24050_Vernon Packaging_Soil Vapor Sampling Report_20210623

Responsive ■ Resourceful ■ Reliable 1
June 23, 2021

Mr. Peter Doorn
Project Manager
Division of Waste Management – Brownfields Program
NC Department of Environmental Quality
1646 Mail Service Center
Raleigh, NC 27699-1646

P: [phone]
E: [e-mail]

Re: Soil Vapor Sampling Report
Vernon Packaging
848, 850 and 860 N. Trade Street
Winston-Salem, Forsyth County, North Carolina
NCBP #24050-20-034
Terracon Project No. 751217006

Dear Mr. Doorn:

On behalf of DPJ Residential, LLC, the Prospective Developer (PD), Terracon Consultants, Inc.
(Terracon) hereby submits this Soil Vapor Sampling Report to evaluate volatile organic
compounds (VOCs) and semi-volatile organic compounds (SVOCs) in soil gas at the above-
referenced site.

Objective
As described in Terracon’s Brownfields Assessment Work Plan dated February 25, 2021, eight
soil vapor probes were to be installed at the site and would be sampled conditionally, based on
the results of the planned soil and groundwater sampling activities. Terracon’s Brownfields
Assessment Report dated April 7, 2021 indicated that soil samples collected at the site contained
the following concentrations of VOCs and/or SVOCs:

◼ The VOC 1,2-dibromoethane was detected in soil sample B-8@7’ at a concentration
exceeding the Inactive Hazardous Sites Branch (IHSB) Protection of Groundwater
Preliminary Soil Remediation Goal (PSRG) but below the Residential Health-Based
PSRG. This detection was J flagged, indicating that the reported concentration was an
estimate.
◼ The VOCs chlorodibromomethane and 1,4-dichlorobenzene were also detected in soil
sample B-8 @ 7’ at concentrations exceeding the laboratory detection limit but below the
respective PSRGs.
Soil Vapor Sampling Report Vernon
Vernon Packaging ■ Winston Salem, NC
June 23, 2021 ■ Terracon Project No. 75217006

Responsive ■ Resourceful ■ Reliable 2
◼ The VOCs 1,4 dichlorobenzene and total xylenes were detected in soil sample B-04@3’
at concentrations exceeding the laboratory detection limit but below the respective
PSRGs.
◼ Multiple SVOCs were reported in soil sample B-8 @ 7’ at concentrations exceeding the
laboratory detection limit but below the respective PSRGs.

Groundwater samples collected at the site contained the following concentrations of VOCs and
SVOCs:

◼ The VOCs chloroform, trans-1,2-dichloroethene, and methyl tert-butyl ether (MTBE) were
all detected in at least one groundwater sample at concentrations exceeding their
respective laboratory detection limits but below their respective 15A NCAC 2L
Groundwater Quality Standards (2L Standards).
◼ The SVOC naphthalene was detected in groundwater sample MW-1 at a concentration
exceeding its laboratory detection limit but below its 2L Standard.

In summary, one soil sample contained the VOC 1,2-dibromomethane at an estimated
concentration exceeding its Protection of Groundwater PSRG. Other VOCs and SVOCs detected
in the soil samples were present at concentrations below their respective Protection of
Groundwater PSRGs. VOCs and SVOCs detected in the groundwater samples were present at
concentrations below their respective 2L Standards. Therefore, with concurrence from the North
Carolina Brownfields Program (NCBP), soil vapor samples were not collected as part of the
Brownfields Assessment.

Because the planned use of the site includes residential development, and based on the emerging
use and interpretation of soil vapor survey data, the NCBP subsequently requested that the soil
vapor sampling activities be completed in accordance with Terracon’s work plan.

Project Background
The site consists of two complete parcels of land (Forsyth County Parcel I.D. Nos. 6835-19-5549
and 6835-19-5759) located at 848 and 860 N. Trade Street (respectively) in Winston Salem,
Forsyth County, North Carolina along with a portion of the south-adjacent parcel (Forsyth County
Parcel I.D. No. 6835-19-5455) located at 850 N. Trade Street (Exhibit 1). The 0.92-acre parcel
located at 848 N. Trade Street is currently occupied by Triad Produce, consisting of one 10,676
square-foot warehouse building and a gravel parking area (Exhibit 2). A 2.46-acre parcel located
at 860 N. Trade Street is currently occupied by Vernon Packaging, consisting of three
interconnected office/warehouse buildings along the southern property boundary, and a gravel
parking/truck storage area and grassed areas to the north. The original building was constructed
in 1978 with building additions in 1986. The buildings comprise approximately 19,000 square
feet. The site also includes a 0.65-acre gravel parking lot portion of the south-adjacent Combs
Produce warehouse property located at 850 N. Trade Street (Forsyth County Parcel I.D. No,
Soil Vapor Sampling Report Vernon
Vernon Packaging ■ Winston Salem, NC
June 23, 2021 ■ Terracon Project No. 75217006

Responsive ■ Resourceful ■ Reliable 3
6835-19-5455). The site operations consist of the temporary storage and distribution of fresh
produce.

Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted practices of
the profession undertaken in similar studies in the same geographical area during the same time.
Terracon makes no warranties, either expressed or implied, regarding the findings, conclusions,
or recommendations. Please note that Terracon does not warrant the work of laboratories,
regulatory agencies, or other third parties supplying information used in the preparation of the
report. These investigation services were performed in accordance with the scope of work agreed
with you, our client, as reflected in our proposal.

Additional Scope Limitations
Findings, conclusions and recommendations resulting from these services are based upon
information derived from the on-site activities and other services, including file reviews, performed
under this scope of work; such information is subject to change over time. Certain indicators of
the presence of hazardous substances, petroleum products, or other constituents may have been
latent, inaccessible, unobservable, not detected or not present during these assessment activities;
thus, we cannot represent that the site is free of hazardous substances, toxic materials, petroleum
products, or other latent conditions beyond those identified during this investigation. Subsurface
conditions may vary from those encountered at specific borings or wells or during other surveys,
tests, assessments, investigations or exploratory services; the data, interpretations, findings, and
our recommendations are based solely upon data obtained at the time and within the scope of
these services.

Soil Gas Sampling Point Installation
As described in Terracon’s Brownfields Assessment Report dated April 7, 2021, a total of eight
soil vapor sampling probes were installed at the site in March, 2021. The sampling probes were
installed in accordance with the procedures described in Terracon’s Work Plan dated February
25, 2021:

◼ Advancement of 2.25-inch diameter borehole to an approximate depth of 10 feet below
ground surface (bgs). The boring for SVP-4 was advanced to a depth of approximately
8 feet bgs using a hand auger.
◼ Installation of a ¼-inch diameter Teflon® tube to approximately 6 inches from the bottom
of the boring and extending 2 feet above ground surface. The bottom end of tube was
equipped with a Geoprobe® implant anchor/drive point and top end of tube was crimped.
◼ Installation of a coarse sand pack around and approximately 2 feet above the bottom of
the tubing.
◼ Installation of 2-foot thick bentonite seal over the sand pack, followed by grout to the
ground surface.

Soil Vapor Sampling Report Vernon
Vernon Packaging ■ Winston Salem, NC
June 23, 2021 ■ Terracon Project No. 75217006

Responsive ■ Resourceful ■ Reliable 4
Terracon returned to the site on June 7, 2021 to assess the condition of the soil vapor probes and
to replace damaged soil vapor probes, as needed. Soil vapor probes SVP-06 and SVP-07 were
previously located in relatively high-traffic areas of the site and the tubing was observed to be
damaged. Therefore, Terracon used a direct-push technology (DPT) drill rig to reinstall the soil
vapor sampling probes to depths of approximately 10 feet bgs in accordance with the work plan
procedures.

Terracon returned to the site on June 8, 2021 to collect the soil vapor samples. The samples
were collected over a 6-minute time interval into 1-liter Summa canisters, in general accordance
with the following protocols:

Shut-In Test
At each soil vapor implant, prior to connection of the sampling train to the implant, a shut-in (dead-
head) test was conducted to check for leaks in the above-ground purge/sampling manifold. The
sample canister and a sacrificial canister (which was not submitted for laboratory analysis) were
connected to the sampling train. The sampling train influent was capped, the sampling canister
remained closed, and the sacrificial canister was opened to create a negative pressure reading
on the sampling train pressure gauge. The sacrificial canister valve was then closed. If there
was an observable loss of vacuum, the fittings were adjusted until the vacuum in the sample train
did not noticeably dissipate.

Helium Tracer Test
For each soil vapor implant sample, following the shut-in test, the purge/sampling train was
connected to the soil vapor sampling implant and a helium tracer gas leak test was conducted.
The tracer gas serves as a QA/QC method to verify the integrity of the seal of the sampling train
to the sample implant. A helium detector was used to verify the presence and concentration of
tracer gas.

The protocol for using a tracer gas was to enclose the tubing and ground interface within a shroud
and enrich the shroud atmosphere to at least 10 percent helium. The purging device (i.e., syringe
or peristaltic pump) was situated inside the shroud and connected to the sampling train by Teflon®
lined tubing running through the shroud. A minimum of three volumes of the vapor implant annulus
and attached Teflon® lined tubing were purged. Purged soil gas was directed to a Tedlar® bag at
the end of each purge volume. Purged soil gas in the Tedlar® bag was then screened for helium
to assess for leaks in the sampling implant seal. The helium concentrations in the shroud and the
the purged soil vapor were documented after each purge volume.

Sample collection commenced after the tracer testing indicated helium concentrations in the vapor
implant were less than or equal to 10 percent of the helium concentration in the shroud, indicating
a sufficiently sealed vapor implant annulus.

Soil Vapor Sampling Report Vernon
Vernon Packaging ■ Winston Salem, NC
June 23, 2021 ■ Terracon Project No. 75217006

Responsive ■ Resourceful ■ Reliable 5
Sample Collection
After completion of the helium tracer test, the valve of the purge device was closed, and the
sample canister valve was opened to collect soil vapor for laboratory analysis. The sample was
collected in a laboratory supplied, batch certified 1.0-liter Summa canister connected to sample
tubing using Swagelok® fittings at the soil vapor implant. The sample canister was filled using a
dedicated flow controller and set to a sample rate of less than or equal to 200 milliliters per minute.
An in-line vacuum gauge was installed to the sample controller to verify initial vacuum levels within
the canister and as an indicator that final equalization had been reached (i.e., sampling was
complete). The sample canister valve was closed when the gauge measured less than 6 inches
of mercury (Hg) vacuum (i.e., sampling was complete). The final vacuum was not allowed to reach
0 inches Hg vacuum.

Sample Analyses
The samples were labeled, packaged and shipped along with a chain-of-custody form to Pace
Analytical Laboratory in Mt. Juliet, Tennessee for analysis of VOCs using U.S. Environmental
Protection Agency (EPA) Method TO-15 and methane using EPA Method 8015M.

Analytical Results
Methane was not detected in the soil vapor samples at concentrations exceeding the laboratory
Reporting Detection Limit. The soil vapor samples contained a variety of VOC constituents. With
the exception of chloroform, the detected VOC concentrations did not exceed their respective
North Carolina Department of Waste Management (NCDWM) Residential Vapor Intrusion
Screening Levels (VISLs). Chloroform was detected in four of the eight samples at concentrations
ranging from 4.12 to 97.3 micrograms per cubic meter (µg/m3), as compared to the VISL of 4.1
µg/m3. The soil vapor sample analytical results are presented on Table 1 and displayed on
Exhibit 3. The laboratory analytical report is included in Appendix A.

Risk Calculator
The soil vapor sample analytical results were input into the Risk Calculator, which was set to
default values. The Risk Calculator indicated that the carcinogenic and hazard index risk values
were not exceeded for site residents, non-residential workers, construction workers or
recreators/trespassers. Copies of selected input and output sheets associated with the Risk
Calculator are presented in Appendix B.

