7401_PittCounty_NorthernUnit_MSWLF_AnnualJan21GW_FID1589416_20210716

kENR USE t7NLY—.—fl ❑Paper Report ❑Electronic Data - Email CD {data loaded; Yes 1 No � _ DoclEyent #:
C DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reaortina Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1, As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
• Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits,
Attach a notification table of any methane gas values that attain or exceed explosive gas levels_ This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1 646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Groundwater Management Associates, Inc,
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Emma H. Shipley, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or A600) October 20-24, 2006)
Northern Unit of the Pitt County 3025 Landfill Road 74-01 '0500 January 13- 14, 2021
Municipal Solid Waste Landfill Greenville, NC
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑ Detection Monitoring FX Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells Methane gas monitoring data
Groundwater monitoring data from private water supply wells Corrective action data (specify)
Leachate monitoring data ❑
Surface water monitoring data Other(specify)
Notification attached?
No. No graundwater or surface water standards were exceeded.
)( Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 26 surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
El Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Emma H. Shipley, P.G. Project Hydrageologist 252-758-3310
Facility Representative Name {Print] Title (Area Code) Telephone Number
7/16/2021 Affix NC Licensed jgpal Geologist Seal
Signature V L/ Date
4300 Sapphire Court, Suite 100, Greenville, NC 27834
Facility Representative Address
C-121 (PG Firm License Number)
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 612009

Compounds Detected At or Above Groundwater or Surface Water Standards during the January 2021 Sampling Event (1/13-
1/14/2021) - Northern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well
ID
Date
Parameter
Results
(pg/L)
MDL
(pg/L)
NC 2L or
28 Std*
(N /L)
IMAC
(pg/L)
MCL
(Ng/L)
Groundwater Samples
MW3
1/14/2021
Cobalt Total
5.973
1.4
1
-
1/14/2021
Vanadium Total
3.29 J
1.4
0.3
-
MW8
1/13/2021
Vanadium Total
2.883
1.4
0.3
-
P07
1/14/2021
Cobalt Total
2.38 J
1.4
1
-
1/14/2021
Vanadium Total
2.313
1.4
0.3
-
P09
1/14/2021
Cobalt Total
2.663
1.4
-
1
-
P16R
1/13/2021
1,4-Dioxane
78 D
1.6
3
-
-
1/14/2021
Barium Total
1100
1.1
700
2000
1/14/2021
1,4-Dioxane
140 D
4
3
-
1/14/2021
Barium Total
1290
1.1
700
2000
1/14/2021
Benzene Total
1.6
0.15
1
5
P29
1/14/2021
Cobalt Total
4.66 J
1.4
-
1
-
1/14/2021
Lead
18
3.1
15
-
15
1/14/2021
Thallium Total
0.2523
0.22
-
0.2
2
1/14/2021
Vanadium Total
36.1
1.4
-
0.3
-
1/14/2021
Arsenic
100
7.6
10
-
10
PZi
1/14/2021
Cobalt Total
2.213
1.4
-
1
-
1/14/2021
Vanadium Total
12.4
1.4
-
0.3
-
PZ2
1/14/2021
1,4-Dioxane
3.6
0.8
3
-
-
Surface WaterSamples
SWi
1/14/2021
Cobalt Total
8.021
1 3.541
1.4
4
-
1/14/2021
1 Lead
3.1
1 0.54"
-
MDL = Method Detection Limit MCL = Federal Maximum Contaminant Level
IMAC = Interim Maximum Allowable Concentration
3 = The analyte was positively identified, but the value is estimated below the reporting limit.
*15A NCAC 2L groundwater standards are listed for all groundwater sampling locations. 15A NCAC 213 standards are listed for
surface water sampling locations (SWI and SW2).
Value represents an EPA action level.
"Value represents an EPA secondary Maximum Contaminant Level
'NC Protective Value for Surface Waters
Concentrations highlighted in yellow were detected above the 2L (or 213) standards.
Concentrations highlighted in orange were detected above the IMAC.
Preliminary analysis of cause and significance of concentrations detected at or above groundwater
or surface water standards:
1,4-Dioxane, barium, benezene, and lead were detected at concentrations exceeding the 15A NCAC 02L groundwater
standards at two groundwater monitoring wells. Of these constituents, only 1,4-dioxane was detected at concentrations
above state standards in groundwater samples collected from just below the southern property ditch (which generally acts as
a local groundwater discharge feature). this is the first occurrence of 1,4-dioxane above the 15A NCAC 02L standard below
the southern ditch. Arsenic was also detected in temporary groundwater piezometer PZ1, but this sample was highly turbid
(NTU = 297), and GMA suspects that a large portion of the arsenic detected in this sample is associated with suspended
particulates and is not representative of true dissolved concentrations. None of the constituents were detected at
concentrateons exceeding state regulatory standards in downgradient surface -water samples, or in deep monitoring wells.
Pitt County has recently completed substantial cap and stormwater repairs and upgrades intended to limit the infiltration of
rainwater into the Southern Landfill Unit and reduce leachate volume and concentrations. If the cap and stormwater
upgrades are successful at the Southern Unit, the County may make similar improvements to the Northern Unit, if needed, at
at future date.

JANUARY 2021 ANNUAL WATER
QUALITY MONITORING EVENT
NORTHERN PORTION OF THE
PITT COUNTY SOLID WASTE
MUNICIPAL LANDFILL
GREENVILLE, PITT COUNTY
PREPARED FOR
MR. TIM CORLEY, PE
ENGINEERING DEPARTMENT
PITT COUNTY
1717 WEST ST" STREET
GREENVILLE, NC 27834
PREPARED BY
GROUNDWATER MANAGEMENT
ASSOCIATES, INC. (GMA)
4300 SAPPHIRE CT., SUITE 100
GREENVILLE, NORTH CAROLINA 27834
TELEPHONE: [phone]
JULY 16, 2021
North Carolina Corporate Engineering License {GMA — Apex, NC) #: C-0654
North Carolina Corporate Geology License (GMA — Greenville & Apex, NC) #: C-121
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TABLE OF CONTENTS
1.0 INTRODUCTION........................................................................................ 1
1.1 Site Background............................................................................... 1
1.2 Physical Setting and Hydrogeology.................................................. 2
2.0 JANUARY 2021 ANNUAL MONITORING EVENT ......................................... 3
2.1 Groundwater Hydrology................................................................... 4
2.2 Sample Collection and Analyses....................................................... 4
2.3 Analytical Results and Discussion.................................................... 5
3.0 WELL P13 VIDEO INSPECTION AND REPAIR ............................................ 6
4.0 WELL REHABILITATION............................................................................ 7
5.0 CONCLUSIONS AND FUTURE WORK.......................................................... 7
6.0 REPORT CERTIFICATION.......................................................................... 8
7.0 REFERENCES............................................................................................. 9
FIGURES
1. Site Layout and Existing Monitoring Network
2. Groundwater and Surface Water Sampling Locations — Northern Unit
3. Equipotential Map for the Surficial Aquifer, January 13, 2021
TABLES
1. Monitoring Well Construction and Elevations
2. Monitoring Well Water Levels and Sample Purge Volumes
3. Staff Gauge Elevations and Water Levels
4. Calculations of Groundwater Velocity
5. Field -Water Quality Parameters
6. Appendix I Target Parameters
7. List of Compounds Detected during the January 2021 Sampling Event

APPENDICES
A. Correspondence from the NC Division of Waste Management
B. Sampling Records
C. Laboratory Report and Chain -of -Custody Forms for Water Samples
D. Well P13D Video Inspection Stills
E. Well Rehabilitation Field Sheets

1.0 INTRODUCTION
The inactive Pitt County Solid Waste Municipal Landfill (Facility Permit #74-01, Figure 1) is
comprised of a Northern Unit that closed in 1990 and a Southern Unit that reached capacity and
closed in 1995. Based on its closure date, the Southern Unit is subject to the September 1993
rules for municipal solid waste landfills (15A NCAC 13B .1600). The Northern Unit, on the other
hand, is subject to the conditions of the solid waste permit and 15A NCAC 13B .0600.
Pitt County (the County) is currently assessing corrective action measures for 1,4-dioxane and
benzene groundwater contamination at the Southern Unit, which lies adjacent to, and south of,
the Northern Unit (Figure 1). Groundwater contamination at the facility is believed to be related
to the degradation of the low -permeability, clay caps that cover each unit. Over time, erosion
of the caps, as well as cracking due to heating/cooling, desiccation, and/or subsidence due to
decomposition of fill material, increases the permeability of these barriers and allows infiltration
of water that can leach contaminants downward into the underlying groundwater.
The County has recently completed substantial cap and stormwater system repairs and
upgrades at the Southern Unit as part of an approved pilot study for corrective action. These
improvements are designed to greatly reduce the infiltration of water through the cap in order
to protect the groundwater from further contamination via leaching from landfill waste. Details
regarding these improvements and the locations and recent concentrations of contaminants
around the Southern Unit can be found in the "January 2021 Semi -Annual Water Quality
Monitoring Event and Pilot Study Update" report dated July 16, 2021 (GMA, 2021).
The County has initially implemented cap and stormwater system repairs and upgrades at the
Southern Unit only, where groundwater contaminants have been detected near the landfill
property boundary. Analytical results from the well installed between the Northern and
Southern Units in 2019, however, indicate that contaminants leaching from the Northern Unit
are moving towards the Southern Unit in some locations. If the pilot study indicates that the
corrective measures implemented for the Southern Unit are working, the County may
implement similar measures at the Northern Unit at a future date.
Pitt County currently monitors groundwater at the Northern Unit on an annual schedule. The
remainder of this report presents the results of the January 2021 monitoring event at the
Northern Unit.
1.1 Site Background
The Pitt County Landfill occupies approximately 156 acres along Allen Road west of the city of
Greenville, NC (Figure 1). The landfill is comprised of a Northern Unit that closed in 1990 and a
Southern Unit that reached capacity and closed in 1995. An east -west trending railroad
(Norfolk Southern Railroad) separates the Northern and Southern Units. The Pitt County landfill
is unlined, and leachate is not collected. The Northern Unit received waste from 1974 until

January 2021 Semiannual Water Quality Monitoring Report
Northern Portion of the Pitt County Solid Waste Municipal Landfill
July 16, 2021
Page 2 of 9
1990, and the Southern Unit received waste from 1991 until 1995. Due to the closure dates,
only the Southern Unit is subject to the September 1993 rules for municipal solid waste landfills
(15A NCAC 13B .1600). Pitt County monitors the Northern Unit in accordance with the
conditions of the solid waste permit and 15A NCAC 13B .0510.
1.2 Physical Setting and Hydrogeology
The Pitt County Landfill lies in the central portion of the Coastal Plain Physiographic Province of
North Carolina, where Cretaceous to Recent age Coastal Plain sedimentary formations overlie
Mesozoic and older basement bedrock (Horton and Zullo, 1991). Coastal Plain sediments and
sedimentary rocks have significant variations in permeability and water -producing capabilities.
High -permeability strata that readily produce usable quantities of water are aquifers, and low -
permeability sediments that restrict the movement of groundwater, either into or out of
aquifers, are confining beds. Coastal Plain aquifers typically use the predominant geologic
formation name that is associated with the aquifer. The two uppermost aquifers at the Pitt
County Landfill are the unconfined Surficial/Yorktown aquifer and the confined Peedee Aquifer.
The Surficial/Yorktown Aquifer is locally composed of fossiliferous clays and sands. The clays
within the unit tend to serve as confining layers and restrict recharge to underlying aquifers
(GMA and McGill, 2001). The Peedee Aquifer consists of unconsolidated sands and sandstones
of the Late Cretaceous age Peedee Formation (Winner & Coble, 1996). In the western half of
Pitt County, the Peedee Aquifer lies directly beneath the Surficial/Yorktown Aquifer, and the
elevation of the top of the Peedee Aquifer is above sea level (GMA and McGill, 2001).
A detailed description of the local site hydrogeology is provided in the Water Quality Monitoring
Plan for the Southern Unit (GMA, 1994). In general, a sandy clay extends from the original land
surface beneath the landfill to depths varying from 6 to 13 feet. A portion of this clay may have
been excavated from areas adjacent to the Southern Unit mound and used as part of the clay
cap for the mound. Coarser, more permeable sediments (silty fine sand, clayey sand, and very
clayey sand) typically exist at depths of 10 to 16 feet. Underlying these more permeable
sediments, at a depth of approximately 16 feet below the original land surface, is a thin,
discontinuous, dark gray clay that ranges from 0.5 to 3.0 feet in thickness, with an average
thickness of 1 foot. This clay layer exists at an elevation of approximately 66 feet above mean
sea level and has previously been referred to as the "66-foot clay" (GMA, 1994). Below this
clay layer lie silty, fine sands. During the installation of deep monitoring well P20D, GMA
observed a silty, clay layer from approximately 45 to 48 feet below the land surface. Below this
clay layer, GMA observed a fine, phosphatic sand. GMA believes the deepest on -site monitoring
wells (e.g. MW1R, MW3, and P20D) may penetrate the top of the Peedee Aquifer, which is
estimated to be about 25 feet thick at the location of the landfill (GMA and McGill, 2001). We
provide a general summary of the stratigraphy below.

January 2021 Semiannual Water Quality Monitoring Report
Northern Portion of the Pitt County Solid Waste Municipal Landfill
July 16, 2021
Page 3 of 9
Average depth of strata relative
Lithology
Geologic Units
to original land surface (feet)
0 — 9.5
sandy clay
surficial sediments
9.5 — 16
silty fine sand, clayey sand, and
very clayey sand
and
Yorktown Formation
16 — 17
dark gray clay
17 — 45
silty, fine sand
45 — 48
silty, clay
Peedee Formation
48 — 60+
fine, phosphatic sand
2.0 7ANUARY 2021 ANNUAL MONITORING EVENT
GMA performed an annual monitoring event at the Northern Unit of the inactive Pitt County
Landfill from January 13 to 14, 2021. GMA performed the work on behalf of Pitt County in
accordance with the approved Water Quality Monitoring Plan (dated September 8, 1994) and
subsequent groundwater policy memos and directives issued by the North Carolina Department
of Environmental Quality (NCDEQ), Division of Waste Management (DWM), Solid Waste Section
(SWS) dated September 10, 1998, and June 14, 2004 (Appendix A).
Twenty-six groundwater monitoring wells and two temporary groundwater piezometers
comprise the groundwater monitoring network for the entire landfill facility (Figure 1, Table 1),
The water -quality monitoring network used for the January 2021 annual monitoring event of
the Northern Unit consists of five background monitoring wells (P4, P5, P6, MW8, and MW1R),
seven shallow' wells located hydraulically down -gradient of the Northern Mound (P2, P7, P9,
P13, P21, P23, and P29), two'deep' wells located hydraulically down -gradient of the Northern
Mound (MW3 and POD), one hydraulically-upgradient surface water sample location (SW1),
two hydraulically-downgradient surface water sample locations (SW2 and SW4), and two
temporary groundwater piezometers (PZ1 and PZ2) (Figure 2).
Monitoring well P16R, located on the north side of the Southern Unit, has historically been used
as a down -gradient sampling location for the Northern Unit. Groundwater elevation data from
recent monitoring events, however, indicate that groundwater at this location currently flows to
the north towards an adjacent ditch, and GMA believes that, at present, groundwater samples
collected from this well represent the groundwater chemistry of leachate from the Southern
Unit. Regardless, well P16R is part of the approved monitoring well network for the Northern
Unit (Appendix I), and thus, we have included groundwater monitoring results for P16R within
this report.

January 2021 Semiannual Water Quality Monitoring Report
Northern Portion of the Pitt County Solid Waste Municipal Landfill
July 16, 2021
Page 4 of 9
2.1 Groundwater Hydrology
GMA measured static water levels in all monitoring wells and temporary piezometers (Table 2)
and at all 13 staff gauges (Table 3) on January 13, 2021. Depth to groundwater in monitoring
wells at the site ranged from approximately 0.47 to 12.13 feet below the land surface.
Estimates of groundwater velocity (Table 4) ranged from approximately 0.001 to 0.024
feet/day, or 0.38 to 8.78 feet/year. These represent relatively slow groundwater velocities.
An equipotential map prepared using these water -level measurements (Figure 3) shows that the
horizontal component of groundwater flow at the Northern Unit was generally directed to the
south and east. A groundwater ridge or area of perched water with groundwater elevations
greater than 80 feet above mean sea level (MSL) likely exists under much of the Northern
Mound. Water from this area may flow to the north towards the northern boundary ditch in
some locations. Regardless, the highest groundwater levels at the facility are located offsite,
just northwest of the landfill boundary near the Pitt County Solid Waste and Recycling site on
Stantonsburg Road. Groundwater samples collected and analyzed from wells in this
hydraulically-upgradient area represent background groundwater chemistry.
The groundwater elevation at instream piezometer PZ1 was slightly higher than the surface
water elevation during the January 2021 monitoring event (Tables 2 and 3). The groundwater
elevation at instream piezometer PZ2, however, was slightly lower than the surface water
elevation. During the January 2021 event, GMA observed a beaver dam just upstream of PZ2
that was partially breached, and impounded water from behind the dam was flowing into the
southern property boundary ditch (Figure 3). The influx of water from the beaver
impoundment caused a higher head in the ditch than in the groundwater beneath the ditch
immediately downstream of the breach. As a result, the ditch was losing water to the
groundwater system (i.e., acting as a groundwater recharge feature) in this area. The water
level measurements collected further downstream, at PZ1, indicate that in this area
groundwater was discharging to the southern boundary ditch, consistent with historic
observations of groundwater and surface water interactions at this location.
2.2 Sample Collection and Analyses
For monitoring of the Northern Unit, GMA analyzed water samples collected from fifteen
monitoring wells, two temporary piezometers, and three surface water sampling locations as
shown in Figure 2. During sampling, GMA collected field water -quality parameters to document
adequate purging prior to sample collection and to aid in evaluating groundwater chemistry at
the site (Table 5). We provide a copy of the well sampling record in Appendix B. Sampling
procedures and analytical methods complied with the approved Water Quality Monitoring Plan
dated September 8, 1994, and subsequent directives issued by the SWS (Appendix I).
GMA transferred all samples to Environmental Conservation Laboratories, Inc. (ENCO) in ice -
filled coolers under chain -of -custody protocol for analysis of Appendix I parameters (Table 6)

January 2021 Semiannual Water Quality Monitoring Report
Northern Portion of the Pitt County Solid Waste Municipal Landfill
July 16, 2021
Page 5 of 9
and 1,4-dioxane. Copies of the chain -of -custody forms and analytical reports are provided in
Appendix C. Consistent with the May 29, 2018 NCDEQ-SWS memo, ENCO analyzed the
samples using EPA -approved analytical methods sufficiently sensitive to detect the presence of
regulated constituents at or below the applicable standard (unless no such method currently
exists, e.g., for vinyl chloride analysis).
2.3 Analytical Results and Discussion
Twenty-one parameters (1,4-dioxane, 1,4-dichlorobenzene, 2-hexanone, acetone, arsenic,
barium, benzene, beryllium, cadmium, carbon disulfide, chlorobenzene, chromium, cobalt,
copper, ethylbenzene, lead, nickel, selenium, thallium, vanadium, and zinc) were detected at
concentrations above their method detection limits (MDL) during the January 2021 sampling
event (Table 7). Five of those constituents (1,4-dioxane, arsenic, barium, benzene, and lead)
were detected at concentrations exceeding the 15A NCAC 2L groundwater standard, and three
additional constituents (cobalt, lead, and vanadium) were detected at concentrations above
their Interim Maximum Allowable Concentration (IMAC) during this monitoring event (Table 7).
A discussion of the details and significance of parameters detected above the NCAC 2L
groundwater standards detections follows.
1,4-Dioxane and barium were detected in well P16R at concentrations exceeding the 15A NCAC
2L groundwater standards. Well P16R has historically been analyzed as a hydraulically down -
gradient sample location for the Northern Unit. Groundwater elevation data provided by the
nearby staff gauge, SG3, however, suggests that the groundwater sample collected from this
well may represent the groundwater chemistry of leachate from the Southern Unit. We provide
a more thorough discussion of the contaminants detected in well P16R, and the plan of action
and pilot study for corrective action to address these contaminants, in the January 2021
monitoring report for the Southern Unit (GMA, 2021).
1,4-Dioxane, barium, benzene, and lead were detected in well P29 at concentrations exceeding
the 15A NCAC 02L groundwater standards. The detection of these contaminants in well P29,
located between the two landfill units, indicates that contaminants may be leaching from both
the Southern and Northern mounds. Neither barium, benzene, nor lead was detected above
regulatory standards in the down -gradient surface water samples or the samples collected from
the in -stream piezometers (PZ1 and PZ2). 1,4-Dioxane, however, was detected at a
concentration just exceeding the 15A NCAC 02L groundwater standard in PZ2. This is the first
exceedance of the 1,4-dioxane groundwater standard at this location. It is unknown whether
the temporary influx of surface water from the nearby beaver impoundment had any effect on
this result. Importantly, barium, benzene, 1,4-dioxane, and lead were not detected above the
15A NCAC 02L groundwater standards in the samples collected from the "deep" down -gradient
monitoring wells, MW3 and P13D.

January 2021 Semiannual Water Quality Monitoring Report
Northern Portion of the Pitt County Solid Waste Municipal Landfill
July 16, 2021
Page 6 of 9
Upgradient surface water sample SW1 contained a concentration of only cobalt above the 15A
NCAC 02B surface -water standards. In recent years, multiple metals have exceeded the
standards at this location (e.g. 7 parameters above the 2B standards in July 2019, GMA 2020).
Metal exceedances at this upgradient surface -water sample location corresponded with highway
construction on the adjoining parcel directly next to the SW1 sampling location. Per the NC
DOT website, construction on the bypass started in August 2016 and was completed in
November of 2019 (NC DOT, 2019). The lab did not detect any of the target parameters above
the 2B surface -water standards in the down -gradient samples, SW2 and SW4.
Zinc, 2-hexanone, and carbon disulfide were detected in the equipment blank. GMA believes
that zinc concentrations are related to residual powder from the manufacturing process used to
produce the powder -free' nitrile gloves that we used during sampling. Nitrile gloves are also
the likely source of the carbon disulfide detected in the equipment blank (USGS, 2012). GMA is
unsure of the source of 2-hexanone in the equipment blank. The lab did not detect 2-hexanone
in any other sample from the January 2021 event.
3.0 WELL P13D VIDEO INSPECTION AND REPAIR
During the January 2021 monitoring event at the Northern Unit of the Pitt County Landfill, GMA
detected an estimated concentration of 1.5 pg/L of 1,4-dioxane in monitoring well P13D. Well
P13D is a "deep" monitoring well screened in the top of the Peedee Aquifer. Although the
detected concentration of 1,4-dioxane was below the 15A NCAC 2L groundwater standard of 3
fag/L, we have not detected 1-4-dioxane in any other "deep" monitoring wells at the facility.
GMA resampled well P13D on March 11, 2021, and detected an estimated concentration of 1.4
pg/Lm, suggesting that the reported concentration in January 2021 is not a laboratory error
(Appendix Q.
In January of 2014, GMA encountered clay and sediment in well P13D at an approximate depth
of 27 feet below the top of casing (TOC), and we initially believed the well had filled in. When
GMA returned to the well in July of 2014, the well was unobstructed and clear to the full well
depth of 54 feet below the TOC. Well P13D is located in close proximity to the gas collection
system and flare. Although we have not encountered any other difficulty measuring water
levels or collecting samples from this well since 2014, GMA recommended that the County video
log the well to check well integrity and ensure that the well was not serving as a conduit for
downward migration of contaminants from the surface or shallow groundwater.
GMA performed a downhole video inspection of the monitoring well on April 8, 2021. The video
inspection revealed that the casing appears to be compromised approximately 0.5 feet below
the land surface (Appendix D). Iron staining visible on the well casing below the damaged area
indicates that, at some point(s) in the past, surface water has entered the well. Project notes

January 2021 Semiannual Water Quality Monitoring Report
Northern Portion of the Pitt County Solid Waste Municipal Landfill
July 16, 2021
Page 7 of 9
indicate that this well was previously repaired in the late 1990s after being hit by a mower.
GMA believes that this repair was unsuccessful, and (based upon video inspection evidence) the
heat of hydration during the cement pad curing process may have caused melting of the PVC.
Due to the shallow nature of the well damage, GMA believes that this well can be repaired
instead of having to be abandoned and replaced. The well repair is scheduled for July 23, 2021.
4.0 WELL REHABILITATION AND MAINTENANCE
Over recent years GMA has noticed an increased frequency of monitoring wells bailing dry (i.e.
water is removed from the well during the purging process faster than water from the formation
can enter the well). Additionally, many of the wells at the Pitt County Landfill remain turbid
after purging, which increases the concentrations of metals in the samples. GMA believes that
many of these monitoring wells, which were installed in the 1990s, are likely affected by a
combination of scale and biological plugging. To extend the life of these monitoring wells, and
to provide representative groundwater samples, Pitt County opted to perform physical well
rehabilitation via surging and pumping all monitoring wells at the facility.
On June 16 and 17, 2021, GMA redeveloped all shallow monitoring wells using a high flow
Waterra° brand inertial foot valve. The foot valve was attached to HDPE tubing, inserted into
the well, and oscillated (pulled up and pushed down) over a short vertical distance. This action
pumps water out of the well while simultaneously surging the well. During the procedure, GMA
monitored for temperature, pH, specific conductance, and turbidity (Appendix Q. GMA also
measured the total well depth before and after the well redevelopment procedure. GMA
removed as much as 0.33 feet of sediment from the bottom of the wells. The effect of these
well redevelopment procedures will be determined after the next monitoring event.
5.0 CONCLUSIONS AND FUTURE WORK
1,4-Dioxane, barium, benzene, and lead were detected at concentrations exceeding the 15A
NCAC 02L groundwater standards at two groundwater monitoring well locations during the
January 2021 monitoring event for the Northern Landfill Unit. Groundwater from one of these
locations, well P16R, may contain leachate from the Southern Unit. Of these constituents, only
1,4-dioxane was detected at a concentration above State standards in groundwater samples
collected from just below the southern ditch, which acts as a local groundwater discharge
feature for the landfill facility, or in downgradient surface -water samples. This is the first
occurrence of 1,4-dioxane above the 15A NCAC 02L standards below the southern ditch. The
downgradient surface water sample, SW4, did not contain any target parameter above the 15A
NCAC 02B surface water standards. Pitt County will collect a confirmation sample during the

January 2021 Semiannual Water Quality Monitoring Report
Northern Portion of the Pitt County Solld Waste Municipal Landoll
July 16, 2021
Page & of 9
]uly 2021 monitoring event of the Southern Landfill Unit to confirm the presence of 1,4-dioxane
above the groundwater standard in this location.
Although the Northern Unit of the Pitt County Landfill is not subject to the 15A NCAC 13B .1600
rules, the unit lies adjacent to, and upgradient of, the Southern Landfill Unit, which is subject to
these rules. Pitt County is currently assessing corrective action measures for 1,4-dioxane and
benzene groundwater contamination at the Southern Unit. In May 2021, the County completed
the planned cap and stormwater system repairs and upgrades at the Southern Unit as part of
the approved pilot study for corrective action (GMA, 2021). These improvements were
designed to greatly reduce the infiltration of water through the cap in order to protect the
groundwater from further contamination via leaching from landfill waste. The County has
initially implemented cap and stormwater system repairs and upgrades at the Southern Unit
only, where groundwater contaminants are closest to the landfill property boundary. If the pilot
study indicates the corrective measures implemented for the Southern Unit are working, the
County may implement similar measures at the Northern Unit at a future date.
Pitt County currently monitors groundwater at the Northern Unit of the Pitt County Solid Waste
Municipal on an annual schedule. The next annual monitoring event for the Northern Unit is
scheduled for ]anuary of 2022. This monitoring event will include the analysis of all water
samples for Appendix I parameters plus 1,4-dioxane.
6.0 REPORT CERTIFICATION
This report was prepared by Ms. Emma H. Shipley, a Project Hydrogeologist for Groundwater
Management Associates, Inc. (GMA). I certify that the information contained in this report is
correct and accurate to the best of my knowledge. GMA is a professional corporation licensed
to practice geology (#C-121) and engineering (#C-0854) in North Carolina.
Emma H. Shipley, P.G.
Project Hydrogeologist
�wrn�prr
Sri
Nr�
z SEAL
mLU
'�R�also�

January 2021 Semiannual Water Quality Monitoring Report
Northern Portion of the Pitt County Solid Waste Municipal Landfill
July 16, 2021
Page 9 of 9
7.0 REFERENCES
Groundwater Management Associates, Inc., 1994, Water Quality Monitoring Plan for the Active
Southern Unit of the Pitt County Landfill, 71 pages.
Groundwater Management Associates, Inc., 2020, July 2020 Semi -Annual Water Quality
Monitoring Event and Pilot Study Update, Greenville, Pitt County, 201 pages.
Groundwater Management Associates, Inc., 2021, January 2021 Semi -Annual Water Quality
Monitoring Event and Pilot Study Update, Greenville, Pitt County, pages.
Groundwater Management Associates, Inc. and McGill and Associates, 2001, Water Resources
Management Plan, Pitt County, North Carolina.
Horton, J.W. and V.A. Zullo, 1991, The Geology of the Carolinas: Carolina Geological Society
Fiftieth Anniversary Volume, 406 pp.
NC DOT, 2019, Southwest Bypass Opens to Traffic ahead of Schedule,
https://www. ncdot.gov/news/press-releases/Pages/2019/2019-11-21-pitt-count
southwest-bypass-opens.aspx, accessed December 4, 2019.
USGS, 2012, Program Evaluation of Volatile Organic Compound (VOC) Blank Data and
Application of Study Reporting Levels to Groundwater Data Collected for the California
GAMA Priority Basin Project, May 2004 through September 2010. Scientific
Investigations Report 2012-5139, 106 pages.
Winner, M.D. and R.W. Coble, 1996, Hydrogeologic Framework of the North Carolina Coastal
Plain, USGS Professional Paper 1404-I, 119 pages.

