MO-88838_96107_CA_IAR_20210517_Initial Abatement Report

IWLighthouse
Technical
ENVIRONMENTAL CONSULTANTS
SOR AND GKOUNDWATER SPMAU S
May 17, 2021
Ms. Mary Anne Rayburn
Isgett Distributers, Inc.
51 Highland Center Boulevard
Asheville, North Carolina 28806-1006
Re: Initial Assessment Report
Isgett Distributers -Used Oil Spill
January 8, 2021
Hilbish Ford
2600 South Cannon Boulevard
Kannapolis, North Carolina
Cabarrus County
Dear Ms. Rayburn
In conjunction with cleanup efforts by Carolina Environmental Response Team (CERT), Lighthouse
Technical (Lighthouse) completed an initial assessment of the impact to soil and groundwater from the
release of petroleum noted above. The results of the post excavation soil analyses and groundwater
samples are included with this report. If you have questions, please contact us at 704-237-4209.
Sincerely,
Lighthouse Technical, P.C.
Steven B. Lucas, L.G.
Environmental Geologist
cc Mooresville Regional Office-NCDEQ
Environmental Consultants -Soil and Groundwater Specialists
Charlotte Roanoke Rapids
P.O. Box 1379, Huntersville, North Carolina 28070
Phone: [phone] - www.lighthousetechcorp.com

2
Initial Site Assessment Report
A. Site Information
Date of Report: May 17, 2021
Date of Release: January 8, 2021
Material Released: Used Oil
Quantity: Unknown (Estimated at 500 to 1,000 gallons)
Responsible Party: Isgett Distributers, Inc.
51 Highland Center Boulevard
Asheville, North Carolina 28806-1006
Contact: Mary Anne Rayburn
Spill Location: Hilbish Ford
2600 South Cannon Boulevard
Kannapolis, North Carolina
Latitude: N 35.459196
Longitude: W-80.610201
Cabarrus County
Source: Handheld GPS at spill location
Cleanup Contractor: CERT
PO Box 681016
Charlotte, North Carolina 28216
877-505-6799
Contact: Shane Roberts
Consultant: Lighthouse Technical, PC
PO Box 1379
Huntersville, North Carolina 28070
704-237-4209
Contact: Steven B. Lucas
Laboratory:
Certification:
RED Lab, LLC
5598 Marvin K. Moss Lane
Wilmington, North Carolina 28409
844-384-7815
Contact: Felicia Owen
I Steven B. Lucas, a Licensed Geologist for Lighthouse Technical,
P.C., do certify that the information contained in this report is correct
and accurate to the best of my knowledge. Lighthouse Technical, P.C.
is licensed to practice geology in North Carolina. The certification
number of the corporation is C-478.
Pace Analytical, Inc.
9800 Kincey Avenue
Huntersville, North Carolina 28078
704-875-9092
Contact: Kevin Herring

B. Site History and Impact
On January 8, 2021, an Isgett Distributers (Isgett) tank truck arrived to deliver a load of transmission
fluid to the Hilbish Ford facility (Hilbish) located at 2600 South Cannon Boulevard in Kannapolis, North
Carolina. To deliver the transmission fluid, Isgett tank truck had to park near two above ground storage
tanks (ASTs) located in the back lot of the dealership. The ASTs stored oil from the garage vehicle
repair operation. The stored oil was a source of fuel for heaters in the Hilbish garage area. As the truck
began to leave, a product pipe on the bottom of one of the ASTs was damaged which allowed oil to leak
from the AST. The oil flowed west across an asphalt parking lot and then south to a storm drain. The
storm drainpipe allowed the oil to flow further west into a wooded utility easement, off the Hilbish Ford
property. The flow of oil continued downslope through under brush, to a dry stream bed, stopping before
it reached Three Mile Branch.
The exact amount of used oil released is unknown however Hilbish estimated the amount to be 500 to
1,000 gallons. Figures 1 and 2 illustrate the location of the incident.
The spilled oil initially impacted the asphalt backlot of the Hilbish facility. The flow of oil also reached
an area of soil parallel with the back lot fence. From the asphalt lot, the oil flowed down a storm drain
inlet and impacted a slope leading to a City of Kannapolis sewer right of way. The sewer right of way
was a large, wooded area with Three Mile Branch flowing north to south at the base of the hill. The oil
reached a dry stream bed just before the stream; however, oil did not reach Three Mile Branch.
The area land use is residential and light industrial. No water supply wells were observed within "line
of site" of the spill area. A sewer main line ran through the center of the right of way, east of Three Mile
Branch. Three Mile Branch was the only surface water body nearby.
A UST-62 24-Hour Notification of Discharge Form was submitted to the Mooresville Office of the North
Carolina Department of Environmental Quality (NCDEQ). Appendix A includes a copy.
C. Free Product Investigation
Carolina Environmental Response Team (CERT) of Charlotte, North Carolina responded to assist with
cleanup and initial abatement activity. CERT recovered 4,000 gallons of petroleum and petroleum
contact water during the initial abatement. The water was generated from pressure washing the Hilbish
rear parking lot and recovery from the areas near Three Mile Branch. No ongoing free product recovery
was necessary after the initial response and excavation of soils.
D. Surface Water Investigation
The day of the incident, CERT placed a containment boom, absorbent booms, and pads along Three Mile
Branch, south of the impacted dry stream bed. Lighthouse was contacted on January 11, 2021 and
walked the spill site that day. Lighthouse observed minimal petroleum sheen in Three Mile Branch and
no free product.

0
E. Initial Response and Abatement Action
As noted above, CERT responded to the incident the day it occurred. Crews began cleanup of the asphalt
lot behind the car dealership using oil dry and absorbent pads. CERT also used a vacuum truck to recover
puddled oil along the back lot fence line. After tracing the spill further west and downhill into the
wooded sewer right of way, absorbent pads and booms were placed in Three Mile Branch as a precaution.
Puddled oil was recovered along the flow path using a vacuum unit.
F. Soil Waste Evaluation
To evaluate the soil waste for disposal, a sample of the impacted soil was collected at the fence line
along the back lot of the Hilbish property. Sample W-1 was submitted to Pace analytical in Huntersville,
North Carolina for analysis for Total Petroleum Hydrocarbon as Gasoline Range (GRO) and Diesel
Range Organics (DRO), methods 8260, 8270 and TCLP metals. The analysis included a DRO result of
115 mg/kg, arsenic at .56 mg/l, barium at .86 mg/1 and cadmium at .0085 mg/l. No compounds were
detected by the 8260 and 8270 analysis. The DRO result is above the states action level of 100 mg/kg.
The arsenic, barium and cadmium detections are below the hazardous waste levels. Appendix B includes
the laboratory report.
G. Excavation of Contaminated Soil and Soil Sampling
Impacted soil was excavated in three areas:
1) A 75-foot-long strip of soil along the fence at the west edge of the Hilbish asphalt back lot
2) The wooded City of Kannapolis right of way down slope and further west under the outfall of
the storm drain outfall
3) Sand and stream gravel were removed in the stream bed near Three Mile Branch.
CERT began excavation of the impacted soils in Area 1 on January 10, 2021. Lighthouse was on site to
collect post excavation samples the next day. Post excavation samples S-1 through S-5 were collected.
The excavation depth ranged from .25 to 1 foot.
Excavation in Area 2 began on January 12, 2021. Post excavation samples S-6 through 5-15 were
collected. The excavated area was 35 feet long, 10 to 12 feet wide and 2.5 to 3 feet deep. Soil removal
extended from the slope from the rear of the Hilbish lot (under the storm water discharge pipe), west to
the graveled access road that ran north to south through the sewer right of way. Groundwater was noted
collecting in the bottom of this excavation.
Oil flowed under the right of way access road and impacted soils near Three Mile Branch (Area 3).
Excavation in Area 3 took place on January 15, 2021. Post excavation soil samples 5-17 through 5-25
were obtained, and groundwater was noted collecting in the bottom of this excavation. Area 3 extended
into a dry stream bed that was filled with sand and gravel. Water and oil were found inches below the
sand surface. A vacuum unit was used to remove oil and petroleum contact water as it collected.
Absorbent pads and booms were also used to recover the oil. Absorbents were removed once there was
no liquid phase hydrocarbon noted.
The soil samples were collected using a stainless -steel spade or hand auger. The sampling instrument
was decontaminated with water and Alconox between sample locations. Each sample was placed in a
laboratory supplied container and submitted to RED Lab, LLC in Charlotte, North Carolina. The soil

samples were analyzed using a QED UVF petroleum analyzer with finger printing calibration. Each
sample was analyzed for Total Petroleum Hydrocarbon -Gasoline Range Organics (TPH-GRO), Diesel
Range Organics (TPH-DRO) and Total BTEX.
The results are illustrated on Table 1. Two areas needed further excavation due to initial TPH DRO
results being greater than the state action level. Sample area S-1 was further excavated to a depth of 1
foot and sample 5-16 was collected. Sample area 5-18 was further excavated to a depth of 1.5 foot and
sample 5-25 was collected.
All post excavation samples had TPH GRO and DRO results below the state action levels. Figures 3 and
4 illustrate the areas of impact and sample locations. Appendix C includes the laboratory reports.
CERT organized disposal of the impacted soil. The total amount of excavated soil was 179.21 tons.
CERT transported the soil to Soil Solutions of the Carolinas in Shelby, North Carolina. Appendix D
includes the waste disposal documentation provided by CERT, including the liquid disposal
documentation.
H. Groundwater Assessment
Two groundwater monitor wells were installed on March 10, 2021. Both wells were installed by a
licensed well driller with Eastern Carolina Environmental Services. Well MW-1 was installed where soil
was impacted below the discharge of the storm drain piping originating in the Hilbish asphalt lot (Area
2). Well MW-2 was installed in Area 3 as it led to the stream bed. The well construction records are
included as Appendix E.
The depth to groundwater ranged from 3.5 feet in well MW-1 to 1.02 feet in well MW-2. Both wells
were bailed of three well volumes before sampling on March 11, 2021. The groundwater samples were
taken to Pace Analytical of Huntersville, North Carolina and submitted for analysis by EPA methods
6200B, 625 Base/ Neutral/Acid (Plus 10 non targeted peaks), MADEP EPH and VPH, Total Metals
Chromium and Lead.
As noted on Table 2, the analysis for MW-1 showed a level of chromium (19.1 ug/1) above the NCAC
2L Class GA Standards. The analysis for MW-2 showed a chromium result of 28.1 ug/l. Lead was
detected at 33.0 ug/l. Benzene was detected at 2.4 ug/l. These results are above the NCAC 2L Class GA
Standards.
Wells MW-1 and MW-2 were further developed on April 21, 2021. Lighthouse returned on April 26,
2021 and bailed each well before sampling for the second time. The samples were analyzed by the same
methods listed above for the March 11, 2021 sampling round. The MW-1 analysis showed non -detect
results for each of the laboratory methods. The MW-2 analysis revealed one compound above the NCAC
2L Class GA Standards, benzene at 1.1 ug/L. The laboratory reports can be found in Appendix F.
I. Conclusions
Hilbish Ford utilized an AST to store oil generated from their auto maintenance activity. The oil was
used to fuel a heating system in the garage. While making a delivery of transmission oil to the facility,
an Isgett delivery truck broke a pipe coming from the AST which caused a release of oil. The spill
impacted an asphalt parking lot at the rear of the facility and soil near the property boundary. The spill
flowed west down a slope and impacted soil in a wooded sewer utility right of way. Further west the

101
flow of oil stopped in a sand bank near Three Mile Branch, the nearest water way. A small amount of
petroleum sheen was initially noted in the stream but no free product.
The cleanup contractor utilized a vacuum truck, absorbent pads and booms to recover the released oil
from the car dealership parking lot, the drainage feature leaving the lot and the sand bank nearest the
stream. Impacted soil was excavated at the rear of the dealership back lot, from the sloped and wooded
utility right of way and the sand bank near the stream.
After soil excavation, post excavation samples were collected. All post excavation samples had TPH
results below the state action levels. Groundwater was observed in the excavations at two locations.
Two groundwater monitor wells were installed and sampled on two dates. Levels of chromium, lead
and benzene were detected above the NCAC 2L Class GA Standards in the first sampling round (March
11, 2021). Both wells were further developed, and the wells were resampled approximately six weeks
after they were initially installed (April 26, 2021). For the last sampling date, all compounds were non -
detect for all methods in MW-1. The only compound detected in MW-2 above the NCAC 2L Class GA
Standard was benzene at 1.1 ug/l.
Based on these lab results for the soil and the downward trend for compounds detected in groundwater,
we recommend closure for the incident. A copy of this report will be forwarded to the NCDEQ
Mooresville regional office. They will review the report and respond accordingly.
J. Report Limitations
This report has been prepared by Lighthouse Technical, P.C. (Lighthouse) for the use of Isgett
Distributers and the North Carolina Department of Environment Quality. The findings and technical
interpretations included in this report are specific to the area of investigation. This assessment of
subsurface conditions has been performed in accordance with generally accepted practices of assessing
the subsurface for contaminants.
The conclusions presented in this report are based on subsurface sampling performed at selected
locations and depths. The data collected represent the conditions at the sample location, at the time of
sample collection only. There may be conditions between borings or samples that differ from those
presented in this report. Such conditions could not be predicted by this assessment.
Lighthouse by virtue of providing the services described in this report, does not assume the responsibility
of the person(s) in charge of the site, or otherwise undertake the responsibility for reporting to any Local,
State, or Federal public agencies as required by law or otherwise to disclose, in a timely manner, unless
so directed by the client, any information that may be necessary to prevent any danger to public health,
safety, or the environment. No warranty expressed or implied is made by the preparation of this report.
0

Table 1
Summary of Soil Sample Laboratory Analysis
Isgett Distributers Used Oil Spill
Hilbish Ford, Kannapolis, North Carolina
Sample ID
Date
Sampled
Sample
Depth (ft.)
Total
gTEX
(mg/kg)
UVF TPH-
GRO
(mg/kg)
State Action
50 mg/kg
UVF TPH-
DRO
(mg/kg)
Level
100 mg/kg
S-1
1/11/2021
0.25
<0.6
127.5
157.8
S-2
1/11/2021
0.25
<0.6
<0.6
1.5
S-3
1/11/2021
0.25
<0.5
<0.5
0.22
S-4
1/11/2021
0.25
<0.6
<0.6
0.25
S-5
1/11/2021
0.25
<0.5
<0.5
0.8
S-6
1/12/2021
3.00
<0.5
<0.5
1
S-7
1/12/2021
2.50
<0.5
<0.5
65.3
S-8
1/12/2021
2.50
<0.7
<0.7
2.3
S-9
1/12/2021
2.00
<0.6
<0.6
0.8
S-10
1/12/2021
1.00
<0.5
<0.5
1.8
S-11
1/12/2021
1.00
<0.4
<0.4
1
S-12
1/12/2021
1.00
<0.5
4.7
7.1
S-13
1/12/2021
2.00
<0.6
<0.6
<0.24
S-14
1/12/2021
0.50
<0.5
<0.5
0.3
S-15
1/12/2021
0.50
<0.4
<0.4
0.8
S-16*
1/13/2021
1.00
<0.6
<0.6
0.3
S-17
1/15/2021
1.50
<0.6
10.1
26.3
S-18
1/15/2021
1.50
<31.7
<31.7
556
S-19
1/15/2021
1.50
<0.6
<0.6
2.8
S-20
1/15/2021
1.50
<0.5
<0.5
57.1
S-21
1/15/2021
1.50
<0.7
<0.7
1.4
S-22
1/15/2021
1.50
<0.8
<0.8
3.8
S-23
1/15/2021
1.50
<0.7
<0.7
0.18
S-24
1/15/2021
1.50
<0.6
<0.6
1.2
S-25**
1/19/2021
1.50
<0.5
<0.5
8.6
Notes:
BTEX-benzene, toluene, ethylbenzene, xylene
mg/kg-Milligrams per kilogram
UVF-Ultraviolet Florescence
PPM-Parts per million (mg/kg)
TPH-GRO-Total Petroleum Hydrocarbon -Gasoline Range Organic
TPH-DRO-Total Petroleum Hydrocarbon -Diesel Range Organic
Concentrations above the state Total Petroleum Hydrocarbon action level
*Resample of S-1
**Resample of S-18

Table 2
Summary of Analytical Results
Monitor Well Samples
Isgett Distribution Used Oil Spill
Hilbish Ford, Kannapolis, North Carolina
Analytical Method
EPA 6010D by EPA
Method 625
MADEP EPH
MADEP VPH
Method 6200
3010A
Aliphatic(
1,2,4-
1,3,5-
Constituent
Aliphatic
Aliphatic
Aromatic
Aliphatic
Aliphatic
Aromatic
Total
Chromium
Lead
All Compounds
C09-C12)
Trimethylb
Trimethylb
Benzene
Ethylbenzene
Toluene
of Concern
(C09-C18)
(C19-C36)
(C9-C22)
(C05-CO8)
(C09-C12)
(C09-C10)
Xylenes
Sample ID
Adjusted
enzene
enzene
Date
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Collected
MW-1
03/11/2021
19.1
5.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4/26/2021
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-2
03/11/2021
28.1
33.0
ND
134
ND
ND
56.3
64.7
54.4
ND
4.9
ND
2.4
2.6
1.9
13.6
4/26/2021
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.1
0.78
1.1
1
ND
2.8
2L Class GA Standards
10
15
0.03
700
10000
200
400
N/A
N/A
N/A
400
400
1
600
600
500
2L Class GSA Standards
10
15
0.03
700
10000
200
400
N/A
N/A
N/A
400
400
1
600
600
N/A
2L Class GCL Standards
I 10000
15000
30
N/A
N/A
N/A
1 N/A
N/A
I N/A
N/A
28500
25000
5000
84500
260000
1 N/A
NOTES:
ND = Not Detected
VPH = Volatile Petroleum Hydrocarbon - Massachusetts Department of
Environmental Protection
EPH = Extractable Petroleum Hydrocarbon - Massachusetts Department of
Environmental Protection
ft. BGS = feet below ground surface
mg/L= milligrams per liter
ug/L = micrograms per liter
Bold data above the 2L Class GA Standards

z
J
Figure 1
Isgett Distributors Used Oil Spill
Hilbish Ford
2600 South Cannon Boulevard
Kannapolis, North Carolina
80.616670 W WGS84 80.600000 W
5� � r 7 .1].t�iae{' .J &ti S� f3ameuG _ 1..:, _ — „V3 •.. ,,,,..;• . !�.
Ji
A;;�.
II-jL5Utah
. t �
_ s-' , S?.,,-'.fy,•9. '�'c�mkeg-�15� � _r.'.
-
L tr{r.•,q ns
LP
Used Oil ASTs
Le `\
�
yy Jf 1
ryt `,t om•+•..• �•.Si .i _ s• e -Y Pc 0':r.,
- hount' Hilbish Ford ;fir
`�•`' ��, fir. ..• _ �, a Syl.
Ch': fc-asyfi •.-,,+ ¢�', t? � ,,+ f, rl,.. , Y- ti k� ��� +'�
r 'g� r • y�Sti - ' 1` i r� . . I � � S I i - �•' � l� �•*�.'a `a
_ '�_- y , Vie+ � .. • ''r
ti ' } � • a 29 � i•� � r
04
r
�1ap,ereated unit c 20fQ Natiorial.Geograp' ic;,2DQ7 Tele alas; Rel. '1J20Q7 ia.
Ind
6
ID I
Ln
rn
z
0 .s 1 M N T
NATIONAL 1OOD 0 Iwo 2000 3" � MILES $o
GEOGRAPHIC , .5 0 WI-OMEFEAS FEET
1O00 0 METERS LO[Kt 03/18/21

Figure 2
Isgett Distributors Used Oil Spill
Hilbish Ford
2600 South Cannon Boulevard
Kannapolis, North Carolina
A

Virginia Street
Asphalt
Parking
Lot
I
I
• S-1 /S-16
Wooded I ��
Very Steep • S-2 ~
Embankment
I �-
Area of Impact I Flow of
Limits of Excavation • S-3 r Spilled Oil
I
• S-4 Asphalt
I /
I f
• S-5
I
Flow of
Spilled Oil
I �
Asphalt
Parking
Lot
Asphalt
Stormwater
Discharge
Pipe
I
Hilbish Ford
Back Lot
I
Wooded I ^ I
Very Steep I I V
Embankment
Fence I
I
I
I
I
I
0 30 Spill Location Coordinates
Feet Soil Sample Location
Scale Approximate and Collection Depth 35.459196 N
-80.610201 W
r- - Lighthouse Figure 3
Isgett Distributing
�+ Used Oil Spill
( Technical,P.C. Post Excavation
'' Environmental Consultants 2600 South Cannon Boulevard
Soil and Groundwater Specialists Soil Sample Locations Kannapolis, North Carolina

Three Mile
Creek
NThree Mile
Creek
0 25
Feet
Scale Approximate
Sewer -_
Line
City of Kannapolis -
Sewer Right of Way -
Gravel
:- Road
Steep
Wooded
Embankment
Steep
Wooded
Embankment
Hilbish Ford _�
Back Lot
Stormwater
Area of Impact Discharge
Limits of Excavation Pipe f
Area of Impact FIOW Of
Limits of Excavation \S-10 Spilled Oil
S-12
Drain
S-14 S-8 S-6
Tile ♦ S-7
S-17 Roadr S-9
S 11
S-19 S-15
f S-13 MW-1
S-20 MW-2 1 :
S-18/S-25
S-21 S-24
S-22 S-23 :
_ _ _ - Area of Vacuum Gravel
Extraction and Oil Road
_= Removal with
Absorbents and
........ Excavation
I .Sewer
Line
Soil Sample Location
and Collection Depth
Steep
Wooded
Embankment
Spill Location Coordinates
35.459196 N
-80.610201 W
Lighthouse Figure 4 Isgett Distributing
- . ;: • ; Technical,P.C. Post Excavation Used oil Spill
' Environmental Consultants Soil Sample Locations 2600 South Cannon Boulevard
-` Soil and Groundwater Specialists Monitor Well Locations Kannapolis, North Carolina

Appendix A

UST-62
24-Hour Notification of Discharge
Form
For Non -UST This torn should be completed and submitted to the UST Section's regional office following a known or suspected release of
Releases of petroleum from a source other than an underground storage tank. This form is required to be submitted within 24 hours of
Petroleum in NC discovery of a known or suspected petroleum release
(DWM USE ONLY)
Suspected Contamination? (Y/N) _X
Release Discovered
Incident # Priority Rank (H,I,L,U) _
Received (time/date)
Confirmed GW Contamination? (YI)
Confirmed Soil Coo lamin lion ?(YIN)
(time/date):
/p Asst
Received By Region
Reported
Samples Taken? (Y!N) Free Pro(Y/N)
by (circle one): Phone, Fax or Report
If Yes(Free product), St a Greatest Thickness: ,Feet
INCIDENT DESCRIPTION
�h
Incident Name: F0
Address (street number/name): a t oo S- C0. mme t 944,
County:
0.
Cityfrown:
1
P1.KH et, b irS
p Code:
Z �9 vg.3
Regional Office (circle one): Asheville, Mooresville. Fayetteville,
Ralei h, Washington, Winningon.
Winston-Salem
Latitude (dedmel degrees): 35, , Vo Aqq Longitude (decimal degrees) : —$p . 60'N 6 7
Obtained by:
❑ GPS
�ectronic topographic map
❑ GIS Address matching
❑ Other
Describe sugpe @d or confirmed releas (nature ofrr��Ilea�se, timIdat of release, quantify ofrelGase, amount of free
mducf /} PrU.,^ 'u: a5v 0/7 T P
a
elide ta(+&-3 F 0�L+�r..�l'il O W, cii . Al &l lu. �o
jctt
lvlro -Z 44-ai-tS fNinS /ej k-q a,c,0b4a^6;k
Describe initial response/abatement (time/date rel ase top7d, yI� anup begur✓compl tod, quantity of product
soil removed, confirmation sam tin iw' RT e w (c/- f S L &J/ -If la jz P.
❑Unknown
Describe location:
(off
0- � &A t.L ft Y!/�IG ��
Des ibe impacted receptors:d fCt t1-LL- r!k
o lL 1<1AL O. l ,% 4 IW ee ,,
SJ P Cti t r �W R LEAPE WAS DISCOVERED (Release coda)
S � p b one)
Observation of Release at Occurrence ❑ Water Supply Well Contamination
❑ Visual or Olfactory Evidence ❑ Surface Water Contamination
❑ Soil Contamination ❑ Other (specify)
❑ Groundwater Contamination
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check one to indicate primary (Check one to indicate primary (Check one) (Check one to indicate primary petroleum product
source) cause) /
type released)
❑ AST (tank) ❑ Spill (Accidental) l7 Petroleum ❑ Gasoline/ Diesel/ ❑ DieseWeg. Oil
44 ❑ Kerosene Blend
yr AST Piping/ Dispenser Spill (Intentional) ❑Both Petroleum
❑
❑ AST Delivery Problem ❑ Cpmosion & Non -Petroleum ❑ E11 — E20
„,/ ❑ E21—E84
Vegetable Oil 100%
eating Oil
❑ OTR Vehicle Tank 4rt' Physical or Mechanical Location ❑ E85 — E99
Lir Waste Oil
❑ OTR Bulk Transport Tank Damage (Check one)
❑ Mineral Oil -no
❑ Equipment Failure ❑ Ethanol 100%
❑ RR Bulk Transport Tank ❑ Facility
PCBs
❑ Mineral Oil
❑ Transformer ❑AST Overfill
❑ Residence
-PCBs
❑ Other Petroleum
❑ Other ❑ AST Installation Problem ❑ Highway/Road
Products
❑ Unknown ❑ Other ❑ Railway
❑ Unknown ❑ Other
Definitions presented on reverse Definitions presented on reverse
Ownershlo
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal S. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
Guidance presented on reverse
w i rums 62 tuvr io/ Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected
List of Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
PARTY RESPONSIBLE FOR RELEASE
(if the source of the release is not an AST system or if it is an AST system and there is a responsible party other than the AST system owner/ operator)
Name of Person/Company
2s ef,L niso�n� bw��rs
Address n ,,
City L
/a 7r-
State
G
Zip Code k
TelephonNum
e �35A3
��dd
AST SYSTEM OWNER (if the source of the release is an AST system)
AST Owner/Company
D
Address s ¢
City
Slate
Zip Code
Telephone Number
AST SYSTEM OPERATOR (if the source of the release is an ASTsystem)
UST Operator/Company (
! J/5� �oc�Q
Address
City
State
Zip Code
Telephone Number
LANDOWNER AT LOCATION OF INCIDENT
Landowner L _ _
Address
City
State
Zip Code
Telephone Number
Draw Sketch of Area or Provide Map (showing incidentsite, location of release, two major road intersections, potential
receptors)
Attach sketch or map to form.
Give Directions to Incident Site Attach directions to formifnecessary.
Person Reporting Incident
Company �s.. spy I42'
Telephone Number qjg 7Y3
Title 0Jf
IAddress Y r ,,,)� 7
Date
UST Form of Sources ; j- .r' V'/K /ly.�� Page 2 of 2
Definitions of Sources /�Gwuv �
AST (Tank): means the tank is used to store product
AST Piping: means the piping and connectors running from the tank to the dispenser or other end -use equipment
AST Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping
AST Delivery Problem: identifies releases that occurred during product delivery to the tank.
OTR Vehicle Tank: means the tank is used to store product to fuel an over the road vehicle
OTA Bulk Transport Tank: means a tank that is used to transport product in bulk over the road (by truck)
RR :bulk Transport Tank: means a tank that is used to transport product in bulk by train
Transformer: means electrical tmnsfanner
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill (Accidental): use this cause when a spill occurs accidentally(e.g., when the delivery hose is disconnected From a fill pipe)
Spill (Intentional): use this cause when a spill occurs intentionally (e.g., intentional dumping or breakage)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion
Equipment failure: use when a release occurs due to equipment failure other than corrosion or physical or mechanical damage
AST Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nonle fails to shut off at the dispenser)
AST Installation Problem: use when the problem is determined to have occurred specifically because the AST system was not installed properly
Other use this option when the cause is known but does not fit into one of the preceding categories
Unknown: use when the cause has not been determined
Guidance: Ownership and Operator Type
Ownership select the category which describes owner of the AST system, bulk transport tank, or other release source
Operator Type select the category which describes the operation in which owner uses the AST system, bulk transport tank, or other release source

