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HomeMy WebLinkAbout6301_MooreCounty_MSWLF_CDLF_April2021GW_FID1586789_20210621ENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: • Prepare one form for each individually monitored unit. • Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). • Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. • Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). • Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): S&ME, Inc. (Consultant for Moore County) Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Edmund Q.B. Henriques Phone: 336-288-7180 E-mail: ehenriques@smeinc.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006) Moore County Landfill 456 Turning Leaf Way, 63-01 .0500 April 12-13, 2021 Aberdeen, North Carolina 28315 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑x Detection Monitoring ❑x Assessment Monitoring x❑ Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells Leachate monitoring data Surface water monitoring data ❑ Methane gas monitoring data Corrective action data (specify) Other(specify) Monitored Natural Attenuation Data Notification attached? No. No groundwater or surface water standards were exceeded. RX Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Edmund Q.B. Henriques, PG Senior Geologist / S&ME, Inc. 336-312-3330 Facility Representa 've Name (Print) Title (Area Code) Telephone Number 0!O! V '06/21/2021 Affix NC Licen Pr �,.► �inn Signature N u Date 8646 W. Market Street, Suite 105, Greensboro NC 27409 Facility Representative Address F-0176 NC PE Firm License Number (if applicable effective May 1, 2009) 14ologist Seal r% 4N_ d} L o Revised 6/2009 L3 PREPARED FOR: Moore County Solid Waste P.O. Box 1927 Carthage, North Carolina 28327 S&ME, Inc. 8646 West Market Street, Suite 105 Greensboro, North Carolina 27409 June 21, 2021 =0 June 21, 2021 Moore County Solid Waste Department P.O. Box 1927 Carthage, North Carolina 28327-1927 Attention: Mr. David Lambert via email: dlambert1 @moorecountync.gov Solid Waste Director Reference: Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Dear Mr. Lambert: S&ME, Inc. (S&ME) is pleased to submit this report documenting water quality monitoring conducted between April 12, 2021 through April 13, 2021 at the Moore County Solid Waste Facility located in Aberdeen, North Carolina. These services have been performed in general accordance with S&ME Proposal No. 43-2000335Rev1, dated August 3, 2020. One copy of this report is attached for your file and one copy has been delivered electronically on your behalf directly to the North Carolina Department of Environmental Quality - Division of Waste Management, Solid Waste Section. S&ME appreciates the opportunity to provide environmental services to Moore County. Please call us if you have any questions or comments. Sincerely, S&ME, Inc. 4 Edmund Q.B. Henriques, P.G. Senior Geologist/Project Manager ehenriques@smeinc.com Samuel P. Watts, P.G. Senior Environmental Consultant swatts@smeinc.com Jaclynne Drummond, Hydrogeologist, Solid Waste Section, Division of Waste Management, NC DEQ, 2090 US Highway 70, Swannanoa, NC 28778, jaclynne.drunnnnond@ncdenr.gov (electronic copy) Jimmy Brown, Landfill Manager, NC, 5227 Hwy 15-501, P.O. Box 1927, Carthage, North Carolina, 28327 (hard copy & electronic copy) S&ME, Inc. 18646 W. Market St, Ste 105 1 Greensboro, NC 27409 1 p 336.288.7180 1 www.smeinc.com Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Table of Contents 1.0 Executive Summary..........................................................................................................2 2.0 Background and Compliance History...........................................................................4 2.1 Background.....................................................................................................................................4 2.2 Compliance History....................................................................................................................... 5 3.0 Methods Employed...........................................................................................................7 3.1 Groundwater Sampling.................................................................................................................7 3.2 Surface Water Sampling................................................................................................................8 4.0 Site Hydrogeology............................................................................................................9 4.1 Groundwater Elevations and Flow Direction............................................................................ 9 4.2 Groundwater Flow Velocity.........................................................................................................9 5.0 Analytical Results...........................................................................................................10 5.1 Groundwater Analytical Data - MSW Landfill........................................................................11 5.2 Groundwater Analytical Data - C&D Landfill........................................................................12 5.3 Groundwater Analytical for Monitored Natural Attenuation Parameters ..........................13 5.4 Groundwater Analytical - Private Water Well........................................................................13 5.5 Surface Water Analytical Data...................................................................................................13 5.6 Quality Control.............................................................................................................................13 6.0 Discussion of Results.....................................................................................................14 7.0 References.........................................................................................................................15 List of Figures Figure 1 Groundwater Elevations and Contours - April 2021 Monitoring Event List of Tables Table 1 Active Monitoring Well Construciton Information Table 2 Groundwater Elevation Data Table 3 Groundwater Field Parameter Data Table 4 Groundwater Conductivities, Gradients, and Flow Velocities Table 5 Groundwater Monitoring Analytical Results (Detected Constituents) Table 6 Surface Water Monitoring Analytical Results (Detected Constituents) Appendices Appendix I -Sampling Forms Appendix II - Laboratory Analytical Reports Appendix III - Historical Analytical Results Appendix IV - Time vs Concentration Charts June 21, 2021 1 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina I S&ME Project No. 4358-20-043A, Task 01 ! 1.0 Executive Summary Between April 12 and April 13, 2021, sixteen monitoring wells and four surface water locations which monitor the Moore County Solid Waste Facility were sampled as part of the first semi-annual monitoring event for 2021. Monitoring wells MW-1, MW-2, MW-3, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9, MW-11SR, MW-11DR, MW- 13SR, MW-13DR, MW-14, MW-15R, MW-17S, MW-17D, MW-18 and MW-19 comprise the groundwater monitoring system for the closed municipal solid waste (MSW) landfill and active Construction & Demolition (C&D) landfill. The off -site water supply well at the Blake Residence was not sampled in accordance with the approved Water Quality Monitoring Plan. Samples were collected from surface water locations SW-1, SW-2, SW- 3, and SW-4. Groundwater and surface water sampling was conducted according to North Carolina Department of Environmental Quality, Division of Waste Management, Solid Waste Section (NCDEQ-SWS) guidelines. Samples were analyzed by a North Carolina certified laboratory. Samples collected were submitted for analysis in accordance with the facility's current NCDEQ-SWS approved Water Quality Monitoring Plan. Analyses of surface water samples collected detected no target constituent at a concentration exceeding the corresponding 15A NCAC 2B Standards (213 Standards). 1,4-Dioxane was detected at surface water sample locations SW-3 and SW-4 at concentrations greater than the corresponding North Carolina In -Stream Target Value for Surface Waters set at 0.35 micrograms per liter (pg/L) for Class WS (I-V) surface waters; however, no surface water standard promulgated by 15A NCAC 2B (213 Standard) currently exists for 1,4-Dioxane. The table below summarizes the MSW landfill monitor well locations where target constituents were detected at concentrations greater than the corresponding 15A NCAC 2L Groundwater Standards (2L Standards) or NCDEQ- SWS Groundwater Protection Standards (GWPS) during the April 2021 monitoring event: April 2021 Groundwater Sampling Event - MSW Landfill Monitoring Wells Constituent Concentration Detected Greater Than 2L Standard or GWPS MSW Landfill Monitoring Wells Parameter 2L Standards or GWPS MW-4 (pg/L) MW-6 (pg/L) MW-7 (pg/L) MW-8 (Ng/L) MW-9 (pg/L) 1,4-Dioxane 3 5.3 3.9 22 30 Benzene 1 2.6 3.2 3.2 Vinyl Chloride 0.03 1.2 2.2 Manganese 50 327 Iron 300 19,300 Note: Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. The 2L Standard exceedances for volatile organic compounds (VOCs) summarized above are generally consistent with historic monitoring results, which previously triggered regulatory requirements for implementation of Corrective Measures for the MSW landfill. In 2018, the NCDEQ-SWS requested all MSW and C&D landfills begin to analyze groundwater samples for 1,4-Dioxane. Thus, the number of observations for this parameter at the facility is currently limited. June 21, 2021 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 ! The table below provides a summary of the C&D landfill monitor well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the April 2021 monitoring event: April 2021 Groundwater Sampling Event - C&D Landfill Monitoring Wells Constituent Concentration Detected Greater Than 2L Standard or GWPS C&D Landfill Monitoring Wells Parameter 2L MW— MW— MW— MW— MW-14 MW— MW-17D MW-18 MW-19 Standard 11SR 11DR 13SR 13DR (Ng/L) 17S (fag/L) (pg/L) (Ng/L) or GWPS (Ng/L) (Ng/L) (Ng/L) (Ng/L (Ng/L) 1,4- 3 7.0 5.3 3.8 3.4 5.2 10 15 7.9 Dioxane Benzene 1 2.7 2.1 1.2 Vinyl 0.3 1.8 2.2 1.6 Chloride Iron 300 123,000 94,700 78,700 8,000 45,900 9,390 1,470 131,000 60,400 Manganese 50 372 178 683 150 67.6 104 241 229 Note: Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. The above listed exceedances are generally similar to the prior monitoring event, with the exception of 1,4- Dioxane at monitoring well MW-19, located adjacent to the property line. Shallow groundwater is estimated to flow to the west from the C&D landfill, with a portion migrating through monitoring well MW-19 prior to reaching Horse Creek, the expected local groundwater discharge point. This exceedance of the 2L Standard for 1,4-Dioxane at monitoring well MW-19, requires Moore County to notify the adjoining property owner (15A NCAC 13B .045(a)(2)) of the exceedance and update the facilities Assessment Monitoring Program (15A NCAC 13B .045(a)(3)). It is noteworthy that in 2020, Moore County initiated negotiations with the adjoining property owner, proposing a land swap that would increase Moore County's land ownership in the area west of the C&D landfill. The land swap would increase the potential to delineate groundwater constituents of concern on property to be owned by the landfill. An informal agreement was reached between the two parties, to divide properties for a land swap and land surveyors are under contract to begin parcel survey work after July 1, 2021. The Alternate Source Demonstration (ASD) prepared by Golder dated, February 28, 2017, indicated that VOCs detected in certain C&D landfill monitoring wells were attributed to the MSW landfill. NCDEQ-SWS responded indicating that they would not approve the ASD for VOCs at the C&D Landfill, at that time. NCDEQ-SWS requested that Moore County implement landfill gas and groundwater corrective action at the closed MSW landfill; and commence assessment monitoring at the C&D landfill pursuant to 15A NCAC 13B .0545. In response to the NCDEQ-SWS request, Moore County commenced with assessment monitoring at the C&D Landfill. At the MSW landfill, a methane cut-off trench was installed in 2018. Solar flares were added to the cut-off trench vents during early 2020. Monitored Natural Attenuation (MNA) was the selected groundwater remedy for the closed MSW landfill. MNA "Performance Monitoring" continue at MSW wells and select C&D wells. June 21, 2021 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Benzene and vinyl chloride in the vicinity of the MSW landfill generally exhibit trends of stable or declining concentrations over time, with a few exceptions. Concentrations of these constituents are not increasing immediately down -gradient of the source area. Due to the recent 2L Standard exceedance for benzene at monitoring well MW-18, concentration trends overtime should be reexamined during each subsequent monitoring event, to better understand the nature and extent of this detection. The size of the analytical data set for 1,4-dioxane is currently insufficient for accurate trend analysis. Considering constituent concentration trends, Moore County plans to continue Assessment Monitoring for the C&D landfill and MNA monitoring of the closed MSW landfill; unless evidence of increasing VOCs concentrations are confirmed or unless Moore County is directed by NCDEQ to proceed to the alternate groundwater remedy. Moore County is proactively evaluating options for alternate groundwater corrective actions that may be appropriate for the CAP contingency plan, including options that would aid in the management of landfill gases, which can contribute to groundwater exceedances. Plans for proposed pilot testing are forthcoming. 2.0 Background and Compliance History 2.1 Background Moore County currently operates a solid waste facility at 456 Turning Leaf Road, in Aberdeen, North Carolina. The facility is owned and operated by Moore County under Solid Waste Permit No. 63-01 issued by the NCDEQ-SWS. The facility includes a municipal solid waste (MSW) transfer facility, a closed unlined MSW landfill and an active C&D landfill unit. The C&D landfill unit and closed MSW landfill are regulated in general accordance with NCDEQ-SWS Permit No. 63-10. Moore County performs groundwater and surface water monitoring on a semiannual basis to comply with the requirements of North Carolina Solid Waste Management Rules (Solid Waste Rules), 15A NCAC 13B. S&ME has prepared this report on behalf of Moore County to present the results of the second monitoring event for 2020 as required by § .0600 and .1632 of the Solid Waste Rules. The Golder Associates NC, Inc. (Golder), Water Quality Monitoring Plan — Moore County Landfill, Permit No. 63-70, Volume 2 — Moore County Design Hydrogeological Report and Monitoring Plans (WQMP) dated December 10, 2019, is the current NCDEQ approved WQMP. Based on the WQMP there are two groundwater compliance well networks, with one background monitoring well providing background data for both networks. The active C&D landfill groundwater monitoring network consists of nine downgradient monitoring wells (MW-4, MW-11 SR, MW-11 DR, MW-13SR, MW-13DR, MW-14, MW-17D, MW-18 and MW-19). One monitoring well (MW-5) is shared by both the C&D landfill and MSW landfill for monitoring background groundwater quality. The closed MSW landfill groundwater monitoring network consists of eight downgradient monitoring wells (MW-1, MW-2, MW-3, MW-6, MW-7, MW-8, MW-9 and MW-15R). In addition, two C&D monitoring wells (MW-4, MW-11SR) are also used as MNA performance monitoring wells to assess groundwater impacts from the MSW landfill. The groundwater monitoring wells represent conditions in the uppermost aquifer underlying the facility, positioned for detection of potential releases from the landfill units; with some wells employed to assess the June 21, 2021 4 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - efficacy of natural attenuation as a corrective measure. Monitoring wells with "D" suffixes to the well identifier, represent wells screened within deeper portions of the surficial aquifer. The WQMP also involves four stream sample locations, one located on Horse Creek upstream of the facility and three sample locations at points downstream of the facility. One private water supply well on a parcel located east of the facility, the Blake residence well, was monitored in accordance with the approved WQMP. The C&D landfill is currently in Assessment Monitoring. The MSW landfill is currently in Corrective Action Monitoring, which includes MNA performance monitoring parameters for most monitoring wells. 2.2 Compliance History Groundwater quality has been monitored at the facility since 1987. Monitoring wells MW-1 through MW-4 monitored down -gradient regions of the MSW landfill, with MW-5 providing background water quality data for the facility. In March 1995, monitoring wells MW-6 through MW-9 were added to monitor the area between the MSW and the C&D landfill. An NCDEQ-SWS letter dated January 23, 1996, presented initial concerns regarding a potential for off -site migration of VOCs from the facility. Moore County voluntarily initiated corrective measure due to concerns of off - site migration of VOCs in groundwater and measured methane gas concentrations. In 1996, the off -site water supply well at the Blake residence (PW-1) was added to the groundwater monitoring program and monitoring of surface water points SW-2 and SW-1, commenced. Additional groundwater monitoring wells (MW-11 S, MW-11 D, MW-125, MW-12D, MW-135, MW-13D, and MW-14) were installed to assess the extent of groundwater impacts, establish monitoring points for the C&D facility, and to collected data to attempt differentiation of MSW groundwater impacts from C&D landfill impacts. Subsequently, monitoring wells MW12S and MW-12D were abandoned due to planned expansion of the C&D landfill, and replaced by monitoring wells MW-16S and MW16D, located further west and downgradient. In November 1999, HDR Engineering Inc. of the Carolinas (HDR) submitted a Work Plan to further investigate groundwater and methane migration concerns, with assessment activities commencing in March 2000. HDR reported the existence of a clay confining unit at depth beneath the landfill, which was reported to limit vertical groundwater contamination. In January 2005, NCDEQ-SWS requested that Moore County complete an assessment of corrective measures and select a remedy in accordance with 15A NCAC 2L .0106. In July 2005, HDR submitted the Assessment of Corrective Measures Report (ACM) to NCDEQ recommending monitored natural attenuation (MNA) as the primary remedy, with a contingency plan for active landfill gas (LFG) remediation if trends of increasing VOC concentrations over time were observed in groundwater. On November 21, 2005, NCDEQ-SWS approved HDR's ACM. In 2005, a shallow trench vent network consisting of a trench and 12 passive LFG vents were installed to address LFG migration concerns. In 2007, the LFG vent network was expanded with the addition of 12 passive LFG vents. In February 2014, three in -waste passive gas vent wells (GV-30, GV-31, and GV-32) were installed as part of the Joyce Engineering, Inc. Contingency Plan Update and Implementation Plan -Revised approved by NCDEQ-SWS on June 5, 2013. HDR prepared a revised Water Quality Monitoring Plan dated July 20, 2006, which was approved by NCDEQ-SWS on October 13, 2006. The 2006 plan involved monitoring all groundwater and surface water monitoring points for June 21, 2021 5 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - North Carolina Appendix I VOCs and the eight Resource Conservation and Recovery Act (RCRA) metals. MNA parameters were added for "performance monitoring" at select wells. In a letter from the NCDEQ-SWS dated April 18, 2008, NCDEQ-SWS agreed to the elimination of hydrogen, carbon dioxide, and volatile fatty acids from the semi-annual monitoring list, and to the completion of groundwater MNA modeling annually. This letter also specified that Moore County collect the full suite of "performance monitoring parameters" in April and October 2011, and present an MNA Corrective Action Evaluation Report (CAER) after completion of the October 2011 sampling event. Golder submitted a CAER report dated May 15, 2012. Subsequently, NCDEQ-SWS granted Moore County permission to continue MNA for another five-year period at the end of which another CAER report was required. Two additional surface water points (SW-3 and SW-4) were added to the compliance monitoring program upon approval of the May 2012 CAER. On March 10, 2016, Moore County met with NCDEQ-SWS to discuss groundwater impacts at the site and the effectiveness of previously implemented corrective actions. In this meeting and in a March 14, 2016, correspondence from NCDEQ-SWS, Moore County was asked to commence assessment monitoring at the C&D landfill or submit an alternate source demonstration (ASD) to demonstrate the impacts observed in the C&D landfill monitoring network were from a source other than the C&D landfill. On behalf of Moore County, Golder submitted the ASD for the Active C&D Landfill, dated February 28, 2017, identifying the upgradient closed MSW landfill as the source of VOCs at downgradient C&D wells. In two letters dated September 28, 2017, the NCDEQ-SWS indicated that they would not approve the ASD for VOCs at the C&D Landfill, at that time. They also requested that Moore County implement landfill gas and groundwater corrective action at the closed MSW landfill; and commence assessment monitoring at the C&D landfill pursuant to 15A NCAC 13B .0545. On December 6, 2017, after additional communications and a meeting with NCDEQ-SWS, Moore County submitted a letter confirming their intention to comply with the NCDEQ-SWS requests and requested an extension to comply, which was approved by NCDEQ-SWS on December 11, 2017. On behalf of Moore County, Golder submitted: A CAER dated October 16, 2017, An Assessment Monitoring Work Plan, dated January 5, 2018. A Landfill Gas Remediation Plan dated January 31, 2018, A Groundwater Corrective Action Milestone Schedule, dated January 31, 2018 (which included the submission of the NC Solid Waste .0500 Groundwater Corrective Action Application), and In accordance with Golder's Assessment Monitoring Work Plan, dated January 5, 2018, monitoring wells MW-11 SR, MW-11 DR, and MW-15R were subsequently installed to replace monitoring wells MW-11 S, MW-11 D, and MW-15. The replacement wells were sampled in June 2018, as part of the first assessment monitoring event for the C&D landfill. Groundwater samples collected from assessment monitoring wells were analyzed for constituents listed in North Carolina Appendix II and the C&D landfill indicator parameters required by NCDEQ-SWS (e.g., chloride, manganese, sulfate, iron, alkalinity, total dissolved solids (TDS), and tetrahydrofuran). Samples from monitoring wells MW-6 and MW-7 were also analyzed for Appendix II constituents, to further assess whether the groundwater impacts detected at the C&D landfill were attributable to the upgradient MSW landfill. In a letter dated February 22, 2018, NCDEQ approved a request made by Moore County to decommission monitoring wells MW-16S and MW-16D and replace them in the groundwater monitoring network with MW-175, June 21, 2021 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 MW-17D, and MW-18 which were to be installed in conjunction with the permitting of new Cell VI of the C&D landfill. Between May 31 and June 4, 2018, monitoring wells MW-17S, MW-17D, and MW-18 were installed, and monitoring wells MW-16S and MW-16D were properly abandoned. Monitoring wells MW-17S and MW-17D were first sampled during the routine semi-annual monitoring event conducted during November 2019. Monitoring well MW-18 was first sampled during the routine semi-annual monitoring event conducted in April 2020. During the April 2020 water quality monitoring event, groundwater monitoring was conducted at the closed MSW landfill in accordance with the approved Water Quality Monitoring Plan and Phase I of the Groundwater Corrective Action Milestone Schedule which was approved by NCDEQ-SWS on February 13, 2018. Phase I of the Groundwater Corrective Action Milestone Schedule included the following activities: Installation of the methane cut-off trench to the south of MW-15 (completed November 2, 2078) Replacement of MW-15 with MW-15R (completed June 1, 2018) Conversion of MW-15 to a compliance methane monitoring well (completed December 7, 2018) Continuation of MNA (as detailed in the approved Water Quality Monitoring Plan) In accordance with the approved Water Quality Monitoring Plan, dated December 10, 2019, hereafter referred to as the WQMP, monitoring wells in the MSW compliance network are corrective action MNA monitoring wells and are currently analyzed for VOCs listed in North Carolina Appendix I, RCRA metals, and an approved suite of MNA parameters (which includes chloride, ethane, ethene, methane, nitrate, sulfate, sulfide, total alkalinity, and total organic carbon). In addition, active C&D monitoring wells MW-4, MW-5, and MW-11SR are also sampled as corrective action MNA monitoring wells and analyzed for the same suite of MNA parameters. Analytical results for the April 2020 water quality monitoring event detected benzene at a concentration of 1.6 pg/L in monitoring well MW-18. Based on this apparent exceedance of the corresponding 2L Standard, a verification sampling event was conducted on June 5, 2020, with laboratory analyses reporting 1.2 pg/L Benzene. Based on the verified exceedance of the 2L Standard for benzene, an update of the Assessment Monitoring Program was required. On June 26, 2020, Golder installed new monitoring well MW-19 down -gradient (in the direction of contaminant migration) of monitoring well MW-18, near the facility boundary. Monitoring well MW- 19 was first sampled during the October 2020 water quality monitoring event, and sampled again in April 2021. The April 2021 monitoring event represents the first semi-annual water quality monitoring event for the facility in 2021. The event was conducted in general conformance with the WQMP, with the addition of sampling monitoring well MW-19, and analyzing the samples for North Carolina Appendix II constituents. 3.0 Methods Employed 3.1 Groundwater Sampling Groundwater sampling took place on April 12 and April 13, 2021. The groundwater monitoring well locations are shown on Figure 1. S&ME personnel performed sampling in general accordance with the facility's updated WQMP. Groundwater samples were collected from monitor wells MW-6, MW-7, MW-8, MW-9, and MW-15R representing the closed MSW landfill. Monitoring wells MW-4 and MW-11SR represent C&D monitoring wells also monitored as MNA performance wells for the MSW landfill. Monitoring wells MW-11 DR, MW-13SR, MW- June 21, 2021 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 13DR, MW-14, MW-175, MW-17D, MW-18, and MW-19 represent the active C&D landfill. Monitoring well MW-5 was sampled as the background well for both landfills. A groundwater sample was not obtained the off -site water supply well located on the Blake property. Details regarding monitoring well construction and monitored aquifer units are shown in Table 1. Prior to collecting groundwater samples, the monitor wells were opened and allowed to equilibrate with atmospheric conditions before gauging the liquid level. Groundwater depths were measured to an accuracy of ±0.01 feet using an electronic water level indicator, which was decontaminated before its initial use and between measurements. The measurements were collected to calculate relative groundwater elevations, to develop a groundwater potentiometric map, and to estimate the hydraulic gradient and groundwater flow direction at the time of the sampling event. Water level measurements are presented in Table 2 and Figure 1. After collection of groundwater levels, low -flow sampling methods were followed to purge and sample groundwater from the monitoring wells. As purging proceeded, an YSI ProPlus& multi -meter with a flow -through cell was used to measure field parameters that included pH, temperature, specific conductance, oxidation- reduction potential (ORP), and dissolved oxygen (DO). Turbidity was measured separately. The field data collected during sampling was recorded on the Low -Flow Groundwater Sampling Forms, included in Appendix I. A groundwater sample, for laboratory analysis, was collected after field parameters stabilized and the turbidity measurement was approximately 10 Nephelometric Turbidity Units (NTUs) or less. In accordance with the WQMP, water quality field parameters are considered stable once achieved for three consecutive measurements: Ph (+/- 0.2 S.U.), conductivity (+/- 5% of reading), temperature Ph (+/- 0.2 CO), and dissolved oxygen (+/- 10% of reading or 0.2 mg/L whichever is greater). ORP was measured and should fall within +/- 10 mV or reading; however, it was not a required stabilization parameter. Even with use of low -flow sampling methods, turbidity values obtained at some wells remained higher than target criteria. Accordingly, some samples were collected without meeting the turbidity goal. The field parameter measurements obtained are presented in Table 3. Groundwater samples from monitoring wells were collected using a peristaltic pump or bladder pump, and transferred directly into sample containers provided by the laboratory. Once filled, the sample containers were sealed, labeled, and placed in a cooler with ice. The samples were managed under chain -of -custody protocols and shipped to Environmental Conservation Laboratories, Inc. (ENCO), a North Carolina -certified laboratory. One blind duplicate sample and one equipment blank sample were collected for quality assurance and quality control (QA/QC). One trip blank accompanied each laboratory package under standard chain -of -custody procedures delivered from the laboratory and returned to the laboratory. Samples were stored in laboratory provided coolers with ice immediately after collection. The samples were delivered to ENCO, a NCDEQ certified laboratory for analysis. The samples were maintained under chain -of -custody procedures through delivery to the laboratory. 3.2 Surface Water Sampling Surface water sampling took place on April 13, 2021. Four surface water samples (SW-1, SW-2, SW-3, and SW-4) were collected from the locations shown in Figure 1. June 21, 2021 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Sample SW-2 was collected from Horse Creek northwest of the C&D landfill, and upstream of the facility. Downstream sample SW-1 was collected from an unnamed tributary of Horse Creek, south of the MSW landfill. Sample SW-3 was collected downstream of SW-1, prior to the tributary discharging into Horse Creek. Sample SW-4 was collected from an unnamed tributary that drains areas north of both the C&D and MSW landfills. After collection, the surface water samples were placed in a cooler with ice and placed under chain -of -custody. Surface water samples SW-1, SW-2, SW-3, and SW-4 were analyzed for North Carolina Appendix I constituents and 1,4- Dioxane. 4.0 Site Hydrogeology 4.1 Groundwater Elevations and Flow Direction The facility is situated within the Inner Coastal Plain Province of North Carolina. The uppermost aquifer beneath the facility is unconfined, approximately 55 feet thick, and consist of sands with thin clay seams, and seams of fine sand; reportedly underlain by a basal restrictive clay layer. The surficial aquifer is recharged by inflow from up - gradient areas and by precipitation infiltration. The uppermost aquifer underlying the landfill is expected to discharge to the local surface water features including Horse Creek and it's unnamed tributaries in the vicinity of the landfill. Shallow monitoring wells were installed in the surficial aquifer. Table 1 summarizes the well construction details for the facility's groundwater monitor wells. Static water level measurements collected during the April 2021 monitoring event (Table 2) were used to calculate the corresponding groundwater elevations based on surveyed top of casing (TOC) elevations. Groundwater elevations for the shallow water table monitoring wells and our interpretation of the groundwater surface expressed as a potentiometric map along with estimated groundwater flow directions shown on Figure 1. Based upon the groundwater potentiometric surface elevations, the overall shallow groundwater flow direction was estimated to be to the west. The hydraulic gradient (i) in the vicinity of a monitoring well was estimated by calculating the vertical difference between the groundwater elevation at a monitoring well and one or more nearby contour lines from Figure 1. This value was then divided by the horizontal distance measured from the well to the selected groundwater elevation contour line, utilizing a line formed perpendicular to the referenced groundwater elevation line. The calculated horizontal hydraulic gradient values determined for select wells are summarized in Table 4. 4.2 Groundwater Flow Velocity An approximate average linear groundwater flow velocity (V) was calculated using the following equation (Freeze and Cherry, 1979): V=Ki n where: V = Average linear groundwater flow velocity [feet per year (ft/yr.)] K = Hydraulic conductivity (ft/yr.) i = Flow gradient as a ratio (ft/ft) n = Effective soil porosity (percent) June 21, 2021 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Aquifer rising and falling head tests were previously performed at the site by HDR. The aquifer test data were used to estimate the hydraulic conductivity of the sediments in the surficial aquifer intersected by the screened intervals of the monitoring wells tested. The hydraulic conductivity, K, values previously measured at the site ranged from 0.84 feet per day (feet/day) to 16 feet/day. An average hydraulic conductivity value of 12.2 feet/day was used for calculating the site -wide flow velocity. The average hydraulic gradient of 0.01' ft/ft was calculated from data presented in Table 4. An effective soil porosity, n, of 25% was used as the site -wide average. The average groundwater flow velocity, V, for the site, using the equation and input values above, was estimated to be 145 feet/year. The average groundwater flow velocity information is summarized in Table 4. 5.0 Analytical Results In general accordance with the WQMP, background and compliance groundwater monitor wells were sampled during the April 2021 sampling event. The samples were analyzed by ENCO as follows: MSW landfill groundwater samples from monitoring wells MW-4, MW-6, MW-7, MW-8, MW-9 and MW- 15R were analyzed for constituents listed in the 40 CFR 258, Appendix I VOC analyte list using the analytical methods that included EPA Method 826013, 1,4-Dioxane by EPA Method 8260D SIM, the Eight RCRA Metals using EPA Method 6010/6020 and EPA Method 7470A. Analyses for MNA parameters included chloride by EPA Method 300.0, nitrate by EPA Method 353.2, nitrite by EPA Method 353.2, sulfate by EPA Method 300.0, sulfide by EPA Method 300.0, Total Alkalinity by EPA Method 310.2, and Total Organic Carbon by EPA Method 9060A. Carbon Dioxide, Ethane, Ethene, and Methane by RSK 175. The active C&D landfill groundwater samples from monitoring wells MW-11 SR, MW-11 DR, MW-13SR, MW-13DR, MW-14, MW-17D, MW-18, and MW-5 were analyzed for constituents listed in the 40 CFR 258, Appendix I analyte list using analytical methods EPA Method 8260B (VOCs), total metals by EPA Method 6010, 6020 and EPA Method 7470A. Classic chemistry indicator parameters chloride by EPA Method 300.0, sulfate by EPA Method 300.0, sulfide by SM 4500S2-D-2011, Total Alkalinity by EPA Method 310.2 and Total Dissolved Solids by Method SM 2540-C2011. Plus 1,4-Dioxane by EPA Method 8260D SIM. The active C&D landfill groundwater sample from monitoring well MW-19 was analyzed for constituents listed in the 40 CFR 258, Appendix II analyte list using analytical methods EPA Method 8260D (VOCs), EPA Method 8270E (SVOCs), EPA Method 8081B (pesticides), EPA Method 8082A (PCBs), EPA Method 8151A (herbicides), total metals by EPA Method 6010, 6020 and EPA Method 7470A. Classic chemistry indicator parameters chloride by EPA Method 300.0, sulfate by EPA Method 300.0, sulfide by SM 4500S2-D-2011, Total Alkalinity by EPA Method 310.2 and Total Dissolved Solids by Method SM 2540-C2011. Plus 1,4- Dioxane by EPA Method 8260D SIM. In addition, two C&D monitoring wells (MW-4, MW-11SR) are also used as MNA performance monitoring wells to assess groundwater impacts from the MSW landfill. The field measurements obtained are summarized on Table 3. A summary of constituents detected in groundwater is presented in Table S. For comparison purposes, these results are shown with their respective 2L Standard, which were revised and became effective April 1, 2013. Where target groundwater constituents have no established 2L Standard, the Method Detection Limit (MDL) is the default 2L Standard. However, the NCDEQ-SWS has listed constituent concentrations protective of groundwater, referred to as the Ground Water Protection June 21, 2021 10 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - Standards (GWPS) established in accordance with the Solid Waste Management Rules, Section .1634(h), which are used as the action level for detections where no 2L Standard is established. The chain -of -custody forms and the laboratory reports from ENCO are provided in Appendix II. Copies of the laboratory reports are provided in Appendix II. Effective December 1, 2006, NCDEQ-SWS changed the standard limits for comparing constituent detections in laboratory analysis from the Practical Quantitation Limits (PQLs) established in 1994 to the Solid Waste Reporting Limits (SWRLs). On February 23, 2007, the Section further revised the reporting limits from the SWRL to the Solid Waste Section Limit (SWSL). The SWSL was defined as the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy. In a memo dated May 29, 2018, the NCDEQ-SWS made a statement that technologies have advanced such over the past 12 years that the majority of the SWSLs are outdated. Given the rapid pace of technology, the NCDEQ- SWS decided that their attempt to continuously update and/or maintain the SWSLs is not warranted. As such, the use of SWSLs will be discontinued. According to the laboratory quality control performed by ENCO, detections above the MDL but below the PQL qualified as estimated values designated by the letter "J". 5.1 Groundwater Analytical Data - MSW Landfill The analytical data was reviewed by comparing constituent detections in the background and MSW compliance monitor wells to the laboratory's MDL. Multiple targeted constituents were detected above the MDL in one or more groundwater samples collected during the April 2021 monitoring event. Constituents with concentrations detected above the laboratory MDLs are summarized on Table S. Appendix III contains a table providing historic groundwater analytical results for constituents with concentration detected above the MDL. The following table provides a summary of the monitoring well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the April 2021 monitoring event: April 2021 Groundwater Sampling Event Constituent Concentrations Detected Greater Than 2L Standard or GWPS Parameter 2L Standards or GWPS MSW Landfill MW-4 (pg/L) Monitoring MW-6 (Ng/L) Wells MW-7 (Ng/L) MW-8 (pg/L) MW-9 (pg/L) 1,4-Dioxane 3 5.3 3.9 22 30 Benzene 1 2.6 3.2 3.2 Vinyl Chloride 0.03 1.2 2.2 Manganese 50 327 Iron 300 19,300 Note: Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. In accordance with NCDEQ-SWS guidance, where the 2L Standard or GWPS for a substance is less than the PQL, the detection of that substance at or above the PQL constitutes a violation of the 2L Standard or GWPS. The table June 21, 2021 11 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 ! above was prepared using this framework, which eliminates constituents reported with estimated concentrations ("Y values). Monitoring well MW-4 is located down -gradient of the MSW landfill and immediately upgradient of the C&D landfill. Monitoring well MW-4 is analyzed for the list of constituents applicable to the C&D landfill, to provide background groundwater quality data for the C&D landfill. Iron and manganese are very common constituents in coastal plain sediment; thus, they are naturally occurring in groundwater. The 2L Standard exceedances for the VOCs summarized above are generally consistent with prior detections, several of which historically triggered regulatory requirements for implementation of Corrective Measures for the MSW landfill. In 2018, the NCDEQ-SWS requested that all MSW and C&D landfills begin to analyze samples for 1,4-Dioxane. Thus, historic data for detections of this parameter at the landfill are limited. Appendix IV contains time vs concentration charts for benzene, vinyl chloride, and 1,4-Dioxane. These charts were prepared to examine trends in concentration changes overtime. 5.2 Groundwater Analytical Data - C&D Landfill The analytical data was reviewed by comparing constituent detections in the background and C&D landfill compliance monitor wells to the laboratory's MDL. Multiple targeted constituents were detected above the MDL in one or more groundwater samples collected during the April 2021 monitoring event. Constituent concentrations detected above the laboratory MDLs are summarized on Table S. Appendix III contains a table providing historic groundwater analytical results for constituents with concentration detected above the MDL. The table below provides a summary of the monitor well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the April 2021 monitoring event: April 2021 Groundwater Sampling Event Constituent Concentration Detected Greater Than 2L Standard or GWPS C&D Landfill Monitoring Wells Parameter 2L MW- MW- MW- MW- MW-14 MW- MW- MW-18 MW-19 Standard 11SR 11DR 13SR 13DR (pg/L) 17S 17D (pg/L) (pg/L) or GWPS (pg/L) (pg/L) (pg/L) (pg/L (pg/L) (pg/L) 1,4- 3 7.0 5.3 3.8 3.4 5.2 10 15 7.9 Dioxane Benzene 1 2.7 2.1 1.2 Vinyl 0.3 1.8 2.2 1.6 Chloride Iron 300 123,000 94,700 78,700 8,000 45,900 9,390 1,470 131,000 60,400 Manganese 50 372 178 683 150 67.6 104 241 229 Note: Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. June 21, 2021 12 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 ! In accordance with NCDEQ-SWS guidance, where the 2L Standard or GWPS for a substance is less than the PQL, the detection of that substance at or above the PQL constitutes a violation of the 2L Standard or GWPS. The table above was prepared using this framework, which eliminates constituents reported with estimated concentrations ("Y values). Appendix IV contains time vs concentration charts for benzene, vinyl chloride, and 1,4-Dioxane. These charts were prepared to examine trends in concentration changes overtime. 5.3 Groundwater Analytical for Monitored Natural Attenuation Parameters Groundwater analytical results for monitoring wells involved in Performance Monitoring for MNA parameters are summarized in Table S. 5.4 Groundwater Analytical — Private Water Well In accordance with the facility's Water Quality Monitoring Plan, the off -site private water well located on the Blake property to the north of the MSW landfill was not sampled during this monitoring event. 5.5 Surface Water Analytical Data Surface water samples were collected from the four designated sample locations illustrated on Figure 1. Horse Creek located west of the landfill is a stream classified by NCDEQ as a WSII, Water Supply. Laboratory analysis of the samples collected were compared to their respective 15A NCAC 2B (revised 6-10-2019) water quality standards for class WS surface waters (213 Standards). Table 6 provides a summary of constituents detected during the April 2021 monitoring event. The following constituents were detected at concentrations greater than their respective 2B Standards during the April 2021 event: April 2021 Surface Water Sampling Event Constituent Concentration Detected Greater Than 2B Standards Sample ID Detected Constituents Above NCAC 2B Standards It is noted that 1,4-Dioxane was detected at surface water sample location SW-3 and SW-4, at concentrations of 2.6 pg/L and 1.1 pg/L, respectively. These concentrations are greater than the corresponding North Carolina In -Stream Target Value for Surface Waters set at 0.35 pg/L for Class WS (I-V) surface waters; however, no 2B Standards currently exists. 