Soil Vapor Sampling Report Vernon
Vernon Packaging ■ Winston Salem, NC
June 23, 2021 ■ Terracon Project No. 75217006

Responsive ■ Resourceful ■ Reliable 6
Terracon appreciates the opportunity to present this report to the NCBP. Terracon is licensed to
practice geology in North Carolina. The certification number of the corporation is F-0869. Should
you have any questions or require additional information, please do not hesitate to contact us at
[phone].

Sincerely,
Terracon Consultants, Inc.

Mark I. Miller, L.G. Edmund Woloszyn Jr., R.E.M.
Senior Geologist Department Manager II
Licensed NC 1715 Environmental Services

Attachments:
Exhibit 1 – Topographic Map
Exhibit 2 – Site Plan with Sampling Locations
Exhibit 3 – Soil Vapor Analytical Results Map
Table 1 – Exterior Soil Gas Sample Analytical Results Summary
Appendix A – Laboratory Analytical Results and Chain of Custody
Appendix B – Risk Calculator Results

Cc: Mr. Porter Jones, DPJ Residential, LLC

EXHIBITS

TOPOGRAPHIC MAP
Vernon Packaging
848, 850 and 860 N. Trade Street
Winston-Salem, NC
TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEY
QUADRANGLES INCLUDE: RURAL HALL, NC (1/1/1994), WALKERTOWN, NC (1/1/1997), WINSTON-SALEM WEST, NC (1/1/1997) and WINSTON-SALEM EAST, NC (1/1/1997).
7327 -G W Friendly Avenue
Greensboro, NC
75217006
Project Manager:
Drawn by:
Checked by:
Approved by:
MIM
EW
EW
1”=2,000’
Vernon Pkg
Feb 2021
2020
Project No.
Scale:
File Name:
Date: 1
Exhibit MIM
APPROXIMATE
SITE BOUNDARY
@A @A
@A
@A
@A
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
!(
!(
!(
!(
!(
!(
!(
!(!(
B-7
B-6
B-4
B-1
B-9/VP-5
B-3/VP-2
B-2/VP-1
B-8/VP-4 B-5/VP-3
B-11/VP-7
B-12/VP-8
B-10/VP-6MW-4
MW-5
MW-3
MW-2MW-1
Source: Esri, Maxar, GeoEye, Earthstar Geographics, CNES/Airbus DS,USDA, USGS, AeroGRID, IGN, and the GIS User Community
0 10050 Feet
75217006
Service Layer Credits: NC Statewide Orthoimagery, Site Boundaryapproximated from Forsyth County GIS and NCDEQ BrownfieldsProgram Site Plan.
Legend
!(Compressor
!(Pole-Mounted Transformer
!(Pad-Mounted Transformer
!(Dumpsters
&>Soil Borings/Soil Vapor Probes
@A Groundwater Monitoring WellsApproximate Parcel BoundaryApproximate Site BoundaryOAK STREETWEST TENTH STREET
Site Plan with Sampling Locations
Vernon Packaging848, 850, and 860 N. Trade StreetWinston-Salem, North CarolinaNORTH TRADE STREETWEST NINTH STREET
MARTIN LUTHERKING JR DR
2
EXHIBITNO.Project No.:
Scale: 1" = 100'
File Name:
Date:Feb. 2021
Vernon Pkg.7327-G West Friendly AvenueGreensboro, NC 27410
Project Manager.: MIMDrawn by:
Reviewed by:
Approved by:EW
AAF
EW
@A @A
@A
@A
@A
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
B-7
B-6
B-4
B-1
B-9/VP-5
B-3/VP-2
B-2/VP-1
B-8/VP-4 B-5/VP-3
B-11/VP-7
B-12/VP-8
B-10/VP-6MW-4
MW-5
MW-3
MW-2MW-1
Source: Esri, Maxar, GeoEye, Earthstar Geographics, CNES/Airbus DS,USDA, USGS, AeroGRID, IGN, and the GIS User Community
0 10050 Feet
75217006
Service Layer Credits: NC Statewide Orthoimagery, Site Boundaryapproximated from Forsyth County GIS and NCDEQ BrownfieldsProgram Site Plan.
Legend
&>Soil Borings/Soil Vapor Probes
@A Groundwater Monitoring WellsApproximate Parcel BoundaryApproximate Site BoundaryOAK STREETWEST TENTH STREET
Soil Vapor Analytical Results Map
Vernon Packaging848, 850, and 860 N. Trade StreetWinston-Salem, North CarolinaNORTH TRADE STREETWEST NINTH STREET
MARTIN LUTHERKING JR DR
3
EXHIBITNO.Project No.:
Scale: 1" = 100'
File Name:
Date:June 2021
Vernon Pkg.7327-G West Friendly AvenueGreensboro, NC 27410
Project Manager.: MIMDrawn by:
Reviewed by:
Approved by:EW
JWR
EW
SVP-1VOCs by TO-15Acetone = 7.06 ug/m3Carbon Disulfide = 2.24 ug/m3Chloroform = 7.25 ug/m3Ethanol = 9.96 ug/m3Trichlorofluoromethane= 4.3 ug/m3Dichlorofluoromethane= 12.4 ug/m3Tetrachloroethylene = 3.81 ug/m3Toluene = 3.59 ug/m3
Only detected concentrations are shownConcentrations in BOLD exceed NCDWM Residential Vapor INtrusion Screenig LevelsConcentrations reported in micrograms per cubic meter (ug/m3)
SVP-2VOCs by TO-15Acetone = 4.68 ug/m3Chloroform = 5.06 ug/m3Chloromethane = 0.632 ug/m3Ethanol = 10.8 ug/m3Trichlorofluoromethane= 7.87 ug/m3Dichlorofluoromethane= 29.7 ug/m3Tetrachloroethylene = 6.52 ug/m3
SVP-3 VOCs by TO-15Acetone = 4.51 ug/m3Ethanol = 10.1 ug/m3Trichloroflouromethane= 12.3 ug/m3Dichloroflouromethane= 63.8 ug/m3Tetrachloroethylene = 4.23 ug/m3Toluene = 1.88 ug/m3
SVP-4VOCs by TO-15Acetone = 6.65 ug/m3Chloroform = 2.75 ug/m3Ethanol = 30.7 ug/m3Trichlorofluoromethane= 104 ug/m3Dichlorofluoromethane= 31 ug/m32-Propanol = 3.54 ug/m3Tetrachloroethylene = 1.54 ug/m3Toluene = 3.42 ug/m3M and P-Xylene = 2.35 ug/m3
SVP-5VOCs by TO-15Acetone = 18.7 ug/m3Chloromethane = 0.932 ug/m3Ethanol = 10.9 ug/m3Trichlorofluoromethane= 203 ug/m3Dichlorofluoromethane= 24.8 ug/m32-Butanone (MEK) = 3.83 ug/m32-Propanol = 7.08 ug/m3Tetrachloroethylene = 1.56 ug/m3Toluene = 3.77 ug/m3M and P-Xylene = 2.16 ug/m3
SVP-6VOCs by TO-15Acetone = 11.5 ug/m3Benzene = 9.04 ug/m3Ethanol = 8.28 ug/m3Ethylbenzene = 4.22 ug/m34-Ethyl Toluene = 4.07 ug/m3Trichlorofluoromethane= 188 ug/m3Dichlorofluoromethane= 7.91 ug/m3Heptane = 0.912 ug/m3Propene = 15.2 ug/m3Tetrachloroethylene = 12.4 ug/m3Toluene = 38 ug/m31,2,4 Trimethylbenzene = 4.48 ug/m31,3,5 Trimethylbenzene = 1.25 ug/m3 SVP-7VOCs by TO-15Acetone = 19.8 ug/m3Benzene = 1.73 ug/m3Carbon Disulfide = 4.95 ug/m3Chloroform = 97.3 ug/m3Cyclohexane = 0.751 ug/m3 Ethanol = 11.7 ug/m3Ethylbenzene = 2.69 ug/m3Trichlorofluoromethane= 36.9 ug/m3Dichlorofluoromethane= 54.9 ug/m3Heptane = 1.09 ug/m3Methyl Chloride = 1.98 ug/m32-Butanone (MEK) = 5.04 ug/m3Propene = 19.6 ug/m3Tetrachloroethylene = 11 ug/m3Toluene = 12 ug/m31,2,4 Trimethylbenzene = 1.27 ug/m3M and P-Xylene = 9.15 ug/m3O-Xylene = 3.24 ug/m3
SVP-8VOCs by TO-15Acetone = 13 ug/m3Chloroform = 4.12 ug/m3Ethanol = 8.16 ug/m3Trichloroflouromethane= 30.9 ug/m3Dichloroflouromethane= 15.4 ug/m32-propanol = 43.3Tetrachloroethylene = 2.68 ug/m3Toluene = 3.55 ug/m3

TABLE

Table 1
Exterior Soil Gas Sample Analytical Results Summary
Vernon Packaging
848, 850 and 860 N. Trade Street
Winston-Salem, North Carolina
Terracon Project No. 75217006
SVP-1 SVP-2 SVP-3 SVP-4 SVP-5 SVP-6 SVP-7 SVP-8
Method Analyte Result Result Result Result Result Result Result Result
ACETONE 7.06 4.68 4.51 6.65 18.7 11.5 19.8 13 19.8 220000
BENZENE <0.639 <0.639 <0.639 <0.639 <0.639 9.04 1.73 <0.639 9.04 12
CARBON DISULFIDE 2.24 <0.622 <0.622 <0.622 <0.622 <0.622 4.95 <0.622 4.95 4900
CHLOROFORM 7.25 5.06 <0.973 2.75 <0.973 <0.973 97.3 4.12 97.3 4.1
CHLOROMETHANE <0.413 0.632 <0.413 <0.413 0.932 <0.413 <0.413 <0.413 0.932 630
CYCLOHEXANE <0.689 <0.689 <0.689 <0.689 <0.689 <0.689 0.751 <0.689 0.751 42000
ETHANOL 9.96 10.8 10.1 30.7 10.9 8.28 11.7 8.16 30.7 NE
ETHYLBENZENE <0.867 <0.867 <0.867 <0.867 <0.867 4.22 2.69 <0.867 4.22 37
4-ETHYL TOLUENE <0.982 <0.982 <0.982 <0.982 <0.982 4.07 <0.982 <0.982 4.07 NE
TRICHLOROFLUOROMETHANE 4.3 7.87 12.3 104 203 188 36.9 30.9 203 NE
DICHLORODIFLUOROMETHANE 12.4 29.7 63.8 31 24.8 7.91 54.9 15.4 63.8 700
HEPTANE <0.818 <0.818 <0.818 <0.818 <0.818 0.912 1.09 <0.818 1.09 2800
METHYLENE CHLORIDE <0.694 <0.694 <0.694 <0.694 <0.694 <0.694 1.98 <0.694 1.98 3400
2-BUTANONE (MEK)<3.69 <3.69 <3.69 <3.69 3.83 <3.69 5.04 <3.69 5.04 35000
2-PROPANOL <3.07 <3.07 <3.07 3.54 7.08 <3.07 <3.07 43.3 43.3 1400
PROPENE <2.15 <2.15 <2.15 <2.15 <2.15 15.2 19.6 <2.15 19.6 NE
TETRACHLOROETHYLENE 3.81 6.52 4.23 1.54 1.56 12.4 11 2.68 12.4 280
TOLUENE 3.59 <1.88 1.88 3.42 3.77 38 12 3.55 38 35000
1,2,4-TRIMETHYLBENZENE <0.982 <0.982 <0.982 <0.982 <0.982 4.48 1.27 <0.982 4.48 420
1,3,5-TRIMETHYLBENZENE <0.982 <0.982 <0.982 <0.982 <0.982 1.25 <0.982 <0.982 1.25 420
M&P-XYLENE <1.73 <1.73 <1.73 2.35 2.16 <1.73 9.15 <1.73 9.15 700
O-XYLENE <0.867 <0.867 <0.867 <0.867 <0.867 <0.867 3.24 <0.867 3.24 700
Notes:
VOCs - volatile organic compounds
Compounds detected in one or more samples shown
Concentrations are reported in micrograms per cubic meter (µg/m3)
Bold indicates concentration above the Reported Detection Limit
indicates concentrations above The NC DWM Residential Screening Level
TO-15
6/8/2021Date Collected
Sample ID NC DWM Residential
Vapor Intrusion
Screening Levels
Maximum Concentration
Reported

