1101_Buncombe_MSWLF_April21GW_FID1596442_20210812

DEN
R USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Bunnell-Lammons Engineering
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Andrew W. Alexander
E-mail: andy.alexander(cDblecorp.com
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Id Buncombe County Landfill 2726 Riverside Drive, Woodfin, NC, 28804 1101-MSWLF .1600 April 28-29, 2021
1979
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑ Detection Monitoring ❑X Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data El
water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Andrew W. Alexander, PG RSM Consulting Hydrogeologist 864-288-1265
Facility Representative Name (Print) Title (Area Code) Telephone Number
�� w a• �E,o•,....=a•d,a ®e,•o.owm, 08-03-2021
Signature Date
6004 Ponders Court, Greenville, SC, 29615
Facility Representative Address
C-284 & C-1538
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
Affix NC Licensed/ Professional Geologist Seal
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REPORT OF WATER QUALITY
SAMPLING AND ANALYSIS
1st SEMI—ANNUAL
EVENT 2021
OLD BUNCOMBE COUNTY LANDFILL
WOODFIN, NORTH CAROLINA
DWM Permit Number 1101-MSWLF-1979
DWR UIC Permit No. WI0100353
Prepared For:
Buncombe County, North Carolina
BLE Project Number J21-14175-05
August 3, 2021
BLE North Carolina Business Licenses C-284 & C-1538
IM 13UNNELL
M LAMMONS
ENGINEERING
6004 Ponders Court I Greenville, 5C 29615
864-288.1265 A 864,286.4330 0 info@hle[orp.com
BLECORMOM

� LAMM(INS
ENGINEERING
August 3, 2021
Buncombe County Solid Waste Department
81 Panther Branch Road
Alexander, North Carolina 28701
Attention: Ms. Kristy Smith
Subject: Report of Water Quality Sampling and Analysis
1" Semi -Annual Event 2021
Old Buncombe County Landfill
Woodfin, North Carolina
DWM Permit Number 1101-MSWLF-1979
DWR UIC Permit No. W10100353
BLE Project Number J21-14175-05
Dear Ms. Smith:
Pursuant to Buncombe County authorization of Bunnell-Lammons Engineering, Inc. (BLE) Proposal Number
J21-14175-05, dated January 15, 2021, BLE has prepared this report of the groundwater and surface water
sampling and laboratory analysis for the 1 s1 semi-annual sampling event of 2021 at the Old Buncombe County
Landfill. Consistent with the North Carolina Division of Waste Management (DWM) — Solid Waste Section
(SWS) and the North Carolina Division of Water Resources (DWR) approved monitoring program, sampling
and analysis will be conducted twice in 2021. This report contains the information required by both the DWM
and DWR to document the sampling and analysis activities for the lst semi-annual sampling event of 2021 in
the State's permanent project record.
Sincerely,
BUNNELL LAMMONs ENGINEERING INC.
Ril . Blais, .LT.
Staff Hydrogeologist
cc: Ms. Jaclynne Drummond — DWM-ARO
Mr. Brett Laverty, P.G. — DWR-ARO
Mr. Michael Rogers, P.G. — DWR-CO
Atel
Andrew W. Ale der, P.G., RSM
Senior Hydrogeologist
Registered, NC #1475
Ilblegvlsvrllsolidwasteprojectslbuncombe county closed lf, ncU4175-05 spring 2021 semi reportlold bclf 1101-mswlf--1979 202121st semi-annual
14175-05.docx
6004 Ponders Court, Greenville, SC 29615 ( H!54.28B.1265 a B64.288.4430 045info@hleMrp com
6LECORP.COM

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Old Buncombe County Landfill — Woodfin, North Carolina August 3, 2021
Report of Groundwater Sampling and Analysis — Is'Semi-Annual Event 2021 BLE Project No. J21-14175-05
TABLE OF CONTENTS
1.0 PROJECT INFORMATION........................................................................................................1
2.0 FIELD ACTIVITIES, SAMPLING, AND ANALYSIS.............................................................1
3.0 GROUNDWATER FLOW........................................................................................................... 2
4.0 RESULTS....................................................................................................................................... 2
4.1 Groundwater.................................................................................................................................... 2
4.2 Surface Water.................................................................................................................................. 3
4.3 Geochemical Parameters for Monitored Natural Attenuation......................................................... 4
5.0 CONCLUSIONS AND RECOMMENDATIONS....................................................................... 4
6.0 QUALIFICATIONS OF REPORT.............................................................................................. 4
7.0 CLOSING.......................................................................................................................................4
Tables
Table 1
SWS Approved Groundwater Sampling and Analysis Matrix
Table 2
SWS Approved Surface Water Sampling and Analysis Matrix
Table 3
Well Construction and Monitoring Well Data
Table 4
Groundwater VOCs
Table 5
Groundwater Field Parameters and Total Metals
Table 6
Surface Water VOCs
Table 7
Surface Water Field Parameters and Total Metals
Table 8
Groundwater Transects for Remedial
Table 9
Groundwater Geochemical Parameters for MNA
Figures
Figure 1
Site Location Map
Figure 2
Groundwater Elevation Contour Map — April 27, 2021
Appendices
Appendix A Field Sampling Logs — Pace Analytical Services, LLC.
Appendix B Laboratory Analytical Data — Pace Analytical Services, LLC.
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Old Buncombe County Landfill — Woodfin, North Carolina August 3, 2021
Report of Groundwater Sampling and Analysis — Is'Semi-Annual Event 2021 BLE Project No. J21-14175-05
1.0 PROJECT INFORMATION
Buncombe County provides post -closure care for the Pre -Subtitle D MSWLF (unlined) located at 2726
Riverside Drive, Woodfin, North Carolina (Figure 1). The county operated the facility as a municipal solid
waste (MSW), industrial solid waste (ISW), and construction and demolition (C&D) landfill. The landfill is
separated into four (4) separate waste areas labeled A through D. Waste areas A, B, and C stopped receiving
waste before October 9, 1991 and waste area D stopped receiving waste on September 27, 1997.
Groundwater and surface water monitoring is performed at the site in accordance with a DWM approved
Corrective Action Plan (CAP) dated September 3, 2014 [DIN 21838 (SCS Engineers File No 09204072.06)]
and a DWM approved Request for Reduction of MNA Parameters dated November 30, 2016 [DIN 27144
(SCS Engineers File No 09204072.14)]. The facility requires semi-annual groundwater and surface water
monitoring and reporting in accordance with the CAP, et seq. Prior to the second semi-annual sampling event
of 2020, BLE submitted (on behalf of Buncombe County) the Report of 1,4-Dioxane Sampling and Analysis
November 2018 to April 2020 dated September 1, 2020 [FID 145059] which was approved by the DWM and
updated the groundwater and surface water matrix.
As part of the correction action at the facility, Buncombe County applied for, and was granted a permit for
subsurface injection of materials for enhanced bioremediation of VOCs in groundwater. The Underground
Injection Control (UIC) Permit (No W10100353) was transmitted by the DWR on September 11, 2015. The
permit issue date was September 15, 2015. The permit was renewed on September 21, 2020 and expires on
August 31, 2025 (effective dates).
The UIC permit requires groundwater monitoring and reporting. We understand that this semi-annual
monitoring report prepared as part of the DWM approved sampling and analysis matrix is sufficient to meet
the monitoring requirements of the UIC permit.
The active groundwater monitoring network for the Closed Buncombe County Landfill consists of one (1)
upgradient (background) well and twenty-three (23) downgradient (compliance, performance, and sentinel)
wells. There are a total of fourteen (14) additional wells that are considering inactive for sampling purposes
and are used for collecting water levels only (Table 1).
Five (5) active surface water monitoring locations have been established for the facility to monitor surface
water quality. The existing surface water locations consist of one (1) upstream (background) location and
four (4) downstream (compliance) locations. Five (5) inactive surface water monitoring locations have
been established but are not sampled (Table 2).
2.0 FIELD ACTIVITIES, SAMPLING, AND ANALYSIS
Groundwater and surface water samples were collected for the I' semi-annual sampling event by personnel
from Pace Analytical Services, LLC. (Pace) of Asheville, North Carolina between April 28-29, 2021.
Groundwater samples were collected from twenty-three (23) of the twenty-four (24) active groundwater
monitoring well locations located on the site (Table 1). One well (MW-24-45) was dry, and therefore, was
not sampled. Additionally, the five (5) surface water locations were sampled during the event (Table 2).
The groundwater and surface water samples were delivered to Pace Analytical Services, LLC. (Pace) of
Columbia, South Carolina and analyzed in the laboratory per the approved monitoring plan. The field
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Old Buncombe County Landfill — Woodfin, North Carolina August 3, 2021
Report of Groundwater Sampling and Analysis — Is'Semi-Annual Event 2021 BLE Project No. J21-14175-05
parameters of dissolved oxygen, pH, redox potential, specific conductance, turbidity, and temperature were
measured in the field by Pace. A copy of the Pace field sampling logs is included in Appendix A. A copy of
the laboratory analytical data is included in Appendix B.
3.0 GROUNDWATER FLOW
The water level data collected during the groundwater sampling event on April 28-29, 2021 is presented in
Table 3. A groundwater elevation contour map is presented as Figure 2 which includes generalized
groundwater flow directions.
4.0 RESULTS
4.1 Groundwater
The results of the groundwater field and laboratory analyses are summarized on Tables 4 and 5 and the
laboratory analytical data is included in Appendix B.
VOC detections during the current sampling event included:
• Acetone (3 wells);
• Benzene (10 wells);
• Carbon Disulfide (3 wells);
• Chlorobenzene (13 wells);
• Chloroethane (11 wells);
• 1,2-Dichlorobenzene (1,2 DCB) (6 wells);
• 1,4-Dichlorobenzene (1,4 DCB) (17 wells);
• 1, 1 -Dichlorethane (1,1 DCA) (12 wells);
• 1,2-Dichlorethane (1,2 DCA) (2 wells);
• cis-1,2-Dichloroethene (cis-DCE) (14 wells);
• trans-1,2-Dichloroethene (trans-DCE) (1 well);
• Ethylbenzene (1 well);
• 2-Butanone (1 well);
• 4-Methyl-2-Pentanone (1 well);
• Tetrachloroethene (7 wells);
• Toluene (2 wells);
• Trichloroethene (3 wells);
• Vinyl chloride (11 wells);
• Total Xylenes (5 wells); and
• 1,4-Dioxane (14 wells).
Total metal detections during the current sampling event included:
• total antimony (2 wells);
• total arsenic (1 well);
• total barium (23 wells);
• total beryllium (2 wells);
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Old Buncombe County Landfill — Woodfin, North Carolina August 3, 2021
Report of Groundwater Sampling and Analysis — Is'Semi-Annual Event 2021 BLE Project No. J21-14175-05
• total cadmium (4 wells);
• total chromium (3 wells);
• total cobalt (9 wells);
• total copper (6 wells);
• total lead (6 wells);
• total nickel (17 wells);
• total selenium (3 wells); and
• total zinc (15 wells).
Please refer to Tables 4 and 5 for a summary of which groundwater constituents exceed North Carolina
Groundwater Quality Standards (NC2L) maximum contaminant levels' (MCLs). It is noted that the
detections of PCE in the groundwater are B-flagged by the laboratory, indicating a laboratory
error.
Field parameters measured in the groundwater included dissolved oxygen, pH, redox potential, specific
conductance, turbidity, and temperature.
4.2 Surface Water
The results of the surface water field and laboratory analyses are summarized on Tables 6 and 7 and the
laboratory analytical data is included in Appendix B.
VOC detections during the current sampling event included:
• 1,4-Dioxane (3 locations).
Total metal detections during the current sampling event included:
• total barium (all locations);
• total cobalt (2 locations);
• total copper (1 location);
• total lead (1 location);
• total nickel (2 locations);
• total selenium (1 location); and
• total zinc (3 locations).
Field parameters measured in the surface water included dissolved oxygen, pH, redox potential, specific
conductance, turbidity, and temperature. Please refer to Table 6 and 7 for a summary of which surface water
constituents and field parameters exceeded their established North Carolina Surface Water Quality Standards
(NC2B)2 standard limits.
' North Carolina Department of Environmental Quality, Classifications of Water Quality Standards, Section 15A NCAC 2L.202, July 24, 2020.
2 North Carolina Department of Environmental Quality, Surface Waters and Wetlands Standards, Section 15A NCAC 02B workbook dated June
10, 2019.
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Old Buncombe County Landfill — Woodfin, North Carolina August 3, 2021
Report of Groundwater Sampling and Analysis — Is'Semi-Annual Event 2021 BLE Project No. J21-14175-05
4.3 Geochemical Parameters for Monitored Natural Attenuation
Buncombe County selected Monitored Natural Attenuation (MNA), Institutional Controls (restrictive cover;
a.k.a. landfill cap), and In Situ Enhanced Bioremediation and Bioaugmentation as the groundwater remedies
for the facility. The selected remedies are in progress. A series of transects along groundwater flow paths were
identified in the CAP, et. Seq, which includes groundwater monitoring wells selected for remedial monitoring.
A summary table which identifies each transect (1 through 5) and associated monitoring wells is included as
Table 8. Sampling for specific geochemical parameters to evaluate remedial performance were performed
during the I't semi-annual event of 2021. Those results are summarized on Table 9 and the laboratory
analytical data is included in Appendix B.
A corrective action evaluation report (CAER) will be submitted by BLE on behalf of Buncombe County later
in 2021.
5.0 CONCLUSIONS AND RECOMMENDATIONS
Semi-annual assessment monitoring was performed during the I' semi-annual event of 2021 in general
accordance with the approved CAP and monitoring plan. Detected constituents which exceed their respective
groundwater and surface water standards are identified on the summary tables. We conclude that the PCE
detections in the groundwater during this event are a result of laboratory error.
We recommend that semi-annual sampling continue in accordance the approved CAP and monitoring plan.
6.0 QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those normally employed
in hydrogeological and environmental assessments of this type. Our evaluation of site conditions has been
based on our understanding of the site and project information and the data provided to BLE.
This report has been prepared on behalf of and exclusively for the use of Buncombe County, North Carolina.
This report and the findings contained herein shall not, in whole or in part, be used or relied upon by any other
party (excluding the DWM and DWR) without BLE's prior written consent.
7.0 CLOSING
We appreciate the opportunity to be of service to Buncombe County, North Carolina. Please contact us at
[phone] if you have any questions or comments.
4 of 4

Tables

Table 1
SWS Approved Groundwater Sampling and Analysis Matrix
Closed Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Standard Semi -Annual Laboratory Parameters
Standard Semi -Annual Field Parameters
Semi -Annual Geochemical Parameters for MNA
Monitoring Well
Well Status
Transect
Number
Appendix I VOCs
(EPA 8260B)
1,4-dioxane
(EPA 8260 SIM)
Appendix II
Full List Appendix I
(Various Methods) Metals
WL
Turb
Temp
pH
ORP
DO
SC
Alkalinity
DH
VFA
TOC
BOD
COD
Chloride
CO2
FeZ
NO3
MEE
SO4
Sulfide
DPL-1
Active
5
Y
Y
O Y
- Y
Y
Y
Y
Y
Y
Y
Y
Y
DPL-2
Injection
4
MW-A
Inactive
-
MW-B
Active
2
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-2
Active
-
Y
O
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-3
Active
3
Y
Y
-
Y
Y
Y
Y
Y
Y
Y
Y
MW-4
Active
4
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-4A
Active
1
Y
Y
-
Y
Y
Y
Y
Y
Y
Y
Y
MW-5
Active
5
Y
Y
O
Y
Y
Y
Y
Y
Y
Y
Y
MW-6
Active
5
Y
Y
O
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-6-192
Active
5
Y
Y
-
Y
Y
Y
Y
Y
Y
Y
Y
MW-7
Active
-
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-8
Inactive
-
Y
MW-9
Abandoned
-
MW-10
Abandoned
MW-12-10
Inactive
-
Y
MW-12-25
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-13-10
Inactive
-
Y
MW-13-35
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-13-132
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-14
Inactive
-
Y
MW-15
Active
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-16
Abandoned
MW-17
Abandoned
MW-17-60
Active
2
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-17-137
Active
2
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-17-310
Active
-
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-18-3
Inactive
-
Y
MW-18-78
Active
5
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-19-4
Inactive
-
Y
MW-19-75
Active
4
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-19-110
Active
4
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-20-3
Inactive
-
Y
MW-20-32
Inactive
Y
MW-21-4
Inactive
-
Y
MW-21-21
Active
3
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-21-94
Active
3
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-22-78
Inactive
-
Y
MW-22-143
Inactive
Y
MW-23-119
Inactive
Y
MW-23-186
Inactive
-
Y
MW-24-45
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-24-160
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Notes:
Typical Events: April (Spring) and October (Fall) BOD = Biologic Oxygen Demand
0 = October (Fall) Only COD = Chemical Oxygen Demand
VOCs = Volatile Organic Compounds 40 CFR Part 258 Appendix I - Constituents for Detection Monitoring (Organics and Inorganics)
SWS Approved Matrix on September 1, 2020 40 CFR Part 258 Appendix II - Constituents for Assessment Monitoring (Full List)
WL = Water Level
ORP = Oxidation Reduction Potential
DO = Dissolved Oxygen
SC = Specific Conductance
DH = Dissolved Hydrogen
VFA = Volatile Fatty Acids
TOC = Total Organic Carbon
Fee = Iron II
NO3 =
Nitrate
MEE
= Methane/Ethene/Ethane
SO4 =
Sulfate
CO2 =
Carbon Dioxide
GW Approved Matrix Tl of Approved 2020-09-01 Closed BCLF GW and SW Matrix for Spring 2021.xlsx
Prepared By: AWA
Checked By: TJD

Table 2
SWS Approved Surface Water Sampling and Analysis Matrix
Closed Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Standard Semi -Annual
Laborator Parameters
Standard Semi -Annual Field Parameters
Surface
Water
Location
Location
Status
Appendix I VOCs
(EPA 8260B)
1,4-dioxane
(EPA 8260 SIM)
Appendix I
Metals
Turb
Temp
pH
ORP
DO
SC
SW-1
Active
Y
-
Y
Y
Y
Y
Y
Y
Y
SW-2
Active
Y
-
Y
Y
Y
Y
Y
Y
Y
SW-2A
Active
Y
Y
Y
Y
Y
Y
Y
Y
Y
SW-3
Active
Y
Y
Y
Y
Y
Y
Y
Y
Y
SW-4
Active
Y
Y
Y
Y
Y
Y
Y
Y
Y
SW-5
Inactive
-
-
-
-
-
-
-
-
-
SW-6
Inactive
-
-
-
-
-
-
-
-
-
SW-7
Inactive
-
-
-
-
-
-
-
-
-
SW-8
Inactive
-
-
-
-
-
-
-
-
-
SW-9
1 Inactive
-
-
-
-
-
-
-
-
-
Notes:
Typical Events: April (Spring) and October (Fall)
VOCs = Volatile Organic Compounds
Y=Yes
40 CFR Part 258 Appendix I - Constituents for Detection Monitoring (Organics and Inorganics)
SWS Approved Matrix on September 1, 2020
SW Approved Matrix T2 of Approved 2020-09-01 Closed BCLF GW and SW Matrix for Spring 2021.xlsx
ORP = Oxidation Reduction Potential
DO = Dissolved Oxygen
SC = Specific Conductance
Prepared By: AWA
Checked By: TJD

Table 3
Well Construction and Monitoring Well Data
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Monitoring
Point
Northing'
Easting'
TOC
Elevation
(ft)'
GS Elevation
(ft)'
Depth to GW
(ft)
April 27, 2021
Groundwater
Elevation (ft)
Well
Depth (ft)'
Screen Depth
(below GS)'
Geology Monitored'
Well
Status/Purpose
DPL-1
714,361.2
928,456.1
2040.73
2038.23
65.00
1975.73
65
55 - 65
Bedrock
Compliance
DPL-2
714,508.1
928,812.6
2112.15
2109.65
A
A
97
87 - 97
Bedrock
Injection
MW-A
714,654.47
931,068.90
2063.37
2061.90
0.00
2063.37
33
23 - 33
Bedrock
DNA
MW-B
713,635.93
930,421.08
1960.86
1960.30
3.76
1957.10
15
5 - 15
Bedrock
Compliance
MW-2
715,052.9
930,063.8
2205.33
2203.40
107.55
2097.78
175
145 - 175
Bedrock
Background
MW-3
713,790.10
929,814.44
1991.15
1989.90
62.85
1928.30
90
60 - 90
Bedrock
Compliance
MW-4
714,177.83
928,875.09
2014.27
2013.60
72.01
1942.26
75
55 - 75
Bedrock
Performance
MW-4A
713,351.70
931,195.02
2083.10
2082.50
66.24
2016.86
77
67 - 77
Bedrock
Compliance
MW-5
714,620.07
928,174.58
2019.73
2019.00
47.81
1971.92
80
70 - 80
Bedrock
Compliance
MW-6
715,103.13
928,152.69
2002.08
2000.30
0.00
2002.08
40
30 - 40
Bedrock
Performance
MW-6-192
715,146.34
928,113.86
2009.02
2006.73
25.14
1983.88
192
182 - 192
Bedrock
Compliance
MW-7
715,604.13
930,534.81
2108.86
2107.70
21.31
2087.55
29
14 - 29
Saprolite
Compliance
MW-8
716,107.98
930,308.94
2079.02
2077.20
24.04
2054.98
38
23 - 38
Saprolite
DNA
MW-9
716,024.04
928,619.48
2061.59
2060.00
A
A
29
14 - 29
Saprolite
DNA
MW-10
716,086.5
929,060.5
2049.67
2047.40
A
A
19
9 - 19
Saprolite
DNA
MW-12-10
DNA
DNA
2028.03
2024.94
Dry
Dry
8
4 - 8
Saprolite
DNA
MW-12-25
713,258.9
931,353.0
2029.98
2026.36
7.76
2022.22
26
16 - 26
Bedrock
Compliance
MW-13-10
713,000.2
931,279.7
2012.26
2009.85
3.53
2008.73
10
4 - 10
Saprolite
DNA
MW-13-35
713,023.1
931,236.9
2017.68
2014.13
5.65
2012.03
35
25 - 35
Bedrock
Compliance
MW-13-132
712,997.8
931,274.0
2012.89
2009.58
22.15
1990.74
132
122 - 132
Bedrock
Performance
MW-14
716,348.1
930,124.0
2053.46
2049.61
6.89
2046.57
55
40 - 55
Bedrock
DNA
MW-15
716,995.2
929,509.6
2028.08
2024.08
4.57
2023.51
72
62 - 72
Bedrock
Compliance
MW-16
716,170.0
929,107.2
2048.13
2045.13
A
A
94
84 - 94
Bedrock
DNA
MW-17
DNA
DNA
DNA
DNA
A
A
DNA
DNA -DNA
DNA
DNA
MW-17-60
713,339.0
930,205.8
1922.97
1920.35
22.30
1900.67
60
50 - 60
Bedrock
Compliance
MW-17-137
713,329.8
930,199.1
1921.73
1919.24
20.87
1900.86
137
127 - 137
Bedrock
Compliance
MW-17-310
713,302.4
930,207.9
DNA
1918.00
0.00
DNA
310
300 - 310
Bedrock
Compliance
MW-18-3
714,130.9
927,843.0
1895.62
1892.62
Dry
Dry
3
1 - 3
Flood Plain
DNA
MW-18-78
714,131.1
927,848.7
1894.62
1891.62
6.60
1888.02
78
1 68 - 78
Bedrock
Sentinel
MW-19-4
713,953.9
928,939.4
1902.27
1898.97
Dry
Dry
4
2 - 4
Flood Plain
DNA
MW-19-75
713,948.7
928,950.0
1900.72
1898.02
9.45
1891.27
75
65 - 75
Bedrock
Compliance
MW-19-110
713,951.7
928,942.4
1901.43
1898.53
10.14
1891.29
110
100 - 110
Bedrock
Sentinel
MW-20-3
713,865.0
929,310.2
1898.90
1895.90
Dry
Dry
3
2 - 3
Flood Plain
DNA
MW-20-32
713,879.0
929,332.7
1899.57
1896.67
6.23
1893.34
32
22 - 32
Bedrock
DNA
MW-21-4
713,810.5
929,567.5
1900.33
1896.73
6.30
1894.03
4
1 2 - 4
Flood Plain
DNA
MW-21-21
713,826.6
929,581.7
1900.49
1897.49
5.06
1895.43
21
11 - 21
Bedrock
Performance
MW-21-94
713,829.5
929,577.5
1901.06
1897.76
7.69
1893.37
94
84 - 94
Bedrock
Sentinel
MW-22-78
716,370.39
930,380.26
2068.13
2065.92
23.77
2044.36
79
69 - 79
Bedrock
DNA
MW-22-143
716,306.96
930,320.49
2068.34
2066.17
43.33
2025.01
148
138 - 148
Bedrock
DNA
MW-23-119
716,014.05
930,476.24
2076.61
2074.37
41.70
2034.91
120
110 - 120
Bedrock
DNA
MW-23-186
716,004.53
930,480.42
2076.43
2074.29
51.29
2025.14
186
176 - 186
Bedrock
DNA
MW-24-45
1711,372.031930,963.221
1932.07
1 1929.82
1 Dry
I Dry
45
35 - 45
Bedrock
I Compliance_]
MW-24-160
1711,435.811931,042.731
1933.24
1 1930.93
1 94.90
1 1838.34
1 160
1 150 - 160
1 Bedrock
I Sentinel
-Data from Table 1, Well Construction Summary, from Old Buncombe County Landfill Corrective Action Plan, by SCS Engineers, Dated September 3, 2014.
2 - Water levels were collected for these wells but no accurate survey data is available.
TOC - Top of Casing
GS - Ground Surface
DNA - Data Not Available
A - Abandoned
14175-05 GW Tables Prepared By: RLB
Table 3 April 2021 Checked By: IAI

Table 4
Groundwater VOCs
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Sampled by Pace Analytical Services, LLC. April 28-29, 2021
TEST
UNITS
MRL
MDL
MCL
MW-B
MW-2
AM-3
MW4
MW4A
MW-5
NM-6
MW-6-192
NM-7
MW-12-25
NM-13-35
MW-13-132
NM-15
MW-17-60
MW-17-137
MW-17-310
MW-18-78
MW-19-75
MW-19-110
MW-21-21
MW-21-94
MW-2445
MW-24-160
DPL-1
Acetone
µg/1
20
5.0
6,000
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
12 J
<5.0
<5.0
<5.0
<5.0
5.2 J
<5.0
<5.0
<5.0
Dry
<5.0
11 J
Acrylonitrile
119/1
20
0.80
NE
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
Dry
<0.80
<0.80
Benzene
µg/1
1.0
0.40
1.0
<0.40
<0.40
1.6
0.86 J
5.6
0.86 J
1.3
<0.40
2.4
<0.40
1.1
1
<0.40
<0.40
<0.40
<0.40
0.53 J
<0.40
<0.40
2.8
<0.40
Dry
<0.40
<0.40
Bromochloromethane
119/1
1.0
0.40
NE
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Bromodichlorometbane
99/1
1.0
0.40
0.6
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Bromoform
119/1
1.0
0.40
4.0
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
1 <0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Carbon Disulfide
119/1
1.0
0.40
700
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
4.2
<0.40
<0.40
<0.40
<0.40
2.7
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
0.53 J
<0.40
Dry
<0.40
<0.40
Bromometbane (Methylbromide)
99/1
2.0
0.40
10.0 (i)
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Carbon tetrachloride
119/1
1.0
0.40
0.3
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Chlorobenzene (mono)
119/1
1.0
0.40
50
<0.40
<0.40
4.4
6
28
8.7
7.5
0.96 J
13
<0.40
5
<0.40
<0.40
<0.40
<0.40
<0.40
4
4.2
0.78 J
32
1.8
Dry
<0.40
<0.40
Chloroethane
99/1
2.0
0.40
3,000
0.61 J
<0.40
3.2
2
<0.40
1.0 J
3.5
0.65 J
3.4
<0.40
<0.40
<0.40
<0.40
<0.40
0.43 J
<0.40
0.70 J
<0.40
0.87 J
<0.40
2.3
Dry
<0.40
<0.40
Chloroform
119/1
1.0
0.40
70
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Chloromethane (Methylchloride)
µg/1
1.0
0.50
3.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
Dry
<0.50
<0.50
Dibromochloromethane
99/1
1.0
0.40
0.4
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
1,2-Dibromo-3-chlompropane; DBCP
119/1
1.0
0.40
0.04
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
1,2-Dibmmoethane; Ethylene dibromide
119/1
1.0
0.40
0.02
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Dibromomethane
µg/1
1.0
0.40
70.0 (i)
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
1,2-Dichlorobenzene
119/1
1.0
0.40
20.0
<0.40
<0.40
0.83 J
0.73 J
4.4
<0.40
<0.40
<0.40
<0.40
<0.40
3.1
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
4
0.44 J
Dry
<0.40
<0.40
1,4-Dichlorobenzene
µg/1
1.0
0.40
6.0
0.75 J
<0.40
7.2
9.5
25
4.8
2.6
0.43 J
5.8
<0.40
16
0.58 J
<0.40
0.53 J
0.68 J
<0.40
3.1
3.2
0.76 J
14
2.8
Dry
<0.40
<0.40
trans-1,4-Dichloro-2-butene
µg/1
2.0
0.50
NE
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
Dry
<0.50
<0.50
1,1-Dichloroethane
119/1
1.0
0.40
6.0
<0.40
<0.40
1.3
7.2
<0.40
0.51 J
1.8
0.69 J
2.1
<0.40
<0.40
<0.40
<0.40
1.1
0.78 J
<0.40
0.98 J
0.47 J
<0.40
2.8
1.2
Dry
<0.40
<0.40
1,2-Dichloroethane
119/1
1.0
0.40
0.4
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
0.43 J
0.42 J
Dry
<0.40
<0.40
IJ-Dichlomethene(-ethylene)
99/1
1.0
0.40
350
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
cis-1,2-Dichloroethene (-ethylene)
119/1
1.0
0.40
70
4.7
<0.40
0.65 J
16
<0.40
<0.40
1.4
<0.40
20
0.57 J
2.7
2.6
<0.40
2.5
0.61 J
<0.40
0.95 J
<0.40
0.93 J
5.8
2.9
Dry
<0.40
<0.40
trans-1,2-Dichloroethene (-ylene)
µg/1
1.0
0.40
100
<0.40
<0.40
<0.40
<0.40
0.44 J
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
1,2-Dichloropropane
99/1
1.0
0.40
0.6
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
cis-1,3-Dichloropropene (-propylene)
119/1
1.0
0.40
0.4
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
trans-1,3-Dichlompropene (-propylene)
µg/1
1.0
0.40
0.4
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Ethylbenzene
99/1
1.0
0.40
600
<0.40
<0.40
<0.40
<0.40
6.8
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
2-Hex anone
µg/1
10.0
2.0
40.0 (1)
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
<2.0
Iodomethane
119/1
5.0
0.40
NE
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Dichlorometbane (Methylene chloride)
99/1
1.0
0.40
5.0
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
2-Butanone (Methyl ethyl ketone)
µg/1
10.0
2.0
4,000
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
3.4 J
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
<2.0
4-Methyl-2-Pentanone
µg/1
10.0
2.0
NE
<2.0
<2.0
<2.0
<2.0
4.9 J
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
<2.0
Styrene
µg/1
1.0
0.41
70.0
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
Dry
<0.41
<0.41
1,1,1,2-Tetrachloroethane
119/1
1.0
0.40
1.0 (i)
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
1,1,2,2-Tetrachloroethane
119/1
1.0
0.40
0.2
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Tetrachloroethene (-ethylene)
99/1
1.0
0.40
0.7
0.68 BJ
<0.40
<0.40
1.2 B
<0.40
<0.40
0.87 BJ
<0.40
<0.40
0.63 BJ
0.66 BJ
0.53 BJ
<0.40
0.54 BJ
0.51 BJ
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Toluene
119/1
1.0
0.40
600
<0.40
<0.40
<0.40
<0.40
2.7
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
0.66 J
<0.40
Dry
<0.40
<0.40
1,1,1-Trichloroethane
119/1
1.0
0.40
200
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
1,1,2-Trlchloroethane
99/1
1.0
0.40
0.6 (i)
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Trichloroethene (-ethylene)
119/1
1.0
0.40
3.0
<0.40
<0.40
<0.40
0.82 J
<0.40
<0.40
<0.40
<0.40
0.60 J
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
0.51 J
<0.40
Dry
<0.40
<0.40
Trichlomfluoromethane
119/1
1.0
0.40
2,000
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
1,2,3-Trichloropropane
99/1
1.0
0.40
0.005
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
<0.40
Vinyl acetate
µg/1
5.0
1.2
88.0(1)
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<12
<1.2
<1.2
<1.2
<1.2
<1.2
<12
<1.2
<12
<1.2
<1.2
<1.2
Dry
<1.2
<1.2
Vinyl chloride
119/1
1.0
0.40
0.03
2.3
<0.40
0.72 J
3
1
<0.40
<0.40
<0.40
<0.40
<0.40
0.61 J
0.91 J
<0.40
1.2
0.74 J
<0.40
0.83 J
<0.40
<0.40
2.2
1.2
Dry
<0.40
<0.40
Total Xylenes
119/1
1.0
0.40
500
<0.40
<0.40
0.89 J
<0.40
12
<0.40
<0.40
<0.40
0.54 J
<0.40
<0.40
<0.40
<0.40
<0.40
0.46 J
<0.40
<0.40
<0.40
<0.40
0.60 J
<0.40
Dry
<0.40
<0.40
1,4-Dioxane
3.0
1.0
3.0
22
NT
95
24
31
73
33
5.6
NT
NT
NT
NT
NT
26
35
NT
53
87
35
30
46
NT
<1.0
JApp. II Volatile Organic Compounds (VOC's) Various Various Various Variousl NT ND NT NT NT ND ND NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT
Notes:
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Updated July 24, 2020
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated April 6, 2018
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
6. MRL = Method Reporting Limit
7. MDL -Minimum Detection Limit
8. NT = Not Tested
9. "J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
10. "B"-flagged data (values detected in the lab blank) are laboratory errors and are presented on this spreadsheet.
14175-05 GW Tables
Table 4 VOC April 2021
Prepared By: RLB
Checked By: IAI

Table 5
Groundwater Field Parameters and Total Metals
Old Buncombe County Landfill
Woodiin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Sam led by Pace Analytical Services, LLC. April 28-29, 2021
TEST
UNITS
MRL
MDL
MCL
MW-B
MW-2
MW-3
MW4
MW4A
MW-5
MW-6
MW-6-192
MW-7
MW-12-25
MW-13-35
MW-13-
132
MW-15
MW-17-60
MW-17-
137
MW-17-
310
MW-18-78
MW-19-75
MW-19-
110
MW-21-21
MW-21-94
MW-24-45
MW-24-
160
DPL-1
pH
S.U.
>6.5, <8.5
6.8
6.1
6.3
5.97
6.11
6.4
6.1
6.29
5.7
6.6
5.9
6.8
12.82
6.9
7.4
8.5
6.3
6.3
7.5
6.4
6.7
Dry
7.39
7.2
Specific Conductance
mmhos/cm
NE
699
135.7
1450
1050
683
1490
1473
473.1
262.2
523.7
340.7
374.0
8058
606
824
144.9
1020
1180
459.7
1580
902
Dry
213.2
1675
Temperature
°C
NE
16.9
21.4
21.8
18.8
22.3
19.1
23.5
18.9
15.9
16.5
17.1
26.2
18.1
20.8
15.9
24.7
15.7
20
16.8
17.1
16.9
Dry
19
30.2
Turbidity
NTU
NE
9.8
8.7
5.9
2.02
5.67
1.1
0.9
3.73
9.3
1.4
2.4
7.4
2.86
4.1
0.7
3.2
4.5
0.5
0.7
4
0.1
Dry
8.08
9.9
Dissolved Oxygen (DO)
mg/L
NE
0.1
5.3
0.6
1.03
3.76
0.3
0.5
0.66
0.1
2.8
2.7
0.8
5.37
2.7
0.8
0.4
1.5
0.8
0.6
0.1
0.2
Dry
1.49
1.7
Redox
mV
NE
-133.3
44.2
-64.1
-4.7
-29.7
-20
-27.2
40.4
36.6
87.0
105.8
-131.4
-100.1
-71.1
-145.1
64.1
-22
-8.9
-119.4
-60.8
-71.5
Dry
-94.4
64.1
Total Antimony (Sb)
µg/1
2.0
0.5
1.0 (i)
<0.50
1.0 J
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
Dry
<0.50
0.80 J
Total Arsenic (As)
µg/1
2.0
1.3
10
1.4 J
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<13
<13
<13
<13
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
Dry
<1.3
<1.3
Total Barium (Ba)
µg/1
5.0
1.3
700
290
25
240
630
670
170
1,700
61
180
58
180
41
220
24
24
3.3 J
75
120
11
120
47
Dry
27
85
Total Beryllium (Be)
µg/1
0.4
0.15
4.0 (i)
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
0.20 J
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
4.1 J
<0.15
<0.15
Dry
<0.15
<0.15
Total Cadmium (Cd)
µg/1
0.5
0.13
2.0
<0.13
<0.13
0.19 J
0.84
0.18 J
<0.13
<0.13
<0.13
0.14 J
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
Dry
<0.13
<0.13
Total Chromium (Cr)
µg/1
5.0
1.3
10.0
<1.3
2.2 J
<1.3
<1.3
<1.3
<1.3
<1.3
<13
<1.3
<1.3
<13
<1.3
12
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
Dry
<1.3
55
Total Cobalt (Co)
µg/1
5.0
1.3
1.0 (i)
<1.3
<1.3
15
76
48
11
<13
<1.3
200
<1.3
1.3 J
<13
<1.3
<13
<1.3
<1.3
<1.3
3.4 J
<1.3
12
<1.3
Dry
<1.3
4.0 J
Total Copper (Cu)
µg/1
5.0
1.3
1000
<1.3
2.7 J
<1.3
<1.3
4.0 J
<1.3
<1.3
<1.3
14
1.3 J
<13
<13
<1.3
<13
<13
<13
<13
<13
<13
<1.3
<1.3
Dry
1.3 J
5.6
Total Lead (Pb)
µg/1
1.0
0.25
15
<0.25
0.77 J
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
0.45 J
<0.25
<0.25
<0.25
1.2
<0.25
<0.25
0.31 J
<0.25
<0.25
<0.25
<0.25
<0.25
Dry
0.74 J
2.1
Total Mercury (Hg)
µg/1
0.20
0.091
1.0
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Total Nickel (Ni)
µg/1
5.0
1.3
100
<1.3
7.5
32
93
9.7
19
11
1.5 J
57
15
4.8 J
2.2 J
<1.3
<1.3
<1.3
<1.3
7.2
22
<1.3
4.6 J
8
Dry
1.6 J
53
Total Selenium (Se)
µg/1
5.0
1.3
20
<1.3
<1.3
1.9 J
<1.3
<1.3
2.1 J
1.3 J
<13
<13
<13
<13
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
Dry
<1.3
<1.3
Total Silver (Ag)
µg/1
1.0
0.25
20
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
Dry
<0.25
<0.25
Total Thallium (Tl)
µg/1
0.5
0.15
0.2 (i)
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
Dry
<0.15
<0.15
Total Tin
µg/1
20
5.0
2,000 (i)
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Total Vanadium (V)
µg/1
5.0
2.5
0.3 (i)
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
Dry
<2.5
<2.5
Total Zinc (Zn)
10
2.5
1,000
<2.5
8.9 J
25
17
2.7 J
<2.5
6.1 J
<2.5
13
9.1 J
8.0 J
6.9 J
<2.5
<2.5
<2.5
3.1 J
<2.5
5.5 J
7.5 J
2.7 J
<2.5
Dry
7.2 J
14
Notes:
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Updated July 24, 2020
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated April 6, 2018
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. MRL = Method Reporting Limit
7. MDL = Minimum Detection Limit
8. NT = Not Tested
9. "I" -flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
14175-05 GW Tables
Table 5 Metals April 2021
Prepared By: RLB
Checked By: IAI

