6001_Mecklenburg_Harrisburg_MSWLF_June21GW_FID1588306_20210707

Y T� ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
Division of Waste Management - Solid Waste
Environmental Monitoring
ReDortina Form
Notice: This
form and
any
information attached
to it are "Public Records"
as defined in NC
General Statute 132-1. As such, these tlocuments are
available for
inspection
and
examination by any
person upon request (NC
General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzvmski, P.G.
E-mail: [e-mail]
Facility name:
Harrisburg Road Landfill
Address:
7817 Harrisburg Road, Charlotte
Phone:[phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Permit # (.0500 or . mou) October 20-24, 2006)
une 15-16, 24, 2021
Environmental Status: (Check all that
apply)
Initial/Background Monitoring Q Detection Monitoring � Assessment Monitoring � Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells Q
Groundwater monitoring data from private water supply wells
Leachate monitoring data ❑
Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
)( Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levelsI and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G. Project Manager 980-314-3855
tHrea �oael ieiepnone Number
Affix NC Licensed/ Professional Geologist Seal
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

MEUKLENBURU COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
July 7, 2021
Jaclynne Drummond
North Carolina Department of Environment
and Natural Resources
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Water Quality Monitoring Report June 2021
Harrisburg Road Landfill, Permit 60-01
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Harrisburg Road Landfill June 15 and June 16, 2021 in accordance with the approved
revised sample and analysis plan dated May 11, 2004. Samples were collected from
eleven monitoring wells (HBW-12A, HBW-12B, HBW-14, HBW-14B, HBW-14C,
1BW44D, HBW47B, HBW-20, HBW-21, HBW-22 and background well HBW-28)
and three surface -water sampling locations (HB2006, HB2008 and, HB2010). Laboratory
analytical data, field -measured data, and a table of results exceeding water quality
standards along with a preliminary explanation of the cause and significance are included
on the electronic data deliverable (EDD) submittal.
The EDD containing the monitoring data are labeled to reflect the units that are used for
reporting. Detection levels and applicable standards have been included for all sampling
locations. Surface water standards listed are the water quality standards established for
freshwater classification for aquatic life as outlined in 15A NCAC 2B "Classification and
Water Quality Standards Applicable to Surface Waters of North Carolina". Groundwater
standards listed are the standards outlined in 15A NCAC 2L "Classification of Water
Quality Standards applicable to the Groundwaters of North Carolina". If the sample is
reported in parts per billion, then the standard is also reported in parts per billion.
Surface -water samples:
PEOPLE • PRIDE • PROGRESS •PARTNERSHIP
2145 Suttle Ave • Charlotte, NC 28208-5237 • [phone] •FAX [phone]
www.wipeoutwaste.com

Page 2
Barium was detected in HB 2006, HB 2008 and HB 2010 at 33.1 ppb, 20.5 ppb and 41.5
ppb, respectively. No other analytes were detected in the surface water samples. Field -
measured parameters for surface -water samples were within the range of established
standards and are summarized in the table below.
Location
Temperature
PH
Specific
Conductivity
Dissolved
OxvLyen
HB2006
22.50 C
TO
0.199 ms/cm
4.35 mg/l
HB2008
21.6° C
7.1
0.234 ms/cm
6.48 mg/l
HB2010
20.40 C
6.8
0.277 ms/cm
5.84 mg/1
Groundwater samples:
Multiple metals were detected above 2L standards. The table below summarizes metals
detections in groundwater samples.
Well ID
Ba
ug/1
Be
ug/l
Cd
ug/l
Cr
ug/1
Co
ug/l
Cu
ug/1
Ni
ug/1
Pb
ug/l
Th
ug/1
Vn
ug/1
Zn
ug/1
HBW12A
48.7
swum---
swum---
9.4
6.3
31.1
6.3
T9
swum --swum
52.5
16.6
HBW12B
38.7
swum---
swum---
swum---
8.2
swum---
swum---
swum---
swum --swum
5.4
-----
HBW1476.2
swum---
swum---
swum---
-----
swum---
swum---
swum---
------
swum---
-----
HBW14B20.6
swum---
swum---
swum---
-----
swum---
swum---
swum---
swum --swum
swum---
-----
HBW14C
71.6
swum---
swum---
5.1
swum---
19.6
swum---
5.9
swum --swum
9.9
-----
HB W 14D
61.8
--swum-
swum---
swum---
swum---
6.0
swum---
swum---
swum --swum
6.6
-----
HBW17B
66.9
swum---
swum---
20.1
27.0
swum---
swum---
swum---
swum---
16.4
HBW-20
29.4
swum---
swum---
6.6
6.4
30.4
5.3
swum---
swum --swum
49.1
17.8
HBW-21
11.8
-----
-swum--
swum---
-----
swum---
ammo---
-----
------
6.2
-----
HBW-22
44.4
-----
--swam-
22.7
-----
-swum--
7.4
swum---
swum---
swum---
-----
HBW-28*
92.3
-----
swum---
-----
126
49.8
15
swum---
swum --swum
10.8
-----
2L Std. ug/l
700
4
2.0
10
1
13000
100
15
0.2
0.3
1,000
Note: Bolded results exceed 2L Standard, *Background Well
The following nine volatile organic compounds ("VOCs") were detected in the sample
collected from well HBW-17B 0
VOC
Sam le Result u /1
2L Standard u /1
Benzene
5.7
1
Tetrachloroeth lene
24.8
0.7
Trichloroeth lene
19.2
2.8
1,1-Dichloroethane
5.5
6
1,2-Dichloro ro ane
8.3
0.6
cis-1,2 Dichloroethene
77.4
70
trans-1,2-Dichloroethene
1.1
100
X lens total
7.4
500
Methylene Chloride
6.1
5
Note: Bolded results exceed 2L Standard

The pH was measured to be more acidic than the standard in the samples collected from
HBW12A, HBW12B, HBW14, HBW14B, HBW14C, HBW14D, HBW17B, HBW20,
4BW21, HBW22 and background monitoring well HBW-28. Field -measured parameters
for groundwater samples are summarized in the following table:
Location
Tem erature
pH
onductivity
HBW12A
14.8
°C
5.9
0.375
ms/cm
HBW12B
15.4
°C
5.8
0.439
ms/cm
HBW14
15.0
°C
5.8
0.314
ms/cm
HBW14B
15.3
°C
6.0
0.229
ms/cm
HBW14C
15.0
°C
5.8
0.210
ms/cm
HBW 14D
15.3
°C
6.3
0.206
ms/cm
HBW 17B
16.9
°C
4.9
0.071
ms/cm
HBW-20
16.1
°C
5.8
0.146
ms/cm
HBW-21
16.2
°C
5.9
0.192
ms/cm
HBW-22
18.1
°C
5.6
0.075
ms/cm
*HBW-28
17.4
°C
5.1
0.035
ms/cm
Note: Bolded results are outside of the 6.5 to 8.5 S.U. range 2L Standard
*Background Well
Please call me at [phone], if you have any questions concerning this report.
Sincerely,
Project Manager
LUESA Solid Waste Services

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Landfill Gas Monitoring Data Form
Facility Name: Harrisburg Road Landfill
Permit Number: 60-01
Date of Sampling: 6/24/2021 NC Landfill Rule (.0500 or .1600): .0500
Name and Position of Sample Collector: David E. Coleman, Environmental Specialist
Type and Serial Number of Gas Meter: Gem 5000 #G507530
Calibration Date of Gas Meter: 4/26/2021 _Date and Time of Field Calibration: 6/24/2021 10:15
Type of Field Calibration Gas (15/15 or 35/50): 35/50
Expiration Date of Field Calibration Gas Canister: Apri12025
Pump Rate of Gas Meter: 120 Seconds _ Ambient Air Temperature: 70 De rees
Barometric Pressure: _29.62 General Weather Conditions: Partly Sunny, Winds E8
Sam le ID
Time
% LEL
% CH4
% CO2
% 02
Comments
M131
14:29
>100
60.1
39.8
.1
Methane Extraction System
MP-2
14:22
>100
5209
25.9
3.9
Methane Extraction System
MP-3
14:15
0
0
0.1
20.3
Methane Extraction System
MP4
14:10
>100
2008
12.2
13.4
Methane Extraction System
MP-5
15:11
0
0
3.2
17.5
MP-6
15:17
0
0
4.9
1208
MP-7
15:24
0
0
6.0
15.2
MP-8
15:32
0
0
7.8
14.6
MP-9A
15:39
0
0
1.6
18.7
MP-913
15:45
0
0
4.2
IT 1
MP-11
1146
>100
6.8
4.3
17.5
MP-12
13*54
0
0
8.6
13.1
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and
attachments are true and correct. I am aware that there are significant penalties for making any false
statement, representation, or certification including the possibility of a fine and imprisonment.
SIGNATURE
TITLE

