3405_Forsyth_RJReynolds_RuralHall_Indus_April21GW_FID1595713_20210804

DENR USE ONLY.t ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reoortina Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
ERM NC, Inc. (consultant)
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Thomas M Wilson
E-mail: tom.wilso
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
R.J. Reynolds Industrial Landfill Edwards Road (S.R. 1903) 34-05 0.0503 April 5-6, 2021
Rural Hall, Forsyth County
Environmental Status: (Check all that apply)
Initial/Background Monitoring Detection Monitoring Assessment Monitoring FX-] Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
Leachate monitoring data 1-1Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment
Thomas M Wilson, PG Principal In Charge 704-541-8345
Facility Representative Name (Print) Title (Area Code) Telephone Number
A-4-2021 Affix NC Licensed/ Professional Geologist Seal
Signature Date
ERM NC, Inc. - 300 Summit Avenue, Suite 330, Charlotte, NC 28203
Facility Representative Address
NC Professional Geologic Corporation # C-470
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

ERM ERM, NC, Inc. Telephone: [phone]
300 West Summit Avenue Fax: [phone]
Suite 330 www.erm.com
Charlotte, NC 28203
August 4, 2021
North Carolina Department of Environmental Quality
Division of Waste Management
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Attention: Ms. Jaclynne Drummond
[e-mail]
Via Email
Subject: Groundwater and Surface Water Monitoring
Semi -Annual Summary Report - April 2021
Permit #34-05 - Edwards Road Landfill
Edwards Road
Rural Hall, Forsyth County, North Carolina
Dear Ms. Drummond:
On behalf of R.J. Reynolds Tobacco Company, ERM NC, Inc. (ERM) is submitting the summary
report for the April 2021 groundwater and surface water monitoring event associated with the subject
property. Please contact Mr. Scott Snow of R.J. Reynolds Tobacco Company at 336-741-2236 or
me if you have any questions or comments.
Sincerely,
1-10
r, W Cam.
Thomas M Wilson, P.G.
Principal In Charge
Attachments:
Environmental Monitoring Reporting Form
Groundwater and Surface Water Monitoring Semi -Annual Summary Report
cc: Mr. Scott Snow - R.J. Reynolds Tobacco Company
Mr. Max Hopkins - R.J. Reynolds Tobacco Company
Mr. Dave Wasiela - ERM

Groundwater & Surface
Water Monitoring Semi-
C RJReynolds Annual Summary Report —
April 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
July 16, 2021
Project No.: 0588865
The business of sustainability ERM

Document details
The details entered below are automatically shown on the cover and the main page footer.
PLEASE NOTE: This table must NOT be removed from this document.
Document title
Groundwater & Surface Water Monitoring Semi -Annual Summary Report — April 2021
Document subtitle
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
Project No.
0588865
Date
July 2021
1.0
Andrew Hollifield
R.J. Reynolds Tobacco Co.
Version
Author
Client Name
Document history
ERM approval to issue
Version
Revision
Author
Reviewed by
Name
Date
Comments
Draft
00
Andrew Hollifield
Alan Martin
Name
00.00.0000
Text
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

Signature Page
July 2021
Groundwater & Surface Water Monitoring
Semi -Annual Summary Report — April 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
for
Alan Martin P.G.
Project Manager
Thomas M. Wilson, P.G.
Principal in Charge
ERM NC, Inc.
300 West Summit Avenue, Suite 330
Charlotte, North Carolina 28203
Phone: [phone]
© Copyright 2021 by ERM Worldwide Group Ltd and / or its affiliates ("ERM").
All rights reserved. No part of this work may be reproduced or transmitted in any form,
or by any means, without the prior written permission of ERM
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING CONTENTS
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
CONTENTS
1. INTRODUCTION................................................................................................................................1
2. HISTORICAL GROUNDWATER AND SURFACE WATER QUALITY.............................................1
3. SUMMARY OF MONITORING PROGRAM.......................................................................................1
4. DESCRIPTION OF WATER QUALITY CONDITIONS...................................................................... 3
4.1 Site Hydrogeology................................................................................................................................3
4.2 Groundwater.........................................................................................................................................4
4.3 Surface Water.......................................................................................................................................5
5. PRELIMINARY ANALYSIS................................................................................................................6
6. REFERENCES................................................................................................................................... 7
List of Figures
Figure 1 Site Location Plan............................................................
Figure2 Site Plan...........................................................................
Figure 3 Groundwater Flow Directions ..........................................
Figure 4 Groundwater Sampling Results — September 2019 ........
Figure 5 Surface Water Sampling Results — September 2019......
Figure 6 Sulfate Isocontour Map - Groundwater ............................
Figure 7 Hydrogeologic Conceptual Model ....................................
Figure 8 Sulfate Trends - Groundwater .........................................
Figure 9 Sulfate Trends — Surface Water ......................................
List of Tables
Table 1 Monitor Well Construction Details..........................................................................
Table 2 Groundwater Elevations.........................................................................................
Table 3 Groundwater and Surface Water Sampling Event Summary Data ........................
Table 4 Groundwater Field Parameters..............................................................................
APPENDIX A HISTORICAL GROUNDWATER AND SURFACE WATER QUALITY
ANALYTICAL DATA
APPENDIX B LABORATORY DATA SHEETS
APPENDIX C GROUNDWATER SAMPLING LOGS
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
INTRODUCTION
INTRODUCTION
In accordance with the February 4, 2014 Corrective Action Plan (ERM NC, Inc.) and the Industrial Solid
Waste Landfill Facility Permit No. 34-05-indus-1986 as amended through August 12, 2011, this report
presents the results of the April 2021 groundwater and surface water sampling event conducted at the
closed Edwards Road Landfill previously operated by R.J. Reynolds Tobacco Company. The closed
landfill is located northeast of the jurisdictional boundaries of Rural Hall, Forsyth County, North Carolina
and the location of the Site along with topographic map coverage of the vicinity are shown on Figure 1.
Historical monitoring data indicate the occurrence of certain inorganic compounds in excess of the North
Carolina Groundwater Standards (15A NCAC 2L) and Surface Water Standards (15A NCAC 2B) in
portions of the landfill site. A Corrective Action Plan (ERM) to restore groundwater quality beyond the
compliance boundary, to stop unacceptable impacts to the adjacent surface waters, and to reduce the
overall groundwater contamination at the facility was approved by the North Carolina Department of
Environmental Quality (NCDEQ, formerly known as Department of Environment and Natural Resources)
on February 19, 2014. The selected remedy includes source area contaminant control via the previous
installation of the synthetic liner (cap) over the limits of waste plus drainage improvements (completed in
2012) to minimize rainfall infiltration, leachate generation and discharge of constituents to groundwater, to
allow intrinsic remediation of the existing affected -groundwater.
Groundwater and surface water monitoring has been conducted semi-annually at the site since the
completion of the synthetic cap installation and the drainage improvements in 2012.
2. HISTORICAL GROUNDWATER AND SURFACE WATER QUALITY
Groundwater and surface water quality monitoring has been conducted in the vicinity of the Edwards
Road Landfill since 1989 in accordance with the conditions of Permit Number 34-05 and subsequent to
the closure of the landfill, in accordance with the approved Post Closure Monitoring Plan. An updated
water quality monitoring plan presented in the February 2014 CAP (ERM) was approved by NCDEQ on
February 19, 2014 and is summarized in Section 3. Figure 2 depicts the locations of the groundwater
monitor wells and surface water sampling locations and Table 1 presents a summary of available well
construction details. Historical laboratory analytical results for available groundwater and surface water
samples are summarized in Appendix A.
3. SUMMARY OF MONITORING PROGRAM
Routine groundwater and surface water monitoring activities were conducted on April 5-6, 2021 and are
summarized in the following table:
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
ling and Analyses Plan
SUMMARY OF MONITORING PROGRAM
Analytical Parameters
Sample
Metals a Total Dissolved
Sulfate
Field
Location I.D.
(EPA 6020B/ Solids
(EPA 300.0)
Parameters b
7074) (SM 2540C)
Groundwater:
W-1
✓ ✓ ✓
✓
W-2
✓ ✓ ✓
✓
W-3
✓ ✓ ✓
✓
W-31B
✓ ✓ ✓
✓
W-6
✓ ✓ ✓
✓
W-7
✓ ✓ ✓
✓
W-8
✓ ✓ ✓
✓
W-9
✓ ✓ ✓
✓
PW-1
✓ ✓ ✓
Dry, no sample collected
✓
PZ-1 c,e
PZ-2 c,e
Dry, no sample collected
PZ-3 c,e
Dry, no sample collected
PZ-4 c,e
Dry, no sample collected
PZ-5
✓ ✓ ✓
PZ-6 d
--
--
PZ-7 d
- - --
--
PZ-8 d
-- -- --
--
PZ-9 d
-- -- --
--
PZ-10 d
-- -- --
--
Subtotal
12
12
12
12
Surface Water:
SS-01
✓
✓
✓
✓
SS-01+150 d
--
--
--
--
SS-01+550 d
--
--
--
--
SS-01+850 d
--
--
--
SS-02
✓
✓
✓
✓
SS-10
--
--
--
SS-15
--
--
--
SS-20
✓
✓
✓
✓
SS-25
✓
✓
✓
✓
SS-30
✓
✓
✓
✓
SS-40
✓
✓
✓
✓
SS-50 ✓ ✓ ✓ ✓
SS-60 ✓ ✓ ✓ ✓
SS-70 ✓ ✓ ✓ ✓
SS-80 ✓ ✓ ✓ ✓
SS-90 ✓ ✓ ✓ ✓
Subtotal 11 11 11 11
TOTAL 23 23 23 23
a Aluminum, barium, cadmium, chromium (total), iron, lead, manganese and selenium.
b Field parameters include temperature, pH, specific conductivity, turbidity, dissolved oxygen, and oxidation-reduction potential.
° PZ-1, PZ-2, PZ-3 and PZ-4 were dry during the April 2021 sampling event.
d Temporary point not included in routine sampling.
e Analysis for all metals analyses in PZ samples discontinued per NCDWM authorization 71912020.
The groundwater and surface water monitoring activities were performed in general accordance with the
techniques presented in the February 2014 CAP. Depth -to -water measurements and groundwater
elevations for available monitor wells from the April 2021 sampling event are presented in Table 2.
Groundwater flow directions are presented on Figure 3. Groundwater and surface water analytical data
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING DESCRIPTION OF WATER QUALITY CONDITIONS
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
from the April 2021 sampling are presented in Table 3. Field collection parameters are provided in Table
4. Historical analytical data for both groundwater and surface water are presented in Appendix A.
Laboratory data sheets for the April 2021 sampling event are presented in Appendix B. Copies of the
sample logs are provided in Appendix C. Groundwater and surface water sample analytical results from
the April 2021 sampling event are presented on Figures 4 and 5, respectively. Figure 6 depicts the
isoconcentration contours of sulfates in groundwater at the site and Figure 7 presents a hydrogeologic
conceptual site model and cross-section. Sulfate concentrations in groundwater and surface water over
time are presented graphically on Figures 8 and 9, respectively.
4. DESCRIPTION OF WATER QUALITY CONDITIONS
The following sections highlight key findings from the analytical results.
4.1 Site Hydrogeology
The Site geology consists of fractured bedrock (gneiss and schist) overlain by partially weathered rock
and a mantle of residual soils near the surface. The depth to bedrock beneath the Site generally ranges
from 10 to 50 feet bgs. The first occurrence of groundwater beneath the upper portion of the site is within
the fractured bedrock. In the lower portions of the site near the streams, groundwater is encountered
within the partially weathered rock above the top of hard bedrock (transition zone).
Shallow groundwater beneath the Site migrates either along the top of bedrock or along the permeable
zones within the shallow fractured bedrock zone and discharges into nearby creeks, namely Leak Creek
and its tributaries. The regional groundwater flow regime within the lower portion of the deep bedrock
aquifer is north-eastward toward the nearest regional drainage feature, Town Fork Creek. The depth to
groundwater in the top -of -rock aquifer zone ranges from approximately 0 feet at the creeks to 13 feet in
shallow monitor wells. The depth to water in the bedrock aquifer ranges from artesian conditions to
approximately 110 feet below ground surface in the measured wells.
Using recent depth to water measurements, Site groundwater elevations and hydraulic gradients for the
Site were calculated as summarized below.
Horizontal Hydraulic Gradient - Saprolite/PWR
April 5, 2021
Well
Reference
Depth to
Head
Head
Distance
Hydraulic
Designation
Elevation
Water
Elevation
Change
Change
Gradient
ft MSL
ft
ft
ft
ft
ft/ft
W-1
822.68
11.65
811.03
31.03
180
0.172
Leak Creek a
1 780.0
0.00
780.0
W-3
804.43
2.35
802.08
16.58
80
0.207
Leak Creek a
785.5
0.00
785.5
Average Hydraulic Gradient
0.190
a Leak Creek bed elevation represents groundwater discharge line
Based on the April 2021 hydraulic gradients, the groundwater flow rate (seepage velocity) in the
saprolite/PWR aquifer zone was calculated as summarized below.
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
urounawater seepage velocity L;aicuiation = Kune
DESCRIPTION OF WATER QUALITY CONDITIONS
where:
K = hydraulic conductivity 0.080 ft/day (estimated)
i = horizontal hydraulic gradient 0.190 ft/ft (measured)
ne = effective porosity 0.25 estimated
Groundwater Seepage Velocity (Saprolite/PWR) =
_ (0.08) ( 0.190) / (0.25) = 6.08 x 10-2 ft/day
or 22 ft/year
The widely spaced locations of the bedrock monitor wells at the Site do not allow for calculation of the
hydraulic gradient and groundwater flow rate of the bedrock aquifer.
4.2 Groundwater
During the April 2021 groundwater sampling event, nine monitor wells were sampled utilizing a low flow,
low volume sample collection technique. Piezometers PZ-1, PZ-2, PZ-3 and PZ-4 were dry during the
sampling event. PZ-5 contained a limited volume of water and a grab sample was collected using a
bailer. PZ-5 contained insufficient water for low -flow sampling or water quality parameter collection.
Presently, samples from groundwater monitoring wells at the Site contain concentrations of sulfates, total
dissolved solids, and three metals above the applicable North Carolina groundwater standards (NC 2L
standard). Sulfate, the primary constituent related to the landfill, was detected in two groundwater
samples in excess of the NC 2L standard. Iron was detected in six of the nine groundwater monitoring
well samples in excess of the NC 2L standard. Manganese was detected in six of the nine groundwater
monitoring well samples in excess of the NC 2L standard. Total chromium was detected in three
groundwater monitoring well samples each in excess of the NC 2L standard. The elevated
concentrations of metals in groundwater samples from the Site monitor wells are likely attributable to their
natural occurrence in groundwater as indicated by historical sample results from onsite background
monitor wells (W-6 and former W-4). Dissolved solids were detected in two of the groundwater
monitoring well samples in excess of the NC 2L standard. Consistent with the historical monitoring
results, no elevated concentrations of sulfates, metals or total dissolved solids were detected in the
groundwater sample collected from off -site monitoring well W-9, located to the southeast and side
gradient of the landfill.
As noted in Section 1, installation of the synthetic cap and construction of drainage improvements over
the limits of waste were completed in September 2012. The April 2021 groundwater samples were
collected approximately 8 1/2 years after the cap installation. As graphically depicted in Figure 8, a
continuing overall trend of decreasing or stable sulfate levels is occurring in both the shallow and deep
aquifer zones at the Site since the implementation of the corrective action in 2012. The April 2021
monitoring results indicate that only two monitor well locations contain groundwater with sulfate levels
above the 2L standard : W-01, screened in the shallow saprolite aquifer zone, and PW-01, screened in
the deep bedrock aquifer zone. Prior to the 2012 cap installation, sulfate levels exceeded the 2L
standard in groundwater at five monitor well locations. The decrease in plume size over time and the
sustained trend of decreasing sulfate concentrations at the Site show that the corrective action has been
effective for remediating both the lateral extent of affected groundwater in the shallow saprolite/partially
weathered rock aquifer zone and the vertical extent of affected groundwater in the deeper bedrock aquifer
zone.
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING DESCRIPTION OF WATER QUALITY CONDITIONS
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
4.3 Surface Water
During the April 2021 sampling event, 11 surface water samples were collected. The April 2021 surface
water monitoring results indicate there are no surface water quality impacts directly attributable to the
landfill. Concentrations of sulfates and total dissolved solids in all of the samples collected during the April
2021 sampling event were below the applicable North Carolina surface water standards (NC 2B
standards). Manganese was below the applicable North Carolina surface water standards in all the
surface water samples. Iron was reported in all 11 surface water samples above the North Carolina
surface water standard however five of the samples were collected from upgradient of the landfill (SS-01,
SS-20, SS-25, SS-30, and SS-50). Chromium was reported in 1 surface water sample (SS-02) above the
applicable North Carolina surface water standards (NC 2B standards). Elevated turbidity levels (>10
NTUs) were observed in all the surface water samples with iron, lead and manganese exceedances.
Overall, April 2021 surface water quality results confirm that the corrective actions at the site have been
effective for the remediation of the surface water quality at the site. Compared to upstream surface water
quality, there have been four confirmed on -site exceedances of surface water quality standards in the
streams since 2014. There have been no exceedances of surface water quality standards downstream of
the landfill (SS-40, SS-80 or SS-90) since installation of the synthetic landfill cap in 2012.
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING PRELIMINARY ANALYSIS
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
5. PRELIMINARY ANALYSIS
The April 2021 monitoring results demonstrate:
■ Sulfate, total dissolved solids, iron, manganese, and total chromium in groundwater samples exceed
the NC 2L standards. The elevated concentrations of metals in groundwater are likely attributable to
their natural occurrence in groundwater.
■ Overall, the groundwater quality data indicate that the concentration trends and area of affected
groundwater have been stabilized or reduced at the Site. Using sulfate as a primary indicator of
landfill -related impacts, the sulfate concentrations in groundwater, both shallow and deep, continue to
show sustained decreasing trends since completion of the landfill cap installation in September 2012.
■ No elevated concentrations of sulfates, metals or total dissolved solids have been detected in the
groundwater sample collected from off -site monitoring well W-9, located to the southeast and side
gradient of the landfill.
■ Consistent with the historical monitoring results, concentrations of sulfates and total dissolved solids
in all 11 surface water samples did not exceed the applicable NC 2B standards. There have been no
exceedances of surface water quality standards downstream of the landfill since the installation of the
synthetic landfill cap in 2012. Iron was detected in all 11 surface water samples above the NC 2B
standard, including the five upgradient, background surface water samples, indicating that the
elevated iron levels are naturally occurring.
■ The April 2021 samples were collected approximately 8 1/2 years after implementation of the
corrective action in 2012 and the monitoring results confirm that sustained groundwater and surface
water quality improvements are occurring at the Site. The water quality improvements indicate that
the cap installation and the drainage improvements at the landfill are effective remedial measures.
The schedule for routine monitoring activities is summarized below.
Target
Activity Completion Date
Conduct Semi -Annual Water Quality Monitoring Event September 2021
Submit Water Quality Monitoring Summary Report to NCDEQ December 2021
Conduct Semi -Annual Water Quality Monitoring Event March 2022
Submit Water Quality Monitoring Summary Report to NCDEQ June 2022
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING REFERENCES
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
6. REFERENCES
Date Title Source
1986-05-29 Solid Waste Permit No. 34-05 issued to R.J. Reynolds Tobacco Company NCDENR
1999-10-19
R. J. Reynolds Tobacco Company Ash Landfill Transition Plan
Geo-Environmental
Consultants, Inc.
2000-01-25
Work Plan for Upgrading Groundwater Monitoring, Phase 11 Ash Fill Area
Geo-Environmental
Consultants, Inc.
2000-03-13
Upgrade of Groundwater Monitoring Program, Phase 11 Ash Fill Area
Shield Environmental
Associates, Inc.
2001-01-02
Modifications to Transition Plan, Permit #34-05
Shield Environmental
Associates, Inc.
2003-12-23
Post Closure Cover Maintenance Plan, Permit #34-05
Shield Environmental
Associates, Inc.
2009-04-17
Compliance Order with Administrative Penalty, Facility #34-05
NCDENR
2009-07-17
Preliminary Site Assessment Work Plan, Facility #34-05
ERM
2009-10-29
Summary Report— Preliminary Site Assessment, Facility #34-05
ERM
2010-11-15
Letter correspondence to NCDENR DWM regarding Off -Site Well
ERM
Locations, Facility #34-05
2011-03-10
Summary Report— Phase 11 Site Assessment
ERM
2011-06-14
Proposed Closure Modification - Edwards Road Landfill, Permit No. 34-05
ERM
2011-08-12
Regulatory approval Letter Of Closure Modification, Permit No. 34-05
NCDENR
2012-04-30
Summary Report — Groundwater Modelling for Site Assessment
ERM
2012-09-21
Construction Quality Assurance for Closure Modification, Permit No. 34-
ERM
05
2012-10-09
Letter correspondence to NCDENR regarding Groundwater Modelling &
ERM
Water Quality Monitoring, Facility #34-05
2012-11-07
Groundwater Corrective Action Permit Modification Application
ERM
2013-10-01
Groundwater Corrective Action Application and Revised Groundwater
ERM
Modelling Scenarios
2013-10-10
Regulatory approval of Groundwater Corrective Action Application
NCDENR
2013-10-11
Regulatory approval of Construction Quality Assurance for Closure
NCDENR
Modification, Permit No. 34-05
2014-02-04
Corrective Action Plan, Permit No. 34-05
ERM
2014-02-19
Regulatory approval of Corrective Action Plan
NCDENR
Various
Groundwater and Surface Water Monitoring Summary Reports — 2010-
ERM
present
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July 2021 Page 7
2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

GROUNDWATER & SURFACE WATER MONITORING
SEMI-ANNUAL SUMMARY REPORT — APRIL 2021
Edwards Road Landfill — Permit # 34-05
Rural Hall, Forsyth County, North Carolina
Figures
Figure 1 Site Location Plan
Figure 2 Site Plan
Figure 3 Groundwater Flow Directions
Figure 4 Groundwater Sampling Results — September 2019
Figure 5 Surface Water Sampling Results — September 2019
Figure 6 Sulfate Isocontour Map - Groundwater
Figure 7 Hydrogeologic Conceptual Model
Figure 8 Sulfate Trends - Groundwater
Figure 9 Sulfate Trends — Surface Water
Tables
Table 1 Monitor Well Construction Details
Table 2 Groundwater Elevations
Table 3 Groundwater and Surface Water Sampling Event Summary Data
Table 4 Groundwater Field Parameters
REFERENCES
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2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

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o � L., `` 's ' ?Ri'�': - - y '� , � �r`.-rI i i +1 .,� .. _ �, �• �' )v �—ti — , �50, � —. ..
y 0 2,000
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=- Legend
Figure 1
Compliance Boundary ±� Limits of Permit Site Location Map
0
Edwards Road Landfill Permit #34-05
R.J. Reynolds Tobacco Co.
ERM NC, Inc.
ERM www.erm.com 1:24,000 1 inch = 2,000 feet Rural Hall, North Carolina
Source: Copyright:© 2013 National Geographic Society, i-cubed Coordinate System: NAD 1983 StatePlane North Carolina RIPS 3200 Feet

SS 170 " PZ-4
SS-80
g00
s, Johnston :.
I(. Al
PZ-2.
/W-2
Al
i� W-1
R. J. P.
Reynolds �Q ,� SS-001+87
g00 0000. ♦ 11�
B�1;_
W 4 W-6 B-5 « SS�1+550 ooF
SS-50 O l�
r ♦ �.� 'fS S-95
' W-3B O
9 inr
B-9
B-10 B 8 SS-01+150 Sprinkle
�7 ..:,�„' �'.• ,
�i goo
� SS-01 Phipps
W-4 W-6 B-11 SS-25
SS-20 W-9
O
Boyd
F
S.'..k' Ken Stewart
W-5 SS-30
B-14 O
SS-10
Freedom
Baptist
Church
Stewart
PZ-1
SS-35
Phipps
Ken Stewart
Dave Stewart
Don Stewart Mozelle
Stewart
1:4,320
S
1 inch = 360 feet
SS-15
4
9p0
"
Freedom
Baptist
Church
i
0 180 360 540
Feet
j
Source. NCOneMaD Data Services dmaaerv. Darcelsl. Forsvth Countv GIs
Data Download (Streets.
buildinasl Sources: Esri.
HERE. Garmin. IntermaD. increment P Coro.. GEBCO. USGS. FAO. NPS. NRCAN. GeoBase,
IGN, Kadaster NL Ordnance Survev,
Esri JaDan. METI. Esri China (Hong Koncl, (c) ODen StreetMaD contributors. and the GIS User Community
N
SS-90
�r All
3
aia Feu
}. huh rp n
R trraf Hall
r
Legend
'L O Saprolite/PWR Monitor Well
O Bedrock Monitor Well
Payne O Abandoned Monitor Well
k Piezometer
E Soil Boring/Piezometer
1i Soil Boring
�.. 4 Surface Water
fE
As -Built Landfill Contours (20')
Compliance Boundary
Limits of Permit
Streams
Parcels
Freeman
Payne
a Notes
1. Contour interval is 20-ft.
2. Limits of landfill are approximate based on
Frierson available historic data.
3. Streams estimated based on NC Floodplain
Mapping Program, 2008
iWagner
Figure 2
Site Area Map
Edwards Road Landfill
Permit #34-05
R.J. Reynolds Tobacco Co.
Rural Hall, North Carolina
ERM NC, Inc.
www.erm.com ERM
Coordinate System: NAD 1983 StatePlane North Carolina RIPS 3200 Feet

1100
Johnston
PZ-3
0
W-8 \
(812.45)
L___"_ PZ-4 .; O
Beck �a W-7 �AW4,`
O 42.58) PZ-5 ``
� � ? Al
PZ-1
0
W-2
PW (8
'/.. R. J. �76) / / �O811.03)Guthrie
(8\
Reynolds
W-4 W-6 O } / ;
�
0
(881.11) I �000i ♦ , boo
♦ W-3
r : • (802.08)
s ' (804.12) q, I
Sprinkle
Reynolds ``e ♦ `
rI / \ Phipps
r ,
'pp0 ~``tea ��
v,
(811.38)
Boyd
Ken Stewart
o
Phipps
7Ke, Stewart
I KFreedom
Hawks 0
a
Freedom Dave Stewart
Stewart Mozelle
BaptistStewart
Church O
1:4,320 1 inch = 360 eet 90o 00 180 360 540
Feet
ayne
Freeman
Payne
� a�
an►a �u
R uraf Hall
Legend
O Saprolite/PWR Monitor Well
O Bedrock Monitor Well
A, Piezometer
Streams
As -Built Landfill Contours (20')
Compliance Boundary
Limits of Permit
Parcels
Regional groundwater flow
Local shallow groundwater flow
Notes
1. Contour interval is 20-ft.
2. Limits of landfill are approximate based on
available historic data.
i Wagner
3. Streams estimated based on NC Floodplain
X,
Mapping Program, 2008
4. Regional and Local Shallow Groundwater
mFlow
based on groundwater modeling
(ERM, 2012)
5. Water Levels measured 05 April 2021.
o:
U
Kleitchens
❑
Q
Figure 3
Groundwater Flow Direction
o °
Edwards Road Landfill
Permit #34-05
R.J. Reynolds Tobacco Co.
Rural Hall, North Carolina
ERM NC, Inc. �d
%
r
www.erm.com ERM
-Source: NCOneMao Data Services (Imaaerv. oarcelsl. Forsvth Countv GIs Data Download (Streets. buildinasl Sources: Esri. HERE. Garmin. Intermao. increment P Coro.. GEBCO. USGS. FAO. NPS. NRCAN. GeoBase. IGN. Kadaster NL. Ordnance Survev, Esri Jaoan. METL Esri China (Nona Konal. (cl ODen StreetMao contributors, and the GIS User Community

