16017_Carolina Medical Electronics_Import Soil Analytical_2021Jul23

1
Peacock, David
From:Justin Ballard <[e-mail]>
Sent:Friday, July 23, 2021 8:06 AM
To:Peacock, David
Cc:Joe Landry
Subject:[External] Import Soil Sample Results - Carolina Medical Electronics
Attachments:Import Soil Results_Carolina Medical Electronics_7-23-2021.pdf
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Hi David, 
As you know, we have been working diligently to identify a borrow source for the Carolina Medical Electronics 
Brownfields property in King.  Joe’s team was able to identify a nearby piece of virgin land that was recently cleared for 
future residential structures.  After the land was cleared, we mobilized to the site to collect in‐situ soil samples for 
export evaluation.  Those sampling results are attached and indicate that this is an ideal borrow source for the 
Brownfields property.  The only compound that exceeded Industrial/Commercial PSRGs was arsenic, and that was from a 
background sample collected at the Brownfields property.  Also attached in the pdf package are two figures.  The borrow 
source figures indicates the area where dirt is proposed to be cut for export to the Brownfields property. 

Joe, please let David know the latest update on your redevelopment schedule (I believe your team had a meeting with 
DEQ yesterday to discuss erosion and sediment control activities) and when you would need DEQ Brownfields approval 
so that this borrow source can be utilized for grading? 

Thanks and please let me know if anyone has any questions.  I will be traveling most of today but can be reached on my 
mobile number listed below. 

Justin Ballard, PG, Project Manager
Hart & Hickman, PC
3921 Sunset Ridge Rd, Ste 301 ꞏ Raleigh, NC 27607
Direct: 919-723-2507 ꞏ Mobile: [phone]
www.harthickman.com   

Table 1Summary of Import Soil Analytical Data Carolina Medical ElectronicsKing, North CarolinaH&H Job No. DMM-001BS-2 BS-DUPDepth (ft bgs)9-12 9-12 9-12 0-3 9-12 0-3 6-8 0-3 0-3 0-3Date7/7/2021 7/7/2021 7/7/2021 7/7/2021 7/7/2021 7/7/2021 7/7/2021 7/7/2021 7/7/2021 7/7/2021VOCs (8260D) (mg/kg)Acetone 25 12,000 140,000 -- --<0.012 <0.013 <0.0110.032 J<0.0110.027 J 0.013 J 0.020 J -- --SVOCs (8270E) (mg/kg)(3)-- -- -- -- --RCRA Metals (6020B/7471B/7199) (mg/kg)Arsenic 5.8 0.68 3.0 3.0 - 4.51.0-18A0.30 0.81 0.70 0.84 2.1 0.87 1.3 1.94.53.0Barium 580 3,100 47,000 13 - 2550-1,000A560 230 250 230 110 160 140 140 25 13Cadmium 3.0 14 200BDL1.0-10B0.28 J 0.024 J 0.021 J 0.032 J<0.00820.043 J<0.0081 <0.0084 <0.0086 <0.0088Chromium, total NE NE NE 26 - 317.0-300A49 48 55 35 58 88 59 69 26 31Chromium, trivalent(3)360,000 23,000 350,000 25-30 NE 48 47 54 34 57 86 58 68 25 30Chromium, hexavalent 3.8 0.31 6.5 1.08 J - 1.26 J NE 0.713 J 0.940 J 0.867 J 0.909 J 1.08 J 1.98 0.762 J 1.09 J 1.08 J 1.26 JLead 270 400 800 19 - 21ND-50A63 31 33 27 20 45 22 26 21 19Mercury 1.0 2.3 9.7 0.13 - 0.220.03-0.52A0.031 J 0.030 J 0.037 0.038 J 0.079 0.071 0.046 0.071 0.22 0.13Selenium 2.1 78 1,200BDL<0.1-0.8A<0.052 <0.054 <0.053 <0.057 <0.053 <0.058 <0.052 <0.054 <0.056 <0.057Silver 3.4 78 1,200 0.080 J - 0.097 JND-5.0C0.10 J 0.079 J 0.085 J 0.094 J 0.096 J 0.085 J 0.096 J 0.098 J 0.097 J 0.080 JNotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021).2) Range of background metals for soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Ref. A. North Carolina soils, B. Southeastern US soils, C. Soils of the conterminous USA3) Trivalent chromium concentrations were calculated as the difference between total chromium and hexavalent chromium concentrations.Sample depth corresponds to depth of grab samples for VOC analysis; all other analyses associated with composite samples. With the exception of metals, only analytes with concentrations above the laboratory method detection limit are shown.Laboratory analytical methods are shown in parentheses.Bold and grey shading values exceed Industrial/Commercial PSRGs.mg/kg = milligrams per kilogram; VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act; ft bgs= feet below ground surface; NE = Not Established; -- = Not Applicable; < = Less than Laboratory Method Detection Limit; BDL = Below Detection Limit.J = compound was detected above the laboratory method detection limit but below the laboratory reporting limit resulting in an estimated concentration. Residential PSRGs (1)ALL BDLSample IDIndustrial/ Commercial PSRGs (1)Site-Specific Background LevelsBS-6 BS-7BS-2BKG-1 BKG-2 Regional Background Metals in Soil(2)BS-1 BS-3 BS-4 BS-5Protection of Groundwater PSRGs (1)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Dynamic Machining x Manufacturing (DMM)/Import Soil Sampling 07_2021/Tables/Import Table.xlsx7/23/2021Table 1 (Page 1 of 1)Hart & Hickman, PC
STOKES COUNTY PIN:
6901391053.000PEACHTREE LANEBS-7-3
BS-6BS-5
BS-1BS-2
BS-3
BS-4
BS-7-4
BS-7-1
BS-7-2
REVISION NO. 0
JOB NO. DMM-001
DATE: 6-30-21
APPENDIX: 1
LEGEND
BORROW SOURCE PROPERTY BOUNDARY
PARCEL LINE
COMPOSITE HORIZONTAL SOIL BORING
LOCATION
COMPOSITE VERTICAL SOIL BORING
LOCATION
APPROXIMATE EXTENT OF SOIL PROPOSED
FOR EXPORT
3921 Sunset Ridge Road, Suite 301
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
License # C-1269 / #C-245 Geology
NOTES:
1. AERIAL IMAGERY OBTAINED FROM GOOGLE EARTH PRO
SERVICES.
2. BASE DATA OBTAINED FROM STOKES COUNTY GIS (2018).
3. HORIZONTAL COMPOSITE SAMPLES COMPRISED OF
ALIQUOTS COLLECTED AT A DEPTH OF APPROXIMATELY
3 FEET BELOW GROUND SURFACE (FT BGS).
4. VERTICAL COMPOSITE SAMPLES COMPRISED OF
ALIQUOTS COLLECTED AT A DEPTHS OF
APPROXIMATELY 3, 6, 9, AND 12 FEET BELOW GROUND
SURFACE (FT BGS)
BORROW SOURCE SAMPLE
LOCATION MAP
CAROLINA MEDICAL ELECTRONICS
157 INDUSTRIAL DRIVE
KINGS, NORTH CAROLINA
S:\AAA-Master Projects\Dynamic Machining x Manufacturing (DMM)\Drawings\Figures_20210630.dwg, APP-D1, 7/23/2021 7:55:46 AM, shaynes
US H
IGHW
AY

5
2
INDU
STR
I
A
L
DR
I
VE
SG-1
SG-2
SG-3
MW-1
MW-1D/1D-5
MW-2
MW-3
MW-4
MW-6
MW-8
MW-7
MW-5
MW-9
MW-10
B-1
B-2
B-4
B-3
BKG-1-1
BKG-1-3
BKG-1-4
BKG-1-2
BKG-2-4
BKG-2-3
BKG-2-2
BKG-2-1
REVISION NO. 0
JOB NO. DMM-001
REDEVELOPMENT PLAN WITH
SAMPLING LOCATIONS
3921 Sunset Ridge Road, Suite 301
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
License # C-1269 / #C-245 Geology
NOTES:
1. AERIAL IMAGERY OBTAINED FROM NC ONEMAP SERVICES
(2018).
2. SUBJECT PARCEL DATA OBTAINED FROM SURVEY PLAT
DATED 5/24/2012. OTHER BASE DATA OBTAINED FROM
STOKES COUNTY GIS (2018).
3. SOIL BORING AND MONITORING WELL LOCATIONS
APPROXIMATED FROM FIGURES INCLUDED IN MINERAL
SPRINGS ENVIRONMENTAL, P.C.'S FEBRUARY 22, 2010
COMPREHENSIVE SITE ASSESSMENT REPORT AND
SEPTEMBER 13, 2010 COMPREHENSIVE SITE ASSESSMENT
REPORT ADDENDUM.
4. SUB-SLAB VAPOR SAMPLE LOCATIONS APPROXIMATED FROM
FIGURES INCLUDED IN BY ECS CAROLINAS, LLP'S APRIL 26,
2012 REPORT OF SUB-SLAB GAS SAMPLING.
5. HORIZONTAL COMPOSITE BACKGROUND SOIL SAMPLES
COMPRISED OF ALIQUOTS COLLECTED AT A DEPTH OF
APPROXIMATELY 3 FEET BELOW GROUND SURFACE (FT BGS).
DATE: 7-21-21
FIGURE NO. 2
CAROLINA MEDICAL ELECTRONICS
157 INDUSTRIAL DRIVE
KINGS, NORTH CAROLINA
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
FUTURE BUILDING
MONITORING WELL LOCATION
DEEP MONITORING WELL LOCATION
SOIL BORING LOCATION
SUB-SLAB VAPOR SAMPLE LOCATION
BACKGROUND HORIZONTAL
COMPOSITE SOIL SAMPLE LOCATION
FORMER 100-GALLON
HOLDING TANK
FORMER 200-GALLON
SEPTIC TANK
POTENTIAL FUTURE EXPANSION AREA - NOT
PART OF CURRENT REDEVELOPMENT PLANS
S:\AAA-Master Projects\Dynamic Machining x Manufacturing (DMM)\Drawings\Figures_20210630.dwg, FIG3, 7/23/2021 7:35:26 AM, shaynes
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
July 21, 2021
Justin Ballard
Hart & Hickman - Raleigh, NC
3921 Sunset Ridge Rd., Suite 301
Raleigh, NC 27607
Project Location: King, NC
Client Job Number:
Project Number: DMM-001
Laboratory Work Order Number: 21G0326
Enclosed are results of analyses for samples received by the laboratory on July 7, 2021. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 118
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 6
Sample Results 10
21G0326-01 10
21G0326-02 17
21G0326-03 24
21G0326-04 31
21G0326-05 38
21G0326-06 45
21G0326-07 52
21G0326-08 59
21G0326-09 66
21G0326-10 69
Sample Preparation Information 72
QC Data 74
Volatile Organic Compounds by GC/MS 74
B285629 74
Semivolatile Organic Compounds by GC/MS 79
B285556 79
Metals Analyses (Total) 84
B285620 84
B285624 85
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 86
B285670 86
Flag/Qualifier Summary 87
Page 2 of 118
Table of Contents
Table of Contents (continued)
Certifications 88
Chain of Custody/Sample Receipt 94
Page 3 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
7/21/2021
Hart & Hickman - Raleigh, NC
3921 Sunset Ridge Rd., Suite 301
Raleigh, NC 27607
ATTN: Justin Ballard
DMM-001
21G0326
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
King, NC
BS-1 21G0326-01 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D-E
BS-2 21G0326-02 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D-E
BS-3 21G0326-03 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D-E
BS-4 21G0326-04 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D-E
BS-5 21G0326-05 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D-E
[TOC_1]Sample Summary[TOC]
Page 4 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
7/21/2021
Hart & Hickman - Raleigh, NC
3921 Sunset Ridge Rd., Suite 301
Raleigh, NC 27607
ATTN: Justin Ballard
DMM-001
21G0326
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
King, NC
BS-6 21G0326-06 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D-E
BS-7 21G0326-07 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D-E
BS-DUP 21G0326-08 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D-E
BKG-1 21G0326-09 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
BKG-2 21G0326-10 Soil 7199 CT PH-0197/NY11742
SM 2540G
SW-846 CT PH-0197/NY11742
SW-846 6020B
SW-846 7471B
Page 5 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
Page 6 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SW-846 6020B
Qualifications:
Matrix spike recovery is outside of control limits. Analysis is in control based on laboratory fortified blank recovery.Possibility of sample
matrix effects that lead to low bias for reported result or non-homogeneous sample aliquot cannot be eliminated.
Analyte & Samples(s) Qualified:
MS-07
Arsenic
21G0326-05[BS-5], B285620-MS1
Selenium
21G0326-05[BS-5], B285620-MS1
Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in the sample. Appropriate or
meaningful recoveries cannot be calculated.