Appendix B

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 22, 2021
Steven Lucas
Lighthouse Technical
PO Box 1379
Huntersville, NC 28078
RE: Project: 21003
Pace Project No.: 92516966
Dear Steven Lucas:
Enclosed are the analytical results for sample(s) received by the laboratory on January 15, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92516966
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 21003
Pace Project No.: 92516966
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92516966001 W-1
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 601 OD
KQ
7
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
EPA 9045D
EWS
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: 21003
Pace Project No.: 92516966
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
92516966001
W-1
EPA 8015C Modified
Diesel Range Organics(C10-C28)
115
mg/kg
EPA 601 OD
Arsenic
0.56
mg/L
EPA 601 OD
Barium
0.86
mg/L
EPA 601 OD
Cadmium
0.0085
mg/L
SW-846
Percent Moisture
17.2
%
EPA 9045D
pH at 25 Degrees C
6.5
Std. Units
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit
Analyzed Qualifiers
6.1
01/19/21 14:18
0.050
01/21/21 11:51
0.25
01/21/21 11:51
0.0050
01/21/21 11:51
0.10
01 /15/21 18:26
0.10
01/22/2113:22 H3
Page 4 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92516966
Method: EPA 8015C Modified
Description: 8015 GCS THC-Diesel
Client: Lighthouse Technical
Date: January 22, 2021
General Information:
1 sample was analyzed for EPA 8015C Modified by Pace Analytical Services Charlotte. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 593623
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92517093001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3132402)
• Diesel Range Organics(C10-C28)
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92516966
Method: EPA 8015C Modified
Description: Gasoline Range Organics
Client: Lighthouse Technical
Date: January 22, 2021
General Information:
1 sample was analyzed for EPA 8015C Modified by Pace Analytical Services Charlotte. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92516966
Method: EPA 6010D
Description: 6010 MET ICP, TCLP
Client: Lighthouse Technical
Date: January 22, 2021
General Information:
1 sample was analyzed for EPA 6010D by Pace Analytical Services Asheville. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3010A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92516966
Method: EPA 7470A
Description: 7470 Mercury, TCLP
Client: Lighthouse Technical
Date: January 22, 2021
General Information:
1 sample was analyzed for EPA 7470A by Pace Analytical Services Asheville. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 7470A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92516966
Method: EPA 8270E
Description: 8270E MSSV Microwave
Client: Lighthouse Technical
Date: January 22, 2021
General Information:
1 sample was analyzed for EPA 8270E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 593630
SO: Surrogate recovery outside laboratory control limits.
• LCS (Lab ID: 3132414)
• Terphenyl-d14 (S)
S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
• BLANK (Lab ID: 3132413)
• Terphenyl-d14 (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92516966
Method: EPA 8270E
Description: 8270E MSSV Microwave
Client: Lighthouse Technical
Date: January 22, 2021
Additional Comments:
PROJECT NARRATIVE
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92516966
Method: EPA 8260D
Description: 8260D/5035A/5030B Volatiles
Client: Lighthouse Technical
Date: January 22, 2021
General Information:
1 sample was analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A/5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 11 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92516966
Method: EPA 9045D
Description: 9045 pH Soil
Client: Lighthouse Technical
Date: January 22, 2021
General Information:
1 sample was analyzed for EPA 9045D by Pace Analytical Services Asheville. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H3: Sample was received or analysis requested beyond the recognized method holding time.
• W-1 (Lab ID:92516966001)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 12 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92516966
Sample: W-1
Lab ID: 92516966001 Collected:
01/11/21 10:00
Received: 01/15/21 16:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified
Preparation
Method:
EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-C28)
115 mg/kg
6.1
1
01/19/21 10:47
01/19/21 14:18
Surrogates
n-Pentacosane (S)
93 %
32-130
1
01/19/21 10:47
01/19/21 14:18
629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified
Preparation
Method:
EPA 5030B
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
ND mg/kg
7.8
1
01/19/21 11:27
01/19/21 21:18
Surrogates
4-Bromofluorobenzene (S)
108 %
66-131
1
01/19/21 11:27
01/19/21 21:18
460-00-4
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method:
EPA 3010A
Leachate Method/Date: EPA 1311; 01/19/21
15:38
Initial pH: 5.88; Final
pH: 2
Pace Analytical Services -Asheville
Arsenic
0.56 mg/L
0.050
1
01/21/2102:33
01/21/2111:51
7440-38-2
Barium
0.86 mg/L
0.25
1
01/21/2102:33
01/21/2111:51
7440-39-3
Cadmium
0.0085 mg/L
0.0050
1
01/21/2102:33
01/21/2111:51
7440-43-9
Chromium
ND mg/L
0.050
1
01/21/2102:33
01/21/2111:51
7440-47-3
Lead
ND mg/L
0.025
1
01/21/2102:33
01/21/2111:51
7439-92-1
Selenium
ND mg/L
0.10
1
01/21/2102:33
01/21/2111:51
7782-49-2
Silver
ND mg/L
0.025
1
01/21/2102:33
01/21/2111:51
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 01/19/21
15:38
Initial pH: 5.88; Final
pH: 2
Pace Analytical Services -Asheville
Mercury
ND mg/L
0.00020
1
01/21/2110:08
01/21/2117:33
7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method:
EPA 3546
Pace Analytical Services - Charlotte
Acenaphthene
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
83-32-9
Acenaphthylene
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
208-96-8
Aniline
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
62-53-3
Anthracene
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
120-12-7
Benzo(a)anthracene
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
56-55-3
Benzo(a)pyrene
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
50-32-8
Benzo(b)fluoranthene
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
191-24-2
Benzo(k)fluoranthene
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
207-08-9
Benzoic Acid
ND ug/kg
2000
1
01/19/21 10:50
01/20/21 01:53
65-85-0
Benzyl alcohol
ND ug/kg
802
1
01/19/21 10:50
01/20/21 01:53
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
101-55-3
Butylbenzylphthalate
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
85-68-7
4-ChIoro-3-methyl phenol
ND ug/kg
802
1
01/19/21 10:50
01/20/21 01:53
59-50-7
4-Chloroaniline
ND ug/kg
802
1
01/19/21 10:50
01/20/21 01:53
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
111-91-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92516966
Sample: W-1 Lab ID: 92516966001 Collected: 01/11/21 10:00 Received: 01/15/21 16:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
bis(2-Chloroethyl) ether
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
111-44-4
2-Chloronaphthalene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
91-58-7
2-Chlorophenol
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
7005-72-3
Chrysene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
53-70-3
Dibenzofuran
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
802
1
01/19/21 10:50
01/20/21 01:53
91-94-1
2,4-Dichlorophenol
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
120-83-2
Diethylphthalate
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
84-66-2
2,4-Dimethylphenol
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
105-67-9
Dimethylphthalate
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
131-11-3
Di-n-butylphthalate
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
802
1
01/19/21 10:50
01/20/21 01:53
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2000
1
01/19/21 10:50
01/20/21 01:53
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
606-20-2
Di-n-octylphthalate
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
117-81-7
Fluoranthene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
206-44-0
Fluorene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
87-68-3
Hexachlorobenzene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
77-47-4
Hexachloroethane
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
193-39-5
Isophorone
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
78-59-1
1-Methylnaphthalene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
90-12-0
2-Methylnaphthalene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
15831-10-4
Naphthalene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
91-20-3
2-Nitroaniline
ND
ug/kg
2000
1
01/19/21 10:50
01/20/21 01:53
88-74-4
3-Nitroaniline
ND
ug/kg
2000
1
01/19/21 10:50
01/20/21 01:53
99-09-2 IL
4-Nitroaniline
ND
ug/kg
802
1
01/19/21 10:50
01/20/21 01:53
100-01-6
Nitrobenzene
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
98-95-3
2-Nitrophenol
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
88-75-5
4-Nitrophenol
ND
ug/kg
2000
1
01/19/21 10:50
01/20/21 01:53
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
401
1
01/19/21 10:50
01/20/21 01:53
108-60-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92516966
Sample: W-1 Lab ID: 92516966001 Collected: 01/11/21 10:00 Received: 01/15/21 16:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D/5035A/5030B Volatiles
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Date: 01/22/2021 02:46 PM
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
802
1
01/19/2110:50
01/20/2101:53
87-86-5
ND
ug/kg
401
1
01/19/2110:50
01/20/2101:53
85-01-8
ND
ug/kg
401
1
01/19/2110:50
01/20/2101:53
108-95-2
ND
ug/kg
401
1
01/19/2110:50
01/20/2101:53
129-00-0
ND
ug/kg
401
1
01/19/2110:50
01/20/2101:53
110-86-1
ND
ug/kg
401
1
01/19/2110:50
01/20/2101:53
120-82-1
ND
ug/kg
401
1
01/19/2110:50
01/20/2101:53
95-95-4
ND
ug/kg
401
1
01/19/2110:50
01/20/2101:53
88-06-2
93
%
21-130
1
01 /19/21 10:50
01 /20/21 01:53
4165-60-0
78
%
19-130
1
01 /19/21 10:50
01 /20/21 01:53
321-60-8
97
%
15-130
1
01 /19/21 10:50
01 /20/21 01:53
1718-51-0
42
%
18-130
1
01/19/2110:50
01/20/2101:53
13127-88-3
41
%
18-130
1
01/19/2110:50
01/20/2101:53
367-12-4
53
%
18-130
1
01/19/2110:50
01/20/2101:53
118-79-6
Analytical Method:
EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
6.3
1
01/19/2110:53
01/19/2115:30
71-43-2
ND
ug/kg
6.3
1
01/19/2110:53
01/19/2115:30
100-41-4
ND
ug/kg
6.3
1
01/19/2110:53
01/19/2115:30
108-88-3
ND
ug/kg
12.5
1
01/19/2110:53
01/19/2115:30
1330-20-7
102
%
70-130
1
01/19/2110:53
01/19/2115:30
2037-26-5
97
%
69-134
1
01/19/2110:53
01/19/2115:30
460-00-4
106
%
70-130
1
01/19/2110:53
01/19/2115:30
17060-07-0
Analytical Method:
SW-846
Pace Analytical Services - Charlotte
17.2
%
0.10
1
01/15/2118:26
Analytical Method:
EPA 9045D
Pace Analytical Services -Asheville
6.5
Std. Units
0.10
1
01/22/21 13:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H3
Page 15 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
QC Batch: 593673
Analysis Method:
EPA 8015C Modified
QC Batch Method: EPA 5030E
Analysis Description:
Gasoline Range Organics
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92516966001
METHOD BLANK: 3132634
Matrix: Solid
Associated Lab Samples: 92516966001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
5.9 01/19/21 13:21
4-Bromofluorobenzene (S)
%
90 66-131
01/19/21 13:21
LABORATORY CONTROL SAMPLE:
3132635
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
49.5 44.0
89 70-130
4-Bromofluorobenzene (S)
%
92 66-131
MATRIX SPIKE SAMPLE:
3132637
92516613003 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 98 107 109
70-145
4-Bromofluorobenzene (S)
%
100
66-131
SAMPLE DUPLICATE: 3132636
92516613002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
ND
4-Bromofluorobenzene (S)
%
89
97
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
QC Batch: 594224 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury TCLP
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92516966001
METHOD BLANK: 3132522
Associated Lab Samples: 92516966001
Parameter Units
Mercury mg/L
LABORATORY CONTROL SAMPLE: 3135429
Parameter Units
Mercury mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.00020 01/21/2116:19
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0.0025 0.0025 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3135430 3135431
MS MSD
92516630001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND 0.0025 0.0025 0.0027 0.0026 106 104 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
QC Batch: 594222 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92516966001
METHOD BLANK: 3132522
Matrix:
Water
Associated Lab Samples: 92516966001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
01/21/2110:14
Barium
mg/L
ND
0.25
01/21/2110:14
Cadmium
mg/L
ND
0.0050
01/21/2110:14
Chromium
mg/L
ND
0.050
01/21/2110:14
Lead
mg/L
ND
0.025
01/21/2110:14
Selenium
mg/L
ND
0.10
01/21/2110:14
Silver
mg/L
ND
0.025
01/21/2110:14
LABORATORY CONTROL SAMPLE:
3135423
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
2.5
2.5
100
80-120
2.5
2.5
98
80-120
2.5
2.5
99
80-120
2.5
2.5
99
80-120
2.5
2.4
96
80-120
2.5
2.6
102
80-120
1.2
1.2
98
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3135424
3135425
MS
MSD
92515804002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.5
2.5
99
101
75-125
1
Barium
mg/L
ND
2.5
2.5
2.4
2.5
96
99
75-125
3
Cadmium
mg/L
ND
2.5
2.5
2.5
2.5
98
100
75-125
2
Chromium
mg/L
ND
2.5
2.5
2.4
2.5
97
100
75-125
2
Lead
mg/L
ND
2.5
2.5
2.4
2.5
95
98
75-125
2
Selenium
mg/L
ND
2.5
2.5
2.6
2.6
102
104
75-125
2
Silver
mg/L
ND
1.2
1.2
1.2
1.2
97
99
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
QC Batch: 593665 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92516966001
METHOD BLANK: 3132598
Matrix:
Solid
Associated Lab Samples: 92516966001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Benzene
ug/kg
ND
5.0
01/19/21 12:00
Ethylbenzene
ug/kg
ND
5.0
01/19/21 12:00
Toluene
ug/kg
ND
5.0
01/19/21 12:00
Xylene (Total)
ug/kg
ND
10.0
01/19/21 12:00
1,2-Dichloroethane-d4 (S)
%
105
70-130
01/19/21 12:00
4-Bromofluorobenzene (S)
%
95
69-134
01/19/21 12:00
Toluene-d8 (S)
%
101
70-130
01/19/21 12:00
LABORATORY CONTROL SAMPLE:
Parameter
3132599
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Benzene
ug/kg
1250
1310
105
70-130
Ethylbenzene
ug/kg
1250
1230
99
70-130
Toluene
ug/kg
1250
1300
104
70-130
Xylene (Total)
ug/kg
3750
3900
104
70-130
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
99
69-134
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3132600
3132601
MS
MSD
92516822001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Benzene
ug/kg
242
16700
16700
18200
16900
107
99
67-130
8
Ethylbenzene
ug/kg
30000
16700
16700
45600
44800
93
89
66-130
2
Toluene
ug/kg
10500
16700
16700
28100
26700
106
97
67-130
5
Xylene (Total)
ug/kg
174000
50200
50200
219000
217000
90
87
63-132
1
1,2-Dichloroethane-d4 (S)
%
95
95
70-130
4-Bromofluorobenzene (S)
%
97
99
69-134
Toluene-d8(S)
%
99
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
QC Batch: 593623
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546
Analysis Description: 8015 Solid GCSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92516966001
METHOD BLANK: 3132400
Matrix: Solid
Associated Lab Samples: 92516966001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 5.0 01/19/21 11:54
n-Pentacosane (S)
%
67 32-130 01/19/21 11:54
LABORATORY CONTROL SAMPLE:
3132401
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
66.4 54.6 82 47-130
n-Pentacosane (S)
%
82 32-130
MATRIX SPIKE SAMPLE:
3132402
92517093001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
307 85.5 468 189
10-133 M1
n-Pentacosane(S)
%
78
32-130
SAMPLE DUPLICATE: 3132403
92517093002 Dup
Parameter
Units
Result Result RPD Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
15.4 13.9 10
n-Pentacosane (S)
%
60 62
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
QC Batch: 593630 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92516966001
METHOD BLANK: 3132413
Associated Lab Samples: 92516966001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
336
01/19/21 15:57
1,2-Dichlorobenzene
ug/kg
ND
336
01/19/21 15:57
1,3-Dichlorobenzene
ug/kg
ND
336
01/19/21 15:57
1,4-Dichlorobenzene
ug/kg
ND
336
01/19/21 15:57
1-Methylnaphthalene
ug/kg
ND
336
01/19/21 15:57
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
336
01/19/21 15:57
2,4,5-Trichlorophenol
ug/kg
ND
336
01/19/21 15:57
2,4,6-Trichlorophenol
ug/kg
ND
336
01/19/21 15:57
2,4-Dichlorophenol
ug/kg
ND
336
01/19/21 15:57
2,4-Dimethylphenol
ug/kg
ND
336
01/19/21 15:57
2,4-Dinitrophenol
ug/kg
ND
1680
01/19/21 15:57
2,4-Dinitrotoluene
ug/kg
ND
336
01/19/21 15:57
2,6-Dinitrotoluene
ug/kg
ND
336
01/19/21 15:57
2-Chloronaphthalene
ug/kg
ND
336
01/19/21 15:57
2-Chlorophenol
ug/kg
ND
336
01/19/21 15:57
2-Methylnaphthalene
ug/kg
ND
336
01/19/21 15:57
2-Methylphenol(o-Cresol)
ug/kg
ND
336
01/19/21 15:57
2-Nitroaniline
ug/kg
ND
1680
01/19/21 15:57
2-Nitrophenol
ug/kg
ND
336
01/19/21 15:57
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
336
01/19/21 15:57
3,3'-Dichlorobenzidine
ug/kg
ND
671
01/19/21 15:57
3-Nitroaniline
ug/kg
ND
1680
01/19/21 15:57
4,6-Dinitro-2-methyl phenol
ug/kg
ND
671
01/19/21 15:57
4-Bromophenylphenyl ether
ug/kg
ND
336
01/19/21 15:57
4-ChIoro-3-methyl phenol
ug/kg
ND
671
01/19/21 15:57
4-Chloroaniline
ug/kg
ND
671
01/19/21 15:57
4-Chlorophenylphenyl ether
ug/kg
ND
336
01/19/21 15:57
4-Nitroaniline
ug/kg
ND
671
01/19/21 15:57
4-Nitrophenol
ug/kg
ND
1680
01/19/21 15:57
Acenaphthene
ug/kg
ND
336
01/19/21 15:57
Acenaphthylene
ug/kg
ND
336
01/19/21 15:57
Aniline
ug/kg
ND
336
01/19/21 15:57
Anthracene
ug/kg
ND
336
01/19/21 15:57
Benzo(a)anthracene
ug/kg
ND
336
01/19/21 15:57
Benzo(a)pyrene
ug/kg
ND
336
01/19/21 15:57
Benzo(b)fluoranthene
ug/kg
ND
336
01/19/21 15:57
Benzo(g,h,i)perylene
ug/kg
ND
336
01/19/21 15:57
Benzo(k)fluoranthene
ug/kg
ND
336
01/19/21 15:57
Benzoic Acid
ug/kg
ND
1680
01/19/21 15:57
Benzyl alcohol
ug/kg
ND
671
01/19/21 15:57
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
METHOD BLANK: 3132413
Matrix:
Solid
Associated Lab Samples: 92516966001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
bis(2-Chloroethoxy)methane
ug/kg
ND
336
01/19/21 15:57
bis(2-Chloroethyl) ether
ug/kg
ND
336
01/19/21 15:57
bis(2-Ethylhexyl)phthalate
ug/kg
ND
336
01/19/21 15:57
Butylbenzylphthalate
ug/kg
ND
336
01/19/21 15:57
Chrysene
ug/kg
ND
336
01/19/21 15:57
Di-n-butylphthalate
ug/kg
ND
336
01/19/21 15:57
Di-n-octylphthalate
ug/kg
ND
336
01/19/21 15:57
Dibenz(a,h)anthracene
ug/kg
ND
336
01/19/21 15:57
Dibenzofuran
ug/kg
ND
336
01/19/21 15:57
Diethylphthalate
ug/kg
ND
336
01/19/21 15:57
Dimethylphthalate
ug/kg
ND
336
01/19/21 15:57
Fluoranthene
ug/kg
ND
336
01/19/21 15:57
Fluorene
ug/kg
ND
336
01/19/21 15:57
Hexachloro-1,3-butadiene
ug/kg
ND
336
01/19/21 15:57
Hexachlorobenzene
ug/kg
ND
336
01/19/21 15:57
Hexachlorocyclopentadiene
ug/kg
ND
336
01/19/21 15:57
Hexachloroethane
ug/kg
ND
336
01/19/21 15:57
Indeno(1,2,3-cd)pyrene
ug/kg
ND
336
01/19/21 15:57
Isophorone
ug/kg
ND
336
01/19/21 15:57
N-Nitroso-di-n-propylamine
ug/kg
ND
336
01/19/21 15:57
N-Nitrosodimethylamine
ug/kg
ND
336
01/19/21 15:57
N-Nitrosodiphenylamine
ug/kg
ND
336
01/19/21 15:57
Naphthalene
ug/kg
ND
336
01/19/21 15:57
Nitrobenzene
ug/kg
ND
336
01/19/21 15:57
Pentachlorophenol
ug/kg
ND
671
01/19/21 15:57
Phenanthrene
ug/kg
ND
336
01/19/21 15:57
Phenol
ug/kg
ND
336
01/19/21 15:57
Pyrene
ug/kg
ND
336
01/19/21 15:57
Pyridine
ug/kg
ND
336
01/19/21 15:57
2,4,6-Tribromophenol (S)
%
51
18-130
01/19/21 15:57
2-Fluorobiphenyl (S)
%
91
19-130
01/19/21 15:57
2-Fluorophenol (S)
%
44
18-130
01/19/21 15:57
Nitrobenzene-d5 (S)
%
91
21-130
01/19/21 15:57
Phenol-d6 (S)
%
45
18-130
01/19/21 15:57
Terphenyl-d14 (S)
%
135
15-130
01/19/21 15:57 S3
Qualifiers
LABORATORY CONTROL SAMPLE:
3132414
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1680
1500
89
47-130
1,2-Dichlorobenzene
ug/kg
1680
1430
85
49-130
1,3-Dichlorobenzene
ug/kg
1680
1370
82
48-130
1,4-Dichlorobenzene
ug/kg
1680
1430
85
49-130
1-Methylnaphthalene
ug/kg
1680
1440
86
54-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
LABORATORY CONTROL SAMPLE:
Parameter
3132414
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
ug/kg
1680
1400
83
38-130
2,4,5-Trichlorophenol
ug/kg
1680
1610
95
49-130
2,4,6-Trichlorophenol
ug/kg
1680
1550
92
50-130
2,4-Dichlorophenol
ug/kg
1680
1590
95
51-130
2,4-Dimethylphenol
ug/kg
1680
1610
96
53-130
2,4-Dinitrophenol
ug/kg
8420
7960
95
39-130
2,4-Dinitrotoluene
ug/kg
1680
1590
94
53-130
2,6-Dinitrotoluene
ug/kg
1680
1610
95
55-130
2-Chloronaphthalene
ug/kg
1680
1440
86
48-130
2-Chlorophenol
ug/kg
1680
1500
89
54-130
2-Methylnaphthalene
ug/kg
1680
1490
89
57-130
2-Methylphenol(o-Cresol)
ug/kg
1680
1480
88
50-130
2-Nitroaniline
ug/kg
3370
2720
81
49-130
2-Nitrophenol
ug/kg
1680
1530
91
50-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1680
1640
97
50-130
3,3'-Dichlorobenzidine
ug/kg
3370
2410
72
47-130
3-Nitroaniline
ug/kg
3370
2120
63
45-130IL
4,6-Dinitro-2-methyl phenol
ug/kg
3370
3280
97
50-142
4-Bromophenylphenyl ether
ug/kg
1680
1660
99
55-130
4-ChIoro-3-methyl phenol
ug/kg
3370
3330
99
52-130
4-Chloroaniline
ug/kg
3370
2410
72
49-130
4-Chlorophenylphenyl ether
ug/kg
1680
1600
95
53-130
4-Nitroaniline
ug/kg
3370
2580
77
51-130
4-Nitrophenol
ug/kg
8420
8020
95
40-130
Acenaphthene
ug/kg
1680
1420
84
56-130
Acenaphthylene
ug/kg
1680
1430
85
58-130
Aniline
ug/kg
1680
1190
71
44-130
Anthracene
ug/kg
1680
1330
79
60-130
Benzo(a)anthracene
ug/kg
1680
1540
92
59-130
Benzo(a)pyrene
ug/kg
1680
1560
93
57-130
Benzo(b)fluoranthene
ug/kg
1680
1620
96
54-130
Benzo(g,h,i)perylene
ug/kg
1680
1560
92
59-130
Benzo(k)fluoranthene
ug/kg
1680
1590
95
54-130
Benzoic Acid
ug/kg
8420
6130
73
19-130
Benzyl alcohol
ug/kg
3370
3060
91
50-130
bis(2-Chloroethoxy)methane
ug/kg
1680
1450
86
55-130
bis(2-Chloroethyl) ether
ug/kg
1680
1500
89
53-130
bis(2-Ethylhexyl)phthalate
ug/kg
1680
1850
110
58-130
Butylbenzylphthalate
ug/kg
1680
1950
116
46-138
Chrysene
ug/kg
1680
1500
89
57-130
Di-n-butylphthalate
ug/kg
1680
1600
95
57-130
Di-n-octylphthalate
ug/kg
1680
1670
99
57-130
Dibenz(a,h)anthracene
ug/kg
1680
1510
90
60-130
Dibenzofuran
ug/kg
1680
1490
89
54-130
Diethylphthalate
ug/kg
1680
1590
94
55-130
Dimethylphthalate
ug/kg
1680
1570
93
57-130
Fluoranthene
ug/kg
1680
1430
85
57-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
LABORATORY CONTROL SAMPLE:
Parameter
3132414
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Fluorene
ug/kg
1680
1520
90
56-130
Hexachloro-1,3-butadiene
ug/kg
1680
1600
95
41-130
Hexachlorobenzene
ug/kg
1680
1630
97
53-130
Hexachlorocyclopentadiene
ug/kg
1680
1340
80
23-130
Hexachloroethane
ug/kg
1680
1430
85
48-130
Indeno(1,2,3-cd)pyrene
ug/kg
1680
1570
93
61-130
Isophorone
ug/kg
1680
1530
91
49-130
N-Nitroso-di-n-propylamine
ug/kg
1680
1600
95
52-130
N-Nitrosodimethylamine
ug/kg
1680
1400
83
45-130
N-Nitrosodiphenylamine
ug/kg
1680
1530
91
56-130
Naphthalene
ug/kg
1680
1390
82
56-130
Nitrobenzene
ug/kg
1680
1460
87
50-130
Pentachlorophenol
ug/kg
3370
3400
101
33-130
Phenanthrene
ug/kg
1680
1480
88
60-130
Phenol
ug/kg
1680
1580
94
54-130
Pyrene
ug/kg
1680
1830
109
61-130
Pyridine
ug/kg
1680
943
56
35-130
2,4,6-Tribromophenol (S)
%
56
18-130
2-Fluorobiphenyl (S)
%
95
19-130
2-Fluorophenol (S)
%
48
18-130
Nitrobenzene-d5(S)
%
96
21-130
Phenol-d6 (S)
%
49
18-130
Terphenyl-d14(S)
%
138
15-130 SO
MATRIX SPIKE SAMPLE:
Parameter
3132415
Units
92516907001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
2190
1920
87
22-130
1,2-Dichlorobenzene
ug/kg
ND
2190
1850
84
23-130
1,3-Dichlorobenzene
ug/kg
ND
2190
1780
81
26-130
1,4-Dichlorobenzene
ug/kg
ND
2190
1830
83
27-130
1-Methylnaphthalene
ug/kg
ND
2190
1840
84
30-130
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
2190
1820
83
30-130
2,4,5-Trichlorophenol
ug/kg
ND
2190
2060
94
26-130
2,4,6-Trichlorophenol
ug/kg
ND
2190
2030
92
23-130
2,4-Dichlorophenol
ug/kg
ND
2190
2060
94
29-130
2,4-Dimethylphenol
ug/kg
ND
2190
2120
97
13-130
2,4-Dinitrophenol
ug/kg
ND
11000
4290
39
10-131
2,4-Dinitrotoluene
ug/kg
ND
2190
1990
90
28-130
2,6-Dinitrotoluene
ug/kg
ND
2190
2030
92
36-130
2-Chloronaphthalene
ug/kg
ND
2190
1840
84
27-130
2-Chlorophenol
ug/kg
ND
2190
1970
90
29-130
2-Methylnaphthalene
ug/kg
ND
2190
1910
87
29-130
2-Methylphenol(o-Cresol)
ug/kg
ND
2190
1910
87
20-130
2-Nitroaniline
ug/kg
ND
4400
3580
81
29-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
MATRIX SPIKE SAMPLE:
3132415
92516907001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Nitrophenol
ug/kg
ND
2190
2000
91
26-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
2190
2110
96
10-176
3,3'-Dichlorobenzidine
ug/kg
ND
4400
3660
83
15-130
3-Nitroaniline
ug/kg
ND
4400
3040
69
28-130IL
4,6-Dinitro-2-methyl phenol
ug/kg
ND
4400
3870
88
15-132
4-Bromophenylphenyl ether
ug/kg
ND
2190
2080
94
35-130
4-Chloro-3-methylphenol
ug/kg
ND
4400
4250
97
30-130
4-Chloroaniline
ug/kg
ND
4400
3350
76
28-130
4-Chlorophenylphenyl ether
ug/kg
ND
2190
2010
92
32-130
4-Nitroaniline
ug/kg
ND
4400
3340
76
30-130
4-Nitrophenol
ug/kg
ND
11000
10000
91
17-130
Acenaphthene
ug/kg
ND
2190
1790
81
29-130
Acenaphthylene
ug/kg
ND
2190
1800
82
31-130
Aniline
ug/kg
ND
2190
1590
72
10-130
Anthracene
ug/kg
ND
2190
1700
77
33-130
Benzo(a)anthracene
ug/kg
ND
2190
1950
89
32-130
Benzo(a)pyrene
ug/kg
ND
2190
1960
89
32-130
Benzo(b)fluoranthene
ug/kg
ND
2190
2000
91
33-130
Benzo(g,h,i)perylene
ug/kg
ND
2190
2050
93
28-130
Benzo(k)fluoranthene
ug/kg
ND
2190
1980
90
31-130
Benzoic Acid
ug/kg
ND
11000
11001
10
10-130
Benzyl alcohol
ug/kg
ND
4400
3960
90
31-130
bis(2-Chloroethoxy)methane
ug/kg
ND
2190
1870
85
30-130
bis(2-Chloroethyl) ether
ug/kg
ND
2190
1930
88
68-130
bis(2-Ethylhexyl)phthalate
ug/kg
ND
2190
2430
110
40-130
Butylbenzylphthalate
ug/kg
ND
2190
2560
116
40-130
Chrysene
ug/kg
ND
2190
1870
85
30-130
Di-n-butylphthalate
ug/kg
ND
2190
2040
93
41-130
Di-n-octylphthalate
ug/kg
ND
2190
2160
98
42-130
Dibenz(a,h)anthracene
ug/kg
ND
2190
2010
92
27-130
Dibenzofuran
ug/kg
ND
2190
1870
85
32-130
Diethylphthalate
ug/kg
ND
2190
1980
90
40-130
Dimethylphthalate
ug/kg
ND
2190
1960
89
37-130
Fluoranthene
ug/kg
ND
2190
1720
78
26-130
Fluorene
ug/kg
ND
2190
1880
86
31-130
Hexachloro-1,3-butadiene
ug/kg
ND
2190
2130
97
20-130
Hexachlorobenzene
ug/kg
ND
2190
2080
95
29-130
Hexachlorocyclopentadiene
ug/kg
ND
2190
1580
72
10-130
Hexachloroethane
ug/kg
ND
2190
1880
85
21-130
Indeno(1,2,3-cd)pyrene
ug/kg
ND
2190
2060
94
28-130
Isophorone
ug/kg
ND
2190
1940
88
32-130
N-Nitroso-di-n-propylamine
ug/kg
ND
2190
2060
94
31-130
N-Nitrosodimethylamine
ug/kg
ND
2190
1720
78
20-130
N-Nitrosodiphenylamine
ug/kg
ND
2190
1960
89
32-130
Naphthalene
ug/kg
ND
2190
1830
83
30-130
Nitrobenzene
ug/kg
ND
2190
1910
87
25-130
Pentachlorophenol
ug/kg
ND
4400
4300
98
10-130
Results presented on this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
MATRIX SPIKE SAMPLE:
Parameter
3132415
Units
92516907001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Phenanthrene
ug/kg
ND
2190
1860
84
34-130
Phenol
ug/kg
ND
2190
2070
94
14-130
Pyrene
ug/kg
ND
2190
2380
108
31-130
Pyridine
ug/kg
ND
2190
1420
65
10-130
2,4,6-Tribromophenol (S)
%
52
18-130
2-Fluorobiphenyl (S)
%
69
19-130
2-Fluorophenol(S)
%
44
18-130
Nitrobenzene-d5 (S)
%
87
21-130
Phenol-d6 (S)
%
46
18-130
Terphenyl-d14 (S)
%
105
15-130
SAMPLE DUPLICATE: 3132416
Parameter
Units
92516907002
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
1-Methylnaphthalene
ug/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
2,4,5-Trichlorophenol
ug/kg
ND
ND
2,4,6-Trichlorophenol
ug/kg
ND
ND
2,4-Dichlorophenol
ug/kg
ND
ND
2,4-Dimethylphenol
ug/kg
ND
ND
2,4-Dinitrophenol
ug/kg
ND
ND
2,4-Dinitrotoluene
ug/kg
ND
ND
2,6-Dinitrotoluene
ug/kg
ND
ND
2-Chloronaphthalene
ug/kg
ND
ND
2-Chlorophenol
ug/kg
ND
ND
2-Methylnaphthalene
ug/kg
ND
ND
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
2-Nitroaniline
ug/kg
ND
ND
2-Nitrophenol
ug/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
3,3'-Dichlorobenzidine
ug/kg
ND
ND
3-Nitroaniline
ug/kg
ND
ND
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
4-Bromophenylphenyl ether
ug/kg
ND
ND
4-ChIoro-3-methyl phenol
ug/kg
ND
ND
4-Chloroaniline
ug/kg
ND
ND
4-Chlorophenylphenyl ether
ug/kg
ND
ND
4-Nitroaniline
ug/kg
ND
ND
4-Nitrophenol
ug/kg
ND
ND
Acenaphthene
ug/kg
ND
ND
Acenaphthylene
ug/kg
ND
ND
RPD Qualifiers
IL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
SAMPLE DUPLICATE: 3132416
Parameter
Units
92516907002
Result
Dup
Result
Aniline
ug/kg
ND
ND
Anthracene
ug/kg
ND
ND
Benzo(a)anthracene
ug/kg
ND
ND
Benzo(a)pyrene
ug/kg
ND
ND
Benzo(b)fluoranthene
ug/kg
ND
ND
Benzo(g,h,i)perylene
ug/kg
ND
ND
Benzo(k)fluoranthene
ug/kg
ND
ND
Benzoic Acid
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
Butylbenzylphthalate
ug/kg
ND
ND
Chrysene
ug/kg
ND
ND
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Fluoranthene
ug/kg
ND
ND
Fluorene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
Isophorone
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenanthrene
ug/kg
ND
ND
Phenol
ug/kg
ND
ND
Pyrene
ug/kg
ND
ND
Pyridine
ug/kg
ND
ND
2,4,6-Tribromophenol (S)
%
38
45
2-Fluorobiphenyl (S)
%
60
73
2-Fluorophenol (S)
%
35
42
Nitrobenzene-d5 (S)
%
69
85
Phenol-d6 (S)
%
36
42
Terphenyl-d14 (S)
%
89
106
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
QC Batch: 593203 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92516966001
SAMPLE DUPLICATE: 3131019
92516631001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 39.9 38.8 3
SAMPLE DUPLICATE: 3131020
20187330002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 90.9 91.1 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92516966
QC Batch: 594656 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92516966001
SAMPLE DUPLICATE: 3137261
92516124001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.9 5.9 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 34