P�.
PW-01-WG-20210405
04/05/2021
Aluminum
620
Barium
47
Cadmium
< 0.5
Chromium
7.9
Iron
8,90
Lead
2.2
Manganese
2,500
Selenium
15
Sulfate
620,000
Dissolved Solids Total
1,500,000
W-6-WG-20210405
04/05/2021
Aluminum
240
Barium
51
Cadmium
Chromium
18
Iron
490
Lead
Manganese
8.4
Selenium
Sulfate
9,000
Dissolved Solids, Total
270,000
W-7-WG-20210405
04/05/2021
Aluminum
1,900
Barium
100
Cadmium
Chromium
2
Iron
Lead
Manganese
99
Selenium
Sulfate
11,000
Dissolved Solids Total
140,000
SS-50
B_9 ---___-- B-10
B-11
NC 2L Groundwater Standard
Aluminum (ug/L)
3,500
Barium (uglL)
700
Cadmium (uglL)
2
Chromium (uglL)
10
Iron (uglL)
300
Lead (ug/L)
15
Manganese (ug/L)
50
Selenium (ug/L)
20
Sulfate (ug/L)
250,000
Dissolved Solids, Total (ug/L)
500,000
1:7,200 1 inch = 6Q0 feet
0 300 600 900
Feet
PZ-05-WG-20210406
04/06/2021
Aluminum
8,200
Barium
93
Cadmium
9.6
Chromium
9.6
Iron
31.000
Lead
3.1
Manganese
390
Selenium
< 5.0
Sulfate
19,000
Dissolved Solids, Total
110,000
r
W-8-WG-20210405
04/05/2021
Aluminum
2,000
Barium
210
Cadmium
< 0.5
Chromium
75
Iron
2.600
Lead
<
Manganese
43
Selenium
16
Sulfate
16,000
Dissolved Solids, Total
150,000
SS-8
PZ-3 SS-90
�SS_-70 `�PZ-4 _ PZ-2 /
PZ-5'_ `` / SS-40
SS'�J
SS-60
SS-65 ` PZ_1
A I� f SS-35
1SS-02
Q� /OW 1 SS-01+850
40,� '♦ �/ B-4 • ' 1
B_5 ASS-01+550
SS-95
B 8 ..., S-01+150
'--� B-7 .
SS-01
B-121*1�
SS-20 SS-25�ra
4 4 O
SS-30
❑B-14 O ^ /
SS-10
0
W-9-WG-20210406
04/06/2021
Aluminum
120
Barium
120
Cadmium
'0.5
Chromium
7.0
Iron
200
Lead
< 1.0
Manganese
< 5.0
Selenium
< 5.0
Sulfate
11,000
Dissolved Solids Total
260,000
A
W-2-WG-20210405
04/05/2021
Aluminum
120
Barium
120
Cadmium
< 0.5
Chromium
< 5.0
Iron
92
Lead
< 1.0
Manganese
83
Selenium
< 5.0
Sulfate
14,000
Dissolved Solids, Total
75,000
7WX
W-1-WG-20210405
04/05/2021
Aluminum
400
Barium
31
Cadmium
< 0.5
Chromium
< 5.0
Iron
1,200
Lead
< 1 _
Manganese
3,600
Selenium
17
Sulfate
770 000
Dissolved Solids Total
1 600 000
Barium
W-313-WG-20210405
04/05/2021
Aluminum
< 40
Barium
56
Cadmium
< 0.5
Chromium
< 5.1
Iron
130
Lead
< 1
Manganese
72
Selenium
Sulfate
16,000
Dissolved Solids, Total
250,000
°+q—
N
v
a
e
f�
l�
v
Luc Q�fhan�°�
Rural Hall
Legend
O Saprolite/PWR Monitor Well
O Bedrock Monitor Well
O Abandoned Monitor Well
z� Piezometer
0 Soil Boring/ Piezometer
1� Soil Boring
4 Surface Water
Streams
As -Built Landfill Contours (20')
triCompliance Boundary
Limits of Permit
0 Parcels
Notes
1. Limits of landfill are approximate based on
available historic data.
2. Streams estimated based on NC Floodplain
Mapping Program, 2008
3. All concentrations in micrograms per liter
(ug/L)
4. Metals analyses in piezometer samples
discontinued in September 2020
5. PZ-01, PZ-03, & PZ-04 were dry
6. PZ-05 has been destroyed
Figure 4
Groundwater Sampling
Results - April 2021
Edwards Road Landfill
Permit #34-05
R.J. Reynolds Tobacco Co.
Rural Hall, North Carolina
ERM NC, Inc. �d
www.erm.com ERM
Source, NCOneMaD Data Services (Imaaerv. Darcelsl. Forsvth Countv GIS Data Download (Streets. buildings) Sources. Esri. HERE, Garmin. Intem— increment P Coro- GEBCO, USGS, FAO, NPS. NRCAN. GeoBase. IGN, Kadaster NL. Ordnance Survev. Esri daoan. METI. Esri China (Nona Kona). (cl ODen StreetMaD contributorsand the GIS User Community

SS-60-WS-20210406
04/06/2021
Aluminum
1,500
Barium
53
Cadmium
< 0.5
Chromium
< 5.0
Iron
1.200
Lead
< 1.0
Manganese
7.8
Selenium
< 5.0
Sulfate
37,000
Dissolved Solids Total
140,000
SS-50-WS-20210406
04/06/2021
Aluminum
1,700
Barium
47
Cadmium
< 0.5
Chromium
14
Iron
2,200
Lead
< 1.0
Manganese
35
Selenium
< 5.0
Sulfate
3,700
Dissolved Solids, Total
69,000
SS-50
nanum
Cadmium
Chromium
F r SS-70-WS-20210406 04/06/2021 SS
Aluminum 1,400 •� Alun
Barium 48 {,'? Bark
Cadmium < 0.5 _� Cadr
Chromium < 5.0 Chro
Iron 1,300 on
Lead < 1.0 Lead
manganese 8.3 Mam
202
100�`' -
S
< 0.5
W V k
< 5.0
I�00
< 1.0
sS-so /
PZ-3 SS-90 -
SS-70 PZ-4 _ O e PZ-2 /
W_7 PZ_5 ASS_ SSS-40 -J
O `SS-60 /
SS-65 , PZ_1
P A SS-35
�► �' ► r .
1 sS-02
SS-90-WS-20210406
04/06/2021
Aluminum
1 400
Barium
55
Cadmium
< 0.5
Chromium
< 5.0
Iron
1 500
Lead
< 1.0
Manganese
12
Selenium
< 5.0
Sulfate
14 000
Dissolved Solids, Total
110000
Aluminum
/ yy_2® Lead
.�. _ Man anese
PW-1 VV 1OV� Selenium
7 SS-01+s50 .. Sulfate
9 O\ (( 1 a - Dissolved Solids, Total
�a \--",,.-'!B-4
W-4 W-6 B 5 �. ; .
O , "I " • SS-01+550
B -� -9
W_3 0 SS-95
B-10 B-8 W-3B ;.
B-7 ♦ SS-01+�yy1550�0
B-12SS 015�i
6 B-11 y SS-20 SS-25 W_9
O
t W-5 SS-30
NC 2B Surface Water Standard
Aluminum (ug/L)
8,000
Barium (ug/L)
21,000
Cadmium (ug/L)
0.3
Chromium (ug/L)
50.1
Iron (ug/L)
1,000
Lead (ug/L)
1.49
Manganese (ug/L)
100
Selenium (ug/L)
5
Sulfate (ug/L)
250,000
Dissolved Solids, Total (ug/L)
500,000
I B-14
0
SS-10
Barium
Cadmium
Chromiun
Iron
Lead
M-ane
m <11 Selenium
o Sulfate
y Dissolved Solids Total
1:7,200 1 inch = fi00 feet
Q 0 300 600 900 g
J Feet d
- 4
1Source: NCOneMap Data Services (Imagery, parcels), Forsyth County GIS Data Download (Streets, buildings) NCDOT GIS Unit
IY
SS-30-WS-20210406
04/06/2021
Aluminum
3,800
Barium
65
Cadmium
< 0.5
Chromium
6.1
Iron
4,100
Lead
1.4
Manganese
32
Selenium
< 5.0
Sulfate
25,000
Dissolved Solids, Total
200,000
it
6 IN
t
N
pia
3
f
Luc Qrfltanr�.
Rurai Hal!
-
Legend
O Saprolite/PWR Monitor Well
O Bedrock Monitor Well
O Abandoned Monitor Well
z� Piezometer
0 Soil Boring/Piezometer
1i Soil Boring
4 Surface Water
16/2021
Streams
2,100
57
- As -Built Landfill Contours (20')
<
0
triCompliance Boundary
2,00000
_
~ Limits of Permit
<1.0
14
0 Parcels
<s.0
23,000
70 000
Notes
SS-02-WS-20210406
04/06/2021
Aluminum
2,000
Barium
58
Cadmium
Chromium
82
Iron
2,900
Lead
I
Manganese
25
Selenium
< 5.0
Sulfate
26,000
Dissolved Solids Total
170,000
SS-01-WS-20210406
04/06/2021
Aluminum
2,800
Barium
66.0
Cadmium
< 0 G
Chromium
<
Iron
3,300
Lead
1.1
Manganese
24
Selenium
Sulfate
20,000
Dissolved Solids Total
170,000
1. Limits of landfill are approximate based on
available historic data.
2. Streams estimated based on NC Floodplain
Mapping Program, 2008
3. All concentrations in micrograms per liter
(ug/L)
Figure 5
Surface Water Sampling
Results - April 2021
Edwards Road Landfill
Permit #34-05
R.J. Reynolds Tobacco Co.
Rural Hall, North Carolina
ERM NC, Inc. �d
www.erm.com ERM
Coordinate System: NAD 1983 StatePlane North Carolina RIPS 3200 Feet
rces: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS, FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, Esri Japan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, and the GIS User Community

> Sulfate Concentrations - Most Recent
Monitoring Wells Piezometers
Date
Sulfate
u /L
PW-01
04/05/2021
620,000
W-01
04/05/2021
770,000
W-02
04/05/2021
14,000
W-03
04/05/2021
110.000
W-03B
04/05/2021
16.000
W-06
04/05/2021
9 000
W-07
04/05/2021
11000
W-08
04/05/2021
16 000
W-09
04/06/2021
11000
Date
Sulfate
u /L
PZ-01
03/07/2016
110,000
PZ-02
09/23/2020
24,000
PZ-04
04/01/2020
37,000
PZ-05
04/06/2021
19,000
NC Groundwater & Surface Water Standard = 250,000 ug/L
Previous sample collected from PZ-03 = 18,000.
See tables and appendices for additional results.
U)
0
CAA . 1
MF
S�
�n
Surface Water
Date
Sulfate
u /L
SS-01
04/06/2021
20,000
SS-02
04/06/2021
26,000
SS-20
04/06/2021
4,300
SS-25
04/06/2021
8,000
SS•30
04/06/2021
25.000
SS-35
09/08/2015
170,000
SS-40
04/06/2021
23,000
SS-50
04/06/2021
3,700
SS-60
04/06/2021
37,000
SS-65
09/08/2015
44,000
SS-70
04/06/2021
9 500
SS-75
09/08/2015
41000
SS-80
04/06/2021
11000
SS-90
04/06/2021
14,000
SS-95
0212412020
160,000
900
+. Johnston
.IA . it
60,9
-�SS-80
(11 000)
SS-70. w-o8
W-07 • (9,500) - 0(16,000)' , 4ss.
�T_
V1,000) SS-605 PZ-05 (23'
lu
r tat (19'OOO)
y s wa02
�ccc - ❑ •' f-_,r�� (14,000)
. W-01�.
R. J. Guthrie
Reynolds 11 OPW-01 Q(770,000)
(620,000)
00
W-06 n ram♦ Sprinkle
4SS-50 �l O (9,000)
(3,700) , '` I (110 0,- r, W 0313
Eel,s,000)
a :fie,..
Reynolds SS-01, .
�(20,000)
Phipps
imom IWO
trf
Payne
Rp-
5�
Frame ieman
1
(A) 0 SS-20 SS-25 W-09 \ . A i
loon Boyd ' " �(4,300) �(8,000) �(11,000)x
Phipps Kleitch
-30 O SS Ken Stewart •
_199.1 0 25 000 —�
_ ( ) ` Ken Stewart
1 ` •
p00b Don`
Stewart �.�
o Don Stewart� Dave
'Stewart
Hawks
Mozelle
Stewart: .
o Freedom tist
CChurch •
r000' •
� 3 .
N
c,
0 1:7,200 1 inch = 800 feet
;r 0 300 600 900
L .. Feet
LI
Source: NCOneMaD Data Services (Imaaew. Darcels). Forsvth Countv GIS Data Download
—lo \A
m goo� NAQ-_2 J4
r RMq�
buildings) Sources: Esri. HERE. Garmin. IntermaD. increment P Coro.. GEB
Freedom
' Baptist
Church
Frier�n
Payne
U
w
1; w
iN R_D 900
o }¢
USGS. FAO. NIPS. NRCAN. GeoBase. IGN. Kadaster NL. Ordnance Survev. Esri JaDan`METL Esri China (Hong Kona). (c) ODen StreetMaD contributors. and the CIS User Communitv
N
A
3
f�
IR"thant''T
Rdrai Hall
Legend
D Saprolite/PWR Monitor Well
0 Bedrock Monitor Well
O Abandoned Monitor Well
� Piezometer
0 Soil Boring/Piezometer
4 Surface Water
Water Supply Well
Streams
As -Built Landfill Contours (20')
trjCompliance Boundary
Limits of Permit
0 Parcels
Sulfate Isoconcentration
Contours
> 250,000 ug/L
> 750,000 ug/L
Notes
1. Contour interval is 20-ft.
2. Limits of landfill are approximate based on
available historic data.
3. Streams estimated based on NC Floodplain
Mapping Program, 2008
Figure 6
Sulfate Isocontour Map
Groundwater
Edwards Road Landfill
Permit #34-05
R.J. Reynolds Tobacco Co.
Rural Hall, North Carolina
ERM NC, Inc.
www.erm.com ERM

0
u
o A
0
1000
950
S
900 1
850 I
800
750
700
d
W 650
600
550
500
r
450
400 L
0
Unnamed
## Tributary
.... �.., . �.... _... -.
:'�+:•'•o::"'�- 1 rr.-r � rri r t r , ,l, ,r:-p-o;".': -�':.�r.i .. to
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IL 0 950
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W-3B is Leak - #-
»..::.: �.�1:p•': �..:;:::..:-: �•. •.. artesian
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m _
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r 850
, rl.-r,•♦w- - - - 1.-r, •�l,r�ir, 00.. ..... : ,: ,.. .: �,: .;.,..-, �.,N.-rt•,
p
- i , i - w i , i - — 1 _ J , - .. - .. .' r • ` - ` f M1 r f 800
,r
- , SS 01 'r, r, r-,..'�!-r!•rr, rr, rr,• r vr�`: r"r_rr. rr,� rr •r ,- rl.rr,-
W-03._
20,0001i,
7F rr rr: ; ];: -. '1; ;r -' ` ' I r'r; 750
yr �,} r. - _ _ .,. .,r ;�r ..
olv'
♦ dC4 rf; rr,• , ; r •, rl; r +,rrir +,rr,` +,rr�/C' rr r!! +r
,q a
9/e@r?r �'-:'•a:= -.� "r=`^=l ;= ;== ;=_'_;4r �9 - 700
620,000f rrc% •� r,rl,rf,r, , l,r,r,^r ,r,r,r ,r,r,r .r,! ag2 r`r
r r.
r-SSI(�'�300:r'r11,000
650
Z0ry�so.p
- -
ii -r :.�rkr%r'irkf,r ir.f,r
r,
-,.;,
:,�.;.� �':,r;`:�
W-03B
r•;,.�,-,�,.�,r,f,.;
rr rr, r rf,-e,rl,^e,r;, r r;
600
Bedrock
,rr,�'r
i5',=, ,. 1, lff,r
s`
r
,!,: r.-, i! �:•. i r e f „� i r I I „! I I, Z' . I r 7
r rr`
♦
-
�r r •rr �; ,tiif�.' ��+':r�,�^+' rrM1�^,ti_f-
550
500
1, k_`r
450
!!!t' r �• 1 -'r r -
�
' . rr,1, r � it � • , r r ,Jr t • ,
400
125 250 375 500 625 750 875 1000 1125 1250 1375 1500 1625 1750 1875 2000 2125 2250 2375 2500 2625 2750 2875 3000
N SS � 70 PZA
�
A
W-, 55-]5
O PZ-5
SSEO� ,
4 SSES 006
■
V j1 [PW ., W.
B.
W4W-5 B�
� - , :W-3 •
' ► Ss-9 W-3B
B-S
1 ss
i ss-0,
Ss-25
0 325 650
Feet Wa ss-30
A
O W8
PZ-2'
SS-00
PZ1/
155-35
rSS 2
W-2
1
SS01,850
1` I
150
a
W 9 l JI
90o A' 11
O Saprolite/PWR Monitor Well
O Bedrock Monitor Well
0 Piezometer
0 Soil Boring/ Piezometer
N Soil Boring
Surface Water
Regional Groundwater Flow
CwCompliance Boundary
C":JLimits of Permit
Sulfate Concentrations - Most Recent
Monitoring Wells Piezometers
Date
Sulfate
(ug/L)
PW-01
04/05/2021
620,000
W-01
04/05/2021
770,000
W-02
04/05/2021
14,000
W-03
04/05/2021
110,000
W-03B
04/05/2021
16,000
W-06
04/05/2021
9,000
W-07
04/05/2021
11000
W-08
04/05/2021
16,000
W-09
04/06/2oz1
11000
Date
Sulfate
(ug/L)
PZ-01
03/07/2016
110,000
PZ-02
09/23/2020
24,000
PZ-04
04/01/2020
37,000
PZ-05
04/06/2021
19,000
NC Groundwater & Surface Water Standard = 250,000 ug/L
Previous sample collected from PZ-03 = 18,000.
See tables and appendices for additional results.
Surface Water
Date
Sulfate
(ug/L)
SS-01
04/06/2021
20,000
SS-02
04/06/2021
26,000
SS-20
04/06/2021
4,300
SS-25
04/06/2021
8,000
SS-30
04/06/2021
25,000
SS-35
09/08/2015
170,000
SS-40
04/06/2021
23,000
SS-50
04/06/2021
3,700
SS-60
04/06/2021
37,000
SS-65
09/08/2015
44,000
SS-70
04/06/2021
9,500
SS-75
09/08/2015
41000
SS-80
04/06/2021
11000
SS-90
04/06/2021
14 000
SS-95
02/24/2020
1so 000
_+ Local Groundwater
Flow
_ Local Perched
-� - Water Flow
Bedrock Fracture
Water Level
Well Details
Casing
F7771 Screen
Subsurface Details
Landfill
Confining Unit
Saprolite
Bedrock
Bedrock
Notes:
? - Estimated /Assumed
Vertical Exaggeration = 2:1
1 inch = 250 feet
Figure 7
Hydrogeologic
Conceptual Model
Edwards Road Landfill
Permit #34-05
R.J. Reynolds Tobacco Co.
Rural Hall, North Carolina
Environmental Resources Management
www.erm.com ERM

4,000
3,500
3,000
2,500
2,000
1,500
1,000
500
MONITORING WELL W-1 ms MONITORING WELL W-2 ms u°h MONITORING WELL W-3
uV
000
SAPROLITEAOLIIFER Synthetic cap
000
000
000
000
000
000
000
0
814
813
812
811
810
809
808
807
806
SOS
.mow
3,Soo,0o0
3,W0,000
SAPROLITE/PWR AQUIFER Synthetic cap
ainstalled 3Q2012
2,500,000
2,o
,OW
1
1,5oo,o00
L,ao0,0ao
soo,oao
0
--
1/I I
L
-j- -
816 3,aao,a0o
814
1,200,000
812
1,000,000
810
800,000
808
806
804 400,000
802 200,am
SOO o
Aso e 1A� 0 'e e ryo°e, ti0d 'e
'p-, ry^ 'P" e ,P0 'e tio'p' le le 0 le ry° ryo°°. 10, e do^O 1p 1011 1011 10 101 'o` 4P Anry 991 94' e0 le 0le le ryooe ryo^° ry^ ho^° ryo ,yo^° ryoti°
MONITORING WELL W3B AMSL BACKGROUND MONITORING WELL W-4 & W-6 AMSL MONITORING WELL W-7
1,000.000
800,000
600,000
400,000
200,000
350,
300,
250,
200,
150,
100,
50,
BEDROCKAQUIFER Synthetic cap
nstalled 3Q2012
GW Elevati
>804.53 (aneaia
jV �VVVV
809
BEDROCKAQUIFER Synthetic cap
installed 3Q2012
700,000
886
2003-Present
200,000
808
800,000
W-4:L20O3.:
884
807
500,000
806
882 150,000
400,000
805
880
300,000
100,000
804
--------
878
803 200,000
50,000
876
802 100,000
n
805
804
803
802
801
800
799
798
797
796
n
AMSL
844
942
840
838
836
834
832
e1101h 1101 e 110^ ,10^ 10^ ,yl 10* I'll l e e 160 e 101^ 1101 ,10l ,yl 109 ,�I'
MONITORING WELL W-8 AIL MONITORING WELL WA AIL wti MONITORING WELL PW-1 AMSL
VV
PWRAQUIFER,
1
000
Installed 4Q2010
81
Synthetic cap
installed 3Q2012
00)
80
000
80
00)
-
80
000
80
000
80
0
79
,�VVV
0 300,000
8
6
4
0
8
SAPROLITE AQUIFER
Synthetic cap _"
installed 3Q2012
jV
808
z5o,000
rY
806
200,000
804
150,000
-
802
100,000
Aft2
800
50,000
798
0
796
,.VVVV
BEDROCKAQUIFER
..
Synthetic cap
864
3,000,000
installed 3Q2012
2,500.000
862
860
2,000,000
"
858
1,500.000
856
1,000,000
854
500.000
852
0
"SO
ti�^" ryQ1 101 10� ,109 10'1� ^o"" ryo1 ,yo" ,log ,10.°' ryoh ^9" ^9" ^9" K 1OcQ ^co'I' 41 ^ ,100� �o ,101 do^4 (100 ,10 ryo'V ryp'17'
LEGEND NC21- GW STD NC213 SW STD FIGUF
Sulfates 250,000 ug/L 250,000 ug/L SULFATE TRENDS - GROUNDWATER
Total Dissolved Solids 500,000 ug/L 500,000 ug/L ERM NC, Inc. EDWARDS ROAD LANDFILL - PERMIT # 34-05 j
Groundwater Table Elevation (above Mean Sea Level) VVT' "•ermXO ' ERM RURAL HALL, NORTH CAROLINA

WL
SURFACE WATER SS-01
400,..E
200,000
Synthetic cap
000,000
installed 3Q2012
800,000
600,000
400,000
200,000
-
9�A : : D�OAd' O�CY ^P' �O Ory N O ONO ON O O �Oti
ryryry tiro ry ryry°°ry ry° ry ry°ry ry°ryn.ryryryryry°ry ry°
�0 SIIRFArF WATER SS3a
rVuuV
3so,0oo
Synthetic cap
installed 302012
300,000
250,000
200,000
150.000
100,000
,
50,000
0
ry� ryo ryo^ ry�ry ry0� e ry°� ryOe ry°, ryo ryo ry°� ry°ti
SURFACE WATER SS-70
250,000
201
151
10[
5[
Synthetic cap
000
installed 3Q2012
000
A
000
000
� •
0
SURFACE WATER SS-02
V
900,000
Synthetic cap
installed 3Q2012
800,000
r
700.000
600,000
500,000
400,000
300,000
-
- - -
200,000
100,000
0
Asa SURFACE WATER SS-40
00,000
Synthetic cap
installed 3Q2012
00,000
oo,000
00,000
-
00,000
-
00,000
MOM
a
'Pe ry,10 ry^^ ry1, ryp f ryOw ry0,1 ry0b ryo 1 hour ryOy ry°'V ry0'1l,
WL SURFACE WATER SS-80
300,
250,
200,
IN,
100,
so,
000
Synthetic cap
installed 3Q2012
000
000
-
000
000
\
000
4
0
�77
LEGEND
NC2L GIN STD NC2B SW STD
Sulfates 250,000 ug/L 250,000 ug/L ERM NC, Inc.
0 Total Dissolved Solids 500,000 ug/L 500,000 ug/L www.erm.com ERM
VL SURFACE WATER SS-25
IN, 000
160,
140,
120,
100,
so,
60,
40,
20,
00o
000
Synthetic cap
installed 3Q2012
000
000
000
`
000
000
000
O '' A ^ ry 6 1 0 N
ry� � ry°O,, � � ry^P ry rv� �E ry
VL SURFACE WATER SS-60
Mo,000
700,000
600,000
s00,0o0
400,000
no,000
200,000
100,000
0
Synthetic cap
installed
3Q42012
u
L
O '1. P '' O � O 9
tio^ ryo`` ryo^ ry°^A ry° ry° ,yo^ ryo^ ryo^ ry° ry°'B 16ry
SURFACE WATER SS-90
600,000
s00,000
400,000
300,000
200,000
100,000
0
'L° ry°° 'V°'1- ° O ' O 9
'V P 'V 'V° O 'V° 'V° 'V° ry°'L° 'Vry ry°'p'