FIGURES

y� r
_m: r'
r
i
ga P21
P16R
P11R''
.;� SOUTHERN UNIT
P19 MW6R`� .. .
ry .I P1r7 P28
4.
`e t SG6 o..
P12
SG8 P20R PZ1
P8
SG7 PZ2
SG2
THIS A NOT INTENDED
IS FOR GENERAL REFERENCEONURPoG P ONIFY RPOSESD SHOULD NOT BE USED, f
AND Is NOT INTENOEO FOR, SURVEYOR ENGINEERING PURPOSES. LOCATIONS ARE APPROXIMATE. �~
GIs sOURGE DATA:
ORTHOIMAGERYOBTAINED FROM NG ONEMAP, IMAGE DATE: FEBRUARY 2020
PARCEL BOUNDARIES FROM PITT COUNTY GIS, http, l/map-pittcc. pp-d.ta.arcgis.wm
LEGEND
G SURFACE WATER SAMPLE TEMPORARY PIEZOMETER DITCHES SCALE IN FEET GMA
STAFF GAUGE )K ABANDONED / LOST WELL 0 00'
`
MONITORING WELL APPROXIMATE PARCEL BOUNDARIES GNOUN DINATE A MANAGEM F NIT A SSO[IAT ES, INC_
File: DRAWINGS/25101 SITE LAYOUTAND EXISTING MONITORING NETWORK DATE: 3/17/2021
FIG 1
PROJECT 25101 PITT COUNTY LANDFILL, GREENVILLE, PITT CO., NC FIGURE 1

P6 P4 �-
.r:;b...
NORTHERN
P13D
a.
- P13
P29 4 P2
P16R
'. SOUTHERN
PZ1
PZ2
r
THIS PRODUCT IS FOR GENERAL REFERENCE PURPOSES ONLYAND SHOULD NOT BE USED,
AND IS NOT INTENDED FOR, SURVEYOR ENGINEERING PURPOSES. LOCATIONSAREAPPROXIMATE.
GIs SOURCE DATA:
ORTHOIMAGERYOSTAINED FROM NC ONEMAP, IMAGE DATE'. FEBRUARY 2020
PARCEL BOUNDARIES FROM PITT COUNTY GIS, https'//map-pitt—p,.d.t, ,,P,is.com /
i
-LEGEND- ���
e SURFACE WATER SAMPLE TEMPORARY PIEZOMETER DITCHES SCALE IN FEET
MONITORING WELL APPROXIMATE PARCEL BOUNDARIES 0� `moo'
- GPOIfN�WAiFP MANAGEMENT ASSG[IAiES, IN[ -
File: DRAWINGS/25101 GROUNDWATER AND SURFACE WATER SAMPLING LOCATIONS - NORTHERN UNIT DATE: 4/14/2021
FIG 2N
PROJECT 25101 PITT COUNTY LANDFILL, GREENVILLE, PITT CO., NC FIGURE 2

THIS PRODUCT IS FOR GENERAL REFERENCE PURPOSES ONLY AND SHOULD NOT BE USED,
AND IS NOT INTENDED FOR, SURVEY OR ENGINEERING PURPOSES. LOCATIONS ARE APPROXIMATE.
GIS SOURCE DATA:
TOPOGRAPHIC CONTOURS OBTAINED FROM NC ONEMAP,
PARCEL BOUNDARIES FROM PITT COUNTY GIS, https://map-pittnc.opendata.arcgis.com
SG10
80.58
:c
I
D
Jco
—
81< F.
R1
P11R
79.29 .s�
79.E
80 �.
u
" �81
P
_ _
!1 19,�
P11 "� $��77.81 '
--� 76.62
78 1'/ 8� �,� P20D1
=MUNN(75.43) o
�P20R,
P1275.'89
77.29' 1.100' SG8
7776 SG7--- ^ ` 72.80 �'PZ2 '
73.33 73 72.45 Z�
75 74 (surface water)
Approximate
location of
beaver dam
(water elevation >2 ft higher)
"r
I .oSG5'
75.540401 P21
`80 �
1
W� 7�1
-8�0_
MW7M�779,8
P26 —
79257
8�p�7W6
. I
74.95
75
J .���♦ 76
'MW3�kZ7
M 4 (76.58)* 78
SG9 '
(75.32) '� p07
X P09� �80; 7,7.03
1
• . ` 76.04
o P23 80�
76.02 �.
MW6R II ` . MW5
■ 7,5:25 SG 3 Ns,' cow
19
�P24` 0SO# ;PO %
71
PZ1 `X 74
72 71.95 P08 Q,
CID
(surface water) 73.09
73
CO SG2 7172
70.47
GENERAL NOTES:
' �P-020W77
78. 33
1
1. TOPOGRAPHIC CONTOUR INTERVAL = 2.0 FEET
2. GROUNDWATER CONTOUR INTERVAL = 1.0 FOOT
3. ARROW INDICATES DIRECTION OF GROUNDWATER FLOW
4. WATER LEVEL ELEVATIONS ARE POSTED BY EACH WELL
5. ( ) INDICATES DATA NOT USED FOR CONTOURING
- LEGEND -
MONITORING WELL
UNMEASURED MONITORING WELL
ABANDONED MONITORING WELL
PROPERTY LINE
�--��
RAILROAD TRACKS
TOPOGRAPHIC CONTOUR
—
POND
GROUNDWATER ELEVATION
CONTOUR
INDICATES DIRECTION OF
GROUNDWATER FLOW
77.31
WATER LEVEL
(FEET ABOVE SEA LEVEL)
----
DITCH
L
STAFF GAUGE
FIGURE 3
DATE 6/3/2021 PROJECT: 25101
DRW BY: AWC CHK BY: EHS
SCALE IN FEET
0 350 700'
1" = 350'
EQUIPOTENTIAL MAP
JAN UARY 13, 2021
A
GMA
= =�-
GROUNDWATER MANAGEMENT ASSOCIATES, INC.

TABLES

Table 1. Monitoring Well Construction and Elevations
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Number,
Easting
(feet)*
Northing
=
fC = J=
U O W
w a
Q>
o°,�
W
U
�
J
7 O W
An a
>
�
J (�N
- Ol
y=
3�a
o=
01 G7
O U
+, (A U)
wJ
a.
e
G o
G7
O O
+,
EJ
E
o o
a CO
w d
= V J
O (AO
1pwa
..
a
ow
W
w Ui
e
= O J
V)
++ Ea
4aWell
o e
W CO
MW1R
2463487.26
676793.08
85.48
82.5
52.98
40.0
50.0
42.5
32.5
MW3
2467253.81
676198.15
82.97
80.5
47.47
35.0
45.0
45.5
35.5
MW4
2466875.66
676066.89
83.58
81.9
21.68
10.0
20.0
71.9
61.9
MW6R
2465083.71
675392.21
80.94
78.15
19.79
7.0
17.0
71.15
61.15
MW8
2464639.20
676915.58
84.41
81.62
16.79
4.0
14.0
77.62
67.62
MW8D
2464553.05
676827.15
84.28
81.37
30.91
18.0
28.0
63.37
53.37
P02
2467254.11
676191.82
84.65
80.6
19.05
11.0
15.0
69.6
65.6
PO4
2463438.60
676616.81
85.02
81.5
21.52
8.0
18.0
73.5
63.5
POs
2463490.61
676797.65
85.94
82.3
17.14
8.5
13.5
73.8
68.8
P06
2463171.35
676568.01
84.72
81.5
17.72
8.5
14.5
73
67
P07
2466875.67
676056.22
85.41
81.9
19.51
11.0
16.0
70.9
65.9
P08
2466074.39
674918.18
85.22
81.4
20.3
9.0
17.0
72.4
64.4
P09
2466189.91
675932.77
84.08
80.1
18.48
9.5
14.5
70.6
65.6
P11R
2463141.14
675651.83
86.04
82.3
19.74
13.0
16.0
69.3
66.3
P12
2463126.32
675048.53
79.31
75.9
20.91
10.5
17.5
65.4
58.4
P13
2466105.04
676161.21
85.8
82
19.8
11.0
16.0
71
66
P13D
2466119.99
676174.03
84.67
81.2
54.97
47.5
51.5
33.7
29.7
Pis
2465472.37
676703.00
87.90
84.25
20.71
4.0
17.0
80.25
67.25
P16R
2464194.10
675837.67
87.44
84.3
17.14
11.0
14.0
73.3
70.3
P17
2463319.94
675286.12
80.38
76.3
15.08
8.0
11.0
68.3
65.3
P19
2463898.87
675403.02
83.9
78.5
18.4
9.0
13.0
69.5
65.5
P20R
2464435.49
675068.13
85.21
81.7
33.51
10.0
30.0
71.7
51.7
P20D
2464583.16
675103.79
84.52
81.5
63.02
50.0
60.0
31.5
21.5
P21
2465286.45
675904.93
82.07
77.8
15.27
8.0
11.0
69.8
66.8
P23
2465657.48
675745.22
82.93
79.4
19.53
11.0
16.0
68.4
63.4
P26
2466246.80
676940.21
84.59
82.2
16.39
9.0
14.0
73.2
68.2
P28
2463542.16
675278.55
77.74
74.8
10.94
3.5
8.0
71.3
66.8
P29
2464558.30
676041.26
85.36
82.4
14.96
7.0
12.0
75.4
70.4
PZ1
2464848.16
675165.00
72.44
70.8
3.39
1.0
1.8
69.8
69.1
PZ2
2464485.95
675009.74
72.89
71.2
3.44
1.0
1.8
70.2
69.5
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid
(NCGS) control based on ties to NCGS Monument 'RUTH' and NCGS Monuments 'MARY'. Horizontal data referenced
to NAD 83(2011). Vertical data referenced to NGVD 29.
BLS = below land surface ASL = above sea level LS = land surface

Table 2. Monitoring Well Water Levels and Sample Purge Volumes
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Date
Elevation
of Top of
Casing
(feet ASL)
Land
Surface
Elevation*
(feet ASL)
Total Well
Depth
below LS
(feet)
Depth to
Water
(feet)
Elevation
of Water
(feet ASL)
Height of
Water in
Well
(feet)
Three
Well
Volumes
(gallons)
Amount
Purged
(gallons)
Number of
Well
Volumes
Purged
Purged to
Dryness?
MW1R
1/13/21
85.48
82.50
50.0
6.54
78.94
46.4
22.6
22.6
3.0
no
MW3
1/13/21
82.97
80.50
45.0
6.39
76.58
41.1
20.0
20.0
3.0
no
MW4
1/13/21
83.58
81.90
20.0
6.34
77.24
not sampled
MW6R
1/13/21
80.94
78.15
17.0
5.69
75.25
14.1
7.1
7.1
3.0
no
MW8
1/13/21
84.41
81.62
14.0
4.83
79.58
12.0
5.8
5.8
3.0
no
MW8D
1/31/21
84.28
81.37
28.0
5.29
78.99
not sampled
P02
1/13/21
84.65
80.60
15.0
6.32
78.33
12.7
6.2
6.2
3.0
no
PO4
1/13/21
85.02
81.50
18.0
4.23
80.79
17.3
8.4
8.4
3.0
no
P05
1/13/21
85.94
82.30
13.5
4.51
81.43
12.6
6.1
5.4
2.7
yes
P06
1/13/21
84.72
81.50
14.5
3.93
1 80.79
13.8
6.7
5.7
2.6
yes
P07
1/13/21
85.41
81.90
16.0
8.38
77.03
11.1
5.4
1 4.1
1 2.3
1 yes
P08
1/13/21
85.22
81.40
17.0
12.13
73.09
not sampled
P09
1/13/21
84.08
80.10
14.5
6.70
77.38
11.8
5.7
4.9
2.6
yes
P11R
1/13/21
86.04
82.30
16.0
6.75
79.29
13.0
6.3
3.2
1.5
yes
P12
1/13/21
79.31
75.90
17.5
2.02
77.29
18.9
9.2
4.9
1.6
yes
P13
1/13/21
85.80
82.00
16.0
7.78
78.02
12.0
5.8
5.8
3.0
no
P13D
1/13/21
84.67
81.20
51.5
8.44
76.23
46.5
22.6
22.6
3.0
no
P15
1/13/21
87.90
84.25
17.0
8.82
79.08
not sampled
P16R
1/13/21
87.44
84.30
14.0
8.89
78.55
8.3
4.0
4.1
3.1
yes
P17
1/13/21
80.38
76.30
11.0
3.76
76.62
11.3
5.5
3.2
1.7
yes
P19
1/13/21
83.90
78.50
13.0
6.09
77.81
12.3
6.0
4.1
2.1
yes
P20R
1/13/21
85.21
81.70
30.0
9.32
75.89
24.2
11.3
11.3
3.0
no
P20D
1/13/21
84.52
81.50
60.0
9.09
75.43
53.9
1 26.2
26.2
1 3.0
no
P21
1/13/21
82.07
77.80
11.0
6.03
76.04
9.2
4.5
3.0
2.0
yes
P23
1/13/21
82.93
79.40
16.0
6.91
76.02
12.6
6.1
6.2
3.0
yes
P26
1/13/21
84.59
82.20
14.0
5.07
79.52
not sampled
P28
1/13/21
77.74
74.80
8.0
2.99
74.75
1 8.0
3.8
3.5
2.7
yes
P29
1/13/21
85.36
82.40
12.0
5.99
79.37
9.0
4.4
4.4
3.0
no
PZ1
1/13/21
72.44
70.80
1.8
0.47
71.97
a grab surface water sample was collected at this location
PZ2
1/13/21
72.89
71.20
1.8
0.47
72.42
a grab surface water sample was collected at this location
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid (NCGS) control based on ties to NCGS
MnniimPnf'RIITH' and NC(;S MnniimPntc'MARY'_ Hnri7nnfaI data rPfPrPnrPrl fn NAn R"i ?nii) VPrfiraI data rPfPrPnrPrl fn N(;Vr) ?9_
ASL = Above Sea Level LS = land surface

Table 3. Staff Gauge Elevations and Water Levels
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Staff
Gauge
Date
Easting
(feet)*
Northing
feet *
Reference
Point
Elevation of
Reference
Point
feet ASL
Staff Gauge
Reading or
Depth to Water
Measurement
(ft)
Elevation of
Water
(feet ASL
SG1
1/13/21
2464589.3
676053.46
4-foot mark
81.06
1.22
78.28
SG2
1/13/21
2466082.36
674856.14
4-foot mark
71.68
2.79
70.47
SG3
1/13/21
2464175.98
675874.46
4-foot mark
80.60
1.56
78.16
SG4
1/13/21
2467192.35
676705.36
4-foot mark
76.38
2.57
74.95
SGS
1/13/21
2465262.23
675928.45
3-foot mark
76.88
1.66
75.54
SG6
1/13/21
2465175.63
675356.1
4-foot mark
74.18
0.91
71.09
SG7
1/13/21
2463215.14
675010.08
3-foot mark
75.13
1.20
73.33
SG8
1/13/21
2463932.14
675059.19
3-foot mark
73.91
1.89
72.80
SG9
1/13/21
2466110.5
676143.36
3-foot mark
76.96
1.36
75.32
SG10
1/14/21
2463086.65
676845.47
3-foot mark
82.02
1.56
80.58
SG11
1/13/21
2463169.96
676528.73
3-foot mark
81.47
0.86
79.33
SG12
1/13/21
2463583.11
676511.02
3-foot mark
81.13
1.19
79.32
SG96
1/13/21
2466366.84
676889.34
3-foot mark
77.83
1.20
76.03
PZ1-SW+
1/13/21
2464848.16
675165.00
TOC
72.44
0.49
71.95
PZ2-SW+
1/13/21
2464485.95
675009.74
TOC
72.89
0.44
72.45
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid
(NCGS) control based on ties to NCGS Monument'RUTH' and NCGS Monuments'MARY. Horizontal data referenced
to NAD 83(2011). Vertical data referenced to NGVD 29.
+ Surface water elevations determined by measurinq depth to surface water from top of casinq
ASL = Above Sea Level
TOC = top of casing

Table 4. Calculations of Groundwater Velocity
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Date
Horizontal
Hydraulic
Gradient
(ft/ft)
Hydraulic
Conductivity
(ft/day)
Effective
Porosity
Horizontal
Groundwater
Velocity
(ft/day)
Horizontal
Groundwater
Velocity
(ft/year)
MW6R
1/13/21
0.003
0.50
0.29
0.005
2.00
PO4
1/13/21
0.009
0.50
0.19
0.022
8.21
P12
1/13/21
0.009
0.20
0.43
0.004
1.48
P20R
1/13/21
0.003
0.10
0.32
0.001
0.38
P28
1/13/21
0.014
0.30
0.17
0.024
8.78

Table S. Field -Water Quality Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Sample
Date
pH
Temp-
erature
(degrees
Celsius)
Specific
Conductance
(µS)
Dissolved
oxygen
(mg/L)
Turbidity during
collection of
organic samples
(ntu)
Turbidity during
collection of
metals samples
(ntu)
MW1R
1/14/2021
5.50
15.2
68
1.9
3.0
3.0
MW3
1/14/2021
4.19
18.4
96
15.1
2.8
2.8
1/14/2021
6.75
15.5
2019
0.8
29
--
MW6R
1/14/2021
--
--
--
--
--
14.2
MW8
1/13/2021
5.66
15.6
108
1.6
306
306
P02
1/14/2021
4.75
18.3
53
32.2
34
34
1/13/2021
5.07
15.6
85
4.6
20
20.2
PO4
1/14/2021
--
--
--
--
--
POS
1/14/2021
5.03
15.2
41
2.4
38
38
P06
1/14/2021
5.36
16.1
73
1.65
15
15
P07
1/14/2021
4.17
17.6
173
0.9
20
20
P09
1/14/2021
4.80
17.3
111
2.0
73
73
P1111
1/14/2021
6.10
15.2
79
1.2
364
364
P12
1/14/2021
5.86
14.8
62
3.70
45
44.7
P13
1/14/2021
5.27
18.1
41
11
34
34.2
P13D
1/14/2021
5.74
18.4
96
0.9
26
26
1/13/2021
6.64
16.2
5205
1.5
115
--
P16R
1/14/2021
--
--
--
--
--
15
P17
1/13/2021
5.88
16.5
228.3
1.8
31
31.10
P19
1/13/2021
3.84
16.3
1459.0
1.3
146
--
1/14/2021
--
--
--
--
--
6
P20R
1/13/2021
5.89
17.5
104
1.7
29
--
1/14/2021
--
--
--
--
--
100.0
P20D
1/14/2021
6.03
17.3
61.3
0.9
70.5
70.5
P21
1/14/2021
7.17
15.7
65
3.2
9
9
1/13/2021
5.72
19.6
59
26.9
59
--
P23
1/14/2021
--
--
--
--
--
9
P28
1/13/2021
5.72
15.0
70
3
269
--
1/14/2021
--
--
--
--
--
133
P29
1/14/2021
4.43
15.1
4732.00
3.4
152
152
SW1
1/14/2021
4.50
9.70
112.40
6.37
29.50
29.50
SW2
1/14/2021
5.79
9.30
169.40
8.22
67.00
67.00
SW4
1/13/2021
5.81
9.00
215.00
7.88
9.23
9.23
PZ1
1/14/2021
5.48
9.80
146.00
16.80
297
297
PZ2
1/14/2021
1 6.30
8.40
676.30
36.50
475
475

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standardsi
DEQ
CAS
2L
IMAC
MCL
Calculated
Number
Name
Other Names
Std.
(Ng�L)
GWP Std
67-64-1
Acetone
2-Propanone
6000
--
--
--
107-13-1
Acrylonitrile
Acrylonitrile
--
--
--
--
7440-36-0
Antimony
Antimony
--
1
6
--
7440-38-2
Arsenic
Arsenic
10
--
10
--
7440-39-3
Barium
Barium
700
--
2000
--
71-43-2
Benzene
Benzene
1
--
5
--
7440-41-7
Beryllium
Beryllium
--
4
4
--
Bromochloromethane;
Methane, bromochloro-
--
--
--
0.6
74-97-5
Chlorobromethane
Bromodichloromethane;
Methane, bromodichloro
0.6
--
80
--
75-27-4
Dichlorobromomethane
Bromoform;
75-25-2
Tribromomethane
Methane, tribromo-
4
--
80
--
7440-43-9
Cadmium
Cadmium
2
--
5
--
75-15-0
Carbon disulfide
Carbon disulfide
700
--
--
--
56-23-5
Carbon tetrachloride
Methane, tetrachloro-
0.3
--
5
--
108-90-7
Chlorobenzene
Benzene, chloro-
50
--
100
--
Chloroethane; Ethyl
Ethane, chloro-
3000
--
--
--
75-00-3
chloride
Chloroform;
67-66-3
Trichloromethane
Methane, trichloro-
70
--
80
--
7440-47-3
Chromium
Chromium
10
--
100
--
7440-48-4
Cobalt
Cobalt
--
1
--
--
7440-50-8
Copper
Copper
1000
--
1300
--
Dibromochloromethane;
124-48-1
Chlorodibromomethane
Methane, dibromochloro
0.4
--
80
--
1,2-Dibromo-3-
Propane, 1,2-dibromo-3-
96-12-8
chloro ro ane; DBCP
chloro-
0.04
--
0.2
--
1,2-Dibromoethane;
106-93-4
Ethylene dibromide; EDB
Ethane, 1,2-dibromo-
0.02
--
0.05
--
o-Dichlorobenzene; 1,2-
95-50-1
Dichlorobenzene
Benzene, 1,2-dichloro-
20
--
600
--
p-Dichlorobenzene; 1,4-
106-46-7
Dichlorobenzene
Benzene, 1,4-dichloro-
6
--
75
--
2-Butene,
110-57-6
trans-1,4-Dichloro-2-butene
E4-dichloro-,
1,1-Dichloroethane;
75-34-3
Eth Ididene chloride
Ethane, 1,1-dichloro-
6
--
--
--

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standardsi
IMAC
DEQ
CAS
2L
(Ng�L)
MCL
Calculated
Number
Name
Other Names
Std.
GWP Std
1,2-Dichloroethene;
Ethane, 1,2-dichloro-
0.4
--
5
--
107-06-2
Ethylene dichloride
1,1-Dichloroethylene; 1,1-
Ethene, 1,1-dichloro-
350
--
7
--
75-35-4
Dichloroethene;
cis-1,2-Dichloroethylene;
Ethene, 1,2-dichloro-,(Z)
70
--
70
--
156-59-2
cis-1,2-Dichloroethene
trans-1,2-Dichloroethylene;
Ethene, 1,2-dichloro-,(E)
100
--
100
--
156-60-5
trans-1,2-Dichloroethene
78-87-5
1,2-Dichloropropane
Propane, 1,2-dichloro-
0.6
--
5
--
cis-1 3-Dichloropropene
1-Propene, 1,3-dichloro-
0.4
--
--
--
10061-01-5
Z -
trans-1 3-Dichloropropene
1-Propene, 1,3-dichloro-
0.4
--
--
--
10061-02-6
E -
100-41-4
Ethylbenzene
Benzene, ethyl-
600
--
700
--
2-Hexanone; Methyl butyl
2-Hexanone
--
40
--
--
591-78-6
ketone
7439-92-1
Lead
Lead
15
--
15
--
Methyl bromide;
Methane, bromo-
--
10
--
--
74-83-9
Bromomethane
Methyl chloride;
Methane, chloro-
3
--
--
--
74-87-3
Chloromethane
Methylene bromide;
Methane, dibromo-
--
70
--
--
74-95-3
Dibromomethane
Methylene chloride;
Methane, dichloro-
5
--
5
--
75-09-2
Dichloromethane
Methyl ethyl ketone; MEK;
2-Butanone
4000
--
--
--
78-93-3
2-Butanone
Methyl iodide;
Methane, iodo-
--
--
--
--
74-88-4
Iodomethane
4-Methyl-2-pentanone;
2-pentanone, 4-methyl-
--
100
--
--
108-10-1
Methyl isobut I ketone
7440-02-0
Nickel
Nickel
100
--
--
--
7782-49-2
Selenium
Selenium
20
--
50
--
7440-22-4
Silver
Silver
20
--
--
--
100-42-5
Styrene
Benzene, ethenyl-
70
--
100
--
1,1,1,2-Tetrachloroethane
Ethane 1112-
_
1
__
630-20-6
tetrachloro�
1,1,2,2-Tetrachloroethane
Ethane 1 1 2 2-
0.2
__
79-34-5
tetrachloro�

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
CAS
2L
IMAC
MCL
Calculated
Number
Name
Other Names
Std.
(Ng�L)
GWP Std
Tetra chIoroethylene;
Tetra ch I oroethen e;
Ethene, tetrachloro-
0.7
--
5
--
127-18-4
Perch loroeth lene
7440-28-0
Thallium
Thallium
--
0.2
2
--
108-88-3
Toluene
Benzene, methyl-
600
--
1000
--
1,1,1-Trichloroethane;
71-55-6
Meth (chloroform
Ethane, 1,1,1-trichloro-
200
--
200
--
Trichloroethylene;
Ethene, trichloro-
3
--
5
--
79-01-6
Trichloroethene
79-00-5
1,1,2-Trichloroethane
Ethane, 1,1,2-trichloro-
--
0.6
5
--
Trichlorofluoromethane;
Methane,trichlorofluoro-
2000
--
--
--
75-69-4
CFC-11
96-18-4
1,2,3-Trichloropropane
Propane, 1,2,3-trichloro-
0.005
--
--
--
7440-62-2
Vanadium
Vanadium
--
3.5
--
--
108-05-4
Vinyl acetate
Acetic acid, ethenylester
--
88
--
--
75-01-4
VIIIYI ullulluu,Ethene,
chloro-
0.03
--
2
--
7440-66-6
Zinc
Zinc
1000
--
--
--
1330-20-7
Xylene (total)
Benzene, dimethyl-
500
--
--
All units are in micrograms per liter (pg/L)
2L STD = 15A NCAC 2L groundwater standard
'Applicable Groundwater Protection Standard is the lower of the listed standards.