60-01 Harrisbura Rd Landfill Methane Wells
4
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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 29, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on June 15, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92544431001 6001-HBW28
EPA 601OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544431002 6001-HBW20
EPA 601OD
IDS
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544431003 6001-HBW14
EPA 601OD
IDS
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544431004 6001-HBW14B
EPA 601OD
IDS
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544431005 6001-HBW14C
EPA 601OD
IDS
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544431006 6001-HBW14D
EPA 601OD
IDS
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544431007 Trip Blank
EPA 8260D
NSCQ
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW28
Lab ID: 92544431001
Collected:
06/15/21
10:20
Received: 06/15/21 15:31 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:28
7440-38-2
Barium
92.3
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 12:28
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 12:28
7440-43-9
Chromium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7440-47-3
Cobalt
126
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7440-48-4
Copper
49.8
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7440-50-8
Lead
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7439-92-1
Nickel
15.0
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:28
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:28
7440-28-0
Vanadium
10.8
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:28
7440-62-2
Zinc
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:28
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND
ug/L
1.0
1
06/25/21 16:49
06/28/21 13:06
7440-28-0 PB
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/15/21 23:04
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/15/21 23:04
107-13-1
Benzene
ND
ug/L
1.0
1
06/15/21 23:04
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/15/21 23:04
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/15/21 23:04
75-27-4
Bromoform
ND
ug/L
1.0
1
06/15/21 23:04
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/15/21 23:04
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/15/21 23:04
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/15/21 23:04
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/15/21 23:04
56-23-5 v1
Chlorobenzene
ND
ug/L
1.0
1
06/15/21 23:04
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/15/21 23:04
75-00-3
Chloroform
ND
ug/L
5.0
1
06/15/21 23:04
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/15/21 23:04
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/15/21 23:04
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/15/21 23:04
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/15/21 23:04
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/15/21 23:04
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 23:04
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 23:04
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/15/21 23:04
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/15/21 23:04
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/15/21 23:04
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 06/29/2021 02:16 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 4 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW28 Lab ID: 92544431001 Collected: 06/15/21 10:20 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:04
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:04
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:04
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:04
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:04
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:04
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/15/21 23:04
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/15/21 23:04
591-78-6
lodomethane
ND
ug/L
20.0
1
06/15/21 23:04
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/15/21 23:04
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/15/21 23:04
108-10-1
Styrene
ND
ug/L
1.0
1
06/15/21 23:04
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/15/21 23:04
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/15/21 23:04
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/15/21 23:04
127-18-4
Toluene
ND
ug/L
1.0
1
06/15/21 23:04
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/15/21 23:04
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/15/21 23:04
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/15/21 23:04
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/15/21 23:04
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/15/21 23:04
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/15/21 23:04
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/15/21 23:04
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/15/21 23:04
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/15/21 23:04
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/15/21 23:04
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
06/15/21 23:04
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
06/15/21 23:04
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
06/15/21 23:04
2037-26-5
Date: 06/29/2021 02:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW20
Lab ID: 92544431002
Collected:
06/15/21
10:50
Received: 06/15/21 15:31 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:54
7440-38-2
Barium
29.4
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 12:54
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 12:54
7440-43-9
Chromium
6.6
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7440-47-3
Cobalt
6.4
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7440-48-4
Copper
30.4
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7440-50-8
Lead
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7439-92-1
Nickel
5.3
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:54
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:54
7440-28-0
Vanadium
49.1
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:54
7440-62-2
Zinc
17.8
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:54
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND
ug/L
1.0
1
06/25/21 16:49
06/28/21 14:56
7440-28-0 PB
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/15/21 23:22
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/15/21 23:22
107-13-1
Benzene
ND
ug/L
1.0
1
06/15/21 23:22
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/15/21 23:22
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/15/21 23:22
75-27-4
Bromoform
ND
ug/L
1.0
1
06/15/21 23:22
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/15/21 23:22
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/15/21 23:22
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/15/21 23:22
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/15/21 23:22
56-23-5 v1
Chlorobenzene
ND
ug/L
1.0
1
06/15/21 23:22
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/15/21 23:22
75-00-3
Chloroform
ND
ug/L
5.0
1
06/15/21 23:22
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/15/21 23:22
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/15/21 23:22
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/15/21 23:22
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/15/21 23:22
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/15/21 23:22
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 23:22
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 23:22
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/15/21 23:22
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/15/21 23:22
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/15/21 23:22
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 06/29/2021 02:16 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 6 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW20 Lab ID: 92544431002 Collected: 06/15/21 10:50 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:22
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:22
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:22
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:22
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:22
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:22
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/15/21 23:22
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/15/21 23:22
591-78-6
lodomethane
ND
ug/L
20.0
1
06/15/21 23:22
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/15/21 23:22
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/15/21 23:22
108-10-1
Styrene
ND
ug/L
1.0
1
06/15/21 23:22
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/15/21 23:22
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/15/21 23:22
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/15/21 23:22
127-18-4
Toluene
ND
ug/L
1.0
1
06/15/21 23:22
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/15/21 23:22
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/15/21 23:22
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/15/21 23:22
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/15/21 23:22
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/15/21 23:22
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/15/21 23:22
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/15/21 23:22
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/15/21 23:22
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/15/21 23:22
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/15/21 23:22
95-47-6
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
06/15/21 23:22
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
06/15/21 23:22
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
06/15/21 23:22
2037-26-5
Date: 06/29/2021 02:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW14
Lab ID: 92544431003
Collected:
06/15/21
12:05
Received: 06/15/21 15:31 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:57
7440-38-2
Barium
76.2
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 12:57
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 12:57
7440-43-9
Chromium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7440-48-4
Copper
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7440-50-8
Lead
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7439-92-1
Nickel
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:57
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:57
7440-28-0
Vanadium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 12:57
7440-62-2
Zinc
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 12:57
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND
ug/L
1.0
1
06/25/21 16:49
06/28/21 15:01
7440-28-0 PB
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/15/21 23:40
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/15/21 23:40
107-13-1
Benzene
ND
ug/L
1.0
1
06/15/21 23:40
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/15/21 23:40
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/15/21 23:40
75-27-4
Bromoform
ND
ug/L
1.0
1
06/15/21 23:40
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/15/21 23:40
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/15/21 23:40
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/15/21 23:40
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/15/21 23:40
56-23-5 v1
Chlorobenzene
ND
ug/L
1.0
1
06/15/21 23:40
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/15/21 23:40
75-00-3
Chloroform
ND
ug/L
5.0
1
06/15/21 23:40
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/15/21 23:40
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/15/21 23:40
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/15/21 23:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/15/21 23:40
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/15/21 23:40
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 23:40
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 23:40
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/15/21 23:40
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/15/21 23:40
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/15/21 23:40
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 06/29/2021 02:16 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 8 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW14 Lab ID: 92544431003 Collected: 06/15/21 12:05 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:40
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:40
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/15/21 23:40
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:40
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:40
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/15/21 23:40
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/15/21 23:40
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/15/21 23:40
591-78-6
lodomethane
ND
ug/L
20.0
1
06/15/21 23:40
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/15/21 23:40
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/15/21 23:40
108-10-1
Styrene
ND
ug/L
1.0
1
06/15/21 23:40
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/15/21 23:40
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/15/21 23:40
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/15/21 23:40
127-18-4
Toluene
ND
ug/L
1.0
1
06/15/21 23:40
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/15/21 23:40
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/15/21 23:40
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/15/21 23:40
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/15/21 23:40
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/15/21 23:40
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/15/21 23:40
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/15/21 23:40
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/15/21 23:40
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/15/21 23:40
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/15/21 23:40
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
06/15/21 23:40
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
06/15/21 23:40
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
06/15/21 23:40
2037-26-5
Date: 06/29/2021 02:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW14B
Lab ID: 92544431004
Collected:
06/15/21
11:50
Received: 06/15/21 15:31 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:01
7440-38-2
Barium
20.6
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:01
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:01
7440-43-9
Chromium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7440-48-4
Copper
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7440-50-8
Lead
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7439-92-1
Nickel
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:01
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:01
7440-28-0
Vanadium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:01
7440-62-2
Zinc
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:01
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND
ug/L
1.0
1
06/25/21 16:49
06/28/21 15:05
7440-28-0 PB
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/15/21 23:58
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/15/21 23:58
107-13-1
Benzene
ND
ug/L
1.0
1
06/15/21 23:58
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/15/21 23:58
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/15/21 23:58
75-27-4
Bromoform
ND
ug/L
1.0
1
06/15/21 23:58
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/15/21 23:58
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/15/21 23:58
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/15/21 23:58
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/15/21 23:58
56-23-5 v1
Chlorobenzene
ND
ug/L
1.0
1
06/15/21 23:58
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/15/21 23:58
75-00-3
Chloroform
ND
ug/L
5.0
1
06/15/21 23:58
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/15/21 23:58
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/15/21 23:58
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/15/21 23:58
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/15/21 23:58
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/15/21 23:58
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 23:58
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 23:58
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/15/21 23:58
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/15/21 23:58
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/15/21 23:58
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 06/29/2021 02:16 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 10 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW14B Lab ID: 92544431004 Collected: 06/15/21 11:50 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/29/2021 02:16 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98
%
104
%
98
%
1.0
1
06/15/21 23:58
75-35-4
1.0
1
06/15/21 23:58
156-59-2
1.0
1
06/15/21 23:58
156-60-5
1.0
1
06/15/21 23:58
78-87-5
1.0
1
06/15/21 23:58
10061-01-5
1.0
1
06/15/21 23:58
10061-02-6
1.0
1
06/15/21 23:58
100-41-4
5.0
1
06/15/21 23:58
591-78-6
20.0
1
06/15/21 23:58
74-88-4
5.0
1
06/15/21 23:58
75-09-2
5.0
1
06/15/21 23:58
108-10-1
1.0
1
06/15/21 23:58
100-42-5
1.0
1
06/15/21 23:58
630-20-6
1.0
1
06/15/21 23:58
79-34-5
1.0
1
06/15/21 23:58
127-18-4
1.0
1
06/15/21 23:58
108-88-3
1.0
1
06/15/21 23:58
71-55-6
1.0
1
06/15/21 23:58
79-00-5
1.0
1
06/15/21 23:58
79-01-6
1.0
1
06/15/21 23:58
75-69-4
1.0
1
06/15/21 23:58
96-18-4
2.0
1
06/15/21 23:58
108-05-4
1.0
1
06/15/21 23:58
75-01-4
1.0
1
06/15/21 23:58
1330-20-7
2.0
1
06/15/21 23:58
179601-23-1
1.0
1
06/15/21 23:58
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/15/21 23:58 460-00-4
06/15/21 23:58 17060-07-0
06/15/21 23:58 2037-26-5
Page 11 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW14C
Lab ID: 92544431005
Collected:
06/15/21
11:30
Received: 06/15/21 15:31 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:04
7440-38-2
Barium
71.6
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:04
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:04
7440-43-9
Chromium
5.1
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7440-48-4
Copper
19.6
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7440-50-8
Lead
5.9
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7439-92-1
Nickel
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:04
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:04
7440-28-0
Vanadium
9.9
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:04
7440-62-2
Zinc
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:04
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND
ug/L
1.0
1
06/25/21 16:49
06/28/21 15:10
7440-28-0 PB
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/16/21 00:16
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/16/21 00:16
107-13-1
Benzene
ND
ug/L
1.0
1
06/16/21 00:16
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/16/21 00:16
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/16/21 00:16
75-27-4
Bromoform
ND
ug/L
1.0
1
06/16/21 00:16
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/16/21 00:16
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/16/21 00:16
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/16/21 00:16
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/16/21 00:16
56-23-5 v1
Chlorobenzene
ND
ug/L
1.0
1
06/16/21 00:16
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/16/21 00:16
75-00-3
Chloroform
ND
ug/L
5.0
1
06/16/21 00:16
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/16/21 00:16
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/16/21 00:16
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/16/21 00:16
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/16/21 00:16
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/16/21 00:16
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 00:16
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 00:16
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/16/21 00:16
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/16/21 00:16
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/16/21 00:16
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 06/29/2021 02:16 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 12 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW14C Lab ID: 92544431005 Collected: 06/15/21 11:30 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/29/2021 02:16 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
97
%
102
%
98
%
1.0
1
06/16/21 00:16
75-35-4
1.0
1
06/16/21 00:16
156-59-2
1.0
1
06/16/21 00:16
156-60-5
1.0
1
06/16/21 00:16
78-87-5
1.0
1
06/16/21 00:16
10061-01-5
1.0
1
06/16/21 00:16
10061-02-6
1.0
1
06/16/21 00:16
100-41-4
5.0
1
06/16/21 00:16
591-78-6
20.0
1
06/16/21 00:16
74-88-4
5.0
1
06/16/21 00:16
75-09-2
5.0
1
06/16/21 00:16
108-10-1
1.0
1
06/16/21 00:16
100-42-5
1.0
1
06/16/21 00:16
630-20-6
1.0
1
06/16/21 00:16
79-34-5
1.0
1
06/16/21 00:16
127-18-4
1.0
1
06/16/21 00:16
108-88-3
1.0
1
06/16/21 00:16
71-55-6
1.0
1
06/16/21 00:16
79-00-5
1.0
1
06/16/21 00:16
79-01-6
1.0
1
06/16/21 00:16
75-69-4
1.0
1
06/16/21 00:16
96-18-4
2.0
1
06/16/21 00:16
108-05-4
1.0
1
06/16/21 00:16
75-01-4
1.0
1
06/16/21 00:16
1330-20-7
2.0
1
06/16/21 00:16
179601-23-1
1.0
1
06/16/21 00:16
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/16/21 00:16 460-00-4
06/16/21 00:16 17060-07-0
06/16/21 00:16 2037-26-5
Page 13 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW14D
Lab ID: 92544431006
Collected:
06/15/21
11:15
Received: 06/15/21 15:31 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:07
7440-38-2
Barium
61.8
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:07
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:07
7440-43-9
Chromium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7440-48-4
Copper
6.0
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7440-50-8
Lead
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7439-92-1
Nickel
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:07
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:07
7440-28-0
Vanadium
6.6
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:07
7440-62-2
Zinc
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:07
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND
ug/L
1.0
1
06/25/21 16:49
06/28/21 15:15
7440-28-0 PB
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/16/21 00:34
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/16/21 00:34
107-13-1
Benzene
ND
ug/L
1.0
1
06/16/21 00:34
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/16/21 00:34
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/16/21 00:34
75-27-4
Bromoform
ND
ug/L
1.0
1
06/16/21 00:34
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/16/21 00:34
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/16/21 00:34
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/16/21 00:34
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/16/21 00:34
56-23-5 v1
Chlorobenzene
ND
ug/L
1.0
1
06/16/21 00:34
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/16/21 00:34
75-00-3
Chloroform
ND
ug/L
5.0
1
06/16/21 00:34
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/16/21 00:34
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/16/21 00:34
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/16/21 00:34
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/16/21 00:34
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/16/21 00:34
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 00:34
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 00:34
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/16/21 00:34
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/16/21 00:34
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/16/21 00:34
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 06/29/2021 02:16 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 14 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: 6001-HBW14D Lab ID: 92544431006 Collected: 06/15/21 11:15 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/29/2021 02:16 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
97
%
104
%
98
%
1.0
1
06/16/21 00:34
75-35-4
1.0
1
06/16/21 00:34
156-59-2
1.0
1
06/16/21 00:34
156-60-5
1.0
1
06/16/21 00:34
78-87-5
1.0
1
06/16/21 00:34
10061-01-5
1.0
1
06/16/21 00:34
10061-02-6
1.0
1
06/16/21 00:34
100-41-4
5.0
1
06/16/21 00:34
591-78-6
20.0
1
06/16/21 00:34
74-88-4
5.0
1
06/16/21 00:34
75-09-2
5.0
1
06/16/21 00:34
108-10-1
1.0
1
06/16/21 00:34
100-42-5
1.0
1
06/16/21 00:34
630-20-6
1.0
1
06/16/21 00:34
79-34-5
1.0
1
06/16/21 00:34
127-18-4
1.0
1
06/16/21 00:34
108-88-3
1.0
1
06/16/21 00:34
71-55-6
1.0
1
06/16/21 00:34
79-00-5
1.0
1
06/16/21 00:34
79-01-6
1.0
1
06/16/21 00:34
75-69-4
1.0
1
06/16/21 00:34
96-18-4
2.0
1
06/16/21 00:34
108-05-4
1.0
1
06/16/21 00:34
75-01-4
1.0
1
06/16/21 00:34
1330-20-7
2.0
1
06/16/21 00:34
179601-23-1
1.0
1
06/16/21 00:34
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/16/21 00:34 460-00-4
06/16/21 00:34 17060-07-0
06/16/21 00:34 2037-26-5
Page 15 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: Trip Blank
Lab ID: 92544431007 Collected:
06/15/21
09:53
Received: 06/15/21 15:31 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/15/21 22:45
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/15/21 22:45
107-13-1
Benzene
ND
ug/L
1.0
1
06/15/21 22:45
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/15/21 22:45
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/15/21 22:45
75-27-4
Bromoform
ND
ug/L
1.0
1
06/15/21 22:45
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/15/21 22:45
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/15/21 22:45
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/15/21 22:45
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/15/21 22:45
56-23-5 v1
Chlorobenzene
ND
ug/L
1.0
1
06/15/21 22:45
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/15/21 22:45
75-00-3
Chloroform
ND
ug/L
5.0
1
06/15/21 22:45
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/15/21 22:45
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/15/21 22:45
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/15/21 22:45
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/15/21 22:45
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/15/21 22:45
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 22:45
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/15/21 22:45
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/15/21 22:45
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/15/21 22:45
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/15/21 22:45
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
06/15/21 22:45
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/15/21 22:45
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/15/21 22:45
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/15/21 22:45
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/15/21 22:45
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/15/21 22:45
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/15/21 22:45
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/15/21 22:45
591-78-6
lodomethane
ND
ug/L
20.0
1
06/15/21 22:45
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/15/21 22:45
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/15/21 22:45
108-10-1
Styrene
ND
ug/L
1.0
1
06/15/21 22:45
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/15/21 22:45
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/15/21 22:45
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/15/21 22:45
127-18-4
Toluene
ND
ug/L
1.0
1
06/15/21 22:45
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/15/21 22:45
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/15/21 22:45
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/15/21 22:45
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/15/21 22:45
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/15/21 22:45
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/15/21 22:45
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/15/21 22:45
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Sample: Trip Blank
Parameters
Lab ID: 92544431007 Collected: 06/15/21 09:53
Results Units Report Limit DF
Received: 06/15/21 15:31 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
06/15/21 22:45
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
06/15/21 22:45
179601-23-1
o-Xylene
ND ug/L
1.0
1
06/15/21 22:45
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95 %
70-130
1
06/15/21 22:45
460-00-4
1,2-Dichloroethane-d4 (S)
101 %
70-130
1
06/15/21 22:45
17060-07-0
Toluene-d8 (S)
97 %
70-130
1
06/15/21 22:45
2037-26-5
Date: 06/29/2021 02:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
QC Batch: 629888 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92544431001, 92544431002, 92544431003, 92544431004, 92544431005, 92544431006
METHOD BLANK: 3310072 Matrix: Water
Associated Lab Samples: 92544431001, 92544431002, 92544431003, 92544431004, 92544431005, 92544431006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
06/28/2112:22
Arsenic
ug/L
ND
10.0
06/28/2112:22
Barium
ug/L
ND
5.0
06/28/2112:22
Beryllium
ug/L
ND
1.0
06/28/2112:22
Cadmium
ug/L
ND
1.0
06/28/2112:22
Chromium
ug/L
ND
5.0
06/28/2112:22
Cobalt
ug/L
ND
5.0
06/28/2112:22
Copper
ug/L
ND
5.0
06/28/2112:22
Lead
ug/L
ND
5.0
06/28/2112:22
Nickel
ug/L
ND
5.0
06/28/2112:22
Selenium
ug/L
ND
10.0
06/28/2112:22
Silver
ug/L
ND
5.0
06/28/2112:22
Thallium
ug/L
ND
10.0
06/28/2112:22
Vanadium
ug/L
ND
5.0
06/28/2112:22
Zinc
ug/L
ND
10.0
06/28/2112:22
LABORATORY CONTROL SAMPLE:
Parameter
3310073
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
480
96
80-120
Arsenic
ug/L
500
466
93
80-120
Barium
ug/L
500
478
96
80-120
Beryllium
ug/L
500
487
97
80-120
Cadmium
ug/L
500
477
95
80-120
Chromium
ug/L
500
463
93
80-120
Cobalt
ug/L
500
465
93
80-120
Copper
ug/L
500
493
99
80-120
Lead
ug/L
500
474
95
80-120
Nickel
ug/L
500
476
95
80-120
Selenium
ug/L
500
466
93
80-120
Silver
ug/L
250
236
94
80-120
Thallium
ug/L
500
470
94
80-120
Vanadium
ug/L
500
470
94
80-120
Zinc
ug/L
500
458
92
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Harrisburg Rd Landfill (Permit
92544431
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3310074
3310075
MS
MSD
92544431001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
489
494
98
99
75-125
1
Arsenic
ug/L
ND
500
500
483
491
96
98
75-125
2
Barium
ug/L
92.3
500
500
578
582
97
98
75-125
1
Beryllium
ug/L
ND
500
500
494
499
99
100
75-125
1
Cadmium
ug/L
ND
500
500
501
507
100
101
75-125
1
Chromium
ug/L
ND
500
500
483
500
96
99
75-125
3
Cobalt
ug/L
126
500
500
602
612
95
97
75-125
2
Copper
ug/L
49.8
500
500
557
568
102
104
75-125
2
Lead
ug/L
ND
500
500
490
498
97
99
75-125
2
Nickel
ug/L
15.0
500
500
501
509
97
99
75-125
2
Selenium
ug/L
ND
500
500
510
515
102
103
75-125
1
Silver
ug/L
ND
250
250
245
248
98
99
75-125
1
Thallium
ug/L
ND
500
500
478
486
96
97
75-125
2
Vanadium
ug/L
10.8
500
500
490
504
96
99
75-125
3
Zinc
ug/L
ND
500
500
489
502
96
99
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
QC Batch: 629483 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92544431001, 92544431002, 92544431003, 92544431004, 92544431005, 92544431006
METHOD BLANK: 3308296
Matrix:
Water
Associated Lab Samples: 92544431001, 92544431002, 92544431003, 92544431004, 92544431005, 92544431006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
06/28/2112:57 PB
LABORATORY CONTROL SAMPLE:
3308297
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
24.2
97 80-120 PB
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3308298 3308299
MS MSD
92544431001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 24.1 24.0 96 96 75-125 0 PB
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
QC Batch: 627330 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92544431001, 92544431002, 92544431003, 92544431004, 92544431005, 92544431006, 92544431007
METHOD BLANK: 3298152 Matrix: Water
Associated Lab Samples: 92544431001, 92544431002, 92544431003, 92544431004, 92544431005, 92544431006, 92544431007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
06/15/21 22:09
1,1,1-Trichloroethane
ug/L
ND
1.0
06/15/21 22:09
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/15/21 22:09
1,1,2-Trichloroethane
ug/L
ND
1.0
06/15/21 22:09
1,1-Dichloroethane
ug/L
ND
1.0
06/15/21 22:09
1,1-Dichloroethene
ug/L
ND
1.0
06/15/21 22:09
1,2,3-Trichloropropane
ug/L
ND
1.0
06/15/21 22:09
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
06/15/21 22:09
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
06/15/21 22:09
1,2-Dichlorobenzene
ug/L
ND
1.0
06/15/21 22:09
1,2-Dichloroethane
ug/L
ND
1.0
06/15/21 22:09
1,2-Dichloropropane
ug/L
ND
1.0
06/15/21 22:09
1,4-Dichlorobenzene
ug/L
ND
1.0
06/15/21 22:09
2-Butanone (MEK)
ug/L
ND
5.0
06/15/21 22:09
2-Hexanone
ug/L
ND
5.0
06/15/21 22:09
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
06/15/21 22:09
Acetone
ug/L
ND
25.0
06/15/21 22:09
Acrylonitrile
ug/L
ND
10.0
06/15/21 22:09
Benzene
ug/L
ND
1.0
06/15/21 22:09
Bromochloromethane
ug/L
ND
1.0
06/15/21 22:09
Bromodichloromethane
ug/L
ND
1.0
06/15/21 22:09
Bromoform
ug/L
ND
1.0
06/15/21 22:09
Bromomethane
ug/L
ND
2.0
06/15/21 22:09
Carbon disulfide
ug/L
ND
2.0
06/15/21 22:09
Carbon tetrachloride
ug/L
ND
1.0
06/15/21 22:09
Chlorobenzene
ug/L
ND
1.0
06/15/21 22:09
Chloroethane
ug/L
ND
1.0
06/15/21 22:09
Chloroform
ug/L
ND
5.0
06/15/21 22:09
Chloromethane
ug/L
ND
1.0
06/15/21 22:09
cis-1,2-Dichloroethene
ug/L
ND
1.0
06/15/21 22:09
cis-1,3-Dichloropropene
ug/L
ND
1.0
06/15/21 22:09
Dibromochloromethane
ug/L
ND
1.0
06/15/21 22:09
Dibromomethane
ug/L
ND
1.0
06/15/21 22:09
Ethylbenzene
ug/L
ND
1.0
06/15/21 22:09
lodomethane
ug/L
ND
20.0
06/15/21 22:09
m&p-Xylene
ug/L
ND
2.0
06/15/21 22:09
Methylene Chloride
ug/L
ND
5.0
06/15/21 22:09
o-Xylene
ug/L
ND
1.0
06/15/21 22:09
Styrene
ug/L
ND
1.0
06/15/21 22:09
Tetrachloroethene
ug/L
ND
1.0
06/15/21 22:09
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
METHOD BLANK: 3298152 Matrix: Water
Associated Lab Samples: 92544431001, 92544431002, 92544431003, 92544431004, 92544431005, 92544431006, 92544431007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
06/15/21 22:09
trans-1,2-Dichloroethene
ug/L
ND
1.0
06/15/21 22:09
trans- 1,3-Dichloropropene
ug/L
ND
1.0
06/15/21 22:09
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
06/15/21 22:09
Trichloroethene
ug/L
ND
1.0
06/15/21 22:09
Trichlorofluoromethane
ug/L
ND
1.0
06/15/21 22:09
Vinyl acetate
ug/L
ND
2.0
06/15/21 22:09
Vinyl chloride
ug/L
ND
1.0
06/15/21 22:09
Xylene (Total)
ug/L
ND
1.0
06/15/21 22:09
1,2-Dichloroethane-d4 (S)
%
99
70-130
06/15/21 22:09
4-Bromofluorobenzene (S)
%
98
70-130
06/15/21 22:09
Toluene-d8 (S)
%
99
70-130
06/15/21 22:09
LABORATORY CONTROL SAMPLE:
Parameter
3298153
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.0
106
70-130
1,1,1-Trichloroethane
ug/L
50
54.5
109
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
46.0
92
70-130
1,1,2-Trichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethane
ug/L
50
44.5
89
70-130
1,1-Dichloroethene
ug/L
50
49.8
100
70-132
1,2,3-Trichloropropane
ug/L
50
46.9
94
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.1
106
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.4
101
70-130
1,2-Dichlorobenzene
ug/L
50
46.7
93
70-130
1,2-Dichloroethane
ug/L
50
50.8
102
70-130
1,2-Dichloropropane
ug/L
50
47.0
94
70-130
1,4-Dichlorobenzene
ug/L
50
49.4
99
70-130
2-Butanone (MEK)
ug/L
100
89.7
90
70-133
2-Hexanone
ug/L
100
93.8
94
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
94.4
94
70-130
Acetone
ug/L
100
98.9
99
70-144
Acrylonitrile
ug/L
250
214
86
70-130
Benzene
ug/L
50
48.6
97
70-130
Bromochloromethane
ug/L
50
49.9
100
70-130
Bromodichloromethane
ug/L
50
52.9
106
70-130
Bromoform
ug/L
50
53.3
107
70-131
Bromomethane
ug/L
50
49.6
99
30-177
Carbon disulfide
ug/L
50
49.4
99
70-133
Carbon tetrachloride
ug/L
50
58.8
118
70-130 v1
Chlorobenzene
ug/L
50
50.9
102
70-130
Chloroethane
ug/L
50
53.8
108
46-131
Chloroform
ug/L
50
50.0
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 29