APPENDIX A
LABORATORY ANALYTICAL RESULTS AND CHAIN OF CUSTODY

ANALYTICAL REPORT
June 11, 2021
Terracon - Greensboro, NC
Sample Delivery Group:L1363895
Samples Received:06/09/2021
Project Number:75217005
Description:Vernon Packaging
Report To:Zach Tidmore
7327-G, West Friendly Ave
Greensboro, NC 27410
Entire Report Reviewed By:
June 11, 2021
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 20:05 1 of 29
June 11, 2021
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 21:53 1 of 29
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
SVP-1 L1363895-01 6
SVP-2 L1363895-02 8
SVP-3 L1363895-03 10
SVP-4 L1363895-04 12
SVP-5 L1363895-05 14
SVP-6 L1363895-06 16
SVP-7 L1363895-07 18
SVP-8 L1363895-08 20
Qc: Quality Control Summary 22
Volatile Organic Compounds (GC) by Method 8015M 22
Volatile Organic Compounds (MS) by Method TO-15 23
Gl: Glossary of Terms 27
Al: Accreditations & Locations 28
Sc: Sample Chain of Custody 29
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SVP-1 L1363895-01 Air Zach Tidmore 06/08/21 13:13 06/09/21 10:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015M WG1686733 1 06/11/21 09:28 06/11/21 09:28 DAH Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1686163 1 06/10/21 12:23 06/10/21 12:23 CAW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SVP-2 L1363895-02 Air Zach Tidmore 06/08/21 13:30 06/09/21 10:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015M WG1686733 1 06/11/21 09:30 06/11/21 09:30 DAH Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1686163 1 06/10/21 13:07 06/10/21 13:07 CAW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SVP-3 L1363895-03 Air Zach Tidmore 06/08/21 15:21 06/09/21 10:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015M WG1686733 1 06/11/21 09:33 06/11/21 09:33 DAH Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1686163 1 06/10/21 13:49 06/10/21 13:49 CAW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SVP-4 L1363895-04 Air Zach Tidmore 06/08/21 16:14 06/09/21 10:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015M WG1686733 1 06/11/21 09:36 06/11/21 09:36 DAH Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1686163 1 06/10/21 14:30 06/10/21 14:30 CAW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SVP-5 L1363895-05 Air Zach Tidmore 06/08/21 16:25 06/09/21 10:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015M WG1686733 1 06/11/21 09:41 06/11/21 09:41 DAH Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1686163 1 06/10/21 15:12 06/10/21 15:12 CAW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SVP-6 L1363895-06 Air Zach Tidmore 06/08/21 16:48 06/09/21 10:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015M WG1686733 1 06/11/21 09:45 06/11/21 09:45 DAH Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1686163 1 06/10/21 15:53 06/10/21 15:53 CAW Mt. Juliet, TN
Collected by Collected date/time Received date/time
SVP-7 L1363895-07 Air Zach Tidmore 06/08/21 17:13 06/09/21 10:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015M WG1686733 1 06/11/21 10:43 06/11/21 10:43 DAH Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1686163 1 06/10/21 16:35 06/10/21 16:35 CAW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SVP-8 L1363895-08 Air Zach Tidmore 06/08/21 17:32 06/09/21 10:15
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC) by Method 8015M WG1686733 1 06/11/21 10:46 06/11/21 10:46 DAH Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1686163 1 06/10/21 17:17 06/10/21 17:17 CAW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 20:05 5 of 29
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1363895
SVP-1
Collected date/time: 06/08/21 13:13
Volatile Organic Compounds (GC) by Method 8015M
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppmv mg/m3 ppmv mg/m3
Methane 74-82-8 16 10.0 6.54 ND ND 1 WG1686733
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 1.25 2.97 2.97 7.06 1 WG1686163
Allyl chloride 107-05-1 76.53 0.200 0.626 ND ND 1 WG1686163
Benzene 71-43-2 78.10 0.200 0.639 ND ND 1 WG1686163
Benzyl Chloride 100-44-7 127 0.200 1.04 ND ND 1 WG1686163
Bromodichloromethane 75-27-4 164 0.200 1.34 ND ND 1 WG1686163
Bromoform 75-25-2 253 0.600 6.21 ND ND 1 WG1686163
Bromomethane 74-83-9 94.90 0.200 0.776 ND ND 1 WG1686163
1,3-Butadiene 106-99-0 54.10 2.00 4.43 ND ND 1 WG1686163
Carbon disulfide 75-15-0 76.10 0.200 0.622 0.720 2.24 1 WG1686163
Carbon tetrachloride 56-23-5 154 0.200 1.26 ND ND 1 WG1686163
Chlorobenzene 108-90-7 113 0.200 0.924 ND ND 1 WG1686163
Chloroethane 75-00-3 64.50 0.200 0.528 ND ND 1 WG1686163
Chloroform 67-66-3 119 0.200 0.973 1.49 7.25 1 WG1686163
Chloromethane 74-87-3 50.50 0.200 0.413 ND ND 1 WG1686163
2-Chlorotoluene 95-49-8 126 0.200 1.03 ND ND 1 WG1686163
Cyclohexane 110-82-7 84.20 0.200 0.689 ND ND 1 WG1686163
Dibromochloromethane 124-48-1 208 0.200 1.70 ND ND 1 WG1686163
1,2-Dibromoethane 106-93-4 188 0.200 1.54 ND ND 1 WG1686163
1,2-Dichlorobenzene 95-50-1 147 0.200 1.20 ND ND 1 WG1686163
1,3-Dichlorobenzene 541-73-1 147 0.200 1.20 ND ND 1 WG1686163
1,4-Dichlorobenzene 106-46-7 147 0.200 1.20 ND ND 1 WG1686163
1,2-Dichloroethane 107-06-2 99 0.200 0.810 ND ND 1 WG1686163
1,1-Dichloroethane 75-34-3 98 0.200 0.802 ND ND 1 WG1686163
1,1-Dichloroethene 75-35-4 96.90 0.200 0.793 ND ND 1 WG1686163
cis-1,2-Dichloroethene 156-59-2 96.90 0.200 0.793 ND ND 1 WG1686163
trans-1,2-Dichloroethene 156-60-5 96.90 0.200 0.793 ND ND 1 WG1686163
1,2-Dichloropropane 78-87-5 113 0.200 0.924 ND ND 1 WG1686163
cis-1,3-Dichloropropene 10061-01-5 111 0.200 0.908 ND ND 1 WG1686163
trans-1,3-Dichloropropene 10061-02-6 111 0.200 0.908 ND ND 1 WG1686163
1,4-Dioxane 123-91-1 88.10 0.200 0.721 ND ND 1 WG1686163
Ethanol 64-17-5 46.10 1.25 2.36 5.28 9.96 B 1 WG1686163
Ethylbenzene 100-41-4 106 0.200 0.867 ND ND 1 WG1686163
4-Ethyltoluene 622-96-8 120 0.200 0.982 ND ND 1 WG1686163
Trichlorofluoromethane 75-69-4 137.40 0.200 1.12 0.766 4.30 1 WG1686163
Dichlorodifluoromethane 75-71-8 120.92 0.200 0.989 2.50 12.4 1 WG1686163
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.200 1.53 ND ND 1 WG1686163
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.200 1.40 ND ND 1 WG1686163
Heptane 142-82-5 100 0.200 0.818 ND ND 1 WG1686163
Hexachloro-1,3-butadiene 87-68-3 261 0.630 6.73 ND ND 1 WG1686163
n-Hexane 110-54-3 86.20 0.630 2.22 ND ND 1 WG1686163
Isopropylbenzene 98-82-8 120.20 0.200 0.983 ND ND 1 WG1686163
Methylene Chloride 75-09-2 84.90 0.200 0.694 ND ND 1 WG1686163
Methyl Butyl Ketone 591-78-6 100 1.25 5.11 ND ND 1 WG1686163
2-Butanone (MEK)78-93-3 72.10 1.25 3.69 ND ND 1 WG1686163
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 1.25 5.12 ND ND 1 WG1686163
Methyl methacrylate 80-62-6 100.12 0.200 0.819 ND ND 1 WG1686163
MTBE 1634-04-4 88.10 0.200 0.721 ND ND 1 WG1686163
Naphthalene 91-20-3 128 0.630 3.30 ND ND 1 WG1686163
2-Propanol 67-63-0 60.10 1.25 3.07 ND ND 1 WG1686163
Propene 115-07-1 42.10 1.25 2.15 ND ND 1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1363895
SVP-1
Collected date/time: 06/08/21 13:13
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Styrene 100-42-5 104 0.200 0.851 ND ND 1 WG1686163
1,1,2,2-Tetrachloroethane 79-34-5 168 0.200 1.37 ND ND 1 WG1686163
Tetrachloroethylene 127-18-4 166 0.200 1.36 0.561 3.81 1 WG1686163
Tetrahydrofuran 109-99-9 72.10 0.200 0.590 ND ND 1 WG1686163
Toluene 108-88-3 92.10 0.500 1.88 0.952 3.59 1 WG1686163
1,2,4-Trichlorobenzene 120-82-1 181 0.630 4.66 ND ND 1 WG1686163
1,1,1-Trichloroethane 71-55-6 133 0.200 1.09 ND ND 1 WG1686163
1,1,2-Trichloroethane 79-00-5 133 0.200 1.09 ND ND 1 WG1686163
Trichloroethylene 79-01-6 131 0.200 1.07 ND ND 1 WG1686163
1,2,4-Trimethylbenzene 95-63-6 120 0.200 0.982 ND ND 1 WG1686163
1,3,5-Trimethylbenzene 108-67-8 120 0.200 0.982 ND ND 1 WG1686163
2,2,4-Trimethylpentane 540-84-1 114.22 0.200 0.934 ND ND 1 WG1686163
Vinyl chloride 75-01-4 62.50 0.200 0.511 ND ND 1 WG1686163
Vinyl Bromide 593-60-2 106.95 0.200 0.875 ND ND 1 WG1686163
Vinyl acetate 108-05-4 86.10 0.200 0.704 ND ND 1 WG1686163
m&p-Xylene 1330-20-7 106 0.400 1.73 ND ND 1 WG1686163
o-Xylene 95-47-6 106 0.200 0.867 ND ND 1 WG1686163
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 91.1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1363895