Table 6
Surface Water VOCs
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Sampled by Pace Analytical Services, LLC. April
28, 2021
TEST
UNITS
MRL
MDL
NC211
SW-1
SW-2
SW-2A
SW-3
SW-4
Acetone
µg/1
20
5.0
2,000
<5.0
<5.0
<5.0
<5.0
<5.0
Acrylonitrile
µg/1
20
0.80
420.0
<0.8
<0.8
<0.8
<0.8
<0.8
Benzene
µg/1
1.0
0.40
51.0
<0.4
<0.4
<0.4
<0.4
<0.4
Bromochloromethane
µg/1
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Bromodichloromethane
µg/1
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Bromoform
µg/1
1.0
0.40
120
<0.4
<0.4
<0.4
<0.4
<0.4
Carbon Disulfide
µg/1
1.0
0.40
100
<0.4
<0.4
<0.4
<0.4
<0.4
Bromomethane (Methylbromide)
µg/1
2.0
0.40
0.04
<0.4
<0.4
<0.4
<0.4
<0.4
Carbon tetrachloride
µg/1
1.0
0.40
1.6
<0.4
<0.4
<0.4
<0.4
<0.4
Chlorobenzene (mono)
µg/1
1.0
0.40
800
<0.4
<0.4
<0.4
<0.4
<0.4
Chlomethane
µg/1
2.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Chloroform
µg/1
1.0
0.40
2,000
<0.4
<0.4
<0.4
<0.4
<0.4
Chloromethane (Methylchloride)
µg/1
1.0
0.50
96.0
<0.5
<0.5
<0.5
<0.5
<0.5
Dibromochloromethane
µg/1
1.0
0.40
21
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dibromo-3-chloropropane; DBCP
µg/1
1.0
0.40
0.13
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dibromoethane; Ethylene dibromide
µg/1
1.0
0.40
0.1
<0.4
<0.4
<0.4
<0.4
<0.4
Dibromomethane
µg/1
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichlorobenzene
µg/1
1.0
0.40
3,000
<0.4
<0.4
<0.4
<0.4
<0.4
1,4-Dichlorobenzene
µg/1
1.0
0.40
900
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,4-Dichloro-2butene
µg/1
2.0
0.50
NE
<0.5
<0.5
<0.5
<0.5
<0.5
1,1-Dichloroethane
µg/1
1.0
0.40
100
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichloroethane
µg/1
1.0
0.40
650
<0.4
<0.4
<0.4
<0.4
<0.4
1,1-Dichloroethene (-ethylene)
µg/1
1.0
0.40
20,000
<0.4
<0.4
<0.4
<0.4
<0.4
cis-1,2-Dichloroethene (-ethylene)
µg/1
1.0
0.40
720
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,2-Dichloroethene (-ylene)
µg/1
1.0
0.40
4,000
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichloropropane
µg/1
1.0
0.40
31.0
<0.4
<0.4
<0.4
<0.4
<0.4
cis-1,3-Dichloropropene (-propylene)
µg/1
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,3-Dichloropropene (-propylene)
µg/1
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Ethylbenzene
µg/1
1.0
0.40
97
<0.4
<0.4
<0.4
<0.4
<0.4
2-Hexanone
µg/1
10
2.0
NE
<2.0
<2.0
<2.0
<2.0
<2.0
Iodomethane
µg/1
5.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Dichloromethane (Methylene chloride)
µg/1
1.0
0.40
1,000
<0.4
<0.4
<0.4
<0.4
<0.4
2-Butanone (Methyl ethyl ketone)
µg/1
10
2.0
26,000
<2.0
<2.0
<2.0
<2.0
<2.0
4-Methyl-2-Pentanone
µg/1
10
2.0
26,000
<2.0
<2.0
<2.0
<2.0
<2.0
Styrene
µg/1
1.0
0.41
NE
<0.4
<0.4
<0.4
<0.4
<0.4
1, 1, 1,2-Tetrachloroethane
µg/1
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
1,1,2,2-Tetrachloroethane
µg/1
1.0
0.40
4.0
<0.4
<0.4
<0.4
<0.4
<0.4
Tetrachloroethene (-ethylene)
µg/1
1.0
0.40
3.3
<0.4
<0.4
<0.4
<0.4
<0.4
Toluene
µg/1
1.0
0.40
11.0
<0.4
<0.4
<0.4
<0.4
<0.4
1, 1, 1 -Trichloroethane
µg/1
1.0
0.40
200,000
<0.4
<0.4
<0.4
<0.4
<0.4
1,1,2-Trichloroethane
µg/1
1.0
0.40
8.9
<0.4
<0.4
<0.4
<0.4
<0.4
Trichloroethene (-ethylene)
µg/1
1.0
0.40
30.0
<0.4
<0.4
<0.4
<0.4
<0.4
Trichlorofluoromethane
µg/1
1.0
0.40
67,000
<0.4
<0.4
<0.4
<0.4
<0.4
1,2,3-Trichloropropane
µg/1
1.0
0.40
0.001
<0.4
<0.4
<0.4
<0.4
<0.4
Vinyl acetate
µg/1
5.0
1.2
NE
<1.2
<1.2
<1.2
<1.2
<1.2
Vinyl chloride
µg/1
1.0
0.40
2.4
<0.4
<0.4
<0.4
<0.4
<0.4
Total Xylenes
µg/1
1.0
0.40
670
<0.4
<0.4
<0.4
<0.4
<0.4
1,4-dioxane
I µg/1
1 3.0
1 1.0
1 80
1 NT
I NT
1 12
1 34
1 68
Notes:
NC2B = North Carolina Surface Water Standards for Class B freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In -Stream Target Values (Workbook Dated 6-10-2019)
NE = Not Established; North Carolina has not established a MCL
NT = Not Tested
MRL = Method Reporting Limit
MDL = Minimum Detection Limit
" J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
Shaded cells indicated exceedances of NC2B Surface Water Standards
14175-05 SW Tables Prepared By: RLB
Table 6 SW VOC (4-28-21) Checked By: IAI

Table 7
Surface Water Field Parameters and Total Metals
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Sampled by Pace Analytical Services, LLC. April
28, 2021
TEST
UNITS
MRL
MDL
NC211
SW-1
NC211
SW-2
NC211
SW-2A
NC211
SW-3
NC211
SW4
pH
S.U. (on -site)
<6.0; >9.0
7.02
<6.0; >9.0
7.2
<6.0; >9.0
7.65
<6.0; >9.0
7.21
<6.0; >9.0
7.91
Specific Conductance
µmhos/cm (on -site)
NE
60.6
NE
52.5
NE
407.9
NE
571.8
NE
1473
Temperature
°C (on -site)
29.0
16.1
29.0
16.3
29.0
14.5
29.0
15.8
29.0
15.0
Turbidity
NTU (on -site)
50.0
10.11
50.0
9.78
50.0
7.82
50.0
35.71
50.0
113.3
Hardness
mg/L
10
2.0
NE
NT
NE
NT
NE
NT
NE
NT
NE
NT
Dissolved Oxygen
mg/L
-
-
<4.0
8.53
<4.0
8.68
<4.0
7.4
<4.0
8.31
<4.0
8.28
Redox
mV
-
-
NE
20.5
NE
19.6
NE
46.3
NE
47.6
NE
59
Total Antimony (Sb)
µg/1
2.0
0.50
640
<0.5
640
<0.5
640
<0.5
5,300
<0.5
5,300
<0.5
Total Arsenic (As)
µg/1
2.0
1.3
10.0
<1.3
10.0
<1.3
10.0
<1.3
10.0
<1.3
10.0
<1.3
Total Barium (Ba)
µg/1
5.0
1.3
21,000
14
21,000
14
21,000
35
21,000
110
21,000
120
Total Beryllium (Be)
µg/1
0.40
0.15
65.0
<0.15
65.0
<0.15
65.0
<0.15
65.0
<0.15
65.0
<0.15
Total Cadmium (Cd)
µg/1
0.50
0.13
0.82
<0.13
0.43
<0.13
2.98
<0.13
4.35
<0.13
8.95
<0.13
Total Chromium (Cr)
µg/1
5.0
1.3
183.07
<1.3
100.36
<1.3
616.02
<1.3
879.9
<1.3
1736.91
<1.3
Total Cobalt (Co)
µg/1
5.0
1.3
4.0
<1.3
4.0
<1.3
4.0
<1.3
4.0
3.2 J
4.0
Total Copper (Cu)
µg/1
5.0
1.3
3.64
<1.3
1.82
<1.3
14.7
5.7
22.16
<1.3
48.45
<1.3
Total Lead (Pb)
µ
1.0
0.25
13.88
0.5 J
6.04
<0.25
71.63
<0.25
114.5
<0.25
273.64
<0.25
Total Mercury (Hg)
µg/1
NT
NT
0.012
NT
0.012
NT
0.012
NT
0.012
NT
0.012
NT
Total Nickel (Ni)
µ
5.0
1.3
144.92
<1.3
77.88
<1.3
507.55
<1.3
733.54
4.0 J
1480.83
20
Total Selenium (Se)
µg/1
5.0
1.3
5.0
<1.3
5.0
<1.3
5.0
<1.3
5.0
<1.3
5.0
1.7 J
Total Silver (Ag)
µg/1
1.0
0.25
0.3
<0.25
0.08
<0.25
3.79
<0.25
8.01
<0.25
33.42
<0.25
Total Thallium (Tl)
µg/1
0.5
0.15
2.0
<0.15
2.0
<0.15
2.0
<0.15
2.0
<0.15
2.0
<0.15
Total Vanadium (V)
µg/l
5.0
2.5
NE
<2.5
NE
<2.5
NE
<2.5
NE
<2.5
NE
<2.5
Total Zinc (Zn)
µg/1
10
2.5
36.2
11
19.44
3.9 J
127.04
1.6 J
183.7
<2.5
371.25
<2.5
Notes:
NC213 = North Carolina Surface Water Standards for Class B freshwater under Title 15A Subchapter 213.
per NC DWR Surface Water Quality Standards, Criteria, & In -Stream Target Values (Workbook Dated 6-10-2019)
Measured values of hardness were utilized to calculate an acute standard at each surface water location for metals highlighted in green.
Hardness values werereported in Report of Water Quality Sampling and Analysis 1st Semi -Annual Event 2020
prepared by BLE, dated July 14, 2020.
NE = Not Established; North Carolina has not established a standard
"J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
Shaded cells indicated exceedances of NC213 Surface Water Standards
MRL = Method Reporting Limit
MDL = Minimum Detection Limit
NT = Not Tested
DNA = Data Not Available
14175-05 SW Tables
Table 7 SW Metals (4-28-20) (2)
Prepared By: RLB
Checked By: IAI

Table 8
Groundwater Transects for Remedial Monitoring
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Transect I
Transect 2
Transect 3
Transect 4
1 Transect 5
MW-4A
MW-B
MW-3
DPL-2 (AB)
MW-6
MW-12-25
MW-17-60
MW-21-21
MW-4
MW-6-192
MW-13-35
MW-17-137
MW-21-194
MW-19-75
MW-5
MW-13-132
MW-19-110
DPL-1
MW-24-45
MW-18-78
MW-24-160
Bold - MNA Performance Well
AB - Abandonded
14175-05 GW Tables
Table 8 Transect Nos. (Spring)

Table 9
Groundwater Geochemical Parameters for MNA
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J21-14175-05
Sam led b Pace Anal ical Services, LLC. April 28-29, 2021
TEST
UNITS
MRL
MDL
MCL
MW-B
MW-2
MW-3
MW-4
MW4A
MW-5
MW-6
MW-6-192
MW-7
MW-12-25
MW-13-35
MW-13-
132
MW-15
MW-17-60
MW-17-
137
MW-17-
310
MW-18-78
MW-19-75
MW-19-
110
MW-21-21
MW-21-94
MW-24-45
MW-24-
160
DPL-1
Dissolved Hydrogen (DH)
nM
1.9
0.49
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Lactic Acid
mg/l
0.50
0.053
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Acetic Acid
mg/l
0.50
0.120
5.0 (i)
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Propionic Acid
mg/l
0.50
0.053
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Formic Acid
1119/1
0.50
0.055
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Butyric Acid
mg/l
0.50
0.058
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
I NT
NT
Pymvic Acid
1119/1
0.50
0.060
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
i-Pentanoic Acid
mg/l
0.50
0.061
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Pentanoic Acid
mg/l
0.50
0.056
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
i-Hexanoic Acid
mg/i
0.50
0.056
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Hexanoic Acid
mg/l
0.50
0.058
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Methane
119/1
5.0
2.5
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Ethane
ug/I
1.0
0.075
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Ethene
119/1
1.0
0.12
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Carbon Dioxide (CO2)
mg/l
0.9
0.127
NE
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
NT
Alkalinity
mg/l
20
20
NE
NT
64
NT
450
NT
NT
570
NT
NT
NT
NT
150
NT
NT
NT
NT
300
410
170
770
310
Dry
70
NT
Sulfide
1119/1
1.0
0.99
NE
NT
1.2
NT
<0.99
NT
NT
<0.99
NT
NT
NT
NT
<0.99
NT
NT
NT
NT
3.7
<0.99
<0.99
1.5
2.6
Dry
1.8
NT
Biological Oxygen Demand (BOD)
mg/l
2.0
0.18
NE
NT
<0.18
NT
<0.18
NT
NT
6.6
NT
NT
NT
NT
<0.18
NT
NT
NT
NT
2.7
<0.18
<0.18
3.7
<0.18
Dry
<0.18
NT
Sulfate
m9/1
1.0
0.2
250
NT
3.2
NT
<0.2
NT
NT
1.1
NT
NT
NT
NT
7.8
NT
NT
NT
NT
2.2
17
12
23
3.3
Dry
23
NT
Nitrate
mg/l
0.10
0.025
10
NT
0.027
NT
<0.025
NT
NT
<0.025
NT
NT
NT
NT
0.028 J
NT
NT
NT
NT
<0.025
0.012 J
<0.025
<0.025
<0.025
Dry
<0.025
NT
Chloride
1119/1
1.0
0.2
250
NT
2.4
NT
0.32 J
NT
NT
160
NT
NT
NT
NT
5.1
NT
NT
NT
NT
150
150
41
70
98
Dry
6.5
NT
Chemical Oxygen Demand (COD)
mg/1
20
20
NE
NT
<20.0
NT
20
NT
NT
42
NT
NT
NT
NT
<20.0
NT
NT
NT
NT
33
40
<20.0
58
28
Dry
<20.0
NT
Total Organic Carbon (TOC)
mg/I
1.0
1.0
NE
NT
11
NT
6.3
NT
NT
15
NT
NT
NT
NT
1.1
NT
NT
NT
NT
8.9
12
2.8
15
7.3
Dry
1.4
NT
Iron H (field measured)
u
NE
NT
ND
NT
6,000
NT
NT
3,000
NT
NT
ND
ND
6,000
NT
4,500
1,500
ND
5,000
>7,000
2,500
2,500
4,500
Dry
500
NT
Notes:
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Updated July 24, 2020
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated April 6, 2018
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. MRL = Method Reporting Limit
7. MDL = Minimum Detection Limit
8. NT = Not Tested
9. "J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
10. ND =Not Detected
14175-05 GW Tables
Table 9 MNA April 2021
Prepared By: RLB
Checked By: IAI

Figures

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REFERENCES:
Mour USGS TOPOGRAPHIC MAP, 7.5
2000 1000 0 2000 4000 r MINUTE SERIES, WEAVERVILLE AND
LEICESTER. NC. QUADRANGLE 2019
APPROXIMATE SCALE IN FEET ;� ,
DRAWN' KLW DATE: 6-15-21 BUNNELL FIGURE
IM
M LAMMONS SITE LOCATION MAP
CHECKED: RLB CAD: BCOLF04—SLM M ENGINEERING CLOSED BUNCOMBE COUNTY LANDFILL
6004 Ponders Court, Greenville, SC 29615 WOODFIN, NORTH CAROLINA 1
APPROVED: JOB NO: J21-14175-05 Phone: [phone] Fax: [phone]

250 125 0 250 500
APPROXIMATE SCALE IN FEET
o�No 00
-'�iht'itttttN�.
N PLAN,
ACTIVE
MONITORING
WELLS
INACTIVE
MONITORING
WELLS
ABANDONED
MONITORING
WELLS
ACTIVE
SURFACE
WATER
SAMPLING
LOCATIONS
INACTIVE
SURFACE
WATER
SAMPLING
LOCATIONS
MW-2
MW-8
MW-9
SW-1
SW-5
MW-3
MW-12-10
MW-10
SW-2
SW-6
MW-4
MW-13-10
MW-16
SW-2A
SW-7
MW-4A
MW-14
MW-17
SW-3
SW-8
MW-5
MW-18-3
DPL-2
SW-4
SW-9
MW-6
MW-19-4
MW-6-192
MW-20-3
MW-7
MW-20-32
MW-12-25
MW-21-4
MW-13-35
MW-22-78
MW-13-132
MW-22-143
MW-15
MW-23-119
MW-17-60
MW-23-186
MW-17-137
MW-A
M W-17-310
MW-18-78
M W-19-75
MW-19-110
MW-21-21
M W-21-94
M W-24-45
MW-24-160
DPL-1
MW-B
NOTE: ACTIVE SAMPLING MONITORING WELLS AND SURFACE LOCATIONS ARE TO BE
SAMPLED AND TESTED TWICE ANNUALLY. INACTIVE MONITORING WELLS ARE TO BE
CHECKED FOR DEPTH TO GROUNDWATER ONLY.
*WATER LEVEL IS DEEP AND NOT USED FOR CONTOURING PURPOSES.
** WATER LEVELS COLLECTED BUT NO VERIFIABLE SURVEY DATA COLLECTED
FOR GROUNDWATER ELEVATION CONTOURING PURPOSES.
NM - NOT MEASURED
MW-2® ACTIVE GROUNDWATER MONITORING WELL
MW-8® INACTIVE GROUNDWATER MONITORING WELL
MW-8 & ABANDONED GROUNDWATER MONITORING WELL
SW-1- ACTIVE SURFACE WATER MONITORING LOCATION
SW-54 INACTIVE SURFACE WATER MONITORING LOCATION
PROPERTY BOUNDARY
SURFACE WATER
POTENTIOMETRIC CONTOUR
GROUNDWATER FLOW DIRECTION
250 125 0 250 500
APPROXIMATE SCALE IN FEET
REVISIONS
No. DESCRIPTION BY
DRAWN: RLB
CHECKED: IAI
APPROVED:
DATE: 6-3-21
CAD FILE: BCOLF-05POT042721
JOB NO: J21-14175-05
BUNNELL
� LAMMONS
ENGINEERING
6004 Ponders Court, Greenville, SC 29615
Phone: [phone] Fax: [phone]
GROUNDWATER ELEVATION CONTOUR MAP — APRIL 27, 2021
OLD BUNCOMBE COUNTY LANDFILL
WOODFIN, NORTH CAROLINA
FIGURE NO.
2

APPENDIX A
FIELD SAMPLING LOGS
PACE ANALYTICAL SERVICES, LLC.

aceAnalytical
PACE ANALYTICAL SERVICES, LLC
106 Vantage Point Drive • West Columbia, SC 29172
Telephone No. 803-791-9700 Fax No. 803-791-9111
www.pacelabs.com
Number li ''D> 3"
Client
Report to Contact
Telephone No. /E-mail
No.
"
Address
Sampler's Signature
Analysis (Attach list if more space is needed)
i €
X
Pa gei of 4
city
State
Zip Code
'�
�_;.�
Lot # Bar Code
-.
Primed Name
(lab use only)
Project Name
e
^�
Pmt No 1 - ^ ✓
P.O. No.
=
Matrix
No of Containers
`; ~
j
8
by Preservative Type
Sample ID / Description
ColleGicn
Collection Time
z
i
g2
Remarks/Cooler I.D.
(Containers V each sample maybe combinad on one fine.)
Date(s)
(Military)
y
g
j
�—
e
t � —
—i,
.3
. I
FUT
Turn Around Time Required (Prior lab approval required farexpedifed TAT.)
Sample Disposal
Possible Hazard Identification
OC Requirements (Specify)
E. Standard - Rush (Specify)
❑ Return to Client ❑ Disposal by Lab
❑ Nan -Hazard ❑ Flammable a Skin Irritant ❑ Poison ❑ Unknown
1. Relinquished by t t- r
Date
Time ''��
1. Received by
Date
Time
t
2. Relinquished by
Date
Time
2. Received by
Date
Time
3. Relinquished by
Date
TIM
3. Received by
Date
Time
4. Relinquished by
Date
Time
4. Laboratory received by
Date
Time
Note: Ali samples are retained for four weeks from receipt
LAB USE ONLY
Temp Blank t? Y ❑ N
unless other arrangements are made.
Received on ice (Circle) Yes No Ice Pack I
Receipt Temp. "C
DISTRIBUTION: WHITE & YELLOW -Return to laboratory with Sample(s); PINK-Field/Client Copy Document Number. ME003N2-01

Document Nam: Field (lata Shcet -.
Date Issued: March 8, 2019
Page: 1 ofZ
aeeatalNic�it-
Dmument Number F-CAR-Ft pA01-rev.Q')
Issuing Authority; Pace Huntersville (7uality
Office
Field Data Sheet
nt.,QL ^ Bu AC. CO. Location: Wy >;a�,tiie Project#: BunG . Go G(oSP� L F Wea,5'
Name and Affiliation (Sampler(s);,Ans
- J 0.Co _
Field Data Sheet Reviews
Name and Affiliation (Inspector): Al A
Date: +d4'r7l By: $RG-
Well Informations
Well ID: i - i
Well Locked: YE / NO / Flushmount )'
Well Diameter:
Construction: ( Steel/Stainless Steel)
Total Well Depth: 6 C' 0 it
Multi Flctgr*: V , C(Radius/12)2 x 3.14 x 7.481
Static Water Level: 65- O 5 ft
Casing Volume: 0 ,163 gallons
Height of Water Column, I.Oa it
CaL 3 Volumes: 0.Ljggallons
Pump Intake: 66. 0 ft
Pure Information
Date Purged: OBI / lg /_Start:
t315 Finish: IS 10 Purge Rate: 5 nt,CIry t+\
Purging Method: IA qua mor i oars
0. Total Volume Purged: 2 5 (gallons/(9L)
Sampling Information
Date Collected: 04 / / t32)
Time Collected: I rL- _ -(am/ 09
Sampling Equipment Used: (A"o.rnovnSvmrt /(instrument ID: V 3�/ � ipt Jl�Sai3
Bottle Type Preservation Analysis Required
Ix 25o yy/ t. Paps+-; Cnuc fops M4,60.15
3X90 M L- V1,00 HG I Ale ArJP Z VoC.
ZxNo m 1- L 0.1 /-I G l 114 D olCo t �L
Field Measurements/Observations
Sample Temp Cq: 3 0 - 2 Time:51-5--._ Turbitity (ntu): 9 . a) Time: 1 9;1 5
Diss Oxy (mg/L)r 1 - "�' Time: 151 </ Fe 2+ mg/L: Thne: —
Specific Cond', (uS): I6 k 5 Time: 1515 Res. Cl (mg/L)/(µg/L): Time:
Sample pH (s a ). Z_ Time 15 15 Odor:__ Ak%J Time: I I
ReDox (mV) i4t • Time: I Appearance: Cloudrime: I S 15
ReDox (EH value):YSI ProPlus +200mV j 6u . ( Other: Time:
General/Weather Observations: ()?I. - 1 .
_ um cloudy/rainy) Temp.'KC (OF) Wind Z- 5 (mph)
Sampler Signature:
Stabilization Test
Time
Purged
T onlp.
(C)
Diss Oxy.
(lug/L)
Spec
Cond.
pI3 (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons ml
Water
level
Other
(US)
(£t)
L
1320
?.2-
I-q
i n
-f.Z
`I►-5
S. j
1Z5
65.3
-1.
91-
1-40-
q3-Z
It-I.9
75
5.3
HSoU-
-0
-t
I 0
Z
2.y
57-q
6Z5
,16
fib.$
Z•1
6�D
-
ti
-5
77
65-3-+

Document Issued: March 8, 2019
Document Name:
F-CAR-FLD-ODI.rev.03
Pare Huntersville Quality Office
Client;
Location:
project
Reviewed Date and BY: +A-ai pw,
Stabilization Tes
2.6100
Time
Temp.
ISS OXY
Spec.
Cond.
pH (s.u.)
ReDox (MV)
Turbidity
Volume Removed
(gallonsQL)
Water. level
(ft)
Other

or z
Document Name. Field data Sheet
Date Woe& Much 8, 2019
68f1Jh?lyllCRl
Page: 1 of _
Document Number F-CAR-FLD-001-rev.03
issuing Authority: Pace Huntersville Quality'
Office
Field Data Sheet
NameandAffiliation (Sampler(s):z:Y- R cs A C4 ,A
Name and Affiliation (Inspector): nil A
Well Information
Well ID: M W - 3
Well Diameter:
Total Well Depth. qS • Oq it
Static Water Level: (7 S I SCA ft
Height of Water Column: F1 5'J ft
Well Locked:
l.F' A 1) or t aoa-c
yid Data Sheet Review:
Date: t(_ a $ -aj By: BRG
Construction: ('1�/Steel/Stainless Steel)
Multi Factor*:W1.3 (•(Radius/12)2x3,14x7.481
Casing volume: gallons
Cal. 3 Volumes: gallons
Pump Intake- ��'S� tt
Purge Information
Date Purged: O1 A / 17 / j_ Start :) t i Q`5_ Finish: Purge Rate: 10 O c n m r\
Purging Method: 3)PA1ccx -ed ��b Total Volume Purged: DQOO ml (gallons /L)
Sampling Information
Date Collected:/--&f IS Time Collected: ) "�!_q _ (am/ m
Sampling Equipment Used: lcd� c—+ed �?LAm0 Instrument ID: 4SL�co�lusib(� Ol,�l!1)ccgzpWtt 3�
Bottle Type
`AOcY)L S na tc
Field Measurements/Observations
Preservation
"Nos
Sample Temp (aC): a\ _7 __Turbidity (ntu):
DissOxy (mg/L): Q , � Time: t " l 0 Fe 2+mg/L:_
Analysis Required
Nc A pP T- onc_tAks-_..__...
N.,c A 9(2 ryo C_
) . `-I Dc o,cc,. _
Time:
Time:
Specific Cond. (uS): I l S Q Time: I `-130 Res. Cl (mg/L)/(ltg/L): --Time: —
Sample pH (s.u.): 6 3___.. Time: I "A 30 Odor:_,_.. _.. (�1�.__� Time:..__t 130 _
ReDox (mV): 6L� , \ Time: l `1 O Appearance: C. I —0 s Time:
ReDox (EH value):YSI ProPlus +200iuV l� Other: -- Time:
General/Weather
Temp._tj:fA_(°F)
Sampler Signature
Stabilization Test
Time
Purged
Teemp.
(C)
Diss Oxy.
(mg/L)
Spec.
Cond.
(us)
pH (s.u.)
ReDox
(m
Turbidity
(ntu)
Volume.
removed
n1V)
(gallons /
L
Water
level (ft)
Other
\\9
DI) ,-V
. b
I�tti
&3
-s$,ro
Ie. (.
bro,�g
D,a'l
016
53.8
•$

Document Name: Field data Sheet
re,•�rvayFnal' lssuinl
Document Number: F-CAR-FLD-001-rev 02
1 of
office
Location: 13 e%✓Lv M Q 5
LC01x5n F' /Liri''l
l.11C1LL. Name and and Affiliationampler(s)i P2 J
lei
Field Data Sheet Review:
Name and Affiliation (Inspector}:
Date: 1, d$ off) By:
Well Information
well ID: r✓l w - 4
Well Locked:
/ NO)
Well Diameter: 2
Construction: (KV/Steel/Stainless Steel)
Total Well Depth: ft
Multi Factor*: `,"
@(Radius/12)2x3.14x7.48I
Static Water Level: 6 • L ft.
Casing Volume:
% 7S2 > > gallons
Height of Water Column: CO 1' I ft
Cal, 3 Volumes:
1,R 5 gadloi)s
Pump Intake:
?J ft
PurQo Information /
Date Purged: . / a? /1 I Statt: Finish: �� Purge Rate: ©o 1-1 r i-
Y-z4"-^ Total Volume Purged:
S p.70 (gall° mis)
Purging Method is-4l w g
Sampling Information
Date Collected: Time Collected: �S (an / n/
Y3 ;�
Sampling Equipment Used: U6I( IV '2-1-9 Instrument ID:
Bottle Type Preservation Analysis Required
IA/'°a M��L'/)
3 A(r,L Vo � .
Field Measurements/Observations
J d
>
Sample Temp (°C)�Time: / 1FS: Turbidity (ntu): •
: —
Time: =
Diss Oxy (mg/4 3 +7 6 Time: N-1' Fe 2+ mg/L:
me:
Spec fie Cond. (uS): 8 Time: / 4-, ' Res. CI
Sample pH (s.u.): �l Time: f Odor: Nd yr
Time: /0-f-
ReDox (mV): a4 Time: / f' Appearance: 6-1-4gs
Time:
ReDox (EH value)`.YSI ProPlus +200mV 1. 3 Other:
-�
GeneraVWeather Observations�t^/a,,'cM
/cloudy/rainy) Templ WindO./a (mPh)
Sampler Signature: 11 ✓GL ' Date:
Stabilization Test
Time
Spec.
Temp. Diss Oxy. ReDox Turbidity
Te
Cus) PH (s.u.) (MV) (ntu)
Volume
moved Water Other
level (ft)
Purged
u m L (
( C) ( g/)
allons mis
(g / )
731� S.9Lf r2 0 3.6�
/00j
14'f
RAJ, 1. s • 94-
"Fl
I.7 �ix�3 c7? �.Ofi �6.6 d?
�a'oo 66,37
lso
-at,e P 3o 6,0
'0 .b�.

Document Name:
Document Issued: November 27, 2018
Field Data Sheet
page&f )- -
Document Number:
Issueing Authority:
F-CAR-FLD-OO1.rev.02 _
Pace Huntersville Quality Office
Client: �r
Location: Q✓ con Q6
Project: L/LL, 0 a F 0
Reviewed Date and By:
Stabilization Test
r
Iffell Ma=ste
Ifuldp1icatfmn.l'.atb=--F
12
I)-. IS:
0.56-70
{
4
A 0
1.0
2 610c
Time
Purged
Temp.
(nC)
Diss Oxy.
(mg/L)
Spec.
Cond.
(u5)
pH (s.u.)
ReDox (mV)
Turbidity
(ntu)
Volume RemovedWater
(gallons/mis)
circle one
level
(ft)
�%'Ti3'ry
Other
G,F?
d.o2
—) 6r o
8,1�`
35- o a
6E�
G.32
76)
0,90
a:LF

�
PaCeAvh7lyflc8f
Document Name: Field data Sheet
lute Issued: March e8, 2019
Pa . I of y'1'
$ '
Document Number F-CAR-FLD-061-rev.63
Issuing .Authority: Pace Huntexsvil7Q Quality
Office
aid be aoa,
Name and Aff illation (Sampler(s) t2!jT " 1 1ZCC
Name and Affiliation (Inspector): A
Well Information
Well ID:, MW '" Jr Well Locked:
Well Diameter: d t
Total Well Depth: '90 Cpv ft
Static Water Level: �7- $3 ft
Heigl tof Water Column: 3P-t7ft
Construction:
Field Data Sheet Review:
Date:Q
'sS NO / Flushmount)
Steel/Stainless Steel)
Multi Factor`: • !il-3 r(Radius/12)2 x3,1$ x 7.r181
Casing Volume: 5 •;� gallons
Cal. 3 Volumes: f Jr. (o gallons
Pump intake: X ft
Purge Information p
DatePurged:�/ ax / all Start: `31� Finish:13S�6 PurgeRate: TOML[ (-ram
Purging Methods_zw_� p� Total Volume Purged: `�QSC) (gallons/01.)
Sampling Inform'' ation 4 Date Collected: /A/ a 1 Time Cotleeted:_Aab- 5 (am/(&
Sampling Equipment Used: B6�p/erp/e. mv__[nstrumentID:
Bottle Type Preservation Analysis Required
5-46r4L Crla�s i{GI Voc 1 �l�;oxaa�
t- Q50MC APCi 61 fads
Field Measurements/Observations
Sample Temp (aC): __• TTime: 3 j_ � Turbidity (ntu): Id Time:
Diss Oxy (mg/L): ©• 3 Time: Fe 2+ mg/L: Time:
SpecificCoiid. (uS): _,I HR.�_ Time: Ties. Cl (mg/L)/(Itg/L): — Time,
Sample pH (s.u.): _�o_ ,Timer Odor:, ��tM cca�S__Time:
ReDox (mV): Time; Appearance: GJtqsC rime:_
ReDox (SH valise):YST I?roPlus +200mV [-?O.O Other:
General/Weather Observations:
Sampler Signature
Stabilization Test
Time:
Temp,__$'(°F)
-ak
C-35-5-
Time
Purged
g
Temp.
°C
( )
Disc Oxy.
( n L
Spec`
Cond.
pH (s.u.)
ReDox
mV
( )
Turbidity
ntu
o Volume
removed
aiimTs
(g /Q/
Water
level
Other
g/)
(us)
( )
(ft)
13PO
6 .3
Q,G
k3m
6,5-a-o
a,
.5
Goo
9.
x 7
1.5
1
>'
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IGIGO
t3
©•$
1 9
-la-
l
.6$
1333
07.
5
I 14
x q
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1#3
1 a
00
14-tg

Do uunent Narne:
Document Issued: March 8, 2019
-
aceAnalytical
Field Data Sheet
Pageaof _o1.
Document Number:
Issueing Authority
(
F-CAR-FLD-001.rev.03
Face Huntetsville Quality Office
Client: "T��0.YtcoEflb�
Location: "ullle Air
Project: &fwrgjr Ca Old LF d6*?-t
Well ID: M
Reviewed Date and By: Q )Pp
Stabilization Test
1.lfe i Diameter
Ifultilahcatiort Factoe
1
0.0405
1.2
_
4.0913
1.625
DAM
2
0.1630
3
0.3670
4
0.6530
6
1.4650
S
2.6100
Time
Purged
g
Temp,Di
( uC)
Ox ,
Y
(mg/L)
Spec.
Cond.
(US)
pH (s.u.)
ReDox (mV)
Turbidity
(ntu}
Volume Removed
(gallonsA&L)
circle one
Water level
Eft)
Other
.3 O
-7,a
e,.3
190
G,
-I6.
y7.9
13 L(s
n. O
1 C)• 3y
150-S
Co. q
--a-s
I 0-co,
M
5,0.0f
-
"

Document Name: Field data Sheet
Document Number: F-CAR-FLD-001-rev.02
Field Data Sheet
f3LF Location: i0u�ca ln6 ✓{
Office
ILOS0617 t.o'1�7 Me✓'1
Name and Affiliation (Samplex(s): NI f J 1 n? 1
ld Data Sheet Review:
Name and Affiliation (Inspector):- -----
SDixte:,)e,�
Well Information
Well ID: %0 G✓ ' 6'/9 z
Well Locked:
NO)
Well Diameter: f7
Construction:
(tV /Steel/Stainless Steel)
Total Well Depth: K ft
Multi Factor*:
1,63 1*(Radius/12)2x3.14x795i
Static Water Level: Z • I y ft.
Casing Volume:
gallons
Height of Water Column: �6 f• ? G ft
Cal. 3 Volumes: 1, f 9 tF.: {gallons
Pump Intake:
] g % ft
In
Purge I
11 Date Purged: _/ / t / Start: IS J Finish: / ° Purge
r r s 11 �a rx ( Total Volume Purged: allons nds)
Purging Method, i� g
samplingInformation
a? 7 Time Collected:
Date Collected:_/_/ /
Sampling Equipment Used: &i, j Instrument ID:
Bottle Type
3
Preservation
act
/{ci,
Analysis Required
U> c
FieldMeasnrements/Observations . r6 tS 3 �3 /Cf'J
Sample Temp (C): Time: Turbidity (ntu): Time:
Diss Oxy (mg/L): D , 6,6
Time:
1 d If Fe 2+ mg/L:
Time: - --
Specific Cond. (uS): LO 9 • /
Time:
/ 6 1 S Res. Cl (mg/L)/(µg/L):
Trim :e �_
Sample pH (s.u,): Zg
Time:
G S Odor: Mu a-
Time:
ReDox (mV): ' `F v F
Time:
(r Appearance:
Time: 6 l
ReDox (EH value):YSI ProPlus +200mv lJ^ 9' Other.
General/Weather Observations•
S Uds
Y G✓a a M
((Q/cloudy/rainy) Temp.
7S('F) Wind0, r (mph)
Sampler Signature
Cr_L:95•..�ti.... T
/,7/A - Date: �., A?-
JS0.Vdd14IXLLor
1

CeRnafyticai'
Document Name Field data Sheet
Date Issued: March 8, 2019
Page: I of 'p,
Document Number. F-CAR-R.,D-p01:-rev.03
Issuing Authority: Pace Huntersville Quality
Office
r
Name and Affiliation (Sanipler(s): y)M —02c2t-'
Name and Affiliation (Inspector):
Well Information
Well ID: M W - % Well Lacked:
Well Diameter:
a"
Total Wel[Depth: a5.3S ro.e £t
Static Water Level: ft
Height of Water Column; Y- ft
Old IF a��1
Field Data Sheet Review:
Date:OH�VA By:
ES NO / Flushmount)
Construction: (E�`,Steet/Stainless Steel)
Multi Factor`:.(x(.Radius/12)2x ,140.481
Casing Volume: ^ gallons
Cal.3 Volumes: gallons
Pump Intake- a�•aS T o. PJft
Purge Information qq Date Purged:�/ a$//Ial Start: 1J�1 Finish:16055 Purge Rate: LIJ�M(�(MfN
Purging Method:_�ca lzd pi tnQ Total Volume Purged: V7C7 (gallons n /L)
Sampling Information
Date Collected: _/ al )—t Time Collected: V20__(am/t0
Sampling Equipment Used: D Pu -e Instrument ID:_*Y. Prop�uA 67�Micro r5��
Bottle Type Preservation Analysis Required
5- �OML G�nss IN I�rok
f - aSh�aL Plws-h,'r Hdh1C�� �( (�oS htefols
Field Measurements/Observations
Sample Temp (eC): 15.6 Time: 1700__Turbidity(ntu):
` 3
Time; 00
Diss Oxy (mg/L), 'Tune:
Fe 2+ mg/L
Specific Cond. (uS): 0(0ca. a Time:
Res. Cl (nig/L)/(lcg/L):
'1'itne:
Sample pH (s.u.); —S �__...._.... .Time: _ —Odor:_
_...._f � ____._._._Time:...-.
ReDox (mV): • sP Time:
Appearance: �It%r_c��
Time:
ReDox (EH value);Y(3I ProPlus +200mV a3ln tC
Other:
Time:
Oenerat/Weather Observations:
Temp.7rg ff) Wind t7'S ((mph)
Sampler Signature
Stabilization Test
Spec.
Volume
Time
Purged
Teemp.
(C)
Diss Oxy.
(ing/L)
Cond.
pH (s.u.)
ReDox
(mV),
Turbidity
removed
(gallons/
Water
level
ether
(US)
(ntu)
i1
(ft}
L
(J�
•(D
Ss
rr
7 10
a
C)1.616
- MT
5,
a.
al_r�
11.1
0,
I.
5-"i
:.s
91.7a-
d0.3
0. �)_
alp.
�'-7
-71
lXm k
l .0
7
al-�

Document Name:
Document Issued: Match 8, 2010
aceA031WICa
Field Data Sheet
Page�-of O�
1
Docuritent Number:
F-CAR-FLD 007.rcv.03'
issueing Authority:
Pace Huntersville Quality Office.
Client;_ PLE / w-lcQmf,- 6--
Location: i ('�2 Aft:
Project: ��Cern C
o, Old L F doal
Well ID: Mw —
Reviewed Date and By: CLA
Stabilization Test
[Well Diameter
R4ultiplication Factor"
1
0.0403
1.2
0.0418
1.625
0.1080
2
0.1630
3
0.3670
4
0.6530
6
1.4630
8
2.6100
Time
Purged
Temp.
(Dc)
Di
(mg/L}
Spec.
Cond;
(US)
pH (s.u.)
ReDox (mV)
Turbidity
(ntu)
Volume RemovedssDxy.
(gallons s L)
circle one
Water level
(ft)
Other
iS`tp
aGA
f3.a
1 ol(5.fo
a.(A
76• (o
13,7
3 c�
al 7
15'45
,'3
;kMO
5,16
5.
00o
al.71
15-5-0
%-5-
0•l
9.Q•0
5 G
73,9
30,G
5-49-0
a!•S(*
RZtloovh
I`J 5
0-1
d3l
5--*7
7r, )L
oo
as 00
1(6057
fn l•
XT
5-7
426- )-
ac'a .3
9 a
off,16
1(ots
15I
0.
P373
5.7
1 Z•
19• a-
13700
aa. si
Y-1000 it
as
i59
0. �
a�9.3
5,7
ply-,
I-i, 5
Igaoo
9s-70
1 3
(59
0.1
•
a 9
37. *7
13. LA
as-7oc>
-S,,
4
0.1
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5-,`b
3(o-3
i0. 7
a7doo I
aa.90
5s
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o_t
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5•
36-1
31700
dJ)J3

z7,
Document Name: Field data Sheet Page: I c
Art' Yr�7ly¢NU;if Issuing Authority: Pace F
Document Number: F-CAR-FLD-001-rev.02 Office
L ` Location: i3,•• to n s s, Protect#:
C�>Jecd [F AtlI/
Name and Affiliation
Name and Affiliation
Well lnfformation
Well ID: M[s -/d'-
Well Diameter:
Total Well Depth: 7S, 7 ° ft
Static Water Level: 3 �15 ft
Height of Water Column:�M• i ft
Well Locked:
Construction:
Field Data Sheet Review:
Date: ()`��a ���( By
/ NO)
Steel/Stainless Steet)
Multillactoe: ` / 6) r(Radius/12)2x3.14x7481
Casing Volume: d 1• � U %S gallons
Cal. 3 Volumes: 3S,0661 9 gallons
Pump Intake: ^%0, 0 o ft
Purge Itefformatiaxn
Date Purged: - / 7R / }' _Stat: tz ti ° Finish: 5 00 Purge Rate:
Purging Method:. �0 " Sy�� t Total Volume Purged: A o0 0 (gtaloi'S16
Sanrpl3n� daaferxtaation _
Date Collected: r f / ?! / Time Collected: 17 I (am/(9)
Sampling Equipment Used:
' ^a t `F "" " lg used
Bottle Tyke
y�
3n�s
Preservation
6/N�s
H�L
Maly,
s eq
//9 C-
Field Measixretments/Observati s
Sample Temp (C): �T ) Z, I Time:
�_7 1=
Turbidity (ntu): a Time:
Diss Oxy (mg/L): S i Time:
y
! � D
Fe 2+ mg/L.
Specific Conti. (uS): Time:
%30r
Res. CI (mg/L)/(µg/L)!-'--I'mie: _
Sample pH (s.u.): 7 Time:
P 0 a^
Odor: a/0 -e Time: 3 b
ReDox (mV): a t 1 Time:
o
/
Appearance: Lw S� < Time: /3of
ReDox(EH value):YSIProPlus+200mV
�5,
/__Pi/ Ste-O Time: /S0
_)Other:
General/Weather Observations:
3yd > 6✓n2M
y/cloudy/rainy) Temp? r (°F) W ndB /0 (mph)
Sampler Signatures Date: 4-
SPAMULAUUR
1Go6
Time
Temp,Diss
Ox .
y
Spec,
Conti.
pH (s.u)
ReDox
Volume
Turbidity
removed
Water
Other
Purged
M
(mg/L)
(US)
(MV)
(nti') (gallons/g)-
level (ft)
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PACE ANALYTICAL SERVICES, LLC
106 Vantage Point Drive - West Columbia, SC 29172
Telephone No. 803-791-9700 Fax No. 803-791-9111
www.pacelabs.com
Number 11,17'913
Client
Report to Contact
Telephone No. /E-mail
Quote No.
Address
Sample SignIture,
Analysis (Attach list it more space is needed)
X-'-,
Page i of f
City
State
Zip Code
Lot # Bar Code
Printed Name
�111 0 0
we
(lab vse only)
Project Name
V-1
C L
Project No., r
P.O. No.
s
Matrix
No of Containers
by Preservative Type
Sample ID Description
Collection colkc'
m 7ar
(Containers for each sample may be combined m me line.)
Date(s)
(Ma'nu 1
9
ti
Remarks Cooler I.D.
<I
1--v\ wi — Ll
t
y
7
V
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Turn Around 'Thrie Required (Prior lab approval required to r I.VIdifed TAT-)
P-o
Sample Disposal
Identification
Possible Hazard Identifition
OC Requirements (Specify)
ll Standard i Rush (Specify)
Return to Client El Disposal by Lab
0 Non -Hazard Ej Flammable '� Skin Irritant C1 Poison El Unknown
1. Relinquished by,
Date
Tme
1. Received by
Date
Time
2,
2. Relinquished by
Date
Time
2. Received by
Date
Time
3. Relinquished by
Date
Time
3. Received by
Date
Time
4. Relinquished by
Date
Time
4. Laboratory received by
Date
Time
Note: All samples are retained for four weeks from receipt
LAB USE ONLY
Temp Blank t'5 Y 0 N
unless other arrangements are made.
Received on ice (circle) Yes No Ice Pack
ReceiptTemp. �C
DISTRIBUTION: WHITE & YELLOW -Return to laboratory with Sample(s), PINK-FieldCkent Copy Document Number ME003N2-01

ZeAnalyficalo'
PACE ANALYTICAL SERVICES, LLC
106 Vantage Point Drive - West Columbia, SC 29172
Telephone No. 803-791-9700 Fax No. 803-791-9111
www.pacelabs.com
Number 0
-
Client
Report to Contact
Telephone No. / E-mailNo.
Quote
L
Address
Sampler's Signature,
Analysis (Attach list If more space is needed)
x
Page °`" of
City
state
Zip Code
Lot # Bar Code
Pohlad Name
<
(lab use only)
Project Name
J
<7,1
Project No.
P.O. No.
Matrix
No of Conlamrs
by PesehaWeZTre
v
Sample ID Description
Collection
Collection lime
Remarks /Cooler LD.
(Containers tor each sample maybe combined on one line.)
v,
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7
Tom Around Time Required (Pniarlaftaplinvivirequired fore.Vedfled TAT.)
Sample Disposal
Possible Hazard Identification
QC Requirements (Specify)
L Standard !-; Rusk(Spechy)
F1 Return to Client D Disposal by Lab
El Non -Hazard [I Flammable L-1 Skin Irritant [I Poison 1:1 Unknown
1. Relinquished by -------
Date
Timg
1. Received by
Date
Time
2. Relinquished by
Date
Time
2. Received by
Date
Time
3. Relinquished by
Date
TIM
3. Received by
Date
Time
4. Relinquished by
Date
Time
I
4. Laboratory received by
Date
Time
I
Note: Ali samples are retained for four weeks from receipt —ILAB
USE ONLY
TempBlank �,Y 11 N
unless other arrangements are made.
Received on ice (Circle) Yes No Ice Pack
Receipt Temp. 'C
DISTRIBUTION: WHITE & YELLOW -Return to laboratory with Sampfe(s), PINK-Field/Client Copy Document Number. ME003N2-01

Dmument Name: Field data Sheet
Date Issued: March &, 2M
I
Id ceRnatyticat'
Page: I of
Document Number F-CAR-FLD-001-red03
lssuing,Authnilty: Pace Huntersville QualityI
�r
Office
Name and Affiliation (Sampler(s):-5;� - e cit- R c al,. Ca,
Name and Affiliation (Inspector): /,-31 A
Well Information
Well ID: M W 7
Well Diameter:
Total Well Depth:
Static Water Level 10 l ft
Height of Water Cotumh:6�'Dcl It
L F Ae i a.oa�
Data Sheet Review:
Date: q - 2�7 - 2-1 By: (rL G-
Well Locked: i(UB / NO / Flushniount )
Construction: (Vl V /Steel/Stainless Steel)
Multi Factor : 0J1 3 r(RadiusC12)2 x 3,14 x.7.4si
Casing Volume: I O , bL gallons
CaL 3 Volumes; b3'94 gallons
Pump lntlake M,00 ft
Purge Information
Date Purged:O�-N_/'a-F / aL_ Start: 09S!�7 Finish: ' Purge RateAS-0 mL)
Purging Method: I) S D . 136AydR r Total Volume Purged: 3(-) C)C? (gallons nl)/L)
Sampling Information
Date Collected:_ 101-A t Time Collectedd—CLO-Q,,__ 1u /pin)
Sampling Equipment Used: �'�Q 13(Qdde- InstrumerAID:
Bottle Type
Field Measurements/Observations
Preservation
Analysis Required
NC MNR (zn
A
Sample Temp (oC): a, . _Time: l Q Q Q Turbidity (ntu): Time: 10 O ()
DissOxy(mg/L): IS7•3 Time: IOQO Fe2+mg/L tvl� Tune: i000
Specific Cond. (uS): \ 3S 7:1 Time: 1 QQ O Res. CI (mg/L)&g/L): --Time: —
Sample pH (s.u.)a---- ___ .Time:, I QOO L (10Q_. _.
Repox (mV): "c'1 . �l: Time: l QGC) Appearances Cl eet �A G--&s Time: 100 0
ReDox (EH value):YSI ProPlus +200mV t 1� • -1 Other: Time:
General/Weather
Wind Q (mph)
Sampler Signature:
Stabilization Test
Time
Purged
Temp.
a
(C)
Diss Oxy.
(mg/L)
Spec
Cond.
u
(}
pH (s.u.)
,, o�i�ta�
ReDax
(mV)
Turbidity
(Diu)
Volume
removed
(gallons/�/
L
Water
level (ft)
Other
�0
1,
138,8
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or
Ducument-(same Field data Sheet
Late issued: March &, 2019!
Pape:. 1 of 1
Document Number HCAR-FL,T7-001-rev:Q3
Issuhig Authority: Pace Htmtersville Quality,
Office
Name and Affiliation (Sampler(s):-,ZM- aLi A cr c L k62A
Name and Affiliation (Inspector): nil
Well Inforination
Well 1Dt M w - %
Well Diameter:
Total Well Depth: y1'bQ It
Static Water Level; O , 00 ft
Height of Water Column: �ft1 6 Q ft
Well Locked:
Data Sheet Review:
Date: 4/'2-9' �-( By: CL.&
Construction /Steel/Stainless Steel)
Multi Factor*: Q•t 6'> ('(Radius/12)2 x3,14 x.7.481
Casing Volume: /- gallons
Cal.3 Volumes; aQ -3LA gallons
Pump Intake: -3clQc ft
Purge Information
Date Purged: q1 lamk_ Start: l�� Q Finish: 11n n Purge Rate: ) `'I Q �
Purghig Method: f osla l kt c M,n Total Volume Purged: IA12 can (gallons/ 11s L)
Sampling Information
Date Collected: 014_/aa l\ Time Collected; Lo S __ (am/ (�m}�
Sampling Equipment Used: {�en5lr lkL pU InstrumentID:_'-/&-Z�()cc)()(.,tSi �3Q(,-�i-,ANC.COrQw 30�q
Bottle Type
Field Measurements/Observations
Preservation Analysis Required
1,4Dcokc e
car) /\j A
Sample Temp (°C): �'J
Time: )-�n'�-___Turbidity
(ntu): Q - c�
Time: YZ)q �—
DissOxy{mg/L):
Time: JAnl
Fe2+mg/Lt 3,Q
Time:
Specific Cond. (uS):
Time: 1 aoS
Res. C1 (litg/L)/(Itg/L): --Time:
Sample pH (s.u.): � \__..
,Timet_1�o
ReDox (mV): - D� .a
Tine: 1 a QK-
Appearance: P�
Tune: 130
ReDox (EH value):YSI ProPlus +200mV 1--� a .a
Other:
Time:
Wind_O-(mph)
Sampler Signature
Stabilization Test
Time
Purged
4Temnp,
Diss Oxy.
(mg/L)
Spec
Cond.
(uS)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons;'m /
L3
Water
level (ft)
Other
6
a•�I.o
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1
1 t5TIna
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1 3
1)00 JL1,1 a,3 1 tIt 6•t-'J"l'3 o•q 1-4ao0 &,ri'8

Document Name: Field data Sheet
Ig
A; rRIYffxV'
Name and Affiliation
Name and Affiliation (Inspector):__
Well Information
Well ID: MhZ
n
Document Number: F-CAR-FLD-001-rev.02 I office
Field Data Sheet
Location: CLJ,I�
_ Qu�✓ws5e� N� Project#: � �%✓
t?/S `PL- Cr, Field Data Sheet Review:
Well Diameter: <
Total Well Depth: 6' a!ft
Static Water Level: �) • a �— ft
NO
Height of Water Coln= ��)l ft
Date:0L1-0- By: Ih7,5
Well Locked: Y / NO)
Construction:
Multi Factor': .46) r(Radius/12)2x3.14x7.48]
Casing Volume: 0.707j gallons
Cal. 3 Volumes: 501 gallons
Pump Intake: —7 f' it
Purge wormat on
Date Purged:. + / � � / R 11 _Stott :�_ Finish: �-'� �Purge Rate:
(00 r,
Purging Method:.ALg404- G' nv Total Volume Purged: (J_�.
(gaUousQ
Sampling hefornmtion
Date Collected:!-F- /!°/ )L I Time Collected: I / �! (am(p�
a ur trument ID: y S NP i fls� l> l
sampling Equipment Used: & 6a n 0 ,CIns
u 11
Bottle "Type
�I—o A t
iL9 s .e
Preservation
/UV N L .
yr✓ s
Analysis Required
n2,�,4 11
Wq It 1
NCB
va I,W
xd�
Field Vieasutevarentls/Observations
Temp U Time:
Turbidity (ntu):
a • 02
Time:!
t
Sample (C):
Diss Oxy (mg/L): f o S Time:
I llr o Fe 2+ mg/L:
6 . 00
Time:
l -
Specific Cond. (US): a Time:
L tf 0 Res. Cl (mg/L)/(µg/L):
Time
Sample pH (s.u.): T r9 Time:
j �r Odor:
5 r G N r
Time:
ReDox (mV): Tine:
I y l J Appearance:
ReDox (EHvalue):YSIProPlus+200mV
j�Other:
une:
`-'
Ceneral/Weather
rainy) Temp. Wind D- 0(mph)
Sampler Signature:
g}�}o�ji'>afiRri TPa$
Q ,,f )i NL Cm //
....�---
Time
Purged
---- ----
Temp.
(C)
Diss Oxy.
(mg/L)
Spec.
Cond.
(US),
pH (s.u.)
ReDox
(mV)
-- Volume
TurbidityWater
removed Outer
level
(ntu) (90ons/ rrils) (ft)
ISfb
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0 6
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Document Name:
Document Issued: November 27, 2018
+'
Field Data sheet
page?'oE _
Document Number:
Issueing Authority:
F-CAR-FLD-001.rev.02 _
Face Hunter"e Quality Office
Client: IJ Le�
Location:CC 03.57o_ 4,-
4 yD tt
Project: C L-o t 4 A �
MUD: M G✓ '
Reviewed Date and By: t}•(I " of,
Stabilization Test
f+yrzll �7n�n�?<=x
'' i.alr��li�ai�axt F a^�ai�"
V _
DANIS
1.623
3
4�i �rs'•<'th
1.46450
Time
Purged
Tem p
(°C)
DissOx .
y
(n-g/L)
Spec'
Cond.
(US)
pH (s.u.)
ReDox (mV)
Turbidity
'
(ntu)
VolumeRerrroved
(gallons
circle o e
Waterlevel
(ft)
Other
�S`fa:
7 a.o
f.>-o
i�5 0
3�•47
2.6
/;D.
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Document Name: Field data Sheet
Date Issued: March 8, 2019
- Pa e: I of
-
. Document Number: F-CAR-FLD-001-rev.03
- Issuing Authority: Pace Huntersville Quality.
Office
Name and Affiliation (Sampler(s):
Name and Affiliation (Inspector):
Well Information
Well ED: . Mw — V Well Locked:
Well Diameter: a t
Total Well Depth: a3 ti-0 ft
Static Water Level: 347/ 3 ft
Height of Water Column: [q .67 ft
Construction:
Multi
_Project #: VWU
Data Sheet Review:
Date: o ti I3,q I )t
'NO / Flushmount )
( VC f Steel/Stainless Steel)
Jo r(Radius/12)2 x 3.14 x 7.48].
Casing Volume: �, o� gallons.
Cal.3 Volumes: ' I- gallons
Pump Intake: ft
Purge Information %rJ%A _
DatePur
ged- / a % /d'i_ Start :13 5-0 Finish: � �a5 Purge Rate: DO6/'tiL /Min
Purging Method:otal Volume Purged: '35'415ZD (gallons/4a)
CF 06.e/
Sampling Information /
Date Collected:/ ppCV� Time Collected: ` a (am/ In
Sampling Equipment Used:1NVt5>i.� � fi_uno InstrumentID: � B®-#OA7�'ocj�i/ � 5
Bottle Type M��J
PJreservati6n Analysis Required 7�
5 -10
L- ClI4SS d 1cI V© /17,1CMP
(- )50,,L NQ03
Field Measurements/Observations
Sample Temp (eC): . to e tl Time:
` 6 3( 'Turbidity (ntu): / 0 Time:
Diss Oxy (mg/L): n • ( Time:
Fe 2+ mg/L: Time:
Specific Cond. (uS): CO 9 Time:
Res. Cl (mg/L)/(µg/L): —^ Time:
Sample pH (s.u.): G . Time:
Odor: FOu-k Time:
ReDox (mV): — t3-3 • 3 Time:
Appearance: Clearw� `nos Time
ReDox (EH value):YSI ProPlus +200mV
(o(o,7 Other: Time: _
General/Weather Observations:
Sampler Signature
Stabilization Test
/630
_(sunny lon /rainy)) Temp. ?O (7) WindS-!!f--(mph)
Time
Purged
Temp.
a
(C)
Diss Oxy.
(mg/L)
Spec'
Cond.
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/
Water
level (ft)
Other
(US)
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Document:Narne:
Field Data Sheet
Document Issued: March 8,.2019,
Pageo,of L-
Document Number:
Issuemg Authority:
-
F-CAR F1.D 001.rev.03
Pace Huntersville Quality Office.
Client: 13LJF/ d5f!✓k¢v�
Location::45l�,,Ye.
Project: &Ndyn�,
Well ID: MUJ — S '
Reviewed Date and By:
Stabilization Test
(%Tell fliameter Nfultip]ication Factor"
1 0.04m
1.2
0.0919 _
1.625
0.108o
2
0.1630
A
MI ,
Time
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g
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o
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DlssOxy.
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circle one
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Document Name: Field data Sheet
Date Issued: Mach 8, 2019
/,�/��
..
Page: I of
ceAnalyf%ca'
- Issuing Authority: acref mtevivi le Quality
1
. Document Number: F-CAR-FLD-001-cev.03
,
Office
Client: 'B L- Location: 5U� C Project #: �o
Name and Affiliation (Sampler(s): C. Field Data Sheet Review:
Name and Affiliation (Inspector);
Date; oq •21.21
Well Information
ui_n in. Yvwo- 12 - rA7a11 T ,:,.Le,i• /I vl]IG, / x1n / FI..°hMnnnr 1
�4
Well Diameter:
Total Well Depth: v '
Static Water Level: 7' X2_ ft
Height of Water Column: 2�-$`� ft
Consttuction: &�_b/Steel/Stainless Steel)
Multi Factor*: 01(43 [•(Radius/12)2x3.14x7.481.
Casing Volume: gallons.
Cal. 3 Volumes: gallons
Pump Intake: t;2-9, O ft
l jOid Lr' Wv((6
By: WS
Puree Information
Date Purged: i / 2q ../ . ( Start: 0?00 Finish: Oi�LS Purge Rate:
Purging Method: ' Sl�l ` � Total Volume' Purged: 3b e) (gallons i /L)
SamplingInformation
Date Collected: -q /21/ {j f} Time Collected: 0/pm) l �l �- �� 'i� D/R.i1 � Tfp
&o Q Ja
Sampling Equipment Used: �-�1, 4 � Instrument ID:
Bottle Type
Field Measurements/Observations
Preservation
L4fv03
rEci�
Analysis Required
Rn-e�� is
Il o e,
Sample Temp (°C):
C S
Time:
d % % D
Turbidity (ntu):
Time:
Digs Oxy (mg/L):
Time:
b %p3.y
Fe 2+ mg/L: N�
Time:.
0936
Specific Cond. (uS):
5z3, %
Time
Cl L _ 90
Res. Cl (mg/L)/(µg/L)--
'- Time:.
Sample pH (s.u.):
47. k'
Time:
01036
Odor: VUTY\P-
- Time:
n %3 0
ReDox (mV):
V 2, D
Time:
O �jV
Appearance:
Time:
6 � 3 n
ReDox (EH value):YSI ProPlus +200mV
- O
Other:
Time:
General/Weather Observations:
t�/cloudy/rainy) Temp.(°F)
Wind--?. (mph)
Sampler Signature
Stabilization Test
Time
Temp.
Dies Oxy.
Cond.
pH (s.u.)
ReDox
Turbidity
oume
remove
Water
ether
Purged
(C)
(mg/L)
(on)
(mV)
(ntu)
(gallons/
level (ft)
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Document Name: Field data Sheet -
Date Issued: March 8, 2019
2i
racBAfA064fcae
-
Page: 1 of
Issuing Authority: Pamty, Runtersville Quali
r
. Document Number: F-CAR-FLD-001-rev.03
_
Office
N--45"
Name and Affiliation (Sampler(s): C-L - P4 c-R.,
Name and Affiliation (Inspector): . lt,a5
Well Diameter: Construction:
dd Data Sheet Review:
Date: o44-z41-at By:dQf
Steel)
Total Well Depth: q©- qq ft Multi Factor*:aft i*(eeRaa'�dius/12)2x3.14x7.48l-
Static Water Level: ft Casing Volume: ���— gallons -
Height of Water Column N 4✓,3 ft Cal. 3 Volumes: 161 1 Z gallons
Pump Intake: ft
Purge Information
r
Date Purged: / Z� ./ ZL� r Start: l!g Finish: / O Z5 Purge Rate: / %r' —,*,Cl v
Purging Method: t�l r 5'l r^ 4 C Total Volume' Purged: �a (gallon/L)
Sampling Information / 0 3 O
Date Collected:/ �y a ( / ( Time Collected: /pm)
Sampling Equipment Used: 1 1 % 5 �ti C ('� Instrument ID:
Bottle Type Preservatiom Analysis Required
c - Asa � �� s F1F/� 3 /'►�t�f�lj
-3 - (/v k-xt Uo c
Field Measurements/Observations
Sample Temp ('C): . % 7 // Time:
f a
Turbidity (ntu): - t
Time:: -
Digs Oxy (mg/L): �Z •7 Time:
/
Fe 2+ mg/L: N J
Time:
J 03 iS
Specific Cond. (uS): yV 7 Time
U3
Res. Cl (mg/L)/(µg/L)i '—
Time:.
Sample pH (s.u.): s.9 Time:
> J3�.
Odor: �Gtil¢
Time.
103 C
ReDox (mV): l o r' g Time:
/ 0.'4 0
J
Appearance: ere r
Time:
% 03
ReDox (EH value):YSI ProPlus +200mV
3 o 5 • K
Other:
Time:
General/Weather Observations:
`/- 21- ZI
Stabilization Test
Wmd_ —(mph)
Time
I Temp.
Dies Oxy.
Spec.
•
pH (s'u.)
ReDox
Turbidity
Volume
removed
(gallons/
Water
level (ft)
Other
Purged
(eC)
(mg/L)
Cus)
(mV)
(ntu)
L
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17.3
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Document Name:
Document Issued: Much 8, 2019
Field Data Sheet
Page &f —
•
/�e�Aalytica►
Document Number:
F-CAR-FLD-001.rev.03
Issueing Authority:
Pace Huntersville Quality Office
Client: SL-e
Location:
Project: 0 . CIO
3
Well ID: IW147 —C 3�j
Reviewed Date and Bv: 0%-IA �S
Stabilization Test
t'TW'ell.E?iexa�aL�r
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4
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Time Temp. Diss Oxy. Spec Turbidity Volume Removed Water level
Dox mV allons,c&L Other
Purged
(C)
(m L
(us)
circle one
IM1
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1 4 7
2.
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Document Name: Field data Sheet
Date Issued: March 8, 2019
J��/
�t'aGBftrwf}cflEal'
Page: 1 of
. Document Number P•CAR-CAR-001-rev.03
Issuing Authority: Pace Huntersville Quality.
t
Office .
Field Data Sheet
Name and Affiliation (Sampler(s): zzg,� - 7a ce A ao, 1 s cQA
Name and Affiliation (Inspector): r J IA
Well Information
Well ID: M (J- 13 13 a
Well Diameter: a"
Total WellDepth: �3�' ft
Static Water Level: ft
Height of Water Column: l \ , bSft
C.R AeffI aQdA
Data Sheet Review:
Date: Lf zq - 21 By: GL C--
Well Locked:
� / NO / Flushmount )
Construction:
(l!V5/Steel/Stainless Steel)
Multi Factor*:
Q,163 (*(Radius/12)2x3.140.48].
Casing Volume: iB �-O gallons.
Cal. 3 Volumes:
� L 60 gallons
Pump Intake:
131 , OQ ft
Purge Information q
Date Purged: QH / a� / _ Start: 133 Q Finish: I33� Purge Rate:O Q MU, rm
Purging Method: otalVolume Purged: 1300 (gallons/ is L)
Samylinglnformation
Date Collected: OBI Q A- Time Collected: )3 S9-- (am/ m)
Sampling Equipment Used: �?lnstrumentID:_ Y CoP( a.SJ#Q�o6fMrCc6mPw{ 59
Bottle Type Preservation Analysis Required
MUFATUMMI
v.
Field Measurements/Observations
Sample Temp (aC : .-0 6 Timer Turbidity (ntu): �_ Time:1 S�
Digs Oxy (mg/L):_ 0 -STime: E S - Fe 2+ mg/L 6 , n Time:
Specific Cond. (uS):Time, l3Si Res. CI (mg/L)/(µg/L): Time:.
Sample pH (s.u.): b ,B Time: 13S c Odor: .. Mihu U s L Time: 1-5
ReDox (mV): 13l , _ Time: 13 Appearance: Q e tr- Time: F:S
ReDox (EH value):YSI ProPlus +200mV 68 Other: Time:
General/Weather Observations: scan.
( unity on /rainy) Temp.471_(OF) Wind a�(mph)
Sampler Signature,
Stabilization Test
Time
Purged
em
Temp.
Diss Oxy.
(mg/L)
Spy'
Cond.PH
(s.u.)
m;dl�lai
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons m /
Water
level (ft)
Other
3>Q
moo
a3,ga
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0--s
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Document Name: Field date Sheet
Date Issued: March 8, 2019
Page: 1of_12—
,. ceAnalyFicai'
Issuing Authority: Pace mtersvilte Quality.
m . Docuent plumber: F-CAR-FLD-001-rev.03
eH
I
L-E
Name and Affiliation (Sampler(s):�G
Name and Affiliation (Inspector):
Well Information
ML'a-/-2- fob
u Well Diameter: p2,
Total Well Depth: 111 D' rO ft
Static Water Level:_ 3'a - 3 1 ft
Height of Water Column:32 � 6 DLit
C_
Data Sheet Review:
Ca-e-LosR,t' 4 W-e((S.
Date: oLi i14-Z( By: V7
Construction: &/Steel/Stainless Steel)
Multi Factor*: 0, 163 [•(Radius/12)2 x 3.14 x 9.48).
Casing Vo)ume: . l � gallons -
Cal. 3 Volumes: `�- gallons
Pump Intake: 57 ` S ft
Puree Information
Date Purged: `' / Start: b Finish: / �50 Purge Rate:
PurgingMethod:�?��5�° �hZ Total VolumePurged: ��No0 (gallons/4D/L)
SamulingInformation
Date Collected: / i5/ 2-1 Time Collected: (am*)
Sampling IquipmentUsed: t� Q L tt 0� ` Instrument ID: c>2�3 jew 1b Q 3SS
Bottle Type
1= x5D w,,L_ PIez-y
3- 4o ti..L- �Ctis�
02 L10 Iva44.4
Preservation
.4,)0 3
14ee
Analysis Required
Vv
Field Measurements/Observations
Sample Temp Cq: ' ° li Time:
/ Turbidity (ntu): Time:
Dias Oxy (mg/L): 02 ` 7 Time:
Fe 2+ m L: �i Time..
g/
Specific Cond. (uS): (v ° b Time:
/ Y Res. Cl (mg/L)/(µg/L): `_ Time:.
Sample pH (s.u.): c/ Time:
4�56' Odor: "n a_ Time:
ReDox (mV): — i!. Time:
. / `�� Appearance: Cken c— Time:
ys�
ReDox (EH value):YSI ProPlus +200mV / Z4; . Other: Time:
General/Weather Observations:
s /cloudy/rainy) Temp. g (OF) Wind--! z (mph)
Stabilization Test
Time
Temp.
Dtss Oxy.
Spec.
•
PH (s.u.)
ReDox
Turbidity
Volume
removed
(gallons/ xof /
Water
level (ft)
der
Purged
(aC)
(mg/L)
S,
(mV)
(ntu)
Aq_-5
2i.
�, l
'SG7
7, n
12' 1'
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1 3, 1
567
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Document Issued. March 8, 2019
Document Name:
.�
Field Data Sheet
Page:! -of 1.
esaalyticaf
Document Number;
F•CAR-FLD-001.rev.03
Issueing Authority:
Pace Huntersville Quality Office
Client: �iJ L E
Location:
II
Project: E� h r C , e-e .
C_(7 S,A LF
W-6
Well ID:
NL\ 7 ` l7 ` 60
Reviewed Date and By: 04 y71
Stabilization Test
' Z 1
Time
Temp.
Diss Oxy.
Spec.
Dox m1
(C
(m L
(us)
KPurged
weU.Dfarrmer
1911al i ReaiicMFactor*
3
0.04115
4. i�?
0.0913
( fi25
CUM
2
0.165m
0,56�
4
0.6 M
1 +4G80
2.6100
Turbidity
Volume Removed
allons/ , L
Water level
Other
circle one
-
/
l Soo
C,
1

Document Name: Field data Sheet
Date Issued: Much 8, 2019
- Page: 1 of 1
e:tntt!}Qksf'y
Issuing Authority: Pace Huntersville Quality_
. Document Number. F-CAR-FLD-001-rev.03
Office
1
`B LE
Name and Affiliation (Sampler(s):
Name and Affiliation (Inspector):
Well Information
wen in. tN\ tn) - ) i - 13
Well Diameter: 1
Total Well Depth: -EY' V ft
Static Water Level: 591 ' 5 % it
Height of Water Columnl• � ft
Construction:
Multi Factor*: 01
Casing Volume:
ee,. eloseeP L-r Wens
Ad Data Sheet Review:
Date:a t-%'t - 2-1 By: l
Steel)
x 3.14 z 7.481.
(, gallons
Cal. 3 Volumes: ``5 • Y `7 gallons
Pump Intake: JJ J ft
Puree Information
Date Purged: Start: 3 D Finish 9 a Purge Rate:'o
Purging Method: `� Total Volume Purged: 320 D (gallons/teL)
Sampling Information
Date Collected: `�. /2�� Time Collected: 1365 (am/og�
Sampling Equipment Used: �Lc«f�La� InstrumentIDY5� A`6--a3 11'"--03s-
Bottle Type Preservation Analysis Required
vutL 0[evs l�No3 n��ls
-s— 40 WtC bt c V
LFc� IM,L— `i -AA A CL - t>
a --
Field Measurements/Observations
Sample Temp (nC): /Time:
L �S
Turbidity (ntu): 6,7 Timer
1355
Diss Oxy (mg/L): 0." Time:
/ 355
Fe 2+mg/L: i, Time:
3 55
Specific Cond. (US): TZL Time:.
l 855
Res. Cl (mg/L)/(µg/L)i '-- Time:.
—
SamplepH(s.u.): �'y Time:
/355.
Odor: k-4� Timei
3
ReDox (mV): r f �S (' Time:
Appearance: Time:
ReDox (EH value):YSI ProPlus +200m.V
Other: Time:
General/Weather Observations:
Sampler Signature
R4u6iti7af-inn Tact
Time
Temp.
Diss Oxy.
Spec.
pH (s.u.)
ReDox
Turbidity
Volume
removed
Water
Other
Purged
(C)
(mg/L)
(mV)
(ntu)
(gallons, n /
level (ft)
(u5)Cond
TI
�3c,
-2.S
—GG.S
2.3
D
6.7
1,6
5; 3,-
7.5
-GG,S
2-3
aQt.3G
f3'(o
1-5,1�
0,7
235.
7.
^I31,
2.
©, V
000
3-1 51

Document Name: Field data Sheet
Date Issued: Much 8, 2019
Page: i of Z
.racefF/uHyFfCaTf'
Issuing Authority: ce untersville Quality.
Document Number: F-CAR-FLD-001-t".03
Office
L�
Name and Affiliation (Sampler(s): 6 -(- 6" `
Name and Affiliation (Inspector): V -ryt�
Well information 31 V
®MMF�
/V t-
Data Sheet Review:
Date:644%-zt By:0
Well Diameter: Construction: W/Steel/Stainless Steel)
Total Well Depth: 12 ay ft Multi Factor' :O'/&3 r(Radius/l2)2x3.1447.481.
Static Water Level: () ft Casing Volume: �!7 1 gallons.
Height of Water Column�0 --2y it Cal. 3 Volumes: E S L gallons
Pump Intake: -JyS • O . (t
z_F Rk
Purge Information
/ — .i ./ Z` Start :
%l n S Finish: 13 05
poxge Rate:2'� 0 ,4/L
Date Purged:
Purging Method-
c
Total VolumePurged:
1/250 (gallons/&/L)
Samuline lnformatiort <—
Date Collecfed:. `t /-?�- 1 Time Collected: / / Ul, a m)
SamP • lireg Equipment
Used:- t i r 5� �C InstrumentID:7 e2®3 IPi O'3ys
.
Bottle Type
Field Measurements/Observations
Preservatipn
MCC -
Analysis Required
Sample Temp (oq °Z �'% Time: 3/ / D
Turbidity (ntu): 3, Z-�
Timer
f 3 / J .
Diss Oxy (mg/L): 0 .w Time:
/ 3 / D
Fe 2+ mg/L: ✓vim
Time:
! 3l o
Specific Cond. (uS): Time:,
! �! a
Res. Cl (mg/L)/(pg/L): '--
Time:.
Sample pH (s.u.): S Time:
/ 3 /
Odor: LUti
Tune:
! 3 Ia
ReDox (mV): G Y; ( Time:
3 10
Appearance: C.1 t Y+
Time:
/
ReDox (EH value):YSI ProPlus +200mV
2 Lc( /
Other:
Time:
General/Weather Observations: .
su y/cloudy/rainy) Temp.(°F) Wind !3 (mph)
Sampler Signature: e Date: z 2-6 z /
Stabilization Test
mp.
Diss Oxy.
Spec.
Cond.
pH (s.u.)
ReDox
Turbidity
Volume
removed
Water
Other
C)
(mg/L)
(US)
(mV)
(ntu)
(gallons/ 1A
level (ft)
,o
.
/0Uv
6,,cj-.�L4
6�rl7t,t
2�U6�
0,
.
Dk5
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2019
�'-ac�l�rlalyticaly
II
Document Name:
Field Data Sheet
Document Number:
F.CAR-FLD-OOl.rev.03
��cLocation: Nc—
Project: _
�hG . Co,ry . CG D � L C l,J•eUs . ' �
Well ID: LJ — 17 ` z,/D
Reviewed Date and By: --
Stabilization Test
FegeZof�-Z-
Issueing Authority:
Pace Hunteesville Quality Office
Wall. Dfamster
1.2
1:629
3
4
fn
3
ic,M l/Sn Fac0M,*
0-ID4 3
O:O912:
0.1.0- 0
t4..1fiSD
O.�•Cs7O
Ofi5sO
1:�690
2.61O3,
Temp.
(00
Diss Oxy.
(mg/L)
Spec.
on
Cond.
(USPurged
pH (s.u.)
ReDox (mV)
Turbidity
(ntu)
Volume Removed
(gallons,/L)
circle one
Water level
(ft)
Other
Time
o'-r.. D
l4),(-/
(°>.N
9n,s
�3,y
oLLtt)
oLt{ b
a .'-(
0,`I
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�./I
Document Name: Field data Sheet
Date Issued: March 812019
Pa
rawrvw yrwai
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority:
Of untersville Quality.
.
Field Data Sheet
Co red L F wa[5
Name and Affiliation (Sampler(s):s-1D5
- tiz- Q Field Data Sheet Review:
Name and Affiliation (Inspector): Al
te-- — r�
Date: Y-ag-d l By: Q ��
Well Information
Well ID: PMW
WellLocked: E NO / Flushmount )
Well Diameter: a��
Construction: ( Steel/Stainless Steel)
Total Well Depth: -46 . 60 ft
Multi Factor*: d.. (6 3 [•(Radius/12)2 x 3.14 x 7.481.
Static Water Level: - Q ft
Casing Volume: I I -3%,J gallons
Height of Water Colum� n:_ft
Cal. 3 Volumes: 3 (- I X gallons
Pump Intake: 7 Lt ft
Purge Information / ^' OStart: � DatePur Purged: � �1 . q3� g mL�VYI1t�
g _L/2Finish: 10(7�i Pux eRate:P(X9
Purging Method: P�.S I :C Total Volume Purged: -:W0 (gallons/4�L)
Sampling Information
Date Collected:0 � pj .2011 Time Collected: 1610 (0/pm)
Sampling Equipment Used: PQt I S-h:.I1-?C R- nrInstrument ID:� ST 33°/�Ti�f�l 7�3
Bottle Type Preservatimn Analysis Required
MtJ Pr be f �
Ne- adsyoc
NC-, r+p0ss- 15
Field Measurements/Observations
Sample Temp (eC):
15 -"�
Time:(010Turbidity
(ntu): C2
( O
Time: WO
Digs Oxy (mg/L):
(• 5
Time:
sole
Fe 2+ mg/L: 6-0
Time; (O ( O
Specific Cond. (uS):
10 20
Time:.
(G 10
Res. Cl (mg/L)/(µg/L):
Time:. --
Sample pH (s.u.):
6.3
Time:
1010
Odor: t95»
Time: I 0 f U
ReDox(mV):
—22-0
Time:
(010
Appearance: Ll
Time: M(0
ReDox (EH value):YSI ProPlus +200xnV
) 7g. 0
Other:
Time:
GeneraVWeather Observations: M%d -
Sampler Signature
Stabilization Test
(su loudy/rainy) Temp. 7 9 (OF) Wind f- - (mph).
nater ON - 2 g - ZarL1
Time
Temp.
Diss Oxy.
Cond.
pH (s.u.)
ReDox
Turbidity
oume
removed
Water
Other
Purged
(C)
(mg/L)
(US)
(m.V)
(ntu)
(gallons ml /
level (ft)
y
15-e
o. �
S9
.3
� L,
1. 1
620
N tc
5.
0 • di
cl
6.1
_ 3-
f . O
—
a
15-
1-Li
M
17.
0r3
209/0
6, 0
115.4
&
1013
1 61. 3
1-14.6
10,3
1 300
b.10
is .
a-5
JtQ15,16.3
-11.5
©- 7-
oo
16J 0