Analyte & Samples(s) Qualified:
MS-19
Barium
21G0326-05[BS-5], B285620-MS1
SW-846 8260D
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Carbon Disulfide
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1
Trichlorofluoromethane (Freon 11)
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
1,1,2-Trichloro-1,2,2-trifluoroethane (F
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1, S061374-CCV1
1,1-Dichloroethylene
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1, S061374-CCV1
Acetone
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1, S061374-CCV1
Carbon Disulfide
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1, S061374-CCV1
Chloroethane
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1, S061374-CCV1
Diethyl Ether
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1, S061374-CCV1
tert-Butyl Alcohol (TBA)
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1, S061374-CCV1
Trichlorofluoromethane (Freon 11)
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285629-BLK1, B285629-BS1, B285629-BSD1, S061374-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Tetrachloroethylene
B285629-BS1, B285629-BSD1, S061374-CCV1
Page 7 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-36
Hexachlorobutadiene
B285629-BS1, B285629-BSD1, S061374-CCV1
SW-846 8270D-E
Qualifications:
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.Analyte & Samples(s) Qualified:
V-04
Benzidine
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285556-BLK1, B285556-BS1, B285556-BSD1, S061419-CCV1, S061498-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Aniline
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285556-BLK1, B285556-BS1, B285556-BSD1, S061419-CCV1, S061498-CCV1
Benzidine
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285556-BLK1, B285556-BS1, B285556-BSD1, S061419-CCV1, S061498-CCV1
Hexachlorocyclopentadiene
21G0326-08[BS-DUP], S061498-CCV1
Pentachlorophenol
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285556-BLK1, B285556-BS1, B285556-BSD1, S061419-CCV1, S061498-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
V-06
4,6-Dinitro-2-methylphenol
B285556-BS1, B285556-BSD1, S061419-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.Analyte & Samples(s) Qualified:
V-20
4,6-Dinitro-2-methylphenol
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], B285556-BLK1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
4-Chloroaniline
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285556-BLK1, B285556-BS1, B285556-BSD1, S061419-CCV1, S061498-CCV1
Benzidine
21G0326-01[BS-1], 21G0326-02[BS-2], 21G0326-03[BS-3], 21G0326-04[BS-4], 21G0326-05[BS-5], 21G0326-06[BS-6], 21G0326-07[BS-7], 21G0326-08[BS-DUP],
B285556-BLK1, B285556-BS1, B285556-BSD1, S061419-CCV1, S061498-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-35
Benzidine
B285556-BS1
Page 8 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 9 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-01
Field Sample #: BS-1
Sample Matrix: Soil
Sampled: 7/7/2021 12:36
[TOC_2]21G0326-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 7/9/21 7:50 MFFmg/Kg dry0.012 7/9/21SW-846 8260D1V-05Acetone
ND 0.0077 7/9/21 7:50 MFFmg/Kg dry0.0012 7/9/21SW-846 8260D1Acrylonitrile
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1Benzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1Bromobenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.0013 7/9/21SW-846 8260D1Bromochloromethane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1Bromodichloromethane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D1Bromoform
ND 0.013 7/9/21 7:50 MFFmg/Kg dry0.0017 7/9/21SW-846 8260D1Bromomethane
ND 0.051 7/9/21 7:50 MFFmg/Kg dry0.0081 7/9/21SW-846 8260D12-Butanone (MEK)
ND 0.13 7/9/21 7:50 MFFmg/Kg dry0.077 7/9/21SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1n-Butylbenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D1sec-Butylbenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D1tert-Butylbenzene
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0077 7/9/21 7:50 MFFmg/Kg dry0.0050 7/9/21SW-846 8260D1V-05, L-04Carbon Disulfide
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1Carbon Tetrachloride
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1Chlorobenzene
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1Chlorodibromomethane
ND 0.026 7/9/21 7:50 MFFmg/Kg dry0.0017 7/9/21SW-846 8260D1V-05Chloroethane
ND 0.0051 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D1Chloroform
ND 0.013 7/9/21 7:50 MFFmg/Kg dry0.0010 7/9/21SW-846 8260D1Chloromethane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D12-Chlorotoluene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D14-Chlorotoluene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.0022 7/9/21SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D1Dibromomethane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D11,2-Dichlorobenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D11,3-Dichlorobenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D11,4-Dichlorobenzene
ND 0.0051 7/9/21 7:50 MFFmg/Kg dry0.0010 7/9/21SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.026 7/9/21 7:50 MFFmg/Kg dry0.0010 7/9/21SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D11,1-Dichloroethane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D11,2-Dichloroethane
ND 0.0051 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1V-051,1-Dichloroethylene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D11,2-Dichloropropane
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D11,3-Dichloropropane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D12,2-Dichloropropane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00090 7/9/21SW-846 8260D11,1-Dichloropropene
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D1trans-1,3-Dichloropropene
ND 0.026 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D1V-05Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 10 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-01
Field Sample #: BS-1
Sample Matrix: Soil
Sampled: 7/7/2021 12:36
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.13 7/9/21 7:50 MFFmg/Kg dry0.024 7/9/21SW-846 8260D11,4-Dioxane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1Ethylbenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D1Hexachlorobutadiene
ND 0.026 7/9/21 7:50 MFFmg/Kg dry0.0087 7/9/21SW-846 8260D12-Hexanone (MBK)
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0051 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.026 7/9/21 7:50 MFFmg/Kg dry0.0028 7/9/21SW-846 8260D1Methylene Chloride
ND 0.026 7/9/21 7:50 MFFmg/Kg dry0.0059 7/9/21SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0051 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D1Naphthalene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1n-Propylbenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D1Styrene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0013 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1Tetrachloroethylene
ND 0.013 7/9/21 7:50 MFFmg/Kg dry0.0031 7/9/21SW-846 8260D1Tetrahydrofuran
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00026 7/9/21SW-846 8260D1Toluene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00064 7/9/21SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D11,1,1-Trichloroethane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D11,1,2-Trichloroethane
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1Trichloroethylene
ND 0.013 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1V-05, L-04Trichlorofluoromethane (Freon 11)
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.0013 7/9/21SW-846 8260D11,2,3-Trichloropropane
ND 0.013 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D1V-051,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00038 7/9/21SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00026 7/9/21SW-846 8260D11,3,5-Trimethylbenzene
ND 0.013 7/9/21 7:50 MFFmg/Kg dry0.00051 7/9/21SW-846 8260D1Vinyl Chloride
ND 0.0051 7/9/21 7:50 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D1m+p Xylene
ND 0.0026 7/9/21 7:50 MFFmg/Kg dry0.00026 7/9/21SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 103 7/9/21 7:5070-130
Toluene-d8 101 7/9/21 7:5070-130
4-Bromofluorobenzene 102 7/9/21 7:5070-130
Page 11 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-01
Field Sample #: BS-1
Sample Matrix: Soil
Sampled: 7/7/2021 12:36
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Acenaphthene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Acenaphthylene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1Acetophenone
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.092 7/8/21SW-846 8270D-E1V-05Aniline
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Anthracene
ND 0.86 7/12/21 14:13 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E1V-04, V-05, V-34Benzidine
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Benzo(a)anthracene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Benzo(a)pyrene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Benzo(b)fluoranthene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.093 7/8/21SW-846 8270D-E1Benzo(g,h,i)perylene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1Benzo(k)fluoranthene
ND 1.3 7/12/21 14:13 IMRmg/Kg dry0.53 7/8/21SW-846 8270D-E1Benzoic Acid
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E1Bis(2-chloroethoxy)methane
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E1Bis(2-chloroethyl)ether
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Bis(2-chloroisopropyl)ether
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Bis(2-Ethylhexyl)phthalate
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.056 7/8/21SW-846 8270D-E14-Bromophenylphenylether
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Butylbenzylphthalate
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Carbazole
ND 0.86 7/12/21 14:13 IMRmg/Kg dry0.059 7/8/21SW-846 8270D-E1V-344-Chloroaniline
ND 0.86 7/12/21 14:13 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E14-Chloro-3-methylphenol
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.051 7/8/21SW-846 8270D-E12-Chloronaphthalene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E12-Chlorophenol
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E14-Chlorophenylphenylether
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Chrysene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.090 7/8/21SW-846 8270D-E1Dibenz(a,h)anthracene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Dibenzofuran
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Di-n-butylphthalate
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.050 7/8/21SW-846 8270D-E11,2-Dichlorobenzene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.049 7/8/21SW-846 8270D-E11,3-Dichlorobenzene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.046 7/8/21SW-846 8270D-E11,4-Dichlorobenzene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E13,3-Dichlorobenzidine
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E12,4-Dichlorophenol
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Diethylphthalate
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.12 7/8/21SW-846 8270D-E12,4-Dimethylphenol
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Dimethylphthalate
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.30 7/8/21SW-846 8270D-E1V-204,6-Dinitro-2-methylphenol
ND 0.86 7/12/21 14:13 IMRmg/Kg dry0.38 7/8/21SW-846 8270D-E12,4-Dinitrophenol
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.086 7/8/21SW-846 8270D-E12,4-Dinitrotoluene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E12,6-Dinitrotoluene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.16 7/8/21SW-846 8270D-E1Di-n-octylphthalate
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E11,2-Diphenylhydrazine/Azobenzene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Fluoranthene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Fluorene
Page 12 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-01
Field Sample #: BS-1
Sample Matrix: Soil
Sampled: 7/7/2021 12:36
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1Hexachlorobenzene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.056 7/8/21SW-846 8270D-E1Hexachlorobutadiene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.18 7/8/21SW-846 8270D-E1Hexachlorocyclopentadiene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.053 7/8/21SW-846 8270D-E1Hexachloroethane
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Indeno(1,2,3-cd)pyrene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Isophorone
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E11-Methylnaphthalene
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E12-Methylnaphthalene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.082 7/8/21SW-846 8270D-E12-Methylphenol
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E13/4-Methylphenol
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1Naphthalene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.094 7/8/21SW-846 8270D-E12-Nitroaniline
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E13-Nitroaniline
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.095 7/8/21SW-846 8270D-E14-Nitroaniline
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Nitrobenzene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E12-Nitrophenol
ND 0.86 7/12/21 14:13 IMRmg/Kg dry0.18 7/8/21SW-846 8270D-E14-Nitrophenol
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1N-Nitrosodimethylamine
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E1N-Nitrosodi-n-propylamine
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Pentachloronitrobenzene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E1V-05Pentachlorophenol
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Phenanthrene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Phenol
ND 0.22 7/12/21 14:13 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Pyrene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.045 7/8/21SW-846 8270D-E1Pyridine
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E11,2,4,5-Tetrachlorobenzene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.056 7/8/21SW-846 8270D-E11,2,4-Trichlorobenzene
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.44 7/12/21 14:13 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 63.9 7/12/21 14:1330-130
Phenol-d6 83.9 7/12/21 14:1330-130
Nitrobenzene-d5 76.8 7/12/21 14:1330-130
2-Fluorobiphenyl 72.5 7/12/21 14:1330-130
2,4,6-Tribromophenol 74.0 7/12/21 14:1330-130
p-Terphenyl-d14 94.3 7/12/21 14:1330-130
Page 13 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-01
Field Sample #: BS-1
Sample Matrix: Soil
Sampled: 7/7/2021 12:36
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.30 0.21 7/12/21 14:17 QNWmg/Kg dry0.037 7/9/21SW-846 6020B5Arsenic
49 5.3 7/12/21 15:13 QNWmg/Kg dry0.32 7/9/21SW-846 6020B5Chromium
63 2.1 7/12/21 15:13 QNWmg/Kg dry0.098 7/9/21SW-846 6020B5Lead
0.031 0.034 7/12/21 11:33 CJVmg/Kg dry0.012 7/9/21SW-846 7471B1JMercury
ND 1.7 7/12/21 15:13 QNWmg/Kg dry0.052 7/9/21SW-846 6020B5Selenium
0.10 0.11 7/12/21 15:13 QNWmg/Kg dry0.0030 7/9/21SW-846 6020B5JSilver
560 110 7/12/21 16:03 QNWmg/Kg dry 7/9/21SW-846 6020B50Barium
0.28 0.43 7/12/21 15:13 QNWmg/Kg dry0.0081 7/9/21SW-846 6020B5JCadmium
Page 14 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-01
Field Sample #: BS-1
Sample Matrix: Soil
Sampled: 7/7/2021 12:36
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
76.8 7/12/21 12:45 GLH% Wt 7/9/21SM 2540G1% Solids
Page 15 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-01
Field Sample #: BS-1
Sample Matrix: Soil
Sampled: 7/7/2021 12:36
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
0.713 - J 1.28 7/16/21 17:16 PTNmg/Kg0.325 7/16/2171991Hexavalent Chromium
Page 16 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-02
Field Sample #: BS-2
Sample Matrix: Soil
Sampled: 7/7/2021 12:24
[TOC_2]21G0326-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.14 7/9/21 8:19 MFFmg/Kg dry0.013 7/9/21SW-846 8260D1V-05Acetone
ND 0.0085 7/9/21 8:19 MFFmg/Kg dry0.0013 7/9/21SW-846 8260D1Acrylonitrile
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1Benzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1Bromobenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.0014 7/9/21SW-846 8260D1Bromochloromethane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1Bromodichloromethane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D1Bromoform
ND 0.014 7/9/21 8:19 MFFmg/Kg dry0.0018 7/9/21SW-846 8260D1Bromomethane
ND 0.057 7/9/21 8:19 MFFmg/Kg dry0.0089 7/9/21SW-846 8260D12-Butanone (MEK)
ND 0.14 7/9/21 8:19 MFFmg/Kg dry0.085 7/9/21SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1n-Butylbenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D1sec-Butylbenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D1tert-Butylbenzene
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0085 7/9/21 8:19 MFFmg/Kg dry0.0055 7/9/21SW-846 8260D1V-05, L-04Carbon Disulfide
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1Carbon Tetrachloride
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1Chlorobenzene
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1Chlorodibromomethane
ND 0.028 7/9/21 8:19 MFFmg/Kg dry0.0018 7/9/21SW-846 8260D1V-05Chloroethane
ND 0.0057 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D1Chloroform
ND 0.014 7/9/21 8:19 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Chloromethane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D12-Chlorotoluene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D14-Chlorotoluene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.0024 7/9/21SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D1Dibromomethane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D11,2-Dichlorobenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D11,3-Dichlorobenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D11,4-Dichlorobenzene
ND 0.0057 7/9/21 8:19 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.028 7/9/21 8:19 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D11,1-Dichloroethane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D11,2-Dichloroethane
ND 0.0057 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1V-051,1-Dichloroethylene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D11,2-Dichloropropane
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D11,3-Dichloropropane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D12,2-Dichloropropane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00099 7/9/21SW-846 8260D11,1-Dichloropropene
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D1trans-1,3-Dichloropropene
ND 0.028 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D1V-05Diethyl Ether
Page 17 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-02
Field Sample #: BS-2
Sample Matrix: Soil
Sampled: 7/7/2021 12:24
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.14 7/9/21 8:19 MFFmg/Kg dry0.026 7/9/21SW-846 8260D11,4-Dioxane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1Ethylbenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D1Hexachlorobutadiene
ND 0.028 7/9/21 8:19 MFFmg/Kg dry0.0096 7/9/21SW-846 8260D12-Hexanone (MBK)
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0057 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.028 7/9/21 8:19 MFFmg/Kg dry0.0031 7/9/21SW-846 8260D1Methylene Chloride
ND 0.028 7/9/21 8:19 MFFmg/Kg dry0.0065 7/9/21SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0057 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D1Naphthalene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1n-Propylbenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D1Styrene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0014 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1Tetrachloroethylene
ND 0.014 7/9/21 8:19 MFFmg/Kg dry0.0034 7/9/21SW-846 8260D1Tetrahydrofuran
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00028 7/9/21SW-846 8260D1Toluene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00071 7/9/21SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D11,1,1-Trichloroethane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D11,1,2-Trichloroethane
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1Trichloroethylene