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: 21003
Pace Project No.: 92516966
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
SO Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /22/2021 02:46 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 21003
Pace Project No.: 92516966
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92516966001
W-1
EPA 3546
593623
EPA 8015C Modified
593716
92516966001
W-1
EPA 5030B
593673
EPA 8015C Modified
593718
92516966001
W-1
EPA 3010A
594222
EPA 6010D
594259
92516966001
W-1
EPA 7470A
594224
EPA 7470A
594353
92516966001
W-1
EPA 3546
593630
EPA 8270E
593754
92516966001
W-1
EPA 5035A/5030B
593665
EPA 8260D
593679
92516966001
W-1
SW-846
593203
92516966001
W-1
EPA 9045D
594656
Date: 01/22/2021 02:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 34

Sample Condition Upon Recelpt(SCUR) Page 1 of 2
ri aeeArlalytical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas Quality office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvillet':� Raleigh❑ Mechanlcsville❑ Atlanta[] Kernersville❑
Samplec Client Name: Project #: WO# : 92516966
Courier: ❑Fed Ex ` ❑UPS ❑U5P5 Clienk II III III II I III II ���
❑ Commercial []pace ❑other: 9251B965
Custody Seal Present? ❑Yes &o Seals Intact? ❑Yes &No T
Date/Initials Person Examining Contents: L. iS JA K\�
Packing Material: ❑Bubble Wrap l5i'ubble Bags ❑None [)q� Other -�•�,� Biological Tissue fr4xen?
Thermometer: ���(� []Yes[]NoRN/A
j�1R Gun ID: 92TO64 Type of Ice. )9 et ❑Blue ❑None
-7 Correction Factor:
Cooler Temp: I Add/Subtract (*Q -0.1
Cooler Temp Corrected (°C):
USDA Regulated Soil (❑ N/A, water sample)
Old samples on Hate in a quarantine tone within the United States: CA, NY, or SC (check maps)?
F— Yes ,Tate
o
Temp should be above freezing to 6°C
❑5amplesout of temp criteria. Samples on ice, coaling process
hashegun
Did samples originate from a foreign source (in4ernationally,
inrindi- w—ii and Pu &rt n;,m) F-ly—
Comments/Dlscrepancy,
Chairi of Custody Present?
es
[]NO
❑N/A
1.
Samples Arrived within Hold Time?
es
[]No
❑NIA
2.
Short Hold Time Analysis (c72 hr.)?
❑Yes
WNo
❑N/A
3,
Rush Turn Around Time Requested?
Dyes
No
❑N/A
R.
Sufficient Volume?
ICYes
[—]No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
Yes
❑Nn
❑No
❑N/A
❑N/A
6.
Containers Intact?
fixes
(--]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[-]Yes
❑Na
/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Yes
J
❑No
❑N/A
9,
Headspace in VOA Vials (>5-6mm)?
Yes
❑Na
N/A
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
❑yes
❑Yes
❑No
❑No
N/A
'N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date:
Fiefd Data Required? ❑Yes ❑No
Page 32 of 34

UR
2of2
aceAnalytrcal
e Condition Upon Recei
Document No.:
F-CAR-CS-033-Rev.o7
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
EMceptlons: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Issuing Authority:
O# 92 �ality OJV%
e—]
�# Project � 169�s —,
PM: 8V
CLIENT: 82~Li Due Date: 01/22/21
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pH Adjustment Log for Preserved Samples
sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot it
Note: Whenever there ;s a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 33 of 34

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Page 34 of 34

Appendix C

QED
J6RO2-
Client: LIGHTHOUSE TECHNICAL
Samples taken
Monday, January 11, 2021
RED LAB
Address: PO BOX 1379
Samples extracted
Monday, January 11, 2021
HUNTERSVILLE, NC
Samples analysed
Tuesday, January 12, 2021
Contact: STEVE LUCAS
Operator
MAX MOYER
Project: 21003
Matrix Sample ID Dilution gTEX
used
GRO DRO TPH Total
Aromatics
16 EPA BSP % Ratios
PAHs
HC Fingerprint Match
CB-C9
CS-C70 C10-C36 C6-C36 C10-C36
C6:10 C�:C
C18+
Soil
S-1 26.0 <0.6
127.5 157.8 285.3 14.7
0.3 0.005
91.3 7.2
1.5
Waste Oil 79.9%,(FCM)
Soil
S-2 25.0 <0.6
<0.6 1.5 1.5 0.7
0.026 <0.008
0 88.4
11.6
Deg.Fuel72.8%,(FCM)
Soil
S-3 22.0 <0.5
<0.5 0.22 0.22 0.05
0.002 <0.007
0 100
0
Residual HC
Soil
S-4 25.0 <0.6
<0.6 0.25 0.25 0.23
0.024 <0.002
0 72.6
27.4
Residual HC
Soil
S-5 21.0 <0.5
<0.5 0.8 0.8 0.4
0.018 <0.002
0 92.5
7.5
V.Deg.Diesel 90.8%,(FCM)
al Calib hQC check
OK
11111pWiffnal FCM QC Check
OK 96.8%
Concentration values m mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification.
Abbreviations:- FCM = Results calculated using Fundamental Calibration Mode
: °/ = confidence of hydrocarbon identification: (PFM) = Poor Fingerprint Match: (T) = Turbid : (P) = Particulate detected
B = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result: (BO) = Background Organics detected:
(OCR) = Outside cal range : (M) = Modifed Result.
% Ratios estimated aromatic carbon number proportions: HC = Hydrocarbon : PHC = Petroleum HC: FP = Fingerprint only. Data generated by HC-1 Analyser

QED Hydrocarbon Fingerprints
Project: 21003 Tuesday, January 12, 2021
S-1: Waste Oil 79.9%,(FCM)
QED
19461
S-3: Residual HC
QC©
700
S-S : V.Deg.Diesel 90.8%,(FCM)
QC©
700

UICIIL
TM
) 3 D 7 0 Dil
� B
RAPID ENVIRONMENTAL DIAGNOSTICS
CHAIN OF CUSTODY AND ANALYTICAL REQUEST FORM
nw'. ' I
5598 Marvin K Moss Lane
MARBIONC Bldg, Suite 2003
Wilmington, NC 28409
Address:
N/ �I' 1/' `�` /
14iwt;,, u�.�1 4 /�
Contact:
`LL%J-�C G� L+G)
Project Ref.:
IPIA�&
Each UVF sample will 6e analyzed for
total BTEX, GRO, DRO, TPH, PAH total
rEITEXandardGC
Analysaromaes cs and
Analyses are for BTEX and Chlorinated
Solvents: VC, 1,1 OCE, 1,2 cis DCE, 1,2
trans DCE, TCE, and PCE. Specify target
analytes In the space provided below.
Small:
Phone#:
cy43-ii 743q
Collected by:
Sd * ' la
Sample Collection
TAT Requested
Analysis Type
initials
Sample ID
Total Wt.
Tare Wt.
Sample Wt.
Date/Time
24 Hour
48 Hour
UVF
GC
I / o
So.g
�to.6
10.2
1204
_
SSZ. 9
41.0
1 1 .9
r� Y
S-
5(•S
.I
lo.y
COMMENTS/REQUESTS:
TARGET GC/UVF ANALYTES:
ellnqulshed by
Accepted by
Date/Time
RED Lab US ONLY
S
Ref. No
/�1
�� MM �6ds
�,
Relinquished by
Accepted by
Date/Time

QED
-Age-c2z,
Client: LIGHTHOUSE TECHNICAL
Samples taken
Tuesday, January 12, 2021
Address: PO BOX 1379
REDLAB
©
samples extracted
Tuesday, January 12, 2021
HUNTERSVILLE, NC
P /.ND INVIRDNNlM�IL D,ADNOITCt
Samples analysed
Thursday, January 14, 2021
Contact: STEVE LUCAS
Operator
MAX MOYER
Project: 21003
Matrix Sample ID
Dilution BTEX
GRO
DR TPH Total
Aromatics
16 EPA
PAHs
Bap % Ratios
7Matchused
c6-c9
Crr-C70C10-036C6-C36
C10-c36
C6:10 C18C
C16+Soil
S-6
20.0 <0.5
<0.5
1 1 0.4
0.026
0.001
0 89.9
10.1
Deg Fuel 7
Soil
--
S-7
22.0 <0.5
<0.5
65.3 65.3 26.6
_1.6
0.033
0 82.1
17.9
Deg.Light Fuel 93.1%,(FCM)
Soil
S-8
29.0 <0.7
<0.7
2.3 2.3 1.4
0.07
<0.003
0 96.8
3.2
Deg.Light Fuel 81.8%,(FCM)
Soil
S-9
26.0 <0.6
<0.6
0.8 0.8 0.25
0.011
<0.008
0 67.8
32.2
V.Deg.LightFuel 41.8%,(FCM)
Soil
S-10
21.0 <0.5
<0.5
1.8 1.8 0.9
0.04
0.001
0189.9.
10.1
V.Deg.PHC 57.3%,(FCM)
Soil
S-11
19.0 <0A
<0.4
1 1 0.4
0.022
0.001
0 86.3
13.7
V.Deg.Light Fuel 66%,(FCM)
Soil
S-12
22.0 <0.5
4.7
7.1 11.8 3.3
0.15
0.004
62.7 30
7.3
V.Deg.PHC 87.7%,(FCM)
Soil
S-13
24.0 <0.6
<_0.6
<0.24 0.05 0.05
0.003
<0.007
0 56.5
43.5
Residual HC
Soil
S-14
22.0 <0.5
<0.5
0.3 0.3 0.18
0.007
<0.001
0 74
26
V.Deg.PHC 45.9%,(FCM)
Soil
S-15
19.0 <0A
<0.4
0.8 0.8 0.06
0.004
<0.0
0 96.5
3.5
Deg Fuel 27.1%,(FCM)
ial Calibrator QC check
OK
CM QC Check
OK 96.0%
Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification.
Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode:
% = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : M = Turbid : (P) = Particulate detected
B = Blank Drift : (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result
: (BO) = Background Organics detected
: (OCR) = Outside cal range : (M) = Modifed
Result.
% Ratios estimated aromatic carbon number proportions:
HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser

Project: 21003
QED Hydrocarbon Fingerprints
Thursday, January 14, 2021
S-9 : V.Deg.Light Fuel 41.8%,(FCM)
S-11: V.Oeg.LightFuel 6696,(FCM) enrMni
S-13 : Residual HC

Client Name:
15�7 v x ■M
t
✓. y::x rw�� #
,. s
F'"""-'
ENVIRONMENTAL DIAGNOSTICS
CHAIN OF CUSTODY AND ANALYTICAL REQUEST FORM
RED Lab, LLC
5598 Marvin K Moss Lane
g, Suite 2003
MARBIONC Bldg,
Wilmington, NC28409
Address:
q 7 1
I
l �Yi-n �. �� �,/c
Contact:
L,•x vc-4
Project Ref.:
Each UVF sample will be analyzed for
total BTEX, GRO, DRO, TPH, PAH total
aromaRAPID rEITEXand C GC
Analyses cs and
Analyses are for BTEX and Chlorinated
Solvents: VC, 1,1 DCE, 1,2 cis DCE, 1,2
trans DCE, TCE, and PCE. Specify target
analytes in the space provided below.
Email:
Phone#:
7cy-Y3.7-ii'3`i
Collected by:
5'40� L
Sample Collection
TAT Requested
Analysis Type
Initials
Sample ID
Total Wt.
Tare Wt.
Sample Wt.
Date/Time
24 Hour
48 Hour
UVF
GC
x
S-
5SP%
S"Ll
yr.-L
jZ.p
133
S S
SO•�/
•3
s5
—�3
51.
41.E
Ip •t
ao
-to
5
i
k.
qI-s
t3.5
;v
s ;
3.�
1.2
61•®
ss
t.-;3
`51.ro
1.®
It.v
Ku
s -;c
S3.2
Li1•Z
11•0
ys5�
"/5
S�•S
I.
1'4.LI
COMMENTS/REQUESTS:
TARGET GC/UVF ANALYTES:
Relinquished y
Accepted by
Date/Time
RED Lab}!SE ONLY
Ref. No
v
a�
3a KM 1 I 11I
Relinquished by
Accepted by
Date/Time

QED
o os
Client: LIGHTHOUSE TECHNICAL
Samples taken Wednesday, January 13, 2021
®
RE ®L'^B
Address: PO BOX 1379
Samples extracted Wednesday, January 13, 2021
w.o,00 a...... A o 0 0 ,
HUNTERSVILLE NC
Samples analysed Thursday, January 14, 2021
Contact: STEVE LUCAS
Operator MAX MOYER
Project: 21003
T03308
Matrix
Sample ID
Dilution
BTEX
GRO
DRO
TPH
Total
16 EPA
gaP
% Ratios
HC Fingerprint Match
used
Aromatics
PAHs
C5:10
C18C
C18+
c6-C9
C5-C10
C10-C35
C6-C35
C10-C35
Soil
S-16 25.0 <0.6
<0.6 0.3 0.3 0.3 0.015 <0.002
0 93.3 6.7
Residual PHC
Initial Calibrator QC check
OK Final FCM QC Check OK 100.3%
Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification.
Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode
: % = confidence of hydrocarbon identification : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected
B = Blank Drift : (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result : (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modified Result.
% Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser

QED Hydrocarbon Fingerprints
Project: 21003
Thursday, January 14, 2021

Client Name:
I.-Qt. 'ra
90 O M
REDLAB
"
RAPID ENVIRONMENTAL DIAGNOSTICS
CHAIN OF CUSTODY AND ANALYTICAL REQUEST FORM
RED Lab, LLC
5598 Marvin K Moss Lane
MARBIONC Bldg, Suite 2003
Wilmington, NC 28409
Address:
n J, d ,,c 13?' j
0A ArC
Contact:
</'''u
Pro'ect Ref.:
'2a 0 (Q3 U,;3
Each UVF sample will be analyzed for
total BTEX, GRO, DRO, TPH, PAH total
aromaPhone#:
Analyses rBTEXandaChGC
Analyses are for BTEX and Chlorinated
Solvents: VC, 1,1 DCE, 1,2 cis DCE, 1,2
trans DCE, TCE, and PCE. Specify target
analytes In the space provided below.
Email:
� "Y 35 7Y3�
Collected by:
s i L�
l� ti
Sample Collection
TAT Requested
Analysis Type
Initials
Sample ID
Total Wt.
Tare Wt.
Sample Wt.
Date /Time
24 Hour
48 Hour
UVF
GC
- B-3L a�
S
So.g
40.3
l .S
COMMENTS/REQUESTS: 6v Asti G ' I
TARGET GC/UVF ANALYTES:
R FIlnquished by
Accepted by
Date/Time
RED Lab USE ONLY
Ref. No
NAM 1f t
Relinquished by
Accepted by
Date/Time

QEDo�
Client: LIGHTHOUSE TECHNICAL
Samples taken
Friday, January 15, 2021
Address: PO BOX 1379
©
RE�LAB
o AaDZ.�ao.NeN.A�-AQNOS.I«
Samples extracted
Friday, January 15, 2021
HUNTERSVILLE, NC
Samples analysed
Monday, January 18, 2021
Contact: STEVE LUCAS
Operator
MAX MOYER
Project: 21003
Matrix Sample ID
Dilution BTEX
GRO
DRO TPH Total
16 EPA
BaP % Ratios
HC Fingerprint Match
used
Aromatics
PAHs
C6-C9
c5-C10
C10-C35 C5-C35 CIO-C35
C6:10 C 8C
C16F
Soil
S-17
24.0 <0.6
10.1
26.3 36A 11.8
0.4
0.003
50.7 42.3
7
V.Deg.PHC 73.6%,(FCM)
Soil
S-18
1269.0 <31.7
<31.7
556 556 231.3
9.5
0.117
0 90.2
9.8
V.Deg.Diesel 88.7%,(FCM)
Soil
S-19
27.0 <0.6
<0.6
2.8 2.8 1.3
0.07
0.002
0 92.8
7.2
Phenolic Compound53.1%,(FCM)
Soil
S-20
23.0 <0.5
<0.5
57.1 57.1 27.3
1.1
0.009
0 89.5
10.5
V.Deg.LighlFuel 84.3%,(FCM)
Soil
S-21
29.0 <0.7
<0.7
1.4 1.4 0.7
0.026
<0.0
0 88.9
11.1
Deg.Fuel60.8%.(FCM)
Soil
S-22
35.0 <0.8
<0.8
3.8 3.8 0.8
0.04
<0.011
0 86.5
13.5
Degraded Oil 30.2%,(FCM)
Soil
S-23
28.0 <0.7
<0.7
0.18 0.18 0.17
0.021
0.006
0 69.5
30.5
Residual HC
Soil
S-24
27.0 <0.6
<0.6
1.2 1.2 0.7
0.031
<0.008
0 86
14
V.Deg.PHC47.1%,(FCM)
ibrator QC check
OK
C Check
OK 101.4%
Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification.
Abbreviations :- FCM = Results calculated using Fundamental Calibration Mode:
% = confidence of hydrocarbon Identification : (PFM) =
Poor Fingerprint Match : (r) = Turbid : (P) = Particulate detected
B = Blank Drift: (SBS)/(LBS) = Site Specific or Library Background Subtraction applied to result:
(BO) = Background Organics detected:
(OCR) = Outside cal range : (M) = Modifed
Result.
% Ratios estimated aromatic carbon number proportions
: HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser

QED Hydrocarbon Fingerprints
Project: 21003
Monday, January 18, 2021
S-18 : V. Deg. Diesel 88.7%, (FCM) I
I a -cc : uegraueu vu ay.c700%ra.wII I
5-24 : V.Deg.PHC 47.1%,(FCM) I
1084
n Jt

Client Name:
T Usf %9e lnni
•. - LAO'
RAPID ENVIRONMENTAL DIAGNOSTICS
CHAIN OF CUSTODY AND ANALYTICAL
REQUEST FORM
RED Lab, LLC
5598 Marvin K Moss Lane
MARBIONC Bldg, Suite 2003
Wilmington, NC28409
Address:
1�" I� 19 � /37 %
M &..Vv4 wl& NC �'D•i�R
Contact:
•s�•-P-�-2 G�ced
Project Ref.:
7 DU
Each sample will be analyzed for
BTEX, GRO, ORO, TPH, PAH total
aromatics and BaP
Email:
Phone9:
Collected by:
/��
Sample Collection
TAT Requested I
Matrix
ISM
Sample ID
UVF
GC BTEX
Tare Wt.
Sample Wt.
Date/nme
24 Hour
48 Hour
l e36
—d —
r
41.2.
%.4/Y
S^ ql
I.Z
•iP
y
— 1
(otal,gWt.
.O
/tt.2.
9.4
40
cl.5
Comments: W L. l•z- I •G
RED��1 labb/b USE ONLY
l�
Relin ulsh d by
Date/Time
Accepted by
Date/Time
-/4 Moo
MM t 115111
k'A
Relinquished by
Date/Time
Accepted by
Date/Time

QED AaR02-
Client: LIGHTHOUSE TECHNICAL Samples taken Tuesday, January 19, 2021
Address: PO BOX 1379 RE ® LAB Samples extracted Tuesday, January 19, 2021
g4q,C gNV,RONNENiw� O,wGN
HUNTERSVILLE, NC Samples analysed Wednesday, January 20, 2021
Contact: STEVE LUCAS Operator MAX MOYER
Project: 21003
7-SoiIS-25
Sample ID Dilution BTEX GRO DRO TPH Total 16 EPA Bap %Ratios HC Fingerprint Match
used Aromatics PAHs
C6-C9 Cs-C10 C10-C36 CS-C35 C10-C35 C6:10 C18C C18+
23.0 <0.5 <0.5 8.6 8.6 3.8 0.2 0.005 0 78.1 21.9 V.Deg.PHC 78.8%,(FCM)
!n,en
' Initial Calibrator OC check OK OK 98.7%
Ctration values in mg/kg for soil samples and mg/L for water samples. Soil values uncorrected for moisture or stone content. Fingerprints provide a tentative hydrocarbon identification.
Abbreviations:- FCM = Results calculated using Fundamental Calibration Mode: %= confidence of hydrocarbon identification: (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate detected
B = Blank Drift : (SBS)I(LBS) = Site Specific or Library Background Subtraction applied to result : (BO) = Background Organics detected : (OCR) = Outside cal range : (M) = Modifed Result.
°/ Ratios estimated aromatic carbon number proportions : HC = Hydrocarbon : PHC = Petroleum HC : FP = Fingerprint only. Data generated by HC-1 Analyser

QED Hydrocarbon Fingerprints
Project: 21003
Wednesday, January 20,2021

LAW
.end uY/li NC S$o'7�
bed
'A10 .3 RAPID ENVIRONMENTAL DIAGNOSTICS
CHAIN OF CUSTODY AND ANALYTICAL
REQUEST FORM
i K Moss Lane
Bldg, Suite 2003
Each sample will be analyzed for
BTEX, GRO, DRO, TPH, PAN total
aromatics and BaP
Sample Collection
TAT Requested
Matrix
(S/W)
Sample ID
UVF
GCBTEX
Total Wt.
Tare Wt.
Sample Wt.
Date/Time
24 Hour 1
48 Hour
Comments; / .
IV
RED Lab USE ONLY
'(
Re uished y
Date/Time
Accepted by
Date/Time
,,
Relinquished by
Date/Time
Accepted by
Date/Time

Appendix D

Soil Solutions of the Carolinas, LLC Manifest #
PO Box 681016, Charlotte NC 28216 Date:
980-298-6003
Environmental Consultant:
Contact:
Phone:
Load It:
Generator
Name:
Address:
City:
I State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. UST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certiflcate of Waste Constituents. I
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: volume:
Truck Driver Signature: Tag #: Date:
Facility
Destination: Soil Solutions of the Carolinas, LLC. 834 Padgett Rd. Shelby, NC 28150.
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

CERTC AR OTTE, NC 28216 FAX:: 7596,1173
TANDEMIMfl AX E / WAD IMAC
(CIR0.E ONE) A°% T I CONCRETE I OWf I M°1M3 I SAND I OTHER
EMAIL: ad.mgcert-um.caR
AMIM
AMI M I IRS
1
TICKET NUNIBER
5
B
19
2
°
10 =leer la
isn-Uut REALLED
3
11
6id
a
12
3

Soil Solutions of the Carolinas, LLC Manifest#
PO Box 681016, Charlotte NC 28216 Date:
980-298-6003
Environmental Consultant;
Contact:
Phone:
Load #:
Generator
Name:
Address:
City:
I State:
,-i
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. LIST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport In commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: Volume:
Truck Driver Signature: Tag #: Date:
Facility
Destination: Soil Solutions of the Carolinas, I.I.C. 834 Padgett Rd. Shelby, NC_28150.
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

CERT
P. 0. BOX 681016 OFFICE: 980-298
.
CHARLOTTE, NC 28218 FAX: [phone] EMAIL: adminCaPcerl-usa,oan
wTE Y
� �' TRUCXTYPE (CIRCLE ONE) nya.
TANDEM /TRI-AXLE/OUAD t TRACTORHOURLY TRUCT�+ CUATOMER NAME W
TIME U
STARTED TIMETOTAL
JOBI JOBNAME AM/PM O
TIME
Prt NAME STOppED AM/PM =
HRS. 4
0�IAADS TOTAL
AUTERWL$ HAULED YARDS =
(CIRCLE ON ASPHALT / Q
ONE) CONCRETE / DlFff / MLLINC / SANO / OTHER
TICKET NUMBER
a2a
t il
6
8 13IL
T
V_-
_
I
T
12 I
G W
�OSTOMlR'B egNATU1K ;�• 1: - _
- 3

Soil Solutions of the Carolinas, LLC Manifest It
PO Box 681016, Charlotte NC 28216 Date:
980-298-6003
Environmental Consultant:
Contact:
Phone:
Load #:
Generator
Name:
Address:
City:
State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. UST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: Volume:
Truck Driver Signature: Tag #: Date:
Facility
Destination: Soil Solutions of the Carolinas, LLC. 834 Padgett Rd. Shelby, NC 28150.
1 certify that the carrier has delivered the materials described above to this faclllty, and 1 hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

CERTP 0. BOX 681016 OFFICE: 980.298-6003
CHARLOTTE, NC 28216 FAX: [phone] EMAIL: [e-mail]
DATE: }
TRUCK NO. TRUCCTYPE (CIRCLEONE)IL
w�c TADM/TREACLE/QUAD/TRACTOR ILyCTOR
HOURLY TRUCK
THE STARTED TOTAL
U
JOB I AM /PM TALE O
JOB �M TIME I
PR NAME STOPPED AM/PM =
HRS. 6
/ OF LOADS TOTAL
MATERW.S HAVLED YARDS Z
(CIRCLE ONE( ASPHALT / CONCRETE / DIRT / Mn 1 wr /SAND /OTHER Q
}
TICKET NUMBER
Q
4Z
t v
5
9 13 C
0
2 5 10 it-'` 2
.. ;� toy"�—.: 1 _ .
I �
12 id.. _ Y1
%1.ISTOr61Y6aDT1ATURE _
- 3
-_-- -

Soil Solutions of the Carolinas, LLC
PO Box 681016, Charlotte NC 28216
980-298-6003
Environmental Consultant:
Contact:
Phone:
Date:
Load #:
Manifest #
Generator
Name:
Address:
City:
I State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. UST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck it: Volume:
Truck Driver Signature: Tag It: Date:
Facility
Destination: Soil Solutions of the Carolinas, LLC. 834 Padgett Rd. Shelby, NC 28150.
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

CERT CHARLOTTE,
BOX 68101 OFFICE: 980-298-6003
ARLOTTE, NO 28216 FAX: [phone] EMAIL: adminOcert-usa.com
TANDEM ITRLA% /WAD/TRACTOR
PR
(CWCLEONE) ASPHALT I CONCRETE I OW I MIL, I SAND I OTHER
a
11BTOMER9=Nx7m
•11• .11I1di.,
AM/PM
AMIPM
TOTAL
YARDS
10
lj
11
15
12
T6
1
W
F
2
�'

Soil Solutions of the Carolinas, LLC Manifest #
PO Box 681016, Charlotte NC 28216 Date:
980-298-6003
Load #:
Environmental Consultant:
Contact:
Phone:
Generator
Name:
Address:
Citv:l
State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. UST or other source)
Generators Certification of waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, 1 am submitting this Certificate of Waste Constituents. I
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are property classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: Volume:
Truck Driver Signature: Tag #: Date:
Facility
Destination: Soil Solutions of the Carolinas, LLC. 834 Padgett Rd. Shelby, NC 28150.
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

CERT
PR
P. O. BOX 681016 OFFICE: 980-298-60M
CHARLOTTE,NC28216 FAX: 70¢596-1173
TANDEM /TRI-AXIE/QUAD/TRACTOR
(COCLEONl ASPHALT 'CONCRETE / DIRT / M0.LwG / SAND / OTHER
12
ATOMMS SONATURE
EMAIL: admin@mn-usacom
RLY TRUCK TIr,7E
Am "M- Tue.. _ ..
LL
O
AMLP.M
i
HRS.
TOTAL
a
YARDS _
C
Z
Q
2
K
YJ
3
I5.3J p
U
16 S
w
i
FOF
15 yj
O
16
w
t
S
3

Soil Solutions of the Carolinas, LLC Manifest#
PO Box 681016, Charlotte NC 28216 Date:
980-298-6003
Environmental Consultant:
Contact:
Phone:
Load #:
Generator
Name:
Address:
City:
State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. LIST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue,) am submitting this Certificate of Waste Constituents. I
certify that 1 am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and 1 hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: Volume:
Truck Driver Signature: Tag #: Date:
Facility
Destination: Soil Solutions of the Carolinas, I.I.C. 834 Padgett Rd. Shelby, NC Z8150.
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

CERT
R O. BOX 681016 OFFICE: 980-298-6003
CHARLOTTE, NO 26216 FAX: [phone] EMAIL: admin@cert-usacom
TANDEM /TRPA%lE / DDAD / TMCTpR
AM/PM
AM/PM
YARDS
(CRUEONEI ASPHALT / CONCRETE / DIRT / MILLM / 8AND / OTHER
I
'LMTOMMS =N ATUIE
a
U

Soil Solutions of the Carolinas, LLC Manifest #
PO Box 681016, Charlotte NC 28216 Date:
980-298-6003
Environmental Consultant:
Contact:
Phone:
Load #:
Generator
Name:
Address:
City:
State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. UST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: Volume:
Truck Driver Signature: Tag #: Date:
Fadi ty
Destination: Soil Solutions of the Carolinas, LLC. 834 Padgett Rd. Shelby, NC 28150.
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

23643360
TICKET NUMBER
I► I®
A
CERTIFIED
AUTOMATED
TRUCK
SCALE
CAT SCALE COMPANY
PO. BOX 630
WALCOTT, IA52773
[phone]
www.catscale.com
THE CAT SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we back up our guarantee with cash.0
WEIGH WHAT WE SAY OR WE PAY® `
If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fine If our scale is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness If we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1-877-CATSCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee.com
for Instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
DATE: 1 —1 3— 21
11.26
20 s64259 SCALE: a05
LOCATION: p I l._UT 56
PURUC WEIGINASTEVS 1 85 E X I T 61?
CERTIRCATS (IF
WEIGHT&MEASURE KAh ^""'
INPRINT SEAL HERE
(IF APPLICABLE)
WEIGH NUMBER
4:259
STEER AXLE 1 7 9 6(-:) l b
DRIVEAXLE'1 b -� IlE•�3
TRAILERAXLE t`7 :1 b
5142C} 1 b
n�rlrtr� i I��, 2,5-- %/ 4­e) t J
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK PRODUCE,PROPERTY, COMMODITY, OR ARTICLE WEIGHED FRE.1GHi ALL kIINDS
CF'H2 D9 0
COMPANY i TRACTOR #, TRAILER # _
WEIGHMASTER OR "i=T.-� TICKET #OF
$L .UG
FEE WEIGHER SIGNATURES "' 1::: i. = a,- _ • x.,; FULL $ WEIGH —
HF ' i. l W Y H I' T (IF REWEIGH)
i-TOfAEI I COPY
0 CAT Stelae Rep 3074 8'20

CERTP O• BOX681016 OFFICE: 980-298-6003
CHARLOTTE, NC 28216 FAX: [phone] EMAIL: adminecart-usacom
DATE: TRUO(NO.
TRUCK TYPE (CIRCLE ONE)
CUSTOMER uAHE
TANDEM/ MAXLEJOUAD I TRACTOR HOURLY TRUCK Tiri
TIME
STARTED TOTAL
JOB/ AM/PM Ttw
JOB NAME
TIME
STOPPED AM/PM
PR NAME
A OF LOADS TOTAL
MATERML$ HAILED YARDS
(CDCLEONE( ASPHALT I CONCRETE I DIRT I MLLM I SAND I DTHER
S 8
13
2
8
/0 14
8 _
lz
:USTOLZW MMATDRE
Y
HRS _
a
CI
z
Q
S
z
t
3

Soil Solutions of the Carolinas, LLC
PO Box 681016, Charlotte NC 28216 Date:
980-298-6003
Load #:
Environmental Consultant:
Contact:
Phone:
Manifest #
Generator
Name:
Address:
City:
State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. UST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, 1 am submitting this Certificate of Waste Constituents. I
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature. Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classed, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: Volume:
Truck Driver Signature: Tag #: Date:
Facility
Destination: Soil Solutions of the Carolinas, LLC. 834 Padgett Rd. Shelby, NC 28150.
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

CERT
P. O. BOX 681016 OFFICE: 980F298-6003
CHARLOTTE, NO 28216 FAX: [phone]
TANDEM /TRLAXLE I WA, /TRAC
(CIRCLEONE) ASPHALT / OONCRErE / DIRT / MILLMO / BAND / OTHER
tt
S
12
USTOIEWSSIS UMM
STARTED
STOPPED
f OF LOAF
HAULED
EMAIL: edmin®cert-usacom
6
HOURLY TRUCK
O
Titir
Q
W
TOTAL
U
AM/PM
TIME
LL
O
AM/PM
1
Y
HRS. 3
TOTAL
IL
YARDS
=
z
m
a
z
a
U
13
V
>
Laic
p
U
_ . is-EEEE
Wis-;16
-----------------
S
--
3

Soil Solutions of the Carolinas, LLC
PO Box 681016, Charlotte NC 28216
980-298-6003
Environmental Consultant:
Contact:
Phone:
Date:
Load #:
Manifest #
Generator
Name:
Address:
City:
State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. UST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, 1 certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are In proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: Volume:
Truck Driver Signature: Tag #: Date:
Facility
Destination: Soil Solutions of the Carolinas, LLC. 834 Padgett Rd. Shelby, NC 28150.
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

CERT
R 0. BOX 681016 OFFICE: 980.298.6003
CHARLOTTE, NC 28216 FAX: [phone]
TANDEM/TRLAXLE IODAD ITRACTOR
(CIRCLE ONE( ASPHALT I OONCRETE I DIRT I MKIM / SAM I OTHER
u
YI
!USTOMEWSSGNATURE
12
HAULED
EMAIL: admin®Den-usa.Dom
AM / PM
AM/PM
TOTAL
YARDS
4
IL
■ U
U
LL
0
O
k=

Soil Solutions of the Carolinas, LLC
PO Box 681016, Charlotte NC 28216
980-298-6003
Environmental Consultant:
Contact:
Phone:
Date:
Load #:
Manifest #
Generator
Name:
Address:
City:
State:
County:
Contact:
Phone:
Waste Origination Point
Address:
Class & Type of Contaminate in soil: Petroleum
Source of contamination: (ex. UST or other source)
Generators Certification of Waste Constituents: In lieu of submitting analytical data (methods 8240 and 8270)
verifying that the waste in question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. 1
certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of
my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
Transporter
Company: Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Truck #: Volume:
Truck Driver Signature: Tag #: Date:
Facility
Destination: Soil Solutions of the Carolinas, LLC. 834 Padgett Rd. Shelby, NC 28150.
1 certify that the carrier has delivered the materials described above to this facility, and 1 hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature: Date:
Company Name: Title:

GERTP 0- BOX681016 OFFICE: 980.298.6003
CHARLOTTE, NO 28216 FAX: [phone] EMAIL: admin@cert-usacom
TANDEM /TRI-AXIS/QUAD/TRACTOR
PR
(CMCLEOIJE) ASPHALT / CONCRETE / DIRT / MILL
ING / &1NO / OTHER
M
2
I
8
MSTOMER's WONATIRIE
HAULED
AM/PM
AM / PM
a

NONaIAURDOUS
1. Serrano, ID Number
2. Page I of
3. Em Menoy P.eap rme Phom
A WeMe Tmaydng Number
WASTEMANIFEST
877-505-6799
5. Gmeratota Name am Meiling Odd
Gemralora See Address (N dfferent Van mdling a00{,rer�a/a11
--Td Tl�-,�,d� r
0
2d00 . GA,to Mu4.
GerlN oes Phone:
fJ
0. Tmmcporler i Company Name
V US. EPA ID Number
CERT
NCR 000155499
71Trarepm,2 Company Name
U.S. EPA ID NUlrher
A. Deei9at e, Facdi, Name and Site Adtlrees
U.S. EPA ID Nmber
Far s Now
9. Wade SNpong; Name and Dasalption
1g.CmMlm¢
ll.TM
12. Unit
Np
7 p,
Duamie
WWd.
1.
W
v
°W
W
2
3
1.
13. Spedal Hendfing lneWNme and Mchhonal lydormafion
1A OENEMTOWSKIFFEROS'S CERTIFICATION: I herabydeclara Ilatlha coolants oIM¢
conegnmend ere ft Jb and aauo&t, de onte l abc m by the prom Nipping mama, aM are dassrad, pedageq
marked and Iebele"laceaded, am are In aJ raepecta In pmpermm MW fabarapon=Ming
to apprwble immaworal aM national govemmental reguiakire
Gemrafte'"enre3 Pdrnadrtyped Name
Signature
ModA Day Year
15.Iotemetmnal SMpmada ❑ Im atf, US.
❑ Evw Iran U.S. Podoe m le r:
Tra der51 raWre M Mm :
Me knotoo U.S.:
¢
16. Tramoorler AcknarAedgment of Remlpt N Mamllala
Tramponer 1 PMkday* uame
Sgrou
Norm NY Year
8
tik�x1v
2
G
Trmsponer2 Phmed ypad Name
Sigrat
Day Year
17, D%orepency
17a. Decrepeney IMimtion Slam ❑ Wantily ❑ TYpa
❑ Reekue ❑ Pared Rejection
❑ FMI Food.
Menttmt Rekrenm Nurnmr.
1%. Alt enom Facility (or Geneator)
U.S. EPA ID Number
�3
17e.SignaWre of Alternate Facility(or Generator)
Mordb Day Year
2
2
N
O
10. Designated Fadkty Owner or Operator CerAfication of receipt of 6-ml...rad by
the manifest except es roan in l
Prinkd4yped Name
Signature
Day Yeer
e i
2d 1
169-BLC-05 11977 (RW.VM) v DESIGNATED FACILITY 1*O GENERATOR

Appendix E

WELL CONSTRUCTION RECORD (GW-1)
For Internal I Est: Only
1. Well Contractor Information:
Thomas J. Benthall, Jr.
Well Contractor Natnc
4508-B
NC Well Contractor Certification Number
Eastern Carolina Environmental Services, Inc.
Company Name
2. Well Construction Permit #: NA
Leal all upplicnble sn11 cYucsirucunu pc roars lt.e. 111r . 1'alarn:.1441/r.
3. Well Use (check well use):
OAgricultural
OGeothermal (Heating/Cooling Supply)
Olndustrial/Commercial
C
OAquirer Recharge
OAquifer Storage and Recovery
OAquifer Test
OExperimental Technology
OGeothermal (Closed Loop)
OGeothermal (Heating/Cooling
OMunicipal/Public
ORcsidential Water Supply (single)
OResidential Water Suppl% (shared)
❑Wells> I(H).(X)O GPD
OGroundwater Rcmedtatlon
OSalinity Barrier
OStormwater Drainage
OSubsidence Control
OTracer
OOther (explain under #21 Itentarks
4. Date Well(s) Completed: 3/10/2021 Well IN MIN-1
Sa. Well Location:
Uplands Co., Inc. - Hilbish Ford NA
Facility/OwnerrNam Facilih ID= (if applicahle1
2600 S. Cannon Blvd., Kannapolis, NC 28083
Physical Address. City, and Zip
Cabarrus 5612955398
County -- Parcel Identification No. (Ply t
Sb. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(ifweil field, one lat/Iong is sufficient)
35.45921 N-80.61095
6. Is(are) the well(s): ItPermanent or OTemporary
7. Is this a repair to an existing well: Ol'es or 15No
Jthis is a repair..(// urn kousi ri srell cvurstmeoiut at%r ratultun took/ eriduu, the uurr,re oI r)+,
n77asr uokler L 21 n-morb xmfitm esr tin the hack of thm. j,rtn.
8. For Geoprobe/DPT or Closed -Loop Geothermal Wells having dw same
construction. only 1 GW-I is needed. Indicate TOTAL NUMI1I:R of%%clls
drilled: wA
9. Total well depth below land surface: 7.50 (ft.)
Mir medliple wells 1vo all depths if rh/jerent (example- .i tar 21A)' mul 2011)(11
10. Static water level below top of casing: 6.00 (or 3.50' BGS) (ft.)
ljscater las-el is abuse cvrship. use -• "
11. Borehole diameter. 3.625 (in.)
I Well construction method: Hand Auger
(i.c auger. rotary. cable, direct push. etc.)
14. WATER ZONES
FRONT
I TO
DESCRIPTION
3.5 ft.
7.5 ft.
surficial aquifer
ft.
ft.
IS. Ot TER CASING for tnuld-cased wells OR LINER(if a le
FROM
I 1'O DIAMETER I
TIIICKKESS I MATERIAL
ft.
I rt. in.
16.1NNERCASING ORTUBING UtmotherusaIclosed-loo
FROM
TO
DIAMETER
TIIICILNE'SS
MATERIAL
0 rt.
2.5 It-
2 in-
0.154 In.
Seh 40 PVC
ft.
It.
in.
17. SCREEN
FROM
TO i
DIAMETER
SLOTS=
TIItCKNESS
MATERIAL
2.5 " 17*5
fL
2 in'
0.010 in.
0.154 in.
Sch 40 PVC
ft. I
rL
in.
IS. GROUT
FROM
I TO
MATERIAL
EMPLACEMEW METHOD & AMOUNT
0 ft'
1.5 fi-
bentonite
gravity flow, <5 lb
ft.
ft.
rL
rt.
19. SAND/GRAVEL
PACK(if a (cable
FROM
1'O
MATERIAL
EMPLACFAIENT METHOD
1.5 ft•
7.5 ft•
#2 washed filter sand
gravity flow
20. DRILLING
LOG fattach addldo:W sheets if necasit
FROM
110
DESCRIPTION color, hardnem rntllrack type, gW* ski etc.
0 ft•
2 5 rt.
Backfill (silly sand)
2.5 ft.
4.5 ft-
Slightly sandy Gay
4.5 ft'
7.5 IL
Micaceous silty fine sand
rt.
rt.
ft.
ft.
ft.
ft.
21. REMARKS
22. ('crtific '
3/11 /2021
7.59711me of tic ontmctor Date
/it .ot„r+n; tier lur,N. I herelor c erulr that 04 welloi) srur lu•eny evimirrictecl no ovetirchotim is -ills
I a. I x, !+' ++_t uluu.,r / d 17 '•I(' n2(' .1)21X) ll'ell t-o,taruc-trr„r Nruudurilk a trllhar a cr,�t-
„I dn% been prrowded r,r rise %vellaaner.
23. Nile diagram or additional well details:
You nm% use the hack of this page to provide additional well construction info
latltl :tics ()s•cl' in Rcmarks lime) You mad• also attach additional pages ifnecessary
24. Sl' B,�IIT'I'Al. INSTRUC" PIONS
Suhntii this G%%'-I within 30 days or well completion per the following:
24a. For All Wells: Original form to Division of Water Resources (DWR).
Inibrination Processing Unit. 1617 MSC. Raleigh. NC 27699-1617
241). For Iniection Yells: Copy to DWR. Underground Injection Control OUC)
Prourttn. 1636 MSC. Raleigh. NC 27699-1636
24c. For Water SuPPIv and Open -Loop Geothermal Return Wells: Copy to the
cutnth environmental healthdepartment of the county where insta
FOR WATER SVPPLV WELLS ONLY: 24d. For Water Wells producing over 100.000 GPD: Copy to DWR. CCPCUA
Permit Program. 1611 MSC. Raleigh. NC 27699-1 11
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
FormGW-1 North Carolina Ik.parsnectstofi•mtieitttxmalt uala.-Di%eston.rl'%%aterRI.-MM's Revised 6-6-20 19