Table 7. List of Compounds Detected during the January 2021 Sampling Event (1/13-1/14/2021)
Northern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well ID
Date
Parameter
Results
(Ng/L)
MDL
I (Ng/L)
NC 2L or 2B
Std* (Ng/L)
IMAC
(Ng/L)
MCL
(Ng/L)
Groundwater Samples
1/13/2021
2-Hexanone
1.9J
0.88
-
40
-
EB
1/13/2021
Carbon Disulfide
53.00
1.5
700
-
1/13/2021
Zinc Total
114.00
4.4
1000
-
5000#
FB
1/14/2021
Acetone
14 J
10
6000
-
-
TB
1/13/2021
Acetone
67
10
6000
-
-
TB
1/13/2021
Acetone
31
10
6000
-
-
MW1R
1/14/2021
Barium Total
54.6
1.1
700
-
2000
1/14/2021
Beryllium Total
0.348 J
0.16
-
4
4
1/14/2021
Barium Total
190
1.1
700
-
2000
1/14/2021
Beryllium Total
0.2213
0.16
-
4
4
MW3
1/14/2021
Cobalt Total
5.97 YO
1.4
-
1
-
1/14/2021
Nickel Total
5.823
2.2
100
-
-
0.3
-
1/14/2021
Vanadium Total
3.293
1.4
1/14/2021
Zinc Total
26.7
4.4
1000
-
50004
1/13/2021
Barium Total
11.8
1.1
700
-
2000
1/13/2021
Beryllium Total
0.3753
0.16
-
4
4
MW8
1/13/2021
Copper Total
1.983
1.6
1000
-
1300^
1/13/2021
Vanadium Total
2.88 J
1.4
-
0.3
-
1/13/2021
Zinc Total
7.243
4.4
1000
-
5000#
P02
1/14/2021
Barium Total
4.163
1.1
700
-
2000
1/14/2021
Barium Total
111
1.1
700
-
2000
PO4
1/14/2021
Copper Total
15.6
1.6
1000
-
1300^
1/14/2021
Zinc Total
4.453
4.4
1000
-
5000#
1/14/2021
Barium Total
12.9
1.1
700
-
2000
P05
1/14/2021
Beryllium Total
0.179 J
0.16
-
4
4
1/14/2021
Copper Total
1.911
1.6
1000
-
1300^
1/14/2021
Barium Total
58.8
1.1
700
-
2000
P06
1/14/2021
Beryllium Total
0.3373
0.16
-
4
4
1/14/2021
Zinc Total
4.893
4.4
1000
-
5000#
1/14/2021
Barium Total
216
1.1
700
-
2000
1/14/2021
Beryllium Total
0.4643
0.16
-
4
4
1/14/2021
Cobalt Total
LL 2.38 J
1.4
-
1
-
P07
1/14/2021
Copper Total
3.12 J
1.6
1000
-
1300^
1/14/2021
Nickel Total
4.141
2.2
100
-
-
1/14/2021
Vanadium Total
2.313
1.4
-
0.3
-
1/14/2021
Barium Total
116
1.1
700
-
2000
1/14/2021
Beryllium Total
0.7611
0.16
-
4
4
P09
1/14/2021
Cobalt Total
2.663
1.4
-
1
-
1/14/2021
Copper Total
2.033
1.6
1000
-
1300^
1/14/2021
Nickel Total
3.103
2.2
100
-
-
1/14/2021
Barium Total
54.2
1.1
700
-
2000
1/14/2021
Beryllium Total
0.2043
0.16
-
4
4
P13
1/14/2021
Chromium Total
1.733
1.4
10
-
100
1/14/2021
Copper Total
2.163
1.6
1000
-
1300^
1/14/2021
Vanadium Total
1.693
1.4
-
0.3
-
P13D
1/14/2021
1,4-Dioxane
1.53
0.8
3
-
-
1/14/2021
Barium Total
100
1.1
700
-
2000
1/13/2021
1,4-Dioxane
78 D
1.6
3
-
-
1/13/2021
Acetone
123
10
6000
-
-
P16R
1/14/2021
Barium Total
1100
1.1
700
-
2000
1/13/2021
Benzene
0.863
0.15
1
-
5
1/14/2021
Chromium Total
2.883
1.4
10
-
100
1/14/2021
Nickel Total
16.6
2.2
100
-
-
P21
1/14/2021
Barium Total
58
1.1
700
-
2000
1/14/2021
Nickel Total
2.531
2.2
100
-
-
Page 1 of 2

Table 7. List of Compounds Detected during the January 2021 Sampling Event (1/13-1/14/2021)
Northern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well ID
Date
Parameter
Results
(p9/L)
MDL
(p9/L)
NC 2L or 2B
Std* (p9/L)
IMAC
(p9/L)
MCL
(p9/L)
1/14/2021
Barium Total
19.6
1.1
700
-
2000
P23
1/14/2021
Zinc Total
7.76 J
4.4
1000
-
5000"
1/14/2021
1,4-Dichlorobenzen
0.893
0.19
6
-
-
-
-
1/14/2021
1,4-Dioxane
140 D
4
3
1/14/2021
Barium Total
1290
1.1
700
-
2000
1/14/2021
Benzene Total
1.6
0.15
1
-
5
1/14/2021
Beryllium Total
0.980 J
0.16
-
4
4
1/14/2021
Chlorobenzene
5.1
0.17
50
-
100
P29
1/14/2021
Cobalt Total
4.663
1.4
-
1
-
1/14/2021
Ethylbenzene
0.48J
0.13
600
-
700
1/14/2021
Lead
18
3.1
15
-
15
1/14/2021
Nickel Total
7.50 J
2.2
100
-
-
1/14/2021
Selenium Total
2.54
1.82
5
-
50
1/14/2021
Thallium Total
0.2523
0.22
-
0.2
2
1/14/2021
Vanadium Total
36.1
1.4
-
0.3
-
1/14/2021
Zinc Total
5.63 J
4.4
1000
-
5000*
1/14/2021
1,4-Dioxane
2.1
0.8
3
-
-
1/14/2021
Arsenic
100
7.6
10
-
10
1/14/2021
Barium Total
101
1.1
700
-
2000
1/14/2021
Cadmium Total
1.72
0.36
2
-
5
PZ1
1/14/2021
Cobalt Total
2.21 J
1.4
-
1
-
1/14/2021
Copper Total
3.41 J
1.6
1000
-
1300^
1/14/2021
Lead
8.463
3.1
15
-
15
1/14/2021
Nickel Total
3.31 J
2.2
100
-
-
1/14/2021
Vanadium Total
12.4
1.4
-
0.3
-
1/14/2021
Zinc Total
26.4
4.4
1000
-
5000"
1/14/2021
1,4-Dioxane
3.6
0.8
3
-
-
PZ2
1/14/2021
Barium Total
190
1.1
700
-
2000
1/14/2021
Cadmium Total
0.3603
0.36
2
-
5
1/14/2021
Zinc Total
18.3
4.4
1000
-
5000"
Surface Water Samples
1/14/2021
Barium Total
23.9
1.1
21,000+
-
2000
1/14/2021
Beryllium Total
0.2121
0.16
6.5
-
4
1/14/2021
Cobalt Total
8.023
1.4
4
-
-
SWi
1/14/2021
Lead
3.54 J
3.1
0.54-
-
-
1/14/2021
Nickel Total
3.413
2.2
16.10-
-
-
1/14/2021
Vanadium Total
2.15 J
1.4
-
-
-
1/14/2021
Zinc Total
15.3
4.4
36.5"
-
50001,
1/14/2021
Barium Total
40.3
1.1
21,000+
-
2000
SW2
1/14/2021
Chromium Total
1.443
1.4
23.81"
-
-
1/14/2021
Zinc Total
18.8
4.4
36.5-
-
5000*
1/13/2021
1,4-Dioxane
3.5
0.8
80+
-
-
SW4
1/13/2021
Barium Total
40
1.1
21,000+
-
2000
1/13/2021
Zinc Total
1 5.973
1 4.4
1 36.5
-
1 5000#
MDL = Method Detection Limit MCL = Federal Maximum Contaminant Level
IMAC = Interim Maximum Allowable Concentration
J = The analyte was positively identified, but the value is estimated below the reporting limit.
*15A NCAC 2L groundwater standards are listed for all groundwater sampling locations. 15A NCAC 2B standards are
listed for surface water sampling locations (SWi, SW2, and SW4).
Value represents an EPA action level.
#Value represents an EPA secondary Maximum Contaminant Level
+NC In -Stream Target Value for Surface Waters
-Hardness-dependent metal standard calculated assuming an in -stream hardness of 25 mg/L of CaCO3
Concentrations highlighted it yellow were detected above the 2L (or 213) standards.
Concentrations highlighted it orange were detected above the IMAC.
Concentrations highlighted it blue! were detected above the EPA MCL.
Page 2of2

APPENDIX A
CORRESPONDENCE FROM THE
NC DIVISION OF WASTE MANAGEMENT

NORTH (.4i2oL,TI` A DWI=AR3'MTzjgT Off'
taMMONTi ENT kNb NATURAL Pr--soUACt�S
'DMX'Qr[ on 'ArA�-$-YM M.AXI-1.7,M�ls
Sc:p;cmbar•lU, i��8
Mr. PI* G_ Dickerson
Pitt Co=y Etrfreer
Pitt County Office Bnildipa
1717 Wesst:'Pifth St -,et
G --xvi le, N.C. 27834 .
Re: Sbmiannml Water Quatty SamphgR-4quiremcnts for the YwLberrt
Pardon ofthr, Pbt:Couaty Landtll (PerMif #74-01).
]scar Mckerson,
A-acotding to vor telephone tonvtr4dCoa yesterday I have; atlachcd two
Ie[ters 4b Ri may help 01mil'y the s=ping re juirementa for. the narth=portion
of Ibd closed Pitt County landfla, The 17ecernber 277, 1994 letter- spocites the
sampling points and amiyses. This letter also axplains that the s--Imiarmual
sampg cvent5 for hlhc mort.�era portion of facility can be conduct d - lin
simultaneously with the southern Subtitle D oei to prey-,-nt-dupllcadon of
samples. Subsequent letw have modified the Sequ red an lyticar methods.
The- Apffl 8, 19 97 letter disCSss&s the hzi�W]4on of Eve new -wells to the
mouitari❑g Vs4m io 1) acquire data ot. Both the verb f,, I and horizonW ground.
water -flow, 2) to detzrmke the continuity of the "gray clay'! layer- benbath the
-.,site and 3) establish true upgra Rest monitor sL-Wons for hez northern portion
oft]: Iant1fIl- With the additions to Ih8 monitoring system yho Section did nfft
see 6e 4o t;ifjtiisetall ccring samples a rouLrsc basisftDihatr7u:ziosing
points P-14, P-15, F 25, P-25, MW-2A and MV213 become oftheirproxfmjty to
wasto. Afler the ffiftW da;a was colleoted on the abovo itcMs 1-3, the Section
did not T�qufie samples to be taken from tho two new decacr Qpgmdient wells.
Additionally, MW-2 was abandoned.
EU summary, thO fallowing monitoring pofAts.shauld be: Sbmpled on a
semlatmtral basis for -she northern portion of the I"dE (this is -not meant to
oxcit%.e prctiously app=ovedmonitoring requirerrztmLfor the smithern pordon):
M)V-1, M-W-3. P-1. P-2. P-C P-5, P-A P-7, P-9, F-13, F-I6, P-21, F-23, the -Mo
nevv upgtadient shallow woUs and the now downgradieeL well ncsted with P-I 3.
Prtt-aFproved swxaee waterloeataons should also be sampled. Poteraiometric
data sliaWd. N— collected our all wells at ilre site dur D mclh sampling episode and
-a p aUnflometric map submitted -with each serniaimusl data paa3ag--
401 o�cr.�n+ 79a.a5, ourrC i7t{1. fi rlL�laf71 .1C 3�4C7
A'!1C?!L Et10-7�3•+1ov6 FAX RSn 711-�IIIIS
M1hl E.'sLld L U pr��RiUH1l'1' t Ar^ 1f1 h. �571vc .Surf Pi`11f.�1ryyrrn- L-[}�};, nCCyu Lraf E O'� l.O �ti-La aLlsxiLh PAF•Cll

If to -County desires to tkop-or add moat Wring lioints to the semiaumual sampling -
routine; please submit piolacsals to the Solid Waste Section for "Oluation.and approval. If you
have auy questions or wmments, please call me at 919-733-0692, cAensiorr 261.
Sincercly,
Ivla- Poindexter, Hydrogeologist
droundwater Compliance Unit
Solid Wye Section
c: Philip Prete
'ferry Dover
Pobby Nelms
Centaal f 1e

NCDENR
North Carolina department of Environment and
Dexter R. Matthews, Director
Mr. Philip G. Dickerson
Pitt County Engineer
Pitt County Office Building
1717 West Fifth Street
Greenville, NC 27834
Division of Waste Management
.Tune 14, 2004
Natural Resources
Michael F. Easley, Governor
William G. Ross Jr., Secretary
RE: Environmental Monitoring Requirements — Pitt County Landfill, Northern Portion (Permit # 74-01)
Dear Mr. Dickerson:
The proposal submitted by Groundwater Management Associates, Inc. (GMA) on behalf of Pitt County to
stop water quality monitoring of the northern portion on the Pitt County Landfill has been reviewed. The
northern portion of the facility is subject to monitoring requirements specified in 15A NCAC 13B .0600.
Rule .0601 (a) states, "The Division shall require a solid waste management facility to provide such
ground -water monitoring capability as the Division detennines to be necessary to detect the effects of the
facility on ground -water in the area." As stated in .0601 (a) (1-5), a number of factors can be used in
making such a determination. In addition to monitoring data, the "type of waste" the landfill accepted, the
ground -water level in the area, and "uses that are being or may be made of any ground -water" that may
have been affected by the facility are all important factors in determining monitoring requirements.
Atter reviewing these factors, the Solid Waste Section will continue to require limited water quality
monitoring at the landfill for the following reasons:
1. There is increased residential and business development on property adjacent to the facility.
Other properties in the general area of the site are also being developed,
2. The landfill is unlined and therefore continues to produce leachate that affects groundwater.
The affected groundwater eventually moves from beneath the site.
3. The leachate may have contaminants that pose a risk to human health and the environment.
4. Although there is public water available in the general area of the landfill, there area number
of potable supply wells within 500 feet of the landfill according to the 2001 Hurricane
Landfill Assessment Project survey for the NC Department of Envirorunent and Natural
Resources.
However a modification of current monitoring requirements will be permitted. Beginning this calendar
year, the Solid Waste Section will allow annual groundwater and surface water monitoring for the northern
portion of the Pitt County Landfill. The wells and surface water locations will be sampled for the same list
of constituents as have been sampled for in the past. Because the hydraulic gradient in the area is low,
groundwater is slow to move and annual sampling should provide adequate detection monitoring for
contaminant releases.
The southern portion will continue to he subject to the monitoring requirements of 15A NCAC 13B .1630
through ,1637,
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone [phone] FAX [phone] Internet http.1//wastenotnc,org
An Equal Oppanurii;y l Af irrnatias Action Employer— Nnied on Dual Purpose Recycled Paper

One additional environmental monitoring issue for the northern portion of the landfill needs to be
addressed, and that is the need to monitor for methane gas. Solid waste management rules require that
concentrations of explosive gases, such as methane, not exceed the lower explosive limit of 5% by volume
at the property boundary (15A NCAC 13B A503). Because of the property development adjacent to the
landfill there should be documentation that there is no threat to public health from the off -site migration of
methane. The only reliable way to insure the detection of methane is to install a permanent methane
monitoring system. The bar punch method with temporary monitoring locations that is being used at the
landfill is not an acceptable method.
Therefore the Solid Waste Section is requiring Pitt County to install a permanent methane monitoring
system along the northern property boundary between the landfill and the adjacent residential property that
is being developed. A methane monitoring plan that includes sampling probe construction design,
proposed probe locations, and sampling methodology should be submitted to the Solid Waste Section for
approval before implementation. A monitoring system installed according to accepted industry standards
can provide more accurate and reproducible information and increase the confidence level that protection
of public health is being served.
Thank you for your cooperation with this important matter. If you have any questions, please call me at
[phone], extension257.
Sincerely,
Larry Rose
Solid Waste section
cc: .lames C. Coffey— Chief, Solid Waste Section
Mark Poindexter — Head, Field Operations Branch
Mark Fry — Eastern District Supervisor
Chuck Boyette — Waste Management Specialist
Pete Moncla, P.G. — GMA, Inc.

Waste Management
ENVIRONMENTAL QUALITY
March 16, 2017
Sent Via Email — iohn.demary@pittcountync.�ov
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Proposal for Assessment of Benzene Contamination Migration
Pitt County MSW Landfill (Northern and Southern)
Pitt County
Solid Waste Permit Number 74-01
DIN 27529
Dear Mr. Demary:
ROY COOPER
MICHAEL S. REGAN
Sec retao
MICHAEL SCOTT
Director
The NC Solid Waste Section has completed a review of the Proposal for Assessment of Benzene
Contamination Migration dated March 15, 2017 (DIN 27528) submitted on your behalf by Groundwater
Management Associates, Inc. (GMA) for the closed Pitt County MSW Landfill, NC Solid Waste Permit
Number 7401. During the January 2017 semiannual water quality monitoring event benzene was
detected at concentrations exceeding the NC 2L Groundwater Standards in two groundwater monitoring
wells.
Based upon the groundwater exceedances, Pitt County is requesting to collect two pore water samples
from the beneath the southern boundary ditch and analyze for Appendix I constituents. The proposed
sampling locations are located downgradient of groundwater monitoring well P20R and will be sampled
during the July 2017 semiannual water quality monitoring event.
As a result, the Proposal for Assessment of Benzene Contamination Migration is approved as described. If
you have any questions, please feel free to contact me by email at [e-mail] or
by phone at 828.296.4706. Thank you for your continued cooperation with this matter.
Sincerely,
L)4—
Jaclynne Drummond
Compliance Hydrogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
State of North Carolina I Environmental Quality I Waste Management
Asheville Regional Office 1 2090 U.S. Highway 70 1 Swannanoa, NC 28778
828 296 4500

cc sent via email: Tim Corley, Pitt County Engineer
Jason Watkins, Field Operations Branch Head
Drew Hammonds, Eastern District Supervisor
Ray Williams, Environmental Senior Specialist
Elizabeth Werner, Permitting Hydrogeologist
Emma Shipley, GMA
Steve Campbell, GMA
Slaivul Nw1hCon}Ilea h k ivlrurunrntal+2ua11ty I WasteManagemenl
Ashevile I funal lftr 1 10%) U.'� I Itghwuy 10 1 5wannanoa, NC 28778
828 2% 4.500

APPENDIX B
SAMPLING RECORDS

are zI
GMA Project 25101. Pitt County Landfill Jan 2620-Field Sheet
Collected By: ;FHs / �.
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Field Parameters
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All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
l = Appendix 1 11 = Appendix Il
GMA 0

GMA Project 25101: Pitt County Landfill Jan 2020 Field Sheet
Collected By: F: Vc S
p m
VField
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? Temp
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Notes swell/lock
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N q
r
a '
x u .
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collected Sampling Sampling
condition, etc.}
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V (in gallons) = 70.5 rlh = 0.4856745 * In
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
GMA
I = Appendix I 11 = Appendix 11

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Collected By: f As Z C 5.
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completion/
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m
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temp Gendact- ©O
Water level Volatiles Metals
Notes [well/lock
Well
,M
F $
a
_ �°
ij 3
pH
[OQ i+Ar(vS) [mg/L) Turbidity
collected Sampling Sampling
condition, etc.)
c,
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�L' end
5• 7
� �. �
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V (in gallons) = 70.5 r 2 h = 0.4856745 * h
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
GMA 0
I = Appendix 1 Ii = Appendix II

GMA Project 25101: Pitt County Landfill Jan 2020 Field Sheet
Collected By: �#}� G s
�
ry.
Field Parameters
Date/Time
Purging
m
5
m
a
a
3 Y
$ v e
o
m
H @
o
e
completion]
,�
oiv
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a
a,
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ai
Temp
@tfl'1^d—uct-
DO
Water level
Volatiles Metals
Notes (well/lock
Well
V,
in
x
p = U
m V
tv 3
3
pH (°�)
it ►(Wl
tmg/Ll
Turbidity.
collected
Sampling Sampling
condition, etc.)
ist
�� �d
[ {�.
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`f , L'
2.
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a
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..�=i1
`1 t ILA
r'Lll
PI2
a I
-
V (in gallons) = 70.5 rah = 0.4856745 * h
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
GMA 0
I = Appendix 1 11= Appendix II

GMA Project 25101: Pitt County Landfill Jan 2020 Field Sheet
Collected By: Ft+S A59
Field Parameters
Date/Time
L
a.+
C
Y
19 £ A O
o
r
19
3 3 ,a
Purging
a
w a d m
> ,a
fl
completion/
£
m
? d o 0°
temp Conduct-
Do
Water level
Volatiles Metals
Notes (welVlock
Well
;°
p
a°
p
M U ?�IV
r,1p� 3
W
PH (°C) ivity (µ5)
Img/L) ,Turbidity
collected
Sampling Sampling
condition, etc.)
(01V Li
M �
!
30
FB
, l
Es
_
I
t3 Zy 57
Collect surface water samples facing upstream. Collect 'from point of confluence for 5W2
EB: Pour lab DI water into bailer and over gloves and rope into ss pitcher then into sample containers.
rB: Use lab DI water to fill sample containers directly. Collect on -site preferably near the dirt road within the landfill.
V (in gallons) = 70.5 r'h = 0.4856745 * h
All wells 2 in in diameter. Use r = 0.083 feet
* = Use Teflon bailers for delayed metals analysis
GMA 0
I = Appendix 1 11= Appendix II

APPENDIX C
LABORATORY REPORT AND CHAIN -OF -CUSTODY FORMS FOR
WATER SAMPLES

ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, February 10, 2021
Groundwater Management Associates, Inc. (GR022)
Attn: Emma Shipley
4300 Sapphire Court, Suite 100
Greenville, NC 27834
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Pitt County Landfill - App I
ENCO Workorder(s): CE00125
Dear Emma Shipley,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, January 15, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 99