ND 0.014 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1L-04, V-05Trichlorofluoromethane (Freon 11)
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.0014 7/9/21SW-846 8260D11,2,3-Trichloropropane
ND 0.014 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D1V-051,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00042 7/9/21SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00028 7/9/21SW-846 8260D11,3,5-Trimethylbenzene
ND 0.014 7/9/21 8:19 MFFmg/Kg dry0.00057 7/9/21SW-846 8260D1Vinyl Chloride
ND 0.0057 7/9/21 8:19 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D1m+p Xylene
ND 0.0028 7/9/21 8:19 MFFmg/Kg dry0.00028 7/9/21SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 100 7/9/21 8:1970-130
Toluene-d8 105 7/9/21 8:1970-130
4-Bromofluorobenzene 100 7/9/21 8:1970-130
Page 18 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-02
Field Sample #: BS-2
Sample Matrix: Soil
Sampled: 7/7/2021 12:24
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Acenaphthene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Acenaphthylene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Acetophenone
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.095 7/8/21SW-846 8270D-E1V-05Aniline
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Anthracene
ND 0.88 7/12/21 14:40 IMRmg/Kg dry0.21 7/8/21SW-846 8270D-E1V-04, V-05, V-34Benzidine
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Benzo(a)anthracene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Benzo(a)pyrene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Benzo(b)fluoranthene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.095 7/8/21SW-846 8270D-E1Benzo(g,h,i)perylene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Benzo(k)fluoranthene
ND 1.3 7/12/21 14:40 IMRmg/Kg dry0.54 7/8/21SW-846 8270D-E1Benzoic Acid
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.059 7/8/21SW-846 8270D-E1Bis(2-chloroethoxy)methane
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Bis(2-chloroethyl)ether
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Bis(2-chloroisopropyl)ether
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Bis(2-Ethylhexyl)phthalate
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E14-Bromophenylphenylether
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Butylbenzylphthalate
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Carbazole
ND 0.88 7/12/21 14:40 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1V-344-Chloroaniline
ND 0.88 7/12/21 14:40 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E14-Chloro-3-methylphenol
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.053 7/8/21SW-846 8270D-E12-Chloronaphthalene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E12-Chlorophenol
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E14-Chlorophenylphenylether
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Chrysene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.092 7/8/21SW-846 8270D-E1Dibenz(a,h)anthracene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Dibenzofuran
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Di-n-butylphthalate
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.052 7/8/21SW-846 8270D-E11,2-Dichlorobenzene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.050 7/8/21SW-846 8270D-E11,3-Dichlorobenzene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.048 7/8/21SW-846 8270D-E11,4-Dichlorobenzene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E13,3-Dichlorobenzidine
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E12,4-Dichlorophenol
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Diethylphthalate
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.12 7/8/21SW-846 8270D-E12,4-Dimethylphenol
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Dimethylphthalate
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.31 7/8/21SW-846 8270D-E1V-204,6-Dinitro-2-methylphenol
ND 0.88 7/12/21 14:40 IMRmg/Kg dry0.39 7/8/21SW-846 8270D-E12,4-Dinitrophenol
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.089 7/8/21SW-846 8270D-E12,4-Dinitrotoluene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E12,6-Dinitrotoluene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.16 7/8/21SW-846 8270D-E1Di-n-octylphthalate
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E11,2-Diphenylhydrazine/Azobenzene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Fluoranthene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Fluorene
Page 19 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-02
Field Sample #: BS-2
Sample Matrix: Soil
Sampled: 7/7/2021 12:24
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Hexachlorobenzene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E1Hexachlorobutadiene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E1Hexachlorocyclopentadiene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.054 7/8/21SW-846 8270D-E1Hexachloroethane
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Indeno(1,2,3-cd)pyrene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Isophorone
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E11-Methylnaphthalene
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E12-Methylnaphthalene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.084 7/8/21SW-846 8270D-E12-Methylphenol
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E13/4-Methylphenol
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Naphthalene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.097 7/8/21SW-846 8270D-E12-Nitroaniline
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E13-Nitroaniline
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.098 7/8/21SW-846 8270D-E14-Nitroaniline
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Nitrobenzene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E12-Nitrophenol
ND 0.88 7/12/21 14:40 IMRmg/Kg dry0.18 7/8/21SW-846 8270D-E14-Nitrophenol
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1N-Nitrosodimethylamine
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1N-Nitrosodi-n-propylamine
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Pentachloronitrobenzene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E1V-05Pentachlorophenol
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Phenanthrene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Phenol
ND 0.23 7/12/21 14:40 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Pyrene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.046 7/8/21SW-846 8270D-E1Pyridine
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.059 7/8/21SW-846 8270D-E11,2,4,5-Tetrachlorobenzene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.057 7/8/21SW-846 8270D-E11,2,4-Trichlorobenzene
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.45 7/12/21 14:40 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 63.4 7/12/21 14:4030-130
Phenol-d6 84.2 7/12/21 14:4030-130
Nitrobenzene-d5 76.4 7/12/21 14:4030-130
2-Fluorobiphenyl 76.0 7/12/21 14:4030-130
2,4,6-Tribromophenol 76.5 7/12/21 14:4030-130
p-Terphenyl-d14 94.4 7/12/21 14:4030-130
Page 20 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-02
Field Sample #: BS-2
Sample Matrix: Soil
Sampled: 7/7/2021 12:24
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.81 0.22 7/12/21 14:20 QNWmg/Kg dry0.037 7/9/21SW-846 6020B5Arsenic
48 5.4 7/12/21 15:16 QNWmg/Kg dry0.33 7/9/21SW-846 6020B5Chromium
31 2.2 7/12/21 15:16 QNWmg/Kg dry0.10 7/9/21SW-846 6020B5Lead
0.030 0.034 7/12/21 11:35 CJVmg/Kg dry0.012 7/9/21SW-846 7471B1JMercury
ND 1.7 7/12/21 15:16 QNWmg/Kg dry0.054 7/9/21SW-846 6020B5Selenium
0.079 0.11 7/12/21 15:16 QNWmg/Kg dry0.0030 7/9/21SW-846 6020B5JSilver
230 11 7/12/21 15:16 QNWmg/Kg dry 7/9/21SW-846 6020B5Barium
0.024 0.44 7/12/21 15:16 QNWmg/Kg dry0.0083 7/9/21SW-846 6020B5JCadmium
Page 21 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-02
Field Sample #: BS-2
Sample Matrix: Soil
Sampled: 7/7/2021 12:24
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
74.8 7/12/21 12:45 GLH% Wt 7/9/21SM 2540G1% Solids
Page 22 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-02
Field Sample #: BS-2
Sample Matrix: Soil
Sampled: 7/7/2021 12:24
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
0.940 - J 1.32 7/16/21 17:24 PTNmg/Kg0.337 7/16/2171991Hexavalent Chromium
Page 23 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-03
Field Sample #: BS-3
Sample Matrix: Soil
Sampled: 7/7/2021 12:16
[TOC_2]21G0326-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.032 0.11 7/9/21 8:47 MFFmg/Kg dry0.010 7/9/21SW-846 8260D1V-05, JAcetone
ND 0.0066 7/9/21 8:47 MFFmg/Kg dry0.00099 7/9/21SW-846 8260D1Acrylonitrile
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1Benzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1Bromobenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Bromochloromethane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1Bromodichloromethane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1Bromoform
ND 0.011 7/9/21 8:47 MFFmg/Kg dry0.0014 7/9/21SW-846 8260D1Bromomethane
ND 0.044 7/9/21 8:47 MFFmg/Kg dry0.0069 7/9/21SW-846 8260D12-Butanone (MEK)
ND 0.11 7/9/21 8:47 MFFmg/Kg dry0.066 7/9/21SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1n-Butylbenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1sec-Butylbenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1tert-Butylbenzene
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0066 7/9/21 8:47 MFFmg/Kg dry0.0043 7/9/21SW-846 8260D1L-04, V-05Carbon Disulfide
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1Carbon Tetrachloride
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1Chlorobenzene
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1Chlorodibromomethane
ND 0.022 7/9/21 8:47 MFFmg/Kg dry0.0014 7/9/21SW-846 8260D1V-05Chloroethane
ND 0.0044 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Chloroform
ND 0.011 7/9/21 8:47 MFFmg/Kg dry0.00088 7/9/21SW-846 8260D1Chloromethane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D12-Chlorotoluene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D14-Chlorotoluene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.0019 7/9/21SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Dibromomethane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D11,2-Dichlorobenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D11,3-Dichlorobenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D11,4-Dichlorobenzene
ND 0.0044 7/9/21 8:47 MFFmg/Kg dry0.00088 7/9/21SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.022 7/9/21 8:47 MFFmg/Kg dry0.00088 7/9/21SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D11,1-Dichloroethane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,2-Dichloroethane
ND 0.0044 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1V-051,1-Dichloroethylene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D11,2-Dichloropropane
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,3-Dichloropropane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D12,2-Dichloropropane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00077 7/9/21SW-846 8260D11,1-Dichloropropene
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1trans-1,3-Dichloropropene
ND 0.022 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1V-05Diethyl Ether
Page 24 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-03
Field Sample #: BS-3
Sample Matrix: Soil
Sampled: 7/7/2021 12:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.11 7/9/21 8:47 MFFmg/Kg dry0.020 7/9/21SW-846 8260D11,4-Dioxane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1Ethylbenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1Hexachlorobutadiene
ND 0.022 7/9/21 8:47 MFFmg/Kg dry0.0075 7/9/21SW-846 8260D12-Hexanone (MBK)
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0044 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.022 7/9/21 8:47 MFFmg/Kg dry0.0024 7/9/21SW-846 8260D1Methylene Chloride
ND 0.022 7/9/21 8:47 MFFmg/Kg dry0.0050 7/9/21SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0044 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1Naphthalene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1n-Propylbenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D1Styrene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0011 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1Tetrachloroethylene
ND 0.011 7/9/21 8:47 MFFmg/Kg dry0.0026 7/9/21SW-846 8260D1Tetrahydrofuran
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00022 7/9/21SW-846 8260D1Toluene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D11,1,1-Trichloroethane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D11,1,2-Trichloroethane
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1Trichloroethylene
ND 0.011 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1L-04, V-05Trichlorofluoromethane (Freon 11)
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D11,2,3-Trichloropropane
ND 0.011 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1V-051,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00033 7/9/21SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00022 7/9/21SW-846 8260D11,3,5-Trimethylbenzene
ND 0.011 7/9/21 8:47 MFFmg/Kg dry0.00044 7/9/21SW-846 8260D1Vinyl Chloride
ND 0.0044 7/9/21 8:47 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1m+p Xylene
ND 0.0022 7/9/21 8:47 MFFmg/Kg dry0.00022 7/9/21SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 114 7/9/21 8:4770-130
Toluene-d8 103 7/9/21 8:4770-130
4-Bromofluorobenzene 104 7/9/21 8:4770-130
Page 25 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-03
Field Sample #: BS-3
Sample Matrix: Soil
Sampled: 7/7/2021 12:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Acenaphthene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Acenaphthylene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Acetophenone
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.099 7/8/21SW-846 8270D-E1V-05Aniline
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Anthracene
ND 0.92 7/12/21 15:07 IMRmg/Kg dry0.22 7/8/21SW-846 8270D-E1V-04, V-05, V-34Benzidine
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Benzo(a)anthracene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Benzo(a)pyrene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Benzo(b)fluoranthene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.099 7/8/21SW-846 8270D-E1Benzo(g,h,i)perylene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Benzo(k)fluoranthene
ND 1.4 7/12/21 15:07 IMRmg/Kg dry0.56 7/8/21SW-846 8270D-E1Benzoic Acid
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Bis(2-chloroethoxy)methane
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Bis(2-chloroethyl)ether
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Bis(2-chloroisopropyl)ether
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Bis(2-Ethylhexyl)phthalate
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E14-Bromophenylphenylether
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Butylbenzylphthalate
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Carbazole
ND 0.92 7/12/21 15:07 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1V-344-Chloroaniline
ND 0.92 7/12/21 15:07 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E14-Chloro-3-methylphenol
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.055 7/8/21SW-846 8270D-E12-Chloronaphthalene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E12-Chlorophenol
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E14-Chlorophenylphenylether
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Chrysene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.096 7/8/21SW-846 8270D-E1Dibenz(a,h)anthracene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Dibenzofuran
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Di-n-butylphthalate
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.054 7/8/21SW-846 8270D-E11,2-Dichlorobenzene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.052 7/8/21SW-846 8270D-E11,3-Dichlorobenzene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.049 7/8/21SW-846 8270D-E11,4-Dichlorobenzene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E13,3-Dichlorobenzidine
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E12,4-Dichlorophenol
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Diethylphthalate
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.13 7/8/21SW-846 8270D-E12,4-Dimethylphenol
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Dimethylphthalate
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.32 7/8/21SW-846 8270D-E1V-204,6-Dinitro-2-methylphenol
ND 0.92 7/12/21 15:07 IMRmg/Kg dry0.41 7/8/21SW-846 8270D-E12,4-Dinitrophenol
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.092 7/8/21SW-846 8270D-E12,4-Dinitrotoluene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E12,6-Dinitrotoluene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.17 7/8/21SW-846 8270D-E1Di-n-octylphthalate
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E11,2-Diphenylhydrazine/Azobenzene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Fluoranthene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Fluorene
Page 26 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-03
Field Sample #: BS-3
Sample Matrix: Soil
Sampled: 7/7/2021 12:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Hexachlorobenzene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1Hexachlorobutadiene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E1Hexachlorocyclopentadiene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.056 7/8/21SW-846 8270D-E1Hexachloroethane
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Indeno(1,2,3-cd)pyrene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E1Isophorone
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E11-Methylnaphthalene
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E12-Methylnaphthalene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.088 7/8/21SW-846 8270D-E12-Methylphenol
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E13/4-Methylphenol
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Naphthalene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E12-Nitroaniline
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.081 7/8/21SW-846 8270D-E13-Nitroaniline
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E14-Nitroaniline
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Nitrobenzene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E12-Nitrophenol
ND 0.92 7/12/21 15:07 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E14-Nitrophenol
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1N-Nitrosodimethylamine
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1N-Nitrosodi-n-propylamine
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Pentachloronitrobenzene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.21 7/8/21SW-846 8270D-E1V-05Pentachlorophenol
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Phenanthrene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Phenol
ND 0.24 7/12/21 15:07 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Pyrene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.048 7/8/21SW-846 8270D-E1Pyridine
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E11,2,4,5-Tetrachlorobenzene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.059 7/8/21SW-846 8270D-E11,2,4-Trichlorobenzene
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.47 7/12/21 15:07 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 62.2 7/12/21 15:0730-130
Phenol-d6 81.5 7/12/21 15:0730-130
Nitrobenzene-d5 76.6 7/12/21 15:0730-130
2-Fluorobiphenyl 77.8 7/12/21 15:0730-130
2,4,6-Tribromophenol 81.4 7/12/21 15:0730-130
p-Terphenyl-d14 102 7/12/21 15:0730-130
Page 27 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-03
Field Sample #: BS-3
Sample Matrix: Soil
Sampled: 7/7/2021 12:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.84 0.23 7/12/21 14:28 QNWmg/Kg dry0.040 7/9/21SW-846 6020B5Arsenic
35 5.8 7/12/21 15:27 QNWmg/Kg dry0.35 7/9/21SW-846 6020B5Chromium
27 2.3 7/12/21 15:27 QNWmg/Kg dry0.11 7/9/21SW-846 6020B5Lead
0.038 0.040 7/12/21 11:37 CJVmg/Kg dry0.013 7/9/21SW-846 7471B1JMercury
ND 1.8 7/12/21 15:27 QNWmg/Kg dry0.057 7/9/21SW-846 6020B5Selenium
0.094 0.12 7/12/21 15:27 QNWmg/Kg dry0.0032 7/9/21SW-846 6020B5JSilver
230 12 7/12/21 15:27 QNWmg/Kg dry 7/9/21SW-846 6020B5Barium