WELL CONSTRUCTION RECORD (GW-1)
For Internal I lu Onl%:
1. Well Contractor Information:
Thomas J. Benthall, Jr.
Well Contractor Nance
4508-B
NC Well Contractor Certification Number
Eastern Carolina Environmental Services, Inc.
Company Name
2. Well Construction Permit M NA
I.As all upplicwhle nct•!l crrllslrrrruun lx•rmilc (i.r. I /l!', ( lenity. State. I irrirarce. wr.1
3. Well Use (check well use):
Water Supply Well:
OAgicultural OMunicipal/Ptthlic
OGeothermal (Heating/Cooling Supply) ORcsidential Water Suppl% (single)
Olndustrial/Commereial OResidential Water Supph (shared)
❑lrriaation OWells> 100.(K)(f 6111) --
Non-Water Supply Well:
OAquifer Recharge
OAquifer Storage and Recovery
OAquifer Test
OExperimenta) Technology
OGeothermal (Closed Loop)
OGeothermal (Heating Coolin
C
OGroundwater Rentediation
OSalinity Barrier
OStorm%%zter Drainage
OSubsidencc Control
O'1'racer
OOther (explain under 021 Remarks)
4. Date Well(s) Completed: 3/10/2021 Well ID# MW-2
52. Well Location:
Uplands Co., Inc. - Hilbish Ford
NA
Facility/Owner Name Facility Wit (ifappticable)
2600 S. Cannon Blvd., Kannapolis, NC 28083
Physical Address. City. and Zip
Cabarrus 5612955398
County
Parcel Ideniirtcamin Nu (PIN I
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(ifwell field. one Iai/long is sufficient)
35.45899 N-80.61074
6. Is(are) the well(s): OPermanent or OTemporary
7. Is this a repair to an existing well: Oyes or ONo
If thin is o repain ill our krunew tn•// evllrrlrlrevtuu mjlrnushtm and explarn the rrarern• W dw
repair under =21 rrmarkr ixtion ar on they hack r!f ihis• filrur.
8. For Geoprobe/DPT or Closed -Loop Geothermal Weils having the same
construction. only ( GW-1 is needed. Indicate TOTAL NUMBER of %%ells
drilled: wA
9. Total well depth below land surface: 4.00 (ft.)
Fur nad iple wells Awl all delwAtc 1 i4fferenl (t=cample- 3 1121M • and ?! l 11111' 1
10. Static water level below top of casing: 2.10 (or 1.02' BGS) (fit.)
1%xwJrr !err! is trho►t• cuxuru. nr. "
IL Borehole diameter. 3.625 (in.)
12. Well construction method: Hand Auger
(i.e. auger. rotary. cable. direct push. etc.)
14. WATER ZONES
FROM
1'O
DESCRIPTION
1.02 ft.
4.0 fr.
surficial aquifer
ft.
rt.
IS. OUTER CASING (for
multi -cased wells)OR
LINER f ap
plc
FROM
I TO
DIAMETER
THICKNESS
I MATERIAL
ft.
I rt.
in.
16. INNER
CASING OR TUBING t:othetnaal
closed -loop)
FROM
To
DIAMETER
THICKNESS
MATERIAL
0 ri.
1.0 ft.
2 In.
0.154 in.
Sch 40 PVC
ft.
ft.
In.
17. S('REFN
FROM
TO
DIAMETER
SLOTS17-F
THICKINESS
MATERIAL
1.0 fa'
4.0 fit. 2
in.
0.010 in.
0.154 in.
Sch 40 PVC
A.
rt.
in.
I& GROUT
FROM
TO
MATERIAL
ESIPLACEMIENTMETHOD & AMOUNT
0 fit•
0.75 ft-
bentonite
gravity flow, <5 lb
ft.
ft.
ft.
ft.
19. SAND/GRAVEL PACK
if applicable)
FROM
TO
MATERIAL
EMPLACEMENT METHOD
0.75 fit•
4.0 ft.
#2 washed fitter sand
gravity flow
ft.
fa
20. DRILLING LOG attach
additional sheets If rmeessa
FROM
I TO
DESCRIPTION (tabr. hardnem sotUroek inw. itrain strr. etc.
0 fit•
2.0 fL
Backfil (silty sand)
2.0 f'•
4.0 fit•
Slightly sandy clay
rt.
fit.
fit.
rt.
fr.
fir.
fir.
fr.
21. RESIARKS
22. Certification:
3/11 /2021
Stgnattttc acenif 't or Date
81 •r;nni, 11u. lure . I he bt 4rrill Ilan tlh' %rr/lh/ u'ai, (ire mi twit.wlrucled too in- onhuttv erah
VI it 1021 ' 01411) ur I .�I N II' 02(' .11200 Well l i,rrrlrtrc rn,ll tilaaclirnl. caul that a cop."
to/ Ihr% reo,nl lun been lrnol',41 c11u flee ere l/ atrne r.
23. Site diagram or additional well details:
You may use the back ol'this page to provide additional well construction info
(add Sec Civet' in Remarks }lox). You may also attach additional pages if necessary
24. St*B,%11'1-l'Al. INSTRUCTIONS
Submit this GW-I within 30 days of well completion per the following:
24a. Fur All %%'ells: Original limn to Division of Water Resources (DWR).
hofivination Processing Unit. 1617 MSC. Raleigh. NC 27699-1617
24h. For Iniection Wells: Copy to DWR. Underground Injection Control OUC)
Program. 16.16 MSC_ Raleigh. NC 27699-1636
lac. For Water Sunniv and Open -Loop Geothermal Return Wells: Copy to the
county environmental health department or the county where insta
FOR WATER StIPPLY WELLS ONLY: 24d. For Water Wells producing over 100.000 GPD: Copy to DWR. CCPCUA
Permit Program. 1611 MSC. Raleigh. 7699-1611
i3a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
Form GW-I North Carolina Depanntcnn ofFmi"inow,14d QuAtn - I lt%tstun r,l'!Pater Rc.uurces Revised 6.6-2018

Appendix F

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 01, 2021
Steven Lucas
Lighthouse Technical
PO Box 1379
Huntersville, NC 28078
RE: Project: 21003
Pace Project No.: 92527373
Dear Steven Lucas:
Enclosed are the analytical results for sample(s) received by the laboratory on March 12, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
1(704)875-9092
HORIZON Database Administrator
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92527373
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 21003
Pace Project No.: 92527373
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92527373001 MW-1
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 6010D
SH1
2
PASI-A
EPA 625.1
PKS
58
PASI-C
SM 6200B
SAS
63
PASI-C
92527373002 MW-2
MADEP EPH
BAJ
5
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 6010D
SH1
2
PASI-A
EPA 625.1
PKS
58
PASI-C
SM 6200B
SAS
63
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
21003
92527373
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92527373001
MW-1
EPA 601 OD
Chromium
19.1
ug/L
5.0
03/18/21 20:59
EPA 601 OD
Lead
5.2
ug/L
5.0
03/18/21 20:59
92527373002
MW-2
MADEP EPH
Aliphatic (C09-C18)
134
ug/L
100
03/24/21 10:21
N2
MADEP VPH
Aliphatic (C05-008)
56.3
ug/L
50.0
03/31/21 17:51
H1,N2
MADEP VPH
Aliphatic (C09-C12)
64.7
ug/L
50.0
03/31/21 17:51
H1,N2
MADEPVPH
Aliphatic(C09-C12)Adjusted
54.4
ug/L
50.0
03/31/21 17:51
N2
EPA 601 OD
Chromium
28.1
ug/L
5.0
03/18/21 21:15
EPA 601 OD
Lead
33.0
ug/L
5.0
03/18/21 21:15
SM 6200B
Benzene
2.4
ug/L
0.50
03/19/21 01:08
SM 6200B
Ethylbenzene
2.6
ug/L
0.50
03/19/21 01:08
SM 6200B
Toluene
1.9
ug/L
0.50
03/19/21 01:08
SM 6200B
1,2,4-Trimethylbenzene
4.9
ug/L
0.50
03/19/21 01:08
SM 6200B
m&p-Xylene
9.2
ug/L
1.0
03/19/21 01:08
SM 6200B
o-Xylene
4.4
ug/L
0.50
03/19/21 01:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92527373
Method: MADEP EPH
Description: MADEP EPH NC Water
Client: Lighthouse Technical
Date: April 01, 2021
General Information:
2 samples were analyzed for MADEP EPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92527373
Method: MADEP VPH
Description: VPH NC Water
Client: Lighthouse Technical
Date: April 01, 2021
General Information:
2 samples were analyzed for MADEP VPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H1: Analysis conducted outside the EPA method holding time.
• MW-1 (Lab ID: 92527373001)
• MW-2 (Lab ID: 92527373002)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92527373
Method: EPA 6010D
Description: 6010 MET ICP
Client: Lighthouse Technical
Date: April 01, 2021
General Information:
2 samples were analyzed for EPA 6010D by Pace Analytical Services Asheville. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3010A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92527373
Method: EPA 625.1
Description: 625 RVE
Client: Lighthouse Technical
Date: April 01, 2021
General Information:
2 samples were analyzed for EPA 625.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 625.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 606500
SO: Surrogate recovery outside laboratory control limits.
• MW-1 (Lab ID: 92527373001)
• 2-Fluorophenol (S)
• MW-2 (Lab ID: 92527373002)
• 2-Fluorophenol (S)
S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
• BLANK (Lab ID: 3195339)
• 2,4,6-Tribromophenol (S)
• Nitrobenzene-d5 (S)
• Terphenyl-d14 (S)
• MW-1 (Lab ID: 92527373001)
• Terphenyl-d14 (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92527373
Method: EPA 625.1
Description: 625 RVE
Client: Lighthouse Technical
Date: April 01, 2021
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92527373
Method: SM 6200B
Description: 6200B MSV
Client: Lighthouse Technical
Date: April 01, 2021
General Information:
2 samples were analyzed for SM 6200B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: 607642
E: Analyte concentration exceeded the calibration range. The reported result is estimated.
• MS (Lab ID: 3201005)
• Toluene
• MSD (Lab ID: 3201006)
• Toluene
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92527373
Sample: MWA Lab ID: 92527373001 Collected: 03/11/21 09:15 Received: 03/12/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
ND
ug/L
100
1
03/16/21 14:56
03/18/21 16:27
N2
Aliphatic (C19-C36)
ND
ug/L
100
1
03/16/21 14:56
03/18/21 16:27
N2
Aromatic (C11-C22)
ND
ug/L
100
1
03/16/21 14:56
03/18/21 16:27
N2
Surrogates
1-Chlorooctadecane (S)
48
%
40-140
1
03/16/21 14:56
03/18/21 16:27
3386-33-2
o-Terphenyl (S)
80
%
40-140
1
03/16/21 14:56
03/18/21 16:27
84-15-1
2-Fluorobiphenyl (S)
76
%
40-140
1
03/16/21 14:56
03/18/21 16:27
321-60-8
2-Bromonaphthalene (S)
76
%
40-140
1
03/16/21 14:56
03/18/21 16:27
580-13-2
VPH NC Water
Analytical Method:
MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
ug/L
50.0
1
03/31/21 17:23
H1,N2
Aliphatic (C09-C12)
ND
ug/L
50.0
1
03/31/21 17:23
H1,N2
Aliphatic(C09-C12)Adjusted
ND
ug/L
50.0
1
03/31/21 17:23
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
03/31/21 17:23
H1,N2
Surrogates
4-Bromofluorobenzene (FID) (S)
97
%
70-130
1
03/31/21 17:23
460-00-4
4-Bromofluorobenzene (PID) (S)
98
%
70-130
1
03/31/21 17:23
460-00-4
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Chromium
19.1
ug/L
5.0
1
03/17/2101:53
03/18/2120:59
7440-47-3
Lead
5.2
ug/L
5.0
1
03/17/21 01:53
03/18/2120:59
7439-92-1
625 RVE
Analytical Method:
EPA 625.1 Preparation Method:
EPA
625.1
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
208-96-8
Anthracene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
7005-72-3
Chrysene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
120-83-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 35

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92527373
Sample: MW-1
Parameters
ANALYTICAL RESULTS
Lab ID: 92527373001 Collected: 03/11/21 09:15 Received: 03/12/21 08:11 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Diethylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
03/16/21 07:14
03/16/21 16:20
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
117-81-7
Fluoranthene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
206-44-0
Fluorene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
193-39-5
Isophorone
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
78-59-1
Naphthalene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
87-86-5
Phenanthrene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
85-01-8
Phenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
108-95-2
Pyrene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:20
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:20
88-06-2
Surrogates
Nitrobenzene-d5 (S)
91
%
10-120
1
03/16/21 07:14
03/16/21 16:20
4165-60-0
2-Fluorobiphenyl (S)
76
%
15-120
1
03/16/21 07:14
03/16/21 16:20
321-60-8
Terphenyl-d14 (S)
132
%
11-131
1
03/16/21 07:14
03/16/21 16:20
1718-51-0
Phenol-d6 (S)
25
%
10-120
1
03/16/21 07:14
03/16/21 16:20
13127-88-3
2-Fluorophenol (S)
8
%
10-120
1
03/16/21 07:14
03/16/21 16:20
367-12-4
2,4,6-Tribromophenol (S)
13
%
10-137
1
03/16/21 07:14
03/16/21 16:20
118-79-6
6200B MSV
Analytical Method:
SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
03/19/2100:50
71-43-2
Bromobenzene
ND
ug/L
0.50
1
03/19/2100:50
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
03/19/2100:50
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
03/19/2100:50
75-27-4
REPORT OF LABORATORY ANALYSIS
S3
SO
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 35

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92527373
Sample: MW-1
ANALYTICAL RESULTS
Lab ID: 92527373001 Collected: 03/11/21 09:15 Received: 03/12/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Bromoform
ND
ug/L
0.50
1
03/19/21 00:50
75-25-2
Bromomethane
ND
ug/L
5.0
1
03/19/21 00:50
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
03/19/21 00:50
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
03/19/21 00:50
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
03/19/21 00:50
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
03/19/21 00:50
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
03/19/21 00:50
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/19/21 00:50
75-00-3
Chloroform
ND
ug/L
0.50
1
03/19/21 00:50
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/19/21 00:50
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
03/19/21 00:50
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
03/19/21 00:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
03/19/21 00:50
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
03/19/21 00:50
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
03/19/21 00:50
106-93-4
Dibromomethane
ND
ug/L
0.50
1
03/19/21 00:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
03/19/21 00:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
03/19/21 00:50
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
03/19/21 00:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
03/19/21 00:50
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
03/19/21 00:50
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
03/19/21 00:50
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
03/19/21 00:50
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
0.50
1
03/19/21 00:50
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
03/19/21 00:50
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
03/19/21 00:50
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
03/19/21 00:50
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
03/19/21 00:50
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
03/19/21 00:50
563-58-6
cis- 1,3-Dichloropropene
ND
ug/L
0.50
1
03/19/21 00:50
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
03/19/21 00:50
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
03/19/21 00:50
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
03/19/21 00:50
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
03/19/21 00:50
87-68-3
Isopropyl benzene (Cumene)
ND
ug/L
0.50
1
03/19/21 00:50
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
03/19/21 00:50
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
03/19/21 00:50
1634-04-4
Naphthalene
ND
ug/L
2.0
1
03/19/21 00:50
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
03/19/21 00:50
103-65-1
Styrene
ND
ug/L
0.50
1
03/19/21 00:50
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
03/19/21 00:50
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
03/19/21 00:50
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
03/19/21 00:50
127-18-4
Toluene
ND
ug/L
0.50
1
03/19/21 00:50
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
03/19/21 00:50
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
03/19/21 00:50
120-82-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92527373
Sample: MW-1
Lab ID: 92527373001 Collected:
03/11/21 09:15
Received: 03/12/21 08:11 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200B MSV
Analytical Method:
SM 6200B
Pace Analytical
Services - Charlotte
1,1,1-Trichloroethane
ND
ug/L
0.50
1
03/19/21 00:50
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
03/19/21 00:50
79-00-5
Trichloroethene
ND
ug/L
0.50
1
03/19/21 00:50
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/19/21 00:50
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
03/19/21 00:50
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
03/19/21 00:50
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
03/19/21 00:50
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
03/19/21 00:50
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
03/19/21 00:50
179601-23-1
o-Xylene
ND
ug/L
0.50
1
03/19/21 00:50
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
03/19/21 00:50
17060-07-0
4-Bromofluorobenzene (S)
94
%
70-130
1
03/19/21 00:50
460-00-4
Toluene-d8 (S)
100
%
70-130
1
03/19/21 00:50
2037-26-5
Date: 04/01 /2021 12:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92527373
Sample: MW-2 Lab ID: 92527373002 Collected: 03/11/21 09:30 Received: 03/12/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
134
ug/L
100
1
03/19/21 07:23
03/24/21 10:21
N2
Aliphatic (C19-C36)
ND
ug/L
100
1
03/19/21 07:23
03/24/21 10:21
N2
Aromatic (C11-C22)
ND
ug/L
100
1
03/19/21 07:23
03/24/21 10:21
N2
Surrogates
1-Chlorooctadecane (S)
46
%
40-140
1
03/19/21 07:23
03/24/21 10:21
3386-33-2
o-Terphenyl (S)
74
%
40-140
1
03/19/21 07:23
03/24/21 10:21
84-15-1
VPH NC Water
Analytical Method:
MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
56.3
ug/L
50.0
1
03/31/21 17:51
H1,N2
Aliphatic (C09-C12)
64.7
ug/L
50.0
1
03/31/21 17:51
H1,N2
Aliphatic(C09-C12)Adjusted
54.4
ug/L
50.0
1
03/31/21 17:51
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
03/31/21 17:51
H1,N2
Surrogates
4-Bromofluorobenzene (FID) (S)
103
%
70-130
1
03/31/21 17:51
460-00-4
4-Bromofluorobenzene (PID) (S)
103
%
70-130
1
03/31/21 17:51
460-00-4
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Chromium
28.1
ug/L
5.0
1
03/17/2101:53
03/18/2121:15
7440-47-3
Lead
33.0
ug/L
5.0
1
03/17/21 01:53
03/18/2121:15
7439-92-1
625 RVE
Analytical Method:
EPA 625.1 Preparation Method:
EPA
625.1
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
208-96-8
Anthracene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
7005-72-3
Chrysene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
105-67-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92527373
Sample: MW-2
Lab ID: 92527373002 Collected:
03/11/21
09:30
Received: 03/12/21 08:11 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical Method:
EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Dimethylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
03/16/21 07:14
03/16/21 16:49
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
117-81-7
Fluoranthene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
206-44-0
Fluorene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
193-39-5
Isophorone
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
78-59-1
Naphthalene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
87-86-5
Phenanthrene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
85-01-8
Phenol
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
108-95-2
Pyrene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
03/16/21 07:14
03/16/21 16:49
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
03/16/21 07:14
03/16/21 16:49
88-06-2
Surrogates
Nitrobenzene-d5 (S)
93
%
10-120
1
03/16/21 07:14
03/16/21 16:49
4165-60-0
2-Fluorobiphenyl (S)
81
%
15-120
1
03/16/21 07:14
03/16/21 16:49
321-60-8
Terphenyl-d14 (S)
119
%
11-131
1
03/16/21 07:14
03/16/21 16:49
1718-51-0
Phenol-d6 (S)
17
%
10-120
1
03/16/21 07:14
03/16/21 16:49
13127-88-3
2-Fluorophenol (S)
4
%
10-120
1
03/16/21 07:14
03/16/21 16:49
367-12-4 SO
2,4,6-Tribromophenol (S)
12
%
10-137
1
03/16/21 07:14
03/16/21 16:49
118-79-6
6200B MSV
Analytical Method:
SM 6200B
Pace Analytical
Services - Charlotte
Benzene
2.4
ug/L
0.50
1
03/19/2101:08
71-43-2
Bromobenzene
ND
ug/L
0.50
1
03/19/2101:08
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
03/19/2101:08
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
03/19/2101:08
75-27-4
Bromoform
ND
ug/L
0.50
1
03/19/2101:08
75-25-2
Bromomethane
ND
ug/L
5.0
1
03/19/2101:08
74-83-9
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 35

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ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92527373
Sample: MW-2 Lab ID: 92527373002 Collected: 03/11/21 09:30 Received: 03/12/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
n-Butylbenzene
ND
ug/L
0.50
1
03/19/21 01:08
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
03/19/21 01:08
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
03/19/21 01:08
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
03/19/21 01:08
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
03/19/21 01:08
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/19/21 01:08
75-00-3
Chloroform
ND
ug/L
0.50
1
03/19/21 01:08
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/19/21 01:08
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
03/19/21 01:08
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
03/19/21 01:08
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
03/19/21 01:08
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
03/19/21 01:08
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
03/19/21 01:08
106-93-4
Dibromomethane
ND
ug/L
0.50
1
03/19/21 01:08
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
03/19/21 01:08
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
03/19/21 01:08
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
03/19/21 01:08
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
03/19/21 01:08
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
03/19/21 01:08
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
03/19/21 01:08
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
03/19/21 01:08
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
03/19/21 01:08
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
03/19/21 01:08
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
03/19/21 01:08
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
03/19/21 01:08
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
03/19/21 01:08
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
03/19/21 01:08
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
03/19/21 01:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
03/19/21 01:08
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
03/19/21 01:08
108-20-3
Ethylbenzene
2.6
ug/L
0.50
1
03/19/21 01:08
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
03/19/21 01:08
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
03/19/21 01:08
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
03/19/21 01:08
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
03/19/21 01:08
1634-04-4
Naphthalene
ND
ug/L
2.0
1
03/19/21 01:08
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
03/19/21 01:08
103-65-1
Styrene
ND
ug/L
0.50
1
03/19/21 01:08
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
03/19/21 01:08
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
03/19/21 01:08
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
03/19/21 01:08
127-18-4
Toluene
1.9
ug/L
0.50
1
03/19/21 01:08
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
03/19/21 01:08
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
03/19/21 01:08
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
03/19/21 01:08
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
03/19/21 01:08
79-00-5
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92527373
Sample: MW-2
Lab ID: 92527373002 Collected:
03/11/21 09:30
Received: 03/12/21 08:11 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Trichloroethene
ND ug/L
0.50
1
03/19/21 01:08
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
03/19/21 01:08
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
03/19/21 01:08
96-18-4
1,2,4-Trimethylbenzene
4.9 ug/L
0.50
1
03/19/21 01:08
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
03/19/21 01:08
108-67-8
Vinyl chloride
ND ug/L
1.0
1
03/19/21 01:08
75-01-4
m&p-Xylene
9.2 ug/L
1.0
1
03/19/21 01:08
179601-23-1
o-Xylene
4.4 ug/L
0.50
1
03/19/21 01:08
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
03/19/21 01:08
17060-07-0
4-Bromofluorobenzene (S)
95 %
70-130
1
03/19/21 01:08
460-00-4
Toluene-d8 (S)
99 %
70-130
1
03/19/21 01:08
2037-26-5
Date: 04/01 /2021 12:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92527373
QC Batch: 610570
QC Batch Method: MADEP VPH
Associated Lab Samples: 92527373001, 92527373002
METHOD BLANK: 3215185
Associated Lab Samples: 92527373001, 92527373002
Parameter
Units
Aliphatic (C05-CO8)
ug/L
Aliphatic (C09-C12)
ug/L
Aromatic (C09-C10)
ug/L
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
QUALITY CONTROL DATA
Analysis Method: MADEP VPH
Analysis Description: VPH NC Water
Laboratory: Pace Analytical Services - Charlotte
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
50.0
03/31 /21 16:55 N2
ND
50.0
03/31 /21 16:55 N2
ND
50.0
03/31 /21 16:55 N2
96
70-130
03/31/2116:55
97
70-130
03/31/2116:55
LABORATORY CONTROL SAMPLE & LCSD:
3215186
3215187
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
297
295
99
98
70-130 1 25 N2
Aliphatic (C09-C12)
ug/L
300
323
323
108
108
70-130 0 25 N2
Aromatic (C09-C10)
ug/L
100
101
99.5
101
99
70-130 1 25 N2
4-Bromofluorobenzene (FID) (S)
%
97
94
70-130
4-Bromofluorobenzene (PID) (S)
%
97
94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
QC Batch: 607051
Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A
Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92527373001, 92527373002
METHOD BLANK: 3198351
Matrix: Water
Associated Lab Samples: 92527373001, 92527373002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Chromium
ug/L
ND 5.0
03/18/2119:54
Lead
ug/L
ND 5.0
03/18/2119:54
LABORATORY CONTROL SAMPLE:
3198352
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Chromium
ug/L
500 516
103 80-120
Lead
ug/L
500 497
99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3198353 3198354
MS MSD
92524737001
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chromium
ug/L ND
500 500 498
503 99 100
75-125 1
Lead
ug/L ND
500 500 489
489 97 97
75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 35