SVP-2
Collected date/time: 06/08/21 13:30
Volatile Organic Compounds (GC) by Method 8015M
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppmv mg/m3 ppmv mg/m3
Methane 74-82-8 16 10.0 6.54 ND ND 1 WG1686733
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 1.25 2.97 1.97 4.68 1 WG1686163
Allyl chloride 107-05-1 76.53 0.200 0.626 ND ND 1 WG1686163
Benzene 71-43-2 78.10 0.200 0.639 ND ND 1 WG1686163
Benzyl Chloride 100-44-7 127 0.200 1.04 ND ND 1 WG1686163
Bromodichloromethane 75-27-4 164 0.200 1.34 ND ND 1 WG1686163
Bromoform 75-25-2 253 0.600 6.21 ND ND 1 WG1686163
Bromomethane 74-83-9 94.90 0.200 0.776 ND ND 1 WG1686163
1,3-Butadiene 106-99-0 54.10 2.00 4.43 ND ND 1 WG1686163
Carbon disulfide 75-15-0 76.10 0.200 0.622 ND ND 1 WG1686163
Carbon tetrachloride 56-23-5 154 0.200 1.26 ND ND 1 WG1686163
Chlorobenzene 108-90-7 113 0.200 0.924 ND ND 1 WG1686163
Chloroethane 75-00-3 64.50 0.200 0.528 ND ND 1 WG1686163
Chloroform 67-66-3 119 0.200 0.973 1.04 5.06 1 WG1686163
Chloromethane 74-87-3 50.50 0.200 0.413 0.306 0.632 1 WG1686163
2-Chlorotoluene 95-49-8 126 0.200 1.03 ND ND 1 WG1686163
Cyclohexane 110-82-7 84.20 0.200 0.689 ND ND 1 WG1686163
Dibromochloromethane 124-48-1 208 0.200 1.70 ND ND 1 WG1686163
1,2-Dibromoethane 106-93-4 188 0.200 1.54 ND ND 1 WG1686163
1,2-Dichlorobenzene 95-50-1 147 0.200 1.20 ND ND 1 WG1686163
1,3-Dichlorobenzene 541-73-1 147 0.200 1.20 ND ND 1 WG1686163
1,4-Dichlorobenzene 106-46-7 147 0.200 1.20 ND ND 1 WG1686163
1,2-Dichloroethane 107-06-2 99 0.200 0.810 ND ND 1 WG1686163
1,1-Dichloroethane 75-34-3 98 0.200 0.802 ND ND 1 WG1686163
1,1-Dichloroethene 75-35-4 96.90 0.200 0.793 ND ND 1 WG1686163
cis-1,2-Dichloroethene 156-59-2 96.90 0.200 0.793 ND ND 1 WG1686163
trans-1,2-Dichloroethene 156-60-5 96.90 0.200 0.793 ND ND 1 WG1686163
1,2-Dichloropropane 78-87-5 113 0.200 0.924 ND ND 1 WG1686163
cis-1,3-Dichloropropene 10061-01-5 111 0.200 0.908 ND ND 1 WG1686163
trans-1,3-Dichloropropene 10061-02-6 111 0.200 0.908 ND ND 1 WG1686163
1,4-Dioxane 123-91-1 88.10 0.200 0.721 ND ND 1 WG1686163
Ethanol 64-17-5 46.10 1.25 2.36 5.75 10.8 B 1 WG1686163
Ethylbenzene 100-41-4 106 0.200 0.867 ND ND 1 WG1686163
4-Ethyltoluene 622-96-8 120 0.200 0.982 ND ND 1 WG1686163
Trichlorofluoromethane 75-69-4 137.40 0.200 1.12 1.40 7.87 1 WG1686163
Dichlorodifluoromethane 75-71-8 120.92 0.200 0.989 6.01 29.7 1 WG1686163
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.200 1.53 ND ND 1 WG1686163
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.200 1.40 ND ND 1 WG1686163
Heptane 142-82-5 100 0.200 0.818 ND ND 1 WG1686163
Hexachloro-1,3-butadiene 87-68-3 261 0.630 6.73 ND ND 1 WG1686163
n-Hexane 110-54-3 86.20 0.630 2.22 ND ND 1 WG1686163
Isopropylbenzene 98-82-8 120.20 0.200 0.983 ND ND 1 WG1686163
Methylene Chloride 75-09-2 84.90 0.200 0.694 ND ND 1 WG1686163
Methyl Butyl Ketone 591-78-6 100 1.25 5.11 ND ND 1 WG1686163
2-Butanone (MEK)78-93-3 72.10 1.25 3.69 ND ND 1 WG1686163
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 1.25 5.12 ND ND 1 WG1686163
Methyl methacrylate 80-62-6 100.12 0.200 0.819 ND ND 1 WG1686163
MTBE 1634-04-4 88.10 0.200 0.721 ND ND 1 WG1686163
Naphthalene 91-20-3 128 0.630 3.30 ND ND 1 WG1686163
2-Propanol 67-63-0 60.10 1.25 3.07 ND ND 1 WG1686163
Propene 115-07-1 42.10 1.25 2.15 ND ND 1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 02
L1363895
SVP-2
Collected date/time: 06/08/21 13:30
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Styrene 100-42-5 104 0.200 0.851 ND ND 1 WG1686163
1,1,2,2-Tetrachloroethane 79-34-5 168 0.200 1.37 ND ND 1 WG1686163
Tetrachloroethylene 127-18-4 166 0.200 1.36 0.961 6.52 1 WG1686163
Tetrahydrofuran 109-99-9 72.10 0.200 0.590 ND ND 1 WG1686163
Toluene 108-88-3 92.10 0.500 1.88 ND ND 1 WG1686163
1,2,4-Trichlorobenzene 120-82-1 181 0.630 4.66 ND ND 1 WG1686163
1,1,1-Trichloroethane 71-55-6 133 0.200 1.09 ND ND 1 WG1686163
1,1,2-Trichloroethane 79-00-5 133 0.200 1.09 ND ND 1 WG1686163
Trichloroethylene 79-01-6 131 0.200 1.07 ND ND 1 WG1686163
1,2,4-Trimethylbenzene 95-63-6 120 0.200 0.982 ND ND 1 WG1686163
1,3,5-Trimethylbenzene 108-67-8 120 0.200 0.982 ND ND 1 WG1686163
2,2,4-Trimethylpentane 540-84-1 114.22 0.200 0.934 ND ND 1 WG1686163
Vinyl chloride 75-01-4 62.50 0.200 0.511 ND ND 1 WG1686163
Vinyl Bromide 593-60-2 106.95 0.200 0.875 ND ND 1 WG1686163
Vinyl acetate 108-05-4 86.10 0.200 0.704 ND ND 1 WG1686163
m&p-Xylene 1330-20-7 106 0.400 1.73 ND ND 1 WG1686163
o-Xylene 95-47-6 106 0.200 0.867 ND ND 1 WG1686163
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 92.1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 03
L1363895
SVP-3
Collected date/time: 06/08/21 15:21
Volatile Organic Compounds (GC) by Method 8015M
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppmv mg/m3 ppmv mg/m3
Methane 74-82-8 16 10.0 6.54 ND ND 1 WG1686733
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 1.25 2.97 1.90 4.51 1 WG1686163
Allyl chloride 107-05-1 76.53 0.200 0.626 ND ND 1 WG1686163
Benzene 71-43-2 78.10 0.200 0.639 ND ND 1 WG1686163
Benzyl Chloride 100-44-7 127 0.200 1.04 ND ND 1 WG1686163
Bromodichloromethane 75-27-4 164 0.200 1.34 ND ND 1 WG1686163
Bromoform 75-25-2 253 0.600 6.21 ND ND 1 WG1686163
Bromomethane 74-83-9 94.90 0.200 0.776 ND ND 1 WG1686163
1,3-Butadiene 106-99-0 54.10 2.00 4.43 ND ND 1 WG1686163
Carbon disulfide 75-15-0 76.10 0.200 0.622 ND ND 1 WG1686163
Carbon tetrachloride 56-23-5 154 0.200 1.26 ND ND 1 WG1686163
Chlorobenzene 108-90-7 113 0.200 0.924 ND ND 1 WG1686163
Chloroethane 75-00-3 64.50 0.200 0.528 ND ND 1 WG1686163
Chloroform 67-66-3 119 0.200 0.973 ND ND 1 WG1686163
Chloromethane 74-87-3 50.50 0.200 0.413 ND ND 1 WG1686163
2-Chlorotoluene 95-49-8 126 0.200 1.03 ND ND 1 WG1686163
Cyclohexane 110-82-7 84.20 0.200 0.689 ND ND 1 WG1686163
Dibromochloromethane 124-48-1 208 0.200 1.70 ND ND 1 WG1686163
1,2-Dibromoethane 106-93-4 188 0.200 1.54 ND ND 1 WG1686163
1,2-Dichlorobenzene 95-50-1 147 0.200 1.20 ND ND 1 WG1686163
1,3-Dichlorobenzene 541-73-1 147 0.200 1.20 ND ND 1 WG1686163
1,4-Dichlorobenzene 106-46-7 147 0.200 1.20 ND ND 1 WG1686163
1,2-Dichloroethane 107-06-2 99 0.200 0.810 ND ND 1 WG1686163
1,1-Dichloroethane 75-34-3 98 0.200 0.802 ND ND 1 WG1686163
1,1-Dichloroethene 75-35-4 96.90 0.200 0.793 ND ND 1 WG1686163
cis-1,2-Dichloroethene 156-59-2 96.90 0.200 0.793 ND ND 1 WG1686163
trans-1,2-Dichloroethene 156-60-5 96.90 0.200 0.793 ND ND 1 WG1686163
1,2-Dichloropropane 78-87-5 113 0.200 0.924 ND ND 1 WG1686163
cis-1,3-Dichloropropene 10061-01-5 111 0.200 0.908 ND ND 1 WG1686163
trans-1,3-Dichloropropene 10061-02-6 111 0.200 0.908 ND ND 1 WG1686163
1,4-Dioxane 123-91-1 88.10 0.200 0.721 ND ND 1 WG1686163
Ethanol 64-17-5 46.10 1.25 2.36 5.35 10.1 B 1 WG1686163
Ethylbenzene 100-41-4 106 0.200 0.867 ND ND 1 WG1686163
4-Ethyltoluene 622-96-8 120 0.200 0.982 ND ND 1 WG1686163
Trichlorofluoromethane 75-69-4 137.40 0.200 1.12 2.19 12.3 1 WG1686163
Dichlorodifluoromethane 75-71-8 120.92 0.200 0.989 12.9 63.8 1 WG1686163
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.200 1.53 ND ND 1 WG1686163
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.200 1.40 ND ND 1 WG1686163
Heptane 142-82-5 100 0.200 0.818 ND ND 1 WG1686163
Hexachloro-1,3-butadiene 87-68-3 261 0.630 6.73 ND ND 1 WG1686163
n-Hexane 110-54-3 86.20 0.630 2.22 ND ND 1 WG1686163
Isopropylbenzene 98-82-8 120.20 0.200 0.983 ND ND 1 WG1686163
Methylene Chloride 75-09-2 84.90 0.200 0.694 ND ND 1 WG1686163
Methyl Butyl Ketone 591-78-6 100 1.25 5.11 ND ND 1 WG1686163
2-Butanone (MEK)78-93-3 72.10 1.25 3.69 ND ND 1 WG1686163
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 1.25 5.12 ND ND 1 WG1686163
Methyl methacrylate 80-62-6 100.12 0.200 0.819 ND ND 1 WG1686163
MTBE 1634-04-4 88.10 0.200 0.721 ND ND 1 WG1686163
Naphthalene 91-20-3 128 0.630 3.30 ND ND 1 WG1686163
2-Propanol 67-63-0 60.10 1.25 3.07 ND ND 1 WG1686163
Propene 115-07-1 42.10 1.25 2.15 ND ND 1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 20:05 10 of 29
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 21:53 10 of 29
SAMPLE RESULTS - 03
L1363895
SVP-3
Collected date/time: 06/08/21 15:21
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Styrene 100-42-5 104 0.200 0.851 ND ND 1 WG1686163