0.032 0.46 7/12/21 15:27 QNWmg/Kg dry0.0087 7/9/21SW-846 6020B5JCadmium
Page 28 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-03
Field Sample #: BS-3
Sample Matrix: Soil
Sampled: 7/7/2021 12:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
71.8 7/12/21 12:45 GLH% Wt 7/9/21SM 2540G1% Solids
Page 29 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-03
Field Sample #: BS-3
Sample Matrix: Soil
Sampled: 7/7/2021 12:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
0.909 - J 1.4 7/16/21 17:29 PTNmg/Kg0.357 7/16/2171991Hexavalent Chromium
Page 30 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-04
Field Sample #: BS-4
Sample Matrix: Soil
Sampled: 7/7/2021 12:09
[TOC_2]21G0326-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.12 7/9/21 9:16 MFFmg/Kg dry0.011 7/9/21SW-846 8260D1V-05Acetone
ND 0.0072 7/9/21 9:16 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Acrylonitrile
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1Benzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1Bromobenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.0012 7/9/21SW-846 8260D1Bromochloromethane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1Bromodichloromethane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D1Bromoform
ND 0.012 7/9/21 9:16 MFFmg/Kg dry0.0016 7/9/21SW-846 8260D1Bromomethane
ND 0.048 7/9/21 9:16 MFFmg/Kg dry0.0075 7/9/21SW-846 8260D12-Butanone (MEK)
ND 0.12 7/9/21 9:16 MFFmg/Kg dry0.072 7/9/21SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1n-Butylbenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D1sec-Butylbenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D1tert-Butylbenzene
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0072 7/9/21 9:16 MFFmg/Kg dry0.0047 7/9/21SW-846 8260D1L-04, V-05Carbon Disulfide
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1Carbon Tetrachloride
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1Chlorobenzene
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1Chlorodibromomethane
ND 0.024 7/9/21 9:16 MFFmg/Kg dry0.0016 7/9/21SW-846 8260D1V-05Chloroethane
ND 0.0048 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D1Chloroform
ND 0.012 7/9/21 9:16 MFFmg/Kg dry0.00096 7/9/21SW-846 8260D1Chloromethane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D12-Chlorotoluene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D14-Chlorotoluene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.0020 7/9/21SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D1Dibromomethane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D11,2-Dichlorobenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D11,3-Dichlorobenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D11,4-Dichlorobenzene
ND 0.0048 7/9/21 9:16 MFFmg/Kg dry0.00096 7/9/21SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.024 7/9/21 9:16 MFFmg/Kg dry0.00096 7/9/21SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D11,1-Dichloroethane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D11,2-Dichloroethane
ND 0.0048 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1V-051,1-Dichloroethylene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D11,2-Dichloropropane
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D11,3-Dichloropropane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D12,2-Dichloropropane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00084 7/9/21SW-846 8260D11,1-Dichloropropene
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D1trans-1,3-Dichloropropene
ND 0.024 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D1V-05Diethyl Ether
Page 31 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-04
Field Sample #: BS-4
Sample Matrix: Soil
Sampled: 7/7/2021 12:09
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.12 7/9/21 9:16 MFFmg/Kg dry0.022 7/9/21SW-846 8260D11,4-Dioxane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1Ethylbenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D1Hexachlorobutadiene
ND 0.024 7/9/21 9:16 MFFmg/Kg dry0.0081 7/9/21SW-846 8260D12-Hexanone (MBK)
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0048 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.024 7/9/21 9:16 MFFmg/Kg dry0.0026 7/9/21SW-846 8260D1Methylene Chloride
ND 0.024 7/9/21 9:16 MFFmg/Kg dry0.0055 7/9/21SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0048 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D1Naphthalene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1n-Propylbenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D1Styrene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0012 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1Tetrachloroethylene
ND 0.012 7/9/21 9:16 MFFmg/Kg dry0.0029 7/9/21SW-846 8260D1Tetrahydrofuran
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00024 7/9/21SW-846 8260D1Toluene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00060 7/9/21SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D11,1,1-Trichloroethane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D11,1,2-Trichloroethane
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1Trichloroethylene
ND 0.012 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1L-04, V-05Trichlorofluoromethane (Freon 11)
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.0012 7/9/21SW-846 8260D11,2,3-Trichloropropane
ND 0.012 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D1V-051,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00036 7/9/21SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00024 7/9/21SW-846 8260D11,3,5-Trimethylbenzene
ND 0.012 7/9/21 9:16 MFFmg/Kg dry0.00048 7/9/21SW-846 8260D1Vinyl Chloride
ND 0.0048 7/9/21 9:16 MFFmg/Kg dry0.00072 7/9/21SW-846 8260D1m+p Xylene
ND 0.0024 7/9/21 9:16 MFFmg/Kg dry0.00024 7/9/21SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 104 7/9/21 9:1670-130
Toluene-d8 104 7/9/21 9:1670-130
4-Bromofluorobenzene 101 7/9/21 9:1670-130
Page 32 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-04
Field Sample #: BS-4
Sample Matrix: Soil
Sampled: 7/7/2021 12:09
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Acenaphthene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Acenaphthylene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Acetophenone
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.097 7/8/21SW-846 8270D-E1V-05Aniline
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Anthracene
ND 0.90 7/12/21 15:34 IMRmg/Kg dry0.21 7/8/21SW-846 8270D-E1V-04, V-05, V-34Benzidine
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Benzo(a)anthracene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Benzo(a)pyrene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Benzo(b)fluoranthene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.097 7/8/21SW-846 8270D-E1Benzo(g,h,i)perylene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Benzo(k)fluoranthene
ND 1.4 7/12/21 15:34 IMRmg/Kg dry0.55 7/8/21SW-846 8270D-E1Benzoic Acid
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1Bis(2-chloroethoxy)methane
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Bis(2-chloroethyl)ether
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Bis(2-chloroisopropyl)ether
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Bis(2-Ethylhexyl)phthalate
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.059 7/8/21SW-846 8270D-E14-Bromophenylphenylether
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Butylbenzylphthalate
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Carbazole
ND 0.90 7/12/21 15:34 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1V-344-Chloroaniline
ND 0.90 7/12/21 15:34 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E14-Chloro-3-methylphenol
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.054 7/8/21SW-846 8270D-E12-Chloronaphthalene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E12-Chlorophenol
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E14-Chlorophenylphenylether
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Chrysene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.094 7/8/21SW-846 8270D-E1Dibenz(a,h)anthracene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Dibenzofuran
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Di-n-butylphthalate
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.053 7/8/21SW-846 8270D-E11,2-Dichlorobenzene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.051 7/8/21SW-846 8270D-E11,3-Dichlorobenzene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.049 7/8/21SW-846 8270D-E11,4-Dichlorobenzene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E13,3-Dichlorobenzidine
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E12,4-Dichlorophenol
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Diethylphthalate
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.13 7/8/21SW-846 8270D-E12,4-Dimethylphenol
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Dimethylphthalate
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.31 7/8/21SW-846 8270D-E1V-204,6-Dinitro-2-methylphenol
ND 0.90 7/12/21 15:34 IMRmg/Kg dry0.40 7/8/21SW-846 8270D-E12,4-Dinitrophenol
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.091 7/8/21SW-846 8270D-E12,4-Dinitrotoluene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E12,6-Dinitrotoluene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.16 7/8/21SW-846 8270D-E1Di-n-octylphthalate
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E11,2-Diphenylhydrazine/Azobenzene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Fluoranthene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Fluorene
Page 33 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-04
Field Sample #: BS-4
Sample Matrix: Soil
Sampled: 7/7/2021 12:09
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Hexachlorobenzene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.059 7/8/21SW-846 8270D-E1Hexachlorobutadiene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E1Hexachlorocyclopentadiene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.055 7/8/21SW-846 8270D-E1Hexachloroethane
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Indeno(1,2,3-cd)pyrene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Isophorone
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E11-Methylnaphthalene
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E12-Methylnaphthalene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.086 7/8/21SW-846 8270D-E12-Methylphenol
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E13/4-Methylphenol
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Naphthalene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.099 7/8/21SW-846 8270D-E12-Nitroaniline
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E13-Nitroaniline
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E14-Nitroaniline
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Nitrobenzene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E12-Nitrophenol
ND 0.90 7/12/21 15:34 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E14-Nitrophenol
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1N-Nitrosodimethylamine
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1N-Nitrosodi-n-propylamine
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Pentachloronitrobenzene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E1V-05Pentachlorophenol
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Phenanthrene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Phenol
ND 0.23 7/12/21 15:34 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Pyrene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.047 7/8/21SW-846 8270D-E1Pyridine
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E11,2,4,5-Tetrachlorobenzene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E11,2,4-Trichlorobenzene
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.46 7/12/21 15:34 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 55.4 7/12/21 15:3430-130
Phenol-d6 75.0 7/12/21 15:3430-130
Nitrobenzene-d5 67.1 7/12/21 15:3430-130
2-Fluorobiphenyl 67.8 7/12/21 15:3430-130
2,4,6-Tribromophenol 75.6 7/12/21 15:3430-130
p-Terphenyl-d14 90.9 7/12/21 15:3430-130
Page 34 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-04
Field Sample #: BS-4
Sample Matrix: Soil
Sampled: 7/7/2021 12:09
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
2.1 0.22 7/12/21 14:31 QNWmg/Kg dry0.037 7/9/21SW-846 6020B5Arsenic
58 5.4 7/12/21 15:29 QNWmg/Kg dry0.33 7/9/21SW-846 6020B5Chromium
20 2.2 7/12/21 15:29 QNWmg/Kg dry0.10 7/9/21SW-846 6020B5Lead
0.079 0.041 7/12/21 11:38 CJVmg/Kg dry0.014 7/9/21SW-846 7471B1Mercury
ND 1.7 7/12/21 15:29 QNWmg/Kg dry0.053 7/9/21SW-846 6020B5Selenium
0.096 0.11 7/12/21 15:29 QNWmg/Kg dry0.0030 7/9/21SW-846 6020B5JSilver
110 11 7/12/21 15:29 QNWmg/Kg dry 7/9/21SW-846 6020B5Barium
ND 0.43 7/12/21 15:29 QNWmg/Kg dry0.0082 7/9/21SW-846 6020B5Cadmium
Page 35 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-04
Field Sample #: BS-4
Sample Matrix: Soil
Sampled: 7/7/2021 12:09
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
73.2 7/12/21 12:46 GLH% Wt 7/9/21SM 2540G1% Solids
Page 36 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-04
Field Sample #: BS-4
Sample Matrix: Soil
Sampled: 7/7/2021 12:09
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
1.08 - J 1.34 7/16/21 17:40 PTNmg/Kg0.342 7/16/2171991Hexavalent Chromium
Page 37 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-05
Field Sample #: BS-5
Sample Matrix: Soil
Sampled: 7/7/2021 12:00
[TOC_2]21G0326-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.027 0.14 7/9/21 9:44 MFFmg/Kg dry0.012 7/9/21SW-846 8260D1V-05, JAcetone
ND 0.0082 7/9/21 9:44 MFFmg/Kg dry0.0012 7/9/21SW-846 8260D1Acrylonitrile
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Benzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Bromobenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.0014 7/9/21SW-846 8260D1Bromochloromethane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Bromodichloromethane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1Bromoform
ND 0.014 7/9/21 9:44 MFFmg/Kg dry0.0018 7/9/21SW-846 8260D1Bromomethane
ND 0.055 7/9/21 9:44 MFFmg/Kg dry0.0086 7/9/21SW-846 8260D12-Butanone (MEK)
ND 0.14 7/9/21 9:44 MFFmg/Kg dry0.082 7/9/21SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1n-Butylbenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1sec-Butylbenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1tert-Butylbenzene
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0082 7/9/21 9:44 MFFmg/Kg dry0.0053 7/9/21SW-846 8260D1L-04, V-05Carbon Disulfide
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Carbon Tetrachloride
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Chlorobenzene
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Chlorodibromomethane
ND 0.027 7/9/21 9:44 MFFmg/Kg dry0.0018 7/9/21SW-846 8260D1V-05Chloroethane
ND 0.0055 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1Chloroform
ND 0.014 7/9/21 9:44 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Chloromethane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D12-Chlorotoluene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D14-Chlorotoluene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.0023 7/9/21SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1Dibromomethane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,2-Dichlorobenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,3-Dichlorobenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,4-Dichlorobenzene
ND 0.0055 7/9/21 9:44 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.027 7/9/21 9:44 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,1-Dichloroethane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D11,2-Dichloroethane
ND 0.0055 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1V-051,1-Dichloroethylene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,2-Dichloropropane
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D11,3-Dichloropropane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D12,2-Dichloropropane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00096 7/9/21SW-846 8260D11,1-Dichloropropene
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1trans-1,3-Dichloropropene
ND 0.027 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1V-05Diethyl Ether
Page 38 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-05
Field Sample #: BS-5
Sample Matrix: Soil
Sampled: 7/7/2021 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.14 7/9/21 9:44 MFFmg/Kg dry0.026 7/9/21SW-846 8260D11,4-Dioxane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Ethylbenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1Hexachlorobutadiene
ND 0.027 7/9/21 9:44 MFFmg/Kg dry0.0093 7/9/21SW-846 8260D12-Hexanone (MBK)
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0055 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.027 7/9/21 9:44 MFFmg/Kg dry0.0030 7/9/21SW-846 8260D1Methylene Chloride
ND 0.027 7/9/21 9:44 MFFmg/Kg dry0.0063 7/9/21SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0055 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1Naphthalene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1n-Propylbenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Styrene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0014 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Tetrachloroethylene
ND 0.014 7/9/21 9:44 MFFmg/Kg dry0.0033 7/9/21SW-846 8260D1Tetrahydrofuran
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00027 7/9/21SW-846 8260D1Toluene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,1,1-Trichloroethane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,1,2-Trichloroethane
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Trichloroethylene
ND 0.014 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1L-04, V-05Trichlorofluoromethane (Freon 11)
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.0014 7/9/21SW-846 8260D11,2,3-Trichloropropane
ND 0.014 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1V-051,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00027 7/9/21SW-846 8260D11,3,5-Trimethylbenzene
ND 0.014 7/9/21 9:44 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Vinyl Chloride
ND 0.0055 7/9/21 9:44 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1m+p Xylene
ND 0.0027 7/9/21 9:44 MFFmg/Kg dry0.00027 7/9/21SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 109 7/9/21 9:4470-130
Toluene-d8 104 7/9/21 9:4470-130
4-Bromofluorobenzene 104 7/9/21 9:4470-130
Page 39 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-05
Field Sample #: BS-5
Sample Matrix: Soil
Sampled: 7/7/2021 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Acenaphthene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Acenaphthylene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Acetophenone
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1V-05Aniline
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Anthracene
ND 0.95 7/12/21 16:00 IMRmg/Kg dry0.22 7/8/21SW-846 8270D-E1V-04, V-05, V-34Benzidine
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Benzo(a)anthracene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Benzo(a)pyrene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Benzo(b)fluoranthene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Benzo(g,h,i)perylene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Benzo(k)fluoranthene
ND 1.4 7/12/21 16:00 IMRmg/Kg dry0.58 7/8/21SW-846 8270D-E1Benzoic Acid
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Bis(2-chloroethoxy)methane
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Bis(2-chloroethyl)ether
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Bis(2-chloroisopropyl)ether
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.082 7/8/21SW-846 8270D-E1Bis(2-Ethylhexyl)phthalate
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E14-Bromophenylphenylether
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Butylbenzylphthalate
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Carbazole
ND 0.95 7/12/21 16:00 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1V-344-Chloroaniline
ND 0.95 7/12/21 16:00 IMRmg/Kg dry0.081 7/8/21SW-846 8270D-E14-Chloro-3-methylphenol
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.057 7/8/21SW-846 8270D-E12-Chloronaphthalene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E12-Chlorophenol