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QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
LABORATORY CONTROL SAMPLE:
Parameter
3298153
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
44.0
88
49-130
46.1
92
70-130
52.2
104
70-130
53.0
106
70-130
55.3
111
70-130
49.3
99
70-130
108
108
47-140
98.7
99
70-130
42.6
85
68-130
49.4
99
70-130
50.5
101
70-130
51.4
103
70-130
50.1
100
70-130
47.0
94
70-130
54.5
109
70-130
78.6
157
25-200
52.0
104
70-130
57.5
115
61-130
97.9
98
70-140
49.3
99
59-142
148
99
70-130
99
70-130
99
70-130
99
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3298154
MS
92544431006 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3298155
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.9
23.9
109
120
70-135
9
1,1,1-Trichloroethane
ug/L
ND
20
20
21.5
24.4
107
122
70-148
13
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.0
20.9
95
105
70-131
10
1,1,2-Trichloroethane
ug/L
ND
20
20
19.7
21.1
99
105
70-136
7
1,1-Dichloroethane
ug/L
ND
20
20
20.1
22.2
101
111
70-147
10
1,1-Dichloroethene
ug/L
ND
20
20
22.2
24.6
111
123
70-158
10
1,2,3-Trichloropropane
ug/L
ND
20
20
19.5
20.7
97
104
67-137
6
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
18.2
19.7
91
99
69-136
8
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.2
22.0
106
110
70-137
4
1,2-Dichlorobenzene
ug/L
ND
20
20
20.0
22.3
100
111
70-133
11
1,2-Dichloroethane
ug/L
ND
20
20
21.0
23.4
105
117
67-138
11
1,2-Dichloropropane
ug/L
ND
20
20
19.5
21.1
98
105
70-138
7
1,4-Dichlorobenzene
ug/L
ND
20
20
20.0
23.1
100
116
70-133
14
2-Butanone (MEK)
ug/L
ND
40
40
33.5
37.6
84
94
61-147
12
2-Hexanone
ug/L
ND
40
40
37.4
39.9
94
100
67-139
6
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
36.1
39.4
90
98
67-136
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3298154
MS
92544431006 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3298155
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
37.1
41.2
93
103
55-159
10
Acrylonitrile
ug/L
ND
100
100
90.4
99.1
90
99
68-140
9
Benzene
ug/L
ND
20
20
19.8
21.1
99
105
67-150
6
Bromochloromethane
ug/L
ND
20
20
20.2
23.1
101
115
70-146
14
Bromodichloromethane
ug/L
ND
20
20
21.5
23.4
108
117
70-138
8
Bromoform
ug/L
ND
20
20
21.3
21.8
106
109
57-138
3
Bromomethane
ug/L
ND
20
20
25.9
31.4
129
157
10-200
19
Carbon disulfide
ug/L
ND
20
20
21.5
24.4
108
122
70-152
13
Carbon tetrachloride
ug/L
ND
20
20
23.9
25.8
119
129
70-147
8
Chlorobenzene
ug/L
ND
20
20
20.8
22.7
104
113
70-137
9
Chloroethane
ug/L
ND
20
20
27.3
30.0
136
150
51-166
10 v1
Chloroform
ug/L
ND
20
20
20.9
23.4
104
117
70-144
11
Chloromethane
ug/L
ND
20
20
18.2
19.4
91
97
24-161
6
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
22.3
101
111
67-148
10
cis-1,3-Dichloropropene
ug/L
ND
20
20
19.9
21.5
99
108
70-142
8
Dibromochloromethane
ug/L
ND
20
20
21.3
22.6
106
113
68-138
6
Dibromomethane
ug/L
ND
20
20
21.3
22.3
107
111
70-134
5
Ethylbenzene
ug/L
ND
20
20
21.8
22.8
109
114
68-143
4
lodomethane
ug/L
ND
40
40
56.5
62.1
141
155
20-161
9
m&p-Xylene
ug/L
ND
40
40
44.4
47.7
111
119
53-157
7
Methylene Chloride
ug/L
ND
20
20
19.2
21.4
96
107
64-148
11
o-Xylene
ug/L
ND
20
20
21.3
22.0
106
110
68-143
3
Styrene
ug/L
ND
20
20
15.9
18.8
79
94
70-136
17
Tetrachloroethene
ug/L
ND
20
20
22.0
23.1
110
115
70-139
5
Toluene
ug/L
ND
20
20
19.0
20.4
95
102
47-157
7
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.3
23.4
107
117
70-149
9
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.1
22.3
106
111
70-138
5
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
17.3
18.8
87
94
31-145
8
Trichloroethene
ug/L
ND
20
20
21.0
23.7
105
118
70-149
12
Trichlorofluoromethane
ug/L
ND
20
20
23.0
25.6
115
128
61-154
11
Vinyl acetate
ug/L
ND
40
40
36.1
40.5
90
101
48-156
12
Vinyl chloride
ug/L
ND
20
20
20.3
22.8
102
114
55-172
11
Xylene (Total)
ug/L
ND
60
60
65.7
69.7
110
116
66-145
6
1,2-Dichloroethane-d4 (S)
%
108
104
70-130
4-Bromofluorobenzene (S)
%
101
102
70-130
Toluene-d8(S)
%
99
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
BATCH QUALIFIERS
Batch: 629782
[PB] Sample field preservation does not meet EPA or method recommendations for this analysis.
ANALYTE QUALIFIERS
PB Sample field preservation does not meet EPA or method recommendations for this analysis.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
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Date: 06/29/2021 02:16 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 29

leAnalyiical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544431
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92544431001
6001-HBW28
EPA 3010A
629888
EPA6010D
629905
92544431002
6001-HBW20
EPA 3010A
629888
EPA6010D
629905
92544431003
6001-HBW14
EPA 3010A
629888
EPA6010D
629905
92544431004
6001-HBW14B
EPA 3010A
629888
EPA6010D
629905
92544431005
6001-HBW14C
EPA 3010A
629888
EPA6010D
629905
92544431006
6001-HBW14D
EPA 3010A
629888
EPA6010D
629905
92544431001
6001-HBW28
EPA 3010A
629483
EPA6020B
629782
92544431002
6001-HBW20
EPA 3010A
629483
EPA6020B
629782
92544431003
6001-HBW14
EPA 3010A
629483
EPA6020B
629782
92544431004
6001-HBW14B
EPA 3010A
629483
EPA6020B
629782
92544431005
6001-HBW14C
EPA 3010A
629483
EPA6020B
629782
92544431006
6001-HBW14D
EPA 3010A
629483
EPA6020B
629782
92544431001
6001-HBW28
EPA 8260D
627330
92544431002
6001-HBW20
EPA 8260D
627330
92544431003
6001-HBW14
EPA 8260D
627330
92544431004
6001-HBW14B
EPA 8260D
627330
92544431005
6001-HBW14C
EPA 8260D
627330
92544431006
6001-HBW14D
EPA 8260D
627330
92544431007
Trip Blank
EPA 8260D
627330
Date: 06/29/2021 02:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 26 of 29

Page Sample Condition Upon Receipt(SCUR) Pa g
r?CmmlytiCci1 � Document No.: Issuing Authority:
f-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvilie `/ Raleigh❑ Mechanicsville❑ Atianta❑ Kernersville❑
sampleCondition Client Name; y Project #: WOE 92544431
p.
Other:
Commercial Pace ❑ 92444431
Custody Seal Present? []yes RNo Seals intact? Dyes ENO
0atellnitials•Aersarr•i<xamining•&ontent
p [aBubble Ba s ❑ other Biological Tissue Frozen?
Packing Material: 08ubble Wra g []None Yes []No QN/A
Thermometer: Wet []Blue ❑None
IR Gun ID: 92TO64 Type of Ice:
® Correction factor:
Cooler Temp: � f � Add/Subtract (°C) _ Temp should he above freezing to 6°C
❑samples out of temp criteria. Samples on ice, coaling process
Cooler Temp Corrected {'Cj:
SQL has begun
USDA Regulated Soil ( [5N/A, water sample) a foreign
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check mapsj7 including
nclud ngDid iHawa(iies land Puenate rto Rico)) ]Yes source (internationally,
❑Yes ❑No Comments/Discrepancy:
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (02 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved anal sis: Samples Field Filtered?
Sample Labels Match COC?
s ❑No L1N/A
s []No ❑N/A
s WNo ❑N/A
F76d. 1—IN/A
lilYes []NO ❑N/A 16-
Yes ❑No [ N/A
Yes ❑No ❑N/A
7-
❑Yes []NO N/A
8.
(Yes [:]NO []N/A
9.
\.J
Headspace iri VOA Vials (>5-6mm)? c❑/Yes ®No N/A 10.
L 4 r Yes ❑Na ❑NIA 11.
Trip Blank Present?
.I
Trip Blank Custody Seals Present? L es Na N/A
Field Data Required? ❑Yes []No
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split Containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date:
Page 27 of 29

uacurnenL lVdMV.
�f d` CB f181Y1C-rT~ Document No.: Issuing Authority:
r . F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechiorination is project I# ` `O# : Q2544431
verified and within the acceptance range for preservation W :/
PM: MWE Due Date: 06/29/21
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT- 92-M CCK CO
* *BoStom..half af_box-is to list_number_of bottles_
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Timepreservation Amount added e
aof rvative Lat q
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this Farm walk he sent to the Korth Carolina DEHNR Certification Office {i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 28 of 29

