Zi
3` lO
GW
7
X
X
[--Total
# of Containers
Sample Kit Prepared By
Dal Time
2
Relinquished By
Daterrime
�•I'i'2i (o�1 5
Received EL
❑ letTiime
-f52 ow
Comments/Special R rling Requirements
Relinquished By
Datamme
Rece By
Dalemme
Relinquished By
Dateff"ime
R awed By
i
Data/Time
Cooler k's 8 Temps on Receipt
Condtion Upon Receipt
_Acceptable Unacceptable
Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW-Surlace Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: 1-1ce H-HCI N-HNO3 3-H2SO4 NO-NaOH O-Other (detzi in comments)
Note An samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this term, unless prior written agreements exist

ENVIRONMENTAL. CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
�O 10775 Central Fort Dr. 4810 Fxecutive Park Court. Suite 111 102-A Woodwinds industrial Ct_
Orlando, FL 32824 Jacksonville, FL 32216fi069 Cary, NG 27514
[phone] [phone] Fax [phone] [phone] Fax [phone] Page J of r
Client Name
115111M l+Iir Manag�_mw>t AI�ac111htR, Inc
Project Number
non#
Project NamatDesc
Kilt Landfill - AM I
Q
W
�
r
p
c
0
Requested
Analyses
Requested Turnaround
Times
Note - Rush requests subjw to
acceptance try the facifity
Standard
Expedited
Due hl_
t
p
$
4
Address
4300 Sepphim Court, Suhs 100
City/ST/Zip
Gnonvile, NC 27834
PO a / Billing Into
a S L `0, )
Reporting Contact
Erna Shipley
Tel
(232) 7158-3310
Fax
Sampler(s) Name, A1ltllallon (Print)
�:sR'1Mc1 �
Billing Contact
Emma Shipley
Samplels) Signature
Site Location; Time Zone
Lab Workorder
CE00125
Preservation
{See
Codes)
(Combine
as necessary)
Item #
Sample ID (Field Identification)
Collection Date
Collection
Time
Camp ! Grab
Matrix
(see codesy
Total a of
Containers
Sample Comments
74Q1-SY119
l • i � 1,1
t') : �-f
Ml-SVV2
1
1 S,;)
SW
7
X
X
7401$W4
1 .13' v
cr. 10
8W
7
X
X
7401-PZ1
It ILI r 2-1
10t SS
GW
7
X
X
7401-P22
t. pi . ZI
10 ; 30
(3W
7
X
X
7401-ES
It 1 3 , Z 1
AV S -7
WA
7
X
X
7401-FO
, i , 21
�.
WA
7
X
X
7401-TilipBtank
WA
2
X
7407-TripEkw*
WA
2
X
­ Total # of Containers 1
Sample Kit Prepared By
D te/Time
Z
Relinquished By
Dale/Time
i -ILI'Z 4;15
Received
Date/Time
1W)
CommentslSpecial Reporting equiremenis
Relinquished By
Daterrime
R
DateRme
Relinquished By
DateMme
rRecelved y
Datemme
Cooler O's & Temps on Receipt
Ooridtion Upon Receipt
Acceptable Unacceptable
Matrix GW-Groundwater SO -Sail OW -Drinking Water SE -Sediment SW -Surface Water WW-Wastewaler A -Air 0-Other (detail in oomments) Preservation. Woe H-HCl N-HNO3 5-42SO4 NO-Na0H 0-01her (deta(fn comments)
Note : All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
ENCO
Work Order: CE00125 Project: Pitt County Landfill - App I
Client: Groundwater Management Associates, Inc. (GR022; Project #: [none]
Logged In 15-Jan-21 11:30 Logged By: John C King 1 I
Preservation Check Performed By: ( Date/Time.
CE00125-01
Cont
Type
Pres (pH)
pH Checked 1
PH Adjusted DatelTime
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
I N I NA
Y 1 M/ NA
L, v
CE00125-02
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
PH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250ml-P+HNO3
<2
rY) I N/ NA
Y N NA
C E00125-04
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
PH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
(Y N / NA
Y / N 'NA
CE00125-05
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
PH Adjusted DateMme
Adjusted
Reagent Used/Comments
A
250rnLP+HNO3
'2
Y' l N / NA
Y N / NA
L/ —
CE00125-06
Cont
Type
Pres (pH)
Requirement
PH Checked I
In Control
PH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
��/ N / NA
Y N"/ NA
CE00125-08
Cont
Type
Pres (pH) PH Checked /
Requirement In Control
PH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2 YIN ! NA
YIN I NA
CE00125-09
Cont
Type
Pres (pH)
Requirement
pH Checked /
in Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y'I/ N 1 NA
Y / / NA
L
CE00125-10
Cont
T e
YP
Pres (pH)
Requirement
pH Checked /
In Control
Date/Time
PH Adjusted Adjusted
Reagent Used/Comments
A
250ml-P+HNO3
<2
YE N/ NA
Y I 1 NA
CE00125-11
Cant
Type
YP
Pres (pH}
Requirement
pH Checked /
In Control
Date/Tirne
PH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
I N/ NA
Y I / NA
C:IELMNT1Prinbwko_PreservationCheck. rpt
Page 1 c

Sample Preservation Verification
ENCO Cary
EJ�ICO
Work Order: CE00125 Project: Pitt County Landfill - App I
Client: Groundwater Management Associates. Inc. (GR022; Project #: [none]
Logged In: 15-Jan-21 11:30 Logged By: John C King C
Preservation Check Performed By: L r--) Date/Time: ` J
CE00125-12
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted DatelTime
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
Y I N/ NA
Y I NA
CE00125-13
Cant
Type
Pres (pH)
pH Checked /
pH Adjusted Date/Time
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
Y/ N / NA
Y 1 I NA
CE00125-1A
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted DateMme
Reagent Used/Comments
Requirement
in Control
Adjusted
A
250mLP+HNO3
<2
I N I NA
Y 01 NA
CE00125-15
Cant
Type
Pres (pH)
Requirement
pH Checked I
In Control
pH Adjusted DaterT'ime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y N/ NA
Y I 1 NA
v
CE00125-16
Cont
Type
Pres (pH)
Requirement
pH Checked I
In Control
pH Adjusted Daterl-ime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
1 <2
Yl / N / NA
Y ! �1 NA
u
CE00125-18
Cant
Type
Pres (pH) pH Checked /
Requirement in Control
pH Adjusted DatelTime Reagent UsedlComments
Adjusted
A
250mLP+HNO3
<2 J I N I NA
Y/ I NA
►n
CE00125-19
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Datemme
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
I N I NA
Y I 1 NA
R
CE00125-21
Cont
yP
Type
Pres (PH)
Requirement
pH Checked/
In Control
ri Adjusted Date/Time
pAdjusted
Reagent UsedlCor�unents
A
25OmLP+HNO3
<2
IIJ / N / NA
Y N / NA
CE00125-23
Cant
T e
YP
Pres (pH)
Requirement
pH Checked /
In Control
Date/Time
pH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
J / N / NA
I Y I N / NA
C:IELMNTIPrintlwko_PreservationCheck. rpt
Pacie

Sample Preservation Verification
ENCO Cary
�uco
Work Order: CE00125 Project: Pitt County Landfill - App I
Client: Groundwater Management Associates, Inc. (GR022) Project #: [none]
Logged In: 15-Jan-21 11:30 Logged By: John C King
Preservation Check Performed By: 0— Fj Date/Time: �S '2 l A'Z6V
CE00125-24
Cont
Type
Pres (pH)
IpHCheckedl
pH Adjusted Date/Time
Reagent Used/Comments
Requirement
I In Control
Adjusted
A
250mLP+HNO3
<2
N I NA
I Y I 1 NA
C E00125-25
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
N ! NA
Y / NA
CE00125-27
Cont
Type
Pres (pH)
Requirement
pH Checked/
In Control
pH Adjusted Date/Time
Adiusted
Reagent Used/Comments i
A
250mLP+HNO3
<2
N I NA
Y I y NA
CE00125-29
Cont
Type
Pres (pH)
Requirement
pH Checked /
I In Control
pH Adjusted Date/Time Reagent Used/Comments
Adjusted
A
250mLP+HNO3
<2
Y,)/ N / NA
Y IC1/ NA
CE00125-30
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2 Ll
/ N / NA
Y / N J NA
CE00125-31
Cont
Type Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3 <2
! N / NA
Y ! / NA
CE00125-32
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DateTTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2 J:D
N/ NA
Y IM NA
CE00125-33
Cont
T e
yp
Pres (pH)
Requirement
pH Chocked 1
In Control
Date/Time
pH Adi�sted Adjusted
Reagent UsedlComments
A
250mLP+HNO3
<2
1 N/ NA
Y/ N NA
CE00125-34
Con1
Yp
Type
Pres (pH)
Requirement
pH Checked/
I Control
DateMme
pH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y I N/ NA
Y/ 1 NA
C:IELMNT1Printlwko_PreservationCheck. rpt page 3 „

Sample Preservation Verification
ENCO Cary
Work Order CE00125 Project: Pitt County Landfill - App
Client: Groundwater Management Associates, Inc. (GR022, Project #: [none]
Logged In 15-Jan-21 11:30 Logged By. John C King
Preservation Check Performed By: _ DateiTfine
CE00125-35
Cant
Type
Pres (pH)
Requirement
pH Checked(
In Control
pH Adjusted Date/Time
Adiusted
Reagent Used/Comments
A
250mLP+HNO3
<2
1 N 1 NA
Y! NA
C E00125-36
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adiusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Yll N I NA
Y/ 1 NA
CE00125-37
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Tme
Adiusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y 1 N / NA
Y / p/ NA
Rea ent Name ID
1
2
pH Strip ID: 65 z j
v
Reacient Name ID
3
4
Rea ent Name iD
5
6
C1ELMNTIPrintlwko_PreservationCheck rpt page 4

2�SQ pCCgF ENCO Laboratories
9e
Accurate. Timely. Responsive. Innovative.
10775 Central Port Drive
Orlando FL, 32824
Phone: [phone] FAX: [phone]
Friday, March 19, 2021
Groundwater Management Associates, Inc. (GR022)
Attn: Emma Shipley
4300 Sapphire Court, Suite 100
Greenville, NC 27834
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Pitt County Landfill - SIM
ENCO Workorder(s): AE02021
Dear Emma Shipley,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, March 12, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Orlando. Data
from outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Kaitlin Dylnicki For David Camacho
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 7

(� �Eo
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-133313
Lab ID: AE02021-01
Sampled: 03/11/21 15:01
Received: 03/12/21 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
03/25/21
03/15/21 10:00
03/15/21 12:03
Client ID: 7401-TripBlank
Lab ID: AE02021-02
Sampled: 03/11/21 00:00
Received: 03/12/21 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
03/25/21
03/15/21 10:00
03/15/21 12:28
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 7

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www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: 7401-P13D Lab ID: AE02021-01
Analvte Results Flag MDL PQL Units Method Notes
1,4-Dioxane 1.4 3 0.80 2.0 ug/L EPA 8260D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 7

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13D Lab Sample ID:AE02021-01 Received: 03/12/21 10:15
Matrix: Ground Water Sampled:03/11/21 15:01 Work Order: AE02021
Project: Pitt County Landfill - SIM Sampled By: Amy Cressman, GMA
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed iy Notes
1,4-Dioxane [123-91-1]^ 1.4 J ug/L 1 0.80 2.0 1C15017 EPA 8260D 03/15/21 12:03 KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes
Toluene-d8 5.6 1 5.00 113 % 75-125 105017 EPA 6260D 03115121 12:03 KKW
Description: 7401-TripBlank Lab Sample ID:AE02021-02 Received: 03/12/21 10:15
Matrix: Water Sampled: 03/11/2100:00 Work Order: AE02021
Project: Pitt County Landfill - SIM Sampled By: ENCO-RDU
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed iy Notes
1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 IC15017 EPA 8260D 03/15/21 12:28 KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes
Toluene-d8 5.9 1 5.00 118 % 75-125 1C15017 EPA 8260D 03115121 12:28 KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 7