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PROJECT NARRATIVE
Client: Groundwater Management Associates, Inc. (GR022)
Project: Pitt County Landfill - App I
Lab ID: CE00125
Overview
Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods
referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in
the QC Remarks section below.
Quality Control Samples
The associated LCS exhibited high bias; since the result is ND, there is no impact (QL-02).
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an acceptable
LCS recovery (QM-07).
Post -digestion spike did not meet method requirements due to confirmed matrix effects (QM-08).
Quality Control Remarks
This compound is a common laboratory contaminant (0-01).
The internal standard(s) for this sample were outside the acceptance limits due to sample matrix interference. The sample
was re -analyzed at a dilution (QI-03).
The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01).
Other Comments
The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any
exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of
the report.
Released By:
Environmental Conservation Laboratories, Inc.
Chuck Smith
Project Manager
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-MW1R
Lab ID: CE00125-01
Sampled: 01/14/21 16:59
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 09:42
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:22
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 17:27
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 11:24
Client ID: 7401-MWlR
Lab ID: CE00125-01RE1
Sampled: 01/14/21 16:59
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:10
Client ID: 7401-MW3
Lab ID: CE00125-02
Sampled: 01/14/21 15:20
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:08
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 10:48
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 17:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 11:50
Client ID: 7401-MW3
Lab ID: CE00125-02RE1
Sampled: 01/14/21 15:20
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:12
Client ID: 7401-MW6R
Lab ID: CE00125-03
Sampled: 01/14/21 08:31
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 18:27
EPA 8260D
EPA 5030B_MS
01/28/21
01/20/21 00:00
01/20/21 12:15
Client ID: 7401-MW6R
Lab ID: CE00125-04
Sampled: 01/14/21 16:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:11
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:26
Client ID: 7401-MW6R
Lab ID: CE00125-04RE1
Sampled: 01/14/21 16:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:14
Client ID: 7401-MW8
Lab ID: CE00125-05
Sampled: 01/13/21 11:09
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/12/21
01/18/21 09:22
01/20/21 10:13
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:43
01/26/21 11:31
EPA 8260D
EPA 5030B_MS
01/27/21
01/14/21 15:24
01/15/21 19:34
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 00:00
01/20/21 12:40
Client ID: 7401-MW8
Lab ID: CE00125-OSRE1
Sampled: 01/13/21 11:09
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/12/21
01/18/21 09:43
02/04/21 15:15
Client ID: 7401-122
Lab ID: CE00125-06
Sampled: 01/14/21 15:05
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:15
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:35
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 18:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 13:19
Client ID: 7401-132
Lab ID: CE00125-06RE1
Sampled: 01/14/21 15:05
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:17
FINAL
This report
relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 3 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-134
Lab ID: CE00125-07
Sampled: 01/13/21 12:15
Received: O1/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
01/27/21
01/14/21 15:24
01/15/21 20:04
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 00:00
01/20/21 13:45
Client ID: 7401-124
Lab ID: CE00125-08
Sampled: 01/14/21 12:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:07
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:39
Client ID: 7401-124
Lab ID: CE00125-08RE1
Sampled: 01/14/21 12:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:18
Client ID: 7401-P5
Lab ID: CE00125-09
Sampled: 01/14/21 17:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:20
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:43
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 19:27
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 14:10
Client ID: 7401-P6
Lab ID: CE00125-10
Sampled: 01/14/21 12:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:10
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:48
EPA 8260D
EPA 5030B_MS
01/28/21
01/19/21 12:39
01/19/21 19:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 14:35
Client ID: 7401-136
Lab ID: CE00125-30RE1
Sampled: 01/14/21 12:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:20
Client ID: 7401-P7
Lab ID: CE00125-11
Sampled: 01/14/21 11:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 10:25
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:52
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 20:27
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 15:00
Client ID: 7401-137
Lab ID: CE00125-11RE1
Sampled: 01/14/21 11:25
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:21
Client ID: 7401-139
Lab ID: CE00125-12
Sampled: 01/14/21 11:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:12
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 11:56
EPA 8260D
EPA 503013_MS
01/28/21
01/19/21 12:39
01/19/21 20:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 15:26
Client ID: 7401-139
Lab ID: CE00125-12RE1
Sampled: 01/14/21 11:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:23
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-P11R
Lab ID: CE00125-13
Sampled: 01/14/21 09:28
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:15
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:01
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 12:39
01/19/21 21:27
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 15:51
Client ID: 7401-P11R
Lab ID: CE00125-13RE1
Sampled: 01/14/21 09:28
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:24
Client ID: 7401-1312
Lab ID: CE00125-14
Sampled: 01/14/21 09:55
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:22
01/20/21 11:22
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:35
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 12:39
01/19/21 21:57
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 00:00
01/20/21 16:16
Client ID: 7401-1213
Lab ID: CE00125-15
Sampled: 01/14/21 14:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:13
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:39
EPA 8260D
EPA 503013_MS
O1/28/21
01/20/21 00:00
01/20/21 16:41
Client ID: 7401-1313
Lab ID: CE00125-15RE1
Sampled: 01/14/21 14:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:29
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 12:39
01/20/21 16:06
Client ID: 7401-1213D
Lab ID: CE00125-16
Sampled: 01/14/21 14:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:35
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:43
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 12:39
01/19/21 22:57
EPA 8260D
EPA 5030B_MS
O1/28/21
01/20/21 00:00
01/20/21 17:07
Client ID: 7401-P13D
Lab ID: CE00125-16RE1
Sampled: 01/14/21 14:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:31
Client ID: 7401-P16R
Lab ID: CE00125-17
Sampled: 01/13/21 15:13
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 8260D
EPA 503013_MS
O1/27/21
01/14/21 15:24
01/15/21 20:34
EPA 8260D
EPA 503013_MS
O1/27/21
01/20/21 00:00
01/20/21 19:13
Client ID: 7401-P16R
Lab ID: CE00125-18
Sampled: 01/14/21 09:07
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:37
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:47
Client ID: 7401-131611
Lab ID: CE00125-18RE1
Sampled: 01/14/21 09:07
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:32
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1337
Lab ID: CE00125-19
Sampled: 01/13/21 15:35
Received: O1/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/12/21
01/18/21 09:33
01/21/21 11:40
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:43
01/26/21 12:52
EPA 8260D
EPA 503013_MS
O1/27/21
01/14/21 15:24
01/15/21 21:04
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 00:00
01/20/21 17:32
Client ID: 7401-1317
Lab ID: CE00125-19RE1
Sampled: 01/13/21 15:35
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:43
02/04/21 15:34
Client ID: 7401-1319
Lab ID: CE00125-20
Sampled: 01/13/21 16:11
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
O1/27/21
01/14/21 15:24
01/15/21 21:34
EPA 8260D
EPA 5030B_MIS
O1/27/21
01/20/21 00:00
01/20/21 19:38
Client ID: 7401-P19
Lab ID: CE00125-21
Sampled: 01/14/21 10:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:42
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 12:56
Client ID: 7401-P19
Lab ID: CE00125-21RE1
Sampled: 01/14/21 10:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:35
Client ID: 7401-P20R
Lab ID: CE00125-22
Sampled: 01/13/21 16:35
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
01/27/21
01/14/21 15:24
01/15/21 22:04
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 00:00
01/20/21 17:57
Client ID: 7401-1320R
Lab ID: CE00125-23
Sampled: 01/14/21 10:18
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:45
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
01/26/21 13:00
Client ID: 7401-132011
Lab ID: CE00125-23RE1
Sampled: 01/14/21 10:18
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:43
02/04/21 15:37
Client ID: 7401-1320D
Lab ID: CE00125-24
Sampled: 01/14/21 16:20
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:47
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 08:29
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 08:33
EPA 8260D
EPA 5030B_MS
O1/28/21
01/20/21 00:00
01/20/21 18:23
EPA 8260D
EPA 503013_MS
O1/28/21
01/20/21 10:35
01/20/21 19:20
Client ID: 7401-12201)
Lab ID: CE00125-24RE1
Sampled: 01/14/21 16:20
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 08:56
Client ID: 7401-P21
Lab ID: CE00125-25
Sampled: 01/14/21 09:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:49
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:04
EPA 8260D
EPA 5030B_MS
O1/28/21
01/20/21 00:00
01/20/21 18:48
EPA 8260D
EPA 503013_MS
O1/28/21
01/20/21 10:35
01/20/21 19:48
FINAL
This report
relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 6 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1321
Lab ID: CE00125-25RE3
Sampled: 01/14/21 09:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:39
Client ID: 7401-1323
Lab ID: CE00125-26
Sampled: 01/13/21 14:55
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
O1/27/21
01/14/21 15:24
01/15/21 22:34
EPA 8260D
EPA 503013_MS
01/27/21
01/20/21 14:20
01/21/21 00:15
Client ID: 7401-1323
Lab ID: CE00125-27
Sampled: 01/14/21 08:45
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:52
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:09
Client ID: 7401-P28
Lab ID: CE00125-28
Sampled: 01/13/21 15:45
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
O1/27/21
01/19/21 11:22
01/19/21 18:30
EPA 8260D
EPA 503013_MS
O1/27/21
01/20/21 14:20
01/21/21 00:40
Client ID: 7401-1328
Lab ID: CE00125-29
Sampled: 01/14/21 10:05
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:54
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:39
Client ID: 7401-1228
Lab ID: CE00125-29RE1
Sampled: 01/14/21 10:05
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:40
Client ID: 7401-1329
Lab ID: CE00125-30
Sampled: 01/14/21 13:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 11:56
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:43
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 18:58
EPA 8260D
EPA 503013_MS
O1/28/21
01/22/21 00:00
01/22/21 18:06
Client ID: 7401-1229
Lab ID: CE00125-30RE1
Sampled: 01/14/21 13:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:42
Client ID: 7401-SW1
Lab ID: CE00125-31
Sampled: 01/14/21 17:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:42
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:48
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 19:25
EPA 8260D
EPA 5030B_MIS
O1/28/21
01/20/21 14:20
01/21/21 01:06
Client ID: 7401-SW1
Lab ID: CE00125-31RE1
Sampled: 01/14/21 17:40
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:43
Client ID: 7401-SW2
Lab ID: CE00125-32
Sampled: 01/14/21 15:37
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:44
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 09:52
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 19:53
EPA 8260D
EPA 5030B_MS
O1/28/21
01/20/21 14:20
01/21/21 01:31
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-SW2
Lab ID: CE00125-32RE3
Sampled: 01/14/21 15:37
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020B
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:48
Client ID: 7401-SW4
Lab ID: CE00125-33
Sampled: 01/13/21 17:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/12/21
01/18/21 09:33
01/21/21 12:46
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:46
01/26/21 09:56
EPA 8260D
EPA 503013_MS
O1/27/21
01/18/21 11:52
01/18/21 20:51
EPA 8260D
EPA 503013_MS
O1/27/21
01/20/21 14:20
01/21/21 01:56
Client ID: 7401-SW4
Lab ID: CE00125-33RE1
Sampled: 01/13/21 17:10
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:46
02/04/21 15:50
Client ID: 7401-PZ1
Lab ID: CE00125-34
Sampled: 01/14/21 10:55
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:48
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 10:01
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 20:20
EPA 8260D
EPA 503013_MS
01/28/21
01/22/21 00:00
01/22/21 17:40
Client ID: 7401-PZ3
Lab ID: CE00125-34RE1
Sampled: 01/14/21 10:55
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:51
Client ID: 7401-PZ2
Lab ID: CE00125-35
Sampled: 01/14/21 10:30
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:51
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 10:05
EPA 8260D
EPA 503013_MS
O1/28/21
01/19/21 11:22
01/19/21 20:47
EPA 8260D
EPA 503013_MS
01/28/21
01/20/21 14:20
01/21/21 02:21
Client ID: 7401-PZ2
Lab ID: CE00125-35RE1
Sampled: 01/14/21 10:30
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
02/04/21 15:53
Client ID: 7401-EB
Lab ID: CE00125-36
Sampled: 01/13/21 16:57
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/12/21
01/18/21 09:33
01/21/21 12:53
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:46
01/26/21 10:09
EPA 8260D
EPA 503013_MS
O1/27/21
01/18/21 11:52
01/18/21 16:17
EPA 8260D
EPA 503013_MS
O1/27/21
01/20/21 14:20
01/21/21 02:47
Client ID: 7401-EB
Lab ID: CE00125-36RE1
Sampled: 01/13/21 16:57
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6020E
EPA 3005A
07/12/21
01/18/21 09:46
02/04/21 15:54
Client ID: 7401-FB
Lab ID: CE00125-37
Sampled: 01/14/21 09:30
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/13/21
01/18/21 09:33
01/21/21 12:56
EPA 6020E
EPA 3005A
07/13/21
01/18/21 09:46
01/26/21 10:13
EPA 8260D
EPA 5030B_MS
O1/28/21
01/19/21 11:22
01/19/21 17:08
Client ID: 7401-FB
Lab ID: CE00125-37RE1
Sampled: 01/14/21 09:30
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
O1/28/21
01/22/21 00:00
01/22/21 11:21
FINAL
This report
relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 99

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-TripBlank
Lab ID: CE00125-38RE3
Sampled: 01/13/21 00:00
Received: O1/15/21 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
O1/27/21
01/25/21 16:38
01/25/21 19:44
Client ID: 7401-TripBlank
Lab ID: CE00125-39RE1
Sampled: 01/13/21 00:00
Received: 01/15/21 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
O1/27/21
01/25/21 16:38
01/25/21 20:12
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 99

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SAMPLE DETECTION SUMMARY
Client ID: 7401-MWlR
Lab ID:
CE00125-01
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
54.6
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.348
J
0.160
1.00
ug/L
EPA 6010D
Client ID: 7401-MW3
Lab ID:
CE00125-02
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
190
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.221
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
5.97
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
5.82
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
3.29
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
26.7
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-MW6R
Lab ID:
CE00125-03
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
6.5
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-MW6R
Lab ID:
CE00125-04
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
2120
1.10
10.0
ug/L
EPA 6010D
Nickel - Total
2.71
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-MW8
Lab ID:
CE00125-05
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
11.8
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.375
J
0.160
1.00
ug/L
EPA 6010D
Copper - Total
1.98
J
1.60
10.0
ug/L
EPA 6010D
Vanadium - Total
2.88
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
7.24
1
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-132
Lab ID:
CE00125-06
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
4.16
J
1.10
10.0
ug/L
EPA 6010D
Client ID: 7401-134
Lab ID:
CE00125-08
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
111
1.10
10.0
ug/L
EPA 6010D
Copper - Total
15.6
1.60
10.0
ug/L
EPA 6010D
Zinc - Total
4.45
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P5
Lab ID:
CE00125-09
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
12.9
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.179
1
0.160
1.00
ug/L
EPA 6010D
Copper - Total
1.91
1
1.60
10.0
ug/L
EPA 6010D
Client ID: 7401-136
Lab ID:
CE00125-10
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
58.8
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.337
J
0.160
1.00
ug/L
EPA 6010D
Zinc - Total
4.89
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-137
Lab ID:
CE00125-11
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
216
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.464
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.38
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
3.12
J
1.60
10.0
ug/L
EPA 6010D
Nickel- Total
4.14
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
2.31
J
1.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 99

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SAMPLE DETECTION SUMMARY
Client ID: 7401-P9
Lab ID:
CE00125-12
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
116
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.761
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.66
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
2.03
J
1.60
10.0
ug/L
EPA 6010D
Nickel- Total
3.10
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-P11R
Lab ID:
CE00125-13
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
99.2
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
1.93
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.38
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
7.10
J
1.60
10.0
ug/L
EPA 6010D
Nickel - Total
3.28
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
4.67
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
39.8
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1312
Lab ID:
CE00125-14
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
34.9
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.553
J
0.160
1.00
ug/L
EPA 6010D
Client ID: 7401-1313
Lab ID:
CE00125-15
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
54.2
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.204
J
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
1.73
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
2.16
J
1.60
10.0
ug/L
EPA 6010D
Vanadium - Total
1.69
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P13D
Lab ID:
CE00125-16
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
1.5
J
0.80
2.0
ug/L
EPA 8260D
Barium - Total
100
1.10
10.0
ug/L
EPA 6010D
Client ID: 7401-P16R
Lab ID:
CE00125-17
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
78
D
1.6
4.0
ug/L
EPA 8260D
Acetone
12
J
10
20
ug/L
EPA 8260D
Benzene
0.86
J
0.15
1.0
ug/L
EPA 8260D
Client ID: 7401-11316R
Lab ID:
CE00125-18
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
1100
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.88
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
16.6
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-1317
Lab ID:
CE00125-19
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
5.0
0.80
2.0
ug/L
EPA 8260D
Barium - Total
147
1.10
10.0
ug/L
EPA 6010D
Benzene
0.43
J
0.15
1.0
ug/L
EPA 8260D
Beryllium - Total
1.43
0.160
1.00
ug/L
EPA 6010D
Chlorobenzene
4.3
0.17
1.0
ug/L
EPA 8260D
Copper - Total
1.89
J
1.60
10.0
ug/L
EPA 6010D
Nickel - Total
2.79
J
2.20
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 99

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SAMPLE DETECTION SUMMARY
Client ID: 7401-1319
Lab ID:
CE00125-20
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,1-Dichloroethane
4.2
0.13
1.0
ug/L
EPA 8260D
1,4-Dichlorobenzene
5.1
0.19
1.0
ug/L
EPA 8260D
1,4-Dioxane
160
D
2.0
5.0
ug/L
EPA 8260D
Benzene
4.0
0.15
1.0
ug/L
EPA 8260D
Chlorobenzene
7.0
0.17
1.0
ug/L
EPA 8260D
cis-1,2-Dichloroethene
2.7
0.15
1.0
ug/L
EPA 8260D
Ethylbenzene
1.8
0.13
1.0
ug/L
EPA 8260D
m,p-Xylenes
0.42
J
0.17
2.0
ug/L
EPA 8260D
o-Xylene
0.56
J
0.065
1.0
ug/L
EPA 8260D
Vinyl chloride
0.57
J
0.32
1.0
ug/L
EPA 8260D
Xylenes (Total)
0.98
J
0.45
3.0
ug/L
EPA 8260D
Client ID: 7401-1319
Lab ID:
CE00125-21
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
1870
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
15.3
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
19.3
1.40
10.0
ug/L
EPA 6010D
Copper - Total
1.72
J
1.60
10.0
ug/L
EPA 6010D
Lead - Total
6.07
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
29.4
2.20
10.0
ug/L
EPA 6010D
Selenium - Total
2.08
1.82
2.00
ug/L
EPA 6020E
Vanadium - Total
1.46
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
120
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-132011
Lab ID:
CE00125-22
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,4-Dioxane
2.1
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-132011
Lab ID:
CE00125-23
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
51.4
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
1.66
0.160
1.00
ug/L
EPA 6010D
Vanadium - Total
2.44
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
12.1
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-132013
Lab ID:
CE00125-24
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
112
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
8.87
0.160
1.00
ug/L
EPA 6010D
Cadmium - Total
0.756
J
0.360
1.00
ug/L
EPA 6010D
Chromium - Total
12.9
1.40
10.0
ug/L
EPA 6010D
Lead - Total
5.43
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
4.31
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
12.6
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
20.1
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1321
Lab ID:
CE00125-25
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
58.0
1.10
10.0
ug/L
EPA 6010D
Nickel - Total
2.53
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-1323
Lab ID:
CE00125-27
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
19.6
1.10
10.0
ug/L
EPA 6010D
Zinc - Total
7.76
J
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 99

(� �Eo
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SAMPLE DETECTION SUMMARY
Client ID: 7401-1328
Lab ID:
CE00125-29
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
38.4
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.741
3
0.160
1.00
ug/L
EPA 6010D
Copper - Total
2.49
3
1.60
10.0
ug/L
EPA 6010D
Nickel- Total
3.16
3
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
1.53
3
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
14.0
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P29
Lab ID:
CE00125-30
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,4-Dichlorobenzene
0.89
3
0.19
1.0
ug/L
EPA 8260D
1,4-Dioxane
140
D
4.0
10
ug/L
EPA 8260D
Barium - Total
1290
1.10
10.0
ug/L
EPA 6010D
Benzene
1.6
0.15
1.0
ug/L
EPA 8260D
Beryllium - Total
0.980
3
0.160
1.00
ug/L
EPA 6010D
Chlorobenzene
5.1
0.17
1.0
ug/L
EPA 8260D
Cobalt - Total
4.66
3
1.40
10.0
ug/L
EPA 6010D
Ethylbenzene
0.48
3
0.13
1.0
ug/L
EPA 8260D
Lead - Total
18.0
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
7.50
3
2.20
10.0
ug/L
EPA 6010D
Selenium - Total
2.54
1.82
2.00
ug/L
EPA 6020E
Vanadium - Total
36.1
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
5.63
3
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1329
Lab ID:
CE00125-30RE3
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Thallium - Total
0.252
3
0.220
2.00
ug/L
EPA 6020E
Client ID: 7401-SW3
Lab ID:
CE00125-31
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
23.9
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.212
3
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
8.02
3
1.40
10.0
ug/L
EPA 6010D
Lead - Total
3.54
3
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
3.41
3
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
2.15
3
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
15.3
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-SW2
Lab ID:
CE00125-32
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
40.3
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
1.44
3
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
18.8
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-SW4
Lab ID:
CE00125-33
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
3.5
0.80
2.0
ug/L
EPA 8260D
Barium - Total
40.0
1.10
10.0
ug/L
EPA 6010D
Zinc - Total
5.97
3
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-PZI
Lab ID:
CE00125-34
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
2.1
0.80
2.0
ug/L
EPA 8260D
Arsenic - Total
100
7.60
10.0
ug/L
EPA 6010D
Barium - Total
101
1.10
10.0
ug/L
EPA 6010D
Cadmium - Total
1.72
0.360
1.00
ug/L
EPA 6010D
Cobalt - Total
2.21
3
1.40
10.0
ug/L
EPA 6010D
Copper - Total
3.41
3
1.60
10.0
ug/L
EPA 6010D
Lead - Total
8.46
3
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
3.31
3
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
12.4
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
26.4
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 99