5.6 Quality Control Quality assurance and quality control of field sampling methods and analytical test methods were assessed by collecting and analyzing one duplicate sample, one equipment blank sample, and one trip blank sample. The duplicate and equipment blank samples were analyzed for Appendix I constituents by the same methods and for June 21, 2021 13 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - the same target constituents as the record samples. Duplicate sample analysis documents the consistency of field sampling methods and the consistency of laboratory testing between samples. Equipment blank sample analysis documents the quality of sampling equipment and decontamination procedures used to reduce the potential of cross -contamination or carry-over effects from sampling equipment used on -site. The trip blank is analyzed for VOCs to document the effect of external conditions on samples/sample containers during lab pack preparation and transportation to and from the site. The concentrations of Appendix I VOCs and inorganic compounds detected in the record and in the duplicate samples collected from monitor well MW-15R were within an acceptable tolerance level and indicate a suitable replication of results from the test procedures. No targeted constituents were detected at concentrations above their respective laboratory method detection limits in the equipment blank sample. In the trip blank sample, no targeted constituents were detected above their respective laboratory MDLs. Some technical limitations exist in the laboratory's reporting of MDLs. MDLs for some VOCs and some inorganic constituents are above the applicable standards. The MDL for vinyl chloride (0.32 pg/L), cobalt (1.4 pg/L), and vanadium (1.4 pg/L) in groundwater are greater than the 2L Standard of 0.03 pg/L for vinyl chloride and the GWPSTs of 1.0 pg/L for cobalt and 0.3 pg/L for vanadium. Therefore, vinyl chloride, cobalt, and vanadium may have been present at concentrations above their respective 2L Standard/GWPS, but were reported as being below their respective MDLs. 6.0 Discussion of Results Moore County continues with assessment monitoring at the C&D Landfill. Monitored Natural Attenuation (MNA) is the selected groundwater remedy for the closed MSW landfill monitoring. MNA "Performance Monitoring" continues at MSW wells and select C&D wells. Analytical results of the April 2021 sampling event were generally consistent prior monitoring data, which demonstrated groundwater near the Moore County Landfill had been impacted by a release of waste constituents from the facility. Impacted groundwater at the facility does not appear to be adversely affecting surface water at the site. Benzene and vinyl chloride in the vicinity of the MSW landfill generally exhibit trends of stable or declining concentrations over time, with a few exceptions. Concentrations of these constituents are not increasing immediately down -gradient of the source area. The sample size of the groundwater data set for 1,4-dioxane is currently insufficient for reliable trend analysis. Benzene, vinyl chloride, and 1,4-dioxane detected at monitoring well MW-18, down -gradient of the C&D landfill, likely originated from the MSW landfill. The second consecutive detection of a 2L Standard exceedance for benzene at monitoring well MW-18, installed in 2020, should be evaluated over the next few sampling events to better understand the nature and extent of this detection. To date, benzene has not been detected in C&D landfill monitoring well MW-19, installed immediately down - gradient of MW-18. During this monitoring event 1,4-dioxane was detected in groundwater samples obtained from multiple MSW and C&D monitoring wells, including well MW-19 at a concentration greater than the corresponding 2L Standard. Furthermore, this monitoring event represent the 2nd consecutive monitoring event where groundwater samples obtained from monitoring well MW-19 were analyzed for the full Appendix II constituent list, to establish a baseline for this well. June 21, 2021 14 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 In consideration of the VOC concentration trends over time, Moore County plans to continue Assessment Monitoring for the C&D landfill and MNA monitoring of the closed MSW landfill; unless evidence of increasing VOCs concentrations are confirmed or unless Moore County is directed by NCDEQ to proceed to the alternate groundwater remedy. Moore County is proactively evaluating options for alternate groundwater corrective actions that may be appropriate for the CAP contingency plan, including options that would aid in the management of landfill gases, which can contribute to groundwater exceedances. 7.0 References Department of Environment and Natural Resources, Division of Water Quality, 75A NC Administrative Code Subchapter 2B .0200 Classifications and Water Quality Standards Applicable to Surface Waters and Wetlands of NC, November 2019. Surface Water Standards Tables updated 06-10-2019. Department of Environment and Natural Resources, Division of Water Quality, 75A NC Administrative Code Subchapter 2L .0200 Groundwater Quality Standards, April 2013. Department of Environment and Natural Resources, Division of Waste Management, 75A NC Administrative Code Subchapter 13B .1634(h) Solid Waste Groundwater Protection Standard, Solid Waste Management Rules, November 2004. Golder Associates NC, Inc. (Golder), Alternate Source Demonstration for Active C&D Landfill, Moore County Construction and Demolition Landfill, NC SWP# 63-01, Submitted to NC DEQ: February 28, 2017. Golder Associates NC, Inc. (Golder), Assessment Monitoring Work Plan, Moore County Construction and Demolition Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 5, 2018. Golder Associates NC, Inc. (Golder), Corrective Action Evaluation Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: May 15, 2012. Golder Associates NC, Inc. (Golder), Groundwater Corrective Action Evaluation Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: October 16, 2017. Golder Associates NC, Inc. (Golder), Groundwater Corrective Action Milestone Schedule, Moore County Closed MSW Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 31, 2018. Golder Associates NC, Inc. (Golder), Landfill Gas Remediation Plan, Moore County Closed MSW Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 31, 2018. Golder Associates NC, Inc. (Golder), Request for Extension, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: December 6, 2017. Golder Associates NC, Inc. (Golder), Request for Monitored Natural Attenuation Parameter Modification, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: January 22, 2008. June 21, 2021 15 Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - Golder Associates NC, Inc. (Golder), Response to Letters Received from NC DEQ Dated September 28, 2077, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: October 26, 2017. Golder Associates NC, Inc. (Golder), Second Semi -Annual Water Quality Monitoring Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: March 29, 2017. Golder Associates NC, Inc. (Golder), Water Quality Monitoring Plan, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: Submitted to NC DEQ: December 10, 2019. HDR Engineering, Inc. of the Carolinas (HDR), Addendum to Plan to Address Potential Contamination, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: March 20, 2000. HDR Engineering, Inc. of the Carolinas (HDR), Assessment of Corrective Measures Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: July 29, 2005. HDR Engineering, Inc. of the Carolinas (HDR), Phase I Environmental Assessment, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: November 30, 1999 HDR Engineering, Inc. of the Carolinas (HDR), Water Quality Monitoring Plan, Moore County Landfill, NC SWP# 63- 01, Submitted to NC DENR: July 20, 2006. Joyce Engineering, Inc., Contingency Plan Update and Implementation Plan - Revised, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: May 16, 2013. North Carolina Department of Environment, Health, and Natural Resources (NC DEHNR), Division of Solid Waste Management, Water Quality Monitoring at Moore County Sanitary Landfill, Moore County Landfill, NC SWP# 63- 01, NC DEHNR to Moore County: January 23, 1996. North Carolina Department of Environment and Natural Resources (NC DENR), Division of Waste Management, Request for Monitored Natural Attenuation Parameter Modification, Moore County Landfill, NC SWP# 63-01, NC DENR to Moore County: April 18, 2008. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Alternate Source Demonstration, Moore County Construction and Demolition Landfill, NC SWP# 63- 01, NC DEQ to Moore County: September 28, 2017. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Groundwater Corrective Action and Landfill Gas Corrective Action, Moore County Closed MSW Landfill, NC SWP# 63-01, NC DEQ to Moore County: September 28, 2017. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Groundwater Corrective Action Milestone Schedule, Moore County Closed MSW Landfill, NC SWP# 63-01, NC DEQ to Moore County: February 13, 2018. June 21, 2021 16 TABLE 1 Active Monitoring Well Construction Information Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A = 0 III MW-1 OR 06/05/87 & 508605.64 1854636.41 Ground Surface Elevation 390.70 Measuring Point Elevation 392.87 Total Well r- 20 Well Depthinates 370.70 Di:ete 2 Interval 6.97 - 17.07 Interval 383.73 - 373.63 Geology of Screened Interval Sand Monitored Landfill Unit MSW Landfill MW-2 06/06/87 508508.07 1853819.73 373.39 375.50 20 353.39 2 7.52-17.77 365.87 - 355.62 Sand MSW Landfill MW-3 06/06/87 508781.79 1852845.34 362.00 363.82 16.5 345.50 2 5.75 - 15.88 356.25 - 346.12 Sand and Silty Clay MSW Landfill MW-4 06/06/87 509793.80 1853641.22 363.40 366.19 15 348.40 2 4.28 -14.09 359.12 - 349.31 Sand and Silty Clay C&D Landfill MW-5 06/06/87 510970.55 1853091.84 384.06 386.61 20 364.06 2 6.96-17.21 377.10 - 366.85 Sand and Clayey Sand Background MW-6 03/06/95 510385.96 1853881.79 403.50 405.86 20 383.50 2 5.00 - 20.00 398.50 - 383.50 Sand to Silty Sand MSW Landfill MW-7 03/06/95 509783.24 1853820.43 399.20 402.01 20 379.20 2 4.00 - 19.00 395.20 - 380.20 Sand, Silt, Silty Sand, Clay MSW Landfill MW-8 03/06/95 509384.99 1853844.10 395.20 397.85 20 375.20 2 5.00 - 20.00 390.20 - 375.20 Sand, Silt, Silty Sand, Clay MSW Landfill MW-9 03/06/95 508964.80 1854268.28 403.70 406.06 30 373.70 2 15.00 - 30.00 388.70 - 373.70 Silty Sand MSW Landfill MW-11SR 06/01/18 510452.38 1852905.36 383.41 386.13 28 355.41 2 18.00 - 28.00 358.13 - 368.13 Clayey Sand C&D Landfill MW-11DR 05/31/18 510453.00 1852911.56 383.41 386.36 44 339.41 2 34.00 - 44.00 342.36 - 332.36 Sand C&D Landfill MW-13SR 06/24/20 509541.34 1853156.68 383.87 386.57 20 363.87 2 10.00-20.00 373.87 - 363.87 Sand C&D Landfill MW-13SD O6124120 509549.23 1853164.04 383.31 385.99 40 343.31 2 30.00-40.00 353.31-343.31 Sand/Clay C&D Landfill MW-14 09/16/96 510056.32 1853641.99 397.88 400.58 20 377.88 2 5.00 - 20.00 392.88 - 377.88 Sand to Silty Sand Upgradient of C&D Landfill MW-15 09/19/96 510597.22 1854401.13 429.31 431.10 35 394.31 2 20.00 - 35.00 409.31 - 394.31 Sand to Silty Sand MSW Landfill MW-15R 05/29/18 510589.03 1854391.51 428.81 431.48 47 381.81 2 37.00 - 47.00 384.48 - 374.48 Sand MSW Landfill MW-17S 05/31/18 509704.03 1852096.70 371.45 374.16 18 353.45 2 8.00 - 18.00 363.45 - 353.45 Sand C&D Landfill MW-17D 06/01/18 509693.71 1852101.52 372.05 374.56 34 338.05 2 29.00 - 34.00 343.05 - 338.05 Clay/Sandy-Clay C&D Landfill MW-18 06/04/18 509369.85 1852249.28 365.35 368.50 13 352.35 2 5.00 - 13.00 360.35 - 352.35 Gravelly Sand, Sand, Sandy Clay C&D Landfill MW-19 06/25/20 509324.26 1852158.78 363.95 366.67 13 350.95 2 5.00-13.00 358.95 - 350.95 Sand C&D Landfill GP-10R O6/25/20 508889.16 1855952.87 431.90 434.21 15 416.90 2 5.00-15.00 426.90 - 416.90 Sand MSW Landfill GP-13R 05/31/18 509405.06 1852208.08 367.1 370.29 10 357.10 2 3.00-10.00 364.10 - 357.10 Sand C&D Landfill GP-14R 05/30/18 509680.01 1852109.63 372.05 374.78 10 362.05 2 3.00 - 10.00 369.05 - 362.05 Clayey Sand to Sand C&D Landfill GP-15R 06/04/18 510038.89 1852041.09 364.85 367.73 10 354.85 2 3.00 -10.00 361.85 - 354.85 Sandy Clay, Gravelly Sand C&D Landfill GP-19 06/25/20 510494.25 1853794.49 397.08 399.33 10 387.08 2 5.00-10.00 393.08 - 387.07 Sand MSW Landfill Notes: 1.) ft AMSL = feet above mean sea level 2.) ft BGS = feet below ground surface 3.) Well construction information for monitoring wells MW-1 through MW-16S/D collected from boring logs and well construction records from HDR Engineering, Inc. of the Carolinas July 2006 Water Quality Monitoring Plan. TOC and Ground Elevations are taken from the July 2005 Assessment of Corrective Measures Report and/or well records where available. 4) Well construction information for monitoring well MW-19 obtained from boring logs and well construction records from Golder, Inc. Active C&D Groundwater Monitoring Network Well ID MW-4 MW-11SR 1` MW-11DR MW-13SR MW-13DR �� MW-14 �,MW-17S MW-17D MW-18 MW-19 TOC Elevation (ft AMSL) 3��366.19 386.1' 386.36 386.57 385.9' 400.58� 374.16 374.56 368.50 366.67 Measurement Date GWE DTW GWE 93TW GWE DTW GWE DTW GWE §DTW GWE DTW' GWE DTW GWE DTW GWE DTW GWE DTW (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) Background Well 10"W Groundwater Monitoring Network Well ID MW-5 MW-1 IN MW-2 ` WW-6 , �W-8 MW-9 MW-15 TOC Elevation 386.61 392.87 ' 375.50 M05.86 , 406.06 431.38 (ft AMSL) Measurement Date GWE DTW GWE DTW GWE jF DTWj GWE DTW GWE DTW WE 1FDTW GWE DTW GWE DTV (ft AMSL) (ft) (ft AMSL) (ft) AMSL) I (ft) (ft AMSL) (ft) (ft AMSL) (ft) AMSL) =11 SL) (ft) (ft AMSL) (ft`1ft AMSL) (ft) TABLE 3 Groundwater Field Parameter Data Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Notes: 1.) mg/L = milligrams per liter 2.) ND = not detected at or above the laboratory reporting limit 8) NS = Not Sampled 3.) NM = not measured 4.) uS/cm = microseimens per centimeter 5.) NTU = Nephelometric Turbidity Units 6.) S.U. = Standard Units 7.) Samples collected using low -flow purge and sample techniques (when possible). TABLE 4 Groundwater Conductivities, Gradients and Calculated Flow Velocities Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project Number 4358-20-043A •ctober MW-1 1.6E+01 25% WNS WNS MW-2 1.6E+01 25% WNS WNS MW-3 3.4E+00 25% WNS WNS MW-4 7.7E+00 25% 0.015 167 MW-5 7.1 E+00 25% 0.020 210 MW-6 9.8E+00 25% 0.020 286 MW-7 8.4E-01 25% 0.019 23 MW-8 1.8E+01 25% 0.007 195 MW-9 4.2E+01 25% 0.006 360 MW-14 8.8E+00 25% 0.019 238 MW-15R 4.8E+00 25% 0.017 118 Mean Values-7 1.22E+01 25% 0.011 145 Notes: (1) Hydraulic Conductivity was calculated from slug tests performed by HDR (2) Effective porosity is an estimated value, actual values will vary (3) Hydraulic gradient calculated by measuring linear feet along a line between selected monitor well and contour line. (4) Seepage velocity v = (K*i)/ne (5) WNM = Well Not Monitored During This Event T:\ENV\Projects\202M4358-20-043A Moore County Routine LFG 8 WQ Monitoring\Task 01 -Semi-Annual Water Quality FV 2020-2021\Working_D....nts Spring 2021 Eent\2021-04 WQMR Tables 20210610Ax . 6/2012021 TABLE 5 Groundwater Analytical Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A or Constituent/Parameter DetectedINFL U - ate 10 GWPS 700 Background MW-5 32.7 W 55.0 22.0 48.3 :D Monitoring MW-14 18.2 Wells MW-17S 136 MW-17D 22.4 MW-18 89.5 MW-19 103 :D Performance for the Closed MW-4 103 Wells MSW Landfill MW-11SR 89.0 MW-11 NS Closed MW-2 NS MSW Monitoring MW-3 NS Wells & MNA MW-6 46.0 Performance Monitoring MW-7 MW-8 38.4 66.6 Wells � MW-9 78.2 25.0 Off -site Private Well 6;" NS Barium u /L 04/13/21 1.1 Cadmium u /L 04/13/21 0.36 1 2 ND 0.526 J 0.572 J ND ND ND ND 0.811 J ND ND ND NS NS NS 1.04 1.25 0.612 J ND 0.855 J NS Cobalt u /L 04/13/21 1.4 10 1 ND 1.63 J ND 1.43 J ND ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS Copper u /L 04/13/21 1.6 10 1000 ND ND 1.97 J ND 3.37 J ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS Lead u /L 04/13/21 3.1 10 15 ND 8.39 J 9.88 J ND 7.00 J 3.98 J ND ND 7.90 J 5.15 J 11.5 NS NS NS 4.25 J 4.39 J 13.9 10.9 13.0 NS Zinc u /L 04/13/21 4.4 10 1000 ND ND 6.32 J ND ND ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS Mercury u /L 04/13/21 0.150 0.200 1 ND ND ND ND ND ND ND ND ND 0.476 ND NS NS NS ND ND ND ND ND NS Iron u /L 04/13/21 22 50 300 ND 94,700 78,700 8,000 45,900 9,390 1,470 131,000 60,400 19,300 123,000 NS NS NS ANR ANR ANR ANR ANR NS Manganese u /L 04/13/21 1.5 10 50 4.80 J 178 683 150 67.6 104 37.3 241 229 327 372 NS NS NS ANR ANR ANR ANR ANR NS Acetone u /L 04/13/21 10.0 20 6000 ND ND ND ND 120 ND ND 11 J 22 ND 10 NS NS NS 46 75 ND ND ND NS Benzene u /L 04/13/21 0.15 1 1 ND 2.1 ND ND ND ND ND 1.2 ND ND 2.7 NS NS NS 2.6 1.0 3.2 3.2 0.78 J NS Chlorobenzene u /L 04/13/21 0.17 1 50 ND 1.3 ND ND 1.5 ND ND 0.91 J ND 0.53 J 1.6 NS NS NS 1.5 0.90 J 3.8 10 ND NS 1,2-Dichlorobenzene u /L 04/13/21 0.19 1 20 ND 0.51 J ND ND ND ND ND 0.55 J ND ND ND NS NS NS ND ND ND ND ND NS 1,4-Dichlorobenzene u /L 04/13/21 0.19 1 6 ND 3.1 ND ND ND ND ND 2.0 ND ND 2.4 NS NS NS 1.6 0.81 J 3.1 2.7 ND NS 1,1,-Dichloroethane ug/L 04/13/21 0.13 1 6 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND 0.56 J ND ND NS cis-1,2-Dichloroethene ug/L 04/13/21 0.15 1 70 ND 3.0 ND ND ND ND ND 2.9 1.5 1.9 1.2 NS NS NS 1.2 0.61 J 0.71 J 1.2 2.5 NS Vinyl chloride ug/L 04/13/21 0.32 1 0.03 ND 2.2 0.86 J ND 0.85 J ND ND 1.6 0.60 J 0.50 J 1.8 NS NS NS 1.2 2.2 ND ND ND NS 1,4-Dioxane ug/L 04/13/21 0.8 2.0 3 ND 5.3 3.8 3.4 5.2 0.90 J 10 15 7.9 5.3 7.0 NS NS NS 1.7 3.9 22 30 2.2 NS Tetrahydrofuran ug/L 04/13/21 0.53 1.0 NS ND ND ND ND ND ND ND ND ND 8.6 7.5 NS NS NS ANR ANR ANR ANR ANR NS Sulfide ug/L 04/13/21 100 10 NA ND 49 J ND ND 370 ND ND 30 J ND ND 110 NS NS NS 0.190 ND 110 160 35 J NS Chloride u /L 04/13/21 2200 5000 NA 2,900 J 22,000 8,400 6,800 15,000 8,200 2,900 51,000 36,000 30,000 34,000 NS NS NS 13,000 10,000 50,000 99,000 D 3,100 J NS Nitrate as N u /L 04/13/21 41 100 NA 1,400 ANR ANR ANR ANR ANR ANR ANR ANR 220 ND NS NS NS ND 0.65 ND ND ND NS Nitrite as N u /L 04/13/21 17 100 NA ND ANR ANR ANR ANR ANR ANR ANR ANR ND ND NS NS NS ND ND ND ND ND NS Total Dissolved Solids u /L 04/13/21 50000 50000 NA ND 270,000 82,000 30,000 74,000 240,000 250,000 470,000 350,000 520,000 680,000 NS NS NS ANR ANR ANR ANR ANR NS Sulfate as SO4 u /L 04/13/21 2900 5000 NA 2,900 12,000 18,000 10,000 19,000 20,000 33,000 45,000 23,000 110,000 14,000 NS NS NS 11,000 ND ND ND 6,800 NS Total Alkalinityas CaCO3 u /L 04/13/21 14000 15000 NA ND 260,000 34,000 21,000 42,000 24,000 160,000 320,000 D 200,000 D 260,000 730,000 D NS NS NS 240,000 300,000 230,000 D 760,000 110,000 NS Total Organic Carbon u /L 04/13/21 540 1000 NA 1,000 ANR ANR ANR ANR ANR ANR ANR ANR 42,000 34,000 NS NS NS 57,000 26,000 18,000 34,000 2,500 NS Nitrate/Nitrite as N u /L 04/13/21 41 100.0 NA 1,400 ANR ANR ANR ANR ANR ANR ANR ANR 220 ND NS NS NS ND 0.65 ND 100 ND NS Ethane u /L 04/13/21 5.1 6 NA ND ANR ANR ANR ANR ANR ANR ANR ANR ND ND NS NS NS ND ND ND ND ND NS Ethene u /L 04/13/21 5.1 6 NA ND ANR ANR ANR ANR ANR ANR ANR ANR ND ND NS NS NS ND ND ND ND ND NS Methane u /L 04/13/21 5.1 6 NA ND ANR ANR ANR ANR ANR ANR ANR ANR 323 3,280 NS NS NS 0.012 5,910 D 6,370 D ND 1,640 NS Carbon dioxide u /L 04/13/21 2070 2500 NA 28,100 ANR ANR ANR ANR ANR ANR ANR ANR 217,000 D 423,000 NS NS NS ND 373,000 D 126,000 ND 242,000 NS Ferrous Iron (Field Measure) ug/L 04/13/21 NA NA I NA 0 ANR ANR ANR ANR ANR ANR ANR ANR 11,000 <10,000 NS NS NS 10,000 >10,000 >10,000 2,400 10,000 NS Notes: 1.) ug/L = Micrograms per liter 2.) ND = Not detected at the stated reporting limit 3.) NA = Not Applicable 4.) J = Estimated concentration reported below Solid Waste Section Limit 5.) ANR = Analysis Not Requested 6.) Bold and highlighted in yellow = Concentration above the current 15A NCAC 02L Groundwater Standard, 7.) NS = Not Sampled 8.) GWPS = Solid Waste Section Groundwater Protection Standard 9.) PQL = Practical quantitation limit - lab specific limit 10.) MDL = Method Detection Limit 15A NCAC 2L IMAC Groundwater Standard, or NC Solid Waste Section Groundwater Protection Standards (GW PS) TAEN\APrcj-t2020413520- MM-County Roud-LFG&WG Ma1.Mg\Task 01-Semi-Annual Water Quality FY 2020-2021\Warkhg_Documenta Sprang 2021 E-62O1-N WGMR Tablea_20210610A.. Page 5of6 TABLE 6 Surface Water Monitoring Analytical Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project Number 4358-20-043A Notes: 1.) MDL = Method Detection Limit 2.) ug/L = micrograms per liter 3.) ND = Not detected at or above MDL 4.) J = Estimated value 5.) -- = Not applicable 6.) Shaded = Constituent exceeds applicable Surface Water Standard 7.) Blanks = Field, trip and method blanks 8.) Surface Water Standards based on WS-II, High Quality Water Classification for Horse Creek and its tributary per 15A NCAC 02B. 9.) SW Standard for lead is a Narrative Standard per 15A NCAC 02B .0211 10.) Upstream and downstream designations based on inspection of site conditions and flow regimes. Reports prior to October 2009 had the designations inadvertently switched. 11.) For standards based on hardness dependent calculations, acute and chronic values shown are based on a worse -case 25 mg/L hardness 12.) NC Protective values are listed within 15A NCAC 02B, but they are not 2B Standards r P N­jada\2020W353-20-0 Mows County Routine LFG& WO Ma nng\Taak0t-Seml-Mnual Water Oualiy FY 2020-2021\WorkinlLDocumenla Spmg 2021 Event12021-00 WOMRTables202108 .4 i �j SW-2 [ F / Wr GROUND OBSCURED SEE ACCURACY NOTE y\ O)\ MW-16S\ PELELL 6\\ \ )ONED)' �� 1\ " C 7— Co Co W-111.48D 37� M W-11 S ��M W-11 D ACTIVE ` C&D 0L 420 430 � GP-18 P BLAKE RESIDENCE (CRAWL SPACE MONITORED) I \_\ °' 3s.6VIU 6 ("�% I � 6 .4. 3 2 1 ° o° ° , G — �. ` ° ° 8 �Jo / I 2 1 10 \� e °°Ilo i o "22'""24- ° 0 0 �W( 8 19 2 23' lyug° 32 o D II ° CLO SED C o�M 71 _ LAN6�FF6�((�� �\ to �yo�D l fr 00 MAINTENANCE SHOP _ c _ --_ -= ° ✓ _ 383.83 / \� IND OBSCURED � \ ACCURACY NOTE �- ^� \ `SW3� REFERENCE: GENERAL SITE FEATURES, LANDFILL LIMITS OF WASTE, PARCEL BOUNDARIES AND WELL LOCATIONS PROVIDED BY GOLDER IN 2020. 0 400 800 GRAPHIC SCALE (IN FEET) 0 U O e \ Q a ` a I J z J 0 0 z cg� Q Q J U 2 Z) 0 0 LU z cf�w T SCALEHOUSE TRANSFER STAll%W.UFFICE _ _ I o I r �c J �7 'v cW-2 o ' ^ SCALE: AS SHOWN SW-1❑ ��� _ DATE: MAY 2021 PARCEL BOUNDARY 4 GROUNDWATER FLOW DIRECTION PROJECT NUMBER ■ ■ APPROXIMATE LIMITS OF WASTE 363.30 MEASURED GROUNDWATER ELEVATION IN MONITORING WELL EXISTING 2 FT GROUND SURFACE CONTOUR O MONITORING WELL 4358-20-043A EXISTING 10 FT GROUND SURFACE CONTOUR O ABANDONED MONITORING WELL FIGURE NO. STREAM, POND AND WETLAND LIMITS PASSIVE LANDFILL GAS VENTS EXISTING ROAD JZ( LANDFILL GAS TRENCH VENT MSW LANDFILL COMPLIANCE BOUNDARY ❑ SURFACE WATER SAMPLE C&D LANDFILL COMPLIANCE BOUNDARY 0 ABANDONED METHANE PROBE 365 — — — POTENTIOMETRIC GROUNDWATER CONTOUR (5ft INTERVAL) A METHANE PROBE Appendices Appendix I -Sampling Forms Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: April 13, 2021 Project Name: Project Location: Project Number: Source Well: MW-4 Purge Time: 35 Minutes Locked?: Yes Sample Date: April 13, 2021 Sampled By: Gary Simcox Sample Time: 12:25 Weather: Sunny I Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 12:15 0.9 100 6.25 16.1 6.4 883 0.2 -41 12.9 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 12:25 Sample End Time: 12:45 Analytical Data Name (1) Gary Simcox Signature Date 4/13/2021 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (10.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 6.04 ft-TOC Total Well Depth: 16.55 ft-TOC Height of Water Column: 10.51 feet Screen Length: 10 feet Stickup: 2.7 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.7 Gal 3 *Well Volume 5.15 Gal 5 *Well Volume 8.58 Gal Purge Method: Peristaltic Pump Start Time: 11:40 End Time: 12:15 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 11.5 ft-TOC Water Column Above Pump Intake: 5.46 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 7.41 ft-TOC Comments: Final Volume Purged: 0.9 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (p5/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 11:40 0.0 --- --- --- --- --- --- --- --- Start Purging 11:45 0.1 100 6.22 16.3 6.4 890 0.4 -55 14.5 11:50 0.3 100 6.25 16.0 6.4 887 0.3 -45 15.2 11:55 0.4 100 6.25 16.0 6.4 885 0.2 -43 17.2 12:00 0.5 100 6.25 16.1 6.4 882 0.2 -42 16.7 12:05 0.7 100 6.25 16.0 6.4 882 0.2 -41 12.5 12:10 0.8 100 6.25 16.0 6.4 881 0.2 -41 12.0 12:15 0.9 100 6.25 16.1 6.4 883 0.2 -41 12.9 Method Qty Container Preservative Method Qty Container Preservative 82606 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 LOW Project Name: Project Location: Project Number: FLOW GROUNDWATER SAMPLIN Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A Phase 1 Y e I Purge Date: April 13, 2021 Source Well: MW-5 Purge Time: 30 Minutes Locked?: Yes Sample Date: April 13, 2021 Sampled By: James Waters Sample Time: 12:50 Weather: Sunny Air Temp: 85° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 12:45 0.8 100 9.13 17.2 4.9 29 5.4 233 2.7 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 1250 Sample End Time: 13:15 Analytical Data Name (1) James Waters Signature /� I/Y(� Date 4/13/2021 convert ORP to Eh, add 205 mV to ORP. Tested for Ferrous Iron using a HACH Model IR-18 (0.0 mg/ Notes: To L) Measuring Point: Top of Casing Depth to Water: 9.13 ft-TOC Total Well Depth: 19.85 ft-TOC Height of Water Column: 10.72 feet Screen Length: 10 feet Stickup: 2.6 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.7 Gal 3 *Well Volume 5.25 Gal 5 *Well Volume 8.75 Gal Purge Method: Peristaltic Pump Start Time: 12:15 End Time: 12:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 13.0 ft-TOC Water Column Above Pump Intake: 3.87 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 10.10 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus and MicroTPW Turbidity Meter Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 12:15 0.0 --- --- --- --- --- --- --- --- Start Purging 12:20 0.1 100 9.13 17.3 5.1 29 5.2 212 5.31 12:25 0.3 100 9.13 17.0 4.8 29 5.3 223 3.28 12:30 0.4 100 9.13 16.9 4.8 29 5.5 225 2.93 12:35 0.5 100 9.13 17.1 4.9 29 5.4 228 1.90 12:40 0.7 100 9.13 17.2 4.8 29 5.3 232 2.28 12:45 0.8 100 9.13 17.2 4.9 29 5.4 233 2.71 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Form Revision Date: 2/12/18 16:00 • • •I I Z IC11 101 Moore County Landfill 4358-20-043A phase 11 Purge Date: April 13, 2021 Project Name: Project Location: Project Number: Source Well: MW-6 Purge Time: 40 Minutes Locked?: Yes Sample Date: April 13, 2021 Sampled By: Gary Simcox Sample Time: 10:55 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 10:45 1.1 100 17.56 16.5 6.3 935 0.4 -98 13.8 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 10:55 Sample End Time: 11:15 Analytical Data Name (1) Gary Simcox Signature Date 4/13/2021 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (10.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 16.26 ft-TOC Total Well Depth: 22.50 ft-TOC Height of Water Column: 6.24 feet Screen Length: 15 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.0 Gal 3 *Well Volume 3.05 Gal 5 *Well Volume 5.09 Gal Purge Method: Peristaltic Pump Start Time: 10:05 End Time: 10:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 20.0 ft-TOC Water Column Above Pump Intake: 3.74 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 17.20 ft-TOC Comments: Final Volume Purged: 1.1 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 10:05 0.0 --- --- --- --- --- --- --- --- Start Purging 10:10 0.1 100 17.18 16.3 6.3 906 0.4 -82 34.5 10:15 0.3 100 17.46 16.2 6.3 920 0.4 -92 29.9 10:20 0.4 100 17.57 16.2 6.3 930 0.4 -97 27.5 10:25 0.5 100 17.56 16.4 6.3 931 0.4 -99 20.0 10:30 0.7 100 17.56 16.4 6.3 936 0.4 -100 19.8 10:35 0.8 100 17.56 16.5 6.3 933 0.3 -100 18.8 10:40 0.9 100 17.56 16.6 6.3 938 0.4 -99 14.9 10:45 1.1 100 17.56 16.5 6.3 935 0.4 -98 13.8 Method Qty Container Preservative Method Qty Container Preservative 82606 SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 LOW Project Name: Project Location: Project Number: FLOW GROUNDWATER SAMPLIN Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A Phase 1 Y e I Purge Date: April 13, 2021 Source Well: MW-7 Purge Time: 30 Minutes Locked?: Yes Sample Date: April 13, 2021 Sampled By: James Waters Sample Time: 11:20 Weather: Sunny Air Temp: 85° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 11:15 0.9 100 16.39 18.0 6.4 843 0.3 -89 8.9 End of Purging Sample Method] Peristaltic Pump 11:20 Sample Start Time:Analytical Sample End Time: 11:45 Data Name (1) James Waters Signature �l �'r Date 4/13/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. MW-7 has a history of going dry, but that does not occur durring this sampling event. Have to set intake no higher than 19 ft. Ferrous iron is > 10 m /L. Measuring Point: Top of Casing Depth to Water: 15.11 ft-TOC Total Well Depth: 22.00 ft-TOC Height of Water Column: 6.89 feet Screen Length: 15 feet Stickup: 2.7 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.1 Gal 3 *Well Volume 3.37 Gal 5 *Well Volume 5.62 Gal Purge Method: Peristaltic Pump Start Time: 10:45 End Time: 11:15 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.0 ft-TOC Water Column Above Pump Intake: 3.89 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 16.08 ft-TOC Comments: Final Volume Purged: 0.9 Gallons Used YSI Pro Plus and MicroTPW Turbidity Meter Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 10:45 0.0 --- --- --- --- --- --- --- --- Start Purging 10:50 0.1 100 15.26 18.4 6.3 801 2.3 -105 10.8 10:55 0.3 100 15.42 18.0 6.3 806 0.9 -105 8.71 11:00 0.4 100 15.60 18.2 6.2 822 0.5 -100 4.70 11:05 0.6 100 15.82 18.0 6.3 833 0.3 -97 4.81 11:10 0.7 100 16.32 18.0 6.3 837 0.3 -93 4.51 11:15 0.9 100 16.39 18.0 6.4 843 0.3 -89 8.86 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Form Revision Date: 2/12/18 16:00 Project Name: Moore County Landfill Project Location: 456 Turning Leaf Way Aberdeen, NC Project Number: 4358-20-043A Phase 1 Purge Date: April 13, 2021 Source Well: MW-8 Purge Time: 30 Minutes Locked?: Yes Sample Date: April 13, 2021 Sampled By: James Waters Sample Time: 10:05 Weather: Sunny Air Temp: 80° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 10:10 0.8 100 13.86 15.2 6.1 821 0.2 -57 4.2 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 1005 Sample End Time: 10:30 Analytical Data Name Signature Date (1) James Waters ou- 4/13/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. MW-8 has white flakes present in the purged water. Ferrous iron is >10 mg/L. Measuring Point: Top of Casing Depth to Water: 13.11 ft-TOC Total Well Depth: 22.00 ft-TOC Height of Water Column: 8.89 feet Screen Length: 15 feet Stickup: 2.6 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.5 Gal 3 *Well Volume 4.35 Gal 5 *Well Volume 7.25 Gal Purge Method: Peristaltic Pump Start Time: 9:40 End Time: 10:10 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 18.0 ft-TOC Water Column Above Pump Intake: 4.89 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 14.33 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus and MicroTPW Turbidity Meter Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 09:40 0.0 --- --- --- --- --- --- --- --- Start Purging 09:45 0.1 100 13.83 15.1 6.1 572 0.3 -42 16.2 09:50 0.3 100 13.90 15.1 6.1 573 0.2 -45 10.8 09:55 0.4 100 13.86 15.2 6.2 770 0.2 -56 5.30 10:00 0.5 100 13.86 15.3 6.1 787 0.2 -59 5.96 10:05 0.7 100 13.86 15.2 6.1 804 0.2 -59 3.80 10:10 0.8 100 13.86 15.2 6.1 821 0.2 -57 4.15 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Form Revision Date: 2/12/18 16:00 Project Name: Moore County Landfill Project Location: 456 Turning Leaf Way Aberdeen, NC Project Number: 4358-20-043A Phase 1 Source Well: MW-9 Locked?: Yes Sampled By: James Waters Weather: Sunny Measuring Point: Top of Casing Depth to Water: 22.23 ft-TOC Total Well Depth: 32.00 ft-TOC Height of Water Column: 9.77 feet Screen Length: 15 1 feet I Stickup: 2.3 ft-GRD Purge Date: April 13, 2021 Purge Time: 30 Minutes Sample Date: April 13, 2021 Sample Time: 9:05 Air Temp: 75' F Well Volume Well Diameter 2 inch Water Volume 1.6 Gal 3 * Well Volume 4.78 Gal 5 * Well Volume 7.97 Gal Purge Method: Peristaltic Pump Start Time: 830 1 End Time: 1 9:00 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): I Pressure:1 I psi Pump Intake Depth from Top of Casing: 28.0 ft-TOC Water Column Above Pump Intake: 5.77 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 23.67 ft-TOC Comments: Final Volume Purged: 1 0.8 Gallons Used YSI Pro Plus and MicroTPW Turbidity Meter Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) meters (Taken at time intervals >_ 5 minutes and purge volumes >_ Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (Ns/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 08:30 0.0 --- --- --- --- --- --- --- --- Start Purging 08:35 0.1 100 22.25 16.9 6.6 1,954 0.9 -89 7.13 08:40 0.3 100 22.26 17.1 6.5 1,950 0.7 -91 4.89 08:45 0.4 100 22.26 17.1 6.5 1,945 0.5 -94 3.88 08:50 0.5 100 22.26 17.3 6.5 1,933 0.4 -95 2.52 08:55 0.7 100 22.26 17.2 6.5 1,932 0.3 -95 4.31 09:00 0.8 100 22.26 17.4 6.5 1,926 0.2 -96 1.66 Final: 09:00 1 0.8 1 100 1 22.26 1 17.4 1 6.5 1 1,926 1 0.2 1 -96 1 1.7 1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 09:05 Sample End Time: 0930 Method Qty Container Preservative Method Qty Container Preservative 8260E SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 James Waters �w a w['� 4/13/2021 To convert ORP to Eh, add 205 mV to ORP. At the beginning of purging, black liquid came from the well and black flakes are noticed troughout purging. Form Revision Date: 2/12/18 16:00 LOW Project Name: Project Location: Project Number: FLOW GROUNDWATER SAMPLIN Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A Phase 1 Y e I Purge Date: April 13, 2021 Source Well: MW-11SR Purge Time: 35 Minutes Locked?: Yes Sample Date: April 13, 2021 Sampled By: James Waters Sample Time: 14:05 Weather: Sunny Air Temp: 85° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 14:00 0.9 100 14.46 18.3 6.5 1,666 0.2 -122 4.1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 1405 Sample End Time: 14:30 Analytical Data Name (1) James Waters Signature 54VY� Date 4/13/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Ferrous iron is >10 mg/L. Measuring Point: Top of Casing Depth to Water: 14.46 ft-TOC Total Well Depth: 31.50 ft-TOC Height of Water Column: 17.04 feet Screen Length: 10 feet Stickup: 2.2 ft-GRD Well Volume Well Diameter 2 inch Water Volume 2.8 Gal 3 *Well Volume 8.34 Gal 5 *Well Volume 13.90 Gal Purge Method: Peristaltic Pump Start Time: 13:25 End Time: 14:00 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 28.0 ft-TOC Water Column Above Pump Intake: 13.54 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 17.85 ft-TOC Comments: Final Volume Purged: 0.9 Gallons Used YSI Pro Plus and MicroTPW Turbidity Meter Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 13:25 0.0 --- --- --- --- --- --- --- --- Start Purging 13:30 0.1 100 14.46 20.2 6.4 1,658 8.5 -126 21.5 13:35 0.3 100 14.46 18.7 6.5 1,669 0.8 -126 4.18 13:45 0.5 100 14.46 18.3 6.6 1,664 0.6 -124 2.02 13:50 0.7 100 14.46 18.6 6.4 1,666 0.3 -123 2.25 13:55 0.8 100 14.46 18.6 6.6 1,666 0.2 -120 2.69 14:00 0.9 100 14.46 18.3 6.5 1,666 0.2 -122 4.06 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Form Revision Date: 2/12/18 16:00 Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: April 12, 2021 Project Name: Project Location: Project Number: Source Well: MW-11 DR Purge Time: 30 Minutes Locked?: Yes Sample Date: April 12, 2021 Sampled By: Gary Simcox Sample Time: 15:10 Weather: Sunny I Air Temp: 55° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 15:05 0.8 100 14.94 18.2 6.5 900 0.4 -149 6.9 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 15:10 Sample End Time: 15:25 Analytical Data Name (1) Gary Simcox Signature Date 4/13/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 14.88 ft-TOC Total Well Depth: 42.20 ft-TOC Height of Water Column: 27.32 feet Screen Length: 10 feet Stickup: 2.45 ft-GRD Well Volume Well Diameter 2 inch Water Volume 4.5 Gal 3 *Well Volume 13.37 Gal 5 *Well Volume 22.29 Gal Purge Method: Peristaltic Pump Start Time: 14:35 End Time: 15:05 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 39.0 ft-TOC Water Column Above Pump Intake: 24.12 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 20.91 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 14:35 0.0 --- --- --- --- --- --- --- --- Start Purging 14:40 0.1 100 14.94 18.4 6.5 903 0.5 -133 11.2 14:45 0.3 100 14.93 18.2 6.5 902 0.4 -141 6.82 14:50 0.4 100 14.94 18.2 6.5 900 0.4 -145 4.83 14:55 0.5 100 14.94 18.4 6.5 899 0.5 -147 5.85 15:00 0.7 100 14.95 18.3 6.5 901 0.4 -148 6.29 15:05 0.8 100 14.94 18.2 6.5 900 0.4 -149 6.89 Method Qty Container Preservative Method Qty Container Preservative 82606 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 LOW Project Name: Project Location: Project Number: FLOW GROUNDWATER SAMPLIN Moore County Landfill 456 Turning Leaf Way, Aberdeen, NC 4358-20-043A Phase 1 Y e I Purge Date: April 13, 2021 Source Well: MW-13SR Purge Time: 55 Minutes Locked?: Yes Sample Date: April 12, 2021 Sampled By: James Waters Sample Time: 14:00 Weather: Sunny Air Temp: 85° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 15:45 1.5 100 10.59 17.7 6.4 346 0.1 -86 8.8 End of Purging Sample Method] Peristaltic Pump 1400 Sample Start Time:Analytical Sample End Time: 14:20 Data Name (1) James Waters9 Signature - 1 a �""°- 4/13/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Electronic field data was lost from the previous day. Sample time and date remains the same (4/12/21, 1400). MW- 13SR was re ur ed to show data that is comparable and a representation of the groundwater at the time of sampling. Measuring Point: Top of Casing Depth to Water: 10.57 ft-TOC Total Well Depth: 22.50 ft-TOC Height of Water Column: 11.93 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.9 Gal 3 *Well Volume 5.84 Gal 5 *Well Volume 9.73 Gal Purge Method: Peristaltic Pump Start Time: 14:50 End Time: 15:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 20.0 ft-TOC Water Column Above Pump Intake: 9.43 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 12.93 ft-TOC Comments: Final Volume Purged: 1.5 Gallons Used YSI Pro Plus and MicroTPW Turbidity Meter Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 14:50 0.0 --- --- --- --- --- --- --- --- Start Purging 14:55 0.1 100 10.60 18.4 6.3 347 0.3 -89 28.5 15:00 0.3 100 10.59 18.4 6.3 345 0.2 -91 22.5 15:05 0.4 100 10.59 18.4 6.2 344 0.2 -92 22.8 15:10 0.5 100 10.59 18.5 6.3 334 0.1 -92 18.3 15:15 0.7 100 10.59 18.6 6.4 344 0.1 -91 15.8 15:20 0.8 100 10.59 17.9 6.3 346 0.1 -91 16.4 15:25 0.9 100 10.59 17.9 6.3 346 0.3 -90 17.0 15:30 1.1 100 10.59 18.2 6.3 345 0.2 -89 15.0 15:35 1.2 100 10.59 17.9 6.2 345 0.1 -86 13.3 15:40 1.3 100 10.59 17.9 6.2 346 0.1 -87 10.4 15:45 1.5 100 10.59 17.7 6.4 346 0.1 -86 8.84 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 LOW Project Name: Project Location: Project Number: FLOW GROUNDWATER SAMPLIN Moore County Landfill 456 Turning Leaf Way, Aberdeen, NC 4358-20-043A Phase 1 Y e I Purge Date: April 13, 2021 Source Well: MW-13DR Purge Time: 40 Minutes Locked?: Yes Sample Date: April 12, 2021 Sampled By: James Waters Sample Time: 15:20 Weather: Sunny Air Temp: 85° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 16:35 1.1 100 11.03 19.8 5.4 94 0.2 110 9.7 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 1520 Sample End Time: 15:40 Analytical Data Name (1) James Waters Signature al "r� Date 4/13/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Electronic field data was lost from the previous day. Sample time and date remains the same (4/12/21, 1520). MW- 13DR was re ur ed to show data that is comparable and a representation of the groundwater at the time of sampling. Measuring Point: Top of Casing Depth to Water: 11.02 ft-TOC Total Well Depth: 43.50 ft-TOC Height of Water Column: 32.48 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 5.3 Gal 3 *Well Volume 15.90 Gal 5 *Well Volume 26.50 Gal Purge Method: Peristaltic Pump Start Time: 15:55 End Time: 16:35 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 37.0 ft-TOC Water Column Above Pump Intake: 25.98 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 17.52 ft-TOC Comments: Final Volume Purged: 1.1 Gallons Used YSI Pro Plus and MicroTPW Turbidity Meter Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 15:55 0.0 --- --- --- --- --- --- --- --- Start Purging 16:00 0.1 100 11.02 20.6 5.4 95 0.2 109 29.4 16:05 0.3 100 11.03 20.2 5.4 94 0.2 109 15.8 16:10 0.4 100 11.03 20.2 5.3 95 0.2 109 15.9 16:15 0.5 100 11.03 20.3 5.4 94 0.2 109 16.6 16:20 0.7 100 11.03 19.8 5.3 94 0.2 110 14.3 16:25 0.8 100 11.03 19.8 5.4 94 0.2 109 12.2 16:30 0.9 100 11.03 20.0 5.4 94 0.1 110 11.4 16:35 1.1 100 11.03 19.8 5.4 94 0.2 110 9.70 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 •IVA Project Name: Project Location: Project Number: 9 011 Ill Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 s I s Purge Date: April 12, 2021 Source Well: MW-14 Purge Time: 45 Minutes Locked?: Yes Sample Date: April 12, 2021 Sampled By: James Waters Sample Time: 17:20 Weather: Sunny Air Temp: 85° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 17:15 1.2 100 16.46 19.0 5.8 228 0.6 -16 8.7 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 1720 Sample End Time: 17:40 Analytical Data Name (1) James Waters Signature a wV104- Date 4/12/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Measuring Point: Top of Casing Depth to Water: 16.32 ft-TOC Total Well Depth: 23.00 ft-TOC Height of Water Column: 6.68 feet Screen Length: 15 feet Stickup: 1.9 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.1 Gal 3 *Well Volume 3.27 Gal 5 *Well Volume 5.45 Gal Purge Method: Peristaltic Pump Start Time: 16:30 End Time: 17:15 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.5 ft-TOC Water Column Above Pump Intake: 3.18 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 17.12 ft-TOC Comments: Final Volume Purged: 1.2 Gallons Used YSI Pro Plus and MicroTPW Turbidity Meter. Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 16:30 0.0 --- --- --- --- --- --- --- --- Start Purging 16:35 0.1 100 16.40 19.9 6.1 359 1.1 -22 19.0 16:40 0.3 100 16.44 19.1 6.0 342 0.7 -28 22.2 16:45 0.4 100 16.46 18.7 6.0 330 0.6 -29 17.9 16:50 0.5 100 16.46 18.6 5.9 298 0.5 -25 18.9 16:55 0.7 100 16.46 18.9 5.8 259 0.4 -20 17.6 17:00 0.8 100 16.46 18.6 5.7 233 0.7 -18 12.6 17:05 0.9 100 16.46 18.6 5.7 231 0.6 -17 11.5 17:10 1.1 100 16.46 18.7 5.8 230 0.6 -18 10.2 17:15 1.2 100 16.46 19.0 5.8 228 0.6 -16 8.70 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 Moore County Landfill 4358-20-043A phase 11 Purge Date: I I April 13, 2021 Project Name: Project Location: Project Number: Source Well: MW-15R Purge Time: 35 Minutes Locked?: Yes Sample Date: April 13, 2021 Sampled By: Gary Simcox Sample Time: 8:50 Weather: Sunny Air Temp: 75' F Water Level & Well Data Measuring Point: Top of Casing Well Volume Depth to Water: 32.50 ft-TOC Well Diameter 2 inch Total Well Depth: 50.20 ft-TOC Water Volume 2.9 Gal Height of Water Column: 17.70 feet 3 * Well Volume 8.67 Gal Screen Length: 10 1 feet I Stickup: 2.5 ft-GRID 5 * Well Volume 14.44 Gal Well Purging Information Purge Method: Bladder Pump Start Time: 8:10 End Time: 8:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 45.0 ft-TOC Water Column Above Pump Intake: 12.50 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 35.63 ft-TOC Comments: Final Volume Purged: 1 0.9 1 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Field Parameters (Taken at time intervals z 5 minutes and purge volumes >_ 1 flow -through cell volume) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp CC) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTLI) Comment 08:10 0.0 --- --- --- --- --- --- --- --- Start Purging 08:20 0.3 100 32.50 15.2 6.2 359 0.5 66 27.2 08:25 0.4 100 32.51 15.3 6.2 365 0.4 -75 28.0 08:30 0.5 100 32.50 15.4 6.2 363 0.4 -78 22.0 08:35 0.7 100 32.50 15.4 6.2 363 0.3 -80 15.5 08:40 0.8 100 32.50 15.5 6.2 362 0.3 -82 14.1 08AS 0.9 100 32.50 15.6 6.2 363 0.3 -83 12.6 Final: 08:45 1 0.9 1 100 1 32.50 1 15.6 1 6.2 1 363 1 0.3 1 -83 1 12.6 1 End of Purging Sample Method: Bladder Pump Sample Start Time: 08:50 Sample End Time: 09:20 Analytical Data Method Qty Container Preservative Method Qty Container Preservative 8260B SM 450OSD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Name Signature Date (1) Gary Simcox 4/13/2021 Notes: Duplicate collected at this location. (Sample time recorded as 0700 hrs) I tested for Ferrous Iron using a HACH Model IR-18 (10.0 mg/L) Form Revision Date: 2/12/18 16:00 Moore County Landfill I I E Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 13, 2020 Source Well: MW-17D Purge Time: 40 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: Gary Simcox Sample Time: Weather: Sunny Air Temp: 75° F Water Level & Well Data Fie Parameters (Taken at time intervals >_ 5 minutes an purge volumes >_ flow -through cell volume) Final: 16:00 1.1 100 24.72 20.9 9.6 385 0.6 -86 62.6 End of Purging Sample Method: Bladder Pump Sample Start Time: Sample End Time: Analytical Data ame Signature Date (1) Gary Simcox 6/11/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Measuring Point: Top of Casing Depth to Water: 20.25 ft-TOC Total Well Depth: 37.30 ft-TOC Height of Water Column: 17.05 feet Screen Length: 5 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 2.8 Gal 3 *Well Volume 8.35 Gal 5 *Well Volume 13.91 Gal Purge Method: Bladder Pump Start Time: 15:20 End Time: 16:00 (If Used) Bladder Pump Control Settings: On (sec): 5 Off (sec): 30 Pressure: 25 psi Pump Intake Depth from Top of Casing: 35.0 ft-TOC Water Column Above Pump Intake: 14.75 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 23.94 ft-TOC Comments: Final Volume Purged: 1.1 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp VC) pH (s.u.) Spec. Cond. (pS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 15:20 0.0 --- --- --- --- --- --- --- --- Start Purging 15:30 0.3 100 20.52 21.8 9.6 366 2.4 -119 152 15:40 0.5 100 22.13 20.9 9.7 395 0.8 -112 112 15:45 0.7 100 23.17 21.0 9.6 390 0.6 -100 80.0 15:50 0.8 100 23.63 21.0 9.6 389 0.6 -96 70.0 15:55 0.9 100 24.15 20.9 9.6 388 0.6 -90 66.7 16:00 1.1 100 24.72 20.9 9.6 385 0.6 -86 62.6 Method Qty Container Preservative Method Qty Container Preservative 82606 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 irLOW FLOW GROUNDWATER SAMPLING FORM = [,.I Moore County Landfill!77' 456 Turning Leaf Way Aberdeen, NC I I Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 13, 2020 Source Well: MW-17S Purge Time: 30 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: Gary Simcox Sample Time: Weather: Sunny Air Temp: 75° F Water Level Well ata We Purging Information Fie Parameters (Taken at time intervals >_ 5 minutes an purge volumes >_ flow -through cellvolume) Final: 16:50 0.8 100 11.09 20.4 5.3 312 1.9 217 12.1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: Sample End Time: Analytical Data (1) James Waters 6/11/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 10.86 ft-TOC Total Well Depth: 21.40 ft-TOC Height of Water Column: 10.54 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.7 Gal 3 Well Volume 5.16 Gal 5 Well Volume 8.60 Gal Purge Method: Peristaltic Pump Start Time: 16:20 End Time: 16:50 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.0 ft-TOC Water Column Above Pump Intake: 8.14 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 12.90 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mUmin Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (p5/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 16:20 0.0 --- --- --- --- --- --- --- --- Start Purging 16:25 0.1 100 11.10 19.8 5.0 304 2.2 224 15.6 16:30 0.3 100 11.09 20.0 5.0 305 2.1 244 16.3 16:35 0.4 100 11.10 19.8 5.1 305 1.8 248 14.7 16:40 0.5 100 11.10 19.9 5.2 306 1.8 234 13.7 16:45 0.7 100 11.10 20.0 5.2 310 1.9 226 12.5 16:50 0.8 100 11.09 20.4 5.3 312 1.9 217 12.1 Method Qty Container Preservative Method C!ty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: April 12, 2021 Project Name: Project Location: Project Number: Source Well: MW-18 Purge Time: 35 Minutes Locked?: Yes Sample Date: April 12, 2021 Sampled By: Gary Simcox Sample Time: 12:50 Weather: Sunny I Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 12:45 0.9 100 6.61 21.1 6.3 1,241 0.5 -121 6.1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 12:50 Sample End Time: 13:35 Analytical Data Name (1) Gary Simcox Signature Date 4/13/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 6.58 ft-TOC Total Well Depth: 16.20 ft-TOC Height of Water Column: 9.62 feet Screen Length: 8 feet Stickup: 2.6 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.6 Gal 3 *Well Volume 4.71 Gal 5 *Well Volume 7.85 Gal Purge Method: Peristaltic Pump Start Time: 12:10 End Time: 12:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 14.0 ft-TOC Water Column Above Pump Intake: 7.42 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 8.44 ft-TOC Comments: Final Volume Purged: 0.9 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 12:10 0.0 --- --- --- --- --- --- --- --- Start Purging 12:15 0.1 100 6.61 21.2 6.3 1,255 0.5 -101 76.0 12:20 0.3 100 6.61 21.0 6.3 1,259 0.4 -107 35.0 12:25 0.4 100 6.61 21.2 6.3 1,255 0.4 -111 24.0 12:30 0.5 100 6.61 21.1 6.4 1,248 0.5 -115 21.0 12:35 0.7 100 6.61 21.1 6.3 1,248 0.4 -118 18.0 12:40 0.8 100 6.61 21.0 6.3 1,244 0.4 -119 7.66 12:45 0.9 100 6.61 21.1 6.3 1,241 0.5 -121 6.13 Method Qty Container Preservative Method Qty Container Preservative 82606 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 • • ° •I I Z IC11 Moore County Landfill 4358-20-043A phase 11 101 Purge Date: April 12, 2021 Project Name: Project Location: Project Number: Source Well: MW-19 Purge Time: 100 Minutes Locked?: Yes Sample Date: April 12, 2021 Sampled By: Gary Simcox Sample Time: 11:00 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 10:55 2.6 100 6.81 16.3 6.3 824 0.4 -46 27.0 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 11:00 Sample End Time: 11:45 Analytical Data Name (1) Gary Simcox Signature Date 4/13/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 6.73 ft-TOC Total Well Depth: 15.70 ft-TOC Height of Water Column: 8.97 feet Screen Length: 8 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.5 Gal 3 *Well Volume 4.39 Gal 5 *Well Volume 7.32 Gal Purge Method: Peristaltic Pump Start Time: 9:15 End Time: 10:55 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 13.5 ft-TOC Water Column Above Pump Intake: 6.77 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 8.42 ft-TOC Comments: Final Volume Purged: 2.6 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 09:15 0.0 --- --- --- --- --- --- --- --- Start Purging 09:20 0.1 100 6.81 14.7 6.4 836 0.4 -18 322 09:25 0.3 100 6.80 14.8 6.3 834 0.4 -24 211 09:30 0.4 100 6.79 14.7 6.3 829 0.4 -30 245 09:35 0.5 100 6.80 14.8 6.3 827 0.4 -32 191 09:40 0.7 100 6.79 15.0 6.3 831 0.3 -31 145 09:45 0.8 100 6.81 15.2 6.3 834 0.4 -31 139 09:50 0.9 100 6.80 15.4 6.3 837 0.4 -35 121 09:55 1.1 100 6.80 15.5 6.4 841 0.5 -36 109 10:05 1.3 100 6.81 15.7 6.4 843 0.4 -37 81.0 10:15 1.6 100 6.79 16.1 6.4 842 0.4 -41 72.0 10:25 1.8 100 6.81 16.1 6.4 833 0.3 -41 51.0 10:35 2.1 100 6.80 16.3 6.3 830 0.3 -44 33.0 10:45 2.4 100 6.79 16.2 6.4 826 0.3 -44 31.0 10:55 2.6 100 6.81 16.3 6.3 824 0.4 -46 27.0 Method Qty Container Preservative Method Qty Container Preservative Full App II SIM 450052 D-2011 8260 D-SIM 310.2 7470 SIM 2540C-2011 300 Moore County Landfill 4358-20-043A phase 11 Purge Date: !A April 12, 2021 Project Name: Project Location: Project Number: Source Well: SW-1 Purge Time: 0 Minutes Locked?: No Sample Date: April 12, 2021 Sampled By: Gary Simcox Sample Time: 15:55 Weather: Sunny Air Temp: 70 ° F Water Level & Well Data Measuring Point: Top of Casing Well Volume Depth to Water: ft-TOC Well Diameter 2 inch Total Well Depth: ft-TOC Water Volume Gal Height of Water Column: feet 3 * Well Volume Gal Screen Length:1 Ifeet I Stickup: ft-GRID 5 * Well Volume Gal Well Purging Information Purge Method: Peristaltic Pump Start Time: 15:55 End Time: 15:55 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: I Gallons Used YSI Pro Plus, Final Volume Purge Rate: I I mL/min Well Purged Dry?: INo I (Yes/No) Field Parameters (Taken at time intervals z 5 minutes and purge volumes >_ 1 flow -through cell volume) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTLI) Comment 15:55 0.0 --- --- --- --- --- --- --- --- Start Purging 15:55 20.9 6.5 215 4.6 -30 16.9 Final: 15:55 1 1 1 1 20.9 1 6.5 1 215 1 4.6 1 -30 1 16.9 1 End of Purging Sample Method: Sample Start Time: 15:55 Sample End Time: Analytical Data Method Qty Container Preservative Method Qty Container Preservative 8260B SM 450OSD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Name Signature Date (1) Gary Simcox 4/13/2021 Notes: Drive on the dirt road towel MW-2. Park at MW-2 and walk south down a path to the creek. I collected sample SW-1 at a location marked with 1" vc and red ribbon. The creek has a red tint but good flow. Form Revision Date: 2/12/18 16:00 • • •I I Z IC11 101 Moore County Landfill 4358-20-043A phase 11 Purge Date: October 15, 2020 Project Name: Project Location: Project Number: Source Well: SW-2 Purge Time: 0 Minutes Locked?: No Sample Date: October 15, 2020 Sampled By: Gary Simcox Sample Time: 17:00 Weather: Sunny Air Temp: 50 ° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes _> 1 low -through cell volume) Final: 17:00 22.1 6.3 38 5.1 110 4.2 End of Purging Sample Method: Sample Start Time: 17:00 Sample End Time: Analytical Data Name Signature Date (1) Gary Simcox 4/13/2021 Notes: I collected sample SW-2 at the end of the trail past the mulch piles. There is a 1" pvc stake with red ribbon marking the location. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: ft-TOC Total Well Depth: ft-TOC Height of Water Column: feet Screen Length: feet Stickup: ft-GRD Well Volume Well Diameter 2 inch Water Volume Gal 3 *Well Volume Gal 5 *Well Volume Gal Purge Method: Peristaltic Pump Start Time: 17:00 End Time: 17:00 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: Gallons Used YSI Pro Plus, Final Volume Purge Rate: mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 17:00 0.0 --- --- --- --- --- Start Purging 17:00 22.1 6.3 38 5.1 110 4.23 Method Qty Container Preservative Method Qty Container Preservative 82606 SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Moore County Landfill 4358-20-043A phase 11 Purge Date: !A October 15, 2020 Project Name: Project Location: Project Number: Source Well: SW-3 Purge Time: 0 Minutes Locked?: No Sample Date: October 15, 2020 Sampled By: Gary Simcox Sample Time: 16:25 Weather: Sunny Air Temp: 50 ° F Water Level & Well Data Measuring Point: Top of Casing Well Volume Depth to Water: ft-TOC Well Diameter 2 inch Total Well Depth: ft-TOC Water Volume Gal Height of Water Column: feet 3 * Well Volume Gal Screen Length:1 Ifeet I Stickup: ft-GRD 5 * Well Volume Gal Well Purging Information Purge Method: Peristaltic Pump Start Time: 16:25 End Time: 16:25 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: I Gallons Used YSI Pro Plus, Final Volume Purge Rate: I I mL/min Well Purged Dry?: I No I (Yes/No) Field Parameters (Taken at time intervals z 5 minutes and purge volumes >_ 1 flow -through cell volume) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTLI) Comment 16:25 0.0 --- --- --- --- --- --- --- --- Start Purging 16:25 21.0 6.5 145 1 5.5 -22 31.0 Final: 16:25 1 1 1 1 21.0 1 6.5 1 145 1 5.5 1 -22 1 31.0 1 End of Purging Sample Method: Sample Start Time: 16:25 Sample End Time: Analytical Data Method Qty Container Preservative Method Qty Container Preservative 8260B SM 450OSD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Name Signature Date (1) Gary Simcox 4/13/2021 Notes: I collected sample SW-3 at a location marked with pink flagging. Drive on the dirt road SE past MW-3 toward MW-2. About 200 yards past MW-3 there is a path marked with pink flagging. Park and walk in another 200 yards to the creek. The creek has a red tint but good flow. Form Revision Date: 2/12/18 16:00 Moore County Landfill 4358-20-043A phase 11 Purge Date: April 13, 2021 Project Name: Project Location: Project Number: Source Well: SW-4 Purge Time: 0 Minutes Locked?: No Sample Date: April 13, 2021 Sampled By: Gary Simcox Sample Time: 13:00 Weather: Sunny Air Temp: 75 ° F Water Level & Well Data Measuring Point: Top of Casing Well Volume Depth to Water: ft-TOC Well Diameter 2 inch Total Well Depth: ft-TOC Water Volume Gal Height of Water Column: feet 3 * Well Volume Gal Screen Length:1 Ifeet I Stickup: ft-GRD 5 * Well Volume Gal Well Purging Information Purge Method: Peristaltic Pump Start Time: 13:00 End Time: 13:00 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: I Gallons Used YSI Pro Plus, Final Volume Purge Rate: I I mL/min Well Purged Dry?: I No I (Yes/No) Field Parameters (Taken at time intervals z 5 minutes and purge volumes >_ 1 flow -through cell volume) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTLI) Comment 13:00 0.0 --- --- --- --- --- --- --- --- Start Purging 13:00 20.8 6.9 176 1 4.8 -27 12.9 Final: 13:00 1 1 1 1 20.8 1 6.9 1 176 1 4.8 1 -27 1 12.9 1 End of Purging Sample Method: Sample Start Time: 13:00 Sample End Time: Analytical Data Method Qty Container Preservative Method Qty Container Preservative 8260B SM 450OSD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Name Signature Date (1) Gary Simcox 4/13/2021 Notes: Walked down the slope at Outfall #1. 1 located the surface water (creek) flowing from NE to SW. I collected sample SW-4 approximatley 100' SW of the intersection of Outfall #1 and the creek. Form Revision Date: 2/12/18 16:00 Appendix II - Laboratory Analytical Reports 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, May 10, 2021 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043A Phase 01, Project Name/Desc: Moore County MSW LF CA ENCO Workorder(s): CE04872 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, April 13, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, O"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 39 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County MSW LF CA Lab ID: CE04872 Overview (� �Eo www.encolabs.com Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an acceptable LCs recovery (QM-07). Precision between duplicate matrix spikes of the same sample was outside acceptance limits (QM-11). Precision between duplicate samples was outside acceptance limits (QM-12). Quality Control Remarks No Comments Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 39 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW6 Lab ID: CE04872-01 Sampled: 04/13/21 10:55 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/15/21 13:23 04/16/21 05:28 EPA 310.2 NO PREP 04/27/21 04/20/21 08:28 04/20/21 11:13 EPA 353.2 NO PREP 04/15/21 10:55 04/14/21 13:37 04/14/21 15:07 EPA 353.2 [CALC] 04/15/21 10:55 04/21/21 10:00 04/21/21 14:29 EPA 353.2 NO PREP 05/11/21 04/21/21 10:00 04/21/21 14:29 EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 04/19/21 12:57 EPA 7470A EPA 7470A 05/11/21 04/19/21 09:05 04/20/21 15:11 EPA 8260D EPA 503013_MS 04/27/21 04/16/21 09:48 04/17/21 04:01 EPA 9060A NO PREP 05/11/21 04/22/21 09:00 04/22/21 21:11 SM 4500S2 D-2011 NO PREP 04/20/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW6 Lab ID: CE04872-01RE1 Sampled: 04/13/21 10:55 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 05/10/21 13:23 EPA 8260D EPA 503013_MS 04/27/21 04/21/21 10:11 04/21/21 11:46 Client ID: 6301-MW6 Lab ID: CE04872-01RE2 Sampled: 04/13/21 10:55 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) RSK 175 Same 04/27/21 04/20/21 00:00 04/20/21 14:41 Client ID: 6301-MW7 Lab ID: CE04872-02 Sampled: 04/13/21 11:20 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/15/21 13:23 04/16/21 05:46 EPA 353.2 NO PREP 04/15/21 11:20 04/14/21 13:37 04/14/21 15:10 EPA 353.2 [CALC] 04/15/21 11:20 04/21/21 10:00 04/21/21 14:31 EPA 353.2 NO PREP 05/11/21 04/21/21 10:00 04/21/21 14:31 EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 04/19/21 12:59 EPA 7470A EPA 7470A 05/11/21 04/19/21 09:05 04/20/21 15:13 EPA 8260D EPA 503013_MS 04/27/21 04/16/21 09:48 04/17/21 04:29 EPA 8260D EPA 503013_MS 04/27/21 04/19/21 13:46 04/20/21 00:25 EPA 9060A NO PREP 05/11/21 04/22/21 09:00 04/22/21 21:33 SM 4500S2 D-2011 NO PREP 04/20/21 04/19/21 16:59 04/19/21 17:12 Client ID: 6301-MW7 Lab ID: CE04872-02RE1 Sampled: 04/13/21 11:20 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 04/27/21 04/15/21 13:20 04/15/21 16:32 EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 05/10/21 13:26 RSK 175 Same 04/27/21 04/20/21 00:00 04/20/21 13:22 Client ID: 6301-MW7 Lab ID: CE04872-02RE2 Sampled: 04/13/21 11:20 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) RSK 175 Same 04/27/21 04/20/21 00:00 04/20/21 14:25 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 39 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW8 Lab ID: CE04872-03 Sampled: 04/13/21 10:05 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/15/21 13:23 04/16/21 06:03 EPA 310.2 NO PREP 04/27/21 04/15/21 13:20 04/15/21 16:04 EPA 353.2 NO PREP 04/15/21 10:05 04/14/21 13:37 04/14/21 15:11 EPA 353.2 [CALC] 04/15/21 10:05 04/21/21 08:28 04/21/21 12:12 EPA 353.2 NO PREP 05/11/21 04/21/21 08:28 04/21/21 12:12 EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 04/19/21 13:02 EPA 7470A EPA 7470A 05/11/21 04/19/21 09:05 04/20/21 15:15 EPA 8260D EPA 503013_MS 04/27/21 04/16/21 09:48 04/17/21 04:57 EPA 9060A NO PREP 05/11/21 04/22/21 07:41 04/22/21 15:57 RSK 175 Same 04/27/21 04/20/21 00:00 04/20/21 10:43 SM 4500S2 D-2011 NO PREP 04/20/21 04/19/21 16:59 04/19/21 17:12 Client ID: 6301-MW8 Lab ID: CE04872-03RE1 Sampled: 04/13/21 10:05 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/27/21 04/21/21 10:11 04/21/21 12:11 RSK 175 Same 04/27/21 04/20/21 00:00 04/20/21 13:54 Client ID: 6301-MW9 Lab ID: CE04872-04 Sampled: 04/13/21 09:05 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(sl EPA 300.0 NO PREP 05/11/21 04/15/21 13:23 04/16/21 06:21 EPA 310.2 NO PREP 04/27/21 04/15/21 13:20 04/15/21 16:04 EPA 353.2 NO PREP 04/15/21 09:05 04/14/21 13:37 04/14/21 15:12 EPA 353.2 [CALC] 04/15/21 09:05 04/21/21 08:28 04/21/21 12:14 EPA 353.2 NO PREP 05/11/21 04/21/21 08:28 04/21/21 12:14 EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 04/19/21 13:04 EPA 7470A EPA 7470A 05/11/21 04/19/21 09:05 04/20/21 15:18 EPA 8260D EPA 503013_MS 04/27/21 04/16/21 09:48 04/17/21 05:25 EPA 9060A NO PREP 05/11/21 04/22/21 09:00 04/22/21 21:56 SM 4500S2 D-2011 NO PREP 04/20/21 04/19/21 16:59 04/19/21 17:12 Client ID: 6301-MW9 Lab ID: CE04872-04RE1 Sampled: 04/13/21 09:05 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/16/21 12:03 04/16/21 22:23 EPA 8260D EPA 5030B_MIS 04/27/21 04/20/21 00:00 04/20/21 22:32 Client ID: 6301-MW9 Lab ID: CE04872-04RE2 Sampled: 04/13/21 09:05 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) RSK 175 Same 04/27/21 04/20/21 00:00 04/20/21 14:57 Client ID: 6301-MW15R Lab ID: CE04872-05 Sampled: 04/13/21 08:50 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/15/21 13:23 04/16/21 06:39 EPA 310.2 NO PREP 04/27/21 04/15/21 13:20 04/15/21 16:05 EPA 353.2 NO PREP 04/15/21 08:50 04/14/21 13:37 04/14/21 15:12 EPA 353.2 [CALC] 04/15/21 08:50 04/21/21 08:28 04/21/21 12:16 EPA 353.2 NO PREP 05/11/21 04/21/21 08:28 04/21/21 12:16 EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 04/19/21 13:06 EPA 7470A EPA 7470A 05/11/21 04/19/21 09:05 04/20/21 15:20 EPA 8260D EPA 503013_MS 04/27/21 04/16/21 09:48 04/17/21 05:53 EPA 9060A NO PREP 05/11/21 04/22/21 07:41 04/22/21 16:58 RSK 175 Same 04/27/21 04/20/21 00:00 04/20/21 11:15 SM 4500S2 D-2011 NO PREP 04/20/21 04/19/21 16:59 04/19/21 17:12 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 39 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW15R Lab ID: CE04872-OSRE3 Sampled: 04/13/21 08:50 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/27/21 04/20/21 00:00 04/20/21 22:57 RSK 175 Same 04/27/21 04/20/21 00:00 04/20/21 14:09 Client ID: 6301-TRIPBLANK Lab ID: CE04872-06 Sampled: 04/13/21 08:50 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/27/21 04/16/21 09:48 04/17/21 06:21 Client ID: 6301-TRIPBLANK Lab ID: CE04872-06RE1 Sampled: 04/13/21 08:50 Received: 04/13/21 16:21 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/27/21 04/20/21 00:00 04/20/21 14:55 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 39 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW6 Lab ID: CE04872-01 Analvte Results Flag MDL Q Units Method Notes 1,4-Dichlorobenzene 1.6 0.76 1.0 ug/L EPA 8260D Acetone 46 10 20 ug/L EPA 8260D Barium - Total 46.0 1.10 10.0 ug/L EPA 6010D Benzene 2.6 0.71 1.0 ug/L EPA 8260D Cadmium - Total 1.04 0.360 1.00 ug/L EPA 6010D Chloride 13 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.5 0.72 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.2 0.53 1.0 ug/L EPA 8260D Sulfate as SO4 11 2.9 5.0 mg/L EPA 300.0 Sulfide 0.19 0.010 0.10 mg/L SM 450052 D-2011 Total Alkalinity as CaCO3 240 D 28 30 mg/L EPA 310.2 Total Organic Carbon 57 0.54 1.0 mg/L EPA 9060A Vinyl chloride 1.2 0.71 1.0 uq/L EPA 8260D I Client ID: 6301-MW6 Lab ID: CE04872-01RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1.7 3 0.80 2.0 ug/L EPA 8260D Lead - Total 4.25 3 3.10 10.0 ug/L EPA 6010D Client ID: 6301-MW6 Lab ID: CE04872-01RE2 Analvte Results Flag MDL PQL Units Method Notes Methane 0.0124 0.00400 0.00500 mg/L RSK 175 Client ID: 6301-MW7 Lab ID: CE04872-02 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 0.81 3 0.76 1.0 ug/L EPA 8260D 1,4-Dioxane 3.9 0.80 2.0 ug/L EPA 8260D Acetone 75 10 20 ug/L EPA 8260D Barium - Total 38.4 1.10 10.0 ug/L EPA 6010D Benzene 1.0 0.71 1.0 ug/L EPA 8260D Cadmium - Total 1.25 0.360 1.00 ug/L EPA 6010D Chloride 10 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 0.90 3 0.72 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.61 3 0.53 1.0 ug/L EPA 8260D Nitrate as N 0.65 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.65 0.041 0.10 mg/L EPA 353.2 Total Organic Carbon 26 0.54 1.0 mg/L EPA 9060A Vinyl chloride 2.2 0.71 1.0 ug/L EPA 8260D Client ID: 6301-MW7 Lab ID: CE04872-02RE3 Analvte Results Flag MDL PQL Units Method Notes Lead - Total 4.39 3 3.10 10.0 ug/L EPA 6010D Total Alkalinity as CaCO3 300 D 28 30 mg/L EPA 310.2 Client ID: 6301-MW7 Lab ID: CE04872-02RE2 Analvte Results Flag MDL PQL Units Method Notes Carbon dioxide 373 D 62.1 75.0 mg/L RSK 175 Methane 5.91 D 0.120 0.150 mg/L RSK 175 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 39 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW8 Lab ID: CE04872-03 Analvte Results Flag MDL Q Units Method Notes 1,4-Dichlorobenzene 3.1 0.76 1.0 ug/L EPA 8260D Barium - Total 66.6 1.10 10.0 ug/L EPA 6010D Benzene 3.2 0.71 1.0 ug/L EPA 8260D Cadmium - Total 0.612 3 0.360 1.00 ug/L EPA 6010D Carbon dioxide 126 2.07 2.50 mg/L RSK 175 Chloride 50 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 3.8 0.72 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.71 3 0.53 1.0 ug/L EPA 8260D Lead - Total 13.9 3.10 10.0 ug/L EPA 6010D Sulfide 0.11 0.010 0.10 mg/L SM 450052 D-2011 Total Alkalinity as CaCO3 230 D 28 30 mg/L EPA 310.2 Total Organic Carbon 18 0.54 1.0 mg/L EPA 9060A Client ID: 6301-MW8 Lab ID: CE04872-03RE1 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 22 0.80 2.0 ug/L EPA 8260D Methane 6.37 D 0.0840 0.105 mg/L RSK 175 Client ID: 6301-MW9 Lab ID: CE04872-04 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 2.7 0.76 1.0 ug/L EPA 8260D Barium - Total 78.2 1.10 10.0 ug/L EPA 6010D Benzene 3.2 0.71 1.0 ug/L EPA 8260D Chlorobenzene 10 0.72 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.2 0.53 1.0 ug/L EPA 8260D Lead - Total 10.9 3.10 10.0 ug/L EPA 6010D Sulfide 0.16 0.010 0.10 mg/L SM 450052 D-2011 Total Alkalinity as CaCO3 760 D 70 75 mg/L EPA 310.2 Total Organic Carbon 34 0.54 1.0 mq/L EPA 9060A I Client ID: 6301-MW9 Lab ID: CE04872-04RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 30 0.80 2.0 ug/L EPA 8260D Chloride 99 D 4.4 10 mg/L EPA 300.0 Client ID: 6301-MW1SR Lab ID: CE04872-05 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 25.0 1.10 10.0 ug/L EPA 6010D Benzene 0.78 3 0.71 1.0 ug/L EPA 8260D Cadmium - Total 0.855 3 0.360 1.00 ug/L EPA 6010D Chloride 3.1 3 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 2.5 0.53 1.0 ug/L EPA 8260D Lead - Total 13.0 3.10 10.0 ug/L EPA 6010D Sulfate as SO4 6.8 2.9 5.0 mg/L EPA 300.0 Sulfide 0.035 3 0.010 0.10 mg/L SM 450052 D-2011 Total Alkalinity as CaCO3 110 14 15 mg/L EPA 310.2 Total Organic Carbon 2.5 0.54 1.0 mg/L EPA 9060A Client ID: 6301-MW1SR Lab ID: CE04872-OSRE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.2 0.80 2.0 ug/L EPA 8260D Carbon dioxide 242 D 43.5 52.5 mg/L RSK 175 Methane 1.64 D 0.0840 0.105 mg/L RSK 175 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CE04872-01 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 10:55 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 15:11 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D15015 EPA 6010D 04/19/21 12:57 JDH Barium [7440-39-3]^ 46.0 ug/L 1 1.10 10.0 1D15015 EPA 6010D 04/19/21 12:57 JDH Cadmium [7440-43-9]^ 1.04 ug/L 1 0.360 1.00 1D15015 EPA 6010D 04/19/21 12:57 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 12:57 JDH Lead [7439-92-1]^ 4.25 J ug/L 1 3.10 10.0 lE07007 EPA 6010D 05/10/21 13:23 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1D15015 EPA 6010D 04/19/21 12:57 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D15015 EPA 6010D 04/19/21 12:57 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 13 mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 05:28 LII Nitrate as N [14797-55-8] 0.041 U mg/L 1 0.041 0.10 [CALC] EPA 353.2 04/21/21 14:29 JAH Nitrate/Nitrite as N^ 0.041 U mg/L 1 0.041 0.10 1D21015 EPA 353.2 04/21/21 14:29 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1D14029 EPA 353.2 04/14/21 15:07 JAH Sulfate as SO4 [14808-79-8]^ 11 mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 05:28 LII Sulfide [18496-25-8]^ 0.19 mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 240 D mg/L 2 28 30 1D20009 EPA 310.2 04/20/21 11:13 JAH Volatile Organic Compounds by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.61 U ug/L 1 0.61 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,1,1-Trichloroethane [71-55-6]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.54 U ug/L 1 0.54 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,1,2-Trichloroethane [79-00-5]^ 0.76 U ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,1-Dichloroethane [75-34-3]^ 0.62 U ug/L 1 0.62 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,1-Dichloroethene [75-35-4]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,2,3-Trichloropropane [96-18-4]^ 0.64 U ug/L 1 0.64 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.96 U ug/L 1 0.96 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,2-Dibromoethane [106-93-4]^ 0.78 U ug/L 1 0.78 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,2-Dichlorobenzene [95-50-1]^ 0.73 U ug/L 1 0.73 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,2-Dichloroethane [107-06-2]^ 0.63 U ug/L 1 0.63 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,2-Dichloropropane [78-87-5]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 1,4-Dichlorobenzene [106-46-7]^ 1.6 ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 2-Butanone [78-93-3]^ 4.5 U ug/L 1 4.5 5.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 2-Hexanone [591-78-6]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 04:01 kkw 4-Methyl-2-pentanone [108-10-1]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 04:01 kkw Acetone [67-64-1]^ 46 ug/L 1 10 20 1D16032 EPA 8260D 04/17/21 04:01 kkw Acrylonitrile [107-13-1]^ 5.0 U ug/L 1 5.0 10 1D16032 EPA 8260D 04/17/21 04:01 kkw Benzene [71-43-2]^ 2.6 ug/L 1 0.71 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw Bromochloromethane [74-97-5]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 39 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CE04872-01 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 10:55 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS A - ENCO Orlando certified analyte [NC 424] Analvte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes Bromodichloromethane [75-27-4]^ 0.52 u ug/L 1 0.52 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Bromoform [75-25-2]^ 0.75 u ug/L 1 0.75 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Bromomethane [74-83-9]^ 0.95 u ug/L 1 0.95 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Carbon disulfide [75-15-0]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Carbon tetrachloride [56-23-5]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Chlorobenzene [308-90-7]^ 1.5 ug/L 1 0.72 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw Chloroethane [75-00-3]^ 0.98 U ug/L 1 0.98 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Chloroform [67-66-3]^ 0.80 U ug/L 1 0.80 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Chloromethane [74-87-3]^ 0.82 U ug/L 1 0.82 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw cis-1,2-Dichloroethene [156-59-2]^ 1.2 ug/L 1 0.53 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw cis-1,3-Dichloropropene [10061-01-5]^ 0.59 U ug/L 1 0.59 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Dibromochloromethane [124-48-1]^ 0.50 u ug/L 1 0.50 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Dibromomethane [74-95-3]^ 0.84 u ug/L 1 0.84 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Ethylbenzene [100-41-4]^ 0.69 u ug/L 1 0.69 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Iodomethane [74-88-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Methylene chloride [75-09-2]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Styrene [100-42-5]^ 0.61 u ug/L 1 0.61 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Tetrachloroethene [127-18-4]^ 0.76 u ug/L 1 0.76 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Toluene [108-88-3]^ 0.72 u ug/L 1 0.72 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw trans-1,2-Dichloroethene [156-60-5]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw trans-1,3-Dichloropropene [10061-02-6]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw trans-1,4-Dichloro-2-butene [110-57-6]^ 0.79 u ug/L 1 0.79 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Trichloroethene [79-01-6]^ 0.89 u ug/L 1 0.89 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Trichlorofluoromethane [75-69-4]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Vinyl acetate [108-05-4]^ 2.5 U ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Vinyl chloride [75-01-4]^ 1.2 ug/L 1 0.71 1.0 1D16032 EPA 8260D 04/17/21 04:01 kkw Xylenes(Total)[1330-20-7]^ 1.3 U ug/L 1 1.3 2.0 ID16032 EPA 8260D 04/17/21 04:01 kkw Surrogates Results DF Spike L v/ % Rec % Rec Limits Batch Method Analyzed " Notes 4-Bromofluorobenzene 54 1 50.0 108 % 41-142 ID16032 EPA 8260D 04117121 04:01 kkw Dibromofluoromethane 53 1 50.0 106 % 53-146 ID16032 EPA 8260D 04117121 04:01 kkw Toluene-& 48 1 50.0 97 % 41-146 ID16032 EPA 8260D 04117121 X 01 kkw Volatile Organic Compounds by GCMS SIM Isotope Dilution A - ENCO Orlando certified analyte [NC 4241 Analvte rCAS Numberl Results Flaa Units DF MDL 4 Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 1.7 1 ug/L 1 0.80 2.0 1D21017 EPA 8260D 04/21/21 11:46 KKW Surrogates Toluene-d8 Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 5.0 1 5.00 100 % 75-125 1D21017 EPA 8260D 04121121 11:46 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CE04872-01 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 10:55 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 2.07 U mg/L 1 2.07 2.50 1D20005 RSK 175 04/20/21 14:41 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 14:41 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 14:41 JMW Methane [74-82-8] 0.0124 mg/L 1 0.00400 0.00500 1D20005 RSK 175 04/20/21 14:41 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 57 mg/L 1 0.54 1.0 1D22022 EPA 9060A 04/22/21 21:11 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CE04872-02 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 11:20 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 15:13 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D15015 EPA 6010D 04/19/21 12:59 JDH Barium [7440-39-3]^ 38.4 ug/L 1 1.10 10.0 1D15015 EPA 6010D 04/19/21 12:59 JDH Cadmium [7440-43-9]^ 1.25 ug/L 1 0.360 1.00 1D15015 EPA 6010D 04/19/21 12:59 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 12:59 JDH Lead [7439-92-1]^ 4.39 J ug/L 1 3.10 10.0 1E07007 EPA 6010D 05/10/21 13:26 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1D15015 EPA 6010D 04/19/21 12:59 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D15015 EPA 6010D 04/19/21 12:59 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 10 mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 05:46 LII Nitrate as N [14797-55-8] 0.65 mg/L 1 0.041 0.10 [CALC] EPA 353.2 04/21/21 14:31 JAH Nitrate/Nitrite as N^ 0.65 mg/L 1 0.041 0.10 1D21015 EPA 353.2 04/21/21 14:31 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1D14029 EPA 353.2 04/14/21 15:10 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 05:46 LII Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1D19020 iM 4500S2 D-2011 04/19/21 17:12 JOC Total Alkalinity as CaCO3 [471-34-1]^ 300 D mg/L 2 28 30 1D15027 EPA 310.2 04/15/21 16:32 JAH Volatile Organic Compounds by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.61 U ug/L 1 0.61 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,1,1-Trichloroethane [71-55-6]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.54 U ug/L 1 0.54 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,1,2-Trichloroethane [79-00-5]^ 0.76 U ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,1-Dichloroethane [75-34-3]^ 0.62 U ug/L 1 0.62 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,1-Dichloroethene [75-35-4]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,2,3-Trichloropropane [96-18-4]^ 0.64 U ug/L 1 0.64 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.96 U ug/L 1 0.96 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,2-Dibromoethane [106-93-4]^ 0.78 U ug/L 1 0.78 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,2-Dichlorobenzene [95-50-1]^ 0.73 U ug/L 1 0.73 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,2-Dichloroethane [107-06-2]^ 0.63 U ug/L 1 0.63 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,2-Dichloropropane [78-87-5]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 1,4-Dichlorobenzene [106-46-7]^ 0.81 J ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 2-Butanone [78-93-3]^ 4.5 U ug/L 1 4.5 5.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 2-Hexanone [591-78-6]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 04:29 kkw 4-Methyl-2-pentanone [108-10-1]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 04:29 kkw Acetone [67-64-1]^ 75 ug/L 1 10 20 1D16032 EPA 8260D 04/17/21 04:29 kkw Acrylonitrile [107-13-1]^ 5.0 U ug/L 1 5.0 10 1D16032 EPA 8260D 04/17/21 04:29 kkw Benzene [71-43-2]^ 1.0 ug/L 1 0.71 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw Bromochloromethane [74-97-5]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 39 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CE04872-02 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 11:20 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS A - ENCO Orlando certified analyte [NC 424] Analvte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes Bromodichloromethane [75-27-4]^ 0.52 u ug/L 1 0.52 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Bromoform [75-25-2]^ 0.75 u ug/L 1 0.75 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Bromomethane [74-83-9]^ 0.95 u ug/L 1 0.95 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Carbon disulfide [75-15-0]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Carbon tetrachloride [56-23-5]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Chlorobenzene [308-90-7]^ 0.90 J ug/L 1 0.72 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw Chloroethane [75-00-3]^ 0.98 u ug/L 1 0.98 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Chloroform [67-66-3]^ 0.80 u ug/L 1 0.80 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Chloromethane [74-87-3]^ 0.82 u ug/L 1 0.82 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw cis-1,2-Dichloroethene [156-59-2]^ 0.61 J ug/L 1 0.53 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw cis-1,3-Dichloropropene [10061-01-5]^ 0.59 u ug/L 1 0.59 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Dibromochloromethane [124-48-1]^ 0.50 u ug/L 1 0.50 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Dibromomethane [74-95-3]^ 0.84 u ug/L 1 0.84 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Ethylbenzene [500-41-4]^ 0.69 u ug/L 1 0.69 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Iodomethane [74-88-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Methylene chloride [75-09-2]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Styrene [100-42-5]^ 0.61 u ug/L 1 0.61 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Tetrachloroethene [127-18-4]^ 0.76 u ug/L 1 0.76 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Toluene [108-88-3]^ 0.72 u ug/L 1 0.72 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw trans-1,2-Dichloroethene [156-60-5]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw trans-1,3-Dichloropropene [10061-02-6]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw trans-1,4-Dichloro-2-butene [110-57-6]^ 0.79 u ug/L 1 0.79 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Trichloroethene [79-01-6]^ 0.89 u ug/L 1 0.89 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Trichlorofluoromethane [75-69-4]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Vinyl acetate [108-05-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Vinyl chloride [75-01-4]^ 2.2 ug/L 1 0.71 1.0 1D16032 EPA 8260D 04/17/21 04:29 kkw Xylenes(Total)[1330-20-7]^ 1.3 U ug/L 1 1.3 2.0 ID16032 EPA 8260D 04/17/21 04:29 kkw Surrogates Results DF Spike L v/ % Rec % Rec Limits Batch Method Analyzed " Notes 4-Bromofluorobenzene 49 1 50.0 99 % 41-142 ID16032 EPA 8260D 04117121 04:29 kkw Dibromofluoromethane 54 1 50.0 109 % 53-146 ID16032 EPA 8260D 04117121 04:29 kkw Toluene-& 52 1 50.0 104 % 41-146 ID16032 EPA 8260D 04117121 04:29 kkw Volatile Organic Compounds by GCMS SIM Isotope Dilution A - ENCO Orlando certified analyte [NC 4241 Analvte rCAS Numberl Results Flaa Units DF MDL 4 Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 3.9 ug/L 1 0.80 2.0 1D19039 EPA 8260D 04/20/21 00:25 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.3 1 5.00 107 % 75-125 1D19039 EPA 8260D 04120121 00:25 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CE04872-02 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 11:20 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 373 D mg/L 30 62.1 75.0 1D20005 RSK 175 04/20/21 14:25 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 13:22 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 13:22 JMW Methane [74-82-8] 5.91 D mg/L 30 0.120 0.150 1D20005 RSK 175 04/20/21 14:25 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed Ay Notes Total Organic Carbon^ 26 mg/L 1 0.54 1.0 1D22022 EPA 9060A 04/22/21 21:33 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CE04872-03 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 10:05 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 15:15 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D15015 EPA 6010D 04/19/21 13:02 JDH Barium [7440-39-3]^ 66.6 ug/L 1 1.10 10.0 1D15015 EPA 6010D 04/19/21 13:02 JDH Cadmium [7440-43-9]^ 0.612 J ug/L 1 0.360 1.00 1D15015 EPA 6010D 04/19/21 13:02 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 13:02 JDH Lead [7439-92-1]^ 13.9 ug/L 1 3.10 10.0 1D15015 EPA 6010D 04/19/21 13:02 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1D15015 EPA 6010D 04/19/21 13:02 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D15015 EPA 6010D 04/19/21 13:02 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 50 mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 06:03 LII Nitrate as N [14797-55-8] 0.041 U mg/L 1 0.041 0.10 [CALC] EPA 353.2 04/21/21 12:12 JAH Nitrate/Nitrite as N^ 0.041 u mg/L 1 0.041 0.10 1D21010 EPA 353.2 04/21/21 12:12 JAH Nitrite as N [14797-65-0]^ 0.017 u mg/L 1 0.017 0.10 1D14029 EPA 353.2 04/14/21 15:11 JAH Sulfate as SO4 [14808-79-8]^ 2.9 u mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 06:03 LII Sulfide [18496-25-8]^ 0.11 mg/L 1 0.010 0.10 1D19020 iM 4500S2 D-2011 04/19/21 17:12 JOC Total Alkalinity as CaCO3 [471-34-1]^ 230 D mg/L 2 28 30 1D15027 EPA 310.2 04/15/21 16:04 JAH Volatile Organic Compounds by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.61 U ug/L 1 0.61 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,1,1-Trichloroethane [71-55-6]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.54 U ug/L 1 0.54 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,1,2-Trichloroethane [79-00-5]^ 0.76 U ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,1-Dichloroethane [75-34-3]^ 0.62 U ug/L 1 0.62 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,1-Dichloroethene [75-35-4]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,2,3-Trichloropropane [96-18-4]^ 0.64 U ug/L 1 0.64 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.96 U ug/L 1 0.96 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,2-Dibromoethane [106-93-4]^ 0.78 U ug/L 1 0.78 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,2-Dichlorobenzene [95-50-1]^ 0.73 U ug/L 1 0.73 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,2-Dichloroethane [107-06-2]^ 0.63 U ug/L 1 0.63 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,2-Dichloropropane [78-87-5]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 1,4-Dichlorobenzene [106-46-7]^ 3.1 ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 2-Butanone [78-93-3]^ 4.5 U ug/L 1 4.5 5.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 2-Hexanone [591-78-6]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 04:57 kkw 4-Methyl-2-pentanone [108-10-1]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 04:57 kkw Acetone [67-64-1]^ 10 U ug/L 1 10 20 1D16032 EPA 8260D 04/17/21 04:57 kkw Acrylonitrile [107-13-1]^ 5.0 U ug/L 1 5.0 10 1D16032 EPA 8260D 04/17/21 04:57 kkw Benzene [71-43-2]^ 3.2 ug/L 1 0.71 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw Bromochloromethane [74-97-5]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 39 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CE04872-03 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 10:05 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS A - ENCO Orlando certified analyte [NC 424] Analvte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes Bromodichloromethane [75-27-4]^ 0.52 u ug/L 1 0.52 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Bromoform [75-25-2]^ 0.75 u ug/L 1 0.75 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Bromomethane [74-83-9]^ 0.95 u ug/L 1 0.95 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Carbon disulfide [75-15-0]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Carbon tetrachloride [56-23-5]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Chlorobenzene [308-90-7]^ 3.8 ug/L 1 0.72 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw Chloroethane [75-00-3]^ 0.98 u ug/L 1 0.98 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Chloroform [67-66-3]^ 0.80 u ug/L 1 0.80 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Chloromethane [74-87-3]^ 0.82 u ug/L 1 0.82 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw cis-1,2-Dichloroethene [1S6-S9-2]^ 0.71 J ug/L 1 0.53 1.0 1D16032 EPA 8260D 04/17/21 04:57 kkw cis-1,3-Dichloropropene [10061-01-5]^ 0.59 u ug/L 1 0.59 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Dibromochloromethane [124-48-1]^ 0.50 u ug/L 1 0.50 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Dibromomethane [74-95-3]^ 0.84 u ug/L 1 0.84 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Ethylbenzene [500-41-4]^ 0.69 u ug/L 1 0.69 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Iodomethane [74-88-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Methylene chloride [75-09-2]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Styrene [100-42-5]^ 0.61 u ug/L 1 0.61 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Tetrachloroethene [127-18-4]^ 0.76 u ug/L 1 0.76 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Toluene [108-88-3]^ 0.72 u ug/L 1 0.72 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw trans-1,2-Dichloroethene [156-60-5]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw trans-1,3-Dichloropropene [10061-02-6]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw trans-1,4-Dichloro-2-butene [110-57-6]^ 0.79 u ug/L 1 0.79 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Trichloroethene [79-01-6]^ 0.89 u ug/L 1 0.89 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Trichlorofluoromethane [75-69-4]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Vinyl acetate [108-05-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Vinyl chloride [75-01-4]^ 0.71 u ug/L 1 0.71 1.