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E14-Chlorophenylphenylether
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Chrysene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.099 7/8/21SW-846 8270D-E1Dibenz(a,h)anthracene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Dibenzofuran
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Di-n-butylphthalate
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.056 7/8/21SW-846 8270D-E11,2-Dichlorobenzene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.053 7/8/21SW-846 8270D-E11,3-Dichlorobenzene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.051 7/8/21SW-846 8270D-E11,4-Dichlorobenzene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E13,3-Dichlorobenzidine
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E12,4-Dichlorophenol
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Diethylphthalate
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.13 7/8/21SW-846 8270D-E12,4-Dimethylphenol
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Dimethylphthalate
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.33 7/8/21SW-846 8270D-E1V-204,6-Dinitro-2-methylphenol
ND 0.95 7/12/21 16:00 IMRmg/Kg dry0.42 7/8/21SW-846 8270D-E12,4-Dinitrophenol
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.095 7/8/21SW-846 8270D-E12,4-Dinitrotoluene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.081 7/8/21SW-846 8270D-E12,6-Dinitrotoluene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.17 7/8/21SW-846 8270D-E1Di-n-octylphthalate
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E11,2-Diphenylhydrazine/Azobenzene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Fluoranthene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.082 7/8/21SW-846 8270D-E1Fluorene
Page 40 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-05
Field Sample #: BS-5
Sample Matrix: Soil
Sampled: 7/7/2021 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Hexachlorobenzene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Hexachlorobutadiene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E1Hexachlorocyclopentadiene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E1Hexachloroethane
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Indeno(1,2,3-cd)pyrene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.081 7/8/21SW-846 8270D-E1Isophorone
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E11-Methylnaphthalene
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E12-Methylnaphthalene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.090 7/8/21SW-846 8270D-E12-Methylphenol
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E13/4-Methylphenol
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Naphthalene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E12-Nitroaniline
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.083 7/8/21SW-846 8270D-E13-Nitroaniline
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E14-Nitroaniline
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Nitrobenzene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E12-Nitrophenol
ND 0.95 7/12/21 16:00 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E14-Nitrophenol
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1N-Nitrosodimethylamine
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1N-Nitrosodi-n-propylamine
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.082 7/8/21SW-846 8270D-E1Pentachloronitrobenzene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.21 7/8/21SW-846 8270D-E1V-05Pentachlorophenol
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Phenanthrene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Phenol
ND 0.24 7/12/21 16:00 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Pyrene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.050 7/8/21SW-846 8270D-E1Pyridine
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E11,2,4,5-Tetrachlorobenzene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E11,2,4-Trichlorobenzene
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.49 7/12/21 16:00 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 61.8 7/12/21 16:0030-130
Phenol-d6 84.1 7/12/21 16:0030-130
Nitrobenzene-d5 75.2 7/12/21 16:0030-130
2-Fluorobiphenyl 78.1 7/12/21 16:0030-130
2,4,6-Tribromophenol 83.0 7/12/21 16:0030-130
p-Terphenyl-d14 106 7/12/21 16:0030-130
Page 41 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-05
Field Sample #: BS-5
Sample Matrix: Soil
Sampled: 7/7/2021 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.87 0.23 7/12/21 14:14 QNWmg/Kg dry0.040 7/9/21SW-846 6020B5MS-07Arsenic
88 5.8 7/12/21 15:11 QNWmg/Kg dry0.35 7/9/21SW-846 6020B5Chromium
45 2.3 7/12/21 15:11 QNWmg/Kg dry0.11 7/9/21SW-846 6020B5Lead
0.071 0.040 7/12/21 11:40 CJVmg/Kg dry0.014 7/9/21SW-846 7471B1Mercury
ND 1.9 7/12/21 15:11 QNWmg/Kg dry0.058 7/9/21SW-846 6020B5MS-07Selenium
0.085 0.12 7/12/21 15:11 QNWmg/Kg dry0.0033 7/9/21SW-846 6020B5JSilver
160 12 7/12/21 15:11 QNWmg/Kg dry 7/9/21SW-846 6020B5MS-19Barium
0.043 0.47 7/12/21 15:11 QNWmg/Kg dry0.0089 7/9/21SW-846 6020B5JCadmium
Page 42 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-05
Field Sample #: BS-5
Sample Matrix: Soil
Sampled: 7/7/2021 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
69.8 7/12/21 12:45 GLH% Wt 7/9/21SM 2540G1% Solids
Page 43 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-05
Field Sample #: BS-5
Sample Matrix: Soil
Sampled: 7/7/2021 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
1.98 1.37 7/16/21 17:45 PTNmg/Kg0.35 7/16/2171991Hexavalent Chromium
Page 44 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-06
Field Sample #: BS-6
Sample Matrix: Soil
Sampled: 7/7/2021 11:52
[TOC_2]21G0326-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.013 0.14 7/9/21 10:13 MFFmg/Kg dry0.012 7/9/21SW-846 8260D1V-05, JAcetone
ND 0.0082 7/9/21 10:13 MFFmg/Kg dry0.0012 7/9/21SW-846 8260D1Acrylonitrile
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Benzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Bromobenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.0014 7/9/21SW-846 8260D1Bromochloromethane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Bromodichloromethane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1Bromoform
ND 0.014 7/9/21 10:13 MFFmg/Kg dry0.0018 7/9/21SW-846 8260D1Bromomethane
ND 0.055 7/9/21 10:13 MFFmg/Kg dry0.0086 7/9/21SW-846 8260D12-Butanone (MEK)
ND 0.14 7/9/21 10:13 MFFmg/Kg dry0.082 7/9/21SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1n-Butylbenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1sec-Butylbenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1tert-Butylbenzene
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0082 7/9/21 10:13 MFFmg/Kg dry0.0053 7/9/21SW-846 8260D1L-04, V-05Carbon Disulfide
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Carbon Tetrachloride
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Chlorobenzene
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Chlorodibromomethane
ND 0.027 7/9/21 10:13 MFFmg/Kg dry0.0018 7/9/21SW-846 8260D1V-05Chloroethane
ND 0.0055 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1Chloroform
ND 0.014 7/9/21 10:13 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Chloromethane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D12-Chlorotoluene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D14-Chlorotoluene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.0023 7/9/21SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1Dibromomethane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,2-Dichlorobenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,3-Dichlorobenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,4-Dichlorobenzene
ND 0.0055 7/9/21 10:13 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.027 7/9/21 10:13 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,1-Dichloroethane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D11,2-Dichloroethane
ND 0.0055 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1V-051,1-Dichloroethylene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,2-Dichloropropane
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D11,3-Dichloropropane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D12,2-Dichloropropane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00096 7/9/21SW-846 8260D11,1-Dichloropropene
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1trans-1,3-Dichloropropene
ND 0.027 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1V-05Diethyl Ether
Page 45 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-06
Field Sample #: BS-6
Sample Matrix: Soil
Sampled: 7/7/2021 11:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.14 7/9/21 10:13 MFFmg/Kg dry0.026 7/9/21SW-846 8260D11,4-Dioxane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Ethylbenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1Hexachlorobutadiene
ND 0.027 7/9/21 10:13 MFFmg/Kg dry0.0093 7/9/21SW-846 8260D12-Hexanone (MBK)
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0055 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.027 7/9/21 10:13 MFFmg/Kg dry0.0030 7/9/21SW-846 8260D1Methylene Chloride
ND 0.027 7/9/21 10:13 MFFmg/Kg dry0.0063 7/9/21SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0055 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1Naphthalene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1n-Propylbenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D1Styrene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0014 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Tetrachloroethylene
ND 0.014 7/9/21 10:13 MFFmg/Kg dry0.0033 7/9/21SW-846 8260D1Tetrahydrofuran
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00027 7/9/21SW-846 8260D1Toluene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00068 7/9/21SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,1,1-Trichloroethane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D11,1,2-Trichloroethane
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Trichloroethylene
ND 0.014 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1L-04, V-05Trichlorofluoromethane (Freon 11)
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.0014 7/9/21SW-846 8260D11,2,3-Trichloropropane
ND 0.014 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1V-051,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00041 7/9/21SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00027 7/9/21SW-846 8260D11,3,5-Trimethylbenzene
ND 0.014 7/9/21 10:13 MFFmg/Kg dry0.00055 7/9/21SW-846 8260D1Vinyl Chloride
ND 0.0055 7/9/21 10:13 MFFmg/Kg dry0.00082 7/9/21SW-846 8260D1m+p Xylene
ND 0.0027 7/9/21 10:13 MFFmg/Kg dry0.00027 7/9/21SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 7/9/21 10:1370-130
Toluene-d8 103 7/9/21 10:1370-130
4-Bromofluorobenzene 101 7/9/21 10:1370-130
Page 46 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-06
Field Sample #: BS-6
Sample Matrix: Soil
Sampled: 7/7/2021 11:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Acenaphthene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Acenaphthylene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Acetophenone
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.095 7/8/21SW-846 8270D-E1V-05Aniline
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Anthracene
ND 0.89 7/12/21 16:27 IMRmg/Kg dry0.21 7/8/21SW-846 8270D-E1V-04, V-05, V-34Benzidine
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Benzo(a)anthracene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Benzo(a)pyrene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Benzo(b)fluoranthene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.096 7/8/21SW-846 8270D-E1Benzo(g,h,i)perylene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Benzo(k)fluoranthene
ND 1.3 7/12/21 16:27 IMRmg/Kg dry0.54 7/8/21SW-846 8270D-E1Benzoic Acid
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1Bis(2-chloroethoxy)methane
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Bis(2-chloroethyl)ether
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Bis(2-chloroisopropyl)ether
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Bis(2-Ethylhexyl)phthalate
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E14-Bromophenylphenylether
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Butylbenzylphthalate
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Carbazole
ND 0.89 7/12/21 16:27 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E1V-344-Chloroaniline
ND 0.89 7/12/21 16:27 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E14-Chloro-3-methylphenol
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.053 7/8/21SW-846 8270D-E12-Chloronaphthalene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E12-Chlorophenol
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E14-Chlorophenylphenylether
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Chrysene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.093 7/8/21SW-846 8270D-E1Dibenz(a,h)anthracene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Dibenzofuran
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Di-n-butylphthalate
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.052 7/8/21SW-846 8270D-E11,2-Dichlorobenzene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.050 7/8/21SW-846 8270D-E11,3-Dichlorobenzene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.048 7/8/21SW-846 8270D-E11,4-Dichlorobenzene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E13,3-Dichlorobenzidine
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E12,4-Dichlorophenol
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Diethylphthalate
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.12 7/8/21SW-846 8270D-E12,4-Dimethylphenol
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Dimethylphthalate
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.31 7/8/21SW-846 8270D-E1V-204,6-Dinitro-2-methylphenol
ND 0.89 7/12/21 16:27 IMRmg/Kg dry0.40 7/8/21SW-846 8270D-E12,4-Dinitrophenol
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.089 7/8/21SW-846 8270D-E12,4-Dinitrotoluene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E12,6-Dinitrotoluene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.16 7/8/21SW-846 8270D-E1Di-n-octylphthalate
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E11,2-Diphenylhydrazine/Azobenzene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Fluoranthene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Fluorene
Page 47 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-06
Field Sample #: BS-6
Sample Matrix: Soil
Sampled: 7/7/2021 11:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Hexachlorobenzene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E1Hexachlorobutadiene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E1Hexachlorocyclopentadiene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.054 7/8/21SW-846 8270D-E1Hexachloroethane
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Indeno(1,2,3-cd)pyrene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Isophorone
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E11-Methylnaphthalene
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E12-Methylnaphthalene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.085 7/8/21SW-846 8270D-E12-Methylphenol
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E13/4-Methylphenol
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Naphthalene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.097 7/8/21SW-846 8270D-E12-Nitroaniline
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E13-Nitroaniline
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.098 7/8/21SW-846 8270D-E14-Nitroaniline
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Nitrobenzene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E12-Nitrophenol
ND 0.89 7/12/21 16:27 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E14-Nitrophenol
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1N-Nitrosodimethylamine
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1N-Nitrosodi-n-propylamine
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Pentachloronitrobenzene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E1V-05Pentachlorophenol
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Phenanthrene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Phenol
ND 0.23 7/12/21 16:27 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Pyrene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.047 7/8/21SW-846 8270D-E1Pyridine
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E11,2,4,5-Tetrachlorobenzene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.057 7/8/21SW-846 8270D-E11,2,4-Trichlorobenzene
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.46 7/12/21 16:27 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 58.8 7/12/21 16:2730-130
Phenol-d6 78.6 7/12/21 16:2730-130
Nitrobenzene-d5 73.7 7/12/21 16:2730-130
2-Fluorobiphenyl 74.9 7/12/21 16:2730-130
2,4,6-Tribromophenol 75.8 7/12/21 16:2730-130
p-Terphenyl-d14 95.2 7/12/21 16:2730-130
Page 48 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-06
Field Sample #: BS-6
Sample Matrix: Soil
Sampled: 7/7/2021 11:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.3 0.21 7/12/21 14:34 QNWmg/Kg dry0.037 7/9/21SW-846 6020B5Arsenic
59 5.3 7/12/21 15:32 QNWmg/Kg dry0.32 7/9/21SW-846 6020B5Chromium
22 2.1 7/12/21 15:32 QNWmg/Kg dry0.098 7/9/21SW-846 6020B5Lead
0.046 0.037 7/12/21 11:42 CJVmg/Kg dry0.013 7/9/21SW-846 7471B1Mercury
ND 1.7 7/12/21 15:32 QNWmg/Kg dry0.052 7/9/21SW-846 6020B5Selenium
0.096 0.11 7/12/21 15:32 QNWmg/Kg dry0.0030 7/9/21SW-846 6020B5JSilver
140 11 7/12/21 15:32 QNWmg/Kg dry 7/9/21SW-846 6020B5Barium
ND 0.43 7/12/21 15:32 QNWmg/Kg dry0.0081 7/9/21SW-846 6020B5Cadmium
Page 49 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-06
Field Sample #: BS-6
Sample Matrix: Soil
Sampled: 7/7/2021 11:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
74.3 7/12/21 12:46 GLH% Wt 7/9/21SM 2540G1% Solids
Page 50 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-06
Field Sample #: BS-6
Sample Matrix: Soil
Sampled: 7/7/2021 11:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
0.762 - J 1.36 7/16/21 17:50 PTNmg/Kg0.348 7/16/2171991Hexavalent Chromium
Page 51 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-07
Field Sample #: BS-7
Sample Matrix: Soil
Sampled: 7/7/2021 14:00
[TOC_2]21G0326-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.020 0.13 7/9/21 10:40 MFFmg/Kg dry0.012 7/9/21SW-846 8260D1V-05, JAcetone
ND 0.0079 7/9/21 10:40 MFFmg/Kg dry0.0012 7/9/21SW-846 8260D1Acrylonitrile
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1Benzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1Bromobenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.0013 7/9/21SW-846 8260D1Bromochloromethane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1Bromodichloromethane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D1Bromoform
ND 0.013 7/9/21 10:40 MFFmg/Kg dry0.0017 7/9/21SW-846 8260D1Bromomethane
ND 0.053 7/9/21 10:40 MFFmg/Kg dry0.0083 7/9/21SW-846 8260D12-Butanone (MEK)
ND 0.13 7/9/21 10:40 MFFmg/Kg dry0.079 7/9/21SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1n-Butylbenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1sec-Butylbenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1tert-Butylbenzene
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0079 7/9/21 10:40 MFFmg/Kg dry0.0052 7/9/21SW-846 8260D1L-04, V-05Carbon Disulfide
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1Carbon Tetrachloride
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1Chlorobenzene
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1Chlorodibromomethane
ND 0.026 7/9/21 10:40 MFFmg/Kg dry0.0017 7/9/21SW-846 8260D1V-05Chloroethane
ND 0.0053 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1Chloroform
ND 0.013 7/9/21 10:40 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Chloromethane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D12-Chlorotoluene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D14-Chlorotoluene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.0022 7/9/21SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1Dibromomethane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D11,2-Dichlorobenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D11,3-Dichlorobenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D11,4-Dichlorobenzene