(� �Eo
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: 7401-PZ2
Lab ID:
CE00125-35
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,4-Dioxane
3.6
0.80
2.0
ug/L
EPA 8260D
Barium - Total
190
1.10
10.0
ug/L
EPA 6010D
Cadmium - Total
0.360
J
0.360
1.00
ug/L
EPA 6010D
Zinc - Total
18.3
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-EB
Lab ID:
CE00125-36
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
2-Hexanone
1.9
J
0.88
5.0
ug/L
EPA 8260D
Carbon disulfide
53
1.5
5.0
ug/L
EPA 8260D
Zinc - Total
114
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-FB
Lab ID:
CE00125-37
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Acetone
14
J
10
20
ug/L
EPA 8260D
Client ID: 7401-TripBlank
Lab ID:
CE00125-38RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Acetone
67
10
20
ug/L
EPA 8260D
0-01
Client ID: 7401-TripBlank
Lab ID:
CE00125-39RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Acetone
31
10
20
ug/L
EPA 8260D
0-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MWlR Lab Sample ID:CE00125-01 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:59 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
17:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
17:27
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Ethylbenzene [500-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
17:27
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
17:27
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 15 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MWlR Lab Sample ID:CE00125-01 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:59 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 17:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 17:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
56
1
50.0
112 %
53-136
IA19023
EPA 8260D
01/19/21 17:27
REF
Dibromofluoromethane
50
1
50.0
99 %
67-129
IA19023
EPA 6260D
01119121 17:27
REF
Toluene-d8
49
1
50.0
98 %
59-134
IA19023
EPA 6260D
01119121 17:27
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:22
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Barium [7440-39-3]^
54.6
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 09:42
JDH
Beryllium [7440-41-7]^
0.348
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 09:42
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 09:42
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:22
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:10
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 09:42
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 11:24
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
108 %
75-125
1A20026
EPA 8260D
01120121 11:24
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW3 Lab Sample ID:CE00125-02 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 15:20 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
17:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
17:57
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
17:57
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
17:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 17 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW3 Lab Sample ID:CE00125-02 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 15:20 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 17:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 17:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
59
1
50.0
117 %
53-136
IA19023
EPA 8260D
01/19/21 17:57
REF
Dibromofluoromethane
54
1
50.0
109 %
67-129
IA19023
EPA 6260D
01119121 17:57
REF
Toluene-d8
55
1
50.0
109 %
59-134
IA19023
EPA 6260D
01119121 17:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 10:48
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Barium [7440-39-3]^
190
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Beryllium [7440-41-7]^
0.221
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 10:08
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:08
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Cobalt[7440-48-4]^
5.97
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Nickel[7440-02-O]^
5.82
J
ug/L
1
2.20
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 10:48
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:08
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:12
RLF
Vanadium [7440-62-2]^
3.29
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Zinc[7440-66-6]^
26.7
ug/L
1
4.40
10.0
lA18012
EPA 6010D
01/20/21 10:08
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 11:50
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.1
1
5.00
103 %
75-125
1A20026
EPA 8260D
01120121 11:50
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CE00125-03 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2108:31 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
18:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
18:27
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
18:27
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
18:27
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 19 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CE00125-03 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2108:31 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 18:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 18:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
59
1
50.0
119 %
53-136
IA19023
EPA 8260D
01119121 18:27
REF
Dibromofluoromethane
52
1
50.0
103 %
67-129
IA19023
EPA 6260D
01119121 16:27
REF
Toluene-d8
54
1
50.0
108 %
59-134
IA19023
EPA 6260D
01119121 16:27
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
6.5
ug/L
1
0.80 2.0
1A20026
EPA 8260D
01/20/21 12:15
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/yzed By Notes
Toluene-d8 5.4 1 5.00 109 % 75-125 1A20026 EPA 8260D 01120121 12:15 KKW
Description: 7401-MW6R Lab Sample ID:CE00125-04 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P-9 L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 11:26
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Barium [7440-39-3]^
2120
ug/L
1
1.10
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18012
EPA 6010D
01/20/21 10:11
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:11
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Nickel[7440-02-O]^
2.71
J
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 11:26
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:14
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:11
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW8 Lab Sample ID:CE00125-05 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 11:09 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
19:34
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
19:34
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
19:34
REF
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
19:34
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 21 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW8 Lab Sample ID:CE00125-05 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 11:09 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 19:34 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 19:34 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
IA14039
EPA 8260D
01115121 19:34
REF
Dibromofluoromethane
47
1
50.0
93 %
67-129
IA14039
EPA 6260D
01115121 19:34
REF
Toluene-d8
48
1
50.0
97 %
59-134
IA14039
EPA 6260D
01115121 19:34
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:31
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Barium [7440-39-3]^
11.8
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:13
JDH
Beryllium [7440-41-7]^
0.375
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 10:13
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:13
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Copper[7440-50-8]^
1.98
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 10:13
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:31
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:13
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:15
RLF
Vanadium [7440-62-2]^
2.88
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:13
JDH
Zinc[7440-66-6]^
7.24
J
ug/L
1
4.40
10.0
lA18012
EPA 6010D
01/20/21 10:13
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 12:40
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.6
1
5.00
112 %
75-125
1A20026
EPA 8260D
01120121 12:40
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P2 Lab Sample ID:CE00125-06 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 15:05 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
18:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
18:57
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
18:57
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
18:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page
23 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P2 Lab Sample ID:CE00125-06 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 15:05 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 18:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 18:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
56
1
50.0
113 %
53-136
IA19023
EPA 8260D
01/19/21 18:57
REF
Dibromofluoromethane
48
1
50.0
97 %
67-129
IA19023
EPA 6260D
01119121 16:57
REF
Toluene-d8
51
1
50.0
103 %
59-134
IA19023
EPA 6260D
01119121 16:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:35
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Barium [7440-39-3]^
4.16
J
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:15
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18012
EPA 6010D
01/20/21 10:15
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:15
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:35
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:17
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:15
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 13:19
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.6
1
5.00
112 %
75-125
1A20026
EPA 8260D
01120121 13:19
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P4 Lab Sample ID:CE00125-07 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 12:15 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
20:04
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
20:04
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Ethylbenzene [500-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
20:04
REF
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
20:04
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 25 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P4 Lab Sample ID:CE00125-07 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 12:15 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 20:04 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 20:04 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA14039
EPA 8260D
01115121 20:04
REF
Dibromofluoromethane
47
1
50.0
95 %
67-129
IA14039
EPA 6260D
01115121 20:04
REF
Toluene-d8
46
1
50.0
91 %
59-134
IA14039
EPA 6260D
01115121 20:04
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
1A20026
EPA 8260D
01/20/21 13:45
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/yzed By Notes
Toluene-d8 4.7 1 5.00 93 % 75-125 1A20026 EPA 8260D 01120121 13:45 KKW
Description: 7401-P4 Lab Sample ID:CE00125-08 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 12:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P-9 L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 11:39
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Barium [7440-39-3]^
111
ug/L
1
1.10
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18012
EPA 6010D
01/20/21 11:07
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:07
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Copper[7440-50-B]^
15.6
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 11:39
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:18
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
Zinc[7440-66-6]^
4.45
J
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 11:07
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P5 Lab Sample ID:CE00125-09 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 17:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
19:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
19:27
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
19:27
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
19:27
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 27 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P5 Lab Sample ID:CE00125-09 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 17:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 19:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 19:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
56
1
50.0
111 %
53-136
IA19023
EPA 8260D
01119121 19:27
REF
Dibromofluoromethane
52
1
50.0
104 %
67-129
IA19023
EPA 6260D
01119121 19:27
REF
Toluene-d8
51
1
50.0
102 %
59-134
IA19023
EPA 6260D
01119121 19:27
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:43
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Barium [7440-39-3]^
12.9
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:20
JDH
Beryllium [7440-41-7]^
0.179
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 10:20
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:20
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Copper[7440-50-8]^
1.91
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 10:20
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:43
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
01/26/21 11:43
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:20
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 14:10
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.8
1
5.00
116 %
75-125
1A20026
EPA 8260D
01120121 14:10
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P6 Lab Sample ID:CE00125-10 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 12:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
19:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
19:57
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
19:57
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
19:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 29 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P6 Lab Sample ID:CE00125-10 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 12:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 19:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 19:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
59
1
50.0
119 %
53-136
IA19023
EPA 8260D
01/19/21 19:57
REF
Dibromofluoromethane
53
1
50.0
105 %
67-129
IA19023
EPA 6260D
01119121 19:57
REF
Toluene-d8
52
1
50.0
104 %
59-134
IA19023
EPA 6260D
01119121 19:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:48
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Barium [7440-39-3]^
58.8
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 11:10
JDH
Beryllium [7440-41-7]^
0.337
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 11:10
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:10
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:48
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:20
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:10
JDH
Zinc[7440-66-6]^
4.89
J
ug/L
1
4.40
10.0
lA18012
EPA 6010D
01/20/21 11:10
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 14:35
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.8
1
5.00
95 %
75-125
1A20026
EPA 8260D
01120121 1425
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 30 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P7 Lab Sample ID:CE00125-11 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 11:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
20:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
20:27
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
20:27
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
20:27
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page
31 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P7 Lab Sample ID:CE00125-11 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 11:25 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 20:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 20:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
57
1
50.0
114 %
53-136
IA19023
EPA 8260D
01119121 20:27
REF
Dibromofluoromethane
51
1
50.0
101 %
67-129
IA19023
EPA 6260D
01119121 20:27
REF
Toluene-d8
52
1
50.0
105 %
59-134
IA19023
EPA 6260D
01119121 20:27
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:52
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Barium [7440-39-3]^
216
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Beryllium [7440-41-7]^
0.464
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 10:25
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 10:25
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Cobalt[7440-48-4]^
2.38
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Copper[7440-50-8]^
3.12
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Nickel[7440-02-O]^
4.14
J
ug/L
1
2.20
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:52
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:21
RLF
Vanadium [7440-62-2]^
2.31
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 10:25
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 10:25
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 15:00
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
5.1
1
5.00
101 %
75-125
1A20026
EPA 8260D
01120121 15:00
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 32 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P9 Lab Sample ID:CE00125-12 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 11:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
20:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
20:57
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
20:57
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
20:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page
33 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P9 Lab Sample ID:CE00125-12 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 11:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 20:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 20:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
53
1
50.0
107 %
53-136
IA19023
EPA 8260D
01119121 20:57
REF
Dibromofluoromethane
46
1
50.0
92 %
67-129
IA19023
EPA 6260D
01119121 20:57
REF
Toluene-d8
49
1
50.0
97 %
59-134
IA19023
EPA 6260D
01119121 20:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 11:56
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Barium [7440-39-3]^
116
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 11:12
JDH
Beryllium [7440-41-7]^
0.761
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 11:12
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:12
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Cobalt[7440-48-4]^
2.66
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 11:12
JDH
Copper[7440-50-8]^
2.03
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 11:12
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Nickel[7440-02-O]^
3.10
J
ug/L
1
2.20
10.0
lA18012
EPA 6010D
01/20/21 11:12
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 11:56
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:23
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 11:12
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 15:26
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.5
1
5.00
110 %
75-125
1A20026
EPA 8260D
01120121 15:26
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P11R Lab Sample ID:CE00125-13 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:28 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21 21:27
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21 21:27
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Ethylbenzene [500-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21 21:27
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21 21:27
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 35 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PllR Lab Sample ID:CE00125-13 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:28 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 21:27 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 21:27 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
58
1
50.0
115 %
53-136
IA19023
EPA 8260D
01119121 21:27
REF
Dibromofluoromethane
49
1
50.0
97 %
67-129
IA19023
EPA 6260D
01119121 21:27
REF
Toluene-d8
50
1
50.0
100 %
59-134
IA19023
EPA 6260D
01119121 21:27
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:01
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Barium [7440-39-3]^
99.2
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Beryllium [7440-41-7]^
1.93
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 11:15
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:15
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Cobalt[7440-48-4]^
2.38
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Copper[7440-50-8]^
7.10
J
ug/L
1
1.60
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Nickel[7440-02-O]^
3.28
J
ug/L
1
2.20
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:01
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:15
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:24
RLF
Vanadium [7440-62-2]^
4.67
J
ug/L
1
1.40
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Zinc[7440-66-6]^
39.8
ug/L
1
4.40
10.0
lA18012
EPA 6010D
01/20/21 11:15
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 15:51
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.5
1
5.00
110 %
75-125
1A20026
EPA 8260D
01120121 15:51
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 36 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CE00125-14 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21 21:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21 21:57
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21 21:57
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21 21:57
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 37 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CE00125-14 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 21:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 21:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
55
1
50.0
110 %
53-136
IA19023
EPA 8260D
01119121 21:57
REF
Dibromofluoromethane
50
1
50.0
101 %
67-129
IA19023
EPA 6260D
01119121 21:57
REF
Toluene-d8
50
1
50.0
100 %
59-134
IA19023
EPA 6260D
01119121 21:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:35
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Barium [7440-39-3]^
34.9
ug/L
1
1.10
10.0
lA18012
EPA 6010D
01/20/21 11:22
JDH
Beryllium [7440-41-7]^
0.553
J
ug/L
1
0.160
1.00
lA18012
EPA 6010D
01/20/21 11:22
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18012
EPA 6010D
01/20/21 11:22
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:35
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
01/26/21 12:35
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18012
EPA 6010D
01/20/21 11:22
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 16:16
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.0
1
5.00
99 %
75-125
1A20026
EPA 8260D
01120121 16:16
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 38 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13 Lab Sample ID:CE00125-15 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 14:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
IA20009
EPA 8260D
01/20/21
16:06
RKY
QL-02,
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
1A20009
EPA 8260D
01/20/21
16:06
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
m,p-Xylenes [108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A20009
EPA 8260D
01/20/21
16:06
RKY
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 39 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13 Lab Sample ID:CE00125-15 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 14:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A20009
EPA 8260D
01/20/21 16:06
RKY QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A20009
EPA 8260D
01/20/21 16:06
RKY
Xylenes (Total) [1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A20009
EPA 8260D
01/20/21 16:06
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
IA20009
EPA 8260D
01120121 16:06
RKY
Dibromofluoromethane
52
1
50.0
105 %
67-129
IA20009
EPA 8260D
01120121 16:06
RKY
Toluene-d8
61
1
50.0
122 %
59-134
IA20009
EPA 6260D
01120121 16:06
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:39
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Barium [7440-39-3]^
54.2
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:13
JDH
Beryllium [7440-41-7]^
0.204
J
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 11:13
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:13
JDH
Chromium [7440-47-3]^
1.73
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:13
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Copper[7440-50-8]^
2.16
J
ug/L
1
1.60
10.0
lA18015
EPA 6010D
01/21/21 11:13
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:39
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:29
RLF
Vanadium [7440-62-2]^
1.69
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:13
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:13
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 16:41
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
1A20026
EPA 8260D
01120121 16:41
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 40 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P131) Lab Sample ID:CE00125-16 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 14:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19023
EPA 8260D
01/19/21
22:57
REF
QL-02
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19023
EPA 8260D
01/19/21
22:57
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19023
EPA 8260D
01/19/21
22:57
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19023
EPA 8260D
01/19/21
22:57
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 41 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13D Lab Sample ID:CE00125-16 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 14:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19023 EPA 8260D 01/19/21 22:57 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19023 EPA 8260D 01/19/21 22:57 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
52
1
50.0
104 %
53-136
IA19023
EPA 8260D
01119121 22:57
REF
Dibromofluoromethane
45
1
50.0
90 %
67-129
IA19023
EPA 6260D
01119121 22:57
REF
Toluene-d8
47
1
50.0
94 %
59-134
IA19023
EPA 6260D
01119121 22:57
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:43
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Barium [7440-39-3]^
100
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:35
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:35
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:35
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:43
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:31
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:35
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.5
J
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 17:07
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.6
1
5.00
92 %
75-125
1A20026
EPA 8260D
01120121 17:07
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 42 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P1611 Lab Sample ID:CE00125-17 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:13 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Acetone [67-64-1]A
12
J
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
20:34
REF
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
20:34
REF
Benzene [71-43-2]A
0.86
J
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
20:34
REF
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
20:34
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 43 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CE00125-17 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:13 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 20:34 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 20:34 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
53
1
50.0
107 %
53-136
IA14039
EPA 8260D
01115121 20:34
REF
Dibromofluoromethane
48
1
50.0
95 %
67-129
IA14039
EPA 6260D
01115121 20:34
REF
Toluene-d8
49
1
50.0
98 %
59-134
IA14039
EPA 6260D
01115121 20:34
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
78
D
ug/L
2
1.6 4.0
1A20026
EPA 8260D
01/20/21 19:13
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/yzed By Notes
Toluene-d8 5.4 1 5.00 108 % 75-125 1A20026 EPA 8260D 01120121 19:13 KKW
Description: 7401-P16R Lab Sample ID:CE00125-18 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:07 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P-9 L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 12:47
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Barium [7440-39-3]^
1100
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:37
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:37
]DH
Chromium [7440-47-3]^
2.88
J
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Nickel[7440-02-O]^
16.6
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 12:47
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:32
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:37
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 44 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CE00125-19 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:35 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Acetone [67-64-1]A
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21 21:04
REF
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21 21:04
REF
Benzene [71-43-2]A
0.43
J
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Chlorobenzene [108-90-7]A
4.3
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21 21:04
REF
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21 21:04
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 45 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CE00125-19 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:35 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 21:04 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 21:04 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
52
1
50.0
103 %
53-136
IA14039
EPA 8260D
01115121 21:04
REF
Dibromofluoromethane
45
1
50.0
91 %
67-129
IA14039
EPA 6260D
01115121 21:04
REF
Toluene-d8
48
1
50.0
96 %
59-134
IA14039
EPA 6260D
01115121 21:04
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020B
01/26/21 12:52
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Barium [7440-39-3]^
147
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:40
JDH
Beryllium [7440-41-7]^
1.43
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 11:40
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:40
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Copper[7440-50-8]^
1.89
J
ug/L
1
1.60
10.0
lA18015
EPA 6010D
01/21/21 11:40
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Nickel[7440-02-O]^
2.79
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 11:40
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020B
01/26/21 12:52
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020B
02/04/21 15:34
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:40
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
5.0
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 17:32
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.0
1
5.00
101 %
75-125
1A20026
EPA 8260D
01120121 1722
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 46 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CE00125-20 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 16:11 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
U
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
U
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
U
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,1-Dichloroethane [75-34-3]A
4.2
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
1,4-Dichlorobenzene [306-46-7]^
5.1
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
2-Butanone [78-93-3]^
1.3
U
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
2-Hexanone [591-78-6]^
0.88
U
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Acetone [67-64-1]^
10
U
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21 21:34
REF
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21 21:34
REF
Benzene [71-43-2]A
4.0
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Bromochloromethane [74-97-5]^
0.48
U
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Bromomethane [74-83-9]^
0.14
U
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
U
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Carbon tetrachloride [56-23-5]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Chlorobenzene [308-90-7]A
7.0
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Chloroethane [75-00-3]^
0.23
U
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Chloromethane [74-87-3]^
0.13
U
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
cis-1,2-Dichloroethene [156-59-2]A
2.7
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
U
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Dibromochloromethane [124-48-1]^
0.17
U
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Dibromomethane [74-95-3]^
0.27
U
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Ethylbenzene [100-41-4]A
1.8
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
m,p-Xylenes[108-38-3/306-42-3]A
0.42
1
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
o-Xylene [95-47-6]A
0.56
1
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21 21:34
REF
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21 21:34
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 47 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CE00125-20 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 16:11 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.57 1 ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 21:34 REF
Xylenes(Total)[1330-20-7]^ 0.98 1 ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 21:34 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
51
1
50.0
101 %
53-136
IA14039
EPA 8260D
01115121 21:34
REF
Dibromofluoromethane
46
1
50.0
92 %
67-129
IA14039
EPA 6260D
01115121 21:34
REF
Toluene-d8
49
1
50.0
97 %
59-134
IA14039
EPA 6260D
01115121 21:34
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
160
D
ug/L
2.5
2.0 5.0
1A20026
EPA 8260D
01/20/21 19:38
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/yzed By Notes
Toluene-d8 5.7 1 5.00 113 % 75-125 1A20026 EPA 8260D 01120121 1928 KKW
Description: 7401-P19 Lab Sample ID:CE00125-21 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P-9 L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 12:56
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Barium [7440-39-3]^
1870
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Beryllium [7440-41-7]^
15.3
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:42
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:42
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Cobalt[7440-48-4]^
19.3
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Copper[7440-50-8]^
1.72
J
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Lead [7439-92-1]^
6.07
J
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Nickel[7440-02-O]^
29.4
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Selenium [7782-49-2]^
2.08
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 12:56
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:35
RLF
Vanadium [7440-62-2]^
1.46
J
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:42
]DH
Zinc[7440-66-6]^
120
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:42
3DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 48 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CE00125-22 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 16:35 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
22:04
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
22:04
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
22:04
REF
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
22:04
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 49 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CE00125-22 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 16:35 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 22:04 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 22:04 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
52
1
50.0
105 %
53-136
IA14039
EPA 8260D
01115121 22:04
REF
Dibromofluoromethane
48
1
50.0
96 %
67-129
IA14039
EPA 6260D
01115121 22:04
REF
Toluene-d8
48
1
50.0
96 %
59-134
IA14039
EPA 6260D
01115121 22:04
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
2.1
ug/L
1
0.80 2.0
1A20026
EPA 8260D
01/20/21 17:57
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/yzed By Notes
Toluene-d8 6.0 1 5.00 119 % 75-125 1A20026 EPA 8260D 01120121 17:57 KKW
Description: 7401-P20R Lab Sample ID:CE00125-23 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:18 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P-9 L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18021
EPA 6020E
01/26/21 13:00
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Barium [7440-39-3]^
51.4
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Beryllium [7440-41-7]^
1.66
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:45
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:45
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18021
EPA 6020E
01/26/21 13:00
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18021
EPA 6020E
02/04/21 15:37
RLF
Vanadium [7440-62-2]^
2.44
J
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
Zinc[7440-66-6]^
12.1
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:45
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 50 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P201) Lab Sample ID:CE00125-24 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:20 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dichloroethane [507-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
IA20009
EPA 8260D
01/20/21
19:20
RKY
QL-02,
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
1A20009
EPA 8260D
01/20/21
19:20
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Ethylbenzene [500-41-4]A
0.13
U
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
m,p-Xylenes [108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A20009
EPA 8260D
01/20/21
19:20
RKY
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 51 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20D Lab Sample ID:CE00125-24 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 16:20 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A20009
EPA 8260D
01/20/21 19:20
RKY QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A20009
EPA 8260D
01/20/21 19:20
RKY
Xylenes (Total) [1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A20009
EPA 8260D
01/20/21 19:20
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
51
1
50.0
103 %
53-136
IA20009
EPA 8260D
01120121 19:20
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA20009
EPA 8260D
01120121 19:20
RKY
Toluene-d8
63
1
50.0
125 %
59-134
IA20009
EPA 6260D
01120121 19:20
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 08:29
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Barium [7440-39-3]^
112
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Beryllium [7440-41-7]^
8.87
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 11:47
JDH
Cadmium [7440-43-9]^
0.756
J
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:47
JDH
Chromium [7440-47-3]^
12.9
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Lead [7439-92-1]^
5.43
J
ug/L
1
3.10
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Nickel[7440-02-0]^
4.31
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 08:33
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Thallium [7440-28-0]^
1.10
UD
ug/L
10
1.10
10.0
1A18022
EPA 6020B
01/26/21 08:56
RLF
QI-03
Vanadium [7440-62-2]^
12.6
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:47
JDH
Zinc[7440-66-6]^
20.1
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:47
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 18:23
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
108 %
75-125
1A20026
EPA 8260D
01120121 18:23
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 52 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P21 Lab Sample ID:CE00125-25 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dichloroethane [507-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
IA20009
EPA 8260D
01/20/21
19:48
RKY
QL-02,
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
1A20009
EPA 8260D
01/20/21
19:48
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Ethylbenzene [500-41-4]A
0.13
U
ug/L
1
0.13
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
m,p-Xylenes [108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A20009
EPA 8260D
01/20/21
19:48
RKY
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 53 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P21 Lab Sample ID:CE00125-25 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2109:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A20009
EPA 8260D
01/20/21 19:48
RKY QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A20009
EPA 8260D
01/20/21 19:48
RKY
Xylenes (Total) [1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A20009
EPA 8260D
01/20/21 19:48
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
49
1
50.0
98 %
53-136
IA20009
EPA 8260D
01/20/21 19:48
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA20009
EPA 8260D
01120121 19:48
RKY
Toluene-d8
63
1
50.0
125 %
59-134
IA20009
EPA 6260D
01120121 19:48
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:04
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Barium [7440-39-3]A
58.0
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:49
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:49
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:49
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Nickel[7440-02-O]^
2.53
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 11:49
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 09:04
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:39
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:49
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20026
EPA 8260D
01/20/21 18:48
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.3
1
5.00
107 %
75-125
1A20026
EPA 8260D
01120121 18:48
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 54 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P23 Lab Sample ID:CE00125-26 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 14:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA14039
EPA 8260D
01/15/21
22:34
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA14039
EPA 8260D
01/15/21
22:34
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Ethylbenzene [500-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA14039
EPA 8260D
01/15/21
22:34
REF
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA14039
EPA 8260D
01/15/21
22:34
REF
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 55 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P23 Lab Sample ID:CE00125-26 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 14:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A14039 EPA 8260D 01/15/21 22:34 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A14039 EPA 8260D 01/15/21 22:34 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
IA14039
EPA 8260D
01115121 22:34
REF
Dibromofluoromethane
49
1
50.0
98 %
67-129
IA14039
EPA 6260D
01115121 22:34
REF
Toluene-d8
49
1
50.0
98 %
59-134
IA14039
EPA 6260D
01115121 22:34
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL P L
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
1A20035
EPA 8260D
01/21/21 00:15
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/yzed By Notes
Toluene-d8 5.7 1 5.00 113 % 75-125 1A20035 EPA 8260D 01121121 00:15 KKW
Description: 7401-P23 Lab Sample ID:CE00125-27 Received: 01/15/21 10:00
Matrix: Ground Water Sampled: 01/14/2108:45 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
E-Q L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020E
01/26/21 09:09
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Barium [7440-39-3]^
19.6
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:52
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:52
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020E
01/26/21 09:09
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020E
01/26/21 09:09
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
Zinc[7440-66-6]^
7.76
J
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:52
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 56 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CE00125-28 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:45 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 18:30
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Benzene [71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Ethylbenzene [500-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 18:30
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 57 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CE00125-28 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/13/21 15:45 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 18:30 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 18:30 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
49
1
50.0
97 %
53-136
IA19015
EPA 8260D
01119121 18:30
REF
Dibromofluoromethane
53
1
50.0
105 %
67-129
IA19015
EPA 6260D
01119121 16 30
REF
Toluene-d8
61
1
50.0
123 %
59-134
IA19015
EPA 6260D
01119121 16 30
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
1A20035
EPA 8260D
01/21/21 00:40
KKW
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/yzed By Notes
Toluene-d8 4.4 1 5.00 87 % 75-125 1A20035 EPA 8260D 01121121 00:40 KKW
Description: 7401-P28 Lab Sample ID:CE00125-29 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:05 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
E-Q L
Batch
Method
Analyzed
By Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020E
01/26/21 09:39
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Barium [7440-39-3]^
38.4
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Beryllium [7440-41-7]^
0.741
J
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 11:54
]DH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:54
]DH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Copper[7440-50-8]^
2.49
J
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Nickel[7440-02-O]^
3.16
J
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020E
01/26/21 09:39
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020E
02/04/21 15:40
RLF
Vanadium [7440-62-2]^
1.53
J
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
Zinc[7440-66-6]^
14.0
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 11:54
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 58 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CE00125-30 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 13:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
1,4-Dichlorobenzene [306-46-7]^
0.89
J
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 18:58
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Benzene [71-43-2]A
1.6
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Chlorobenzene [108-90-7]A
5.1
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Ethylbenzene [100-41-4]A
0.48
J
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 18:58
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 59 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CE00125-30 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 13:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 18:58 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 18:58 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA19015
EPA 8260D
01119121 18:58
REF
Dibromofluoromethane
51
1
50.0
101 %
67-129
IA19015
EPA 6260D
01119121 16:58
REF
Toluene-d8
62
1
50.0
123 %
59-134
IA19015
EPA 6260D
01119121 16:58
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:43
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 11:56
JDH
Barium [7440-39-3]^
1290
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Beryllium [7440-41-7]^
0.980
J
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 11:56
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 11:56
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 11:56
JDH
Cobalt[7440-48-4]^
4.66
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 11:56
JDH
Lead [7439-92-1]^
18.0
ug/L
1
3.10
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Nickel[7440-02-O]^
7.50
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Selenium [7782-49-2]^
2.54
ug/L
2
1.82
2.00
lAlS022
EPA 6020B
01/26/21 09:43
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 11:56
JDH
Thallium [7440-28-0]^
0.252
J
ug/L
2
0.220
2.00
lAlS022
EPA 6020B
02/04/21 15:42
RLF
Vanadium [7440-62-2]^
36.1
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Zinc[7440-66-6]^
5.63
J
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 11:56
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
140
D
ug/L
5
4.0
10
1A22042
EPA 8260D
01/22/21 18:06
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
109 %
75-125
1A22042
EPA 8260D
01122121 18:06
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 60 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CE00125-31 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/14/21 17:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 19:25
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Benzene [71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 19:25
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 61 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CE00125-31 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/14/21 17:40 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 19:25 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 19:25 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA19015
EPA 8260D
01/19/21 19:25
REF
Dibromofluoromethane
52
1
50.0
103 %
67-129
IA19015
EPA 6260D
01119121 19:25
REF
Toluene-c48
61
1
50.0
121 %
59-134
IA19015
EPA 6260D
01119121 19:25
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:48
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:42
JDH
Barium [7440-39-3]^
23.9
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Beryllium [7440-41-7]^
0.212
J
ug/L
1
0.160
1.00
lA18015
EPA 6010D
01/21/21 12:42
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:42
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:42
JDH
Cobalt[7440-48-4]^
8.02
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:42
JDH
Lead [7439-92-1]^
3.54
J
ug/L
1
3.10
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Nickel[7440-02-O]^
3.41
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 09:48
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:42
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:43
RLF
Vanadium [7440-62-2]^
2.15
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Zinc[7440-66-6]^
15.3
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 12:42
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20035
EPA 8260D
01/21/21 01:06
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
107 %
75-125
1A20035
EPA 8260D
01121121 01:06
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 62 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CE00125-32 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/14/21 15:37 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 19:53
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Benzene [71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 19:53
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 63 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CE00125-32 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/14/21 15:37 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 19:53 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 19:53 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
50
1
50.0
101 %
53-136
IA19015
EPA 8260D
01119121 19:53
REF
Dibromofluoromethane
52
1
50.0
104 %
67-129
IA19015
EPA 6260D
01119121 19:53
REF
Toluene-c48
62
1
50.0
124 %
59-134
IA19015
EPA 6260D
01119121 19:53
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:52
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Barium [7440-39-3]^
40.3
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:44
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:44
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:44
JDH
Chromium [7440-47-3]^
1.44
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:44
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 09:52
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:48
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:44
JDH
Zinc[7440-66-6]^
18.8
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 12:44
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20035
EPA 8260D
01/21/21 01:31
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
1A20035
EPA 8260D
01121121 01:31
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 64 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW4 Lab Sample ID:CE00125-33 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/13/21 17:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA18028
EPA 8260D
01/18/21
20:51
REF
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
IA18028
EPA 8260D
01/18/21
20:51
REF
QL-02,
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
1A18028
EPA 8260D
01/18/21
20:51
REF
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
1A18028
EPA 8260D
01/18/21
20:51
REF
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Ethylbenzene [500-41-4]A
0.13
u
ug/L
1
0.13
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
1A18028
EPA 8260D
01/18/21
20:51
REF
m,p-Xylenes [108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A18028
EPA 8260D
01/18/21
20:51
REF
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 65 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW4 Lab Sample ID:CE00125-33 Received: 01/15/21 10:00
Matrix: Surface Water Sampled:01/13/21 17:10 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A18028
EPA 8260D
01/18/21 20:51
REF QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A18028
EPA 8260D
01/18/21 20:51
REF
Xylenes(Total)[1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A18028
EPA 8260D
01/18/21 20:51
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
48
1
50.0
96 %
53-136
IA16028
EPA 8260D
01116121 20:51
REF
Dibromofluoromethane
53
1
50.0
107 %
67-129
IA16028
EPA 8260D
01118121 20:51
REF
Toluene-d8
61
1
50.0
121 %
59-134
IA16028
EPA 6260D
01118121 20:51
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 09:56
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Barium [7440-39-3]A
40.0
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:46
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:46
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:46
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 09:56
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:50
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Zinc[7440-66-6]^
5.97
J
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 12:46
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]A
3.5
ug/L
1
0.80
2.0
1A20035
EPA 8260D
01/21/21 01:56
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.3
1
5.00
105 %
75-125
1A20035
EPA 8260D
01121121 01:56
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 66 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ1 Lab Sample ID:CE00125-34 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 20:20
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 20:20
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 67 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ1 Lab Sample ID:CE00125-34 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:55 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 20:20 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 20:20 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
48
1
50.0
96 %
53-136
IA19015
EPA 8260D
01119121 20:20
REF
Dibromofluoromethane
51
1
50.0
102 %
67-129
IA19015
EPA 6260D
01119121 20:20
REF
Toluene-d8
61
1
50.0
122 %
59-134
IA19015
EPA 6260D
01119121 20:20
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 10:01
RLF
Arsenic[7440-38-2]^
100
ug/L
1
7.60
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Barium [7440-39-3]^
101
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:48
JDH
Cadmium [7440-43-9]^
1.72
ug/L
1
0.360
1.00
lA18015
EPA 6010D
01/21/21 12:48
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:48
JDH
Cobalt[7440-48-4]^
2.21
J
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Copper[7440-50-8]^
3.41
J
ug/L
1
1.60
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Lead [7439-92-1]^
8.46
J
ug/L
1
3.10
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Nickel[7440-02-O]^
3.31
J
ug/L
1
2.20
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 10:01
RLF
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:48
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:51
RLF
Vanadium [7440-62-2]^
12.4
ug/L
1
1.40
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Zinc[7440-66-6]^
26.4
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 12:48
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
2.1
ug/L
1
0.80
2.0
1A22042
EPA 8260D
01/22/21 17:40
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
108 %
75-125
1A22042
EPA 8260D
01122121 17:40
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 68 of 99