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Xylenes(Total)[1330-20-7]^ 1.3 u ug/L 1 1.3 2.0 ID16032 EPA 8260D 04/17/21 04:57 kkw Surrogates Results DF Spike L v/ % Rec % Rec Limits Batch Method Analyzed " Notes 4-Bromofluorobenzene 55 1 50.0 110 % 41-142 ID16032 EPA 8260D 04117121 04:57 kkw Dibromofluoromethane 54 1 50.0 107 % 53-146 ID16032 EPA 8260D 04117121 04:57 kkw Toluene-& 46 1 50.0 93 % 41-146 ID16032 EPA 8260D 04117121 04:57 kkw Volatile Organic Compounds by GCMS SIM Isotope Dilution A - ENCO Orlando certified analyte [NC 4241 Analvte rCAS Numberl Results Flaa Units DF MDL 4 Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 22 ug/L 1 0.80 2.0 1D21017 EPA 8260D 04/21/21 12:11 KKW Surrogates Toluene-d8 Results DF Spike Lv/ %Rec %Rec Limits Batch Method Ana 8 y Notes 4.9 1 5.00 99 % 75-125 1D21017 EPA 8260D 04121121 12:11 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CE04872-03 Received: 04/13/21 16:21 Matrix: Ground Water Sampled:04/13/21 10:05 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 126 mg/L 1 2.07 2.50 1D20005 RSK 175 04/20/21 10:43 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 10:43 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 10:43 JMW Methane [74-82-8] 6.37 D mg/L 21 0.0840 0.105 1D20005 RSK 175 04/20/21 13:54 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 18 mg/L 1 0.54 1.0 1D22009 EPA 9060A 04/22/21 15:57 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CE04872-04 Received: 04/13/21 16:21 Matrix: Ground Water Sampled: 04/13/2109:05 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 15:18 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D15015 EPA 6010D 04/19/21 13:04 JDH Barium [7440-39-3]^ 78.2 ug/L 1 1.10 10.0 1D15015 EPA 6010D 04/19/21 13:04 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D15015 EPA 6010D 04/19/21 13:04 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 13:04 JDH Lead [7439-92-1]^ 10.9 ug/L 1 3.10 10.0 1D15015 EPA 6010D 04/19/21 13:04 JDH Selenium [7782-49-2]^ 6.20 u ug/L 1 6.20 10.0 1D15015 EPA 6010D 04/19/21 13:04 JDH Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 1D15015 EPA 6010D 04/19/21 13:04 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 99 D mg/L 2 4.4 10 1D16017 EPA 300.0 04/16/21 22:23 LII Nitrate as N [14797-55-8] 0.041 u mg/L 1 0.041 0.10 [CALC] EPA 353.2 04/21/21 12:14 JAH Nitrate/Nitrite as N^ 0.041 u mg/L 1 0.041 0.10 1D21010 EPA 353.2 04/21/21 12:14 JAH Nitrite as N [14797-65-0]^ 0.017 u mg/L 1 0.017 0.10 1D14029 EPA 353.2 04/14/21 15:12 JAH Sulfate as SO4 [14808-79-8]^ 2.9 u mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 06:21 LII Sulfide [18496-25-8]^ 0.16 mg/L 1 0.010 0.10 1D19020 iM 4500S2 D-2011 04/19/21 17:12 JOC Total Alkalinity as CaCO3 [471-34-1]^ 760 D mg/L 5 70 75 1D15027 EPA 310.2 04/15/21 16:04 JAH Volatile Organic Compounds by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.61 U ug/L 1 0.61 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,1,1-Trichloroethane [71-55-6]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.54 U ug/L 1 0.54 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,1,2-Trichloroethane [79-00-5]^ 0.76 U ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,1-Dichloroethane [75-34-3]^ 0.62 U ug/L 1 0.62 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,1-Dichloroethene [75-35-4]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,2,3-Trichloropropane [96-18-4]^ 0.64 U ug/L 1 0.64 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.96 U ug/L 1 0.96 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,2-Dibromoethane [106-93-4]^ 0.78 U ug/L 1 0.78 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,2-Dichlorobenzene [95-50-1]^ 0.73 U ug/L 1 0.73 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,2-Dichloroethane [107-06-2]^ 0.63 U ug/L 1 0.63 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,2-Dichloropropane [78-87-5]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 1,4-Dichlorobenzene [106-46-7]^ 2.7 ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 2-Butanone [78-93-3]^ 4.5 U ug/L 1 4.5 5.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 2-Hexanone [591-78-6]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 05:25 kkw 4-Methyl-2-pentanone [108-10-1]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 05:25 kkw Acetone [67-64-1]^ 10 U ug/L 1 10 20 1D16032 EPA 8260D 04/17/21 05:25 kkw Acrylonitrile [107-13-1]^ 5.0 U ug/L 1 5.0 10 1D16032 EPA 8260D 04/17/21 05:25 kkw Benzene [71-43-2]^ 3.2 ug/L 1 0.71 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw Bromochloromethane [74-97-5]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 39 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CE04872-04 Received: 04/13/21 16:21 Matrix: Ground Water Sampled: 04/13/2109:05 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS A - ENCO Orlando certified analyte [NC 424] Analvte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes Bromodichloromethane [75-27-4]^ 0.52 u ug/L 1 0.52 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Bromoform [75-25-2]^ 0.75 u ug/L 1 0.75 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Bromomethane [74-83-9]^ 0.95 u ug/L 1 0.95 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Carbon disulfide [75-15-0]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Carbon tetrachloride [56-23-5]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Chlorobenzene [308-90-7]^ 10 ug/L 1 0.72 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw Chloroethane [75-00-3]^ 0.98 U ug/L 1 0.98 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Chloroform [67-66-3]^ 0.80 U ug/L 1 0.80 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Chloromethane [74-87-3]^ 0.82 U ug/L 1 0.82 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw cis-1,2-Dichloroethene [1S6-S9-2]^ 1.2 ug/L 1 0.53 1.0 1D16032 EPA 8260D 04/17/21 05:25 kkw cis-1,3-Dichloropropene [10061-01-5]^ 0.59 U ug/L 1 0.59 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Dibromochloromethane [124-48-1]^ 0.50 u ug/L 1 0.50 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Dibromomethane [74-95-3]^ 0.84 u ug/L 1 0.84 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Ethylbenzene [100-41-4]^ 0.69 u ug/L 1 0.69 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Iodomethane [74-88-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Methylene chloride [75-09-2]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Styrene [100-42-5]^ 0.61 u ug/L 1 0.61 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Tetrachloroethene [127-18-4]^ 0.76 u ug/L 1 0.76 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Toluene [108-88-3]^ 0.72 u ug/L 1 0.72 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw trans-1,2-Dichloroethene [156-60-5]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw trans-1,3-Dichloropropene [10061-02-6]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw trans-1,4-Dichloro-2-butene [110-57-6]^ 0.79 u ug/L 1 0.79 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Trichloroethene [79-01-6]^ 0.89 u ug/L 1 0.89 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Trichlorofluoromethane [75-69-4]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Vinyl acetate [108-05-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Vinyl chloride [75-01-4]^ 0.71 u ug/L 1 0.71 1.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Xylenes(Total)[1330-20-7]^ 1.3 u ug/L 1 1.3 2.0 ID16032 EPA 8260D 04/17/21 05:25 kkw Surrogates Results DF Spike L v/ % Rec % Rec Limits Batch Method Analyzed " Notes 4-Bromofluorobenzene 53 1 50.0 107 % 41-142 ID16032 EPA 8260D 04117121 05:25 kkw Dibromofluoromethane 51 1 50.0 101 % 53-146 ID16032 EPA 8260D 04117121 05:25 kkw Toluene-& 54 1 50.0 109 % 41-146 ID16032 EPA 8260D 04117121 05:25 kkw Volatile Organic Compounds by GCMS SIM Isotope Dilution A - ENCO Orlando certified analyte [NC 4241 Analvte rCAS Numberl Results Flaa Units DF MDL 4 Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 30 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 22:32 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 4.9 1 5.00 98 % 75-125 1D20044 EPA 8260D 04120121 22:32 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CE04872-04 Received: 04/13/21 16:21 Matrix: Ground Water Sampled: 04/13/2109:05 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 2.07 U mg/L 1 2.07 2.50 1D20005 RSK 175 04/20/21 14:57 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 14:57 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 14:57 JMW Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 1D20005 RSK 175 04/20/21 14:57 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 34 mg/L 1 0.54 1.0 1D22022 EPA 9060A 04/22/21 21:56 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CE04872-05 Received: 04/13/21 16:21 Matrix: Ground Water Sampled: 04/13/2108:50 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 15:20 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D15015 EPA 6010D 04/19/21 13:06 JDH Barium [7440-39-3]^ 25.0 ug/L 1 1.10 10.0 1D15015 EPA 6010D 04/19/21 13:06 JDH Cadmium [7440-43-9]^ 0.855 J ug/L 1 0.360 1.00 1D15015 EPA 6010D 04/19/21 13:06 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 13:06 JDH Lead [7439-92-1]^ 13.0 ug/L 1 3.10 10.0 1D15015 EPA 6010D 04/19/21 13:06 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1D15015 EPA 6010D 04/19/21 13:06 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D15015 EPA 6010D 04/19/21 13:06 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 3.1 J mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 06:39 LII Nitrate as N [14797-55-8] 0.041 U mg/L 1 0.041 0.10 [CALC] EPA 353.2 04/21/21 12:16 JAH Nitrate/Nitrite as N^ 0.041 U mg/L 1 0.041 0.10 1D21010 EPA 353.2 04/21/21 12:16 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1D14029 EPA 353.2 04/14/21 15:12 JAH Sulfate as SO4 [14808-79-8]^ 6.8 mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 06:39 LII Sulfide [18496-25-8]^ 0.035 J mg/L 1 0.010 0.10 1D19020 >M 4500S2 D-2011 04/19/21 17:12 JOC Total Alkalinity as CaCO3 [471-34-1]^ 110 mg/L 1 14 15 1D15027 EPA 310.2 04/15/21 16:05 JAH Volatile Organic Compounds by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.61 U ug/L 1 0.61 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,1,1-Trichloroethane [71-55-6]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.54 U ug/L 1 0.54 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,1,2-Trichloroethane [79-00-5]^ 0.76 U ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,1-Dichloroethane [75-34-3]^ 0.62 U ug/L 1 0.62 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,1-Dichloroethene [75-35-4]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,2,3-Trichloropropane [96-18-4]^ 0.64 U ug/L 1 0.64 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.96 U ug/L 1 0.96 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,2-Dibromoethane [106-93-4]^ 0.78 U ug/L 1 0.78 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,2-Dichlorobenzene [95-50-1]^ 0.73 U ug/L 1 0.73 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,2-Dichloroethane [107-06-2]^ 0.63 U ug/L 1 0.63 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,2-Dichloropropane [78-87-5]^ 0.80 U ug/L 1 0.80 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 1,4-Dichlorobenzene [106-46-7]^ 0.76 U ug/L 1 0.76 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 2-Butanone [78-93-3]^ 4.5 U ug/L 1 4.5 5.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 2-Hexanone [591-78-6]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 05:53 kkw 4-Methyl-2-pentanone [108-10-1]^ 2.5 U ug/L 1 2.5 5.0 1D16032 EPA 8260D 04/17/21 05:53 kkw Acetone [67-64-1]^ 10 U ug/L 1 10 20 1D16032 EPA 8260D 04/17/21 05:53 kkw Acrylonitrile [107-13-1]^ 5.0 U ug/L 1 5.0 10 1D16032 EPA 8260D 04/17/21 05:53 kkw Benzene [71-43-2]^ 0.78 J ug/L 1 0.71 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw Bromochloromethane [74-97-5]^ 0.94 U ug/L 1 0.94 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 39 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CE04872-05 Received: 04/13/21 16:21 Matrix: Ground Water Sampled: 04/13/2108:50 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS A - ENCO Orlando certified analyte [NC 424] Analvte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes Bromodichloromethane [75-27-4]^ 0.52 u ug/L 1 0.52 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Bromoform [75-25-2]^ 0.75 u ug/L 1 0.75 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Bromomethane [74-83-9]^ 0.95 u ug/L 1 0.95 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Carbon disulfide [75-15-0]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Carbon tetrachloride [56-23-5]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Chlorobenzene [508-90-7]^ 0.72 u ug/L 1 0.72 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Chloroethane [75-00-3]^ 0.98 u ug/L 1 0.98 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Chloroform [67-66-3]^ 0.80 u ug/L 1 0.80 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Chloromethane [74-87-3]^ 0.82 u ug/L 1 0.82 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw cis-1,2-Dichloroethene [156-59-2]^ 2.5 ug/L 1 0.53 1.0 1D16032 EPA 8260D 04/17/21 05:53 kkw cis-1,3-Dichloropropene [10061-01-5]^ 0.59 U ug/L 1 0.59 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Dibromochloromethane [124-48-1]^ 0.50 u ug/L 1 0.50 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Dibromomethane [74-95-3]^ 0.84 u ug/L 1 0.84 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Ethylbenzene [500-41-4]^ 0.69 u ug/L 1 0.69 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Iodomethane [74-88-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Methylene chloride [75-09-2]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Styrene [100-42-5]^ 0.61 u ug/L 1 0.61 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Tetrachloroethene [127-18-4]^ 0.76 u ug/L 1 0.76 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Toluene [108-88-3]^ 0.72 u ug/L 1 0.72 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw trans-1,2-Dichloroethene [156-60-5]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw trans-1,3-Dichloropropene [10061-02-6]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw trans-1,4-Dichloro-2-butene [110-57-6]^ 0.79 u ug/L 1 0.79 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Trichloroethene [79-01-6]^ 0.89 u ug/L 1 0.89 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Trichlorofluoromethane [75-69-4]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Vinyl acetate [108-05-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Vinyl chloride [75-01-4]^ 0.71 u ug/L 1 0.71 1.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Xylenes(Total)[1330-20-7]^ 1.3 u ug/L 1 1.3 2.0 ID16032 EPA 8260D 04/17/21 05:53 kkw Surrogates Results DF Spike L v/ % Rec % Rec Limits Batch Method Analyzed " Notes 4-Bromofluorobenzene 54 1 50.0 107 % 41-142 ID16032 EPA 8260D 04117121 05:53 kkw Dibromofluoromethane 56 1 50.0 112 % 53-146 ID16032 EPA 8260D 04117121 05:53 kkw Toluene-& 53 1 50.0 107 % 41-146 ID16032 EPA 8260D 04117121 05:53 kkw Volatile Organic Compounds by GCMS SIM Isotope Dilution A - ENCO Orlando certified analyte [NC 4241 Analvte rCAS Numberl Results Flaa Units DF MDL 4 Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 2.2 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 22:57 KKW Surrogates Toluene-d8 Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 5.0 1 5.00 100 % 75-125 1D20044 EPA 8260D 04120121 22:57 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CE04872-05 Received: 04/13/21 16:21 Matrix: Ground Water Sampled: 04/13/2108:50 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: Gary Simcox/James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 242 D mg/L 21 43.5 52.5 1D20005 RSK 175 04/20/21 14:09 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 11:15 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1D20005 RSK 175 04/20/21 11:15 JMW Methane [74-82-8] 1.64 D mg/L 21 0.0840 0.105 1D20005 RSK 175 04/20/21 14:09 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 2.5 mg/L 1 0.54 1.0 1D22009 EPA 9060A 04/22/21 16:58 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 39 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIPBLANK Lab Sample ID:CE04872-06 Received: 04/13/21 16:21 Matrix: Water Sampled: 04/13/2108:50 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.61 u ug/L 1 0.61 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,1,1-Trichloroethane [71-55-6]^ 0.80 u ug/L 1 0.80 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,1,2,2-Tetrachloroethane [79-34-5]A 0.54 u ug/L 1 0.54 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,1,2-Trichloroethane [79-00-5]^ 0.76 u ug/L 1 0.76 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,1-Dichloroethane [75-34-3]^ 0.62 u ug/L 1 0.62 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,1-Dichloroethene [75-35-4]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,2,3-Trichloropropane [96-18-4]^ 0.64 u ug/L 1 0.64 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.96 u ug/L 1 0.96 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,2-Dibromoethane [106-93-4]^ 0.78 u ug/L 1 0.78 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,2-Dichlorobenzene [95-50-1]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,2-Dichloroethane [107-06-2]^ 0.63 u ug/L 1 0.63 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,2-Dichloropropane [78-87-5]^ 0.80 u ug/L 1 0.80 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 1,4-Dichlorobenzene [106-46-7]^ 0.76 u ug/L 1 0.76 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 2-Butanone [78-93-3]^ 4.5 u ug/L 1 4.5 5.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 2-Hexanone [591-78-6]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 06:21 kkw 4-Methyl-2-pentanone [108-10-1]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Acetone[67-64-1]A 10 u ug/L 1 10 20 ID16032 EPA 8260D 04/17/21 06:21 kkw Acrylonitrile [107-13-1]^ 5.0 u ug/L 1 5.0 10 ID16032 EPA 8260D 04/17/21 06:21 kkw Benzene[71-43-2]A 0.71 u ug/L 1 0.71 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Bromochloromethane [74-97-5]A 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Bromodichloromethane [75-27-4]^ 0.52 u ug/L 1 0.52 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Bromoform [75-25-2]^ 0.75 u ug/L 1 0.75 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Bromomethane [74-83-9]A 0.95 u ug/L 1 0.95 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Carbon disulfide [75-15-0]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Carbon tetrachloride [56-23-5]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Chlorobenzene [108-90-7]A 0.72 u ug/L 1 0.72 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Chloroethane [75-00-3]^ 0.98 u ug/L 1 0.98 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Chloroform [67-66-3]^ 0.80 u ug/L 1 0.80 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Chloromethane [74-87-3]^ 0.82 u ug/L 1 0.82 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw cis-1,2-Dichloroethene [156-59-2]^ 0.53 u ug/L 1 0.53 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw cis-1,3-Dichloropropene [10061-01-5]^ 0.59 u ug/L 1 0.59 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Dibromochloromethane [124-48-1]A 0.50 u ug/L 1 0.50 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Dibromomethane [74-95-3]^ 0.84 u ug/L 1 0.84 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Ethylbenzene [100-41-4]A 0.69 u ug/L 1 0.69 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Iodomethane [74-88-4]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Methylene chloride [75-09-2]^ 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Styrene [100-42-5]^ 0.61 u ug/L 1 0.61 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Tetrachloroethene [127-18-4]^ 0.76 u ug/L 1 0.76 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Toluene [108-88-3]^ 0.72 u ug/L 1 0.72 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw trans-1,2-Dichloroethene [156-60-5]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw trans-1,3-Dichloropropene [10061-02-6]^ 0.73 u ug/L 1 0.73 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw trans-1,4-Dichloro-2-butene [110-57-6]A 0.79 u ug/L 1 0.79 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Trichloroethene [79-01-6]^ 0.89 u ug/L 1 0.89 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Trichlorofluoromethane [75-69-4]^ 0.94 u ug/L 1 0.94 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Vinyl acetate [108-05-4]A 2.5 u ug/L 1 2.5 5.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Vinyl chloride [75-01-4]^ 0.71 u ug/L 1 0.71 1.0 ID16032 EPA 8260D 04/17/21 06:21 kkw Xylenes(Total)[1330-20-7]^ 1.3 u ug/L 1 1.3 2.0 ID16032 EPA 8260D 04/17/21 06:21 kkw FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 39 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIPBLANK Lab Sample ID:CE04872-06 Received: 04/13/21 16:21 Matrix: Water Sampled: 04/13/2108:50 Work Order: CE04872 Project: Moore County MSW LF CA Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Orlando certified analyte [NC 424] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 106 % 41-142 1D16032 EPA 6260D 04117121 06:21 kkw Dibromofluoromethane 52 1 50.0 104 % 53-146 ID16032 EPA 6260D 04117121 06:21 kkw Toluene-d8 51 1 50.0 102 % 41-146 ID16032 EPA 6260D 04117121 06:21 kkw Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 ID20044 EPA 8260D 04/20/21 14:55 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffly Notes Toluene-d8 5.2 1 5.00 104 % 75-125 1D20044 EPA 8260D 04120121 14:55 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch ID19009 - EPA 7470A Blank (1D19009-BLK1) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:04 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (11319009-BS1) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:07 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Mercury 5.28 0.200 ug/L 5.00 106 80-120 Matrix Spike (1D19009-MS1) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:11 Source: CE04871-07 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Mercury 5.23 0.200 ug/L 5.00 0.150 U 105 75-125 Matrix Spike Dup (11319009-MSDI) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:14 Source: CE04871-07 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Mercury 5.04 0.200 ug/L 5.00 0.150 U 101 75-125 4 25 Post Spike (11319009-PS1) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:16 Source: CE04871-07 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Mercury 5.41 0.200 ug/L 5.00 0.0300 108 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch ID15015 - EPA 3005A Blank (1D35015-BLK3) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:31 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L LCS (1D15015-BSI) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:36 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Arsenic 203 10.0 ug/L 200 101 80-120 Barium 215 10.0 ug/L 200 107 80-120 Cadmium 20.4 1.00 ug/L 20.0 102 80-120 Chromium 205 10.0 ug/L 200 102 80-120 Lead 212 10.0 ug/L 200 106 80-120 Selenium 204 10.0 ug/L 200 102 80-120 Silver 209 10.0 ug/L 200 105 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1D15015 - EPA 3005A - Continued Matrix Spike (1D15015-MS1) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:39 Source: CE04871-14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 202 10.0 ug/L 200 7.60 U 101 75-125 Barium 231 10.0 ug/L 200 20.8 105 75-125 Cadmium 20.4 1.00 ug/L 20.0 0.360 U 102 75-125 Chromium 202 10.0 ug/L 200 1.40 U 101 75-125 Lead 210 10.0 ug/L 200 4.55 103 75-125 Selenium 198 10.0 ug/L 200 6.20 U 99 75-125 Silver 205 10.0 ug/L 200 1.90 U 103 75-125 Matrix Spike Dup (1D35015-MSDl) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:46 Source: CE04871-14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 209 10.0 ug/L 200 7.60 U 105 75-125 4 20 Barium 236 10.0 ug/L 200 20.8 107 75-125 2 20 Cadmium 20.7 1.00 ug/L 20.0 0.360 U 103 75-125 1 20 Chromium 207 10.0 ug/L 200 1.40 U 103 75-125 2 20 Lead 212 10.0 ug/L 200 4.55 104 75-125 1 20 Selenium 204 10.0 ug/L 200 6.20 U 102 75-125 3 20 Silver 210 10.0 ug/L 200 1.90 U 105 75-125 3 20 Post Spike (11315015-PSI) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:49 Source: CE04871-14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.196 0.0100 mg/L 0.200 0.00250 97 80-120 Barium 0.226 0.0100 mg/L 0.200 0.0208 103 80-120 Cadmium 0.0199 0.00100 mg/L 0.0200 -0.000123 99 80-120 Chromium 0.197 0.0100 mg/L 0.200 -0.000556 98 80-120 Lead 0.207 0.0100 mg/L 0.200 0.00455 101 80-120 Selenium 0.192 0.0100 mg/L 0.200 -0.0109 96 80-120 Silver 0.205 0.0100 mg/L 0.200 0.000876 102 80-120 Batch 1 E07007 - EPA 3005A Blank (3E07007-BLK1) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 12:45 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 3.10 U 10.0 ug/L Blank (3E07007-BLK2) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 12:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 3.10 U 10.0 ug/L LCS (3E07007-BSI) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 12:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 193 10.0 ug/L 200 97 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1E07007 - EPA 3005A - Continued Matrix Spike (lE07007-MS1) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 13:00 Source: CE05406-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 160 10.0 ug/L 200 3.10 U 80 75-125 Matrix Spike Dup (1E07007-MSD1) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 13:02 Source: CE05406-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 163 10.0 ug/L 200 3.10 U 81 75-125 2 20 Post Spike (lE07007-PSI) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 13:05 Source: CE05406-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 0.169 0.0100 mg/L 0.200-0.00126 85 80-120 Classical Chemistry Parameters - Quality Control Batch ID14029 - NO PREP Blank (lD14029-BLKI) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 14:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (lD14029-BSI) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 15:15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.96 0.10 mg/L 1.00 96 90-110 Matrix Spike (111314029-MS3) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 14:50 Source: CE04807-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 Matrix Spike (1D14029-MS2) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 14:53 Source: CE04807-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.92 0.10 mg/L 1.00 0.017 U 92 90-110 Matrix Spike Dup (1D14029-MSD1) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 14:51 Source: CE04807-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.98 0.10 mg/L 1.00 0.017 U 98 90-110 2 10 Batch ID15027 - NO PREP Blank (1D35027-BLK3) Prepared: 04/15/2021 13:20 Analyzed: 04/15/2021 15:49 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1 D15027 - NO PREP - Continued LCS (111315027-BSI) Prepared: 04/15/2021 13:20 Analyzed: 04/15/2021 15:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 100 80-120 Matrix Spike (111315027-MS3) Prepared: 04/15/2021 13:20 Analyzed: 04/15/2021 15:52 Source: CE04575-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 170 15 mg/L 37.8 120 124 80-120 QM-07 Matrix Spike Dup (1D35027-MSD1) Prepared: 04/15/2021 13:20 Analyzed: 04/15/2021 15:52 Source: CE04575-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 170 15 mg/L 37.8 120 136 80-120 3 25 QM-07 Batch ID15028 - NO PREP Blank (1D35028-BLK1) Prepared: 04/15/2021 13:23 Analyzed: 04/15/2021 23:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (1D15028-BSI) Prepared: 04/15/2021 13:23 Analyzed: 04/16/2021 00:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 51 5.0 mg/L 50.0 102 90-110 Sulfate as SO4 50 5.0 mg/L 50.0 101 90-110 Matrix Spike (111315028-MS3) Prepared: 04/15/2021 13:23 Analyzed: 04/16/2021 01:21 Source: CE04663-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 520 E 10 mg/L 40.0 480 106 90-110 Sulfate as SO4 51 10 mg/L 40.0 11 100 90-110 Matrix Spike (ID15028-MS2) Prepared: 04/15/2021 13:23 Analyzed: 04/16/2021 02:14 Source: CE04808-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 50 5.0 mg/L 20.0 26 123 90-110 Sulfate as SO4 19 5.0 mg/L 20.0 2.9 U 97 90-110 Matrix Spike Dup (1D35028-MSDi) Prepared: 04/15/2021 13:23 Analyzed: 04/16/2021 01:38 Source: CE04663-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 520 E 10 mg/L 40.0 480 111 90-110 0.4 10 Sulfate as SO4 46 10 mg/L 40.0 11 88 90-110 10 10 Batch ID16007 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1 D16007 - NO PREP - Continued Blank (1D16007-BLK1) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (1D16007-BS1) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.44 0.10 mg/L 0.401 109 80-120 Duplicate (1D36007-DUP3) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Source: CE04541-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 1.3 0.50 mg/L 1.2 5 25 Matrix Spike (1D16007-MS1) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Source: CE04541-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 3.5 0.50 mg/L 2.00 1.2 112 80-120 Matrix Spike Dup (1D36007-MSD1) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Source: CE04541-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 3.6 0.50 mg/L 2.00 1.2 117 80-120 3 25 Batch ID16017 - NO PREP Blank (lD16017-BLK3) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 15:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L LCS (1D16017-BS1) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 15:36 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 51 5.0 mg/L 50.0 103 90-110 Matrix Spike (1D16017-MS3) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 16:12 Source: CE04314-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 900 50 mg/L 200 66 415 90-110 QM-07 Matrix Spike (1D16017-MS2) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 17:05 Source: CE04575-03RE3 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 24 5.0 mg/L 20.0 3.8 103 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1 D16017 - NO PREP - Continued Matrix Spike Dup (lD16017-MSDI) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 16:29 Source: CE04314-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 890 50 mg/L 200 66 412 90-110 0.7 10 QM-07 Batch ID19020 - NO PREP Blank (1D39020-BLK3) Prepared: 04/19/2021 16:59 Analyzed: 04/19/2021 17:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (1D39020-BSI) Prepared: 04/19/2021 16:59 Analyzed: 04/19/2021 17:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.42 0.10 mg/L 0.401 106 80-120 Duplicate (1D19020-DUP1) Prepared: 04/19/2021 16:59 Analyzed: 04/19/2021 17:12 Source: CE04872-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L 0.010 U 25 Matrix Spike (1D19020-MS3) Prepared: 04/19/2021 16:59 Analyzed: 04/19/2021 17:12 Source: CE04872-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.26 0.10 mg/L 0.401 0.010 U 65 80-120 QM-07 Matrix Spike Dup (1D39020-MSD1) Prepared: 04/19/2021 16:59 Analyzed: 04/19/2021 17:12 Source: CE04872-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.24 0.10 mg/L 0.401 0.010 U 60 80-120 8 25 QM-07 Batch ID20009 - NO PREP Blank (1D20009-BLK1) Prepared: 04/20/2021 08:28 Analyzed: 04/20/2021 10:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (1D20009-BS1) Prepared: 04/20/2021 08:28 Analyzed: 04/20/2021 11:00 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 102 80-120 Matrix Spike (1D20009-MS3) Prepared: 04/20/2021 08:28 Analyzed: 04/20/2021 11:01 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 230 E 15 mg/L 37.8 210 46 80-120 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 30 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1D20009 - NO PREP - Continued Matrix Spike Dup (1D20009-MSDI) Prepared: 04/20/2021 08:28 Analyzed: 04/20/2021 11:02 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 230 E 15 mg/L 37.8 210 48 80-120 0.4 25 QM-07 Batch ID21010 - NO PREP Blank (1D21010-BLK3) Prepared: 04/21/2021 08:28 Analyzed: 04/21/2021 11:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (1D23030-BSI) Prepared: 04/21/2021 08:28 Analyzed: 04/21/2021 11:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.2 0.10 mg/L 1.25 99 90-110 Matrix Spike (1D23010-MS1) Prepared: 04/21/2021 08:28 Analyzed: 04/21/2021 11:45 Source: CE03388-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.54 0.10 mg/L 0.521 0.041 U 104 90-110 Matrix Spike (111323030-MS2) Prepared: 04/21/2021 08:28 Analyzed: 04/21/2021 11:51 Source: CE04663-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.60 0.10 mg/L 0.521 0.084 99 90-110 Matrix Spike Dup (1D23030-MSD1) Prepared: 04/21/2021 08:28 Analyzed: 04/21/2021 11:47 Source: CE03388-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.59 0.10 mg/L 0.521 0.041 U 112 90-110 8 10 QM-07 Batch ID21015 - NO PREP Blank (1D21015-BLK1) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 13:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (1D23015-BS3) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 13:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 1.25 102 90-110 Matrix Spike (1D23015-MS3) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 13:52 Source: CE04807-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.57 0.10 mg/L 0.521 0.041 U 109 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 39 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1D21015 - NO PREP - Continued (� �Eo www.encolabs.com Matrix Spike (111323015-MS2) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 14:01 Source: CE04807-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.57 0.10 mg/L 0.521 0.041 U 109 90-110 Matrix Spike Dup (1D23015-MSDl) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 13:54 Source: CE04807-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.58 0.10 mg/L 0.521 0.041 U 112 90-110 2 10 QM-07 Volatile Organic Compounds by GCMS - Quality Control Batch ID16032 - EPA 5030E MS Blank (1D36032-BLKl) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 21:59 Analvte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dich loroethane 1,1-Dich loroethene 1,2,3-Trichloropropane 1,2-Di bromo-3-ch loropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,4-Dichlorobenzene 2-Butanone 2-Hexanone 4-Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromod ich lorometha ne Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1, 2-Dich loroethene cis-1,3-Dich loropropene D i b ro m oc h l o ro m et h a n e Dibromomethane Ethylbenzene Iodomethane Result Flaq POL Units 0.61 U 1.0 ug/L 0.80 U 1.0 ug/L 0.54 U 1.0 ug/L 0.76 U 1.0 ug/L 0.62 U 1.0 ug/L 0.94 U 1.0 ug/L 0.64 U 1.0 ug/L 0.96 U 1.0 ug/L 0.78 U 1.0 ug/L 0.73 U 1.0 ug/L 0.63 U 1.0 ug/L 0.80 U 1.0 ug/L 0.76 U 1.0 ug/L 4.5 U 5.0 ug/L 2.5 U 5.0 ug/L 2.5 U 5.0 ug/L 10 U 20 ug/L 5.0 U 10 ug/L 0.71 U 1.0 ug/L 0.94 U 1.0 ug/L 0.52 U 1.0 ug/L 0.75 U 1.0 ug/L 0.95 U 1.0 ug/L 2.5 U 5.0 ug/L 0.94 U 1.0 ug/L 0.72 U 1.0 ug/L 0.98 U 1.0 ug/L 0.80 U 1.0 ug/L 0.82 U 1.0 ug/L 0.53 U 1.0 ug/L 0.59 U 1.0 ug/L 0.50 U 1.0 ug/L 0.84 U 1.0 ug/L 0.69 U 1.0 ug/L 2.5 U 5.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 32 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1D16032 - EPA 5030B MS - Continued Blank (SD36032-BLK1) Continued Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 21:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Methylene chloride 2.5 U 5.0 ug/L Styrene 0.61 U 1.0 ug/L Tetrachloroethene 0.76 U 1.0 ug/L Toluene 0.72 U 1.0 ug/L trans-1,2-Dichloroethene 0.73 U 1.0 ug/L trans-1,3-Dichloropropene 0.73 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.79 U 1.0 ug/L Trichloroethene 0.89 U 1.0 ug/L Trichlorofluoromethane 0.94 U 1.0 ug/L Vinyl acetate 2.5 U 5.0 ug/L Vinyl chloride 0.71 U 1.0 ug/L Xylenes (Total) 1.3 U 2.0 ug/L 4-Bromofluorobenzene 52 ug/L 50.0 104 41-142 Dibromofluoromethane 55 ug/L 50.0 110 53-146 Toluene-d8 54 ug/L 50.0 108 41-146 LCS (ID16032-BSI) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 20:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 89 47-139 Benzene 18 1.0 ug/L 20.0 92 56-136 Chlorobenzene 19 1.0 ug/L 20.0 94 51-139 Toluene 19 1.0 ug/L 20.0 97 64-131 Trichloroethene 17 1.0 ug/L 20.0 83 62-135 4-Bromofluorobenzene 54 ug/L 50.0 107 41-142 Dibromofluoromethane 55 ug/L 50.0 110 53-146 Toluene-c48 55 ug/L 50.0 110 41-146 Matrix Spike (11316032-1VIS3) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 20:35 Source: AE03128-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.94 U 114 47-139 QM-11 Benzene 21 1.0 ug/L 20.0 0.71 U 106 56-136 Chlorobenzene 20 1.0 ug/L 20.0 0.72 U 102 51-139 Toluene 21 1.0 ug/L 20.0 0.72 U 107 64-131 Trichloroethene 18 1.0 ug/L 20.0 0.89 U 91 62-135 4-Bromofluorobenzene 53 ug/L 50.0 106 41-142 Dibromofluoromethane 56 ug/L 50.0 Ili 53-146 Toluene-d8 53 ug/L 50.0 106 41-146 Matrix Spike Dup (11316032-MS131) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 21:03 Source: AE03128-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.94 U 88 47-139 26 16 QM-11 Benzene 21 1.0 ug/L 20.0 0.71 U 103 56-136 3 14 Chlorobenzene 21 1.0 ug/L 20.0 0.72 U 103 51-139 0.8 13 Toluene 21 1.0 ug/L 20.0 0.72 U 103 64-131 4 16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 33 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch ID16032 - EPA 5030B MS - Continued Matrix Spike Dup (1D16032-MSD1) Continued Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 21:03 Source: AE03128-01 Analvte Result Flaq Trichloroethene 19 POL Units 1.0 ug/L Spike Source Level Result 20.0 0.89 U %REC RPD %REC Limits RPD Limit Notes 96 62-135 5 20 4-Bromofluorobenzene 52 Dibromofluoromethane 54 Toluene-d8 55 u91L u91L u91L 50.0 50.0 50.0 103 41-142 109 53-146 110 41-146 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch ID19039 - EPA 5030E MS Blank (1D39039-BLK3) Prepared: 04/19/2021 13:46 Analyzed: 04/19/2021 23:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-d8 5.0 u91L 5.00 101 75-125 LCS (1D19039-BS1) Prepared: 04/19/2021 13:46 Analyzed: 04/20/2021 09:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 28 2.0 ug/L 25.0 114 80-133 Toluene-d8 4.8 u91L 5.00 96 75-125 Matrix Spike (1D19039-MS1) Prepared: 04/19/2021 13:46 Analyzed: 04/19/2021 22:19 Source: CE04872-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 30 2.0 ug/L 25.0 3.9 104 80-133 Toluene-d8 5.4 u91L 5.00 108 75-125 Matrix Spike Dup (111319039-MSDI) Prepared: 04/19/2021 13:46 Analyzed: 04/19/2021 22:44 Source: CE04872-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 30 2.0 ug/L 25.0 3.9 106 80-133 1 19 Toluene-d8 4.9 u91L 5.00 98 75-125 Batch ID20044 - EPA 5030B MS Blank (1D20044-BLK3) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 14:15 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-d8 4.9 u91L 5.00 99 75-125 LCS (1D20044-BSI) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 13:21 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 99 80-133 Toluene-d8 4.9 u91L 5.00 98 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 1D20044 - EPA 5030B MS - Continued Matrix Spike (1D20044-MS1) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 23:23 Source: AE03123-15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 1.1 95 80-133 Toluene-& 4.9 ug/L 5.00 98 75-125 Matrix Spike Dup (1D20044-MSD1) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 23:48 Source: AE03123-15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 1.1 96 80-133 0.7 19 Toluene-d8 5.2 u91L 5.00 104 75-125 Batch ID21017 - EPA 5030E MS Blank (1D21017-BLK3) Prepared: 04/21/2021 00:00 Analyzed: 04/21/2021 10:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-d8 4.9 u91L 5.00 98 75-125 LCS (1D23017-BS1) Prepared: 04/21/2021 00:00 Analyzed: 04/21/2021 09:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 100 80-133 Toluene-d8 4.8 u91L 5.00 97 75-125 Matrix Spike (1D23017-MS1) Prepared: 04/21/2021 00:00 Analyzed: 04/21/2021 19:47 Source: AE03180-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 99 E 2.0 ug/L 25.0 72 107 80-133 Toluene-d8 5.0 u91L 5.00 101 75-125 Matrix Spike Dup (1D21017-MSD1) Prepared: 04/21/2021 00:00 Analyzed: 04/21/2021 20:12 Source: AE03180-01 Analvte Result Flaq POL 1,4-Dioxane 97 E 2.0 Units ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 25.0 72 100 80-133 2 19 Toluene-d8 52 u91L 5.00 105 75-125 Dissolved Gases by GC - Quality Control Batch ID20005 - Same Blank (111320005-BL11(l) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 09:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 of 39 QUALITY CONTROL DATA Dissolved Gases by GC - Quality Control Batch ID20005 - Same - Continued (� �Eo www.encolabs.com LCS (1D20005-BSI) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 09:00 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 45.4 2.50 mg/L 45.8 99 70-130 Ethane 0.325 0.00600 mg/L 0.323 101 70-130 Ethene 0.317 0.00600 mg/L 0.302 105 70-130 Methane 0.177 0.00500 mg/L 0.172 103 70-130 LCS Dup (1D20005-BSD1) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 09:15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 45.4 2.50 mg/L 45.8 99 70-130 0.009 30 Ethane 0.322 0.00600 mg/L 0.323 100 70-130 0.9 30 Ethene 0.318 0.00600 mg/L 0.302 105 70-130 0.05 30 Methane 0.175 0.00500 mg/L 0.172 102 70-130 0.7 30 Duplicate (1D20005-DUP1) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 15:13 Source: AE03029-04REI Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 108 UD 130 mg/L 108 U 30 Ethane 0.265 UD 0.312 mg/L 0.265 U 30 Ethene 0.265 UD 0.312 mg/L 0.265 U 30 Methane 1.42 D 0.260 mg/L 3.41 82 30 QM-12 Classical Chemistry Parameters - Quality Control Batch ID22009 - NO PREP Blank (1D22009-BLK3) Prepared: 04/22/2021 07:41 Analyzed: 04/22/2021 09:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.54 U 1.0 mg/L LCS (1D22009-BSI) Prepared: 04/22/2021 07:41 Analyzed: 04/22/2021 09:28 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 46 1.0 mg/L 50.0 92 85-115 Matrix Spike (1D22009-MS3) Prepared: 04/22/2021 07:41 Analyzed: 04/22/2021 10:08 Source: AE03191-01RE3 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 45 1.0 mg/L 50.0 1.1 88 85-115 Matrix Spike Dup (1D22009-MSD1) Prepared: 04/22/2021 07:41 Analyzed: 04/22/2021 10:31 Source: AE03191-01REI Analvte Total Organic Carbon Batch ID22022 - NO PREP Result Flaq POL 44 1.0 Spike Source %REC Units Level Result %REC Limits RPD mg/L 50.0 1.1 87 85-115 2 RPD Limit Notes 21 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 36 of 39 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch ID22022 - NO PREP - Continued Blank (1D22022-BLK1) Prepared: 04/22/2021 09:00 Analyzed: 04/22/2021 18:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.54 U 1.0 mg/L LCS (11322022-BS1) Prepared: 04/22/2021 09:00 Analyzed: 04/22/2021 19:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 45 1.0 mg/L 50.0 91 85-115 Matrix Spike (1D22022-MS3) Prepared: 04/22/2021 09:00 Analyzed: 04/22/2021 19:44 Source: AE03191-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 41 1.0 mg/L 50.0 1.1 81 85-115 QM-07 Matrix Spike Dup (1D22022-MSDS) Prepared: 04/22/2021 09:00 Analyzed: 04/22/2021 20:07 Source: AE03191-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 41 1.0 mg/L 50.0 1.1 79 85-115 2 21 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 37 of 39 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 38 of 39 n a n a z m � P1 m W t p° '� °c m' m l71 W W O) W a Co W CA y 3 � � LA ro � l�j O? = q N (T1 a a W O ..a C] ryla, O � ij� © rl. ,i�a a v _ l� �'. m �3 � C m a 6 � ,rt a .J O �i 0a O fO 0� (D 0 O �\ P m m o w n (D C G z _ � CCC777 y N ,C b �{ VI 47 7] V V23 71 23 3 m and m m ,may ` 0 v V' H � -3 1 3 W �v+ 2 T- z O. CD rz� o 9 Qt CD Q d G} G3 m age "3 � L71 iJ1 U1 UI � o 4 16 � a ° n X X X X X 82600 Appendix 1,$2500 SaM ID w X X X X �+ Ag,As,B9,Cd,C+r,Pb,Se an d = g w o O C N a u X X X X 9 AkaHntty310.2,ChixWe 300.Nttrtte W N 7 363.2 o� a X �� � a X X X X Hg O_ - 0 o X X X X m q Nox 353.2 C X X X �>c - RSK 175 + CO2 F z X X X X Sulfate 300 o a( X X X X X Sulfide SM4500-5 0 n TOC 9060A n 3 'm y- _ n r @ a o w W a z 0 � 0 o m 3 m� 3 3 W 3 T� �- m ao X Q m N m m o {//�4�/yyV��//, m m b 6 -C y fV � p p rL cr a 98 m o Z m n 0 +� T a X 0 N � A o z am z a n O z (n o C a D Wit gz N � Q rn �b C d cr n O 3 Sample Preservation Verification Imr ENCO Cary Work Order: CE04872 Project: Moore County MSW LF CA Client: S&ME, Inc. (SM004) Project #: 4358-20-043A Phase 01 Logged In: 13-Apr-21 16:54 Logged By: Rachel An onis Preservation Check Performed By: Date/Time: ls' C E 04872-01 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted DateTBme Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 � Y l N l NA Y I 1 NA C 250mLP+ZnAc+NaOH >9 Y N / NA Y N / NA l l D 250mLP+H2SO4 <2 YJ N I NA Y/ N NA CE04872-02 Cont Type Pres (pH) Requirement pH Checked I In Control Date/Time PH Adjusted Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 / N / NA Y (EY NA C 250mLP+ZnAc+NaOH >9 Y/ N 1 NA Y/ N NA D 250mLP+H2SO4 <2 Y/ N/ NA Y/ N 1 NA CE04872-03 Cont Type Pres (pH) Requirement pH Checked I In Control pH Adjusted DatelTime Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y I N/ NA Y/ N` NA G 250mLP+ZnAc+NaOH >9 Y/ N/ NA Y N I NA D 250mLP+H2SO4 <2 / N I NA I Y N NA C E 04872-04 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 N / NA Y /(NY NA C 250mLP+ZnAc+NaOH >9 I N/ NA Y N/ NA D 250mLP+H2SO4 <2 Y N I NA Y/ N I NA C E04872-05 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 1 N/ NA Y N l NA C 250mLP+ZnAc+NaOH >9 / N / NA Y / N I NA D 250mLP+H2SO4 <2 Y I N/ NA Y/ NA Rea ent Name ID 1 u (D �A�\qn 2 pH Strip ID: PH Strips C0F0555 Rea ent Name ID 3 4 Rea ent Name ID 5 6 C:lelmntlPniiitiWKu_rreservatlonuneck.rpt Page 1 of 1 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, May 10, 2021 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043A Phase 01, Project Name/Desc: Moore County Active C & D LF - Spring ENCO Workorder(s): CE04871 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, April 13, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, O"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 98 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County Active C & D LF - Spring Lab ID: CE04871 (� �Eo www.encolabs.com Overview Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The associated LCS exhibited high bias; since the result is ND, there is no impact (QL-02). The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an acceptable LCs recovery (QM-07). Post -digestion spike did not meet method requirements due to confirmed matrix effects (QM-08). Precision between duplicate matrix spikes of the same sample was outside acceptance limits (QM-11). Precision between duplicate samples was outside acceptance limits (QM-12). Quality Control Remarks Result may be biased high. Associated CV standard exceeded the upper control limit (J-04). Result may be biased low. Assocaited CV standard did not meet the minimum control limit (J-05). The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01). Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 98 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW4 Lab ID: CE04871-01 Sampled: 04/13/21 12:25 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/16/21 12:03 04/16/21 20:02 EPA 353.2 NO PREP 04/15/21 12:25 04/14/21 13:37 04/14/21 15:05 EPA 353.2 [CALC] 04/15/21 12:25 04/21/21 10:00 04/21/21 14:24 EPA 353.2 NO PREP 05/11/21 04/21/21 10:00 04/21/21 14:24 EPA 6010D EPA 3005A 10/10/21 04/14/21 16:10 04/19/21 10:18 EPA 6020B EPA 3005A 10/10/21 04/15/21 10:43 04/20/21 08:58 EPA 7470A EPA 7470A 05/11/21 04/19/21 08:56 04/20/21 12:37 EPA 8260D EPA 503013_MS 04/27/21 04/22/21 14:56 04/23/21 17:40 EPA 9060A NO PREP 05/11/21 04/20/21 07:38 04/20/21 16:55 RSK 175 Same 04/27/21 04/15/21 15:31 04/15/21 21:05 SM 2540C-2011 NO PREP 04/20/21 04/20/21 12:00 04/22/21 08:42 SM 450052 D-2011 NO PREP 04/20/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW4 Lab ID: CE04871-OIRE1 Sampled: 04/13/21 12:25 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/20/21 11:55 04/20/21 18:22 EPA 310.2 NO PREP 04/27/21 04/20/21 08:28 04/20/21 12:01 EPA 8260D EPA 503013_MS 04/27/21 04/20/21 00:00 04/20/21 16:37 RSK 175 Same 04/27/21 04/16/21 08:00 04/16/21 14:54 Client ID: 6301-MW5 Lab ID: CE04871-02 Sampled: 04/13/21 13:15 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/16/21 12:03 04/16/21 20:19 EPA 310.2 NO PREP 04/27/21 04/20/21 08:28 04/20/21 11:05 EPA 353.2 NO PREP 04/15/21 13:15 04/14/21 13:37 04/14/21 15:06 EPA 353.2 [CALC] 04/15/21 13:15 04/21/21 10:00 04/21/21 14:26 EPA 353.2 NO PREP 05/11/21 04/21/21 10:00 04/21/21 14:26 EPA 6010D EPA 3005A 10/10/21 04/14/21 16:10 04/19/21 10:57 EPA 6020E EPA 3005A 10/10/21 04/15/21 10:43 04/20/21 09:03 EPA 7470A EPA 7470A 05/11/21 04/19/21 08:56 04/20/21 12:39 EPA 8260D EPA 503013_MS 04/27/21 04/22/21 14:56 04/23/21 18:07 EPA 9060A NO PREP 05/11/21 04/20/21 07:38 04/20/21 17:18 RSK 175 Same 04/27/21 04/15/21 15:31 04/15/21 21:21 SM 2540C-2011 NO PREP 04/20/21 04/20/21 09:35 04/22/21 08:40 SM 450052 D-2011 NO PREP 04/20/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW5 Lab ID: CE04871-02RE1 Sampled: 04/13/21 13:15 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 04/27/21 04/20/21 00:00 04/20/21 17:02 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 98 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW11SR Lab ID: CE04871-03 Sampled: 04/13/21 14:05 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/16/21 12:03 04/16/21 20:37 EPA 353.2 NO PREP 04/15/21 14:05 04/14/21 13:37 04/14/21 15:06 EPA 353.2 [CALC] 04/15/21 14:05 04/21/21 10:00 04/21/21 14:27 EPA 353.2 NO PREP 05/11/21 04/21/21 10:00 04/21/21 14:27 EPA 6010D EPA 3005A 10/10/21 04/14/21 16:10 04/19/21 11:00 EPA 6020B EPA 3005A 10/10/21 04/15/21 10:43 04/20/21 09:07 EPA 7470A EPA 7470A 05/11/21 04/19/21 08:56 04/20/21 12:44 EPA 8260D EPA 503013_MS 04/27/21 04/22/21 14:56 04/23/21 18:35 EPA 9060A NO PREP 05/11/21 04/20/21 07:38 04/20/21 17:36 RSK 175 Same 04/27/21 04/15/21 15:31 04/15/21 21:37 SM 2540C-2011 NO PREP 04/20/21 04/19/21 13:41 04/20/21 13:53 SM 450052 D-2011 NO PREP 04/20/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW11SR Lab ID: CE04871-03RE1 Sampled: 04/13/21 14:05 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 04/27/21 04/20/21 08:28 04/20/21 12:01 EPA 8260D EPA 503013_MS 04/27/21 04/20/21 00:00 04/20/21 17:28 RSK 175 Same 04/27/21 04/16/21 08:00 04/16/21 15:10 Client ID: 6301-MW11DR Lab ID: CE04871-04 Sampled: 04/12/21 15:10 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/10/21 04/16/21 12:03 04/16/21 20:55 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:02 EPA 6020B EPA 3005A 10/09/21 04/15/21 10:43 04/20/21 09:11 EPA 7470A EPA 7470A 05/10/21 04/19/21 08:56 04/20/21 12:46 EPA 8260D EPA 503013_MS 04/26/21 04/22/21 12:28 04/22/21 23:23 SM 2540C-2011 NO PREP 04/19/21 04/19/21 13:41 04/20/21 13:53 SM 450052 D-2011 NO PREP 04/19/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW11DR Lab ID: CE04871-04RE1 Sampled: 04/12/21 15:10 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 04/26/21 04/20/21 08:28 04/20/21 12:02 EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 17:53 Client ID: 6301-MW13SR Lab ID: CE04871-05 Sampled: 04/12/21 14:00 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/10/21 04/16/21 12:03 04/16/21 21:12 EPA 310.2 NO PREP 04/26/21 04/20/21 08:28 04/20/21 11:08 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:04 EPA 6020E EPA 3005A 10/09/21 04/15/21 10:43 04/20/21 09:31 EPA 7470A EPA 7470A 05/10/21 04/19/21 08:56 04/20/21 12:49 EPA 8260D EPA 503013_MS 04/26/21 04/22/21 12:28 04/22/21 23:51 SM 254OC-2011 NO PREP 04/19/21 04/19/21 13:41 04/20/21 13:53 SM 450052 D-2011 NO PREP 04/19/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW13SR Lab ID: CE04871-OSRE1 Sampled: 04/12/21 14:00 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 18:18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 98 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW13DR Lab ID: CE04871-06 Sampled: 04/12/21 15:20 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/10/21 04/16/21 12:03 04/16/21 21:30 EPA 310.2 NO PREP 04/26/21 04/20/21 08:28 04/20/21 11:09 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:07 EPA 6020B EPA 3005A 10/09/21 04/15/21 10:43 04/20/21 09:36 EPA 7470A EPA 7470A 05/10/21 04/19/21 08:56 04/20/21 13:07 EPA 8260D EPA 5030B_MS 04/26/21 04/22/21 12:28 04/23/21 00:18 SM 254OC-2011 NO PREP 04/19/21 04/19/21 13:41 04/20/21 13:53 SM 4500S2 D-2011 NO PREP 04/19/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW13DR Lab ID: CE04871-06RE1 Sampled: 04/12/21 15:20 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 18:44 Client ID: 6301-MW14 Lab ID: CE04871-07 Sampled: 04/12/21 17:20 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/10/21 04/15/21 13:23 04/16/21 03:07 EPA 310.2 NO PREP 04/26/21 04/20/21 08:28 04/20/21 11:09 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:09 EPA 6020B EPA 3005A 10/09/21 04/15/21 10:43 04/20/21 09:40 EPA 7470A EPA 7470A 05/10/21 04/19/21 09:05 04/20/21 14:09 EPA 8260D EPA 503013_MS 04/26/21 04/22/21 12:28 04/23/21 00:46 SM 2540C-2011 NO PREP 04/19/21 04/19/21 13:41 04/20/21 13:53 SM 4500S2 D-2011 NO PREP 04/19/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW14 Lab ID: CE04871-07RE1 Sampled: 04/12/21 17:20 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 04/26/21 04/20/21 00:00 04/20/21 19:09 Client ID: 6301-MW17S Lab ID: CE04871-08 Sampled: 04/12/21 11:45 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/10/21 04/15/21 13:23 04/16/21 03:24 EPA 310.2 NO PREP 04/26/21 04/20/21 08:28 04/20/21 11:10 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:16 EPA 6020E EPA 3005A 10/09/21 04/15/21 10:43 04/20/21 09:44 EPA 7470A EPA 7470A 05/10/21 04/19/21 09:05 04/20/21 14:45 EPA 8260D EPA 5030B_MS 04/26/21 04/22/21 12:28 04/23/21 01:14 SM 2540C-2011 NO PREP 04/19/21 04/19/21 13:41 04/20/21 13:53 SM 4500S2 D-2011 NO PREP 04/19/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW17S Lab ID: CE04871-08RE1 Sampled: 04/12/21 11:45 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 19:34 Client ID: 6301-MW17D Lab ID: CE04871-09 Sampled: 04/12/21 10:05 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/10/21 04/15/21 13:23 04/16/21 03:42 EPA 310.2 NO PREP 04/26/21 04/20/21 08:28 04/20/21 11:11 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:19 EPA 6020E EPA 3005A 10/09/21 04/16/21 10:33 04/20/21 10:46 EPA 7470A EPA 7470A 05/10/21 04/19/21 09:05 04/20/21 14:47 EPA 8260D EPA 503013_MS 04/26/21 04/22/21 12:28 04/23/21 01:42 SM 254OC-2011 NO PREP 04/19/21 04/19/21 13:41 04/20/21 13:53 SM 4500S2 D-2011 NO PREP 04/19/21 04/16/21 09:48 04/16/21 10:11 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 98 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW17D Lab ID: CE04871-09RE3 Sampled: 04/12/21 10:05 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 20:00 Client ID: 6301-MW18 Lab ID: CE04871-10 Sampled: 04/12/21 12:50 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/10/21 04/15/21 13:23 04/16/21 04:00 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:21 EPA 6020E EPA 3005A 10/09/21 04/16/21 10:33 04/20/21 10:50 EPA 7470A EPA 7470A 05/10/21 04/19/21 09:05 04/20/21 14:50 EPA 8081E EPA 3510C 04/19/21 05/29/21 04/19/21 08:08 04/27/21 11:56 EPA 8082A EPA 3510C 04/12/22 05/29/21 04/19/21 08:12 04/27/21 11:56 EPA 8151A EPA 3510C 04/19/21 05/29/21 04/19/21 15:30 04/22/21 17:53 EPA 8260D EPA 503013_MS 04/26/21 04/22/21 12:28 04/23/21 02:10 EPA 9014 Same 04/26/21 04/15/21 07:26 04/19/21 18:19 SM 254OC-2011 NO PREP 04/19/21 04/19/21 13:41 04/20/21 13:53 SM 4500S2 D-2011 NO PREP 04/19/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW18 Lab ID: CE04871-30RE1 Sampled: 04/12/21 12:50 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 04/26/21 04/20/21 08:28 04/20/21 12:03 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 05/10/21 13:12 EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 20:25 EPA 8270E EPA 3510C—MS 04/19/21 05/27/21 04/17/21 08:58 04/23/21 15:12 Client ID: 6301-MW19 Lab ID: CE04871-11 Sampled: 04/12/21 11:00 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/10/21 04/15/21 13:23 04/16/21 04:53 EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:23 EPA 6020B EPA 3005A 10/09/21 04/16/21 10:33 04/20/21 10:54 EPA 7470A EPA 7470A 05/10/21 04/19/21 09:05 04/20/21 14:52 EPA 8081E EPA 3510C 04/19/21 05/29/21 04/19/21 08:08 04/27/21 12:13 EPA 8082A EPA 3510C 04/12/22 05/29/21 04/19/21 08:12 04/27/21 12:13 EPA 8151A EPA 3510C 04/19/21 05/29/21 04/19/21 15:30 04/22/21 18:19 EPA 8260D EPA 503013_MS 04/26/21 04/22/21 12:28 04/23/21 02:37 EPA 9014 Same 04/26/21 04/15/21 07:26 04/19/21 18:27 SM 254OC-2011 NO PREP 04/19/21 04/19/21 13:41 04/20/21 13:53 SM 4500S2 D-2011 NO PREP 04/19/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-MW19 Lab ID: CE04871-11RE1 Sampled: 04/12/21 11:00 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 04/26/21 04/20/21 08:28 04/20/21 12:03 EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 20:51 EPA 8270E EPA 3510C—MS 04/19/21 05/27/21 04/17/21 08:58 04/23/21 15:41 Client ID: 6301-SW1 Lab ID: CE04871-12 Sampled: 04/12/21 15:55 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:26 EPA 7470A EPA 7470A 05/10/21 04/19/21 09:05 04/20/21 14:54 EPA 8260D EPA 503013_MS 04/26/21 04/22/21 12:28 04/23/21 03:05 Client ID: 6301-SW1 Lab ID: CE04871-12RE1 Sampled: 04/12/21 15:55 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 21:16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 98 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-SW2 Lab ID: CE04871-13 Sampled: 04/12/21 17:00 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 10/09/21 04/14/21 16:10 04/19/21 11:28 EPA 7470A EPA 7470A 05/10/21 04/19/21 09:05 04/20/21 14:56 EPA 8260D EPA 503013_MS 04/26/21 04/22/21 12:28 04/23/21 03:33 Client ID: 6301-SW2 Lab ID: CE04871-13RE1 Sampled: 04/12/21 17:00 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 21:41 Client ID: 6301-SW3 Lab ID: CE04871-14 Sampled: 04/12/21 16:25 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 10/09/21 04/15/21 10:31 04/19/21 11:34 EPA 7470A EPA 7470A 05/10/21 04/19/21 09:05 04/20/21 14:59 EPA 8260D EPA 5030B_MIS 04/26/21 04/22/21 12:28 04/23/21 04:01 Client ID: 6301-SW3 Lab ID: CE04871-14RE1 Sampled: 04/12/21 16:25 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 22:07 Client ID: 6301-SW4 Lab ID: CE04871-15 Sampled: 04/13/21 13:00 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 04/19/21 12:06 EPA 6020E EPA 3005A 10/10/21 04/16/21 10:33 04/20/21 10:58 EPA 7470A EPA 7470A 05/11/21 04/19/21 09:05 04/20/21 15:01 EPA 8260D EPA 5030B_MS 04/27/21 04/20/21 00:00 04/20/21 15:46 EPA 8260D EPA 503013_MS 04/27/21 04/22/21 11:34 04/23/21 01:32 Client ID: 6301-DUPLICATE Lab ID: CE04871-16 Sampled: 04/13/21 08:00 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 05/11/21 04/15/21 13:23 04/16/21 05:10 EPA 310.2 NO PREP 04/27/21 04/20/21 08:28 04/20/21 11:13 EPA 6010D EPA 3005A 10/10/21 04/15/21 10:31 04/19/21 12:08 EPA 6020E EPA 3005A 10/10/21 04/16/21 10:33 04/20/21 11:03 EPA 7470A EPA 7470A 05/11/21 04/19/21 09:05 04/20/21 15:04 EPA 8260D EPA 503013_MS 04/27/21 04/20/21 00:00 04/20/21 16:12 EPA 8260D EPA 503013_MS 04/27/21 04/22/21 11:34 04/23/21 01:59 SM 254OC-2011 NO PREP 04/20/21 04/19/21 13:41 04/20/21 13:53 SM 4500S2 D-2011 NO PREP 04/20/21 04/16/21 09:48 04/16/21 10:11 Client ID: 6301-TRIPBLANK Lab ID: CE04871-17 Sampled: 04/12/21 10:05 Received: 04/13/21 16:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 04/26/21 04/20/21 00:00 04/20/21 15:21 EPA 8260D EPA 5030B_MS 04/26/21 04/21/21 17:40 04/22/21 08:22 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 98 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW4 Lab ID: CE04871-01 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 103 1.10 10.0 ug/L EPA 6010D Chloride 30 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 0.53 J 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.9 0.15 1.0 ug/L EPA 8260D Iron - Total 19300 22.0 50.0 ug/L EPA 6010D Lead - Total 5.15 J 3.10 10.0 ug/L EPA 6010D Manganese - Total 327 1.50 10.0 ug/L EPA 6010D Mercury - Total 0.476 0.150 0.200 ug/L EPA 7470A Methane 0.323 0.00400 0.00500 mg/L RSK 175 Nitrate as N 0.22 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.22 0.041 0.10 mg/L EPA 353.2 Tetrahydrofuran 8.6 0.53 1.0 ug/L EPA 8260D Total Dissolved Solids 520 10 10 mg/L SM 2540C-2011 Total Organic Carbon 42 0.54 1.0 mg/L EPA 9060A Vinyl chloride 0.50 1 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW4 Lab ID: CE04871-01RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 5.3 0.80 2.0 ug/L EPA 8260D Carbon dioxide 217 D 10.4 12.5 mg/L RSK 175 Sulfate as SO4 110 D 5.8 10 mg/L EPA 300.0 Total Alkalinity as CaCO3 260 D 70 75 mg/L EPA 310.2 Client ID: 6301-MWS Lab ID: CE04871-02 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 32.7 1.10 10.0 ug/L EPA 6010D Carbon dioxide 28.1 2.07 2.50 mg/L RSK 175 Chloride 2.9 J 2.2 5.0 mg/L EPA 300.0 Manganese - Total 4.80 J 1.50 10.0 ug/L EPA 6010D Nitrate as N 1.4 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 1.4 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 2.9 J 2.9 5.0 mg/L EPA 300.0 Total Organic Carbon 1.0 0.54 1.0 mq/L EPA 9060A I Client ID: 6301-MW11SR Lab ID: CE04871-03 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 2.4 0.19 1.0 ug/L EPA 8260D Acetone 10 1 10 20 ug/L EPA 8260D Barium - Total 89.0 1.10 10.0 ug/L EPA 6010D Benzene 2.7 0.15 1.0 ug/L EPA 8260D Chloride 34 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.6 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.2 0.15 1.0 ug/L EPA 8260D Iron - Total 123000 22.0 50.0 ug/L EPA 6010D Lead - Total 11.5 3.10 10.0 ug/L EPA 6010D Manganese - Total 372 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 14 2.9 5.0 mg/L EPA 300.0 Sulfide 0.11 0.010 0.10 mg/L SM 450052 D-2011 Tetrahydrofuran 7.5 0.53 1.0 ug/L EPA 8260D Total Dissolved Solids 680 10 10 mg/L SM 2540C-2011 Total Organic Carbon 34 0.54 1.0 mg/L EPA 9060A Vinyl chloride 1.8 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW11SR Lab ID: CE04871-03RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 7.0 0.80 2.0 ug/L EPA 8260D Carbon dioxide 423 D 72.4 87.5 mg/L RSK 175 Methane 3.28 D 0.140 0.175 mg/L RSK 175 Total Alkalinity as CaCO3 730 D 70 75 mg/L EPA 310.2 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 98 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW11DR Lab ID: CE04871-04 Analvte Results Flag MDL Q Units Method Notes 1,2-Dichlorobenzene 0.51 J 0.19 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 3.1 0.19 1.0 ug/L EPA 8260D Barium - Total 55.0 1.10 10.0 ug/L EPA 6010D Benzene 2.1 0.15 1.0 ug/L EPA 8260D Cadmium - Total 0.526 J 0.360 1.00 ug/L EPA 6010D Chloride 22 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.3 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 3.0 0.15 1.0 ug/L EPA 8260D Cobalt - Total 1.63 J 1.40 10.0 ug/L EPA 6010D Iron - Total 94700 22.0 50.0 ug/L EPA 6010D Lead - Total 8.39 J 3.10 10.0 ug/L EPA 6010D Manganese - Total 178 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 12 2.9 5.0 mg/L EPA 300.0 Sulfide 0.049 J 0.010 0.10 mg/L SM 4500S2 D-2011 Total Dissolved Solids 270 10 10 mg/L SM 2540C-2011 Vinyl chloride 2.2 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW11DR Lab ID: CE04871-04RE1 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 5.3 0.80 2.0 ug/L EPA 8260D Total Alkalinity as CaCO3 260 D 70 75 mg/L EPA 310.2 Client ID: 6301-MW13SR Lab ID: CE04871-05 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 22.0 1.10 10.0 ug/L EPA 6010D Cadmium - Total 0.572 J 0.360 1.00 ug/L EPA 6010D Chloride 8.4 2.2 5.0 mg/L EPA 300.0 Copper - Total 1.97 J 1.60 10.0 ug/L EPA 6010D Iron - Total 78700 22.0 50.0 ug/L EPA 6010D Lead - Total 9.88 J 3.10 10.0 ug/L EPA 6010D Manganese - Total 683 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 18 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 34 14 15 mg/L EPA 310.2 Total Dissolved Solids 82 10 10 mg/L SM 2540C-2011 Vinyl chloride 0.86 J 0.32 1.0 ug/L EPA 8260D Zinc - Total 6.32 J 4.40 10.0 ug/L EPA 6010D Client ID: 6301-MW13SR Lab ID: CE04871-05RE1 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 3.8 0.80 2.0 ug/L EPA 8260D Client ID: 6301-MW13DR Lab ID: CE04871-06 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 48.3 1.10 10.0 ug/L EPA 6010D Chloride 6.8 2.2 5.0 mg/L EPA 300.0 Cobalt - Total 1.43 1 1.40 10.0 ug/L EPA 6010D Iron - Total 8000 22.0 50.0 ug/L EPA 6010D Manganese - Total 150 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 10 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 21 14 15 mg/L EPA 310.2 Total Dissolved Solids 30 10 10 mg/L SM 2540C-2011 Client ID: 6301-MW13DR Lab ID: CE04871-06RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 3.4 0.80 2.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 98 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW34 Lab ID: CE04871-07 Analvte Results Flag MDL Q Units Method Notes Acetone 120 10 20 ug/L EPA 8260D Barium - Total 18.2 1.10 10.0 ug/L EPA 6010D Chloride 15 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.5 0.17 1.0 ug/L EPA 8260D Copper - Total 3.37 J 1.60 10.0 ug/L EPA 6010D Iron - Total 45900 22.0 50.0 ug/L EPA 6010D Lead - Total 7.00 J 3.10 10.0 ug/L EPA 6010D Manganese - Total 67.6 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 19 2.9 5.0 mg/L EPA 300.0 Sulfide 0.37 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 42 14 15 mg/L EPA 310.2 Total Dissolved Solids 74 10 10 mg/L SM 2540C-2011 Vinyl chloride 0.85 J 0.32 1.0 uq/L EPA 8260D I Client ID: 6301-MW34 Lab ID: CE04871-07RE3 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 5.2 0.80 2.0 ug/L EPA 8260D Client ID: 6301-MW17S Lab ID: CE04871-08 Analvte Results Flag MDL Q Units Method Notes Barium - Total 136 1.10 10.0 ug/L EPA 6010D Chloride 8.2 2.2 5.0 mg/L EPA 300.0 Iron - Total 9390 22.0 50.0 ug/L EPA 6010D Lead - Total 3.98 J 3.10 10.0 ug/L EPA 6010D Manganese - Total 104 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 20 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 24 14 15 mg/L EPA 310.2 Total Dissolved Solids 240 10 10 mg/L SM 2540C-2011 Client ID: 6301-MW17S Lab ID: CE04871-08RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 0.90 J 0.80 2.0 ug/L EPA 8260D Client ID: 6301-MW17D Lab ID: CE04871-09 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 22.4 1.10 10.0 ug/L EPA 6010D Chloride 2.9 J 2.2 5.0 mg/L EPA 300.0 Iron - Total 1470 22.0 50.0 ug/L EPA 6010D Manganese - Total 37.3 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 33 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 160 14 15 mg/L EPA 310.2 Total Dissolved Solids 250 10 10 mg/L SM 2540C-2011 Client ID: 6301-MW17D Lab ID: CE04871-09RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 10 0.80 2.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 98 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW38 Lab ID: CE04871-10 Analvte Results Flag MDL Q Units Method Notes 1,2-Dichlorobenzene 0.55 J 0.19 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 2.0 0.19 1.0 ug/L EPA 8260D Acetone 11 1 10 20 ug/L EPA 8260D Barium - Total 89.5 1.10 10.0 ug/L EPA 6010D Benzene 1.2 0.15 1.0 ug/L EPA 8260D Cadmium - Total 0.811 J 0.360 1.00 ug/L EPA 6010D Chloride 51 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 0.91 J 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 2.9 0.15 1.0 ug/L EPA 8260D Iron - Total 131000 22.0 50.0 ug/L EPA 6010D Manganese - Total 241 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 45 2.9 5.0 mg/L EPA 300.0 Sulfide 0.030 J 0.010 0.10 mg/L SM 4500S2 D-2011 Total Dissolved Solids 470 10 10 mg/L SM 2540C-2011 Vinyl chloride 1.6 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW38 Lab ID: CE04871-10RE1 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 15 0.80 2.0 ug/L EPA 8260D Total Alkalinity as CaCO3 320 D 70 75 mg/L EPA 310.2 Client ID: 6301-MW19 Lab ID: CE04871-11 Analvte Results Flag MDL PQL Units Method Notes Acetone 22 10 20 ug/L EPA 8260D Barium - Total 103 1.10 10.0 ug/L EPA 6010D Chloride 36 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 1.5 0.15 1.0 ug/L EPA 8260D Iron - Total 60400 22.0 50.0 ug/L EPA 6010D Lead - Total 7.90 J 3.10 10.0 ug/L EPA 6010D Manganese - Total 229 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 23 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 350 10 10 mg/L SM 2540C-2011 Vinyl chloride 0.60 J 0.32 1.0 uq/L EPA 8260D Client ID: 6301-MW19 Lab ID: CE04871-11RE1 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 7.9 0.80 2.0 ug/L EPA 8260D Total Alkalinity as CaCO3 200 D 70 75 mg/L EPA 310.2 Client ID: 6301-SW3 Lab ID: CE04871-12 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 21.4 1.10 10.0 ug/L EPA 6010D Lead - Total 3.53 J 3.10 10.0 ug/L EPA 6010D Client ID: 6301-SW3 Lab ID: CE04871-12RE1 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.7 0.80 2.0 ug/L EPA 8260D Client ID: 6301-SW2 Lab ID: CE04871-13 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 14.0 1.10 10.0 ug/L EPA 6010D Client ID: 6301-SW3 Lab ID: CE04871-14 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 20.8 1.10 10.0 ug/L EPA 6010D Lead - Total 4.55 J 3.10 10.0 ug/L EPA 6010D Client ID: 6301-SW3 Lab ID: CE04871-14RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.6 0.80 2.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 98 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-SW4 Lab ID: CE04871-15 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1.1 J 0.80 2.0 ug/L EPA 8260D Barium - Total 20.7 1.10 10.0 ug/L EPA 6010D Client ID: 6301-DUPLICATE Lab ID: CE04871-16 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 0.61 J 0.19 1.0 ug/L EPA 8260D Barium - Total 25.3 1.10 10.0 ug/L EPA 6010D Benzene 0.69 J 0.15 1.0 ug/L EPA 8260D Cadmium - Total 0.821 J 0.360 1.00 ug/L EPA 6010D Chloride 3.3 J 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 0.55 J 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 2.2 0.15 1.0 ug/L EPA 8260D Cobalt - Total 1.79 J 1.40 10.0 ug/L EPA 6010D Copper - Total 4.25 J 1.60 10.0 ug/L EPA 6010D Iron - Total 107000 22.0 50.0 ug/L EPA 6010D Lead - Total 11.9 3.10 10.0 ug/L EPA 6010D Manganese - Total 87.3 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 6.8 2.9 5.0 mg/L EPA 300.0 Sulfide 0.010 1 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 45 14 15 mg/L EPA 310.2 Total Dissolved Solids 12 10 10 mg/L SM 2540C-2011 Vinyl chloride 0.74 J 0.32 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CE04871-01 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 12:25 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22033 EPA 8260D 04/23/21 17:40 ref 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22033 EPA 8260D 04/23/21 17:40 ref 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 ID22033 EPA 8260D 04/23/21 17:40 ref Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22033 EPA 8260D 04/23/21 17:40 ref Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 ID22033 EPA 8260D 04/23/21 17:40 ref Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22033 EPA 8260D 04/23/21 17:40 ref Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Chlorobenzene [308-90-7]A 0.53 J ug/L 1 0.17 1.0 1D22033 EPA 8260D 04/23/21 17:40 ref Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref cis-1,2-Dichloroethene [156-59-2]A 1.9 ug/L 1 0.15 1.0 1D22033 EPA 8260D 04/23/21 17:40 ref cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 ID22033 EPA 8260D 04/23/21 17:40 ref Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Tetrahydrofuran [109-99-9]A 8.6 ug/L 1 0.53 1.0 1D22033 EPA 8260D 04/23/21 17:40 ref Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 ID22033 EPA 8260D 04/23/21 17:40 ref Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22033 EPA 8260D 04/23/21 17:40 ref Vinyl chloride [75-01-4]A 0.50 J ug/L 1 0.32 1.0 1D22033 EPA 8260D 04/23/21 17:40 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CE04871-01 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 12:25 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22033 EPA 8260D 04/23/21 17:40 ref Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 47 1 50.0 94 % 53-136 ID22033 EPA 6260D 04123121 17:40 ref Dlbromofluoromethane 45 1 50.0 89 % 67-129 1D22033 EPA 6260D 04123121 17:40 ref Toluene-& 48 1 50.0 96 % 59-134 1D22033 EPA 6260D 04123121 17:40 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.476 ug/L 1 0.150 0.200 1D19008 EPA 7470A 04/20/21 12:37 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D15017 EPA 6020B 04/20/21 08:58 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Barium [7440-39-3]^ 103 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 10:18 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 10:18 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Cobalt [7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Iron [7439-89-6]^ 19300 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Lead [7439-92-1]^ 5.15 J ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Manganese [7439-96-5]^ 327 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D15017 EPA 6020B 04/20/21 08:58 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D15017 EPA 6020B 04/20/21 08:58 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 10:18 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 30 mg/L 1 2.2 5.0 1D16017 EPA 300.0 04/16/21 20:02 UI Nitrate as N [14797-55-8] 0.22 mg/L 1 0.041 0.10 [CALC] EPA 353.2 04/21/21 14:24 JAH Nitrate/Nitrite as N^ 0.22 mg/L 1 0.041 0.10 1D21015 EPA 353.2 04/21/21 14:24 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1D14029 EPA 353.2 04/14/21 15:05 JAH Sulfate as SO4 [14808-79-B]^ 110 D mg/L 2 5.8 10 1D20027 EPA 300.0 04/20/21 18:22 ZGW Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 260 D mg/L 5 70 75 1D20009 EPA 310.2 04/20/21 12:01 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CE04871-01 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 12:25 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 5.3 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 16:37 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 4.9 1 5.00 97 % 75-125 ID20044 EPA 6260D 04120121 16:37 KKW Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 217 D mg/L 5 10.4 12.5 1D16017 RSK 175 04/16/21 14:54 JMW Ethane [74-84-0] 0.00510 u mg/L 1 0.00510 0.00600 1D15045 RSK 175 04/15/21 21:05 JMW Ethene [74-85-1] 0.00510 u mg/L 1 0.00510 0.00600 1D15045 RSK 175 04/15/21 21:05 JMW Methane [74-82-8] 0.323 mg/L 1 0.00400 0.00500 1D15045 RSK 175 04/15/21 21:05 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Dissolved Solids 520 mg/L 1 10 10 1D19050 SM 254OC-2011 04/22/21 08:42 AAL Total Organic Carbon^ 42 mg/L 1 0.54 1.0 1D20004 EPA 9060A 04/20/21 16:55 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CE04871-02 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 13:15 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22033 EPA 8260D 04/23/21 18:07 ref 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22033 EPA 8260D 04/23/21 18:07 ref 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22033 EPA 8260D 04/23/21 18:07 ref Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22033 EPA 8260D 04/23/21 18:07 ref Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22033 EPA 8260D 04/23/21 18:07 ref Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22033 EPA 8260D 04/23/21 18:07 ref Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22033 EPA 8260D 04/23/21 18:07 ref Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22033 EPA 8260D 04/23/21 18:07 ref Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22033 EPA 8260D 04/23/21 18:07 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CE04871-02 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 13:15 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1D22033 EPA 8260D 04/23/21 18:07 ref Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22033 EPA 8260D 04/23/21 18:07 ref Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 47 1 50.0 93 % 53-136 ID22033 EPA 6260D 04123121 18:07 ref Dibromofluoromethane 45 1 50.0 90 % 67-129 1D22033 EPA 6260D 04123121 18:07 ref Toluene-d8 49 1 50.0 97 % 59-134 1D22033 EPA 8260D 04123121 18:07 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 ID19008 EPA 7470A 04/20/21 12:39 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 u ug/L 2 0.740 2.00 1D15017 EPA 6020B 04/20/21 09:03 RLF Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Barium [7440-39-3]^ 32.7 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Beryllium [7440-41-7]^ 0.160 u ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 10:57 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 10:57 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Cobalt [7440-48-4]^ 1.40 u ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Copper[7440-50-8]^ 1.60 u ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Iron [7439-89-6]^ 22.0 u ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Manganese [7439-96-5]^ 4.80 J ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Nickel[7440-02-0]^ 2.20 u ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Selenium [7782-49-2]^ 1.82 u ug/L 2 1.82 2.00 1D15017 EPA 6020B 04/20/21 09:03 RLF Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Thallium [7440-28-0]^ 0.220 u ug/L 2 0.220 2.00 1D15017 EPA 6020B 04/20/21 09:03 RLF Vanadium [7440-62-2]^ 1.40 u ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Zinc[7440-66-6]^ 4.40 u ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 10:57 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 2.9 J mg/L 1 2.2 5.0 1D16017 EPA 300.0 04/16/21 20:19 UI Nitrate as N [14797-55-8] 1.4 mg/L 1 0.041 0.10 [CALC] EPA 353.2 04/21/21 14:26 JAH Nitrate/Nitrite as N^ 1.4 mg/L 1 0.041 0.10 1D21015 EPA 353.2 04/21/21 14:26 JAH Nitrite as N [14797-65-0]^ 0.017 u mg/L 1 0.017 0.10 1D14029 EPA 353.2 04/14/21 15:06 JAH Sulfate as SO4 [14808-79-B]^ 2.9 J mg/L 1 2.9 5.0 1D16017 EPA 300.0 04/16/21 20:19 LJI Sulfide [18496-25-8]^ 0.010 u mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 u mg/L 1 14 15 1D20009 EPA 310.2 04/20/21 11:05 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CE04871-02 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 13:15 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 17:02 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.1 1 5.00 103 % 75-125 ID20044 EPA 6260D 04120121 17:02 KKW Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 28.1 mg/L 1 2.07 2.50 1D15045 RSK 175 04/15/21 21:21 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1D15045 RSK 175 04/15/21 21:21 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1D15045 RSK 175 04/15/21 21:21 JMW Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 ID15045 RSK 175 04/15/21 21:21 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Dissolved Solids 10 U mg/L 1 10 10 ID19049 SM 254OC-2011 04/22/21 08:40 AAL Total Organic Carbon^ 1.0 mg/L 1 0.54 1.0 1D20004 EPA 9060A 04/20/21 17:18 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CE04871-03 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 14:05 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref 1,4-Dichlorobenzene [306-46-7]^ 2.4 ug/L 1 0.19 1.0 1D22033 EPA 8260D 04/23/21 18:35 ref 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 ID22033 EPA 8260D 04/23/21 18:35 ref 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 ID22033 EPA 8260D 04/23/21 18:35 ref 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 ID22033 EPA 8260D 04/23/21 18:35 ref Acetone [67-64-1]A 10 J ug/L 1 10 20 1D22033 EPA 8260D 04/23/21 18:35 ref Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22033 EPA 8260D 04/23/21 18:35 ref Benzene [71-43-2]A 2.7 ug/L 1 0.15 1.0 1D22033 EPA 8260D 04/23/21 18:35 ref Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 ID22033 EPA 8260D 04/23/21 18:35 ref Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Chlorobenzene [308-90-7]A 1.6 ug/L 1 0.17 1.0 1D22033 EPA 8260D 04/23/21 18:35 ref Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref cis-1,2-Dichloroethene [156-59-2]A 1.2 ug/L 1 0.15 1.0 1D22033 EPA 8260D 04/23/21 18:35 ref cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22033 EPA 8260D 04/23/21 18:35 ref Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Tetrahydrofuran [109-99-9]A 7.5 ug/L 1 0.53 1.0 1D22033 EPA 8260D 04/23/21 18:35 ref Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22033 EPA 8260D 04/23/21 18:35 ref Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 ID22033 EPA 8260D 04/23/21 18:35 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CE04871-03 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 14:05 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 1.8 ug/L 1 0.32 1.0 1D22033 EPA 8260D 04/23/21 18:35 ref Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22033 EPA 8260D 04/23/21 18:35 ref Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 47 1 50.0 94 % 53-136 ID22033 EPA 6260D 04123121 18:35 ref Dibromofluoromethane 44 1 50.0 89 % 67-129 1D22033 EPA 6260D 04123121 18:35 ref Toluene-d8 49 1 50.0 98 % 59-134 1D22033 EPA 8260D 04123121 18:35 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 ID19008 EPA 7470A 04/20/21 12:44 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D15017 EPA 6020B 04/20/21 09:07 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Barium [7440-39-3]^ 89.0 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:00 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:00 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Cobalt [7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Iron [7439-89-6]^ 123000 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Lead [7439-92-1]^ 11.5 ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Manganese [7439-96-5]^ 372 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D15017 EPA 6020B 04/20/21 09:07 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D15017 EPA 6020B 04/20/21 09:07 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:00 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 34 mg/L 1 2.2 5.0 1D16017 EPA 300.0 04/16/21 20:37 UI Nitrate as N [14797-55-8] 0.041 U mg/L 1 0.041 0.10 [CALC] EPA 353.2 04/21/21 14:27 JAH Nitrate/Nitrite as N^ 0.041 U mg/L 1 0.041 0.10 1D21015 EPA 353.2 04/21/21 14:27 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1D14029 EPA 353.2 04/14/21 15:06 JAH Sulfate as SO4 [14808-79-8]^ 14 mg/L 1 2.9 5.0 1D16017 EPA 300.0 04/16/21 20:37 UI Sulfide [18496-25-8]^ 0.11 mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 730 D mg/L 5 70 75 1D20009 EPA 310.2 04/20/21 12:01 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CE04871-03 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 14:05 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 7.0 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 17:28 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.0 1 5.00 99 % 75-125 ID20044 EPA 6260D 04120121 17:28 KKW Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 423 D mg/L 35 72.4 87.5 1D16017 RSK 175 04/16/21 15:10 JMW Ethane [74-84-0] 0.00510 u mg/L 1 0.00510 0.00600 1D15045 RSK 175 04/15/21 21:37 JMW Ethene [74-85-1] 0.00510 u mg/L 1 0.00510 0.00600 1D15045 RSK 175 04/15/21 21:37 JMW Methane [74-82-8] 3.28 D mg/L 35 0.140 0.175 1D16017 RSK 175 04/16/21 15:10 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Dissolved Solids 680 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL Total Organic Carbon^ 34 mg/L 1 0.54 1.0 1D20004 EPA 9060A 04/20/21 17:36 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CE04871-04 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 15:10 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.51 J ug/L 1 0.19 1.0 1D22018 EPA 8260D 04/22/21 23:23 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 1,4-Dichlorobenzene [306-46-7]^ 3.1 ug/L 1 0.19 1.0 1D22018 EPA 8260D 04/22/21 23:23 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/22/21 23:23 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 ID22018 EPA 8260D 04/22/21 23:23 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/22/21 23:23 RKY Benzene [71-43-2]A 2.1 ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/22/21 23:23 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Chlorobenzene [108-90-7]^ 1.3 ug/L 1 0.17 1.0 1D22018 EPA 8260D 04/22/21 23:23 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY cis-1,2-Dichloroethene [156-59-2]^ 3.0 ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/22/21 23:23 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/22/21 23:23 RKY QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/22/21 23:23 RKY Vinyl chloride [75-01-4]^ 2.2 ug/L 1 0.32 1.0 1D22018 EPA 8260D 04/22/21 23:23 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CE04871-04 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 15:10 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/22/21 23:23 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 ID22018 EPA 6260D 04122121 23:23 RKY Dlbromofluoromethane 53 1 50.0 107 % 67-129 1D22018 EPA 6260D 04122121 23:23 RKY Toluene-c48 57 1 50.0 113 % 59-134 1D22018 EPA 6260D 04122121 23:23 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19008 EPA 7470A 04/20/21 12:46 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D15017 EPA 6020B 04/20/21 09:11 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Barium [7440-39-3]^ 55.0 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:02 JDH Cadmium [7440-43-9]^ 0.526 J ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:02 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Cobalt[7440-48-4]^ 1.63 J ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Iron [7439-89-6]^ 94700 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Lead [7439-92-1]^ 8.39 J ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Manganese [7439-96-5]^ 178 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D15017 EPA 6020B 04/20/21 09:11 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D15017 EPA 6020B 04/20/21 09:11 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:02 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes Chloride [16887-00-6]^ 22 mg/L 1 2.2 5.0 1D16017 EPA 300.0 04/16/21 20:55 UI Sulfate as SO4 [14808-79-B]^ 12 mg/L 1 2.9 5.0 1D16017 EPA 300.0 04/16/21 20:55 UI Sulfide [18496-25-8]^ 0.049 J mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 260 D mg/L 5 70 75 1D20009 EPA 310.2 04/20/21 12:02 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CE04871-04 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 15:10 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 5.3 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 17:53 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.0 1 5.00 101 % 75-125 ID20044 EPA 6260D 04120121 17:53 KKW Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 270 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CE04871-05 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 14:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/22/21 23:51 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22018 EPA 8260D 04/22/21 23:51 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/22/21 23:51 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY cis-1,2-Dichloroethene [156-59-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Tetrahydrofuran [109-99-9]A 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/22/21 23:51 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/22/21 23:51 RKY Vinyl chloride [75-01-4]A 0.86 J ug/L 1 0.32 1.0 1D22018 EPA 8260D 04/22/21 23:51 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CE04871-05 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 14:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/22/21 23:51 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 ID22018 EPA 6260D 04122121 23:51 RKY Dlbromofluoromethane 51 1 50.0 102 % 67-129 1D22018 EPA 6260D 04122121 23:51 RKY Toluene-c48 59 1 50.0 118 % 59-134 1D22018 EPA 6260D 04122121 23:51 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19008 EPA 7470A 04/20/21 12:49 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D15017 EPA 6020B 04/20/21 09:31 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Barium [7440-39-3]^ 22.0 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:04 JDH Cadmium [7440-43-9]^ 0.572 J ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:04 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Cobalt [7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Copper[7440-50-8]^ 1.97 J ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Iron [7439-89-6]^ 78700 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Lead [7439-92-1]^ 9.88 J ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Manganese [7439-96-5]^ 683 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D15017 EPA 6020B 04/20/21 09:31 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D15017 EPA 6020B 04/20/21 09:31 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Zinc[7440-66-6]^ 6.32 J ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:04 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 8.4 mg/L 1 2.2 5.0 1D16017 EPA 300.0 04/16/21 21:12 UI Sulfate as SO4 [14808-79-B]^ 18 mg/L 1 2.9 5.0 1D16017 EPA 300.0 04/16/21 21:12 UI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 34 mg/L 1 14 15 1D20009 EPA 310.2 04/20/21 11:08 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CE04871-05 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 14:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 