1,1,2,2-Tetrachloroethane 79-34-5 168 0.200 1.37 ND ND 1 WG1686163
Tetrachloroethylene 127-18-4 166 0.200 1.36 0.623 4.23 1 WG1686163
Tetrahydrofuran 109-99-9 72.10 0.200 0.590 ND ND 1 WG1686163
Toluene 108-88-3 92.10 0.500 1.88 ND 1.88 1 WG1686163
1,2,4-Trichlorobenzene 120-82-1 181 0.630 4.66 ND ND 1 WG1686163
1,1,1-Trichloroethane 71-55-6 133 0.200 1.09 ND ND 1 WG1686163
1,1,2-Trichloroethane 79-00-5 133 0.200 1.09 ND ND 1 WG1686163
Trichloroethylene 79-01-6 131 0.200 1.07 ND ND 1 WG1686163
1,2,4-Trimethylbenzene 95-63-6 120 0.200 0.982 ND ND 1 WG1686163
1,3,5-Trimethylbenzene 108-67-8 120 0.200 0.982 ND ND 1 WG1686163
2,2,4-Trimethylpentane 540-84-1 114.22 0.200 0.934 ND ND 1 WG1686163
Vinyl chloride 75-01-4 62.50 0.200 0.511 ND ND 1 WG1686163
Vinyl Bromide 593-60-2 106.95 0.200 0.875 ND ND 1 WG1686163
Vinyl acetate 108-05-4 86.10 0.200 0.704 ND ND 1 WG1686163
m&p-Xylene 1330-20-7 106 0.400 1.73 ND ND 1 WG1686163
o-Xylene 95-47-6 106 0.200 0.867 ND ND 1 WG1686163
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 93.7 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 20:05 11 of 29
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 21:53 11 of 29
SAMPLE RESULTS - 04
L1363895
SVP-4
Collected date/time: 06/08/21 16:14
Volatile Organic Compounds (GC) by Method 8015M
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppmv mg/m3 ppmv mg/m3
Methane 74-82-8 16 10.0 6.54 ND ND 1 WG1686733
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 1.25 2.97 2.80 6.65 1 WG1686163
Allyl chloride 107-05-1 76.53 0.200 0.626 ND ND 1 WG1686163
Benzene 71-43-2 78.10 0.200 0.639 ND ND 1 WG1686163
Benzyl Chloride 100-44-7 127 0.200 1.04 ND ND 1 WG1686163
Bromodichloromethane 75-27-4 164 0.200 1.34 ND ND 1 WG1686163
Bromoform 75-25-2 253 0.600 6.21 ND ND 1 WG1686163
Bromomethane 74-83-9 94.90 0.200 0.776 ND ND 1 WG1686163
1,3-Butadiene 106-99-0 54.10 2.00 4.43 ND ND 1 WG1686163
Carbon disulfide 75-15-0 76.10 0.200 0.622 ND ND 1 WG1686163
Carbon tetrachloride 56-23-5 154 0.200 1.26 ND ND 1 WG1686163
Chlorobenzene 108-90-7 113 0.200 0.924 ND ND 1 WG1686163
Chloroethane 75-00-3 64.50 0.200 0.528 ND ND 1 WG1686163
Chloroform 67-66-3 119 0.200 0.973 0.565 2.75 1 WG1686163
Chloromethane 74-87-3 50.50 0.200 0.413 ND ND 1 WG1686163
2-Chlorotoluene 95-49-8 126 0.200 1.03 ND ND 1 WG1686163
Cyclohexane 110-82-7 84.20 0.200 0.689 ND ND 1 WG1686163
Dibromochloromethane 124-48-1 208 0.200 1.70 ND ND 1 WG1686163
1,2-Dibromoethane 106-93-4 188 0.200 1.54 ND ND 1 WG1686163
1,2-Dichlorobenzene 95-50-1 147 0.200 1.20 ND ND 1 WG1686163
1,3-Dichlorobenzene 541-73-1 147 0.200 1.20 ND ND 1 WG1686163
1,4-Dichlorobenzene 106-46-7 147 0.200 1.20 ND ND 1 WG1686163
1,2-Dichloroethane 107-06-2 99 0.200 0.810 ND ND 1 WG1686163
1,1-Dichloroethane 75-34-3 98 0.200 0.802 ND ND 1 WG1686163
1,1-Dichloroethene 75-35-4 96.90 0.200 0.793 ND ND 1 WG1686163
cis-1,2-Dichloroethene 156-59-2 96.90 0.200 0.793 ND ND 1 WG1686163
trans-1,2-Dichloroethene 156-60-5 96.90 0.200 0.793 ND ND 1 WG1686163
1,2-Dichloropropane 78-87-5 113 0.200 0.924 ND ND 1 WG1686163
cis-1,3-Dichloropropene 10061-01-5 111 0.200 0.908 ND ND 1 WG1686163
trans-1,3-Dichloropropene 10061-02-6 111 0.200 0.908 ND ND 1 WG1686163
1,4-Dioxane 123-91-1 88.10 0.200 0.721 ND ND 1 WG1686163
Ethanol 64-17-5 46.10 1.25 2.36 16.3 30.7 1 WG1686163
Ethylbenzene 100-41-4 106 0.200 0.867 ND ND 1 WG1686163
4-Ethyltoluene 622-96-8 120 0.200 0.982 ND ND 1 WG1686163
Trichlorofluoromethane 75-69-4 137.40 0.200 1.12 18.5 104 1 WG1686163
Dichlorodifluoromethane 75-71-8 120.92 0.200 0.989 6.26 31.0 1 WG1686163
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.200 1.53 ND ND 1 WG1686163
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.200 1.40 ND ND 1 WG1686163
Heptane 142-82-5 100 0.200 0.818 ND ND 1 WG1686163
Hexachloro-1,3-butadiene 87-68-3 261 0.630 6.73 ND ND 1 WG1686163
n-Hexane 110-54-3 86.20 0.630 2.22 ND ND 1 WG1686163
Isopropylbenzene 98-82-8 120.20 0.200 0.983 ND ND 1 WG1686163
Methylene Chloride 75-09-2 84.90 0.200 0.694 ND ND 1 WG1686163
Methyl Butyl Ketone 591-78-6 100 1.25 5.11 ND ND 1 WG1686163
2-Butanone (MEK)78-93-3 72.10 1.25 3.69 ND ND 1 WG1686163
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 1.25 5.12 ND ND 1 WG1686163
Methyl methacrylate 80-62-6 100.12 0.200 0.819 ND ND 1 WG1686163
MTBE 1634-04-4 88.10 0.200 0.721 ND ND 1 WG1686163
Naphthalene 91-20-3 128 0.630 3.30 ND ND 1 WG1686163
2-Propanol 67-63-0 60.10 1.25 3.07 1.44 3.54 1 WG1686163
Propene 115-07-1 42.10 1.25 2.15 ND ND 1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 20:05 12 of 29
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 21:53 12 of 29
SAMPLE RESULTS - 04
L1363895
SVP-4
Collected date/time: 06/08/21 16:14
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Styrene 100-42-5 104 0.200 0.851 ND ND 1 WG1686163
1,1,2,2-Tetrachloroethane 79-34-5 168 0.200 1.37 ND ND 1 WG1686163
Tetrachloroethylene 127-18-4 166 0.200 1.36 0.227 1.54 1 WG1686163
Tetrahydrofuran 109-99-9 72.10 0.200 0.590 ND ND 1 WG1686163
Toluene 108-88-3 92.10 0.500 1.88 0.907 3.42 1 WG1686163
1,2,4-Trichlorobenzene 120-82-1 181 0.630 4.66 ND ND 1 WG1686163
1,1,1-Trichloroethane 71-55-6 133 0.200 1.09 ND ND 1 WG1686163
1,1,2-Trichloroethane 79-00-5 133 0.200 1.09 ND ND 1 WG1686163
Trichloroethylene 79-01-6 131 0.200 1.07 ND ND 1 WG1686163
1,2,4-Trimethylbenzene 95-63-6 120 0.200 0.982 0.267 1.31 1 WG1686163
1,3,5-Trimethylbenzene 108-67-8 120 0.200 0.982 ND ND 1 WG1686163
2,2,4-Trimethylpentane 540-84-1 114.22 0.200 0.934 ND ND 1 WG1686163
Vinyl chloride 75-01-4 62.50 0.200 0.511 ND ND 1 WG1686163
Vinyl Bromide 593-60-2 106.95 0.200 0.875 ND ND 1 WG1686163
Vinyl acetate 108-05-4 86.10 0.200 0.704 ND ND 1 WG1686163
m&p-Xylene 1330-20-7 106 0.400 1.73 0.542 2.35 1 WG1686163
o-Xylene 95-47-6 106 0.200 0.867 ND ND 1 WG1686163
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 91.4 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 20:05 13 of 29
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 21:53 13 of 29
SAMPLE RESULTS - 05
L1363895
SVP-5
Collected date/time: 06/08/21 16:25
Volatile Organic Compounds (GC) by Method 8015M
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppmv mg/m3 ppmv mg/m3
Methane 74-82-8 16 10.0 6.54 ND ND 1 WG1686733
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 1.25 2.97 7.86 18.7 1 WG1686163
Allyl chloride 107-05-1 76.53 0.200 0.626 ND ND 1 WG1686163
Benzene 71-43-2 78.10 0.200 0.639 ND ND 1 WG1686163
Benzyl Chloride 100-44-7 127 0.200 1.04 ND ND 1 WG1686163
Bromodichloromethane 75-27-4 164 0.200 1.34 ND ND 1 WG1686163
Bromoform 75-25-2 253 0.600 6.21 ND ND 1 WG1686163
Bromomethane 74-83-9 94.90 0.200 0.776 ND ND 1 WG1686163
1,3-Butadiene 106-99-0 54.10 2.00 4.43 ND ND 1 WG1686163
Carbon disulfide 75-15-0 76.10 0.200 0.622 ND ND 1 WG1686163
Carbon tetrachloride 56-23-5 154 0.200 1.26 ND ND 1 WG1686163
Chlorobenzene 108-90-7 113 0.200 0.924 ND ND 1 WG1686163
Chloroethane 75-00-3 64.50 0.200 0.528 ND ND 1 WG1686163
Chloroform 67-66-3 119 0.200 0.973 ND ND 1 WG1686163
Chloromethane 74-87-3 50.50 0.200 0.413 0.451 0.932 1 WG1686163
2-Chlorotoluene 95-49-8 126 0.200 1.03 ND ND 1 WG1686163
Cyclohexane 110-82-7 84.20 0.200 0.689 ND ND 1 WG1686163
Dibromochloromethane 124-48-1 208 0.200 1.70 ND ND 1 WG1686163
1,2-Dibromoethane 106-93-4 188 0.200 1.54 ND ND 1 WG1686163
1,2-Dichlorobenzene 95-50-1 147 0.200 1.20 ND ND 1 WG1686163
1,3-Dichlorobenzene 541-73-1 147 0.200 1.20 ND ND 1 WG1686163
1,4-Dichlorobenzene 106-46-7 147 0.200 1.20 ND ND 1 WG1686163
1,2-Dichloroethane 107-06-2 99 0.200 0.810 ND ND 1 WG1686163
1,1-Dichloroethane 75-34-3 98 0.200 0.802 ND ND 1 WG1686163
1,1-Dichloroethene 75-35-4 96.90 0.200 0.793 ND ND 1 WG1686163
cis-1,2-Dichloroethene 156-59-2 96.90 0.200 0.793 ND ND 1 WG1686163
trans-1,2-Dichloroethene 156-60-5 96.90 0.200 0.793 ND ND 1 WG1686163
1,2-Dichloropropane 78-87-5 113 0.200 0.924 ND ND 1 WG1686163
cis-1,3-Dichloropropene 10061-01-5 111 0.200 0.908 ND ND 1 WG1686163
trans-1,3-Dichloropropene 10061-02-6 111 0.200 0.908 ND ND 1 WG1686163
1,4-Dioxane 123-91-1 88.10 0.200 0.721 ND ND 1 WG1686163
Ethanol 64-17-5 46.10 1.25 2.36 5.79 10.9 B 1 WG1686163
Ethylbenzene 100-41-4 106 0.200 0.867 ND ND 1 WG1686163