TABLE 1
MONITOR WELL CONSTRUCTION DETAILS
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Page 1 of 1
Outer
Ground
TOC
Boring
Casing
Screened
Geologic
Well
Install
Elevation
Elevation
Depth
Depth
Interval
Zone
ID
Date
Latitude
Longitude
(ft MSL)
(ft MSL)
(ft BGL)
(ft BGL)
(ft BGL)
Screened
Comments
Former supply well, pump removed (8/09): 6 inch dia. gals. casing; Construction details per
405
Clayton Well Drilling log and video inspection by ERM (8/09 & 4/10); Open rock to 405 ft, Total
PW-1
5/26/87
36.2499455°
-80.2779362°
920.51
920.66
(soft bottom
21.5
21.5-405
Bedrock
well yield 25 gpm with no other obvious water -bearing zones below 103 ft (Clayton). Silted in to
819.69
at 326)
326 ft (video).
W-1
10/13/87
36.2500121°
-80.2757441'
822.68
20.5
NA
10-20
Saprolite
2 inch dia. PVC, Well replaced 11/93, DWM permit -required sample location
W-2
12/6/89
36.2504070°
-80.2753700'
824.21
827.30
17
NA
7-17
Sap/PWR
2 inch dia. PVC, DWM permit -required sample location, (alternate IDs MW-1A, RH-MW-002)
W-3
12/7/89
36.2486237'
-80.2761346'
802.00
804.43
17
NA
7-17
Sap/PWR
2 inch dia. PVC, DWM permit -required sample location, (alternate IDs W-3A, W-2A, RH-MW-003)
W-3B
5/14/04
36.2485693°
-80.2761875'
801.23
804.32
210
Unknown
190-210
Bedrock
2 inch dia. PVC, DWM permit -required sample location, Artesian well
W-4
6/8/93
36.24693455'
-80.28491769° �
NE
NE
188
NA
138-188
Bedrock
2 inch dia. PVC, damaged, abandoned 8127103, former background well, replaced with W-6 in 2003.
W-5
5/17/93
36.24629033° "
-80.27862892° *
NE
NE
24
NA
13-23.5
Bedrock
2 inch dia PVC, Phase 3 permanent MW
W-6
8/22/03
36.2490276'
-80.2819968'
977.93
980.71
200
NA
170-200
Bedrock
2 inch dia. PVC, DWM permit -required sample location, (alternate IDs MW-6), current
background well, replaced W-4 as background well in 2003
W-7
12/15/10
36.2517944°
-80.2798058'
929.51
931.58
341
NA
42-341
Bedrock
6 inch dia. open -rock hole, 6" galavanized casing to 42 ft bgs, TOC value for 6" casing
W-8
12/14/10
36.2524760°
-80.2744895'
859.39
861.67
129
NA
45-65
PWR
2 inch dia. PVC
W-9
12/13/10
36.2469581°
-80.2750675'
909.35
911.38
259
NA
229-259
Bedrock
2 inch dia. PVC, Ken Stewart's pasture,
B-9
5/20/93
36.24819778' "
-80.28420462° "
NE
NE
23
NA
18-22.5
Saprolite
2 inch dia PVC, Phase 3 temporary piezometer, abandoned Dec. 2019
B-10
5/19/93
36.24815194' `
-80.28243419' *
NE
NE
14
NA
9-13.5
Saprolite
2 inch dia PVC, Phase 3 temporary piezometer, not located Oct. 2009 or Dec. 2019
B-11
5/20/93
36.24695712' "
-80.28385595° '
NE
NE
54
NA
48-53
Saprolite
2 inch dia PVC, Phase 3 temporary piezometer, not located Dec. 2019
B-12
5/19/93
36.24765518°
-80.28079913° *
NE
NE
8.5
NA
3.5-8
Saprolite
2 inch dia PVC, Phase 3 temporary piezometer, no protective well box around well
B-14
5/20/93
36.2461299° *
-80.28188639° "
NE
I NE
54
NA
48-53
Saprolite
2 inch dia PVC, Phase 3 temporary piezometer, abandoned Dec. 2019
PZ-1
3/15/16
36.25134616'
-80.2740505' '
NE
NE
1.5
NA
1.0 - 1.5
Alluvium
1 inch dia PVC temporary piezometer. Originally installed 12/2010. Replaced 3/2016
PZ-2
12/15/10
36.25229952' '
-80.27330537' '
NE
NE
4.0
NA
3.0 - 4.0
Alluvium
1 inch dia PVC temporary piezometer
PZ-3
12/15/10
36.25292715'
-80.27477259' '
NE
NE
1.5
NA
0.5 - 1.5
Alluvium
1 inch dia PVC temporary piezometer
PZ-4
12/16/10
36.25225065' '
-80.27644449' '
NE
NE
5.0
NA
4.2 - 5.0
Alluvium
1 inch dia PVC temporary piezometer
PZ-5
12/16/10
36.25178958'
-80.27767072' '
NE
NE
5.0
NA
3.0 - 5.0
Alluvium
1 inch dia PVC temporary piezometer
PZ-6
2/18/20
NE
NE
NE
834.3'
3.5
NA
1.5 - 3.5
Fill/Saprolit
1 inch dia PVC temporary piezometer installed for boil evaluation at ST-1
PZ-7
2/18/20
NE
NE
NE
833.7 *
4.5
NA
1.5-4.5
Fill/Saprolit
1 inch dia PVC temporary piezometer installed for boil evaluation at ST-1
PZ-8
2/18/20
NE
NE
NE
830.7'
5.0
NA
2.0 - 5.0
Fill/Saprolit
1 inch dia PVC temporary piezometer installed for boil evaluation at ST-1
PZ-9
2/18/20
NE
NE
NE
834.6 *
4.5
NA
1.5-4.5
Fill/Saprolit
1 inch dia PVC temporary piezometer installed for boil evaluation at ST-1
PZ-10
2/24/20
NE
NE
NE
839.9'
4.0
NA
1.0 - 4.0
Fill/Saprolit
1 inch dia PVC temporary piezometer installed for boil evaluation at ST-1
NE - Not Established BGL - Below ground level NM - Not Measured
MSL - above mean sea level BTOC - Below top of casing " - Estimated value
RJRTI Tables RJRT Ash LF.xlsAl. Well Construction
PWR = Partially Weathered Rock
Survey data by Lawrence Associates, P.A., January 4, 2010, January 4, 2011 & February 28, 2011

TABLE 2
GROUNDWATER ELEVATIONS
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Monitor Well ID
PW-01
W-01
W-02
W-03
W-03B
TOC Elevation
920.7
822.7
827.3
804.4
804.3
Start Screen Depth
21.5
10
7
7
190
End Screen Depth
405
20
17
17
210
Geologic Unit
Bedrock
Saprolite
Saprolite/PWR
Saprolite/PWR
Bedrock -Artesian
Date
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
2006-10-19
11.59
811.09
13.32
813.98
7.54
796.89
Artesian
2007-04-27
10.88
811.80
13.96
813.34
6.98
797.45
Artesian
-
2007-11-19
13.29
809.39
16.08
811.22
7.78
796.65
Artesian
2008-04-30
12.84
809.84
14.68
812.62
7.04
797.39
Artesian
-
2009-04-30
13.23
809.45
15.18
812.12
7.12
797.31
Artesian
2009-10-12
72.00
848.66
14.53
808.15
17.50
809.80
7.63
796.80
-1.22
805.54
2010-04-19
67.00
853.66
10.75
811.93
14.16
813.14
6.37
798.06
-1.05
805.37
2010-10-11
12.04
810.64
15.85
811.45
6.99
797.44
-0.89
805.21
2011-01-05
11.97
810.71
13.53
813.77
6.88
797.55
-0.98
805.30
2011-02-28
65.30
855.36
11.66
811.02
14.57
812.73
6.65
797.78
-1.37
805.69
2011-04-20
64.75
855.91
10.92
811.76
14.05
813.25
6.25
798.18
-1.63
805.95
2011-10-17
12.55
810.13
15.18
812.12
7.24
797.19
-1.36
805.68
2012-02-06
64.96
855.70
11.97
810.71
13.52
813.78
6.52
797.91
Artesian
2012-03-16
11.95
810.73
15.45
811.85
6.64
797.79
Artesian
-
2012-09-24
66.03
854.63
11.93
810.75
15.36
811.94
4.87
799.56
Artesian
2013-04-17
65.80
854.86
11.98
810.70
14.03
813.27
4.51
799.92
Artesian
-
2013-09-10
66.75
853.91
13.01
809.67
15.75
811.55
3.45
800.98
Artesian
2014-04-07
56.15
864.51
11.74
810.94
16.76
810.54
3.29
801.14
Artesian
-
2014-09-03
67.28
853.38
14.37
808.31
16.65
810.65
3.29
801.14
Artesian
2015-04-02
64.75
855.91
13.29
809.39
13.93
813.37
3.78
800.65
Artesian
-
2015-09-08
--
-
--
-
2015-09-10
65.49
855.17
15.18
807.50
17.01
810.29
4.20
800.23
Artesian
-
2016-03-08
62.75
857.91
12.42
810.26
13.32
813.98
2.80
801.63
Artesian
2016-09-06
67.21
853.45
14.92
807.76
16.68
810.62
3.31
801.12
Artesian
-
2017-03-27
65.34
855.32
15.50
807.18
15.33
811.97
3.89
800.54
Artesian
2017-09-25
65.50
855.16
16.02
806.66
16.89
810.41
3.32
801.11
Artesian
-
2018-03-05
66.00
854.66
16.10
806.58
11.90
815.40
4.45
799.98
Artesian
2018-09-12
65.44
855.22
15.88
806.80
16.95
810.35
4.24
800.19
Artesian
2019-03-19
61.00
859.66
11.20
811.48
6.23
821.07
1.88
802.55
0.00
804.32
2019-03-20
--
-
--
-
2019-09-03
65.50
855.16
15.05
807.63
16.23
811.07
319
801.24
0.00
804.32
2020-02-13
67.61
853.05
10.31
812.37
5.03
822.27
2.98
801.45
0.21
804.11
2020-02-18
67
67.02
853.66
853.64
11.76
11.8
810.92
810.88
6.11
6.12
821.19
821.18
3.24
3.24
801.19
801.19
0.07
0.08
804.25
804.24
2020-02-24
66.70
853.96
12.81
809.87
6.13
821.17
3.38
801.05
0.20
804.12
2020-03-04
66.82
853.84
12.29
810.39
6.29
821.01
3.43
801.00
0.21
804.11
2020-03-31
66.38
854.28
13.28
809.40
13.23
814.07
3.43
801.00
1.05
803.27
2020-09-22
67.42
853.24
15.02
807.66
15.38
811.92
3.81
800.62
0.50
803.82
2021-04-05
63.90
856.76
11.65
811.03
9.64
817.66
2.35
802.08
0.20
804.12
Notes:
NE = Not Established
MSL = above mean sea level
BTOC = Below Top of Casing
PWR = Partially Weathered Rock
BGL - Below ground level
Artesian condition -Value
represents water level
above permanent TOC.
Measured via temporary
standpipe installed on
permanent casing.
Page 1 of 4

TABLE 2
GROUNDWATER ELEVATIONS
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Monitor Well ID
W-05
W-06
W-07
W-08
W-09
TOC Elevation
980.7
931.6
861.7
911.4
Start Screen Depth
13
170
42
45
229
End Screen Depth
23.5
200
341
65
259
Geologic Unit
Bedrock
Bedrock
Bedrock
PWR
Bedrock
Date
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
2006-10-19
--
--
99.00
881.71
--
--
--
--
--
--
2007-04-27
--
-
94.48
886.23
--
--
--
-
--
--
2007-11-19
--
--
105.00
875.71
--
--
--
-
--
--
2008-04-30
--
-
99.29
881.42
--
--
--
-
--
--
2009-04-30
--
--
98.28
882.43
--
-
--
-
--
--
2009-10-12
10.08
99.64
881.07
2010-04-19
8.38
98.29
882.42
2010-10-11
9.73
-
98.93
881.78
2011-01-05
9.67
98.92
881.79
94.73
836.85
52.67
809.00
110.47
800.91
2011-02-28
9.50
-
99.01
881.70
94.59
836.99
53.45
808.22
112.03
799.35
2011-04-20
7.85
98.42
882.29
94.20
837.38
53.54
808.13
110.03
801.35
2011-10-17
-
99.41
881.30
2012-02-06
99.22
881.49
94.71
836.87
54.74
806.93
109.84
801.54
2012-03-16
-
-
99.05
881.66
2012-09-24
99.63
881.08
96.05
835.53
55.47
806.20
110.26
801.12
2013-04-17
-
-
99.04
881.67
95.80
835.78
57.40
804.27
108.62
802.76
2013-09-10
98.86
881.85
94.71
836.87
54.20
807.47
110.23
801.15
2014-04-07
-
-
98.23
882.48
95.26
836.32
54.01
807.66
110.86
800.52
2014-09-03
98.93
881.78
94.90
836.68
52.78
808.89
110.68
800.70
2015-04-02
-
99.45
881.26
94.52
837.06
56.22
805.45
110.50
800.88
2015-09-08
58.22
803.45
110.50
800.88
2015-09-10
-
-
99.51
881.20
95.23
836.35
2016-03-08
98.62
882.09
93.95
837.63
59.01
802.66
110.06
801.32
2016-09-06
-
-
98.90
881.81
94.05
837.53
53.19
808.48
110.11
801.27
2017-03-27
99.10
881.61
94.41
837.17
56.00
805.67
109.90
801.48
2017-09-25
-
-
99.68
881.03
95.01
836.57
56.96
804.71
109.30
802.08
2018-03-05
99.94
880.77
94.60
836.98
60.60
801.07
110.30
801.08
2018-09-12
-
100.05
880.66
94.83
836.75
61.60
800.07
110.33
801.05
2019-03-19
--
--
--
-
2019-03-20
98.59
882.12
92.07
839.51
58.35
803.32
110.06
801.32
2019-09-03
99.46
881.25
92.98
838.60
52.28
809.39
109.54
801.84
2020-02-13
93.41
887.30
91.72
839.86
53.37
808.30
2020-02-18
--
--
99.14
99.12
881.57
881.59
92.08
92.09
839.5
839.49
53.34
53.33
808.33
808.34
--
2020-02-24
-
99.13
881.58
92.25
839.33
53.45
808.22
2020-03-04
99.14
881.57
92.23
839.35
53.49
808.18
2020-03-31
-
99.00
881.71
91.81
839.77
52.99
808.68
110.00
801.38
2020-09-22
100.05
880.66
92.60
838.98
51.12
810.55
100.00
811.38
2021-04-05
--
-
99.60
881.11
89.00
842.58
49.22
812.45
100.00
811.38
Notes:
NE = Not Established
MSL = above mean sea leve
BTOC = Below Top of Casin
PWR = Partially Weathered
BGL - Below ground level
Artesian condition -Value
represents water level
above permanent TOC.
Measured via temporary
standpipe installed on
permanent casing.
Page 2 of 4

TABLE 2
GROUNDWATER ELEVATIONS
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Monitor Well ID
TOC Elevation
B-09
B-12
PZ-06
PZ-07
PZ-08
834.3
833.7
830.7
Start Screen Depth
End Screen Depth
18
3.5
1.5
1.5
2
22.5
8
3.5
4.5
5
Geologic Unit
Saprolite
Saprolite
Fill Soil/Saprolite
Fill Soil/Saprolite
Fill Soil/Saprolite
Date
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
2006-10-19
--
--
--
--
--
--
--
--
--
--
2007-04-27
--
--
--
--
2007-11-19
--
--
--
--
--
--
--
--
--
--
2008-04-30
--
--
--
--
2009-04-30
--
--
--
--
--
--
--
--
--
--
2009-10-12
20.40
--
10.26
--
--
--
--
--
--
--
2010-04-19
18.78
--
6.18
--
--
--
--
--
--
2010-10-11
21.63
--
9.40
--
--
--
--
--
--
--
2011-01-05
22.05
--
9.05
--
--
--
--
--
--
2011-02-28
22.63
--
--
--
--
--
2011-04-20
21.45
--
5.46
--
--
--
--
--
--
2011-10-17
--
--
--
--
2012-02-06
--
--
--
--
--
--
--
--
--
--
2012-03-16
--
--
--
--
2012-09-24
--
--
--
--
--
--
--
--
--
--
2013-04-17
--
--
--
--
2013-09-10
--
--
--
--
--
--
--
--
--
--
2014-04-07
--
--
--
--
2014-09-03
--
--
--
--
--
--
--
--
--
--
2015-04-02
--
--
--
--
2015-09-08
--
--
--
--
--
--
--
--
--
--
2015-09-10
--
--
--
--
2016-03-08
--
--
--
--
--
--
--
--
--
--
2016-09-06
--
--
--
--
2017-03-27
--
--
--
--
--
--
--
--
--
--
2017-09-25
--
--
--
--
2018-03-05
--
--
--
--
--
--
--
--
--
--
2018-09-12
--
--
--
--
2019-03-19
--
--
--
--
--
--
--
--
--
--
2019-03-20
--
--
--
--
2019-09-03
--
--
--
--
--
--
--
--
--
--
2020-02-13
--
--
--
--
Dry
Dry
Dry
--
2020-02-18
--
--
--
--
--
--
--
--
--
--
2020-02-24
--
--
--
--
Dry
D
--
Dry
--
2020-03-04
.87
8240
9.69
824.018
Dry
2020-03-31
824.31
2020-09-22
--
--
--
2021-04-O5
--
--
--
--
Notes:
NE = Not Established
MSL = above mean sea levc
BTOC = Below Top of Casin
PW R = Partially Weathered
BGL - Below ground level
Artesian condition - Value
represents water level
above permanent TOG.
Measured via temporary
standpipe installed on
permanent casing.
Page 3 of 4

TABLE 2
GROUNDWATER ELEVATIONS
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Monitor Well ID
TOC Elevation
Start Screen Depth
End Screen Depth
Geologic Unit
PZ-09
PZ-10
834.6
839.9
1.5
1
4.5
4
Fill SoillSaprolite
Fill SoillSaprolite
Date
Depth to
Water (ft
BTOC)
Groundwater
Elev MSL)
Depth to
Water (ft
BTOC)
Groundwater
Elev (ft MSL)
2006-10-19
2007-04-27
2007-11-19
2008-04-30
2009-04-30
2009-10-12
2010-04-19
2010-10-11
2011-01-05
2011-02-28
2011-04-20
2011-10-17
2012-02-06
2012-03-16
2012-09-24
2013-04-17
2013-09-10
2014-04-07
2014-09-03
2015-04-02
2015-09-08
2015-09-10
--
2016-03-08
2016-09-06
2017-03-27
2017-09-25
--
2018-03-05
2018-09-12
2019-03-19
2019-03-20
--
2019-09-03
2020-02-13
Dry
Dry
2020-02-18
--
--
--
--
2020-02-24
Dry
9.25
830.64
2020-03-04
Dry
8.64
831.25
2020-03-31
d
8.70
831.19
2020-09-22
2021-04-OS
Notes:
NE = Not Established
MSL = above mean sea levc
BTOC = Below Top of Casin
PW R = Partially Weathered
BGL - Below ground level
Artesian condition - Value
represents water level
above permanent TOG.
Measured via temporary
standpipe installed on
permanent casing.
Page 4 of 4

TABLE 3
GROUNDWATER AND SURFACE WATER ANALYTICAL RESULTS
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
1 of 1
N
N
O
N
O
N
C_
E
£
_
E
'6
O`
R
O
3
N
N
w
>
N l0
e
3
a
m
U
U
O
o
m
J
2
y
y
LAAnal
o f
NC 2L Groundwater Standard
3,500
700
2
10
300
15
50
20
250,000
500,000
NC 26 Surface Water Standard
8,000
21,000
0.3
50.1
1,000
1.49
100
5
250,000
500,000
Sample
I
Location/ID
Sample Date
Groundwater Monitoring Wells
PW-01
4/5/2021
620
47
< 0.5
7.9
8,900
2.2
2,500
15
620,000
1,500,000
W-01
4/5/2021
400 S
31
< 0.5
< 5
1,200
< 1
3,600 S
17 S
770,000
1,600,000 H
W-02
4/5/2021
120
120
< 0.5
< 5
92
< 1
83
< 5
14,000
75,000
W-03
4/5/2021
< 40
28
< 0.5
< 5
55
< 1
32
6.7
110,000
360,000
W-03B
4/5/2021
< 40
56
< 0.5
< 5
130
< 1
72
< 5
16,000
250,000
W-06
4/5/2021
240
51
< 0.5
18
490
< 1
8.4
< 5
9,000 S
270,000
W-07
4/5/2021
1,900
1 100
< 0.5
1 22
1 5,300
1 < 1
99
< 5
1 11,000
1 140,000
W-08
4/5/2021
2,000
210
< 0.5
75
2,600
< 1
43
16
16,000
150,000
W-09
4/6/2021
120
120
< 0.5
7
200
< 1
< 5
< 5
11,000
260,000
PZ-05
4/6/2021
19,000
110,000
Surface Water
SS-01
4/6/2021
2,800
66
< 0.5
< 5
3,300
1.1
24
< 5
20,000
170,000
SS-02
4/6/2021
2,000
58
< 0.5
82
2,900
< 1
25
< 5
26,000
170,000
SS-20
4/6/2021
2,300
45
< 0.5
< 5
2,600
< 1
42
< 5
4,300
90,000
SS-25
4/6/2021
2,600
48
< 0.5
< 5
2,800
< 1
26
< 5
8,000
90,000
SS-30
4/6/2021
3,800
65
< 0.5
6.1
4,100
1.4
32
< 5
25,000
200,000
SS-40
4/6/2021
2,100
57
< 0.5
< 5
2,000
< 1
14
< 5
23,000
170,000
SS-50
4/6/2021
1,700
47
< 0.5
14
2,200
< 1
35
< 5
3,700
69,000
SS-60
4/6/2021
1,500
53
< 0.5
< 5
1,200
< 1
7.8
< 5
37,000
140,000
SS-70
4/6/2021
1,400
48
< 0.5
< 5
1,300
< 1
8.3
< 5
9,500
89,000
SS-80
4/6/2021
1,100
56
<0.5
<5
1,200
<1
6.8
<5
11,000
100,000
SS-90
4/6/2021
1,400
55
< 0.5
< 5
1,500
< 1
12
< 5
14,000
110,000
Notes:
All concentrations in micrograms per liter (pg/L) unless otherwise noted.
NE - Not established
No freshwater aquatic life standard established for barium, manganese, sulfate, and dissolved solids. Water Supply criteria presented.
Bold with gray background indicates exceedance of applicable NC Groundwater or Surface Water Standard
PAProjects\0588865 R.J. Reynolds Tobacco Co. LF 2021 Quarterly Inspec.AM\Routine Monitoring & Inspections\01 GW Monitoring\2021-04 GWS\Report-Tables\186278419-ALEII-T3-XTAB-BASE (15).xlsx

TABLE 4
GROUNDWATER AND SURFACE WATER FIELD PARAMETER RESULTS
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
N
_
E
O
G7
Cn
• 5
v
y
E
''
Z
e: E
x
O
R
O W
3
.y
O
'
E
r
'O N
fW a1
Analyte
C.
H V
V
H
O (L
o E
NC 2L Groundwater Standard
6.5-8.5
NE
NE
NE
NE
NE
NC 2B Surface Water Standard
6.0-9.0
NE
NE
NE
NE
NE
Sample
Result
Result
Result
Result
Result
Result
Location/ID
Sample Date
Groundwater Monitoring Wells
PW-01
4/5/2021
6.6
17.9
1880
58.9
85
0.43
W-01
4/5/2021
6.6
23.8
25800
0
220
0.4
W-02
4/5/2021
6.9
18.3
990
52.7
163
1.48
W-03
4/5/2021
6.5
22.7
5130
0
318
0.88
W-03B
4/5/2021
8.0
20.3
3130
0
-23
2.91
W-06
1 4/5/2021
9.7
1 17.4
1 372
1 1.8
1 16
1 4.83
W-07
4/5/2021
6.4
17.1
166
29.4
323
7.19
W-08
4/5/2021
5.9
19.9
157
94.9
1
242
1
4.54
W-09
4/6/2021
11.6
18.0
676
0
-84
0.51
Surface Water
SS-01
4/6/2021
8.1
13.0
185
52
268
9.72
SS-02
4/6/2021
8.1
14.3
200
30.2
290
10.1
SS-20
4/6/2021
8.0
17.1
53
37.7
264
7.67
SS-25
4/6/2021
8.6
12.6
78
59.2
199
9.6
SS-30
4/6/2021
8.1
12.9
217
64
252
9.56
SS-40
4/6/2021
8.1
13.8
181
26.1
286
8.11
SS-50
4/6/2021
7.6
15.8
63
47.4
290
9.42
SS-60
4/6/2021
7.8
13.0
153
7.5
294
8.09
SS-70
4/6/2021
7.9
13.6
76
6.3
290
7.95
SS-80
4/6/2021
7.9
12.8
81
8.9
288
9.26
SS-90
1 4/6/2021
1 8.0
1 12.2
1 118
12
1 271
1 9.71
Notes:
All concentrations in micrograms per liter (pg/L) unless otherwise noted.
NE - Not established
No freshwater aquatic life standard established for barium, manganese, sulfate, and dissolved solids. Water Supply criteria presented.
Bold with gray background indicates exceedance of applicable NC Groundwater or Surface Water Standard
1 of 1
P:\Projects\0588865 R.J. Reynolds Tobacco Co. LF 2021 Quarterly Inspec.AM\Routine Monitoring & Inspections\01 GW Monitoring\2021-04 GWS\Report-Tables\186278419-ALEII-T4-XTAB-
BASE (13).xlsx

APPENDIX A HISTORICAL GROUNDWATER AND SURFACE WATER
QUALITY ANALYTICAL DATA
www.erm.com Version: 1.0 Project No.: 0588865 Client: R.J. Reynolds Tobacco Co. July 2021
2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34.05
RURAL HALL, NORTH CAROLINA
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Page 1 of 9

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34.05
RURAL HALL, NORTH CAROLINA
.
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Page 2 of 9

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34.05
RURAL HALL, NORTH CAROLINA
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Page 3 of 9

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34.05
RURAL HALL, NORTH CAROLINA
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Page 4 of 9

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34.05
RURAL HALL, NORTH CAROLINA
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Page 5 of 9

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34.05
RURAL HALL, NORTH CAROLINA
•
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Page 6 of 9

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34.05
RURAL HALL, NORTH CAROLINA
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Page 7 of 9

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34.05
RURAL HALL, NORTH CAROLINA
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Page 8 of 9

APPENDIX Al
GROUNDWATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL • PERMIT 34-05
RURAL HALL, NORTH CAROLINA
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Notes:
All concentrations In micrograms per lter (uWL) unless otherwise noted
NE - Not established
--- Not sampled
B - Detected In the method blank
J - Estimated result < LOQ and > DL
Bold with gray background indicates exosedance of NC Groundwater Standard
Analysis for arseniq copper, mercury, silver, zinc, nitrates & TOC discontinued in 2014 per Corrective Action Plan (ERM, 2f2014).
NSA — Location inaccessible; no sample collected
NSB - Obstruction In well; no sample collected
NBC - Wall dry; no sample collected
NSD - Insufficient vdume; no sample collected
NSE - Wall damaged; no sample collected
NSF - Pump broken; no sample collected
NSG - Surface water location dry; no sample collected
Page 9 of 9