ND 0.0053 7/9/21 10:40 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.026 7/9/21 10:40 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D11,1-Dichloroethane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D11,2-Dichloroethane
ND 0.0053 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1V-051,1-Dichloroethylene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D11,2-Dichloropropane
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D11,3-Dichloropropane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D12,2-Dichloropropane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00093 7/9/21SW-846 8260D11,1-Dichloropropene
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1trans-1,3-Dichloropropene
ND 0.026 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D1V-05Diethyl Ether
Page 52 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-07
Field Sample #: BS-7
Sample Matrix: Soil
Sampled: 7/7/2021 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.13 7/9/21 10:40 MFFmg/Kg dry0.025 7/9/21SW-846 8260D11,4-Dioxane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1Ethylbenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D1Hexachlorobutadiene
ND 0.026 7/9/21 10:40 MFFmg/Kg dry0.0090 7/9/21SW-846 8260D12-Hexanone (MBK)
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0053 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.026 7/9/21 10:40 MFFmg/Kg dry0.0029 7/9/21SW-846 8260D1Methylene Chloride
ND 0.026 7/9/21 10:40 MFFmg/Kg dry0.0061 7/9/21SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0053 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D1Naphthalene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1n-Propylbenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D1Styrene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0013 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1Tetrachloroethylene
ND 0.013 7/9/21 10:40 MFFmg/Kg dry0.0032 7/9/21SW-846 8260D1Tetrahydrofuran
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00026 7/9/21SW-846 8260D1Toluene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00066 7/9/21SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D11,1,1-Trichloroethane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D11,1,2-Trichloroethane
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1Trichloroethylene
ND 0.013 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1L-04, V-05Trichlorofluoromethane (Freon 11)
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.0013 7/9/21SW-846 8260D11,2,3-Trichloropropane
ND 0.013 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D1V-051,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00040 7/9/21SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00026 7/9/21SW-846 8260D11,3,5-Trimethylbenzene
ND 0.013 7/9/21 10:40 MFFmg/Kg dry0.00053 7/9/21SW-846 8260D1Vinyl Chloride
ND 0.0053 7/9/21 10:40 MFFmg/Kg dry0.00079 7/9/21SW-846 8260D1m+p Xylene
ND 0.0026 7/9/21 10:40 MFFmg/Kg dry0.00026 7/9/21SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 111 7/9/21 10:4070-130
Toluene-d8 104 7/9/21 10:4070-130
4-Bromofluorobenzene 105 7/9/21 10:4070-130
Page 53 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-07
Field Sample #: BS-7
Sample Matrix: Soil
Sampled: 7/7/2021 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Acenaphthene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Acenaphthylene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Acetophenone
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.099 7/8/21SW-846 8270D-E1V-05Aniline
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Anthracene
ND 0.93 7/12/21 16:53 IMRmg/Kg dry0.22 7/8/21SW-846 8270D-E1V-04, V-05, V-34Benzidine
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Benzo(a)anthracene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Benzo(a)pyrene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Benzo(b)fluoranthene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Benzo(g,h,i)perylene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Benzo(k)fluoranthene
ND 1.4 7/12/21 16:53 IMRmg/Kg dry0.57 7/8/21SW-846 8270D-E1Benzoic Acid
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E1Bis(2-chloroethoxy)methane
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Bis(2-chloroethyl)ether
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Bis(2-chloroisopropyl)ether
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Bis(2-Ethylhexyl)phthalate
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E14-Bromophenylphenylether
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Butylbenzylphthalate
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E1Carbazole
ND 0.93 7/12/21 16:53 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1V-344-Chloroaniline
ND 0.93 7/12/21 16:53 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E14-Chloro-3-methylphenol
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.055 7/8/21SW-846 8270D-E12-Chloronaphthalene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E12-Chlorophenol
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E14-Chlorophenylphenylether
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Chrysene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.097 7/8/21SW-846 8270D-E1Dibenz(a,h)anthracene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Dibenzofuran
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Di-n-butylphthalate
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.054 7/8/21SW-846 8270D-E11,2-Dichlorobenzene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.052 7/8/21SW-846 8270D-E11,3-Dichlorobenzene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.050 7/8/21SW-846 8270D-E11,4-Dichlorobenzene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E13,3-Dichlorobenzidine
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E12,4-Dichlorophenol
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Diethylphthalate
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.13 7/8/21SW-846 8270D-E12,4-Dimethylphenol
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Dimethylphthalate
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.32 7/8/21SW-846 8270D-E1V-204,6-Dinitro-2-methylphenol
ND 0.93 7/12/21 16:53 IMRmg/Kg dry0.41 7/8/21SW-846 8270D-E12,4-Dinitrophenol
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.093 7/8/21SW-846 8270D-E12,4-Dinitrotoluene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E12,6-Dinitrotoluene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.17 7/8/21SW-846 8270D-E1Di-n-octylphthalate
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E11,2-Diphenylhydrazine/Azobenzene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Fluoranthene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Fluorene
Page 54 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-07
Field Sample #: BS-7
Sample Matrix: Soil
Sampled: 7/7/2021 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Hexachlorobenzene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E1Hexachlorobutadiene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E1Hexachlorocyclopentadiene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.057 7/8/21SW-846 8270D-E1Hexachloroethane
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Indeno(1,2,3-cd)pyrene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Isophorone
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E11-Methylnaphthalene
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E12-Methylnaphthalene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.088 7/8/21SW-846 8270D-E12-Methylphenol
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E13/4-Methylphenol
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Naphthalene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E12-Nitroaniline
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.081 7/8/21SW-846 8270D-E13-Nitroaniline
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E14-Nitroaniline
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1Nitrobenzene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E12-Nitrophenol
ND 0.93 7/12/21 16:53 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E14-Nitrophenol
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1N-Nitrosodimethylamine
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1N-Nitrosodi-n-propylamine
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.080 7/8/21SW-846 8270D-E1Pentachloronitrobenzene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.21 7/8/21SW-846 8270D-E1V-05Pentachlorophenol
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E1Phenanthrene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Phenol
ND 0.24 7/12/21 16:53 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Pyrene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.049 7/8/21SW-846 8270D-E1Pyridine
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.062 7/8/21SW-846 8270D-E11,2,4,5-Tetrachlorobenzene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E11,2,4-Trichlorobenzene
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.48 7/12/21 16:53 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 67.8 7/12/21 16:5330-130
Phenol-d6 89.1 7/12/21 16:5330-130
Nitrobenzene-d5 80.5 7/12/21 16:5330-130
2-Fluorobiphenyl 83.1 7/12/21 16:5330-130
2,4,6-Tribromophenol 85.8 7/12/21 16:5330-130
p-Terphenyl-d14 105 7/12/21 16:5330-130
Page 55 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-07
Field Sample #: BS-7
Sample Matrix: Soil
Sampled: 7/7/2021 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.9 0.22 7/12/21 14:37 QNWmg/Kg dry0.038 7/9/21SW-846 6020B5Arsenic
69 5.5 7/12/21 15:34 QNWmg/Kg dry0.33 7/9/21SW-846 6020B5Chromium
26 2.2 7/12/21 15:34 QNWmg/Kg dry0.10 7/9/21SW-846 6020B5Lead
0.071 0.041 7/12/21 11:44 CJVmg/Kg dry0.014 7/9/21SW-846 7471B1Mercury
ND 1.8 7/12/21 15:34 QNWmg/Kg dry0.054 7/9/21SW-846 6020B5Selenium
0.098 0.11 7/12/21 15:34 QNWmg/Kg dry0.0031 7/9/21SW-846 6020B5JSilver
140 11 7/12/21 15:34 QNWmg/Kg dry 7/9/21SW-846 6020B5Barium
ND 0.44 7/12/21 15:34 QNWmg/Kg dry0.0084 7/9/21SW-846 6020B5Cadmium
Page 56 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-07
Field Sample #: BS-7
Sample Matrix: Soil
Sampled: 7/7/2021 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
71.2 7/12/21 12:47 GLH% Wt 7/9/21SM 2540G1% Solids
Page 57 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-07
Field Sample #: BS-7
Sample Matrix: Soil
Sampled: 7/7/2021 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
1.09 - J 1.37 7/16/21 18:26 PTNmg/Kg0.349 7/16/2171991Hexavalent Chromium
Page 58 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-08
Field Sample #: BS-DUP
Sample Matrix: Soil
Sampled: 7/7/2021 00:00
[TOC_2]21G0326-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.12 7/9/21 11:07 MFFmg/Kg dry0.011 7/9/21SW-846 8260D1V-05Acetone
ND 0.0073 7/9/21 11:07 MFFmg/Kg dry0.0011 7/9/21SW-846 8260D1Acrylonitrile
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1Benzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1Bromobenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.0012 7/9/21SW-846 8260D1Bromochloromethane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1Bromodichloromethane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D1Bromoform
ND 0.012 7/9/21 11:07 MFFmg/Kg dry0.0016 7/9/21SW-846 8260D1Bromomethane
ND 0.049 7/9/21 11:07 MFFmg/Kg dry0.0077 7/9/21SW-846 8260D12-Butanone (MEK)
ND 0.12 7/9/21 11:07 MFFmg/Kg dry0.073 7/9/21SW-846 8260D1V-05tert-Butyl Alcohol (TBA)
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1n-Butylbenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D1sec-Butylbenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D1tert-Butylbenzene
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0073 7/9/21 11:07 MFFmg/Kg dry0.0048 7/9/21SW-846 8260D1L-04, V-05Carbon Disulfide
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1Carbon Tetrachloride
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1Chlorobenzene
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1Chlorodibromomethane
ND 0.024 7/9/21 11:07 MFFmg/Kg dry0.0016 7/9/21SW-846 8260D1V-05Chloroethane
ND 0.0049 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D1Chloroform
ND 0.012 7/9/21 11:07 MFFmg/Kg dry0.00098 7/9/21SW-846 8260D1Chloromethane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D12-Chlorotoluene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D14-Chlorotoluene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.0021 7/9/21SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D1Dibromomethane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D11,2-Dichlorobenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D11,3-Dichlorobenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D11,4-Dichlorobenzene
ND 0.0049 7/9/21 11:07 MFFmg/Kg dry0.00098 7/9/21SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.024 7/9/21 11:07 MFFmg/Kg dry0.00098 7/9/21SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D11,1-Dichloroethane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D11,2-Dichloroethane
ND 0.0049 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1V-051,1-Dichloroethylene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D11,2-Dichloropropane
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D11,3-Dichloropropane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D12,2-Dichloropropane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00085 7/9/21SW-846 8260D11,1-Dichloropropene
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D1trans-1,3-Dichloropropene
ND 0.024 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D1V-05Diethyl Ether
Page 59 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-08
Field Sample #: BS-DUP
Sample Matrix: Soil
Sampled: 7/7/2021 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.12 7/9/21 11:07 MFFmg/Kg dry0.023 7/9/21SW-846 8260D11,4-Dioxane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1Ethylbenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D1Hexachlorobutadiene
ND 0.024 7/9/21 11:07 MFFmg/Kg dry0.0083 7/9/21SW-846 8260D12-Hexanone (MBK)
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0049 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.024 7/9/21 11:07 MFFmg/Kg dry0.0027 7/9/21SW-846 8260D1Methylene Chloride
ND 0.024 7/9/21 11:07 MFFmg/Kg dry0.0056 7/9/21SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0049 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D1Naphthalene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1n-Propylbenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D1Styrene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0012 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1Tetrachloroethylene
ND 0.012 7/9/21 11:07 MFFmg/Kg dry0.0029 7/9/21SW-846 8260D1Tetrahydrofuran
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00024 7/9/21SW-846 8260D1Toluene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00061 7/9/21SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D11,1,1-Trichloroethane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D11,1,2-Trichloroethane
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1Trichloroethylene
ND 0.012 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1L-04, V-05Trichlorofluoromethane (Freon 11)
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.0012 7/9/21SW-846 8260D11,2,3-Trichloropropane
ND 0.012 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D1V-051,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00037 7/9/21SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00024 7/9/21SW-846 8260D11,3,5-Trimethylbenzene
ND 0.012 7/9/21 11:07 MFFmg/Kg dry0.00049 7/9/21SW-846 8260D1Vinyl Chloride
ND 0.0049 7/9/21 11:07 MFFmg/Kg dry0.00073 7/9/21SW-846 8260D1m+p Xylene
ND 0.0024 7/9/21 11:07 MFFmg/Kg dry0.00024 7/9/21SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 7/9/21 11:0770-130
Toluene-d8 102 7/9/21 11:0770-130
4-Bromofluorobenzene 99.6 7/9/21 11:0770-130
Page 60 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-08
Field Sample #: BS-DUP
Sample Matrix: Soil
Sampled: 7/7/2021 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E1Acenaphthene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Acenaphthylene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Acetophenone
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.096 7/8/21SW-846 8270D-E1V-05Aniline
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Anthracene
ND 0.90 7/13/21 16:43 IMRmg/Kg dry0.21 7/8/21SW-846 8270D-E1V-04, V-05, V-34Benzidine
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1Benzo(a)anthracene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Benzo(a)pyrene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.070 7/8/21SW-846 8270D-E1Benzo(b)fluoranthene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.097 7/8/21SW-846 8270D-E1Benzo(g,h,i)perylene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Benzo(k)fluoranthene
ND 1.4 7/13/21 16:43 IMRmg/Kg dry0.55 7/8/21SW-846 8270D-E1Benzoic Acid
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E1Bis(2-chloroethoxy)methane
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Bis(2-chloroethyl)ether
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.11 7/8/21SW-846 8270D-E1Bis(2-chloroisopropyl)ether
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Bis(2-Ethylhexyl)phthalate
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.059 7/8/21SW-846 8270D-E14-Bromophenylphenylether
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Butylbenzylphthalate
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.076 7/8/21SW-846 8270D-E1Carbazole
ND 0.90 7/13/21 16:43 IMRmg/Kg dry0.061 7/8/21SW-846 8270D-E1V-344-Chloroaniline
ND 0.90 7/13/21 16:43 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E14-Chloro-3-methylphenol
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.054 7/8/21SW-846 8270D-E12-Chloronaphthalene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E12-Chlorophenol
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E14-Chlorophenylphenylether
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Chrysene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.094 7/8/21SW-846 8270D-E1Dibenz(a,h)anthracene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.068 7/8/21SW-846 8270D-E1Dibenzofuran
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.065 7/8/21SW-846 8270D-E1Di-n-butylphthalate
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.053 7/8/21SW-846 8270D-E11,2-Dichlorobenzene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.051 7/8/21SW-846 8270D-E11,3-Dichlorobenzene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.048 7/8/21SW-846 8270D-E11,4-Dichlorobenzene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E13,3-Dichlorobenzidine
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E12,4-Dichlorophenol
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E1Diethylphthalate
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.13 7/8/21SW-846 8270D-E12,4-Dimethylphenol
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Dimethylphthalate
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.31 7/8/21SW-846 8270D-E14,6-Dinitro-2-methylphenol
ND 0.90 7/13/21 16:43 IMRmg/Kg dry0.40 7/8/21SW-846 8270D-E12,4-Dinitrophenol
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.090 7/8/21SW-846 8270D-E12,4-Dinitrotoluene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E12,6-Dinitrotoluene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.16 7/8/21SW-846 8270D-E1Di-n-octylphthalate
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E11,2-Diphenylhydrazine/Azobenzene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Fluoranthene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Fluorene
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-08
Field Sample #: BS-DUP
Sample Matrix: Soil
Sampled: 7/7/2021 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Hexachlorobenzene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.059 7/8/21SW-846 8270D-E1Hexachlorobutadiene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E1V-05Hexachlorocyclopentadiene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.055 7/8/21SW-846 8270D-E1Hexachloroethane