4-Ethyltoluene 622-96-8 120 0.200 0.982 ND ND 1 WG1686163
Trichlorofluoromethane 75-69-4 137.40 0.200 1.12 36.1 203 1 WG1686163
Dichlorodifluoromethane 75-71-8 120.92 0.200 0.989 5.02 24.8 1 WG1686163
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.200 1.53 ND ND 1 WG1686163
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.200 1.40 ND ND 1 WG1686163
Heptane 142-82-5 100 0.200 0.818 ND ND 1 WG1686163
Hexachloro-1,3-butadiene 87-68-3 261 0.630 6.73 ND ND 1 WG1686163
n-Hexane 110-54-3 86.20 0.630 2.22 ND ND 1 WG1686163
Isopropylbenzene 98-82-8 120.20 0.200 0.983 ND ND 1 WG1686163
Methylene Chloride 75-09-2 84.90 0.200 0.694 ND ND 1 WG1686163
Methyl Butyl Ketone 591-78-6 100 1.25 5.11 ND ND 1 WG1686163
2-Butanone (MEK)78-93-3 72.10 1.25 3.69 1.30 3.83 1 WG1686163
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 1.25 5.12 ND ND 1 WG1686163
Methyl methacrylate 80-62-6 100.12 0.200 0.819 ND ND 1 WG1686163
MTBE 1634-04-4 88.10 0.200 0.721 ND ND 1 WG1686163
Naphthalene 91-20-3 128 0.630 3.30 ND ND 1 WG1686163
2-Propanol 67-63-0 60.10 1.25 3.07 2.88 7.08 1 WG1686163
Propene 115-07-1 42.10 1.25 2.15 ND ND 1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 20:05 14 of 29
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 21:53 14 of 29
SAMPLE RESULTS - 05
L1363895
SVP-5
Collected date/time: 06/08/21 16:25
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Styrene 100-42-5 104 0.200 0.851 ND ND 1 WG1686163
1,1,2,2-Tetrachloroethane 79-34-5 168 0.200 1.37 ND ND 1 WG1686163
Tetrachloroethylene 127-18-4 166 0.200 1.36 0.230 1.56 1 WG1686163
Tetrahydrofuran 109-99-9 72.10 0.200 0.590 ND ND 1 WG1686163
Toluene 108-88-3 92.10 0.500 1.88 1.00 3.77 1 WG1686163
1,2,4-Trichlorobenzene 120-82-1 181 0.630 4.66 ND ND 1 WG1686163
1,1,1-Trichloroethane 71-55-6 133 0.200 1.09 ND ND 1 WG1686163
1,1,2-Trichloroethane 79-00-5 133 0.200 1.09 ND ND 1 WG1686163
Trichloroethylene 79-01-6 131 0.200 1.07 ND ND 1 WG1686163
1,2,4-Trimethylbenzene 95-63-6 120 0.200 0.982 ND ND 1 WG1686163
1,3,5-Trimethylbenzene 108-67-8 120 0.200 0.982 ND ND 1 WG1686163
2,2,4-Trimethylpentane 540-84-1 114.22 0.200 0.934 ND ND 1 WG1686163
Vinyl chloride 75-01-4 62.50 0.200 0.511 ND ND 1 WG1686163
Vinyl Bromide 593-60-2 106.95 0.200 0.875 ND ND 1 WG1686163
Vinyl acetate 108-05-4 86.10 0.200 0.704 ND ND 1 WG1686163
m&p-Xylene 1330-20-7 106 0.400 1.73 0.499 2.16 1 WG1686163
o-Xylene 95-47-6 106 0.200 0.867 ND ND 1 WG1686163
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 91.6 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 20:05 15 of 29
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Terracon - Greensboro, NC 75217005 L1363895 06/11/21 21:53 15 of 29
SAMPLE RESULTS - 06
L1363895
SVP-6
Collected date/time: 06/08/21 16:48
Volatile Organic Compounds (GC) by Method 8015M
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppmv mg/m3 ppmv mg/m3
Methane 74-82-8 16 10.0 6.54 ND ND 1 WG1686733
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 1.25 2.97 4.85 11.5 1 WG1686163
Allyl chloride 107-05-1 76.53 0.200 0.626 ND ND 1 WG1686163
Benzene 71-43-2 78.10 0.200 0.639 2.83 9.04 1 WG1686163
Benzyl Chloride 100-44-7 127 0.200 1.04 ND ND 1 WG1686163
Bromodichloromethane 75-27-4 164 0.200 1.34 ND ND 1 WG1686163
Bromoform 75-25-2 253 0.600 6.21 ND ND 1 WG1686163
Bromomethane 74-83-9 94.90 0.200 0.776 ND ND 1 WG1686163
1,3-Butadiene 106-99-0 54.10 2.00 4.43 ND ND 1 WG1686163
Carbon disulfide 75-15-0 76.10 0.200 0.622 ND ND 1 WG1686163
Carbon tetrachloride 56-23-5 154 0.200 1.26 ND ND 1 WG1686163
Chlorobenzene 108-90-7 113 0.200 0.924 ND ND 1 WG1686163
Chloroethane 75-00-3 64.50 0.200 0.528 ND ND 1 WG1686163
Chloroform 67-66-3 119 0.200 0.973 ND ND 1 WG1686163
Chloromethane 74-87-3 50.50 0.200 0.413 ND ND 1 WG1686163
2-Chlorotoluene 95-49-8 126 0.200 1.03 ND ND 1 WG1686163
Cyclohexane 110-82-7 84.20 0.200 0.689 ND ND 1 WG1686163
Dibromochloromethane 124-48-1 208 0.200 1.70 ND ND 1 WG1686163
1,2-Dibromoethane 106-93-4 188 0.200 1.54 ND ND 1 WG1686163
1,2-Dichlorobenzene 95-50-1 147 0.200 1.20 ND ND 1 WG1686163
1,3-Dichlorobenzene 541-73-1 147 0.200 1.20 ND ND 1 WG1686163
1,4-Dichlorobenzene 106-46-7 147 0.200 1.20 ND ND 1 WG1686163
1,2-Dichloroethane 107-06-2 99 0.200 0.810 ND ND 1 WG1686163
1,1-Dichloroethane 75-34-3 98 0.200 0.802 ND ND 1 WG1686163
1,1-Dichloroethene 75-35-4 96.90 0.200 0.793 ND ND 1 WG1686163
cis-1,2-Dichloroethene 156-59-2 96.90 0.200 0.793 ND ND 1 WG1686163
trans-1,2-Dichloroethene 156-60-5 96.90 0.200 0.793 ND ND 1 WG1686163
1,2-Dichloropropane 78-87-5 113 0.200 0.924 ND ND 1 WG1686163
cis-1,3-Dichloropropene 10061-01-5 111 0.200 0.908 ND ND 1 WG1686163
trans-1,3-Dichloropropene 10061-02-6 111 0.200 0.908 ND ND 1 WG1686163
1,4-Dioxane 123-91-1 88.10 0.200 0.721 ND ND 1 WG1686163
Ethanol 64-17-5 46.10 1.25 2.36 4.39 8.28 B 1 WG1686163
Ethylbenzene 100-41-4 106 0.200 0.867 0.974 4.22 1 WG1686163
4-Ethyltoluene 622-96-8 120 0.200 0.982 0.829 4.07 1 WG1686163
Trichlorofluoromethane 75-69-4 137.40 0.200 1.12 33.4 188 1 WG1686163
Dichlorodifluoromethane 75-71-8 120.92 0.200 0.989 1.60 7.91 1 WG1686163
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.200 1.53 ND ND 1 WG1686163
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.200 1.40 ND ND 1 WG1686163
Heptane 142-82-5 100 0.200 0.818 0.223 0.912 1 WG1686163
Hexachloro-1,3-butadiene 87-68-3 261 0.630 6.73 ND ND 1 WG1686163
n-Hexane 110-54-3 86.20 0.630 2.22 ND ND 1 WG1686163
Isopropylbenzene 98-82-8 120.20 0.200 0.983 ND ND 1 WG1686163
Methylene Chloride 75-09-2 84.90 0.200 0.694 ND ND 1 WG1686163
Methyl Butyl Ketone 591-78-6 100 1.25 5.11 ND ND 1 WG1686163
2-Butanone (MEK)78-93-3 72.10 1.25 3.69 ND ND 1 WG1686163
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 1.25 5.12 ND ND 1 WG1686163
Methyl methacrylate 80-62-6 100.12 0.200 0.819 ND ND 1 WG1686163
MTBE 1634-04-4 88.10 0.200 0.721 ND ND 1 WG1686163
Naphthalene 91-20-3 128 0.630 3.30 ND ND 1 WG1686163
2-Propanol 67-63-0 60.10 1.25 3.07 ND ND 1 WG1686163
Propene 115-07-1 42.10 1.25 2.15 8.80 15.2 1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 06
L1363895
SVP-6
Collected date/time: 06/08/21 16:48
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Styrene 100-42-5 104 0.200 0.851 ND ND 1 WG1686163
1,1,2,2-Tetrachloroethane 79-34-5 168 0.200 1.37 ND ND 1 WG1686163
Tetrachloroethylene 127-18-4 166 0.200 1.36 1.82 12.4 1 WG1686163
Tetrahydrofuran 109-99-9 72.10 0.200 0.590 ND ND 1 WG1686163
Toluene 108-88-3 92.10 0.500 1.88 10.1 38.0 1 WG1686163
1,2,4-Trichlorobenzene 120-82-1 181 0.630 4.66 ND ND 1 WG1686163
1,1,1-Trichloroethane 71-55-6 133 0.200 1.09 ND ND 1 WG1686163
1,1,2-Trichloroethane 79-00-5 133 0.200 1.09 ND ND 1 WG1686163
Trichloroethylene 79-01-6 131 0.200 1.07 ND ND 1 WG1686163
1,2,4-Trimethylbenzene 95-63-6 120 0.200 0.982 0.913 4.48 1 WG1686163
1,3,5-Trimethylbenzene 108-67-8 120 0.200 0.982 0.255 1.25 1 WG1686163
2,2,4-Trimethylpentane 540-84-1 114.22 0.200 0.934 ND ND 1 WG1686163
Vinyl chloride 75-01-4 62.50 0.200 0.511 ND ND 1 WG1686163
Vinyl Bromide 593-60-2 106.95 0.200 0.875 ND ND 1 WG1686163
Vinyl acetate 108-05-4 86.10 0.200 0.704 ND ND 1 WG1686163
m&p-Xylene 1330-20-7 106 0.400 1.73 4.46 19.3 1 WG1686163
o-Xylene 95-47-6 106 0.200 0.867 1.20 5.20 1 WG1686163
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 93.6 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 07
L1363895
SVP-7
Collected date/time: 06/08/21 17:13
Volatile Organic Compounds (GC) by Method 8015M
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppmv mg/m3 ppmv mg/m3
Methane 74-82-8 16 10.0 6.54 ND ND 1 WG1686733
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 1.25 2.97 8.35 19.8 1 WG1686163
Allyl chloride 107-05-1 76.53 0.200 0.626 ND ND 1 WG1686163
Benzene 71-43-2 78.10 0.200 0.639 0.543 1.73 1 WG1686163
Benzyl Chloride 100-44-7 127 0.200 1.04 ND ND 1 WG1686163
Bromodichloromethane 75-27-4 164 0.200 1.34 ND ND 1 WG1686163
Bromoform 75-25-2 253 0.600 6.21 ND ND 1 WG1686163
Bromomethane 74-83-9 94.90 0.200 0.776 ND ND 1 WG1686163
1,3-Butadiene 106-99-0 54.10 2.00 4.43 ND ND 1 WG1686163
Carbon disulfide 75-15-0 76.10 0.200 0.622 1.59 4.95 1 WG1686163
Carbon tetrachloride 56-23-5 154 0.200 1.26 ND ND 1 WG1686163
Chlorobenzene 108-90-7 113 0.200 0.924 ND ND 1 WG1686163