APPENDIX A2
SURFACE WATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
-lyte
E
-
m
ci
E
E.
ci
coi
o
E
f
mm
-
z
'z
m
M
a
>
6
o
a
U
-
1j
E
N
c
u
H
z
E
-
a
u
a
K
J
a
r
O
C 2B Surface Water
Standard
8,000
10
21,000
0.3
50.1
5.79
1,000
1.49
100
0.012
5
1.34
76.01
10,000
250,000
500,000
NE
6.0-9.0
NE
NE
50
NE
NE
Sample
Date
SS-01
4/29/1988
118
8
86
<5
<1,
15
220
64,000
220,000
2,810
6.8
SS-01
7/13/1989
100
--
-
--
< 10
< 10
-
-
-
--
--
--
--
-
-
-
SS-01
9/6/1990
a
64
< 5
< 5
7.9
SS-01
9/21/1990
140
< 10
'80
4.8
200
< 20
< 0.2
< 5
< 10
< 20
520
40,000
352,000
12,060
7.18
11.6
490
SS-01
10/23/1991
109
< 10
'80
<
)0
< 20
< 0.2
< 5
< 10
< 20
150
108,000
248,000
12,000
7.9
17.2
381
SS-01
3/25/1992
4,150
< 10
< 80
3.4
5,000
1 15.8
64
< 0.2
< 5
< 10
< 20
250
9,400
185,000
14,000
5.8
11.3
126
SS-01
9/29/1992
< 100
< 10
'100
160
-
85
< 0.2
< 5
< 10
< 20
190
84,000
241,000
2,000
5.73
13.8
356
SS-01
3/31/1993
< 200
< 10
< 100
400
77
< 0.2
< 5
< 10
29
1,340
70,400
127,000
2,000
5.89
13
207
SS-01
9/17/19931
240
1 < 10
< 125
598
28
< 0.2
< 5
< 10
< 20
1 450
77,400
1 251,000
3,000
7.07
20.9
360
SS-01
3/30/1994
220
< 10
< 120
873
30
< 0.2
< 5
< 10
< 20
250
30,600
108,000
5,000
5.88
14
380
SS-01
9/30/1994
1,300
<10
<250
1,690
6
84
<0.2
<5
<10
430
64,800
255,000
30,000
7.05
19.1
332
SS-01
3/31/1995
3,580
<10
<250
2,440
106
<0.2
<5
<10
246
190
48,900
211,000
7.75
13.9
290
SS-01
9/29/1995
200
< 10
< 250
358
7
38
< 0.2
< 5
< 10
500
70,000
264,000
3,740
5.16
13.9
458
SS-01
3/30/1996
279
<10
<250
547
14
<0.2
<5
<10
185
31,300
129,000
1,790
6.68
11
193
SS-01
9/27/1996
125
< 10
< 250
300
5
21
< 0.2
< 5
< 10
95
290
56,100
225,000
2,360
7.65
19
336
SS-01
3/29/1997
307
< 10
< 250
552
16
< 0.2
< 5
< 10
13
225
30,000
138,000
3,040
7.63
16
94
SS-01
9/17/1997
476
< 10
< 250
835
40
< 0.2
< 5
< 10
169
625
47,400
224,000
1,670
7.9
19
319
SS-01
3/27/1998
190
< 10
< 250
685
12
< 42
< 10
< 10
61
680
38,700
163,000
5,230
7.64
18.6
473
SS-01
9/30/1998
126
< 10
< 250
540
6
33
< 0.2
< 10
< 10
< 20
300
28,000
177,000
4,090
7.2
18
322
SS-01
3/31/1999
239
< 10
< 250
332
44
< 0.2
< 10
< 10
< 20
120
63,200
191,000
2,490
7.1
16
247
SS-01
9/29/1999
1,530
< 10
< 250
3,330
5
88
< 0.2
< 10
< 10
< 20
90
23,200
143,000
8,810
7.83
16
308
SS-01
3/16/2000
117
< 10
< 250
1,940
922
< 0.2
< 10
< 10
< 20
199
50,900
202,000
3,780
SS-01
9/15/2000
327
< 10
< 250
166
38
< 0.2
< 10
< 10
< 20
160
26,100
157,000
5,080
7.32
19
410
SS-01
3/23/2001
< 100
< 10
< 250
158
10
< 0.2
< 10
< 10
< 20
< 50
26,100
113,000
2,810
6.9
1 16
150
SS-01
10/4/2001
116
< 10
< 250
10
29
< 0.2
< 10
< 10
< 20
300
1 99,000
343,000
1 5,300
7.39
19
440
SS-01
3/28/2002
< 100
< 10
< 250
201
10
< 10
< 10
27
320
41,900
177,000
3,180
7.03
11
400
SS-01
10/3/2002
317
< 10
< 250
767
52
< 0.2
< 10
< 10
< 20
750
73,300
300,000
3,070
19
330
SS-01
3/25/20031
673
1 < 10
< 250
607
24
< 0.2
< 10
< 10
< 20
115
31,600
119,000
2,080
6.87
18
440
SS-01
10/2/2003
< 100
< 10
< 250
705
72
< 0.2
< 10
< 10
< 20
446
29,400
181,000
2,380
6.33
15
249
SS-01
4/28/2004
< 100
< 10
< 250
179
80
< 0.2
< 10
< 10
< 20
374
70,400
176,000
2,060
11.7
281
SS-01
10/26/2004
145
< 10
< 250
132
36
< 0.2
< 10
< 10
< 20
209
58,800
217,000
2,620
397
SS-01
4/27/2005
< 100
< 10
< 250
105
11
< 0.2
< 10
< 10
< 20
149
41,400
174,000
2,150
294
SS-01
10/20/2005
347
< 10
< 250
84
453
15
< 0.2
< 10
< 10
55
288
47,600
213,000
9,500
232
SS-01
10/19/2006
937
< 10
< 250
1,630
130
< 0.2
< 10
< 10
22
226
1 59,200
168,000
2,970
423
SS-01
4/27/2007
446
< 10
< 250
1,240
18
< 0.2
< 10
< 10P50.9
188
27,400
128,000
3,600
209
SS-01
11/19/2007
< 100
< 10
< 250
'0
104
11
< 0.2
< 10
< 10
117
61,500
243,000
3,540
371
SS-01
4/30/2008
170
< 10
< 250
'0
242
21
< 0.2
< 10
< 10
238
56,300
171,000
2,690
260
SS-01
10/29/2008
< 100
< 10
56.4
0.3
0
3
20.6
6
0.05
< 10
< 10
229
76,300
254,000
2,870
392
SS-01
4/30/2009
< 100
< 10
64.8
-10
< 10
77.8
SA
8.3
< 0.2
9.9
< 10
302
52,300
211,000
4,470
325
SS-01
8/26/2009
72
<1
<5
160
14
<20
45,000
8.1
22
1,490
10
94
9.05
SS-01
10/12/2009
89 J
2.7 J
63
< 0.08
0.8 J
1.1J
86
7.3 J
< 0.0084
< 2.4
< 0.12
370
49,000
240,000
7.83
13.1
2,380
8.9
160
12.7
SS-01
4/19/2010
190
< 10
64
< 5
240
12
< 0.2
< 20
< 5
400
33,000
190,000
4,900
8.12
11.97
557
63.1
199
10.68
SS-01
10/11/2010
52 J
1.1 J
71
1.6J
160
16J
< 0.2
< 5
640
40,000
240,000
7.8
16.54
455
8
107
12.77
SS-01
4/20/2011
62
< 1
66
5
280
13
< 0.1
< 1
1 300
30,000
140,000
3,400
7.59
17.98
270
4
211
9.71
SS-01
10/18/2011
153
< 5
76.7
5
190
9.6
< 0.2
< 10
250
1 39,200
210,000
5,700
7.54
16.94
289
8.3
236
9.56
SS-01
3/16/2012
170
< 5
82.5
5
238
11
< 0.2
< 10
= 0.2
1 37,400
221,000
4,800
7.8
15.73
359
2.46
-27
11.3
SS-01
9/24/2012
147
< 5
94.1
5
146
10.2
< 0.2
< 10
450
47,700
257,000
7.71
15.68
589
21.3
153
8.65
SS-01
4/17/2013
366
< 10
73.5
5
492
12.4
< 0.2
< 10
141
29,000
131,000
4,410
8.03
20.89
297
4.9
76.3
6.87
SS-01
9/9/2013
179
< 10
87.1
5
240
18.1
< 0.2
< 10
470
41,700
203,000
7,210
8.36
20.64
347
5.4
-173
9.4
SS-01
4l6/2014
< 100
62.2
5
137
60.6
< 10
70,000
224,000
4,100
7.93
9.59
381
5.1
142.2
11.65
SS-01
9l3/2014
122
82.6
s
264
< 5
64.7
< 10
93,400
339,000
7.99
21.12
396
8.01
47A
7.32
SS-01
4l1/2015
146
72.2
291
<5
58.6
<10
69,100
216,000
7.75
17.09
552
3.1
39.6
9.74
SS-01
9l9/2015
7,600
190
11
12 000
6.2 J
660
< 20
93,000
280,000 6
SS-01
3l8/2016
240
63
350
< 1
20
< 1
29,000
93,000
8.88
9.1
439.5
98.1
12.3
SS-01
9l7/2016
71
67
220
< 1
6.3
< 1
35,000
200,000
SS-01
9l7/2016
57
72
210
< 1
5.2
< 1
32,000
210,000
8.6
21.9
298
3.6
49
8.1
Page 1 of 8

APPENDIX A2
SURFACE WATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Anal e
E
-
m
0
E
0
0o
o
E
f
m
in
-
z
'z
m
M
aa
>
-6u
o
-
=
1j
E
E
N
c
m'
H
z
E
-
a
u
K
O
J
a
O
o.
'o
C 2B Surface Water
Standard
8,000
10
21,000
0.3
50.1
5.79
1,000
1.49
100
0.012
5
1.34
76.01
10,000
250,000
500,000
NE
6.0-9.0
NE
NE
50
NE
NE
Sample
Data
SS-01
3/27/2017
160
61
1,400
800
3.6 J
460,000
1,000,000E
L58
16.95
1.31
68
10.6
SS-01
5/8/2017
590 B
57
5
660
6.8
_ 5
23,000
150,000
SS-01
9/25/2017
130 B
84
5
250
8.6
5
40,000
240,000
8.03
20.21
322
3.33
61
8.23
SS-01
3/5/2018
55
69
5
140
9.2
5
38,000
190,000
8.06
11.11
289
3.2
186
10.28
SS-01
9/11/2018
150
84
5
470
22
5
36,000
1,200,0001
8.07
21.8
380
6.07
101
5.84
SS-01
3/18/2019
230
51
5
590
7.4
5
20,000
150,000
L72
11.7
211.8
9.98
212.9
13.45
SS-01
9/4/2019
250
77
5
380
11
7
32,000
200,000
8.11
19.6
292.7
12.4
-28.6
6.39
SS-01
2/17/20201
3,100
1
64
5
3,400
1.2
26
23,000
150,000
7.79
10.38
219
34.9
216
9.58
SS-01
2/24/2020
1,200
63
5
1,600
16
25,000
170,000
8.64
7.74
233
16.2
192
10.95
SS-01
4/l/2020
490
59
5
690
8.6
26,000
150,000
8.53
11.7
224.9
34.2
49.5
8.58
SS-01
9/23/2020
1,000
82
5
1,400
25
31,000
200,000
7.72
15.5
316.2
34.2
16.7
7.06
SS-01
4/6/2021
2,800
66
5
3,300
1.1
24
20,000
170,000
8.07
12.95
185
52
268
9.72
SS-01+150
2/17/2020
2,700
61
5
3400
1.2
24
21,000
150,000
7.84
10.42
208
33.1
232
9.76
SS-01+150
2/24/2020
1,500
67
5
1700
49
34,000
180,000
8.16
7.77
198
17.8
209
12.08
SS-01+550
2/17/2020
2,400
60
5
2,700
1
32
26,000
160,000
7.71
10.19
207
26.4
234
10.26
SS-01+550
2/24/2020
1,300
65
5
1400
33
33,000
170,000
8.32
7.9
256
13.2
205
10.26
SS-01+850
2/17/2020
2,500
59
5
2,700
36
29,000
160,000
7.69
10.01
221
25.2
243
9.42
SS-01+850
2/24/2020
1,100
66
5
1,300
27
33,000
180,000
8.18
7.94
249
13.9
207
12.28
SS-02
9/21/1990
130
94
4.6
100
<20
1,140
47,000
141,000
15,000
7.52
14.6
607
SS-02
10/23/1991
170
820
711
10
< 10
80
1,020
490 000
806,000
10,000
7.82
18
1,280
SS-02
3/26/1992
7,650
30
2.1
8070
12.9
130
1 10
<10
<20
250
13,100
149,000
12,000
6.04
11.5
111
SS-02
9/30/1992
330
'10
< 250
< 10
< 20
550
183,000
474,000
3,000
6.07
15.1
778
SS-02
3/31/19931
208
1 <10
< 250
675
327
'10
< 10
< 20
350
70,400
185,000
4,000
5.81
14.1
341
SS-02
9/17/1993
470
<10
<250
1,270
722
<10
<10
<20
2,300
154,000
523000
4,000
7.48
22.2
754
SS-02
3/30/1994
220
<10
<250
32
1,120
117
<10
<10
165
320
40,000
143,000
5.99
14.4
692
SS-02
9/30/1994
120
<10
< 250
28
470
356
< 10
< 10
24
325
135,000
397,000
37,900
7.39
18.6
573
SS-02
3/31/1995
165
<10
< 250
526
332
< 10
< 10
41
750
102,000
342,000
7.87
14.5
496
SS-02
9/29/1995
406
<10
< 250
1,020
6
598
< 10
< 10
< 20
1,030
155,000
505,000
2,680
5.6
13.5
1,095
SS-02
3/30/1996
426
<10
< 250
787
250
< 10
< 10
< 20
190
30,600
198,000
2,990
6.53
12
282
SS-02
9/27/1996
61
<10
< 250
227
10
262
< 10
< 10
47
750
147,000
409,000
3,190
7.59
20
613
SS-02
3/29/1997
209
<10
< 250
1
644
246
< 10
< 10
10
450
72,800
255,000
2,470
7.83
16
224
SS-02
9/17/1997
165
<10
<250
!0<
428
6
333
<5
<10
0 153
2,210
160,000
562000
2,430
7.8
18
826
SS-02
3/27/19981
220
1 <10
< 250
10
960
363
< 10
< 10
32
550
94,200
324,000
3,960
7.75
17.5
1 724
SS-02
9/30/1998
100
<10
<250
!0
595
351
<10
<10
<20
1,550
89,200
444,000
6,850
7.4
19
368
SS-02
3/31/1999
129
<10
<250
'n
947
587
<10
<10
<20
1,550
204,000
420,000
3,260
7.4
17
340
SS-02
9/29/1999
1,380
<10
<250
3030
147
<10
<10
21
160
45,700
173,000
8,100
7.62
17
623
SS-02
3/16/2000
< 100
<10
< 250
960
464
< 10
< 10
< 20
1,180
175,000
500,000
3,750
SS-02
9/15/2000
283
<10
<250
225
416
<10
<10
<20
1,240
170,000
439,000
6,580
7.44
20
640
SS-02
3/23/2001
108
<10
<250
260
7
135
<10
<10
34
103
71,900
224,000
3,080
6.6
16
170
SS-02
10/4/2001
166
<10
< 250
746
8
910
< 10
< 10
< 20
6,320
421,000
1,250,000
27,000
7.21
19
680
SS-02
3/28/2002
121
<10
< 250
502
1
206
< 10
< 10
< 20
320
127,000
405,000
2,970
7.39
11
510
SS-02
10/3/2002
220
<10
< 250
494
549
< 10
< 10
< 20
1,110
266,000
517,000
4,280
5.84
18
130
SS-02
3/25/2003
1,570
1 <10
<250
1280
6
264
<10
<10
24
162
90,300
234,000
1,910
6.03
18
1,260
SS-02 FD
3/25/2003
1,750
<10
< 250
1,320
265
< 10
< 10
24
194
94,600
235,000
2,000
6.03
18
1,260
SS-02
10/2/2003
< 100
<10
< 250
1,010
546
< 10
< 10
< 20
610
115,000
395,000
2,500
6.51
14
556
SS-02
4/28/2004
109
<10
I < 250
400
417
< 10
< 10
< 20
608
220,000
394,000
2,260
12.7
623
SS-02
10/26/2004
216
<10
< 250
839
582
< 10
< 10
< 20
2,000
276,000
554,000
3,060
807
SS-02
4/27/2005
< 100
<10
< 250
356
272
< 10
< 10
< 20
648
37,600
460,000
2,480
737
SS-02
10/20/2005
< 100
<10
< 250
10
72
1,120
330
< 10
< 10
48
546
240,000
571 000
3,400
419
SS-02
10/19/2006
530
< 10
< 250
20
1,060
534
< 10
< 10
32
299
204,000
422,000
3,490
550
SS-02
4/27/2007
389
< 10
< 250
< 20
< 20
811
488
< 10
< 10
< 20
333
439,000
1 303,000
1 4,420
511
SS-02
11/19/2007
< 100
< 10
< 250
< 2
< 20
< 20
136
308
< 10
< 10
23
258
1 300,000
1 647,000
1 3,540
908
Page 2 of 8

APPENDIX A2
SURFACE WATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Anal e
E
E
-
m
E
000o
E
?
n
o
o
m
E
u
f
`a
z
m
w
M
aa
>
o
o
o
-
O
a^
1j
°
E
N
c
u
H
z
-
E
-
a
u
K
a
J
a
O
°e
C 2B Surface Water
Standard
8,000
10
21,000
0.3
50.1
5.79
1,000
1.49
100
0.012
5
1.34
76.01
10,000
250,000
500,000
NE
6.0-9.0
NE
NE
50
NE
NE
Sample
Data
SS-02
4/30/2008
<10
<250
278
254
46
285
159,000
371,000
2,740
--
--
569
-
--
SS-02
10/29/2008
< 10
56.3
0.24
' ^
128
318
14.2
407
342,000
708,000
3,430
1,070
SS-02
4/30/2009
<10
60.8
89A
222
19.2
499
201,000
518000
3,390
821
SS-02
8/26/2009
-
-
71
--
110
220
--
20
-
-
-
310000
--
--
7.78
21.55
2,120
6.4
101
6.38
SS-02
10/12/2009
43 J
5.1 J
60
0.8 J
45 J
48
< 0.
150
320
210,000
510,000
7.8
13.29
3,360
8.7
123
12.95
SS-02
4/19/2010
<100
<1
64
260
260
'1.03
420
150,000
390,000
6,300
7.61
10.57
632
60.1
181
10.21
SS-02
10/11/2010
< 250
1.1 J
69
1.4 J
270
310
8.9
6.4 J
1,200
250,000
660,000
7.62
15.24
999
113
8.29
SS-02
4/20/2011
<40
63
270
150
4
630
120,000
360,000
3,000
7.55
18.62
602
4.2
241
9.7
SS-02
10/18/2011
< 100
74.9
5
181
266
< 10
470
202,000
582,000
7,300
7.36
17.63
536
4.6
248
9.7
SS-02
3/16/2012
< 100
71.8
5
171
65.8
'10
1,600
152,000
614,000
6,300
7.55
15.36
781
3.4
14.5
11.52
SS-02
9/25/2012
< 100
97.6
5
236
301
< 10
1,600
400,000
858,000
8.46
16.16
1,420
9.7
181
9.08
SS-02
4/17/2013
194
71A
5
242
110
<10
-
214
79,100
207,000
5,030
8.14
20.8
382
4.7
79.6
7.97
SS-02
9/10/2013
<100
83
5
135
102
<10
1,160
167,000
493,000
6,290
8.03
19.79
1 657
8.2
99.8
7.11
SS-02
4/6/2014
133
56A
5
194
21.2
< 10
87,000
277,000
5,000
8.88
445
7.52
138.1
12.13
SS-02
9/3/2014
< 100
83.7
68.6
11.1
< 10
158,000
526,000
8.14
733
2.45
61.3
5.09
SS-02
4/1/2015
<100
59
96.1
16.7
<10
92,200
297,000
8.13
508
1.81
9.6
8.13
SS-02
9/8/2015
260J
100
1.1 J
450
70
<20
160,000
460,000
SS-02
3/8/2016
150
65
260
36
1.7
61,000
180,000
8.41368.4
122229il
227.1
11.32
SS-02
9/7/2016
150
81
5
490
44
< 1
86,000
300,000
8.5
452
4.6
89
8.4
SS-02
3/27/2017
65
74
5
210
11
< 5
68,000
250,000 B
7.2
403
1.8
169
9.62
SS-02
9/25/2017
86 B
88
5
200
43
< 5
88,000
310,000
7.95
458
1.18
183.9
8.41
SS-02
3/5/2018
37 J
69
5
160
27
< 5
92,000
300,000
7.99
457
4.6
179
11.75
SS-02
9/11/2018
<40
83
5
250
52
<5
89,000
320,000
L86
533
4.8
110
5.12
SS-02
3/18/2019
150
47
5
530
23
< 5
34,999
170,000
6.89
10.7
249.7
7.68
175.3
12.34
SS-02
9/3/2019
150
80
5
240
30
< 5
60,000
250,000
7.43
22.6
375.8
8.62
-15.4
6.3
SS-02
2/17/20201
1,900
1
60
1
5
2,400
34
< 5
30,000
160,000
7.64
9.95
216
24.8
265
9.28
SS-02
2/24/2020
1,100
68
5
1,300
40
<5
42,000
190,000
7.99
8.12
294
21.4
208
11.96
SS-02
4/1/2020
450
47
5
580
18
<5
38,000
150,000
9.13
12.4
245.4
13.5
42.7
9.13
SS-02 FD
4/1/2020
400
46
600
18
<5
38,000
160,000
SS-02
9/23/2020
1,200
74
1,400
39
<5
49,000
230,000
L99
15.6
371.9
28.4
9
7.32
SS-02
4/6/2021
2,000
58
82
2,900
25
< 0.2
< 5
26,000
170,000
8.12
14.28
200
30.2
290
10.1
SS-10
8/11/2009
65
12,000
400
<20
11,000
7.13
20.63
1,890
42.9
40
3.38
SS-15
8/11/2009
52
5
900
35
<20
7,500
7.84
20.7
1,840
52.5
114
9.65
SS-20
8/11/2009
58
5
800
46
8,200
8.35
23.85
1,112
27.3
58
7.63
SS-20
4/21/2011
190
5
550
17
10.1
10
100
4,800
96,000
1,900
7.66
14.64
87
14.2
128
9.4
SS-20
9/24/2012
378
< 5
5
1 580
< 5
51.1
< 0.2
- n
< 0.02
3,600
89,000
7.3
15.55
146
10.3
159
8.55
SS-20
4/17/2013
788
< 10
5
1,050
< 5
19.8
< 0.2
< 20
5,590
55,000
2,760
7.53
19.76
283
7.2
158
8.7
SS-20
9/9/2013
456
< 10
5
1,170
< 5
48.4
< 0.2
< 10
274
3,610
78,000
2,280
7.37
21.69
97
9.7
24.2
8.37
SS-20
4/6/2014
126
p
5
269
6
< 10
5,200
68,000
1,900
8.05
9.56
212
14.4
134.7
10.32
SS-20
9/3/2014
818
5
2,450
71.4
< 10
3,600
97,000
7.35
20.59
100
20.9
-12.5
5.33
SS-20
4/1/2015
2,320
5
4840
99.1
<10
5,000
66,000
7.72
14.85
103
7.26
7.2
7.59
SS-20
9l9/2015
4,700
5.8 J
7 600170<
20
3,900
90,000 B
SS-20
3/8/2016
470<
0.1
< 5
450
8.9
< 1
4,300
65,000
7.91
12.1
73.5
113.9
8.72
SS-20
9/7/2016
310
1
'5
1,100
36
< 1
1,600
89,000
7.6
19.4
80
3.2
59
8.4
SS-20
3/27/2017
2,400
120
5
4,700
1.4
280
< 5
3,100
62,000 B
7.49
16.29
179
9.7
97.8
8.97
SS-20
9/25/2017
3,200 B
110
4.6 J
5,500
1.6
140
< 5
2,900
69,000
6.87
20.41
84
16.1
-22.3
6.04
SS-20
3/5/2018
120
57
5
420
23
<5
4,100
80,000
7.62
10.77
74
7
201
9.63
SS-20
9/11/2018
370
67
5
1600
85
<5
3,300
75,000
7.56
21.3
116.5
24.3
70
5.11
SS-20
3/18/2019
550
54
5
680
8.1
< 5
4,300
84,000
7.48
10.5
70.3
13.2
219.4
8.86
SS-20
9/3/2019
3,700
110
5
5300
2
130
<5
3,100
94,000
6.03
20.7
101.4
23.9
16.8
6.56
SS-20
2/17/2020
2,200
51
5
2,500
1
19
< 5
8,700
79,000
7.53
9,000
86
23
227
8.96
SS-20
2/24/2020
1,400
49
<5
1800
16
<5
8,800
86,000
8.56
7.1
97
15.8
190
9.83
SS-20
4/l/2020
1,800
47
<0.5
<5
1600
13
<5
9,300
76,000
6.59
11.8
88.1
23.4
73.1
9.41
Page 3 of 8