0
l'
TEMP in C
Received on
Ice
(YIN)
e5to y
Sealed
Cooler
YIL�
Samples
Intact
(YIN)
ITEM #
1 �
m
n
0
0
0
0
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Fco
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#
A M
SAMPLETYPE (G=GRAB C=COMP)
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°
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°
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=
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°
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6
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ro
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a
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s
Page 29 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 29, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on June 15, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92544439001 6001-HB2006
EPA 601OD
IDS
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
52
PASI-C
92544439002 6001-HB2008
EPA 601OD
IDS
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
52
PASI-C
92544439003 6001-HB2010
EPA 601OD
IDS
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Sample: 6001-HB2006 Lab ID: 92544439001 Collected: 06/15/21 13:25 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:10
7440-38-2
Barium
33.1
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:10
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:10
7440-43-9
Chromium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7440-48-4
Copper
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7440-50-8
Lead
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7439-92-1
Nickel
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:10
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:10
7440-28-0
Vanadium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:10
7440-62-2
Zinc
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:10
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
06/27/2117:52
06/28/2111:41
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/16/21 14:43
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/16/21 14:43
107-13-1
Benzene
ND
ug/L
1.0
1
06/16/21 14:43
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/16/21 14:43
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/16/21 14:43
75-27-4
Bromoform
ND
ug/L
1.0
1
06/16/21 14:43
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/16/21 14:43
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/16/21 14:43
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/16/21 14:43
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/16/21 14:43
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/16/21 14:43
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/16/21 14:43
75-00-3
Chloroform
ND
ug/L
5.0
1
06/16/21 14:43
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/16/21 14:43
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/16/21 14:43
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/16/21 14:43
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/16/21 14:43
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/16/21 14:43
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 14:43
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 14:43
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/16/21 14:43
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/16/21 14:43
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/16/21 14:43
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Sample: 6001-HB2006 Lab ID: 92544439001 Collected: 06/15/21 13:25 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/16/21 14:43
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/16/21 14:43
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/16/21 14:43
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/16/21 14:43
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/16/21 14:43
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/16/21 14:43
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/16/21 14:43
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/16/21 14:43
591-78-6
lodomethane
ND
ug/L
20.0
1
06/16/21 14:43
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/16/21 14:43
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/16/21 14:43
108-10-1
Styrene
ND
ug/L
1.0
1
06/16/21 14:43
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/16/21 14:43
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/16/21 14:43
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/16/21 14:43
127-18-4
Toluene
ND
ug/L
1.0
1
06/16/21 14:43
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/16/21 14:43
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/16/21 14:43
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/16/21 14:43
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/16/21 14:43
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/16/21 14:43
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/16/21 14:43
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/16/21 14:43
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/16/21 14:43
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/16/21 14:43
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/16/21 14:43
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
06/16/21 14:43
460-00-4
1,2-Dichloroethane-d4 (S)
110
%
70-130
1
06/16/21 14:43
17060-07-0
Toluene-d8 (S)
109
%
70-130
1
06/16/21 14:43
2037-26-5
Date: 06/29/2021 02:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Sample: 6001-HB2008 Lab ID: 92544439002 Collected: 06/15/21 13:40 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:14
7440-38-2
Barium
20.5
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:14
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:14
7440-43-9
Chromium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7440-48-4
Copper
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7440-50-8
Lead
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7439-92-1
Nickel
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:14
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:14
7440-28-0
Vanadium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:14
7440-62-2
Zinc
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:14
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
06/27/2117:52
06/28/2113:32
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/16/21 16:47
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/16/21 16:47
107-13-1
Benzene
ND
ug/L
1.0
1
06/16/21 16:47
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/16/21 16:47
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/16/21 16:47
75-27-4
Bromoform
ND
ug/L
1.0
1
06/16/21 16:47
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/16/21 16:47
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/16/21 16:47
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/16/21 16:47
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/16/21 16:47
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/16/21 16:47
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/16/21 16:47
75-00-3
Chloroform
ND
ug/L
5.0
1
06/16/21 16:47
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/16/21 16:47
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/16/21 16:47
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/16/21 16:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/16/21 16:47
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/16/21 16:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 16:47
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 16:47
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/16/21 16:47
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/16/21 16:47
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/16/21 16:47
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Sample: 6001-HB2008 Lab ID: 92544439002 Collected: 06/15/21 13:40 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/16/21 16:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/16/21 16:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/16/21 16:47
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/16/21 16:47
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/16/21 16:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/16/21 16:47
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/16/21 16:47
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/16/21 16:47
591-78-6
lodomethane
ND
ug/L
20.0
1
06/16/21 16:47
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/16/21 16:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/16/21 16:47
108-10-1
Styrene
ND
ug/L
1.0
1
06/16/21 16:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/16/21 16:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/16/21 16:47
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/16/21 16:47
127-18-4
Toluene
ND
ug/L
1.0
1
06/16/21 16:47
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/16/21 16:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/16/21 16:47
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/16/21 16:47
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/16/21 16:47
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/16/21 16:47
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/16/21 16:47
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/16/21 16:47
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/16/21 16:47
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/16/21 16:47
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/16/21 16:47
95-47-6
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
06/16/21 16:47
460-00-4
1,2-Dichloroethane-d4 (S)
109
%
70-130
1
06/16/21 16:47
17060-07-0
Toluene-d8 (S)
111
%
70-130
1
06/16/21 16:47
2037-26-5
Date: 06/29/2021 02:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Sample: 6001-HB2010 Lab ID: 92544439003 Collected: 06/15/21 12:15 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:17
7440-38-2
Barium
41.5
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:17
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/27/21 17:17
06/28/21 13:17
7440-43-9
Chromium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7440-48-4
Copper
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7440-50-8
Lead
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7439-92-1
Nickel
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7440-02-0
Selenium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:17
7782-49-2
Silver
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7440-22-4
Thallium
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:17
7440-28-0
Vanadium
ND
ug/L
5.0
1
06/27/21 17:17
06/28/21 13:17
7440-62-2
Zinc
ND
ug/L
10.0
1
06/27/21 17:17
06/28/21 13:17
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
06/27/2117:52
06/28/2113:36
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/16/21 17:04
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/16/21 17:04
107-13-1
Benzene
ND
ug/L
1.0
1
06/16/21 17:04
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/16/21 17:04
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/16/21 17:04
75-27-4
Bromoform
ND
ug/L
1.0
1
06/16/21 17:04
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/16/21 17:04
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/16/21 17:04
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/16/21 17:04
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/16/21 17:04
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/16/21 17:04
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/16/21 17:04
75-00-3
Chloroform
ND
ug/L
5.0
1
06/16/21 17:04
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/16/21 17:04
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/16/21 17:04
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/16/21 17:04
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/16/21 17:04
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/16/21 17:04
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 17:04
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/16/21 17:04
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/16/21 17:04
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/16/21 17:04
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/16/21 17:04
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Sample: 6001-HB2010 Lab ID: 92544439003 Collected: 06/15/21 12:15 Received: 06/15/21 15:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/16/21 17:04
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/16/21 17:04
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/16/21 17:04
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/16/21 17:04
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/16/21 17:04
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/16/21 17:04
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/16/21 17:04
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/16/21 17:04
591-78-6
lodomethane
ND
ug/L
20.0
1
06/16/21 17:04
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/16/21 17:04
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/16/21 17:04
108-10-1
Styrene
ND
ug/L
1.0
1
06/16/21 17:04
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/16/21 17:04
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/16/21 17:04
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/16/21 17:04
127-18-4
Toluene
ND
ug/L
1.0
1
06/16/21 17:04
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/16/21 17:04
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/16/21 17:04
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/16/21 17:04
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/16/21 17:04
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/16/21 17:04
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/16/21 17:04
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/16/21 17:04
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/16/21 17:04
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/16/21 17:04
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/16/21 17:04
95-47-6
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
06/16/21 17:04
460-00-4
1,2-Dichloroethane-d4 (S)
112
%
70-130
1
06/16/21 17:04
17060-07-0
Toluene-d8 (S)
107
%
70-130
1
06/16/21 17:04
2037-26-5
Date: 06/29/2021 02:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
QC Batch: 629888 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92544439001, 92544439002, 92544439003
METHOD BLANK: 3310072 Matrix: Water
Associated Lab Samples: 92544439001, 92544439002, 92544439003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
06/28/2112:22
10.0
06/28/2112:22
5.0
06/28/2112:22
1.0
06/28/2112:22
1.0
06/28/2112:22
5.0
06/28/2112:22
5.0
06/28/2112:22
5.0
06/28/2112:22
5.0
06/28/2112:22
5.0
06/28/2112:22
10.0
06/28/2112:22
5.0
06/28/2112:22
10.0
06/28/2112:22
5.0
06/28/2112:22
10.0
06/28/2112:22
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3310073
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
480
96
80-120
Arsenic
ug/L
500
466
93
80-120
Barium
ug/L
500
478
96
80-120
Beryllium
ug/L
500
487
97
80-120
Cadmium
ug/L
500
477
95
80-120
Chromium
ug/L
500
463
93
80-120
Cobalt
ug/L
500
465
93
80-120
Copper
ug/L
500
493
99
80-120
Lead
ug/L
500
474
95
80-120
Nickel
ug/L
500
476
95
80-120
Selenium
ug/L
500
466
93
80-120
Silver
ug/L
250
236
94
80-120
Thallium
ug/L
500
470
94
80-120
Vanadium
ug/L
500
470
94
80-120
Zinc
ug/L
500
458
92
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Harrisburg Rd Landfill (Permit
92544439
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3310074
3310075
MS
MSD
92544431001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
489
494
98
99
75-125
1
Arsenic
ug/L
ND
500
500
483
491
96
98
75-125
2
Barium
ug/L
92.3
500
500
578
582
97
98
75-125
1
Beryllium
ug/L
ND
500
500
494
499
99
100
75-125
1
Cadmium
ug/L
ND
500
500
501
507
100
101
75-125
1
Chromium
ug/L
ND
500
500
483
500
96
99
75-125
3
Cobalt
ug/L
126
500
500
602
612
95
97
75-125
2
Copper
ug/L
49.8
500
500
557
568
102
104
75-125
2
Lead
ug/L
ND
500
500
490
498
97
99
75-125
2
Nickel
ug/L
15.0
500
500
501
509
97
99
75-125
2
Selenium
ug/L
ND
500
500
510
515
102
103
75-125
1
Silver
ug/L
ND
250
250
245
248
98
99
75-125
1
Thallium
ug/L
ND
500
500
478
486
96
97
75-125
2
Vanadium
ug/L
10.8
500
500
490
504
96
99
75-125
3
Zinc
ug/L
ND
500
500
489
502
96
99
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
QC Batch: 629890 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92544439001, 92544439002, 92544439003
METHOD BLANK: 3310079
Matrix:
Water
Associated Lab Samples: 92544439001, 92544439002, 92544439003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
06/28/2111:33
LABORATORY CONTROL SAMPLE:
3310080
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
24.3
97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3310081 3310082
MS MSD
92544439001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 24.2 24.2 97 97 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
QC Batch: 627470 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92544439001, 92544439002, 92544439003
METHOD BLANK: 3298650 Matrix:
Associated Lab Samples: 92544439001, 92544439002, 92544439003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
06/16/21 11:48
1,1,1-Trichloroethane
ug/L
ND
1.0
06/16/21 11:48
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/16/21 11:48
1,1,2-Trichloroethane
ug/L
ND
1.0
06/16/21 11:48
1,1-Dichloroethane
ug/L
ND
1.0
06/16/21 11:48
1,1-Dichloroethene
ug/L
ND
1.0
06/16/21 11:48
1,2,3-Trichloropropane
ug/L
ND
1.0
06/16/21 11:48
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
06/16/21 11:48
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
06/16/21 11:48
1,2-Dichlorobenzene
ug/L
ND
1.0
06/16/21 11:48
1,2-Dichloroethane
ug/L
ND
1.0
06/16/21 11:48
1,2-Dichloropropane
ug/L
ND
1.0
06/16/21 11:48
1,4-Dichlorobenzene
ug/L
ND
1.0
06/16/21 11:48
2-Butanone (MEK)
ug/L
ND
5.0
06/16/21 11:48
2-Hexanone
ug/L
ND
5.0
06/16/21 11:48
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
06/16/21 11:48
Acetone
ug/L
ND
25.0
06/16/21 11:48
Acrylonitrile
ug/L
ND
10.0
06/16/21 11:48
Benzene
ug/L
ND
1.0
06/16/21 11:48
Bromochloromethane
ug/L
ND
1.0
06/16/21 11:48
Bromodichloromethane
ug/L
ND
1.0
06/16/21 11:48
Bromoform
ug/L
ND
1.0
06/16/21 11:48
Bromomethane
ug/L
ND
2.0
06/16/21 11:48
Carbon disulfide
ug/L
ND
2.0
06/16/21 11:48
Carbon tetrachloride
ug/L
ND
1.0
06/16/21 11:48
Chlorobenzene
ug/L
ND
1.0
06/16/21 11:48
Chloroethane
ug/L
ND
1.0
06/16/21 11:48
Chloroform
ug/L
ND
5.0
06/16/21 11:48
Chloromethane
ug/L
ND
1.0
06/16/21 11:48
cis-1,2-Dichloroethene
ug/L
ND
1.0
06/16/21 11:48
cis-1,3-Dichloropropene
ug/L
ND
1.0
06/16/21 11:48
Dibromochloromethane
ug/L
ND
1.0
06/16/21 11:48
Dibromomethane
ug/L
ND
1.0
06/16/21 11:48
Ethylbenzene
ug/L
ND
1.0
06/16/21 11:48
lodomethane
ug/L
ND
20.0
06/16/21 11:48
m&p-Xylene
ug/L
ND
2.0
06/16/21 11:48
Methylene Chloride
ug/L
ND
5.0
06/16/21 11:48
o-Xylene
ug/L
ND
1.0
06/16/21 11:48
Styrene
ug/L
ND
1.0
06/16/21 11:48
Tetrachloroethene
ug/L
ND
1.0
06/16/21 11:48
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
METHOD BLANK: 3298650 Matrix:
Associated Lab Samples: 92544439001, 92544439002, 92544439003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
06/16/21 11:48
trans-1,2-Dichloroethene
ug/L
ND
1.0
06/16/21 11:48
trans- 1,3-Dichloropropene
ug/L
ND
1.0
06/16/21 11:48
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
06/16/21 11:48
Trichloroethene
ug/L
ND
1.0
06/16/21 11:48
Trichlorofluoromethane
ug/L
ND
1.0
06/16/21 11:48
Vinyl acetate
ug/L
ND
2.0
06/16/21 11:48
Vinyl chloride
ug/L
ND
1.0
06/16/21 11:48
Xylene (Total)
ug/L
ND
1.0
06/16/21 11:48
1,2-Dichloroethane-d4 (S)
%
106
70-130
06/16/21 11:48
4-Bromofluorobenzene (S)
%
102
70-130
06/16/21 11:48
Toluene-d8 (S)
%
109
70-130
06/16/21 11:48
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3298651
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.6
103
70-130
1,1,1-Trichloroethane
ug/L
50
50.1
100
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.6
105
70-130
1,1,2-Trichloroethane
ug/L
50
50.9
102
70-130
1,1-Dichloroethane
ug/L
50
49.9
100
70-130
1,1-Dichloroethene
ug/L
50
51.7
103
70-132
1,2,3-Trichloropropane
ug/L
50
54.0
108
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
52.5
105
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.6
105
70-130
1,2-Dichlorobenzene
ug/L
50
49.2
98
70-130
1,2-Dichloroethane
ug/L
50
51.8
104
70-130
1,2-Dichloropropane
ug/L
50
48.9
98
70-130
1,4-Dichlorobenzene
ug/L
50
49.1
98
70-130
2-Butanone (MEK)
ug/L
100
96.3
96
70-133
2-Hexanone
ug/L
100
101
101
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
100
100
70-130
Acetone
ug/L
100
97.2
97
70-144
Acrylonitrile
ug/L
250
240
96
70-130
Benzene
ug/L
50
50.9
102
70-130
Bromochloromethane
ug/L
50
49.6
99
70-130
Bromodichloromethane
ug/L
50
51.0
102
70-130
Bromoform
ug/L
50
55.1
110
70-131
Bromomethane
ug/L
50
52.5
105
30-177
Carbon disulfide
ug/L
50
48.3
97
70-133
Carbon tetrachloride
ug/L
50
49.9
100
70-130
Chlorobenzene
ug/L
50
49.9
100
70-130
Chloroethane
ug/L
50
58.1
116
46-131
Chloroform
ug/L
50
50.8
102
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
LABORATORY CONTROL SAMPLE:
Parameter
3298651
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
43.2
86
49-130
49.7
99
70-130
52.5
105
70-130
53.3
107
70-130
49.4
99
70-130
50.1
100
70-130
104
104
47-140
102
102
70-130
46.2
92
68-130
49.8
100
70-130
51.9
104
70-130
48.4
97
70-130
49.5
99
70-130
49.5
99
70-130
52.8
106
70-130
60.2
120
25-200
49.1
98
70-130
46.1
92
61-130
120
120
70-140
44.7
89
59-142
151
101
70-130
102
70-130
104
70-130
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3298652
MS
92544439001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3298653
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.7
22.0
109
110
70-135
1
1,1,1-Trichloroethane
ug/L
ND
20
20
23.6
23.8
118
119
70-148
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.8
22.3
109
111
70-131
2
1,1,2-Trichloroethane
ug/L
ND
20
20
22.1
21.7
111
109
70-136
2
1,1-Dichloroethane
ug/L
ND
20
20
23.6
23.6
118
118
70-147
0
1,1-Dichloroethene
ug/L
ND
20
20
24.9
24.7
124
124
70-158
1
1,2,3-Trichloropropane
ug/L
ND
20
20
21.5
22.2
107
111
67-137
4
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.1
21.6
106
108
69-136
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.3
22.1
106
110
70-137
4
1,2-Dichlorobenzene
ug/L
ND
20
20
21.2
21.6
106
108
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
21.9
21.5
110
108
67-138
2
1,2-Dichloropropane
ug/L
ND
20
20
22.6
22.6
113
113
70-138
0
1,4-Dichlorobenzene
ug/L
ND
20
20
21.9
22.2
110
111
70-133
1
2-Butanone (MEK)
ug/L
ND
40
40
47.7
46.7
119
117
61-147
2
2-Hexanone
ug/L
ND
40
40
43.1
45.1
108
113
67-139
5
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
45.0
44.6
113
112
67-136
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3298652
MS
92544439001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3298653
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
46.9
46.1
117
115
55-159
2
Acrylonitrile
ug/L
ND
100
100
113
110
113
110
68-140
2
Benzene
ug/L
ND
20
20
22.6
22.6
113
113
67-150
0
Bromochloromethane
ug/L
ND
20
20
22.3
21.7
112
108
70-146
3
Bromodichloromethane
ug/L
ND
20
20
22.9
22.4
114
112
70-138
2
Bromoform
ug/L
ND
20
20
20.6
20.7
103
104
57-138
1
Bromomethane
ug/L
ND
20
20
22.9
23.0
114
115
10-200
1
Carbon disulfide
ug/L
ND
20
20
22.9
22.9
115
115
70-152
0
Carbon tetrachloride
ug/L
ND
20
20
24.3
23.8
122
119
70-147
2
Chlorobenzene
ug/L
ND
20
20
22.2
22.6
111
113
70-137
2
Chloroethane
ug/L
ND
20
20
24.9
25.2
125
126
51-166
1
Chloroform
ug/L
ND
20
20
23.7
23.8
118
119
70-144
1
Chloromethane
ug/L
ND
20
20
22.1
22.1
110
110
24-161
0
cis-1,2-Dichloroethene
ug/L
ND
20
20
23.9
23.5
119
117
67-148
2
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.4
22.0
112
110
70-142
2
Dibromochloromethane
ug/L
ND
20
20
21.8
22.0
109
110
68-138
1
Dibromomethane
ug/L
ND
20
20
21.4
21.1
107
105
70-134
1
Ethylbenzene
ug/L
ND
20
20
23.0
23.1
115
116
68-143
1
lodomethane
ug/L
ND
40
40
42.9
43.4
107
109
20-161
1
m&p-Xylene
ug/L
ND
40
40
46.0
46.3
115
116
53-157
1
Methylene Chloride
ug/L
ND
20
20
23.5
23.1
118
115
64-148
2
o-Xylene
ug/L
ND
20
20
22.5
22.7
113
113
68-143
1
Styrene
ug/L
ND
20
20
22.2
22.6
111
113
70-136
2
Tetrachloroethene
ug/L
ND
20
20
21.8
22.2
109
111
70-139
2
Toluene
ug/L
ND
20
20
22.5
22.3
112
111
47-157
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.4
24.0
122
120
70-149
2
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.8
21.5
109
108
70-138
1
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
20.1
21.1
101
106
31-145
5
Trichloroethene
ug/L
ND
20
20
21.8
22.2
109
111
70-149
2
Trichlorofluoromethane
ug/L
ND
20
20
23.5
23.5
118
117
61-154
0
Vinyl acetate
ug/L
ND
40
40
49.1
48.2
123
121
48-156
2
Vinyl chloride
ug/L
ND
20
20
22.8
22.5
114
113
55-172
1
Xylene (Total)
ug/L
ND
60
60
68.6
69.0
114
115
66-145
1
1,2-Dichloroethane-d4 (S)
%
111
109
70-130
4-Bromofluorobenzene (S)
%
102
104
70-130
Toluene-d8(S)
%
104
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/29/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Harrisburg Rd Landfill (Permit
Pace Project No.: 92544439
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92544439001
6001-HB2006
EPA 3010A
629888
EPA6010D
629905
92544439002
6001-HB2008
EPA 3010A
629888
EPA6010D
629905
92544439003
6001-HB2010
EPA 3010A
629888
EPA6010D
629905
92544439001
6001-HB2006
EPA 3010A
629890
EPA6020B
629906
92544439002
6001-HB2008
EPA 3010A
629890
EPA6020B
629906
92544439003
6001-HB2010
EPA 3010A
629890
EPA6020B
629906
92544439001
6001-HB2006
EPA 8260D
627470
92544439002
6001-HB2008
EPA8260D
627470
92544439003
6001-HB2010
EPA8260D
627470
Date: 06/29/2021 02:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 21