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
QC Batch: 607642 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92527373001, 92527373002
METHOD BLANK: 3201003
Associated Lab Samples: 92527373001, 92527373002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
03/19/21 00:32
1,1,1-Trichloroethane
ug/L
ND
0.50
03/19/21 00:32
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
03/19/21 00:32
1,1,2-Trichloroethane
ug/L
ND
0.50
03/19/21 00:32
1,1-Dichloroethane
ug/L
ND
0.50
03/19/21 00:32
1,1-Dichloroethene
ug/L
ND
0.50
03/19/21 00:32
1,1-Dichloropropene
ug/L
ND
0.50
03/19/21 00:32
1,2,3-Trichlorobenzene
ug/L
ND
2.0
03/19/21 00:32
1,2,3-Trichloropropane
ug/L
ND
0.50
03/19/21 00:32
1,2,4-Trichlorobenzene
ug/L
ND
2.0
03/19/21 00:32
1,2,4-Trimethylbenzene
ug/L
ND
0.50
03/19/21 00:32
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
03/19/21 00:32
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
03/19/21 00:32
1,2-Dichlorobenzene
ug/L
ND
0.50
03/19/21 00:32
1,2-Dichloroethane
ug/L
ND
0.50
03/19/21 00:32
1,2-Dichloropropane
ug/L
ND
0.50
03/19/21 00:32
1,3,5-Trimethylbenzene
ug/L
ND
0.50
03/19/21 00:32
1,3-Dichlorobenzene
ug/L
ND
0.50
03/19/21 00:32
1,3-Dichloropropane
ug/L
ND
0.50
03/19/21 00:32
1,4-Dichlorobenzene
ug/L
ND
0.50
03/19/21 00:32
2,2-Dichloropropane
ug/L
ND
0.50
03/19/21 00:32
2-Chlorotoluene
ug/L
ND
0.50
03/19/21 00:32
4-Chlorotoluene
ug/L
ND
0.50
03/19/21 00:32
Benzene
ug/L
ND
0.50
03/19/21 00:32
Bromobenzene
ug/L
ND
0.50
03/19/21 00:32
Bromochloromethane
ug/L
ND
0.50
03/19/21 00:32
Bromodichloromethane
ug/L
ND
0.50
03/19/21 00:32
Bromoform
ug/L
ND
0.50
03/19/21 00:32
Bromomethane
ug/L
ND
5.0
03/19/21 00:32
Carbon tetrachloride
ug/L
ND
0.50
03/19/21 00:32
Chlorobenzene
ug/L
ND
0.50
03/19/21 00:32
Chloroethane
ug/L
ND
1.0
03/19/21 00:32
Chloroform
ug/L
ND
0.50
03/19/21 00:32
Chloromethane
ug/L
ND
1.0
03/19/21 00:32
cis-1,2-Dichloroethene
ug/L
ND
0.50
03/19/21 00:32
cis-1,3-Dichloropropene
ug/L
ND
0.50
03/19/21 00:32
Dibromochloromethane
ug/L
ND
0.50
03/19/21 00:32
Dibromomethane
ug/L
ND
0.50
03/19/21 00:32
Dichlorodifluoromethane
ug/L
ND
0.50
03/19/21 00:32
Diisopropyl ether
ug/L
ND
0.50
03/19/21 00:32
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 35

leAnalyiical
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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
METHOD BLANK: 3201003
Associated Lab Samples: 92527373001, 92527373002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
03/19/21 00:32
Hexachloro-1,3-butadiene
ug/L
ND
2.0
03/19/21 00:32
Isopropylbenzene (Cumene)
ug/L
ND
0.50
03/19/21 00:32
m&p-Xylene
ug/L
ND
1.0
03/19/21 00:32
Methyl-tert-butyl ether
ug/L
ND
0.50
03/19/21 00:32
Methylene Chloride
ug/L
ND
2.0
03/19/21 00:32
n-Butylbenzene
ug/L
ND
0.50
03/19/21 00:32
n-Propylbenzene
ug/L
ND
0.50
03/19/21 00:32
Naphthalene
ug/L
ND
2.0
03/19/21 00:32
o-Xylene
ug/L
ND
0.50
03/19/21 00:32
sec-Butylbenzene
ug/L
ND
0.50
03/19/21 00:32
Styrene
ug/L
ND
0.50
03/19/21 00:32
tert-Butyl benzene
ug/L
ND
0.50
03/19/21 00:32
Tetrachloroethene
ug/L
ND
0.50
03/19/21 00:32
Toluene
ug/L
ND
0.50
03/19/21 00:32
trans-1,2-Dichloroethene
ug/L
ND
0.50
03/19/21 00:32
trans- 1,3-Dichloropropene
ug/L
ND
0.50
03/19/21 00:32
Trichloroethene
ug/L
ND
0.50
03/19/21 00:32
Trichlorofluoromethane
ug/L
ND
1.0
03/19/21 00:32
Vinyl chloride
ug/L
ND
1.0
03/19/21 00:32
1,2-Dichloroethane-d4 (S)
%
97
70-130
03/19/21 00:32
4-Bromofluorobenzene (S)
%
94
70-130
03/19/21 00:32
Toluene-d8 (S)
%
100
70-130
03/19/21 00:32
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3201004
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
48.5
97
60-140
1,1,1-Trichloroethane
ug/L
50
44.2
88
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
46.9
94
60-140
1,1,2-Trichloroethane
ug/L
50
47.1
94
60-140
1,1-Dichloroethane
ug/L
50
44.3
89
60-140
1,1-Dichloroethene
ug/L
50
46.4
93
60-140
1,1-Dichloropropene
ug/L
50
45.3
91
60-140
1,2,3-Trichlorobenzene
ug/L
50
49.0
98
60-140
1,2,3-Trichloropropane
ug/L
50
49.7
99
60-140
1,2,4-Trichlorobenzene
ug/L
50
49.7
99
60-140
1,2,4-Trimethylbenzene
ug/L
50
47.6
95
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
49.4
99
60-140
1,2-Dibromoethane (EDB)
ug/L
50
48.2
96
60-140
1,2-Dichlorobenzene
ug/L
50
49.5
99
60-140
1,2-Dichloroethane
ug/L
50
41.3
83
60-140
1,2-Dichloropropane
ug/L
50
43.5
87
60-140
1,3,5-Trimethylbenzene
ug/L
50
46.4
93
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
LABORATORY CONTROL SAMPLE:
Parameter
3201004
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
50.2
100
60-140
1,3-Dichloropropane
ug/L
50
47.1
94
60-140
1,4-Dichlorobenzene
ug/L
50
50.4
101
60-140
2,2-Dichloropropane
ug/L
50
45.6
91
60-140
2-Chlorotoluene
ug/L
50
46.9
94
60-140
4-Chlorotoluene
ug/L
50
45.9
92
60-140
Benzene
ug/L
50
45.3
91
60-140
Bromobenzene
ug/L
50
47.1
94
60-140
Bromochloromethane
ug/L
50
47.6
95
60-140
Bromodichloromethane
ug/L
50
43.3
87
60-140
Bromoform
ug/L
50
48.0
96
60-140
Bromomethane
ug/L
50
47.9
96
60-140
Carbon tetrachloride
ug/L
50
48.8
98
60-140
Chlorobenzene
ug/L
50
49.4
99
60-140
Chloroethane
ug/L
50
43.3
87
60-140
Chloroform
ug/L
50
43.2
86
60-140
Chloromethane
ug/L
50
43.2
86
60-140
cis-1,2-Dichloroethene
ug/L
50
43.1
86
60-140
cis-1,3-Dichloropropene
ug/L
50
46.8
94
60-140
Dibromochloromethane
ug/L
50
49.2
98
60-140
Dibromomethane
ug/L
50
49.5
99
60-140
Dichlorodifluoromethane
ug/L
50
49.2
98
60-140
Diisopropyl ether
ug/L
50
40.8
82
60-140
Ethylbenzene
ug/L
50
48.2
96
60-140
Hexachloro-1,3-butadiene
ug/L
50
46.8
94
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.9
98
60-140
m&p-Xylene
ug/L
100
97.1
97
60-140
Methyl-tert-butyl ether
ug/L
50
44.3
89
60-140
Methylene Chloride
ug/L
50
44.6
89
60-140
n-Butylbenzene
ug/L
50
47.9
96
60-140
n-Propylbenzene
ug/L
50
46.3
93
60-140
Naphthalene
ug/L
50
51.1
102
60-140
o-Xylene
ug/L
50
48.4
97
60-140
sec-Butylbenzene
ug/L
50
47.5
95
60-140
Styrene
ug/L
50
49.1
98
60-140
tert-Butyl benzene
ug/L
50
39.8
80
60-140
Tetrachloroethene
ug/L
50
49.3
99
60-140
Toluene
ug/L
50
47.2
94
60-140
trans-1,2-Dichloroethene
ug/L
50
45.0
90
60-140
trans- 1,3-Dichloropropene
ug/L
50
46.2
92
60-140
Trichloroethene
ug/L
50
49.1
98
60-140
Trichlorofluoromethane
ug/L
50
48.6
97
60-140
Vinyl chloride
ug/L
50
44.3
89
60-140
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
96
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3201005
3201006
MS
MSD
92527693003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
<62.2
4000
4000
4130
4160
103
104
60-140
1
1,1,1-Trichloroethane
ug/L
<66.4
4000
4000
3950
3960
99
99
60-140
0
1,1,2,2-Tetrachloroethane
ug/L
<45.0
4000
4000
3850
3930
96
98
60-140
2
1,1,2-Trichloroethane
ug/L
<65.0
4000
4000
4000
4070
100
102
60-140
2
1,1-Dichloroethane
ug/L
<73.4
4000
4000
3810
3920
95
98
60-140
3
1,1-Dichloroethene
ug/L
<69.6
4000
4000
4170
4260
104
107
60-140
2
1,1-Dichloropropene
ug/L
<85.4
4000
4000
3940
4010
99
100
60-140
2
1,2,3-Trichlorobenzene
ug/L
<161
4000
4000
4260
4370
106
109
60-140
3
1,2,3-Trichloropropane
ug/L
<52.2
4000
4000
3980
4190
100
105
60-140
5
1,2,4-Trichlorobenzene
ug/L
<128
4000
4000
4260
4350
106
109
60-140
2
1,2,4-Trimethylbenzene
ug/L
12100
4000
4000
15700
16100
90
100
60-140
3
1,2-Dibromo-3-chloropropane
ug/L
<68.0
4000
4000
3940
4100
99
103
60-140
4
1,2-Dibromoethane (EDB)
ug/L
515
4000
4000
4540
4650
101
103
60-140
2
1,2-Dichlorobenzene
ug/L
<67.8
4000
4000
4220
4340
106
108
60-140
3
1,2-Dichloroethane
ug/L
337
4000
4000
3830
3790
87
86
60-140
1
1,2-Dichloropropane
ug/L
<71.0
4000
4000
3780
3850
95
96
60-140
2
1,3,5-Trimethylbenzene
ug/L
3100
4000
4000
6970
7190
97
102
60-140
3
1,3-Dichlorobenzene
ug/L
<68.0
4000
4000
4300
4390
108
110
60-140
2
1,3-Dichloropropane
ug/L
<56.8
4000
4000
3920
3950
98
99
60-140
1
1,4-Dichlorobenzene
ug/L
<66.6
4000
4000
4290
4350
107
109
60-140
1
2,2-Dichloropropane
ug/L
<77.6
4000
4000
2830
2800
71
70
60-140
1
2-Chlorotoluene
ug/L
<64.2
4000
4000
4190
4500
105
112
60-140
7
4-Chlorotoluene
ug/L
<64.8
4000
4000
3970
4020
99
101
60-140
1
Benzene
ug/L
17000
4000
4000
20500
20600
88
91
60-140
1
Bromobenzene
ug/L
<58.0
4000
4000
4070
4130
102
103
60-140
1
Bromochloromethane
ug/L
<93.6
4000
4000
4070
4150
102
104
60-140
2
Bromodichloromethane
ug/L
<61.4
4000
4000
3730
3750
93
94
60-140
1
Bromoform
ug/L
<68.2
4000
4000
3910
3960
98
99
60-140
1
Bromomethane
ug/L
<332
4000
4000
4190
4360
105
109
60-140
4
Carbon tetrachloride
ug/L
<66.6
4000
4000
4360
4440
109
111
60-140
2
Chlorobenzene
ug/L
<56.8
4000
4000
4270
4260
107
107
60-140
0
Chloroethane
ug/L
<130
4000
4000
4880
4830
122
121
60-140
1
Chloroform
ug/L
<70.6
4000
4000
3740
3880
94
97
60-140
4
Chloromethane
ug/L
<108
4000
4000
3180
3320
79
83
60-140
4
cis-1,2-Dichloroethene
ug/L
<76.8
4000
4000
3780
3800
95
95
60-140
0
cis-1,3-Dichloropropene
ug/L
<73.0
4000
4000
3730
3770
93
94
60-140
1
Dibromochloromethane
ug/L
<71.8
4000
4000
4090
4150
102
104
60-140
2
Dibromomethane
ug/L
<78.8
4000
4000
4160
4250
104
106
60-140
2
Dichlorodifluoromethane
ug/L
<69.2
4000
4000
4060
4030
101
101
60-140
1
Diisopropyl ether
ug/L
103
4000
4000
3550
3590
86
87
60-140
1
Ethylbenzene
ug/L
4920
4000
4000
9040
9120
103
105
60-140
1
Hexachloro-1,3-butadiene
ug/L
<306
4000
4000
4010
4040
100
101
60-140
1
Isopropylbenzene (Cumene)
ug/L
396
4000
4000
4690
4720
107
108
60-140
0
m&p-Xylene
ug/L
17000
8000
8000
25000
25500
101
106
60-140
2
Methyl-tert-butyl ether
ug/L
252
4000
4000
3910
4010
92
94
60-140
2
Methylene Chloride
ug/L
<390
4000
4000
3900
3910
97
98
60-140
0
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3201005
3201006
MS
MSD
92527693003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
<98.0
4000
4000
4890
4980
122
125
60-140
2
n-Propylbenzene
ug/L
<68.0
4000
4000
5300
5410
133
135
60-140
2
Naphthalene
ug/L
2580
4000
4000
7150
7480
114
123
60-140
5
o-Xylene
ug/L
7420
4000
4000
11500
11600
103
105
60-140
1
sec-Butylbenzene
ug/L
<80.0
4000
4000
4320
4420
108
111
60-140
2
Styrene
ug/L
117
4000
4000
4360
4380
106
107
60-140
0
tert-Butyl benzene
ug/L
<64.6
4000
4000
3510
3540
88
89
60-140
1
Tetrachloroethene
ug/L
<58.4
4000
4000
4280
4290
107
107
60-140
0
Toluene
ug/L
39600
4000
4000
42200
42200
63
63
60-140
0 E
trans-1,2-Dichloroethene
ug/L
<79.2
4000
4000
3940
3910
98
98
60-140
1
trans- 1,3-Dichloropropene
ug/L
<72.6
4000
4000
3670
3690
92
92
60-140
1
Trichloroethene
ug/L
<76.6
4000
4000
4370
4360
109
109
60-140
0
Trichlorofluoromethane
ug/L
<59.6
4000
4000
5080
5100
127
127
60-140
0
Vinyl chloride
ug/L
<77.2
4000
4000
3720
3800
93
95
60-140
2
1,2-Dichloroethane-d4 (S)
%
97
96
70-130
4-Bromofluorobenzene (S)
%
98
97
70-130
Toluene-d8(S)
%
97
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
QC Batch: 606500 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92527373001, 92527373002
METHOD BLANK: 3195339
Associated Lab Samples: 92527373001, 92527373002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
03/15/21 15:29
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
03/15/21 15:29
2,4,6-Trichlorophenol
ug/L
ND
10.0
03/15/21 15:29
2,4-Dichlorophenol
ug/L
ND
5.0
03/15/21 15:29
2,4-Dimethylphenol
ug/L
ND
10.0
03/15/21 15:29
2,4-Dinitrophenol
ug/L
ND
50.0
03/15/21 15:29
2,4-Dinitrotoluene
ug/L
ND
5.0
03/15/21 15:29
2,6-Dinitrotoluene
ug/L
ND
5.0
03/15/21 15:29
2-Chloronaphthalene
ug/L
ND
5.0
03/15/21 15:29
2-Chlorophenol
ug/L
ND
5.0
03/15/21 15:29
2-Nitrophenol
ug/L
ND
5.0
03/15/21 15:29
3,3'-Dichlorobenzidine
ug/L
ND
10.0
03/15/21 15:29
4,6-Dinitro-2-methyl phenol
ug/L
ND
10.0
03/15/21 15:29
4-Bromophenylphenyl ether
ug/L
ND
5.0
03/15/21 15:29
4-ChIoro-3-methyl phenol
ug/L
ND
5.0
03/15/21 15:29
4-Chlorophenylphenyl ether
ug/L
ND
5.0
03/15/21 15:29
4-Nitrophenol
ug/L
ND
10.0
03/15/21 15:29
Acenaphthene
ug/L
ND
5.0
03/15/21 15:29
Acenaphthylene
ug/L
ND
5.0
03/15/21 15:29
Anthracene
ug/L
ND
5.0
03/15/21 15:29
Benzo(a)anthracene
ug/L
ND
5.0
03/15/21 15:29
Benzo(a)pyrene
ug/L
ND
5.0
03/15/21 15:29
Benzo(b)fluoranthene
ug/L
ND
5.0
03/15/21 15:29
Benzo(g,h,i)perylene
ug/L
ND
5.0
03/15/21 15:29
Benzo(k)fluoranthene
ug/L
ND
5.0
03/15/21 15:29
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
03/15/21 15:29
bis(2-Chloroethyl) ether
ug/L
ND
5.0
03/15/21 15:29
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
03/15/21 15:29
Butylbenzylphthalate
ug/L
ND
5.0
03/15/21 15:29
Chrysene
ug/L
ND
5.0
03/15/21 15:29
Di-n-butylphthalate
ug/L
ND
5.0
03/15/21 15:29
Di-n-octylphthalate
ug/L
ND
5.0
03/15/21 15:29
Dibenz(a,h)anthracene
ug/L
ND
5.0
03/15/21 15:29
Diethylphthalate
ug/L
ND
5.0
03/15/21 15:29
Dimethylphthalate
ug/L
ND
5.0
03/15/21 15:29
Fluoranthene
ug/L
ND
5.0
03/15/21 15:29
Fluorene
ug/L
ND
5.0
03/15/21 15:29
Hexachloro-1,3-butadiene
ug/L
ND
5.0
03/15/21 15:29
Hexachlorobenzene
ug/L
ND
5.0
03/15/21 15:29
Hexachlorocyclopentadiene
ug/L
ND
10.0
03/15/21 15:29
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92527373
METHOD BLANK: 3195339
Associated Lab Samples: 92527373001, 92527373002
Parameter
Units
Hexachloroethane
ug/L
Indeno(1,2,3-cd)pyrene
ug/L
Isophorone
ug/L
N-Nitroso-di-n-propylamine
ug/L
N-Nitrosodimethylamine
ug/L
N-Nitrosodiphenylamine
ug/L
Naphthalene
ug/L
Nitrobenzene
ug/L
Pentachlorophenol
ug/L
Phenanthrene
ug/L
Phenol
ug/L
Pyrene
ug/L
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
QUALITY CONTROL DATA
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
5.0
03/15/2115:29
ND
5.0
03/15/2115:29
ND
10.0
03/15/2115:29
ND
5.0
03/15/2115:29
ND
5.0
03/15/2115:29
ND
10.0
03/15/2115:29
ND
5.0
03/15/2115:29
ND
5.0
03/15/2115:29
ND
10.0
03/15/2115:29
ND
5.0
03/15/2115:29
ND
5.0
03/15/2115:29
ND
5.0
03/15/2115:29
140
10-137
03/15/2115:29 S3
120
15-120
03/15/2115:29
90
10-120
03/15/2115:29
131
10-120
03/15/2115:29 S3
75
10-120
03/15/2115:29
165
11-131
03/15/2115:29 S3
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3195340
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
32.9
66
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
42.0
84
36-166
2,4,6-Trichlorophenol
ug/L
50
45.5
91
37-144
2,4-Dichlorophenol
ug/L
50
44.5
89
1-191
2,4-Dimethylphenol
ug/L
50
46.5
93
32-119
2,4-Dinitrophenol
ug/L
250
262
105
1-181
2,4-Dinitrotoluene
ug/L
50
45.0
90
39-139
2,6-Dinitrotoluene
ug/L
50
52.0
104
50-158
2-Chloronaphthalene
ug/L
50
38.5
77
60-118
2-Chlorophenol
ug/L
50
41.3
83
23-134
2-Nitrophenol
ug/L
50
51.2
102
29-182
3,3'-Dichlorobenzidine
ug/L
100
93.1
93
1-262
4,6-Dinitro-2-methyl phenol
ug/L
100
111
111
1-181
4-Bromophenylphenyl ether
ug/L
50
47.1
94
53-127
4-Chloro-3-methylphenol
ug/L
100
90.5
91
22-147
4-Chlorophenylphenyl ether
ug/L
50
43.5
87
25-158
4-Nitrophenol
ug/L
250
129
51
1-132
Acenaphthene
ug/L
50
43.4
87
47-145
Acenaphthylene
ug/L
50
44.4
89
33-145
Anthracene
ug/L
50
47.2
94
1-166
Benzo(a)anthracene
ug/L
50
48.6
97
33-143
Benzo(a)pyrene
ug/L
50
49.2
98
17-163
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
LABORATORY CONTROL SAMPLE:
Parameter
3195340
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(b)fluoranthene
ug/L
50
47.6
95
24-159
Benzo(g,h,i)perylene
ug/L
50
49.4
99
1-219
Benzo(k)fluoranthene
ug/L
50
48.6
97
11-162
bis(2-Chloroethoxy)methane
ug/L
50
45.6
91
33-184
bis(2-Chloroethyl) ether
ug/L
50
48.5
97
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
54.0
108
8-158
Butylbenzylphthalate
ug/L
50
52.4
105
1-152
Chrysene
ug/L
50
47.3
95
17-168
Di-n-butylphthalate
ug/L
50
48.9
98
1-118
Di-n-octylphthalate
ug/L
50
57.5
115
4-146
Dibenz(a,h)anthracene
ug/L
50
50.3
101
1-227
Diethylphthalate
ug/L
50
45.8
92
1-114
Dimethylphthalate
ug/L
50
43.8
88
1-112
Fluoranthene
ug/L
50
47.8
96
26-137
Fluorene
ug/L
50
45.3
91
59-121
Hexachloro-1,3-butadiene
ug/L
50
30.0
60
24-116
Hexachlorobenzene
ug/L
50
43.6
87
1-152
Hexachlorocyclopentadiene
ug/L
50
24.3
49
25-150
Hexachloroethane
ug/L
50
30.8
62
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
50.6
101
1-171
Isophorone
ug/L
50
46.9
94
21-196
N-Nitroso-di-n-propylamine
ug/L
50
46.0
92
1-230
N-Nitrosodimethylamine
ug/L
50
36.1
72
25-150
N-Nitrosodiphenylamine
ug/L
50
44.5
89
25-150
Naphthalene
ug/L
50
37.9
76
21-133
Nitrobenzene
ug/L
50
47.4
95
35-180
Pentachlorophenol
ug/L
100
95.0
95
14-176
Phenanthrene
ug/L
50
45.6
91
54-120
Phenol
ug/L
50
26.8
54
5-112
Pyrene
ug/L
50
45.0
90
52-115
2,4,6-Tribromophenol (S)
%
115
10-137
2-Fluorobiphenyl (S)
%
93
15-120
2-Fluorophenol(S)
%
67
10-120
Nitrobenzene-d5 (S)
%
108
10-120
Phenol-d6 (S)
%
50
10-120
Terphenyl-d14 (S)
%
120
11-131
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
QC Batch: 606882 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92527373001
METHOD BLANK: 3197263
Matrix:
Water
Associated Lab Samples: 92527373001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
ug/L
ND
100
03/18/21 09:59 N2
Aliphatic (C19-C36)
ug/L
ND
100
03/18/21 09:59 N2
Aromatic (C11-C22)
ug/L
ND
100
03/18/21 09:59 N2
1-Chlorooctadecane (S)
%
60
40-140
03/18/21 09:59
2-Bromonaphthalene (S)
%
86
40-140
03/18/21 09:59
2-Fluorobiphenyl (S)
%
86
40-140
03/18/21 09:59
o-Terphenyl (S)
%
90
40-140
03/18/21 09:59
LABORATORY CONTROL SAMPLE & LCSD:
3197264
3197265
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
ug/L
300
246
215
82
72
40-140 14 50 N2
Aliphatic (C19-C36)
ug/L
400
451
376
113
94
40-140 18 50 N2
Aromatic (C11-C22)
ug/L
850
707
698
83
82
40-140 1 50 N2
1-Chlorooctadecane (S)
%
71
56
40-140
2-Bromonaphthalene (S)
%
89
96
40-140
2-Fluorobiphenyl (S)
%
88
96
40-140
o-Terphenyl(S)
%
91
89
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92527373
QC Batch: 607854 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92527373002
METHOD BLANK: 3202160
Associated Lab Samples: 92527373002
Parameter
Units
Aliphatic (C09-C18)
ug/L
Aliphatic (C19-C36)
ug/L
Aromatic (C11-C22)
ug/L
1-Chlorooctadecane (S)
%
o-Terphenyl(S)
%
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
100
03/24/2109:00 N2
ND
100
03/24/2109:00 N2
ND
100
03/24/2109:00 N2
79
40-140
03/24/2109:00
86
40-140
03/24/2109:00
LABORATORY CONTROL SAMPLE & LCSD:
3202161
3202162
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
ug/L
300
226
173
75
58
40-140 27 50 N2
Aliphatic (C19-C36)
ug/L
400
423
380
106
95
40-140 11 50 N2
Aromatic (C11-C22)
ug/L
850
675
606
79
71
40-140 11 50 N2
1-Chlorooctadecane (S)
%
71
66
40-140
o-Terphenyl(S)
%
86
80
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 35

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: 21003
Pace Project No.: 92527373
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H1 Analysis conducted outside the EPA method holding time.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
SO Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2021 12:00 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
21003
92527373
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92527373001
MW-1
MADEP EPH
606882
MADEP EPH
607110
92527373002
MW-2
MADEP EPH
607854
MADEP EPH
608802
92527373001
MW-1
MADEP VPH
610570
92527373002
MW-2
MADEP VPH
610570
92527373001
MW-1
EPA 3010A
607051
EPA 6010D
607083
92527373002
MW-2
EPA 3010A
607051
EPA 6010D
607083
92527373001
MW-1
EPA 625.1
606500
EPA 625.1
606544
92527373002
MW-2
EPA 625.1
606500
EPA 625.1
606544
92527373001
MW-1
SM 6200B
607642
92527373002
MW-2
SM 6200B
607642
Date: 04/01 /2021 12:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 35

%p'�/Jc Sample Condition Upon Receipt(SCUR) Page 1 of 2
, i AnalyficaI Document No.: Issuing Authority:
I F•CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Wuntersville Q Raleigh[] Mechanicsville❑ Atlanta[] Kernersville❑
ReceiptSample j Client Name: Project K: ' wo# : 92527373
Courier: []Fed Ex ❑UPS ❑USPS ❑Client �� ��� �� �� �� �� ���� ���
❑ Commercial ❑Pace ❑Other: 92527373
Custody Seal Present? Oyes [ANo Seals Intact? []yes MNo
Date/Initials Person Examining Contents;'
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
❑Yes []No []N/A
Thermometer: [jWet ❑Blue ❑None
>a IR Gun ID: Type of Ice:
Correction Factor:
Cooler Temp: Add/Subtract ('C) 0.0°C Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples an ice, cooling process
Cooler Temp Corrected ('C): has begun
USDA Regulated Soil (Ri N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
r—t.,_ inrindino Hawaii and Puerto Ricol? nYes nNo
Comments/Discrepancy,
Chain of Custody Present?
`QYes
[]NO
❑N/A
1.
Samples Arrived within Hold Time?
Myes
(]NO
[I N/A
2.
Short Hold Time Analysis (472 hr.)?
❑Yes
[6No
[I N/A
3.
Rush Turn Around Time Requested?
❑Yes
QNo
[I N/A
4.
Sufficient Volume?
MYes
❑No
[I N/A
5.
Correct Containers Used?
-Pace Containers Used?
;]Yes
byes
[]NO
[]NO
❑N/A
❑N/A
6.
Containers Intact?
'byes
ONO
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[]No
®N/A
8.
Sample Labels Match COC?
-Includes. Date/rime/ID/Analysis Matrix:
Headspace in VOA Vials (>5.6mm)?
"Oyes
Ely
❑No
MNo
[]N/A
❑N/A
9.
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]yes
[/]No
❑No
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Project Manager SCURF Review:
Lot ID of splitcontainers:
Date:
Field Data Required? ❑Yes []NO
Project Manager SRF Review: Date:
Page 33 of 35

Sample Condition Upon Recei
ace Analytical Document No.:
J f-CAR-CS-033-Rev,07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/801S (water) DOC, LLHg
**Bottom half of box is to list number of bottles
t(SCUR) Page 2 of 2
Issuing Authority:
Pace Carolinas Quality Office
Project #
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Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
Amount of Preservative
lot 9
adjusted
added
r-rliAraHnn
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Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 34 of 35