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch IC15017 - EPA 5030E MS
Blank (1C15017-BLK3) Prepared: 03/15/2021 00:00 Analyzed: 03/15/2021 09:43
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 0.80 U 2.0 ug/L
Toluene-& 5.6 ug/L 5.00 113 75-125
LCS (1C15017-BS1) Prepared: 03/15/2021 00:00 Analyzed: 03/15/2021 09:17
Spike
Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,4-Dioxane
21
2.0
ug/L
25.0
85
80-133
Toluene-d8
5.6
ug/L
5.00
112
75-125
Matrix Spike (1C15017-MS1)
Prepared: 03/15/2021 00:00 Analyzed: 03/15/2021 13:19
Source: AD07508-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,4-Dioxane
25
2.0
ug/L
25.0
2.8
87
80-133
Toluene-d8 5.6 ug/L 5.00 111 75-125
Matrix Spike Dup (1C15017-MSD1) Prepared: 03/15/2021 00:00 Analyzed: 03/15/2021 13:44
Source: AD07508-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit
1,4-Dioxane 25 2.0 ug/L 25.0 2.8 88 80-133 1 19
112
i oiuene-oa
5.6
5.00
75-125
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 7

(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 7

14 ENVIRONMENTAL. CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
C� 10775 Central Port Dr 4810 Executive Park Court, Sulte 111 102-A Woodwinds Industrial Cl
Orlando, FL 32824 Jacksonville, FL 32216-SM Cary, NC 27511
[phone] [phone] Fax [phone] (919) 467.3M Fax [phone] Page _L of
Client Narne
GRKlndv,,%Wr f WM*eMWA IAxsoaal9s, WW. (GRM!
Prolm Number
Inonal
Requested
Analyses
Requested Turnaround
Times
Nate :Rush requests sub)act to
aooeplarlce by the laality
X Standard
-
_ Expedited
Due
O
_�
U)
0
0
[aka
_ _
Address
4300 Sapphire Court, Suite 100
Protect NamwDesc
Pitt County Landfill - SIM
CitylSTfZip
Greenville, NC 27834
PO 4 1 Billing Info
T61
[phone]
Fax
Reporting Contact
Emma Shipley
Sampler(s) Name, Affiliation (Print)
RM4 (feq,IN) at &MA
Billing Contact
Emmma Shipley
sampl r l signal re
h�
slia Location / Time zone
'�� Ca�nt►I C-at�4cr•� �{-or,jarj
Lab Workorder
Preservation
(See
Codes)
(Combine
as necessary)
Item 0Sample
ID {Field ldentification}
Collection Date
Collection
Time
Comp i Gran
Matrix
(see codes)
Total R of
Containers
r
Samp a omments
7401-P131)
QW
3
X
7401 TdpBIw*
WA
2
X
7401-TdVRa&
WA
2
X
<- Total # of Containers
Sample Krt Prepared By
&fume
Hall nqu B
DaIsMrre
Fiore,, 8
Da Imp
nm nlslSpecial Reporting Requirements
Relinquished By
DateRmel
Receive By
at me
Relinquished By
DalwTime
Received By
DatalTime
Cooler n's 8 Temps on Receipt 9j2Co7ACeptab
n Receipt
le Unacceplabie
Matrix GWGroundwater SO -Sal DW-Drinking Water SE-Secilment SW -Surface Water WW-Wastewater A -Air O-Other (detaiE in comments) Preservation: I -Ice H-HCI N-HNO3 S-1­12SO4 flo-NaOH 0-01har (detait In comments)
Note All samples submitted to ENCO Labs are to accordance with the terms and conditions listed on the reverse of this kxm, unless prior written agreements exist