APPENDIX A2
SURFACE WATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Anal e
E.1
E
-
m
E
00
E
?
n
0o
o
o
m
E
u
f
E
`a
z
m
w
M
aa
>
o
o
o
-
O
a^
1j
°
E
E
N
c
u
m'
H
z
-
E
-
a
u
K
a
O
J
a
O
o.
'o
C 2B Surface Water
Standard
8,000
10
21,000
0.3
50.1
5.79
1,000
1.49
100
0.012
5
1.34
76.01
10,000
250,000
500,000
NE
6.0-9.0
NE
NE
50
NE
NE
Sample
Data
SS-20
9/23/2020
4,800
59
6000
2
88
8,000
120,000
6.88
15.7
128.9
85.6
1,280
7.3
SS-20
4/6/2021
2,300
45
5
2,600
< 1
42
4,300
90,000
8.04
17.09
53
37.7
264
7.67
SS-25
8/11/2009
60
5
590
< 5
53
28,000
8.35
22.07
1,830
32.1
75
7.57
SS-25
4/21/2011
150
50
5
<1
470
8.2
40
5,000
100,000
1,900
7.59
14.79
89
15.5
128
9.66
SS-25
9/24/2012
508
52.2
5
<5
1580
103
22
39,800
156,000
7.19
15.94
257
13.6
145
8.44
SS-25
4/17/2013
820
54.9
5
<5
1170
32.6
<20
5,810
62,000
2,940
L49
19.64
336
6.8
163
8.9
SS-25
9/9/2013
345
54.3
5
<5
809
23.8
60.9
3,650
82,000
2,590
7.39
20.34
134
5.9
23.7
8.26
SS-25
4/6/2014
310
51.1
5
555
< 5
13.8
5,500
75,000
2,000
7.12
9.64
83
11.9
86.6
10.42
SS-25
9/3/2014
2,000
83.3
5
3,880
< 5
79.3
3,400
100,000
7.41
21.37
92
32.1
-11.9
5.63
SS-25
4/1/2015
292
53A
5
649
<5
10.6
a
5,200
74,000
7.14
14.95
89
9.45
16.3
5.93
SS-25
9/9/2015
660
63
0
1,500
< 10
58
20
3,700
85,00013
SS-25
3/8/2016
1,700
92
5
2,500
1.8
90
1
4,700
83,000
8.29
12.8
72.9
63
11.8
SS-25
9/7/2016
1,400
77
5
3,200
< 1
81
1
1,700
86,000
8
19.7
64
2.9
43
8.2
SS-25
3/27/2017
390
62
590
< 1
9.4
-
3,100
73,000 B
7.55
16.72
121
7.4
101
8.02
SS-25
9/25/2017
780 B
56
1.6 J
1,200
0.29 J
27
-
2,500
74,000
7.13
19.99
88
11.5
15.3
6.9
SS-25
3/5/2018
210
47
400
15
-
4,200
1 78,000
7.77
1 11.44
78
13.5
191
8.84
SS-25
9/11/2018
270
53
1,100
32
-
2,600
88,000
7.19
1 21.4
122.7
18.3
82.8
5.04
SS-25
3/18/2019
610
51
5
700
5.5
-
4,400
69,000
7.84
1 10.3
70.3
14.4
226.5
1 8.44
SS-25
9/3/2019
1,700
70
5
2,700
45
-
3,200
100,000
6.2
21.2
99.8
60.12
8.9
6.02
SS-25
2/17/2020
2,800
55
5
3,600
1.5
25
-
8,500
81,000
7.5
9.62
79
33.5
251
8.82
SS-25
2/24/2020
1,300
46
5
1,500
9.8
-
8,700
93,000
8.42
7.3
86
24.9
199
10.2
SS-25
4/l/2020
1,700
48
5
1500
9.5
-
9,200
70,000
6.85
11.7
88.7
20.8
71
9.8
SS-25
9/23/2020
4,400
58
5
4900
1.8
60
-
8,300
110,000
6.81
15.6
125
91
1,157
7.46
SS-25
4/6/2021
2,600
48
5
2,800
26
-
8,000
90,000
8.58
12.62
78
59.2
199
9.6
SS-30
8/11/2009
72
5
150
25
20
95,000
8.53
22.82
5,250
21.7
57
8.1
SS-30
1/5/2011
77
5
330
<
130
10
63,000
370,000
8.63
3.9
388
6.9
132
10.43
SS-30
4/20/2011
<40
67
5
220
8.9
1
330
27,000
160,000
2,800
7.35
17.87
283
3.9
238
9.47
SS-30
9/24/2012
163
88
5
175
19.8
280
84,700
312,000
7.76
15.38
567
14.9
152
8.77
SS-30
4/17/2013
352
76A
5
455
13.2
194
31,000
144,000
18,200
7.82
21.06
268
8.7
62.1
6.24
SS-30
9/9/2013
158
86.2
5
237
18.6
498
45,600
220,000
4,990
8.06
20.44
318
4.59
17.9
7.13
SS-30
4/6/2014
< 100
61.6
5
159
33,200
170,000
4,000
L97
9.47
270
5.52
159.3
16.21
SS-30
9/3/2014
145
84.3
5
277
16A
10
43,600
253,000
8.41
21.41
308
11
16.6
6.96
SS-30
4/1/2015
173
67.1
5
291
11.2
10
43,200
191,000
L92
16.48
348
6.3
6.2
7.66
SS-30
9/9/2015
<400
86
0
110
5.8 J
20
98,000
280,000 6
SS-30
3/8/2016
870
67
5
1,000
32
1
31,000
150,000
8.49
9.3
275
164.2
12.04
SS-30
9/7/2016
470
70
5
970
44
1
48,000
270,000
8.5
21.6
357
2.8
48
8.5
SS-30
3/27/2017
160
70
5
370
10
-
41,000
200,0008
7.76
16.05
343
2.8
114
10.33
SS-30
9/25/2017
200 B
91
5
360
11
41,000
220,000
7.89
20.88
335
3.76
66.3
7.84
SS-30
3/5/2018
66
64
5
180
9.8
51,000
240,000
7.96
16.99
357
9.7
197
10.97
SS-30
9/11/2018
130
71
5
480
26
52,000
260,000
8.1
21.3
442
10.2
106
6.1
SS-30
3/18/2019
360
54
5
880
19
24,000
150,000
7.89
11.5
238.7
13
216.7
10.14
SS-30
9/4/2019
350
86
5
570
14
-
34,000
220,000
7.99
19.5
301.4
14.4
-28.6
6.39
SS-30
2/17/2020
3,200
64
5
3600
1.5
62
-
27,000
200,000
7.59
10.08
240
9.65
259
9.85
SS-30
2/24/2020
1,800
66
5
2 500
65
-
32,000
210,000
8.45
7.58
269
24.2
202
10.23
SS-30
4/l/2020
1,300
59
1800
18
-
31,000
160,000
7.36
11.8
261.9
24.1
63.3
10.12
SS-30
9/23/2020
3,800
81
4300
1.4
56
-
37,000
220,000
7.48
15.5
339.8
61.1
18.2
7.46
SS-30
4/6/2021
3,800
65
6.1
4100
1.4
32
-
25,000
200,000
8.09
12.89
217
64
2529.56
SS-35
9/8/2015
100
0
72 J
28
20
170,000
470,000
SS-40
8/26/2009
91
5
80
22
< 20
300 000
7.82
21.33
2,050
7.1
89
7.89
SS-40
4/20/2011
57
59
5
330
59
0.25
2.1
810
110,000
270,000
2,900
7.3
17.54
494
4.6
223
10.23
SS-40
9/25/2012
< 100
112
< 5
139
39
< 0.2
2,000
297 000
755 000
8
14.75
1,260
9.8
174
9.28
SS-40
4/17/2013
221
< 10
60.7
< 1
< 5
294
< 5
25.7
< 0.2
0
179
73,200
195,000
4,980
8.23
19.9
329
4.9
68.9
6.94
Page 4 of 8

APPENDIX A2
SURFACE WATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Anal e
E.1
-
m
0
E
0
0o
o
3
E
f
E
m
in
-
z
'z
m
M
aa
>
o
I I
o
-
I
1j
E
N
c
u
H
z
E
-
a
u
K
J
a
O
o.
C 2B Surface Water
Standard
8,000
10
21,000
0.3
50.1
5.79
1,000
1.49
100
0.012
5
1.34
76.01
10,000
250,000
500,000
NE
6.0-9.0
NE
NE
50
NE
NE
Sample
Data
SS-40
9/10/2013
89.6
92.5
15.5
20A
1,440
165,000
450,000
6,230
7.92
19.75
610
5.7
87.8
8.43
SS-40
4/6/2014
-
-
53.2
5
-
185
11.5
--
--
-
-
81,600
256,000
16,200
9.18
13.95
397
8.31
138.7
11.39
SS-40
9/3/2014
_.
86.5
5
58.1
9.5
152,000
473,000
8.06
23.72
689
2.45
69.4
4.91
SS-40
4/1/2015
< 100
58.5
5
154
10.8
84,200
264,000
8.01
18.32
469
4.19
13.5
8.25
SS-40
9/8/2015
210 J
110
0
370
48
160,000
440,000
SS-40
3/8/2016
220
62
5
310
12
57,000
180,000
8.41
8.9
332.7
238.2
13.44
SS-40
9/7/2016
540
94
5
1300
100
78,000
290,000
8.2
21
427
3.2
121
7.7
SS-40
3/27/2017
91
67
5
240
7.9
65,000
230,000 B
L98
16.88
357
1.8
154
111.1
SS-40
9/25/2017
100 B
85
5
210
17
80,000
280,000
8.07
19.85
425
3.24
121
8.57
SS-40
3/5/2018
45
64
5
130
5.8
84,000
290,000
8.19
9.79
417
2.6
190
11.82
SS-40
9/11/2018
<40
79
5
210
14
78,000
300,000
L73
22
498
5.03
99.5
4.91
SS-40
3/18/2019
160
47
5
480
9.3
-
32,000
150,000
7.44
10.4
230.8
7.92
175.8
12.25
SS-40
9/3/2019
75
77
5
190
10
-
51,000
230,000
7.04
1 21.9
1 336.2
4.27
-1.4
5.58
SS-40
2/17/2020
2,600
60
5
3,000
1
29
-
27,000
150,000
7.67
8.96
1 200
11.13
248
11.18
SS-40
2/24/2020
1,200
66
5
1,300
17
-
37,000
1 190,000
7.85
7.52
268
10.3
207
13.79
SS-40
4/l/2020
280
48
5
400
9
-
24,000
110,000
8.65
11.9
192.4
10.9
29.2
9.97
SS-40
9/23/2020
550
73
5
740
22
-
42,000
230,000
8.1
15.2
296.6
22.4
2.5
7.01
SS-40
4/6/20211
2,100
1
57
5
2,000
14
-
23,000
170,000
8.1
13.76
181
26.1
286
8.11
SS-50
8/11/2009
29
5
2,900
180
5,600
7.79
25.4
1,180
32
-21
8.52
SS-50
4/21/2011
120
< 1
36
5
< 1
1,100
85
0
130
3,700
71,000
2,000
6.91
14.66
85
16.3
92
9.88
SS-50
9/25/2012
410
<5
41.9
5
<=
1,640
110
10
140
- 2
72,000
8.65
17.58
161
9.6
16
8.76
SS-50
4/17/2013
-
-
-
-
-
-
--
--
--
--
-
--
-
-
-
SS-50
9/9/2013
-
-
-
--
-
-
-
--
--
--
-
-
-
-
-
SS-50
4/6/2014
_
_N46
--
--
--
--
-
-
-
-
SS-50
9/3/2014
-
-
--
-
-
-
--
-
--
-
-
-
-
-
SS-50
4/1/2015
886
4,620
168
10
2,900
63,000
7
13.5
90
18.8
-6.3
13.7
SS-50
9/9/2015
160000
1.6J
250
850,000
100
16,000
40
640J
75,000B
SS-50
3/8/2016
930
1,700
46
1
7.89
12.5
71.9
111.8
9.84
SS-50
9/7/2016
410
2,900
180
1
000
99,000
8
22.8
121
3.6
50
6.9
SS-50
3/27/2017
230
<0.5
<5
650
13
-
1,600
130,000
6.46
18.32
9
47.4
195
11.54
SS-50
9/25/2017
960 B
--2.1
J
2 200
0.56 J
93
-
1,300
23,000
6.86
20.27
84
14.7
13.2
7.71
SS-50
3/5/2018
86
--
5
-
530
22
--
-
-
-
-
2,900
68,000
--
7.38
11.41
74
14.8
213
11.87
SS-50
9/11/2018
SS-50
3/18/2019
240
40
740
< 1
25
3,700
72,000
7.45
9.7
73
11.8
145.8
8.69
SS-50
9/3/2019
1,400
54
3,000
< 1
93
1,400
78,000
5.22
22
104.2
24.8
6.8
6.85
SS-50
4/l/2020
660
47
2300
196
2,800
74,000
7.6
12.4
74.3
31.5
22.1
9.81
SS-50
9/23/2020
820
58
4400
1.1
180
5
1,200
71,000
7.25
15.1
68.3
28
1,470
8.03
SS-50
4/6/2021
1,700
47
14
2,200
35
5
3,700
69,000
7.63
15.84
63
47.4
290
9.42
SS-60
8/26/2009
-
--
140
5
--
280
15
980
--
20
-
--
-
350,000
--
--
7.06
20.34
4,040
65.9
10
6.69
SS-60
4/21/2011
68
61
5
240
< 1
11
4.1
120
130,000
270,000
2,700
7.15
15.9
446
14.3
177
8.89
SS-60
9/25/2012
120
75.9
1 5
312
<5
85
58,100
191,000
8.43
12.53
337
11.7
179
8.75
SS-60
4/17/2013
534
< 10
63A
5
667
< 5
43.8
164,000
274,000
4,170
7.8
20.15
380
1 8.6
70.6
10.79
SS-60
9/10/2013
103
< 10
120
5
116
< 5
75.5
2,120
275,000
1 663,000
6,150
L47
20.97
423
8.4
87.6
8.17
SS-60
4/6/2014
154
64.9
5
175
< 5
5.7
119,000
234,000
3,300
7.59
13.63
421
5.94
186.4
12.81
SS-60
9/4/2014
< 100
127
5
709
537
16.8
290,000
717,000
7.13
20.84
845
7.26
-3.4
4.53
SS-60
4/1/2015
1,320
93
5
2140
69.5
i0
159,000
359,000
7.07
9.72
538
18.8
1.56
6.6
SS-60
9/8/2015
190 J
57
0
410
33
20
13,000
110,000
SS-60
3/8/2016
510
68
5
410
8.6
3
120,000
270,000
7.83
9.3
375.2
252.1
10.62
SS-60
9/7/2016
780
130
5
2,400
160
1
250,000
490,000
7.5
20.1
666
4.7
39
6.5
SS-60
3/27/2017
4,500
160
5.5
7,800
2.7
190
1.5 J
190,000
410,000 B
7.08
14.69
4
297
194
7.03
SS-60
9/25/2017
34 BJ
130
5
260
89
5
270,000
570 000
7.31
18.92
763
1.16
54
3.31
SS-60
3/5/2018
140
93
280
19
5
170,000
370,000
7.13
L08
522
44.7
156
12.41
SS-60
9/11/2018
<40
120
810
330
5
2:4 000
620000
7.33
21.5
916
4.97
76.3
2.06
SS-60
3/18/2019
560
41
750
7.9
-
13,000
78,000
7.19
11.2
90.7
12.6
213
12.51
Page 5 of 8

APPENDIX A2
SURFACE WATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Anal e
E.1
E
-
m
E
0
E
?
0
n
coi
o
o
m
E
u
f
E
m
`a
in
-
z
m
'z
w
m
M
aa
>
o
o
o
-
O
a^
=
1j
°
E
E
N
c
u
m'
H
z
-
E
-
a
u
K
a
O
J
a
O
°e
'o
C 2B Surface Water
Standard
8,000
10
21,000
0.3
50.1
5.79
1,000
1.49
100
0.012
5
1.34
76.01
10,000
250,000
500,000
NE
6.0-9.0
NE
NE
50
NE
NE
Sample
Data
SS-60
4/l/2020
650
-
54
-
--
690
7.3
--
i
-
--
--
62,000
160,000
--
7.4
11.4
231.7
13.7
78.9
7.91
SS-60
9/23/2020
200
53
490
< 1
25
- 5
9,300
110,000
8.55
15.5
119.3
6.12
-8.8
6.86
SS-60
4/6/2021
1,500
53
1,200
< 1
7.8
- 5
37,000
140,000
7.84
13.04
153
7.5
294
8.09
SS-65
9/8/2015
780
80
1.3 J
1,300
'10
96
20
44,000
150,000
SS-70
8/26/2009
120
5
1100
<5
250
20
65,000
6.94
20.55
2,520
6.8
91
6.44
SS-70
4/21/20111
160
<
50
5
380
<1
5.8r0.1
<1
53
23,000
92,000
2,300
6.99
16.39
138
8.3
189
10.27
SS-70
9/25/2012
120
< 5
824
5
303
< 5
58.7
< 10
10
< 0.02
61,300
203,000
8.15
12.58
367
10.1
143
8.34
SS-70
4/17/2013
694
<10
51.3
5
986
< 5
13.4<
10
< 20
24,100
89,000
3,330
L98
19.28
129
7.3
60.9
7.67
SS-70
9/10/2013
135
<10
58.8
5
299
<5
13.610
1,390
28,600
123,000
3,510
L89
20.87
419
7.6
85.3
8.07
SS-70
4/6/2014
374
47.7
5
479
<5
5.310
21,000
86,000
2,300
7.5
13.28
125
8.3
165
9.85
SS-70
9/4/2014
<100
79.9
5
305
<5
71.110
35,000
146,000
7.7
21.04
217
3.68
22.3
7.26
SS-70
4/1/2015
147
55.1
5
282
<5
8.410
27,300
93,000
7.36
11.13
159
1.56
5.01
8.21
SS-70
9/8/2015
95 J
71
0
260
27
20
33,000
160,000
SS-70
3/8/2016
640
47
5
540
5.7
1
18,000
90,000
8.17
10
112.5
244.2
11.35
SS-70
9/7/2016
160
52
470
18
1
1,600
81,000
7.5
19.9
93
5.3
1 26
7.6
SS-70
3/27/2017
170
56
270
4.2J
-
21,000
93,000B
7.5
16.52
722
6.2
170
7.92
SS-70
9/25/2017
350 B
62
1.3 J
530
28
-
11,000
74,000
7.53
19.21
122
7.69
158.8
7.14
SS-70
3/5/2018
78
44
150
7.2
-
20,000
91,000
7.32
10.96
120
1.4
197
7.9
SS-70
9/11/2018
86
60
-
480
31
-
8,000
97,000
7.67
21.4
152
4.94
111
5.3
SS-70
3/18/2019
360
45
5
500
5.7
-
14,000
83,000
7.5
11
96
10.2
209.7
10.53
SS-70
9/3/2019
91
55
5
410
27
-
16,000
110,000
6.72
22
137.7
4.27
2.3
5.14
SS-70
4/1/2020
630
43
5
840
14
-
12,000
77,000
7.21
11.9
86.7
14.4
62.9
9.74
SS-70
9/23/2020
170
57
5
350
12
-
12,000
96,000
8.21
15.7
75.4
5.61
12.8
8.31
SS-70
4/6/20211
1,400
1
48
1
5
1300
8.3
-
9,500
89,000
7.87
13.58
76
6.3
290
7.95
SS-75
9/8/2015
--
78
0
--
230
26
--
9.9 J
--
--
-
41,000
170,000
--
-
-
-
-
-
-
--
120
5
--
250
25
--
--
--
-
82,000
--
--
7.13
20.63
5,190
5.8
100
8.34
SS-80
4/21/2011
110
56
5
310
99
27,000
120,000
2,100
6.8
15.52
161
6.8
92
10.61
SS-80
9/25/2012
192
87
5
263
15,9
<0.02
74,600
270,000
8.53
11.69
1 399
4.8
205
9.08
SS-80
4/17/2013
643
52.5
5
921
7.5
<20
27,600
88,000
3,170
7.43
20.14
139
7.6
70.8
7.14
SS-80
9/10/2013
110
< 10
71.5
5
211
8.3
10
265
47,600
152,000
3,430
7.67
21.64
417
6.9
87.9
7.92
SS-80
4/6/2014
180
53.7
5
328
3
17,500
84,000
2,400
7.39
13.87
106
8.7
136.2
11.78
SS-80
9/4/20141
149
1
81.1
5
436
16.8
10
30,100
155,000
8.09
21.23
245
11.3
17.5
6.98
SS-80
4/1/2015
246
58.1
5
382
7.1
25,500
89,000
7.88
12.8
162
4.37
4.37
9.57
SS-80
9/8/2015
<400
84
0
180
14J
41,000
170,000
SS-80
3/8/2016
640
54
5
530
6.4
24,000
110,000
8.45
8.8
124.3
236.8
11.32
SS-80
9/7/2016
140
63
5
430
9.7
13,000
110,000
7.7
21
98
2.7
53
8.2
SS-80
3/27/2017
100
62
5
200
2.5 J
21,000
110,000 B
7.97
1 16.04
156
1.7
165
8.96
SS-80
9/25/2017
98 B
71
5
250
6.8
21,000
110,000
7.68
18.95
158
2.97
146.5
8.89
SS-80
3/5/2018
74
51
5
190
10
21,000
96,000
7.57
10.92
127
0.9
185
15.18
SS-80
9/11/2018
490
73
5
1,200
34
-
16,000
110,000
8.19
21
191
5.55
109
5.72
SS-80
3/18/2019
400
45
5
560
-
13,000
90,000
7.64
9.9
96.8
9.89
196.2
9.74
SS-80
9/3/20191
240
1
67
1
5
500
9.9
-
13,000
130,000
6.65
21.7
142.6
6.32
8.1
5.64
SS-80
4/1/2020
510
50
5
680
5.8
-
10,000
76,000
L24
11.7
87.3
13.3
83.4
10.86
SS-80
9/23/2020
470
65
5
840
17
-
10,000
120,000
8.04
15.1
123.3
9.46
1 19.1
9.02
SS-80
4/6/2021
1,100
56
5
1,200
6.8
-
11,000
100,000
7.88
12.8
81
8.9
288
9.26
SS-90
1/4/2011
44
5
1,200
16
10
26,000
97,000
8.42
3
390
4.2
152
10.55
SS-90
1/4/2011
44
5
1,200
16
26,000
97,000
8.42
3
390
4.2
152
10.55
SS-90
4/20/2011
83
57
5
330
21
2.1
330
56,000
130,000
2,600
6.69
16.92
292
4.6
293
11.68
SS-90
9/25/2012
121
115
5
212
< 5
30.4
980
202,000
511 000
8.14
11.93
840
12.1
207
8.96
SS-90
4/17/2013
491
56
<5
7-<5
17.4
<5
34.9
38,900
127,000
3,690
7.94
19.71
203
6.9
66
7.59
SS-90
9/10/2013
148
< 10
86.6
< 1
<5
265
'5
32.4
10
< 5
< 10
642
121,000
283,000
4,920
7.86
11.19
429
7.9
91.6
7.26
Page 6 of 8

APPENDIX A2
SURFACE WATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Anal e
E.1
-
m
0
E
0
0o
o
3
E
f
E
m
in
-
z
2m
M
aa
>
-6u
o
-
=
1j
E
E
N
c
m'
H
z
E
-
a
u
K
O
J
a
O
o.
'o
C 2B Surface Water
Standard
8,000
10
21,000
0.3
50.1
5.79
1,000
1.49
100
0.012
5
1.34
76.01
10,000
250,000
500,000
NE
6.0-9.0
NE
NE
50
NE
NE
Sample
Data
SS-90
4/6/2014
154
48.5
274
9.4
-
0
45,300
151,000
3,300
8.87
15.09
255
5.62
120.9
15.44
SS-90
9/3/2014
< 100
90.8
77.5
16
10
94,500
357,000
7.48
23.51
518
5.56
65.3
6.43
SS-90
4/1/2015
125
58
189
9
10
51,400
166,000
8.81
11.35
318
5.95
5.95
9.92
SS-90
9/8/2015
290 J
100
1 1
530
80
20
110,000
340,000
SS-90
3/8/2016
390
58
470
11
1
33,000
110,000
8.35
8.5
210.3
239.3
13.08
SS-90
9/7/2016
40
73
230
17
1
49,000
200,000
8
20.8
2,886
1.8
48
9
SS-90
3/27/2017
160
62
5
340
12
-
40,000
100,000 B
8.2
16.52
256
1.9
152
11.09
SS-90
9/25/20171
72 B
1
79
5
160
10
48,000
200,000
7.88
19.1
284
1.47
153.2
8.7
SS-90
3/5/2018
51
54
5
120
5.8
48'000
170,000
L78
9.59
262
2.2
192
10.09
SS-90
9/11/2018
54
72
5
280
15
46,000
210,000
8.66
21.2
387
4.95
114
6.8
SS-90
3/18/2019
140
45
5
340
7.4
20,000
110,000
7.54
9.8
150.9
8.02
170.9
12.29
SS-90
9/3/2019
71
69
5
230
8.2
-
31,000
160,000
6.59
22.2
229.1
12.9
12.9
6.44
SS-90
2/17/2020
1,900
49
5
1,900
11
-
17,000
120,000
7.52
8.37
129
12.8
234
11.43
SS-90
2/24/2020
780
52
5
850
8.6
-
22,000
130,000
8.1
7.44
162
5.3
198
16.19
SS-90
4/l/2020
200
47
5
300
8.3
-
22,000
110,000
8.68
11.3
154.5
10.7
59.2
12.61
SS-90
9/23/2020
200
64
5
400
17
-
24,000
140,000
8.45
14.8
208.8
10.7
40.8
9.74
SS-90
4/6/20211
1,400
1
55
5
1500
12
-
14,000
110,000
8.04
12.21
118
12
271
9.71
SS-95
2/17/2020
360
62
5
660
330
-
94,000
270,000
7.34
9.51
378
8.2
165
8.55
SS-95
2/24/2020
140
fib
5
650
540
5.
160,000
390,000
8.08
7.51
599
18.5
200
10.12
M W-001
9/30/1994
2,580
16
< 250
44
23,200
6,490
< 10
< 1
1 35
2,950
787,000
2,230,000
258,000
7.39
22.5
3,140
MW-001
3/31/1995
660
<10
<250
5,150
2,360
<10
<10
155
8,880
794000
2540000
459,000
7.8
17.5
3,680
M W-001
9/29/1995
156
<10
< 250
5,240
8
4,880
< 10
< 10
< 20
1,030
801,000
2,660,000
4,950
5.41
14.8
4,220
MW-001
3/30/1996
112
<10
< 250
2
5,020
<
5,400
< 10
< 10
< 20
2,080
2,340,000
6,650
7.18
15
3,050
MW-001
9/27/1996
167
<10
<250
9
4530
<10
<10
66
1,700
1,010,000
2700,000
4,040
7.32
23
1,510
MW-001
3/17/1997
164
<10
<250
3,660
5400
<10
<10
55
608
1,160,000
3000,000
6,430
7.2
22
3,660
MW-001
3/29/1997
97
<10
<250
6,180
5460
<10
<10
10
1,290
1,050,000
2460,000
4,310
7.5
22
1,770
M W-001
3/27/1998
< 100
10
< 250
11,400
5,900
< 10
< 10
21
290
942,000
2,780,000
4,430
7.19
23.4
1,419
MW-001
9/30/1998
274
<10
<250
4,940
<10
<10
<20
666000
2700,000
15,400
7.6
20
1,200
MW-001
3/31/1999
<100
<10
<250
7,550
6
4,450
<10
<10
<20
600
1,560,000
2930,000
7,920
7.3
18
1,021
M W-001
9/29/1999
877
< 10
< 250
6,770
862
< 10
< 10
80
3,360
330,000
715,000
13,300
7.08
18
2,930
M W-001
3/16/2000
410
< 10
< 250
72,000
4,540
< 10
< 10
1,090
948,000
2,610,000
10,600
M W-001
9/15/2000
< 100
< 10
< 250
2,020
3,480
< 10
< 10
6,270
894,000
2,470,000
5,210
6.57
19
980
M W-001
3/23/2001
144
< 10
< 250
4
35,900
12
4,070
< 10
< 10
480
926,000
2,630,000
5,850
6.5
17
480
MW-001 FD
3/23/2001
< 100
< 10
< 250
!0
6,900
7
4,190
< 10
< 10
350
939 000
2,640,000
7,520
6.5
17
480
MW-001
10/4/2001
204
< 10
< 250
'0
915
7
< 10
< 10
186,000
7'800
6.28
20
300
M W-001
3/28/2002
< 100
< 10
< 250
IO
<27
5,100
< 10
< 10
< 20
280
1,000,002
3,010,000
3,770
6.44
12
1,080
MW-001
10/3/2002
< 100
< 10
< 250
2
1
1,520
< 10
< 10
< 20
1,820
1,030,000
2,940,000
4,940
6.67
18
370
MW-001 FD
10/3/2002
< 100
< 10
< 250
2
24
1,580
< 10
< 10
< 20
1,780
1,040,000
2,860,000
5,120
5.67
18
370
MW-001
3/25/2003
< 100
< 10
< 250
6,690
6
P3.560
< 10
< 10
25
406
846,000
2 530 000
3,720
6.62
17
330MW-001
10/2/2003
< 100
< 10
< 250
11 300
7
< 10
< 10
42
174
916,000
2 710,000
3,920
5.59
15
3,050
MW-001 FD
10/2/2003
< 100
< 10
< 250
11 400
6
< 10
< 10
< 20
< 5L
958,000
2 690,000
3,900
5.59
15
3,170
MW-001
4/28/2004
< 100
< 10
< 250
11 100
6
< 10
< 10
< 20
< 50
11460,0001
2,550,000
5,360
17.3
2,860
MW-001
10/26/2004
< 100
< 10
< 250
<
5,250
4,550
< 10
< 10
< 20
287
1,190,000
2,950,000
3,640
3,480
MW-001
4/27/2005
< 100
< 10
< 250
2
7,630
7
1 5,730
< 10
< 10
< 20
< 50
1,100,000
2,550,000
4,710
2,870
MW-001
10/20/2005
1,630
< 10
< 250
4
28
103,000
6
4,880
< 10
< 10
57
428
403,000
3,010,000
89,000
529
MW-001
10/19/2006
172
< 10
< 250
2
347
27,400
3,600
< 10
< 10
27
139
1,320,000
2,850,000
4,370
2,000
MW-001
4/27/2007
< 100
< 10
< 250
5,360
2,380
< 10
< 10
< 20
287
1,380,000
2,750,000
4,010
4,830
MW-001
11/19/2007
< 100
42
< 250
2
48,200
3,280
< 10
< 10
25
1,560,000
3,060,000
3,820
31300
MW-001
4/30/2008
< 100
<10
< 250
9,680
2,990
< 10
< 10
22
155
1,100,000
2,910,000
3,380
4,880
MW-001
10/29/2008
< 100
<10
68.7
4,840
3.5
2,880
< 10
< 10
< 10
188,000
3,060,000
3,510
4,200
MW-001
4/30/2009
< 100
<10
77.4
1.8
3.6
4,080
4.4
3,100
< 10
< 10
< 10
264
37,700
2,904,000
3,940
4,070
Page 7 of 8