5ampke tonditian Upon Receipt{SOUR} �°6�
�'�c3f�lCril�-~ ➢ocument No.: Issuing Authority:
F-LAR•CS-033-Rev.07 Pate Carolinas Quality Office
Laboratory receiving samples:
ood ❑ Hurstersville Raleigh❑ Mechanicsville❑ Atlanta[]KernersviH❑ e
Asheville ❑ Eden❑ Greenw
Sample Condition Client Name: Project #: WQ# : 92544439
I Z t 'e ,_ 1 r r
Commercial SIPace
Custody Seal Present? []yes
[]Other:
NNo Seals intact? Dyes
92544439
P Nubble Has None Other Blological Tissue Frozen?
Packing Material: QBubble Vdra !3 Yes []No gN/A
Thermometer: Owet ❑Blue []None
ZJIR Gun ID: 92TO64 Type of Ice:
Correction Factor:
�� Add/Subtract (°Cy Q Tempshould he above freezing to 5°C
Cooler Temp: nsarnples out of temp criteria- Samples on ice, cooling process
Cooler Temp Corrected ('C): J . �� has begun
USDA Regulated Soil ( [5N/A, water samples
Did samples originate in a quarantine zone within the United States: CA, NY, or Sc (check mapsl7 D cludngid lHawa('iles gand Puerto
Roca)?❑❑
yes source ('sntemNtianally, o
ilYes nNo r.,__.nt,1niscreuancv:
I
f Custody Present?s Arrived within Hold Time?old.Tlme Analysis (02 hr,j?rn AroundTlme Requested?
nt Volume? Containers Used?e Containers Used?ners Intact?ed analysis: Samples Field Filtered?
Labels Match COC?
LJ
Yes
[]NO
❑N/A
1.
ges
❑No
❑N/A
2-
]yes
No
❑N/A
3.
Dyes
No
❑N/A
4.
Yes
❑No
❑N/A
S.
myes
❑No
❑N/A
6.
Yes
C3No
❑N/A
Yes
(IN.
N/A
7.
Yes
LjN0
N/A
g•
Yes
❑No
❑N/A
9.
❑Yes NoLCIN/A10.
Headspace iriVOAVWS (>5-6MM)? Trip Blank Present? 1QNaTrip clank Custody Seals Present? es �No
Field Data Required? ❑Yes ❑Na
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Date/Time:
Date:
Date:
Project Manager SRF Review:
Page 19 of 21

9
uacurneM Ndme
Document No.:
F-CAR-CS-033-Rev.07
Issuing Authority:
Pace Carolinas Qua Iity Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TCC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Botto.m_half_nf_box._is_to_list_number_of.bottles_—_ _...__. _.__..
Project wa# : 92544439
PM: MWB Due Date: 06/29/21
CLIENT: 92-MECK CO
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Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative
adjusted I added
Lot d
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 20 of 21