APPENDIX D
WELL REHABILITATION FIELD SHEETS

Monitoring Well Rehabilitation Field Sheet
Project Name:
Pitt County Landfill
Project No: 25101 Date: 6 kb 1\ Crew: C7S 4 A(.3I✓
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P13
in
2
ft MSL
82
Height ft
3.8
ft BLS
11.0 - 16.0
Listed Well Depth
Initial Well Depth
u�
�'
Final Well Depth
1(ftbelowTOC)
C
(including stickup; ft)
19.8
(ft below TOC)
U
Inspection Checklist: Does the well have a lockable cap or lid? ©/ Yes ❑ No Is the vent hole clear and unobstructed? U,Yes ❑ No
Is the well tag present, labeled, and legible? d Yes ❑ No Is a concrete pad installed and visible? d Yes ❑ No
Is reference point marked on the TOC? l( Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes 12( No
Are the protective posts damaged? ❑ Yes I( No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? © Yes ❑ No
Reh b/Development Procedures Employed:
(Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
ICJ Waterra ❑ Bailing
Time
Water
Level
ft BTOC)
Pumping
Rate
gpm)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
p H
Sp.
Cond.
(PS/cm)
Turbidity
(NTU)
db
START
cq .z
v•
1�
5 -55'
l • d
qq
5: 1
�7.�
7
`L
{"y"1
\
2•v
21,2.
S,s3
�iy,o
►o u--
c,,,, c�C - MIT
`i'.L\
1,.�-
'.1.•2-
SAS;
�-y-SS
vx-o+
D
31
[7-1
S12`i
c'c, +
O.A 'f ra
-SS
`1. 3
\q.SS
5. 2
y4s . Z
wc'c
D�
Notes: 1 `
U d b(d4� via') ovtyvv�y ��tlCUI�- �o ��Iv�l�.;e $ C�,� p�� 'JGCt�GI�•l o�,trL�
C
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: _�(, Crew: C j S G
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P7
in
2
ft MSL
81.9 J
Height ft
3.51
ft BLS
11.0 - 16.0
Listed Well Depth
Initial Well Depth
C, . �,
ZC:
Final Well Depth
i
(including stickup; ft)
19.51
(ft below TOC)
t •
(ft below TOC)
Inspection Checklist: `
Does the well have a lockable cap or lid? 17 Yes ❑ No Is the vent hole clear and unobstructed? © Yes ❑ No
Is the well tag present, labeled, and legible? d Yes ❑ No Is a concrete pad installed and visible? E7 Yes ❑ No
Is reference point marked on the TOC? Of Yes', ❑ No Is the pad cracked or deteriorated? ❑ Yes 12 No
Are the protective posts damaged? ❑ Yes Cif No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? ID Yes ❑ No
Rehab/Development Procedures Employed:
q/Brushing ❑ Surge Block Qi aterra ❑ Bailing
❑ Pumping / Overpumping, Pump description:
Time
Water
Level
ft BTOC
Pumping
Rate
(gpm)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
P H
SP.
Cond.
(PS/cm)
Turbidity
(NTU)
j 1 "L�
Cr
START
22,1
',11
ql*�b
12
2?7, %
C`
r va
cj�'� , e✓�
Notes:
w e�t b(a
a -\)JA b�U5h
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: (� 1�� �2( Crew:
—T
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P9
in
2
ft MSL
80.1
1 Height ft
3.98
ft BLS
9.5 - 14.5
Listed Well Depth
Initial Well Depth,
�� Z
Final Well Depths
25
�--1 LP '
(including stickup; ft)
18.48
(ft below TOC)
(ft below TOC)
o- �
Inspection Checklist:
Does the well have a lockable cap or lid? 2/Yes ❑ No Is the vent hole clear and unobstructed? E `Yes ❑ No
Is the well tag present, labeled, and legible? C"Yes ❑ No Is a concrete pad installed and visible? E Yes ❑ No
Is reference point marked on the TOC? i;' Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes R No
Are the protective posts damaged? ❑ Yes ❑ No 63-IN/A
Does the pad slope away from the casing to prevent water from ponding?7 Yes ❑ No
Rehab/Development Procedures Employed: /
❑ Brushing ❑ Surge Block CD'Waterra
❑ Pumping / Overpumping, Pump description:
❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
g m)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
p H
Sp.
Cond.
(PS/cm)
Turbidity
(NTU)
1'�•ZU
&, ale
START
1�:2�S
C;, 2�
`�
i.
11 �5,
54 -7
4vCO
v
2I.c,
i- ,Si
1204,1
W 2
Z,
-11.10
y.S l
Notes:
�Le�) nc\ nova, 'Jo P,
(G�Ic�C� i+(1 �1 GtV1� Obi VlSi�j1� p4kv1
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: /i -_ I2! Crew: C.) > -i tiwc
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P21
in
2
ft MSL
77.8
Height ft
4.27
ft BLS
8.0 - 11.0
Listed Well Depth
Initial Well Depth
,
Final Well Depth
(including stickup; ft)
15.27
(ft below TOC)
(ft below TOC)
i
Inspection Checklist:
Does the well have a lockable cap or lid? dYes ❑ No Is the vent hole clear and unobstructed? Co,' -Yes ❑ No
Is the well tag present, labeled, and legible? o/Yes ❑ No Is a concrete pad installed and visible? 0 Yes ❑ No
Is reference point marked on the TOC? ©' Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes D-No
Are the protective posts damaged? ❑ Yes ❑ No U N/A
Does the pad slope away from the casing to prevent water from ponding? Yes ❑ No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
LT Waterra ❑ Bailing
Time
Water
Level
ft STOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
Sp.
Cond.
(µS/cm)
Turbidity
(NTU)
START
up
4.5
I'�• h
c),q
���
` 6"..7
(c-e-3.C`j
SA",
2C--
1-7,U'
C1
'�e1,5
92,0
'7�)o
to
Notes:
ccngee `aJ f%5S Ay CGeeJ w4 Vi,u 5Avau,) �ltSihlk pc,44co n04 druYrla
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Project Name:
Monitoring Well Rehabilitation Field Sheet
Pitt County Landfill Project No: 25101 Date: 0 (s 21 Crew: CJ5 r 1
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P23
in
2
ft MSL
79.4
Height ft
3.53
ft BLS
11.0 - 16.0
Listed Well Depth
Initial Well Depth
%U't ,
Final Well Depth
(including stickup; ft
19.53
(ft below TOC)
(ft below TOC)
1 - -•8
Inspection Checklist:
Does the well have a lockable cap or lid? Ix"Yes ❑ No Is the vent hole clear and unobstructed? Yes ❑ No
Is the well tag present, labeled, and legible? IR'Yes ❑ No Is a concrete pad installed and visible? ❑ Yes 3 No
Is reference point marked on the TOC? ❑ Yes A No Is the pad cracked or deteriorated? ❑ Yes ❑ No
Are the protective posts damaged? ❑ Yes ❑ No [ rhllA ccl J
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No k� 1
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block Waterra ❑ Bailing
❑ Pumping / Overpumping, Pump description:
Time
.,
Water
Level
ft BTOC
—7 ,
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
START
ore�r<.t
gal
Well
Volumes
Temp
(°C)
21,1
pH
Sp.
Cond.
(PS/cm)
ZN,q
Turbidity
(NTU)
IUo✓
�:_
z
,C
W6C'+
--/GC
Notes:
CG Ire, Cd (U�- \f6��[k 14rqx CYueol bV'-f4, rU�
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
a
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: j / 7 /,'( Crew: C 3 5 1-
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P12
in
2
ft MSL
75.9
Hei ht ft
3.41
ft BLS
10.5 - 17.5
Listed Well Depth
Initial Well Depth
ci
1'
Final Well Depth
t �. ;
l 9
(including stickup; ft)
20,91
(ft below TOC)
(ft below TOC)
Inspection Checklist: i fx-i
Does the well have a lockable cap or lid? oYes ❑ No Is the vent hole clear and unobstructed? ❑ Yes i7 No
Is the well tag present, labeled, and legible? ❑ Yes EY No Is a concrete pad installed and visible? ❑ Yes M No
Is reference point marked on the TOC? 1p-Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes ❑ No =`?
Are the protective posts damaged? ❑ Yes ❑ No [1IN/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No;+
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
n"W' aterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
(g m)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
Sp.
Cond.
(IS/cm)
Turbidity
(NTU)
9 % `jb
2 ,'5 L
START
0'.35
612
11.7
4:3�39
57,7
T,a-7
yp
v71
jq.
5 5-
$'-y5
1,Z
S.Sj
57��
ie���+
cvevr
v.'• S
l -► j
1cc-t.�
5.5C�
x 6
izx�u
(� 5`"�` vcicl
5�` )
(Pb,Z.
i000,<
CcCJra
Notes:
�5 tD �7C C� �� iN�eo� (;06 5 mall 4vtt5
wkke - .G \ qra� , fn\�My
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: a l I t Crew: C j5 4 Ak)C
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P11R
in
2
ft MSL
82.3
Height ft
3.74
ft BLS
13.0 - 16.0
Listed Well Depth
Initial Well Depth
{
Final Well Depth
r
l 7
(including stickup; ft)
19•74
: below TOC)
� i`4
ft below TOC
( )
Inspection Checklist: s
Does the well have a lockable cap or lid? i(Yes ❑ N$ �s the vent hole clear and unobstructed? GV Yes ❑ No
Is the well tag present, labeled, and legible? E Yes Is a concrete pad installed and visible? ❑ Yes 6d No
Is reference point marked on the TOC? Q( Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes ❑ No
Are the protective posts damaged? ❑ Yes 19 No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
�r
0 Waterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
g m)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
SP.
Cond.
(µS/cm)
Turbidity
(NTU)
�(; I
`t , , _•
START
c(' Zb
S
C"i, i
H�° i
Notes:
W L�kt1 VJCQ '5
"D'om old Lt6Lve5 ; 0YII q;c Maw"
i 0 wCkK -6.vjcr65 evl� O
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: is 1 i i/ ?t Crew:
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P28
in
2
ft MSL
74.8
Height ft
2.94
ft BLS
3.5 - 8.0
Listed Well Depth
Initial Well Depth
1 ,,
Final Well Depth
(including stickup; ft)
10.94
(ft below TOC)
{
(ft below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? ® Yes; ❑ No Is the vent hole clear and unobstructed?'[J'Yes ❑ No
Is the well tag present, labeled, and legible? "es ❑ No Is a concrete pad installed and visible? I]'Yes ❑ No
Is reference point marked on the TOC?'dyes ❑ No Is the pad cracked or deteriorated? ❑ Yes I -No
Are the protective posts damaged? ❑ Yes ❑ No INN/A
Does the pad slope away from the casing to prevent water from ponding? M Yes ❑ No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block E�Waterra ❑ Bailing
❑ Pumping / Overpumping, Pump description:
Time
Water
Level
ft BTOC
Pumping
Rate
gpm)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
p H
Sp.
Cond.
(VS/cm)
Turbidity
(NTU)
cl -I
START
Notes:
bijWL df � s mirNk
�vyj dry
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: 1 7f' ZI Crew:
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P20R
in
2
ft MSL
81.7
Hei ht ft
3.51
ft BLS
10.0 - 30.0
Listed Well Depth
Initial Well Depth
Final Well Depth
' � Ci,
tJ
(including stickup; ft)
33.51
(ft below TOC)
19 ,
(ft below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? P'Yes ❑ No Is the vent hole clear and unobstructed? RI/Yes ❑ No
Is the well tag present, labeled, and legible? dYes ❑ No Is a concrete pad installed and visible? ❑ Yes ©'No
Is reference point marked on the TOC? ❑ Yes 12/No Is the pad cracked or deteriorated? ❑ Yes ❑ No vT
Are the protective posts damaged? ❑ Yes ❑ No C�-'N/A fU r+
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
e" ;Y
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
❑/Waterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
(gpm)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
Sp.
Cond.
(µS/cm)
Turbidity
(NTU)
Jcl
C"
START
1i 00
� . i'\
V5 rz
w'-c;
o
-1, 5
IL1
lwc —
.3 - W cL-1e6c' 'i, icw
�`.to
C\.S
2&.�
/.t.l�
17.12
IL-It%2
aoc>-"'
0 L ,:cv'
%1-.16
2.2-5
19(2-
b,ILl
i 1W
cLY-0 +
- law
11.'Zc�
v5.�—
�r1.`�
b.1z
II:Z�
i9
1600
Notes:
c4flj qee a. (cm Lvo-k
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: I,- j ( 1 ;�-J Crew: CJ 5 -I- 4ur—
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P17
in
2
ft MSL
76.3
Hei ht ft
4.08
ft BLS
8.0 - 11.0
Listed Well Depth
Initial Well Depth
Final Well Depth
(including stickup; ft)
15.08
(ft below TOC)
(ft below TOC)Fir,'
Inspection Checklist: `
Does the well have a lockable cap or lid? [3 Yes ❑ No Is the vent hole clear and unobstructed? a Yes ❑ No
Is the well tag present, labeled, and legible? 2/yes ❑ No Is a concrete pad installed and visible? El Yes ❑ No
Is reference point marked on the TOC? Ca -"/Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes ©'No
Are the protective posts damaged? ❑ Yes ❑ No [P/N/A
Does the pad slope away from the casing to prevent water from ponding? 0 Yes ❑ No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block Cti3" Waterra
❑ Pumping / Overpumping, Pump description:
❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
(g m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
Sp'
Cond.
(µS/cm)
Turbidity
(NTU)
0
START
t9,01
17u?, V
1066 fi
ll 5v
2,25
S
�7, Z
C� G�
i ' I
�br3o r
d�+echer i' Vi�.f ice 1 0�'t1
c w{,►t d�
Notes:
��il Slav -I c� Ui � t1,r�'9j �5�'�`�
df�
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: J�"i /�., Crew: c,)5
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
MW6R
in
2
ft MSL
78.15
Height ft
2.79
ft BLS
7.0 - 17.0
Listed Well Depth
Initial Well Depth
I /
l`�
Final Well Depth
�.
'�0
(including stickup; ft)
19,79
(ft below TOC)
!
(ft below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? 0 Yes ❑ No Is the vent hole clear and unobstructed?U Yes ❑ No
Is the well tag present, labeled, and legible? EJ Yes ❑ No Is a concrete pad installed and visible? ❑ Yes O'No
Is reference point marked on the TOC? ❑ Yes ©" No Is the pad cracked or deteriorated? ❑ Yes ❑ No
Are the protective posts damaged? L Yes ❑ No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No 1
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block Q'Waterra ❑ Bailing
❑ Pumping / Overpumping, Pump description:
Time
Water
Level
ft BTOC
Pumping
Rate
(g m)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(C)
pH
Sp.
Cond.
(µS/cm)
Turbidity
(NTU)
.2 7
START
3 3C)
2
2b.'7
2AZl,,-
75'
23.'3
�0:73
51 pro
'19,7
U72
209J
,�,�� �
OR
3. 50
l-71
I zo&
iooc +
e2
Notes: J
i UGt{� 6 JOY r -J
4 S0� i n AV Ot if UG
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: ((-' / 171 Z 1 Crew: (__;5 •F AW,C
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P16R
in
2
ft MSL
84.3
JHei ht ft
3.14
ft BLS
11.0 - 14.0
Listed Well Depth
Initial Well Depth
_
��
Final Well Depth
�r
+ 7. `r
(including stickup; ft)
17.14
(ft below TOC)
1
(ft below TOC)
/
Inspection Checklist:
Does the well have a lockable cap or lid? El'Yes ❑ No Is the vent hole clear and unobstructed? Q` Yes ❑ No
Is the well tag present, labeled, and legible? Yes ❑ No Is a concrete pad installed and visible? 0 Yes Er No
Is reference point marked on the TOC? ❑ Yes ©" No Is the pad cracked or deteriorated? GYVes ❑ No
Are the protective posts damaged? ❑ Yes CJ/No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes C-No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
aWaterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
TempC)
(
pH
Sp.
Cond.
(VS/cm)
Turbidity
(NTU)
L;77
START
S ti
V-n
c.we-.-
o Gli� 6r�
eoc
Notes:
,)'ee2 ri Gt�✓vY�(J Viel ( GY1Cv�� -pad b u 4cj vP
5
i to - lJC6 -�o LW SA n� f V&VI
u)aka� j �0 on�
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: ( /7/ Crew:
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P19
in
2
ft MSL
78.5
Hei ht ft
5.4
ft BLS
9.0 - 13.0
Listed Well Depth
Initial Well Depth
I 22—
Final Well Depth
(including stickup; ft)
18.4
(ft below TOC)
(ft below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? 4'Yes ❑ No Is the vent hole clear and unobstructed? ,p'Yes ❑ No
Is the well tag present, labeled, and legible? Q'Yes ❑ No Is a concrete pad installed and visible? C1 Yes ❑ No
Is reference point marked on the TOC? 0' Yes ❑ No Is the pad cracked or deteriorated? 0—Yes 0 No
Are the protective posts damaged? ❑ Yes ❑ No El''N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
❑ Waterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
(gpm
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
Sp.
Cond.
(VS/cm)
Turbidity
(NTU)
O�
START
a 5
Hof
Zi.�5
R52
Vc�
eft.
I�
3h
iq.3
9.61
2\ -`\
(-,
l �-t2v
1uoU
b!2
,,Co
i472
UMO t
R
`22.0
i-1.ao
Iy—I
kocca
6
Notes:
Parameter
Stabilization Criteria
❑
H
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: �r M2j Crew:
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P29
in
2
ft MSL
82.4
Height ft
2.96
ft BLS
7.0 -12.0
Listed Well Depth
Initial Well Depth
•,
i
Final Well Depth
�(ft
(including stickup; ft)
14.96
(ft below TOC)
below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? Ep/es ❑ No Is the vent hole clear and unobstructed? ®'Yes ❑ No
Is the well tag present, labeled, and legible? l' Yes ❑ No Is a concrete pad installed and visible? ❑ Yes ❑'No
Is reference point marked on the TOC? ©'Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes ❑ No
Are the protective posts damaged? ❑ Yes ❑ No i -N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
Rehab/Development Procedures Employed: /"
❑ Brushing ❑ Surge Block t Waterra
❑ Pumping / Overpumping, Pump description:
❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
Sp.
Cond.
(µS/cm)
Turbidity
(NTU)
k,o ';
b , 7 �`7
1
► J, 2-1
951
t
START
GP.
�•7-7-5
/0
t1-76
[ r�
1 W I`7
� i��
{
11,.. ,�
� (
L�ILJ.
,
'7 71.c
). •! t/tY-�,C;{, llJ
1
1.
Notes:
6(k�f( 15 nftA(� OV �VJ�15 / PUJ'A� 404P
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

APPENDIX E
AS -BUILT DRAWINGS FOR THE SOUTHERN UNIT
CAP REPAIR AND STORMWATER UPGRADE

10
0
Q
0
a
Z
Bear G ru
fiel 43 I3
Falkl d r
33 30`
o
22
Fountain 121 43
264
258
264
gill Greenville
13 son
264A 33
Grimesland
13 W* terville
258 43
SITE o
Chocowi�
yden
02
a ton
VICINITY MAP
NOT TO SCALE,
NORTH CAROLINA
TWC PROJECT NO..O 2566-BH
COUNTY COMMISSIONERS
TOM COULSON
ANN FLOYD HUGGINS MARY PERKINS-WILLIAM1
AM M
%I I
AL q
sue] allffl I 1111111 1 A
THE WOOTEN COMPANY
120 North Boylan Avenue Raleigh NC 27603-1423
919.828.0531 fax [phone]
License Number: F-0115
RECORD DRAWING - 07/27/2021
Revised per Record Documents as annotated by the
Contractor. Revisions from the original design paps
were made with the review and appro val o f the Engineer.
1`1/IIIIf If f/1
`4bQ��F ESS�O<r'Ly�'S
SEAL _
047020
DESIGN ONLY f'
MCP FEs's%
SEA
"fill - WO
r_.
�.�try ran
w:
f+?
x.tr.�a•JJ ry:.
LANDFILL RD.
SITE
q�M
PROJECT AREA MAP
NOT TO SCALE
C-0.1 / SHEET 1 OF 12