APPENDIX A2
SURFACE WATER ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Anal e
E.1
-
m
0
E
0
0o
om'
E
z
M
aa
>
o
o
-
Ij
E
N
c
u
H
z
E
-
a
u
K
O
J
a
O
o.
'o
C 2B Surface Water
Standard
8,000
10
21,000
0.3
50.1
5.79
1,000
1.49
100
0.012
5
1.34
76.01
10,000
250,000
500,000
NE
6.0-9.0
NE
NE
50
NE
NE
Sample
Data
MW-003
9/30/1994
1,770
113
3,370
2,200
<10
<1.
96
200
159,000
415,000
20,100
6.89
19.6
519
MW-003
3/31/1995
4,860
5,980
<10
<10
32
100
294000
625000
7.56
13.6
896
MW-003
9/29/1995
1,640
=2
<2u
3,420
7
2,940
<10
<10
104
463
314000
740000
3,740
4.89
14
1,040
MW-003
3/30/1996
11400
'S0
<20
23300
9
3,160
<10
<10
126
130
222,000
552,000
3,830
7.18
12
750
MW-003
9/27/1996
110
-250
< 20
1,010
7
2,360
< 10
< 10
30
160
283 000
737,000
6,730
7.6
20
974
MW-003
3/29/1997
238
<10
<250
20
1930
3,050
1
<10
20
180
809000
807,000
4,170
7.76
16
590
MW-003
9/17/1997
169
<10
<250
'n
715
5
3,060
<10
212
330
562000
1,290,000
5,290
7.7
19
1,650
MW-003
3/27/19981
270
1 <10
<250
2,500
1 3,370
1
<10
41
250
929,000
6,980
7.2
1 20
1,214
MW-003
9/30/19981
353
1 <10
<250
1,380
1
<10
1
780
367000
1,280,000
10,100
6.9
19
920
M W-003
3/31/1999
= 100
< W
< 250
4,830
5,550
10
< 10
190
482,000
842,000
7,580
7.1
16
592
MW-003
9/29/1999
677
<10
<250
1,940
894
<10
<10
<20
100
258000
413,000
8,140
7.65
19
741
M W-003
9/15/2000
224
< 10
< 250
2,380
2,800
< 10
< 10
< 20
160
550,000
1 260 000
8,580
7.06
21
680
M W-003
3/23/2001
< 100
< 10
< 250
3,690
10
2,250
< 10
< 10
30
230
530,000
1 230 000
5,720
6.6
17
640
MW-003
10/4/2001
< 100
< 10
< 250
4,240
6
3,650
< 10
< 10
< 20
80
592 000
1 440,000
30,000
7
20
600
MW-003
3/28/2002
<100
<10
<250
5,620
2,180
<10
<10
<20
110
682000
1590,000
5,360
6.37
13
680
MW-003
10/3/2002
<100
<10
<250
2
6,510
5,290
<10
<10
<20
932000
1900,000
8,510
6.22
19
150
MW-003
3/25/2003
3,280
<10
<250
6170
8
4,290
<10
<10
8
88
784000
1520000
1,340
6.36
18
110
M W-003
10/2/20031
634
1 < 10
< 250
5,950
8
6,750
< 10
< 10
50
174
765,000
1,420,000
3,970
6.12
14
1,460
MW-003
4/28/2004
152
< 10
< 250
8,370
6,720
< 10
< 10
< 20
224
1,040,000
1,810,000
3,890
12.1
2,030
MW-003
10/26/2004
554
< 10
< 250
5
16,300
4,220
< 10
< 10
36
289
1,070,000
2140,000
5,160
2,150
MW-003
4/27/2005
< 100
< 10
< 250
2
4,470
6,110
< 10
< 10
< 20
246
1,075,000
2,090,000
4,050
2,320
MW-003
10/20/2005
< 100
< 10
< 250
5
27
7,900
5,870
< 10
< 10
44
279
1,300,000
2,090,000
30,000
1,060
MW-003
10/19/2006
<100
<10
1,460
6040
4,550
<10
<10
21
281
11170,0001
1920000
4,200
1,370
M W-003
4/27/2007
< 100
< 10
< 250
8,330
4,190
< 10
< 10
< 20
290
1,130,0001
2,130,0001
3,830
2,230
MW-003
11/19/2007
< 100
< 10
< 250
8 200
6,000
< 10
< 10
< 20
64
1,680,000
2 550 000
4,590
2,710
MW-003
4/30/2008
< 100
< 10
< 250
J
1
3,360
3,800
< 10
< 10
37
297
2,090,000
2110 000
3,560
2,290
MW-003
10/29/2008
< 100
< 10
59.3
10
2,880
2.3
4,360
< 10
< 10
< 10
171
988,000
2,360,0001
3,480
2,740
M W-003
4/30/2009
< 100
< 10
53.2
< 10
4,620
1 7.2
4,960
< 10
< 10
14.6
337
261,000
1 2,460,0001
4,110
2,930
Notes:
All concentrations in micrograms per liter (ug1L) unless otherwise noted
NE - Not established
-- - Not sampled
B - Detected in the method blank
J - Estimated result < LOQ and > DL
Bold with gray background indicates-eedance of NC Surface Water Standard
Analysis for arsenic, copper, mercury, silver, Arc, nitrates & TOC discontinued in 2014 per Corrective Action Plan (ERM, 212014).
NSA - Location inaccessible; no sample collected
NSB - Obstruction in well; no sample collected
NSC - Well dry; no sample collected
NSD - Insufficient volume; no sample collected
NSE - Well damaged; no sample collected
NSF - Pump broken; no sample collected
NSG - Surface water location dry; no sample collected
Page 8 of 8

APPENDIX A3
QA/QC ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
W
�
O
O
9
N
t6
U
d
>
U
E
N
Z
O
t6
E
m
E
a
a
c
L
E
E
E
y
?
y
m
o
0
E
N
3
E
O
O-
'o
rn
U
N
N
V
A
w
R
R
Analyte
3
Q
Q
m
.a
U
U
a
U
c
m
J
m
d
fA
N
c
N
Z
N
F
F
NC 2L
Groundwater
3.5
0.01
0.7
0.002
0.01
1
0.3
0.015
0.05
0.001
0.02
0.02
1
10
250
500
NE
Date
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Field Blank
9/30/1998
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 1
3/31 /1999
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.19
< 5
< 5
2.18
9/15/2000
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 1
3/23/2001
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
0.006
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
14
< 1
10/4/2001
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
0.006
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.3
< 5
15
< 2
3/28/2002
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.01
< 0.01
< 0.02
< 0.05
< 5
14
< 1
10/3/2002
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
6
< 1
3/25/2003
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.198
< 5
< 5
< 1
10/2/2003
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 1
4/28/2004
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
6
< 1
10/26/2004
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.151
< 5
10
2.18
4/27/2005
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
12
1.79
10/20/2005
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.101
< 5
< 5
< 0.5
10/19/2006
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 0.5
4/27/2007
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 0.5
11 /19/2007
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 0.5
4/30/2008
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.336
< 5
< 5
< 0.5
10/29/2008
< 0.1
< 0.01
0.0031
< 0.001
< 0.01
< 0.01
< 0.05
< 0.01
< 0.01
0.00002
< 0.01
0.0022
0.01
< 0.05
< 10
< 5
< 0.5
4/30/2009
< 0.1
< 0.01
0.0077
< 0.001
< 0.01
< 0.01
< 0.05
0.0045
0.008
< 0.0002
< 0.01
< 0.01
< 0.01
< 0.05
< 10
90
< 0.5
Page 1 of 2

APPENDIX A3
QA/QC ANALYTICAL RESULTS SUMMARY
EDWARDS ROAD LANDFILL - PERMIT 34-05
RURAL HALL, NORTH CAROLINA
Ul
�
O
O
9
N
R
m
U
U
E
EE
N
Z
O
R
E
R
a
c
L
E
E
y
3
d
m
o
0
E
N
3
E
O
a
6
U
N
N
V
i
w
R
5
Analyte
3
Q
Q
m
.a
U
U
a
U
c
m
J
m
r2
d
2
N
>
N
c
N
Z
y
H
F
NC 2L
Groundwater
3.5
0.01
0.7
0.002
0.01
1
0.3
0.015
0.05
0.001
0.02
0.02
1
10
250
500
NE
Date
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Trip Blank
9/30/1998
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 1
3/31 /1999
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.22
< 5
15
< 1
9/15/2000
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 1
3/23/2001
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
14
1.03
10/4/2001
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.4
< 5
12
2
3/28/2002
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.01
< 0.01
< 0.02
< 0.05
< 5
14
1.03
10/3/2002
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 0.5
3/25/2003
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
0.197
< 5
7
< 1
10/2/2003
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
7
< 1
4/28/2004
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
16
< 1
10/26/2004
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
8
1.29
4/27/2005
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
14
1.76
10/20/2005
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
6
< 0.5
10/19/2006
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 0.5
4/27/2007
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 0.5
11 /19/2007
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 0.5
4/30/2008
< 0.1
< 0.01
< 0.25
< 0.002
< 0.02
< 0.02
< 0.1
< 0.005
< 0.01
< 0.0002
< 0.01
< 0.01
< 0.02
< 0.05
< 5
< 5
< 0.5
10/29/2008
< 0.1
< 0.01
0.0046
< 0.001
< 0.01
< 0.01
< 0.05
< 0.01
< 0.01
0.00001
< 0.01
< 0.01
< 0.01
< 0.05
< 10
< 5
< 0.5
4/30/2009
< 0.1
< 0.01
0.0086
0.0003
< 0.01
< 0.01
< 0.05
< 0.01
0.0071
< 0.0002
< 0.01
< 0.01
< 0.01
< 0.05
< 10
85
< 0.5
9/8/2016
< 0.1
< 0.01
0.0086
0.0003
< 0.01
< 0.01
< 0.05
< 0.01
0.0071
< 0.0002
< 0.01
< 0.01
< 0.01
< 0.05
< 10
85
< 0.5
Notes:
All concentrations in milligrams per liter (mg/L) unless otherwise noted
NE - Not established
-- Not sampled
Bold with gray background indicates exceedance of NC Groundwater Standard
Analysis for arsenic, copper, mercury, silver, zinc, nitrates & TOC discontinued in 2014 per Corrective Action Plan (ERM, 2/2014).
Page 2 of 2

APPENDIX B LABORATORY DATA SHEETS
www.erm.com Version: 1.0 Project No.: 0588865 Client: R.J. Reynolds Tobacco Co. July 2021
2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

0
aceAnalytical
Report of Analysis
ERM NC, Inc.
300 West Summit Avenue
Suite 330
Charlotte, NC 28203
Attention: Alan Martin
Project Name: RJRT Rural Hall
Project Number: 0551517
Lot Number:WD07090
Date Completed:04/19/2021
Revision Date: 05/07/2021
05/07/2021 4:35 PM
Approved and released by:
Project Manager I: Hannah K. Lucas
PCCRFO
24r
ANSI National Accreditation Board
qe0
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 108

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
ERM NC, Inc.
Lot Number: WD07090
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
This report supersedes and replaces any prior reports issued under this lot number. Sample -010 metals
and mecury results were removed to match test requested on chain of custody.
TDS Analysis- Method SM 2540C
The analysis was initially preformed within holding time but was reanalyzed due to high residual mass.
The reanalysis confirms original results and therefore the first run will be reported.
Metals Analysis- Method 6020113/7470A
Samples WD07090-001 - 020 were improperly preserved in the field with H2SO4 instead of HNO3. The
preservative is compatible with the analysis requested.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 108

PACE ANALYTICAL SERVICES, LLC
Sample Summary
ERM NC, Inc.
Lot Number: WD07090
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
W-1-WG-20210405
Aqueous
04/05/20211350
04/07/2021
002
W-2-WG-20210405
Aqueous
04/05/20211405
04/07/2021
003
W-3-WG-20210405
Aqueous
04/05/20211205
04/07/2021
004
W-3B-WG-20210405
Aqueous
04/05/20211200
04/07/2021
005
W-6-WG-20210405
Aqueous
04/05/20211230
04/07/2021
006
W-7-WG-20210405
Aqueous
04/05/20211600
04/07/2021
007
W-8-WG-20210405
Aqueous
04/05/20211450
04/07/2021
008
W-9-WG-20210406
Aqueous
04/06/20210915
04/07/2021
009
PW-01-WG-20210405
Aqueous
04/05/20211330
04/07/2021
010
PZ-05-WG-20210406
Aqueous
04/06/20211130
04/07/2021
011
SS-25-WS-20210406
Aqueous
04/06/20211020
04/07/2021
012
SS-30-WS-20210406
Aqueous
04/06/20211030
04/07/2021
013
SS-01-WS-20210406
Aqueous
04/06/20211040
04/07/2021
014
SS-90-WS-20210406
Aqueous
04/06/20211100
04/07/2021
015
SS-80-WS-20210406
Aqueous
04/06/20211110
04/07/2021
016
SS-70-WS-20210406
Aqueous
04/06/20211120
04/07/2021
017
SS-60-WS-20210406
Aqueous
04/06/20211135
04/07/2021
018
SS-40-WS-20210406
Aqueous
04/06/20211145
04/07/2021
019
SS-20-WS-20210406
Aqueous
04/06/20211230
04/07/2021
020
SS-02-WS-20210406
Aqueous
04/06/20211200
04/07/2021
021
SS-50-WS-20210406
Aqueous
04/06/20211300
04/07/2021
(21 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 108

PACE ANALYTICAL SERVICES, LLC
Detection Summary
ERM NC, Inc.
Lot Number: WD07090
Sample
Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
W-1-WG-20210405
Aqueous
Sulfate
300.0
770
mg/L
16
001
W-1-WG-20210405
Aqueous
TDS
SM 2540C-
1600
H
mg/L
16
001
W-1-WG-20210405
Aqueous
Aluminum
6020B
400
S
ug/L
18
001
W-1-WG-20210405
Aqueous
Barium
6020B
31
ug/L
18
001
W-1-WG-20210405
Aqueous
Iron
6020B
1200
ug/L
18
001
W-1-WG-20210405
Aqueous
Manganese
6020B
3600
S
ug/L
18
001
W-1-WG-20210405
Aqueous
Selenium
6020B
17
S
ug/L
18
002
W-2-WG-20210405
Aqueous
Sulfate
300.0
14
mg/L
19
002
W-2-WG-20210405
Aqueous
TDS
SM 2540C-
75
mg/L
19
002
W-2-WG-20210405
Aqueous
Aluminum
6020B
120
ug/L
21
002
W-2-WG-20210405
Aqueous
Barium
6020B
120
ug/L
21
002
W-2-WG-20210405
Aqueous
Iron
6020B
92
ug/L
21
002
W-2-WG-20210405
Aqueous
Manganese
6020B
83
ug/L
21
003
W-3-WG-20210405
Aqueous
Sulfate
300.0
110
mg/L
22
003
W-3-WG-20210405
Aqueous
TDS
SM 2540C-
360
mg/L
22
003
W-3-WG-20210405
Aqueous
Barium
6020B
28
ug/L
24
003
W-3-WG-20210405
Aqueous
Iron
6020B
55
ug/L
24
003
W-3-WG-20210405
Aqueous
Manganese
6020B
32
ug/L
24
003
W-3-WG-20210405
Aqueous
Selenium
6020B
6.7
ug/L
24
004
W-3B-WG-20210405
Aqueous
Sulfate
300.0
16
mg/L
25
004
W-3B-WG-20210405
Aqueous
TDS
SM 2540C-
250
mg/L
25
004
W-3B-WG-20210405
Aqueous
Barium
6020B
56
ug/L
27
004
W-3B-WG-20210405
Aqueous
Iron
6020B
130
ug/L
27
004
W-3B-WG-20210405
Aqueous
Manganese
6020B
72
ug/L
27
005
W-6-WG-20210405
Aqueous
Sulfate
300.0
9.0
S
mg/L
28
005
W-6-WG-20210405
Aqueous
TDS
SM 2540C-
270
mg/L
28
005
W-6-WG-20210405
Aqueous
Aluminum
6020B
240
ug/L
30
005
W-6-WG-20210405
Aqueous
Barium
6020B
51
ug/L
30
005
W-6-WG-20210405
Aqueous
Chromium
6020B
18
ug/L
30
005
W-6-WG-20210405
Aqueous
Iron
6020B
490
ug/L
30
005
W-6-WG-20210405
Aqueous
Manganese
6020B
8.4
ug/L
30
006
W-7-WG-20210405
Aqueous
Sulfate
300.0
11
mg/L
31
006
W-7-WG-20210405
Aqueous
TDS
SM 2540C-
140
mg/L
31
006
W-7-WG-20210405
Aqueous
Aluminum
6020B
1900
ug/L
33
006
W-7-WG-20210405
Aqueous
Barium
6020B
100
ug/L
33
006
W-7-WG-20210405
Aqueous
Chromium
6020B
22
ug/L
33
006
W-7-WG-20210405
Aqueous
Iron
6020B
5300
ug/L
33
006
W-7-WG-20210405
Aqueous
Manganese
6020B
99
ug/L
33
007
W-8-WG-20210405
Aqueous
Sulfate
300.0
16
mg/L
34
007
W-8-WG-20210405
Aqueous
TDS
SM 2540C-
150
mg/L
34
007
W-8-WG-20210405
Aqueous
Aluminum
6020B
2000
ug/L
36
007
W-8-WG-20210405
Aqueous
Barium
6020B
210
ug/L
36
007
W-8-WG-20210405
Aqueous
Chromium
6020B
75
ug/L
36
007
W-8-WG-20210405
Aqueous
Iron
6020B
2600
ug/L
36
007
W-8-WG-20210405
Aqueous
Manganese
6020B
43
ug/L
36
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 108

Detection Summary (Continued)
Lot Number: WD07090
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
007
W-8-WG-20210405
Aqueous
Selenium
6020B
16
ug/L
36
008
W-9-WG-20210406
Aqueous
Sulfate
300.0
11
mg/L
37
008
W-9-WG-20210406
Aqueous
TDS
SM 2540C-
260
mg/L
37
008
W-9-WG-20210406
Aqueous
Aluminum
6020B
120
ug/L
39
008
W-9-WG-20210406
Aqueous
Barium
6020B
120
ug/L
39
008
W-9-WG-20210406
Aqueous
Chromium
6020B
7.0
ug/L
39
008
W-9-WG-20210406
Aqueous
Iron
6020B
200
ug/L
39
009
PW-01-WG-20210405
Aqueous
Sulfate
300.0
620
mg/L
40
009
PW-01-WG-20210405
Aqueous
TDS
SM 2540C-
1500
mg/L
40
009
PW-01-WG-20210405
Aqueous
Aluminum
6020B
620
ug/L
42
009
PW-01-WG-20210405
Aqueous
Barium
6020B
47
ug/L
42
009
PW-01-WG-20210405
Aqueous
Chromium
6020B
7.9
ug/L
42
009
PW-01-WG-20210405
Aqueous
Iron
6020B
8900
ug/L
42
009
PW-01-WG-20210405
Aqueous
Lead
6020B
2.2
ug/L
42
009
PW-01-WG-20210405
Aqueous
Manganese
6020B
2500
ug/L
42
009
PW-01-WG-20210405
Aqueous
Selenium
6020B
15
ug/L
42
010
PZ-05-WG-20210406
Aqueous
Sulfate
300.0
19
mg/L
43
010
PZ-05-WG-20210406
Aqueous
TDS
SM 2540C-
110
mg/L
43
011
SS-25-WS-20210406
Aqueous
Sulfate
300.0
8.0
mg/L
44
011
SS-25-WS-20210406
Aqueous
TDS
SM 2540C-
90
mg/L
44
011
SS-25-WS-20210406
Aqueous
Aluminum
6020B
2600
ug/L
46
011
SS-25-WS-20210406
Aqueous
Barium
6020B
48
ug/L
46
011
SS-25-WS-20210406
Aqueous
Iron
6020B
2800
ug/L
46
011
SS-25-WS-20210406
Aqueous
Manganese
6020B
26
ug/L
46
012
SS-30-WS-20210406
Aqueous
Sulfate
300.0
25
mg/L
47
012
SS-30-WS-20210406
Aqueous
TDS
SM 2540C-
200
mg/L
47
012
SS-30-WS-20210406
Aqueous
Aluminum
6020B
3800
ug/L
49
012
SS-30-WS-20210406
Aqueous
Barium
6020B
65
ug/L
49
012
SS-30-WS-20210406
Aqueous
Chromium
6020B
6.1
ug/L
49
012
SS-30-WS-20210406
Aqueous
Iron
6020B
4100
ug/L
49
012
SS-30-WS-20210406
Aqueous
Lead
6020B
1.4
ug/L
49
012
SS-30-WS-20210406
Aqueous
Manganese
6020B
32
ug/L
49
013
SS-01-WS-20210406
Aqueous
Sulfate
300.0
20
mg/L
50
013
SS-01-WS-20210406
Aqueous
TDS
SM 2540C-
170
mg/L
50
013
SS-01-WS-20210406
Aqueous
Aluminum
6020B
2800
ug/L
52
013
SS-01-WS-20210406
Aqueous
Barium
6020B
66
ug/L
52
013
SS-01-WS-20210406
Aqueous
Iron
6020B
3300
ug/L
52
013
SS-01-WS-20210406
Aqueous
Lead
6020B
1.1
ug/L
52
013
SS-01-WS-20210406
Aqueous
Manganese
6020B
24
ug/L
52
014
SS-90-WS-20210406
Aqueous
Sulfate
300.0
14
mg/L
53
014
SS-90-WS-20210406
Aqueous
TDS
SM 2540C-
110
mg/L
53
014
SS-90-WS-20210406
Aqueous
Aluminum
6020B
1400
ug/L
55
014
SS-90-WS-20210406
Aqueous
Barium
6020B
55
ug/L
55
014
SS-90-WS-20210406
Aqueous
Iron
6020B
1500
ug/L
55
014
SS-90-WS-20210406
Aqueous
Manganese
6020B
12
ug/L
55
015
SS-80-WS-20210406
Aqueous
Sulfate
300.0
11
mg/L
56
015
SS-80-WS-20210406
Aqueous
TDS
SM 2540C-
100
mg/L
56
015
SS-80-WS-20210406
Aqueous
Aluminum
6020B
1100
ug/L
58
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 108