3.8 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 18:18 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 4.9 1 5.00 99 % 75-125 ID20044 EPA 6260D 04120121 18:18 KKW Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 82 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CE04871-06 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 15:20 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 00:18 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22018 EPA 8260D 04/23/21 00:18 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 00:18 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/23/21 00:18 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 ID22018 EPA 8260D 04/23/21 00:18 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CE04871-06 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 15:20 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 00:18 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 56 1 50.0 113 % 53-136 ID22018 EPA 6260D 04123121 00:16 RKY Dlbromofluoromethane 52 1 50.0 105 % 67-129 1D22018 EPA 6260D 04123121 00:16 RKY Toluene-c48 56 1 50.0 111 % 59-134 1D22018 EPA 6260D 04123121 00:18 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MOIL P L Batch Method Analyzed gy Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19008 EPA 7470A 04/20/21 13:07 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed By Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D15017 EPA 6020B 04/20/21 09:36 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Barium [7440-39-3]^ 48.3 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:07 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:07 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Cobalt[7440-48-4]^ 1.43 J ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Iron [7439-89-6]^ 8000 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Manganese [7439-96-S]^ ISO ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D15017 EPA 6020B 04/20/21 09:36 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D15017 EPA 6020B 04/20/21 09:36 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:07 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed gy Notes Chloride [16887-00-6]^ 6.8 mg/L 1 2.2 5.0 1D16017 EPA 300.0 04/16/21 21:30 LJI Sulfate as SO4 [14808-79-B]^ 30 mg/L 1 2.9 5.0 1D16017 EPA 300.0 04/16/21 21:30 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 21 mg/L 1 14 15 1D20009 EPA 310.2 04/20/21 11:09 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CE04871-06 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 15:20 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 3.4 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 18:44 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 104 % 75-125 ID20044 EPA 6260D 04120121 18:44 KKW Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 30 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 30 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CE04871-07 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 17:20 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 00:46 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Acetone [67-64-1]A 120 ug/L 1 10 20 1D22018 EPA 8260D 04/23/21 00:46 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 00:46 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Chlorobenzene [108-90-7]A 1.5 ug/L 1 0.17 1.0 1D22018 EPA 8260D 04/23/21 00:46 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY cis-1,2-Dichloroethene [156-59-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Naphthalene [91-20-3]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Tetrahydrofuran [109-99-9]A 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/23/21 00:46 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/23/21 00:46 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CE04871-07 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 17:20 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.85 J ug/L 1 0.32 1.0 1D22018 EPA 8260D 04/23/21 00:46 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 00:46 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 57 1 50.0 113 % 53-136 ID22018 EPA 8260D 04123121 00:46 RKY Dibromofluoromethane 55 1 50.0 109 % 67-129 1D22018 EPA 6260D 04123121 00:46 RKY Toluene-d8 59 1 50.0 117 % 59-134 1D22018 EPA 6260D 04123121 00:46 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 ID19009 EPA 7470A 04/20/21 14:09 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D15017 EPA 6020B 04/20/21 09:40 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Barium [7440-39-3]^ 18.2 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:09 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:09 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Cobalt [7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Copper[7440-50-8]^ 3.37 J ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Iron [7439-89-6]^ 45900 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Lead [7439-92-1]^ 7.00 J ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Manganese [7439-96-5]^ 67.6 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D15017 EPA 6020B 04/20/21 09:40 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D15017 EPA 6020B 04/20/21 09:40 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:09 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 15 mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 03:07 LJI Sulfate as SO4 [14808-79-B]^ 19 mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 03:07 LJI Sulfide [18496-25-8]^ 0.37 mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 42 mg/L 1 14 15 1D20009 EPA 310.2 04/20/21 11:09 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 32 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CE04871-07 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 17:20 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 5.2 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 19:09 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.4 1 5.00 108 % 75-125 ID20044 EPA 6260D 04120121 19:09 KKW Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 74 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 33 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CE04871-08 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:45 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 01:14 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22018 EPA 8260D 04/23/21 01:14 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 01:14 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/23/21 01:14 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 ID22018 EPA 8260D 04/23/21 01:14 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CE04871-08 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:45 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 01:14 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 57 1 50.0 114 % 53-136 ID22018 EPA 6260D 04123121 01:14 RKY Dlbromofluoromethane 52 1 50.0 105 % 67-129 1D22018 EPA 6260D 04123121 01:14 RKY Toluene-c48 58 1 50.0 117 % 59-134 1D22018 EPA 6260D 04123121 01:14 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 14:45 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D15017 EPA 6020B 04/20/21 09:44 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Barium [7440-39-3]^ 136 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:16 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:16 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Cobalt [7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Iron [7439-89-6]^ 9390 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Lead [7439-92-1]^ 3.98 J ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Manganese [7439-96-S]^ 104 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D15017 EPA 6020B 04/20/21 09:44 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D15017 EPA 6020B 04/20/21 09:44 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:16 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes Chloride [16887-00-6]^ 8.2 mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 03:24 UI Sulfate as SO4 [14808-79-B]^ 20 mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 03:24 UI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 24 mg/L 1 14 15 1D20009 EPA 310.2 04/20/21 11:10 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CE04871-08 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:45 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 0.90 J ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 19:34 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 4.9 1 5.00 97 % 75-125 ID20044 EPA 6260D 04120121 19:34 KKW Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 240 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 36 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CE04871-09 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 10:05 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 01:42 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22018 EPA 8260D 04/23/21 01:42 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 01:42 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/23/21 01:42 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 ID22018 EPA 8260D 04/23/21 01:42 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 37 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CE04871-09 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 10:05 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 01:42 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 ID22018 EPA 6260D 04123121 01:42 RKY Dlbromofluoromethane 54 1 50.0 109 % 67-129 1D22018 EPA 6260D 04123121 01:42 RKY Toluene-c48 58 1 50.0 116 % 59-134 1D22018 EPA 6260D 04123121 01:42 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 14:47 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D16014 EPA 6020B 04/20/21 10:46 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Barium [7440-39-3]^ 22.4 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:19 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:19 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Cobalt [7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Iron [7439-89-6]^ 1470 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Manganese [7439-96-S]^ 37.3 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D16014 EPA 6020B 04/20/21 10:46 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D16014 EPA 6020B 04/20/21 10:46 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:19 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 2.9 J mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 03:42 LJI Sulfate as SO4 [14808-79-B]^ 33 mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 03:42 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 160 mg/L 1 14 15 1D20009 EPA 310.2 04/20/21 11:11 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 38 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CE04871-09 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 10:05 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 10 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 20:00 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 4.9 1 5.00 98 % 75-125 ID20044 EPA 6260D 04120121 20:00 KKW Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 250 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 39 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE04871-10 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 12:50 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,1-Dichloropropene [563-58-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,2,4-Trichlorobenzene [120-82-1]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.55 J ug/L 1 0.19 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,3-Dichlorobenzene [541-73-1]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,3-Dichloropropane [142-28-9]^ 0.16 U ug/L 1 0.16 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 1,4-Dichlorobenzene [106-46-7]^ 2.0 ug/L 1 0.19 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY 2,2-Dichloropropane [594-20-7]^ 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 3-Chloropropene[107-05-1]^ 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Acetone [67-64-1]^ 11 J ug/L 1 10 20 1D22018 EPA 8260D 04/23/21 02:10 RKY Acetonitrile [75-05-8]^ 5.0 U ug/L 1 5.0 10 ID22018 EPA 8260D 04/23/21 02:10 RKY Acrolein [107-02-8]^ 4.0 U ug/L 1 4.0 10 ID22018 EPA 8260D 04/23/21 02:10 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 02:10 RKY Benzene [71-43-2]^ 1.2 ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Chlorobenzene [108-90-7]^ 0.91 J ug/L 1 0.17 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Chloroprene [126-99-8]^ 0.64 U ug/L 1 0.64 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY QV-01 cis-1,2-Dichloroethene [156-59-2]^ 2.9 ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Dichlorodifluoromethane [75-71-8]^ 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Ethyl Methacrylate [97-63-2]^ 0.38 U ug/L 1 0.38 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY Hexachlorobutadiene [87-68-3]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 02:10 RKY QL-02 Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 02:10 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 40 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE04871-10 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 12:50 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed AX Notes Isobutyl alcohol [78-83-1]^ 11 U ug/L 1 11 50 1D22018 EPA 8260D 04/23/21 02:10 RKY QL-02 Methacrylonitrile [126-98-7]^ 4.9 U ug/L 1 4.9 10 1D22018 EPA 8260D 04/23/21 02:10 RKY Methyl Methacrylate [80-62-6]^ 0.51 U ug/L 1 0.51 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Propionitrile [107-12-0]^ 5.0 U ug/L 1 5.0 10 1D22018 EPA 8260D 04/23/21 02:10 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Vinyl chloride [75-01-4]^ 1.6 ug/L 1 0.32 1.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 02:10 RKY Surrogates Results DF Spike LN % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 59 1 50.0 117 % 53-136 ID22018 EPA 6260D 04123121 02:10 RKY Dibromofluoromethane 52 1 50.0 103 % 67-129 1D22018 EPA 6260D 04123121 02:10 RKY Toluene-d8 57 1 50.0 114 % 59-134 ID22018 EPA 6260D 04123121 02:10 RKY Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,2,4,5-Tetrachlorobenzene [95-94-3]^ 3.4 U ug/L 1 3.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 1,3,5-Trinitrobenzene [99-35-4]^ 3.0 U ug/L 1 3.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM QV-01 1,3-Dinitrobenzene [99-65-0]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 1,4-Naphthoquinone [130-15-4]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 1,4-Phenylenediamine [106-50-3]^ 4.0 U ug/L 1 4.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 1-Naphthylamine [134-32-7]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,3,4,6-Tetrachlorophenol[58-90-2]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,4,5-Trichlorophenol[95-95-4]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,4,6-Trichlorophenol[88-06-2]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,4-Dichlorophenol[120-83-2]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,4-Di methyl phenol[105-67-9]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,4-Dinitrophenol[51-28-5]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,4-Dinitrotoluene [121-14-2]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,6-Dichlorophenol[87-65-0]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2,6-Dinitrotoluene [606-20-2]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2-Acetylaminofluorene [53-96-3]^ 3.1 U ug/L 1 3.1 10 1D17004 EPA 8270E 04/23/21 15:12 DFM QV-01 2-Chloronaphthalene [91-58-7]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2-Chlorophenol[95-57-8]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2-Methyl-4,6-dinitrophenol[534-52-1]^ 3.3 U ug/L 1 3.3 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2- Methyl naphthalene [91-57-6]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 41 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE04871-10 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 12:50 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 2-Methylphenol[95-48-7]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2-Naphthylamine [91-59-8]^ 3.0 U ug/L 1 3.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2-Nitroaniline [88-74-4]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 2-Nitrophenol[88-75-5]^ 1.1 U ug/L 1 1.1 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 3 & 4-Methylphenol[108-39-4/106-44-5]^ 2.1 U ug/L 1 2.1 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 3,3'-Dichlorobenzidine [91-94-1]^ 3.5 U ug/L 1 3.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM QV-01 3,3'-Dimethylbenzidine [119-93-7]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 3-Methylcholanthrene [56-49-5]^ 1.3 U ug/L 1 1.3 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 3-Nitroaniline [99-09-2]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 4-Aminobiphenyl[92-67-1]^ 3.5 u ug/L 1 3.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 4-Bromophenyl-phenylether[101-55-3]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 4-Chloro-3-methylphenol[59-50-7]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 4-Chloroaniline [106-47-8]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 4-Chlorophenyl-phenylether[7005-72-3]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 4-Nitroaniline [100-01-6]^ 3.2 U ug/L 1 3.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 4-Nitrophenol[100-02-7]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 5-Nitro-o-toluidine [99-55-8]^ 3.2 u ug/L 1 3.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 7,12-Di methyl benz(a)anth racene 1.4 U ug/L 1 1.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM [57-97-6]^ a,a-Dimethylphenethylamine [122-09-8]^ 3.5 U ug/L 1 3.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Acenaphthene [83-32-9]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Acenaphthylene[208-96-8]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Acetophenone[98-86-2]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Anthracene [120-12-7]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Benzo(a)anthracene [56-55-3]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Benzo(a)pyrene [50-32-8]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Benzo(b)fluoranthene [205-99-2]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Benzo(g,hJ)perylene [191-24-2]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM QV-01 Benzo(k)fluoranthene [207-08-9]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Benzylalcohol [100-51-6]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Bis(2-chloroethoxy)methane [111-91-1]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Bis(2-chloroethyl)ether[111-44-4]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Bis(2-chloroisopropyl)ether[108-60-1]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Bis(2-ethylhexyl)phthalate [117-81-7]^ 1.9 U ug/L 1 1.9 5.0 1D17004 EPA 8270E 04/23/21 15:12 DFM Butyl benzylphtha late [85-68-7]^ 3.8 U ug/L 1 3.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM QV-01 Chlorobenzilate [510-15-6]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Chrysene [218-01-9]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Diallate [2303-16-4]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Dibenzo(a,h)anthracene [53-70-3]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:12 DFM QV-01 Dibenzofuran [132-64-9]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Diethylphtha late [84-66-2]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Dimethoate [60-51-5]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Dimethylphtha late [131-11-3]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Di-n-butylphthalate [84-74-2]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Di-n-octylphthalate [117-84-0]^ 3.1 U ug/L 1 3.1 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Disulfoton [298-04-4]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Ethyl methanesulfonate [62-50-0]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 42 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE04871-10 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 12:50 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Famphur[52-85-7]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Fluoranthene [206-44-0]^ 3.1 U ug/L 1 3.1 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Fluorene [86-73-7]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Hexachlorobenzene [118-74-1]1 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Hexachlorobutadiene [87-68-3]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Hexachlorocyclopentadiene [77-47-4]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Hexachloroethane [67-72-1]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Hexachloropropene [1888-71-7]^ 6.8 U ug/L 1 6.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM QV-01 Indeno(1,2,3-cd)pyrene [193-39-5]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM QV-01 Isodrin [465-73-6]^ 1.5 U ug/L 1 1.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Isophorone [78-59-1]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Isosafrole [120-58-1]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Kepone[143-50-0]^ 7.2 U ug/L 1 7.2 20 1D17004 EPA 8270E 04/23/21 15:12 DFM Methapyrilene [91-80-5]^ 4.8 U ug/L 1 4.8 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Methyl Methanesulfonate [66-27-3]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Methyl parathion [298-00-0]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Nitrobenzene [98-95-3]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM N-Nitrosodiethylamine [55-18-5]^ 2.1 U ug/L 1 2.1 10 1D17004 EPA 8270E 04/23/21 15:12 DFM N-Nitrosodimethylamine [62-75-9]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:12 DFM N-Nitrosodi-n-butylamine [924-16-3]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:12 DFM N-Nitroso-di-n-propylamine [621-64-7]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:12 DFM N-nitrosodiphenylamine/Diphenylamine 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM [86-30-6/122-39-4]^ N-Nitrosomethylethylamine [10595-95-6]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:12 DFM N-Nitrosopiperidine [100-75-4]^ 2.1 U ug/L 1 2.1 10 1D17004 EPA 8270E 04/23/21 15:12 DFM N-Nitrosopyrrolidine [930-55-2]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:12 DFM 0,0,0-Triethylphosphorothioate 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM [126-68-1]^ o-Toluidine [95-53-4]^ 1.6 U ug/L 1 1.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Parathion [56-38-2]^ 1.7 U ug/L 1 1.7 10 1D17004 EPA 8270E 04/23/21 15:12 DFM p-Dimethylaminoazobenzene [60-11-7]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Pentachlorobenzene [608-93-5]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Pentachloronitrobenzene [82-68-8]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Phenacetin [62-44-2]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Phenanthrene [85-01-8]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Phenol[108-95-2]^ 1.7 U ug/L 1 1.7 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Phorate [298-02-2]^ 2.1 U ug/L 1 2.1 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Pronamide[23950-58-5]^ 1.7 U ug/L 1 1.7 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Pyrene [129-00-0]^ 3.5 U ug/L 1 3.5 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Safrole [94-59-7]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Thionazin [297-97-2]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:12 DFM Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 2,4,6-Tribromophenol 89 1 100 89 % 10-179 1D17004 EPA 8270E 04123121 15:12 DFM 2-Fluorobiphenyl 40 1 50.0 79 % 10-149 1D17004 EPA 8270E 04123121 15:12 DFM 2-Fluorophenol 43 1 100 43 % 10-110 1D17004 EPA 8270E 04123121 15:12 DFM Nitrobenzene-d5 37 1 50.0 74 % 10-149 1D17004 EPA 8270E 04123121 15:12 DFM Phenol-d5 34 1 100 34 % 10-88 1D17004 EPA 8270E 04123121 15:12 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 43 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE04871-10 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 12:50 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Terphenyl-d14 36 1 50.0 72 % 10-166 ID17004 EPA 8270E 04123121 15:12 DFM Organochlorine Pesticides by GC ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed gy Notes 4,4'-DDD [72-54-8]^ 0.044 U ug/L 1 0.044 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK 4,4'-DDE[72-55-9]^ 0.048 U ug/L 1 0.048 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK 4,4'-DDT [50-29-3]^ 0.049 U ug/L 1 0.049 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Aldrin [309-00-2]^ 0.041 U ug/L 1 0.041 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK alpha-BHC [319-84-6]^ 0.036 U ug/L 1 0.036 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK beta-BHC [319-85-7]^ 0.041 U ug/L 1 0.041 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Chlordane (tech) [12789-03-6]^ 0.37 U ug/L 1 0.37 0.50 1D19004 EPA 8081B 04/27/21 11:56 LSK Chlordane -alpha [5103-71-9]^ 0.048 U ug/L 1 0.048 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Chlordane -gamma [5103-74-2]^ 0.042 U ug/L 1 0.042 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK delta-BHC [319-86-8]^ 0.048 U ug/L 1 0.048 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Dieldrin [60-57-1]^ 0.045 U ug/L 1 0.045 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Endosulfan I[959-98-8]^ 0.045 U ug/L 1 0.045 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Endosulfan II[33213-65-9]^ 0.038 U ug/L 1 0.038 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Endosulfan sulfate [1031-07-8]^ 0.032 U ug/L 1 0.032 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Endrin [72-20-8]^ 0.041 U ug/L 1 0.041 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Endrin aldehyde [7421-93-4]^ 0.049 U ug/L 1 0.049 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK gamma-BHC [58-89-9]^ 0.034 U ug/L 1 0.034 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Heptachlor[76-44-8]^ 0.047 U ug/L 1 0.047 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Heptachlor epoxide [1024-57-3]^ 0.037 U ug/L 1 0.037 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Methoxychlor[72-43-5]^ 0.048 U ug/L 1 0.048 0.050 1D19004 EPA 8081B 04/27/21 11:56 LSK Toxaphene[8001-35-2]^ 0.28 U ug/L 1 0.28 1.0 1D19004 EPA 8081B 04/27/21 11:56 LSK Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes 2,4,5,6-TCMX 0.67 1 1.00 67 % 10-139 1D19004 EPA 8081E 0412712111:56 LSK Decachlorobiphenyl 0.80 1 1.00 80 % 10-122 1D19004 EPA 8081E 0412712111:56 LSK Polychlorinated Biphenyls by GC ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes PCB-1016/1242 [12674-11-2/53469-21-9]^ 0.48 U ug/L 1 0.48 0.50 1D19005 EPA 8082A 04/27/21 11:56 LSK PCB-1221[11104-28-2]^ 0.43 U ug/L 1 0.43 0.50 1D19005 EPA 8082A 04/27/21 11:56 LSK PCB-1232[11141-16-5]^ 0.50 U ug/L 1 0.50 0.50 1D19005 EPA 8082A 04/27/21 11:56 LSK PCB-1248[12672-29-6]^ 0.45 U ug/L 1 0.45 0.50 1D19005 EPA 8082A 04/27/21 11:56 LSK PCB-1254[11097-69-1]^ 0.43 U ug/L 1 0.43 0.50 1D19005 EPA 8082A 04/27/21 11:56 LSK PCB-1260[11096-82-5]^ 0.47 U ug/L 1 0.47 0.50 1D19005 EPA 8082A 04/27/21 11:56 LSK Surrogates 2,4,5,E-TCMX Decachlorobiphenyl Results DF Spike L v/ % Rec % Rec Limits Batch Method 0.75 1 1.00 75 % 10-126 1D19005 EPA 6062A 1.0 1 1.00 102 % 10-129 1D19005 EPA 6062A Ana/vzed By Notes 0412712111:56 L5K 0412712111:56 L5K FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 44 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE04871-10 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 12:50 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 14:50 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D16014 EPA 6020B 04/20/21 10:50 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Barium [7440-39-3]^ 89.5 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Beryllium [7440-41-7]1 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:21 JDH Cadmium [7440-43-9]^ 0.811 J ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:21 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Iron [7439-89-6]^ 131000 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 lE07007 EPA 6010D 05/10/21 13:12 JDH Manganese [7439-96-5]^ 241 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D16014 EPA 6020B 04/20/21 10:50 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D16014 EPA 6020B 04/20/21 10:50 RLF Tin [7440-31-5]^ 2.90 U ug/L 1 2.90 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Vanadium [7440-62-2]1 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:21 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 51 mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 04:00 UI Cyanide (total) [57-12-5]^ 0.0049 U mg/L 1 0.0049 0.010 1D15002 EPA 9014 04/19/21 18:19 JAH Sulfate as SO4 [14808-79-8]^ 45 mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 04:00 UI Sulfide [18496-25-8]^ 0.030 J mg/L 1 0.010 0.10 1D16007 >M 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 320 D mg/L 5 70 75 1D20009 EPA 310.2 04/20/21 12:03 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 15 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 20:25 KKW Surrogates Results DF Spike LN % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-c48 4.8 1 5.00 97 % 75-125 ID20044 EPA 6260D 04120121 20:25 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 45 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE04871-10 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 12:50 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Chlorinated Herbicides by GC A - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 2,4,5-T [93-76-5]^ 0.28 U ug/L 1 0.28 0.50 1D19043 EPA 8151A 04/22/21 17:53 FCV 2,4,5-TP (Silvex) [93-72-1]^ 0.44 U ug/L 1 0.44 0.50 1D19043 EPA 8151A 04/22/21 17:53 FCV 2,4-D [94-75-7]^ 0.27 U ug/L 1 0.27 0.50 1D19043 EPA 8151A 04/22/21 17:53 FCV Dinoseb [88-85-7]^ 0.32 U ug/L 1 0.32 0.50 1D19043 EPA 8151A 04/22/21 17:53 FCV Pentachlorophenol[87-86-5]^ 0.19 U ug/L 1 0.19 0.50 1D19043 EPA 8151A 04/22/21 17:53 FCV Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 2,4-DCAA I'S 1 2,00 90 % 37-134 1D19043 EPA 6151A 04122121 17:53 FCV Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 470 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 46 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE04871-11 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,1-Dichloropropene [563-58-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,2,4-Trichlorobenzene [120-82-1]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,3-Dichlorobenzene [541-73-1]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,3-Dichloropropane [142-28-9]^ 0.16 U ug/L 1 0.16 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 2,2-Dichloropropane [594-20-7]^ 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 3-Chloropropene[107-05-1]^ 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Acetone [67-64-1]^ 22 ug/L 1 10 20 1D22018 EPA 8260D 04/23/21 02:37 RKY Acetonitrile [75-05-8]^ 5.0 U ug/L 1 5.0 10 ID22018 EPA 8260D 04/23/21 02:37 RKY Acrolein [107-02-8]^ 4.0 U ug/L 1 4.0 10 ID22018 EPA 8260D 04/23/21 02:37 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 02:37 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Chloroprene [126-99-8]^ 0.64 U ug/L 1 0.64 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY QV-01 cis-1,2-Dichloroethene [156-59-2]^ 1.5 ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Dichlorodifluoromethane [75-71-8]^ 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Ethyl Methacrylate [97-63-2]^ 0.38 U ug/L 1 0.38 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY Hexachlorobutadiene [87-68-3]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 02:37 RKY QL-02 Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 02:37 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 47 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE04871-11 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed AX Notes Isobutyl alcohol [78-83-1]^ 11 U ug/L 1 11 50 1D22018 EPA 8260D 04/23/21 02:37 RKY QL-02 Methacrylonitrile [126-98-7]^ 4.9 U ug/L 1 4.9 10 1D22018 EPA 8260D 04/23/21 02:37 RKY Methyl Methacrylate [80-62-6]^ 0.51 U ug/L 1 0.51 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Propionitrile [107-12-0]^ 5.0 U ug/L 1 5.0 10 1D22018 EPA 8260D 04/23/21 02:37 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Vinyl chloride [75-01-4]^ 0.60 J ug/L 1 0.32 1.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 02:37 RKY Surrogates Results DF Spike LN % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 105 % 53-136 ID22018 EPA 6260D 04123121 02:37 RKY Dibromofluoromethane 52 1 50.0 104 % 67-129 1D22018 EPA 6260D 04123121 02:37 RKY Toluene-d8 58 1 50.0 115 % 59-134 ID22018 EPA 6260D 04123121 02:37 RKY Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,2,4,5-Tetrachlorobenzene [95-94-3]^ 3.4 U ug/L 1 3.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 1,3,5-Trinitrobenzene [99-35-4]^ 3.0 U ug/L 1 3.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM QV-01 1,3-Dinitrobenzene [99-65-0]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 1,4-Naphthoquinone [130-15-4]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 1,4-Phenylenediamine [106-50-3]^ 4.0 U ug/L 1 4.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 1-Naphthylamine [134-32-7]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,3,4,6-Tetrachlorophenol[58-90-2]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,4,5-Trichlorophenol[95-95-4]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,4,6-Trichlorophenol[88-06-2]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,4-Dichlorophenol [120-83-2]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,4-Di methyl phenol[105-67-9]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,4-Dinitrophenol [51-28-5]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,4-Dinitrotoluene [121-14-2]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,6-Dichlorophenol [87-65-0]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2,6-Dinitrotoluene [606-20-2]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2-Acetylaminofluorene [53-96-3]^ 3.1 U ug/L 1 3.1 10 1D17004 EPA 8270E 04/23/21 15:41 DFM QV-01 2-Chloronaphthalene [91-58-7]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2-Chlorophenol[95-57-8]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2-Methyl-4,6-dinitrophenol[534-52-1]^ 3.3 U ug/L 1 3.3 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2- Methyl naphthalene [91-57-6]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 48 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE04871-11 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 2-Methylphenol[95-48-7]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2-Naphthylamine [91-59-8]^ 3.0 U ug/L 1 3.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2-Nitroaniline [88-74-4]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 2-Nitrophenol[88-75-5]^ 1.1 U ug/L 1 1.1 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 3 & 4-Methylphenol[108-39-4/106-44-5]^ 2.1 U ug/L 1 2.1 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 3,3'-Dichlorobenzidine [91-94-1]^ 3.5 U ug/L 1 3.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM QV-01 3,3'-Dimethylbenzidine [119-93-7]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 3-Methylcholanthrene [56-49-5]^ 1.3 U ug/L 1 1.3 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 3-Nitroaniline [99-09-2]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 4-Aminobiphenyl[92-67-1]^ 3.5 u ug/L 1 3.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 4-Bromophenyl-phenylether[101-55-3]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 4-Chloro-3-methylphenol[59-50-7]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 4-Chloroaniline [106-47-8]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 4-Chlorophenyl-phenylether[7005-72-3]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 4-Nitroaniline [100-01-6]^ 3.2 U ug/L 1 3.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 4-Nitrophenol[100-02-7]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 5-Nitro-o-toluidine [99-55-8]^ 3.2 u ug/L 1 3.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 7,12-Di methyl benz(a)anth racene 1.4 U ug/L 1 1.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM [57-97-6]^ a,a-Dimethylphenethylamine [122-09-8]^ 3.5 U ug/L 1 3.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Acenaphthene[83-32-9]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Acenaphthylene[208-96-8]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Acetophenone[98-86-2]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Anthracene [120-12-7]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Benzo(a)anthracene [56-55-3]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Benzo(a)pyrene [50-32-8]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Benzo(b)fluoranthene [205-99-2]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Benzo(g,hJ)perylene [191-24-2]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM QV-01 Benzo(k)fluoranthene[207-08-9]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Benzylalcohol [100-51-6]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Bis(2-chloroethoxy)methane [111-91-1]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Bis(2-chloroethyl)ether[111-44-4]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Bis(2-chloroisopropyl)ether[108-60-1]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Bis(2-ethylhexyl)phthalate [117-81-7]^ 1.9 U ug/L 1 1.9 5.0 1D17004 EPA 8270E 04/23/21 15:41 DFM Butyl benzylphtha late [85-68-7]^ 3.8 U ug/L 1 3.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM QV-01 Chlorobenzilate [510-15-6]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Chrysene [218-01-9]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Diallate [2303-16-4]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Dibenzo(a,h)anthracene [53-70-3]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:41 DFM QV-01 Dibenzofuran [132-64-9]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Diethylphtha late [84-66-2]^ 2.4 U ug/L 1 2.4 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Dimethoate [60-51-5]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Dimethylphtha late [131-11-3]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Di-n-butylphthalate [84-74-2]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Di-n-octylphthalate [117-84-0]^ 3.1 U ug/L 1 3.1 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Disulfoton [298-04-4]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Ethyl methanesulfonate [62-50-0]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 49 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE04871-11 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Famphur[52-85-7]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Fluoranthene [206-44-0]^ 3.1 U ug/L 1 3.1 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Fluorene [86-73-7]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Hexachlorobenzene [118-74-1]1 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Hexachlorobutadiene [87-68-3]^ 2.8 U ug/L 1 2.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Hexachlorocyclopentadiene [77-47-4]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Hexachloroethane [67-72-1]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Hexachloropropene [1888-71-7]^ 6.8 U ug/L 1 6.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM QV-01 Indeno(1,2,3-cd)pyrene [193-39-5]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM QV-01 Isodrin [465-73-6]^ 1.5 U ug/L 1 1.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Isophorone [78-59-1]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Isosafrole [120-58-1]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Kepone[143-50-0]^ 7.2 U ug/L 1 7.2 20 1D17004 EPA 8270E 04/23/21 15:41 DFM Methapyrilene [91-80-5]^ 4.8 U ug/L 1 4.8 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Methyl Methanesulfonate [66-27-3]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Methyl parathion [298-00-0]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Nitrobenzene [98-95-3]^ 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM N-Nitrosodiethylamine [55-18-5]^ 2.1 U ug/L 1 2.1 10 1D17004 EPA 8270E 04/23/21 15:41 DFM N-Nitrosodimethylamine [62-75-9]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:41 DFM N-Nitrosodi-n-butylamine [924-16-3]^ 2.0 U ug/L 1 2.0 10 1D17004 EPA 8270E 04/23/21 15:41 DFM N-Nitroso-di-n-propylamine [621-64-7]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:41 DFM N-nitrosodiphenylamine/Diphenylamine 2.5 U ug/L 1 2.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM [86-30-6/122-39-4]^ N-Nitrosomethylethylamine [10595-95-6]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:41 DFM N-Nitrosopiperidine [100-75-4]^ 2.1 U ug/L 1 2.1 10 1D17004 EPA 8270E 04/23/21 15:41 DFM N-Nitrosopyrrolidine [930-55-2]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:41 DFM 0,0,0-Triethylphosphorothioate 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM [126-68-1]^ o-Toluidine [95-53-4]^ 1.6 U ug/L 1 1.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Parathion [56-38-2]^ 1.7 U ug/L 1 1.7 10 1D17004 EPA 8270E 04/23/21 15:41 DFM p-Dimethylaminoazobenzene [60-11-7]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Pentachlorobenzene [608-93-5]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Pentachloronitrobenzene [82-68-8]^ 1.9 U ug/L 1 1.9 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Phenacetin [62-44-2]^ 2.7 U ug/L 1 2.7 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Phenanthrene[85-01-8]^ 2.6 U ug/L 1 2.6 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Phenol[108-95-2]^ 1.7 U ug/L 1 1.7 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Phorate [298-02-2]^ 2.1 U ug/L 1 2.1 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Pronamide[23950-58-5]^ 1.7 U ug/L 1 1.7 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Pyrene [129-00-0]^ 3.5 U ug/L 1 3.5 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Safrole [94-59-7]^ 2.2 U ug/L 1 2.2 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Thionazin [297-97-2]^ 2.3 U ug/L 1 2.3 10 1D17004 EPA 8270E 04/23/21 15:41 DFM Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 2,4,6-Tribromophenol 77 1 100 77 % 10-179 1D17004 EPA 8270E 04123121 15:41 DFM 2-Fluorobiphenyl 33 1 50.0 66 % 10-149 1D17004 EPA 8270E 04123121 15:41 DFM 2-Fluorophenol 35 1 100 35 % 10-110 1D17004 EPA 8270E 04123121 15:41 DFM Nitrobenzene-d5 32 1 50.0 64 % 10-149 1D17004 EPA 8270E 04123121 15:41 DFM Phenol-d5 28 1 100 28 % 10-88 1D17004 EPA 8270E 04123121 15:41 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 50 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE04871-11 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Terphenyl-d14 32 1 50.0 64 % 10-166 ID17004 EPA 8270E 04123121 15:41 DFM Organochlorine Pesticides by GC ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed gy Notes 4,4'-DDD [72-54-8]^ 0.044 U ug/L 1 0.044 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK 4,4'-DDE [72-55-9]^ 0.048 U ug/L 1 0.048 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK 4,4'-DDT [50-29-3]^ 0.049 U ug/L 1 0.049 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Aldrin [309-00-2]^ 0.041 U ug/L 1 0.041 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK alpha-BHC [319-84-6]^ 0.036 U ug/L 1 0.036 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK beta-BHC [319-85-7]^ 0.041 U ug/L 1 0.041 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Chlordane (tech) [12789-03-6]^ 0.37 U ug/L 1 0.37 0.50 1D19004 EPA 8081B 04/27/21 12:13 LSK Chlordane -alpha [5103-71-9]^ 0.048 U ug/L 1 0.048 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Chlordane -gamma [5103-74-2]^ 0.042 U ug/L 1 0.042 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK delta-BHC [319-86-8]^ 0.048 U ug/L 1 0.048 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Dieldrin [60-57-1]^ 0.045 U ug/L 1 0.045 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Endosulfan I[959-98-8]^ 0.045 U ug/L 1 0.045 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Endosulfan II[33213-65-9]^ 0.038 U ug/L 1 0.038 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Endosulfan sulfate [1031-07-8]^ 0.032 U ug/L 1 0.032 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Endrin [72-20-8]^ 0.041 U ug/L 1 0.041 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Endrin aldehyde [7421-93-4]^ 0.049 U ug/L 1 0.049 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK gamma-BHC [58-89-9]^ 0.034 U ug/L 1 0.034 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Heptachlor[76-44-8]^ 0.047 U ug/L 1 0.047 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Heptachlor epoxide [1024-57-3]^ 0.037 U ug/L 1 0.037 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Methoxychlor[72-43-5]^ 0.048 U ug/L 1 0.048 0.050 1D19004 EPA 8081B 04/27/21 12:13 LSK Toxaphene[8001-35-2]^ 0.28 U ug/L 1 0.28 1.0 1D19004 EPA 8081B 04/27/21 12:13 LSK Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes 2,4,5,6-TCMX 0.61 1 1.00 61 % 10-139 1D19004 EPA 8081E 04127121 12:13 LSK Decachlorobiphenyl 0.74 1 1.00 74 % 10-122 1D19004 EPA 8081E 04127121 12:13 LSK Polychlorinated Biphenyls by GC ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes PCB-1016/1242 [12674-11-2/53469-21-9]^ 0.48 U ug/L 1 0.48 0.50 1D19005 EPA 8082A 04/27/21 12:13 LSK PCB-1221[11104-28-2]^ 0.43 U ug/L 1 0.43 0.50 1D19005 EPA 8082A 04/27/21 12:13 LSK PCB-1232[11141-16-5]^ 0.50 U ug/L 1 0.50 0.50 1D19005 EPA 8082A 04/27/21 12:13 LSK PCB-1248[12672-29-6]^ 0.45 U ug/L 1 0.45 0.50 1D19005 EPA 8082A 04/27/21 12:13 LSK PCB-1254[11097-69-1]^ 0.43 U ug/L 1 0.43 0.50 1D19005 EPA 8082A 04/27/21 12:13 LSK PCB-1260[11096-82-5]^ 0.47 U ug/L 1 0.47 0.50 1D19005 EPA 8082A 04/27/21 12:13 LSK Surrogates 2,4,5,E-TCMX Decachlorobiphenyl Results DF Spike L v/ % Rec % Rec Limits Batch Method 0.71 1 1.00 71 % 10-126 1D19005 EPA 6062A 0.93 1 1.00 93 % 10-129 1D19005 EPA 6062A Ana/vzed By Notes 04127121 12:13 LSK 04127121 12:13 LSK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 51 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE04871-11 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1D19009 EPA 7470A 04/20/21 14:52 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D16014 EPA 6020B 04/20/21 10:54 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Barium [7440-39-3]^ 103 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Beryllium [7440-41-7]1 0.160 U ug/L 1 0.160 1.00 1D14041 EPA 6010D 04/19/21 11:23 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:23 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Iron [7439-89-6]^ 60400 ug/L 1 22.0 50.