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SAMPLETYPE (G=GRAB C=COMP)
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Page 35 of 35

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
May 13, 2021
Steven Lucas
Lighthouse Technical
PO Box 1379
Huntersville, NC 28078
RE: Project: 21003
Pace Project No.: 92535202
Dear Steven Lucas:
Enclosed are the analytical results for sample(s) received by the laboratory on April 27, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyler Forney for
Kevin Herring
[e-mail]
1(704)875-9092
HORIZON Database Administrator
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92535202
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 21003
Pace Project No.: 92535202
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92535202001 MW-1
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 601OD
SH1
2
PASI-A
EPA 625.1
PKS
62
PASI-C
SM 6200B
SAS
63
PASI-C
92535202002 MW-2
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 601OD
SH1
2
PASI-A
EPA 625.1
PKS
59
PASI-C
SM 6200B
SAS
63
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 37

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9800 Kincey Ave. Suite 100
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[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
21003
92535202
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92535202001
MW-1
EPA 625.1
4.023:Unknown
10.91
ug/L
04/30/21 16:21
EPA 625.1
4.323:Unknown
6.6J
ug/L
04/30/21 16:21
EPA 625.1
12.740:Unknown
10.1 J
ug/L
04/30/21 16:21
EPA 625.1
17.595:Unknown
171J
ug/L
04/30/21 16:21
92535202002
MW-2
EPA 625.1
4.322:Unknown
5AJ
ug/L
04/30/21 16:50
SM 6200B
Benzene
1.1
ug/L
0.50
04/30/21 16:39
SM 6200B
Ethylbenzene
1.0
ug/L
0.50
04/30/21 16:39
SM 6200B
1,2,4-Trimethylbenzene
1.1
ug/L
0.50
04/30/21 16:39
SM 6200B
1,3,5-Trimethylbenzene
0.78
ug/L
0.50
04/30/21 16:39
SM 6200B
m&p-Xylene
2.8
ug/L
1.0
04/30/21 16:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92535202
Method: MADEP EPH
Description: MADEP EPH NC Water
Client: Lighthouse Technical
Date: May 13, 2021
General Information:
2 samples were analyzed for MADEP EPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 617337
SO: Surrogate recovery outside laboratory control limits.
• BLANK (Lab ID: 3248164)
• 1-Chlorooctadecane (S)
• LCS (Lab ID: 3248165)
• 1-Chlorooctadecane (S)
• LCSD (Lab ID: 3248166)
• 1-Chlorooctadecane (S)
• MW-1 (Lab ID: 92535202001)
• 1-Chlorooctadecane (S)
• MW-2 (Lab ID: 92535202002)
• 1-Chlorooctadecane (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92535202
Method: MADEP EPH
Description: MADEP EPH NC Water
Client: Lighthouse Technical
Date: May 13, 2021
Analyte Comments:
QC Batch: 617337
P2: Re -extraction or re -analysis could not be performed due to insufficient sample amount.
• MW-1 (Lab ID: 92535202001)
• 1-Chlorooctadecane (S)
• MW-2 (Lab ID: 92535202002)
• 1-Chlorooctadecane (S)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92535202
Method: MADEP VPH
Description: VPH NC Water
Client: Lighthouse Technical
Date: May 13, 2021
General Information:
2 samples were analyzed for MADEP VPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H1: Analysis conducted outside the EPA method holding time.
• MW-1 (Lab ID: 92535202001)
• MW-2 (Lab ID: 92535202002)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92535202
Method: EPA 6010D
Description: 6010 MET ICP
Client: Lighthouse Technical
Date: May 13, 2021
General Information:
2 samples were analyzed for EPA 6010D by Pace Analytical Services Asheville. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3010A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92535202
Method: EPA 625.1
Description: 625 RVE
Client: Lighthouse Technical
Date: May 13, 2021
General Information:
2 samples were analyzed for EPA 625.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 625.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 617047
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
- LCS (Lab ID: 3246570)
- Pyrene
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 617047
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92535607003
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
- MS (Lab ID: 3246571)
- Hexachloroethane
- MSD (Lab ID: 3246572)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92535202
Method: EPA 625.1
Description: 625 RVE
Client: Lighthouse Technical
Date: May 13, 2021
QC Batch: 617047
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92535607003
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• Hexachloroethane
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 21003
Pace Project No.: 92535202
Method: SM 6200B
Description: 6200B MSV
Client: Lighthouse Technical
Date: May 13, 2021
General Information:
2 samples were analyzed for SM 6200B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 617384
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92535061007
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3248371)
• Toluene
• MSD (Lab ID: 3248372)
• Toluene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 11 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92535202
Sample: MWA Lab ID: 92535202001 Collected: 04/26/21 17:00 Received: 04/27/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
ND
ug/L
100
1
04/30/21 12:59
05/03/21 15:46
N2
Aliphatic (C19-C36)
ND
ug/L
100
1
04/30/21 12:59
05/03/21 15:46
N2
Aromatic (C11-C22)
ND
ug/L
100
1
04/30/21 12:59
05/03/21 15:46
N2
Surrogates
1-Chlorooctadecane (S)
27
%
40-140
1
04/30/21 12:59
05/03/21 15:46
3386-33-2
P2,SO
o-Terphenyl (S)
82
%
40-140
1
04/30/21 12:59
05/03/21 15:46
84-15-1
2-Fluorobiphenyl (S)
89
%
40-140
1
04/30/21 12:59
05/03/21 15:46
321-60-8
2-Bromonaphthalene (S)
94
%
40-140
1
04/30/21 12:59
05/03/21 15:46
580-13-2
VPH NC Water
Analytical Method:
MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
ug/L
50.0
1
05/11/21 19:12
H1,N2
Aliphatic (C09-C12)
ND
ug/L
50.0
1
05/11/21 19:12
H1,N2
Aliphatic(C09-C12)Adjusted
ND
ug/L
50.0
1
05/11/21 19:12
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
05/11/21 19:12
H1,N2
Surrogates
4-Bromofluorobenzene (FID) (S)
102
%
70-130
1
05/11/21 19:12
460-00-4
4-Bromofluorobenzene (PID) (S)
103
%
70-130
1
05/11/21 19:12
460-00-4
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Chromium
ND
ug/L
5.0
1
04/30/21 01:55
04/30/21 17:08
7440-47-3
Lead
ND
ug/L
5.0
1
04/30/21 01:55
04/30/21 17:08
7439-92-1
625 RVE
Analytical Method:
EPA 625.1 Preparation Method:
EPA
625.1
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
208-96-8
Anthracene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
7005-72-3
Chrysene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
120-83-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 37

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[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92535202
Sample: MW-1 Lab ID: 92535202001 Collected: 04/26/21 17:00 Received: 04/27/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Diethylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
04/29/21 11:52
04/30/21 16:21
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
117-81-7
Fluoranthene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
206-44-0
Fluorene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
193-39-5
Isophorone
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
78-59-1
Naphthalene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
87-86-5
Phenanthrene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
85-01-8
Phenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
108-95-2
Pyrene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:21
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:21
88-06-2
Surrogates
Nitrobenzene-d5 (S)
92
%
10-120
1
04/29/21 11:52
04/30/21 16:21
4165-60-0
2-Fluorobiphenyl (S)
74
%
15-120
1
04/29/21 11:52
04/30/21 16:21
321-60-8
Terphenyl-d14 (S)
116
%
11-131
1
04/29/21 11:52
04/30/21 16:21
1718-51-0
Phenol-d6 (S)
50
%
10-120
1
04/29/21 11:52
04/30/21 16:21
13127-88-3
2-Fluorophenol (S)
60
%
10-120
1
04/29/21 11:52
04/30/21 16:21
367-12-4
2,4,6-Tribromophenol (S)
95
%
10-137
1
04/29/21 11:52
04/30/21 16:21
118-79-6
Tentatively Identified Compounds
Unknown
10.91
ug/L
1
04/29/21 11:52
04/30/21 16:21
Unknown
6.6J
ug/L
1
04/29/21 11:52
04/30/21 16:21
Unknown
10.1J
ug/L
1
04/29/21 11:52
04/30/21 16:21
Unknown
171J
ug/L
1
04/29/21 11:52
04/30/21 16:21
REPORT OF LABORATORY ANALYSIS
L1
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92535202
Sample: MW-1 Lab ID: 92535202001 Collected: 04/26/21 17:00 Received: 04/27/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
04/30/21 16:21
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/30/21 16:21
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
04/30/21 16:21
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/30/21 16:21
75-27-4
Bromoform
ND
ug/L
0.50
1
04/30/21 16:21
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/30/21 16:21
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
04/30/21 16:21
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/30/21 16:21
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
04/30/21 16:21
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/30/21 16:21
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/30/21 16:21
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/30/21 16:21
75-00-3
Chloroform
ND
ug/L
0.50
1
04/30/21 16:21
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/30/21 16:21
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/30/21 16:21
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/30/21 16:21
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/30/21 16:21
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/30/21 16:21
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/30/21 16:21
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/30/21 16:21
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/30/21 16:21
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/30/21 16:21
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/30/21 16:21
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/30/21 16:21
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/30/21 16:21
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/30/21 16:21
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/30/21 16:21
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/30/21 16:21
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/30/21 16:21
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/30/21 16:21
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/30/21 16:21
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/30/21 16:21
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/30/21 16:21
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/30/21 16:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
04/30/21 16:21
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
04/30/21 16:21
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
04/30/21 16:21
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/30/21 16:21
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
04/30/21 16:21
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/30/21 16:21
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/30/21 16:21
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/30/21 16:21
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/30/21 16:21
103-65-1
Styrene
ND
ug/L
0.50
1
04/30/21 16:21
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/30/21 16:21
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/30/21 16:21
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92535202
Sample: MW-1 Lab ID: 92535202001 Collected: 04/26/21 17:00 Received: 04/27/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
04/30/21 16:21
127-18-4
Toluene
ND
ug/L
0.50
1
04/30/21 16:21
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/30/21 16:21
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/30/21 16:21
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/30/21 16:21
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/30/21 16:21
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/30/21 16:21
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/30/21 16:21
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/30/21 16:21
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
04/30/21 16:21
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
04/30/21 16:21
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/30/21 16:21
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
04/30/21 16:21
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/30/21 16:21
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
04/30/21 16:21
17060-07-0
4-Bromofluorobenzene (S)
89
%
70-130
1
04/30/21 16:21
460-00-4
Toluene-d8(S)
95
%
70-130
1
04/30/21 16:21
2037-26-5
Date: 05/13/2021 02:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92535202
Sample: MW-2 Lab ID: 92535202002 Collected: 04/26/21 17:20 Received: 04/27/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
ND
ug/L
100
1
04/30/21 12:59
05/03/21 16:14
N2
Aliphatic (C19-C36)
ND
ug/L
100
1
04/30/21 12:59
05/03/21 16:14
N2
Aromatic (C11-C22)
ND
ug/L
100
1
04/30/21 12:59
05/03/21 16:14
N2
Surrogates
1-Chlorooctadecane (S)
29
%
40-140
1
04/30/21 12:59
05/03/21 16:14
3386-33-2
P2,SO
o-Terphenyl (S)
79
%
40-140
1
04/30/21 12:59
05/03/21 16:14
84-15-1
2-Fluorobiphenyl (S)
88
%
40-140
1
04/30/21 12:59
05/03/21 16:14
321-60-8
2-Bromonaphthalene (S)
93
%
40-140
1
04/30/21 12:59
05/03/21 16:14
580-13-2
VPH NC Water
Analytical Method:
MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
ug/L
50.0
1
05/11/21 20:09
H1,N2
Aliphatic (C09-C12)
ND
ug/L
50.0
1
05/11/21 20:09
H1,N2
Aliphatic(C09-C12)Adjusted
ND
ug/L
50.0
1
05/11/21 20:09
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
05/11/21 20:09
H1,N2
Surrogates
4-Bromofluorobenzene (FID) (S)
98
%
70-130
1
05/11/21 20:09
460-00-4
4-Bromofluorobenzene (PID) (S)
98
%
70-130
1
05/11/21 20:09
460-00-4
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Chromium
ND
ug/L
5.0
1
04/30/21 01:55
04/30/21 17:11
7440-47-3
Lead
ND
ug/L
5.0
1
04/30/21 01:55
04/30/21 17:11
7439-92-1
625 RVE
Analytical Method:
EPA 625.1 Preparation Method:
EPA
625.1
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
208-96-8
Anthracene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
7005-72-3
Chrysene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
120-83-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92535202
Sample: MW-2 Lab ID: 92535202002 Collected: 04/26/21 17:20 Received: 04/27/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Diethylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
04/29/21 11:52
04/30/21 16:50
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
117-81-7
Fluoranthene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
206-44-0
Fluorene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
193-39-5
Isophorone
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
78-59-1
Naphthalene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
87-86-5
Phenanthrene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
85-01-8
Phenol
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
108-95-2
Pyrene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
04/29/21 11:52
04/30/21 16:50
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
04/29/21 11:52
04/30/21 16:50
88-06-2
Surrogates
Nitrobenzene-d5(S)
48
%
10-120
1
04/29/21 11:52
04/30/21 16:50
4165-60-0
2-Fluorobiphenyl (S)
39
%
15-120
1
04/29/21 11:52
04/30/21 16:50
321-60-8
Terphenyl-d14 (S)
65
%
11-131
1
04/29/21 11:52
04/30/21 16:50
1718-51-0
Phenol-d6 (S)
26
%
10-120
1
04/29/21 11:52
04/30/21 16:50
13127-88-3
2-Fluorophenol (S)
34
%
10-120
1
04/29/21 11:52
04/30/21 16:50
367-12-4
2,4,6-Tribromophenol (S)
50
%
10-137
1
04/29/21 11:52
04/30/21 16:50
118-79-6
Tentatively Identified Compounds
Unknown
5AJ
ug/L
1
04/29/21 11:52
04/30/21 16:50
6200B MSV
Analytical Method:
SM 6200B
Pace Analytical
Services - Charlotte
Benzene
1.1
ug/L
0.50
1
04/30/2116:39
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/30/2116:39
108-86-1
REPORT OF LABORATORY ANALYSIS
L1
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92535202
Sample: MW-2 Lab ID: 92535202002 Collected: 04/26/21 17:20 Received: 04/27/21 08:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Bromochloromethane
ND
ug/L
0.50
1
04/30/21 16:39
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/30/21 16:39
75-27-4
Bromoform
ND
ug/L
0.50
1
04/30/21 16:39
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/30/21 16:39
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
04/30/21 16:39
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/30/21 16:39
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
04/30/21 16:39
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/30/21 16:39
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/30/21 16:39
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/30/21 16:39
75-00-3
Chloroform
ND
ug/L
0.50
1
04/30/21 16:39
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/30/21 16:39
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/30/21 16:39
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/30/21 16:39
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/30/21 16:39
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/30/21 16:39
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/30/21 16:39
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/30/21 16:39
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/30/21 16:39
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/30/21 16:39
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/30/21 16:39
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/30/21 16:39
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/30/21 16:39
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/30/21 16:39
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/30/21 16:39
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/30/21 16:39
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/30/21 16:39
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/30/21 16:39
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/30/21 16:39
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/30/21 16:39
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/30/21 16:39
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/30/21 16:39
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
04/30/21 16:39
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
04/30/21 16:39
108-20-3
Ethylbenzene
1.0
ug/L
0.50
1
04/30/21 16:39
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/30/21 16:39
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
04/30/21 16:39
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/30/21 16:39
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/30/21 16:39
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/30/21 16:39
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/30/21 16:39
103-65-1
Styrene
ND
ug/L
0.50
1
04/30/21 16:39
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/30/21 16:39
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/30/21 16:39
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
04/30/21 16:39
127-18-4
Toluene
ND
ug/L
0.50
1
04/30/21 16:39
108-88-3
REPORT OF LABORATORY ANALYSIS
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Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 37