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ2 Lab Sample ID:CE00125-35 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:30 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Acetone [67-64-1]^
10
u
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 20:47
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 20:47
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 69 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ2 Lab Sample ID:CE00125-35 Received: 01/15/21 10:00
Matrix: Ground Water Sampled:01/14/21 10:30 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 20:47 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 20:47 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
49
1
50.0
97 %
53-136
IA19015
EPA 8260D
01119121 20:47
REF
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA19015
EPA 6260D
01119121 20:47
REF
Toluene-d8
62
1
50.0
124 %
59-134
IA19015
EPA 6260D
01119121 20:47
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 10:05
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Barium [7440-39-3]A
190
ug/L
1
1.10
10.0
lA18015
EPA 6010D
01/21/21 12:51
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:51
JDH
Cadmium [7440-43-9]A
0.360
J
ug/L
1
0.360
1.00
lA18015
EPA 6010D
01/21/21 12:51
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 10:05
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:53
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:51
JDH
Zinc[7440-66-6]A
18.3
ug/L
1
4.40
10.0
lA18015
EPA 6010D
01/21/21 12:51
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]A
3.6
ug/L
1
0.80
2.0
1A20035
EPA 8260D
01/21/21 02:21
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
104 %
75-125
1A20035
EPA 8260D
01121121 02:21
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 70 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CE00125-36 Received: 01/15/21 10:00
Matrix: Water Sampled:01/13/21 16:57 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
U
ug/L
1
0.17
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
U
ug/L
1
0.12
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
U
ug/L
1
0.28
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
U
ug/L
1
0.14
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA18028
EPA 8260D
01/18/21
16:17
REF
2-Butanone [78-93-3]^
1.3
U
ug/L
1
1.3
5.0
IA18028
EPA 8260D
01/18/21
16:17
REF
QL-02,
QV-01
2-Hexanone [591-78-6]^
1.9
1
ug/L
1
0.88
5.0
IA18028
EPA 8260D
01/18/21
16:17
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
Acetone [67-64-1]^
10
U
ug/L
1
10
20
1A18028
EPA 8260D
01/18/21
16:17
REF
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Bromomethane [74-83-9]^
0.14
U
ug/L
1
0.14
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Carbon disulfide [75-15-0]^
53
ug/L
1
1.5
5.0
IA18028
EPA 8260D
01/18/21
16:17
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Ethylbenzene [100-41-4]^
0.13
u
ug/L
1
0.13
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
1A18028
EPA 8260D
01/18/21
16:17
REF
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
1A18028
EPA 8260D
01/18/21
16:17
REF
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 71 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CE00125-36 Received: 01/15/21 10:00
Matrix: Water Sampled:01/13/21 16:57 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Vinyl acetate [108-05-4]^ 0.95
U
ug/L
1
0.95
5.0
1A18028
EPA 8260D
01/18/21 16:17
REF QV-01
Vinyl chloride [75-01-4]^ 0.32
U
ug/L
1
0.32
1.0
1A18028
EPA 8260D
01/18/21 16:17
REF
Xylenes(Total)[1330-20-7]^ 0.45
U
ug/L
1
0.45
3.0
1A18028
EPA 8260D
01/18/21 16:17
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA16028
EPA 8260D
01116121 16:17
REF
Dibromofluoromethane
54
1
50.0
108 %
67-129
IA16028
EPA 8260D
01118121 16:17
REF
Toluene-d8
61
1
50.0
122 %
59-134
IA16028
EPA 6260D
01118121 16:17
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 10:09
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Barium [7440-39-3]^
1.10
U
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:53
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:53
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 10:09
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
02/04/21 15:54
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Zinc[7440-66-6]^
114
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 12:53
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A20035
EPA 8260D
01/21/21 02:47
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
104 %
75-125
1A20035
EPA 8260D
01121121 02:47
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 72 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CE00125-37 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/14/2109:30 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Acetone [67-64-1]A
14
J
ug/L
1
10
20
IA19015
EPA 8260D
01/19/21 17:08
REF
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Benzene [71-43-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Chlorobenzene [108-90-7]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Ethylbenzene [100-41-4]A
0.13
u
ug/L
1
0.13
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.17
u
ug/L
1
0.17
2.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA19015
EPA 8260D
01/19/21 17:08
REF
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 73 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CE00125-37 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/14/2109:30 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1A19015 EPA 8260D 01/19/21 17:08 REF
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1A19015 EPA 8260D 01/19/21 17:08 REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
IA19015
EPA 8260D
01/19/21 17:08
REF
Dibromofluoromethane
52
1
50.0
104 %
67-129
IA19015
EPA 6260D
01119121 17:08
REF
Toluene-d8
61
1
50.0
122 %
59-134
IA19015
EPA 6260D
01119121 17:08
REF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
1A18022
EPA 6020B
01/26/21 10:13
RLF
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Barium [7440-39-3]^
1.10
U
ug/L
1
1.10
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
1A18015
EPA 6010D
01/21/21 12:56
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
1A18015
EPA 6010D
01/21/21 12:56
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
1A18022
EPA 6020B
01/26/21 10:13
RLF
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
1A18022
EPA 6020B
01/26/21 10:13
RLF
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
1A18015
EPA 6010D
01/21/21 12:56
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
1A22042
EPA 8260D
01/22/21 11:21
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.0
1
5.00
101 %
75-125
1A22042
EPA 8260D
01122121 11:21
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 74 of 99

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CE00125-38 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/13/2100:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dichloroethane [507-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Acetone [67-64-1]A
67
ug/L
1
10
20
IA25038
EPA 8260D
01/25/21 19:44
RKY
0-01
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
IA25038
EPA 8260D
01/25/21 19:44
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Ethylbenzene[500-41-4]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Iodomethane[74-88-4]A
1.7
U
ug/L
1
1.7
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA25038
EPA 8260D
01/25/21 19:44
RKY
QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 75 of 99

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www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CE00125-38 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/13/2100:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flaa
Units
DF
MDL P(—L
Batch
Method
Analyzed
By Notes
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32 1.0
1A25038
EPA 8260D
01/25/21 19:44
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45 3.0
1A25038
EPA 8260D
01/25/21 19:44
RKY
Surrogates
Results
DF
Spike LN
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
IA25038
EPA 8260D
01125121 19:44
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA25038
EPA 6260D
01125121 19:44
RKY
Toluene-d8
62
1
50.0
124 %
59-134
IA25038
EPA 6260D
01125121 19:44
RKY
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 76 of 99

0Nk"q09
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ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CE00125-39 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/13/2100:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Acetone [67-64-1]A
31
ug/L
1
10
20
IA25038
EPA 8260D
01/25/21
20:12
RKY
0-01
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
IA25038
EPA 8260D
01/25/21
20:12
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Iodomethane[74-88-4]A
1.7
U
ug/L
1
1.7
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
IA25038
EPA 8260D
01/25/21
20:12
RKY
QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only
be reproduced in full.
Page 77 of 99

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CE00125-39 Received: 01/15/21 10:00
Matrix: Water Sampled: 01/13/2100:00 Work Order: CE00125
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flaa
Units
DF
MDL PDL
Batch
Method
Analyzed
By Notes
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32 1.0
1A25038
EPA 8260D
01/25/21 20:12
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45 3.0
1A25038
EPA 8260D
01/25/21 20:12
RKY
Surrogates
Results
DF
Spike LN
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
50
1
50.0
99 %
53-136
IA25038
EPA 8260D
01125121 20:12
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
IA25038
EPA 8260D
01125121 20:12
RKY
Toluene-d8
61
1
50.0
122 %
59-134
IA25038
EPA 8260D
01125121 20:12
RKY
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 78 of 99

(� �Eo
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A14039 - EPA 5030E MS
Blank (3A34039-BLK1) Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 14:32
Analvte
Result
Flaq
POL
Units
1, 1, 1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 79 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A14039 - EPA 5030E MS - Continued
Blank (SA34039-BLK1) Continued Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 14:32
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene
54
ug/L
50.0 107 53-136
Dibromofluoromethane
49
u91L
50.0 98 67-129
Toluene-d8
49
ug/L
50.0 98 59-134
LCS (1A14039-BS1)
Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 12:32
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
107
75-133
Benzene
18
1.0
ug/L
20.0
91
80-134
Chlorobenzene
18
1.0
ug/L
20.0
92
80-120
Toluene
19
1.0
ug/L
20.0
93
71-120
Trichloroethene
19
1.0
ug/L
20.0
93
74-120
4-Bromofluorobenzene
55
ug/L
50.0
109
53-136
Dibromofluoromethane
50
u91L
50.0
99
67-129
Toluene-d8
52
u91L
50.0
105
59-134
Matrix Spike (3A14039-MS1)
Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 13:02
Source: CE00684-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
24
1.0
ug/L
20.0
0.21 U
118
75-133
Benzene
18
1.0
ug/L
20.0
0.15 U
92
80-134
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
92
80-120
Toluene
18
1.0
ug/L
20.0
0.14 U
92
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
97
74-120
4-Bromofluorobenzene
52
u91L
50.0
104
53-136
Dibromofluoromethane
48
u91L
50.0
97
67-129
Toluene-d8
49
u91L
50.0
98
59-134
Matrix Spike Dup (3A14039-MSD1)
Prepared: 01/14/2021 15:24 Analyzed: 01/15/2021 13:32
Source: CE00684-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
26
1.0
ug/L
20.0
0.21 U
128
75-133
8
20
Benzene
21
1.0
ug/L
20.0
0.15 U
103
80-134
11
17
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
103
80-120
11
16
Toluene
20
1.0
ug/L
20.0
0.14 U
102
71-120
10
17
Trichloroethene
23
1.0
ug/L
20.0
0.15 U
113
74-120
15
22
4-Bromofluorobenzene 57 u91L 50.0 115 53-136
Dibromofluoromethane 53 u91L 50.0 106 67-129
Toluene-d8 57 u91L 50.0 113 59-134
Batch IA18028 - EPA 5030E MS
Blank (3A38028-BLK3) Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 15:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L
1,1,1-Trichloroethane 0.12 U 1.0 ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 80 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A18028 - EPA 5030E MS - Continued
Blank (SA38028-BLK1) Continued Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 15:50
Analvte
Result
Flaq
POL
Units
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 50 u91L 50.0 100 53-136
Dibromofluoromethane 53 u91L 50.0 105 67-129
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 81 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A18028 - EPA 5030E MS - Continued
Blank (SA38028-BLK1) Continued Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 15:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 62 u91L 50.0 124 59-134
LCS (1A18028-BS1) Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 13:59
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
114
75-133
Benzene
22
1.0
ug/L
20.0
110
80-134
Chlorobenzene
22
1.0
ug/L
20.0
108
80-120
Toluene
22
1.0
ug/L
20.0
109
71-120
Trichloroethene
21
1.0
ug/L
20.0
107
74-120
4-Bromofluorobenzene
49
u91L
50.0
99
53-136
Dibromofluoromethane
51
u91L
50.0
103
67-129
Toluene-d8
62
u91L
50.0
123
59-134
Matrix Spike (3A18028-MS1)
Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 14:27
Source: CE00929-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
114
75-133
Benzene
22
1.0
ug/L
20.0
0.15 U
109
80-134
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
108
80-120
Toluene
22
1.0
ug/L
20.0
0.14 U
109
71-120
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
105
74-120
4-Bromofluorobenzene
51
u91L
50.0
101
53-136
Dibromofluoromethane
52
u91L
50.0
104
67-129
Toluene-d8
62
u91L
50.0
125
59-134
Matrix Spike Dup (3A18028-MSD1)
Prepared: 01/18/2021 11:52 Analyzed: 01/18/2021 14:55
Source: CE00929-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
22
1.0
ug/L
20.0
0.21 U
112
75-133
2
20
Benzene
21
1.0
ug/L
20.0
0.15 U
104
80-134
5
17
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
106
80-120
2
16
Toluene
21
1.0
ug/L
20.0
0.14 U
104
71-120
5
17
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
100
74-120
4
22
4-Bromofluorobenzene 51 u91L 50.0 102 53-136
Dibromofluoromethane 53 u91L 50.0 106 67-129
Toluene-& 62 u91L 50.0 125 59-134
Batch IA19015 - EPA 5030E MS
Blank (lA19015-BLK3) Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 15:45
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
FINAL
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full. Page 82 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A19015 - EPA 5030E MS - Continued
Blank (SA3901S-BLK1) Continued Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 15:45
Analvte
Result
Flaq
POL
Units
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 51 u91L 50.0 102 53-136
Dibromofluoromethane 52 u91L 50.0 104 67-129
Toluene-d8 62 u91L 50.0 124 59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 83 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A19015 - EPA 5030E MS - Continued
LCS (1A19015-BS1) Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 13:55
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
24
1.0
ug/L
20.0
122
75-133
Benzene
23
1.0
ug/L
20.0
114
80-134
Chlorobenzene
23
1.0
ug/L
20.0
114
80-120
Toluene
23
1.0
ug/L
20.0
113
71-120
Trichloroethene
22
1.0
ug/L
20.0
111
74-120
4-Bromofluorobenzene
50
u91L
50.0
100
53-136
Dibromofluoromethane
51
u91L
50.0
102
67-129
Toluene-d8
61
u91L
50.0
121
59-134
Matrix Spike (3A19015-MS1)
Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 14:22
Source: CE00929-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
117
75-133
Benzene
22
1.0
ug/L
20.0
0.15 U
111
80-134
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
111
80-120
Toluene
22
1.0
ug/L
20.0
0.14 U
110
71-120
Trichloroethene
22
1.0
ug/L
20.0
0.15 U
109
74-120
4-Bromofluorobenzene
51
u91L
50.0
102
53-136
Dibromofluoromethane
51
u91L
50.0
103
67-129
Toluene-d8
62
u91L
50.0
124
59-134
Matrix Spike Dup (lA19015-MSD1)
Prepared: 01/19/2021 11:22 Analyzed: 01/19/2021 14:50
Source: CE00929-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
117
75-133
0.4
20
Benzene
22
1.0
ug/L
20.0
0.15 U
109
80-134
1
17
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
110
80-120
0.7
16
Toluene
22
1.0
ug/L
20.0
0.14 U
111
71-120
0.6
17
Trichloroethene
22
1.0
ug/L
20.0
0.15 U
108
74-120
2
22
4-Bromofluorobenzene
49
u91L
50.0
99
53-136
Dibromofluoromethane
50
u91L
50.0
101
67-129
Toluene-d8
60
u91L
50.0
121
59-134
Batch IA19023 - EPA 5030B MS
Blank (3A39023-131-K3) Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 16:27
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
FINAL
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full. Page 84 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A19023 - EPA 5030E MS - Continued
Blank (SA39023-BLK1) Continued Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 16:27
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit Notes
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
4-Bromofluorobenzene
57
ug/L
50.0
114
53-136
Dibromofluoromethane
51
ug/L
50.0
102
67-129
Toluene-d8
53
u91L
50.0
106
59-134
LCS (1A19023-BSI)
Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 14:13
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit Notes
1,1-Dichloroethene
22
1.0
ug/L
20.0
111
75-133
Benzene
18
1.0
ug/L
20.0
90
80-134
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be reproduced in
full.
Page 85 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A19023 - EPA 5030E MS - Continued
LCS (1A19023-BS1) Continued Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 14:13
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Chlorobenzene
18
1.0
ug/L
20.0 92 80-120
Toluene
19
1.0
ug/L
20.0 93 71-120
Trichloroethene
20
1.0
ug/L
20.0 98 74-120
4-Bromofluorobenzene
59
u91L
50.0 117 53-136
Dibromofluoromethane
53
u91L
50.0 106 67-129
Toluene-d8
54
u91L
50.0 107 59-134
Matrix Spike (3A19023-MS1)
Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 14:56
Source: CE00929-10
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
115
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
93
80-134
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
94
80-120
Toluene
19
1.0
ug/L
20.0
0.14 U
93
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
94
74-120
4-Bromofluorobenzene
61
u91L
50.0
123
53-136
Dibromofluoromethane
55
ug/L
50.0
110
67-129
Toluene-d8
54
u91L
50.0
108
59-134
Matrix Spike Dup (3A19023-MSD1)
Prepared: 01/19/2021 12:39 Analyzed: 01/19/2021 15:26
Source: CE00929-10
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
105
75-133
9
20
Benzene
18
1.0
ug/L
20.0
0.15 U
88
80-134
6
17
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
89
80-120
5
16
Toluene
18
1.0
ug/L
20.0
0.14 U
90
71-120
4
17
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
96
74-120
1
22
4-Bromofluorobenzene 56 u91L 50.0 112 53-136
Dibromofluoromethane 51 u91L 50.0 102 67-129
Toluene-d8 52 u91L 50.0 104 59-134
Batch IA20009 - EPA 5030E MS
Blank (3A20009-BLK3) Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 15:10
Analvte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1, 2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dich loroethane
1,1-Dichloroethene
1, 2, 3-Trich I o rop ropa ne
1,2-Di bromo-3-ch loropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
FINAL
Spike Source %REC
Result
Flaq
POL
Units Level Result %REC Limits
0.17
U
1.0
ug/L
0.12
U
1.0
ug/L
0.28
U
1.0
ug/L
0.14
U
1.0
ug/L
0.13
U
1.0
ug/L
0.21
U
1.0
ug/L
0.23
U
1.0
ug/L
0.48
U
1.0
ug/L
0.66
U
1.0
ug/L
0.19
U
1.0
ug/L
0.21
U
1.0
ug/L
0.10
U
1.0
ug/L
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit Notes
Page 86 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IA20009 - EPA 5030E MS - Continued
Blank (SA20009-BLK1) Continued Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 15:10
Analvte
Result
Flaq
POL
Units
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 50
u91L
50.0 100 53-136
Dibromofluoromethane 51
u91L
50.0 101 67-129
Toluene-d8 61
u91L
50.0 122 59-134
LCS (1A20009-BSI)
Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 13:18
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
113
75-133
Benzene
22
1.0
ug/L
20.0
109
80-134
Chlorobenzene
21
1.0
ug/L
20.0
105
80-120
Toluene
22
1.0
ug/L
20.0
108
71-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 87 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IA20009 - EPA 5030E MS - Continued
LCS (1A20009-BSI) Continued Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 13:18
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Trichloroethene
21
1.0
ug/L
20.0
104
74-120
4-Bromofluorobenzene
49
u91L
50.0
96
53-136
Dibromofluoromethane
50
u91L
50.0
100
67-129
Toluene-d8
62
u91L
50.0
123
59-134
Matrix Spike (1A20009-MS1)
Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 13:46
Source: CE01004-05
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
22
1.0
ug/L
20.0
0.21 U
110
75-133
Benzene
22
1.0
ug/L
20.0
0.15 U
109
80-134
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
108
80-120
Toluene
22
1.0
ug/L
20.0
0.14 U
108
71-120
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
105
74-120
4-Bromofluorobenzene
51
u91L
50.0
102
53-136
Dibromofluoromethane
49
u91L
50.0
96
67-129
Toluene-d8
62
u91L
50.0
124
59-134
Matrix Spike Dup (1A20009-MSD1)
Prepared: 01/20/2021 10:35 Analyzed: 01/20/2021 14:14
Source: CE01004-05
Spike
Source
%REC
RPD
Analvte
Result Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
106
75-133
4
20
Benzene
21
1.0
ug/L
20.0
0.15 U
107
80-134
2
17
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
107
80-120
2
16
Toluene
21
1.0
ug/L
20.0
0.14 U
106
71-120
1
17
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
102
74-120
3
22
4-Bromofluorobenzene 49 u91L 50.0 99 53-136
Dibromofluoromethane 49 u91L 50.0 98 67-129
Toluene-d8 61 u91L 50.0 123 59-134
Batch IA25038 - EPA 5030E MS
Blank (1A25038-BLK1) Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 18:50
Analvte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,3-Trichloropropane
1,2-Di bromo-3-ch loropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,4-Dichlorobenzene
2-Butanone
FINAL
Spike Source %REC
Result
Flaq
POL
Units Level Result %REC Limits
0.17
U
1.0
ug/L
0.12
U
1.0
ug/L
0.28
U
1.0
ug/L
0.14
U
1.0
ug/L
0.13
U
1.0
ug/L
0.21
U
1.0
ug/L
0.23
U
1.0
ug/L
0.48
U
1.0
ug/L
0.66
U
1.0
ug/L
0.19
U
1.0
ug/L
0.21
U
1.0
ug/L
0.10
U
1.0
ug/L
0.19
U
1.0
ug/L
1.3
U
5.0
ug/L
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit Notes
Page 88 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch IA25038 - EPA 5030E MS - Continued
Blank (SA25038-BLK1) Continued Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 18:50
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
4-Bromofluorobenzene
51
u91L
50.0
102
53-136
Dibromofluoromethane
52
u91L
50.0
104
67-129
Toluene-d8
61
u91L
50.0
123
59-134
LCS (1A25038-BSI)
Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 17:00
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
22
1.0
ug/L
20.0
108
75-133
Benzene
20
1.0
ug/L
20.0
101
80-134
Chlorobenzene
22
1.0
ug/L
20.0
109
80-120
Toluene
21
1.0
ug/L
20.0
104
71-120
Trichloroethene
22
1.0
ug/L
20.0
110
74-120
4-Bromofluorobenzene 49 u91L 50.0 97 53-136
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 89 of 99

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1A25038 - EPA 5030E MS - Continued
LCS (1A25038-BSI) Continued Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 17:00
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Dibromofluoromethane 50 u91L 50.0 101 67-129
Toluene-& 61 u91L 50.0 122 59-134
Matrix Spike (3A25038-MS1) Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 17:27
Source: CE01183-03
Spike
Source
%REC RPD
Analvte
Result Flan
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
25
1.0
ug/L
20.0
0.21 U
123
75-133
Benzene
21
1.0
ug/L
20.0
0.15 U
103
80-134
Chlorobenzene
23
1.0
ug/L
20.0
0.17 U
115
80-120
Toluene
21
1.0
ug/L
20.0
0.14 U
106
71-120
Trichloroethene
23
1.0
ug/L
20.0
0.15 U
114
74-120
4-Bromofluorobenzene
49
u91L
50.0
96
53-136
Dibromofluoromethane
52
u91L
50.0
103
67-129
Toluene-d8
60
u91L
50.0
120
59-134
Matrix Spike Dup (1A25038-MSDS)
Prepared: 01/25/2021 16:38 Analyzed: 01/25/2021 17:55
Source: CE01183-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
24
1.0
ug/L
20.0
0.21 U
118
75-133
4
20
Benzene
21
1.0
ug/L
20.0
0.15 U
107
80-134
4
17
Chlorobenzene
23
1.0
ug/L
20.0
0.17 U
113
80-120
2
16
Toluene
21
1.0
ug/L
20.0
0.14 U
105
71-120
0.4
17
Trichloroethene
22
1.0
ug/L
20.0
0.15 U
112
74-120
2
22
4-Bromofluorobenzene 50 u91L 50.0 99 53-136
Dibromofluoromethane 54 u91L 50.0 108 67-129
Toluene-d8 61 u91L 50.0 123 59-134
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch IA28012 - EPA 3005A
Blank (3A38012-BLK3) Prepared: 01/18/2021 09:22 Analyzed: 01/20/2021 09:36
Analvte
Result
Flaq
POL
Units
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 90 of 99

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1A18012 - EPA 3005A - Continued
LCS (IA18012-BSI) Prepared: 01/18/2021 09:22 Analyzed: 01/20/2021 09:44
Spike
Source
%REC
RPD
Analvte
Result
F
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Arsenic
205
10.0
ug/L
200
102
80-120
Barium
219
10.0
ug/L
200
109
80-120
Beryllium
20.4
1.00
ug/L
20.0
102
80-120
Cadmium
20.8
1.00
ug/L
20.0
104
80-120
Chromium
208
10.0
ug/L
200
104
80-120
Cobalt
211
10.0
ug/L
200
105
80-120
Copper
205
10.0
ug/L
200
103
80-120
Lead
207
10.0
ug/L
200
104
80-120
Nickel
218
10.0
ug/L
200
109
80-120
Silver
214
10.0
ug/L
200
107
80-120
Vanadium
206
10.0
ug/L
200
103
80-120
Zinc
212
10.0
ug/L
200
106
80-120
Matrix Spike (1A18012-MS1)
Prepared: 01/18/2021
09:22 Analyzed: 01/20/2021 09:47
Source: CE00125-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Arsenic
210
10.0
ug/L
200
7.60 U
105
75-125
Barium
276
10.0
ug/L
200
54.6
111
75-125
Beryllium
21.4
1.00
ug/L
20.0
0.348
105
75-125
Cadmium
21.0
1.00
ug/L
20.0
0.360 U
105
75-125
Chromium
212
10.0
ug/L
200
1.40 U
106
75-125
Cobalt
212
10.0
ug/L
200
1.40 U
106
75-125
Copper
208
10.0
ug/L
200
1.60 U
104
75-125
Lead
208
10.0
ug/L
200
3.10 U
104
75-125
Nickel
220
10.0
ug/L
200
2.20 U
110
75-125
Silver
215
10.0
ug/L
200
1.90 U
107
75-125
Vanadium
211
10.0
ug/L
200
1.40 U
105
75-125
Zinc
217
10.0
ug/L
200
4.40 U
109
75-125
Matrix Spike Dup (1AI8012-MSDI)
Prepared: 01/18/2021
09:22 Analyzed: 01/20/2021 09:49
Source: CE00125-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Arsenic
212
10.0
ug/L
200
7.60 U
106
75-125
0.9
20
Barium
279
10.0
ug/L
200
54.6
112
75-125
0.8
20
Beryllium
21.6
1.00
ug/L
20.0
0.348
106
75-125
1
20
Cadmium
21.2
1.00
ug/L
20.0
0.360 U
106
75-125
0.6
20
Chromium
215
10.0
ug/L
200
1.40 U
108
75-125
1
20
Cobalt
214
10.0
ug/L
200
1.40 U
107
75-125
0.8
20
Copper
210
10.0
ug/L
200
1.60 U
105
75-125
1
20
Lead
210
10.0
ug/L
200
3.10 U
105
75-125
1
20
Nickel
223
10.0
ug/L
200
2.20 U
111
75-125
1
20
Silver
217
10.0
ug/L
200
1.90 U
109
75-125
1
20
Vanadium
213
10.0
ug/L
200
1.40 U
107
75-125
1
20
Zinc
218
10.0
ug/L
200
4.40 U
109
75-125
0.2
20
Post Spike (1A18012-PS1)
Prepared: 01/18/2021
09:22 Analyzed: 01/20/2021 09:52
Source: CE00125-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be reproduced in
full.
Page 91 of 99