Document Issued: March 8, 2019
Document Name:
zof ?�
Field Data Sheet
Page
Document Number:
F-CAR-FLD-00I.rev.03
Issuein Authority;
g
Pace HuntersvIRe Quality Office
Client: 191— E - (3, (Nc . C.O • -
Location: .Wadd ,f1 NC
Project: SV11C-C Cle) S LEE UJeWU5
Weil ID: rA1h), %q - T75
Reviewed Dateand By:
Stabilization Test
'elrcll.t:7�n. E-r .._.
'�.Irrl�glice'Ricn T' blt".t`"31 ....
1 �2g
Bi.17J3:[N
a.1�a a
31
0.3 6 r 4
4.
OJ 6WO
,6,
1.4680
2.6100
Turbidity
(ntu)
(gallonsl(BVL)
circle one
L'6�1't�
Y✓•
r Y
®��
Y
I®®
•
�
♦ Y .
♦ Y Y i
�®

pjrl
Document Name: Field date Sheet
Date Issued: March 8, 2019
Page: a-
P�1}
eeArkllj4icaf
1 of
Issuing Authority: Pace Huntersville Quality.
///
.Document Number: F-CAR-FLD-001-rev.03
Office
Field Data Sheet
Name and Affiliation (Sampler(s): J05 - 0O-CAP—
Name and Affiliation (Inspector): /V P(
Well Information
Weu iD: Mw - I ot . 35
Well Diameter: .f2�tjl
Total Well Depth: f 6 �2 ft
Static Water Level: �1. 55 ft
Height of Water Column: b$ 97 ft
Well Locked:
Construction:
05zj1-r wu1S
Field Data Sheet Review:
Date: 1-49-dI By: krl-
/ NO / Flushmount )
ySteel/Stainless Steel)
Multi Factor*: 0. r(Radius/12)2x3.140.481.
Casing Volume: I I - I b gallons.
Cal.3 Volumes: 33, 4g gallons
Pump Intake: 16 -O (t
Puree Information
Date Purged: O'-I 0 �X(Start : It 0 Finish: IILIO Purge Rate: ZOo m L / v ' , Yl
Purging Method: I Y t 1 �u { a ��i C PuTotal Volume Purged: '4000 (gallons/eL)
Sampling Information
Date Collected: O—t- _/ */ Time Collected: 1_� kM3pm)
Sampling Equipment Used:InstrumentID: 4 STiy33°/ I7�1 Ic1°2 3
Bottle Type Preservation Analysis Required
WIN /Gf4--
N t_ Uj! Tyo c
AJL nwr MrtaiS
r�
t K
Field Measurements/Observations
Sample Temp (oC): �-0 •4 Time: (I LI 5
Turbidity (ntu): 0. 5 Time: 111•(Cj
Diss Oxy (mg/L): 0.9 Time: 1146
Fe 2+ mg/L: - �- Time: ) l
Specific Cond. (uS): 11190 Time:. 1145
Res. Cl (mg/L)/(µg/L)`. — Time:. —
Sample pH (s.u.): 63 Time: 1 1 LI 5 .
Odor: MO Time: 1 t S
ReDox (mV): — si. �1 Time: 11 t.1 5
Appearance: C (Cay Time: I LI y
ReDox (EH value):YSI ProPlus +200mV
Other: Time:
General/Weather Observations:.FA(k-%w-1
sut f cloudy/rac y,) Temp.(°F) Wind L(1
Sampler Signature: Date:0�1
Stabilization Test
Time
Temp.
Diss Oxy.
Spec.
Cond.PH
(s.u.)
ReDox
Turbidity
volume
removed
WatflrOffier
Purged
(°C)
(mg/L)
(mV)
(ntu)
(gallons
level
.)6
1210
6,
- .5
D,6
roar
9-S121U
_3
-5,i.
(3,t
1t s
1 . �1
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1117
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Document Issued: March 8, 2019
Document Name:
2.
Field Data Sheet
Paget -of
4
�C.,7�lyliCi`
Document [Number:
F-CAR-FGD-001.rev.03
Issuein S Authority;
Pace Huntersville Quality Office
Client: Bar - 17JnC_ Co, aGl Z9.2�
Location: W ooAC'n. 161 G
Project: Bt1OG CO GIOS<d 1-1r WQ.IIS
Well ID; MW - Iq - }y
Reviewed Date and Sv: N"a9 "a� i m6c
Stabilization Test
R�?4f'ed1.E}iazaz=tea•..
hIwlti�pltt�....".-,..-,..__z_,...r
. alianPaaboa"
01660
4
D.fi5 rD
6
1 463'0
1.6100
Nell
Spec
Cond.
I
Turbidity
(ntu)
IN MI
circle one

Document Name: Field data Sheet
Date Issued: March 8, 2019
Ce.1lk?l}-Elsafy
•.
Page: 1of
Number: P•CAR-CAR-001-rev.03
Issuing Authority: Pace Huntersville Quality.
Y
t
.Document
Office
Glased LFwelt5
Name and Affiliation (Sampler(s): _N DS' - PG CO— Field Data Sheet Review:
Name and Affiliation (Inspector): NAB- y
Date: �j J9 d( By:
Well Information 14QRfr
Well ID: ./A W '. 0
Well Locked: (QD NO / Flushmount )
Well Diameter: 2
Construction: (I S? teel/Stainless Steel)
Total Well Depth: I I �% ft
Multi Factor*: 0.1 3 r(Radius/12)2 x 3.14 x 7.48]
Static Water Level: IC) . Z �J ft
Casing Volume: 1b A5 gallons
Height of Water Column: (a • 2- ft
Cal. 3 Volumes: gallons
Pump Intake: l l 1 . ft
Purge Information
Date Purged:_ C4 ) start: % Z 4 5- Finish: 130J Purge Rate: 20 0 rNU nn Ul,
Purging Method: PPS S'-4c- fume Total Volume Purged: 9600 (gallons/&L)
Sampling Information ,, ��
Date Collected: Da /�._ nTime Collected: 0o (am/em
Sampling Equipment Used: PU t�� Irtl�S�Yog'CoInstrument ID: V 57=�6530ii /rT�in�6U
Bottle Type Preservation �equired
,Soy-Z 9•tdtl
MO N K1+
nfc �CpT MGf;s.lS
fyc A-PQ I V
Field Measurements/Observations; Sample Temp (eC): 1 & • D Time: (31 o Turbidity (ntu): (2• % Time: 1310
Diss Oxy (mg/L): 0 • b Time: 130 Fe 2+ mg/L: 2. 5 Time: 13 I G
Specific Cond. (uS): C1461A Time: t3i O Res. Cl (mg/L)/(µg/L): Time:. —
Sample pH (s. u.): 1.5 Time: 13(0 Odor: . F&,I_ Time: 1310
ReDox (mV):—119.4 Time: (3 U) Appearance: (?.ar Time: '3 ld
ReDox (EH value):YSI ProPlus +200ntV �i0. 6 Other: Time:
General/Weather Observations: fv -w -
Sampler Signature
Stabilization Test
G•2
Wind 1323(mph)
Time
Temp.
nC
Diss Oxy.
Spec.
Cond.
pH (s.u.)
ReDox
Turbidity
oume
removed
Water
Purged
ge
� )
m L
( g/)
(US)
m
( �
ntu
( )
lions is
(ga /
level(ft)Other
(150
3,7
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11,
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n

Document Name: Field data Sheet
Date Issued: March 8, 2019
aC@rinafpFkaly
Page: I of
Number: F-CAR-FLD-001-rev.03
- Issuing Authority: Pace Huntersville Quality.
t
.Document
Office .
Name and Affiliation (Sampler(s): 'Vp0 "
Name and Affiliation (Inspector): Iva
Well Information
Well 1D: MW- W " 1
WellDiameter: a''
Total Well Depth: ft
Static Water Level: ft
Height of Water Column:- , 36 ft
Well Locked:
Construction:
Multi
Data Sheet Review:
Date: o lll� By:
' NO / Flushmount )
eel/Stainless Steel)
r(Radius/12)2 x 3.14 x 7.48].
Casing Volume:
3,0
gallons
Cal. 3 Volumes;
` /,D
gallons
Pump Intake:
} a 1
ft
0/0/ L)rCtf)/
Purge Information �q _ /
Date Purged') a/ ./ ai Start:�Finish: lal� PurgeRate:R M'• M
Purging Method: leYiSI��C �� Total Volume Purged:d (gallonsJ'L)
Samnlinir Information
Date Collected: Time Collected: IaaO (am/ m)
Sampling Equipment Used: f P n`g 1'�ll; fp it,(, ID: I Ev te.5a'
Bottle Type Preservation Analysis Required
MNA
Field Measurements/Observations
Sample Temp (°C): . 17> Time: l a Turbidity (ntu): qa ® Time: (;) D-a
Digs Oxy (mg/L): 0. ( Time: Fe 2+ mg/L: a, 9 Time:
Specific Cond. (uS): I5W Time: Res. Cl (mg/L)/(µ /L): Time:.
Sample pH (s.u.): Ll . Time: Odor: Time:
ReDox (mV): 00,% Time: Appearance: Clear- Time:
ReDox (EH value):YSI ProPlus +200mV 13 % Other: Time:
General/Weather Observations: LolleAka, l itvr. 4nr HVdaAm a5,tba -, =
_(sunny/ ou rainy) Temp. ?7 (°F) Wind � /a (mph)
Sampler Signature: ZLI.4 - -A Date: 1 ag a(
Stabilization Test
Time
Temp.
Diss Oxy.
Spec.
PH (s.u.)
ReDox
Turbidity
o ume
removed
Water
Other
Purged
(oC)
(mg/L)
(US)
(mV)
(ntu)
(gallons/ nO/
Ll
level (ft)
ly5
[Tb
11 I
In3
to.
-5o•i
�,7
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$-!(o
fb yr
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IA
(5q3
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9.16
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9 G
155
1 119
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191
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17.
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Document Name: Field data Sheet
Date Issued: March 2019
B fJ'Ek y
Page: 1 of _
Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Runterwille Quali 4'-
t
.Document
Office .
LG doDt
Name and Affiliation (Sampler(s):_ ik
Name and Affiliation (Inspector): 40
Well Information
Well ID:
Well Diameter: a t
Total Well Depth: ?u ►9 ft
Static Water Level: 70 �Et
Height of Water Column:56� 3a ft
Well Locked:
Construction:
Data Sheet Review:
Date; �d0.�� By.
'NO / Flushmount )
eel/Stainless Steel)
Multi Factor*: 1163 [*(Radius/12)2 x 3.14 x 7.18)
Casing Volume: /q • % gallons.
Cal. 3 Volumes: 'y' gallons
91 �-
Pump Intake: ,� ft
Purge Information
Date Purged: t / 20 / Start: 095t� Finish: NC )Purge Rate:J� MG`ML
Ii
Purging Method: Rr 5io—k,L et_, 0 Total Volume Purged: 6750 (gallonsAOL)
Sampling Information
Date Collected:_/eYi / oil Time Collected: If%T� a /pm)
Sampling Equipment Used:-risw�Gc ?Lmp Instrument ID: hp(W VC407, M, Vb7ftd
Bottle Type
Preservatipn
Analysis Required
MNA
Field Measurements/Observations
Sample Temp (aC): I . pI Time: I 0 q''5 Turbidity (ntu): Time: o ti J�
Digs Oxy (mg/L): C)r a- Time: Fe 2+ mg/L: '! • S Time:
Specific Cond. (uS): Qri- Time:. Res. Cl (mg/L)/(µg/L): Time:.
Sample pH (s.u.): (oa 7 Time: Odor: Eou, Time:
ReDox (mV): % I •Jam' Time: Appearance: 000f . Time:
ReDox (EH value):YSI ProPlus +200mV 1a$ 6 Other: Time:
General/Weather Observations: (.A<<eC'I-lor" me -r., toQ0
Temp. 7a (7)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
CC)
Digs Oxy.
(mg/L)
Spec.
PH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/O/
Water
level (ft)
Other
(US)
01
i .7
g5
(6.1
�-54
D. r .
7
7.9a
c©0
i .
c r t
906
.•1
O.t ;
Pas
7-ga
Dao
101
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90
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Document Name:
Document Issued: March 8,.2019
arc
eeAtt��lyficaf
Field ' Data Sheet
Pagea-of X
Doc unient Number:
Issueing. Authority;
f
F CAR-FLD-001.rev.R3
Pace Huntersville Quality Office.
%
Client: 13� I �UCYDMIpe n,
Location; ..A6I11cf NC.
Project: styncorebe Co,61a LF ao w
Well ID: mw-at- 94
Reviewed Date and By
Stabilization Test'
tlrell Diameter
Multiplicatiort Factor"'
1
0.0403
1.2
0.0918
1.625
0.1030
2
0.1630
3
0.3670
4
0.6530
6
1.4680
3
2.6100
Time
Purged
Temp.
o
(C)
Diss Oxy.
(mg/L)
Spec.
Cord.
us)
(us)'
pH (s.u.)
ReDox (my)
Turbidity
(ntu)
Volume RemovedWater
(gallons Is
circle e )
level
()
Other
Inn
Moj
0.3
90a
G,7
-'70-
0,1
5'a5'
7A50�
o3S
-7.0
0.a
0;)
l
-73. ®
a I
7, s a
t7g0
1(o-9
O,a
90P
-71.7
7S
7.

Document Name: Field data Sheet Page: 10
" acer D80%P? - Issuing Authority: Pace H
Document Number: F-CAR-FLD-001-rev.02 Office
27,2018
Name and Affiliation
CIr)Jr-a LF A"--'p
Ce held Data Sheet Review:
Name and Affiliation (Inspector): �—
Well Infformaation
WellID: AVIV t / d c
Well Diameter:
Total Well Depth:ft
Static Water Level:_ — C ft
Height of Water Column: 6')r k
Well Locked:
Date: 0tt-Z9'Z�
/ NO)
Construction: /Steel/Stainless Steel)
Multi Factor*: j 161 [*(Radius/12)2 6IW ?81
Casing Volume D, S 6 011- gallons
Cal.3 Volumes: � X.' k20 b t gallons
Pump Intake: S• D ft
By: �92
Purge Irdormati®n J dL V-/
2/ 'b 6`l" purge �S�" r,..,.�
Date Purged: � / +15 / Start : I3J Finish: � g //�� 5
Purging Method: At-A(0o1'-.c_ !✓ } Total Volume Purged: } S 0 (gallons/ s�us1' J /G V p
Samyling hdonnation
Date Collected: 6 / i4v --I Time Collected: 6 N "� (an&
Sampling Equipment Used: 91 9 d 04" ®v^i Instrument ID: !7s r `F ``l 4 k/ .')- ;)'
Bottle'Type Paeservation Analysis Required
Mtj rc/o✓S n�tr✓
Field MeasuremaentS/Observations
Sample Temp (C): 1' , O Time:
/ F1' Turbidity (ntu): • 0?
Time:
(. " Time:
Dins Oxy (mg/L): `�
6 �s Fe 2+ m L: 0
g/
Time: -
Specific Ccmd. (uS): A I b • 1 Time:
/ 6 `P` Res. Cl (mg/L)/(µg/L):
Sample pH (s.u.): 7, 39 Time:
NPr Odor: 3Ltt 97 0,1
Time:
ReDox (mV): -- T me:J
Appearance:C
T me l 6�
ReDox (EH Value):YSI PTOPIlls+200mV
!ov . b Other:
GeneraJ/Weathes Observations: 0 u
c caf` y
Temp.
Wind s'ry (mph)
sunn clou /rainy)
CF)
Sampler Signature:/ ✓�! r�
Date: z/
SIA VddfLCLAUll
8 CDi
Time
Temp.
Diss Oxy.
Spec.
Cond.
pH (s.u.)
ReDox
Volume
TurbidityWater
removed
Other
Purged
Cq
(mg/L)
(US)
(mV)
(ntu) (gsllons/mis)
leyel(ft)
,fb . _,Y
GIS�E�
lso
a,�,;
z.2
J az. f
S�`5
�S•�
-779• of
al h• I
�, F �
-�iJ•
/`f.� : 3 DDJ
Div -»
b !�
) �r�
D

>
Document Name:
Document Issued: November 27, 2018
Field Data sheet
pagd--Of �-
Document Number:
Issuemg Authority:
F-CAR-PLD-001sev.02
Pace Huntersville Quality Office
Client: 6 L 4
Location; 8uw("M& LLa,Fp Ge=
Project: I(L.0 L--�
Well ID:
Reviewed Date and By: ZG Z( ty5
Stabilization Test
6sf"~11 �+2s7rn�bar
"a1ra1?'i�a+,ix3n�`a�^car`
1.2
625
0-16 0
4
d=
1.4 LT
5;
2-6100
Time
Purged
15
Temp.
(°C)
DissOxy.
(mg/L)
.Spec.
Cond:
(US)'
pH �s.u.)
-
ReDox (mV)
-
Turbidity
(ntu)
VolumeRemoved"
(gallon rnl)
cycle one
Water level
O
14A�,-
'
Other
6
19, 1
f4,13,?
GT6
i;ro
13
'`l

GftVirl�,�'ItG'aTl
I Date Issued: November
Docume ment Na: Field dV, 2011ata Sheet I
Lt
Document Number: F-CAR-FLD-001-rev.02
Name and Affiliation (Sampler(s): /' ,11 rf 9 S a
Name and Affiliation (Inspector):- _
Well information
Office
CLo 3ed LF �' (✓ J
Data Sheet Review:
Date: 0q -Z g+21 By: Y' S
Well ID: (ny } Well Locked: Q5S / NO)
11
Well Diameter: Construction St 1 St inl St 1
Total Well Depth: �7, I It
Static Water Level: % 7 I It.
Height of Water Column: �' ft
V / ee / a ess ee )
Multi Factor":,_43— r(Radius/12)2 x 3.14 x 7.491
Casing Volume: 0, 0 3 X ( gallons
Ca1.3 Volumes: - D'o,')e gallons
Pump Intake: ft
Purge Information
Date Purged: —t-- j Start : <: Finish: Purge Rate:
Purging Method: Total Volume Purged: —" (gallons/mis)
Sampling Information
Date Collected: `{ / d2l a ( Time Collected: / / 0
(a Pm
Sampling Equipment Used: Ins�ument ID:
Bottle Type Preservation Analysis Required
(n/1✓rFi �!/-,✓ i F/� °- v,�t e fa J9lb/�0/r
Field_ Measurements/Observations
Sample TempA
Diss Oxy (mg
Specific Cond
Sample pH (s
ReDox (mV)
ReDox (EH value):YSI ProPlus +20i
Ceneral/Weather Observations:
NO 1AM1l1 PA/ —
Sampler Signature:(
Stabilization Test
Time: Turbidity (ntu):
Time: Fe 2+ mg/L:_
Time: Res. CI (me/Lb
Time:
Time:
_ Odor: Time:
—Appearance:
Other: Time:
Innyl/cloudy/rainy) Temp. Bo ff) Windy"� (mph)
�n�rP. CF - x1 - t- r
Time
Purged
Temp.
(°C)
D ss Oxy.
(mg/L)
Spec.
Cond.PH
(s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
(gallons/nds)
Water
level (it)
Other

ZeAnalyficalo
PACE ANALYTICAL SERVICES, LLC
106 Vantage Point Drive • West Columbia, SC 29172
Telephone No.803-791-9700 Fax No. 803-791-9111
www.pacelabs.com
Number 11,911
Client
Report to Contact
Telephone No. / E-mail
Quote No.
Address
Sampler's Signature
_
X' - --
Analysis (Attach list d more space is needed)
Page o/
City
State
Zip Code
-
-
-
:'
-
-
Lot #Bar Code
(lab use only)
Printed Name
Project Name
Project No.
P.O. No.
A
ae
�E
Matrix
No of Containers
by Preservative Type
Sample ID /Description
(Contatners for each sample maybe wintined on one line.)
Collection
Date(s)
cofiew n pine
(Military)
g
a
N
S
g
o
2
c LL
Remarks l Cooler LD.
Vx
Tam Around Tame Required(Pricrlabapprovalrequired farexpedded TAT.)
❑ Standard ^_. Rush(SpecW)
Sample Disposal
D Return to Client G Disposalby Lab
Possible Hazard Identification
❑ Non -Hazard ❑ Flammable ❑ Skin Irritant Cr Poison ❑ Unknown
QC Requirements (Specify)
1. Relinquished by
Date
Time
1. Received by -' __.
Date
Time
2. Relinquished by
Date
Time
2. Received by
Date
Time
3. Relinquished by
Date
Time
3. Received by
Date
Time
4. Relinquished by
Date
Time
4. Laboratory received by
Date
Time
Note: All samples are retained for four weeksfrom receipt
unless other arrangements are made.
LAB USE ONLY
Rece ed on ice (C rote) Yes No !ce Pack
Receipt Temp. 'C
Temp Blank i Y ❑ N
DISTRIBUTION: WHITE & YELLOW -Return to laboratory with Sample(&); PINK-Field/Chent Copy Document Number: ME003N2-01

�B/47�7fyrr'al.,.
Document Name: Field data Sheet
Document Number: F-CAR-FLD-001-rev.02
Page: 1 of i
ig AuNority. Pace Auntersvffle Quality
Office
Dint
L. Z
Field Data Sheet
Name and Affiliation (Sampler(s): /' e' S 1017 EIdDa Sheet ReviewName and Affiliation (Inspector): p I �$1
Well Infformation
We4� 50- I WellLec-ked----( PcFO)
Well Diameter: �
Total Well Depth: ft
Static Water Level: ft.
Height of Water Column: f ft
Furge Imiormation
Date Purged..
Construc?iex—EPvEf teeffStainlessSteel)
Multi Factor*- r(Radius/12)2 x 3.14 x 7.491
Casing Volume: gallons
Cal. 3 Volumes: �— gallons
Pump Intake: ft
Finish: Purge Rate:
0
Purging Methc:d-. - -- -Total Volume Pux'ged eal ans/mis)
Sam�lan� 3rvfcrmation
�u Date Collected: N / �?/ ri Time Collected: (�/P m) �y
d
Sampling Equipment Used: G !L 176 Instrument ID: `Yl '� O- ( � � ?
Bottle Type Reservation Analysis Required
) �Lsr , , U NA10s /yd, lI
d/ L L'
Field Measurements/Observations
0% 1
Sample Temp (°C):Y
i 6 `l Ti me:
4`
Turbidity ntu : / F , I I
( . )
Time:
Diss Oxy (mg/L):
g'' > Time:
ai 4-
Fe 2+ mg/L:
Specific Cond. (uS):
6 0• Time:
°
Res. Cl
Sample pH (s.u.):
? Time:
4
Odor: Nv -1L
Time: �5 _
__
ReDox (mV):
_
'�- � ' s Time:
9 FV
Appearance: Q-k4 .
Time:
ReDox (EH value):YSI ProPlus +200mi
d
C
/� e-q, ,
Other:
4ig2.61
General/Weather Observations:
—
u y cloudy/rainy) Temp. I'
CF) Wind b --(mph)
Sampler Signature
p
('��—
Date:
$IdlYdBfl+aYLYUYI
Time
Purged_
AG56
Temp. .
('C)
Diss Ox .
Y
(mg/L)
Spec
Cond.
(US)
ReDox
pH (s.u.) (mV)
volume
Turbidity Water
(ntu) removed level (ft) Other
(galions/mis)

Document Name: Field data Sheet
Document Number: F-CAR-FLD-001-rev.02
Date ]ssued: November 27 12018
Page: 1 of 1
�g Autfioxit .Pace Huntersville Quality
Office
AL/ -
Name and Affiliation (Sampler(s): hl>1 f'J2
Name and Affiliation (Inspector):- _
Well information
Well Locked:
Well Diameter: ,..,,e,,Cpnsmction: (
Total Well Depth: ,tt //' Multi Factor*:_
Static Water Level: f . Casing Volume:
Height of Water Column: ft Cal. 3 Volumes:
Pump Intake:_
Purge Irif rmalawr / .
Date Purged:._/ / Fin
Field Data Sheet Review:
Date: 0'k,` `81,),( By:
YES / NO)
C/Steel/Stainless Steel)
r(Radius/12)2 x 3.14 x 7.491
gallons
gallons
ft
h: Purge Rate:
Purging Method 142/( Total Volume
(gallons/mis)
Sampling Information
Date Collected: 4 /Lyi II Time Collected: o &pm)
Sampling Equipment Used: Gs e7r Instrument ID: ys ll 0 G w/ d r
SottleType Preservation Analysis Required
Field Measureneents/Observations
a C . look � Turbidity ntu. T . 7 2 Time: / 0 R �
Sample Temp (C): � `L_Time: Y ( . )
Diss Oxy (mg/L): Time:
I' A O Fe 2+ mg/L.—Time:,
Specific Cond. (uS): T . 5 Time:
I 0 h ° Res. CI (mg/L)/(µg/L):
Sample pH (s.u.): x l `� Time:
r J 1 Odor: nyo „ c Time /V X
...._.._. _.
ReDox(mV): ��7.6 Time:
i JI`1i Appearance: C y.2.� rs� Tune: l 0 y. o
ReDox (EH value):YSI ProPInS +200n V
Z r g,1 Other: --�— Timer
General/Weather Observations: 'Vj
unn /cloudy/rainy) Temp. (°F) GVnda-r' (mph)
Sampler Signature: cy/` �'�
Date: - } Z ''
JLa VaxxGi8xiulS
Time
Purged
acsL
Temp.
CC)
Diss Oxy.
(mg/L)
Spec.
Cond.
(US)
pH (s.u.)
ReDox
(mV)
Turbidity lume Water
remove Other
(nur) (gallons/cols) el (ft)
('

Document Name: Field data Sheet
Dacunent Number: F-CAR-FLD-001-rev.02
2018
l of
office
UL L
Client: t L' Location: 05y r e
Name and Affiliation (Sampler(s):
Name and Affiliation (Inspector):_
Well Infforsmation
Wrff,ff:
Well Diameter:
Total Well Depth: t t
Static Water Level:
Height of Water Column: \ It
puree lnformati®n
Date Purged:
Well Locked:
Construction:
Multi Factor*:
a� Project#:�`" CLofe.A 6� Sl✓ �
T
ta Sheet Review: 9 �1a3�a1 By.
( YES / NO)
'VC/Steel/Stainless Steel)
r(Radius/12)2 x 3.14 x 7.481
Casing Volume: gal oun t
r,A LF )
Cal, 3 Volumes: gallons
Pump Intake: ft
F n sh: Purge Rate:
Purging Method:. }' Total Volume Purged:
Sampling Information
O
Date Collected:— / �7/' / Time Collected: Z4P � � m)
Sampling Equipment Used: Gxt,q 6 Instrument ID:
,l x re
Bottle Type
/c
3v�� s
Preservation
ffA—) .
�I-
Analysis Required
A&I,11
//d
FieldMeasnrelments/Observations
�/
Sample Temp (C): Time: 160 Turbidity (nta): ` iz ^ '
T me:A D l
Diss Oxy (mg/L): % �f Time: _ I a.5 Fe 2+ mg/L:
Time:
Specific Cond. (uS): Time: 0lo Res. CI
Sample pH (s.u.): �r �, Time: i 3 a Odor: N-s --t
Time: 3
- _o �
ReDox (mV): �6 � 3 Tim) Appearance: C e �,¢ 2
r
Time: I ° 6e:
ReDox (EH value):YSI PtnPlus +200mV a Ltt. Other:
CeneraVWea$herObservations 5v,1� S �✓�ae
—
(sunny/cloudy/rainy) Temp. �?
("F) Wind U `a (mph)
Date:r
Sampler Signature:
oeuvaaaenu
Time
Purged
Temp.
( q
D ss Ox .
(mg/L)
Spec
S�
(US),
pH (s.u.)
ReDox
(mV)
Turbidity VolumeConeWater
(nta) removed
(gallons/mis)
level (ft)
Other

0 uet-
Date Issued: November 27, 2018Page:
Document Name: Field data Sheet
1 of
", RCEdy1fO1!('
Issuing Authority; Pace Huntersville Quabty
Document Number: F-CAR-FLD-001-xev.02
Office
Client b L / Location: u/oc:
Name and Affiliation (Sampler(s): it �d9/9 I
Name and Affiliation (Inspector):_
Well information
WeH4P- 5w -' Well Locked:
Well Diameter:
Total Well Depth: tiC I µ ft
Static Water Level: ft
Height of Water Column: ft
Date
Purging
Sampling Information
Construction:
Multi Factor*:
Casing Volume:
Cal. 3 Volumes:
Data Sheet Review:
Date: cAnn )x
( YES / NO)
�C/Steel/Stainless Steel)
r(Radius/12)2 x 3.14 x 7.481
gallons
gallons
Pump Intake: ft
_ Finish: Purge Rate:
rf Vel �utge l' (gallons/mis)
Date Collected: Time Collected: / 4
Sampling Equipment Used: D rt 4 h Instrument ID: `7-K1 S` t, L 4�,
Bottle Type Preservation Analysis Required
)3 H C V9 u
Field Measurements/Observations
Sample Temp (°C): /J�, Z Time:0(-1— Turbidity (nm): . S' 1 Time:
Diss Oxy (mg/L): i / Time: Fe 2+ mg/L
—lSme: ---_._
Specific Cond. (uS): t Time: Res. Cl (mg/L)/(µg/L):
� lime:
Sample pH (s.u.): F / Time: Odor: N0 oa o 2
Time:
ReDox (mV): ' -�7 4 Time: Appearance: Ng zy
Time:
ReDox (EH value):YSI ProPlus +200mV S `f Other: -'-Time:
General/Weather Observations:
DyCiCAs� 14,114M Esimky/(lo 4y`/rainy) Temp.
Wind-9- (mph)
Sampler Signature: . Date:
Stabilization Test
Time
Purged
Temp.
(°C)
Diss Oxy.
(mg/L)
Spec.
Con(uS) d.
pH (s.u.)'
ReDox
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Turbidity
(ntu)
em�d
(gallons/mls)
Water
level (ft)
Other
�--
-�>.l-
off

Dale Issued: November 27, 2018
Document Name: FieIddate Sheet Page: lof_(
EfF1&i43rePL`Hrr Issuing AatholnT Pace Huntersville Quality
Document Numbex: F-CAR-FLD-DDl-xev.02 Office
Field Data Sheet
#: L1916 f? �a
Name and Affiliation (Sampler(s): M I /
aaSheet ReviewName
and Affiliation (Inspector):. �
By.
LD
: I ��`
Well InffornmtioA
Well ID: S W
WellLocked:
(YES / NO)
Well Di' ter:
Construction:
VC/St eel/9ta mess Steel)
TotalWell'Dep _ At
Multi Factor' :
r3�1 *2Ra//dies/122 x 3.14 x 7.491
[
✓�
Static Water Level: ( 8'r /
Casing Volume:
gallons
Height of Water Column: ft
Cal. 3 Volumesr
gallons
1
Pump Intake:
ft
Fume Inf n
Date Purged:._/_ tart:
_ Finish:�t}urge�a�t��/
�F
Purging Method.
Total Volume
Purged: /mis)
D uh
Sampling Wormation /
Date Collected: / / '` / Time Collected: /l'0+— �a/pm)
�� �CF26
Sampling Equipment Used: G 2 9 n Instrument ID: �l S
Bottle Type Preservation Analysis Required
f Pia,-xt l',1�
3 v,
Field Measurements/®bservat ons
3
( 3
Sample Temp (°C): - ( I O Time:
0 d
.
Turbidity (ntu):
T me:
Dies Oxy (mg/ L): 7' l' e Time:
I /J +
Fe 2+ mgJL:
T me:
Specific Cond. (nS): y Time:
110 v
Res. 0 (mg/LY(µg/L):
Time:
Sample pH (s.u.): •` / Time:
�/ J
Odor:
Time: _
ReDox(mV): �4. ° Time:
//D`
Appearance
ReDox (EH value):YSI PmPlus +200mV .
�' 9• 0
Other:
1me:
C eneral/Weathea Observations: O t/�
— r
_fsCnny�c ou y/rainy) Temp.7P(OF)
Wind-0 G (mph)
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stamuzanon
Time
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iesc
Temp. D ss Oxy.
(°C) (mg/L)
c
Spec.
(us)
ReDox TurbidityVolume
Water
pH (s.u.) removed Other
(mV) (Tit(gallons/mis) level(ft)
ll l D
S. % 7
14-

APPENDIX B
LABORATORY ANALYTICAL DATA -
PACE ANALYTICAL SERVICES, LLC.