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Lead [7439-92-1]^ 7.90 J ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Manganese [7439-96-S]^ 229 ug/L 1 1.50 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D16014 EPA 6020B 04/20/21 10:54 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D16014 EPA 6020B 04/20/21 10:54 RLF Tin [7440-31-5]^ 2.90 U ug/L 1 2.90 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Vanadium [7440-62-2]1 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D14041 EPA 6010D 04/19/21 11:23 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 36 mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 04:53 UI Cyanide (total) [57-12-5]^ 0.0049 U mg/L 1 0.0049 0.010 1D15002 EPA 9014 04/19/21 18:27 JAH Sulfate as SO4 [14808-79-8]^ 23 mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 04:53 UI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 200 D mg/L 5 70 75 1D20009 EPA 310.2 04/20/21 12:03 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 7.9 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 20:51 KKW Surrogates Results DF Spike LN % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-c48 5.0 1 5.00 99 % 75-125 ID20044 EPA 6260D 04120121 20:51 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 52 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE04871-11 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 11:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Chlorinated Herbicides by GC A - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 2,4,5-T [93-76-5]^ 0.28 U ug/L 1 0.28 0.50 1D19043 EPA 8151A 04/22/21 18:19 FCV 2,4,5-TP (Silvex) [93-72-1]^ 0.44 U ug/L 1 0.44 0.50 1D19043 EPA 8151A 04/22/21 18:19 FCV 2,4-D [94-75-7]^ 0.27 U ug/L 1 0.27 0.50 1D19043 EPA 8151A 04/22/21 18:19 FCV Dinoseb [88-85-7]^ 0.32 U ug/L 1 0.32 0.50 1D19043 EPA 8151A 04/22/21 18:19 FCV Pentachlorophenol[87-86-5]^ 0.19 U ug/L 1 0.19 0.50 1D19043 EPA 8151A 04/22/21 18:19 FCV Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 2,4-DCAA 1,4 1 2,00 68 % 37-134 1D19043 EPA 6151A 04/22/21 16:19 FCV Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 350 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 53 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW1 Lab Sample ID:CE04871-12 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 15:55 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 03:05 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22018 EPA 8260D 04/23/21 03:05 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 03:05 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/23/21 03:05 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/23/21 03:05 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 54 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SWI Lab Sample ID:CE04871-12 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 15:55 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1D22018 EPA 8260D 04/23/21 03:05 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 03:05 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 57 1 50.0 114 % 53-136 ID22018 EPA 8260D 04123121 03:05 RKY Dibromofluoromethane 57 1 50.0 114 % 67-129 1D22018 EPA 6260D 04123121 03:05 RKY Toluene-d8 59 1 50.0 118 % 59-134 1D22018 EPA 6260D 04123121 03:05 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 ID19009 EPA 7470A 04/20/21 14:54 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:26 JDH Barium [7440-39-3]^ 21.4 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:26 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:26 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:26 JDH Lead [7439-92-1]^ 3.53 J ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:26 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1D14041 EPA 6010D 04/19/21 11:26 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:26 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 2.7 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 21:16 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 4.9 1 5.00 99 % 75-125 1D20044 EPA 8260D 04120121 21:16 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 55 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW2 Lab Sample ID:CE04871-13 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 17:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 03:33 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22018 EPA 8260D 04/23/21 03:33 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 03:33 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/23/21 03:33 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/23/21 03:33 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 56 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW2 Lab Sample ID:CE04871-13 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 17:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1D22018 EPA 8260D 04/23/21 03:33 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 03:33 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 55 1 50.0 111 % 53-136 ID22018 EPA 8260D 04123121 03:33 RKY Dibromofluoromethane 53 1 50.0 107 % 67-129 1D22018 EPA 6260D 04123121 03:33 RKY Toluene-d8 58 1 50.0 116 % 59-134 1D22018 EPA 6260D 04123121 03:33 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 ID19009 EPA 7470A 04/20/21 14:56 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D14041 EPA 6010D 04/19/21 11:28 JDH Barium [7440-39-3]^ 14.0 ug/L 1 1.10 10.0 1D14041 EPA 6010D 04/19/21 11:28 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D14041 EPA 6010D 04/19/21 11:28 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D14041 EPA 6010D 04/19/21 11:28 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1D14041 EPA 6010D 04/19/21 11:28 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1D14041 EPA 6010D 04/19/21 11:28 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D14041 EPA 6010D 04/19/21 11:28 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 21:41 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.2 1 5.00 104 % 75-125 1D20044 EPA 8260D 04120121 21:41 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 57 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW3 Lab Sample ID:CE04871-14 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 16:25 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22018 EPA 8260D 04/23/21 04:01 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22018 EPA 8260D 04/23/21 04:01 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22018 EPA 8260D 04/23/21 04:01 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22018 EPA 8260D 04/23/21 04:01 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22018 EPA 8260D 04/23/21 04:01 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 58 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW3 Lab Sample ID:CE04871-14 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/12/21 16:25 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1D22018 EPA 8260D 04/23/21 04:01 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22018 EPA 8260D 04/23/21 04:01 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 55 1 50.0 109 % 53-136 ID22018 EPA 8260D 04123121 04:01 RKY Dibromofluoromethane 56 1 50.0 112 % 67-129 1D22018 EPA 6260D 04123121 04:01 RKY Toluene-d8 57 1 50.0 114 % 59-134 1D22018 EPA 6260D 04123121 04:01 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 ID19009 EPA 7470A 04/20/21 14:59 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D15015 EPA 6010D 04/19/21 11:34 JDH Barium [7440-39-3]^ 20.8 ug/L 1 1.10 10.0 1D15015 EPA 6010D 04/19/21 11:34 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1D15015 EPA 6010D 04/19/21 11:34 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 11:34 JDH Lead [7439-92-1]^ 4.55 J ug/L 1 3.10 10.0 1D15015 EPA 6010D 04/19/21 11:34 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1D15015 EPA 6010D 04/19/21 11:34 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D15015 EPA 6010D 04/19/21 11:34 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 2.6 ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 22:07 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 4.9 1 5.00 98 % 75-125 1D20044 EPA 8260D 04120121 22:07 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 59 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW4 Lab Sample ID:CE04871-15 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 13:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID22019 EPA 8260D 04/23/21 01:32 ref 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID22019 EPA 8260D 04/23/21 01:32 ref 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22019 EPA 8260D 04/23/21 01:32 ref Acetone [67-64-1]A 10 U ug/L 1 10 20 ID22019 EPA 8260D 04/23/21 01:32 ref Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22019 EPA 8260D 04/23/21 01:32 ref Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID22019 EPA 8260D 04/23/21 01:32 ref Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22019 EPA 8260D 04/23/21 01:32 ref Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22019 EPA 8260D 04/23/21 01:32 ref Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID22019 EPA 8260D 04/23/21 01:32 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 60 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW4 Lab Sample ID:CE04871-15 Received: 04/13/21 16:20 Matrix: Ground Water Sampled:04/13/21 13:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1D22019 EPA 8260D 04/23/21 01:32 ref Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22019 EPA 8260D 04/23/21 01:32 ref Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 47 1 50.0 94 % 53-136 ID22019 EPA 6260D 04123121 01:32 ref Dibromofluoromethane 45 1 50.0 89 % 67-129 1D22019 EPA 6260D 04123121 01:32 ref Toluene-d8 49 1 50.0 98 % 59-134 1D22019 EPA 8260D 04123121 01:32 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 ID19009 EPA 7470A 04/20/21 15:01 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 u ug/L 2 0.740 2.00 1D16014 EPA 6020B 04/20/21 10:58 RLF Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Barium [7440-39-3]^ 20.7 ug/L 1 1.10 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Beryllium [7440-41-7]^ 0.160 u ug/L 1 0.160 1.00 1D15015 EPA 6010D 04/19/21 12:06 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 1D15015 EPA 6010D 04/19/21 12:06 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Cobalt [7440-48-4]^ 1.40 u ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Copper[7440-50-8]^ 1.60 u ug/L 1 1.60 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Nickel[7440-02-0]^ 2.20 u ug/L 1 2.20 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Selenium [7782-49-2]^ 6.20 u ug/L 1 6.20 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Selenium [7782-49-2]^ 1.82 u ug/L 2 1.82 2.00 1D16014 EPA 6020B 04/20/21 10:58 RLF Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Thallium [7440-28-0]^ 0.220 u ug/L 2 0.220 2.00 1D16014 EPA 6020B 04/20/21 10:58 RLF Vanadium [7440-62-2]^ 1.40 u ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Zinc[7440-66-6]^ 4.40 u ug/L 1 4.40 10.0 1D15015 EPA 6010D 04/19/21 12:06 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl 1,4-Dioxane [123-91-1]^ Surrogates Toluene-d8 Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1.1 J ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 15:46 KKW Results DF Soike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes 4.9 1 5.00 98 % 75-125 1 D20044 EPA 8260D 04120121 15:46 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 61 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CE04871-16 Received: 04/13/21 16:20 Matrix: Ground Water Sampled: 04/13/2108:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref 1,4-Dichlorobenzene [306-46-7]^ 0.61 J ug/L 1 0.19 1.0 1D22019 EPA 8260D 04/23/21 01:59 ref 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 ID22019 EPA 8260D 04/23/21 01:59 ref 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 ID22019 EPA 8260D 04/23/21 01:59 ref 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID22019 EPA 8260D 04/23/21 01:59 ref Acetone [67-64-1]^ 10 U ug/L 1 10 20 ID22019 EPA 8260D 04/23/21 01:59 ref Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID22019 EPA 8260D 04/23/21 01:59 ref Benzene [71-43-2]A 0.69 J ug/L 1 0.15 1.0 1D22019 EPA 8260D 04/23/21 01:59 ref Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 ID22019 EPA 8260D 04/23/21 01:59 ref Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Chlorobenzene [308-90-7]A 0.55 J ug/L 1 0.17 1.0 1D22019 EPA 8260D 04/23/21 01:59 ref Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref cis-1,2-Dichloroethene [156-59-2]A 2.2 ug/L 1 0.15 1.0 1D22019 EPA 8260D 04/23/21 01:59 ref cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID22019 EPA 8260D 04/23/21 01:59 ref Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID22019 EPA 8260D 04/23/21 01:59 ref Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 ID22019 EPA 8260D 04/23/21 01:59 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 62 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CE04871-16 Received: 04/13/21 16:20 Matrix: Ground Water Sampled: 04/13/2108:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 0.74 J ug/L 1 0.32 1.0 1D22019 EPA 8260D 04/23/21 01:59 ref Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D22019 EPA 8260D 04/23/21 01:59 ref Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 46 1 50.0 93 % 53-136 ID22019 EPA 6260D 04123121 01:59 ref Dibromofluoromethane 45 1 50.0 90 % 67-129 1D22019 EPA 6260D 04123121 01:59 ref Toluene-d8 49 1 50.0 97 % 59-134 1D22019 EPA 8260D 04123121 01:59 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 ID19009 EPA 7470A 04/20/21 15:04 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1D16014 EPA 6020B 04/20/21 11:03 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Barium [7440-39-3]^ 25.3 ug/L 1 1.10 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1D15015 EPA 6010D 04/19/21 12:08 JDH Cadmium [7440-43-9]^ 0.821 J ug/L 1 0.360 1.00 1D15015 EPA 6010D 04/19/21 12:08 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Cobalt[7440-48-4]^ 1.79 J ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Copper[7440-50-8]^ 4.25 J ug/L 1 1.60 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Iron [7439-89-6]^ 107000 ug/L 1 22.0 50.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Lead [7439-92-1]^ 11.9 ug/L 1 3.10 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Manganese [7439-96-5]^ 87.3 ug/L 1 1.50 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1D16014 EPA 6020B 04/20/21 11:03 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1D16014 EPA 6020B 04/20/21 11:03 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1D15015 EPA 6010D 04/19/21 12:08 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 3.3 J mg/L 1 2.2 5.0 1D15028 EPA 300.0 04/16/21 05:10 LJI Sulfate as SO4 [14808-79-B]^ 6.8 mg/L 1 2.9 5.0 1D15028 EPA 300.0 04/16/21 05:10 LJI Sulfide [18496-25-8]^ 0.010 J mg/L 1 0.010 0.10 1D16007 iM 4500S2 D-2011 04/16/21 10:11 JOC Total Alkalinity as CaCO3 [471-34-1]^ 45 mg/L 1 14 15 1D20009 EPA 310.2 04/20/21 11:13 JAH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 63 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CE04871-16 Received: 04/13/21 16:20 Matrix: Ground Water Sampled: 04/13/2108:00 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: Gary Simcox/James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analvte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 16:12 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 4.9 1 5.00 98 % 75-125 ID20044 EPA 6260D 04120121 16:12 KKW Classical Chemistry Parameters Analyte rCAS Numberl Total Dissolved Solids Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 12 mg/L 1 10 10 1D19007 SM 254OC-2011 04/20/21 13:53 AAL FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 64 of 98 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIPBLANK Lab Sample ID:CE04871-17 Received: 04/13/21 16:20 Matrix: Water Sampled:04/12/21 10:05 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 ID21037 EPA 8260D 04/22/21 08:22 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 ID21037 EPA 8260D 04/22/21 08:22 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 ID21037 EPA 8260D 04/22/21 08:22 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY QV-01 Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 ID21037 EPA 8260D 04/22/21 08:22 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 ID21037 EPA 8260D 04/22/21 08:22 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 65 of 98 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIPBLANK Lab Sample ID:CE04871-17 Received: 04/13/21 16:20 Matrix: Water Sampled:04/12/21 10:05 Work Order: CE04871 Project: Moore County Active C & D LF - Spring Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1D21037 EPA 8260D 04/22/21 08:22 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1D21037 EPA 8260D 04/22/21 08:22 RKY QV-01 Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 57 1 50.0 114 % 53-136 ID21037 EPA 6260D 04122121 08:22 RKY Dibromofluoromethane 53 1 50.0 106 % 67-129 1D21037 EPA 6260D 04122121 06:22 RKY Toluene-d8 58 1 50.0 116 % 59-134 1D21037 EPA 6260D 04122121 06:22 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1D20044 EPA 8260D 04/20/21 15:21 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed & Notes Toluene-d8 5.1 1 5.00 103 % 75-125 1D20044 EPA 8260D 04120121 15:21 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 66 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1D21037 - EPA 5030B MS Blank (1D21037-BLK1) Prepared: 04/21/2021 17:40 Analyzed: 04/22/2021 06:59 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 67 of 98 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1 D21037 - EPA 5030B MS - Continued (� �Eo www.encolabs.com Blank (ID21037-BLK1) Continued Prepared: 04/21/2021 17:40 Analyzed: 04/22/2021 06:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 57 u91L 50.0 113 53-136 Dibromofluoromethane 55 u91L 50.0 110 67-129 Toluene-d8 58 u91L 50.0 117 59-134 LCS (1D21037-BSI) Prepared: 04/21/2021 17:40 Analyzed: 04/22/2021 05:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 121 75-133 Benzene 22 1.0 ug/L 20.0 109 80-134 Chlorobenzene 22 1.0 ug/L 20.0 108 80-120 Toluene 21 1.0 ug/L 20.0 107 71-120 Trichloroethene 22 1.0 ug/L 20.0 111 74-120 Matrix Spike (1D23037-MS1) Prepared: 04/21/2021 17:40 Analyzed: 04/22/2021 05:35 Source: CE05456-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 57 1.0 ug/L 47.0 2.1 118 75-133 Benzene 46 1.0 ug/L 47.0 0.15 U 97 80-134 Chlorobenzene 46 1.0 ug/L 47.0 0.17 U 98 80-120 Toluene 44 1.0 ug/L 47.0 0.14 U 93 71-120 Trichloroethene 48 1.0 ug/L 47.0 0.15 U 101 74-120 Matrix Spike Dup (11323037-MS131) Prepared: 04/21/2021 17:40 Analyzed: 04/22/2021 06:03 Source: CE05456-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 60 1.0 ug/L 47.0 2.1 123 75-133 4 20 Benzene 49 1.0 ug/L 47.0 0.15 U 105 80-134 8 17 Chlorobenzene 47 1.0 ug/L 47.0 0.17 U 101 80-120 2 16 Toluene 48 1.0 ug/L 47.0 0.14 U 103 71-120 10 17 Trichloroethene 52 1.0 ug/L 47.0 0.15 U 110 74-120 8 22 Batch 1D22018 - EPA 5030E MS Blank (1D22018-BLK1) Prepared: 04/22/2021 14:02 Analyzed: 04/22/2021 19:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,1-Dichloropropene 0.15 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2,4-Trichlorobenzene 0.14 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 68 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1D22018 - EPA 5030B MS - Continued Blank (SD22018-BLK1) Continued Prepared: 04/22/2021 14:02 Analyzed: 04/22/2021 19:40 Analvte Result Flaq POL Units 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,3-Dichlorobenzene 0.15 U 1.0 ug/L 1,3-Dichloropropane 0.16 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2,2-Dichloropropane 0.28 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 3-Chloropropene 0.11 U 1.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acetonitrile 5.0 U 10 ug/L Acrolein 4.0 U 10 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L Chloroprene 0.64 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Dichlorodifluoromethane 0.20 U 1.0 ug/L Ethyl Methacrylate 0.38 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Hexachlorobutadiene 0.22 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Isobutyl alcohol 11 U 50 ug/L Methacrylonitrile 4.9 U 10 ug/L Methyl Methacrylate 0.51 U 1.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Propionitrile 5.0 U 10 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 69 of 98 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch ID22018 - EPA 5030B MS - Continued Blank (1D22018-BLK1) Continued Prepared: 04/22/2021 14:02 Analyzed: 04/22/2021 19:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 57 u91L 50.0 113 53-136 Dibromofluoromethane 53 u91L 50.0 107 67-129 Toluene-d8 57 u91L 50.0 113 59-134 LCS (1D22018-BS1) Prepared: 04/22/2021 14:02 Analyzed: 04/22/2021 17:47 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Mina Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 109 75-133 Benzene 20 1.0 ug/L 20.0 101 80-134 Chlorobenzene 20 1.0 ug/L 20.0 102 80-120 Toluene 21 1.0 ug/L 20.0 104 71-120 Trichloroethene 21 1.0 ug/L 20.0 106 74-120 4-8romofluorobenzene 56 u91L 50.0 112 53-136 Dibromofluoromethane 52 u91L 50.0 103 67-129 Toluene-& 58 u91L 50.0 116 59-134 Matrix Spike (1D22018-MS1) Prepared: 04/22/2021 14:02 Analyzed: 04/22/2021 18:15 Source: CE05893-02 Spike Source %REC RPD Analvte Result Flaa Q Units Level Res 1 %REC Limits RPD Limit Notes 1,1-Dichloroethene 26 1.0 ug/L 20.0 0.21 U 131 75-133 Benzene 23 1.0 ug/L 20.0 0.15 U 113 80-134 Chlorobenzene 24 1.0 ug/L 20.0 0.17 U 118 80-120 Toluene 23 1.0 ug/L 20.0 0.14 U 117 71-120 Trichloroethene 25 1.0 ug/L 20.0 0.15 U 123 74-120 QM-07 4-Bromofluorobenzene 57 u91L 50.0 114 53-136 Dibromofluoromethane 51 u91L 50.0 102 67-129 Toluene-d8 57 U91L 50.0 114 59-134 Matrix Spike Dup (1D22018-MSD1) Prepared: 04/22/2021 14:02 Analyzed: 04/22/2021 18:44 Source: CE05893-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Limit Notes 1,1-Dichloroethene 25 1.0 ug/L 20.0 0.21 U 123 75-133 7 20 Benzene 21 1.0 ug/L 20.0 0.15 U 104 80-134 8 17 Chlorobenzene 23 1.0 ug/L 20.0 0.17 U 115 80-120 3 16 Toluene 23 1.0 ug/L 20.0 0.14 U 113 71-120 4 17 Trichloroethene 23 1.0 ug/L 20.0 0.15 U 113 74-120 8 22 4-Bromofluorobenzene 60 u91L 50.0 120 53-136 Dibromofluoromethane 52 u91L 50.0 104 67-129 Toluene-& 57 u9/L 50.0 114 59-134 Batch ID22019 - EPA 5030B MS FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 70 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1D22019 - EPA 5030B MS - Continued Blank (11322019-BLK1) Prepared: 04/22/2021 13:34 Analyzed: 04/22/2021 16:56 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 71 of 98 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1D22019 - EPA 5030B MS - Continued (� �Eo www.encolabs.com Blank (ID22019-BLK1) Continued Prepared: 04/22/2021 13:34 Analyzed: 04/22/2021 16:56 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 47 ug/L 50.0 94 53-136 Dibromofluoromethane 45 u91L 50.0 90 67-129 Toluene-d8 48 u91L 50.0 97 59-134 LCS (1D22019-BSI) Prepared: 04/22/2021 13:34 Analyzed: 04/22/2021 15:07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 101 75-133 Benzene 20 1.0 ug/L 20.0 99 80-134 Chlorobenzene 19 1.0 ug/L 20.0 97 80-120 Toluene 19 1.0 ug/L 20.0 94 71-120 Trichloroethene 22 1.0 ug/L 20.0 108 74-120 Matrix Spike (1D22019-MS1) Prepared: 04/22/2021 13:34 Analyzed: 04/22/2021 15:34 Source: CE05527-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.83 101 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 94 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 94 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 90 71-120 Trichloroethene 29 1.0 ug/L 20.0 9.0 101 74-120 Matrix Spike Dup (11322019-MS131) Prepared: 04/22/2021 13:34 Analyzed: 04/22/2021 16:02 Source: CE05527-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 0.83 104 75-133 3 20 Benzene 20 1.0 ug/L 20.0 0.15 U 99 80-134 6 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 4 16 Toluene 19 1.0 ug/L 20.0 0.14 U 93 71-120 3 17 Trichloroethene 31 1.0 ug/L 20.0 9.0 108 74-120 5 22 Batch 1D22033 - EPA 5030B MS Blank (1D22033-BLK1) Prepared: 04/22/2021 14:56 Analyzed: 04/23/2021 11:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 72 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch ID22033 - EPA 5030B MS - Continued Blank (SD22033-BLK1) Continued Prepared: 04/22/2021 14:56 Analyzed: 04/23/2021 11:46 Analvte Result Flaq POL Units 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 46 u91L 50.0 93 53-136 Dibromofluoromethane 44 u91L 50.0 88 67-129 Toluene-d8 49 u91L 50.0 97 59-134 LCS (11322033-BSI) Prepared: 04/22/2021 14:56 Analyzed: 04/23/2021 09:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 95 75-133 Benzene 19 1.0 ug/L 20.0 95 80-134 Chlorobenzene 19 1.0 ug/L 20.0 96 80-120 Toluene 18 1.0 ug/L 20.0 90 71-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 73 of 98 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1D22033 - EPA 5030B MS - Continued (� �Eo www.encolabs.com LCS (111322033-BSI) Continued Prepared: 04/22/2021 14:56 Analyzed: 04/23/2021 09:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichloroethene 20 1.0 ug/L 20.0 101 74-120 Matrix Spike (1D22033-MS1) Prepared: 04/22/2021 14:56 Analyzed: 04/23/2021 10:24 Source: CE05893-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 101 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 100 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 19 1.0 ug/L 20.0 0.14 U 93 71-120 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 105 74-120 Matrix Spike Dup (1D22033-MSD1) Prepared: 04/22/2021 14:56 Analyzed: 04/23/2021 10:51 Source: CE05893-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 92 75-133 10 20 Benzene 19 1.0 ug/L 20.0 0.15 U 95 80-134 5 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 94 80-120 3 16 Toluene 18 1.0 ug/L 20.0 0.14 U 88 71-120 6 17 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 100 74-120 6 22 Semivolatile Organic Compounds by GCMS - Quality Control Batch ID17004 - EPA 3510C MS Blank (1D37004-BLK3) Prepared: 04/17/2021 08:58 Analyzed: 04/21/2021 13:15 Analvte 1,2,4,5-Tetrachlorobenzene 1,3,5-Trin itrobenzene 1,3-Dinitrobenzene 1,4-Naphthoquinone 1,4-Phenylened iami ne 1-Naphthylamine 2,3,4,6-Tetrach lorophenol 2,4, 5-Trich t o rop hen o f 2,4, 6-Trich t o rop hen o f 2,4-Dichlorophenol 2,4-Di methyl phenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dichlorophenol 2,6-Dinitrotoluene 2-Acetyla m i nofl u o rene 2-Chloronaphthalene 2-Chlorophenol 2-Methyl-4,6-din itrophenol 2- Methyl naphthalene 2-Methylphenol 2-Naphthylamine Result Flaq POL Units 3.4 U 10 ug/L 3.0 U 10 ug/L 2.5 U 10 ug/L 2.5 U 10 ug/L 4.0 U 10 ug/L 2.2 U 10 ug/L 2.4 U 10 ug/L 2.5 U 10 ug/L 2.6 U 10 ug/L 2.6 U 10 ug/L 2.3 U 10 ug/L 2.6 U 10 ug/L 2.6 U 10 ug/L 2.0 U 10 ug/L 2.5 U 10 ug/L 3.1 U 10 ug/L 2.8 U 10 ug/L 2.2 U 10 ug/L 3.3 U 10 ug/L 2.8 U 10 ug/L 2.0 U 10 ug/L 3.0 U 10 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes QV-01 QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 74 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 1D17004 - EPA 3510C MS - Continued Blank (SD37004-BLK1) Continued Prepared: 04/17/2021 08:58 Analyzed: 04/21/2021 13:15 Analvte Result Flaq POL Units 2-Nitroaniline 2.5 U 10 ug/L 2-Nitrophenol 1.1 U 10 ug/L 3 & 4-Methylphenol 2.1 U 10 ug/L 3,3'-Dichlorobenzidine 3.5 U 10 ug/L 3,3'-Dimethylbenzidine 2.2 U 10 ug/L 3-Methylcholanthrene 1.3 U 10 ug/L 3-Nitroaniline 2.6 U 10 ug/L 4-Aminobiphenyl 3.5 U 10 ug/L 4-Bromophenyl-phenylether 2.4 U 10 ug/L 4-Chloro-3-methylphenol 2.4 U 10 ug/L 4-Chloroaniline 2.0 U 10 ug/L 4-Chlorophenyl-phenylether 2.6 U 10 ug/L 4-Nitroaniline 3.2 U 10 ug/L 4-Nitrophenol 2.8 U 10 ug/L 5-Nitro-o-toluidine 3.2 U 10 ug/L 7,12-Di methyl benz(a)anth racene 1.4 U 10 ug/L a,a-Dimethylphenethylamine 3.5 U 10 ug/L Acenaphthene 2.7 U 10 ug/L Acenaphthylene 2.6 U 10 ug/L Acetophenone 2.0 U 10 ug/L Anthracene 2.4 U 10 ug/L Benzo(a)anthracene 2.4 U 10 ug/L Benzo(a)pyrene 2.2 U 10 ug/L Benzo(b)fluoranthene 2.8 U 10 ug/L Benzo(g,h,i)perylene 2.4 U 10 ug/L Benzo(k)fluoranthene 2.4 U 10 ug/L Benzyl alcohol 2.4 U 10 ug/L Bis(2-chloroethoxy)methane 2.4 U 10 ug/L Bis(2-chloroethyl)ether 2.6 U 10 ug/L Bis(2-chloroisopropyl)ether 2.5 U 10 ug/L Bis(2-ethylhexyl)phthalate 1.9 U 5.0 ug/L Butyl benzylphtha late 3.8 U 10 ug/L Chlorobenzilate 2.4 U 10 ug/L Chrysene 2.2 U 10 ug/L Diallate 1.9 U 10 ug/L Dibenzo(a,h)anthracene 2.3 U 10 ug/L Dibenzofuran 2.6 U 10 ug/L Diethylphtha late 2.4 U 10 ug/L Dimethoate 2.3 U 10 ug/L Dimethylphthalate 2.5 U 10 ug/L Di-n-butylphthalate 2.8 U 10 ug/L Di-n-octylphthalate 3.1 U 10 ug/L Disulfoton 2.0 U 10 ug/L Ethyl methanesulfonate 2.2 U 10 ug/L Famphur 2.7 U 10 ug/L Fluoranthene 3.1 U 10 ug/L Fluorene 2.5 U 10 ug/L Hexachlorobenzene 2.3 U 10 ug/L Hexachlorobutadiene 2.8 U 10 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes QV-01 QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 75 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 1D17004 - EPA 3510C MS - Continued Blank (SD37004-BLK1) Continued Prepared: 04/17/2021 08:58 Analyzed: 04/21/2021 13:15 Analvte Result Flaq POL Units Hexachlorocyclopentadiene 2.7 U 10 ug/L Hexachloroethane 2.6 U 10 ug/L Hexachloropropene 6.8 U 10 ug/L Indeno(1,2,3-cd)pyrene 2.2 U 10 ug/L Isodrin 1.5 U 10 ug/L Isophorone 2.5 U 10 ug/L Isosafrole 2.2 U 10 ug/L Kepone 7.2 U 20 ug/L Methapyrilene 4.8 U 10 ug/L Methyl Methanesulfonate 2.2 U 10 ug/L Methyl parathion 2.5 U 10 ug/L Nitrobenzene 2.5 U 10 ug/L N-Nitrosodiethylamine 2.1 U 10 ug/L N-Nitrosodimethylamine 1.9 U 10 ug/L N-Nitrosodi-n-butylamine 2.0 U 10 ug/L N-Nitroso-di-n-propylamine 2.3 U 10 ug/L N-nitrosodiphenylamine/Diphenylamine 2.5 U 10 ug/L N-Nitrosomethylethylamine 1.9 U 10 ug/L N-Nitrosopiperidine 2.1 U 10 ug/L N-Nitrosopyrrolidine 1.9 U 10 ug/L 0,0,0-Triethylphosphorothioate 2.2 U 10 ug/L o-Toluidine 1.6 U 10 ug/L Parathion 1.7 U 10 ug/L p-Dimethylaminoazobenzene 2.6 U 10 ug/L Pentachlorobenzene 2.7 U 10 ug/L Pentachloronitrobenzene 1.9 U 10 ug/L Phenacetin 2.7 U 10 ug/L Phenanthrene 2.6 U 10 ug/L Phenol 1.7 U 10 ug/L Phorate 2.1 U 10 ug/L Pronamide 1.7 U 10 ug/L Pyrene 3.5 U 10 ug/L Safrole 2.2 U 10 ug/L Thionazin 2.3 U 10 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes QV-01 J-05 QV-01 2,4,6-Tribromophenol 62 ug/L 100 62 10-179 2-Fluorobiphenyl 39 ug/L 50.0 79 10-149 2-Fluorophenol 58 u91L 100 58 10-110 Nitrobenzene-d5 40 ug/L 50.0 80 10-149 Phenol-d5 50 ug/L 100 50 10-88 TerphenyhdM 48 u91L 50.0 95 10-188 LCS (11317004-BSI) Prepared: 04/17/2021 08:58 Analyzed: 04/21/2021 13:44 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 42 10 ug/L 50.0 85 40-109 4-Chloro-3-methylphenol 50 10 ug/L 50.0 100 58-121 4-Nitrophenol 45 10 ug/L 50.0 90 33-105 J-04 Acenaphthene 48 10 ug/L 50.0 97 39-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 76 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 1D17004 - EPA 3510C MS - Continued LCS (11337004-113SI) Continued Prepared: 04/17/2021 08:58 Analyzed: 04/21/2021 13:44 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes N-Nitroso-di-n-propylamine 45 10 ug/L 50.0 90 48-126 Phenol 33 10 ug/L 50.0 66 19-78 Pyrene 51 10 ug/L 50.0 101 44-137 2,4,6-Tribromophenol 110 ug/L 100 114 10-179 2-Fluorobiphenyl 46 ug/L 50.0 95 10-149 2-Fluorophenol 69 ug/L 100 69 10-110 Nitrobenzene-d5 46 ug/L 50.0 93 10-149 Phenohd5 61 ug/L 100 61 10-88 Terphenyl-d14 54 ug/L 50.0 109 10-188 Matrix Spike (1D17004-MS3) Prepared: 04/17/2021 08:58 Analyzed: 04/21/2021 14:13 Source: CE05675-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 42 10 ug/L 50.0 2.2 U 83 40-109 4-Chloro-3-methylphenol 48 10 ug/L 50.0 2.4 U 97 58-121 4-Nitrophenol 41 10 ug/L 50.0 2.8 U 82 33-105 3-04 Acenaphthene 47 10 ug/L 50.0 2.7 U 95 39-125 N-Nitroso-di-n-propylamine 44 10 ug/L 50.0 2.3 U 88 48-126 Phenol 32 10 ug/L 50.0 1.7 U 63 19-78 Pyrene 51 10 ug/L 50.0 3.5 U 102 44-137 2,4,6-Tribromophenol 100 ug/L 100 100 10-179 2-Fluorobiphenyl 44 ug/L 50.0 69 10-149 2-Fluorophenol 63 ug/L 100 63 10-110 Nitrobenzene-d5 43 ug/L 50.0 86 10-149 Phenol-d5 55 ug/L 100 55 10-88 Terphenyl-d14 51 ug/L 50.0 102 10-188 Matrix Spike Dup (1D37004-MSD1) Prepared: 04/17/2021 08:58 Analyzed: 04/21/2021 14:43 Source: CE05675-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 42 10 ug/L 50.0 2.2 U 84 40-109 0.9 22 4-Chloro-3-methylphenol 49 10 ug/L 50.0 2.4 U 99 58-121 2 22 4-Nitrophenol 43 10 ug/L 50.0 2.8 U 86 33-105 5 27 J-04 Acenaphthene 49 10 ug/L 50.0 2.7 U 99 39-125 4 25 N-Nitroso-di-n-propylamine 43 10 ug/L 50.0 2.3 U 87 48-126 2 23 Phenol 32 10 ug/L 50.0 1.7 U 63 19-78 0.03 18 Pyrene 55 10 ug/L 50.0 3.5 U 110 44-137 8 24 2,4,6-Tribromophenol 110 ug/L 100 109 10-179 2-Fluorobiphenyl 46 ug/L 50.0 92 10-149 2-Fluorophenol 66 ug/L 100 66 10-110 Nitrobenzene-d5 45 u91L 50.0 90 10-149 Phenol-d5 55 ug/L 100 55 10-88 Terphenyl-d14 57 ug/L 50.0 114 10-188 Organochlorine Pesticides by GC - Quality Control Batch ID19004 - EPA 3510C FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 77 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Organochlorine Pesticides by GC - Quality Control Batch 1D19004 - EPA 3510C - Continued Blank (1D19004-BLK1) Prepared: 04/19/2021 08:08 Analyzed: 04/27/2021 09:23 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 4,4'-DDD 0.044 U 0.050 ug/L 4,4'-DDE 0.048 U 0.050 ug/L 4,4'-DDT 0.049 U 0.050 ug/L Aldrin 0.041 U 0.050 ug/L alpha-BHC 0.036 U 0.050 ug/L beta-BHC 0.041 U 0.050 ug/L Chlordane (tech) 0.37 U 0.50 ug/L Chlordane -alpha 0.048 U 0.050 ug/L Chlordane -gamma 0.042 U 0.050 ug/L delta-BHC 0.048 U 0.050 ug/L Dieldrin 0.045 U 0.050 ug/L Endosulfan I 0.045 U 0.050 ug/L Endosulfan II 0.038 U 0.050 ug/L Endosulfan sulfate 0.032 U 0.050 ug/L Endrin 0.041 U 0.050 ug/L Endrin aldehyde 0.049 U 0.050 ug/L gamma-BHC 0.034 U 0.050 ug/L Heptachlor 0.047 U 0.050 ug/L Heptachlor epoxide 0.037 U 0.050 ug/L Methoxychlor 0.048 U 0.050 ug/L Toxaphene 0.28 U 1.0 ug/L 2,4,5,E-TCMX 0.62 u9/L 1.00 62 10-139 Decachlorobiphenyl 0.74 u91L 1.00 74 10-122 LCS (11319004-BSI) Prepared: 04/19/2021 08:08 Analyzed: 04/27/2021 09:39 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 4,4'-DDT 1.1 0.050 ug/L 1.00 111 37-139 Dieldrin 0.97 0.050 ug/L 1.00 97 46-132 Endrin 0.94 0.050 ug/L 1.00 94 43-133 2,4,5,E-TCMX 0.65 u91L 1.00 65 10-139 Decachlorobiphenyl 0.84 u91L 1.00 84 10-122 Matrix Spike (1D19004-MS1) Prepared: 04/19/2021 08:08 Analyzed: 04/27/2021 09:53 Source: CE05675-09 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 4,4'-DDT 0.90 0.050 ug/L 1.00 0.049 U 90 37-139 Dieldrin 1.0 0.050 ug/L 1.00 0.045 U 105 46-132 Endrin 1.0 0.050 ug/L 1.00 0.041 U 101 43-133 2,4,5,E-TCMX 0.64 u91L 1.00 64 10-139 Decachlorobiphenyl 0.88 u91L 1.00 88 10-122 Matrix Spike Dup (11319004-MS131) Prepared: 04/19/2021 08:08 Analyzed: 04/27/2021 10:10 Source: CE05675-09 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 4,4'-DDT 1.1 0.050 ug/L 1.00 0.049 U ill 37-139 21 26 Dieldrin 1.0 0.050 ug/L 1.00 0.045 U 105 46-132 0 27 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 78 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Organochlorine Pesticides by GC - Quality Control Batch ID19004 - EPA 3510C - Continued Matrix Spike Dup (1D19004-MSD1) Continued Prepared: 04/19/2021 08:08 Analyzed: 04/27/2021 10:10 Source: CE05675-09 Analvte Result Flaq Endrin 1.0 POL Units 0.050 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 1.00 0.041 U 102 43-133 1 26 2,4,5,6-TCMX 0.72 Decachlorobiphenyl 0.91 ug/L u91L 1.00 72 10-139 1.00 91 10-122 Polychlorinated Biphenyls by GC - Quality Control Batch IDI9005 - EPA 3510C Blank (1D39005-BLK3) Prepared: 04/19/2021 08:12 Analyzed: 04/27/2021 10:24 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 0.48 U 0.50 ug/L PCB-1221 0.43 U 0.50 ug/L PCB-1232 0.50 U 0.50 ug/L PCB-1248 0.45 U 0.50 ug/L PCB-1254 0.43 U 0.50 ug/L PCB-1260 0.47 U 0.50 ug/L 2,4,5,E-TCMX 0.68 ug/L 1.00 68 10-128 Decachlorobiphenyl 0.92 u91L 1.00 92 10-129 LCS (1D19005-BS1) Prepared: 04/19/2021 08:12 Analyzed: 04/27/2021 10:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 10 0.50 ug/L 10.0 102 43-123 PCB-1260 10 0.50 ug/L 10.0 103 41-125 2,4,5,6-TCMX 0.61 u91L 1.00 61 10-128 Decachlorobiphenyl 0.81 u91L 1.00 81 10-129 Matrix Spike (1D19005-MS1) Prepared: 04/19/2021 08:12 Analyzed: 04/27/2021 10:55 Source: CE05675-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 13 0.50 ug/L 10.0 0.48 U 127 43-123 QM-07 PCB-1260 14 0.50 ug/L 10.0 0.47 U 137 41-125 QM-07 2,4,5,6-TCMX 0.80 u91L 1.00 80 10-128 Decachlorobiphenyl 1.1 u91L 1.00 112 10-129 Matrix Spike Dup (11319005-MS131) Prepared: 04/19/2021 08:12 Analyzed: 04/27/2021 11:11 Source: CE05675-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 11 0.50 ug/L 10.0 0.48 U 115 43-123 10 23 PCB-1260 12 0.50 ug/L 10.0 0.47 U 124 41-125 10 31 2,4,5,6-TCMX 0.79 u91L 1.00 79 10-128 Decachlorobiphenyl 1.1 u91L 1.00 113 10-129 Metals by EPA 6000/7000 Series Methods - Quality Control Batch ID19008 - EPA 7470A FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 79 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch 1D1900B - EPA 7470A - Continued Blank (1D19008-BLK1) Prepared: 04/19/2021 08:56 Analyzed: 04/20/2021 11:49 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (11319008-BS1) Prepared: 04/19/2021 08:56 Analyzed: 04/20/2021 11:51 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.06 0.200 ug/L 5.00 101 80-120 Matrix Spike (1D19008-MS1) Prepared: 04/19/2021 08:56 Analyzed: 04/20/2021 11:56 Source: CE04574-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.02 0.200 ug/L 5.00 0.150 U 100 75-125 Matrix Spike Dup (11319008-MS131) Prepared: 04/19/2021 08:56 Analyzed: 04/20/2021 11:58 Source: CE04574-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.05 0.200 ug/L 5.00 0.150 U 101 75-125 0.6 25 Post Spike (11319008-PS1) Prepared: 04/19/2021 08:56 Analyzed: 04/20/2021 12:00 Source: CE04574-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.54 0.200 ug/L 5.00 0.0530 110 75-125 Batch ID19009 - EPA 7470A Blank (lD19009-BLKI) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (lD19009-BSI) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.28 0.200 ug/L 5.00 106 80-120 Matrix Spike (1D19009-MS1) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:11 Source: CE04871-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.23 0.200 ug/L 5.00 0.150 U 105 75-125 Matrix Spike Dup (1D19009-MSD1) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:14 Source: CE04871-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.04 0.200 ug/L 5.00 0.150 U 101 75-125 4 25 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 80 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch ID19009 - EPA 7470A - Continued Post Spike (SD39009-PS3) Prepared: 04/19/2021 09:05 Analyzed: 04/20/2021 14:16 Source: CE04871-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.41 0.200 ug/L 5.00 0.0300 108 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch ID14041 - EPA 3005A Blank (1D34041-BLK1) Prepared: 04/14/2021 16:10 Analyzed: 04/19/2021 10:15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Beryllium 0.160 U 1.00 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Cobalt 1.40 U 10.0 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Manganese 1.50 U 10.0 ug/L Nickel 2.20 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L Tin 2.90 U 10.0 ug/L Vanadium 1.40 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (1D14041-BS1) Prepared: 04/14/2021 16:10 Analyzed: 04/19/2021 10:21 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 198 10.0 ug/L 200 99 80-120 Barium 212 10.0 ug/L 200 106 80-120 Beryllium 20.1 1.00 ug/L 20.0 101 80-120 Cadmium 20.3 1.00 ug/L 20.0 101 80-120 Chromium 203 10.0 ug/L 200 101 80-120 Cobalt 207 10.0 ug/L 200 103 80-120 Copper 202 10.0 ug/L 200 101 80-120 Iron 1080 50.0 ug/L 1000 108 80-120 Lead 207 10.0 ug/L 200 103 80-120 Manganese 203 10.0 ug/L 200 101 80-120 Nickel 213 10.0 ug/L 200 106 80-120 Selenium 205 10.0 ug/L 200 103 80-120 Silver 207 10.0 ug/L 200 103 80-120 Tin 203 10.0 ug/L 200 102 80-120 Vanadium 198 10.0 ug/L 200 99 80-120 Zinc 213 10.0 ug/L 200 106 80-120 Matrix Spike (1D14041-MS3) Prepared: 04/14/2021 16:10 Analyzed: 04/19/2021 10:24 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 81 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch ID14041 - EPA 3005A - Continued Matrix Spike (1D14041-MS3) Continued Prepared: 04/14/2021 16:10 Analyzed: 04/19/2021 10:24 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 208 10.0 ug/L 200 7.60 U 104 75-125 Barium 316 10.0 ug/L 200 103 107 75-125 Beryllium 20.8 1.00 ug/L 20.0 0.160 U 104 75-125 Cadmium 20.0 1.00 ug/L 20.0 0.360 U 100 75-125 Chromium 207 10.0 ug/L 200 1.40 U 103 75-125 Cobalt 209 10.0 ug/L 200 1.40 U 105 75-125 Copper 204 10.0 ug/L 200 1.60 U 102 75-125 Iron 20500 50.0 ug/L 1000 19300 122 75-125 Lead 210 10.0 ug/L 200 5.15 102 75-125 Manganese 543 10.0 ug/L 200 327 108 75-125 Nickel 215 10.0 ug/L 200 2.20 U 107 75-125 Selenium 200 10.0 ug/L 200 6.20 U 100 75-125 Silver 209 10.0 ug/L 200 1.90 U 104 75-125 Tin 208 10.0 ug/L 200 2.90 U 104 75-125 Vanadium 204 10.0 ug/L 200 1.40 U 102 75-125 Zinc 218 10.0 ug/L 200 4.40 U 109 75-125 Matrix Spike Dup (1D14041-MSD1) Prepared: 04/14/2021 16:10 Analyzed: 04/19/2021 10:26 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 209 10.0 ug/L 200 7.60 U 104 75-125 0.09 20 Barium 320 10.0 ug/L 200 103 108 75-125 1 20 Beryllium 21.1 1.00 ug/L 20.0 0.160 U 106 75-125 1 20 Cadmium 20.3 1.00 ug/L 20.0 0.360 U 101 75-125 2 20 Chromium 210 10.0 ug/L 200 1.40 U 105 75-125 1 20 Cobalt 213 10.0 ug/L 200 1.40 U 106 75-125 2 20 Copper 206 10.0 ug/L 200 1.60 U 103 75-125 0.9 20 Iron 20700 50.0 ug/L 1000 19300 139 75-125 0.8 20 QM-07 Lead 212 10.0 ug/L 200 5.15 103 75-125 1 20 Manganese 545 10.0 ug/L 200 327 109 75-125 0.5 20 Nickel 218 10.0 ug/L 200 2.20 U 109 75-125 2 20 Selenium 204 10.0 ug/L 200 6.20 U 102 75-125 2 20 Silver 212 10.0 ug/L 200 1.90 U 106 75-125 1 20 Tin 210 10.0 ug/L 200 2.90 U 105 75-125 1 20 Vanadium 207 10.0 ug/L 200 1.40 U 104 75-125 2 20 Zinc 221 10.0 ug/L 200 4.40 U 111 75-125 2 20 Post Spike (111314041-PSI) Prepared: 04/14/2021 16:10 Analyzed: 04/19/2021 10:28 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.184 0.0100 mg/L 0.200 -0.00425 92 80-120 Barium 0.289 0.0100 mg/L 0.200 0.103 93 80-120 Beryllium 0.0183 0.00100 mg/L 0.0200 -0.000185 91 80-120 Cadmium 0.0177 0.00100 