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.10 7/8/21SW-846 8270D-E1Indeno(1,2,3-cd)pyrene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.077 7/8/21SW-846 8270D-E1Isophorone
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E11-Methylnaphthalene
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E12-Methylnaphthalene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.086 7/8/21SW-846 8270D-E12-Methylphenol
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.075 7/8/21SW-846 8270D-E13/4-Methylphenol
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.063 7/8/21SW-846 8270D-E1Naphthalene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.098 7/8/21SW-846 8270D-E12-Nitroaniline
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.079 7/8/21SW-846 8270D-E13-Nitroaniline
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.099 7/8/21SW-846 8270D-E14-Nitroaniline
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.067 7/8/21SW-846 8270D-E1Nitrobenzene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E12-Nitrophenol
ND 0.90 7/13/21 16:43 IMRmg/Kg dry0.19 7/8/21SW-846 8270D-E14-Nitrophenol
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1N-Nitrosodimethylamine
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.069 7/8/21SW-846 8270D-E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.064 7/8/21SW-846 8270D-E1N-Nitrosodi-n-propylamine
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.078 7/8/21SW-846 8270D-E1Pentachloronitrobenzene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.20 7/8/21SW-846 8270D-E1V-05Pentachlorophenol
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.073 7/8/21SW-846 8270D-E1Phenanthrene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.066 7/8/21SW-846 8270D-E1Phenol
ND 0.23 7/13/21 16:43 IMRmg/Kg dry0.074 7/8/21SW-846 8270D-E1Pyrene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.047 7/8/21SW-846 8270D-E1Pyridine
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.060 7/8/21SW-846 8270D-E11,2,4,5-Tetrachlorobenzene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.058 7/8/21SW-846 8270D-E11,2,4-Trichlorobenzene
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.072 7/8/21SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.46 7/13/21 16:43 IMRmg/Kg dry0.071 7/8/21SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 58.4 7/13/21 16:4330-130
Phenol-d6 76.3 7/13/21 16:4330-130
Nitrobenzene-d5 72.1 7/13/21 16:4330-130
2-Fluorobiphenyl 72.8 7/13/21 16:4330-130
2,4,6-Tribromophenol 78.8 7/13/21 16:4330-130
p-Terphenyl-d14 97.3 7/13/21 16:4330-130
Page 62 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-08
Field Sample #: BS-DUP
Sample Matrix: Soil
Sampled: 7/7/2021 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.70 0.22 7/12/21 14:40 QNWmg/Kg dry0.037 7/9/21SW-846 6020B5Arsenic
55 5.4 7/12/21 15:37 QNWmg/Kg dry0.33 7/9/21SW-846 6020B5Chromium
33 2.2 7/12/21 15:37 QNWmg/Kg dry0.10 7/9/21SW-846 6020B5Lead
0.037 0.035 7/12/21 11:45 CJVmg/Kg dry0.012 7/9/21SW-846 7471B1Mercury
ND 1.7 7/12/21 15:37 QNWmg/Kg dry0.053 7/9/21SW-846 6020B5Selenium
0.085 0.11 7/12/21 15:37 QNWmg/Kg dry0.0030 7/9/21SW-846 6020B5JSilver
250 11 7/12/21 15:37 QNWmg/Kg dry 7/9/21SW-846 6020B5Barium
0.021 0.43 7/12/21 15:37 QNWmg/Kg dry0.0082 7/9/21SW-846 6020B5JCadmium
Page 63 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-08
Field Sample #: BS-DUP
Sample Matrix: Soil
Sampled: 7/7/2021 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
73.5 7/12/21 12:47 GLH% Wt 7/9/21SM 2540G1% Solids
Page 64 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-08
Field Sample #: BS-DUP
Sample Matrix: Soil
Sampled: 7/7/2021 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
0.867 - J 1.31 7/16/21 19:34 PTNmg/Kg0.335 7/16/2171991Hexavalent Chromium
Page 65 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-09
Field Sample #: BKG-1
Sample Matrix: Soil
Sampled: 7/7/2021 16:06
[TOC_2]21G0326-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
4.5 0.23 7/12/21 14:42 QNWmg/Kg dry0.039 7/9/21SW-846 6020B5Arsenic
26 5.7 7/12/21 15:39 QNWmg/Kg dry0.34 7/9/21SW-846 6020B5Chromium
21 2.3 7/12/21 15:39 QNWmg/Kg dry0.10 7/9/21SW-846 6020B5Lead
0.22 0.037 7/12/21 11:47 CJVmg/Kg dry0.013 7/9/21SW-846 7471B1Mercury
ND 1.8 7/12/21 15:39 QNWmg/Kg dry0.056 7/9/21SW-846 6020B5Selenium
0.097 0.11 7/12/21 15:39 QNWmg/Kg dry0.0032 7/9/21SW-846 6020B5JSilver
25 11 7/12/21 15:39 QNWmg/Kg dry 7/9/21SW-846 6020B5Barium
ND 0.45 7/12/21 15:39 QNWmg/Kg dry0.0086 7/9/21SW-846 6020B5Cadmium
Page 66 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-09
Field Sample #: BKG-1
Sample Matrix: Soil
Sampled: 7/7/2021 16:06
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
73.2 7/12/21 12:47 GLH% Wt 7/9/21SM 2540G1% Solids
Page 67 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-09
Field Sample #: BKG-1
Sample Matrix: Soil
Sampled: 7/7/2021 16:06
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
1.08 - J 1.35 7/16/21 18:31 PTNmg/Kg0.345 7/16/2171991Hexavalent Chromium
Page 68 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-10
Field Sample #: BKG-2
Sample Matrix: Soil
Sampled: 7/7/2021 17:15
[TOC_2]21G0326-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
3.0 0.23 7/12/21 14:45 QNWmg/Kg dry0.040 7/9/21SW-846 6020B5Arsenic
31 5.8 7/12/21 15:41 QNWmg/Kg dry0.35 7/9/21SW-846 6020B5Chromium
19 2.3 7/12/21 15:41 QNWmg/Kg dry0.11 7/9/21SW-846 6020B5Lead
0.13 0.035 7/12/21 11:54 CJVmg/Kg dry0.012 7/9/21SW-846 7471B1Mercury
ND 1.8 7/12/21 15:41 QNWmg/Kg dry0.057 7/9/21SW-846 6020B5Selenium
0.080 0.12 7/12/21 15:41 QNWmg/Kg dry0.0032 7/9/21SW-846 6020B5JSilver
13 12 7/12/21 15:41 QNWmg/Kg dry 7/9/21SW-846 6020B5Barium
ND 0.46 7/12/21 15:41 QNWmg/Kg dry0.0088 7/9/21SW-846 6020B5Cadmium
Page 69 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-10
Field Sample #: BKG-2
Sample Matrix: Soil
Sampled: 7/7/2021 17:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
71.9 7/12/21 12:47 GLH% Wt 7/9/21SM 2540G1% Solids
Page 70 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 7/7/2021
Work Order: 21G0326Sample Description:Project Location: King, NC
Sample ID: 21G0326-10
Field Sample #: BKG-2
Sample Matrix: Soil
Sampled: 7/7/2021 17:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
1.26 - J 1.37 7/16/21 18:37 PTNmg/Kg0.35 7/16/2171991Hexavalent Chromium
Page 71 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: % Solids Analytical Method: SM 2540G
Lab Number [Field ID]Batch Date
B285670 07/09/2121G0326-01 [BS-1]
B285670 07/09/2121G0326-02 [BS-2]
B285670 07/09/2121G0326-03 [BS-3]
B285670 07/09/2121G0326-04 [BS-4]
B285670 07/09/2121G0326-05 [BS-5]
B285670 07/09/2121G0326-06 [BS-6]
B285670 07/09/2121G0326-07 [BS-7]
B285670 07/09/2121G0326-08 [BS-DUP]
B285670 07/09/2121G0326-09 [BKG-1]
B285670 07/09/2121G0326-10 [BKG-2]
Prep Method: SW-846 3050B Analytical Method: SW-846 6020B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B285620 07/09/211.53 50.021G0326-01 [BS-1]
B285620 07/09/211.54 50.021G0326-02 [BS-2]
B285620 07/09/211.51 50.021G0326-03 [BS-3]
B285620 07/09/211.58 50.021G0326-04 [BS-4]
B285620 07/09/211.53 50.021G0326-05 [BS-5]
B285620 07/09/211.58 50.021G0326-06 [BS-6]
B285620 07/09/211.60 50.021G0326-07 [BS-7]
B285620 07/09/211.57 50.021G0326-08 [BS-DUP]
B285620 07/09/211.50 50.021G0326-09 [BKG-1]
B285620 07/09/211.50 50.021G0326-10 [BKG-2]
Prep Method: SW-846 7471 Analytical Method: SW-846 7471B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B285624 07/09/210.567 50.021G0326-01 [BS-1]
B285624 07/09/210.592 50.021G0326-02 [BS-2]
B285624 07/09/210.526 50.021G0326-03 [BS-3]
B285624 07/09/210.505 50.021G0326-04 [BS-4]
B285624 07/09/210.533 50.021G0326-05 [BS-5]
B285624 07/09/210.539 50.021G0326-06 [BS-6]
B285624 07/09/210.518 50.021G0326-07 [BS-7]
B285624 07/09/210.589 50.021G0326-08 [BS-DUP]
B285624 07/09/210.548 50.021G0326-09 [BKG-1]
B285624 07/09/210.598 50.021G0326-10 [BKG-2]
Prep Method: SW-846 5035 Analytical Method: SW-846 8260D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B285629 07/09/215.08 10.021G0326-01 [BS-1]
B285629 07/09/214.73 10.021G0326-02 [BS-2]
B285629 07/09/216.35 10.021G0326-03 [BS-3]
B285629 07/09/215.71 10.021G0326-04 [BS-4]
B285629 07/09/215.25 10.021G0326-05 [BS-5]
B285629 07/09/214.93 10.021G0326-06 [BS-6]
B285629 07/09/215.31 10.021G0326-07 [BS-7]
B285629 07/09/215.57 10.021G0326-08 [BS-DUP]
[TOC_1]Sample Preparation Information[TOC]
Page 72 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546 Analytical Method: SW-846 8270D-E
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B285556 07/08/2130.0 1.0021G0326-01 [BS-1]
B285556 07/08/2130.0 1.0021G0326-02 [BS-2]
B285556 07/08/2130.0 1.0021G0326-03 [BS-3]
B285556 07/08/2130.0 1.0021G0326-04 [BS-4]
B285556 07/08/2130.0 1.0021G0326-05 [BS-5]
B285556 07/08/2130.0 1.0021G0326-06 [BS-6]
B285556 07/08/2130.0 1.0021G0326-07 [BS-7]
B285556 07/08/2130.0 1.0021G0326-08 [BS-DUP]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B285629 - SW-846 5035
[TOC_3]B285629[TOC]
Blank (B285629-BLK1) Prepared & Analyzed: 07/09/21
Acetone mg/Kg wet0.10 V-05ND
Acrylonitrile mg/Kg wet0.0060ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010ND
2-Butanone (MEK)mg/Kg wet0.040ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.10 V-05ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060 L-04, V-05ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020 V-05ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040 V-05ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020 V-05ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040ND
[TOC_1]QC Data[TOC]
Page 74 of 118
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B285629 - SW-846 5035
Blank (B285629-BLK1) Prepared & Analyzed: 07/09/21
Methylene Chloride mg/Kg wet0.020ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020ND
Naphthalene mg/Kg wet0.0040ND
n-Propylbenzene mg/Kg wet0.0020ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 L-04, V-05ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 V-05ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 1020.0512
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1010.0504
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1020.0510
LCS (B285629-BS1) Prepared & Analyzed: 07/09/21
Acetone mg/Kg wet0.10 0.200 V-0570-16076.10.152
Acrylonitrile mg/Kg wet0.0060 0.0200 70-1301040.0208
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-13096.10.0192
Benzene mg/Kg wet0.0020 0.0200 70-13099.10.0198
Bromobenzene mg/Kg wet0.0020 0.0200 70-1301000.0200
Bromochloromethane mg/Kg wet0.0020 0.0200 70-1301300.0260
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-1301080.0216
Bromoform mg/Kg wet0.0020 0.0200 70-1301010.0202
Bromomethane mg/Kg wet0.010 0.0200 40-13088.10.0176
2-Butanone (MEK)mg/Kg wet0.040 0.200 70-16098.80.198
tert-Butyl Alcohol (TBA)mg/Kg wet0.10 0.200 V-0540-13075.40.151
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-13092.10.0184
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-1301090.0218
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-1601040.0208
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 70-13096.30.0193
Carbon Disulfide mg/Kg wet0.0060 0.200 V-05, L-0470-13069.6 *0.139
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-1301140.0227
Chlorobenzene mg/Kg wet0.0020 0.0200 70-1301090.0218
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-1301160.0231
Chloroethane mg/Kg wet0.020 0.0200 V-05, J70-13081.60.0163
Chloroform mg/Kg wet0.0040 0.0200 70-1301040.0208
Chloromethane mg/Kg wet0.010 0.0200 70-1301050.0210
2-Chlorotoluene mg/Kg wet0.0020 0.0200 70-1301100.0221
Page 75 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B285629 - SW-846 5035
LCS (B285629-BS1) Prepared & Analyzed: 07/09/21
4-Chlorotoluene mg/Kg wet0.0020 0.0200 70-1301090.0217
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 70-13079.50.0159
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-1301090.0217
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301060.0212
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301050.0209
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301100.0220
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301080.0216
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-1301020.0204
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 40-1601010.0202
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-13096.50.0193
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-1301130.0226
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 V-0570-13070.90.0142
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301010.0201
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301020.0204
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-1301070.0214
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-1301040.0208
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13098.60.0197
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-1301050.0210
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13093.90.0188
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-1301010.0202
Diethyl Ether mg/Kg wet0.020 0.0200 V-05, J70-13072.30.0145
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-1301060.0212
1,4-Dioxane mg/Kg wet0.10 0.200 40-1601110.221
Ethylbenzene mg/Kg wet0.0020 0.0200 70-1301100.0220
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 V-3670-1601200.0240
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-1601050.209
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-1301080.0216
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-13099.30.0199
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 70-13083.90.0168
Methylene Chloride mg/Kg wet0.020 0.0200 40-1601190.0237
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 70-16098.60.197
Naphthalene mg/Kg wet0.0040 0.0200 40-13091.50.0183
n-Propylbenzene mg/Kg wet0.0020 0.0200 70-1301080.0215
Styrene mg/Kg wet0.0020 0.0200 70-1301040.0209
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 70-1301150.0231
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-13092.60.0185
Tetrachloroethylene mg/Kg wet0.0020 0.0200 V-2070-1301200.0241
Tetrahydrofuran mg/Kg wet0.010 0.0200 70-13091.60.0183
Toluene mg/Kg wet0.0020 0.0200 70-1301090.0219
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13088.20.0176
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13088.90.0178
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13095.70.0191
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-1301140.0228
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-1301000.0201
Trichloroethylene mg/Kg wet0.0020 0.0200 70-1301040.0208
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 V-05, L-0470-13066.4 *0.0133
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-1301050.0209
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 V-0570-13078.40.0157
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-1301110.0222
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-1301090.0219
Vinyl Chloride mg/Kg wet0.010 0.0200 40-13079.90.0160
Page 76 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B285629 - SW-846 5035
LCS (B285629-BS1) Prepared & Analyzed: 07/09/21
m+p Xylene mg/Kg wet0.0040 0.0400 70-1301090.0437
o-Xylene mg/Kg wet0.0020 0.0200 70-1301080.0217
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 97.00.0485
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1020.0512
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1070.0536
LCS Dup (B285629-BSD1) Prepared & Analyzed: 07/09/21
Acetone mg/Kg wet0.10 0.200 25 V-0570-16074.2 2.590.148
Acrylonitrile mg/Kg wet0.0060 0.0200 2570-13094.7 9.360.0189
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-13093.0 3.280.0186
Benzene mg/Kg wet0.0020 0.0200 2570-13096.0 3.180.0192
Bromobenzene mg/Kg wet0.0020 0.0200 2570-13093.0 7.350.0186
Bromochloromethane mg/Kg wet0.0020 0.0200 2570-130117 10.40.0234
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-130103 5.020.0206
Bromoform mg/Kg wet0.0020 0.0200 2570-13098.1 2.710.0196
Bromomethane mg/Kg wet0.010 0.0200 2540-13086.0 2.410.0172
2-Butanone (MEK)mg/Kg wet0.040 0.200 2570-16094.4 4.480.189
tert-Butyl Alcohol (TBA)mg/Kg wet0.10 0.200 25 V-0540-13083.8 10.50.168
n-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13089.8 2.530.0180
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-130111 1.270.0221
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-160104 0.2870.0209
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 2570-13092.2 4.350.0184
Carbon Disulfide mg/Kg wet0.0060 0.200 25 L-04, V-0570-13064.8 7.20*0.130
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-130109 3.680.0219
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-130107 1.570.0215
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130105 9.900.0209
Chloroethane mg/Kg wet0.020 0.0200 25 V-05, J70-13076.1 6.980.0152
Chloroform mg/Kg wet0.0040 0.0200 2570-13099.3 4.720.0199
Chloromethane mg/Kg wet0.010 0.0200 2570-130102 3.480.0203
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-130107 3.030.0214
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-130105 3.280.0210
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 2570-13076.0 4.500.0152
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-130104 4.130.0209
Dibromomethane mg/Kg wet0.0020 0.0200 2570-130108 2.060.0216
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130105 0.6660.0211
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130105 4.560.0210
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130113 4.350.0225
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-130104 1.840.0208
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 25 J40-16090.8 10.60.0182
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-13095.0 1.570.0190
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130106 6.590.0211
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 25 V-0570-13070.9 0.000.0142
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13094.5 6.350.0189
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13098.8 3.190.0198
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-130106 0.4690.0213
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-130110 5.340.0219
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13088.3 11.00.0177
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-13097.4 7.700.0195
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13093.0 0.9630.0186
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-130101 0.000.0202
Diethyl Ether mg/Kg wet0.020 0.0200 25 V-05, J70-13081.1 11.50.0162
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-130106 0.2830.0212
Page 77 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B285629 - SW-846 5035
LCS Dup (B285629-BSD1) Prepared & Analyzed: 07/09/21
1,4-Dioxane mg/Kg wet0.10 0.200 5040-160101 9.270.201
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-130106 3.800.0212
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 25 V-3670-160112 6.550.0224
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-160107 1.900.213
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-130103 4.740.0206
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-13095.9 3.480.0192
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 2570-13083.8 0.1190.0168
Methylene Chloride mg/Kg wet0.020 0.0200 2540-160116 2.390.0232
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 2570-160103 4.470.206
Naphthalene mg/Kg wet0.0040 0.0200 2540-13092.1 0.6540.0184
n-Propylbenzene mg/Kg wet0.0020 0.0200 2570-130100 7.120.0200
Styrene mg/Kg wet0.0020 0.0200 2570-130101 3.710.0201
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 2570-130116 0.08660.0231
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-13085.3 8.210.0171
Tetrachloroethylene mg/Kg wet0.0020 0.0200 25 V-2070-130119 1.090.0238
Tetrahydrofuran mg/Kg wet0.010 0.0200 2570-13089.5 2.320.0179
Toluene mg/Kg wet0.0020 0.0200 2570-130105 4.010.0210
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13087.0 1.370.0174
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13087.6 1.470.0175
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13091.7 4.270.0183
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130104 8.800.0209
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130102 1.970.0205
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-13097.2 6.860.0194