Chloroethane 75-00-3 64.50 0.200 0.528 ND ND 1 WG1686163
Chloroform 67-66-3 119 0.200 0.973 20.0 97.3 1 WG1686163
Chloromethane 74-87-3 50.50 0.200 0.413 ND ND 1 WG1686163
2-Chlorotoluene 95-49-8 126 0.200 1.03 ND ND 1 WG1686163
Cyclohexane 110-82-7 84.20 0.200 0.689 0.218 0.751 1 WG1686163
Dibromochloromethane 124-48-1 208 0.200 1.70 ND ND 1 WG1686163
1,2-Dibromoethane 106-93-4 188 0.200 1.54 ND ND 1 WG1686163
1,2-Dichlorobenzene 95-50-1 147 0.200 1.20 ND ND 1 WG1686163
1,3-Dichlorobenzene 541-73-1 147 0.200 1.20 ND ND 1 WG1686163
1,4-Dichlorobenzene 106-46-7 147 0.200 1.20 ND ND 1 WG1686163
1,2-Dichloroethane 107-06-2 99 0.200 0.810 ND ND 1 WG1686163
1,1-Dichloroethane 75-34-3 98 0.200 0.802 ND ND 1 WG1686163
1,1-Dichloroethene 75-35-4 96.90 0.200 0.793 ND ND 1 WG1686163
cis-1,2-Dichloroethene 156-59-2 96.90 0.200 0.793 ND ND 1 WG1686163
trans-1,2-Dichloroethene 156-60-5 96.90 0.200 0.793 ND ND 1 WG1686163
1,2-Dichloropropane 78-87-5 113 0.200 0.924 ND ND 1 WG1686163
cis-1,3-Dichloropropene 10061-01-5 111 0.200 0.908 ND ND 1 WG1686163
trans-1,3-Dichloropropene 10061-02-6 111 0.200 0.908 ND ND 1 WG1686163
1,4-Dioxane 123-91-1 88.10 0.200 0.721 ND ND 1 WG1686163
Ethanol 64-17-5 46.10 1.25 2.36 6.18 11.7 1 WG1686163
Ethylbenzene 100-41-4 106 0.200 0.867 0.621 2.69 1 WG1686163
4-Ethyltoluene 622-96-8 120 0.200 0.982 ND ND 1 WG1686163
Trichlorofluoromethane 75-69-4 137.40 0.200 1.12 6.57 36.9 1 WG1686163
Dichlorodifluoromethane 75-71-8 120.92 0.200 0.989 11.1 54.9 1 WG1686163
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.200 1.53 ND ND 1 WG1686163
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.200 1.40 ND ND 1 WG1686163
Heptane 142-82-5 100 0.200 0.818 0.267 1.09 1 WG1686163
Hexachloro-1,3-butadiene 87-68-3 261 0.630 6.73 ND ND 1 WG1686163
n-Hexane 110-54-3 86.20 0.630 2.22 ND ND 1 WG1686163
Isopropylbenzene 98-82-8 120.20 0.200 0.983 ND ND 1 WG1686163
Methylene Chloride 75-09-2 84.90 0.200 0.694 0.570 1.98 1 WG1686163
Methyl Butyl Ketone 591-78-6 100 1.25 5.11 ND ND 1 WG1686163
2-Butanone (MEK)78-93-3 72.10 1.25 3.69 1.71 5.04 1 WG1686163
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 1.25 5.12 ND ND 1 WG1686163
Methyl methacrylate 80-62-6 100.12 0.200 0.819 ND ND 1 WG1686163
MTBE 1634-04-4 88.10 0.200 0.721 ND ND 1 WG1686163
Naphthalene 91-20-3 128 0.630 3.30 ND ND 1 WG1686163
2-Propanol 67-63-0 60.10 1.25 3.07 ND ND 1 WG1686163
Propene 115-07-1 42.10 1.25 2.15 11.4 19.6 1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 07
L1363895
SVP-7
Collected date/time: 06/08/21 17:13
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Styrene 100-42-5 104 0.200 0.851 0.223 0.949 1 WG1686163
1,1,2,2-Tetrachloroethane 79-34-5 168 0.200 1.37 ND ND 1 WG1686163
Tetrachloroethylene 127-18-4 166 0.200 1.36 1.62 11.0 1 WG1686163
Tetrahydrofuran 109-99-9 72.10 0.200 0.590 ND ND 1 WG1686163
Toluene 108-88-3 92.10 0.500 1.88 3.19 12.0 1 WG1686163
1,2,4-Trichlorobenzene 120-82-1 181 0.630 4.66 ND ND 1 WG1686163
1,1,1-Trichloroethane 71-55-6 133 0.200 1.09 ND ND 1 WG1686163
1,1,2-Trichloroethane 79-00-5 133 0.200 1.09 ND ND 1 WG1686163
Trichloroethylene 79-01-6 131 0.200 1.07 ND ND 1 WG1686163
1,2,4-Trimethylbenzene 95-63-6 120 0.200 0.982 0.258 1.27 1 WG1686163
1,3,5-Trimethylbenzene 108-67-8 120 0.200 0.982 ND ND 1 WG1686163
2,2,4-Trimethylpentane 540-84-1 114.22 0.200 0.934 ND ND 1 WG1686163
Vinyl chloride 75-01-4 62.50 0.200 0.511 ND ND 1 WG1686163
Vinyl Bromide 593-60-2 106.95 0.200 0.875 ND ND 1 WG1686163
Vinyl acetate 108-05-4 86.10 0.200 0.704 ND ND 1 WG1686163
m&p-Xylene 1330-20-7 106 0.400 1.73 2.11 9.15 1 WG1686163
o-Xylene 95-47-6 106 0.200 0.867 0.747 3.24 1 WG1686163
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 93.3 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 08
L1363895
SVP-8
Collected date/time: 06/08/21 17:32
Volatile Organic Compounds (GC) by Method 8015M
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppmv mg/m3 ppmv mg/m3
Methane 74-82-8 16 10.0 6.54 ND ND 1 WG1686733
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 1.25 2.97 5.45 13.0 1 WG1686163
Allyl chloride 107-05-1 76.53 0.200 0.626 ND ND 1 WG1686163
Benzene 71-43-2 78.10 0.200 0.639 ND ND 1 WG1686163
Benzyl Chloride 100-44-7 127 0.200 1.04 ND ND 1 WG1686163
Bromodichloromethane 75-27-4 164 0.200 1.34 ND ND 1 WG1686163
Bromoform 75-25-2 253 0.600 6.21 ND ND 1 WG1686163
Bromomethane 74-83-9 94.90 0.200 0.776 ND ND 1 WG1686163
1,3-Butadiene 106-99-0 54.10 2.00 4.43 ND ND 1 WG1686163
Carbon disulfide 75-15-0 76.10 0.200 0.622 ND ND 1 WG1686163
Carbon tetrachloride 56-23-5 154 0.200 1.26 ND ND 1 WG1686163
Chlorobenzene 108-90-7 113 0.200 0.924 ND ND 1 WG1686163
Chloroethane 75-00-3 64.50 0.200 0.528 ND ND 1 WG1686163
Chloroform 67-66-3 119 0.200 0.973 0.847 4.12 1 WG1686163
Chloromethane 74-87-3 50.50 0.200 0.413 ND ND 1 WG1686163
2-Chlorotoluene 95-49-8 126 0.200 1.03 ND ND 1 WG1686163
Cyclohexane 110-82-7 84.20 0.200 0.689 ND ND 1 WG1686163
Dibromochloromethane 124-48-1 208 0.200 1.70 ND ND 1 WG1686163
1,2-Dibromoethane 106-93-4 188 0.200 1.54 ND ND 1 WG1686163
1,2-Dichlorobenzene 95-50-1 147 0.200 1.20 ND ND 1 WG1686163
1,3-Dichlorobenzene 541-73-1 147 0.200 1.20 ND ND 1 WG1686163
1,4-Dichlorobenzene 106-46-7 147 0.200 1.20 ND ND 1 WG1686163
1,2-Dichloroethane 107-06-2 99 0.200 0.810 ND ND 1 WG1686163
1,1-Dichloroethane 75-34-3 98 0.200 0.802 ND ND 1 WG1686163
1,1-Dichloroethene 75-35-4 96.90 0.200 0.793 ND ND 1 WG1686163
cis-1,2-Dichloroethene 156-59-2 96.90 0.200 0.793 ND ND 1 WG1686163
trans-1,2-Dichloroethene 156-60-5 96.90 0.200 0.793 ND ND 1 WG1686163
1,2-Dichloropropane 78-87-5 113 0.200 0.924 ND ND 1 WG1686163
cis-1,3-Dichloropropene 10061-01-5 111 0.200 0.908 ND ND 1 WG1686163
trans-1,3-Dichloropropene 10061-02-6 111 0.200 0.908 ND ND 1 WG1686163
1,4-Dioxane 123-91-1 88.10 0.200 0.721 ND ND 1 WG1686163
Ethanol 64-17-5 46.10 1.25 2.36 4.33 8.16 B 1 WG1686163
Ethylbenzene 100-41-4 106 0.200 0.867 ND ND 1 WG1686163
4-Ethyltoluene 622-96-8 120 0.200 0.982 ND ND 1 WG1686163
Trichlorofluoromethane 75-69-4 137.40 0.200 1.12 5.49 30.9 1 WG1686163
Dichlorodifluoromethane 75-71-8 120.92 0.200 0.989 3.11 15.4 1 WG1686163
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 0.200 1.53 ND ND 1 WG1686163
1,2-Dichlorotetrafluoroethane 76-14-2 171 0.200 1.40 ND ND 1 WG1686163
Heptane 142-82-5 100 0.200 0.818 ND ND 1 WG1686163
Hexachloro-1,3-butadiene 87-68-3 261 0.630 6.73 ND ND 1 WG1686163
n-Hexane 110-54-3 86.20 0.630 2.22 ND ND 1 WG1686163
Isopropylbenzene 98-82-8 120.20 0.200 0.983 ND ND 1 WG1686163
Methylene Chloride 75-09-2 84.90 0.200 0.694 ND ND 1 WG1686163
Methyl Butyl Ketone 591-78-6 100 1.25 5.11 ND ND 1 WG1686163
2-Butanone (MEK)78-93-3 72.10 1.25 3.69 ND ND 1 WG1686163
4-Methyl-2-pentanone (MIBK)108-10-1 100.10 1.25 5.12 ND ND 1 WG1686163
Methyl methacrylate 80-62-6 100.12 0.200 0.819 ND ND 1 WG1686163
MTBE 1634-04-4 88.10 0.200 0.721 ND ND 1 WG1686163
Naphthalene 91-20-3 128 0.630 3.30 ND ND 1 WG1686163
2-Propanol 67-63-0 60.10 1.25 3.07 17.6 43.3 1 WG1686163
Propene 115-07-1 42.10 1.25 2.15 ND ND 1 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 08
L1363895
SVP-8
Collected date/time: 06/08/21 17:32
Volatile Organic Compounds (MS) by Method TO-15
CAS #Mol. Wt.RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Styrene 100-42-5 104 0.200 0.851 ND ND 1 WG1686163
1,1,2,2-Tetrachloroethane 79-34-5 168 0.200 1.37 ND ND 1 WG1686163
Tetrachloroethylene 127-18-4 166 0.200 1.36 0.394 2.68 1 WG1686163
Tetrahydrofuran 109-99-9 72.10 0.200 0.590 ND ND 1 WG1686163
Toluene 108-88-3 92.10 0.500 1.88 0.943 3.55 1 WG1686163
1,2,4-Trichlorobenzene 120-82-1 181 0.630 4.66 ND ND 1 WG1686163
1,1,1-Trichloroethane 71-55-6 133 0.200 1.09 ND ND 1 WG1686163
1,1,2-Trichloroethane 79-00-5 133 0.200 1.09 ND ND 1 WG1686163
Trichloroethylene 79-01-6 131 0.200 1.07 ND ND 1 WG1686163
1,2,4-Trimethylbenzene 95-63-6 120 0.200 0.982 ND ND 1 WG1686163
1,3,5-Trimethylbenzene 108-67-8 120 0.200 0.982 ND ND 1 WG1686163
2,2,4-Trimethylpentane 540-84-1 114.22 0.200 0.934 ND ND 1 WG1686163
Vinyl chloride 75-01-4 62.50 0.200 0.511 ND ND 1 WG1686163
Vinyl Bromide 593-60-2 106.95 0.200 0.875 ND ND 1 WG1686163
Vinyl acetate 108-05-4 86.10 0.200 0.704 ND ND 1 WG1686163