Detection Summary (Continued)
Lot Number: WD07090
Sample Sample ID Matrix Parameter Method Result Q Units Page
015
SS-80-WS-20210406
Aqueous
Barium
6020B
56
ug/L
58
015
SS-80-WS-20210406
Aqueous
Iron
6020B
1200
ug/L
58
015
SS-80-WS-20210406
Aqueous
Manganese
6020B
6.8
ug/L
58
016
SS-70-WS-20210406
Aqueous
Sulfate
300.0
9.5
mg/L
59
016
SS-70-WS-20210406
Aqueous
TDS
SM 2540C-
89
mg/L
59
016
SS-70-WS-20210406
Aqueous
Aluminum
6020B
1400
ug/L
61
016
SS-70-WS-20210406
Aqueous
Barium
6020B
48
ug/L
61
016
SS-70-WS-20210406
Aqueous
Iron
6020B
1300
ug/L
61
016
SS-70-WS-20210406
Aqueous
Manganese
6020B
8.3
ug/L
61
017
SS-60-WS-20210406
Aqueous
Sulfate
300.0
37
mg/L
62
017
SS-60-WS-20210406
Aqueous
TDS
SM 2540C-
140
mg/L
62
017
SS-60-WS-20210406
Aqueous
Aluminum
6020B
1500
ug/L
64
017
SS-60-WS-20210406
Aqueous
Barium
6020B
53
ug/L
64
017
SS-60-WS-20210406
Aqueous
Iron
6020B
1200
ug/L
64
017
SS-60-WS-20210406
Aqueous
Manganese
6020B
7.8
ug/L
64
018
SS-40-WS-20210406
Aqueous
Sulfate
300.0
23
mg/L
65
018
SS-40-WS-20210406
Aqueous
TDS
SM 2540C-
170
mg/L
65
018
SS-40-WS-20210406
Aqueous
Aluminum
6020B
2100
ug/L
67
018
SS-40-WS-20210406
Aqueous
Barium
6020B
57
ug/L
67
018
SS-40-WS-20210406
Aqueous
Iron
6020B
2000
ug/L
67
018
SS-40-WS-20210406
Aqueous
Manganese
6020B
14
ug/L
67
019
SS-20-WS-20210406
Aqueous
Sulfate
300.0
4.3
mg/L
68
019
SS-20-WS-20210406
Aqueous
TDS
SM 2540C-
90
mg/L
68
019
SS-20-WS-20210406
Aqueous
Aluminum
6020B
2300
ug/L
70
019
SS-20-WS-20210406
Aqueous
Barium
6020B
45
ug/L
70
019
SS-20-WS-20210406
Aqueous
Iron
6020B
2600
ug/L
70
019
SS-20-WS-20210406
Aqueous
Manganese
6020B
42
ug/L
70
020
SS-02-WS-20210406
Aqueous
Sulfate
300.0
26
mg/L
71
020
SS-02-WS-20210406
Aqueous
TDS
SM 2540C-
170
mg/L
71
020
SS-02-WS-20210406
Aqueous
Aluminum
6020B
2000
ug/L
73
020
SS-02-WS-20210406
Aqueous
Barium
6020B
58
ug/L
73
020
SS-02-WS-20210406
Aqueous
Chromium
6020B
82
ug/L
73
020
SS-02-WS-20210406
Aqueous
Iron
6020B
2900
ug/L
73
020
SS-02-WS-20210406
Aqueous
Manganese
6020B
25
ug/L
73
021
SS-50-WS-20210406
Aqueous
Sulfate
300.0
3.7
mg/L
74
021
SS-50-WS-20210406
Aqueous
TDS
SM 2540C-
69
mg/L
74
021
SS-50-WS-20210406
Aqueous
Aluminum
6020B
1700
ug/L
76
021
SS-50-WS-20210406
Aqueous
Barium
6020B
47
ug/L
76
021
SS-50-WS-20210406
Aqueous
Chromium
6020B
14
ug/L
76
021
SS-50-WS-20210406
Aqueous
Iron
6020B
2200
ug/L
76
021
SS-50-WS-20210406
Aqueous
Manganese
6020B
35
ug/L
76
(134 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-001
Description: W-1-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1350
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
2
(Sulfate) 300.0
50 04/12/2021 1538 AMR
88845
2
(TDS) SM 2540C-2011
1 04/14/2021 0020 MOM
88929
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
770
50 mg/L 2
TDS
SM 2540C-2011
1600 H
25 mg/L 2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 7 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-001
Description: W-1-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1350
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1744 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 8 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-001
Description: W-1-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1350
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1725 BPK
04/09/2021 0402 88352
2
3005A
6020B
10
04/09/2021 2241 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
400 S
40
ug/L
1
Barium
7440-39-3
6020B
31
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
1200
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
3600 S
50
ug/L
2
Selenium
7782-49-2
6020B
17 S
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 9 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-002
Description: W-2-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1405
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 1652 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
14
1.0 mg/L 1
TDS
SM 254OC-2011
75
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 10 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-002
Description: W-2-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1405
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1747 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 11 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-002
Description: W-2-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1405
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 04/09/2021 1756 BPK 04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
120
40
ug/L
1
Barium
7440-39-3
6020B
120
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
92
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
83
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 12 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-003
Description: W-3-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1205
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 1709 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
110
1.0 mg/L 1
TDS
SM 254OC-2011
360
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 13 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-003
Description: W-3-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1205
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1750 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 14 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-003
Description: W-3-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1205
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 04/09/2021 1802 BPK 04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
ND
40
ug/L
1
Barium
7440-39-3
6020B
28
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
55
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
32
5.0
ug/L
1
Selenium
7782-49-2
6020B
6.7
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 15 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-004
Description: W-3B-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1200
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 1726 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
16
1.0 mg/L 1
TDS
SM 254OC-2011
250
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 16 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-004
Description: W-3B-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1200
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1752 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 17 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-004
Description: W-3B-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1200
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 04/09/2021 1809 BPK 04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
ND
40
ug/L
1
Barium
7440-39-3
6020B
56
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
130
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
72
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 18 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-005
Description: W-6-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1230
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 1743 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
9.0 S
1.0 mg/L 1
TDS
SM 254OC-2011
270
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 19 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-005
Description: W-6-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1230
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1800 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 20 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-005
Description: W-6-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1230
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1827 BPK
04/09/2021 0402 88352
2
3005A
6020B
5
04/13/2021 2121 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
240
200
ug/L
2
Barium
7440-39-3
6020B
51
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
18
5.0
ug/L
1
Iron
7439-89-6
6020B
490
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
8.4
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 21 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-006
Description: W-7-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1600
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 1908 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
11
1.0 mg/L 1
TDS
SM 254OC-2011
140
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 22 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-006
Description: W-7-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1600
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1808 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 23 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-006
Description: W-7-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1600
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1833 BPK
04/09/2021 0402 88352
2
3005A
6020B
10
04/13/2021 1457 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
1900
400
ug/L
2
Barium
7440-39-3
6020B
100
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
22
5.0
ug/L
1
Iron
7439-89-6
6020B
5300
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
99
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 24 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-007
Description: W-8-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1450
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 1924 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
16
1.0 mg/L 1
TDS
SM 254OC-2011
150
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 25 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-007
Description: W-8-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1450
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1811 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 26 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-007
Description: W-8-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1450
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1839 BPK
04/09/2021 0402 88352
2
3005A
6020B
10
04/13/2021 1512 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
2000
400
ug/L
2
Barium
7440-39-3
6020B
210
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
75
5.0
ug/L
1
Iron
7439-89-6
6020B
2600
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
43
5.0
ug/L
1
Selenium
7782-49-2
6020B
16
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 27 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-008
Description: W-9-WG-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 0915
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 1941 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
11
1.0 mg/L 1
TDS
SM 254OC-2011
260
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 28 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-008
Description: W-9-WG-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 0915
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1814 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 29 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-008
Description: W-9-WG-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 0915
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1 04/09/2021 1852 BPK
04/09/2021 0402 88352
2
3005A
6020B
1 04/13/2021 1531 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
120
40
ug/L
2
Barium
7440-39-3
6020B
120
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
7.0
5.0
ug/L
1
Iron
7439-89-6
6020B
200
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
ND
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 30 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-009
Description: PW-01-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1330
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
5 04/08/2021 1958 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
620
5.0 mg/L 1
TDS
SM 254OC-2011
1500
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 31 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-009
Description: PW-01-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1330
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1816 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 32 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-009
Description: PW-01-WG-20210405 Matrix: Aqueous
Date Sampled:04/05/2021 1330
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1858 BPK
04/09/2021 0402 88352
2
3005A
6020B
10
04/13/2021 1538 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
620
400
ug/L
2
Barium
7440-39-3
6020B
47
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
7.9
5.0
ug/L
1
Iron
7439-89-6
6020B
8900
50
ug/L
1
Lead
7439-92-1
6020B
2.2
1.0
ug/L
1
Manganese
7439-96-5
6020B
2500
50
ug/L
2
Selenium
7782-49-2
6020B
15
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 33 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-010
Description: PZ-05-WG-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1130
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2015 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
19
1.0 mg/L 1
TDS
SM 254OC-2011
110
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 34 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-011
Description: SS-25-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1020
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2032 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
8.0
1.0 mg/L 1
TDS
SM 254OC-2011
90
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 35 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-011
Description: SS-25-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1020
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1822 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 36 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-011
Description: SS-25-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1020
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1910 BPK
04/09/2021 0402 88352
2
3005A
6020B
50
04/13/2021 1553 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
2600
2000
ug/L
2
Barium
7440-39-3
6020B
48
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
2800
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
26
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 37 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-012
Description: SS-30-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1030
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2049 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
25
1.0 mg/L 1
TDS
SM 254OC-2011
200
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 38 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-012
Description: SS-30-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1030
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1824 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 39 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-012
Description: SS-30-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1030
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1917 BPK
04/09/2021 0402 88352
3
3005A
6020B
50
04/14/2021 1337 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
3800
2000
ug/L
3
Barium
7440-39-3
6020B
65
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
6.1
5.0
ug/L
1
Iron
7439-89-6
6020B
4100
50
ug/L
1
Lead
7439-92-1
6020B
1.4
1.0
ug/L
1
Manganese
7439-96-5
6020B
32
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 40 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-013
Description: SS-01-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1040
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2106 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 0034 SJL
88315
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
20
1.0 mg/L 1
TDS
SM 254OC-2011
170
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 41 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-013
Description: SS-01-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1040
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/09/2021 1827 CMS2 04/09/2021 1255 88500
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 42 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-013
Description: SS-01-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1040
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1923 BPK
04/09/2021 0402 88352
2
3005A
6020B
50
04/13/2021 1623 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
2800
2000
ug/L
2
Barium
7440-39-3
6020B
66
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
3300
50
ug/L
1
Lead
7439-92-1
6020B
1.1
1.0
ug/L
1
Manganese
7439-96-5
6020B
24
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 43 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-014
Description: SS-90-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1100
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2157 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
14
1.0 mg/L 1
TDS
SM 254OC-2011
110
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 44 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-014
Description: SS-90-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1100
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/14/2021 1717 CMS2 04/13/2021 1206 88501
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 45 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-014
Description: SS-90-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1100
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1929 BPK
04/09/2021 0402 88352
2
3005A
6020B
10
04/13/2021 1630 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
1400
400
ug/L
2
Barium
7440-39-3
6020B
55
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
1500
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
12
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 46 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-015
Description: SS-80-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1110
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2247 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
11
1.0 mg/L 1
TDS
SM 254OC-2011
100
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 47 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-015
Description: SS-80-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1110
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/14/2021 1720 CMS2 04/13/2021 1206 88501
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 48 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-015
Description: SS-80-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1110
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1948 BPK
04/09/2021 0402 88352
2
3005A
6020B
10
04/13/2021 1638 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
1100
400
ug/L
2
Barium
7440-39-3
6020B
56
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
1200
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
6.8
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 49 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-016
Description: SS-70-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1120
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2304 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
9.5
1.0 mg/L 1
TDS
SM 254OC-2011
89
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 50 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-016
Description: SS-70-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1120
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/14/2021 1723 CMS2 04/13/2021 1206 88501
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 51 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-016
Description: SS-70-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1120
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 1954 BPK
04/09/2021 0402 88352
2
3005A
6020B
10
04/13/2021 1645 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
1400
400
ug/L
2
Barium
7440-39-3
6020B
48
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
1300
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
8.3
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 52 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-017
Description: SS-60-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1135
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2321 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
37
1.0 mg/L 1
TDS
SM 254OC-2011
140
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 53 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-017
Description: SS-60-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1135
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/14/2021 1725 CMS2 04/13/2021 1206 88501
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 54 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-017
Description: SS-60-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1135
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 2000 BPK
04/09/2021 0402 88352
2
3005A
6020B
10
04/13/2021 1653 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
1500
400
ug/L
2
Barium
7440-39-3
6020B
53
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
1200
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
7.8
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 55 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-018
Description: SS-40-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1145
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2338 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
23
1.0 mg/L 1
TDS
SM 254OC-2011
170
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 56 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-018
Description: SS-40-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1145
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/14/2021 1728 CMS2 04/13/2021 1206 88501
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 57 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-018
Description: SS-40-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1145
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 2006 BPK
04/09/2021 0402 88352
3
3005A
6020B
10
04/14/2021 1345 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
2100
400
ug/L
3
Barium
7440-39-3
6020B
57
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
2000
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
14
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 58 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-019
Description: SS-20-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1230
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/08/2021 2355 AMR
88524
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
4.3
1.0 mg/L 1
TDS
SM 254OC-2011
90
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 59 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-019
Description: SS-20-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1230
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/14/2021 1741 CMS2 04/13/2021 1206 88501
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 60 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-019
Description: SS-20-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1230
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 2012 BPK
04/09/2021 0402 88352
2
3005A
6020B
50
04/13/2021 1708 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
2300
2000
ug/L
2
Barium
7440-39-3
6020B
45
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
ND
5.0
ug/L
1
Iron
7439-89-6
6020B
2600
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
42
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 61 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-020
Description: SS-02-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1200
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/09/2021 1633 AMR
88729
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
26
1.0 mg/L 1
TDS
SM 254OC-2011
170
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 62 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-020
Description: SS-02-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1200
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/14/2021 1744 CMS2 04/13/2021 1206 88501
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 63 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-020
Description: SS-02-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1200
Date Received:04/07/2021
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
04/09/2021 2018 BPK
04/09/2021 0402 88352
3
3005A
6020B
10
04/14/2021 1352 BPK
04/09/2021 0402 88352
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
2000
400
ug/L
3
Barium
7440-39-3
6020B
58
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
82
5.0
ug/L
1
Iron
7439-89-6
6020B
2900
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
25
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 64 of 108

Inorganic non-metals
Client:ERM NC, Inc. Laboratory ID:WD07090-021
Description: SS-50-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1300
Date Received:04/07/2021
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Sulfate) 300.0
1 04/09/2021 1650 AMR
88729
1
(TDS) SM 2540C-2011
1 04/08/2021 2130 SJL
88457
CAS Analytical
Parameter
Number Method
Result Q
LOQ Units Run
Sulfate
300.0
3.7
1.0 mg/L 1
TDS
SM 254OC-2011
69
25 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 65 of 108

CVAA
Client:ERM NC, Inc. Laboratory ID:WD07090-021
Description: SS-50-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1300
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 04/14/2021 1747 CMS2 04/13/2021 1206 88501
Parameter
Mercury
CAS Analytical
Number Method Result Q LOQ Units Run
7439-97-6 7470A ND 0.00020 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 66 of 108

ICP-MS Metals
Client:ERM NC, Inc. Laboratory ID:WD07090-021
Description: SS-50-WS-20210406 Matrix: Aqueous
Date Sampled:04/06/2021 1300
Date Received:04/07/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 04/12/2021 2137 BPK 04/12/2021 0435 88494
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6020B
1700
40
ug/L
1
Barium
7440-39-3
6020B
47
5.0
ug/L
1
Cadmium
7440-43-9
6020B
ND
0.50
ug/L
1
Chromium
7440-47-3
6020B
14
5.0
ug/L
1
Iron
7439-89-6
6020B
2200
50
ug/L
1
Lead
7439-92-1
6020B
ND
1.0
ug/L
1
Manganese
7439-96-5
6020B
35
5.0
ug/L
1
Selenium
7782-49-2
6020B
ND
5.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 67 of 108

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 68 of 108

Inorganic non-metals - MB
Sample ID: WQ88315-001 Matrix: Aqueous
Batch: 88315
Analytical Method: SM 2540C-2011
Parameter Result Q Dil LOQ Units Analysis Date
TDS
ND
25 mg/L 04/07/2021 2321
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 69 of 108

Inorganic non-metals - LCS
Sample ID: WQ88315-002 Matrix: Aqueous
Batch: 88315
Analytical Method: SM 2540C-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TDS 1500 1500 1 99 90-110 04/07/2021 2321
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 70 of 108

Inorganic non-metals - Duplicate
Sample ID: WD07090-003DU Matrix: Aqueous
Batch: 88315
Analytical Method: SM 2540C-2011
Sample
Amount Result %RPD
Parameter (mg/L) (mg/L) Q Dil % RPD Limit Analysis Date
TDS 360 370 1 2.7 20 04/07/2021 2321
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 71 of 108

Inorganic non-metals - Duplicate
Sample ID: WD07090-005DU Matrix: Aqueous
Batch: 88315
Analytical Method: SM 2540C-2011
Sample
Amount Result %RPD
Parameter (mg/L) (mg/L) Q Dil % RPD Limit Analysis Date
TDS 270 280 1 2.2 20 04/07/2021 2321
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 72 of 108

Inorganic non-metals - MB
Sample ID: WQ88457-001 Matrix: Aqueous
Batch: 88457
Analytical Method: SM 2540C-2011
Parameter Result Q Dil LOQ Units Analysis Date
TDS
ND
25 mg/L 04/08/2021 2036
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 73 of 108

Inorganic non-metals - LCS
Sample ID: WQ88457-002 Matrix: Aqueous
Batch: 88457
Analytical Method: SM 2540C-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TDS 1500 1500 1 99 90-110 04/08/2021 2036
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 74 of 108

Inorganic non-metals - MB
Sample ID: WQ88524-001 Matrix: Aqueous
Batch: 88524
Analytical Method: 300.0
Parameter Result Q Dil LOQ Units Analysis Date
Sulfate ND 1 1.0 mg/L 04/08/2021 1215
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 75 of 108

Inorganic non-metals - LCS
Sample ID: WQ88524-002 Matrix: Aqueous
Batch: 88524
Analytical Method: 300.0
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 20 1 98 90-110 04/08/2021 1323
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 76 of 108

Inorganic non-metals - MS
Sample ID: WD07090-OO5MS Matrix: Aqueous
Batch: 88524
Analytical Method: 300.0
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 9.0 10 18 1 90 90-110 04/08/2021 1834
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 77 of 108

Inorganic non-metals - MSD
Sample ID: WD07090-OO5MD Matrix: Aqueous
Batch: 88524
Analytical Method: 300.0
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 9.0 10 18 N 1 89 0.83 90-110 20 04/08/2021 1851
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 78 of 108

Inorganic non-metals - MS
Sample ID: WD07090-014MS Matrix: Aqueous
Batch: 88524
Analytical Method: 300.0
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 14 10 24 1 95 90-110 04/08/2021 2214
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 79 of 108

Inorganic non-metals - MSD
Sample ID: WD07090-014MD Matrix: Aqueous
Batch: 88524
Analytical Method: 300.0
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 14 10 24 1 92 1.5 90-110 20 04/08/2021 2231
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 80 of 108

Inorganic non-metals - MB
Sample ID: WQ88729-001 Matrix: Aqueous
Batch: 88729
Analytical Method: 300.0
Parameter Result Q Dil LOQ Units Analysis Date
Sulfate ND 1 1.0 mg/L 04/09/2021 1525
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 81 of 108

Inorganic non-metals - LCS
Sample ID: WQ88729-002 Matrix: Aqueous
Batch: 88729
Analytical Method: 300.0
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 20 1 98 90-110 04/09/2021 1559
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 82 of 108

Inorganic non-metals - MS
Sample ID: WD07090-O21MS Matrix: Aqueous
Batch: 88729
Analytical Method: 300.0
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 3.7 10 13 1 98 90-110 04/09/2021 1706
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 83 of 108

Inorganic non-metals - MSD
Sample ID: WD07090-O21MD Matrix: Aqueous
Batch: 88729
Analytical Method: 300.0
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 3.7 10 14 1 98 0.36 90-110 20 04/09/2021 1723
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 84 of 108

Inorganic non-metals - MB
Sample ID: WQ88845-001 Matrix: Aqueous
Batch: 88845
Analytical Method: 300.0
Parameter Result Q Dil LOQ Units Analysis Date
Sulfate ND 1 1.0 mg/L 04/12/2021 1251
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 85 of 108

Inorganic non-metals - LCS
Sample ID: WQ88845-002 Matrix: Aqueous
Batch: 88845
Analytical Method: 300.0
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 19 1 97 90-110 04/12/2021 1325
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 86 of 108

Inorganic non-metals - MB
Sample ID: WQ88929-001 Matrix: Aqueous
Batch: 88929
Analytical Method: SM 2540C-2011
Parameter Result Q Dil LOQ Units Analysis Date
TDS
ND
25 mg/L 04/14/2021 0020
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 87 of 108

Inorganic non-metals - LCS
Sample ID: WQ88929-002 Matrix: Aqueous
Batch: 88929
Analytical Method: SM 2540C-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TDS 1500 1500 1 98 90-110 04/14/2021 0020
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 88 of 108

Inorganic non-metals - Duplicate
Sample ID: WD07090-001DU Matrix: Aqueous
Batch: 88929
Analytical Method: SM 2540C-2011
Sample
Amount Result %RPD
Parameter (mg/L) (mg/L) Q Dil % RPD Limit Analysis Date
TDS 1600 1600 1 0.63 20 04/14/2021 0020
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 89 of 108

ICP-MS Metals - MB
Sample ID: WQ88352-001 Matrix: Aqueous
Batch: 88352 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 04/09/2021 0402
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Aluminum
ND
1
40
ug/L
04/09/2021 1713
Barium
ND
1
5.0
ug/L
04/09/2021 1713
Cadmium
ND
1
0.50
ug/L
04/09/2021 1713
Chromium
ND
1
5.0
ug/L
04/09/2021 1713
Iron
ND
1
50
ug/L
04/09/2021 1713
Lead
ND
1
1.0
ug/L
04/09/2021 1713
Manganese
ND
1
5.0
ug/L
04/09/2021 1713
Selenium
ND
1
5.0
ug/L
04/09/2021 1713
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 90 of 108

ICP-MS Metals - LCS
Sample ID: WQ88352-002 Matrix: Aqueous
Batch: 88352 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 04/09/2021 0402
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Aluminum
100
110
1
108
80-120
04/09/2021 1719
Barium
100
100
1
102
80-120
04/09/2021 1719
Cadmium
100
96
1
96
80-120
04/09/2021 1719
Chromium
100
99
1
99
80-120
04/09/2021 1719
Iron
1000
1000
1
100
80-120
04/09/2021 1719
Lead
100
97
1
97
80-120
04/09/2021 1719
Manganese
100
98
1
98
80-120
04/09/2021 1719
Selenium
100
92
1
92
80-120
04/09/2021 1719
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 91 of 108

ICP-MS Metals - MS
Sample ID: WD07090-001MS
Matrix: Aqueous
Batch: 88352
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
04/09/2021
0402
Sample
Spike
Amount
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q
Dil
% Rec
Limit
Analysis Date
Aluminum
400
100
590
N
1
190
75-125
04/09/2021 1731
Barium
31
100
130
1
99
75-125
04/09/2021 1731
Cadmium
ND
100
91
1
91
75-125
04/09/2021 1731
Chromium
ND
100
94
1
94
75-125
04/09/2021 1731
Iron
1200
1000
2100
1
96
75-125
04/09/2021 1731
Lead
ND
100
97
1
97
75-125
04/09/2021 1731
Manganese
3600
100
3700
10
101
75-125
04/09/2021 2247
Selenium
17
100
150
N
1
128
75-125
04/09/2021 1731
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 92 of 108

ICP-MS Metals - MSD
Sample ID: WD07090-001MD
Matrix: Aqueous
Batch: 88352
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
04/09/2021 0402
Sample
Spike
Amount
Amount
Result
%Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Aluminum
400
100
620
N 1
217
4.5
75-125
20
04/09/2021 1737
Barium
31
100
130
1
99
0.00
75-125
20
04/09/2021 1737
Cadmium
ND
100
92
1
92
0.49
75-125
20
04/09/2021 1737
Chromium
ND
100
92
1
92
2.0
75-125
20
04/09/2021 1737
Iron
1200
1000
2000
1
85
5.3
75-125
20
04/09/2021 1737
Lead
ND
100
98
1
98
1.9
75-125
20
04/09/2021 1737
Manganese
3600
100
3600
N 10
4.0
2.7
75-125
20
04/09/2021 2253
Selenium
17
100
150
N 1
129
0.41
75-125
20
04/09/2021 1737
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 93 of 108

ICP-MS Metals - MB
Sample ID: WQ88494-001 Matrix: Aqueous
Batch: 88494 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 04/12/2021 0435
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Aluminum
ND
1
40
ug/L
04/12/2021 2122
Barium
ND
1
5.0
ug/L
04/12/2021 2122
Cadmium
ND
1
0.50
ug/L
04/12/2021 2122
Chromium
ND
1
5.0
ug/L
04/12/2021 2122
Iron
ND
1
50
ug/L
04/12/2021 2122
Lead
ND
1
1.0
ug/L
04/12/2021 2122
Manganese
ND
1
5.0
ug/L
04/12/2021 2122
Selenium
ND
1
5.0
ug/L
04/12/2021 2122
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 94 of 108

ICP-MS Metals - LCS
Sample ID: WQ88494-002 Matrix: Aqueous
Batch: 88494 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 04/12/2021 0435
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Aluminum
100
110
1
110
80-120
04/12/2021 2130
Barium
100
99
1
99
80-120
04/12/2021 2130
Cadmium
100
90
1
90
80-120
04/12/2021 2130
Chromium
100
100
1
102
80-120
04/12/2021 2130
Iron
1000
970
1
97
80-120
04/12/2021 2130
Lead
100
100
1
101
80-120
04/12/2021 2130
Manganese
100
100
1
102
80-120
04/12/2021 2130
Selenium
100
89
1
89
80-120
04/12/2021 2130
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 95 of 108

CVAA -MB
Sample ID: WQ88500-001 Matrix: Aqueous
Batch: 88500 Prep Method:
Analytical Method: 7470A Prep Date: 04/09/2021 1255
Parameter Result Q Dil LOQ Units Analysis Date
Mercury ND 1 0.00020 mg/L 04/09/2021 1739
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 96 of 108

CVAA - LCS
Sample ID: WQ88500-002 Matrix: Aqueous
Batch: 88500 Prep Method:
Analytical Method: 7470A Prep Date: 04/09/2021 1255
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury 0.0020 0.0016 1 81 80-120 04/09/2021 1742
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 97 of 108

CVAA - MS
Sample ID: WD07090-004MS Matrix: Aqueous
Batch: 88500 Prep Method:
Analytical Method: 7470A Prep Date: 04/09/2021 1255
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury ND 0.0020 0.0018 1 90 80-120 04/09/2021 1755
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 98 of 108

CVAA - MSD
Sample ID: WD07090-004MD Matrix: Aqueous
Batch: 88500 Prep Method:
Analytical Method: 7470A Prep Date: 04/09/2021 1255
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Mercury ND 0.0020 0.0016 1 82 9.3 80-120 20 04/09/2021 1758
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 99 of 108

CVAA -MB
Sample ID: WQ88501-001 Matrix: Aqueous
Batch: 88501 Prep Method:
Analytical Method: 7470A Prep Date: 04/13/2021 1206
Parameter Result Q Dil LOQ Units Analysis Date
Mercury ND 1 0.00020 mg/L 04/14/2021 1712
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 100 of 108

CVAA - LCS
Sample ID: WQ88501-002 Matrix: Aqueous
Batch: 88501 Prep Method:
Analytical Method: 7470A Prep Date: 04/13/2021 1206
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury 0.0020 0.0018 1 89 80-120 04/14/2021 1715
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 101 of 108

CVAA - MS
Sample ID: WD07090-018MS Matrix: Aqueous
Batch: 88501 Prep Method:
Analytical Method: 7470A Prep Date: 04/13/2021 1206
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury ND 0.0020 0.0019 1 93 80-120 04/14/2021 1731
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 102 of 108

CVAA - MSD
Sample ID: WD07090-018MD Matrix: Aqueous
Batch: 88501 Prep Method:
Analytical Method: 7470A Prep Date: 04/13/2021 1206
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Mercury ND 0.0020 0.0017 1 86 7.7 80-120 20 04/14/2021 1733
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 103 of 108

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 104 of 108

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 105 of 108

PACE ANALYTICAL SERVICES, LLC
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 106 of 108

PACE ANALYTICAL SERVICES, LLC
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 107 of 108