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Page 21 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 30, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on June 16, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92544681001 6001-HBW12A
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544681002 6001-HBW12B
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544681003 6001-HBW21
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
PM1
52
PASI-C
92544681004 6001-HBW22
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544681005 6001-HBW17B
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
92544681006 Trip Blank
EPA 8260D
NSCQ
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW12A Lab ID: 92544681001 Collected: 06/16/21 10:00 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:32
7440-38-2 BC
Barium
48.7
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/29/21 11:39
06/29/21 19:32
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/29/21 11:39
06/29/21 19:32
7440-43-9
Chromium
9.4
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7440-47-3
Cobalt
6.3
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7440-48-4
Copper
31.1
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7440-50-8
Lead
7.9
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7439-92-1
Nickel
6.3
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7440-02-0
Selenium
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:32
7782-49-2
Silver
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7440-22-4
Thallium
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:32
7440-28-0
Vanadium
52.5
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:32
7440-62-2
Zinc
16.6
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:32
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
Date: 06/30/2021 01:20 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
1.0
1
06/27/2117:52 06/28/2113:44
7440-28-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
06/17/2101:07
67-64-1
ND
ug/L
10.0
1
06/17/2101:07
107-13-1
ND
ug/L
1.0
1
06/17/2101:07
71-43-2
ND
ug/L
1.0
1
06/17/2101:07
74-97-5
ND
ug/L
1.0
1
06/17/2101:07
75-27-4
ND
ug/L
1.0
1
06/17/2101:07
75-25-2
ND
ug/L
2.0
1
06/17/2101:07
74-83-9
ND
ug/L
5.0
1
06/17/2101:07
78-93-3
ND
ug/L
2.0
1
06/17/2101:07
75-15-0
ND
ug/L
1.0
1
06/17/2101:07
56-23-5 v1
ND
ug/L
1.0
1
06/17/2101:07
108-90-7
ND
ug/L
1.0
1
06/17/2101:07
75-00-3
ND
ug/L
5.0
1
06/17/2101:07
67-66-3
ND
ug/L
1.0
1
06/17/2101:07
74-87-3
ND
ug/L
2.0
1
06/17/2101:07
96-12-8
ND
ug/L
1.0
1
06/17/2101:07
124-48-1
ND
ug/L
1.0
1
06/17/2101:07
106-93-4
ND
ug/L
1.0
1
06/17/2101:07
74-95-3
ND
ug/L
1.0
1
06/17/2101:07
95-50-1
ND
ug/L
1.0
1
06/17/2101:07
106-46-7
ND
ug/L
1.0
1
06/17/2101:07
110-57-6 v1
ND
ug/L
1.0
1
06/17/2101:07
75-34-3
ND
ug/L
1.0
1
06/17/2101:07
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW12A Lab ID: 92544681001 Collected: 06/16/21 10:00 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/17/21 01:07
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/17/21 01:07
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/17/21 01:07
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/17/21 01:07
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/17/21 01:07
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/17/21 01:07
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/17/21 01:07
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/17/21 01:07
591-78-6
lodomethane
ND
ug/L
20.0
1
06/17/21 01:07
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/17/21 01:07
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/17/21 01:07
108-10-1
Styrene
ND
ug/L
1.0
1
06/17/21 01:07
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/17/21 01:07
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/17/21 01:07
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/17/21 01:07
127-18-4
Toluene
ND
ug/L
1.0
1
06/17/21 01:07
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/17/21 01:07
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/17/21 01:07
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/17/21 01:07
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/17/21 01:07
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/17/21 01:07
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/17/21 01:07
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/17/21 01:07
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/17/21 01:07
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/17/21 01:07
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/17/21 01:07
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
06/17/21 01:07
460-00-4
1,2-Dichloroethane-d4 (S)
119
%
70-130
1
06/17/21 01:07
17060-07-0
Toluene-d8 (S)
97
%
70-130
1
06/17/21 01:07
2037-26-5
Date: 06/30/2021 01:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW12B Lab ID: 92544681002 Collected: 06/16/21 10:15 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:38
7440-38-2 BC
Barium
38.7
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/29/21 11:39
06/29/21 19:38
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/29/21 11:39
06/29/21 19:38
7440-43-9
Chromium
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7440-47-3
Cobalt
8.2
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7440-48-4
Copper
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7440-50-8
Lead
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7439-92-1
Nickel
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7440-02-0
Selenium
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:38
7782-49-2
Silver
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7440-22-4
Thallium
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:38
7440-28-0
Vanadium
5.4
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:38
7440-62-2
Zinc
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:38
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
Date: 06/30/2021 01:20 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
1.0
1
06/27/2117:52 06/28/2113:52
7440-28-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
06/17/2101:25
67-64-1
ND
ug/L
10.0
1
06/17/2101:25
107-13-1
ND
ug/L
1.0
1
06/17/2101:25
71-43-2
ND
ug/L
1.0
1
06/17/2101:25
74-97-5
ND
ug/L
1.0
1
06/17/2101:25
75-27-4
ND
ug/L
1.0
1
06/17/2101:25
75-25-2
ND
ug/L
2.0
1
06/17/2101:25
74-83-9
ND
ug/L
5.0
1
06/17/2101:25
78-93-3
ND
ug/L
2.0
1
06/17/2101:25
75-15-0
ND
ug/L
1.0
1
06/17/2101:25
56-23-5 v1
ND
ug/L
1.0
1
06/17/2101:25
108-90-7
ND
ug/L
1.0
1
06/17/2101:25
75-00-3
ND
ug/L
5.0
1
06/17/2101:25
67-66-3
ND
ug/L
1.0
1
06/17/2101:25
74-87-3
ND
ug/L
2.0
1
06/17/2101:25
96-12-8
ND
ug/L
1.0
1
06/17/2101:25
124-48-1
ND
ug/L
1.0
1
06/17/2101:25
106-93-4
ND
ug/L
1.0
1
06/17/2101:25
74-95-3
ND
ug/L
1.0
1
06/17/2101:25
95-50-1
ND
ug/L
1.0
1
06/17/2101:25
106-46-7
ND
ug/L
1.0
1
06/17/2101:25
110-57-6 v1
ND
ug/L
1.0
1
06/17/2101:25
75-34-3
ND
ug/L
1.0
1
06/17/2101:25
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW12B Lab ID: 92544681002 Collected: 06/16/21 10:15 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/17/21 01:25
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/17/21 01:25
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/17/21 01:25
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/17/21 01:25
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/17/21 01:25
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/17/21 01:25
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/17/21 01:25
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/17/21 01:25
591-78-6
lodomethane
ND
ug/L
20.0
1
06/17/21 01:25
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/17/21 01:25
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/17/21 01:25
108-10-1
Styrene
ND
ug/L
1.0
1
06/17/21 01:25
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/17/21 01:25
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/17/21 01:25
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/17/21 01:25
127-18-4
Toluene
ND
ug/L
1.0
1
06/17/21 01:25
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/17/21 01:25
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/17/21 01:25
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/17/21 01:25
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/17/21 01:25
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/17/21 01:25
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/17/21 01:25
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/17/21 01:25
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/17/21 01:25
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/17/21 01:25
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/17/21 01:25
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
06/17/21 01:25
460-00-4
1,2-Dichloroethane-d4 (S)
115
%
70-130
1
06/17/21 01:25
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
06/17/21 01:25
2037-26-5
Date: 06/30/2021 01:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW21 Lab ID: 92544681003 Collected: 06/16/21 09:45 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:44
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/29/2111:39
06/29/2119:44
7440-38-2 BC
Barium
11.8
ug/L
5.0
1
06/29/2111:39
06/29/2119:44
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/29/2111:39
06/29/2119:44
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/29/2111:39
06/29/2119:44
7440-43-9
Chromium
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:44
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:44
7440-48-4
Copper
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:44
7440-50-8
Lead
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:44
7439-92-1
Nickel
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:44
7440-02-0
Selenium
ND
ug/L
10.0
1
06/29/2111:39
06/29/2119:44
7782-49-2
Silver
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:44
7440-22-4
Thallium
ND
ug/L
10.0
1
06/29/2111:39
06/29/2119:44
7440-28-0
Vanadium
6.2
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:44
7440-62-2
Zinc
ND
ug/L
10.0
1
06/29/2111:39
06/29/2119:44
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
1.0
1
06/27/2117:52 06/28/2114:01
7440-28-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
06/18/2114:11
67-64-1
ND
ug/L
10.0
1
06/18/2114:11
107-13-1
ND
ug/L
1.0
1
06/18/2114:11
71-43-2
ND
ug/L
1.0
1
06/18/2114:11
74-97-5
ND
ug/L
1.0
1
06/18/2114:11
75-27-4
ND
ug/L
1.0
1
06/18/2114:11
75-25-2
ND
ug/L
2.0
1
06/18/2114:11
74-83-9
ND
ug/L
5.0
1
06/18/2114:11
78-93-3
ND
ug/L
2.0
1
06/18/2114:11
75-15-0
ND
ug/L
1.0
1
06/18/2114:11
56-23-5
ND
ug/L
1.0
1
06/18/2114:11
108-90-7
ND
ug/L
1.0
1
06/18/2114:11
75-00-3
ND
ug/L
5.0
1
06/18/2114:11
67-66-3
ND
ug/L
1.0
1
06/18/2114:11
74-87-3
ND
ug/L
2.0
1
06/18/2114:11
96-12-8
ND
ug/L
1.0
1
06/18/2114:11
124-48-1
ND
ug/L
1.0
1
06/18/2114:11
106-93-4
ND
ug/L
1.0
1
06/18/2114:11
74-95-3
ND
ug/L
1.0
1
06/18/2114:11
95-50-1
ND
ug/L
1.0
1
06/18/2114:11
106-46-7
ND
ug/L
1.0
1
06/18/2114:11
110-57-6
ND
ug/L
1.0
1
06/18/2114:11
75-34-3
ND
ug/L
1.0
1
06/18/2114:11
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW21 Lab ID: 92544681003 Collected: 06/16/21 09:45 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/18/21 14:11
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/18/21 14:11
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/18/21 14:11
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/18/21 14:11
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/18/21 14:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/18/21 14:11
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/18/21 14:11
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/18/21 14:11
591-78-6
lodomethane
ND
ug/L
20.0
1
06/18/21 14:11
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/18/21 14:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/18/21 14:11
108-10-1
Styrene
ND
ug/L
1.0
1
06/18/21 14:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/18/21 14:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/18/21 14:11
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/18/21 14:11
127-18-4
Toluene
ND
ug/L
1.0
1
06/18/21 14:11
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/18/21 14:11
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/18/21 14:11
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/18/21 14:11
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/18/21 14:11
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/18/21 14:11
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/18/21 14:11
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/18/21 14:11
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/18/21 14:11
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/18/21 14:11
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/18/21 14:11
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
06/18/21 14:11
460-00-4
1,2-Dichloroethane-d4 (S)
109
%
70-130
1
06/18/21 14:11
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
06/18/21 14:11
2037-26-5
Date: 06/30/2021 01:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW22 Lab ID: 92544681004 Collected: 06/16/21 09:25 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/29/2111:39
06/29/2119:51
7440-38-2 BC
Barium
44.4
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/29/2111:39
06/29/2119:51
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/29/2111:39
06/29/2119:51
7440-43-9
Chromium
22.7
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7440-47-3
Cobalt
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7440-48-4
Copper
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7440-50-8
Lead
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7439-92-1
Nickel
7.4
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7440-02-0
Selenium
ND
ug/L
10.0
1
06/29/2111:39
06/29/2119:51
7782-49-2
Silver
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7440-22-4
Thallium
ND
ug/L
10.0
1
06/29/2111:39
06/29/2119:51
7440-28-0
Vanadium
ND
ug/L
5.0
1
06/29/2111:39
06/29/2119:51
7440-62-2
Zinc
ND
ug/L
10.0
1
06/29/2111:39
06/29/2119:51
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
Date: 06/30/2021 01:20 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
1.0
1
06/27/2117:52 06/28/2114:18
7440-28-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
06/17/2101:43
67-64-1
ND
ug/L
10.0
1
06/17/2101:43
107-13-1
ND
ug/L
1.0
1
06/17/2101:43
71-43-2
ND
ug/L
1.0
1
06/17/2101:43
74-97-5
ND
ug/L
1.0
1
06/17/2101:43
75-27-4
ND
ug/L
1.0
1
06/17/2101:43
75-25-2
ND
ug/L
2.0
1
06/17/2101:43
74-83-9
ND
ug/L
5.0
1
06/17/2101:43
78-93-3
ND
ug/L
2.0
1
06/17/2101:43
75-15-0
ND
ug/L
1.0
1
06/17/2101:43
56-23-5 v1
ND
ug/L
1.0
1
06/17/2101:43
108-90-7
ND
ug/L
1.0
1
06/17/2101:43
75-00-3
ND
ug/L
5.0
1
06/17/2101:43
67-66-3
ND
ug/L
1.0
1
06/17/2101:43
74-87-3
ND
ug/L
2.0
1
06/17/2101:43
96-12-8
ND
ug/L
1.0
1
06/17/2101:43
124-48-1
ND
ug/L
1.0
1
06/17/2101:43
106-93-4
ND
ug/L
1.0
1
06/17/2101:43
74-95-3
ND
ug/L
1.0
1
06/17/2101:43
95-50-1
ND
ug/L
1.0
1
06/17/2101:43
106-46-7
ND
ug/L
1.0
1
06/17/2101:43
110-57-6 v1
ND
ug/L
1.0
1
06/17/2101:43
75-34-3
ND
ug/L
1.0
1
06/17/2101:43
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW22 Lab ID: 92544681004 Collected: 06/16/21 09:25 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2021 01:20 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
99
%
115
%
99
%
1.0
1
06/17/21 01:43
75-35-4
1.0
1
06/17/21 01:43
156-59-2
1.0
1
06/17/21 01:43
156-60-5
1.0
1
06/17/21 01:43
78-87-5
1.0
1
06/17/21 01:43
10061-01-5
1.0
1
06/17/21 01:43
10061-02-6
1.0
1
06/17/21 01:43
100-41-4
5.0
1
06/17/21 01:43
591-78-6
20.0
1
06/17/21 01:43
74-88-4
5.0
1
06/17/21 01:43
75-09-2
5.0
1
06/17/21 01:43
108-10-1
1.0
1
06/17/21 01:43
100-42-5
1.0
1
06/17/21 01:43
630-20-6
1.0
1
06/17/21 01:43
79-34-5
1.0
1
06/17/21 01:43
127-18-4
1.0
1
06/17/21 01:43
108-88-3
1.0
1
06/17/21 01:43
71-55-6
1.0
1
06/17/21 01:43
79-00-5
1.0
1
06/17/21 01:43
79-01-6
1.0
1
06/17/21 01:43
75-69-4
1.0
1
06/17/21 01:43
96-18-4
2.0
1
06/17/21 01:43
108-05-4
1.0
1
06/17/21 01:43
75-01-4
1.0
1
06/17/21 01:43
1330-20-7
2.0
1
06/17/21 01:43
179601-23-1
1.0
1
06/17/21 01:43
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/17/21 01:43 460-00-4
06/17/21 01:43 17060-07-0
06/17/21 01:43 2037-26-5
Page 11 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW17B Lab ID: 92544681005 Collected: 06/16/21 10:40 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7440-36-0
Arsenic
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:57
7440-38-2 BC
Barium
66.9
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7440-39-3
Beryllium
ND
ug/L
1.0
1
06/29/21 11:39
06/29/21 19:57
7440-41-7
Cadmium
ND
ug/L
1.0
1
06/29/21 11:39
06/29/21 19:57
7440-43-9
Chromium
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7440-47-3
Cobalt
20.1
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7440-48-4
Copper
27.0
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7440-50-8
Lead
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7439-92-1
Nickel
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7440-02-0
Selenium
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:57
7782-49-2
Silver
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7440-22-4
Thallium
ND
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:57
7440-28-0
Vanadium
ND
ug/L
5.0
1
06/29/21 11:39
06/29/21 19:57
7440-62-2
Zinc
16.4
ug/L
10.0
1
06/29/21 11:39
06/29/21 19:57
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
Date: 06/30/2021 01:20 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
1.0
1
06/27/2117:52 06/28/2114:26
7440-28-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
06/17/2102:01
67-64-1
ND
ug/L
10.0
1
06/17/2102:01
107-13-1
5.7
ug/L
1.0
1
06/17/2102:01
71-43-2
ND
ug/L
1.0
1
06/17/2102:01
74-97-5
ND
ug/L
1.0
1
06/17/2102:01
75-27-4
ND
ug/L
1.0
1
06/17/2102:01
75-25-2
ND
ug/L
2.0
1
06/17/2102:01
74-83-9
ND
ug/L
5.0
1
06/17/2102:01
78-93-3
ND
ug/L
2.0
1
06/17/2102:01
75-15-0
ND
ug/L
1.0
1
06/17/2102:01
56-23-5 v1
ND
ug/L
1.0
1
06/17/2102:01
108-90-7
ND
ug/L
1.0
1
06/17/2102:01
75-00-3
ND
ug/L
5.0
1
06/17/2102:01
67-66-3
ND
ug/L
1.0
1
06/17/2102:01
74-87-3
ND
ug/L
2.0
1
06/17/2102:01
96-12-8
ND
ug/L
1.0
1
06/17/2102:01
124-48-1
ND
ug/L
1.0
1
06/17/2102:01
106-93-4
ND
ug/L
1.0
1
06/17/2102:01
74-95-3
ND
ug/L
1.0
1
06/17/2102:01
95-50-1
ND
ug/L
1.0
1
06/17/2102:01
106-46-7
ND
ug/L
1.0
1
06/17/2102:01
110-57-6 v1
5.5
ug/L
1.0
1
06/17/21 02:01
75-34-3
ND
ug/L
1.0
1
06/17/2102:01
107-06-2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 12 of 31