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1AlB012 - EPA 3005A - Continued
Post Spike (SA38012-PS3) Continued
Prepared: 01/18/2021 09:22 Analyzed: 01/20/2021 09:52
Source: CE00125-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit
Notes
Arsenic
0.237
0.0100
mg/L
0.200
0.000328
118
80-120
Barium
0.298
0.0100
mg/L
0.200
0.0546
122
80-120
QM-08
Beryllium
0.0236
0.00100
mg/L
0.0200
0.000348
116
80-120
Cadmium
0.0235
0.00100
mg/L
0.0200
-0.000371
117
80-120
Chromium
0.235
0.0100
mg/L
0.200
-0.000303
118
80-120
Cobalt
0.235
0.0100
mg/L
0.200
0.000142
117
80-120
Copper
0.231
0.0100
mg/L
0.200
0.000378
115
80-120
Lead
0.232
0.0100
mg/L
0.200
-0.00127
116
80-120
Nickel
0.245
0.0100
mg/L
0.200
0.000137
122
80-120
QM-08
Silver
0.224
0.0100
mg/L
0.200
-0.000314
112
80-120
Vanadium
0.233
0.0100
mg/L
0.200
0.000410
116
80-120
Zinc
0.241
0.0100
mg/L
0.200
0.00199
120
80-120
Batch 1AIB015 - EPA 3005A
Blank (3A38015-BLK1)
Prepared: 01/18/2021 09:33 Analyzed: 01/21/2021 11:09
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (1A18015-BSI)
Prepared: 01/18/2021 09:33 Analyzed: 01/21/2021 11:16
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
Arsenic
216
10.0
ug/L
200
108
80-120
Barium
223
10.0
ug/L
200
112
80-120
Beryllium
21.2
1.00
ug/L
20.0
106
80-120
Cadmium
21.8
1.00
ug/L
20.0
109
80-120
Chromium
214
10.0
ug/L
200
107
80-120
Cobalt
215
10.0
ug/L
200
107
80-120
Copper
211
10.0
ug/L
200
106
80-120
Lead
217
10.0
ug/L
200
109
80-120
Nickel
224
10.0
ug/L
200
112
80-120
Silver
218
10.0
ug/L
200
109
80-120
Vanadium
213
10.0
ug/L
200
106
80-120
Zinc
220
10.0
ug/L
200
110
80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 92 of 99

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1AlBO15 - EPA 3005A - Continued
Matrix Spike (1A18015-MS3)
Prepared:
01/18/2021
09:33 Analyzed: 01/21/2021 11:21
Source: CE00125-15
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
213
10.0
ug/L
200
7.60 U
107 75-125
Barium
261
10.0
ug/L
200
54.2
103 75-125
Beryllium
21.9
1.00
ug/L
20.0
0.204
108 75-125
Cadmium
21.7
1.00
ug/L
20.0
0.360 U
109 75-125
Chromium
217
10.0
ug/L
200
1.73
108 75-125
Cobalt
218
10.0
ug/L
200
1.40 U
109 75-125
Copper
212
10.0
ug/L
200
2.16
105 75-125
Lead
216
10.0
ug/L
200
3.10 U
108 75-125
Nickel
228
10.0
ug/L
200
2.20 U
114 75-125
Silver
219
10.0
ug/L
200
1.90 U
109 75-125
Vanadium
216
10.0
ug/L
200
1.69
107 75-125
Zinc
224
10.0
ug/L
200
4.40 U
112 75-125
Matrix Spike Dup (3A18015-MSD1)
Prepared:
01/18/2021
09:33 Analyzed: 01/21/2021 11:23
Source: CE00125-15
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
215
10.0
ug/L
200
7.60 U
107 75-125 0.8
20
Barium
267
10.0
ug/L
200
54.2
106 75-125 2
20
Beryllium
22.0
1.00
ug/L
20.0
0.204
109 75-125 0.9
20
Cadmium
22.0
1.00
ug/L
20.0
0.360 U
110 75-125 1
20
Chromium
220
10.0
ug/L
200
1.73
109 75-125 1
20
Cobalt
220
10.0
ug/L
200
1.40 U
110 75-125 1
20
Copper
215
10.0
ug/L
200
2.16
106 75-125 1
20
Lead
219
10.0
ug/L
200
3.10 U
109 75-125 1
20
Nickel
231
10.0
ug/L
200
2.20 U
116 75-125 1
20
Silver
222
10.0
ug/L
200
1.90 U
111 75-125 2
20
Vanadium
219
10.0
ug/L
200
1.69
108 75-125 1
20
Zinc
227
10.0
ug/L
200
4.40 U
113 75-125 1
20
Post Spike (SA18015-PS1)
Prepared:
01/18/2021
09:33 Analyzed: 01/21/2021 11:25
Source: CE00125-15
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.214
0.0100
mg/L
0.200
-0.00225
107
80-120
Barium
0.275
0.0100
mg/L
0.200
0.0542
111
80-120
Beryllium
0.0219
0.00100
mg/L
0.0200
0.000204
108
80-120
Cadmium
0.0218
0.00100
mg/L
0.0200
0.000124
108
80-120
Chromium
0.219
0.0100
mg/L
0.200
0.00173
109
80-120
Cobalt
0.216
0.0100
mg/L
0.200
8.44E-5
108
80-120
Copper
0.212
0.0100
mg/L
0.200
0.00216
105
80-120
Lead
0.215
0.0100
mg/L
0.200
0.000524
107
80-120
Nickel
0.226
0.0100
mg/L
0.200
0.00131
112
80-120
Silver
0.222
0.0100
mg/L
0.200
-0.000938
111
80-120
Vanadium
0.217
0.0100
mg/L
0.200
0.00169
108
80-120
Zinc
0.223
0.0100
mg/L
0.200
0.00273
110
80-120
Batch IA18021 - EPA 3005A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 93 of 99

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1AlBO21 - EPA 3005A - Continued
Blank (3A38021-BLK3) Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 10:44
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (1A18021-BSI)
Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 10:52
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
22.4
1.00
ug/L
20.0 112 80-120
Selenium
21.7
1.00
ug/L
20.0 109 80-120
Thallium
22.1
1.00
ug/L
20.0 111 80-120
Matrix Spike (1A18021-MS1)
Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 10:56
Source: CE00125-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
40.8
2.00
ug/L
40.0 0.740 U 102 75-125
Selenium
39.6
2.00
ug/L
40.0 1.82 U 99 75-125
Thallium
40.5
2.00
ug/L
40.0 0.570 100 75-125
Matrix Spike Dup (3A18021-MSD1)
Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 11:01
Source: CE00125-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
44.8
2.00
ug/L
40.0 0.740 U 112 75-125 9
20
Selenium
41.2
2.00
ug/L
40.0 1.82 U 103 75-125 4
20
Thallium
44.2
2.00
ug/L
40.0 0.570 109 75-125 9
20
Post Spike (SA38021-PS3)
Prepared: 01/18/2021 09:43 Analyzed: 01/26/2021 11:05
Source: CE00125-02
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
21.4
1.00
ug/L
20.0 0.0196 107 75-125
Selenium
20.1
1.00
ug/L
20.0 0.0374 100 75-125
Thallium
21.3
1.00
ug/L
20.0 0.285 105 75-125
Batch lAlBO22 - EPA 3005A
Blank (3A38022-BLK1)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:25
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (1A18022-BSI)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:38
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
Antimony
19.2
1.00
ug/L
20.0
96
80-120
Selenium
19.7
1.00
ug/L
20.0
99
80-120
Thallium
19.3
1.00
ug/L
20.0
96
80-120
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be reproduced in
full. Page 94 of 99

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 1AlBO22 - EPA 3005A - Continued
Matrix Spike (1A18022-MS3)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:43
Source: CE00125-24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Antimony
40.0
2.00
ug/L
40.0 0.740 U 100 75-125
Selenium
36.5
2.00
ug/L
40.0 1.82 U 91 75-125
Thallium
28.2
2.00
ug/L
40.0 0.220 U 71 75-125
QM-07
Matrix Spike Dup (3A18022-MSDS)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:47
Source: CE00125-24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Antimony
40.3
2.00
ug/L
40.0 0.740 U 101 75-125 0.7
20
Selenium
40.7
2.00
ug/L
40.0 1.82 U 102 75-125 11
20
Thallium
28.2
2.00
ug/L
40.0 0.220 U 70 75-125 0.07
20
QM-07
Post Spike (SA38022-PS1)
Prepared: 01/18/2021 09:46 Analyzed: 01/26/2021 08:51
Source: CE00125-24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Antimony
20.5
1.00
ug/L
20.0 0.0648 102 75-125
Selenium
19.0
1.00
ug/L
20.0 -1.08 95 75-125
Thallium
14.6
1.00
ug/L
20.0 0.0727 73 75-125
QM-08
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch IA20026 - EPA 5030E MS
Blank (1A20026-BLK3)
Prepared: 01/20/2021 00:00 Analyzed: 01/20/2021 10:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
0.80
U
2.0
ug/L
Toluene-&
5.0
u91L
5.00 99 75-125
LCS (1A20026-BSI)
Prepared: 01/20/2021 00:00 Analyzed: 01/20/2021 10:29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
23
2.0
ug/L
25.0 94 80-133
Toluene-&
5.2
u91L
5.00 104 75-125
Matrix Spike (1A20026-MS1)
Prepared: 01/20/2021 00:00 Analyzed: 01/20/2021 20:03
Source: CE00125-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
24
2.0
ug/L
25.0 0.80 U 95 80-133
Toluene-&
5.7
u91L
5.00 114 75-125
Matrix Spike Dup (1A20026-MSDS)
Prepared: 01/20/2021 00:00 Analyzed: 01/20/2021 20:28
Source: CE00125-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
25
2.0
ug/L
25.0 0.80 U 98 80-133 3
19
Toluene-&
5.3
u91L
5.00 105 75-125
Batch IA20035 - EPA 5030E MS
FINAL This
report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 95 of 99

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch IA20035 - EPA 5030E MS - Continued
Blank (1A20035-BLKI)
Prepared: 01/20/2021 14:20 Analyzed: 01/20/2021 23:25
Spike Source
%REC
RPD
Analvte
Result Flaq
POL
Uni
Level Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
0.80 U
2.0
ug/L
Toluene-&
5.0
u91L
5.00
99 75-125
LCS (IA20035-BSI)
Prepared: 01/20/2021 14:20 Analyzed: 01/20/2021 21:44
Spike Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
24
2.0
ug/L
25.0
96 80-133
Toluene-&
5.8
u91L
5.00
115 75-125
Matrix Spike (3A20035-MSS)
Prepared: 01/20/2021 14:20 Analyzed: 01/20/2021 22:09
Source: CE00125-26
Spike Source
%REC
RPD
An
Result Flao
POL
Units
Level Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
25
2.0
ug/L
25.0 0.80 U
101 80-133
Toluene-&
5.2
u91L
5,00 103 75-125
Matrix Spike Dup (1A20035-MSD1)
Prepared: 01/20/2021 14:20 Analyzed: 01/20/2021 22:34
Source: CE00125-26
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
25
2.0
ug/L
25.0 0.80 U 100 80-133 0.6
19
Toluene-d8
4.6
u91L
5.00 92 75-125
Batch IA22042 - EPA 5030E MS
Blank (1A22042-BLKI)
Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 10:49
Spike Source %REC
RPD
Analvte
Result
Flaa
POL
Uni
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
0.80
U
2.0
ug/L
Toluene-&
5.4
u91L
5.00 108 75-125
LCS (1A22042-BS1)
Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 10:24
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
26
2.0
ug/L
25.0 104 80-133
Toluene-&
5.4
u91L
5.00 108 75-125
Matrix Spike (3A22042-MS1)
Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 19:46
Source: CE00125-30
Spike Source %REC
RPD
Analvte
Result
Flaa
POL
Uni
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
280
10
ug/L
125 140 109 80-133
Toluene-d8
27
u9/L
25.0 108 75-125
Matrix Spike Dup (1A22042-MSD1)
Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 20:11
Source: CE00125-30
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
270
10
ug/L
125 140 107 80-133 1
19
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 96 of 99

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch IA22042 - EPA 5030E MS - Continued
Matrix Spike Dup (1A22042-MSDS) Continued Prepared: 01/22/2021 00:00 Analyzed: 01/22/2021 20:11
Source: CE00125-30
Spike Source %REC RPD
Analvte Result Flaq PQL Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 27 ug/L 25.0 109 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 97 of 99

(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
0-01 This compound is a common laboratory contaminant.
QI-03 The internal standard(s) for this sample were outside the acceptance limits due to sample matrix
interference. The sample was reanalyzed at a dilution.
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 98 of 99

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
E NkCC-� 1DT75 Central Port Dr. 4810 Executive Paris Court, Suite 111 102-A Woodwinds Industrial C1.
Orlando, FL 32824 Jacksonville. FL 32216-8089 Cary, NC 275t1ce INE �Mw
[phone] [phone] Fax [phone] (919} 467-3090 Fax t919) 467-3515 Page _L Of J
Client Name
01101WKNOw t AnadebW kXL (GAM)
Projecl Number
11 e
Requested
Analyses
Requested Turnaround
Times
Note: Rush requests subject la
acceptance by the facility
zl_� Standard
Expedited
Due
! 0
S�
r
x
r
32
m
G
k
m
x
U
rj Iq
Address
4300 IanrF"rr`9 C�+Q�te 100
oL Y ~
Project Narnstoesc
PHt=dkapLl I
City/STOp
Greenville, NC 27834
PO 11) Billing Info
1,5 It i
Tel
{2 )
52 7W3310
Fax
Reporting Contact
Emma Shi play
Sample((s) Name. Affiliation (Print)
Bating Contact
Emma Shipley
Sampler(s) Signature
Site Location I Time Zone
Lab Workorder
CE00125
Prettervatlon
(See
Codes)
(Combine
as necessary)
Item u
Sample ID (Feld Identification)
Collection Date
Collection
Time
Comp I Grab
Matrix
(see codes)
Total it of
Containers
Sample Comments
74014MIR
1-14.21
74014AW3
1- 1 y- 2
1 S: 'LJ
Gw
7
X
X
ak
,.'� �'.( "z'
'�` ;`��
Gw
7
X
X
�
�
Al401-MMR
7401-MW8
I -13 -2l
I l °- �
Gw
7
X
X
74014P2
I_ .2,1
5` p5
Gw
7
X
X
7401-P4
GW
7
X
X
7401-P5
I -Iy�ZI
t .'
Gw
7
X
X
7401-Pe
l- l'i - 21
12 ; 0
Gw
7
X
X
7401-P7
I- I _ -LI
Gw
7
X
X
7401-P9
- 1 -Zjl
I' ` o
Gw
7
X
X
7401-P11R
�1`I
C) r Zc•,
v
Gw
7
X
X
'1'7
<-- Total 1! Of Containers n
Sample Kit Prepared Byl
on tin
z
Relinquished By
Dalr�me
'j'`�� _I
Received
Dalamme
Comments!Speelal R rting Requirements
Relinquished By
DateMme
lived
Dalerriime
Relinquished By
Deterrime
Recei By
Datamme
Coder n's & Temps on
oon Rempl u
— �'l.V — \
Corldfion U Receipt
Acceptable Unacceptable
Matrix: f3W-Gmundwrater SO -Soil DWDrinking Water SE-Sedimerd SW -Surface Water WW-Wastewater A -Air er (detail in comments) Praaervatiom f-lce H-HCl WU 3 S•H2SO4 NO-NaOH O-Other (detal in comments)
Nola: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

14 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
�O 10776 Central Pert Dr 4810 Executive Park Court, Suite 111 102-A Woodwinds Indusrnal Cl.
Orlando, FL 32824 Jacksonville, FL 32216-8069 Cary, NG 27511
[phone] [phone] Fax [phone] [phone] Fax (919) a67-3515 Page -2
3—
of
Client Name
Project Number
Requested
Analyses
Requested Turnaround
p
�tr> IarA p�tllent AasooWftss, Inc. (GF4=
[nme
Times
Address - - - - ---
�
Note :Rush requests subtecl to
Pro*1 NNameMesc
4300 Sapphire Court, Suite 1 GO
PKt CoUnly LMM ^ AM I
�
acceptance by the facility
PO 01 Billing Info
City/STFGp
t'
x
Greertviae, NC 27834
5 i i5I
Reporting Contact
0
K Standard
Tel
i..x
[phone]
Emme Shipley
` Expedited
Due
Samplers) Name. Affiliation (Print)
Billing Conlacl
CM Sht l G,
Emma Shipley
po
.Sampler(s) Signature
Site Location / Time zone
Lab Work order
F>-
Preservation
(See
Codes)
(Combine
as necessary)
`tea_ `nne'F 1 }/� a��+
�+EVO ■ `�.+
-
Collection
Matrix
Total 1r of
Item d
Sample IV )Field Identification)
Collection Dale
Time
Comp ! Grab
(see codes)
Containers
Sample Comments
7401-P12
I-M-21
+SS
6r&b
7401-P13
i -j -2
' 0
GW
7
X
X
7401-P130
t- ry - r
! y' 0 0
Qw
7
X
X
7401-P18R
j • 0 !Z—V4•
>s'`3 :0-1
GW
7
X
X
7401-P17
1- 13 - ZI
I Si 3S
GW
7
X
X
7401-P19
Vs !' t,o'
�,�t ;i°
GW
T
X
X
7401-P20R
t t3`v7. 1W
GW
7
X
X
74014220D
, 1 W, LI
GW
7
X
X
7401-P21
, 7-1
91.00
GW
7
X
X
7401-P23
l ,. .L
Ss 5
GW
7
X
X
7401-P20
t, r�
>~5 s
OW
7
X
X
7401-P29
} i Zi
3` lO
GW
7
X
X
[--Total
# of Containers
Sample Kit Prepared By
Dal Time
2
Relinquished By
Daterrime
�•I'i'2i (o�1 5
Received EL
❑ letTiime
-f52 ow
Comments/Special R rling Requirements
Relinquished By
Datamme
Rece By
Dalemme
Relinquished By
Dateff"ime
R awed By
i
Data/Time
Cooler k's 8 Temps on Receipt
Condtion Upon Receipt
_Acceptable Unacceptable
Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW-Surlace Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: 1-1ce H-HCI N-HNO3 3-H2SO4 NO-NaOH O-Other (detzi in comments)
Note An samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this term, unless prior written agreements exist

ENVIRONMENTAL. CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
�O 10775 Central Fort Dr. 4810 Fxecutive Park Court. Suite 111 102-A Woodwinds industrial Ct_
Orlando, FL 32824 Jacksonville, FL 32216fi069 Cary, NG 27514
[phone] [phone] Fax [phone] [phone] Fax [phone] Page J of r
Client Name
115111M l+Iir Manag�_mw>t AI�ac111htR, Inc
Project Number
non#
Project NamatDesc
Kilt Landfill - AM I
Q
W
�
r
p
c
0
Requested
Analyses
Requested Turnaround
Times
Note - Rush requests subjw to
acceptance try the facifity
Standard
Expedited
Due hl_
t
p
$
4
Address
4300 Sepphim Court, Suhs 100
City/ST/Zip
Gnonvile, NC 27834
PO a / Billing Into
a S L `0, )
Reporting Contact
Erna Shipley
Tel
(232) 7158-3310
Fax
Sampler(s) Name, A1ltllallon (Print)
�:sR'1Mc1 �
Billing Contact
Emma Shipley
Samplels) Signature
Site Location; Time Zone
Lab Workorder
CE00125
Preservation
{See
Codes)
(Combine
as necessary)
Item #
Sample ID (Field Identification)
Collection Date
Collection
Time
Camp ! Grab
Matrix
(see codesy
Total a of
Containers
Sample Comments
74Q1-SY119
l • i � 1,1
t') : �-f
Ml-SVV2
1
1 S,;)
SW
7
X
X
7401$W4
1 .13' v
cr. 10
8W
7
X
X
7401-PZ1
It ILI r 2-1
10t SS
GW
7
X
X
7401-P22
t. pi . ZI
10 ; 30
(3W
7
X
X
7401-ES
It 1 3 , Z 1
AV S -7
WA
7
X
X
7401-FO
, i , 21
�.
WA
7
X
X
7401-TilipBtank
WA
2
X
7407-TripEkw*
WA
2
X
­ Total # of Containers 1
Sample Kit Prepared By
D te/Time
Z
Relinquished By
Dale/Time
i -ILI'Z 4;15
Received
Date/Time
1W)
CommentslSpecial Reporting equiremenis
Relinquished By
Daterrime
R
DateRme
Relinquished By
DateMme
rRecelved y
Datemme
Cooler O's & Temps on Receipt
Ooridtion Upon Receipt
Acceptable Unacceptable
Matrix GW-Groundwater SO -Sail OW -Drinking Water SE -Sediment SW -Surface Water WW-Wastewaler A -Air 0-Other (detail in oomments) Preservation. Woe H-HCl N-HNO3 5-42SO4 NO-Na0H 0-01her (deta(fn comments)
Note : All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
ENCO
Work Order: CE00125 Project: Pitt County Landfill - App I
Client: Groundwater Management Associates, Inc. (GR022; Project #: [none]
Logged In 15-Jan-21 11:30 Logged By: John C King 1 I
Preservation Check Performed By: ( Date/Time.
CE00125-01
Cont
Type
Pres (pH)
pH Checked 1
PH Adjusted DatelTime
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
I N I NA
Y 1 M/ NA
L, v
CE00125-02
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
PH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250ml-P+HNO3
<2
rY) I N/ NA
Y N NA
C E00125-04
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
PH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
(Y N / NA
Y / N 'NA
CE00125-05
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
PH Adjusted DateMme
Adjusted
Reagent Used/Comments
A
250rnLP+HNO3
'2
Y' l N / NA
Y N / NA
L/ —
CE00125-06
Cont
Type
Pres (pH)
Requirement
PH Checked I
In Control
PH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
��/ N / NA
Y N"/ NA
CE00125-08
Cont
Type
Pres (pH) PH Checked /
Requirement In Control
PH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2 YIN ! NA
YIN I NA
CE00125-09
Cont
Type
Pres (pH)
Requirement
pH Checked /
in Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y'I/ N 1 NA
Y / / NA
L
CE00125-10
Cont
T e
YP
Pres (pH)
Requirement
pH Checked /
In Control
Date/Time
PH Adjusted Adjusted
Reagent Used/Comments
A
250ml-P+HNO3
<2
YE N/ NA
Y I 1 NA
CE00125-11
Cant
Type
YP
Pres (pH}
Requirement
pH Checked /
In Control
Date/Tirne
PH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
I N/ NA
Y I / NA
C:IELMNT1Prinbwko_PreservationCheck. rpt
Page 1 c

Sample Preservation Verification
ENCO Cary
EJ�ICO
Work Order: CE00125 Project: Pitt County Landfill - App I
Client: Groundwater Management Associates. Inc. (GR022; Project #: [none]
Logged In: 15-Jan-21 11:30 Logged By: John C King C
Preservation Check Performed By: L r--) Date/Time: ` J
CE00125-12
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted DatelTime
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
Y I N/ NA
Y I NA
CE00125-13
Cant
Type
Pres (pH)
pH Checked /
pH Adjusted Date/Time
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
Y/ N / NA
Y 1 I NA
CE00125-1A
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted DateMme
Reagent Used/Comments
Requirement
in Control
Adjusted
A
250mLP+HNO3
<2
I N I NA
Y 01 NA
CE00125-15
Cant
Type
Pres (pH)
Requirement
pH Checked I
In Control
pH Adjusted DaterT'ime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y N/ NA
Y I 1 NA
v
CE00125-16
Cont
Type
Pres (pH)
Requirement
pH Checked I
In Control
pH Adjusted Daterl-ime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
1 <2
Yl / N / NA
Y ! �1 NA
u
CE00125-18
Cant
Type
Pres (pH) pH Checked /
Requirement in Control
pH Adjusted DatelTime Reagent UsedlComments
Adjusted
A
250mLP+HNO3
<2 J I N I NA
Y/ I NA
►n
CE00125-19
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Datemme
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
I N I NA
Y I 1 NA
R
CE00125-21
Cont
yP
Type
Pres (PH)
Requirement
pH Checked/
In Control
ri Adjusted Date/Time
pAdjusted
Reagent UsedlCor�unents
A
25OmLP+HNO3
<2
IIJ / N / NA
Y N / NA
CE00125-23
Cant
T e
YP
Pres (pH)
Requirement
pH Checked /
In Control
Date/Time
pH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
J / N / NA
I Y I N / NA
C:IELMNTIPrintlwko_PreservationCheck. rpt
Pacie

Sample Preservation Verification
ENCO Cary
�uco
Work Order: CE00125 Project: Pitt County Landfill - App I
Client: Groundwater Management Associates, Inc. (GR022) Project #: [none]
Logged In: 15-Jan-21 11:30 Logged By: John C King
Preservation Check Performed By: 0— Fj Date/Time: �S '2 l A'Z6V
CE00125-24
Cont
Type
Pres (pH)
IpHCheckedl
pH Adjusted Date/Time
Reagent Used/Comments
Requirement
I In Control
Adjusted
A
250mLP+HNO3
<2
N I NA
I Y I 1 NA
C E00125-25
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
N ! NA
Y / NA
CE00125-27
Cont
Type
Pres (pH)
Requirement
pH Checked/
In Control
pH Adjusted Date/Time
Adiusted
Reagent Used/Comments i
A
250mLP+HNO3
<2
N I NA
Y I y NA
CE00125-29
Cont
Type
Pres (pH)
Requirement
pH Checked /
I In Control
pH Adjusted Date/Time Reagent Used/Comments
Adjusted
A
250mLP+HNO3
<2
Y,)/ N / NA
Y IC1/ NA
CE00125-30
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2 Ll
/ N / NA
Y / N J NA
CE00125-31
Cont
Type Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3 <2
! N / NA
Y ! / NA
CE00125-32
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DateTTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2 J:D
N/ NA
Y IM NA
CE00125-33
Cont
T e
yp
Pres (pH)
Requirement
pH Chocked 1
In Control
Date/Time
pH Adi�sted Adjusted
Reagent UsedlComments
A
250mLP+HNO3
<2
1 N/ NA
Y/ N NA
CE00125-34
Con1
Yp
Type
Pres (pH)
Requirement
pH Checked/
I Control
DateMme
pH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y I N/ NA
Y/ 1 NA
C:IELMNT1Printlwko_PreservationCheck. rpt page 3 „

Sample Preservation Verification
ENCO Cary
Work Order CE00125 Project: Pitt County Landfill - App
Client: Groundwater Management Associates, Inc. (GR022, Project #: [none]
Logged In 15-Jan-21 11:30 Logged By. John C King
Preservation Check Performed By: _ DateiTfine
CE00125-35
Cant
Type
Pres (pH)
Requirement
pH Checked(
In Control
pH Adjusted Date/Time
Adiusted
Reagent Used/Comments
A
250mLP+HNO3
<2
1 N 1 NA
Y! NA
C E00125-36
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adiusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Yll N I NA
Y/ 1 NA
CE00125-37
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Tme
Adiusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y 1 N / NA
Y / p/ NA
Rea ent Name ID
1
2
pH Strip ID: 65 z j
v
Reacient Name ID
3
4
Rea ent Name iD
5
6
C1ELMNTIPrintlwko_PreservationCheck rpt page 4

ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
10775 Central Port Drive
Orlando FL, 32824
Phone: [phone] FAX: [phone]
Friday, March 19, 2021
Groundwater Management Associates, Inc. (GR022)
Attn: Emma Shipley
4300 Sapphire Court, Suite 100
Greenville, NC 27834
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Pitt County Landfill - SIM
ENCO Workorder(s): AE02021
Dear Emma Shipley,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, March 12, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Orlando. Data
from outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Kaitlin Dylnicki For David Camacho
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 7

(� �Eo
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-133313
Lab ID: AE02021-01
Sampled: 03/11/21 15:01
Received: 03/12/21 10:15
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
03/25/21
03/15/21 10:00
03/15/21 12:03
Client ID: 7401-TripBlank
Lab ID: AE02021-02
Sampled: 03/11/21 00:00
Received: 03/12/21 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
03/25/21
03/15/21 10:00
03/15/21 12:28
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 7