PACE ANALYTICAL SERVICES, LLC
San)pIts ReceiptCl klist tSRCJ (FOEVOUIC-15} RevlSed-9/?W2020
Jrc�r7 '17t+ 1
Is.SuingAuthcfity. Pace eNV-VIM- P€i� i Of 1
Sample Receipt Cbeeldist (SRC)
Client GAV
C'.colCT Jnspccted Lot 4L WD07090
Meatls ofreceipt:
d I'r-ce Client UPS YedEx Other,
Yes , N a
_Iv$u
I - Vv'r ckstody .ePalA prc:ant or- diet�uuicTff
Nei
NA 2, Ifc: study suers weu'e fres�nt, w(!l'e thf!'y inlid Witwkik�!n'7
pN Scrip ID; tea: ;x
C hlorre S..rip IL), NA _ _ fwsted la Jiicz
Original tempeizAum upon rev ipt 117crived (Cormcmd) relnprrraturs upon reix{jpt 9v4tirid Snap -Cup ID; HA
2 5 2'2.$ a v,8
31 3 RA jNA C IqA INA
Ieth-ad [V]'el1'kptr,11urr Blank Q 1-1_S BUt:iv: Ilt Oun ID; ' IF, Cria CbMet'on TauLLer 0 aO
ediod of coolant,
Yet rrr D Ice Paco _Q D1ti+ la: NOrte
El Yes ❑ids Q ETA If temperatu, c of ari v coriler ex at id 6,4°C, W25 Proj�ecr MWIagur Notified?F'
as Woo(14A by. plinric i a tiaii ! hwc-to-taCe (crr k —Quie)-
Ye-9No 1 NA 4- Is tho c74111tni mial =11 der's packinjg sli p attamhed to JJs A)rm7
Ye.. No
5- W=pro aroistOdy praced"rr•s (reltnquishedJreceived) FoIIoxred?
Yes No
6. Were sauplr; 611s listed oo the COC?
Yes N01
7_ WnP sample IrDS listed mn .4 sanl Pie Containers7
V Yes NO1
Vas oo-llection dtt°e & time; fisted on the 00i ?
.V" Yes
9. Vas nollectiorkdateRr. bole listed on all =Mplc
#LNa
csQ
10, Did aiII V4ntainer labelinibmnarion (ID, daretime) aexz with tlw COO
o
11. WQrl tests to br rQfornktxf I:sted on t1le CDC?
Yes ©No 12: Dili a!;-rnpla5 un-itic in J-m pmpar nontai-Lim for each trrt aadlor in ,good condi tidn
(unhixrken, lids on, atc,)?
Yes LJ 113. W-m adcquate sample volume available?
Y;s No ] . Vsfcrc fll1 a1up1tm moeived widtiu 3- the holdin 1i_wi or49 hours, wfijC1evrr ULNTrMs firs:'?
Yes N0 15, VU°em any mny sles ountainers this ' 'excess (Circle 2ti 0 salnpl�i Nu t J istad on C4C?
[] i'os. Q Tee �✓ tJ.4 16. For VOA and 1t4K- r 75 satnph�, wore bubbles present L'p"a_sJ e' ('l."cr 6ttti,n it diameter)
in ar.y of-tho VOA vials?
d 'It ss LJ No NA 1'7- Wr:re. all DjZ0jmet1161T itrient smr,pEcs received At a plc Or- 2?
Yea No JAI 4, Vr ere all Cyanide saiytpi es recej- xud ft a pld > 12 and vulyde satnples received m $ 1 I >
Y ❑Flo ] 1 ere aL' &p� icab e .yf17 [ 1cy#rrt�-1r�,i{6 }5-1 rfit} < O,Smg;L) samplos free or
residua! cd 1un1te'+
❑ YQ3 0 No T1Nk Z0, Wert dicer remark;?tquesui {i-e, r stCd dilutions, MVIdSD des
iV iati;.ns, etc...l
correctly franscribed fron the 4 ;'Ic iota OW (Virkme.nt;Wf.non iii ]'jNjS'?
Yi x Na 21. 1Vas t>we srote,�umbor listen on the t3wltai iw label° jf, Cluutc g x,} _
Sample Presery_ation Nast be cnmplend far any sariplc(s) inco=tly preserved or with ljQidsp3w_) -
Sample(s) k were recuivad inomitcril orascr4 oral were id;U!51Q i accordingly
i:i sample rWXiviafg with NA mi., of Circle one: I-12SO4, HNO3, HU, MeDH Lnh% .�R P VA
Tim clef Vre :atio.i '4.1 Ifm0T-; than One preservativu is needed, piMoe uotc in the ell— rMelit' bM:o�r_
�linpie(s) r_rti were mcived with bubble. �,6 mm iri diameter.
atr�ples(sj vn �vere rece3'iEd wilth TRC>0,5 inFfi. (rFA19 isNo) and wr a '—
idjuslew accordingly insanipiereceivirrgwith sodium thinsliifata Na2920,)wEth Skliealy ID: fin
barc4jde;;abejSLppjod by. JRG2 Daf� ; 0F1{?7fiLU2I
Camrnmis:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 108 of 108

APPENDIX C GROUNDWATER SAMPLING LOGS
www.erm.com Version: 1.0 Project No.: 0588865 Client: R.J. Reynolds Tobacco Co. July 2021
2021-04 Edwards Rd LF Rural Hall GW Report R1.docx

WATER MATRIX SAMPLING t+
FIELD DATA FORM
Site Name: RJRT Edwards Road Landfill Job #:0551517
Sample Type: Circle one- (Monitor Well, DPT, Surface Water, Potable WSW; other)
Sample ID: W,
Date: "5 ` .z
Sampling Personnel:
Andrew H. MtchntpR.
Weather Conditions: u/
Partly Cloudy, Cloudy, Rain;
Other
Time:
Well Type: Flush Surface Completion, Stick U pletion
Well Locked: es No Lock Present: es No
Well Tag Present:
Well ID info. on Tag:
No
Q) No
Well Bolted: Yes, No, /
Well Cap: es No
Well Cap Condition:
oo Replace, Other;
Well Pad Condition: o
Cracked, Replace, Other:
Well Location: as
Asphalt, Concrete,
Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
51 0 15, 20
feet -other:
Depth to Water (D.T.W):
Field Parameters measured
%
with: l� ,��
Well Diameter:
Casing Type:
4, 6, s
KSSteel
Inches -other:
other:
Purge Rate:
mUrnin
Sampling Device:
P Ista ic, Monsoon,
Grundfos, Bailer, PDB, Other:
Tubing Type: Polyethylene
Pump Intake (ft below M.P.): 2 5
Measuring Point:
Color: z
TOC
Odor:
other:
Yes, dro
Time:
min
olume
ur ed
DTW:
feet
Temp
(°C)
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria 2
F(gallons)
(see note+/
below)3
3%
0.1 unit
3%
10%
10 mV
-
10%4
v
v�
q127.0
S
0
d'
Ki
-
70.
®Y
.Z
3,77
,
5
01
Official Sampling Date &Time: � SO
Samples Collected: Analysis Requested: Preservative:
Notes:
(1) - Do not measure depth to bottom of well until after purging and sampling to reduce resuspending fines that may be resting on the well bottom.
(2) -Stabilization criteria based on three most recent consecutive measurements.
(3) - Total dravdovm In well to be less than 0.1 m (0.32 tt). Purging rate to be lowered as necessary to keep drawdown helow 0.1 m (0.32 fl).
Hold Time (days): Lab:

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: RJRT Edwards Road Landfill Job #:0551517
Sample Type: Circle one - (Monitor Well, DPT, Surface Water, Potable WSW; other)
WIN
Sample ID: '
Date: "
Sampling Personnel: Andrew H. MicPMMt . r
Weather Conditiponsw Stjnn Partly Cloudy, Cloudy, Rain; Otherl.
Time:
Well Type: Flush Surface
Well Locked: Qed No
Well Bolted: Yes, N
Well Pad Condition: ood,
Additional Comments:
Completion, Stic U ompletion Well Tag Present:
Lock Present % No Well ID info. on Tag:
Well Cap: s, No Well Cap Condition:
racked, Replace, Other: Well Location' Grass,
No
No
c c28, Replace, Other;
, Concrete, Woods, Other;
Total Depth of Well (T.D.):
Depth to Water (D.T.W): t't
Field Parameters measured with:
Screen Length:
Well Diameter:
Casing Type:
5, 10, 151 20
21 41 s, a
PVC, Steel
feet -other:
Inches -other:
other:
Purge Rate: mUrnin
Tubing Type: Polyethylene
Pump Intake (ft below M.P.):
Sampling Device:
Measuring Point:
Color:
Peristaltic, Monsoon, Grundfos, Bailer, PDB, Other:
TOC other:
Odor: Yes, No
Time:
min
Stabalization
Criteria
Volume
Pur ed
(gallons)
DTW:
feet
(see note
below)3
Temp
eC)
3%
pH
std units
0.1 unit
SPC
uS/cm
3%
r
DO
m /L
10%
r
ORP
mV
10 mV
Turb
NTU
10%'
%
Comments:
lL!
`dtol�.
Official Sampling Date &Time:
Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab:
Notes:
(i) - Do not measure depth to bottom of vrell until after purging and sampling to reduce resuspending fines that may 6e resting on the well bottom.
(2) -Stabilization cdteda based on three most recent consecutive measurements.
(3)-Total dravdown in well to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep dravdo�m below 0.1 m (0.32 ft).

WATER MATRIX SAMPLING {
FIELD DATA FORM
ERM
Site Name: RJRT Edwards Road Landfill Job #:0551517
Sample Type: Circle one - (Monitor Well, DPT, Surface Water, Potable WSW; other)
Sample ID:
Date:
o
Sampling Personnel:
Weather Conditions: n
Andrew H. MiskteaHk
Partly Cloudy, Cloudy, Rain;
Other
Time:
Well Type: Flush Surface
Well Locked: es, No
Well Bolted: Yes, No, /A
Well Pad Condition: G oo
Completion, Stick U C pletion
Lock Present: No
Well Cap: es, No
Cracked, Replace, Other:
Well Tag Present:
Well ID info. on Tag:
Well Cap Condition:
Well Location: Grass,
es No
Y s No
oo Replace, Other;
Asphalt, Concrete, _V Other;
Additional Comments:
Total Depth of Well (T.D.): 7
Depth to Water (D.T.W): t+t r
Field Parameters measured w
Screen Length: 5, 15, 20
Well Diameter: a, 63 s
Casing Type: P Steel
feet -other:
Inches -other:
other:
Purge Rate: mUmin
Tubing Type: Polyethylene
Pump Intake (ft below M.P.):
Sampling Device: Penrbtic, Monsoon, Grundfos, Bailer, PDB, Other:
Measuring Poi : TOC other:
Color: Clew Odor: Yes, I t)
Time:
min
Volume
Purged
DTW:
feet
Temp
°C
std
pH
units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria2
(gallons)
(see note
below)'
+/.
3%
+/-
0.1 unit
+/-
3%
+/-
10%
+b
10 mV
tQAj
+/-
10°�4
r
MK
01
52
5b6 0
o
1, L
, 9'
3.k
d 4
Official Sampling Date &Time:
Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab:
Notes:
(t) - Do not measure depth to bottom of vrell until after purging and sampling to reduce resuspending fines that may 6e resting on the well bottom.
(2) -Stabilization cdteda based on three most recent consecutive measurements.
(3) -Total drawdovm in well to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep drawdovm below 0.1 m (0.32 ft).

WATER MATRIX SAMPLING }
FIELD DATA FORM
Site Name: RJRT Edwards Road Landfill Job #:0551517
Sample Type: Circle one - (Mo ti ?Well, DPT, Surface Water, Potable WSW; other)
Sample ID: M*1�
Date:' r
Sampling Personnel:
Andrew H. N}ieHeaf-R�'
Weather Conditions: S n ,
Partly Cloudy, Cloudy, Rain; Other
Time: % t> j0
Well Type: Flush Surface Completion, Stick Upo pletion
Well Tag Present:
YO No
Well Locked: Yes, 1)
Lock Present: es; No
Well ID info. on Tag:
a No
Well Bolted: Yes, No, !
Well Cap: N
Well Cap Condition:
G6 Replace, Other;
Well Pad Condition: G
Cracked, Replace, Other:
Well Location: Grass, Asphalt,
Concrete,
W o Other;
Additional Comments:
Total Depth of Well (T.D.):
!
Screen Length:
51 10, 15,
feet -other:
Depth to Water (D.T.W): 0)
e't
Well Diameter:
a, s,
a
Inches -other:
Field Parameters measured
with: Pot
Casing Type:
Steel
other:
Purge Rate:
mUmin
Sampling Device:
Pej Is Itic,
Monsoon,
Grundfos, Bailer, PDB, Other:
Tubing Type: Polyethylene
Measuring Point:
TOC
other:
Pump Intake (ft below M.P.):
Color: e
Odor:
Yes, Qtp
Time:
min
Purged
DTW:
feet
Temp
°C
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization(see
Criteria 2
Z(gallons)
note+/
be loev)3
3%
0.1 unit
3%
10%
10 mV
-
10%4
20
It
I
NO
y*
c
1 11
cU
Official Sampling Date &Time:
Samples Collected: Analysis Requested: Preservative:
Notes•
(1) - Do not measure depth to bottom of vrell until after purging and sampling to reduce resuspending fines that may be resting on the yell bottom.
(2) -Stabilization criteria based on three most recent consecutive measurements.
(3) - Total dravdovm in well to be Tess than 0.1 m (g.32 ft). Purging rate to be lowered as necessary to keep draadown below 0.1 m (g.32 ft).
Hold Time (days): Lab:

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: RJRT Edwards Road Landfill
Job #:0551517
Sample Type: Circle oneCw Monitor Well PT, Surface Water, Potable WSW; other)
Sample ID:
Date: ->S / Z
Sampling Personnel:
Andrew H. Mi eal R.
Weather Conditions: unny,
Partly Cloudy, Cloudy, Rain; Other
Time: I S S
Well Type: Flush Surface Completion, stick Up Completion
Well Locked: ` es Lock Present es) No
Well Tag Present:
Well ID info. on Tag:
Yes No
es No
Well Bolted: Yes, No, /A
Well Cap: , No
Well Cap Condition:
Goo Replace, Other;
Well Pad Condition: Goo Cracked, Replace, Other:
Well Location: Grass,
Asphalt,
Concrete,
Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
caU
Screen Length:
51 % 15, 20
feet -other: 0
Depth to Water (D.T.W): ttl
Field Parameters measured
Purge Rate:N
Tubing Type: Polyethylene
Pump Intake (ft below M.P.):
with: f4brZjjR
mt./min
11cl J:':�r
Well Diameter: g� 4, s, a
Casing Type: C/ Steel
Sampling Device: Peristaltic, Monsoon,
Measuring Point: TOC
Color: Odor:
Inches -other:
other:
rundfos Bailer, PDB, Other:
other:
Yes, No
Time:
DTW:
Temp
pH
SPC
DO
ORP
Turb
min
feet
CC)
std units
uS/cm
m /L
mV
NTU
E(gallons)
Stabalization(see
Criteria2
note
below)3
+/-
3%
+A
0.1 unit
+/-
3%
+/-
10%
+/-
10 mV
+/-
10e�4
Comments:
1 l s"S o
Its 4 5w
q, 6 lb
s
L>s ao
I 668
16.38
6 4
G3
36 4
34
37
010
,ot
G�•3o
S
cU
(0 8
IZt , zo
146 Ly
q.5?
3q(�I
5,ig
,�
119:7=
ZS
Il. c
01161
373
S .C9
1L-tsv
LI-O
11)0 5
I�, S�j
c(r 65
3�Z
L-t z3z
LI.83
13
Ih
z. Z
l
Official Sampling Date &Time: OL%lC;��Z
Z 3
Preservative: Hold Time (days): Lab:
Notes:
(1)- Do not measure depth to bottom o(vrell until aRer purging and sampling to reduce resuspending Rnes that may be resting on the well bottom.
(2) -Stabilization cdteda based on three most recent consecutive measurements.
(3) -Total drakdovm In well to be less than 0.1 m (0.32 R). Purging rate to be lowered as necessary to keep drattdovm below 0.1 m (0.32 R).

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: RJRT Edwards Road Landfill Job #:0551517
Sample Type: Circle one- (Monitor Well, DPT, Surface Water, Potable WSW; other)
Sample ID: 4,3 - - CG -
Date: G �- p 5
Sampling Personnel: <
Zo z_�'—
ndrew Micheal R.
Weather Conditions: unny,
artlyCloudy, Cloudy, Rain;
Other
Time: J ! 3
Well Type: Flush Surface Completion, Stick Up Completion
Well Locked: No Lock Present: No
Well Tag Present:
Well ID info. on Tag:
No
Yes, No
Well Bolted: Yes, No,
Well Cap: es, No
Well Cap Condition
Vjoocl, Replace, Other;
Well Pad Condition: oo , Cracked, Replace, Other:
Well Location: _rass
Asphalt, Concrete,
Woods, Other;
Additional Comments:
Total Depth of Well (T.D.): 1c.1
I
Screen Length:
51 101 153
20
feet -other: 0 Per.1 t;o(CC'
Depth to Water (D.T.W): tt1
Field Parameters measured
with: n (zz,g0
Well Diameter:
Casing Type:
2) 41 ds
PVC, ite
Inches -other:
other:
Purge Rate:. I s-U
Tubing Type: Polyethylene
Pump Intake (ft below M.P.):
ml./min
ZGU
Sampling Device:
Measuring Point:
Color:
Peristaltic, Monsoon,
TOC
Odor:
rund Bailer, PDB, Other:
other:
Yes, No
me
ed
DTW:
feet
Temp
°C
pH
std units
SPCrDO
uS/cm
ORP
mV
Turb
NTU
Comments:
ffaon
ons)
(see note
below)'
+/-
3%
I ,it
I7,o
+/-
0.1 unit
6.51
6.41
6•u3
+/-
3%
i O
16 5
166
r zl306
�.6
10 mV
355
10%°
6c( 3
56,1br95
I6,�a
6.39
1b�
.6z
z5Z
`-t3.3
ZOO
16.�0
6.3
66
3.35
313
31,44
L5
I;.00
6 �i0
166
q.ZZ
3ZI
L9.6
il.o&
04I
1&630
Official Sampling Date &Time:600
Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab:
Notes:
(1)- Do not measure depth to hc[[om of v:ell until after purging and sampling to reduce resuspending (nes that maybe resfing on the well bottom.
(2) - Stabllizatlon criteda based on three most recent consecutive measurements.
(3) - Total draKdovm In well to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep dra��down below 0.1 m (0.32 ft).

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: RJRT Edwards Road Landfill
Job #:0551517
Sample Type: Circle one Monitor.Wel PT, Surface Water, Potable WSW; other)
Sample ID: L�) c. N Zt U'-( U S
Date: V C (0 5/ z
I
Sampling Personnel:
Andrew icheal R.
Weather Conditions: unny Partly Cloudy, Cloudy,
Rain; Other
Time: 9 'l UP
Well Type: Flush Surface
Completion, tick Up Completio
Well Tag Present: tAY
No
Well Locked: <Ye No
Lock Present: es No
Well ID info. on Tag:
(Ye, No
Well Bolted: Yes, No, /A
Well Pad Condition: o
Well Cap: Yes No
Cracked, Replace, Other:
Well Cap Condition:
Well Location: ras
o od, Replace, Other;
, Asphalt, Concrete, Woods, Other;
Additional Comments:
Total Depth of Well (T.D.): ( Z
Depth to Water (D.T.W): 0)
Field Parameters measured with: %%(0Cz-JAF>/;'
Purge Rate: n..( �(o mUmin
Screen Length:
Well Diameter:
Casing Type:
Sampling Device:
58 101 1510
Q% 4, s, a
PV , steel
Peristaltic, Monsoon,
feet -other:
Inches -other:
other:
rundf , Bailer, PDB, Other:
Tubing Type: Polyethylene
Pump Intake (ft below M.P.):
Measuring Point:
Color:
TOC
Odor:
other:
Yes, No
Time:
min
Volume
Pur ed
DTW:
feet
Temp
(°C)
pH
stdunits
SpC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
�--
I — I• _ _ ^' "—
— — Comments: — -
Stabalization
Criteria
(gallons)
(see note
below)3
+/-
3%
+/-
0.1 unit
+/-
3%
+/-
10%
+/-
10 mV
+/-
10%
I'A
s
Il•`10
6,Z5
Zc)
1 q 6
• O S'
186
Z 0
1 i6
�G
13L.
Ic
o6a945
G 05
106
3sbb
I1Z
IZ
)6
iq, l0
6.o-&
!}G
` at L4
1
t 36
Zo
25
I " .0
I, 7 el
6.`t7
S, Ct 5
t L6
160
k, zC
tot a '*A a(
Zlq
Z 30
114
! I G
3U
I`t .del
S.`t�l
I S4
Lot .SK
MHz
Official Sampling Date &Time: so
Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab:
Notes:
(1) - Do not measure depth to hottom or vrell until after purging and sampling to reduce resuspending fines that may be resting on the well hottom.
(2) - Slahilization criteria based on three most recent consecutive measurements.
(3) -Total dravdovm In yell to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep drawdown below 0.1 m (0.32 ft).

WATER MATRIX SAMPLING
FIELD DATA FORM
ERM
Site Name: RJRT Edwards Road Landfill Job #:0551517
Sample Type: Circle one =41%tlonitorWRII, DPT, Surface Water, Potable WSW; other)
Sample ID: w l - +-•.�Cr
Date: U4-1 e�cvC• Z
Sampling Personnel:
_ c
Andrew . Micheal R.
Weather Conditions:( Sunn
Partly Cloudy, Cloudy,
Rain; Other
Time: DE�tkD
Well Type: Flush Surface
Well Locked: Ye , No
Completion, -Stick Up Completi6i7
Lock Present: Yes; --No-- —
Well Tag Present:
Well ID info. on Tag.
Yes No
No
Well Bolted: Yes, No, i /A)
Well Cap: Ya, No
Well Cap Condition:
LQcL J Replace, Other;
Well Pad Condition: Good,
Cracked, Replace, Other:
Well Location Gras),
Asphalt,
Concrete,
Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
z (,
Screen Length:
51 % 15, 20 3 c� feet -other:
Depth to Water (D.T.W): ttl
Field Parameters measured with: ,- T�t7:k
Well Diameter: C2 41 61 s
Casing Type: PAC; Steel
Inches -other:
other:
Purge Rate: ti / � v
mUrnin
Sampling Device:
Peristaltic,
Monsoon,
Gmndfos� Bailer, PDB, Other:
Tubing Type: Polyethylene
Pump Intake (ft below M.P.): a ., s
Measuring Point:
Color:
TOC
Odor:
other:
Yes, No
ime:
min
Volume
Pur ed
DTW:
feet
Temp
°C)
pH
std units
SpC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
]Stabalization
(gallons)
(see noteriteria2
below)3
3%
0.1 unit
3%
10%
10 mV
10%4
Ito `15�
tv Z
3 ci
0S"0:1
-3C
c>
t5
1�.Ux
II.45-3
6 4 1
e.
2�
r
II.SG
i�7�
v.G3
-70
v o
l3_
Id703
II.S�
v"1Z
56
c>.0
Official Sampling Date &Time: (✓ ` � � b � l ` � / ocl f
Samples Collected: Analysis Requested: Preservative:
Notes:
(7) - Do not measure depth to bottom of vrell until after purging and sampling to reduce resuspending Rnes that may be resfing on the well bottom.
(2)- Stabilizafion criteria based on three most recent consecutive measurements.
(3) -Total draxdovm in wall to be less than 0.1 m (0.32 R). Purging rate to be lowered as necessary to keep drawdo�m below 0.1 m (0.32 ft).
Hold Time (days): Lab:

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: RJRT Edwards Road Landfill Job #:0551517
Sample Type: Circle one - onitor Well DPT, Surface Water, Potable WSW; other)
Sample ID: IZX%)
Date: 0 �t /0! z
Sampling Personnel: nd ew H. Micheal R.
Weather Conditions: nny
Partly Cloudy, Cloudy, Rain;
Other
Time: 3 C> C: )
Well Type: Flush Surface Co Stick Up Completion
Well Locked: Yes, 40) Lock Present: Yes, 196)
Well Bolted: Yes, No, / Well Cap: es, No
Well Tag Present:
Well ID info. on Tag:
Well Cap Condition:
Ye No
a No
oo ; Replace, Other;
Well Pad Condition: Good,
Cracked, Replace, Other:
Well Location: Grass,
Asphalt,
oncr Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
gi �10 t:)
Screen Length:
5, 101 151
20
feet -other: oi�c� 3c.�;ce:4c
Depth to Water (D.T.W): (t)
Field Parameters measured
with: Nvt'K 3 A
Well Diameter:
Casing Type:
21 a, (n� a
PvC, tee
Inches -other:
other:
Purge Rate: U
Tubing Type: Polyethylene
Pump Intake (ft below M.P.):
mUmin
'Z u Cj
Sampling Device:
Measuring Point:
Color:
Peristaltic, Monsoon, rundfos Bailer, PDB, Other:
TOC other:
Odor: Yes, No
Time:
min
Volume
Pur ed
DTW:
feet
Temp
eC
std
pH
units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria2
(gallons)
(see note
below)3
+/-
3%
+b
0.1 unit
+/-
3%
10%
10 my
10%4
tsc,� c;
S
tl Z(
I� 38
L .
(O.
L
S6
Io'oL O
I>✓ CCU
C�.GfJ
OLz
I S
3Z•5
C L(ti
(0 Su
l 5
12 . sz
G
sY,
i Vigo
Lot
� 1- �(
Z�
ZS
I� t vG
(,:
ji `t
l�j
0.�1 (
Lt1•u
I�.SS
�•�S
/�f30
c,,�l
F3�
so.�
Official Sampling Date &Time: `j/US 1 Z ( I 18 3 JCS
Samples Collected: Analysis Requested: Preservative:
Notes:
(1) - Do not measure depth to bottom of vrell until after purging and sampling to reduce resuspending fines that may be resting on the yell bottom.
(2)-Stabilizatlon criteria based on three most recent consecutive measurements.
(3) - Total draxdovm in wall to be less than 0.7 m (0.32 ft). Purging rate to be lowered as necessary to keep draxdown below 0.1 m (0.32 fl).
Hold Time (days): Lab:

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: RJRT Edwards Road Landfill
Sample Type: Circle one - (Monitor Well, DP Surfar,
Job #:0551517
Potable WSW; other)
Sample ID: ' u rL(=OQ(LL
C.,.) P Te_ IZ
Date: r) c. I / U 6 / Z
(
Sampling Personnel:
Andrew H. Micheal R.
Weather Conditions: Sun
Partly Cloudy, Cloudy,
Rain; Other
Time:
Well Type: Flush Surface
Completion, Stick Up Completion
Well Tag Present:
Yes, No
Well Locked: Yes, No
Lock Present: Yes, No
Well ID info. on Tag:
Yes, No
Well Bolted: Yes, No, N/A
Well Cap:. Yes, No
Well Cap Condition:
Good, Replace, Other;
Well Pad Condition: Good,
Cracked, Replace, Other:
Well Location: Grass, Asphalt,
Concrete, Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
screen
Length:
53 101 151 20
feet -other:
Depth to Water (D.T.W): (1)
Well Diameter:
21 4, 61
s
Inches -other:
Field Parameters measured
with:
Casing Type:
PVC, Steel
other:
Purge Rate:
mUmin
Sampling Device:
Peristaltic,
Monsoon, Grundfos, Bailer, PDB, Other:
Tubing Type: Polyethylene
Measuring Point:
TOC
other:
Pump Intake (ft below M.P.):
Color:
Odor:
Yes, No
Time:
min
Volume
Purged
DTW:
feet
Temp
°C)
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria2
(gallons)
(see note
below)3
+/-
3%
+b
0.1 unit
+/-
3%
+/-
10%
+/-
10 mV
+/-
10%4
tzZ z
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Official Sampling Date &Time: /
Samples Collected: Analysis Requested: Preservative: Hold Time (days):
Notes:
(1) - Do not measure depth [o bottom of well until after purging and sampling to red
(2) -Stabilization criteria based on three most recent consecutive measurements.
(3) -Total dravdovm in wall to be less than 0.1 m (0.32 ft). Purging rate to be low-
>nding foes that may be resting on the vrell bottom.
_..ary to eep drawdovm helow 0.1 m (0.32 fq.
Lab:

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ERM has over 160 offices across the following
countries and territories worldwide
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