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: 6001-HBW17B Lab ID: 92544681005 Collected: 06/16/21 10:40 Received: 06/16/21 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2021 01:20 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
77.4
ug/L
1.1
ug/L
8.3
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
6.1
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
24.8
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
19.2
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
7.4
ug/L
ND
ug/L
7.4
ug/L
102
%
118
%
99
%
1.0
1
06/17/21 02:01
75-35-4
1.0
1
06/17/21 02:01
156-59-2
1.0
1
06/17/21 02:01
156-60-5
1.0
1
06/17/21 02:01
78-87-5
1.0
1
06/17/21 02:01
10061-01-5
1.0
1
06/17/21 02:01
10061-02-6
1.0
1
06/17/21 02:01
100-41-4
5.0
1
06/17/21 02:01
591-78-6
20.0
1
06/17/21 02:01
74-88-4
5.0
1
06/17/21 02:01
75-09-2
5.0
1
06/17/21 02:01
108-10-1
1.0
1
06/17/21 02:01
100-42-5
1.0
1
06/17/21 02:01
630-20-6
1.0
1
06/17/21 02:01
79-34-5
1.0
1
06/17/21 02:01
127-18-4
1.0
1
06/17/21 02:01
108-88-3
1.0
1
06/17/21 02:01
71-55-6
1.0
1
06/17/21 02:01
79-00-5
1.0
1
06/17/21 02:01
79-01-6
1.0
1
06/17/21 02:01
75-69-4
1.0
1
06/17/21 02:01
96-18-4
2.0
1
06/17/21 02:01
108-05-4
1.0
1
06/17/21 02:01
75-01-4
1.0
1
06/17/21 02:01
1330-20-7
2.0
1
06/17/21 02:01
179601-23-1
1.0
1
06/17/21 02:01
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/17/21 02:01 460-00-4
06/17/21 02:01 17060-07-0
06/17/21 02:01 2037-26-5
Page 13 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: Trip Blank
Lab ID: 92544681006 Collected:
06/16/21
09:11
Received: 06/16/21 13:12 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/17/21 00:49
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/17/21 00:49
107-13-1
Benzene
ND
ug/L
1.0
1
06/17/21 00:49
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/17/21 00:49
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/17/21 00:49
75-27-4
Bromoform
ND
ug/L
1.0
1
06/17/21 00:49
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/17/21 00:49
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/17/21 00:49
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/17/21 00:49
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/17/21 00:49
56-23-5 v1
Chlorobenzene
ND
ug/L
1.0
1
06/17/21 00:49
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/17/21 00:49
75-00-3
Chloroform
ND
ug/L
5.0
1
06/17/21 00:49
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/17/21 00:49
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/17/21 00:49
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/17/21 00:49
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/17/21 00:49
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/17/21 00:49
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/17/21 00:49
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/17/21 00:49
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/17/21 00:49
110-57-6 v1
1,1-Dichloroethane
ND
ug/L
1.0
1
06/17/21 00:49
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/17/21 00:49
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
06/17/21 00:49
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/17/21 00:49
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/17/21 00:49
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/17/21 00:49
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/17/21 00:49
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/17/21 00:49
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/17/21 00:49
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/17/21 00:49
591-78-6
lodomethane
ND
ug/L
20.0
1
06/17/21 00:49
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/17/21 00:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/17/21 00:49
108-10-1
Styrene
ND
ug/L
1.0
1
06/17/21 00:49
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/17/21 00:49
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/17/21 00:49
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/17/21 00:49
127-18-4
Toluene
ND
ug/L
1.0
1
06/17/21 00:49
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/17/21 00:49
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/17/21 00:49
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/17/21 00:49
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/17/21 00:49
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/17/21 00:49
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/17/21 00:49
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/17/21 00:49
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
Sample: Trip Blank
Parameters
Lab ID: 92544681006 Collected: 06/16/21 09:11
Results Units Report Limit DF
Received: 06/16/21 13:12 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
06/17/21 00:49
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
06/17/21 00:49
179601-23-1
o-Xylene
ND ug/L
1.0
1
06/17/21 00:49
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
06/17/21 00:49
460-00-4
1,2-Dichloroethane-d4 (S)
114 %
70-130
1
06/17/21 00:49
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
06/17/21 00:49
2037-26-5
Date: 06/30/2021 01:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
QC Batch: 630001 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92544681001, 92544681002, 92544681003, 92544681004, 92544681005
METHOD BLANK: 3310514 Matrix: Water
Associated Lab Samples: 92544681001, 92544681002, 92544681003, 92544681004, 92544681005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
06/29/2119:05
Arsenic
ug/L
ND
10.0
06/29/2119:05
Barium
ug/L
ND
5.0
06/29/2119:05
Beryllium
ug/L
ND
1.0
06/29/2119:05
Cadmium
ug/L
ND
1.0
06/29/2119:05
Chromium
ug/L
ND
5.0
06/29/2119:05
Cobalt
ug/L
ND
5.0
06/29/2119:05
Copper
ug/L
ND
5.0
06/29/2119:05
Lead
ug/L
ND
5.0
06/29/2119:05
Nickel
ug/L
ND
5.0
06/29/2119:05
Selenium
ug/L
ND
10.0
06/29/2119:05
Silver
ug/L
ND
5.0
06/29/2119:05
Thallium
ug/L
ND
10.0
06/29/2119:05
Vanadium
ug/L
ND
5.0
06/29/2119:05
Zinc
ug/L
ND
10.0
06/29/2119:05
LABORATORY CONTROL SAMPLE:
Parameter
3310515
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
501
100
80-120
Arsenic
ug/L
500
494
99
80-120
Barium
ug/L
500
494
99
80-120
Beryllium
ug/L
500
506
101
80-120
Cadmium
ug/L
500
492
98
80-120
Chromium
ug/L
500
491
98
80-120
Cobalt
ug/L
500
483
97
80-120
Copper
ug/L
500
515
103
80-120
Lead
ug/L
500
487
97
80-120
Nickel
ug/L
500
498
100
80-120
Selenium
ug/L
500
488
98
80-120
Silver
ug/L
250
243
97
80-120
Thallium
ug/L
500
491
98
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
481
96
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Harrisburg Rd Landfill #60-01
92544681
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3310516
3310517
MS
MSD
92544680001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
500
502
100
100
75-125
0
Arsenic
ug/L
ND
500
500
488
495
98
99
75-125
1
Barium
ug/L
121
500
500
607
606
97
97
75-125
0
Beryllium
ug/L
ND
500
500
496
495
99
99
75-125
0
Cadmium
ug/L
ND
500
500
496
498
99
100
75-125
0
Chromium
ug/L
ND
500
500
488
482
97
96
75-125
1
Cobalt
ug/L
4AJ
500
500
476
474
94
94
75-125
0
Copper
ug/L
ND
500
500
503
498
100
100
75-125
1
Lead
ug/L
ND
500
500
484
484
97
97
75-125
0
Nickel
ug/L
3.6J
500
500
490
490
97
97
75-125
0
Selenium
ug/L
ND
500
500
521
517
104
103
75-125
1
Silver
ug/L
ND
250
250
247
244
99
98
75-125
1
Thallium
ug/L
ND
500
500
481
485
96
97
75-125
1
Vanadium
ug/L
6.5
500
500
495
489
98
97
75-125
1
Zinc
ug/L
ND
500
500
491
489
97
96
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
QC Batch: 629890 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92544681001, 92544681002, 92544681003, 92544681004, 92544681005
METHOD BLANK: 3310079
Matrix:
Water
Associated Lab Samples: 92544681001, 92544681002, 92544681003, 92544681004, 92544681005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
06/28/2111:33
LABORATORY CONTROL SAMPLE:
3310080
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
24.3
97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3310081 3310082
MS MSD
92544439001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 24.2 24.2 97 97 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
QC Batch: 627620 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92544681001, 92544681002, 92544681004, 92544681005, 92544681006
METHOD BLANK: 3299601 Matrix: Water
Associated Lab Samples: 92544681001, 92544681002, 92544681004, 92544681005, 92544681006
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
06/16/21 17:33
1,1,1-Trichloroethane
ug/L
ND
1.0
06/16/21 17:33
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/16/21 17:33
1,1,2-Trichloroethane
ug/L
ND
1.0
06/16/21 17:33
1,1-Dichloroethane
ug/L
ND
1.0
06/16/21 17:33
1,1-Dichloroethene
ug/L
ND
1.0
06/16/21 17:33
1,2,3-Trichloropropane
ug/L
ND
1.0
06/16/21 17:33
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
06/16/21 17:33
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
06/16/21 17:33
1,2-Dichlorobenzene
ug/L
ND
1.0
06/16/21 17:33
1,2-Dichloroethane
ug/L
ND
1.0
06/16/21 17:33
1,2-Dichloropropane
ug/L
ND
1.0
06/16/21 17:33
1,4-Dichlorobenzene
ug/L
ND
1.0
06/16/21 17:33
2-Butanone (MEK)
ug/L
ND
5.0
06/16/21 17:33
2-Hexanone
ug/L
ND
5.0
06/16/21 17:33
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
06/16/21 17:33
Acetone
ug/L
ND
25.0
06/16/21 17:33
Acrylonitrile
ug/L
ND
10.0
06/16/21 17:33
Benzene
ug/L
ND
1.0
06/16/21 17:33
Bromochloromethane
ug/L
ND
1.0
06/16/21 17:33
Bromodichloromethane
ug/L
ND
1.0
06/16/21 17:33
Bromoform
ug/L
ND
1.0
06/16/21 17:33
Bromomethane
ug/L
ND
2.0
06/16/21 17:33
Carbon disulfide
ug/L
ND
2.0
06/16/21 17:33
Carbon tetrachloride
ug/L
ND
1.0
06/16/21 17:33
Chlorobenzene
ug/L
ND
1.0
06/16/21 17:33
Chloroethane
ug/L
ND
1.0
06/16/21 17:33
Chloroform
ug/L
ND
5.0
06/16/21 17:33
Chloromethane
ug/L
ND
1.0
06/16/21 17:33
cis-1,2-Dichloroethene
ug/L
ND
1.0
06/16/21 17:33
cis-1,3-Dichloropropene
ug/L
ND
1.0
06/16/21 17:33
Dibromochloromethane
ug/L
ND
1.0
06/16/21 17:33
Dibromomethane
ug/L
ND
1.0
06/16/21 17:33
Ethylbenzene
ug/L
ND
1.0
06/16/21 17:33
lodomethane
ug/L
ND
20.0
06/16/21 17:33
m&p-Xylene
ug/L
ND
2.0
06/16/21 17:33
Methylene Chloride
ug/L
ND
5.0
06/16/21 17:33
o-Xylene
ug/L
ND
1.0
06/16/21 17:33
Styrene
ug/L
ND
1.0
06/16/21 17:33
Tetrachloroethene
ug/L
ND
1.0
06/16/21 17:33
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
METHOD BLANK: 3299601 Matrix: Water
Associated Lab Samples: 92544681001, 92544681002, 92544681004, 92544681005, 92544681006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
06/16/21 17:33
trans-1,2-Dichloroethene
ug/L
ND
1.0
06/16/21 17:33
trans- 1,3-Dichloropropene
ug/L
ND
1.0
06/16/21 17:33
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
06/16/21 17:33 v1
Trichloroethene
ug/L
ND
1.0
06/16/21 17:33
Trichlorofluoromethane
ug/L
ND
1.0
06/16/21 17:33
Vinyl acetate
ug/L
ND
2.0
06/16/21 17:33
Vinyl chloride
ug/L
ND
1.0
06/16/21 17:33
Xylene (Total)
ug/L
ND
1.0
06/16/21 17:33
1,2-Dichloroethane-d4 (S)
%
108
70-130
06/16/21 17:33
4-Bromofluorobenzene (S)
%
97
70-130
06/16/21 17:33
Toluene-d8 (S)
%
99
70-130
06/16/21 17:33
LABORATORY CONTROL SAMPLE:
Parameter
3299602
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
54.8
110
70-130
1,1,1-Trichloroethane
ug/L
50
55.2
110
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
44.9
90
70-130
1,1,2-Trichloroethane
ug/L
50
50.1
100
70-130
1,1-Dichloroethane
ug/L
50
44.9
90
70-130
1,1-Dichloroethene
ug/L
50
49.1
98
70-132
1,2,3-Trichloropropane
ug/L
50
48.3
97
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.8
104
70-132
1,2-Dibromoethane (EDB)
ug/L
50
48.6
97
70-130
1,2-Dichlorobenzene
ug/L
50
50.3
101
70-130
1,2-Dichloroethane
ug/L
50
55.9
112
70-130
1,2-Dichloropropane
ug/L
50
46.2
92
70-130
1,4-Dichlorobenzene
ug/L
50
51.9
104
70-130
2-Butanone (MEK)
ug/L
100
84.4
84
70-133
2-Hexanone
ug/L
100
89.0
89
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
93.8
94
70-130
Acetone
ug/L
100
92.3
92
70-144
Acrylonitrile
ug/L
250
208
83
70-130
Benzene
ug/L
50
47.7
95
70-130
Bromochloromethane
ug/L
50
48.4
97
70-130
Bromodichloromethane
ug/L
50
57.5
115
70-130
Bromoform
ug/L
50
55.4
111
70-131
Bromomethane
ug/L
50
51.2
102
30-177
Carbon disulfide
ug/L
50
44.7
89
70-133
Carbon tetrachloride
ug/L
50
62.6
125
70-130 v1
Chlorobenzene
ug/L
50
50.1
100
70-130
Chloroethane
ug/L
50
53.1
106
46-131
Chloroform
ug/L
50
50.1
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
LABORATORY CONTROL SAMPLE:
Parameter
3299602
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
45.4
91
49-130
45.3
91
70-130
52.7
105
70-130
54.9
110
70-130
56.9
114
70-130
49.0
98
70-130
99.3
99
47-140
100
100
70-130
47.9
96
68-130
50.4
101
70-130
51.9
104
70-130
52.1
104
70-130
50.1
100
70-130
46.4
93
70-130
57.0
114
70-130
69.3
139
25-200 v1
52.0
104
70-130
57.7
115
61-130
96.4
96
70-140
44.3
89
59-142
151
100
70-130
110
70-130
100
70-130
100
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3299603
MS
92544711002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3299604
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.8
22.4
109
112
70-135
3
1,1,1-Trichloroethane
ug/L
ND
20
20
20.3
20.2
102
101
70-148
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.9
21.2
104
106
70-131
2
1,1,2-Trichloroethane
ug/L
ND
20
20
20.2
20.4
101
102
70-136
1
1,1-Dichloroethane
ug/L
ND
20
20
20.3
20.4
101
102
70-147
0
1,1-Dichloroethene
ug/L
ND
20
20
20.9
21.0
105
105
70-158
1
1,2,3-Trichloropropane
ug/L
ND
20
20
20.9
21.2
105
106
67-137
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
22.6
22.2
113
111
69-136
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.9
22.1
109
110
70-137
1
1,2-Dichlorobenzene
ug/L
ND
20
20
22.1
22.5
110
112
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
19.2
19.5
96
97
67-138
2
1,2-Dichloropropane
ug/L
ND
20
20
20.4
20.4
102
102
70-138
0
1,4-Dichlorobenzene
ug/L
ND
20
20
22.4
22.7
112
114
70-133
1
2-Butanone (MEK)
ug/L
ND
40
40
36.8
37.3
92
93
61-147
1
2-Hexanone
ug/L
ND
40
40
37.8
38.7
94
97
67-139
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
37.5
38.3
94
96
67-136
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3299603
MS
92544711002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3299604
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
39.0
39.0
98
97
55-159
0
Acrylonitrile
ug/L
ND
100
100
94.2
96.2
94
96
68-140
2
Benzene
ug/L
ND
20
20
20.3
20.6
102
103
67-150
1
Bromochloromethane
ug/L
ND
20
20
21.2
21.9
106
109
70-146
3
Bromodichloromethane
ug/L
ND
20
20
19.7
19.8
98
99
70-138
1
Bromoform
ug/L
ND
20
20
21.3
22.0
106
110
57-138
3
Bromomethane
ug/L
ND
20
20
22.8
23.0
114
115
10-200
1
Carbon disulfide
ug/L
ND
20
20
20.6
20.7
103
104
70-152
1
Carbon tetrachloride
ug/L
ND
20
20
21.2
21.8
106
109
70-147
3
Chlorobenzene
ug/L
ND
20
20
22.2
22.6
111
113
70-137
2
Chloroethane
ug/L
ND
20
20
21.7
21.2
108
106
51-166
2
Chloroform
ug/L
ND
20
20
21.0
21.3
105
106
70-144
1
Chloromethane
ug/L
ND
20
20
18.9
18.6
94
93
24-161
1 v2
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.2
19.9
101
99
67-148
1
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.2
20.4
101
102
70-142
1
Dibromochloromethane
ug/L
ND
20
20
21.6
21.8
108
109
68-138
1
Dibromomethane
ug/L
ND
20
20
21.5
22.0
107
110
70-134
2
Ethylbenzene
ug/L
ND
20
20
22.1
22.6
110
113
68-143
3
lodomethane
ug/L
ND
40
40
41.2
42.0
103
105
20-161
2
m&p-Xylene
ug/L
ND
40
40
44.4
45.6
111
114
53-157
3
Methylene Chloride
ug/L
ND
20
20
18.3
18.5
92
93
64-148
1
o-Xylene
ug/L
ND
20
20
21.8
21.8
109
109
68-143
0
Styrene
ug/L
ND
20
20
21.7
22.1
108
110
70-136
2
Tetrachloroethene
ug/L
ND
20
20
23.1
23.3
115
116
70-139
1
Toluene
ug/L
ND
20
20
20.6
20.8
103
104
47-157
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.4
20.7
102
103
70-149
1
trans- 1,3-Dichloropropene
ug/L
ND
20
20
19.9
20.0
99
100
70-138
0
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
19.7
20.1
98
101
31-145
2
Trichloroethene
ug/L
ND
20
20
20.9
21.9
105
109
70-149
4
Trichlorofluoromethane
ug/L
ND
20
20
19.9
20.3
100
101
61-154
2
Vinyl acetate
ug/L
ND
40
40
41.7
41.5
104
104
48-156
0
Vinyl chloride
ug/L
ND
20
20
20.1
20.0
100
100
55-172
1
Xylene (Total)
ug/L
ND
60
60
66.2
67.4
110
112
66-145
2
1,2-Dichloroethane-d4 (S)
%
97
99
70-130
4-Bromofluorobenzene (S)
%
98
99
70-130
Toluene-d8(S)
%
98
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
QC Batch: 627663 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92544681003
METHOD BLANK: 3299871
Associated Lab Samples: 92544681003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
06/18/21 11:30
1,1,1-Trichloroethane
ug/L
ND
1.0
06/18/21 11:30
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/18/21 11:30
1,1,2-Trichloroethane
ug/L
ND
1.0
06/18/21 11:30
1,1-Dichloroethane
ug/L
ND
1.0
06/18/21 11:30
1,1-Dichloroethene
ug/L
ND
1.0
06/18/21 11:30
1,2,3-Trichloropropane
ug/L
ND
1.0
06/18/21 11:30
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
06/18/21 11:30
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
06/18/21 11:30
1,2-Dichlorobenzene
ug/L
ND
1.0
06/18/21 11:30
1,2-Dichloroethane
ug/L
ND
1.0
06/18/21 11:30
1,2-Dichloropropane
ug/L
ND
1.0
06/18/21 11:30
1,4-Dichlorobenzene
ug/L
ND
1.0
06/18/21 11:30
2-Butanone (MEK)
ug/L
ND
5.0
06/18/21 11:30
2-Hexanone
ug/L
ND
5.0
06/18/21 11:30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
06/18/21 11:30
Acetone
ug/L
ND
25.0
06/18/21 11:30
Acrylonitrile
ug/L
ND
10.0
06/18/21 11:30
Benzene
ug/L
ND
1.0
06/18/21 11:30
Bromochloromethane
ug/L
ND
1.0
06/18/21 11:30
Bromodichloromethane
ug/L
ND
1.0
06/18/21 11:30
Bromoform
ug/L
ND
1.0
06/18/21 11:30
Bromomethane
ug/L
ND
2.0
06/18/21 11:30
Carbon disulfide
ug/L
ND
2.0
06/18/21 11:30
Carbon tetrachloride
ug/L
ND
1.0
06/18/21 11:30
Chlorobenzene
ug/L
ND
1.0
06/18/21 11:30
Chloroethane
ug/L
ND
1.0
06/18/21 11:30
Chloroform
ug/L
ND
5.0
06/18/21 11:30
Chloromethane
ug/L
ND
1.0
06/18/21 11:30
cis-1,2-Dichloroethene
ug/L
ND
1.0
06/18/21 11:30
cis-1,3-Dichloropropene
ug/L
ND
1.0
06/18/21 11:30
Dibromochloromethane
ug/L
ND
1.0
06/18/21 11:30
Dibromomethane
ug/L
ND
1.0
06/18/21 11:30
Ethylbenzene
ug/L
ND
1.0
06/18/21 11:30
lodomethane
ug/L
ND
20.0
06/18/21 11:30
m&p-Xylene
ug/L
ND
2.0
06/18/21 11:30
Methylene Chloride
ug/L
ND
5.0
06/18/21 11:30
o-Xylene
ug/L
ND
1.0
06/18/21 11:30
Styrene
ug/L
ND
1.0
06/18/21 11:30
Tetrachloroethene
ug/L
ND
1.0
06/18/21 11:30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
METHOD BLANK: 3299871
Associated Lab Samples: 92544681003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
06/18/21 11:30
trans-1,2-Dichloroethene
ug/L
ND
1.0
06/18/21 11:30
trans- 1,3-Dichloropropene
ug/L
ND
1.0
06/18/21 11:30
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
06/18/21 11:30
Trichloroethene
ug/L
ND
1.0
06/18/21 11:30
Trichlorofluoromethane
ug/L
ND
1.0
06/18/21 11:30
Vinyl acetate
ug/L
ND
2.0
06/18/21 11:30
Vinyl chloride
ug/L
ND
1.0
06/18/21 11:30
Xylene (Total)
ug/L
ND
1.0
06/18/21 11:30
1,2-Dichloroethane-d4 (S)
%
106
70-130
06/18/21 11:30
4-Bromofluorobenzene (S)
%
103
70-130
06/18/21 11:30
Toluene-d8 (S)
%
100
70-130
06/18/21 11:30
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3299872
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
58.5
117
70-130
1,1,1-Trichloroethane
ug/L
50
54.7
109
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
53.4
107
70-130
1,1,2-Trichloroethane
ug/L
50
50.7
101
70-130
1,1-Dichloroethane
ug/L
50
51.6
103
70-130
1,1-Dichloroethene
ug/L
50
53.0
106
70-132
1,2,3-Trichloropropane
ug/L
50
53.6
107
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
52.6
105
70-132
1,2-Dibromoethane (EDB)
ug/L
50
56.2
112
70-130
1,2-Dichlorobenzene
ug/L
50
54.7
109
70-130
1,2-Dichloroethane
ug/L
50
50.8
102
70-130
1,2-Dichloropropane
ug/L
50
52.5
105
70-130
1,4-Dichlorobenzene
ug/L
50
55.0
110
70-130
2-Butanone (MEK)
ug/L
100
109
109
70-133
2-Hexanone
ug/L
100
117
117
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
109
109
70-130
Acetone
ug/L
100
114
114
70-144
Acrylonitrile
ug/L
250
259
104
70-130
Benzene
ug/L
50
50.6
101
70-130
Bromochloromethane
ug/L
50
53.2
106
70-130
Bromodichloromethane
ug/L
50
53.5
107
70-130
Bromoform
ug/L
50
52.7
105
70-131
Bromomethane
ug/L
50
53.1
106
30-177
Carbon disulfide
ug/L
50
49.6
99
70-133
Carbon tetrachloride
ug/L
50
54.2
108
70-130
Chlorobenzene
ug/L
50
53.5
107
70-130
Chloroethane
ug/L
50
52.8
106
46-131
Chloroform
ug/L
50
53.3
107
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
LABORATORY CONTROL SAMPLE:
Parameter
3299872
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Chloromethane
ug/L
50
50.7
101
49-130
cis-1,2-Dichloroethene
ug/L
50
52.2
104
70-130
cis-1,3-Dichloropropene
ug/L
50
53.1
106
70-130
Dibromochloromethane
ug/L
50
57.0
114
70-130
Dibromomethane
ug/L
50
50.8
102
70-130
Ethylbenzene
ug/L
50
55.3
111
70-130
lodomethane
ug/L
100
119
119
47-140
m&p-Xylene
ug/L
100
111
111
70-130
Methylene Chloride
ug/L
50
53.0
106
68-130
o-Xylene
ug/L
50
54.3
109
70-130
Styrene
ug/L
50
55.5
111
70-130
Tetrachloroethene
ug/L
50
52.9
106
70-130
Toluene
ug/L
50
50.7
101
70-130
trans-1,2-Dichloroethene
ug/L
50
52.9
106
70-130
trans- 1,3-Dichloropropene
ug/L
50
54.9
110
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
65.1
130
25-200
Trichloroethene
ug/L
50
50.1
100
70-130
Trichlorofluoromethane
ug/L
50
46.4
93
61-130
Vinyl acetate
ug/L
100
119
119
70-140
Vinyl chloride
ug/L
50
46.2
92
59-142
Xylene (Total)
ug/L
150
165
110
70-130
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3299873
MS
92544751002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3299874
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.8
21.7
114
109
70-135
5
1,1,1-Trichloroethane
ug/L
ND
20
20
23.0
21.5
115
108
70-148
7
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.1
20.9
110
104
70-131
6
1,1,2-Trichloroethane
ug/L
ND
20
20
21.5
19.9
107
100
70-136
8
1,1-Dichloroethane
ug/L
ND
20
20
22.9
21.4
115
107
70-147
7
1,1-Dichloroethene
ug/L
ND
20
20
23.7
21.9
119
110
70-158
8
1,2,3-Trichloropropane
ug/L
ND
20
20
21.1
19.8
106
99
67-137
7
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
22.9
21.4
115
107
69-136
7
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
23.1
20.8
116
104
70-137
11
1,2-Dichlorobenzene
ug/L
ND
20
20
22.4
20.4
112
102
70-133
9
1,2-Dichloroethane
ug/L
ND
20
20
20.5
19.6
102
98
67-138
5
1,2-Dichloropropane
ug/L
ND
20
20
23.0
21.1
115
105
70-138
9
1,4-Dichlorobenzene
ug/L
ND
20
20
22.4
21.1
112
105
70-133
6
2-Butanone (MEK)
ug/L
ND
40
40
43.0
41.2
108
103
61-147
4
2-Hexanone
ug/L
ND
40
40
43.3
41.3
108
103
67-139
5
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
40.3
38.8
101
97
67-136
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3299873
MS
92544751002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3299874
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
43.7
42.0
109
105
55-159
4
Acrylonitrile
ug/L
ND
100
100
108
103
108
103
68-140
5
Benzene
ug/L
ND
20
20
22.4
21.1
112
106
67-150
6
Bromochloromethane
ug/L
ND
20
20
23.3
22.0
116
110
70-146
6
Bromodichloromethane
ug/L
ND
20
20
21.8
20.3
109
101
70-138
7
Bromoform
ug/L
ND
20
20
21.8
20.2
109
101
57-138
7
Bromomethane
ug/L
ND
20
20
18.4
19.1
92
96
10-200
4
Carbon disulfide
ug/L
ND
20
20
23.1
22.1
116
110
70-152
5
Carbon tetrachloride
ug/L
ND
20
20
22.6
21.0
113
105
70-147
8
Chlorobenzene
ug/L
ND
20
20
22.3
21.2
111
106
70-137
5
Chloroethane
ug/L
ND
20
20
25.0
23.4
125
117
51-166
7
Chloroform
ug/L
ND
20
20
23.5
22.2
118
111
70-144
6
Chloromethane
ug/L
ND
20
20
18.2
17.9
91
90
24-161
2
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.7
21.1
114
105
67-148
8
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.8
20.7
109
104
70-142
5
Dibromochloromethane
ug/L
ND
20
20
22.6
20.6
113
103
68-138
10
Dibromomethane
ug/L
ND
20
20
21.3
19.9
107
100
70-134
7
Ethylbenzene
ug/L
ND
20
20
22.1
21.3
111
106
68-143
4
lodomethane
ug/L
ND
40
40
68.3
62.9
171
157
20-161
8 M1
m&p-Xylene
ug/L
ND
40
40
44.8
42.0
112
105
53-157
6
Methylene Chloride
ug/L
ND
20
20
22.8
20.8
114
104
64-148
9
o-Xylene
ug/L
ND
20
20
22.6
21.1
113
105
68-143
7
Styrene
ug/L
ND
20
20
22.0
21.1
110
105
70-136
4
Tetrachloroethene
ug/L
ND
20
20
21.7
20.9
109
104
70-139
4
Toluene
ug/L
ND
20
20
21.8
20.7
109
104
47-157
5
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.4
22.0
117
110
70-149
6
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.4
20.5
107
103
70-138
4
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
18.2
17.1
91
86
31-145
6
Trichloroethene
ug/L
ND
20
20
22.3
20.8
112
104
70-149
7
Trichlorofluoromethane
ug/L
ND
20
20
19.5
18.8
98
94
61-154
4
Vinyl acetate
ug/L
ND
40
40
44.3
41.8
111
105
48-156
6
Vinyl chloride
ug/L
ND
20
20
21.3
19.7
107
98
55-172
8
Xylene (Total)
ug/L
ND
60
60
67.3
63.1
112
105
66-145
6
1,2-Dichloroethane-d4 (S)
%
99
98
70-130
4-Bromofluorobenzene (S)
%
101
99
70-130
Toluene-d8(S)
%
99
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Harrisburg Rd Landfill #60-01
Pace Project No.: 92544681
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2021 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 31