GENERAL NOTES:
I
i1
Z
m
ao
0
U
4-'
a_ tz
v
�l M
n! M V
A
AREA
MECH
MECHANICAL
ABAND
ABANDONED
MFR
MANUFACTURER
ABC
AGGREGATE BASE COURSE
MH
MANHOLE
AC
ACRES
MJ
MECHANICJOT
AFF
ABOVE FINISHED FLOOR
MIN
MINIMUM
AL
ALUMINUM
MON
MONUMENT
APPRX
APPROXIMATE
ASPH
ASPHALT
ASSY
ASSEMBLY
N/A
NOT AVAT-ABLE
AVG
AVERAGE
N
NORTH
ARV
AIR RELEASE VALVE
NAD 83
NORTH AMERICAN DATUM 1983
AZ
AZIMUTH
NCWN
NORMAL CROWN
AWWA
AMERICAN WATER WORKS ASSOCIATION
NC GRID
NORTH CAROLINA GRID
NCGS
NORTH C AROLINA GEODETIC SURVEY
No.
NUMBER
B-B
BACK OF CURB TO BACK OF CURB
N/R
NOT REQUIRED
BLDG
BUILDING
NTS
NOT TO SCALE
BM
BENCHMARK
NOM
NOMINAL
BOA
BLOW -OFF ASSEMBLY
NWL
NORMAL WATER LEVEL
BOT
BOTTOM
BW
BARB WIRE
OC
ON CENTER
OD
OUTSIDE DIAMETER
C&G
CURB AND GUTTER
O/H
OVERHEAD
CB
CATCH BASIN
ORIG
ORIGINAL.
C
CENTERLINE
CIP
CAST IRON PIPE
CI
CURB INLET
PC
POINT OF CURVATURE
CLR
CLEARANCE
PED
PEDESTAL_
CM
CONCRETE MONUMENT
PE
PLAIN END
CMP
CORRUGATED METAL PIPE
PI
POINT OF INTERSECTION
CMU
CONCRETE MASONARY UNIT
PIV
POST INDICATOR VALVE
CO
CLEAN OUT
P
PROPERTY LINE
CONC
CONCRETE
PP
POWER PDLE
CONT
CONTINUOUS
PRV
PRESSURI-E REDUCING VALVE
CONSTR
CONSTRUCTION
PSI
POUNDS PER SQUARE INCH
CONTR
CONTRACTOR
PVC
POLYVIN'L CHLORIDE
COR
CORNER
PT
POINT Oft POINT OF TANGENCY
CP
CONTROL POINT
PUE
PERMANENT UTILITY EASEMENT
CPED
CABLE TV PEDESTAL
PVMT
PAVEMENT
CULV
CULVERT
R
RADIUS
D
DEPTH
R/W
RIGHT 01: WAY
DI
DROP INLET
RCP
REINFORCED CONCRETE PIPE
DIA
DIAMETER
REF
REFERENCE
DIP
DUCTILE IRON PIPE
REQ'D
REQUIRED
DIM
DIMENSION
RET
RETAINING
DISCH
DISCHARGE
REV
R`-VISED
DIST
DISTANCE
RPZ
REDUCED PRESSURE ZONE
DNF
DID NOT FIND
RPM
REVOLUTIONS PER MINUTE
DOT
DEPARTMENT OF TRANSPORTATION
REINF
REINFORCED
DW
DOMESTIC WATER
RT
RIGHT
DELTA
S/W
SIDEWAL.K
E
EAST
SAN
SANITARY
E-E
EDGE OF PAVEMENT TO EDGE OF PAVEMENT
SCH
SCHEDULE
EA
EACH
SDMH
STORM DRAINAGE MANHOLE
EFF
EFFLUENT
SF
SILT FENCE
EIP
EXISTING IRON PIPE
SHT
SHEET
EL
ELEVATION
SGNL
SIGNAL POLE
ELEC
ELECTRIC
S
SOUTH
EPED
ELECTRIC PEDESTAL
SPECS
SPECIFICATIONS
EP
EDGE OF PAVEMENT
SQ
SQUARE
EW
EACH WAY
SSMH
SANITARY SEWER MANHOLE
Ex
EXISTING
SSTL
STAINLESS STEEL_
EXPJT
EXPANSION JOINT
ST
STREET
STA.
STATION
STD
STANDARD
FEE
FINISHED FLOOR ELEVATION
SYM
SYMBOL
FIG
FINISHED GRADE
FH
FIRE HYDRANT'
FIN
FINISH
T
TANGENT
FLG
FLAG
TBM
TEMPORARY BENCH MARK
FLNG
FLANGE
TCP
TERRA COTTA PIPE
FM
FORCE MAIN
TDD
TEMPORARY DIVERSION DITCH
FOHH
FIBER OPTIC HAND HOLE
THH
TELPHONE HAND HOLE
FOM
FIBER OPTIC MARKER
TPHN
TELEPHONE
FOPED
FIBER OPTIC PEDESTAL
TPED
TELEPHONE PEDESTAL
FP
FIRE PROTECTION
TEMP
TEMPORARY
FPS
FEET PER SECOND
THK
THICK
FT
FEET
TOC
TOP OF CURB
FTG
FOOTING
TOP
TOP OF SLOPE
TOW
TOP OF WALL
TP
TELEPHONE POLE
G
GAS
TRANS
TRANSFORMER
GA
GAGE
TRFCBX
TRAFFIC: SIGNAL CONTROL BOX
ALV
GA
GALVANIZED
TRFCPL
TRAFFIC: SIGNAL POLE
G
GAS METER
TCE
TEMPORARY CONSTRUCTION EASEMENT
GPM
GALLONS PER MINUTE
TYP
TYPICAL
GR
GRADE
GV
GATE VALVE
GYP
GYPSUM
UMKR
UTILITY MARKER
LJ/G
UNDERGROUND
UP
UTILITY POLE
HCP
HANDICAPPED
HH
HAND HOLE
HT
HEIGHT
VC
VERTICAL CURVE
HOR
HORIZONTAL
VCP
VITRIFIED CLAY PIPE
HP
HORSE POWER
VERT
VFRTIG%L
HWA
HIGH WATER ALARM
VOL
VOLUME
HWL
HIGH WATER LEVEL
VPC
VERTIGaL POINT OF CURVATURE
HYD
HYDRANT
VPI
VERTICAL POINT OF INTERSECTION
VPT
VERTIGNL POINT OF TANGENCY
ID
INSIDE DIAMETER
IN
INCH
W/
WITH
IN/HR
INCHES PER HOUR
WL
WATER LINE
INF
INFLUENT
WM
WATER METER
INT
INTERSECT
WT
WEIGHT
INV
INVERT
WV
WATER VALVE
IPS
IRON PIPE SET
WTP
WATER TREATMENT PLANT
ISL
ISLAND
WWF
WELDED WIRE FABRIC
WWTP
WASTE WATER TREATMENT PLANT
JB
JUNCTION BOX
YI
YARD INLET
KWY KEYWAY
LF
LINEAR FEET
L
LENGTH
LP
LIGHT POLE
LT
LEFT
LWL
LOW WATER LEVEL
MAX MAXIMUM
MATL MATERIAL
1. EXISTING UTILITIES ARE LOCATED APPROXIMATELY ON THE DRAWINGS. CONTRACTOR SHALL. CONTACT UTILITY LOCATE TO CONFIRM THE
LOCATIONS OF ALL EXISTING TELEPHONE, ELECTRICAL AND TV CABLES, GAS LINES AND OTHER UTILITIES AT LEAST 48 HOURS PRIOR TO
COMMENCING WORK. CONTRACTOR RESPONSIBLE FOR VERIFYING EXACT LOCATION OF THESE EXISTING UTILITIES. THE COST TO REPAIR THESE
FACILITIES IF DAMAGED, SHALL BE THE RESPONSIBILITY OF THE CONTRACTOR.
2. THE CONTRACTOR SHALL NOTIFY NCDOT AT LEAST 48 HOURS PRIOR TO BEGINNING ANY WORK WITHIN NCDOT RIGHTS -OF -WRY. RIGHTS -OF -WAY
AND/OR TEMPORARY EASEMENT ARE THE LIMITS FOR CONSTRUCTION.
3. THE CONTRACTOR SHALL TAKE PRECAUTIONS NOT TO DISTURB EXISTING PROPERTY CORNER MARKERS. PROPERTY CORNERS, RIGHTS -OF -WAY
LINES, AND EASEMENTS SHALL BE CLEARLY MARKED FOR CONSTRUCTION LIMITS. ALL DISTURBED PROPERTY CORNERS SHALL BE REPLACED BY A
REGISTERED LAND SURVEYOR.
4. TEMPORARILY REMOVE MINOR ITEMS AS REQUIRED FOR THE INSTALLATION OF THE UTILITY. MINOR ITEMS SHALL INCLUDE, BUT ARE NOT
LIMITED TO, EXISTING SIGNS, MAIL BOXES, FENCES, AND STORM SEWER PIPES. FENCES WITHIN RIGHTS -OF -WAY SHALL BE RELOCATED TO THE
RIGHT-OF-WAY LINE AND FENCES WITHIN EASEMENTS SHALL BE REMOVED UNLESS OTHERWISE NOTED. INCLUDE COST IN THE PER FOOT COST OF
THE UTILITY BEING INSTALLED.
5. SUPPORT EXISTING POLES, FENCES, CULVERTS, PAVEMENT, UTILITIES, CURBING AND OTHER STRUCTURES DURING CONSTRUCTION. REPAIR
DAMAGED ITEMS TO THEIR ORIGINAL CONDITION AT NO ADDITIONAL COST.
6. OPEN CUT PAVED DRIVEWAYS PER SPECIFICATION. PROVIDE PAVEMENT PATCHING PER DETAIL. UNPAVED ROADS OR DRIVEWAYS SHALL BE
PROVIDED WITH STONE PER PATCHING DETAIL.
7. 6 INCHES OF NCDOT ABC AGGREGATE SHALL BE PROVIDED FOR THE FULL WIDTH OF UNPAVED DRIVEWAYS AND ROADS FROM THE EDGE OF THE
ROAD SHOULDER TO 10 FEET PAST THE OPPOSITE SIDE OF THE PIPE TRENCH AND OTHER AREAS OF EXISTING DRIVEWAYS AND DISTURBED DURING
CONSTRUCTION.
8. EXCAVATED MATERIAL SHALL NOT BE PLACED ON THE ROADWAYS AT ANY TIME, UNLESS APPROVED BY THE NCDOT DISTRICT ENGINEER.
9. EDGE OF UTILITY TRENCH SHALL BE NO CLOSER THAN 3 FEET TO THE EXISTING EDGE OF PAVEMENT.
10. IF ANY OF THE NEW MANHOLE STRUCTURES ARE EXPOSED IN ANY PORTION OF THE ROADWAY SIDE DITCH, THE DITCH SHALL BE PIPED, BACKFILLED,
TAMPED, GRADED FOR, POSITIVE DRAINAGE, AND SEEDED. IF CONDITIONS WARRANT PIPING THE DITCH, DRAINAGE STRUCTURES MAY BE REQUIRED;
THEREFORE, PLEASE CONTACT THE NCDOT. THE EXISTING DITCH SHALL NOT BE REALIGNED FROM THE ORIGINAL CONDITION WITHOUT APPROVAL
FROM THE NCDOT.
11. ALL SEWER SERVICES TO BE INSTALLED TO RIGHT-OF-WAY AT MINIMUM GRADE FROM THE MAIN UNLESS OTHERWISE APPROVED BY THE ENGINEER.
12. THE LIMITS OF DISTURBANCE SHALL BE THE RIGHT-OF-WAY, PERMANENT EASEMENT OR TEMPORARY EASEMENT.
13. SANITARY SEWER SERVICES ON EXISTING LINES SHALL BE SEALTITES TEE BY GENERAL ENGINEERING COMPANY, OR EQUAL.
EROSTON CONTROL NOTES:
1. INSTALL SILT FENCE OVER AND AROUND TOP OF EXISTING PIPE AND INLETS AT DISTURBED AREAS.
2. INSTALL SILT FENCE AROUND SPOIL PILES.
3. PROVIDE EROSION CONTROL MEASURES AROUND STOCK/WASTE PILES AND STAGING AREAS AS APPROVED BY ENGINEER.
Notify NC811 Three Full Working bays Before Digging
� 6
Dial 811 or 1-800-632-4949, or visit www.nc8ll.org
INDEX TO DRAWINGS
C-0.1 COVER SHEET
C-0.2 INDEX OF SHEETS, ABBREVIATIONS, GENERAL NOTES AND LEGEND
C-l.l EXISTING CONDITIONS AND DEMOLITION OVERALL PLAN
C-1.2 GRADING PLAN
C-1-3 SECTIONS
C-1.4 SECTIONS THROUGH NEW TRENCHES
C-1.5 EROSION CONTROL
C-1.6 EROSION CONTROL STANDARD NOTES
C-2.1 SOIL, AND EROSION CONTROL DETAILS
C-2.2 STORMWATER DETAILS
C-3.1 DIGITIZED CONTOURS FROM ORIGINAL DESIGN
C-3.2 SURVEYED ELEVATION CONTOURS
C-3.3 VOLUME COMPARISON
C-3.4 DRAINAGE LABELS AND PHOTOS
SURVEY
I i:IS;TIN�.S
ABM
BENCHMARK
YBM
TEMPORARYBENCHMARK
23 CM
CONCRETE MONUMENT
0
IRON PIPE
E01
HUB & 'PACK
0
NAIL
C7
NAIL & CAP
0
PK NAIL
CONIFEROUS TREE
CTRI:E
'�
DECIDUOUS TREE
DTREE
O
SHRUB
SHB
L-FICEND
WATER
NI-W
EXISTH
G
D°
GV
IVA TER VALVE
FI t
FIRE HYDRANT'
a
REDUCER/INCREASER
•
0-0<
M,
AIR RELEASE.
■
o
I,VM
WATER METER
•
c
PLUG
PLUG
•
6
YH
YARD HYDRANT
•
0
WELL
WELL
—W
WATER LINE
10
PLUG VALVE
PV
NEW
N
0
SEWI=-R
UTILIIIES
EXISTING
''ll'"°
EXISTING
N! W
(S) MH
MANHOLE
©
0 PP
POWER POLE
o
CLEAN OUT
•
I-( I P
LIGHT POLE
CO
_SS__
SEWER I.ITNE
SS
� GUY
GUY WIRE
- FM --
FORCE MAIN
FM
° TV
CABLE TV PEDESTAL
M TPED
TELEPHONE PEDESTAL
❑ TRAN
TRANSFORMER
_G
GAS LINE
STORM DRAINAGE
EXISTING NEW EXi`.I WG
I DI DROP INLET
0 GI CURB INLET
(i YI YARD INLET
p FED; FLARED END SECTION
STMH MANHOLE
PIPE
DIA. MATERIAI.
EROSION CONTROL
NEW
DITCH l SWALE
STONE CHECK DAM
INLET PROTECTION
RIP -RAP
SILT FENCE
t—+F—i-- ■
MISC.
FONT STYLES
EXISTING
PROPOSED FEATURES
— — — PL —
PROPERTY LINE
EXISTING FEATURES
11-\,�V-1-
WOODS LINE
--- - - — R/W - -
RIGHT-OF-WAY
ELEVV,
MAJOR CONTOUR
ELEV.
MINOR CONTOUR
PERM. UTILITY EASEMENT ! .... 1
cn
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SEAL _
04 0020
DESIGN ONLY
I H I CAq
.�`,,,"
• Q '9 .
1=
3�0
�cK `
DESIGNED BY:
DFB
DRAWN BY:
JTH, KES, EML
CHECKED BY:
DFB
PROJECT NO.:
2 566-BH
DATE:
AUGUST 2020
SCALE:
AS NOTED
C-0,2