0
aceAnalytical
Report of Analysis
Bunnell-Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Attention: Andy Alexander
Project Name: Closed Buncombe County Landfill Wells
Project Number: J21-14175-05
Lot Number:WD30017
Date Completed:05/16/2021
N
N
NO � � J
05/19/2021 8:36 AM
Approved and released by:
Project Manager II: Lucas Odom
pCCgF�
24r�A
SOA
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 175

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Bunnell-Lammons Engineering, Inc.
Lot Number: WD30017
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Inorganic Non -Metals
The following samples were diluted due to the nature of the sample matrix for NO3 analysis: WD30017-
015, WD30017-022. The LOQ has been elevated to reflect the dilution.
Reanalysis of the following sample was performed outside of the analytical holding time for NO3 analysis:
WD30017-010. This sample was reanalyzed due to matrix interference during initial analysis.
The BOD method blank result was higher than the method -required limit of 0.20mg/L. The seed
correction factor was below the method range. No corrective action is required as the BOD calculation
adjusts for variances in the SCF. Associated samples have been qualified witha "4" and 7" respectively.
VOCs by GC/MS
The laboratory control sample (LCS) for analytical batch 92125 exceeded acceptance criteria for Acetone.
This analytes is biased high but not detected in the samples affected. In addition, this batch recovered
trans-1,4-Dichloro-2-butene below method criteria. An LOQ standard was analyzed, and the target
analyte was detected. Since the associated samples are non -detect, no corrective action was taken.
Associated samples have been qualified with an 'U'.
The laboratory control sample (LCS) for analytical batch 92172 exceeded acceptance criteria for Acetone,
2-Butanone, and 2-Hexanone. These analytes are biased high but not detected in the samples affected.
Associated samples have been qualified with an 'U'.
The method blank associated with batch 92056 yielded "J" value detections for Chloroform and
Tetrachloroethene. No corrective action is required as these are estimated values recovered below the
LOQ. Associated detections have been qualified with a "B".
Subcontracted Analysis
The analysis for VFA, MEE, CO2, and H have been performed by Pace Gulf Coast. This data has been
ammended to this report starting on page 154.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] whw.pacelabs.com
Page 2 of 175

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WD30017
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
DPL-1
Aqueous
04/28/20211515
04/29/2021
002
MW-3
Aqueous
04/28/20211430
04/29/2021
003
MW-4A
Aqueous
04/28/20211455
04/29/2021
004
MW-5
Aqueous
04/28/20211355
04/29/2021
005
MW-6-192
Aqueous
04/28/20211615
04/29/2021
006
MW-7
Aqueous
04/28/20211700
04/29/2021
007
MW-15
Aqueous
04/28/20211305
04/29/2021
008
Trip Blank
Aqueous
04/28/2021
009
MW-2
Aqueous
04/29/20211000
04/30/2021
010
MW-6
Aqueous
04/29/20211205
04/30/2021
011
MW-4
Aqueous
04/29/20211410
04/30/2021
012
MW-B
Aqueous
04/29/20211630
04/30/2021
013
MW-12-25
Aqueous
04/29/20210930
04/30/2021
014
MW-13-35
Aqueous
04/29/20211030
04/30/2021
015
MW-13-132
Aqueous
04/29/20211355
04/30/2021
016
MW-17-60
Aqueous
04/29/20211455
04/30/2021
017
MW-17-137
Aqueous
04/29/20211355
04/30/2021
018
MW-17-310
Aqueous
04/29/20211310
04/30/2021
019
MW-18-78
Aqueous
04/29/20211010
04/30/2021
020
MW-19-75
Aqueous
04/29/20211145
04/30/2021
021
MW-19-110
Aqueous
04/29/20211310
04/30/2021
022
MW-21-21
Aqueous
04/29/20211220
04/30/2021
023
MW-21-94
Aqueous
04/29/20211045
04/30/2021
024
MW-24-160
Aqueous
04/29/20211645
04/30/2021
025
Field Blank
Aqueous
04/29/2021 1300
04/30/2021
026
Trip Blank
Aqueous
04/29/2021
04/30/2021
027
Trip Blank
Aqueous
04/29/2021
04/30/2021
(27 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 175

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WD30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
DPL-1
Aqueous
Acetone
8260D
11
J
ug/L
13
001
DPL-1
Aqueous
Antimony
6020B
0.80
J
ug/L
14
001
DPL-1
Aqueous
Barium
6020B
85
ug/L
14
001
DPL-1
Aqueous
Chromium
6020B
55
ug/L
14
001
DPL-1
Aqueous
Cobalt
6020B
4.0
J
ug/L
14
001
DPL-1
Aqueous
Copper
6020B
5.6
ug/L
14
001
DPL-1
Aqueous
Lead
6020B
2.1
ug/L
14
001
DPL-1
Aqueous
Nickel
6020B
53
ug/L
14
001
DPL-1
Aqueous
Zinc
6020B
14
ug/L
15
002
MW-3
Aqueous
1,4-Dioxane
8260D (SIM)
95
ug/L
16
002
MW-3
Aqueous
Benzene
8260D
1.6
ug/L
16
002
MW-3
Aqueous
Chlorobenzene
8260D
4.4
ug/L
16
002
MW-3
Aqueous
Chloroethane
8260D
3.2
ug/L
16
002
MW-3
Aqueous
1,2-Dichlorobenzene
8260D
0.83
J
ug/L
16
002
MW-3
Aqueous
1,4-Dichlorobenzene
8260D
7.2
ug/L
16
002
MW-3
Aqueous
1,1-Dichloroethane
8260D
1.3
ug/L
16
002
MW-3
Aqueous
cis- 1,2-Dichloroethene
8260D
0.65
J
ug/L
16
002
MW-3
Aqueous
Vinyl chloride
8260D
0.72
J
ug/L
17
002
MW-3
Aqueous
Xylenes (total)
8260D
0.89
J
ug/L
17
002
MW-3
Aqueous
Barium
6020B
240
ug/L
17
002
MW-3
Aqueous
Cadmium
6020B
0.19
J
ug/L
17
002
MW-3
Aqueous
Cobalt
6020B
15
ug/L
17
002
MW-3
Aqueous
Nickel
6020B
32
ug/L
17
002
MW-3
Aqueous
Selenium
6020B
1.9
J
ug/L
18
002
MW-3
Aqueous
Zinc
6020B
25
ug/L
18
003
MW-4A
Aqueous
1,4-Dioxane
8260D (SIM)
31
ug/L
19
003
MW-4A
Aqueous
Benzene
8260D
5.6
ug/L
19
003
MW-4A
Aqueous
Chlorobenzene
8260D
28
ug/L
19
003
MW-4A
Aqueous
1,2-Dichlorobenzene
8260D
4.4
ug/L
19
003
MW-4A
Aqueous
1,4-Dichlorobenzene
8260D
25
ug/L
19
003
MW-4A
Aqueous
trans- 1,2-Dichloroethene
8260D
0.44
J
ug/L
19
003
MW-4A
Aqueous
Ethylbenzene
8260D
6.8
ug/L
20
003
MW-4A
Aqueous
4-Methyl-2-pentanone
8260D
4.9
J
ug/L
20
003
MW-4A
Aqueous
Toluene
8260D
2.7
ug/L
20
003
MW-4A
Aqueous
Vinyl chloride
8260D
1.0
ug/L
20
003
MW-4A
Aqueous
Xylenes (total)
8260D
12
ug/L
20
003
MW-4A
Aqueous
Barium
6020B
670
ug/L
20
003
MW-4A
Aqueous
Cadmium
6020B
0.18
J
ug/L
20
003
MW-4A
Aqueous
Cobalt
6020B
48
ug/L
20
003
MW-4A
Aqueous
Copper
6020B
4.0
J
ug/L
20
003
MW-4A
Aqueous
Nickel
6020B
9.7
ug/L
20
003
MW-4A
Aqueous
Zinc
6020B
2.7
J
ug/L
21
004
MW-5
Aqueous
1,4-Dioxane
8260D (SIM)
73
ug/L
22
004
MW-5
Aqueous
Benzene
8260D
0.86
J
ug/L
22
004
MW-5
Aqueous
Chlorobenzene
8260D
8.7
ug/L
22
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 175

Detection Summary (Continued)
Lot Number: WD30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
004
MW-5
Aqueous
Chloroethane
8260D
1.0
J
ug/L
22
004
MW-5
Aqueous
1,4-Dichlorobenzene
8260D
4.8
ug/L
22
004
MW-5
Aqueous
1,1-Dichloroethane
8260D
0.51
J
ug/L
22
004
MW-5
Aqueous
Barium
6020B
170
ug/L
23
004
MW-5
Aqueous
Cobalt
6020B
11
ug/L
23
004
MW-5
Aqueous
Nickel
6020B
19
ug/L
23
004
MW-5
Aqueous
Selenium
6020B
2.1
J
ug/L
24
005
MW-6-192
Aqueous
1,4-Dioxane
8260D (SIM)
5.6
ug/L
25
005
MW-6-192
Aqueous
Chlorobenzene
8260D
0.96
J
ug/L
25
005
MW-6-192
Aqueous
Chloroethane
8260D
0.65
J
ug/L
25
005
MW-6-192
Aqueous
1,4-Dichlorobenzene
8260D
0.43
J
ug/L
25
005
MW-6-192
Aqueous
1,1-Dichloroethane
8260D
0.69
J
ug/L
25
005
MW-6-192
Aqueous
Barium
6020B
61
ug/L
26
005
MW-6-192
Aqueous
Nickel
6020B
1.5
J
ug/L
26
006
MW-7
Aqueous
Benzene
8260D
2.4
ug/L
28
006
MW-7
Aqueous
Chlorobenzene
8260D
13
ug/L
28
006
MW-7
Aqueous
Chloroethane
8260D
3.4
ug/L
28
006
MW-7
Aqueous
1,4-Dichlorobenzene
8260D
5.8
ug/L
28
006
MW-7
Aqueous
1,1-Dichloroethane
8260D
2.1
ug/L
28
006
MW-7
Aqueous
cis- 1,2-Dichloroethene
8260D
20
ug/L
28
006
MW-7
Aqueous
Trichloroethene
8260D
0.60
J
ug/L
29
006
MW-7
Aqueous
Xylenes (total)
8260D
0.54
J
ug/L
29
006
MW-7
Aqueous
Barium
6020B
180
ug/L
29
006
MW-7
Aqueous
Beryllium
6020B
0.20
J
ug/L
29
006
MW-7
Aqueous
Cadmium
6020B
0.14
J
ug/L
29
006
MW-7
Aqueous
Cobalt
6020B
200
ug/L
29
006
MW-7
Aqueous
Copper
6020B
14
ug/L
29
006
MW-7
Aqueous
Lead
6020B
0.45
J
ug/L
29
006
MW-7
Aqueous
Nickel
6020B
57
ug/L
29
006
MW-7
Aqueous
Zinc
6020B
13
ug/L
29
007
MW-15
Aqueous
Acetone
8260D
12
J
ug/L
30
007
MW-15
Aqueous
Barium
6020B
220
ug/L
31
007
MW-15
Aqueous
Chromium
6020B
12
ug/L
31
007
MW-15
Aqueous
Lead
6020B
1.2
ug/L
31
009
MW-2
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
64
mg CaCO3/L
32
009
MW-2
Aqueous
Chloride
9056A
2.4
mg/L
32
009
MW-2
Aqueous
Nitrate - N
9056A
0.027
mg/L
32
009
MW-2
Aqueous
Sulfate
9056A
3.2
mg/L
32
009
MW-2
Aqueous
Sulfide
SM 4500-S2 F-
1.2
mg/L
32
009
MW-2
Aqueous
TOC
SM 5310C-
11
mg/L
32
009
MW-2
Aqueous
Antimony
6020B
1.0
J
ug/L
34
009
MW-2
Aqueous
Barium
6020B
25
ug/L
34
009
MW-2
Aqueous
Chromium
6020B
2.2
J
ug/L
34
009
MW-2
Aqueous
Copper
6020B
2.7
J
ug/L
34
009
MW-2
Aqueous
Lead
6020B
0.77
J
ug/L
34
009
MW-2
Aqueous
Nickel
6020B
7.5
ug/L
34
009
MW-2
Aqueous
Zinc
6020B
8.9
J
ug/L
34
010
MW-6
Aqueous
Alkalinity @ pH 4.5 su
SM 2320B-
570
mg CaCO3/L
35
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 175

Detection Summary (Continued)
Lot Number: WD30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
010
MW-6
Aqueous
BOD, 5 day
SM 521013-
6.6
47
mg/L
35
010
MW-6
Aqueous
Chloride
9056A
160
mg/L
35
010
MW-6
Aqueous
COD
SM 5220D-
42
mg/L
35
010
MW-6
Aqueous
Sulfate
9056A
1.1
mg/L
35
010
MW-6
Aqueous
TOC
SM 5310C-
15
mg/L
35
010
MW-6
Aqueous
1,4-Dioxane
8260D (SIM)
33
ug/L
35
010
MW-6
Aqueous
Benzene
8260D
1.3
ug/L
35
010
MW-6
Aqueous
Carbon disulfide
8260D
4.2
ug/L
36
010
MW-6
Aqueous
Chlorobenzene
8260D
7.5
ug/L
36
010
MW-6
Aqueous
Chloroethane
8260D
3.5
ug/L
36
010
MW-6
Aqueous
1,4-Dichlorobenzene
8260D
2.6
ug/L
36
010
MW-6
Aqueous
1,1-Dichloroethane
8260D
1.8
ug/L
36
010
MW-6
Aqueous
cis- 1,2-Dichloroethene
8260D
1.4
ug/L
36
010
MW-6
Aqueous
Tetrachloroethene
8260D
0.87
BJ
ug/L
36
010
MW-6
Aqueous
Barium
6020B
1700
ug/L
37
010
MW-6
Aqueous
Nickel
6020B
11
ug/L
37
010
MW-6
Aqueous
Selenium
6020B
1.3
J
ug/L
37
010
MW-6
Aqueous
Zinc
6020B
6.1
J
ug/L
37
011
MW-4
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
450
mg CaCO3/1-
38
011
MW-4
Aqueous
Chloride
9056A
0.32
J
mg/L
38
011
MW-4
Aqueous
COD
SM 5220D-
20
mg/L
38
011
MW-4
Aqueous
TOC
SM 5310C-
6.3
mg/L
38
011
MW-4
Aqueous
1,4-Dioxane
8260D (SIM)
24
ug/L
38
011
MW-4
Aqueous
Benzene
8260D
0.86
J
ug/L
38
011
MW-4
Aqueous
Chlorobenzene
8260D
6.0
ug/L
39
011
MW-4
Aqueous
Chloroethane
8260D
2.0
ug/L
39
011
MW-4
Aqueous
1,2-Dichlorobenzene
8260D
0.73
J
ug/L
39
011
MW-4
Aqueous
1,4-Dichlorobenzene
8260D
9.5
ug/L
39
011
MW-4
Aqueous
1,1-Dichloroethane
8260D
7.2
ug/L
39
011
MW-4
Aqueous
cis- 1,2-Dichloroethene
8260D
16
ug/L
39
011
MW-4
Aqueous
Tetrachloroethene
8260D
1.2
B
ug/L
39
011
MW-4
Aqueous
Trichloroethene
8260D
0.82
J
ug/L
39
011
MW-4
Aqueous
Vinyl chloride
8260D
3.0
ug/L
39
011
MW-4
Aqueous
Barium
6020B
630
ug/L
40
011
MW-4
Aqueous
Cadmium
6020B
0.84
ug/L
40
011
MW-4
Aqueous
Cobalt
6020B
76
ug/L
40
011
MW-4
Aqueous
Nickel
6020B
93
ug/L
40
011
MW-4
Aqueous
Zinc
6020B
17
ug/L
40
012
MW-B
Aqueous
1,4-Dioxane
8260D (SIM)
22
ug/L
41
012
MW-B
Aqueous
Chloroethane
8260D
0.61
J
ug/L
41
012
MW-B
Aqueous
1,4-Dichlorobenzene
8260D
0.75
J
ug/L
41
012
MW-B
Aqueous
cis- 1,2-Dichloroethene
8260D
4.7
ug/L
41
012
MW-B
Aqueous
Tetrachloroethene
8260D
0.68
BJ
ug/L
42
012
MW-B
Aqueous
Vinyl chloride
8260D
2.3
ug/L
42
012
MW-B
Aqueous
Arsenic
6020B
1.4
J
ug/L
42
012
MW-B
Aqueous
Barium
6020B
290
ug/L
42
013
MW-12-25
Aqueous
cis-1,2-Dichloroethene
8260D
0.57
J
ug/L
44
013
MW-12-25
Aqueous
Tetrachloroethene
8260D
0.63
BJ
ug/L
44
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 175

Detection Summary (Continued)
Lot Number: WD30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
013
MW-12-25
Aqueous
Barium
6020B
58
ug/L
45
013
MW-12-25
Aqueous
Copper
6020B
1.3
J
ug/L
45
013
MW-12-25
Aqueous
Nickel
6020B
15
ug/L
45
013
MW-12-25
Aqueous
Zinc
6020B
9.1
J
ug/L
45
014
MW-13-35
Aqueous
Benzene
8260D
1.1
ug/L
46
014
MW-13-35
Aqueous
Chlorobenzene
8260D
5.0
ug/L
46
014
MW-13-35
Aqueous
1,2-Dichlorobenzene
8260D
3.1
ug/L
46
014
MW-13-35
Aqueous
1,4-Dichlorobenzene
8260D
16
ug/L
46
014
MW-13-35
Aqueous
cis-1,2-Dichloroethene
8260D
2.7
ug/L
46
014
MW-13-35
Aqueous
Tetrachloroethene
8260D
0.66
BJ
ug/L
46
014
MW-13-35
Aqueous
Vinyl chloride
8260D
0.61
J
ug/L
47
014
MW-13-35
Aqueous
Barium
6020B
180
ug/L
47
014
MW-13-35
Aqueous
Cobalt
6020B
1.3
J
ug/L
47
014
MW-13-35
Aqueous
Nickel
6020B
4.8
J
ug/L
47
014
MW-13-35
Aqueous
Zinc
6020B
8.0
J
ug/L
47
015
MW-13-132
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
150
mg CaCO3/1-
48
015
MW-13-132
Aqueous
Chloride
9056A
5.1
mg/L
48
015
MW-13-132
Aqueous
Nitrate - N
9056A
0.028
J
mg/L
48
015
MW-13-132
Aqueous
Sulfate
9056A
7.8
mg/L
48
015
MW-13-132
Aqueous
TOC
SM 5310C-
1.1
mg/L
48
015
MW-13-132
Aqueous
Benzene
8260D
1.0
ug/L
48
015
MW-13-132
Aqueous
Carbon disulfide
8260D
2.7
ug/L
48
015
MW-13-132
Aqueous
1,4-Dichlorobenzene
8260D
0.58
J
ug/L
49
015
MW-13-132
Aqueous
cis- 1,2-Dichloroethene
8260D
2.6
ug/L
49
015
MW-13-132
Aqueous
Tetrachloroethene
8260D
0.53
BJ
ug/L
49
015
MW-13-132
Aqueous
Vinyl chloride
8260D
0.91
J
ug/L
49
015
MW-13-132
Aqueous
Barium
6020B
41
ug/L
50
015
MW-13-132
Aqueous
Nickel
6020B
2.2
J
ug/L
50
015
MW-13-132
Aqueous
Zinc
6020B
6.9
J
ug/L
50
016
MW-17-60
Aqueous
1,4-Dioxane
8260D (SIM)
26
ug/L
51
016
MW-17-60
Aqueous
1,4-Dichlorobenzene
8260D
0.53
J
ug/L
51
016
MW-17-60
Aqueous
1, 1 -Dichloroethane
8260D
1.1
ug/L
51
016
MW-17-60
Aqueous
cis- 1,2-Dichloroethene
8260D
2.5
ug/L
51
016
MW-17-60
Aqueous
Tetrachloroethene
8260D
0.54
BJ
ug/L
52
016
MW-17-60
Aqueous
Vinyl chloride
8260D
1.2
ug/L
52
016
MW-17-60
Aqueous
Barium
6020B
24
ug/L
52
017
MW-17-137
Aqueous
1,4-Dioxane
8260D (SIM)
35
ug/L
54
017
MW-17-137
Aqueous
Chloroethane
8260D
0.43
J
ug/L
54
017
MW-17-137
Aqueous
1,4-Dichlorobenzene
8260D
0.68
J
ug/L
54
017
MW-17-137
Aqueous
1, 1 -Dichloroethane
8260D
0.78
J
ug/L
54
017
MW-17-137
Aqueous
cis-1,2-Dichloroethene
8260D
0.61
J
ug/L
54
017
MW-17-137
Aqueous
Tetrachloroethene
8260D
0.51
BJ
ug/L
55
017
MW-17-137
Aqueous
Vinyl chloride
8260D
0.74
J
ug/L
55
017
MW-17-137
Aqueous
Xylenes (total)
8260D
0.46
J
ug/L
55
017
MW-17-137
Aqueous
Barium
6020B
24
ug/L
55
018
MW-17-310
Aqueous
2-Butanone (MEK)
8260D
3.4
J
ug/L
57
018
MW-17-310
Aqueous
Barium
6020B
3.3
J
ug/L
58
018
MW-17-310
Aqueous
Lead
6020B
0.31
J
ug/L
58
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Page 7 of 175

Detection Summary (Continued)
Lot Number: WD30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
018
MW-17-310
Aqueous
Zinc
6020B
3.1
J
ug/L
58
019
MW-18-78
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
300
mg CaCO3/L
59
019
MW-18-78
Aqueous
BOD, 5 day
SM 5210B-
2.7
mg/L
59
019
MW-18-78
Aqueous
Chloride
9056A
150
mg/L
59
019
MW-18-78
Aqueous
COD
SM 5220D-
33
mg/L
59
019
MW-18-78
Aqueous
Sulfate
9056A
2.2
mg/L
59
019
MW-18-78
Aqueous
Sulfide
SM 4500-S2 F-
3.7
mg/L
59
019
MW-18-78
Aqueous
TOC
SM 5310C-
8.9
mg/L
59
019
MW-18-78
Aqueous
1,4-Dioxane
8260D (SIM)
53
ug/L
59
019
MW-18-78
Aqueous
Benzene
8260D
0.53
J
ug/L
59
019
MW-18-78
Aqueous
Chlorobenzene
8260D
4.0
ug/L
60
019
MW-18-78
Aqueous
Chloroethane
8260D
0.70
J
ug/L
60
019
MW-18-78
Aqueous
1,4-Dichlorobenzene
8260D
3.1
ug/L
60
019
MW-18-78
Aqueous
1, 1 -Dichloroethane
8260D
0.98
J
ug/L
60
019
MW-18-78
Aqueous
cis-1,2-Dichloroethene
8260D
0.95
J
ug/L
60
019
MW-18-78
Aqueous
Vinyl chloride
8260D
0.83
J
ug/L
60
019
MW-18-78
Aqueous
Barium
6020B
75
ug/L
61
019
MW-18-78
Aqueous
Nickel
6020B
7.2
ug/L
61
020
MW-19-75
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
410
mg CaCO3/1-
62
020
MW-19-75
Aqueous
Chloride
9056A
150
mg/L
62
020
MW-19-75
Aqueous
COD
SM 5220D-
40
mg/L
62
020
MW-19-75
Aqueous
Nitrate - N
9056A
0.012
J
mg/L
62
020
MW-19-75
Aqueous
Sulfate
9056A
17
mg/L
62
020
MW-19-75
Aqueous
TOC
SM 5310C-
12
mg/L
62
020
MW-19-75
Aqueous
1,4-Dioxane
8260D (SIM)
87
ug/L
62
020
MW-19-75
Aqueous
Acetone
8260D
5.2
JL
ug/L
62
020
MW-19-75
Aqueous
Chlorobenzene
8260D
4.2
ug/L
63
020
MW-19-75
Aqueous
1,4-Dichlorobenzene
8260D
3.2
ug/L
63
020
MW-19-75
Aqueous
1, 1 -Dichloroethane
8260D
0.47
J
ug/L
63
020
MW-19-75
Aqueous
Barium
6020B
120
ug/L
64
020
MW-19-75
Aqueous
Cobalt
6020B
3.4
J
ug/L
64
020
MW-19-75
Aqueous
Nickel
6020B
22
ug/L
64
020
MW-19-75
Aqueous
Zinc
6020B
5.5
J
ug/L
64
021
MW-19-110
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
170
mg CaCO3/1-
65
021
MW-19-110
Aqueous
Chloride
9056A
41
mg/L
65
021
MW-19-110
Aqueous
Sulfate
9056A
12
mg/L
65
021
MW-19-110
Aqueous
TOC
SM 5310C-
2.8
mg/L
65
021
MW-19-110
Aqueous
1,4-Dioxane
8260D (SIM)
35
ug/L
65
021
MW-19-110
Aqueous
Chlorobenzene
8260D
0.78
J
ug/L
66
021
MW-19-110
Aqueous
Chloroethane
8260D
0.87
J
ug/L
66
021
MW-19-110
Aqueous
1,4-Dichlorobenzene
8260D
0.76
J
ug/L
66
021
MW-19-110
Aqueous
cis- 1,2-Dichloroethene
8260D
0.93
J
ug/L
66
021
MW-19-110
Aqueous
Barium
6020B
11
ug/L
67
021
MW-19-110
Aqueous
Nickel
6020B
4.1
J
ug/L
67
021
MW-19-110
Aqueous
Zinc
6020B
7.5
J
ug/L
67
022
MW-21-21
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
770
mg CaCO3/L
68
022
MW-21-21
Aqueous
BOD, 5 day
SM 521013-
3.7
mg/L
68
022
MW-21-21
Aqueous
Chloride
9056A
70
mg/L
68
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Page 8 of 175

Detection Summary (Continued)
Lot Number: WD30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
022
MW-21-21
Aqueous
COD
SM 5220D-
58
mg/L
68
022
MW-21-21
Aqueous
Sulfate
9056A
23
mg/L
68
022
MW-21-21
Aqueous
Sulfide
SM 4500-S2 F-
1.5
mg/L
68
022
MW-21-21
Aqueous
TOC
SM 5310C-
15
mg/L
68
022
MW-21-21
Aqueous
1,4-Dioxane
8260D (SIM)
30
ug/L
68
022
MW-21-21
Aqueous
Benzene
8260D
2.8
ug/L
68
022
MW-21-21
Aqueous
Carbon disulfide
8260D
0.53
J
ug/L
69
022
MW-21-21
Aqueous
Chlorobenzene
8260D
32
ug/L
69
022
MW-21-21
Aqueous
1,2-Dichlorobenzene
8260D
4.0
ug/L
69
022
MW-21-21
Aqueous
1,4-Dichlorobenzene
8260D
14
ug/L
69
022
MW-21-21
Aqueous
1,1-Dichloroethane
8260D
2.8
ug/L
69
022
MW-21-21
Aqueous
1,2-Dichloroethane
8260D
0.43
J
ug/L
69
022
MW-21-21
Aqueous
cis- 1,2-Dichloroethene
8260D
5.8
ug/L
69
022
MW-21-21
Aqueous
Toluene
8260D
0.66
J
ug/L
69
022
MW-21-21
Aqueous
Trichloroethene
8260D
0.51
J
ug/L
69
022
MW-21-21
Aqueous
Vinyl chloride
8260D
2.2
ug/L
69
022
MW-21-21
Aqueous
Xylenes (total)
8260D
0.60
J
ug/L
69
022
MW-21-21
Aqueous
Barium
6020B
120
ug/L
70
022
MW-21-21
Aqueous
Cobalt
6020B
12
ug/L
70
022
MW-21-21
Aqueous
Nickel
6020B
4.6
J
ug/L
70
022
MW-21-21
Aqueous
Zinc
6020B
2.7
J
ug/L
70
023
MW-21-94
Aqueous
Alkalinity @ pH 4.5 su
SM 2320B-
310
mg CaCO3/L
71
023
MW-21-94
Aqueous
Chloride
9056A
98
mg/L
71
023
MW-21-94
Aqueous
COD
SM 5220D-
28
mg/L
71
023
MW-21-94
Aqueous
Sulfate
9056A
3.3
mg/L
71
023
MW-21-94
Aqueous
Sulfide
SM 4500-S2 F-
2.6
mg/L
71
023
MW-21-94
Aqueous
TOC
SM 5310C-
7.3
mg/L
71
023
MW-21-94
Aqueous
1,4-Dioxane
8260D (SIM)
46
ug/L
71
023
MW-21-94
Aqueous
Chlorobenzene
8260D
1.8
ug/L
72
023
MW-21-94
Aqueous
Chloroethane
8260D
2.3
ug/L
72
023
MW-21-94
Aqueous
1,2-Dichlorobenzene
8260D
0.44
J
ug/L
72
023
MW-21-94
Aqueous
1,4-Dichlorobenzene
8260D
2.8
ug/L
72
023
MW-21-94
Aqueous
1,1-Dichloroethane
8260D
1.2
ug/L
72
023
MW-21-94
Aqueous
1,2-Dichloroethane
8260D
0.42
J
ug/L
72
023
MW-21-94
Aqueous
cis- 1,2-Dichloroethene
8260D
2.9
ug/L
72
023
MW-21-94
Aqueous
Vinyl chloride
8260D
1.2
ug/L
72
023
MW-21-94
Aqueous
Barium
6020B
47
ug/L
73
023
MW-21-94
Aqueous
Nickel
6020B
8.0
ug/L
73
024
MW-24-160
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
70
mg CaCO3/L
74
024
MW-24-160
Aqueous
Chloride
9056A
6.5
mg/L
74
024
MW-24-160
Aqueous
Sulfate
9056A
23
mg/L
74
024
MW-24-160
Aqueous
Sulfide
SM 4500-S2 F-
1.8
mg/L
74
024
MW-24-160
Aqueous
TOC
SM 5310C-
1.4
mg/L
74
024
MW-24-160
Aqueous
Barium
6020B
27
ug/L
76
024
MW-24-160
Aqueous
Copper
6020B
1.3
J
ug/L
76
024
MW-24-160
Aqueous
Lead
6020B
0.74
J
ug/L
76
024
MW-24-160
Aqueous
Nickel
6020B
1.6
J
ug/L
76
024
MW-24-160
Aqueous
Zinc
6020B
7.2
J
ug/L
76
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 175

Detection Summary (Continued)
Lot Number: WD30017
Sample Sample ID Matrix Parameter Method Result Q Units Page
025 Field Blank Aqueous Barium 6020B 2.8 J ug/L 78
(286 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-001
Description: DPL-1 Matrix: Aqueous
Date Sampled:04/28/2021 1515
Date Received:04/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
2 5030B
8260D (SIM) 1 05/04/2021 2318 CJL2
91160
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
2
Run 2 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211158 BWS
91880
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
11 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-001
Description: DPL-1 Matrix: Aqueous
Date Sampled:04/28/2021 1515
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211158 BWS 91880
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
105 70-130
1,2-Dichloroethane-d4
90 70-130
Toluene-d8
95 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/03/2021 1833 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
0.80 J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
85
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
55
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
4.0 J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
5.6
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
2.1
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
53
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-001
Description: DPL-1 Matrix: Aqueous
Date Sampled:04/28/2021 1515
Date Received:04/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1833 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
14
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-002
Description: MW-3 Matrix: Aqueous
Date Sampled:04/28/2021 1430
Date Received:04/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0245 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
95
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
98 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211223 BWS
91880
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
1.6
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
4.4
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
3.2
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
0.83 J
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
7.2
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
1.3
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
0.65 J
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-002
Description: MW-3 Matrix: Aqueous
Date Sampled:04/28/2021 1430
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211223 BWS 91880
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.72 J
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
0.89 J
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
107 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
96 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/03/2021 1839 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
240
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.19 J
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
15
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
32
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-002
Description: MW-3 Matrix: Aqueous
Date Sampled:04/28/2021 1430
Date Received:04/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1839 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
1.9 J
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
25
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-003
Description: MW-4A Matrix: Aqueous
Date Sampled:04/28/2021 1455
Date Received:04/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0310 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
31
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211248 BWS
91880
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
5.6
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
28
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
4.4
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
25
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5 8260D
0.44 J
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-003
Description: MW-4A Matrix: Aqueous
Date Sampled:04/28/2021 1455
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211248 BWS 91880
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
6.8
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
4.9 J
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
2.7
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
1.0
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
12
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
110 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
96 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/03/2021 1845 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
670
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.18 J
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
48
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
4.0 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
9.7
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-003
Description: MW-4A Matrix: Aqueous
Date Sampled:04/28/2021 1455
Date Received:04/29/2021
ICP-MS Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2021 1845 BNW 05/03/2021 0426 90835
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Selenium
7782-49-2
Silver
7440-22-4
Thallium
7440-28-0
Vanadium
7440-62-2
Zinc
7440-66-6
6020B
ND
5.0
1.3
ug/L 1
6020B
ND
1.0
0.25
ug/L 1
6020B
ND
0.50
0.15
ug/L 1
6020B
ND
5.0
2.5
ug/L 1
6020B
2.7 J
10
2.5
ug/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-004
Description: MW-5 Matrix: Aqueous
Date Sampled:04/28/2021 1355
Date Received:04/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0334 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
73
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
98 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211313 BWS
91880
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
0.86 J
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
8.7
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
1.0 J
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
4.8
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
0.51 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-004
Description: MW-5 Matrix: Aqueous
Date Sampled:04/28/2021 1355
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211313 BWS 91880
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
111 70-130
1,2-Dichloroethane-d4
95 70-130
Toluene-d8
99 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/03/2021 1851 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
170
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
11
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
19
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-004
Description: MW-5 Matrix: Aqueous
Date Sampled:04/28/2021 1355
Date Received:04/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1851 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
2.1 J
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-005
Description: MW-6-192 Matrix: Aqueous
Date Sampled:04/28/2021 1615
Date Received:04/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
2 5030B
8260D (SIM) 1 05/04/2021 2342 CJL2
91160
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
5.6
3.0
1.0
ug/L
2
Run 2 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211338 BWS
91880
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
0.96 J
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
0.65 J
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
0.43 J
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
0.69 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-005
Description: MW-6-192 Matrix: Aqueous
Date Sampled:04/28/2021 1615
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211338 BWS 91880
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
109 70-130
1,2-Dichloroethane-d4
95 70-130
Toluene-d8
98 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/03/2021 1857 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
61
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
1.5 J
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-005
Description: MW-6-192 Matrix: Aqueous
Date Sampled:04/28/2021 1615
Date Received:04/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1857 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-006
Description: MW-7 Matrix: Aqueous
Date Sampled:04/28/2021 1700
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20210312 CJL2 91967
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
2.4
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
13
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
3.4
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
5.8
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
2.1
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
20
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-006
Description: MW-7 Matrix: Aqueous
Date Sampled:04/28/2021 1700
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20210312 CJL2
91967
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
0.60 J
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
0.54 J
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
100 70-130
1,2-Dichloroethane-d4
109 70-130
Toluene-d8
106 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1903 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
180
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
0.20 J
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.14 J
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
200
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
14
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.45 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
57
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
13
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-007
Description: MW-15 Matrix: Aqueous
Date Sampled:04/28/2021 1305
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20210337 CJL2 91967
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
12 J
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-007
Description: MW-15 Matrix: Aqueous
Date Sampled:04/28/2021 1305
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20210337 CJL2
91967
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
100 70-130
1,2-Dichloroethane-d4
109 70-130
Toluene-d8
107 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1407 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
220
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
12
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
1.2
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND S
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-009
Description: MW-2 Matrix: Aqueous
Date Sampled:04/29/2021 1000
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 05/01/2021 1458 DAK
90903
1 (BOD, 5 day) SM 521OB-2011
1 05/05/2021 1709 SJL
04/30/2021 1957
90831
1 (Chloride) 9056A
1 05/01/2021 0646 AMR
90993
1 (COD) SM 5220D-2011
1 05/04/2021 1527 AMR
91121
1 (Nitrate - N) 9056A
1 05/01/2021 0646 AMR
90992
1 (Sulfate) 9056A
1 05/01/2021 0646 AMR
90994
1 (Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1 (TOC) SM 531OC-2011
1 05/01/2021 0013 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 232OB-2011
64
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521OB-2011
ND 47
2.0
0.18
mg/L
1
Chloride
9056A
2.4
1.0
0.25
mg/L
1
COD
SM 5220D-2011
ND
20
20
mg/L
1
Nitrate - N
9056A
0.027
0.020
0.0050
mg/L
1
Sulfate
9056A
3.2
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
1.2
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
11
1.0
1.0
mg/L
1
Volatile Organic Compounds
by GUMS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 05/12/20210402 CJL2
91967
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL
= Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J =
Estimated result
< LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-009
Description: MW-2 Matrix: Aqueous
Date Sampled:04/29/2021 1000
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20210402 CJL2 91967
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
102
70-130
1,2-Dichloroethane-d4
110
70-130
Toluene-d8
108
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 3005A
6020B
1 05/07/2021 1445 BPK 05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method Result Q
LOQ DL
Units Run
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-009
Description: MW-2 Matrix: Aqueous
Date Sampled:04/29/2021 1000
Date Received:04/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep
Date
Batch
1 3005A
6020B 1 05/07/2021 1445 BPK
05/07/2021
0324 90837
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
1.0
J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
25
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
2.2
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
2.7
J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.77
J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
7.5
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
8.9
J
10
2.5
ug/L
1
Footnote(s): 4-Blank depletion > 0.20 mg/L 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-010
Description: MW-6 Matrix: Aqueous
Date Sampled:04/29/2021 1205
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 05/01/2021 1513 DAK
90903
1
(BOD, 5 day) SM 521OB-2011
1 05/05/2021 1711 SJL
04/30/2021 2010
90831
1
(Chloride) 9056A
1 05/01/2021 0846 AMR
90993
2
(COD) SM 5220D-2011
1 05/06/2021 0853 AMR
91352
2
(Nitrate - N) 9056A
10 05/04/2021 1557 AMR
91255
1
(Sulfate) 9056A
1 05/01/2021 0846 AMR
90994
1
(Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1
(TOC) SM 531OC-2011
1 05/01/2021 0027 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
570
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
6.6 47
2.0
0.18
mg/L
1
Chloride
9056A
160
1.0
0.25
mg/L
1
COD
SM 5220D-2011
42
20
20
mg/L
2
Nitrate - N
9056A
ND H
0.20
0.050
mg/L
2
Sulfate
9056A
1.1
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
15
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0423 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
33
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
99 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20211248 BWS
92056
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
1.3
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-010
Description: MW-6 Matrix: Aqueous
Date Sampled:04/29/2021 1205
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211248 BWS 92056
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
4.2
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
7.5
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
3.5
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
2.6
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
1.8
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
1.4
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
0.87 BJ
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-010
Description: MW-6 Matrix: Aqueous
Date Sampled:04/29/2021 1205
Date Received:04/30/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
98 70-130
1,2-Dichloroethane-d4
87 70-130
Toluene-d8
89 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1452 BPK
05/07/2021 0324
90837
2 3005A
6020B 10 05/07/2021 1721 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
1700
50
13
ug/L
2
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
11
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
1.3 J
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
6.1 J
10
2.5
ug/L
1
Footnote(s): 4-Blank depletion > 0.20 mg/L 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-011
Description: MW-4 Matrix: Aqueous
Date Sampled:04/29/2021 1410
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 05/01/2021 1530 DAK
90903
1
(BOD, 5 day) SM 521OB-2011
1 05/05/2021 2027 SJL
04/30/2021 2311 90869
1
(Chloride) 9056A
1 05/01/2021 1005 AMR
90993
2
(COD) SM 5220D-2011
1 05/06/2021 0854 AMR
91352
1
(Nitrate - N) 9056A
1 05/01/2021 1005 AMR
90992
1
(Sulfate) 9056A
1 05/01/2021 1005 AMR
90994
1
(Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1
(TOC) SM 531OC-2011
1 05/01/2021 0106 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
450
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521OB-2011
ND
2.0
0.18
mg/L
1
Chloride
9056A
0.32 J
1.0
0.25
mg/L
1
COD
SM 5220D-2011
20
20
20
mg/L
2
Nitrate - N
9056A
ND
0.020
0.0050
mg/L
1
Sulfate
9056A
ND
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
6.3
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0448 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
24
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20211313 BWS
92056
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
0.86 J
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 36 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-011
Description: MW-4 Matrix: Aqueous
Date Sampled:04/29/2021 1410
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211313 BWS 92056
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
6.0
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
2.0
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
0.73 J
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
9.5
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
7.2
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
16
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
1.2 B
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
0.82 J
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
3.0
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 37 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-011
Description: MW-4 Matrix: Aqueous
Date Sampled:04/29/2021 1410
Date Received:04/30/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
106 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
97 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1459 BPK
05/07/2021 0324
90837
2 3005A
6020B 10 05/07/2021 1728 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
630
50
13
ug/L
2
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.84
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
76
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
93
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
17
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 38 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-012
Description: MW-B Matrix: Aqueous
Date Sampled:04/29/2021 1630
Date Received:04/30/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0513 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
22
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
102 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20211338 BWS
92056
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
0.61 J
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
0.75 J
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
4.7
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-012
Description: MW-B Matrix: Aqueous
Date Sampled:04/29/2021 1630
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211338 BWS 92056
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.68 BJ
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
2.3
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
103 70-130
1,2-Dichloroethane-d4
90 70-130
Toluene-d8
94 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/07/2021 1522 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
1.4 J
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
290
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-012
Description: MW-B Matrix: Aqueous
Date Sampled:04/29/2021 1630
Date Received:04/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1522 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-013
Description: MW-12-25 Matrix: Aqueous
Date Sampled:04/29/2021 0930
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211403 BWS 92056
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
0.57 J
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
0.63 BJ
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 42 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-013
Description: MW-12-25 Matrix: Aqueous
Date Sampled:04/29/2021 0930
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20211403 BWS
92056
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
104 70-130
1,2-Dichloroethane-d4
91 70-130
Toluene-d8
96 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1529 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
58
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.3 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
15
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
9.1 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-014
Description: MW-13-35 Matrix: Aqueous
Date Sampled:04/29/2021 1030
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211428 BWS 92056
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
1.1
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
5.0
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
3.1
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
16
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
2.7
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
0.66 BJ
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 44 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-014
Description: MW-13-35 Matrix: Aqueous
Date Sampled:04/29/2021 1030
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20211428 BWS
92056
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
0.61 J
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
104 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
97 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1537 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
180
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
1.3 J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
4.8 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
8.0 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-015
Description: MW-13-132 Matrix: Aqueous
Date Sampled:04/29/2021 1355
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 05/01/2021 1537 DAK
90903
1 (BOD, 5 day) SM 521OB-2011
1 05/05/2021 2028 SJL
04/30/2021 2315 90869
2 (Chloride) 9056A
1 05/04/2021 1617 AMR
91200
1 (COD) SM 5220D-2011
1 05/04/2021 1527 AMR
91121
1 (Nitrate - N) 9056A
5 05/01/2021 0746 AMR
90992
1 (Sulfate) 9056A
5 05/01/2021 0746 AMR
90994
1 (Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1 (TOC) SM 531OC-2011
1 05/01/2021 0119 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 232OB-2011
150
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521OB-2011
ND
2.0
0.18
mg/L
1
Chloride
9056A
5.1
1.0
0.25
mg/L
2
COD
SM 5220D-2011
ND
20
20
mg/L
1
Nitrate - N
9056A
0.028 J
0.10
0.025
mg/L
1
Sulfate
9056A
7.8
5.0
1.3
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
1.1
1.0
1.0
mg/L
1
Volatile Organic Compounds
by GUMS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 05/12/20211453 BWS
92056
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
1.0
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
2.7
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J = Estimated result
< LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 46 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-015
Description: MW-13-132 Matrix: Aqueous
Date Sampled:04/29/2021 1355
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211453 BWS 92056
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
0.58 J
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
2.6
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
0.53 BJ
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
0.91 J
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
105
70-130
1,2-Dichloroethane-d4
89
70-130
Toluene-d8
95
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 3005A
6020B
1 05/07/2021 1544 BPK 05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method Result Q
LOQ DL
Units Run
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 47 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-015
Description: MW-13-132 Matrix: Aqueous
Date Sampled:04/29/2021 1355
Date Received:04/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1544 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
41
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
2.2 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
6.9 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 48 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-016
Description: MW-17-60 Matrix: Aqueous
Date Sampled:04/29/2021 1455
Date Received:04/30/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0538 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
26
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
101 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20211518 BWS
92056
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
0.53 J
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
1.1
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
2.5
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 49 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-016
Description: MW-17-60 Matrix: Aqueous
Date Sampled:04/29/2021 1455
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211518 BWS 92056
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.54 BJ
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
1.2
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
109 70-130
1,2-Dichloroethane-d4
94 70-130
Toluene-d8
101 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/07/2021 1551 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
24
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 50 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-016
Description: MW-17-60 Matrix: Aqueous
Date Sampled:04/29/2021 1455
Date Received:04/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1551 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 51 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-017
Description: MW-17-137 Matrix: Aqueous
Date Sampled:04/29/2021 1355
Date Received:04/30/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0602 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
35
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20211543 BWS
92056
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
0.43 J
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
0.68 J
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
0.78 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
0.61 J
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 52 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-017
Description: MW-17-137 Matrix: Aqueous
Date Sampled:04/29/2021 1355
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211543 BWS 92056
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.51 BJ
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.74 J
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
0.46 J
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
107 70-130
1,2-Dichloroethane-d4
95 70-130
Toluene-d8
99 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/07/2021 1559 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
24
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 53 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-017
Description: MW-17-137 Matrix: Aqueous
Date Sampled:04/29/2021 1355
Date Received:04/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1559 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 54 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-018
Description: MW-17-310 Matrix: Aqueous
Date Sampled:04/29/2021 1310
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20211510 TML 92034
2 5030B 8260D 1 05/13/20211411 BWS 92201
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
3.4 J
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 55 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-018
Description: MW-17-310 Matrix: Aqueous
Date Sampled:04/29/2021 1310
Date Received:04/30/2021
Volatile Organic Compounds by
GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20211510 TML
92034
2 5030B
8260D 1 05/13/20211411 BWS
92201
CAS Analytical
Parameter
Number Method Result
Q
LOQ
DL
Units
Run
1,1,1-Trichloroethane
71-55-6 8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance Run 2
Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
Bromofluorobenzene
98 70-130 112
70-130
1,2-Dichloroethane-d4
92 70-130 91
70-130
Toluene-d8
96 70-130 98
70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1606 BPK 05/07/2021
0324
90837
CAS Analytical
Parameter
Number Method Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
3.3 J
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.31 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
3.1 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 56 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-019
Description: MW-18-78 Matrix: Aqueous
Date Sampled:04/29/2021 1010
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 05/01/2021 1545 DAK
90903
1
(BOD, 5 day) SM 521OB-2011
1 05/05/2021 2032 SJL
04/30/2021 2321 90869
1
(Chloride) 9056A
1 05/01/2021 0706 AMR
90993
2
(COD) SM 5220D-2011
1 05/06/2021 0854 AMR
91352
1
(Nitrate - N) 9056A
1 05/01/2021 0706 AMR
90992
1
(Sulfate) 9056A
1 05/01/2021 0706 AMR
90994
1
(Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1
(TOC) SM 531OC-2011
1 05/01/2021 0132 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
300
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
2.7
2.0
0.18
mg/L
1
Chloride
9056A
150
1.0
0.25
mg/L
1
COD
SM 5220D-2011
33
20
20
mg/L
2
Nitrate - N
9056A
ND
0.020
0.0050
mg/L
1
Sulfate
9056A
2.2
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
3.7
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
8.9
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0627 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
53
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/13/20210245 JDF
92125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
0.53 J
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 57 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-019
Description: MW-18-78 Matrix: Aqueous
Date Sampled:04/29/2021 1010
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210245 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
4.0
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
0.70
J
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
L
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
3.1
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
0.98
J
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
0.95
J
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
0.83
J
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 58 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-019
Description: MW-18-78 Matrix: Aqueous
Date Sampled:04/29/2021 1010
Date Received:04/30/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
96 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
98 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1614 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
75
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
7.2
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 59 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-020
Description: MW-19-75 Matrix: Aqueous
Date Sampled:04/29/2021 1145
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 05/01/2021 1552 DAK
90903
1
(BOD, 5 day) SM 521OB-2011
1 05/05/2021 2035 SJL
04/30/2021 2327 90869
1
(Chloride) 9056A
1 05/01/2021 0906 AMR
90993
2
(COD) SM 5220D-2011
1 05/06/2021 0854 AMR
91352
1
(Nitrate - N) 9056A
1 05/01/2021 0906 AMR
90992
1
(Sulfate) 9056A
1 05/01/2021 0906 AMR
90994
1
(Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1
(TOC) SM 531OC-2011
1 05/01/2021 0145 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
410
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521OB-2011
ND
2.0
0.18
mg/L
1
Chloride
9056A
150
1.0
0.25
mg/L
1
COD
SM 5220D-2011
40
20
20
mg/L
2
Nitrate - N
9056A
0.012 J
0.020
0.0050
mg/L
1
Sulfate
9056A
17
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
12
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0651 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
87
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/13/20210308 JDF
92125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
5.2 JL
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 60 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-020
Description: MW-19-75 Matrix: Aqueous
Date Sampled:04/29/2021 1145
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210308 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
4.2
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND L
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
3.2
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
0.47 J
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 61 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-020
Description: MW-19-75 Matrix: Aqueous
Date Sampled:04/29/2021 1145
Date Received:04/30/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
91 70-130
Toluene-d8
95 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1621 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
120
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
3.4 J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
22
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
5.5 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 62 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-021
Description: MW-19-110 Matrix: Aqueous
Date Sampled:04/29/2021 1310
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 05/01/2021 1559 DAK
90903
1
(BOD, 5 day) SM 521OB-2011
1 05/05/2021 2055 SJL
04/30/2021 2334 90869
1
(Chloride) 9056A
1 05/01/2021 0925 AMR
90993
2
(COD) SM 5220D-2011
1 05/06/2021 0854 AMR
91352
1
(Nitrate - N) 9056A
1 05/01/2021 0925 AMR
90992
1
(Sulfate) 9056A
1 05/01/2021 0925 AMR
90994
1
(Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1
(TOC) SM 531OC-2011
1 05/01/2021 0158 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 232OB-2011
170
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521OB-2011
ND
2.0
0.18
mg/L
1
Chloride
9056A
41
1.0
0.25
mg/L
1
COD
SM 5220D-2011
ND
20
20
mg/L
2
Nitrate - N
9056A
ND
0.020
0.0050
mg/L
1
Sulfate
9056A
12
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
2.8
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0716 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
35
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/13/20210330 JDF
92125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 63 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-021
Description: MW-19-110 Matrix: Aqueous
Date Sampled:04/29/2021 1310
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210330 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
0.78
J
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
0.87
J
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
L
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
0.76
J
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
0.93
J
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 64 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-021
Description: MW-19-110 Matrix: Aqueous
Date Sampled:04/29/2021 1310
Date Received:04/30/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
98 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1629 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
11
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
4.1 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
7.5 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 65 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-022
Description: MW-21-21 Matrix: Aqueous
Date Sampled:04/29/2021 1220
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 05/01/2021 1609 DAK
90903
1
(BOD, 5 day) SM 521OB-2011
1 05/05/2021 2100 SJL
04/30/2021 2336
90869
1
(Chloride) 9056A
5 05/01/2021 0945 AMR
90993
1
(COD) SM 5220D-2011
1 05/04/2021 1543 AMR
91123
1
(Nitrate - N) 9056A
5 05/01/2021 0945 AMR
90992
1
(Sulfate) 9056A
5 05/01/2021 0945 AMR
90994
1
(Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1
(TOC) SM 531OC-2011
1 05/01/2021 0211 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
770
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
3.7
2.0
0.18
mg/L
1
Chloride
9056A
70
5.0
1.3
mg/L
1
COD
SM 5220D-2011
58
20
20
mg/L
1
Nitrate - N
9056A
ND
0.10
0.025
mg/L
1
Sulfate
9056A
23
5.0
1.3
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
1.5
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
15
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0741 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
30
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/13/20210352 JDF
92125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
2.8
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 66 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-022
Description: MW-21-21 Matrix: Aqueous
Date Sampled:04/29/2021 1220
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210352 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
0.53
J
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
32
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
L
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
4.0
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
14
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
2.8
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
0.43
J
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
5.8
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
0.66
J
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
0.51
J
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
2.2
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
0.60
J
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 67 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-022
Description: MW-21-21 Matrix: Aqueous
Date Sampled:04/29/2021 1220
Date Received:04/30/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
96 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1651 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
120
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
12
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
4.6 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
2.7 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 68 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-023
Description: MW-21-94 Matrix: Aqueous
Date Sampled:04/29/2021 1045
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 05/01/2021 1617 DAK
90903
1
(BOD, 5 day) SM 521OB-2011
1 05/05/2021 2106 SJL
04/30/2021 2359 90869
1
(Chloride) 9056A
1 05/01/2021 0726 AMR
90993
2
(COD) SM 5220D-2011
1 05/06/2021 0855 AMR
91352
1
(Nitrate - N) 9056A
1 05/01/2021 0726 AMR
90992
1
(Sulfate) 9056A
1 05/01/2021 0726 AMR
90994
1
(Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1
(TOC) SM 531OC-2011
1 05/01/2021 0225 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
310
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521OB-2011
ND
2.0
0.18
mg/L
1
Chloride
9056A
98
1.0
0.25
mg/L
1
COD
SM 5220D-2011
28
20
20
mg/L
2
Nitrate - N
9056A
ND
0.020
0.0050
mg/L
1
Sulfate
9056A
3.3
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
2.6
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
7.3
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 1320 TML
91095
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
46
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
100 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/13/20210415 JDF
92125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 69 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-023
Description: MW-21-94 Matrix: Aqueous
Date Sampled:04/29/2021 1045
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210415 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
1.8
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
2.3
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND L
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
0.44 J
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
2.8
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
1.2
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
0.42 J
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
2.9
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
1.2
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 70 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-023
Description: MW-21-94 Matrix: Aqueous
Date Sampled:04/29/2021 1045
Date Received:04/30/2021
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
96 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
97 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1658 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
47
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
8.0
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 71 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-024
Description: MW-24-160 Matrix: Aqueous
Date Sampled:04/29/2021 1645
)ate Received:04/30/2021
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 05/01/2021 1623 DAK
90903
1 (BOD, 5 day) SM 521OB-2011
1 05/05/2021 2108 SJL
05/01/2021 0001
90869
1 (Chloride) 9056A
1 05/01/2021 1025 AMR
90993
1 (COD) SM 5220D-2011
1 05/04/2021 1527 AMR
91121
1 (Nitrate - N) 9056A
1 05/01/2021 1025 AMR
90992
1 (Sulfate) 9056A
1 05/01/2021 1025 AMR
90994
1 (Sulfide) SM 4500-S2 F-2011
1 05/05/2021 2008 GDC
91461
1 (TOC) SM 531OC-2011
1 05/01/2021 0238 AAB
90858
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 232OB-2011
70
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521OB-2011
ND
2.0
0.18
mg/L
1
Chloride
9056A
6.5
1.0
0.25
mg/L
1
COD
SM 5220D-2011
ND
20
20
mg/L
1
Nitrate - N
9056A
ND
0.020
0.0050
mg/L
1
Sulfate
9056A
23
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
1.8
1.0
1.0
mg/L
1
TOC
SM 531OC-2011
1.4
1.0
1.0
mg/L
1
Volatile Organic Compounds
by GUMS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 05/13/20210437 JDF
92125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL
= Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J =
Estimated result
< LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 72 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-024
Description: MW-24-160 Matrix: Aqueous
Date Sampled:04/29/2021 1645
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210437 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND L
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
99
70-130
1,2-Dichloroethane-d4
92
70-130
Toluene-d8
96
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 3005A
6020B
1 05/07/2021 1706 BPK 05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method Result Q
LOQ DL
Units Run
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 73 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-024
Description: MW-24-160 Matrix: Aqueous
Date Sampled:04/29/2021 1645
Date Received:04/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep
Date
Batch
1 3005A
6020B 1 05/07/2021 1706 BPK
05/07/2021
0324 90837
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
27
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.3
J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.74
J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
1.6
J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
7.2
J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 74 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-025
Description: Field Blank Matrix: Aqueous
Date Sampled:04/29/2021 1300
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20211136 BWS 92172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND L
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND L
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 75 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-025
Description: Field Blank Matrix: Aqueous
Date Sampled:04/29/2021 1300
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/13/20211136 BWS
92172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
101 70-130
1,2-Dichloroethane-d4
108 70-130
Toluene-d8
106 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/07/2021 1713 BPK
05/07/2021 0324 90837
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
2.8 J
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 76 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-026
Description: Trip Blank Matrix: Aqueous
Date Sampled:04/29/2021
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210201 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND L
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 77 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-026
Description: Trip Blank Matrix: Aqueous
Date Sampled:04/29/2021
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210201 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
95 70-130
90 70-130
94 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 78 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-027
Description: Trip Blank Matrix: Aqueous
Date Sampled:04/29/2021
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210223 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND L
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 79 of 175