m&p-Xylene 1330-20-7 106 0.400 1.73 ND ND 1 WG1686163
o-Xylene 95-47-6 106 0.200 0.867 ND ND 1 WG1686163
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 91.8 WG1686163
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1686733
Volatile Organic Compounds (GC) by Method 8015M L1363895-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3666040-3 06/11/21 09:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ppmv ppmv ppmv
Methane U 6.98 10.0
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3666040-1 06/11/21 09:10 • (LCSD) R3666040-2 06/11/21 09:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppmv ppmv ppmv %%%%%
Methane 500 460 433 92.0 86.6 79.0-115 6.05 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1686163
Volatile Organic Compounds (MS) by Method TO-15 L1363895-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3665984-3 06/10/21 10:49
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Acetone U 0.584 1.25
Allyl Chloride U 0.114 0.200
Benzene U 0.0715 0.200
Benzyl Chloride U 0.0598 0.200
Bromodichloromethane U 0.0702 0.200
Bromoform U 0.0732 0.600
Bromomethane U 0.0982 0.200
1,3-Butadiene U 0.104 2.00
Carbon disulfide U 0.102 0.200
Carbon tetrachloride U 0.0732 0.200
Chlorobenzene U 0.0832 0.200
Chloroethane U 0.0996 0.200
Chloroform U 0.0717 0.200
Chloromethane U 0.103 0.200
2-Chlorotoluene U 0.0828 0.200
Cyclohexane U 0.0753 0.200
Dibromochloromethane U 0.0727 0.200
1,2-Dibromoethane U 0.0721 0.200
1,2-Dichlorobenzene U 0.128 0.200
1,3-Dichlorobenzene U 0.182 0.200
1,4-Dichlorobenzene U 0.0557 0.200
1,2-Dichloroethane U 0.0700 0.200
1,1-Dichloroethane U 0.0723 0.200
1,1-Dichloroethene U 0.0762 0.200
cis-1,2-Dichloroethene U 0.0784 0.200
trans-1,2-Dichloroethene U 0.0673 0.200
1,2-Dichloropropane U 0.0760 0.200
cis-1,3-Dichloropropene U 0.0689 0.200
trans-1,3-Dichloropropene U 0.0728 0.200
1,4-Dioxane U 0.0833 0.200
Ethylbenzene U 0.0835 0.200
4-Ethyltoluene U 0.0783 0.200
Trichlorofluoromethane U 0.0819 0.200
Dichlorodifluoromethane U 0.137 0.200
1,1,2-Trichlorotrifluoroethane U 0.0793 0.200
1,2-Dichlorotetrafluoroethane U 0.0890 0.200
Heptane U 0.104 0.200
Hexachloro-1,3-butadiene U 0.105 0.630
n-Hexane U 0.206 0.630
Isopropylbenzene U 0.0777 0.200
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1686163
Volatile Organic Compounds (MS) by Method TO-15 L1363895-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3665984-3 06/10/21 10:49
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Methylene Chloride U 0.0979 0.200
Methyl Butyl Ketone U 0.133 1.25
2-Butanone (MEK)U 0.0814 1.25
4-Methyl-2-pentanone (MIBK)U 0.0765 1.25
Methyl Methacrylate U 0.0876 0.200
MTBE U 0.0647 0.200
Naphthalene U 0.350 0.630
2-Propanol U 0.264 1.25
Propene U 0.0932 1.25
Styrene U 0.0788 0.200
1,1,2,2-Tetrachloroethane U 0.0743 0.200
Tetrachloroethylene U 0.0814 0.200
Tetrahydrofuran U 0.0734 0.200
Toluene U 0.0870 0.500
1,2,4-Trichlorobenzene U 0.148 0.630
1,1,1-Trichloroethane U 0.0736 0.200
1,1,2-Trichloroethane U 0.0775 0.200
Trichloroethylene U 0.0680 0.200
1,2,4-Trimethylbenzene U 0.0764 0.200
1,3,5-Trimethylbenzene U 0.0779 0.200
2,2,4-Trimethylpentane U 0.133 0.200
Vinyl chloride U 0.0949 0.200
Vinyl Bromide U 0.0852 0.200
Vinyl acetate U 0.116 0.200
m&p-Xylene U 0.135 0.400
o-Xylene U 0.0828 0.200
Ethanol 0.590 J 0.265 1.25
(S) 1,4-Bromofluorobenzene 92.4 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3665984-1 06/10/21 09:30 • (LCSD) R3665984-2 06/10/21 10:10
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Ethanol 3.75 3.41 3.45 90.9 92.0 55.0-148 1.17 25
Propene 3.75 3.13 3.06 83.5 81.6 64.0-144 2.26 25
Dichlorodifluoromethane 3.75 3.90 3.87 104 103 64.0-139 0.772 25
1,2-Dichlorotetrafluoroethane 3.75 3.89 3.86 104 103 70.0-130 0.774 25
Chloromethane 3.75 3.20 3.17 85.3 84.5 70.0-130 0.942 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1686163
Volatile Organic Compounds (MS) by Method TO-15 L1363895-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3665984-1 06/10/21 09:30 • (LCSD) R3665984-2 06/10/21 10:10
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Vinyl chloride 3.75 3.53 3.57 94.1 95.2 70.0-130 1.13 25
1,3-Butadiene 3.75 2.98 2.99 79.5 79.7 70.0-130 0.335 25
Bromomethane 3.75 4.50 4.42 120 118 70.0-130 1.79 25
Chloroethane 3.75 3.75 3.75 100 100 70.0-130 0.000 25
Trichlorofluoromethane 3.75 4.15 4.12 111 110 70.0-130 0.726 25
1,1,2-Trichlorotrifluoroethane 3.75 3.94 3.91 105 104 70.0-130 0.764 25
1,1-Dichloroethene 3.75 3.54 3.50 94.4 93.3 70.0-130 1.14 25
1,1-Dichloroethane 3.75 3.55 3.55 94.7 94.7 70.0-130 0.000 25
Acetone 3.75 3.53 3.49 94.1 93.1 70.0-130 1.14 25
2-Propanol 3.75 3.21 3.21 85.6 85.6 70.0-139 0.000 25
Carbon disulfide 3.75 3.78 3.71 101 98.9 70.0-130 1.87 25
Methylene Chloride 3.75 3.00 2.91 80.0 77.6 70.0-130 3.05 25
MTBE 3.75 3.63 3.60 96.8 96.0 70.0-130 0.830 25
trans-1,2-Dichloroethene 3.75 3.51 3.54 93.6 94.4 70.0-130 0.851 25
n-Hexane 3.75 3.28 3.27 87.5 87.2 70.0-130 0.305 25
Vinyl acetate 3.75 2.65 2.70 70.7 72.0 70.0-130 1.87 25
Methyl Ethyl Ketone 3.75 3.58 3.68 95.5 98.1 70.0-130 2.75 25
cis-1,2-Dichloroethene 3.75 3.48 3.50 92.8 93.3 70.0-130 0.573 25
Chloroform 3.75 3.72 3.76 99.2 100 70.0-130 1.07 25
Cyclohexane 3.75 3.65 3.67 97.3 97.9 70.0-130 0.546 25
1,1,1-Trichloroethane 3.75 3.78 3.77 101 101 70.0-130 0.265 25
Carbon tetrachloride 3.75 3.85 3.86 103 103 70.0-130 0.259 25
Benzene 3.75 3.83 3.87 102 103 70.0-130 1.04 25
1,2-Dichloroethane 3.75 3.69 3.69 98.4 98.4 70.0-130 0.000 25
Heptane 3.75 3.23 3.28 86.1 87.5 70.0-130 1.54 25
Trichloroethylene 3.75 4.03 4.00 107 107 70.0-130 0.747 25
1,2-Dichloropropane 3.75 3.59 3.61 95.7 96.3 70.0-130 0.556 25
1,4-Dioxane 3.75 3.67 3.68 97.9 98.1 70.0-140 0.272 25
Bromodichloromethane 3.75 3.80 3.82 101 102 70.0-130 0.525 25
cis-1,3-Dichloropropene 3.75 3.65 3.63 97.3 96.8 70.0-130 0.549 25
4-Methyl-2-pentanone (MIBK)3.75 3.30 3.32 88.0 88.5 70.0-139 0.604 25
Toluene 3.75 3.91 3.94 104 105 70.0-130 0.764 25
trans-1,3-Dichloropropene 3.75 3.63 3.63 96.8 96.8 70.0-130 0.000 25
1,1,2-Trichloroethane 3.75 4.02 4.04 107 108 70.0-130 0.496 25
Tetrachloroethylene 3.75 4.36 4.36 116 116 70.0-130 0.000 25
Methyl Butyl Ketone 3.75 3.29 3.31 87.7 88.3 70.0-149 0.606 25
Dibromochloromethane 3.75 4.03 4.08 107 109 70.0-130 1.23 25
1,2-Dibromoethane 3.75 4.05 4.09 108 109 70.0-130 0.983 25
Chlorobenzene 3.75 4.15 4.20 111 112 70.0-130 1.20 25
Ethylbenzene 3.75 4.01 4.01 107 107 70.0-130 0.000 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1686163
Volatile Organic Compounds (MS) by Method TO-15 L1363895-01,02,03,04,05,06,07,08
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3665984-1 06/10/21 09:30 • (LCSD) R3665984-2 06/10/21 10:10
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
m&p-Xylene 7.50 7.96 8.01 106 107 70.0-130 0.626 25
o-Xylene 3.75 3.89 3.86 104 103 70.0-130 0.774 25
Styrene 3.75 3.96 3.96 106 106 70.0-130 0.000 25
Bromoform 3.75 4.03 4.04 107 108 70.0-130 0.248 25
1,1,2,2-Tetrachloroethane 3.75 3.86 3.87 103 103 70.0-130 0.259 25
4-Ethyltoluene 3.75 4.07 4.04 109 108 70.0-130 0.740 25
1,3,5-Trimethylbenzene 3.75 4.11 4.09 110 109 70.0-130 0.488 25
1,2,4-Trimethylbenzene 3.75 4.03 4.00 107 107 70.0-130 0.747 25
1,3-Dichlorobenzene 3.75 4.35 4.30 116 115 70.0-130 1.16 25
1,4-Dichlorobenzene 3.75 4.39 4.38 117 117 70.0-130 0.228 25
Benzyl Chloride 3.75 3.56 3.54 94.9 94.4 70.0-152 0.563 25
1,2-Dichlorobenzene 3.75 4.28 4.26 114 114 70.0-130 0.468 25
1,2,4-Trichlorobenzene 3.75 4.25 4.16 113 111 70.0-160 2.14 25
Hexachloro-1,3-butadiene 3.75 4.22 4.11 113 110 70.0-151 2.64 25
Naphthalene 3.75 4.15 4.04 111 108 70.0-159 2.69 25
Allyl Chloride 3.75 3.10 3.02 82.7 80.5 70.0-130 2.61 25
2-Chlorotoluene 3.75 3.97 3.96 106 106 70.0-130 0.252 25
Methyl Methacrylate 3.75 3.51 3.52 93.6 93.9 70.0-130 0.284 25
Tetrahydrofuran 3.75 3.12 3.16 83.2 84.3 70.0-137 1.27 25
2,2,4-Trimethylpentane 3.75 3.39 3.35 90.4 89.3 70.0-130 1.19 25
Vinyl Bromide 3.75 4.52 4.35 121 116 70.0-130 3.83 25
Isopropylbenzene 3.75 4.05 4.04 108 108 70.0-130 0.247 25
(S) 1,4-Bromofluorobenzene 92.9 92.3 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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APPENDIX B
RISK CALCULATOR RESULTS