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 25 L-04, V-0570-13062.2 6.53*0.0124
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-13098.1 6.410.0196
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 25 V-0570-13077.1 1.670.0154
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-130106 4.520.0212
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-130111 1.180.0221
Vinyl Chloride mg/Kg wet0.010 0.0200 2540-13074.8 6.590.0150
m+p Xylene mg/Kg wet0.0040 0.0400 2570-13097.7 11.20.0391
o-Xylene mg/Kg wet0.0020 0.0200 2570-130104 4.040.0208
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 95.00.0475
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1080.0538
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1050.0523
Page 78 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B285556 - SW-846 3546
[TOC_3]B285556[TOC]
Blank (B285556-BLK1) Prepared: 07/08/21 Analyzed: 07/12/21
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34 V-05ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-04, V-05, V-34ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66 V-34ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 V-20ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 79 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B285556 - SW-846 3546
Blank (B285556-BLK1) Prepared: 07/08/21 Analyzed: 07/12/21
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34 V-05ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 65.64.37
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 85.65.71
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 75.42.51
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 77.82.59
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 80.95.40
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1093.62
LCS (B285556-BS1) Prepared: 07/08/21 Analyzed: 07/12/21
Acenaphthene mg/Kg wet0.17 1.67 40-14077.21.29
Acenaphthylene mg/Kg wet0.17 1.67 40-14080.61.34
Acetophenone mg/Kg wet0.34 1.67 40-14075.11.25
Aniline mg/Kg wet0.34 1.67 V-0510-14068.11.13
Anthracene mg/Kg wet0.17 1.67 40-14088.41.47
Benzidine mg/Kg wet0.66 1.67 V-04, V-05, V-34,
V-35
40-1401061.76
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14090.11.50
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14083.81.40
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14085.91.43
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14090.71.51
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14088.11.47
Benzoic Acid mg/Kg wet1.0 1.67 30-13074.51.24
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14076.91.28
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14084.31.41
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14091.31.52
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-14092.71.55
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14080.51.34
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14089.21.49
Carbazole mg/Kg wet0.17 1.67 40-14085.81.43
4-Chloroaniline mg/Kg wet0.66 1.67 V-3410-14063.41.06
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13083.41.39
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14072.11.20
Page 80 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B285556 - SW-846 3546
LCS (B285556-BS1) Prepared: 07/08/21 Analyzed: 07/12/21
2-Chlorophenol mg/Kg wet0.34 1.67 30-13078.11.30
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14080.11.34
Chrysene mg/Kg wet0.17 1.67 40-14085.01.42
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14091.41.52
Dibenzofuran mg/Kg wet0.34 1.67 40-14083.31.39
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14088.01.47
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14075.31.26
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14071.41.19
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14074.31.24
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 20-14086.71.45
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13079.71.33
Diethylphthalate mg/Kg wet0.34 1.67 40-14084.31.41
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13076.21.27
Dimethylphthalate mg/Kg wet0.34 1.67 40-14084.01.40
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 V-0630-1301011.68
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13082.61.38
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 40-1401001.67
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-1401021.70
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14091.31.52
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 40-14086.81.45
Fluoranthene mg/Kg wet0.17 1.67 40-14087.71.46
Fluorene mg/Kg wet0.17 1.67 40-14080.71.34
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14084.61.41
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14074.61.24
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 40-14060.41.01
Hexachloroethane mg/Kg wet0.34 1.67 40-14073.51.23
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14090.51.51
Isophorone mg/Kg wet0.34 1.67 40-14081.81.36
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14075.51.26
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14084.41.41
2-Methylphenol mg/Kg wet0.34 1.67 30-13072.51.21
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13074.91.25
Naphthalene mg/Kg wet0.17 1.67 40-14075.81.26
2-Nitroaniline mg/Kg wet0.34 1.67 40-14099.81.66
3-Nitroaniline mg/Kg wet0.34 1.67 30-14087.21.45
4-Nitroaniline mg/Kg wet0.34 1.67 40-14084.71.41
Nitrobenzene mg/Kg wet0.34 1.67 40-14079.31.32
2-Nitrophenol mg/Kg wet0.34 1.67 30-13084.51.41
4-Nitrophenol mg/Kg wet0.66 1.67 30-1301111.84
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14090.61.51
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 40-14098.91.65
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14073.71.23
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14089.41.49
Pentachlorophenol mg/Kg wet0.34 1.67 V-0530-13049.90.831
Phenanthrene mg/Kg wet0.17 1.67 40-14087.51.46
Phenol mg/Kg wet0.34 1.67 30-13075.01.25
Pyrene mg/Kg wet0.17 1.67 40-14085.71.43
Pyridine mg/Kg wet0.34 1.67 30-14048.80.814
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14075.51.26
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14075.61.26
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13087.01.45
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13081.41.36
Page 81 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B285556 - SW-846 3546
LCS (B285556-BS1) Prepared: 07/08/21 Analyzed: 07/12/21
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 70.74.71
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 91.76.12
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 84.02.80
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 85.52.85
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 89.15.94
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1173.89
LCS Dup (B285556-BSD1) Prepared: 07/08/21 Analyzed: 07/12/21
Acenaphthene mg/Kg wet0.17 1.67 3040-14072.9 5.651.22
Acenaphthylene mg/Kg wet0.17 1.67 3040-14075.5 6.511.26
Acetophenone mg/Kg wet0.34 1.67 3040-14063.3 17.01.06
Aniline mg/Kg wet0.34 1.67 50 V-0510-14054.7 21.80.912
Anthracene mg/Kg wet0.17 1.67 3040-14086.0 2.821.43
Benzidine mg/Kg wet0.66 1.67 30 V-04, V-05, V-3440-14098.2 7.321.64
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14085.5 5.261.42
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14079.4 5.371.32
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14081.5 5.301.36
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14085.3 6.111.42
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14081.5 7.811.36
Benzoic Acid mg/Kg wet1.0 1.67 5030-13065.7 12.61.09
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14064.1 18.11.07
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14071.6 16.31.19
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14074.8 19.91.25
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14084.1 9.751.40
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14077.5 3.721.29
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14083.8 6.291.40
Carbazole mg/Kg wet0.17 1.67 3040-14083.0 3.361.38
4-Chloroaniline mg/Kg wet0.66 1.67 30 V-3410-14057.2 10.20.954
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13079.7 4.611.33
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14069.1 4.251.15
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13064.7 18.81.08
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14076.3 4.941.27
Chrysene mg/Kg wet0.17 1.67 3040-14081.8 3.811.36
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14082.6 10.11.38
Dibenzofuran mg/Kg wet0.34 1.67 3040-14080.1 3.941.33
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14083.4 5.391.39
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14066.2 12.81.10
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14065.5 8.621.09
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14066.4 11.31.11
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 5020-14076.8 12.21.28
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13071.4 10.91.19
Diethylphthalate mg/Kg wet0.34 1.67 3040-14078.9 6.591.32
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13069.1 9.771.15
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14080.1 4.751.34
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30 V-0630-13097.9 2.701.63
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13082.1 0.5591.37
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14093.8 6.801.56
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14095.7 6.491.60
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14081.7 11.11.36
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 3040-14082.6 4.941.38
Fluoranthene mg/Kg wet0.17 1.67 3040-14082.7 5.871.38
Fluorene mg/Kg wet0.17 1.67 3040-14078.5 2.661.31
Page 82 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B285556 - SW-846 3546
LCS Dup (B285556-BSD1) Prepared: 07/08/21 Analyzed: 07/12/21
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14082.2 2.971.37
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14064.5 14.51.08
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 3040-14051.7 15.60.861
Hexachloroethane mg/Kg wet0.34 1.67 3040-14064.0 13.81.07
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14085.4 5.871.42
Isophorone mg/Kg wet0.34 1.67 3040-14071.9 12.91.20
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14067.1 11.71.12
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14073.9 13.21.23
2-Methylphenol mg/Kg wet0.34 1.67 3030-13065.3 10.41.09
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13066.5 11.91.11
Naphthalene mg/Kg wet0.17 1.67 3040-14066.2 13.61.10
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14093.6 6.391.56
3-Nitroaniline mg/Kg wet0.34 1.67 3030-14082.8 5.201.38
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14082.6 2.411.38
Nitrobenzene mg/Kg wet0.34 1.67 3040-14069.3 13.51.15
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13072.5 15.41.21
4-Nitrophenol mg/Kg wet0.66 1.67 5030-130107 3.351.78
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14085.4 5.891.42
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 3040-14094.9 4.191.58
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14059.5 21.30.992
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14089.8 0.4461.50
Pentachlorophenol mg/Kg wet0.34 1.67 30 V-0530-13047.3 5.190.789
Phenanthrene mg/Kg wet0.17 1.67 3040-14084.2 3.801.40
Phenol mg/Kg wet0.34 1.67 3030-13063.5 16.61.06
Pyrene mg/Kg wet0.17 1.67 3040-14080.7 5.941.35
Pyridine mg/Kg wet0.34 1.67 3030-14050.1 2.510.834
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14069.3 8.531.16
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14064.8 15.41.08
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13080.5 7.741.34
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13079.7 2.091.33
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 58.53.90
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 78.55.23
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 71.62.39
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 78.92.63
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 83.65.57
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1093.64
Page 83 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B285620 - SW-846 3050B
[TOC_3]B285620[TOC]
Blank (B285620-BLK1) Prepared: 07/09/21 Analyzed: 07/12/21
Arsenic mg/Kg wet0.17 J0.10
Chromium mg/Kg wet4.1ND
Lead mg/Kg wet1.7ND
Selenium mg/Kg wet1.3ND
Silver mg/Kg wet0.083ND
Barium mg/Kg wet8.3ND
Cadmium mg/Kg wet0.33ND
LCS (B285620-BS1) Prepared: 07/09/21 Analyzed: 07/12/21
Arsenic mg/Kg wet0.99 170 82.9-117.697.1165
Chromium mg/Kg wet49 101 82.1-117.8104105
Lead mg/Kg wet20 140 82.9-117.1102143
Selenium mg/Kg wet16 182 79.7-120.396.9176
Silver mg/Kg wet0.99 50.1 80.2-12010351.7
Barium mg/Kg wet99 183 82.5-117.599.1181
Cadmium mg/Kg wet4.0 89.5 82.8-117.310089.5
LCS Dup (B285620-BSD1) Prepared: 07/09/21 Analyzed: 07/12/21
Arsenic mg/Kg wet1.0 170 3082.9-117.697.4 0.370166
Chromium mg/Kg wet50 101 3082.1-117.8102 2.20103
Lead mg/Kg wet20 140 3082.9-117.1103 0.719144
Selenium mg/Kg wet16 182 3079.7-120.396.7 0.264176
Silver mg/Kg wet1.0 50.1 3080.2-120106 2.4453.0
Barium mg/Kg wet100 183 2082.5-117.5102 3.35188
Cadmium mg/Kg wet4.0 89.5 2082.8-117.3101 1.1190.5
Duplicate (B285620-DUP1) Prepared: 07/09/21 Analyzed: 07/12/21 Source: 21G0326-05
Arsenic mg/Kg dry0.24 354.260.905 0.867
Chromium mg/Kg dry5.9 356.2582.5 87.8
Lead mg/Kg dry2.4 359.4941.2 45.4
Selenium mg/Kg dry1.9 35NCNDND
Silver mg/Kg dry0.12 35 J2.840.0871 0.0847
Barium mg/Kg dry12 3514.3185161
Cadmium mg/Kg dry0.47 35 J29.80.0317 0.0428
Matrix Spike (B285620-MS1) Prepared: 07/09/21 Analyzed: 07/12/21 Source: 21G0326-05
Arsenic mg/Kg dry0.47 23.7 MS-0775-12561.2 *15.3 0.867
Chromium mg/Kg dry24 23.7 75-12592.911087.8
Lead mg/Kg dry9.5 23.7 75-12512173.9 45.4
Selenium mg/Kg dry7.6 23.7 MS-0775-12547.6 *11.3 ND
Silver mg/Kg dry0.47 23.7 75-12590.721.6 0.0847
Barium mg/Kg dry47 23.7 MS-1975-125195*207 161
Cadmium mg/Kg dry1.9 23.7 75-12595.022.5 0.0428
Page 84 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
Batch B285624 - SW-846 7471
[TOC_3]B285624[TOC]
Blank (B285624-BLK1) Prepared: 07/09/21 Analyzed: 07/12/21
Mercury mg/Kg wet0.025ND
LCS (B285624-BS1) Prepared: 07/09/21 Analyzed: 07/12/21
Mercury mg/Kg wet0.75 15.6 59.3-140.412619.7
LCS Dup (B285624-BSD1) Prepared: 07/09/21 Analyzed: 07/12/21
Mercury mg/Kg wet0.75 15.6 2059.3-140.4113 11.517.6
Page 85 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B285670 - % Solids
[TOC_3]B285670[TOC]
Duplicate (B285670-DUP2) Prepared: 07/09/21 Analyzed: 07/12/21 Source: 21G0326-01
% Solids % Wt 50.45976.5 76.8
Duplicate (B285670-DUP3) Prepared: 07/09/21 Analyzed: 07/12/21 Source: 21G0326-02
% Solids % Wt 50.24274.9 74.8
Duplicate (B285670-DUP4) Prepared: 07/09/21 Analyzed: 07/12/21 Source: 21G0326-03
% Solids % Wt 51.0972.6 71.8
Duplicate (B285670-DUP5) Prepared: 07/09/21 Analyzed: 07/12/21 Source: 21G0326-04
% Solids % Wt 51.4674.3 73.2
Duplicate (B285670-DUP6) Prepared: 07/09/21 Analyzed: 07/12/21 Source: 21G0326-05
% Solids % Wt 51.2570.7 69.8
Duplicate (B285670-DUP7) Prepared: 07/09/21 Analyzed: 07/12/21 Source: 21G0326-07
% Solids % Wt 50.46171.5 71.2
Page 86 of 118
Table of Contents
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Matrix spike recovery is outside of control limits. Analysis is in control based on laboratory fortified blank
recovery.Possibility of sample matrix effects that lead to low bias for reported result or non-homogeneous sample
aliquot cannot be eliminated.
MS-07
Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in
the sample. Appropriate or meaningful recoveries cannot be calculated.
MS-19
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for
this compound.
V-06
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
V-35
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
V-36
[TOC_1]Flag/Qualifier Summary[TOC]
Page 87 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 in Soil
NY,CT,NH,NC,ME,VAHexavalent Chromium
SW-846 6020B in Soil
NY,VA,NH,NC,MEArsenic
NY,NC,MEChromium
NY,NC,MELead
NY,VA,NH,NC,MESelenium
NY,NC,MESilver
NY,NCBarium
NY,NC,MECadmium
SW-846 7471B in Soil
CT,NH,NY,NC,ME,VAMercury
SW-846 8260D in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
[TOC_1]Certifications[TOC]
Page 88 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Soil
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270D-E in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
Page 89 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D-E in Soil
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VADibenzofuran
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine/Azobenzene
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
Page 90 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D-E in Soil
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
SW-846 8270D-E in Water
CT,NY,NC,ME,NH,VAAcenaphthene
CT,NY,NC,ME,NH,VAAcenaphthylene
NY,NCAcetophenone
CT,NY,NC,ME,VAAniline
CT,NY,NC,ME,NH,VAAnthracene
CT,NY,NC,ME,NH,VABenzidine
CT,NY,NC,ME,NH,VABenzo(a)anthracene
CT,NY,NC,ME,NH,VABenzo(a)pyrene
CT,NY,NC,ME,NH,VABenzo(b)fluoranthene
CT,NY,NC,ME,NH,VABenzo(g,h,i)perylene
CT,NY,NC,ME,NH,VABenzo(k)fluoranthene
NY,NC,ME,NH,VABenzoic Acid
CT,NY,NC,ME,NH,VABis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VABis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VABis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VABis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA4-Bromophenylphenylether
CT,NY,NC,ME,NH,VAButylbenzylphthalate
NCCarbazole
CT,NY,NC,ME,NH,VA4-Chloroaniline
CT,NY,NC,ME,NH,VA4-Chloro-3-methylphenol
Page 91 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D-E in Water
CT,NY,NC,ME,NH,VA2-Chloronaphthalene
CT,NY,NC,ME,NH,VA2-Chlorophenol
CT,NY,NC,ME,NH,VA4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VAChrysene
CT,NY,NC,ME,NH,VADibenz(a,h)anthracene
CT,NY,NC,ME,NH,VADibenzofuran
CT,NY,NC,ME,NH,VADi-n-butylphthalate
CT,NY,NC,ME,NH,VA1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA2,4-Dichlorophenol
CT,NY,NC,ME,NH,VADiethylphthalate
CT,NY,NC,ME,NH,VA2,4-Dimethylphenol
CT,NY,NC,ME,NH,VADimethylphthalate
CT,NY,NC,ME,NH,VA4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VADi-n-octylphthalate
NY,NC1,2-Diphenylhydrazine/Azobenzene
CT,NY,NC,ME,NH,VAFluoranthene
NY,NC,ME,NH,VAFluorene
CT,NY,NC,ME,NH,VAHexachlorobenzene
CT,NY,NC,ME,NH,VAHexachlorobutadiene
CT,NY,NC,ME,NH,VAHexachlorocyclopentadiene
CT,NY,NC,ME,NH,VAHexachloroethane
CT,NY,NC,ME,NH,VAIndeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NC,ME,NH,VA2-Methylnaphthalene
CT,NY,NC,NH,VA2-Methylphenol
CT,NY,NC,NH,VA3/4-Methylphenol
CT,NY,NC,ME,NH,VANaphthalene
CT,NY,NC,ME,NH,VA2-Nitroaniline
CT,NY,NC,ME,NH,VA3-Nitroaniline
CT,NY,NC,ME,NH,VA4-Nitroaniline
CT,NY,NC,ME,NH,VANitrobenzene
CT,NY,NC,ME,NH,VA2-Nitrophenol
CT,NY,NC,ME,NH,VA4-Nitrophenol
CT,NY,NC,ME,NH,VAN-Nitrosodimethylamine
CT,NY,NC,ME,NH,VAN-Nitrosodi-n-propylamine
NCPentachloronitrobenzene
CT,NY,NC,ME,NH,VAPentachlorophenol
CT,NY,NC,ME,NH,VAPhenanthrene
CT,NY,NC,ME,NH,VAPhenol
CT,NY,NC,ME,NH,VAPyrene
Page 92 of 118
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D-E in Water
CT,NY,NC,ME,NH,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NC,ME,NH,VA1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2022
PH-0165Connecticut Department of Publilc HealthCT 12/31/2022
10899 NELAPNew York State Department of HealthNY 04/1/2022
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2022
LAO00112Rhode Island Department of HealthRI 12/30/2021
652North Carolina Div. of Water QualityNC 12/31/2021
MA007 NELAPNew Jersey DEPNJ 06/30/2022
E871027 NELAPFlorida Department of HealthFL 06/30/2022
LL720741Vermont Department of Health Lead LaboratoryVT 07/30/2022
MA00100State of MaineME 06/9/2023
460217Commonwealth of VirginiaVA 12/14/2021
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2021
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2022
25703North Carolina Department of HealthNC-DW 07/31/2021
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2022
9100Dept. of Env, Great Lakes, and EnergyMI 09/6/2021
Page 93 of 118
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Page 94 of 118
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Table of Contents
Page 117 of 118
Table of Contents
Page 118 of 118
Table of Contents