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30017-027
Description: Trip Blank Matrix: Aqueous
Date Sampled:04/29/2021
Date Received:04/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/13/20210223 JDF 92125
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
97 70-130
92 70-130
98 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 80 of 175

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 81 of 175

Inorganic non-metals - BOD Blank and GGA
Matrix: Aqueous
Batch: 90831 SCF: 0.6
Analytical Method: SM 521 OB-2011 SCF Range: 0.6 - 1.0
Result
Avg. Result
Sample ID
Depl
Avg. Depl (mg/L)
(mg/L) Q
Limit
Prep Date
Analysis Date
WQ90831-041 (Blank)
0.21
4
0.2
04/30/2021 1809
05/05/2021 1556
WQ90831-141 (Blank)
0.26
4
0.2
04/30/2021 1809
05/05/2021 1556
WQ90831-241 (Blank)
0.21
0.23
4
0.2
04/30/2021 1809
05/05/2021 1556
WQ90831-035 (GGA)
169.2
47
167.5-228.5
04/30/2021 1816
05/05/2021 1600
WQ90831-135 (GGA)
180.2
47
167.5-228.5
04/30/2021 1816
05/05/2021 1559
WQ90831-235 (GGA)
191.7
180.4 47
167.5-228.5
04/30/2021 1817
05/05/2021 1600
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 82 of 175

Inorganic non-metals - MB
Sample ID: WQ90858-001 Matrix: Aqueous
Batch: 90858
Analytical Method: SM 531 OC-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
TOC ND 1 1.0 1.0 mg/L 04/30/2021 2241
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 83 of 175

Inorganic non-metals - LCS
Sample ID: WQ90858-002 Matrix: Aqueous
Batch: 90858
Analytical Method: SM 531 OC-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TOC 20 19 1 97 90-110 04/30/2021 2254
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 84 of 175

Inorganic non-metals - BOD Blank and GGA
Matrix: Aqueous
Batch: 90869 SCF: 0.5
Analytical Method: SM 521 OB-2011 SCF Range: 0.6 - 1.0
Result Avg. Result
Sample ID
Depl
Avg. Depl (mg/L) (mg/L) Q
Limit
Prep Date
Analysis Date
WQ90869-041 (Blank)
0.31
4
0.2
04/30/2021 2255
05/05/2021 2016
WQ90869-141 (Blank)
0.17
0.2
04/30/2021 2255
05/05/2021 2016
WQ90869-241 (Blank)
0.05
0.18
0.2
04/30/2021 2256
05/05/2021 2016
WQ90869-035 (GGA)
162.1 1
167.5-228.5
04/30/2021 2302
05/05/2021 2020
WQ90869-135 (GGA)
178.6
167.5-228.5
04/30/2021 2302
05/05/2021 2020
WQ90869-235 (GGA)
181.6 174.1
167.5-228.5
04/30/2021 2303
05/05/2021 2020
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 85 of 175

Inorganic non-metals - LCS
Sample ID: WQ90903-002 Matrix: Aqueous
Batch: 90903
Analytical Method: SM 2320B-2011
Spike
Amount Result %Rec
Parameter (mg CaCO3/L) (mg CaCO3/L) Q Dil % Rec Limit Analysis Date
Alkalinity @ pH 4.5 su 100 100 1 100 90-110 05/01/2021 1419
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 86 of 175

Inorganic non-metals - Duplicate
Sample ID: WD30017-009DU Matrix: Aqueous
Batch: 90903
Analytical Method: SM 2320B-2011
Sample
Amount Result %RPD
Parameter (mg CaCO3/L) (mg CaCO3/L) 0 Dil % RPD Limit Analysis Date
Alkalinity @ pH 4.5 su 64 64 1 0.090 20 05/01/2021 1505
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 87 of 175

Inorganic non-metals - MB
Sample ID: WQ90992-001 Matrix: Aqueous
Batch: 90992
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Nitrate - N ND 1 0.020 0.0050 mg/L 05/01/2021 0426
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 88 of 175

Inorganic non-metals - LCS
Sample ID: WQ90992-002 Matrix: Aqueous
Batch: 90992
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.80 0.85 1 106 80-120 05/01/2021 0606
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 89 of 175

Inorganic non-metals - LCSD
Sample ID: WQ90992-003 Matrix: Aqueous
Batch: 90992
Analytical Method: 9056A
Spike
Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Nitrate - N 0.80 0.81 1 101 4.8 80-120 20 05/01/2021 0626
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 90 of 175

Inorganic non-metals - MB
Sample ID: WQ90993-001 Matrix: Aqueous
Batch: 90993
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride ND 1 1.0 0.25 mg/L 05/01/2021 0426
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 91 of 175

Inorganic non-metals - LCS
Sample ID: WQ90993-002 Matrix: Aqueous
Batch: 90993
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 21 1 103 80-120 05/01/2021 0606
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 92 of 175

Inorganic non-metals - LCSD
Sample ID: WQ90993-003 Matrix: Aqueous
Batch: 90993
Analytical Method: 9056A
Spike
Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Chloride 20 20 1 102 0.24 80-120 20 05/01/2021 0626
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 93 of 175

Inorganic non-metals - MB
Sample ID: WQ90994-001 Matrix: Aqueous
Batch: 90994
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate ND 1 1.0 0.25 mg/L 05/01/2021 0426
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 94 of 175

Inorganic non-metals - LCS
Sample ID: WQ90994-002 Matrix: Aqueous
Batch: 90994
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 20 1 102 80-120 05/01/2021 0606
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 95 of 175

Inorganic non-metals - LCSD
Sample ID: WQ90994-003 Matrix: Aqueous
Batch: 90994
Analytical Method: 9056A
Spike
Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 20 20 1 102 0.24 80-120 20 05/01/2021 0626
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 96 of 175

Inorganic non-metals - MB
Sample ID: WQ91121-001 Matrix: Aqueous
Batch: 91121
Analytical Method: SM 5220D-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
COD ND 1 20 20 mg/L 05/04/2021 1524
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 97 of 175

Inorganic non-metals - LCS
Sample ID: WQ91121-002 Matrix: Aqueous
Batch: 91121
Analytical Method: SM 5220D-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
COD 40 41 1 102 95-105 05/04/2021 1524
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 98 of 175

Inorganic non-metals - MB
Sample ID: WQ91200-001 Matrix: Aqueous
Batch: 91200
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride ND 1 1.0 0.25 mg/L 05/04/2021 1257
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 99 of 175

Inorganic non-metals - LCS
Sample ID: WQ91200-002 Matrix: Aqueous
Batch: 91200
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 21 1 103 80-120 05/04/2021 1337
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 100 of 175

Inorganic non-metals - MS
Sample ID: WD30017-015MS Matrix: Aqueous
Batch: 91200
Analytical Method: 9056A
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 5.1 10 15 1 102 80-120 05/04/2021 1716
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 101 of 175

Inorganic non-metals - MSD
Sample ID: WD30017-015MD Matrix: Aqueous
Batch: 91200
Analytical Method: 9056A
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Chloride 5.1 10 15 1 102 0.42 80-120 20 05/04/2021 1736
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 102 of 175

Inorganic non-metals - MB
Sample ID: WQ91255-001 Matrix: Aqueous
Batch: 91255
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Nitrate - N ND 1 0.020 0.0050 mg/L 05/04/2021 1257
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 103 of 175

Inorganic non-metals - LCS
Sample ID: WQ91255-002 Matrix: Aqueous
Batch: 91255
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.80 0.88 1 110 80-120 05/04/2021 1337
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 104 of 175

Inorganic non-metals - MB
Sample ID: WQ91352-001 Matrix: Aqueous
Batch: 91352
Analytical Method: SM 5220D-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
COD ND 1 20 20 mg/L 05/06/2021 0852
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 105 of 175

Inorganic non-metals - LCS
Sample ID: WQ91352-002 Matrix: Aqueous
Batch: 91352
Analytical Method: SM 5220D-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
COD 40 39 1 96 95-105 05/06/2021 0853
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 106 of 175

Inorganic non-metals - MB
Sample ID: WQ91461-001 Matrix: Aqueous
Batch: 91461
Analytical Method: SM 4500-S2 F-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfide ND 1 1.0 1.0 mg/L 05/05/2021 2008
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 107 of 175

Inorganic non-metals - LCS
Sample ID: WQ91461-002 Matrix: Aqueous
Batch: 91461
Analytical Method: SM 4500-S2 F-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfide 10 10 1 100 80-120 05/05/2021 2008
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 108 of 175

Inorganic non-metals - LCSD
Sample ID: WQ91461-003 Matrix: Aqueous
Batch: 91461
Analytical Method: SM 4500-S2 F-2011
Spike
Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfide 10 10 1 100 0.00 80-120 20 05/05/2021 2008
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 109 of 175

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ91037-001 Matrix: Aqueous
Batch: 91037 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 05/03/2021 2257
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
93 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 110 of 175

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ91037-002 Matrix: Aqueous
Batch: 91037 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 46 1 93 70-130 05/03/2021 2155
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
96 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 111 of 175

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ91095-001 Matrix: Aqueous
Batch: 91095 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 05/04/2021 1018
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
98 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 112 of 175

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ91095-002 Matrix: Aqueous
Batch: 91095 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 50 1 100 70-130 05/04/2021 0915
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
103 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 113 of 175

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ91160-001 Matrix: Aqueous
Batch: 91160 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 05/04/2021 2219
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
96 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 114 of 175

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ91160-002 Matrix: Aqueous
Batch: 91160 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 47 1 94 70-130 05/04/2021 2122
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
95 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 115 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91880-001 Matrix: Aqueous
Batch: 91880 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/11/2021 0945
Acrylonitrile
ND
1
20
0.80
ug/L
05/11/2021 0945
Benzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Bromoform
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/11/2021 0945
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/11/2021 0945
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Chloroethane
ND
1
2.0
0.40
ug/L
05/11/2021 0945
Chloroform
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/11/2021 0945
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/11/2021 0945
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/11/2021 0945
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
2-Hexanone
ND
1
10
2.0
ug/L
05/11/2021 0945
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/11/2021 0945
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/11/2021 0945
Methylene chloride
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Styrene
ND
1
1.0
0.41
ug/L
05/11/2021 0945
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Tetrachloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Toluene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Trichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 116 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91880-001 Matrix: Aqueous
Batch: 91880 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/11/2021 0945
Vinyl chloride
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Xylenes (total)
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 100 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 117 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91880-002 Matrix: Aqueous
Batch: 91880 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
110
1
107
60-140
05/11/2021 0841
Acrylonitrile
100
100
1
105
70-130
05/11/2021 0841
Benzene
50
45
1
89
70-130
05/11/2021 0841
Bromochloromethane
50
47
1
93
70-130
05/11/2021 0841
Bromodichloromethane
50
48
1
95
70-130
05/11/2021 0841
Bromoform
50
45
1
90
70-130
05/11/2021 0841
Bromomethane (Methyl bromide)
50
45
1
89
70-130
05/11/2021 0841
2-Butanone (MEK)
100
100
1
102
70-130
05/11/2021 0841
Carbon disulfide
50
45
1
91
70-130
05/11/2021 0841
Carbon tetrachloride
50
43
1
87
70-130
05/11/2021 0841
Chlorobenzene
50
45
1
90
70-130
05/11/2021 0841
Chloroethane
50
43
1
86
70-130
05/11/2021 0841
Chloroform
50
44
1
87
70-130
05/11/2021 0841
Chloromethane (Methyl chloride)
50
43
1
86
60-140
05/11/2021 0841
1,2-Dibromo-3-chloropropane (DBCP)
50
52
1
105
70-130
05/11/2021 0841
Dibromochloromethane
50
50
1
100
70-130
05/11/2021 0841
1,2-Dibromoethane (EDB)
50
49
1
98
70-130
05/11/2021 0841
Dibromomethane (Methylene bromide)
50
47
1
93
70-130
05/11/2021 0841
trans- 1,4-Dichloro-2-butene
50
44
1
89
70-130
05/11/2021 0841
1,2-Dichlorobenzene
50
47
1
93
70-130
05/11/2021 0841
1,4-Dichlorobenzene
50
44
1
88
70-130
05/11/2021 0841
1,1-Dichloroethane
50
46
1
91
70-130
05/11/2021 0841
1,2-Dichloroethane
50
47
1
93
70-130
05/11/2021 0841
1,1-Dichloroethene
50
44
1
88
70-130
05/11/2021 0841
cis- 1,2-Dichloroethene
50
46
1
92
70-130
05/11/2021 0841
trans- 1,2-Dichloroethene
50
44
1
89
70-130
05/11/2021 0841
1,2-Dichloropropane
50
46
1
93
70-130
05/11/2021 0841
cis- 1,3-Dichloropropene
50
45
1
90
70-130
05/11/2021 0841
trans- 1,3-Dichloropropene
50
45
1
90
70-130
05/11/2021 0841
Ethylbenzene
50
46
1
93
70-130
05/11/2021 0841
2-Hexanone
100
100
1
101
70-130
05/11/2021 0841
Methyl iodide (lodomethane)
50
46
1
93
70-130
05/11/2021 0841
4-Methyl-2-pentanone
100
98
1
98
70-130
05/11/2021 0841
Methylene chloride
50
45
1
90
70-130
05/11/2021 0841
Styrene
50
52
1
104
70-130
05/11/2021 0841
1,1,1,2-Tetrachloroethane
50
49
1
98
70-130
05/11/2021 0841
1,1,2,2-Tetrachloroethane
50
50
1
99
70-130
05/11/2021 0841
Tetrachloroethene
50
44
1
88
70-130
05/11/2021 0841
Toluene
50
47
1
95
70-130
05/11/2021 0841
1,1,1-Trichloroethane
50
45
1
91
70-130
05/11/2021 0841
1,1,2-Trichloroethane
50
48
1
96
70-130
05/11/2021 0841
Trichloroethene
50
42
1
84
70-130
05/11/2021 0841
Trichlorofluoromethane
50
40
1
80
70-130
05/11/2021 0841
1,2,3-Trichloropropane
50
49
1
99
70-130
05/11/2021 0841
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 118 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91880-002
Matrix: Aqueous
Batch: 91880
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
47
1 93
60-140
05/11/2021 0841
Vinyl chloride
50
43
1 86
70-130
05/11/2021 0841
Xylenes (total)
100
98
1 98
70-130
05/11/2021 0841
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 89 70-130
Toluene-d8 90 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 119 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91967-001 Matrix: Aqueous
Batch: 91967 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/11/2021 2215
Acrylonitrile
ND
1
20
0.80
ug/L
05/11/2021 2215
Benzene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Bromoform
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/11/2021 2215
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/11/2021 2215
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Chloroethane
ND
1
2.0
0.40
ug/L
05/11/2021 2215
Chloroform
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/11/2021 2215
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/11/2021 2215
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/11/2021 2215
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
2-Hexanone
ND
1
10
2.0
ug/L
05/11/2021 2215
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/11/2021 2215
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/11/2021 2215
Methylene chloride
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Styrene
ND
1
1.0
0.41
ug/L
05/11/2021 2215
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Tetrachloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Toluene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Trichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 2215
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 120 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91967-001 Matrix: Aqueous
Batch: 91967 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/11/2021 2215
Vinyl chloride
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Xylenes (total)
ND
1
1.0
0.40
ug/L
05/11/2021 2215
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 108 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 121 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91967-002 Matrix: Aqueous
Batch: 91967 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
100
1
100
60-140
05/11/2021 2043
Acrylonitrile
100
100
1
103
70-130
05/11/2021 2043
Benzene
50
50
1
101
70-130
05/11/2021 2043
Bromochloromethane
50
50
1
99
70-130
05/11/2021 2043
Bromodichloromethane
50
50
1
100
70-130
05/11/2021 2043
Bromoform
50
46
1
91
70-130
05/11/2021 2043
Bromomethane (Methyl bromide)
50
49
1
98
70-130
05/11/2021 2043
2-Butanone (MEK)
100
100
1
104
70-130
05/11/2021 2043
Carbon disulfide
50
51
1
101
70-130
05/11/2021 2043
Carbon tetrachloride
50
50
1
100
70-130
05/11/2021 2043
Chlorobenzene
50
50
1
100
70-130
05/11/2021 2043
Chloroethane
50
48
1
96
70-130
05/11/2021 2043
Chloroform
50
47
1
95
70-130
05/11/2021 2043
Chloromethane (Methyl chloride)
50
50
1
101
60-140
05/11/2021 2043
1,2-Dibromo-3-chloropropane (DBCP)
50
44
1
87
70-130
05/11/2021 2043
Dibromochloromethane
50
54
1
108
70-130
05/11/2021 2043
1,2-Dibromoethane (EDB)
50
51
1
102
70-130
05/11/2021 2043
Dibromomethane (Methylene bromide)
50
49
1
98
70-130
05/11/2021 2043
trans- 1,4-Dichloro-2-butene
50
51
1
102
70-130
05/11/2021 2043
1,2-Dichlorobenzene
50
48
1
97
70-130
05/11/2021 2043
1,4-Dichlorobenzene
50
48
1
95
70-130
05/11/2021 2043
1,1-Dichloroethane
50
49
1
98
70-130
05/11/2021 2043
1,2-Dichloroethane
50
49
1
97
70-130
05/11/2021 2043
1,1-Dichloroethene
50
52
1
104
70-130
05/11/2021 2043
cis- 1,2-Dichloroethene
50
48
1
95
70-130
05/11/2021 2043
trans- 1,2-Dichloroethene
50
51
1
102
70-130
05/11/2021 2043
1,2-Dichloropropane
50
49
1
99
70-130
05/11/2021 2043
cis- 1,3-Dichloropropene
50
54
1
108
70-130
05/11/2021 2043
trans- 1,3-Dichloropropene
50
48
1
96
70-130
05/11/2021 2043
Ethylbenzene
50
52
1
103
70-130
05/11/2021 2043
2-Hexanone
100
99
1
99
70-130
05/11/2021 2043
Methyl iodide (lodomethane)
50
52
1
104
70-130
05/11/2021 2043
4-Methyl-2-pentanone
100
110
1
107
70-130
05/11/2021 2043
Methylene chloride
50
49
1
98
70-130
05/11/2021 2043
Styrene
50
55
1
110
70-130
05/11/2021 2043
1,1,1,2-Tetrachloroethane
50
51
1
102
70-130
05/11/2021 2043
1,1,2,2-Tetrachloroethane
50
50
1
99
70-130
05/11/2021 2043
Tetrachloroethene
50
52
1
104
70-130
05/11/2021 2043
Toluene
50
51
1
102
70-130
05/11/2021 2043
1,1,1-Trichloroethane
50
52
1
103
70-130
05/11/2021 2043
1,1,2-Trichloroethane
50
51
1
102
70-130
05/11/2021 2043
Trichloroethene
50
51
1
102
70-130
05/11/2021 2043
Trichlorofluoromethane
50
50
1
100
70-130
05/11/2021 2043
1,2,3-Trichloropropane
50
50
1
99
70-130
05/11/2021 2043
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 122 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91967-002
Matrix: Aqueous
Batch: 91967
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
48
1 96
60-140
05/11/2021 2043
Vinyl chloride
50
50
1 100
70-130
05/11/2021 2043
Xylenes (total)
100
100
1 105
70-130
05/11/2021 2043
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 95 70-130
Toluene-d8 101 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 123 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92034-001 Matrix: Aqueous
Batch: 92034 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/12/2021 0944
Acrylonitrile
ND
1
20
0.80
ug/L
05/12/2021 0944
Benzene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Bromoform
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/12/2021 0944
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/12/2021 0944
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Chloroethane
ND
1
2.0
0.40
ug/L
05/12/2021 0944
Chloroform
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/12/2021 0944
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/12/2021 0944
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/12/2021 0944
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
2-Hexanone
ND
1
10
2.0
ug/L
05/12/2021 0944
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/12/2021 0944
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/12/2021 0944
Methylene chloride
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Styrene
ND
1
1.0
0.41
ug/L
05/12/2021 0944
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Toluene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Trichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/12/2021 0944
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/12/2021 0944
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 124 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92034-001 Matrix: Aqueous
Batch: 92034 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
Vinyl chloride ND 1 1.0 0.40 ug/L 05/12/2021 0944
Xylenes (total) ND 1 1.0 0.40 ug/L 05/12/2021 0944
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 87 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 125 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92034-002 Matrix: Aqueous
Batch: 92034 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
88
1
88
60-140
05/12/2021 0824
Acrylonitrile
100
98
1
98
70-130
05/12/2021 0824
Benzene
50
50
1
101
70-130
05/12/2021 0824
Bromochloromethane
50
47
1
95
70-130
05/12/2021 0824
Bromodichloromethane
50
46
1
93
70-130
05/12/2021 0824
Bromoform
50
50
1
100
70-130
05/12/2021 0824
Bromomethane (Methyl bromide)
50
49
1
98
70-130
05/12/2021 0824
2-Butanone (MEK)
100
100
1
101
70-130
05/12/2021 0824
Carbon disulfide
50
56
1
113
70-130
05/12/2021 0824
Carbon tetrachloride
50
50
1
100
70-130
05/12/2021 0824
Chlorobenzene
50
48
1
97
70-130
05/12/2021 0824
Chloroethane
50
50
1
99
70-130
05/12/2021 0824
Chloroform
50
48
1
97
70-130
05/12/2021 0824
Chloromethane (Methyl chloride)
50
46
1
92
60-140
05/12/2021 0824
1,2-Dibromo-3-chloropropane (DBCP)
50
44
1
88
70-130
05/12/2021 0824
Dibromochloromethane
50
49
1
98
70-130
05/12/2021 0824
1,2-Dibromoethane (EDB)
50
49
1
98
70-130
05/12/2021 0824
Dibromomethane (Methylene bromide)
50
47
1
93
70-130
05/12/2021 0824
trans- 1,4-Dichloro-2-butene
50
46
1
92
70-130
05/12/2021 0824
1,2-Dichlorobenzene
50
49
1
98
70-130
05/12/2021 0824
1,4-Dichlorobenzene
50
50
1
99
70-130
05/12/2021 0824
1,1-Dichloroethane
50
53
1
106
70-130
05/12/2021 0824
1,2-Dichloroethane
50
45
1
90
70-130
05/12/2021 0824
1,1-Dichloroethene
50
51
1
102
70-130
05/12/2021 0824
cis- 1,2-Dichloroethene
50
51
1
102
70-130
05/12/2021 0824
trans- 1,2-Dichloroethene
50
53
1
107
70-130
05/12/2021 0824
1,2-Dichloropropane
50
48
1
96
70-130
05/12/2021 0824
cis- 1,3-Dichloropropene
50
50
1
100
70-130
05/12/2021 0824
trans- 1,3-Dichloropropene
50
49
1
98
70-130
05/12/2021 0824
Ethylbenzene
50
51
1
102
70-130
05/12/2021 0824
2-Hexanone
100
94
1
94
70-130
05/12/2021 0824
Methyl iodide (lodomethane)
50
52
1
103
70-130
05/12/2021 0824
4-Methyl-2-pentanone
100
94
1
94
70-130
05/12/2021 0824
Methylene chloride
50
48
1
96
70-130
05/12/2021 0824
Styrene
50
51
1
102
70-130
05/12/2021 0824
1,1,1,2-Tetrachloroethane
50
47
1
94
70-130
05/12/2021 0824
1,1,2,2-Tetrachloroethane
50
47
1
94
70-130
05/12/2021 0824
Toluene
50
50
1
100
70-130
05/12/2021 0824
1,1,1-Trichloroethane
50
50
1
100
70-130
05/12/2021 0824
1,1,2-Trichloroethane
50
47
1
93
70-130
05/12/2021 0824
Trichloroethene
50
49
1
98
70-130
05/12/2021 0824
Trichlorofluoromethane
50
45
1
89
70-130
05/12/2021 0824
1,2,3-Trichloropropane
50
44
1
88
70-130
05/12/2021 0824
Vinyl acetate
50
50
1
100
60-140
05/12/2021 0824
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 126 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92034-002
Matrix: Aqueous
Batch: 92034
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
Vinyl chloride
50
46
1 92
70-130 05/12/2021 0824
Xylenes (total)
100
100
1 101
70-130 05/12/2021 0824
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 88 70-130
1,2-Dichloroethane-d4 79 70-130
Toluene-d8 88 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 127 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92056-001 Matrix: Aqueous
Batch: 92056 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/12/2021 1210
Acrylonitrile
ND
1
20
0.80
ug/L
05/12/2021 1210
Benzene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Bromoform
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/12/2021 1210
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/12/2021 1210
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Chloroethane
ND
1
2.0
0.40
ug/L
05/12/2021 1210
Chloroform
0.60 J
1
1.0
0.40
ug/L
05/12/2021 1210
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/12/2021 1210
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/12/2021 1210
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/12/2021 1210
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
2-Hexanone
ND
1
10
2.0
ug/L
05/12/2021 1210
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/12/2021 1210
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/12/2021 1210
Methylene chloride
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Styrene
ND
1
1.0
0.41
ug/L
05/12/2021 1210
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Tetrachloroethene
0.54 J
1
1.0
0.40
ug/L
05/12/2021 1210
Toluene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Trichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/12/2021 1210
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 128 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92056-001 Matrix: Aqueous
Batch: 92056 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/12/2021 1210
Vinyl chloride
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Xylenes (total)
ND
1
1.0
0.40
ug/L
05/12/2021 1210
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 95 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 129 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92056-002 Matrix: Aqueous
Batch: 92056 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
95
1
95
60-140
05/12/2021 0834
Acrylonitrile
100
100
1
104
70-130
05/12/2021 0834
Benzene
50
51
1
102
70-130
05/12/2021 0834
Bromochloromethane
50
51
1
101
70-130
05/12/2021 0834
Bromodichloromethane
50
51
1
103
70-130
05/12/2021 0834
Bromoform
50
45
1
90
70-130
05/12/2021 0834
Bromomethane (Methyl bromide)
50
48
1
95
70-130
05/12/2021 0834
2-Butanone (MEK)
100
98
1
98
70-130
05/12/2021 0834
Carbon disulfide
50
55
1
111
70-130
05/12/2021 0834
Carbon tetrachloride
50
51
1
103
70-130
05/12/2021 0834
Chlorobenzene
50
49
1
99
70-130
05/12/2021 0834
Chloroethane
50
50
1
99
70-130
05/12/2021 0834
Chloroform
50
49
1
99
70-130
05/12/2021 0834
Chloromethane (Methyl chloride)
50
45
1
91
60-140
05/12/2021 0834
1,2-Dibromo-3-chloropropane (DBCP)
50
52
1
104
70-130
05/12/2021 0834
Dibromochloromethane
50
53
1
105
70-130
05/12/2021 0834
1,2-Dibromoethane (EDB)
50
51
1
101
70-130
05/12/2021 0834
Dibromomethane (Methylene bromide)
50
49
1
98
70-130
05/12/2021 0834
trans- 1,4-Dichloro-2-butene
50
46
1
92
70-130
05/12/2021 0834
1,2-Dichlorobenzene
50
50
1
99
70-130
05/12/2021 0834
1,4-Dichlorobenzene
50
48
1
96
70-130
05/12/2021 0834
1,1-Dichloroethane
50
53
1
105
70-130
05/12/2021 0834
1,2-Dichloroethane
50
49
1
99
70-130
05/12/2021 0834
1,1-Dichloroethene
50
53
1
106
70-130
05/12/2021 0834
cis- 1,2-Dichloroethene
50
55
1
111
70-130
05/12/2021 0834
trans- 1,2-Dichloroethene
50
51
1
103
70-130
05/12/2021 0834
1,2-Dichloropropane
50
52
1
104
70-130
05/12/2021 0834
cis- 1,3-Dichloropropene
50
49
1
99
70-130
05/12/2021 0834
trans- 1,3-Dichloropropene
50
48
1
96
70-130
05/12/2021 0834
Ethylbenzene
50
52
1
105
70-130
05/12/2021 0834
2-Hexanone
100
100
1
100
70-130
05/12/2021 0834
Methyl iodide (lodomethane)
50
53
1
106
70-130
05/12/2021 0834
4-Methyl-2-pentanone
100
99
1
99
70-130
05/12/2021 0834
Methylene chloride
50
50
1
101
70-130
05/12/2021 0834
Styrene
50
57
1
113
70-130
05/12/2021 0834
1,1,1,2-Tetrachloroethane
50
53
1
106
70-130
05/12/2021 0834
1,1,2,2-Tetrachloroethane
50
51
1
102
70-130
05/12/2021 0834
Tetrachloroethene
50
54
1
107
70-130
05/12/2021 0834
Toluene
50
53
1
106
70-130
05/12/2021 0834
1,1,1-Trichloroethane
50
53
1
106
70-130
05/12/2021 0834
1,1,2-Trichloroethane
50
51
1
102
70-130
05/12/2021 0834
Trichloroethene
50
50
1
99
70-130
05/12/2021 0834
Trichlorofluoromethane
50
48
1
96
70-130
05/12/2021 0834
1,2,3-Trichloropropane
50
49
1
98
70-130
05/12/2021 0834
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 130 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92056-002
Matrix: Aqueous
Batch: 92056
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
50
1 99
60-140
05/12/2021 0834
Vinyl chloride
50
49
1 98
70-130
05/12/2021 0834
Xylenes (total)
100
110
1 109
70-130
05/12/2021 0834
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 89 70-130
Toluene-d8 94 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 131 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92125-001 Matrix: Aqueous
Batch: 92125 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/12/2021 2215
Acrylonitrile
ND
1
20
0.80
ug/L
05/12/2021 2215
Benzene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Bromoform
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/12/2021 2215
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/12/2021 2215
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Chloroethane
ND
1
2.0
0.40
ug/L
05/12/2021 2215
Chloroform
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/12/2021 2215
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/12/2021 2215
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/12/2021 2215
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
2-Hexanone
ND
1
10
2.0
ug/L
05/12/2021 2215
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/12/2021 2215
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/12/2021 2215
Methylene chloride
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Styrene
ND
1
1.0
0.41
ug/L
05/12/2021 2215
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Tetrachloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Toluene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Trichloroethene
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/12/2021 2215
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 132 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92125-001 Matrix: Aqueous
Batch: 92125 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/12/2021 2215
Vinyl chloride
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Xylenes (total)
ND
1
1.0
0.40
ug/L
05/12/2021 2215
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 92 70-130
Toluene-d8 95 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 133 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92125-002 Matrix: Aqueous
Batch: 92125 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
150
N 1
154
60-140
05/12/2021 2108
Acrylonitrile
100
110
1
110
70-130
05/12/2021 2108
Benzene
50
52
1
105
70-130
05/12/2021 2108
Bromochloromethane
50
54
1
108
70-130
05/12/2021 2108
Bromodichloromethane
50
48
1
96
70-130
05/12/2021 2108
Bromoform
50
48
1
95
70-130
05/12/2021 2108
Bromomethane (Methyl bromide)
50
48
1
97
70-130
05/12/2021 2108
2-Butanone (MEK)
100
130
1
127
70-130
05/12/2021 2108
Carbon disulfide
50
61
1
122
70-130
05/12/2021 2108
Carbon tetrachloride
50
52
1
103
70-130
05/12/2021 2108
Chlorobenzene
50
53
1
105
70-130
05/12/2021 2108
Chloroethane
50
51
1
101
70-130
05/12/2021 2108
Chloroform
50
53
1
106
70-130
05/12/2021 2108
Chloromethane (Methyl chloride)
50
46
1
93
60-140
05/12/2021 2108
1,2-Dibromo-3-chloropropane (DBCP)
50
50
1
99
70-130
05/12/2021 2108
Dibromochloromethane
50
51
1
103
70-130
05/12/2021 2108
1,2-Dibromoethane (EDB)
50
53
1
106
70-130
05/12/2021 2108
Dibromomethane (Methylene bromide)
50
49
1
98
70-130
05/12/2021 2108
trans- 1,4-Dichloro-2-butene
50
27
N 1
54
70-130
05/12/2021 2108
1,2-Dichlorobenzene
50
55
1
110
70-130
05/12/2021 2108
1,4-Dichlorobenzene
50
54
1
107
70-130
05/12/2021 2108
1,1-Dichloroethane
50
52
1
105
70-130
05/12/2021 2108
1,2-Dichloroethane
50
47
1
94
70-130
05/12/2021 2108
1,1-Dichloroethene
50
57
1
114
70-130
05/12/2021 2108
cis- 1,2-Dichloroethene
50
58
1
115
70-130
05/12/2021 2108
trans- 1,2-Dichloroethene
50
55
1
111
70-130
05/12/2021 2108
1,2-Dichloropropane
50
50
1
100
70-130
05/12/2021 2108
cis- 1,3-Dichloropropene
50
51
1
103
70-130
05/12/2021 2108
trans- 1,3-Dichloropropene
50
53
1
106
70-130
05/12/2021 2108
Ethylbenzene
50
55
1
110
70-130
05/12/2021 2108
2-Hexanone
100
100
1
101
70-130
05/12/2021 2108
Methyl iodide (lodomethane)
50
58
1
116
70-130
05/12/2021 2108
4-Methyl-2-pentanone
100
100
1
100
70-130
05/12/2021 2108
Methylene chloride
50
55
1
109
70-130
05/12/2021 2108
Styrene
50
55
1
110
70-130
05/12/2021 2108
1,1,1,2-Tetrachloroethane
50
51
1
102
70-130
05/12/2021 2108
1,1,2,2-Tetrachloroethane
50
52
1
104
70-130
05/12/2021 2108
Tetrachloroethene
50
51
1
102
70-130
05/12/2021 2108
Toluene
50
54
1
108
70-130
05/12/2021 2108
1,1,1-Trichloroethane
50
56
1
113
70-130
05/12/2021 2108
1,1,2-Trichloroethane
50
51
1
103
70-130
05/12/2021 2108
Trichloroethene
50
52
1
104
70-130
05/12/2021 2108
Trichlorofluoromethane
50
45
1
90
70-130
05/12/2021 2108
1,2,3-Trichloropropane
50
50
1
100
70-130
05/12/2021 2108
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 134 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92125-002
Matrix: Aqueous
Batch: 92125
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
56
1 112
60-140
05/12/2021 2108
Vinyl chloride
50
46
1 93
70-130
05/12/2021 2108
Xylenes (total)
100
110
1 108
70-130
05/12/2021 2108
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 93 70-130
1,2-Dichloroethane-d4 81 70-130
Toluene-d8 93 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 135 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92172-001 Matrix: Aqueous
Batch: 92172 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/13/2021 1035
Acrylonitrile
ND
1
20
0.80
ug/L
05/13/2021 1035
Benzene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Bromoform
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/13/2021 1035
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/13/2021 1035
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Chloroethane
ND
1
2.0
0.40
ug/L
05/13/2021 1035
Chloroform
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/13/2021 1035
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/13/2021 1035
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/13/2021 1035
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
2-Hexanone
ND
1
10
2.0
ug/L
05/13/2021 1035
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/13/2021 1035
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/13/2021 1035
Methylene chloride
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Styrene
ND
1
1.0
0.41
ug/L
05/13/2021 1035
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Tetrachloroethene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Toluene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Trichloroethene
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/13/2021 1035
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 136 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92172-001 Matrix: Aqueous
Batch: 92172 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/13/2021 1035
Vinyl chloride
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Xylenes (total)
ND
1
1.0
0.40
ug/L
05/13/2021 1035
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 110 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 137 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92172-002 Matrix: Aqueous
Batch: 92172 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q
Dil
% Rec
Limit
Analysis Date
Acetone
100
230
N
1
233
60-140
05/13/2021 0933
Acrylonitrile
100
110
1
111
70-130
05/13/2021 0933
Benzene
50
49
1
97
70-130
05/13/2021 0933
Bromochloromethane
50
53
1
107
70-130
05/13/2021 0933
Bromodichloromethane
50
54
1
108
70-130
05/13/2021 0933
Bromoform
50
56
1
113
70-130
05/13/2021 0933
Bromomethane (Methyl bromide)
50
57
1
115
70-130
05/13/2021 0933
2-Butanone (MEK)
100
170
N
1
167
70-130
05/13/2021 0933
Carbon disulfide
50
52
1
104
70-130
05/13/2021 0933
Carbon tetrachloride
50
48
1
97
70-130
05/13/2021 0933
Chlorobenzene
50
49
1
98
70-130
05/13/2021 0933
Chloroethane
50
57
1
114
70-130
05/13/2021 0933
Chloroform
50
50
1
101
70-130
05/13/2021 0933
Chloromethane (Methyl chloride)
50
64
1
129
60-140
05/13/2021 0933
1,2-Dibromo-3-chloropropane (DBCP)
50
57
1
115
70-130
05/13/2021 0933
Dibromochloromethane
50
54
1
109
70-130
05/13/2021 0933
1,2-Dibromoethane (EDB)
50
54
1
108
70-130
05/13/2021 0933
Dibromomethane (Methylene bromide)
50
53
1
107
70-130
05/13/2021 0933
trans- 1,4-Dichloro-2-butene
50
59
1
119
70-130
05/13/2021 0933
1,2-Dichlorobenzene
50
52
1
104
70-130
05/13/2021 0933
1,4-Dichlorobenzene
50
49
1
98
70-130
05/13/2021 0933
1,1-Dichloroethane
50
49
1
98
70-130
05/13/2021 0933
1,2-Dichloroethane
50
51
1
103
70-130
05/13/2021 0933
1,1-Dichloroethene
50
49
1
99
70-130
05/13/2021 0933
cis- 1,2-Dichloroethene
50
51
1
101
70-130
05/13/2021 0933
trans- 1,2-Dichloroethene
50
50
1
101
70-130
05/13/2021 0933
1,2-Dichloropropane
50
53
1
107
70-130
05/13/2021 0933
cis- 1,3-Dichloropropene
50
58
1
116
70-130
05/13/2021 0933
trans- 1,3-Dichloropropene
50
60
1
120
70-130
05/13/2021 0933
Ethylbenzene
50
52
1
105
70-130
05/13/2021 0933
2-Hexanone
100
140
N
1
142
70-130
05/13/2021 0933
Methyl iodide (lodomethane)
50
49
1
98
70-130
05/13/2021 0933
4-Methyl-2-pentanone
100
130
1
128
70-130
05/13/2021 0933
Methylene chloride
50
49
1
99
70-130
05/13/2021 0933
Styrene
50
57
1
114
70-130
05/13/2021 0933
1,1,1,2-Tetrachloroethane
50
50
1
101
70-130
05/13/2021 0933
1,1,2,2-Tetrachloroethane
50
52
1
104
70-130
05/13/2021 0933
Tetrachloroethene
50
49
1
97
70-130
05/13/2021 0933
Toluene
50
52
1
105
70-130
05/13/2021 0933
1,1,1-Trichloroethane
50
49
1
98
70-130
05/13/2021 0933
1,1,2-Trichloroethane
50
53
1
105
70-130
05/13/2021 0933
Trichloroethene
50
48
1
96
70-130
05/13/2021 0933
Trichlorofluoromethane
50
48
1
96
70-130
05/13/2021 0933
1,2,3-Trichloropropane
50
50
1
100
70-130
05/13/2021 0933
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 138 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92172-002
Matrix: Aqueous
Batch: 92172
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
52
1 104
60-140
05/13/2021 0933
Vinyl chloride
50
63
1 125
70-130
05/13/2021 0933
Xylenes (total)
100
110
1 109
70-130
05/13/2021 0933
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 103 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 139 of 175