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 21003
Pace Project No.: 92535202
Sample: MW-2
Lab ID: 92535202002 Collected:
04/26/21 17:20
Received: 04/27/21 08:11 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200B MSV
Analytical Method:
SM 6200B
Pace Analytical
Services - Charlotte
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/30/21 16:39
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/30/21 16:39
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/30/21 16:39
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/30/21 16:39
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/30/21 16:39
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/30/21 16:39
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/30/21 16:39
96-18-4
1,2,4-Trimethylbenzene
1.1
ug/L
0.50
1
04/30/21 16:39
95-63-6
1,3,5-Trimethylbenzene
0.78
ug/L
0.50
1
04/30/21 16:39
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/30/21 16:39
75-01-4
m&p-Xylene
2.8
ug/L
1.0
1
04/30/21 16:39
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/30/21 16:39
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
112
%
70-130
1
04/30/21 16:39
17060-07-0
4-Bromofluorobenzene (S)
91
%
70-130
1
04/30/21 16:39
460-00-4
Toluene-d8(S)
90
%
70-130
1
04/30/21 16:39
2037-26-5
Date: 05/13/2021 02:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 21003
Pace Project No.: 92535202
QC Batch: 619708
QC Batch Method: MADEP VPH
Associated Lab Samples: 92535202001, 92535202002
METHOD BLANK: 3260395
Associated Lab Samples: 92535202001, 92535202002
Parameter
Units
Aliphatic (C05-CO8)
ug/L
Aliphatic (C09-C12)
ug/L
Aromatic (C09-C10)
ug/L
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
QUALITY CONTROL DATA
Analysis Method: MADEP VPH
Analysis Description: VPH NC Water
Laboratory: Pace Analytical Services - Charlotte
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
50.0
05/11/2118:15 N2
ND
50.0
05/11/2118:15 N2
ND
50.0
05/11/2118:15 N2
99
70-130
05/11/2118:15
100
70-130
05/11/2118:15
LABORATORY CONTROL SAMPLE & LCSD:
3260396
3260397
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
276
282
92
94
70-130 2 25 N2
Aliphatic (C09-C12)
ug/L
300
316
325
105
108
70-130 3 25 N2
Aromatic (C09-C10)
ug/L
100
97.9
105
98
105
70-130 7 25 N2
4-Bromofluorobenzene (FID) (S)
%
106
105
70-130
4-Bromofluorobenzene (PID) (S)
%
104
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
QC Batch: 617289 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92535202001, 92535202002
METHOD BLANK: 3248071 Matrix: Water
Associated Lab Samples: 92535202001, 92535202002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chromium ug/L ND 5.0 04/30/2115:19
Lead ug/L ND 5.0 04/30/2115:19
LABORATORY CONTROL SAMPLE: 3248072
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chromium ug/L 500 503 101 80-120
Lead ug/L 500 474 95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3248073 3248074
MS MSD
92534954010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chromium ug/L ND 500 500 496 504 99 101 75-125 2
Lead ug/L ND 500 500 457 462 91 92 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
QC Batch: 617384 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92535202001, 92535202002
METHOD BLANK: 3248369
Associated Lab Samples: 92535202001, 92535202002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
04/30/21 11:32
1,1,1-Trichloroethane
ug/L
ND
0.50
04/30/21 11:32
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
04/30/21 11:32
1,1,2-Trichloroethane
ug/L
ND
0.50
04/30/21 11:32
1,1-Dichloroethane
ug/L
ND
0.50
04/30/21 11:32
1,1-Dichloroethene
ug/L
ND
0.50
04/30/21 11:32
1,1-Dichloropropene
ug/L
ND
0.50
04/30/21 11:32
1,2,3-Trichlorobenzene
ug/L
ND
2.0
04/30/21 11:32
1,2,3-Trichloropropane
ug/L
ND
0.50
04/30/21 11:32
1,2,4-Trichlorobenzene
ug/L
ND
2.0
04/30/21 11:32
1,2,4-Trimethylbenzene
ug/L
ND
0.50
04/30/21 11:32
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
04/30/21 11:32
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
04/30/21 11:32
1,2-Dichlorobenzene
ug/L
ND
0.50
04/30/21 11:32
1,2-Dichloroethane
ug/L
ND
0.50
04/30/21 11:32
1,2-Dichloropropane
ug/L
ND
0.50
04/30/21 11:32
1,3,5-Trimethylbenzene
ug/L
ND
0.50
04/30/21 11:32
1,3-Dichlorobenzene
ug/L
ND
0.50
04/30/21 11:32
1,3-Dichloropropane
ug/L
ND
0.50
04/30/21 11:32
1,4-Dichlorobenzene
ug/L
ND
0.50
04/30/21 11:32
2,2-Dichloropropane
ug/L
ND
0.50
04/30/21 11:32
2-Chlorotoluene
ug/L
ND
0.50
04/30/21 11:32
4-Chlorotoluene
ug/L
ND
0.50
04/30/21 11:32
Benzene
ug/L
ND
0.50
04/30/21 11:32
Bromobenzene
ug/L
ND
0.50
04/30/21 11:32
Bromochloromethane
ug/L
ND
0.50
04/30/21 11:32
Bromodichloromethane
ug/L
ND
0.50
04/30/21 11:32
Bromoform
ug/L
ND
0.50
04/30/21 11:32
Bromomethane
ug/L
ND
5.0
04/30/21 11:32
Carbon tetrachloride
ug/L
ND
0.50
04/30/21 11:32
Chlorobenzene
ug/L
ND
0.50
04/30/21 11:32
Chloroethane
ug/L
ND
1.0
04/30/21 11:32
Chloroform
ug/L
ND
0.50
04/30/21 11:32
Chloromethane
ug/L
ND
1.0
04/30/21 11:32
cis-1,2-Dichloroethene
ug/L
ND
0.50
04/30/21 11:32
cis-1,3-Dichloropropene
ug/L
ND
0.50
04/30/21 11:32
Dibromochloromethane
ug/L
ND
0.50
04/30/21 11:32
Dibromomethane
ug/L
ND
0.50
04/30/21 11:32
Dichlorodifluoromethane
ug/L
ND
0.50
04/30/21 11:32
Diisopropyl ether
ug/L
ND
0.50
04/30/21 11:32
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
METHOD BLANK: 3248369
Associated Lab Samples: 92535202001, 92535202002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
04/30/21 11:32
Hexachloro-1,3-butadiene
ug/L
ND
2.0
04/30/21 11:32
Isopropylbenzene (Cumene)
ug/L
ND
0.50
04/30/21 11:32
m&p-Xylene
ug/L
ND
1.0
04/30/21 11:32
Methyl-tert-butyl ether
ug/L
ND
0.50
04/30/21 11:32
Methylene Chloride
ug/L
ND
2.0
04/30/21 11:32
n-Butylbenzene
ug/L
ND
0.50
04/30/21 11:32
n-Propylbenzene
ug/L
ND
0.50
04/30/21 11:32
Naphthalene
ug/L
ND
2.0
04/30/21 11:32
o-Xylene
ug/L
ND
0.50
04/30/21 11:32
sec-Butylbenzene
ug/L
ND
0.50
04/30/21 11:32
Styrene
ug/L
ND
0.50
04/30/21 11:32
tert-Butyl benzene
ug/L
ND
0.50
04/30/21 11:32
Tetrachloroethene
ug/L
ND
0.50
04/30/21 11:32
Toluene
ug/L
ND
0.50
04/30/21 11:32
trans-1,2-Dichloroethene
ug/L
ND
0.50
04/30/21 11:32
trans- 1,3-Dichloropropene
ug/L
ND
0.50
04/30/21 11:32
Trichloroethene
ug/L
ND
0.50
04/30/21 11:32
Trichlorofluoromethane
ug/L
ND
1.0
04/30/21 11:32
Vinyl chloride
ug/L
ND
1.0
04/30/21 11:32
1,2-Dichloroethane-d4 (S)
%
109
70-130
04/30/21 11:32
4-Bromofluorobenzene (S)
%
93
70-130
04/30/21 11:32
Toluene-d8 (S)
%
101
70-130
04/30/21 11:32
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3248370
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
52.2
104
60-140
1,1,1-Trichloroethane
ug/L
50
54.1
108
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
49.2
98
60-140
1,1,2-Trichloroethane
ug/L
50
50.2
100
60-140
1,1-Dichloroethane
ug/L
50
53.2
106
60-140
1,1-Dichloroethene
ug/L
50
57.0
114
60-140
1,1-Dichloropropene
ug/L
50
54.7
109
60-140
1,2,3-Trichlorobenzene
ug/L
50
45.0
90
60-140
1,2,3-Trichloropropane
ug/L
50
49.4
99
60-140
1,2,4-Trichlorobenzene
ug/L
50
47.2
94
60-140
1,2,4-Trimethylbenzene
ug/L
50
47.9
96
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
53.1
106
60-140
1,2-Dibromoethane (EDB)
ug/L
50
52.9
106
60-140
1,2-Dichlorobenzene
ug/L
50
47.7
95
60-140
1,2-Dichloroethane
ug/L
50
46.3
93
60-140
1,2-Dichloropropane
ug/L
50
51.7
103
60-140
1,3,5-Trimethylbenzene
ug/L
50
49.0
98
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
LABORATORY CONTROL SAMPLE:
Parameter
3248370
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
49.0
98
60-140
1,3-Dichloropropane
ug/L
50
54.6
109
60-140
1,4-Dichlorobenzene
ug/L
50
48.7
97
60-140
2,2-Dichloropropane
ug/L
50
55.6
111
60-140
2-Chlorotoluene
ug/L
50
50.0
100
60-140
4-Chlorotoluene
ug/L
50
49.4
99
60-140
Benzene
ug/L
50
54.5
109
60-140
Bromobenzene
ug/L
50
51.8
104
60-140
Bromochloromethane
ug/L
50
54.1
108
60-140
Bromodichloromethane
ug/L
50
46.8
94
60-140
Bromoform
ug/L
50
55.6
111
60-140
Bromomethane
ug/L
50
47.3
95
60-140
Carbon tetrachloride
ug/L
50
55.3
111
60-140
Chlorobenzene
ug/L
50
51.7
103
60-140
Chloroethane
ug/L
50
40.1
80
60-140
Chloroform
ug/L
50
46.0
92
60-140
Chloromethane
ug/L
50
43.5
87
60-140
cis-1,2-Dichloroethene
ug/L
50
54.2
108
60-140
cis-1,3-Dichloropropene
ug/L
50
51.8
104
60-140
Dibromochloromethane
ug/L
50
58.3
117
60-140
Dibromomethane
ug/L
50
49.9
100
60-140
Dichlorodifluoromethane
ug/L
50
42.2
84
60-140
Diisopropyl ether
ug/L
50
51.1
102
60-140
Ethylbenzene
ug/L
50
49.6
99
60-140
Hexachloro-1,3-butadiene
ug/L
50
47.2
94
60-140
Isopropylbenzene(Cumene)
ug/L
50
48.8
98
60-140
m&p-Xylene
ug/L
100
100
100
60-140
Methyl-tert-butyl ether
ug/L
50
48.0
96
60-140
Methylene Chloride
ug/L
50
49.2
98
60-140
n-Butylbenzene
ug/L
50
48.3
97
60-140
n-Propylbenzene
ug/L
50
49.9
100
60-140
Naphthalene
ug/L
50
44.9
90
60-140
o-Xylene
ug/L
50
48.5
97
60-140
sec-Butylbenzene
ug/L
50
48.6
97
60-140
Styrene
ug/L
50
51.2
102
60-140
tert-Butyl benzene
ug/L
50
41.8
84
60-140
Tetrachloroethene
ug/L
50
50.1
100
60-140
Toluene
ug/L
50
49.2
98
60-140
trans-1,2-Dichloroethene
ug/L
50
53.4
107
60-140
trans- 1,3-Dichloropropene
ug/L
50
52.0
104
60-140
Trichloroethene
ug/L
50
51.5
103
60-140
Trichlorofluoromethane
ug/L
50
42.9
86
60-140
Vinyl chloride
ug/L
50
43.2
86
60-140
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
96
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3248371
3248372
MS
MSD
92535061007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
5000
5000
5290
5350
106
107
60-140
1
1,1,1-Trichloroethane
ug/L
ND
5000
5000
5440
5600
109
112
60-140
3
1,1,2,2-Tetrachloroethane
ug/L
ND
5000
5000
5070
5350
101
107
60-140
5
1,1,2-Trichloroethane
ug/L
ND
5000
5000
5230
5150
105
103
60-140
2
1,1-Dichloroethane
ug/L
ND
5000
5000
5440
5620
109
112
60-140
3
1,1-Dichloroethene
ug/L
ND
5000
5000
6150
6240
123
125
60-140
1
1,1-Dichloropropene
ug/L
ND
5000
5000
5650
5750
113
115
60-140
2
1,2,3-Trichlorobenzene
ug/L
ND
5000
5000
4640
4900
93
98
60-140
6
1,2,3-Trichloropropane
ug/L
ND
5000
5000
5120
5250
102
105
60-140
2
1,2,4-Trichlorobenzene
ug/L
ND
5000
5000
4830
5010
97
100
60-140
4
1,2,4-Trimethylbenzene
ug/L
3200
5000
5000
8350
8430
103
104
60-140
1
1,2-Dibromo-3-chloropropane
ug/L
ND
5000
5000
5030
5300
101
106
60-140
5
1,2-Dibromoethane (EDB)
ug/L
ND
5000
5000
5400
5550
108
111
60-140
3
1,2-Dichlorobenzene
ug/L
ND
5000
5000
5050
5170
101
103
60-140
2
1,2-Dichloroethane
ug/L
ND
5000
5000
4780
4880
96
98
60-140
2
1,2-Dichloropropane
ug/L
ND
5000
5000
5350
5410
107
108
60-140
1
1,3,5-Trimethylbenzene
ug/L
ND
5000
5000
6030
6100
121
122
60-140
1
1,3-Dichlorobenzene
ug/L
ND
5000
5000
5140
5480
103
110
60-140
6
1,3-Dichloropropane
ug/L
ND
5000
5000
5680
5670
114
113
60-140
0
1,4-Dichlorobenzene
ug/L
ND
5000
5000
5120
5250
102
105
60-140
3
2,2-Dichloropropane
ug/L
ND
5000
5000
5420
5630
108
113
60-140
4
2-Chlorotoluene
ug/L
ND
5000
5000
5430
5800
109
116
60-140
7
4-Chlorotoluene
ug/L
ND
5000
5000
5270
5410
105
108
60-140
3
Benzene
ug/L
20300
5000
5000
25600
25200
107
98
60-140
2
Bromobenzene
ug/L
ND
5000
5000
5390
5500
108
110
60-140
2
Bromochloromethane
ug/L
ND
5000
5000
5360
5430
107
109
60-140
1
Bromodichloromethane
ug/L
ND
5000
5000
4790
4820
96
96
60-140
1
Bromoform
ug/L
ND
5000
5000
5340
5470
107
109
60-140
2
Bromomethane
ug/L
ND
5000
5000
5350
5360
107
107
60-140
0
Carbon tetrachloride
ug/L
ND
5000
5000
5330
5170
107
103
60-140
3
Chlorobenzene
ug/L
ND
5000
5000
5400
5510
108
110
60-140
2
Chloroethane
ug/L
ND
5000
5000
5230
5360
105
107
60-140
2
Chloroform
ug/L
ND
5000
5000
4510
4730
90
95
60-140
5
Chloromethane
ug/L
ND
5000
5000
4620
4580
92
92
60-140
1
cis-1,2-Dichloroethene
ug/L
ND
5000
5000
5320
5430
106
109
60-140
2
cis-1,3-Dichloropropene
ug/L
ND
5000
5000
5140
5160
103
103
60-140
0
Dibromochloromethane
ug/L
ND
5000
5000
5840
5930
117
119
60-140
2
Dibromomethane
ug/L
ND
5000
5000
5250
5040
105
101
60-140
4
Dichlorodifluoromethane
ug/L
ND
5000
5000
4500
4490
90
90
60-140
0
Diisopropyl ether
ug/L
ND
5000
5000
4960
5260
99
105
60-140
6
Ethylbenzene
ug/L
4090
5000
5000
9560
9570
109
110
60-140
0
Hexachloro-1,3-butadiene
ug/L
ND
5000
5000
5480
5470
110
109
60-140
0
Isopropylbenzene(Cumene)
ug/L
146
5000
5000
5410
5530
105
108
60-140
2
m&p-Xylene
ug/L
14100
10000
10000
25400
25900
113
117
60-140
2
Methyl-tert-butyl ether
ug/L
ND
5000
5000
4920
5460
96
107
60-140
10
Methylene Chloride
ug/L
ND
5000
5000
5130
5700
103
114
60-140
11
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3248371
3248372
MS
MSD
92535061007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
5000
5000
5390
5360
106
105
60-140
1
n-Propylbenzene
ug/L
ND
5000
5000
5760
5910
115
118
60-140
3
Naphthalene
ug/L
ND
5000
5000
4790
5270
87
97
60-140
10
o-Xylene
ug/L
6220
5000
5000
11600
11800
107
112
60-140
2
sec-Butylbenzene
ug/L
ND
5000
5000
5450
5460
109
109
60-140
0
Styrene
ug/L
ND
5000
5000
5300
5440
106
109
60-140
3
tert-Butyl benzene
ug/L
ND
5000
5000
4560
4670
91
93
60-140
2
Tetrachloroethene
ug/L
ND
5000
5000
5490
5570
110
111
60-140
1
Toluene
ug/L
42700
5000
5000
44200
43100
31
9
60-140
3 M1
trans-1,2-Dichloroethene
ug/L
ND
5000
5000
5720
6170
114
123
60-140
8
trans- 1,3-Dichloropropene
ug/L
ND
5000
5000
5150
5110
103
102
60-140
1
Trichloroethene
ug/L
195
5000
5000
5610
5850
108
113
60-140
4
Trichlorofluoromethane
ug/L
ND
5000
5000
5630
5540
113
111
60-140
1
Vinyl chloride
ug/L
ND
5000
5000
4550
4510
91
90
60-140
1
1,2-Dichloroethane-d4 (S)
%
101
105
70-130
4-Bromofluorobenzene (S)
%
97
100
70-130
Toluene-d8(S)
%
98
94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
QC Batch: 617047 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92535202001, 92535202002
METHOD BLANK: 3246569
Associated Lab Samples: 92535202001, 92535202002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
04/30/21 08:22
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
04/30/21 08:22
2,4,6-Trichlorophenol
ug/L
ND
10.0
04/30/21 08:22
2,4-Dichlorophenol
ug/L
ND
5.0
04/30/21 08:22
2,4-Dimethylphenol
ug/L
ND
10.0
04/30/21 08:22
2,4-Dinitrophenol
ug/L
ND
50.0
04/30/21 08:22
2,4-Dinitrotoluene
ug/L
ND
5.0
04/30/21 08:22
2,6-Dinitrotoluene
ug/L
ND
5.0
04/30/21 08:22
2-Chloronaphthalene
ug/L
ND
5.0
04/30/21 08:22
2-Chlorophenol
ug/L
ND
5.0
04/30/21 08:22
2-Nitrophenol
ug/L
ND
5.0
04/30/21 08:22
3,3'-Dichlorobenzidine
ug/L
ND
10.0
04/30/21 08:22
4,6-Dinitro-2-methyl phenol
ug/L
ND
10.0
04/30/21 08:22
4-Bromophenylphenyl ether
ug/L
ND
5.0
04/30/21 08:22
4-ChIoro-3-methyl phenol
ug/L
ND
5.0
04/30/21 08:22
4-Chlorophenylphenyl ether
ug/L
ND
5.0
04/30/21 08:22
4-Nitrophenol
ug/L
ND
10.0
04/30/21 08:22
Acenaphthene
ug/L
ND
5.0
04/30/21 08:22
Acenaphthylene
ug/L
ND
5.0
04/30/21 08:22
Anthracene
ug/L
ND
5.0
04/30/21 08:22
Benzo(a)anthracene
ug/L
ND
5.0
04/30/21 08:22
Benzo(a)pyrene
ug/L
ND
5.0
04/30/21 08:22
Benzo(b)fluoranthene
ug/L
ND
5.0
04/30/21 08:22
Benzo(g,h,i)perylene
ug/L
ND
5.0
04/30/21 08:22
Benzo(k)fluoranthene
ug/L
ND
5.0
04/30/21 08:22
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
04/30/21 08:22
bis(2-Chloroethyl) ether
ug/L
ND
5.0
04/30/21 08:22
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
04/30/21 08:22
Butylbenzylphthalate
ug/L
ND
5.0
04/30/21 08:22
Chrysene
ug/L
ND
5.0
04/30/21 08:22
Di-n-butylphthalate
ug/L
ND
5.0
04/30/21 08:22
Di-n-octylphthalate
ug/L
ND
5.0
04/30/21 08:22
Dibenz(a,h)anthracene
ug/L
ND
5.0
04/30/21 08:22
Diethylphthalate
ug/L
ND
5.0
04/30/21 08:22
Dimethylphthalate
ug/L
ND
5.0
04/30/21 08:22
Fluoranthene
ug/L
ND
5.0
04/30/21 08:22
Fluorene
ug/L
ND
5.0
04/30/21 08:22
Hexachloro-1,3-butadiene
ug/L
ND
5.0
04/30/21 08:22
Hexachlorobenzene
ug/L
ND
5.0
04/30/21 08:22
Hexachlorocyclopentadiene
ug/L
ND
10.0
04/30/21 08:22
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
METHOD BLANK: 3246569
Associated Lab Samples: 92535202001, 92535202002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloroethane
ug/L
ND
5.0
04/30/21 08:22
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
04/30/21 08:22
Isophorone
ug/L
ND
10.0
04/30/21 08:22
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
04/30/21 08:22
N-Nitrosodimethylamine
ug/L
ND
5.0
04/30/21 08:22
N-Nitrosodiphenylamine
ug/L
ND
10.0
04/30/21 08:22
Naphthalene
ug/L
ND
5.0
04/30/21 08:22
Nitrobenzene
ug/L
ND
5.0
04/30/21 08:22
Pentachlorophenol
ug/L
ND
10.0
04/30/21 08:22
Phenanthrene
ug/L
ND
5.0
04/30/21 08:22
Phenol
ug/L
ND
5.0
04/30/21 08:22
Pyrene
ug/L
ND
5.0
04/30/21 08:22
2,4,6-Tribromophenol (S)
%
76
10-137
04/30/21 08:22
2-Fluorobiphenyl (S)
%
80
15-120
04/30/21 08:22
2-Fluorophenol(S)
%
53
10-120
04/30/21 08:22
Nitrobenzene-d5 (S)
%
87
10-120
04/30/21 08:22
Phenol-d6 (S)
%
47
10-120
04/30/21 08:22
Terphenyl-d14 (S)
%
104
11-131
04/30/21 08:22
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3246570
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
33.5
67
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
40.2
80
36-166
2,4,6-Trichlorophenol
ug/L
50
30.5
61
37-144
2,4-Dichlorophenol
ug/L
50
40.1
80
1-191
2,4-Dimethylphenol
ug/L
50
44.4
89
32-119
2,4-Dinitrophenol
ug/L
250
85.0
34
1-181
2,4-Dinitrotoluene
ug/L
50
51.9
104
39-139
2,6-Dinitrotoluene
ug/L
50
51.3
103
50-158
2-Chloronaphthalene
ug/L
50
39.2
78
60-118
2-Chlorophenol
ug/L
50
34.1
68
23-134
2-Nitrophenol
ug/L
50
35.2
70
29-182
3,3'-Dichlorobenzidine
ug/L
100
116
116
1-262
4,6-Dinitro-2-methyl phenol
ug/L
100
45.8
46
1-181
4-Bromophenylphenyl ether
ug/L
50
54.3
109
53-127
4-Chloro-3-methylphenol
ug/L
100
88.2
88
22-147
4-Chlorophenylphenyl ether
ug/L
50
45.8
92
25-158
4-Nitrophenol
ug/L
250
60.8
24
1-132
Acenaphthene
ug/L
50
43.6
87
47-145
Acenaphthylene
ug/L
50
45.4
91
33-145
Anthracene
ug/L
50
50.9
102
1-166
Benzo(a)anthracene
ug/L
50
55.2
110
33-143
Benzo(a)pyrene
ug/L
50
54.6
109
17-163
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
LABORATORY CONTROL SAMPLE:
Parameter
3246570
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Benzo(b)fluoranthene
ug/L
50
58.5
117
24-159
Benzo(g,h,i)perylene
ug/L
50
51.8
104
1-219
Benzo(k)fluoranthene
ug/L
50
56.2
112
11-162
bis(2-Chloroethoxy)methane
ug/L
50
43.6
87
33-184
bis(2-Chloroethyl) ether
ug/L
50
43.3
87
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
62.2
124
8-158
Butylbenzylphthalate
ug/L
50
62.8
126
1-152
Chrysene
ug/L
50
52.6
105
17-168
Di-n-butylphthalate
ug/L
50
55.7
111
1-118
Di-n-octylphthalate
ug/L
50
61.1
122
4-146
Dibenz(a,h)anthracene
ug/L
50
52.2
104
1-227
Diethylphthalate
ug/L
50
51.4
103
1-114
Dimethylphthalate
ug/L
50
48.3
97
1-112
Fluoranthene
ug/L
50
52.9
106
26-137
Fluorene
ug/L
50
47.0
94
59-121
Hexachloro-1,3-butadiene
ug/L
50
30.9
62
24-116
Hexachlorobenzene
ug/L
50
48.0
96
1-152
Hexachlorocyclopentadiene
ug/L
50
34.8
70
25-150
Hexachloroethane
ug/L
50
28.2
56
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
51.7
103
1-171
Isophorone
ug/L
50
44.3
89
21-196
N-Nitroso-di-n-propylamine
ug/L
50
45.9
92
1-230
N-Nitrosodimethylamine
ug/L
50
31.0
62
25-150
N-Nitrosodiphenylamine
ug/L
50
49.6
99
25-150
Naphthalene
ug/L
50
37.3
75
21-133
Nitrobenzene
ug/L
50
39.0
78
35-180
Pentachlorophenol
ug/L
100
58.1
58
14-176
Phenanthrene
ug/L
50
49.6
99
54-120
Phenol
ug/L
50
25.7
51
5-112
Pyrene
ug/L
50
57.8
116
52-115 L1
2,4,6-Tribromophenol (S)
%
103
10-137
2-Fluorobiphenyl (S)
%
85
15-120
2-Fluorophenol(S)
%
43
10-120
Nitrobenzene-d5 (S)
%
85
10-120
Phenol-d6 (S)
%
47
10-120
Terphenyl-d14 (S)
%
120
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3246571
3246572
MS
MSD
92535607003 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/L
ND 50
50
27.5
23.9
55
48
44-142
14
2,2'-Oxybis(1-chloropropane)
ug/L
ND 50
50
27.9
23.9
56
48
36-166
16
2,4,6-Trichlorophenol
ug/L
ND 50
50
41.8
37.5
84
75
37-144
11
2,4-Dichlorophenol
ug/L
ND 50
50
40.5
35.7
81
71
1-191
13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3246571
3246572
MS
MSD
92535607003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
2,4-Dimethylphenol
ug/L
ND
50
50
40.8
35.5
82
71
32-119
14
2,4-Dinitrophenol
ug/L
ND
250
250
190
220
76
88
1-181
14
2,4-Dinitrotoluene
ug/L
ND
50
50
41.7
38.3
83
77
39-139
9
2,6-Dinitrotoluene
ug/L
ND
50
50
41.6
38.4
83
77
50-158
8
2-Chloronaphthalene
ug/L
ND
50
50
37.0
33.2
74
66
60-118
11
2-Chlorophenol
ug/L
ND
50
50
32.4
28.7
65
57
23-134
12
2-Nitrophenol
ug/L
ND
50
50
37.4
32.9
75
66
29-182
13
3,3'-Dichlorobenzidine
ug/L
ND
100
100
101
85.1
101
85
1-262
17
4,6-Dinitro-2-methyl phenol
ug/L
ND
100
100
97.5
89.8
98
90
1-181
8
4-Bromophenylphenyl ether
ug/L
ND
50
50
47.8
41.8
96
84
53-127
13
4-Chloro-3-methylphenol
ug/L
ND
100
100
80.2
72.4
80
72
22-147
10
4-Chlorophenylphenyl ether
ug/L
ND
50
50
41.3
37.9
83
76
25-158
9
4-Nitrophenol
ug/L
ND
250
250
191
187
77
75
1-132
3
Acenaphthene
ug/L
ND
50
50
40.1
36.2
80
72
47-145
10
Acenaphthylene
ug/L
ND
50
50
40.2
36.6
80
73
33-145
9
Anthracene
ug/L
ND
50
50
44.9
39.4
90
79
1-166
13
Benzo(a)anthracene
ug/L
ND
50
50
49.6
43.9
99
88
33-143
12
Benzo(a)pyrene
ug/L
ND
50
50
50.2
44.5
100
89
17-163
12
Benzo(b)fluoranthene
ug/L
ND
50
50
53.5
48.3
107
97
24-159
10
Benzo(g,h,i)perylene
ug/L
ND
50
50
51.5
45.9
103
92
1-219
11
Benzo(k)fluoranthene
ug/L
ND
50
50
49.4
45.0
99
90
11-162
9
bis(2-Chloroethoxy)methane
ug/L
ND
50
50
37.3
33.1
75
66
33-184
12
bis(2-Chloroethyl) ether
ug/L
ND
50
50
34.1
30.3
68
61
12-158
12
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
50
49.2
42.8
98
86
8-158
14
Butylbenzylphthalate
ug/L
ND
50
50
51.1
44.3
102
89
1-152
14
Chrysene
ug/L
ND
50
50
49.3
43.7
99
87
17-168
12
Di-n-butylphthalate
ug/L
ND
50
50
45.9
41.5
92
83
1-118
10
Di-n-octylphthalate
ug/L
ND
50
50
49.3
43.9
99
88
4-146
12
Dibenz(a,h)anthracene
ug/L
ND
50
50
51.1
46.3
102
93
1-227
10
Diethylphthalate
ug/L
ND
50
50
43.3
39.4
87
79
1-114
9
Dimethylphthalate
ug/L
ND
50
50
41.6
37.8
83
76
1-112
9
Fluoranthene
ug/L
ND
50
50
46.7
42.3
93
85
26-137
10
Fluorene
ug/L
ND
50
50
41.3
37.6
83
75
59-121
9
Hexachloro-1,3-butadiene
ug/L
ND
50
50
24.5
20.7
49
41
24-116
17
Hexachlorobenzene
ug/L
ND
50
50
44.4
39.0
89
78
1-152
13
Hexachlorocyclopentadiene
ug/L
ND
50
50
31.2
27.0
62
54
25-150
15
Hexachloroethane
ug/L
ND
50
50
17.8
14.5
36
29
40-113
20 M1
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
52.1
46.6
104
93
1-171
11
Isophorone
ug/L
ND
50
50
37.1
32.6
74
65
21-196
13
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
35.2
30.5
70
61
1-230
14
N-Nitrosodimethylamine
ug/L
ND
50
50
29.9
27.2
60
54
25-150
10
N-Nitrosodiphenylamine
ug/L
ND
50
50
43.6
37.0
87
74
25-150
16
Naphthalene
ug/L
ND
50
50
31.8
27.2
64
54
21-133
16
Nitrobenzene
ug/L
ND
50
50
34.0
29.4
68
59
35-180
14
Pentachlorophenol
ug/L
ND
100
100
96.2
86.5
96
87
14-176
11
Phenanthrene
ug/L
ND
50
50
44.3
38.9
89
78
54-120
13
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3246571
3246572
MS
MSD
92535607003 Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits RPD Qual
Phenol
ug/L
ND 50
50 31.0
27.6
62
55
5-112 12
Pyrene
ug/L
ND 50
50 48.1
40.9
96
82
52-115 16
2,4,6-Tribromophenol (S)
%
106
92
10-137
2-Fluorobiphenyl (S)
%
73
63
15-120
2-Fluorophenol(S)
%
57
49
10-120
Nitrobenzene-d5(S)
%
70
60
10-120
Phenol-d6 (S)
%
57
50
10-120
Terphenyl-d14 (S)
%
100
84
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 21003
Pace Project No.: 92535202
QC Batch: 617337 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92535202001, 92535202002
METHOD BLANK: 3248164
Matrix:
Water
Associated Lab Samples:
92535202001, 92535202002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Aliphatic (C09-C18)
ug/L
ND
100
05/03/21 12:32
N2
Aliphatic (C19-C36)
ug/L
ND
100
05/03/21 12:32
N2
Aromatic (C11-C22)
ug/L
ND
100
05/03/21 12:32
N2
1-Chlorooctadecane (S)
%
30
40-140
05/03/21 12:32
SO
2-Bromonaphthalene (S)
%
93
40-140
05/03/21 12:32
2-Fluorobiphenyl (S)
%
88
40-140
05/03/21 12:32
o-Terphenyl(S)
%
70
40-140
05/03/21 12:32
LABORATORY CONTROL SAMPLE & LCSD:
3248165
3248166
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qualifiers
Aliphatic (C09-C18)
ug/L
300
177
182
59
61
40-140
3 50 N2
Aliphatic (C19-C36)
ug/L
400
309
303
77
76
40-140
2 50 N2
Aromatic (C11-C22)
ug/L
850
601
660
71
78
40-140
9 50 N2
1-Chlorooctadecane (S)
%
34
35
40-140
SO
2-Bromonaphthalene (S)
%
88
86
40-140
2-Fluorobiphenyl (S)
%
87
84
40-140
o-Terphenyl(S)
%
74
81
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 37

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: 21003
Pace Project No.: 92535202
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
P2 Re -extraction or re -analysis could not be performed due to insufficient sample amount.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
21003
92535202
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92535202001
MW-1
MADEP EPH
617337
MADEP EPH
617691
92535202002
MW-2
MADEP EPH
617337
MADEP EPH
617691
92535202001
MW-1
MADEP VPH
619708
92535202002
MW-2
MADEP VPH
619708
92535202001
MW-1
EPA 3010A
617289
EPA 6010D
617316
92535202002
MW-2
EPA 3010A
617289
EPA 6010D
617316
92535202001
MW-1
EPA 625.1
617047
EPA 625.1
617343
92535202002
MW-2
EPA 625.1
617047
EPA 625.1
617343
92535202001
MW-1
SM 6200B
617384
92535202002
MW-2
SM 6200B
617384
Date: 05/13/2021 02:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 34 of 37

Document Name:
Document Revised: October 28, 2020
�-80Analyfical'
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Sample Condition Client fName: ,� Project #: WO# : 92Jr35202
Courler: ❑Fed Ex ❑LIPS ❑USPS Client 1111111111111111111111
❑ Commercial ❑Pace ❑Other: g2535202
f
Custody Seal Present? Des ao Seals intact? [:]Yes t�;ko , / C
Date/Initials Person Examining Contents: V1
Packing Material: ❑Bubble/�W1rap �ubble Bags []None ❑ Other Biological Tissue Frozen?
ThermoIR Gun 1U: L1 r "f ❑Yes ❑No�V/A
7Wet ❑Blue [)None
Type of ice:
Correction Factor:
Cooler Teri Add/Subtract {'C) O.O'C Temp should be above freezing to VC
/� 113 [:]Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C): � - has begun
USDA Regulated 5oil (JE� N/A, water sample)
Did sample originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (i,r µ`},e�rnationally,
nYes TNo W—H � 4 0� ,t,, D�� D MV— 111Af-
Cam ments/Discrepa ncy:
Chain of Custody Present?
Yes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
[-]No
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
[-]Yes
No
N/A
3.
Rush Turn Around Time Requested?
❑Yes
No
❑N/A
4.
Sufficient Volume?
-yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
Yes
❑rvo
[]No
❑N/A
❑N/A
6.
Containers Intact?
yes
[]No
❑N/A
7.
Dissolved analysis; Samples Field Filtered?
❑Yes
[]No
NIA
9.
Sample labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
'MYes
J i
v/ !
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
SUo
[]NIA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
-Baio
`0 o
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Lot ID of split containers:
Field Data Required? ❑Yes []No
Project Manager SCURF Review:
Date:
Project Manager SRF Review: Date:
Page 35 of 37

Document Name:
Document Revised: October 28, 2020
�aceAnalyiical'
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Project # Wo## : g25352m2
PM: KLH1 Due Date: @5/06/21
CLIENT: 92—Lighthcus
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--L\N
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 4
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
out of hold, incorrect preservative, out of temp, incorrect containers.
Page 36 of 37

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Page 37 of 37

Beverly, Trudy
From: Beverly, Trudy
Sent: Friday, May 21, 2021 3:10 PM
To: [e-mail]
Cc: Bell, Wes
Subject: RE: [External] Isgett Distributers used oil spill-Hilbish Ford, Kannapolis, NC (1-8-21)
Received.
Thank you,
Trudy
OPIF 5Qi i K. M
D�. E
M n+
mental 4w ��
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httos://dea.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-mans
File Review Procedures:
hops://deq.ne. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
bit.ps://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htti)s:Hfiles.ne.izov/ncdea[Waste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.l)df
https:Hfiles.nc.gov/ncdeq/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: [e-mail] [mailto:[e-mail]]
Sent: Friday, May 21, 2021 1:14 PM
To: Beverly, Trudy <[e-mail]>
Cc: Bell, Wes <[e-mail]>
Subject: [External] Isgett Distributers used oil spill-Hilbish Ford, Kannapolis, NC (1-8-21)
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Hi Trudy
The report for this spill cleanup is attached. Let me know if you have questions.
Thanks
Steve
Steven B. Lucas, L.G.

Environmental Geologist
Lighthouse Technical, P.C.
PO Box 1379
Huntersville, North Carolina 28070
704-237-4209 Office
704-439-7439 Cell
www.lighthousetechcorp.com