w
i
Q
;Z�
cx
TBM: #1
CAP
Elew 82.16
TBM: #2
REBAR/CAP
Elev: 79.62
TBM: #3
REBAR CAP
Elev: 76.54
NOTES:
ALL EXISTING CATCH BASINS TO BE REMOVED.
ALL DRAIN PIPE INVERTS TO REMAIN. DRAIN PIPES
WITH EXISTING DAMAGE TO BE REMOVED WITH ENGINEER'S APPROVAL.
VENT
TBM 2
LEGEND
EXISTING DRAINAGE
PIPE (TO REMAIN)
EXISTING CATCH BASIN Ll
(TO BE DEMOLISHED)
MONITORING WELL MW
SLOPE OF CAP XX%
® �, .Ho 0
Z
0
ce.
0�
U
Lu Q4 U
OC
100' 50, 0 100' 200' 300'
SCALE: I" -- 100'
z
Z
Q
U
CL
z
0
z
t
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SEAL -
047020 _
V
DESIGN ONLY
iiiii iii a !!!!
_ 3 A� e
- 3 pY�dR
o •'•-�t
C C.
CoS/
DESIGNED BY:
DFB
DRAWN BY:
JTH, KMS, EML
CHECKED BY:
DFB
PROJECT NO-:
2566-BH
DATE:
AUGUST2020
SCALE:
AS SHOWN