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ92201-001 Matrix: Aqueous
Batch: 92201 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
Tetrachloroethene ND 1 1.0 0.40 ug/L 05/13/2021 1310
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 108 70-130
1,2-Dichloroethane-d4 92 70-130
Toluene-d8 98 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 140 of 175

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ92201-002
Matrix: Aqueous
Batch: 92201
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
Tetrachloroethene
50
48
1 96 70-130 05/13/2021 1207
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 95 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 141 of 175

ICP-MS Metals - MB
Sample ID: WQ90835-001 Matrix: Aqueous
Batch: 90835 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 05/03/2021 0426
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
05/03/2021 1615
Arsenic
ND
1
2.0
1.3
ug/L
05/03/2021 1615
Barium
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Beryllium
ND
1
0.40
0.15
ug/L
05/03/2021 1615
Cadmium
ND
1
0.50
0.13
ug/L
05/03/2021 1615
Chromium
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Cobalt
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Copper
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Lead
ND
1
1.0
0.25
ug/L
05/03/2021 1615
Nickel
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Selenium
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Silver
ND
1
1.0
0.25
ug/L
05/03/2021 1615
Thallium
ND
1
0.50
0.15
ug/L
05/03/2021 1615
Vanadium
ND
1
5.0
2.5
ug/L
05/03/2021 1615
Zinc
ND
1
10
2.5
ug/L
05/03/2021 1615
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 142 of 175

ICP-MS Metals - LCS
Sample ID: WQ90835-002 Matrix: Aqueous
Batch: 90835 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 05/03/2021 0426
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
100
1
102
80-120
05/03/2021 1621
Arsenic
100
98
1
98
80-120
05/03/2021 1621
Barium
100
100
1
101
80-120
05/03/2021 1621
Beryllium
100
110
1
114
80-120
05/03/2021 1621
Cadmium
100
94
1
94
80-120
05/03/2021 1621
Chromium
100
96
1
96
80-120
05/03/2021 1621
Cobalt
100
95
1
95
80-120
05/03/2021 1621
Copper
100
99
1
99
80-120
05/03/2021 1621
Lead
100
100
1
103
80-120
05/03/2021 1621
Nickel
100
97
1
97
80-120
05/03/2021 1621
Selenium
100
85
1
85
80-120
05/03/2021 1621
Silver
100
100
1
102
80-120
05/03/2021 1621
Thallium
100
100
1
101
80-120
05/03/2021 1621
Vanadium
100
96
1
96
80-120
05/03/2021 1621
Zinc
100
88
1
88
80-120
05/03/2021 1621
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 143 of 175

ICP-MS Metals - MB
Sample ID: WQ90837-001 Matrix: Aqueous
Batch: 90837 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 05/07/2021 0324
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
05/07/2021 1353
Arsenic
ND
1
2.0
1.3
ug/L
05/07/2021 1353
Barium
ND
1
5.0
1.3
ug/L
05/07/2021 1353
Beryllium
ND
1
0.40
0.15
ug/L
05/07/2021 1353
Cadmium
ND
1
0.50
0.13
ug/L
05/07/2021 1353
Chromium
ND
1
5.0
1.3
ug/L
05/07/2021 1353
Cobalt
ND
1
5.0
1.3
ug/L
05/07/2021 1353
Copper
ND
1
5.0
1.3
ug/L
05/07/2021 1353
Lead
ND
1
1.0
0.25
ug/L
05/07/2021 1353
Nickel
ND
1
5.0
1.3
ug/L
05/07/2021 1353
Selenium
ND
1
5.0
1.3
ug/L
05/07/2021 1353
Silver
ND
1
1.0
0.25
ug/L
05/07/2021 1353
Thallium
ND
1
0.50
0.15
ug/L
05/07/2021 1353
Vanadium
ND
1
5.0
2.5
ug/L
05/07/2021 1353
Zinc
ND
1
10
2.5
ug/L
05/07/2021 1353
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 144 of 175

ICP-MS Metals - LCS
Sample ID: WQ90837-002 Matrix: Aqueous
Batch: 90837 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 05/07/2021 0324
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
100
1
105
80-120
05/07/2021 1400
Arsenic
100
99
1
99
80-120
05/07/2021 1400
Barium
100
100
1
102
80-120
05/07/2021 1400
Beryllium
100
99
1
99
80-120
05/07/2021 1400
Cadmium
100
97
1
97
80-120
05/07/2021 1400
Chromium
100
100
1
101
80-120
05/07/2021 1400
Cobalt
100
100
1
103
80-120
05/07/2021 1400
Copper
100
110
1
106
80-120
05/07/2021 1400
Lead
100
110
1
106
80-120
05/07/2021 1400
Nickel
100
100
1
102
80-120
05/07/2021 1400
Selenium
100
88
1
88
80-120
05/07/2021 1400
Silver
100
100
1
102
80-120
05/07/2021 1400
Thallium
100
110
1
106
80-120
05/07/2021 1400
Vanadium
100
100
1
102
80-120
05/07/2021 1400
Zinc
100
100
1
101
80-120
05/07/2021 1400
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 145 of 175

ICP-MS Metals - MS
Sample ID: WD30017-007MS
Matrix: Aqueous
Batch: 90837
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
05/07/2021
0324
Sample
Spike
Amount
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q
Dil
% Rec
Limit
Analysis Date
Antimony
ND
100
110
1
108
75-125
05/07/2021 1415
Arsenic
ND
100
85
1
85
75-125
05/07/2021 1415
Barium
220
100
320
1
102
75-125
05/07/2021 1415
Beryllium
ND
100
92
1
92
75-125
05/07/2021 1415
Cadmium
ND
100
97
1
97
75-125
05/07/2021 1415
Chromium
12
100
100
1
90
75-125
05/07/2021 1415
Cobalt
ND
100
85
1
85
75-125
05/07/2021 1415
Copper
ND
100
81
1
81
75-125
05/07/2021 1415
Lead
1.2
100
94
1
93
75-125
05/07/2021 1415
Nickel
ND
100
81
1
81
75-125
05/07/2021 1415
Selenium
ND
100
90
1
90
75-125
05/07/2021 1415
Silver
ND
100
88
1
88
75-125
05/07/2021 1415
Thallium
ND
100
95
1
95
75-125
05/07/2021 1415
Vanadium
ND
100
94
1
94
75-125
05/07/2021 1415
Zinc
ND
100
75
1
75
75-125
05/07/2021 1415
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 146 of 175

ICP-MS Metals - MSD
Sample ID: WD30017-007MD
Matrix: Aqueous
Batch: 90837
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
05/07/2021 0324
Sample
Spike
Amount
Amount
Result
%Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Antimony
ND
100
110
1
108
0.039
75-125
20
05/07/2021 1422
Arsenic
ND
100
86
1
86
1.4
75-125
20
05/07/2021 1422
Barium
220
100
330
1
107
1.5
75-125
20
05/07/2021 1422
Beryllium
ND
100
92
1
92
0.081
75-125
20
05/07/2021 1422
Cadmium
ND
100
98
1
98
0.71
75-125
20
05/07/2021 1422
Chromium
12
100
100
1
91
0.73
75-125
20
05/07/2021 1422
Cobalt
ND
100
86
1
86
1.1
75-125
20
05/07/2021 1422
Copper
ND
100
81
1
81
0.16
75-125
20
05/07/2021 1422
Lead
1.2
100
94
1
93
0.23
75-125
20
05/07/2021 1422
Nickel
ND
100
81
1
81
0.11
75-125
20
05/07/2021 1422
Selenium
ND
100
92
1
92
1.6
75-125
20
05/07/2021 1422
Silver
ND
100
89
1
89
1.1
75-125
20
05/07/2021 1422
Thallium
ND
100
94
1
94
1.1
75-125
20
05/07/2021 1422
Vanadium
ND
100
94
1
94
0.48
75-125
20
05/07/2021 1422
Zinc
ND
100
74
N 1
74
0.57
75-125
20
05/07/2021 1422
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 147 of 175

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 148 of 175

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f Yes 3, Were v.apercusmclypror��xJure&(re [inquishe&ruzeived)followed?
6. Wem sxritp!e lUs listed on the COC9
7, Were samp[c IDs lisicd ❑R aJI mill' cDntaimrsf
Yes -N" R_ Was oo;lECOV a date 8t t;me lisird on [he COC'i
Yes No 9, Was colle-; irjn date & tI Ine listr:d 1- all simple cenmillcrs-
,� Yes ❑ Ne IU_ Did �dI container label infirimalion (ID, aaec. tame) ogee with lihe CC1C
Yex Nu 11_ Wei--- teals uF W- pertgmr d fisted of the COC?
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des No 13. was a.Jrc{uate sample volt�rne availahm?
Y'o No 14. Were All sall pl-s received within :i hum, wh icha�ver cx,ri Ies i
YGs. r "u �5. CI a any sample-5 containerg�^;r x Circla ori�;) sain les Not Iistud an COC'
[:1 Yw V]No DNA 16. Parr VOA ant! KKK-175 u3�ip�c�w�r� 13b7es presEsn[:} °raa size" (-/:'or6ytm in di
in any ❑f Ch a VOA via Is?
V. Ya-q Nu NA I?, Were all 1}IWVrnc'ta[sr'rtutrient samples received at a pH e< 2? —
YRMS M1 J NA I.N. Wem aR cva_iidj, salllf;[M reeeived at a pH > 12 and sulfudie tan 1ae rexe[ved at a P14
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_ rasiJuaI chWi.m?
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•'es 1 21. will
a thti lucre 11umbw listed an t}re t:antairrer Jebel? If � C t1o0a Y Wn
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noceivadwith bubbles �-6 Inm in dianye
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 150 of 175

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Samples Receipt CheGUSllt {SRC) (MLODIRC-15)
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p ID; ` i'� Chl;rinc %t 13, 2r.3e� Tegte({ by_ aRit2
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Method of cusrizmt:
❑� ❑det Ice Ela, P�lC5 1 .J Dr Icc ❑ None
QYes LNo
VONA�_ lft'utperOureOriff' cooler exLrG!ledb.U"U.Waserojccthiana '-NO'ilwQ+[I?
T3ht W&S T4U=fried]: Iltione fert]Rili !aC@-t'sceCJL'Cli 8]]s'.
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+ 7Q14 is the ctrmrll Cial a4ttrler'a packing sl attaci:cd i tlti`g fprm?
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d
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7, Wnrt:.;ample 11�3 113ted [m all Sairlplc collminc s?
f
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b- W� onl lectiOn date time listed on the CC)C .
Ye; lti9
9, WAS oglleCtiun ram � Ilene llsxd On ail 3an1j}1c Cui3Grrrrs"
J Yt!, [� No
'0. JD; l HIJ ooaltpincr lalsel :riformatior[ (Ib, dolt, lima) a ruw with 1}tv C0 7
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] 1 _ W= tars 10 Lie }herformud 11.�1er1 rm tho COC"'
Imo, I}id slf �Hmpir an'i4e in tnc proper c�oTuai:ters fo, ems, kst nntffnr in
Sri Yes L.-II No goad cantitoan
(unbrakcn, lids nn, Oro. _
Ycs h o 13. Was a,dcquate sanhpie vol nmc. ava iable?
Yes , Na 14. Wcrc ail sarlMlf�g IW6VCd wilhirt'h the bolding time or 48 hours, ;yhj wyer wracs
Y: S ' l 15_ Were imy satn lc%5 containers mi Nit 'excess (circle rtrnc) 3ampk* Not l iS" au COC
E] ❑ No N. ]b. For VOA and HSK-175 sa nphn, were buhlrles prc3errt "peas izc" (W'or 4nhm in di
in aln oftlse VOA "ials?
No NA 17_ Were all samples Trxoiveda,apHnP��'�
Yes No NA l S. Wr.-e all cytunide slum les reoid vcd at ;a pH > 12 and sul tide sarrkpies rooeivcd at a F H
❑, Yes ❑ N43 R. k4'rru all angyhca to ;�f3{1 11ty�ulule;phcnol!t57. , , s:rni,lcs free
Y L,�
i❑ No .N.4 . CrG cliertL remarkslrequests {t.e, reiltiMed dilutions, Malm9D drsigratiortE, eie_..l
corr2dly tFM1t -ibed from tlhe t_ M into the co:n1Trenl seLxiorh in LJKS?
Yos i No 1_ Was :he ttntC nuDkWF fished On t'Lte oop:Fainer Iabc . if vzs, un[r. 4 21369
iarflipli: Fraser, K#ian (R7ust br carnple44xl feu' 8ry �alltpie(s) jT3CDM ctly p3wim tad c,r with Peod.space_)
temple{ j ^ were rcccived itlow'I'vAly rzewrved and Were adjustod acci
i sample rccci%ing with KA .. —ill i, Pf cimle unc. i-l2SO4, [ 1 3,1iCi,1TaQH irSln SR # 1tiA
-rne of preservallbrh �A 1 P morn ban Dno preservm iva is nMded, p base hbOW in the conhnhe rls belaw.
arrpic(s NA _wcrrstiOtiVedhWi ltbubhlas>Cr men indiame
umplen(L;) Ph were reocivcd w;lh T14C [�.S m 1L (lf l9 is r�0) dnd wi
*5'M dirgly i:n smiplc receiving wi:h aodimn thiosullfau� (NR2s203) wit}t Sheaiy 1D: MA
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Page i of 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 153 of 175

aceAna lytical
LELAP CERTIFICATE NUMBER: 01955
DOD-ELAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
PERFORMED BY
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 05/18/2021
Report Y 211050509
�1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i III
Project WD30017 Closed Buncombe Wells
Deliver To
Lucas Odom
Pace Analytical Services South Carolina
106 Vantage Point Drive
West Columbia, SC 29172
803 791 9700
L*
PJLA
wAting
WD ELAP
Additional Recipients
NONE
ISO
17025
Pace Gulf Coast Report#: 221050509 Page 1 of 22
Page 154 of 175

Report#: 221050509
aceAnarytical
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
" Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
Pace Gulf Coast Report 221050509
Pace Gulf Coast Report#: 221050509 Page 2 of 22
Page 155 of 175

1 _21Analytical
Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Certifications
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Pace Gulf Coast Report#: 221050509 Page 3 of 22
Page 156 of 175

Report#: 221050509
aceAnarytical
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Case Narrative
Client: Pace Analytical Services South Carolina Report: 221050509
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Pace Gulf Coast Report#: 221050509 Page 4 of 22
Page 157 of 175

aceAnarytical
Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date:
05/18/2021
Sample Summary
LAB ID
Client ID
Matrix
Collect Date
Receive Date
22105050901
MW-2
Water
04/29/202110:00
05/04/2021 10:21
22105050902
MW-4
Water
04/29/202114:10
05/04/2021 10:21
22105050903
MW-6
Water
04/29/202112:05
05/04/2021 10:21
22105050904
MW-13-132
Water
04/29/202113:55
05/04/2021 10:21
22105050905
MW-18-78
Water
04/29/202110:10
05/04/2021 10:21
22105050906
MW-19-75
Water
04/29/202111:45
05/04/2021 10:21
22105050907
MW-19-110
Water
04/29/202113:10
05/04/2021 10:21
22105050908
MW-21-21
Water
04/29/202112:20
05/04/2021 10:21
22105050909
MW-21-94
Water
04/29/202110:45
05/04/2021 10:21
22105050910
MW-24-160
Water
04/29/202116:45
05/04/2021 10:21
22105050911
MW-2 (1-12)
Bubble Strip
04/29/2021 10:00
05/04/2021 10:21
22105050912
MW-4 (1-12)
Bubble Strip
04/29/2021 14:10
05/04/2021 10:21
22105050913
MW-6 (1-12)
Bubble Strip
04/29/2021 12:05
05/04/2021 10:21
22105050914
MW-13-132 (H2)
Bubble Strip
04/29/2021 13:55
05/04/2021 10:21
22105050915
MW-18-78 (1-12)
Bubble Strip
04/29/2021 10:10
05/04/2021 10:21
22105050916
MW-19-75 (1-12)
Bubble Strip
04/29/2021 11:45
05/04/2021 10:21
22105050917
MW-19-110 (1-12)
Bubble Strip
04/29/2021 13:10
05/04/2021 10:21
22105050918
MW-21-21 (1-12)
Bubble Strip
04/29/2021 12:20
05/04/2021 10:21
22105050919
MW-21-94 (1-12)
Bubble Strip
04/29/2021 10:45
05/04/2021 10:21
22105050920
MW-24-160 (1-12)
Bubble Strip
04/29/2021 16:45
05/04/2021 10:21
Pace Gulf Coast Report#: 221050509 Page 5 of 22
Page 158 of 175

aceAnarytical
Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date:
05/18/2021
Detect Summary
LAB ID
Client ID
Method
Parameter
Result
Units
22105050901
MW-2
AM23G
Acetic Acid
0.37J
mg/L
22105050901
MW-2
AM23G
Formic Acid
4.6
mg/L
22105050901
MW-2
AM20GAX
Ethane
1.2
ug/L
22105050901
MW-2
AM20GAX
Ethene
31
ug/L
22105050901
MW-2
AM20GAX
Methane
5200
ug/L
22105050901
MW-2
EPA RSK-175
Carbon Dioxide
17300
ug/L
22105050902
MW-4
AM23G
Acetic Acid
0.66J
mg/L
22105050902
MW-4
AM23G
Butyric Acid
0.15J
mg/L
22105050902
MW-4
AM23G
Formic Acid
10
mg/L
22105050902
MW-4
AM20GAX
Methane
3.6J
ug/L
22105050902
MW-4
EPA RSK-175
Carbon Dioxide
162000
ug/L
22105050903
MW-6
AM23G
Acetic Acid
2.7J
mg/L
22105050903
MW-6
AM23G
Formic Acid
52
mg/L
22105050903
MW-6
AM20GAX
Ethane
0.20J
ug/L
22105050903
MW-6
AM20GAX
Methane
680
ug/L
22105050903
MW-6
EPA RSK-175
Carbon Dioxide
179000
ug/L
22105050904
MW-13-132
AM23G
Acetic Acid
2.7J
mg/L
22105050904
MW-13-132
AM23G
Formic Acid
48
mg/L
22105050904
MW-13-132
AM20GAX
Ethane
0.79J
ug/L
22105050904
MW-13-132
AM20GAX
Ethene
0.29J
ug/L
22105050904
MW-13-132
AM20GAX
Methane
3500
ug/L
22105050904
MW-13-132
EPA RSK-175
Carbon Dioxide
15800
ug/L
22105050905
MW-18-78
AM23G
Acetic Acid
2.9J
mg/L
22105050905
MW-18-78
AM23G
Formic Acid
45
mg/L
22105050905
MW-18-78
AM20GAX
Ethene
0.70J
ug/L
22105050905
MW-18-78
AM20GAX
Methane
450
ug/L
22105050905
MW-18-78
EPA RSK-175
Carbon Dioxide
121000
ug/L
22105050906
MW-19-75
AM23G
Acetic Acid
2.6J
mg/L
22105050906
MW-19-75
AM23G
Formic Acid
53
mg/L
22105050906
MW-19-75
AM20GAX
Ethane
0.62J
ug/L
22105050906
MW-19-75
AM20GAX
Methane
1400
ug/L
22105050906
MW-19-75
EPA RSK-175
Carbon Dioxide
94400
ug/L
22105050907
MW-19-110
AM23G
Acetic Acid
0.52J
mg/L
22105050907
MW-19-110
AM23G
Formic Acid
12
mg/L
22105050907
MW-19-110
AM20GAX
Ethane
0.18J
ug/L
22105050907
MW-19-110
AM20GAX
Methane
170
ug/L
22105050907
MW-19-110
EPA RSK-175
Carbon Dioxide
3840
ug/L
22105050908
MW-21-21
AM23G
Acetic Acid
3.8J
mg/L
22105050908
MW-21-21
AM23G
Formic Acid
47
mg/L
22105050908
MW-21-21
AM20GAX
Ethane
0.32J
ug/L
22105050908
MW-21-21
AM20GAX
Ethene
0.46J
ug/L
22105050908
MW-21-21
AM20GAX
Methane
2200
ug/L
22105050908
MW-21-21
EPA RSK-175
Carbon Dioxide
341000
ug/L
22105050909
MW-21-94
AM23G
Acetic Acid
2AJ
mg/L
Pace Gulf Coast Report#: 221050509 Page 6 of 22
Page 159 of 175

aceAnarytical
Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date:
05/18/2021
Detect Summary (Continued)
LAB ID
Client ID
Method
Parameter
Result
Units
22105050909
MW-21-94
AM23G
Formic Acid
49
mg/L
22105050909
MW-21-94
AM20GAX
Ethane
0.75J
ug/L
22105050909
MW-21-94
AM20GAX
Ethene
0.28J
ug/L
22105050909
MW-21-94
AM20GAX
Methane
2000
ug/L
22105050909
MW-21-94
EPA RSK-175
Carbon Dioxide
77100
ug/L
22105050910
MW-24-160
AM23G
Acetic Acid
0.27J
mg/L
22105050910
MW-24-160
AM23G
Formic Acid
5.3
mg/L
22105050910
MW-24-160
AM20GAX
Ethene
0.36J
ug/L
22105050910
MW-24-160
AM20GAX
Methane
35
ug/L
22105050910
MW-24-160
EPA RSK-175
Carbon Dioxide
1360
ug/L
22105050911
MW-2 (H2)
AM20GAX
Hydrogen
120
nM
22105050912
MW-4 (H2)
AM20GAX
Hydrogen
0.76J
nM
22105050913
MW-6 (H2)
AM20GAX
Hydrogen
22
nM
22105050914
MW-13-132 (H2)
AM20GAX
Hydrogen
20
nM
22105050916
MW-19-75 (H2)
AM20GAX
Hydrogen
0.95J
nM
22105050917
MW-19-110 (H2)
AM20GAX
Hydrogen
3.4
nM
22105050918
MW-21-21 (H2)
AM20GAX
Hydrogen
8.4
nM
22105050919
MW-21-94 (H2)
AM20GAX
Hydrogen
17
nM
22105050920
MW-24-160 (H2)
AM20GAX
Hydrogen
4.2
nM
Pace Gulf Coast Report#: 221050509 Page 7 of 22
Page 160 of 175

Report#: 221050509
10;aceAr�alytrca!
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 10:00 LAB ID 22105050901
M W-2
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 5 05/13/202110:14 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 17300 635 4500 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/08/202117:01 MOS 710558
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.37J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
4.6
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202111:21 JCK2 710674
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
1.2
0.075
1.0
ug/L
74-85-1
Ethene
31
0.12
1.0
ug/L
74-82-8
Methane
5200
2.5
5.0
ug/L
Collect Date 04/29/2021 14:10 LAB ID 22105050902
M W-4
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 05/13/202110:24 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 162000 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 2 05/08/202117:54 MOS 710558
CAS# Parameter
64-19-7 Acetic Acid
107-92-6 Butyric Acid
Result DL LOQ Units
0.66J 0.25 1.0 mg/L
0.15J 0.12 1.0 mg/L
Pace Gulf Coast Report#: 221050509 Page 8 of 22
Page 161 of 175

aceAnalytica! Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 14:10 LAB ID 22105050902
M W-4
Receive Date 05/04/2021 10:21 Matrix Water
AM23G (Continued)
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 2 05/08/202117:54 MOS 710558
CAS#
Parameter
Result
DL
LOQ
Units
64-18-6
Formic Acid
10
0.11
1.0
mg/L
142-62-1
Hexanoic Acid
0.12U
0.12
1.0
mg/L
646-07-1
i-Hexanoic Acid
0.11 U
0.11
1.0
mg/L
503-74-2
i-Pentanoic Acid
0.12U
0.12
1.0
mg/L
50-21-5
Lactic Acid
0.11 U
0.11
1.0
mg/L
109-52-4
Pentanoic Acid
0.11 U
0.11
1.0
mg/L
79-09-4
Propionic Acid
0.11 U
0.11
1.0
mg/L
127-17-3
Pyruvic Acid
0.12U
0.12
1.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202111:32 JCK2 710674
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
74-82-8
Methane
3.6J
2.5
5.0
ug/L
Collect Date 04/29/2021 12:05 LAB ID 22105050903
MW-6
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 05/13/202110:36 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 179000 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 05/08/202118:47 MOS 710558
CAS#
Parameter
64-19-7
Acetic Acid
107-92-6
Butyric Acid
64-18-6
Formic Acid
142-62-1
Hexanoic Acid
646-07-1
i-Hexanoic Acid
503-74-2
i-Pentanoic Acid
50-21-5
Lactic Acid
109-52-4
Pentanoic Acid
79-09-4
Propionic Acid
127-17-3
Pyruvic Acid
Result
DL
LOQ
Units
2.7J
1.2
5.0
mg/L
0.58U
0.58
5.0
mg/L
52
0.55
5.0
mg/L
0.58U
0.58
5.0
mg/L
0.56U
0.56
5.0
mg/L
0.61 U
0.61
5.0
mg/L
0.53U
0.53
5.0
mg/L
0.56U
0.56
5.0
mg/L
0.53U
0.53
5.0
mg/L
0.60U
0.60
5.0
mg/L
Pace Gulf Coast Report#: 221050509 Page 9 of 22
Page 162 of 175

aceAnalytica! Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 12:05 LAB ID 22105050903
MW-6
Receive Date 05/04/2021 10:21 Matrix Water
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202111:44 JCK2 710674
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.20J
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
74-82-8
Methane
680
2.5
5.0
ug/L
Collect Date 04/29/2021 13:55 LAB ID 22105050904
MW-13-132
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 5 05/13/202110:46 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 15800 635 4500 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 05/08/202119:41 MOS 710558
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
2.7J
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
48
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.53U
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.60U
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202111:55 JCK2 710674
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.79J
0.075
1.0
ug/L
0.29J
0.12
1.0
ug/L
3500
2.5
5.0
ug/L
Pace Gulf Coast Report#: 221050509 Page 10 of 22
Page 163 of 175

aceAnalytica! Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 10:10 LAB ID 22105050905
MW-18-78
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 05/13/202110:52 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 121000 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 05/08/202122:21 MOS 710558
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
2.9J
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
45
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.53U
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.60U
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202112:07 JCK2 710674
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.70J
0.12
1.0
ug/L
74-82-8
Methane
450
2.5
5.0
ug/L
Collect Date 04/29/2021 11:45 LAB ID 22105050906
MW-19-75
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 05/13/202110:56 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 94400 1270 9000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 05/08/202123:14 MOS 710558
CAS# Parameter
64-19-7 Acetic Acid
107-92-6 Butyric Acid
Result DL LOQ Units
2.6J 1.2 5.0 mg/L
0.58U 0.58 5.0 mg/L
Pace Gulf Coast Report#: 221050509 Page 11 of 22
Page 164 of 175

aceArulytrca! Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 11:45 LAB ID 22105050906
MW-19-75
Receive Date 05/04/2021 10:21 Matrix Water
AM23G (Continued)
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 05/08/202123:14 MOS 710558
CAS#
Parameter
Result
DL
LOQ
Units
64-18-6
Formic Acid
53
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.53U
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.60U
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202112:19 JCK2 710674
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.62J
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
74-82-8
Methane
1400
2.5
5.0
ug/L
Collect Date 04/29/2021 13:10 LAB ID 22105050907
MW-19-110
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/13/202111:02 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 3840 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 2 05/09/202100:08 MOS 710558
CAS#
Parameter
64-19-7
Acetic Acid
107-92-6
Butyric Acid
64-18-6
Formic Acid
142-62-1
Hexanoic Acid
646-07-1
i-Hexanoic Acid
503-74-2
i-Pentanoic Acid
50-21-5
Lactic Acid
109-52-4
Pentanoic Acid
79-09-4
Propionic Acid
127-17-3
Pyruvic Acid
Result
DL
LOQ
Units
0.52J
0.25
1.0
mg/L
0.12U
0.12
1.0
mg/L
12
0.11
1.0
mg/L
0.12U
0.12
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.12U
0.12
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.12U
0.12
1.0
mg/L
Pace Gulf Coast Report#: 221050509 Page 12 of 22
Page 165 of 175