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Harrisburg Rd Landfill #60-01
92544681
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92544681001
6001-HBW12A
EPA 3010A
630001
EPA6010D
630321
92544681002
6001-HBW12B
EPA 3010A
630001
EPA6010D
630321
92544681003
6001-HBW21
EPA 3010A
630001
EPA6010D
630321
92544681004
6001-HBW22
EPA 3010A
630001
EPA6010D
630321
92544681005
6001-HBW17B
EPA 3010A
630001
EPA6010D
630321
92544681001
6001-HBW12A
EPA 3010A
629890
EPA6020B
629906
92544681002
6001-HBW12B
EPA 3010A
629890
EPA6020B
629906
92544681003
6001-HBW21
EPA 3010A
629890
EPA6020B
629906
92544681004
6001-HBW22
EPA 3010A
629890
EPA6020B
629906
92544681005
6001-HBW17B
EPA 3010A
629890
EPA6020B
629906
92544681001
6001-H BW 12A
EPA 8260D
627620
92544681002
6001-HBW12B
EPA 8260D
627620
92544681003
6001-HBW21
EPA 8260D
627663
92544681004
6001-HBW22
EPA 8260D
627620
92544681005
6001-HBW17B
EPA 8260D
627620
92544681006
Trip Blank
EPA 8260D
627620
Date: 06/30/2021 01:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 31

uocumeni ivame:
Sample Condition Upon Receii
c7C13 nals/tlCa%— Document No.:
F-CAR-CS-033-Rev.07
VaLUMCHL RCVJ]CU. V6lUUC1 ", GURU
SCURI Page 1 of 2
Issuing Authority:
Pace Caralinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville � Raleigh❑ Mechanicsville[]Atlanta❑ Kernersville❑
r
Sample• Client Name:Upon Receipt Project 4:
WO : 92544681
II ! 111 III II II II
❑ Commercial ❑Pace ❑Other:
92544681
Custody Seal Present? ❑Yes 'ONo Seals Intact? []Yes '®No
Date/Jnitial&oerson-EMamining-Gontent
Packing Material: ❑Bubble Wrap NBubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes ❑No gN/A
j.,IR Gun ID: 92TO64 Type or Ice: ""et ❑slue ❑None
0 . Correction Factor:
Cooler Temp: L Add/Subtract (°C) -0.1 Temp should be above freezing to 6•C
❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected('C): _)� 7t% hasbegun
USDA Regulated Soil ('Q N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC {check maps)? Did samples originate frarn a foreign source (internationally,
17Iv— mr'l , including Hawaii and Puerto Rico)? nYes r]No
Comments/Discrepancy:
Chain of Custody Present?
§g�Pes
[]No
❑N/A
1.
Samples Arrived within Hold Time?
g1res
❑No
❑NIA
2.
Short Hold Time Analysis (e72 fir.)?
❑Yes
WNo
[_]N/A
3.
Rush Turn Around Time Requested?
❑Yes
%No
❑N/A
4.
Sufficient Volume?
Yes
[:]No
[]N/A
5.
Correct Containers Used?
-Pace Containers Used?
[Yes
EffYes
[]No
No
❑N/A
❑NIA
6.
Containers Intact?
Yes
❑No
[—)N/A
7.
Dissolved analysis: Samples Field Filtered?
QYes
❑No
/A
B.
Sample Labels Match COC?
Ryes
[:]No
❑NIA
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
a
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
lZes
Yes
DIN
❑No
❑N/A
[—]N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Lot ID of split containers:
Date:
Date:
Field Data Required? ❑Yes []No
Page 29 of 31

uocument Name
uvLuMent nVV13t u. —UUM, co, LLGV
Document No.:
F•CAR-CS-033•Rev,07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
* *Bottom_half_of_box_is_to list_number_of_bottles_.—_._..._. _ __ -
Issuing Authority:
4 Pace Carolinas Quality Office
Project i WO# : 92544681
PM: MWB Due Dale: 06/30/21
CLIENT: 92-MECK CO
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pH Adjustment Log for Preserved Samples
Sample 10 Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative jot q
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
out of hold, incorrect preservative, out of temp, incorrect containers.
Page 30 of 31

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Page 31 of 31
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