V Ljl
00 NIT Nml
21.8'
U4 INV=121.81 fir''V,NT mow
10s j
VA1
O
VAL
'ZI �, 70
-- ------------
.VT;
p _U7
L
7 7. 1--
P19
NEW DRAINAGE 2.
PIPE RAISE IW=783'
CONTOUR ON
It It OUTER EDGE 1-0
104'. SEE Dl
w PMW
17 P28 DRAINAGEINV=76.9'
NEW DRAINAGE
PIPE, RAISE
ti CONTOUR ON =10
AREAS OF CAP REPAIR, OUTER EDGE TO
SEE 5/C-2.1 125'. SEE DTI.. •
2/C-2.2
5
•
mw
----------- ------- BMW
P20R -
-----------
------------ ----------------- -----
-----------
---------------------- ti -
Lr)
c
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130
B'
C-1.3
w I
Q - ____ , I PROPOSED DRAINAGE PIPE
NEW GRADING.
SEE NOTE 2.
-7-
120
EX15TING
1 GRADE
1 '" z
I --- -- --
z
POSITIVE
<
m DRAINAGE TO
J
I CATCH BASIN
F-
cu
0
Ito
0+00 0+50 1+00
1+50
2+00 2+50 3+00 3+50
CI_ kz
Ln
SECTION C-C (TYPICAL)
SCALE: 1"=50'HZ
Zu N
V
QM574
hl
"IN \{t,,,����"�'
- -------- 3r
-MW6R
--------------
INV=72.0'
jam-
EW=72.5'
NOTES:
1. AREAS OF CAP REPAIR SHOWN ARE APPROXIMATE. EXACT
LOCATIONS TO BE FLAGGED IN FIELD.
2. TOPSOIL SHALL BE ADDED TO PROVIDE POSITIVE DRAINAGE
TO CATCH BASINS AND TO INSURE ALL CATCH BASIN INLETS
ARE AT GRADE.
3. MINIMUM COVER OF 3 INCHES ON DRAIN PIPE.
as a
V)
z
4. AREAS OF CAP REPAIR TO HAVE TOPSOIL REMOVED AND
L)
0
GROUND SCRAPED FLAT ABOVE WASTE. REPAIR TO INCLUDE
z Ei
18" IMPERMEABLE LAYER AND 6" TOPSOIL ABOVE, PER DETAIL
o Z
>
5/C-2.2.
uj
Q
2
0
L)
u.j
w
DRAINAGE
PIPE
ELEVATION
LENGTH
A
EL. 125'
1925 LF
B
EL. 104'
2747 LF
* SEE DETAIL SHEET FOR PIPE, BERM AND TRENCH INFORMATION.
LEGEND
VISIBLE EROSION AREA TO BE
REPAIRED
-20% _ SLOPE OF CAP
NEW TRENCH -RAISE CONTOUR
ON OUTER EDGE OF TRENCH
TO 125'
NEW TRENCH -RAISE CONTOUR
ON OUTER EDGE OF TRENCH
TO 104'
REGRADE TO ELIMINATE PONDING
I B 0 PROPOSED CATCH BASIN
EXISTING DRAINAGE PIPE
100, 50, 0 100, 200' 300,
SCALE: I 100'
S S
Z
SEAL
047020
q,...
DESIGN ONLY
DESIGNED BY:
DFB
DRAWN BY:
JTH, KMS, EML
CHECKED BY:
DFB
PROJECT NO.:
2566-BH
DATE:
AUGUST 2020
SCALE:
AS SHOWN
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EROSION & SEDIMENT CONTROL CONSTRUCTION SEQUENCE
1. OBTAIN EROSION AND SEDIMENTATION CONTROL PLAN APPROVAL FROM NCDENR AND ANY OTHER APPLICABLE PERMITS. CONTACT 9. THE CONTRACTOR SHALL INSPECT ALL SEDIMENT AND EROSION CONTROL DEVICES AT LEAST ONCE A WEEK AND AFTER EVERY RAIN FALL
LAND QUALITY AT [phone]. EVENT. THE CONTRACTOR SHALL MAINTAIN THE DEVICES ACCORDING TO THE NORTH CAROLINA EROSION AND SEDIMENT CONTROL
PLANNING AND DESIGN MANUAL. SEE ALSO MAINTENANCE PLAN ON THIS SHEET. NEEDED REPAIRS WILL BE PERFORMED IMMEDIATELY TO
2. COORDINATE AND INSTALL CONSTRUCTION ENTRANCE WITH DESIGNATED INGRESS/EGRESS POINT AS SHOWN ON PLANS. ANY DEVICES THAT ARE FAILING OR NOT FUNCTIONING APPROPRIATELY.
3. CLEAR SITE ONLY AS NECESSARY TO INSTALL EROSION CONTRO_ DEVICES. INSTALL SEDIMENT TRAPS THEN RUNOFF CONTROL AND
CONVEYANCE SYSTEMS AS INDICATED ON PLANS.
4, ONCE ALL EROSION CONTROL DEVICES HAVE BEEN PROPERLY INSTALLED, NOTIFY ENGINEER FOR SITE INSPECTION. ONCE EROSION
CONTROL DEVICES ARE APPROVED, BEGIN CONSTRUCTION ACTI✓ITIES, SEE NOTE 5.
5. THE SEDIMENTATION POLLUTION CONTROL ACT WAS AMENDED IN 2006 TO REQUIRE THAT PERSONS RESPONSIBLE FOR LAND
DISTURBING ACTIVITIES INSPECT A PROJECT AFTER EACH PHASE OF THE PROJECT TO MAKE SURE THAT THE APPROVED EROSION AND
SEDIMENTATION CONTROL PLAN IS BEING FOLLOWED. RJLES DI7AILING THE DOCUMENTATION OF THESE INSPECTIONS TOOK EFFECT
OCTOBER 1, 2010. THE SELF -INSPECTION PROGRAM IS SEPARAT= FROM THE WEEKLY SELF --MONITORING OF THE NPDES STORMWATER
PERMIT FOR CONSTRUCTION ACTIVITIES. THE FOCUS OF THE SELF INSPECTION REPORT IS THE INSTALLATION AND MAINTENANCE OF
EROSION AND SEDIMENTATION CONTROL_ MEASURES ACCORDING TO THE APPROVED PLAN. THE INSPECTIONS SHOULD BE CONDUCTED
AFTER EACH PHASE OF THE PROJECT, AND CONTINUED UNTIL PERMANENT GROUND COVER IS ESTABLISHED. SELF -INSPECTION REPORTS
ARE AVAILABLE ON THE LAND QUALITY WEB SITE: http://www.dIr.enr.state.nc.us/pages/sedimentation_new.html. THE CONTRACTOR SHALL
ENSURE i-HAT DOCUMENTATION OF INSPECTIONS WILL BE RECORDED ON A SINGLE COPY OF THE APPROVED EROSION AND
SEDIMENTATION CONTROL PLAN. THIS PLAN AND ANY INSPECTION REPORTS SHALL BE MADE AVAILABLE ON THE PROJECT SITE.
6. ANY SEEPAGE PUMPED OUT OF STRUCTURE EXCAVATIONS OR TRENCHES SHALL BE PUMPED THROUGH A DEWATERING BAG AS
MANUFACTURED BY DANDY OR EQUAL.
7. ESTABLISH A PERMANENT GROUNDCOVER FOR ALL DISTURBED AREAS CONSISTENT WITH THE GROUND STABILIZATION
REQUIREMENTS INCLUDED IN NOTE 9 BELOW FOLLOWING COMPLETION OF CONSTRUCTION DEVELOPMENT.
8. GROUND STABILIZATION SHALL OCCUR AS FOLLOWS:
A. FOR PERIMETER DIKES, SWALES, DITCHES AND SLOPES - STABILIZATION TIME FRAME SHALL BE 7 DAYS, NO EXCEPTIONS.
B. FOR SLOPES STEEPER THAN 3:1 - STABILZATION TIME FRAME SHALL BE 7 DAYS. STABILIZATION TIME FRAME EXCEPTION
IF SLOPES ARE 10 FEET OR LESS IN LENGTH AND ARE NOT STEEPER THAN 2:1, 14 DAYS ARE ALLOWED.
C. FOR SLOPES 3:1 OR FLATTER - STABILIZATION TIME FRAME SHALL BE 14 DAYS. STABILIZATION TIME FRAME EXCEPTION
7-DAYS FOR SLOPES GREATER THAN SO FEET IN LENGTH.
D. FOR ALL OTHER AREAS WITH SLOPES FLATTER THAN 4:1 - STABILIZATION TIME FRAME SHALL BE 14 DAYS, NO EXCEPTIONS
(EXCEPT FOR PERIMETERS AND HQW ZONES).
10 COMPLETE FINAL GRADING AND APPLY PERMANENT SEEDING AND MULCHING CONSISTENT WITH THE GROUND STABILIZATION
REQUIREMENTS (SEE NOTE 9) AND PROJECT SPECIFICATIONS.
11. AFTER ALL SEDIMENT PRODUCING AREAS HAVE BEEN PERMANENTLY STABILIZED, CONTRACTOR SHALL REMOVE THE TEMPORARY
MEASURES AND ALL THE UNSTABLE SEDIMENT. SMOOTH THE AREA TO BLEND WITH THE ADJOINING AREAS AND STABILIZE PROPERLY
WITH THE APPLICATION OF SEED AND MULCH ACCORDING TO THE SCHEDULE AND DETAILS INCLUDED ON THE PLANS AND/OR
CONTAINED IN THE PROJECT MANUAL.
12. REMOVE ALL SILT FENCING MATERIALS, SILT FENCE OUTLETS AND UNSTABLE SEDIMENT DEPOSITS AND BRING THE AREA TO GRADE AND
STABILIZE IT AFTER THE CONTRIBUTING DRAINAGE AREA HAS BEEN PERMANENTLY AND PROPERLY STABILIZED.
13. SEE ALSO NCDENR EROSION AND SEDIMENTATION CONTROL PLANNING AND DESIGN MANUAL, APPENDICES AND SPECIFICATIONS.
14. CONDITIONS MAY ARISE DURING CONSTRUCTION THAT REQUIRES MODIFICATION TO THE CONSTRUCTION SEQUENCE AND OR CHANGES TO
THE LOCATIONS OF CERTAIN EROSION CONTROL MEASURES. CONTRACTOR MAY MAKE DISCRETIONARY MODIFICATIONS TO BETTER MANAGE
SEDIMENT AND EROSION CONTROL ONLY AFTER APPROVAL BY ENGINEER.
15. ALL STOCKPILES SHALL HAVE A MAXIMUM SIDESLOPE OF 2:1 AND SHALL NOT EXCEED A MAXIMUM HEIGHT OF 10 FEET. STOCKPILES MUST BE
LOCATED 50 FEET FROM STORM DRAINS AND STREAMS UNLESS NO REASONABLE ALTERNATIVES ARE AVAILABLE. PROVIDE SILT FENCE W/
OUTLET AROUND STOCK PILE AREA.
16. PER NPDES REQUIREMENTS, A RAIN GAUGE, SELF -INSPECTIONS RECORDS, PERMIT AND S&E PLAN ARE REQUIRED TO BE MAINTAINED ON
SITE AND ACCESSIBLE DURING INSPECTION. IT IS RECOMMENDED THAT THESE ITEMS BE PLACED IN A PERMITS BOX AT THE BEGINNING OR
ENTRANCE OF THE PROJECT.
Ili'. EROSION AND SEDIMENT CONTROL (E&SC) PERMIT AND A CERTIFICATE OF COVERAGE (COC) MIDST BE OBTAINED BEFORE ANY LAND
DISTURBING ACTIVITIES OCCUR. THE COC CAN BE OBTAINED BY FILLING OUT THE ELECTRONIC NOTICE OF INTENT (e-NOI) FORM AT
DEQ.NC.GOV/NCGO1. PLEASE NOTE, THE e-NOI FORM MAY BE FILLED OUT ONCE THE PLANS HAVE BEEN APPROVED. A COPY OF THE E&SC
PERMIT, THE COC, AND A HARD COPY OF THE PLAN MUST BE KEPT ON SITE, PREFERABLY IN A PERMITS BOX AND ACCESSIBLE DURING
INSPECTIONS.
18. WHEN THE PROJECT IS COMPLETE, THE PERMITTEE SHALL CONTACT DEMLR TO CLOSE OUT THE E&SC PLAN. AFTER DEMLR INFORMS THE
PERMITTEE OF THE PROJECT CLOSEOUT, VIA INSPECTION REPORT, THE PERMITTEE SAHLL VISIT DEG.NC.GOV/NCGO1 TO SUBMIT AN
ELECTRONIC NOTICE OF TERMINATION (e-NOT). A $100 ANNUAL GENERAL PERMIT FEE WILL BE CHARGED UNTIL THE e-NOI HAS BEEN
FILLED OUT.
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DATE:
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PART III
SELF -INSPECTION, RECORDKEEPING AND REPORTING
SECTION A: SELF -INSPECTION
Self -inspections are required during normal business hours in accordance with the table
below. When adverse weather or site conditions would cause the safety of the inspection
personnel to be in jeopardy, the inspection may be delayed until the next business day on
which it is safe to perform the inspection. In addition, when a storm event of equal to or
greater than 1.0 inch occurs outside of normal business hours, the self -inspection shall be
performed upon the commencement of the next business day. Any time when inspections
were delayed shall be noted in the Inspection Record.
Frequency
Inspect
(during normal
Inspection records must include:
business hours)
(1) Rain gauge
Daily
Daily rainti l amounts.
maintained in
It no daily rain gauge observations are made during weekend or
good working
holiday periods, anc no individuai-day rainfall in`ormation is I
order
available, record the cumulative rain measurement for those un-
attended days (and this will determine it a site inspection is
needed). Days an which no rainfall occurred shall be recorded as
"zero." the permittee may use another rain -monitoring device
approved by the Division
At least once per
1. Identificatinn of the measures inspected,
(2) F&SC
Measures
7 calendar days
2. Da _c and time of the inspection,
and within 24
3. Name of the person performing the Inspection,
hours of a rain
4. Indication of whether the measures were operating
event > 1.0 inch in
properly,
24 hours
5. Description of maintenance needs for the measure,
6. Description, evidence_ and date of corrective actions taken_
At least once per
(3) Stormwater
1. Identification of the discharge outtalls inspected,
discharge
7 calendar days
2- Date and time of the inspection,
outtalls (SDOs)
and within 24
3. Name of the person performing the inspection,
hours of a rain
4. Evidence of indicators of stormwater pollution such as oil
event> 1.0 inch in
sheen, floating or suspended solids or discoloration,
24 hours
5. Indication of visible sediment leaving the site,
(4) Perimeter of
_
At least once per
6. Description, evidence and date of corrective actions taken.
If visible sedimentation is found outside site limits, then a record
site
7 calendar days
of the following shall be made:
and within 24
1. Actions taken to clean up or stabilize the sediment that has left
hours of a rain
the site limits,
event> 1.0 irch in
2. Desrri ptinn, evk9Pnre, and date of corrective actions Taken, and
24 hours
3. An explanation as to the actions taken to control future
releases.
(5) Streams or
At least orce per
If the stream or wetland has increased visible sedimentation or a
wetlands onsite
7 calendar days
stream has visible increased turbidity from the construction
or offsite
and within 24
activity, then a record of the following shall be made:
(where
hours of a rain
1. Description, evidence and date of corrective actions taken, and
accessible)
event> 1.0 inch in
2. Records of the required reports to the appropriate Division
24 ho.irs
Regional Office per Part III, Section C, Item (2)(a) of this permit
of this permit.
(6) Ground
After each phase
1. The phase of grading (installation of perimeter E&SC
stabilization
of grading
measures, clearing and grubbing, installation of storm
measures
drainage facilities, completion of all land -disturbing
activity, construction or redevelopment, permanent
ground cover).
2. Documentation that the required ground stabilization
measures have beer provided within the required
timeframe or an assurance that they will be provided as
soon a5 possible,
NOTE: The rain inspection resets the required 7 calendar day inspection requirement.
NORTH CAROLINA
f! Environmental Quality
PART III
SELF -INSPECTION, RECORDKEEPING AND REPORTING
SECTION B: RECORDKEEPING
1. E&SC Plan Documentation
The approved E&SC plan as well as any approved deviation shall be kept on the site. The
approved E&SC plan must be kept up-to-date throughout the coverage under this permit.
The following items pertaining to the E&SC plan shall be documented in the manner
described:
_ -
Item to Document
- _---
Documentation Requirements
(a) Each E&SC Measure has been installed
Initial and date each E&SC Measure on a copy
and does not significantly deviate from the
of the approved E&SC Plan or complete, date
locations, dimensions and relative elevatiors
and sign an inspection report that lists each
shown on the approved E&SC Plan.
E&SC Measure shown on the approved E&SC
Plan. This documentation is required upon the
initial installation of the E&SC Measures or if
the E&SC Measures are modified after initial
installation.
(b) A phase of grading has been completed.
', Initial and date a copy of the approved E&SC
Plan or complete, date and sign an inspection
report to indicate completion of the
construction phase.
(c) Ground cover is located and 7nstalled
1 Initial and date a copy of the approved E&SC
in accordarce with the approved E&SC
Plan or complete, date and sign an inspection
Plan.
report to indicate compliance with approved
i ground cover specifications.
(d) The maintenance and repair
Complete, date and sign an inspection report.
requirements for all E&SC Measures
have been performed. j
(e) Corrective actions have been taken Initial and date a copy of the approved E&SC
to E&SC Measures. Plan or complete, date and sign an inspection
report to indicate the completion of the
j corrective action.
2. Additional Documentation
In addition to the E&SC Plan documents above, the following items shall be kept on the
site
and available for agency inspectors at all times during normal business hours, unless the
Division provides a site -specific exemption based on unique site conditions that make this
requirement not practical:
(a) This general permit as well as the certificate of coverage, after it is received.
(b) Records of inspections made during the previous 30 days. The permittee shall record
the required observations on the Inspection Record Form provided by the Division or
a similar inspection form that includes all the required elements. Use of
electronically -available records in lieu of the required paper copies will be allowed if
shown to provide equal access and utility as the hard -copy records.