(� �Eo
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: 7401-P13D Lab ID: AE02021-01
Analvte Results Flag MDL Q Units Method Notes
1,4-Dioxane 1.4 3 0.80 2.0 ug/L EPA 8260D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 7

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13D Lab Sample ID:AE02021-01 Received: 03/12/21 10:15
Matrix: Ground Water Sampled:03/11/21 15:01 Work Order: AE02021
Project: Pitt County Landfill - SIM Sampled By: Amy Cressman, GMA
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl
Results
Flag
Units DF MDL PDL
Batch
Method
Analyzed
By
Notes
1,4-Dioxane [123-91-1]^
1.4
J
ug/L 1 0.80 2.0
1C15017
EPA 8260D
03/15/21 12:03
KKW
Surrogates
Results
DF
Spike Lv/ % Rec % Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
Toluene-d8
5.6
1
5.00 113 % 75-125
IC15017
EPA 8260D
03115121 12:03
KKW
Description: 7401-TripBlank
Lab Sample ID:AE02021-02
Received: 03/12/21 10:15
Matrix: Water
Sampled: 03/11/2100:00
Work Order: AE02021
Project: Pitt County Landfill - SIM
Sampled By: ENCO-RDU
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units DF MDL PQL
Batch
Method
Analyzed
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L 1 0.80 2.0
1C15017
EPA 8260D
03/15/21 12:28
KKW
Surrogates
Results
DF
Snike Lv/ % Rec % Rec Limits
Batch
Method
Analyzed
"
Notes
Toluene-d8
5.9
1
5.00 118 % 75-125
1C15017
EPA 8260D
03115121 12:28
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 7

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch IC15017 - EPA 5030E MS
Blank (1C15017-BLK3) Prepared: 03/15/2021 00:00 Analyzed: 03/15/2021 09:43
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 0.80 U 2.0 ug/L
Toluene-d8 5.6 ug/L 5.00 113 75-125
LCS (1C15017-BS1) Prepared: 03/15/2021 00:00 Analyzed: 03/15/2021 09:17
Spike Source %REC RPD
Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 21 2.0 ug/L 25.0 85 80-133
Toluene-d8 5.6 ug/L 5.00 112 75-125
Matrix Spike (1C15017-MS1) Prepared: 03/15/2021 00:00 Analyzed: 03/15/2021 13:19
Source: AD07508-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 25 2.0 ug/L 25.0 2.8 87 80-133
Toluene-d8 5.6 ug/L 5.00 111 75-125
Matrix Spike Dup (1C15017-MSD1) Prepared: 03/15/2021 00:00 Analyzed: 03/15/2021 13:44
Source: AD07508-01
Spike Source
Analvte Result Flaq POL Units Level Result %REC
1,4-Dioxane 25 2.0 ug/L 25.0 2.8 88
Toluene-d8 5.6 ug/L 5.00 112
%REC RPD
Limits RPD Limit Notes
80-133 1 19
75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 7

(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 7

14 ENVIRONMENTAL. CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
C� 10775 Central Port Dr 4810 Executive Park Court, Sulte 111 102-A Woodwinds Industrial Cl
Orlando, FL 32824 Jacksonville, FL 32216-SM Cary, NC 27511
[phone] [phone] Fax [phone] (919) 467.3M Fax [phone] Page _L of
Client Narne
GRKlndv,,%Wr f WM*eMWA IAxsoaal9s, WW. (GRM!
Prolm Number
Inonal
Requested
Analyses
Requested Turnaround
Times
Nate :Rush requests sub)act to
aooeplarlce by the laality
X Standard
-
_ Expedited
Due
O
_�
U)
0
0
[aka
_ _
Address
4300 Sapphire Court, Suite 100
Protect NamwDesc
Pitt County Landfill - SIM
CitylSTfZip
Greenville, NC 27834
PO 4 1 Billing Info
T61
[phone]
Fax
Reporting Contact
Emma Shipley
Sampler(s) Name, Affiliation (Print)
RM4 (feq,IN) at &MA
Billing Contact
Emmma Shipley
sampl r l signal re
h�
slia Location / Time zone
'�� Ca�nt►I C-at�4cr•� �{-or,jarj
Lab Workorder
Preservation
(See
Codes)
(Combine
as necessary)
Item 0Sample
ID {Field ldentification}
Collection Date
Collection
Time
Comp i Gran
Matrix
(see codes)
Total R of
Containers
r
Samp a omments
7401-P131)
QW
3
X
7401 TdpBIw*
WA
2
X
7401-TdVRa&
WA
2
X
<- Total # of Containers
Sample Krt Prepared By
&fume
Hall nqu B
DaIsMrre
Fiore,, 8
Da Imp
nm nlslSpecial Reporting Requirements
Relinquished By
DateRmel
Receive By
at me
Relinquished By
DalwTime
Received By
DatalTime
Cooler n's 8 Temps on Receipt 9j2Co7ACeptab
n Receipt
le Unacceplabie
Matrix GWGroundwater SO -Sal DW-Drinking Water SE-Secilment SW -Surface Water WW-Wastewater A -Air O-Other (detaiE in comments) Preservation: I -Ice H-HCI N-HNO3 S-1­12SO4 flo-NaOH 0-01har (detait In comments)
Note All samples submitted to ENCO Labs are to accordance with the terms and conditions listed on the reverse of this kxm, unless prior written agreements exist

APPENDIX D
WELL P13D VIDEO INSPECTION STILLS

Downhole video still showing the location of well casing damage
at 3.18 feet below the top of the well casing.
Iron staining provides evidence of past migration
of surface water down the well casing.

APPENDIX E
WELL REHABILITATION FIELD SHEETS

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: 6--I6-'-\ Crew: C.3S 4 A,u(,
Well Information
Well ID
Well Diam.
Sti
LS Elegy. ckupft
screen Interval
P13
in
2
ft MSL 82 i ht
3.8 ft BLS)
11.0 - 16.0
Listed Well Depth
Initial Well Depth
+ ��
Final Well Depth
419
(including stickup, ft)
19,8
(ft below TOC)
j
(ft below TOC)
Inspection Checklist: Does the well have a lockable rap or lid? ©(Yes ❑ No Is the vent hole clear and unobstructed? W'Yes ❑ No
Is the well tag present, labeled, and legible? d Yes ❑ No Is a concrete pad installed and visible? d Yes ❑ No
Is reference point marked on the TOC? i( Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes d No
Are the protective posts damaged? ❑ Yes I( No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? m Yes ❑ No
Reh b/Development Procedures Employed:
Brushing ❑ Surge Block Q1 Waterra ❑ Bailing
❑ Pumping / Overpumping, Pump description:
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
Sp.
Cond.
bs/cm)
Turbidity
(NTU)
t{� '.r��
Cl A-.�
-'i�-
1`_7
%
,C�i • S
`�. 1
STARTT
!i
J
�.�7' LU
w ekA A/
L(•�lU
Z•U
2-1. Z
S,G3
LN-C,
iOfu
MO
C1 ��
.�
'41.1,
S A
Li4-�'
1Ocu
0
]I
CV
S, 3 Z
r j��, j
� ;�D �r
OL l 6i- �LA13
Notes:
l lo t A'� tp� �`'� Wv �
Parameter
Stabilization Criteria
CI
H
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+j- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name:
Pitt County Landfill
Project No: 25101 Date: Crew:
Well Information
Well ID
I
Well Diarn.
LS Elev.
IStickup
IScreen Interval
P7
in
2
ft MSL
81.9
Hei ht ft
3.51 ft BLS
11.0 -16.A
Listed Well Depth
Initial Well Depth
ti
Final Well Depth r _l
+'
(including stickup; ft)
19.51
[ft below TOC)
+ '
(ft below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? I�Y ❑ No Is the vent hole clear and unobstructed? 21 Yes ❑ No
Is the well tag present, labeled, and legible? TYes ❑ No Is a concrete pad installed and visible? i1 Yes ❑ No
Is reference point marked on the TOC? ® Yes ❑ No 15 the pad cracked or deteriorated? ❑ Yes 0' No
Are the protective posts damaged? ❑ Yes d No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? dyes ❑ No
Rehab/Development Procedures Employed:
Q/Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
Q] aterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
{�C}
pH
Sp.
Cond.
(µsicm)
Turbidity
(NTl!}
o!7 s
'�;, '
START
w.yam
S2.6
'\bco4-
0R-
i4 .SC'
C'
21,Ur
y.75�
-)I.C1
Notes:
VOh
Parameter
Stabilization Criteria
❑
H
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name:
Pitt County Landfill
Project No: 25101 Date: �' ��p � i Crew: [ S k +%L
Well Information
Well ID
Well Diam.
LS EIev.
Stickup
Screen Interval
P9
in
2
ft MSL
130.1
Height ft
3.98
ft BLS
9.5 -14.5
Listed Well Depth
Initial Well Depth
�•
��+2
Final Well Depth
(including stickup; ft)
18,rfg
{ft below TOC]
[ft below TOC]
Inspection Checklist:
Does the well have a lockable cap or lid? M Yes ❑ No Is the vent hole clear and unobstructed? Y'Yes ❑ No
Is the well tag present, labeled, and legible? [ "Yes ❑ No Is a concrete pad installed and visible? B'Yes ❑ No
Is reference point marked on the TOC? i�' Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes 0 -No
Are the protective posts damaged? ❑ Yes ❑ No DIN jA
Does the pad slope away from the casing to prevent water from ponding? `If Yes ❑ No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
I/
®D lWaterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g, clarity of water and
success of development)
gal
Well
Volumes
Temp
[°C]
pH
Sp.
Cond.
��SJcm]
Turbidity
{NTu]
A
START
25
LJ
113,E
'5-4-7
"21-6
L\-Sy
I2L 2
J7 • ��
I r��
41 . G
`S' S 4 V
201. 1
Z
L\.w�
Notes: vt ' V1 f �A aVj1 f0��5 . Ul ► 4 e l
(:G1J V� k �tvJ p v l � . \6(7 to-() f 1'1bq CG � � � G� r7
�c, f27 11�� � 1. ' ? r�G'•4'Yk. G'
Parameter
Stabilization Criteria
❑
pH
+1- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
-+1- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: 4 /IQ 12t Crew: CJ 5 -g
Well Information
Well ID
Well Diam.
LS Efe�.
Stickup
Screen Interval
P21
in
2
ft MSL
77.8 Hei ht ft
4.27
ft BLS
8.D - ii.fl
Listed Well Depth
Initial Well Depth
— r
I +`a1 7 ,
Final Well Depth
,
(including stickup; ft)
15,27
(ft beloi
(ft below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? O'Yes ❑ No Is the vent hole clear and unobstructed? ® _Yes ❑ No
Is the well tag present, labeled, and legible?byes ❑ No Is a concrete pad installed and visible? 0 Yes ❑ No
Is reference paint marked on the TOC? ID, Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes O—No
Are the protective posts damaged? ❑ Yes ❑ No IQ/N/A
Does the pad slope away from the casing to prevent water from ponding? E�-Yes ❑ No
RehablDevelopment Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping J Overpumping, Pump description:
O" Waterra ❑ Bailing
Time
14
Water
Level
ft BTOC
C;.
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e•g• clarity of water and
success of development)
START
gal
f� y
Well
Volumes
Temp
[ C]
rr
P H
l,5
Sp.
Cond.
(µS/Cm)
lST F� I ' La
Turgidity
(NTU]
}
I LP
Notes:
wy&k pad A�CG'Oej o4 V' U 5�Yavj , 'v i5' b.� pc'­Cn no4 daMar,�
44pelt] of alit ��r � � ►� tL �
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Tem rature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name:
Pitt County Landfill
Project No: 25101 Date: Crew: C,a j r 4VW
Well Information
Well ID
I
Well Diam.
LS Elev.
Stickup
Screen Interval
P23
in
2
ft MSL
79.4
Hei ht ft
3.53
ft BLS 11.0 - 16.0
Listed Well Depth
Initial Well Depth
,• - - • >
Final Well Depth
`= r"
[including stickup; ft]
19.53
{ft below
{ft below TOC]
Inspection Checklist:
Does the well have a lockable cap or lid? CT"Yes ❑ No Is the vent hole clear and unobstructed? 0� Yes ❑ No
Is the well tag present, labeled, and legible? ❑' Yes ❑ No Is a concrete pad installed and visible? ❑ Yes o Ho
Is reference point marked on the TOC? ❑ Yes A No Is the pad cracked or deteriorated? ❑ Yes ❑ No
Are the protective posts damaged? ❑ Yes ❑ No 0'-N/A ,t
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
cc .�s Ic I
Rehab/ Development Procedures Employed:
❑ Brushing ❑ Surge Block Waterra ❑ Bailing
❑ Pumping / Overpumping, Pump description:
Time
Water
Level
ft STOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
°
pH
Sp.
Cond.
(PS/cm)
Turbidity D
,FLU
! i
START
: o S
57
2
2 ..�
VA kion
k
�R
I
A
r�.0
lvGc ;
G;;CrrCirr ' �Li itl r' c{ �ti
213
S. W Zy
`%� �-
b�.
22 1 J
L
�C?ti 7
302
Notes: `
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 1011/6 or less than 10 NTUs
,I,
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: j l 1 1 1f Crew: C 3 +
Well Information
Well ID
Well Diam.
LS Elev. Stickup
Screen Interval
P12
in 2
ft MSL 75.9 Hei ht ft 3.41
ft BLS)
10.5 -17.5
Listed Well Depth
Initial Well Depth
ti !' al Final Well Depth
0 ,
`t I
(including stickup; ft)
20.91
(ft below TOC]
(ft below TOC)
•
Inspection Checklist: rV-, 4f-
Does the well have a lockable cap or lid? or Yes ❑ No Is the vent hole clear and unobstructed? ❑ Yes © No
Is the well tag present, labeled, and legible? ❑ Yes m/No Is a concrete pad installed and visible? ❑ Yes V' No
Is reference point marked on the TOC? [Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes ❑ No
Are the protective posts damaged? ❑ Yes ❑ No NIA `
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No � 3 l
Rehab/ Development Procedures Employed: �
❑ Brushing ❑ Surge Block Waterra
❑ Pumping / Overpumping, Pump description:
❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
rn)
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(C)
pH
5p•
Cond•
(gs1cm)
Turbidity
(NTU)
START
0
L i
19,7
1 5,39
57,7
7,e-7
,a'.
0:-1
tiA-
S ' z
13
3 '.Ll 5
r`1, S Cf
1
Ubl
t00 7
Notes:
Ned to
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: ! I7 ? Crew: C s5 .i AIiC
Well Information
Well ID
Well Diam.
LS Elev. Stickup
Screen Interval
T
P11R
in
2
ft MSL 82.3 Hei ht ft 3.74
ft BLS
13.0 -16.0
Listed Well Depth
Initial Well Depth
ii `,�
—
Final Well Depth
(including stickup; ft)
19.74
(ft below TOC)
(ft below TOC)
Inspection Checklist: / /
Does the well have a lockable cap or lid? 6d Yes El s the vent hole clear and unobstructed? GI' Yes ❑ No
Is the well tag present, labeled, and leg ibl ? AfYes ; 49 Is a concrete pad installed and visible? ❑ Yes ld No
Is reference point marked on the TOC? QYes/ ❑ No ""* �� � Is the pad cracked or deteriorated? ❑ Yes ❑ No A� �§
Are the protective posts damaged? ❑ Yes © No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
M Waterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
Comments
n
{eg' clatY of water and
success of development)
9 al
Well
Volumes
Temp
(°Cj
p H
Sp.
Cond.
(µSIcm)
Turbidity
{NIL!]
15
r]i 17
START
Zd
u:8
I� 7
K,ci l
-78 U7
q
�5
2,-1
-5,00
—IS.5
LL
r..
r't-7
i, 4CV 5 ji9[ rrwi� r
Notes:
w aki VICeS
Cr4 'vi• 1y�
1 oom CA 40,v6 , cr �ctr�►C rl�t t r i n �� wGr ; �►n J
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
Cl
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: ul j-7l2� Crew:
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
I P28
in
2
ft IVISL
74.8 Height ft
2.94 ft BLS 3.5 - 8.D
Listed Well Depth
Initial Well Depth
7
l 1, Z-7
Final Well Depth
(including stickup; ft)
10.94
(ft below TOC]
(ft below TOC]
Inspection Checklist: /
Does the well have a lockable cap or lid? ® Yes ❑ No Is the vent hole clear and unobstructed?1© Yes ❑ No
Is the well tag present, labeled, and legible? M/Yes ❑ No Is a concrete pad installed and visible? 0'Yes ❑ No
Is reference point marked on the TCC? dyes ❑ No Is the pad cracked or deteriorated? 11 Yes 0--No
Are the protective posts damaged? ❑ Yes ❑ No WN/A
Does the pad slope away from the casing to prevent water from ponding? L�YYes ❑ No
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block rWaterra
❑ Pumping / ❑verpumping, Pump description:
F1 Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
g rn
Cumulative Total
Removed
Water Characteristics
Comments
{e.g. clarity of water and
success of development)_
gal
Well
Volumes
Temp
{°C}
p H
Sp.
Cond.
(PS/cm)
Turbidity
(NTU)
START
55
1,75
Z1. -75
a
, ow
5- %3 I
U,Z A
! 6 f 0 -r-
C ! 2' ' LZ ( J Nj d
Notes:
Tvo 6r)
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name:
Pitt County Landfill
Project No: 25101. Date: C, f ?i L1 Crew:
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P20R
in
2
it MSL
81.7
Hei ht ft
3.51
ft BLS
10.0 - 30.0
Listed Well Depth
Initial Well Depth r} Final Well Depth
3L �(ft
(including stickup; ft)
33.51
{ft below TOC] . below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? B�Yes ❑ No Is the vent hole clear and unobstructed? E Yes ❑ No
Is the well tag present, labeled, and legible? ©"Yes ❑ No Is a concrete pad installed and visible? ❑ Yes ®'No
Is reference point marked on the TOO ❑ Yes 12f No Is the pad cracked or deteriorated? ❑ Yes ❑ No
Are the protective posts damaged? ❑ Yes ❑ No Q N/A N
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
�Y 1
Rehab/ Development Procedures Employed.
❑ Brushing ❑ Surge Block
❑ Pumping / Overpurnping, Pump description:
❑/Waterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
{e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C)
pH
Sp.
Turbidity
Cond. {NTU)
(AS/cm)
START
67 c)
a-+L
20.
� . i �
jSS`{ 1Zs
11c
O-I �yr�1�-
I S
•�"5
)L' 1
LIST:. -i
I
-31n Lt GL�'L& •kL ICiL+�l
�j lC3
C1.5
7_uy -�
4a.1�.
`"l�-
Ic7iJ�
[7f� �4�h„. bEv ►c�J
l .• I
Z
1 t f[
, i
F �� ilk°
L C7� �7 i
d{.f 7 r'rt. C'v
tiS
►kl
iZ
1kl
�l
�2``
1600 k
op-
'k�' 50
�1
��.5
-1Z
13� 1
�►.r
aQ
Notes:
c4 fl� 51R a (GVI ci/�P—k -Pi
c� ) t,4 <:)�-( X'l rK -sav\) 10 P6•'&f ))O C�4
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/•- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: u h I //c! Crew: Gi5 -I- ► Lk-e-
Well Information
Well ID
Well Diam.
S Elegy.
Stickup
Screen Interval
P17
in
2ft
MSL
76.3
Hei ht ft
4.08
ft BLS
8A - 11A
Listed Well Depth
Io
nitial Well Depth
1 a - -S[)
Final Well Depth
1 I S, 5 v
(including stickup; ft)
15.0$
ft below TOC)
(ft below TOC)
Inspection Checklist: /
Does the well have a lockable cap or lid? Pr Yes ❑ No Is the vent hole clear and unobstructed? 8/Yes ❑ No
Is the well tag present, labeled, and legible? ©/Yes ❑ No Is a concrete pad installed and visible? El Yes ❑ No
Is reference point marked on the TOC? M-'/Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes ©'No
Are the protective posts damaged? ❑ Yes ❑ No I3/N/A
Does the pad slope away from the casing to prevent water from ponding? 0 Yes ❑ No
Rehab/ Development Procedures Employed:
❑ Brushing ❑ Surge Block
Cl Pumping / Overpumping, Pump description:
EvI Waterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
state
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C}
p H
Sp.
Cond.
(PS/cm)
Turbidity
(NTU]
AWK
ASTART
2tZ5
tci.ol
-5,i-I
lWiv
it266 t-
cam. d�
Notes:
�Pa l
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
5 cific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: [� 10 12_1 Crew: "5 t i4l %-;c.
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval —r
MW611
in
2
ft MSL
78.15
Hei ht ft Z.79
ft B!5
7.D - 17.0
Listed Well Depth
Initial Well Depth
e Final Well Depth
�,
lot �' 0
(including stickup; ft)
19.79
(ft below TOC)
! (ft below TOC)
'
Inspection Checklist:
Does the well have a lockable cap or lid? d Yes ❑ No Is the vent hole clear and unobstructed? U❑ Yes ❑ No
Is the well tag present, labeled, and legible? lJ Yes ❑ No Is a concrete pad installed and visible? ❑ Yes 11-No
Is reference point marked on the TOC? ❑ Yes L4' No Is the pad cracked or deteriorated? ❑ Yes ❑ No kff�
Are the protective posts damaged? Yes ❑ No ❑ N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No l
Rehab/Development Procedures Employed:
❑ Brushing ❑ Surge Block "aterra ❑ Bailing
❑ Pumping / Overpumping, Pump description:
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
{�C}
pH
Sp.
Cond.
(PS/cm)
Turbidity
{NTU}
I �] Z 7
%,
START
kl 30
Z
20,-7
U t. o
=1
loci
b
1'S,-5SJ
7
'73
►
io,,o
c�
lGr-72
��`1�
1Ctii r
GQ
3:;7�
71
W&
Lz
Notes:
14 '01- -54y� to ut
Parameter
Stabilization Criteria
❑
H
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 109l0 or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: to r I -71,71 Crew: (•�,D •F AW(
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P16R
in
2
ft MSL
84.3 Hei ht ft
3.14
ft BLS 11.8 - 14.0
Listed Well Depth
Initial Well Depth
Jl �}
Final Well Depth
r
l
(including stickup; ft)
17.14
(It below TOC]
1
(ft below TUC)
Inspection Checklist: ,
Does the well have a lockable cap or lid? C�Yes ❑ No Is the vent hole clear and unobstructed? El Yes ❑ No
Is the well tag present, labeled, and legible? dYes ❑ No Is a concrete pad installed and visible? 0 Yes C No
Is reference point marked on the TOO ❑ Yes IT No Is the pad cracked or deteriorated? IYYes ❑ No
Are the protective posts damaged? ❑ Yes EAo ❑ N/A ct�. 1112 `A' x` D' C' 4 uJ
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ©'No
Rehab/ Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpumping, Pump description:
❑,Waterra ❑ Bailing
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of develo ment
gal
Well
Volumes
C,
pH
Sp',
con.
{µ5/cm]
T (NTrU ry
,
, LL-7
START
'' [[
•ice,
c.�,.,�r
U Gir�{ 6"�
7j[.�
f _ 1 U
i i� . ll'
-7. 1
?,8
Notes:
�c V �j�-e �p
Parameter
Stabilization Criteria
❑
pH
+/- 0.1 unit
❑
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
Cl
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: b 1 / i/2( Crew:
Well Information
Well ID
Well Diam.
LS Elev.
Stickup
Screen Interval
P19
in
2
ft MSL
78.5
Hei ht ft
5.4
ft BLS
9.0 -13.0
Listed Well Depth
Initial Well Depth - -
Final Well Depth
i(ftbelowTO
{including stickup; ft}
18,4
eft below TOC} i + w '—
C}
Inspection Checklist: 11
Does the well have a lockable cap or lid? [yr Yes ❑ No Is the vent hole clear and unobstructed?,17'"Yes ❑ No
Is the well tag present, labeled, and legible? Q'Yes ❑ No Is a concrete pad installed and visible? o' Yes ❑ No
Is reference point marked on the TCC? ❑"Yes ❑ No Is the pad cracked or deteriorated? "es f] No
Are the protective posts damaged? ❑ Yes ❑ No ©'N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
Rehab/ Development Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / ❑verpumping, Pump description:
❑ Waterra ❑ Sailing
Time
Water
Level
ft STOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of development)
gal
Well
Volumes
Temp
(°C}
pH
$P•
Cond.
(PS/cm)
Turbidity
[NT+�)
START
3
i� l
3
1�-f 1
iow��
a�
18
L Cx,,
ilf-Z
LOOO i
, ,
2�•a
�.�o
�y�>
>c�ox'-�
4{L
Notes:
}
fJYl�;r G 1 -P_�, \Ja6d ck�o' L
Parameter
Stabilization Criteria
❑
PH
+/- 0.1 unit
©
Temperature
Less than 3% variance
❑
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUS
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA

Monitoring Well Rehabilitation Field Sheet
Project Name: Pitt County Landfill Project No: 25101 Date: �O17171 Crew: C-6 t 4yic:
Well Information
Well ID
I
Well D"tam.
LS Elev.
IStickup
I
Screen Interval
P29
in
2
ft MSL
82.4
[Height ft
2.96
ft BLS 7.0 -12.0
Listed Well Depth
Initial Well Depth
7 ,•
15
Final Well Depth
~�
(including stickup; ft)
14.96
(:below TOC)
(ft below TOC)
Inspection Checklist:
Does the well have a lockable cap or lid? Q/es ❑ No Is the vent hole clear and unobstructed? C9'Yes ❑ No
Is the well tag present, labeled, and legible? P'Yes ❑ No Is a concrete pad installed and visible? ❑ Yes ❑-No
Is reference point marked on the TOC? ©'Yes ❑ No Is the pad cracked or deteriorated? ❑ Yes ❑ No I`
Are the protective posts damaged? ❑ Yes ❑ No 11'N/A
Does the pad slope away from the casing to prevent water from ponding? ❑ Yes ❑ No
i� rl
Rehab/De►►elopment Procedures Employed:
❑ Brushing ❑ Surge Block
❑ Pumping / Overpurnping, Pump description:
Waterra ❑ Baiiing
Time
Water
Level
ft BTOC
Pumping
Rate
m
Cumulative Total
Removed
Water Characteristics
Comments
(e.g. clarity of water and
success of develo meat
gal
Well
Volumes
Temp
(0C)
pH
Sp.
Cond.
(µS/cm)
Turbidity
{NTU)
LP + %
START
i '��
F.•�'f
� l�
'-i.�]
��a4L�
�F'w..'G�
L�14�.^C4�.li��
q .-77
2{,��
d
Notes:
wa& �Qofi �Ocko� q'Afr 15 00
Parameter
Stabilization Criteria
❑
H
+/- 0.1 unit
❑
Temperature
Less than 3% variance
Cl
Specific Conductance
Less than 10% variance
❑
Turbidity
+/- 10% or less than 10 NTUs
INDICATOR PARAMETERS HAVE STABILIIED WHEN 3 CONSECUTIVE READINGS ARE WITHIN STABILIZATION CRITERIA