Report#: 221050509
10;aceAr�alytrca!
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 13:10 LAB ID 22105050907
MW-19-110
Receive Date 05/04/2021 10:21 Matrix Water
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202112:30 JCK2 710674
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.18J
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
74-82-8
Methane
170
2.5
5.0
ug/L
Collect Date 04/29/2021 12:20 LAB ID 22105050908
MW-21-21
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 30 05/13/202111:14 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 341000 3810 27000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 05/09/202101:01 MOS 710558
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
3.8J
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
47
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.53U
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.60U
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202112:42 JCK2 710674
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.32J
0.075
1.0
ug/L
0.46J
0.12
1.0
ug/L
2200
2.5
5.0
ug/L
Pace Gulf Coast Report#: 221050509 Page 13 of 22
Page 166 of 175

Report#: 221050509
10;aceAr�alytrca!
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 10:45 LAB ID 22105050909
MW-21-94
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 5 05/13/202111:18 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 77100 635 4500 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 05/09/202101:55 MOS 710558
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
2.4J
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
49
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.53U
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.60U
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202112:53 JCK2 710674
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.75J
0.075
1.0
ug/L
74-85-1
Ethene
0.28J
0.12
1.0
ug/L
74-82-8
Methane
2000
2.5
5.0
ug/L
Collect Date 04/29/2021 16:45 LAB ID 22105050910
MW-24-160
Receive Date 05/04/2021 10:21 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/13/202111:23 BMR 711077
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 1360 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/09/202102:48 MOS 710558
CAS# Parameter
64-19-7 Acetic Acid
107-92-6 Butyric Acid
Result DL LOQ Units
0.27J 0.12 0.50 mg/L
0.058U 0.058 0.50 mg/L
Pace Gulf Coast Report#: 221050509 Page 14 of 22
Page 167 of 175

aceAnalytica! Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 16:45 LAB ID 22105050910
MW-24-160
Receive Date 05/04/2021 10:21 Matrix Water
3G (Continued)
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/09/202102:48 MOS 710558
CAS#
Parameter
Result
DL
LOQ
Units
64-18-6
Formic Acid
5.3
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/11/202113:05 JCK2 710674
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.36J
0.12
1.0
ug/L
74-82-8
Methane
35
2.5
5.0
ug/L
Collect Date 04/29/2021 10:00 LAB ID 22105050911
MW-2 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 8 05/10/202116:14 JCK2 710741
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 120 3.9 15 nM
Collect Date 04/29/2021 14:10 LAB ID 22105050912
MW-4 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202113:58 JCK2 710741
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
0.76J
0.49
1.9
nM
Pace Gulf Coast Report#: 221050509 Page 15 of 22
Page 168 of 175

aceAnalytica! Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 12:05 LAB ID 22105050913
MW-6 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202114:16 JCK2 710741
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 22 0.49 1.9 nM
Collect Date 04/29/2021 13:55 LAB ID 22105050914
MW-13-132 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202114:34 JCK2 710741
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 20 0.49 1.9 nM
Collect Date 04/29/2021 10:10 LAB ID 22105050915
MW-18-78 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202114:46 JCK2 710741
CAS# Parameter
1333-74-0 Hydrogen
AM20GAX
Result
DL
LOQ
Units
0.49U
0.49
1.9
nM
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202114:46 JCK2 710741
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 0.49U 0.49 1.9 nM
Collect Date 04/29/2021 11:45 LAB ID 22105050916
MW-19-75 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202114:58 JCK2 710741
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
0.95J
0.49
1.9
nM
Pace Gulf Coast Report#: 221050509 Page 16 of 22
Page 169 of 175

Report#: 221050509
10;aceAr�alytrca!
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
Sample Results
Collect Date 04/29/2021 13:10 LAB ID 22105050917
MW-19-110 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202115:11 JCK2 710741
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 3.4 0.49 1.9 nM
Collect Date 04/29/2021 12:20 LAB ID 22105050918
MW-21-21 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202115:25 JCK2 710741
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 8.4 0.49 1.9 nM
Collect Date 04/29/2021 10:45 LAB ID 22105050919
MW-21-94 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202115:37 JCK2 710741
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 17 0.49 1.9 nM
Collect Date 04/29/2021 16:45 LAB ID 22105050920
MW-24-160 (H2)
Receive Date 05/04/2021 10:21 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 05/10/202115:50 JCK2 710741
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
4.2
0.49
1.9
nM
Pace Gulf Coast Report#: 221050509 Page 17 of 22
Page 170 of 175

1 21'Amlytical
Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
GC Volatiles QC Summary
Analytical Batch Client ID
MB711077
LCS711077
LCSD711077
711077 LAB ID
2185672
2185673
2185674
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
05/13/21 09:31
05/13/21 09:37
05/13/21 09:43
Matrix
Water
Water
Water
EPA RSK-175
Units
ug/L
Spike
I Result
%R
Control
Spike
Result
I
%R
I
RPD
I
RPD
I
Result
DLI
Added
Limits%R
1 Added
Limit
Carbon Dioxide 124-38-9
127U
127
8700
8580
99
38 - 147
8700
8750
101
2
40
Pace Gulf Coast Report#: 221050509 Page 18 of 22
Page 171 of 175

1 21'Amlytical
Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
General Chemistry QC Summary
Analytical Batch Client ID
MB710558
LCS710558
LCSD710558
710558 LAB ID
2182968
2182969
2182970
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
05/08/21 10:47
05/08/21 09:53
05/08/21 20:34
Matrix
Water
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Acetic Acid
64-19-7
0.12U
0.12
2.0
1.9
96
70 - 130
2.0
1.9
96
0
20
Butyric Acid
107-92-6
0.058U
0.058
2.0
1.9
96
70 - 130
2.0
1.9
96
0
20
Formic Acid
64-18-6
0.055U
0.055
2.0
1.8
89
70 - 130
2.0
1.8
90
1
20
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
1.8
93
70 - 130
2.0
1.8
92
0
20
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
2.0
98
70 - 130
2.0
1.8
88
11
20
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
1.9
94
70 - 130
2.0
1.9
95
1
20
Lactic Acid
50-21-5
0.053U
0.053
2.0
1.8
88
70 - 130
2.0
1.8
89
1
20
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
1.8
92
70 - 130
2.0
1.8
93
0
20
Propionic Acid
79-09-4
0.053U
0.053
2.0
1.8
91
70 - 130
2.0
1.8
91
0
20
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
1.8
88
70 - 130
2.0
1.8
90
2
20
Pace Gulf Coast Report#: 221050509 Page 19 of 22
Page 172 of 175

1 21'Amlytical
Report#: 221050509
Project ID: WD30017 Closed Buncombe Wells Report Date: 05/18/2021
General Chromatography QC Summary
Analytical Batch Client ID
MB710741
LCS710741
LCSD710741
710741 LAB ID
2183943
2183944
2183945
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
05/10/21 10:52
05/10/21 11:08
05/10/21 11:21
Matrix
AM20GAX
Units
nM
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Hydrogen 1333-74-0
0.49U
1 0.491
121
9.5180
1 70 - 130
1 121
10185
1
20
Analytical Batch
Client ID
MB710674
LCS710674
LCSD710674
710674
LAB ID
2183699
2183700
2183701
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
05/11/21 10:46
05/11/21 10:12
05/11/21 10:24
Matrix
Water
Water
Water
AM20GAX
Units
ug/L
Spike
I Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits'/, R
Added
Limit
Ethane
74-84-0
0.075U
0.075
97
99
102
70-130
97
100
103
1
20
Ethene
74-85-1
0.12U
0.12
120
120
104
70 - 130
120
130
107
2
20
Methane
74-82-8
2.5U
2.5
380
380
100
70 - 130
380
390
101
2
20
Pace Gulf Coast Report#: 221050509 Page 20 of 22
Page 173 of 175

Chain of Custody
workorder: WD30017 Workorder Name: Closed Buncombe Wells Owner Received Date: 30-Apr
!- aceAnalytfcal
Results Requested By: 14-May
Report To: Subcontract To:
Requested Analysis
Pace Analytical West Columbia Pace Gulf Coast
106 Vantage Point Dr. Ruth Welsh
West Columbia, SC 29172
803-206-9537
Lucas Odom PreserveTIXIXIXI
Q
j
v
m
o
v
=
V;
o
ry
U
-o
m
u,
g
LAB USE ONLYI
Item
Sample ID
Sample
Type
Collect
Date/Time
Lab ID
Matrix
1
MW-2
Grab
04/29/21 @ 1000
WD30017-009
aqueous
2
MW-4
Grab
04/29/21 @ 1410
WD30017-011
aqueous
X
X
X
3
MW-6
Grab
04/29/21 @ 1205
WD30017-010
aqueous
X
X
X
3
4
MW-13-132
Grab
04/29/21 @ 1355
WD30017-015
aqueous
X
X
X
I-
5
MW-18-78
Grab
04/29/21 @ 1010
WD30017-019
aqueous
X
X
X
6
MW-19-75
Grab
04/29/21 @ 1145
WD30017-020
aqueous
X
X
X
Lo-
7
MW-19-110
Grab
04/29/21 @ 1310
WD30017-021
aqueous
X
X
X
8
MW-21-21
Grab
04/29/21 @ 1220
WD30017-022
aqueous
X
X
X
MW-21-94
Grab
04/29/21 @ 1045
WD30017-023
aqueous
--i
X
X
X
�]
iL
10
MW-24-160
Grab
04/29/21 @ 1645
WD30017-024
aqueous
i9
X
X
X
(]
Transfers
RelptksedBy
Date/Time
Reveived By
Date/Time
Comments
1
3 (�
report "J" values
121UE3ewpm
�
2
MA
VAM•2
3
Cooler Temperature on Receipt °CI Custody Seal Y or N Received on Ice Y or N I Sample Intact Y or N
***In order to maintain client confidentiality, location/name of the sampling site, sampler's name and signature may not be provided on this COC
This chain of custody is considered complete as is since this information is available in the owner laboratory.
Friday, June 17, 201611:01:34 AM Ii I (At-,51 -�, L U5 1�305 FMT-ALL-C-002rev.0(
Client ID: Shealy Envir - Pace Analytical Services South Carolina
SDG: 221050509
PM: RWe
Pace Gulf Coast Report#: 221050509 Page 21 of 22
Page 174 of 175

i'auaimiytn:s SAMPLE RECEIVING CHECKLIST IIIIIIAIIIII
SAMPLE DELIVERY GROUP
221050509
CHECKLIST
YES
NO
Client PM RUUe
Transport Method
Samples received with proper thermal preservation?
*❑
❑
Shealy Envir - Pace Analytical
FEDDC
Services South Carolina
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
*❑
*❑
❑
❑
Profile Number
Received By
285031
N/bane, Dodie K
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
*❑
0
❑
❑
Line Item(s)
Receive Date(s)
1 - LHC and Perm gases VFA
05/04/21
2- Hydrogen
Preservative added to any containers?
❑
0
If received, was headspace for VOC water containers < 6mm?
0
❑
Samples collected in containers provided by Pace Gulf Coast?
0
❑
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer ID E38
Temp °C
None
None
166334654385
2.6
NOTES
Pevision 1.6
Pace Gulf Coast Report#: 221050509
Page 175 of 175
Page 1 of 1
Page 22 of 22

0
aceAnalytical
Report of Analysis
Bunnell-Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Attention: Andy Alexander
Project Name: Closed Buncombe County Landfill Surface Water
Project Number: J21-14175-05
Lot Number:WD30011
Date Completed:05/12/2021
05/19/2021 8:29 AM
Approved and released by:
Project Manager II: Lucas Odom
PCCRF�
24rA
SOA
/
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 39

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Bunnell-Lammons Engineering, Inc.
Lot Number: WD30011
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] whw.pacelabs.com
Page 2 of 39

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WD30011
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
SW-1
Aqueous
04/28/20210945
04/29/2021
002
SW-2
Aqueous
04/28/20211020
04/29/2021
003
SW-2A
Aqueous
04/28/20211030
04/29/2021
004
SW-3
Aqueous
04/28/20211145
04/29/2021
005
SW-4
Aqueous
04/28/20211105
04/29/2021
006
Trip Blank
Aqueous
04/28/2021
04/29/2021
(6 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 39

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WD30011
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
SW-1
Aqueous
Barium
6020B
14
ug/L
6
001
SW-1
Aqueous
Lead
6020B
0.50
J
ug/L
6
001
SW-1
Aqueous
Zinc
6020B
11
ug/L
6
002
SW-2
Aqueous
Barium
6020B
14
ug/L
8
002
SW-2
Aqueous
Zinc
6020B
3.9
J
ug/L
8
003
SW-2A
Aqueous
1,4-Dioxane
8260D (SIM)
12
ug/L
9
003
SW-2A
Aqueous
Barium
6020B
35
ug/L
10
003
SW-2A
Aqueous
Copper
6020B
5.7
ug/L
10
003
SW-2A
Aqueous
Nickel
6020B
1.6
J
ug/L
10
004
SW-3
Aqueous
1,4-Dioxane
8260D (SIM)
34
ug/L
12
004
SW-3
Aqueous
Barium
6020B
110
ug/L
13
004
SW-3
Aqueous
Cobalt
6020B
3.2
J
ug/L
13
004
SW-3
Aqueous
Nickel
6020B
4.0
J
ug/L
13
005
SW-4
Aqueous
1,4-Dioxane
8260D (SIM)
68
ug/L
15
005
SW-4
Aqueous
Barium
6020B
120
ug/L
16
005
SW-4
Aqueous
Cobalt
6020B
10
ug/L
16
005
SW-4
Aqueous
Nickel
6020B
20
ug/L
16
005
SW-4
Aqueous
Selenium
6020B
1.7
J
ug/L
17
(18 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-001
Description: SW-1 Matrix: Aqueous
Date Sampled:04/28/2021 0945
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211525 TML 91866
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-001
Description: SW-1 Matrix: Aqueous
Date Sampled:04/28/2021 0945
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211525 TML
91866
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
101 70-130
1,2-Dichloroethane-d4
111 70-130
Toluene-d8
110 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1751 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
14
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.50 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
11
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-002
Description: SW-2 Matrix: Aqueous
Date Sampled:04/28/2021 1020
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211549 TML 91866
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-002
Description: SW-2 Matrix: Aqueous
Date Sampled:04/28/2021 1020
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211549 TML
91866
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
101 70-130
1,2-Dichloroethane-d4
111 70-130
Toluene-d8
112 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1757 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
14
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
3.9 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-003
Description: SW-2A Matrix: Aqueous
Date Sampled:04/28/2021 1030
Date Received:04/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0106 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
12
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
96 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211613 TML
91866
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-003
Description: SW-2A Matrix: Aqueous
Date Sampled:04/28/2021 1030
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211613 TML 91866
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
99 70-130
1,2-Dichloroethane-d4
111 70-130
Toluene-d8
109 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/03/2021 1803 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
35
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
5.7
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
1.6 J
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-003
Description: SW-2A Matrix: Aqueous
Date Sampled:04/28/2021 1030
Date Received:04/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1803 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-004
Description: SW-3 Matrix: Aqueous
Date Sampled:04/28/2021 1145
Date Received:04/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0131 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
34
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
98 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/12/20210229 CJL2
91963
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-004
Description: SW-3 Matrix: Aqueous
Date Sampled:04/28/2021 1145
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/12/20210229 CJL2 91963
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
102 70-130
1,2-Dichloroethane-d4
90 70-130
Toluene-d8
94 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/03/2021 1809 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
110
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
3.2 J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
4.0 J
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-004
Description: SW-3 Matrix: Aqueous
Date Sampled:04/28/2021 1145
Date Received:04/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1809 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-005
Description: SW-4 Matrix: Aqueous
Date Sampled:04/28/2021 1105
Date Received:04/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 05/04/2021 0156 CJL2
91037
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
68
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
98 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 05/11/20211133 BWS
91880
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-005
Description: SW-4 Matrix: Aqueous
Date Sampled:04/28/2021 1105
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211133 BWS 91880
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
107 70-130
1,2-Dichloroethane-d4
96 70-130
Toluene-d8
100 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 05/03/2021 1815 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
120
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
10
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
20
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-005
Description: SW-4 Matrix: Aqueous
Date Sampled:04/28/2021 1105
Date Received:04/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 05/03/2021 1815 BNW
05/03/2021 0426 90835
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
1.7 J
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-006
Description: Trip Blank Matrix: Aqueous
Date Sampled:04/28/2021
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211043 BWS 91880
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 39

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WD30011-006
Description: Trip Blank Matrix: Aqueous
Date Sampled:04/28/2021
Date Received:04/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 05/11/20211043 BWS 91880
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
114 70-130
96 70-130
101 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 39

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 39

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ91037-001 Matrix: Aqueous
Batch: 91037 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 05/03/2021 2257
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
93 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 39

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ91037-002 Matrix: Aqueous
Batch: 91037 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 46 1 93 70-130 05/03/2021 2155
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
96 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 39

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91866-001 Matrix: Aqueous
Batch: 91866 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/11/2021 1007
Acrylonitrile
ND
1
20
0.80
ug/L
05/11/2021 1007
Benzene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Bromoform
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/11/2021 1007
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/11/2021 1007
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Chloroethane
ND
1
2.0
0.40
ug/L
05/11/2021 1007
Chloroform
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/11/2021 1007
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/11/2021 1007
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/11/2021 1007
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
2-Hexanone
ND
1
10
2.0
ug/L
05/11/2021 1007
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/11/2021 1007
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/11/2021 1007
Methylene chloride
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Styrene
ND
1
1.0
0.41
ug/L
05/11/2021 1007
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Tetrachloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Toluene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Trichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 1007
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 39

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91866-001 Matrix: Aqueous
Batch: 91866 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/11/2021 1007
Vinyl chloride
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Xylenes (total)
ND
1
1.0
0.40
ug/L
05/11/2021 1007
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 111 70-130
Toluene-d8 111 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 39

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91866-002
Matrix:
Aqueous
Batch: 91866
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
110
1
106
60-140
05/11/2021 0842
Acrylonitrile
100
110
1
107
70-130
05/11/2021 0842
Benzene
50
51
1
103
70-130
05/11/2021 0842
Bromochloromethane
50
51
1
103
70-130
05/11/2021 0842
Bromodichloromethane
50
52
1
104
70-130
05/11/2021 0842
Bromoform
50
53
1
106
70-130
05/11/2021 0842
Bromomethane (Methyl bromide)
50
51
1
101
70-130
05/11/2021 0842
2-Butanone (MEK)
100
110
1
113
70-130
05/11/2021 0842
Carbon disulfide
50
52
1
104
70-130
05/11/2021 0842
Carbon tetrachloride
50
50
1
101
70-130
05/11/2021 0842
Chlorobenzene
50
51
1
101
70-130
05/11/2021 0842
Chloroethane
50
52
1
104
70-130
05/11/2021 0842
Chloroform
50
51
1
102
70-130
05/11/2021 0842
Chloromethane (Methyl chloride)
50
54
1
107
60-140
05/11/2021 0842
1,2-Dibromo-3-chloropropane (DBCP)
50
53
1
106
70-130
05/11/2021 0842
Dibromochloromethane
50
52
1
104
70-130
05/11/2021 0842
1,2-Dibromoethane (EDB)
50
51
1
102
70-130
05/11/2021 0842
Dibromomethane (Methylene bromide)
50
51
1
102
70-130
05/11/2021 0842
trans- 1,4-Dichloro-2-butene
50
57
1
113
70-130
05/11/2021 0842
1,2-Dichlorobenzene
50
51
1
102
70-130
05/11/2021 0842
1,4-Dichlorobenzene
50
49
1
99
70-130
05/11/2021 0842
1,1-Dichloroethane
50
52
1
105
70-130
05/11/2021 0842
1,2-Dichloroethane
50
51
1
102
70-130
05/11/2021 0842
1,1-Dichloroethene
50
52
1
103
70-130
05/11/2021 0842
cis- 1,2-Dichloroethene
50
52
1
104
70-130
05/11/2021 0842
trans- 1,2-Dichloroethene
50
52
1
105
70-130
05/11/2021 0842
1,2-Dichloropropane
50
53
1
105
70-130
05/11/2021 0842
cis- 1,3-Dichloropropene
50
55
1
111
70-130
05/11/2021 0842
trans- 1,3-Dichloropropene
50
56
1
112
70-130
05/11/2021 0842
Ethylbenzene
50
53
1
107
70-130
05/11/2021 0842
2-Hexanone
100
120
1
119
70-130
05/11/2021 0842
Methyl iodide (lodomethane)
50
47
1
95
70-130
05/11/2021 0842
4-Methyl-2-pentanone
100
120
1
117
70-130
05/11/2021 0842
Methylene chloride
50
50
1
100
70-130
05/11/2021 0842
Styrene
50
56
1
112
70-130
05/11/2021 0842
1,1,1,2-Tetrachloroethane
50
50
1
101
70-130
05/11/2021 0842
1,1,2,2-Tetrachloroethane
50
51
1
102
70-130
05/11/2021 0842
Tetrachloroethene
50
50
1
100
70-130
05/11/2021 0842
Toluene
50
53
1
106
70-130
05/11/2021 0842
1,1,1-Trichloroethane
50
50
1
100
70-130
05/11/2021 0842
1,1,2-Trichloroethane
50
50
1
101
70-130
05/11/2021 0842
Trichloroethene
50
49
1
99
70-130
05/11/2021 0842
Trichlorofluoromethane
50
46
1
93
70-130
05/11/2021 0842
1,2,3-Trichloropropane
50
50
1
101
70-130
05/11/2021 0842
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 39

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91866-002
Matrix:
Aqueous
Batch: 91866
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Vinyl acetate
50
51
1
101
60-140
05/11/2021 0842
Vinyl chloride
50
54
1
108
70-130
05/11/2021 0842
Xylenes (total)
100
110
1
109
70-130
05/11/2021 0842
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 99 70-130
Toluene-d8 100 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 39

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91880-001 Matrix: Aqueous
Batch: 91880 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/11/2021 0945
Acrylonitrile
ND
1
20
0.80
ug/L
05/11/2021 0945
Benzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Bromoform
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/11/2021 0945
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/11/2021 0945
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Chloroethane
ND
1
2.0
0.40
ug/L
05/11/2021 0945
Chloroform
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/11/2021 0945
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/11/2021 0945
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/11/2021 0945
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
2-Hexanone
ND
1
10
2.0
ug/L
05/11/2021 0945
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/11/2021 0945
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/11/2021 0945
Methylene chloride
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Styrene
ND
1
1.0
0.41
ug/L
05/11/2021 0945
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Tetrachloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Toluene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Trichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 0945
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 39

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91880-001 Matrix: Aqueous
Batch: 91880 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/11/2021 0945
Vinyl chloride
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Xylenes (total)
ND
1
1.0
0.40
ug/L
05/11/2021 0945
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 100 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 39

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91880-002
Matrix:
Aqueous
Batch: 91880
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
110
1
107
60-140
05/11/2021 0841
Acrylonitrile
100
100
1
105
70-130
05/11/2021 0841
Benzene
50
45
1
89
70-130
05/11/2021 0841
Bromochloromethane
50
47
1
93
70-130
05/11/2021 0841
Bromodichloromethane
50
48
1
95
70-130
05/11/2021 0841
Bromoform
50
45
1
90
70-130
05/11/2021 0841
Bromomethane (Methyl bromide)
50
45
1
89
70-130
05/11/2021 0841
2-Butanone (MEK)
100
100
1
102
70-130
05/11/2021 0841
Carbon disulfide
50
45
1
91
70-130
05/11/2021 0841
Carbon tetrachloride
50
43
1
87
70-130
05/11/2021 0841
Chlorobenzene
50
45
1
90
70-130
05/11/2021 0841
Chloroethane
50
43
1
86
70-130
05/11/2021 0841
Chloroform
50
44
1
87
70-130
05/11/2021 0841
Chloromethane (Methyl chloride)
50
43
1
86
60-140
05/11/2021 0841
1,2-Dibromo-3-chloropropane (DBCP)
50
52
1
105
70-130
05/11/2021 0841
Dibromochloromethane
50
50
1
100
70-130
05/11/2021 0841
1,2-Dibromoethane (EDB)
50
49
1
98
70-130
05/11/2021 0841
Dibromomethane (Methylene bromide)
50
47
1
93
70-130
05/11/2021 0841
trans- 1,4-Dichloro-2-butene
50
44
1
89
70-130
05/11/2021 0841
1,2-Dichlorobenzene
50
47
1
93
70-130
05/11/2021 0841
1,4-Dichlorobenzene
50
44
1
88
70-130
05/11/2021 0841
1,1-Dichloroethane
50
46
1
91
70-130
05/11/2021 0841
1,2-Dichloroethane
50
47
1
93
70-130
05/11/2021 0841
1,1-Dichloroethene
50
44
1
88
70-130
05/11/2021 0841
cis- 1,2-Dichloroethene
50
46
1
92
70-130
05/11/2021 0841
trans- 1,2-Dichloroethene
50
44
1
89
70-130
05/11/2021 0841
1,2-Dichloropropane
50
46
1
93
70-130
05/11/2021 0841
cis- 1,3-Dichloropropene
50
45
1
90
70-130
05/11/2021 0841
trans- 1,3-Dichloropropene
50
45
1
90
70-130
05/11/2021 0841
Ethylbenzene
50
46
1
93
70-130
05/11/2021 0841
2-Hexanone
100
100
1
101
70-130
05/11/2021 0841
Methyl iodide (lodomethane)
50
46
1
93
70-130
05/11/2021 0841
4-Methyl-2-pentanone
100
98
1
98
70-130
05/11/2021 0841
Methylene chloride
50
45
1
90
70-130
05/11/2021 0841
Styrene
50
52
1
104
70-130
05/11/2021 0841
1,1,1,2-Tetrachloroethane
50
49
1
98
70-130
05/11/2021 0841
1,1,2,2-Tetrachloroethane
50
50
1
99
70-130
05/11/2021 0841
Tetrachloroethene
50
44
1
88
70-130
05/11/2021 0841
Toluene
50
47
1
95
70-130
05/11/2021 0841
1,1,1-Trichloroethane
50
45
1
91
70-130
05/11/2021 0841
1,1,2-Trichloroethane
50
48
1
96
70-130
05/11/2021 0841
Trichloroethene
50
42
1
84
70-130
05/11/2021 0841
Trichlorofluoromethane
50
40
1
80
70-130
05/11/2021 0841
1,2,3-Trichloropropane
50
49
1
99
70-130
05/11/2021 0841
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 39

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91880-002
Matrix:
Aqueous
Batch: 91880
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Vinyl acetate
50
47
1
93
60-140
05/11/2021 0841
Vinyl chloride
50
43
1
86
70-130
05/11/2021 0841
Xylenes (total)
100
98
1
98
70-130
05/11/2021 0841
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 89 70-130
Toluene-d8 90 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 39

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91963-001 Matrix: Aqueous
Batch: 91963 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
05/11/2021 2149
Acrylonitrile
ND
1
20
0.80
ug/L
05/11/2021 2149
Benzene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Bromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Bromodichloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Bromoform
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
05/11/2021 2149
2-Butanone (MEK)
ND
1
10
2.0
ug/L
05/11/2021 2149
Carbon disulfide
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Chlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Chloroethane
ND
1
2.0
0.40
ug/L
05/11/2021 2149
Chloroform
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
05/11/2021 2149
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Dibromochloromethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
05/11/2021 2149
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
05/11/2021 2149
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Ethylbenzene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
2-Hexanone
ND
1
10
2.0
ug/L
05/11/2021 2149
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
05/11/2021 2149
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
05/11/2021 2149
Methylene chloride
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Styrene
ND
1
1.0
0.41
ug/L
05/11/2021 2149
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Tetrachloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Toluene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Trichloroethene
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
05/11/2021 2149
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 39

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ91963-001 Matrix: Aqueous
Batch: 91963 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
05/11/2021 2149
Vinyl chloride
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Xylenes (total)
ND
1
1.0
0.40
ug/L
05/11/2021 2149
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 108 70-130
1,2-Dichloroethane-d4 95 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 39

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91963-002
Matrix:
Aqueous
Batch: 91963
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
92
1
92
60-140
05/11/2021 2036
Acrylonitrile
100
110
1
108
70-130
05/11/2021 2036
Benzene
50
49
1
98
70-130
05/11/2021 2036
Bromochloromethane
50
49
1
99
70-130
05/11/2021 2036
Bromodichloromethane
50
49
1
98
70-130
05/11/2021 2036
Bromoform
50
44
1
88
70-130
05/11/2021 2036
Bromomethane (Methyl bromide)
50
51
1
102
70-130
05/11/2021 2036
2-Butanone (MEK)
100
96
1
96
70-130
05/11/2021 2036
Carbon disulfide
50
52
1
104
70-130
05/11/2021 2036
Carbon tetrachloride
50
48
1
97
70-130
05/11/2021 2036
Chlorobenzene
50
47
1
94
70-130
05/11/2021 2036
Chloroethane
50
53
1
107
70-130
05/11/2021 2036
Chloroform
50
47
1
95
70-130
05/11/2021 2036
Chloromethane (Methyl chloride)
50
49
1
98
60-140
05/11/2021 2036
1,2-Dibromo-3-chloropropane (DBCP)
50
53
1
105
70-130
05/11/2021 2036
Dibromochloromethane
50
49
1
99
70-130
05/11/2021 2036
1,2-Dibromoethane (EDB)
50
50
1
99
70-130
05/11/2021 2036
Dibromomethane (Methylene bromide)
50
48
1
97
70-130
05/11/2021 2036
trans- 1,4-Dichloro-2-butene
50
46
1
91
70-130
05/11/2021 2036
1,2-Dichlorobenzene
50
48
1
96
70-130
05/11/2021 2036
1,4-Dichlorobenzene
50
45
1
90
70-130
05/11/2021 2036
1,1-Dichloroethane
50
50
1
100
70-130
05/11/2021 2036
1,2-Dichloroethane
50
49
1
97
70-130
05/11/2021 2036
1,1-Dichloroethene
50
51
1
101
70-130
05/11/2021 2036
cis- 1,2-Dichloroethene
50
50
1
100
70-130
05/11/2021 2036
trans- 1,2-Dichloroethene
50
49
1
98
70-130
05/11/2021 2036
1,2-Dichloropropane
50
49
1
99
70-130
05/11/2021 2036
cis- 1,3-Dichloropropene
50
47
1
94
70-130
05/11/2021 2036
trans- 1,3-Dichloropropene
50
45
1
91
70-130
05/11/2021 2036
Ethylbenzene
50
49
1
98
70-130
05/11/2021 2036
2-Hexanone
100
98
1
98
70-130
05/11/2021 2036
Methyl iodide (lodomethane)
50
52
1
104
70-130
05/11/2021 2036
4-Methyl-2-pentanone
100
99
1
99
70-130
05/11/2021 2036
Methylene chloride
50
49
1
97
70-130
05/11/2021 2036
Styrene
50
54
1
107
70-130
05/11/2021 2036
1,1,1,2-Tetrachloroethane
50
50
1
99
70-130
05/11/2021 2036
1,1,2,2-Tetrachloroethane
50
49
1
98
70-130
05/11/2021 2036
Tetrachloroethene
50
47
1
94
70-130
05/11/2021 2036
Toluene
50
51
1
101
70-130
05/11/2021 2036
1,1,1-Trichloroethane
50
51
1
101
70-130
05/11/2021 2036
1,1,2-Trichloroethane
50
49
1
98
70-130
05/11/2021 2036
Trichloroethene
50
46
1
92
70-130
05/11/2021 2036
Trichlorofluoromethane
50
50
1
99
70-130
05/11/2021 2036
1,2,3-Trichloropropane
50
48
1
96
70-130
05/11/2021 2036
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 39

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ91963-002
Matrix:
Aqueous
Batch: 91963
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Vinyl acetate
50
48
1
95
60-140
05/11/2021 2036
Vinyl chloride
50
51
1
102
70-130
05/11/2021 2036
Xylenes (total)
100
100
1
103
70-130
05/11/2021 2036
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 95 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 39

ICP-MS Metals - MB
Sample ID: WQ90835-001 Matrix: Aqueous
Batch: 90835 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 05/03/2021 0426
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
05/03/2021 1615
Arsenic
ND
1
2.0
1.3
ug/L
05/03/2021 1615
Barium
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Beryllium
ND
1
0.40
0.15
ug/L
05/03/2021 1615
Cadmium
ND
1
0.50
0.13
ug/L
05/03/2021 1615
Chromium
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Cobalt
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Copper
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Lead
ND
1
1.0
0.25
ug/L
05/03/2021 1615
Nickel
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Selenium
ND
1
5.0
1.3
ug/L
05/03/2021 1615
Silver
ND
1
1.0
0.25
ug/L
05/03/2021 1615
Thallium
ND
1
0.50
0.15
ug/L
05/03/2021 1615
Vanadium
ND
1
5.0
2.5
ug/L
05/03/2021 1615
Zinc
ND
1
10
2.5
ug/L
05/03/2021 1615
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 39

ICP-MS Metals - LCS
Sample ID: WQ90835-002
Matrix:
Aqueous
Batch: 90835
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
05/03/2021 0426
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
100
1
102
80-120
05/03/2021 1621
Arsenic
100
98
1
98
80-120
05/03/2021 1621
Barium
100
100
1
101
80-120
05/03/2021 1621
Beryllium
100
110
1
114
80-120
05/03/2021 1621
Cadmium
100
94
1
94
80-120
05/03/2021 1621
Chromium
100
96
1
96
80-120
05/03/2021 1621
Cobalt
100
95
1
95
80-120
05/03/2021 1621
Copper
100
99
1
99
80-120
05/03/2021 1621
Lead
100
100
1
103
80-120
05/03/2021 1621
Nickel
100
97
1
97
80-120
05/03/2021 1621
Selenium
100
85
1
85
80-120
05/03/2021 1621
Silver
100
100
1
102
80-120
05/03/2021 1621
Thallium
100
100
1
101
80-120
05/03/2021 1621
Vanadium
100
96
1
96
80-120
05/03/2021 1621
Zinc
100
88
1
88
80-120
05/03/2021 1621
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 36 of 39

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 37 of 39

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PACE ANALYTICAL SERVICES, LLC
Salrrlpies lteeeLpt rha&INtISM) IME0018C-15) Re% sed:9;2912020
�e:kr JyPie�' ;ssi ing Authority: Pace ENS' - WCG-L Page 1 of 1
Sample Receipt CheeWst (SR )
lien[: OoDlorin5>ccta i bWdale, rrt{'l. ! fAJvw�.rrt1 i rlt : 1a11"MILI
Means of rec4ipt: V Pace LSffnnnt j7UPS U lledEx El Other.
❑ Y
Nil
were uLi_srody �cals prescnr mn 'hc cooler?
klifCUSLIPLky
17 Ye
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wcrc pre.wriL, wtrr Li7ew i3118 ;I irI Id u10.1I kwlrla
'Odgiiial
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tennperature upon rc�,eipt/DeL' VOd ( kej) tmnplrLturr. Ligon re[eipi 'Mnlid SnapJCup ID: NA
1-6 f L_6 r(+ NA y MA oC N,4 INA eC NA jNA + C
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MMR'thod of coo -wit, 0 Wet Ice ED I" NCICS ❑ 1)L ' Ice ❑ NOM
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s. 1: reniperatur�,- Df Lmy cook? execcdcd G,0°C, WiL5 Pra]cct Manugw Nu ifitxl7
1'M was NtrAml b} -: phoilu f tiaisiJ i fate-du-[iwv (eirclz uric),
Yes
I Lj No
vg IAA
4, Is the cortlmercial cmricr's packing slip attmficd to tlii� form?
WIT Yes
LJ No
Ji_ WPre. proper ruslody proLmdLlres (rclinclufn11crWed?
,r -(es
I DNO
6. Wcrc 5;:1mpk Os I:sted an the OOP:°
❑ YyiHNU
J� sNo
7. Wciv 5anipir, IDs I'Stcd orsAll %viol; CoMtaihdrs?
3. Was 3Mllr.ctinn der.;& thr, li Si;d nn tlC CO
[Z Yes
Lj No
9. Wns oalivq' iun d4w & Urnc ]iA;;d un all sample 4urilairters?
yet
❑ lqa
I I}ir all rnnLai Kl F l.ahel inCnnYlMIM (M, da-e. dme) a see wish the C{lM
'r',-.4
No
I I_ Wcrc Lms tki hn lirrk n ned listed ixi Lhc COC?
❑� Y::s
❑�Ncr
12. DId all sampIcs arrive is the prop,7 containers fcr each test vrWor in good condition ;
Oobrokcar ]ids an, etc,)?
[� Y,.k
Alt,
13_ Was adaguam aarwp le vDlume available? s
4
--5
Iglu
14_ Wem D11 sample; received wiLbin % the haldfitg time c,' 46 hours, w1i ichever comes fir3t? - -
U Yes
No
15. W= atTy nrtt ks cmcaincrs missiriE 'cxcess {circk onc) saLnpIcs Not listcxi on COM
�`f*-
-No
❑NA
16- Foe• VOA irnd RSK-175.yttmpl'!srWere Wbblr5 present >"pe�L-.5i7jL (14"cw 6mnl in rJi 'eLeY)
J11 any {ll'tILC VOA k'lLllS?
1C0s
LJ No
NA
L7. Wcm all DRUr'mcta]slnutrimc sarlplcs rcrci%rcd at a pi-1 of-'Z?
❑ Yes
Ll No
Z N A
1 K. W= al I C ar idc samt pl cs L%ccc iv-od ac s pi I > ] 2 and sulfide sartl pies rwz:ivcd at a pli >= #'
❑-'as
❑No
❑1'VA
] _ Were a I I app i DaWe N H3Tl KN.cyani p acne 5.1, 4 _57n MInp es Toe
Iesid--Ifd �hlodirl ° '
Yam.
❑ "
NA
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20- W'em el iertl rorwrlcs�(requescs Q.t - regLL led Uutions, MSi SD desipdiom> etc—)
L:ommly transcri6W from the COC into llic� cam mcrri scucion in L] MS?
Yes
i * AlL7
'21. W9.9 the rote n-,1"ber IWed on ?h� rantainPF Ifibel? IFyus, Quote #
Sample Yreservatiall (i+'t'JSt be aamp:CLCd fur any 5ampk(s) ioc rrcctly prc9crvcC or %%-ith hcadspauc.)
IiTime
5aMple(S) NA wvem received incorrerxly preserved andwere adjusted acma
n sample recoiving wish MA r -_ m L of circle one: HN 03, H U, NaO H tr5i ng SK t+ '4
ofpvm vatian "4A....._... 1: mare tlinn one preservative is IweJed, please hkate in dso comm ants below_
ingly—
Samples) rt were rcxmivpl with hubHzA>6 mn1 in diom
r.
Samples(s) rwn were race Ned mritll TRC > D, S mWL (If # 19 is fro) and wera
adjusted a,:cordljigly in sample mce=v-11g with SiXliLIM 111iMilfaLe (Na?01) Wil.11 Shealy ID:
Sly hrocdc JaL cis applied by: dRr',� Date, 44,1(00.1
Comrtlents�
r
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 39