(c) All data used to complete the Notice of Intent and older inspection records shall be
maintained for a period of three years after project completion and made available
upon request. [40 CFR 122.41]
SELF -INSPECTION, RECORDKEEPING AND REPORTING
SECTION C: REPORTING
1. Occurrences that must be reported
Permittees shall report the following occurrences:
(a) Visible sediment deposition in a stream or wetland.
(b) Oil spills if:
• They are 25 gallons or more,
• They are less than 25 gallons but cannot be cleaned up within 24 hours,
• They cause sheen on surface waters (rega-dless of volume), or
• They are within 100 feet of surface waters (regardless of volume).
(a) Releases of hazardous substances in excess of reportable quantities under Section 311.
of the Clean Water Act (Ref: 40 CFR 110.3 and 40 CFR 117.3) or Section 102 of CERCLA
(Ref: 40 CFR 302-4) or G.S. 143-215.85.
(b) Anticipated bypasses and unanticipated bypasses.
(c) Noncompliance with the conditions of this permit that may endanger health or the
environment.
2. Reporting Timeframes and Other Requirements
After a permittee becomes aware of an occurrence that must be reported, he shall contact
the appropriate Division regional office within the timeframes and in accordance with the
other requirements listed below. Occurrences outside normal business hours may also be
reported to the Division's Emergency Response personnel at [phone], (800)
858-0368 or [phone].
Occurrence
(a) Visible sediment
deposition in a
stream or wetland
(b) oil spills and
release of
hazardous
substances per Item
'I (b)-(c.) above
(c) Anticipated
bypasses [40 CFR
122.41(m)(3)j
(d) Unanticipated
bypasses [40 CFR
122.41(m)(3)]
(e) Noncompliance
with the conditions
of this permit that
may endanger
health or the
environmont[40
CFR 122.41(I)(7)]
Reporting Tim_efra_mes (After Discovery) and Other Requirements
• Within 24 hours, an oral or electronic notification.
Within 7 calendar days, a report that contains a description of the
sediment and actions taken to address the cause of the deposition -
Division staff may waive the requirement for a written report on a
case -by -case basis.
• If the stream is named on the as impaired for sediment -
related causes, the permiitee may be required to perform additional
monitoring„ inspections or apply more stringent practices if staff
detemaine that additional requirements are needed to assure compliance
with the federal or state impaired -waters conditions.
+ Within 24 hours, an oral or electronic notification. The notification
shall include information about the date, time, nature, volume and
location of the spill or release.
(+ A report at least ten days before the date of the bypass, if possible.
The report shall include an evaluation of the anticipated quality and
( effect of the bypass-_-
+ Within 24 hours, an oral or electronic notification.
+ Within 7 calendar days, a report that includes an evaluation of the
quality and effect of the bypass.
+ Within 24 hours, an oral or electronic notification.
+ Within 7 calendar days, a report that contains a description of the
noncompliance, and its causes; the period of noncompliance,
including exact dates and times, and if the noncompliance has not
been corrected, the anticipated time noncompliance is expected to
continue; and steps taken or planned to reduce, eliminate, and
prevent reoccurrence of the noncompliance. [40 CFR 1.22.41(I)(6).
+ Division staff may waive the requirement for a written report on a
case -by case basis.
L NCGOI SELF-INSPEC-FION, REC RD.KEEPING AND REPORTING EFFECTIVE: 04/01/19
GROUND STABILIZATION AND MATERIALS HANDLING PRACTICES FOR COMPLIANCE WITH
THE NCG01 CONSTRUCTION GENERAL PERMIT
Implementing the details and specifications on this plan sheet will result in the construction'
activity being considered compliant with the Ground Stabilizaticn and Materials Handling
sections of the NCG01 Construction General Permit (Sections E and F, respectively). The
permittee shall comply with the Erosion and Sediment Control plan approved by the
delegated authority having jurisdiction. All details and specifications shown on this sheet
may not apply depending on site conditions and the delegated authority having jurisdiction.',
SECTION E: GROUND STABILIZATION
Required Ground Stabilization Timeframes
Stabilize within this
Site Area Description
many calendar
Timeframe variations
days after ceasing
land disturbance
(a) Perimeter dikes,
swales, ditches, and
7
None
perimeter slopes
(b) High Quality Water
7
None
(HOW) Zones
(c) Slopes steeper than
If slopes are 10' or less in length and are
3:1
not steeper than 2:1, 14 days are
allowed
-7 days for slopes greater than 50' in
length and with slopes steeper than 4:1
-7 days for perimeter dikes, swales,
(d) Slopes 3:1 to 4:1
14
ditches, perimeter slopes and HOW
Zones
-10 days for Falls Lake Watershed
-7 days for perimeter dikes, swales,
(e) Areas with slopes
ditches, perimeter slopes and HQW Zones
flatter than 4:1
14
-10 days for Falls Lake Watershed unless
there is zero slope
Note: After the permanent cessation of construction activities, any areas with temporary
ground stabilization shall be converted to permanent ground stabilization as soon as
practicable but in no case longer than 90 calendar days after the: last land disturbing
activity. Temporary ground stabilization shall be maintained in a manner to render the
surface stable against accelerated erosion until permanent ground stabilization is achieved.
GROUND STABILIZATION SPECIFICATION
Stabilize the ground sufficiently so that rain
will not dislodge the soil. Use one of the
techniques in the table below:
Temporary Stabilization
Permanent Stabilization
• Temporary grass seed covered with straw of
• Permanent grass seed covered with straw or
other mulches and tackifiers
other mulches and tackitiers
• Hydroseeding
• Geotextile fabrics such as permanent soil
• Rolled erosion control products with or
reinforcement matting
without temporary grass seed
• Hydroseeding
+ Appropriately applied straw or other mulch
• Shrubs or other permanent plantings covered
• Plastic sheeting
with mulch
• Uniform and evenly- distributed ground cover
sufficient to restrain erosion
• Structural methods such as concrete, asphalt or
retaining walls
• Rolled erosion control products with grass seed
POLYACRYLAMIDES (PAMS) AND FLOCCULANTS
1. Select flocculants that are appropriate for the soils being exposed during
construction, selecting from the NC DWR list of Approved PAMS/F(occu(ants.
2. Apply flocculants at or before the inlets to Erosion and Sediment Control Measures.
3. Apply flocculants at the concentrations specified in the NC DWR List of Approved
PAMS/Flocculants and in accordance with the manufacturer's instructions.
4. Provide ponding area for containment of treated Stormwater before discharging
offsite.
5. Store flocculants in leak -proof containers that are kept under storm -resistant cover
or surrounded by secondary containment structures.
EQUIPMENT AND VEHICLE MAINTENANCE
1. Maintain vehicles and equipment to prevent discharge of fluids.
2. Provide drip pans under any stored equipment.
3. Identify leaks and repair as soon as feasible, or remove leaking equipment from the
project.
4. Collect all spent fluids, store in separate containers and properly dispose as
hazardous waste (recycle when possible).
5. Remove leaking vehicles and construction equipment from service until the problem
has been corrected.
6. Bring used fuels, lubricants, coolants, hydraulic fluids and other petroleum products !,
to a recycling or disposal center that handles these materials.
LITTER, BUILDING MATERIAL AND LAND CLEARING WASTE
1. Never bury or burn waste. Place litter and debris in approved waste containers.
2. Provide a sufficient number and size of waste containers (e.g dumpster, trash
receptacle) on site to contain construction and domestic wastes.
3. Locate waste containers at least 50 feet away from storm drain inlets and surface
waters unless no other alternatives are reasonably available.
4. Locate waste containers on areas that do not receive substantial amounts of runoff
from upland areas and does not drain directly to a storm drain, stream or wetland.
5. Cover waste containers at the end of each workday and before storm events or
provide secondary containment. Repair or replace damaged waste containers.
6. Anchor all lightweight items in waste containers during times of high winds.
7. Empty waste containers as needed to prevent overflow. Clean up immediately if
containers overflow.
$. Dispose waste off -site at an approved disposal facility.
9. On business days, clean up and dispose of waste in designated waste containers.
PAINT AND OTHER LIQUID WASTE
1. Do not dump paint and other liquid waste into storm drains, streams or wetlands.
2. Locate paint washouts at least 50 feet away from storm drain inlets and surface
waters unless no other alternatives are reasonably available.
3. Contain liquid wastes in a controlled area.
4. Containment must be labeled, sized and placed appropriately for the needs of site.
5. Prevent the discharge of soaps, solvents, detergents and other liquid wastes from
construction sites.
PORTABLE TOILETS
1. Install portable toilets on level ground, at least 50 feet away from storm drains,
streams or wetlands unless there is no alternative reasonably available. If 50 foot
offset is not attainable, provide relocation of portable toilet behind silt fence or place
on a gravel pad and surround with sand bags.
2. Provide staking or anchoring of portable toilets during periods of high winds or in high!
foot traffic areas.
I
3. Monitor portable toilets for leaking and properly dispose of any leaked material. I
Utilize a licensed sanitary waste hauler to remove leaking portable toilets and replace
with properly operating unit.
EARTHEN STOCKPILE MANAGEMENT
1. Show stockpile locations on plans. Locate earthen --material stockpile areas at least
50 feet away from storm drain inlets, sediment basins, perimeter sediment controls
and surface waters unless it can be shown no other alternatives are reasonably
available.
2. Protect stockpile with silt fence installed along toe of slope with a minimum offset of
five feet from the toe of stockpile.
3. Provide stable stone access point when feasible.
4. Stabilize stockpile within the timeframes provided on this sheet and in accordance
with the approved plan and any additional requirements. Soil stabilization is defined
as vegetative, physical or chemical coverage techniques that will restrain accelerated
erosion on disturbed soils for temporary or permanent control needs.
w., ,r; NORTH CAROLINA
Environmental Quality
ONSITE CONCRETE WASHOUT
STRUCTURE WITH 1-14ER
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CONCRETE WASHOUTS
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���E GRA���S�C��
1. Do not discharge concrete or cement slurry from the site.
2. Dispose of, or recycle settled, hardened concrete residue in accordance with local
and state solid waste regulations and at a't approved facility.
3. Manage washout from mortar mixers in accordance with the above item and in
addition place the mixer and associated materials on impervious barrier and within
lot perimeter silt fence.
4. Install temporary concrete washouts per local requirements, where applicable. If an
alternate metnod or product is to be used, contact your approval authority for
review and approval. If local standard details are not available, use one of the two
types of temporary concrete washouts provided on this detail.
5. Do not use concrete washouts for dewatering or storing defective curb or sidewalk
sections. Stormwater accumulated within the washout may not be pumped into or
discharged to the storm drain system or receiving surface waters. Liquid waste must
be pumped out and removed from project.
6. Locate washouts at least 50 feet from star rn drain inlets and surface waters unless it
can be shown that no other alternatives are reasonably available. At a minimum,
install protection of storm drain inlet(s) closest to the washout which could receive
spills or overflow.
7. Locate washouts in an easily accessible area, on level ground and install a stone
entrance pad in front of the washout. Additional controls may be required by the
approving authority.
8. Install at least one sign directing concrete trucks to the washout within the project
limits. Post signage on the washout itself to identify this location.
9. Remove leavings from the washout when at approximately 75% capacity to limit
overflow everts. Replace the tarp, sand bags or other temporary structural
components when no longer functional. When utilizing alternative or proprietary
products, followmanufacturer's instructions.
10. At the completion of the concrete work, remove remaining leavings and dispose of
in an approved disposal facility. Fill pit, if applicable, and stabilize any disturbance
caused by removal of washout.
HERBICIDES, PESTICIDES AND RODENTiCIDES
1.� Store and app y herbicides, pesticides and rodenticides in accordance with label
restrictions.
2. Store herbicides, pesticides and mclenticices in their original containers with the
label, which lists directions for use, ingred ents and first aid steps in case of
accidental poisoning.
3. Do not store herbicides, pesticides and rodenticides in areas where flooding is
possible or where they may spill or leak in.o wells, stormwater drains, ground water
or surface water, if a spill occurs, clean area immediately.
4. Do not stockpile these materials onsite.
HAZARDOUS AND TOXIC WASTE
1. Create designated hazardous waste collection areas on -site.
2. Place hazardous waste containers under cover or in secondary containment.
3. Do not store hazardous chemicals, drums or bagged materials directly on the ground.
EFFECTIVE: 04/01 / 19
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DESIGNED BY:
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DRAWN BY:
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CHECKED BY:
DFB
PROJECT NO.:
2566-BH
DATE:
jUL.Y 2020
SCALE:
AS SHOWN

STONE FILTER OF 1" GRAVEL PLACED
AGAINST FENCING WHERE REQUIRED.
8'-0" MAX 81-0" MAX
WIRE
MESH
SILT
FENCE
FILTERING MESH BACKING
n o ' ANCHOR
' ' �c�� '
FABRIC ;� � / DITCH
u
LLJ
|co ~�--1�3 LB/FT STEEL p0�T� (TYp)
NOTES: ' '
1. POSTS SET AT DEPTH OF 4' FOR EARTH BACKFILL. ANCHOR DITCH IS 8"X 4" AND FILL IS TO BE COMPACTED.
2. PROVIDE ADEQUATE EXCAVATION AHEAD OF SILT FENCE TO ACT AS A VELOCITY BREAK AND SILT TRAP.
3. CONTRACTOR MAY USE MATERIAL ORMETHOD UPON APPROVAL FROM ENGINEER.
4. FLOW SHALL NOTRUN PARALLEL WITH THE FENCE. END OF SILT FENCE NEEDS TO BE TURNED UPHILL.
5. SEE NCSTATE DE{lPRACTICE STANDARDS }6SPECIFICATIONS.
MAINTENANCE
l. INSPECT SEDIMENT FENCES AT LEAST ONCE A WEEK AND AFTER EACH RAINFALL > 11N. MAKE ANY REQUIRED
REPAIRS IMMEDIATELY.
I. ANY DAMAGED FABRIC SHOULD 8EREPLACED IMMEDIATELY.
3. SEDIMENT WILL BE REMOVED FROM BEHIND SEDIMENT FENCE WHEN ACCUMULATION REACHES 6 INC-IIES.
SEDIMENT FENCE WILL BEREPAIRED ASNECESSARY TO MAINTAIN ABARRIER AND PROVIDE ADEQUATE STORAGE
VOLUME FOR THE NEXT RAIN EVENT.
4. SILT FENCE SHOULD NOT BE USED ALONE BELOW GRADED SLOPES GREATER THAN 10, IN HEIGHT.
SILT FENCE
C-2.1 NOT TO SCALE
n��-� l �A^ i� AND |
`�..,.��~ | . , .,../`' . _., '"." '` '
�
/
al: fescue 2Q0 (4 _U O SO.FT.)
NURSE !` '\||5
-------'- -
Be{we*r, May 1 c� � ^ } b. odd 1C | 15 |b/ocre {S4rdog/oss.
Before May 1, or otfer Aju 15. o./ucre, rye (groin).
3[ED|NC NO-__5
Oct
POSSIBLE Feb Apr 15
Avoid sond'rq [r.x/ ]:v (o "on. If rnua� be done cl. c [r-u. ccc 4O b/oc'_-
Apply cr,d cccord*r.(- to
gruurcl
"y''c"'`i`^ "'`=`"'e jr,d ',00C, '^~^`'^ ° '" '" ' '"'~e'
Ij
Un cronno/s/oo a|opos 000ve W/a negnl'cro /r o'o/nzge rng
1er~porury !lnirgu,opp|y lb/o-re; g,oin st~ow and anc-ior by
stcp|i-ig over (1e iop.Re[e' in oeioiy [or *h ry
[ring 7 opp|icooe.
Mulch ood onohn'�r� rncterio|o nrus� no� be cr|owed t dowr
s|o�.)as where ik*y ccr, doc drainage (Jcv*oes.
M/dN-F� NANC[
|nspe' '.'| 'eDoir req..je-)�|v.Rwfe/[izein 'ute n*r-11cr of the [o||o-wing
yeori �/�e on3(esis n' o�p!y 15J b/ccra ^� l���C� �ow r �uio'y
c � hef 2 � i he �
o '8�| c nc s� �
AGGREGATE
NOTES:
l. ENTRANCE APPLICABLE AT ALL POINTS OF INGRESS AND EGRESS UNTIL SITE IS STABILIZED.
Z. CONSTRUCTION ENTRANCE SHALL BE PLACED FOR MAXIMUM UTILITY BY ALL CONSTRUCTION VEHICLES.
3- PERIODIC TOP DRESSING AND ROUTINE MAINTENANCE SHALL BE PROVIDED ON ENTRANCE AS REQUIRED.
CONTRACTOR SHALL STOCKPILE FRESH STONE ONSITE.
4. ANY MATERIAL THAT MAKES IT TO EXISTING PUBLIC ROADWAY SHALL BE REMOVED AND CLEANED
NMI
N� Lei ON
NOT TO SCALE
�
Si 10 ° :1\ | [!` ` /\|\] |� K]/\K.
o'|[osc
Se'iceo ,�j kz; zu
<u--- |os;�-cezo !
N :yie,s �/edmu-i odd �)5 |b/cc/u, Pe'i
2. A,jg. 1b use �nscnrified se''ceo�seed.
J. V/nn,e o nect cppeoronce 's r`�t xoricec Cnc suooUiuim 4�
Boh�o§roas or 15 b/n:re D*rr-udog'mss.
Between Moy lcrd Aug.`5.mid 1� |h/ccrc Cerrron rniUe� or 15 M/ocre �t.ngo-1�''i
Prior Vcy 1u.- after A(x].15. ndo ZO b/oc'e rye (grcin).
DA|[S
3-3- PJ5S19-E
A./g 2' - 3ep- 11, A.jg ?D- Cc' 7�
� �u� 15 V(--r 21 oz l Apr lb
besl. [n' io|/`csoie, orc |oie wintcr \--speJezas.Oyorooeding of Kobe {espodez./
seeding io| /�n��o is v-ry ef`*ciive. Use -innj|ed Berrnudog'oss secd i-i fc|.
''U'L �N�NOWEK[S !
- —
Aopy lime ond [erUizor ocoording to soilt-esIs, o\ opp/y 4.0001 |o/ocro
uro|!irnestone o�c 1,OOO �b/ocre 1�-1O 1O fsr[!i/e'�
1.30,O'5.00O b/ooro g-cm ut,ow, or ccwvcie7| cover of sui.'
� -�(erioi �ncnor 'nu|ch -)y toc<irg with osohot 'ov�rg`or rei['n0_ Nc./g
onchoring rnet�od un y�een slopes.
�erer'/ ': n the second year ur|eosg'ow�h is �,jJy odeq,Aota.Noy be nnowed once
or iwicr o yecr'out -noWng is ici [-�eneed. [a-jizc`o,d r|c-) oor~ogod
do(o|y,
AS NOTED ON DRAWING
DITCH |NV
4" OF *57 GRANULAR STONE
lujult"I low
NOT TO SCALE
SIDE VIEW
-~-45°
(TYP}
RIP -RAP NCD{}T CLASS U
EROSION CONTROL STONE (ECS
FILTER FABRIC, M|RAF||4JS
FILTER OF I INCH DIAMETER # 57
WASHED STONE
NOTE:
SIoFENCcFABRIC mOVERLAP
HARDWARE CLOTH BY 12 INCHES
MAINTENANCE
INSPECT SILT FENCE OUTLET EVERY SEVEN DAYS
�
AND WITHIN 34HR8AFTER EVERY 1IN. RAIN
EVENT. REMOVE ACCUMULATED SEDIMENT.
REMOVE CONTAMINATED STONE AND REPLACE.
�
SILT FENCE FABRIC ON
WIRE FENCE
3' LONG MIN., 2"x4l" STEEL POSTS
TYI.INBT
' OR BASIN \
\
- - IN
J L. J-#57STONE
r= r= C= 8h}_�� /|
V,^^-°^
GATHER EXCESS
1/4" WIRE MESH AT CORNERS
NOTES:
l. DRIVE POSTS INTO THE GROUND TDADEPTH 0F1.5/
2. WIRE MESH SHALL 8EHARDWARE CLOTH (Z3GAUGE MlN]AND SHALL HAVE MESH
OPENINGS. BURY FABRIC 1'ANDEXTEND TDTHE TOP OFTHE POSTS.
3.SEDIMENT CONTROL STONE SHALL 8E#S7STONE. HEIGHT OFSTONE ATWIRE MESH
SHALL. 8E12INCHES.
4. FASTEN FABRIC SECURELY ATTHE CORNER POSTS.
NOT TO SCALE
Oct 00.
00
HARDWARE CLOTH
ON WIRE FENCE
PLAN VIEW
STEEL FENCE POST
GRADE 1.0
STEEL FENCE POST SET
- HARDWARE CLOTH �` | MAXIMUM 2FEET Ap«n/ | WIRE FENCE
---
FENCE FABRIC 6 INCHES INTO THE TRENCH
FRONT VIEW
SILT
FENCE
OUTLET
NOT TO SCALE
[&B
P MAX. SPACING
VERLAP
0 OM
TOP ALONG EDGES
LU
Lu STAPLE LOCATIONS (TYP.)
Cn
ULJ
00 GRADE SLOPE
ACROSS MIDDLE
Lu
Lu F-- NETTING OR MATTING
INSTALLATION OF LINER: MAINTENANCE:
1.) APPLY LIME, FERTILIZER, AND SEED BEFORE LAYING LINER. INSPECT PERIODICALLY OK
Z.) LAY LINER FROM TOP 0FSLOPE OR CHANNEL AND UNROLL AFTER RAINSTORMS FOR
E�OSJONORFAILURE REPAIR
ITDOVVN�HEGRAD� 4LUJVVNETTIMGTOLAYLD0�ELY '
� /\LLVV�SHEDQUTAREASBY
WITH WRINKLES. DO �
� ' RE -GRADING, RE -SEEDING,
" ANDQE'lNSl�LLI0GLINER
3) BURY DEEP, � AND MULCH AS&EUUIRE|]'
COVER VVITHSOIL AND TAMP FIR�4LY. PROVIDE STAPLES
(1''WIDE x6"LONG MlN.)AND OVERLAP ASSHOWN
ABOVE.
NORTH AMERICAN GREEN S150 OR EQUAL.
TEMP LINER DETAIL
r7
NOT TO SCALE
ALL DITCHES SHALL BE LINED WITH
�
CHECKED BY:
[)FB
PROJECT NO.:
2566-BH
DATE:
AUGUST202O
SCALE:
AS NOTED