mg/L 0.0200 -0.000370 89 80-120 Chromium 0.182 0.0100 mg/L 0.200 -0.000106 91 80-120 Cobalt 0.185 0.0100 mg/L 0.200 0.000380 92 80-120 Copper 0.179 0.0100 mg/L 0.200 -0.00185 89 80-120 Iron 20.0 0.0500 mg/L 1.00 19.3 73 80-120 QM-08 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 82 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch ID14041 - EPA 3005A - Continued Post Spike (SD34041-PS3) Continued Prepared: 04/14/2021 16:10 Analyzed: 04/19/2021 10:28 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 0.184 0.0100 mg/L 0.200 0.00515 89 80-120 Manganese 0.508 0.0100 mg/L 0.200 0.327 90 80-120 Nickel 0.190 0.0100 mg/L 0.200 0.000420 95 80-120 Selenium 0.174 0.0100 mg/L 0.200 -0.0183 87 80-120 Silver 0.188 0.0100 mg/L 0.200 0.00110 93 80-120 Tin 0.185 0.0100 mg/L 0.200 -0.000263 93 80-120 Vanadium 0.179 0.0100 mg/L 0.200 -0.00279 89 80-120 Zinc 0.193 0.0100 mg/L 0.200 0.00190 96 80-120 Batch ID15015 - EPA 3005A Blank (1D1SO1S-BLK3) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:31 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Beryllium 0.160 U 1.00 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Cobalt 1.40 U 10.0 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Manganese 1.50 U 10.0 ug/L Nickel 2.20 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L Vanadium 1.40 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (1D1SOIS-BSI) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:36 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 203 10.0 ug/L 200 101 80-120 Barium 215 10.0 ug/L 200 107 80-120 Beryllium 20.4 1.00 ug/L 20.0 102 80-120 Cadmium 20.4 1.00 ug/L 20.0 102 80-120 Chromium 205 10.0 ug/L 200 102 80-120 Cobalt 208 10.0 ug/L 200 104 80-120 Copper 204 10.0 ug/L 200 102 80-120 Iron 1070 50.0 ug/L 1000 107 80-120 Lead 212 10.0 ug/L 200 106 80-120 Manganese 205 10.0 ug/L 200 102 80-120 Nickel 215 10.0 ug/L 200 107 80-120 Selenium 204 10.0 ug/L 200 102 80-120 Silver 209 10.0 ug/L 200 105 80-120 Vanadium 200 10.0 ug/L 200 100 80-120 Zinc 214 10.0 ug/L 200 107 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 83 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1D15015 - EPA 3005A - Continued Matrix Spike (1D15015-MS1) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:39 Source: CE04871-14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 202 10.0 ug/L 200 7.60 U 101 75-125 Barium 231 10.0 ug/L 200 20.8 105 75-125 Beryllium 20.1 1.00 ug/L 20.0 0.160 U 100 75-125 Cadmium 20.4 1.00 ug/L 20.0 0.360 U 102 75-125 Chromium 202 10.0 ug/L 200 1.40 U 101 75-125 Cobalt 206 10.0 ug/L 200 1.40 U 103 75-125 Copper 202 10.0 ug/L 200 1.60 U 101 75-125 Iron 15300 50.0 ug/L 1000 17300 NR 75-125 QM-07 Lead 210 10.0 ug/L 200 4.55 103 75-125 Manganese 244 10.0 ug/L 200 44.7 100 75-125 Nickel 213 10.0 ug/L 200 2.20 U 107 75-125 Selenium 198 10.0 ug/L 200 6.20 U 99 75-125 Silver 205 10.0 ug/L 200 1.90 U 103 75-125 Vanadium 197 10.0 ug/L 200 1.40 U 99 75-125 Zinc 213 10.0 ug/L 200 4.40 U 107 75-125 Matrix Spike Dup (1D15015-MSD1) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:46 Source: CE04871-14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 209 10.0 ug/L 200 7.60 U 105 75-125 4 20 Barium 236 10.0 ug/L 200 20.8 107 75-125 2 20 Beryllium 20.6 1.00 ug/L 20.0 0.160 U 103 75-125 3 20 Cadmium 20.7 1.00 ug/L 20.0 0.360 U 103 75-125 1 20 Chromium 207 10.0 ug/L 200 1.40 U 103 75-125 2 20 Cobalt 210 10.0 ug/L 200 1.40 U 105 75-125 2 20 Copper 207 10.0 ug/L 200 1.60 U 103 75-125 2 20 Iron 17400 50.0 ug/L 1000 17300 12 75-125 13 20 QM-07 Lead 212 10.0 ug/L 200 4.55 104 75-125 1 20 Manganese 252 10.0 ug/L 200 44.7 103 75-125 3 20 Nickel 217 10.0 ug/L 200 2.20 U 109 75-125 2 20 Selenium 204 10.0 ug/L 200 6.20 U 102 75-125 3 20 Silver 210 10.0 ug/L 200 1.90 U 105 75-125 3 20 Vanadium 202 10.0 ug/L 200 1.40 U 101 75-125 2 20 Zinc 217 10.0 ug/L 200 4.40 U 109 75-125 2 20 Post Spike (SD15015-PS1) Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:49 111 Source: CE04871-14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.196 0.0100 mg/L 0.200 0.00250 97 80-120 Barium 0.226 0.0100 mg/L 0.200 0.0208 103 80-120 Beryllium 0.0196 0.00100 mg/L 0.0200 -0.000139 98 80-120 Cadmium 0.0199 0.00100 mg/L 0.0200 -0.000123 99 80-120 Chromium 0.197 0.0100 mg/L 0.200 -0.000556 98 80-120 Cobalt 0.201 0.0100 mg/L 0.200 -0.000261 101 80-120 Copper 0.197 0.0100 mg/L 0.200 -0.000192 98 80-120 Iron 18.2 0.0500 mg/L 1.00 17.3 85 80-120 Lead 0.207 0.0100 mg/L 0.200 0.00455 101 80-120 Manganese 0.241 0.0100 mg/L 0.200 0.0447 98 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 84 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1D15015 - EPA 3005A - Continued Post Spike (SD35015-PS3) Continued Prepared: 04/15/2021 10:31 Analyzed: 04/19/2021 11:49 Source: CE04871-14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nickel 0.209 0.0100 mg/L 0.200 0.000192 104 80-120 Selenium 0.192 0.0100 mg/L 0.200 -0.0109 96 80-120 Silver 0.205 0.0100 mg/L 0.200 0.000876 102 80-120 Vanadium 0.192 0.0100 mg/L 0.200 -0.00149 96 80-120 Zinc 0.210 0.0100 mg/L 0.200 0.00102 104 80-120 Batch ID15017 - EPA 3005A Blank (1D35017-BLK3) Prepared: 04/15/2021 10:43 Analyzed: 04/20/2021 02:44 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 0.370 U 1.00 ug/L Selenium 0.910 U 1.00 ug/L Thallium 0.110 U 1.00 ug/L LCS (1D35017-BSI) Prepared: 04/15/2021 10:43 Analyzed: 04/20/2021 02:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 19.5 1.00 ug/L 20.0 97 80-120 Selenium 18.8 1.00 ug/L 20.0 94 80-120 Thallium 19.6 1.00 ug/L 20.0 98 80-120 Matrix Spike (1D15017-MS3) Prepared: 04/15/2021 10:43 Analyzed: 04/20/2021 04:19 Source: CE04672-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 39.8 2.00 ug/L 40.0 0.740 U 99 75-125 Selenium 42.0 2.00 ug/L 40.0 1.82 U 105 75-125 Thallium 40.3 2.00 ug/L 40.0 0.220 U 101 75-125 Matrix Spike Dup (1D35017-MSD1) Prepared: 04/15/2021 10:43 Analyzed: 04/20/2021 04:23 Source: CE04672-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 39.6 2.00 ug/L 40.0 0.740 U 99 75-125 0.6 20 Selenium 40.7 2.00 ug/L 40.0 1.82 U 102 75-125 3 20 Thallium 40.2 2.00 ug/L 40.0 0.220 U 100 75-125 0.3 20 Post Spike (111315017-PSI) Prepared: 04/15/2021 10:43 Analyzed: 04/20/2021 04:27 Source: CE04672-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 22.3 1.00 ug/L 20.0 0.00921 111 75-125 Selenium 20.8 1.00 ug/L 20.0 -0.228 104 75-125 Thallium 22.4 1.00 ug/L 20.0 0.0433 112 75-125 Batch ID16014 - EPA 3005A Blank (1D36014-BLK3) Prepared: 04/16/2021 10:33 Analyzed: 04/20/2021 09:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 85 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1D16014 - EPA 3005A - Continued Blank (SD36014-BLK1) Continued Prepared: 04/16/2021 10:33 Analyzed: 04/20/2021 09:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 0.370 U 1.00 ug/L Selenium 0.910 U 1.00 ug/L Thallium 0.110 U 1.00 ug/L LCS (1D16014-BS1) Prepared: 04/16/2021 10:33 Analyzed: 04/20/2021 09:53 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 20.0 1.00 ug/L 20.0 100 80-120 Selenium 19.0 1.00 ug/L 20.0 95 80-120 Thallium 20.5 1.00 ug/L 20.0 102 80-120 Matrix Spike (1D16014-MS1) Prepared: 04/16/2021 10:33 Analyzed: 04/20/2021 09:57 Source: CE04871-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 41.9 2.00 ug/L 40.0 0.740 U 105 75-125 Selenium 39.6 2.00 ug/L 40.0 1.82 U 99 75-125 Thallium 40.3 2.00 ug/L 40.0 0.220 U 101 75-125 Matrix Spike Dup (1D16014-MSD1) Prepared: 04/16/2021 10:33 Analyzed: 04/20/2021 10:01 Source: CE04871-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 40.9 2.00 ug/L 40.0 0.740 U 102 75-125 2 20 Selenium 37.9 2.00 ug/L 40.0 1.82 U 95 75-125 4 20 Thallium 39.7 2.00 ug/L 40.0 0.220 U 99 75-125 1 20 Post Spike (SD16014-PS1) Prepared: 04/16/2021 10:33 Analyzed: 04/20/2021 10:06 Source: CE04871-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 22.7 1.00 ug/L 20.0 0.0178 114 75-125 Selenium 22.5 1.00 ug/L 20.0 -0.210 112 75-125 Thallium 22.2 1.00 ug/L 20.0 0.0591 111 75-125 Batch IE07007 - EPA 3005A Blank (3E07007-BLK1) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 12:45 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 3.10 U 10.0 ug/L Blank (3E07007-BLK2) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 12:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 3.10 U 10.0 ug/L LCS (3E07007-BSI) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 12:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 86 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch IE07007 - EPA 3005A - Continued LCS (1E07007-BS1) Continued Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 12:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 193 10.0 ug/L 200 97 80-120 Matrix Spike (lE07007-MS1) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 13:00 Source: CE05406-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 160 10.0 ug/L 200 3.10 U 80 75-125 Matrix Spike Dup (3E07007-MSD1) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 13:02 Source: CE05406-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 163 10.0 ug/L 200 3.10 U 81 75-125 2 20 Post Spike (SE07007-PS1) Prepared: 05/07/2021 09:43 Analyzed: 05/10/2021 13:05 Source: CE05406-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 0.169 0.0100 mg/L 0.200-0.00126 85 80-120 Classical Chemistry Parameters - Quality Control Batch ID14029 - NO PREP Blank (1D34029-BLK1) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 14:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (111314029-BS3) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 15:15 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.96 0.10 mg/L 1.00 96 90-110 Matrix Spike (1D14029-MS3) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 14:50 Source: CE04807-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 Matrix Spike (1D14029-MS2) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 14:53 Source: CE04807-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.92 0.10 mg/L 1.00 0.017 U 92 90-110 Matrix Spike Dup (1D34029-MSDl) Prepared: 04/14/2021 13:37 Analyzed: 04/14/2021 14:51 Source: CE04807-01 Analvte Nitrite as N Batch ID15002 - Same Result Flaq POL 0.98 0.10 Spike Source %REC Units Level Result %REC Limits RPD mg/L 1.00 0.017 U 98 90-110 2 RPD Limit Notes 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 87 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1D15002 - Same - Continued Blank (1D15002-BLK1) Prepared: 04/15/2021 07:26 Analyzed: 04/19/2021 18:15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.0049 U 0.010 mg/L LCS (11315002-BS1) Prepared: 04/15/2021 07:26 Analyzed: 04/19/2021 18:17 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.16 0.010 mg/L 0.150 106 85-115 Matrix Spike (1D15002-MS3) Prepared: 04/15/2021 07:26 Analyzed: 04/19/2021 18:24 Source: CE04871-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.15 0.010 mg/L 0.150 0.0049 U 101 85-115 Matrix Spike (1D15002-MS2) Prepared: 04/15/2021 07:26 Analyzed: 04/19/2021 18:29 Source: CE04871-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.14 0.010 mg/L 0.150 0.0049 U 94 85-115 Matrix Spike Dup (11335002-MS131) Prepared: 04/15/2021 07:26 Analyzed: 04/19/2021 18:26 Source: CE04871-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.15 0.010 mg/L 0.150 0.0049 U 102 85-115 1 20 Batch ID15028 - NO PREP Blank (1D35028-BLK3) Prepared: 04/15/2021 13:23 Analyzed: 04/15/2021 23:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (11315028-BS1) Prepared: 04/15/2021 13:23 Analyzed: 04/16/2021 00:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 51 5.0 mg/L 50.0 102 90-110 Sulfate as SO4 50 5.0 mg/L 50.0 101 90-110 Matrix Spike (1D15028-MS1) Prepared: 04/15/2021 13:23 Analyzed: 04/16/2021 01:21 Source: CE04663-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 520 E 10 mg/L 40.0 480 106 90-110 Sulfate as SO4 51 10 mg/L 40.0 11 100 90-110 Matrix Spike (1D15028-MS2) Prepared: 04/15/2021 13:23 Analyzed: 04/16/2021 02:14 Source: CE04808-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 50 5.0 mg/L 20.0 26 123 90-110 Sulfate as SO4 19 5.0 mg/L 20.0 2.9 U 97 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 88 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1D1502B - NO PREP - Continued Matrix Spike Dup (1D15028-MSD1) Prepared: 04/15/2021 13:23 Analyzed: 04/16/2021 01:38 Source: CE04663-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 520 E 10 mg/L 40.0 480 111 90-110 0.4 10 Sulfate as SO4 46 10 mg/L 40.0 11 88 90-110 10 10 Batch ID16007 - NO PREP Blank (1D16007-BLK3) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (1D16007-BS1) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.44 0.10 mg/L 0.401 109 80-120 Duplicate (11336007-DUP3) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Source: CE04541-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 1.3 0.50 mg/L 1.2 5 25 Matrix Spike (1D16007-MS3) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Source: CE04541-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 3.5 0.50 mg/L 2.00 1.2 112 80-120 Matrix Spike Dup (1D36007-MSD1) Prepared: 04/16/2021 09:48 Analyzed: 04/16/2021 10:11 Source: CE04541-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 3.6 0.50 mg/L 2.00 1.2 117 80-120 3 25 Batch ID16017 - NO PREP Blank (1D36017-BLK3) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 15:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (1D16017-BS1) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 15:36 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 51 5.0 mg/L 50.0 103 90-110 Sulfate as SO4 50 5.0 mg/L 50.0 101 90-110 Matrix Spike (1D16017-MS3) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 16:12 Source: CE04314-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 89 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1 D16017 - NO PREP - Continued Matrix Spike (1D16017-MS3) Continued Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 16:12 Source: CE04314-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 900 50 mg/L 200 66 415 90-110 QM-07 Sulfate as SO4 390 50 mg/L 200 29 U 195 90-110 QM-07 Matrix Spike (1D16017-MS2) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 17:05 Source: CE04575-03RE3 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 24 5.0 mg/L 20.0 3.8 103 90-110 Sulfate as SO4 18 5.0 mg/L 20.0 2.9 U 88 90-110 QM-07 Matrix Spike Dup (1D36017-MSDl) Prepared: 04/16/2021 12:03 Analyzed: 04/16/2021 16:29 Ill Source: CE04314-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 890 50 mg/L 200 66 412 90-110 0.7 10 QM-07 Sulfate as SO4 390 50 mg/L 200 29 U 194 90-110 0.3 10 QM-07 Batch ID20009 - NO PREP Blank (1D20009-BLK1) Prepared: 04/20/2021 08:28 Analyzed: 04/20/2021 10:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (111320009-BS1) Prepared: 04/20/2021 08:28 Analyzed: 04/20/2021 11:00 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 102 80-120 Matrix Spike (1D20009-MS3) Prepared: 04/20/2021 08:28 Analyzed: 04/20/2021 11:01 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 230 E 15 mg/L 37.8 210 46 80-120 QM-07 Matrix Spike Dup (1D20009-MSDS) Prepared: 04/20/2021 08:28 Analyzed: 04/20/2021 11:02 Source: CE04871-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 230 E 15 mg/L 37.8 210 48 80-120 0.4 25 QM-07 Batch ID20027 - NO PREP Blank (1D20027-BLK3) Prepared: 04/20/2021 11:55 Analyzed: 04/20/2021 14:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfate as SO4 2.9 U 5.0 mg/L LCS (1D20027-BSI) Prepared: 04/20/2021 11:55 Analyzed: 04/20/2021 15:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 90 of 98 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1 D20027 - NO PREP - Continued (� �Eo www.encolabs.com LCS (111320027-BSI) Continued Prepared: 04/20/2021 11:55 Analyzed: 04/20/2021 15:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfate as SO4 51 5.0 mg/L 50.0 102 90-110 Matrix Spike (1D20027-MS3) Prepared: 04/20/2021 11:55 Analyzed: 04/20/2021 15:26 Source: CE04541-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfate as SO4 40 5.0 mg/L 20.0 21 94 90-110 Matrix Spike Dup (1D20027-MSD1) Prepared: 04/20/2021 11:55 Analyzed: 04/20/2021 15:43 Source: CE04541-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfate as SO4 40 5.0 mg/L 20.0 21 97 90-110 1 10 Batch ID21015 - NO PREP Blank (1D21015-BLK1) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 13:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (1D23015-BS1) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 13:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 1.25 102 90-110 Matrix Spike (1D23015-MS3) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 13:52 Source: CE04807-06 Spike Source %REC RPD Analyte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.57 0.10 mg/L 0.521 0.041 U 109 90-110 Matrix Spike (1D23015-MS2) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 14:01 Source: CE04807-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.57 0.10 mg/L 0.521 0.041 U 109 90-110 Matrix Spike Dup (1D23015-MSDi) Prepared: 04/21/2021 10:00 Analyzed: 04/21/2021 13:54 Source: CE04807-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.58 0.10 mg/L 0.521 0.041 U 112 90-110 2 10 QM-07 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch ID19039 - EPA 5030E MS Blank (1D39039-BLK3) Prepared: 04/19/2021 13:46 Analyzed: 04/19/2021 23:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 91 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 1D19039 - EPA 5030B MS - Continued Blank (ID39039-BLK1) Continued Prepared: 04/19/2021 13:46 Analyzed: 04/19/2021 23:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 5.0 ug/L 5.00 101 75-125 LCS (1D19039-BS1) Prepared: 04/19/2021 13:46 Analyzed: 04/20/2021 09:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 28 2.0 ug/L 25.0 114 80-133 Toluene-d8 4.8 u91L 5.00 96 75-125 Matrix Spike (1D19039-MS1) Prepared: 04/19/2021 13:46 Analyzed: 04/19/2021 22:19 Source: AE03148-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 30 2.0 ug/L 25.0 3.9 104 80-133 Toluene-d8 5.4 u91L 5.00 108 75-125 Matrix Spike Dup (1D19039-MSD1) Prepared: 04/19/2021 13:46 Analyzed: 04/19/2021 22:44 Source: AE03148-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 30 2.0 ug/L 25.0 3.9 106 80-133 1 19 Toluene-d8 4.9 u91L 5.00 98 75-125 Batch ID20044 - EPA 5030E MS Blank (1D20044-BLK3) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 14:15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-d8 4.9 u91L 5.00 99 75-125 LCS (1D20044-BSI) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 13:21 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 99 80-133 Toluene-d8 4.9 u91L 5.00 98 75-125 Matrix Spike (1D20044-MS1) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 23:23 Source: CE04871-15 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 1.1 95 80-133 Toluene-d8 4.9 u91L 5.00 98 75-125 Matrix Spike Dup (11)20044-MSDI) Prepared: 04/20/2021 00:00 Analyzed: 04/20/2021 23:48 Source: CE04871-15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 1.1 96 80-133 0.7 19 Toluene-d8 5.2 u91L 5.00 104 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 92 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Chlorinated Herbicides by GC - Quality Control Batch ID29043 - EPA 3510C Blank (1D19043-BLK3) Prepared: 04/19/2021 15:30 Analyzed: 04/22/2021 15:20 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-T 0.28 U 0.50 ug/L 2,4,5-TP (Silvex) 0.44 U 0.50 ug/L 2,4-D 0.27 U 0.50 ug/L Dinoseb 0.32 U 0.50 ug/L Pentachlorophenol 0.19 U 0.50 ug/L 2, 4-DCAA 1.6 ug/L 2.00 80 37-134 LCS (11319043-BSI) Prepared: 04/19/2021 15:30 Analyzed: 04/22/2021 16:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 1.2 0.50 ug/L 2.00 61 24-135 2,4-D 1.1 0.50 ug/L 2.00 54 20-134 2,4-DC4A 1.6 ug/L 2.00 78 37-134 Matrix Spike (1D19043-MS3) Prepared: 04/19/2021 15:30 Analyzed: 04/22/2021 16:36 Source: AE03056-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 6.6 2.5 ug/L 10.0 2.2 U 66 24-135 2,4-D 7.0 2.5 ug/L 10.0 1.4 U 70 20-134 2,4-OCAA 6.7 U91L 10.0 87 37-134 Matrix Spike Dup (1D19043-MSDI) Prepared: 04/19/2021 15:30 Analyzed: 04/22/2021 17:02 Source: AE03056-01 Analvte 2,4,5-TP (Silvex) 2,4-D Result Flaq POL 5.0 2.5 4.7 2.5 Units ug/L ug/L Spike Source %REC Level Result %REC Limits RPD 10.0 2.2 U 50 24-135 27 10.0 1.4 U 47 20-134 39 RPD Limit Notes 19 QM-11 19 QM-11 2,4-DCAA 5.6 ug/L 10.0 56 37-134 Dissolved Gases by GC - Quality Control Batch IDIS045 - Same Blank (1D15045-BLK1) Prepared: 04/15/2021 14:45 Analyzed: 04/15/2021 16:51 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L LCS (11315045-BSI) Prepared: 04/15/2021 14:45 Analyzed: 04/15/2021 16:09 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 44.7 2.50 mg/L 45.8 98 70-130 Ethane 0.333 0.00600 mg/L 0.323 103 70-130 Ethene 0.323 0.00600 mg/L 0.302 107 70-130 Methane 0.181 0.00500 mg/L 0.172 105 70-130 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 93 of 98 QUALITY CONTROL DATA Dissolved Gases by GC - Quality Control Batch 1D15O45 - Same - Continued (� �Eo www.encolabs.com LCS Dup (1D15045-BSD3) Prepared: 04/15/2021 14:45 Analyzed: 04/15/2021 16:25 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 44.9 2.50 mg/L 45.8 98 70-130 0.4 30 Ethane 0.326 0.00600 mg/L 0.323 101 70-130 2 30 Ethene 0.320 0.00600 mg/L 0.302 106 70-130 0.9 30 Methane 0.180 0.00500 mg/L 0.172 105 70-130 0.6 30 Duplicate (111315045-DUP1) Prepared: 04/15/2021 14:45 Analyzed: 04/16/2021 08:04 Source: AE02928-16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 8.96 2.50 mg/L 25.8 97 30 QM-12 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.00400 U 0.00500 mg/L 0.00400 U 30 Batch ID16O17 - Same Blank (lD16017-BLK3) Prepared: 04/16/2021 08:00 Analyzed: 04/16/2021 10:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L LCS (1D16017-BS1) Prepared: 04/16/2021 08:00 Analyzed: 04/16/2021 09:55 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 45.2 2.50 mg/L 45.8 99 70-130 Ethane 0.331 0.00600 mg/L 0.323 103 70-130 Ethene 0.326 0.00600 mg/L 0.302 108 70-130 Methane 0.181 0.00500 mg/L 0.172 105 70-130 LCS Dup (1D16017-BSD1) Prepared: 04/16/2021 08:00 Analyzed: 04/16/2021 10:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 45.2 2.50 mg/L 45.8 99 70-130 0.2 30 Ethane 0.324 0.00600 mg/L 0.323 100 70-130 2 30 Ethene 0.321 0.00600 mg/L 0.302 106 70-130 2 30 Methane 0.178 0.00500 mg/L 0.172 103 70-130 1 30 Duplicate (1D16017-DUP1) Prepared: 04/16/2021 08:00 Analyzed: 04/16/2021 16:16 Source: AE03027-01RE3 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L 2.07 U 30 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.00400 U 0.00500 mg/L 0.00400 U 30 Classical Chemistry Parameters - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 94 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1D19007 - NO PREP Blank (1D39007-BLK3) Prepared: 04/19/2021 13:41 Analyzed: 04/20/2021 13:53 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 10 U 10 mg/L LCS (1D19007-BSI) Prepared: 04/19/2021 13:41 Analyzed: 04/20/2021 13:53 Analvte Total Dissolved Solids Result Flaq 100 POL 10 Units mg/L Spike Level 100 Source Result %REC %REC Limits RPD 102 90-110 RPD Limit Notes Duplicate (1D19007-DUP3) Prepared: 04/19/2021 13:41 Analyzed: 04/20/2021 13:53 Source: AE00466-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 20 10 mg/L 20 0 20 Batch 1D19049 - NO PREP Blank (1D39049-BLK3) Prepared: 04/20/2021 09:35 Analyzed: 04/22/2021 08:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 10 U 10 mg/L LCS (1D39049-BSI) Prepared: 04/20/2021 09:35 Analyzed: 04/22/2021 08:40 Analvte Total Dissolved Solids Result Flaq 100 POL 10 Units mg/L Spike Level 100 Source Result %REC %REC Limits RPD 100 90-110 RPD Limit Notes Duplicate (11319049-DUP3) Prepared: 04/20/2021 09:35 Analyzed: 04/22/2021 08:40 Source: AE02611-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 1400 10 mg/L 1400 0 20 Batch 1D19050 - NO PREP Blank (1D39050-BLK3) Prepared: 04/20/2021 12:00 Analyzed: 04/22/2021 08:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 10 U 10 mg/L LCS (1D19050-BSI) Prepared: 04/20/2021 12:00 Analyzed: 04/22/2021 08:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 96 10 mg/L 100 96 90-110 Duplicate (1D19050-DUP1) Prepared: 04/20/2021 12:00 Analyzed: 04/22/2021 08:42 Source: AE02056-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 710 10 mg/L 690 2 20 Batch ID20004 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 95 of 98 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch ID20004 - NO PREP - Continued Blank (1D20004-BLK1) Prepared: 04/20/2021 07:38 Analyzed: 04/20/2021 09:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.54 U 1.0 mg/L LCS (11320004-BS1) Prepared: 04/20/2021 07:38 Analyzed: 04/20/2021 09:23 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 53 1.0 mg/L 50.0 107 85-115 Matrix Spike (1D20004-MS3) Prepared: 04/20/2021 07:38 Analyzed: 04/20/2021 10:04 Source: AE02865-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 56 1.0 mg/L 50.0 2.2 108 85-115 Matrix Spike Dup (11320004-MS131) Prepared: 04/20/2021 07:38 Analyzed: 04/20/2021 10:28 Source: AE02865-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 56 1.0 mg/L 50.0 2.2 108 85-115 0.6 21 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 96 of 98 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. 3-04 Result may be biased high. Associated calibration verification standard exceeded the upper control limit. 1-05 Result may be biased low. Associated calibration verification standard did not meet the minimum control limit. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test). QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QM-12 Precision between duplicate samples was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 97 of 98 Z m > C_1 n v a C�1 Z C m m w Ci v w • V y w � m 70 O! m Im 4�mcoW W coCDCDv m �. W Q Q O O O L7 G m �n N r� i71 a r,. m K a g Z m w ~ c .« � cn ,n ;w 4% A1,14, i N V\ Vl W N $ r m m m ~3 4- � 4 P1 tG ro C JON FL ffi m •� p o r CO 80 3 t2F Clt CO CO m QO a o � n X X 8081 B Appendix 2 X X 8082AAppendix 2,8159AAppendix 2 @ W ° a j rR. X X x x x $ BMW AppeNIX1,82W m 2 EMW*Md,8260D SMIA ID i N o 82500 Appendbc 2,8280D n �+ X X N EldendsdM20OD SIIM ID fm6 o X X X X c 8260D,828pD Appendix 1,82$0D m X x 8270E Appendix 2 a m w i'C Sb,Se.$n TE,V,Zn x 4 C a a Ap,A%ELe,Be,Cd.Co,Ce,Cu.Fe,Mn,NI,Pb, 4 1 X X X X X X X X - Sb^TI,V,2n m AO,AM,B«,Be,CA,Co,C+,Cu,NI,Pb,Sb,Je, $RTI,V,In 3 DCD g X gg,As,Ba,Cd,Cr,Pb,Se G a n � 0 0 v � W o a o _ 1 m w m I a CCD m d frl C 3 `I a o ro a ID g` 3 C N 3 c CD9- Q y -4 c m (U Q s a v '� y i CL 2 a o D- v LID �0om V F Z i. en 0 m 0 a Z m Z n 0 O Z m r Z N IiL D Po N m O o s m w ro 0 m U) CS K 3 m_ n a [l x 3 � m n3 m z X N `i/ En. ~ m 3 m O " N W CZ 6 q N IA CL m m �` Cy _ m � _{] a p W I#i m K Z e 3 z n A o FI'Ico � pp m � to m v w o N CD L OD q N � � O w m y p �{ F O in w o a a. M m j�Q�t m Dam W z C,2 [cN(-� a Q z FL o MA 3 m ti)W m Jl• Y' m� _ m m m ^ W w m m a O 9 a 8 x. x CD N � 5w �a T m 0 .0. to o �. a m g a = a A 0 8081 B Appendix 2 5 d 8082AAppsndixZSifiIAAppendbc2 ,bT m m o m m n ,—j :38280D Appenft 1,82eW cExhnX*d,826W SIN iD _ y o 82$00 AppeNtm 2,826M ' 0 6 E�mended,82000 W ID z m 82®QD,811*1 Appendlx 4,8280D 6 0 m, X X X ExbendedA280D SIN ID K a Appendix 2 8270E m 0 N Aa,As,de,Ba,Cd,Ca,Cr,Cu,Fa,Mn,N1,Pb, of Sb,S,,SA,TI,V zr, i6 = AeAs,BY,Be,Gd,Co.Cr.Cu.FeMn,NI.Pb, x o X Sb,S%TI,V,2n a m o AQ,A aa,Be,Cd,CO.Cr,Cu Nk,Pb,$b.Se, a' X So,T1,V,Zn 3 x X Ag,As,Ba,Cd,Cr,Pb,5e m �m Q-EV CD m O C o C° w m go m m _ CD cN 2L m CDm 3 3 m w 3 m o00 — m X � m 1 C _ g N C c 61 (D N ri, sn CD Q_, qaq Q p d s v 3 s = Q R o � z o. N O m w m 0 A Z A 3 �m z a 0 0 z N m G m5� oW=.o 8 r W z CP O A O fn M vu > o m N IN J fD o_ w cr Vti A 0 9 Sample Preservation Verification ENCO Cary Work Order: CE04871 Project: Moore County Active C & D LP - Spring Client: S&ME, Inc. (SM004) Project #: 4358-20-043A Phase 01 Logged In: 13-Apr-21 16:34 Logged By: Rachel Xn oni�h Preservation Check Performed By: Dateffirn \'�. C E04871-01 Cont Type Pres (pH) Requirement pH Checked I In Control pH Adjusted Date�me Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y '/ N I NA Y 1 N NA C 250mLP+ZnAc+NaOH >9 Y N I NA Y N NA D — --T 250mLP+H2SO4 <2 Y V N I NA YIN NA I C E 04871-02 Cont Type Pres (pH) Requirement pH Checked 1 In Control pH Adjusted DatelTime Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y I N! NA Y N I NA C 250mLP+ZnAc+NaOH >9 Y/ N/ NA Y I N I NA rD 250mLP+H2SO4 <2 Y / N I NA Y ! / NA C F 04871-03 Cant Type yp Pres (pH) Requirement pH Checked / In Control pH Adjusted Date[Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y/ N/ NA Y VNj NA C 250mLP+ZnAc+NaOH >9 Y N I NA Y NA D 250mLP+H2SO4 <2 Y N I NA Y N/ NA C E 04871-04 Cont Type Pres (pH) pH Checked 1 Date/Time pH Adjusted Reagent Used/Comments Requirement In Control Adjusted B 250mLP+HNO3 <2 Y I N I NA Y N NA C 250mLP+ZnAc+NaOH >9 Y! N I NA Y N NA C E04871-05 Cont Type Pres (pH) pH Checked / pH Adjusted Date�me Reagent Used/Comments Requirement In Control Adjusted B 250mLP+HNO3 <2 YJ I N 1 NA Y N '/ NA C 250mLP+ZnAc+NaOH >9 Y�r N I NA Y/ N NA C F04871-0C, Cont Type Pres (pH) pH Checked 1 pH Adjusted Date/Time Reagent Used/Comments Requirement In Control Adjusted B 250mLP+HNO3 <2 / N I NA Y 1 NA C 250mLP+ZnAc+NaOH >9 Y / N / NA Y / / NA CAelmntlPrintlwko_Preservation Check. rpt Page 1 of 3 Sample Preservation Verification ENCO Cary Work Order: CE04871 Client: S&ME, Inc. (SM004) ENCO Project: Moore County Active C & D LF - Spring Project #: 4358-20-043A Phase 01 Logged In: 13-Apr-21 16:34 Logged By: Rachel Ann oni �7 �} Preservation Check Performed By: Date/Time. V� 1 1 C E04871-07 Cont yp Type Pres (PH) Requirement pH Checked I In Control pH Adjusted Date/Ttme Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y) I N/ NA Y N 1 NA C 250mLP+ZnAc+NaOH >9 Y N/ NA Y N/ NA C F 04871-08 Cont Type yp Pres (PH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y I N/ NA Y N NA C 250mLP+ZnAc+NaOH >9 Y/ N/ NA Y N NA C E04871-09 Cont Type Pres (PH) Requirement pH Checked I In Control PH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 J Y/ N I NA Y / NA C 250mLP+ZnAc+NaOH >9 YIN / NA Y N NA CE04871-10 Cont Type Pres (PH) Requirement PH Checked 1 In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments C 250mLA (PEST) Pest pH 5-9 Y I N/ NA Y fNj NA G 250mLP+HNO3 <2 Y / N / NA Y N / NA H 250mLP+NaOH >12 Y I N/ NA Y I UNI NA I 250mLP+ZnAc+NaOH >9 Y N I NA I YIN / NA C E 04871-11 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments C 250mLA (PEST) Pest pH 5-9 Y' I N I NA Y I N/ NA G 250mLP+HNO3 <2 Y / N / NA Y / NA H 250mLP+NaOH >12 Y I N/ NA Y/ N/ NA ! 250mLP+ZnAc+NaOH >9 I IDN I NA YIN / NA CE04871-12 Cont Type Pres (pH) Requirement pH Checked 1 In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 V—)1 N / NA Y �JN / NA C:lelmntlPrintlwko_PreservationCheck.rpt Page 2 of 3 Sample Preservation Verification ENCo Cary Work Order: CE04871 Client: S&ME, Inc. (SM004) Project: Moore County Active C & D LF - Spring Project #: 4358-20-043A Phase 01 Logged In: 13-Apr-21 16:34 Logged By: Rachel Ann Y nis Preservation Check Performed By: Date/Time: %2) C E 04871-13 Gant Type Pres (pH) pH Checked I Requirement In Control pH Adjusted DateMme Adjusted Reagent UsedlComments A 250mLP+HNO3 <2 Y 1 N/ NA Y 1 N/ NA CE04871-14 Conk Type Pres (pH) pH Checked I pH Adjusted Date(Time Reagent Used/Comments Requirement In Control Adjusted A 25{ImLP+HNO3 <2 Y I N I NA Y I N NA C E04871-16 Cont Type Pres (pH) pH Checked 1 pH Adjusted DatelTime Reagent Used/Comments Requirement In Control Adjusted A 250mLP+HNO3 <2 Y/ N I NA Y 1 N 1 NA C E04871-16 Cont Type Pres (pH) pH Checked / PH Adjusted Date/Time Reagent Used/Comments Requirement In Control Adjusted 6 25omLP+HNO3 r? ` Y ! N / NAFY ! N / NAC 250mLP+ZnAc+NaOH >9 Y I N I NAIN NA Rea ent Name ID 1 2 pH Strip ID' PH Strips COF0555 Rea ent Name ID 3 4 Rea ent Name ID 5 6 C:lelmntlPrin1kWK0_Nreservation Check. rpt Page 3 of 3 Appendix III — Historical Analytical Results TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A SCuent/Parameter Units Am Antimony ug/L 06/20/18 0.74 2 NC21- IMAC = 1 ug/L ug/L 11/27/18 0.74 2 EPA MCL = 6 ug/L ug/L 04/02/19 0.74 2 ug/L 11/19/19 0.74 2 ug/L 04/07/20 0.74 2 ug/L 10/13/20 0.74 2 ug/L 04/13/21 0.74 2 -- -- MW-JJJP��� ND ND ND ND ND ND ND ND NO NO NO NO NO NO ND ND NO NO Active :D Monitoring MW-14 ND ND ND ND ND ND ND Wells MW-17S -- -- NO NO NO NO MW-17D -- -- ND ND ND ND MW-18 -- -- ND ND ND MW-1 9 -- -- ND ND MW-4 maw-M11SAWD ND NO NO NO NO NO NO ND ND ND ND ND ND ND -- -- NS MW-2 -- -- NS Closed MSW Monitoring MW-3 -- -- NS Wells MW-6 ND -- ANR & MNA Performance Aamw-, ND -- ANR Monitoring -- -- ANR Wells m�W -- -- ANR -- -- ANR -- -- NS Arsenic ug/L 03/05/90 -- -- NO ND ND NO ND ND NC 2L = 10 ug/L ug/L 03/21/91 ND NO ND ND NO NO EPA MCL = 10 ug/L ug/L 03/10/92 ND NO ND ND NO NO ug/L 04/20/95 ND ND ND ND NO NO ug/L 06/27/95 NO ug/L 09/22/95 ND ND ND ND ND NO NO ug/L 03/28/96 ND ND ND ND ND ND NO NO ug/L 10/29/96 ND ND ND ND ND NO ND NO ug/L 04/08/97 ND ND ND ND ND NO ND NO ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/30/98 ND ND ND ND ND NO ND NO ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 10/21/99 ND ND ND 18 ND NO ND NO ug/L 03/14/00 -- NO ug/L 04/19/00 ND ND ND ND ND NO ND NO ug/L 10/17/00 ND ND ND ND ND NO ND NO ug/L 04/10/01 ND ND ND ND ND NO ND NO ug/L 10/11/01 ND ND ND ND ND NO ND ND ug/L 04/18/02 ND ND ND ND ND NO ND ND ug/L 10/08/02 -- -- -- ND -- 11 -- -- -- -- -- -- -- -- -- 19 ND ND 10 ND ND ug/L 04/09/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- 11 ND ND NO 10 ND ug/L 10/13/03 ND ND 14 17 14 14 11 ND ug/L 04/26/04 ND ND ND ND ND NO 12 ND ug/L 10/25/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- 15 ND ND NO 14 ND ug/L 04/04/05 -- -- -- 10 -- 10 -- -- -- -- -- -- -- -- -- 10 15 10 29 10 ND ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- 13 15 12 21 ND ND ug/L 04/28/06 ND 11 NO NO ND NO 12 ND ND 11 16 ND ug/L 10/09/06 ND 13 NO NO ND NO 14 ND ND NO 11 ND ug/L 04/24/07 ND ND NO NO ND NO ND ND ND 38 27 ND ug/L 10/30/07 10 ND ND NO NO ND NO 3.2 J ND ND 6.9 J 7.8 J ND ug/L 04/23/08 10 ND ND NO 3.2 J ND NO ND ND ND NO 2.3 J ND ug/L 10/06/08 10 ND ND NO NO ND NO ND ND ND NO 7.7 J ND ug/L 04/13/09 10 ND 5.1 J NO NO ND NO 8.2 J 17.1 6.6 J 11.4 10.1 J ND ug/L 10/15/09 10 5.30 J 6.47 J 5.54 J 6.53 J 2.86 J NO 8.63 J 18.3 11.6 15.9 12.6 ND ug/L 04/26/10 10 ND 10.8 NO 3.14 J ND 3.50 J 14.2 31.0 8.54 J 13.4 28.5 ND ug/L 10/19/10 10 5.16 J 24.9 NO NO ND NO 29.5 33.0 22.6 28.0 26.6 ND ug/L 04/18/11 10 ND 20.0 NO 3.29 B ND 5.35 B 18.7 14.6 B 16.1 B 19.2 14.6 B 5.39 B ug/L 10/10/11 10 ND ND NO NO ND 2.96 J 5.48 J 4.73 J 5.67 J 19.0 Dry 5.26 J ug/L 04/17/12 10 4.42 B ND NO NO 4.31 B 3.32 B ND 29.4 ND 17.9 B Dry NO ug/L 10/09/12 10 ND 6.36 J NO 2.90 J ND 2.91 J 9.82 J 21.6 9.74 J 10.7 Dry NO ug/L 04/15/13 10 3.97 B ND 5.21 B 2.87 B ND 4.42 B 17.8 NO ND 14.7 B Dry NO ug/L 09/30/13 10 ND 9.62 J NO NO ND NO 24.5 32.0 20.3 18.0 Dry ND ug/L 04/16/14 10 ND 8.25 J NO NO ND NO 23.3 19.7 15.2 19.5 Dry ND ug/L 10/15/14 5.4 10 Dry ND NO NO ND NO 6.99 J 10.8 14.1 38.6 Dry ND ug/L 04/15/15 5.4 -- 10 ND -- NO -- -- -- -- NO -- ND ND NO 20.3 21.8 ND 8.41 J Dry ND ug/L 10/07/15 5.4 10 ND ND NO ND ND NO ND 20.0 ND 32.4 8.73 J ND ug/L 04/11/16 5.4 -- 10 ND -- NO -- -- -- -- NO -- ND ND NO 12.6 27.0 11.3 38.7 29.6 ND ug/L 11/30/16 6.8 10 ND 48.1 (ND) NO ND ND NO 65.8 (ND) 20.4 (ND) 14.9 (ND) 85.6 (41.9) 39.6 (42.4) ND (Dissolved) ug/L 11/30/16 6.8 10 (Verification Event) ug/L 02/09/17 6.8 -- 10 ND -- -- -- -- -- -- -- -- -- -- -- -- -- -- 40.5 -- (Dissolved) ug/L 02/09/17 6.8 10 -- -- -- 39.0 ug/L 04/11/17 6.8 -- 10 ND -- 7.78 J -- -- -- -- NO -- NO ND NO 10.5 8.67 J ND 53.7 31.8 ND ug/L 12/12/17 6.8 -- 10 ND -- 19.3 -- -- -- -- NO -- NO ND NO 25.9 21.5 8.49 J 53.2 25.4 ND ug/L 06/20/18 7.6 -- 10 ND NO 22.7 -- -- -- -- NO ND NO ND NO 22.8 ND ND 38.6 ND -- ug/L 11/27/18 7.6 10 -- ND NO ND -- -- -- -- NO ND NO ND NO ND 14.9 ND 38.4 ND ND ug/L 04/02/19 7.6 10 -- ND NO ND -- -- -- -- NO ND ND ND NO ND 11.7 ND ND ND ND ug/L 11/19/19 7.6 10 -- ND NO ND NO ND -- -- NO ND ND ND NO ND ND ND 36.5 ND ND ug/L 04/07/20 7.6 10 -- ND NO ND NO ND ND -- NO ND -- -- -- ND ND ND 23.8 ND -- ug/L 10/13/20 7.6 10 -- ND NO ND NO ND NO ND NO ND NO ND ND ND NO ND NO ND 64.8 ND -- ug/L 04/13/21 7.6 10 -- ND NO ND NO ND NO ND NO ND ND ND NS NS NS ND NO ND ND ND NS Z:\Sh,re\SME\Ops\ENV,,]d 030Y35&O0 3AMo Co My ReuOne LFGBWGMon,g\Teek01-Semi-Annual Wale,OualityF2020-2021\WOAIng_Docu-Spbng2021 Even02020-10WOMRTabI-App-,.- Page 1 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Sa Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells ��Kjl Detected Monitoring Constituent/Parameter Barium Units ug/L a 03/05/90 PWO PQL SWSL MW-5 �3b MW-14 MW-11 7S MW-17D W-4 15 MW -11SR 57 MW-2 27 MW-3 13 MW-6 MW-7 MW-8 MW-9�! PW-I NC 2L = 700 ug/L ug/L 03/21/91 35 23 73 66 23 ND EPA IVICL = 2000 ug/L ug/L 03/10/92 30 23 43 69 12 ND ug/L 04/20195 ND -- -- -- -- NO ND NO NO ND ug/L 06/27/95 ND ug/L 09/22/95 ND ND ND ND ND NO ND ug/L 03/28196 ND ND ND NO ND NO NO ND ug/L 10/29/96 ND ND ND ND ND NO ND ND ug/L 04/08197 ND ND NO ND NO NO ND ND ug/L 10/29197 ND ND NO ND ND NO ND ND ug/L 04/30/98 ND ND ND ND ND NO ND ND ug/L 10/14198 ND ND NO ND ND NO ND ND ug/L 04/27199 ND ND NO ND ND NO ND ND ug/L 10/21/99 ND ND ND ND ND NO ND ND ug/L 03/14100 ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 ND ND ND ND ND NO ND ND ug/L 04/10/01 ND ND NO ND NO NO ND ND ug/L 10/11/01 ND ND ND ND ND NO ND ND ug/L 04/18/02 ND ND ND ND ND NO ND ND ug/L 10/08/02 ND ND NO ND NO NO ND ND ug/L 04/09/03 ND ND ND ND ND NO ND ND ug/L 10/13/03 ND ND NO ND NO NO ND ND ug/L 04/26104 ND ND NO ND ND NO ND ND ug/L 10/25/04 ND ND ND ND ND NO ND ND ug/L 04/04105 ND ND NO ND ND NO ND ND ug/L 10/04105 ND ND NO ND ND NO ND ND ug/L 04/28/06 ND ND ND NO ND NO ND ND ND NO ND ND ug/L 10/09106 ND ND NO NO NO NO NO ND NO NO ND ND ug/L 04/24/07 ND ND NO NO ND NO ND NO ND NO ND ND ug/L 10/30/07 100 13.5 J 44.4 J 52.8 J 46.6 J 65.8 J 13.8 J 40.1 J 17.0 J 60.3 J 80.2 J 15.5 J 14.6 J ug/L 04/23108 100 11.9 J 42.6 J 31.7 J 57.1 J 55.4 J 12.1 J 59.5 J 26.8 J 52.1 J 81.1 J 12.3 J 14.8 J ug/L 10/06/08 100 12.8 J 45.7 J 41.8 J 40.9 J 58.8 J 13.8 J 42.0 J 31.2 J 51.4 J 83.1 J 12.4 J 15.6 J ug/L 04/13109 100 11.5 J 51.3 J 56.0 J 49.5 J 65.8 J 17.2 J 42.6 J 36.7 J 81.6 J 89.8 J 14.9 J 14.5 J ug/L 10/15109 100 13.7 J 44.7 J 72.6 J 28.6 J 66.7 J 19.1 J 40.0 J 33.9 J 67.5 J 78.6 J 20.8 J 14.5 J ug/L 04/26/10 100 9.47 J 49.9 J 54.7 J 43.3 J 66.0 J 19.8 J 39.8 J 33.4 J 67.2 J 80.3 J 11.7 J 14.8 J ug/L 10/19/10 100 16.6 J 42.4 J 29.5 J 31.4 J 52.6 J 14.9 J 29.5 J 25.2 J 53.9 J 69.7 J 13.6 J 11.8 J ug/L 04/18/11 100 13.1 J 48.1 J 41.9 J 48.8 J 64.8 J 21.4 J 40.2 J 28.2 J 70.3 J 81.9 J 17.5 J 15.4 J ug/L 10/10/11 100 14.3 J 47.5 J 71.2 J 46.1 J 66.7 J 22.0 J 39.9 J 30.1 J 71.7 J 74.7 J Dry 15.5 J ug/L 04/17/12 100 19.5 J 52.1 J 40.5 J 62.7 J 75.0 J 21.7 J 39.8 J 30.1 J 67.5 J 84.9 J Dry 15.5 J ug/L 10/09/12 100 15.4 J 54.3 J 10.1 J 52.0 J 68.1 J 18.8 J 39.5 J 39.7 J 64.2 J 73.0 J Dry 14.7 J ug/L 04/15/13 100 14.6 J 49.4 J 26.8 J 40.5 J 60.8 J 20.4 J 42.7 J 36.7 J 78.4 J 86.4 J Dry 14.6 J ug/L 09/30/13 100 12.4 J 56.5 J 24.5 J 35.8 J 38.3 J 21.1 J 50.5 J 47.1 J 65.3 J 90.1 J Dry 14.9 J ug/L 04/16/14 100 13.6 J 47.3 J 15.9 J 35.3 J 41.8 J 15.2 J 42.6 J 28.9 J 60.6 J 102 Dry 16.2 J ug/L 10/15/14 1 100 Dry 50.4 J 25.9 J 33.6 J 46.3 J 25.5 J 49.3 J 31.1 J 103 98.4 J Dry 23.1 J ug/L 04/15/15 1 100 15.6 J 49.2 J 95.6 J 46.6 J 53.3 J 32.9 J 45.0 J 28.4 J 74.7 J 93.7 J Dry 18.2 J ug/L 10/07/15 1 100 14.7 J 45.8 J 21.2 J 30.4 J 52.1 J 25.2 J 36.6 J 28.6 J 88.8 J 92.8 J 12.6 J 15.8 J ug/L 04/11/16 1 100 13.7 J 41.5 J 69.3 J 31.9 J 38.8 J 34.0 J 44.4 J 28.6 J 65.5 J 84.0 J 8.38 J 18.5 J ug/L 11/30/16 1 100 14.4 B 36.7 B 38.3 B 28.6 B 38.2 B 30.0 B 44.5 J 24.2 B 75.1 J 84.2 J 8.70 B 17.8 B ug/L 04/11/17 1 100 14.5 J 45.3 J 28.5 J 29.9 J 54.5 J 32.6 J 45.0 J 26.6 J 99.7 J 106 9.34 J 18.6 J ug/L 12/12/17 1 100 12.9 J 43.5 J 35.6 J 34.8 J 55.6 J 36.8 J 47.9 J 28.6 J 77.3 J 98.2 J 14.5 J 18.7 J ug/L 06/20/18 1.1 -- 100 11.7 J 58.2 J 39.8 J 40.3 J 59.9 J 26.7 J 57.0 J 31.8 J 42.7 J 33.3 J 76.3 J 89.3 J 38.6 J -- ug/L 11/27/18 1.1 10 -- 13.9 53.1 40.4 60.4 68.4 30.5 38.7 31.9 38.9 39.2 50.5 78.8 32.3 20.2 ug/L 04/02/19 1.1 10 15.4 49.0 37.8 54.9 98.0 30.4 38.3 33.5 37.8 40.8 54.2 78.4 38.9 20.8 ug/L 11/19/19 1.1 10 14.5 59.3 56.9 68.3 16.5 -- 53.9 71.2 37.8 54.9 38.5 52.7 38.3 102 117 19.8 20.7 ug/L 04/07/20 1.1 10 12.8 54.7 42.2 91.8 10.6 86.7 -- 43.0 69.3 -- -- -- 42.9 25.7 69 83 40.0 -- ug/L 10/13/20 1.1 10 15.4 52.7 19.1 44.0 44.6 87.9 33.4 83.8 59.5 25.9 72.8 26.7 34.7 33.9 41.0 34.4 75.6 95.5 27.5 19.0 ug/L 04/13/21 1.1 10 32.7 55.0 22 48.3 18.2 136.0 22.4 89.5 103 103.0 89.0 NS NS NS 46.0 38.4 66.6 78.2 25.0 NS Z:\Sh,re\SME\Op,\ENV r,jed 020Y35&O3A - Co M R-, LFG & WQ M-g\-k 01 - S-- ... I - Q,,Ilty F 2020-2021 W-Iffig --- Spd,g -1 -020-10 WQMR T,- For App-,.- Page 2 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active :D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells ��Kjl WDetected Monitoring n.t'ituent/Parameter Cadmium Units ug/L apdo 5 -- PQL -- SWSL --ND-- -- -- -- -- -- ND -- ND ND ND -- -- -- -- -- ND NC 2L = 2 ug/L ug/L 03/21/91 -- -- -- ND -- -- -- -- -- -- ND -- ND ND ND -- -- -- -- -- ND EPA MCL = 5 ug/L ug/L 03/10/92 ND ND ND ND ND ND ug/L 04/20/95 -- -- -- ND -- -- -- -- -- -- -- -- -- -- -- ND ND NO NO -- ND ug/L 06/27/95 ND ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- -- ND ND ND NO -- ND ug/L 03/28/96 -- -- -- ND -- -- -- -- -- -- -- -- ND ND -- ND ND NO NO -- ND ug/L 10/29/96 ND ND ND ND ND NO ND ND ug/L 04/08/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/30/98 ND ND ND ND ND NO ND ND ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/21/99 ND ND ND ND ND NO ND ND ug/L 03/14/00 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/18/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/09/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/13/03 -- -- -- 2 -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/26/04 -- -- -- 1 -- ND -- -- -- -- -- -- -- -- -- 1 ND ND NO ND ND ug/L 10/25/04 1 ND ND ND ND NO ND ND ug/L 04/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/28/06 -- -- -- ND -- ND -- -- -- -- ND -- ND ND NO ND 1 ND 1 2 ND ug/L 10/09/06 -- -- -- ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 04/24/07 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/30/07 -- -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 04/23/08 -- -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 10/06/08 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/15/09 -- -- 1 ND -- ND -- -- -- -- NO -- ND ND 0.487 J ND ND ND NO ND ND ug/L 04/26/10 -- -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 10/19/10 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/18/11 -- -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 10/10/11 -- -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND 0.685 J ND NO Dry ND ug/L 04/17/12 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/09/12 -- -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO Dry ND ug/L 04/15/13 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 09/30/13 1 ND ND NO ND ND NO 1.15 0.722 J ND NO Dry ND ug/L 04/16/14 -- -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO Dry ND ug/L 10/15/14 0.36 1 Dry ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/15 0.36 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/07/15 0.36 -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 04/11/16 0.36 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 11/30/16 0.36 -- 1 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 04/11/17 0.36 -- 1 ND -- ND -- -- -- -- NO -- ND ND NO 0.585 J ND ND 0.696 J ND ND ug/L 12/12/17 0.36 1 ND -- ND NO ND ND NO ND ND 0.734 J NO ND 0.371 J ug/L 06/20/18 0.36 -- 1 ND 0.500 B ND -- -- -- -- NO ND ND ND NO ND ND ND NO ND -- ug/L 11/27/18 0.36 1 -- ND NO ND -- -- -- -- NO ND ND ND NO ND ND ND NO ND ND ug/L 04/02/19 0.36 1 ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 11/19/19 0.36 1 -- ND NO 0.409 J ND ND -- -- NO ND ND ND NO ND ND ND NO ND ND ug/L 04/07/20 0.36 1 ND NO ND ND ND ND NO ND ND ND ND NO ND ug/L 10/13/20 0.36 1 ND 1.09 1.03 NO 1.93 ND ND 1.26 ND NO 1.11 ND ND NO 2.16 1.57 1.67 0.662 J 1.92 ug/L 04/13/21 0.36 1 -- ND 0.526 J 0.572 J NO NO ND ND 0.811 J ND ND ND NS NS NS 1.04 1.25 0.612 J NO 0.855 JI NS Z:\Sh,re\SME\Ops\ENV rojed 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waler Qualgy F 2020-2021\W-Ing_Dx-- Spring 2021 Even02020-10 WOMR Tables For App—,.— Page 3of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active :D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells ��Kjl & Detected Monitoring Chromium ug/L 5 -- PQL -- SWSL --ND-- -- -- -- -- -- ND -- ND ND ND -- -- -- -- -- ND NC 2L = 10 ug/L ug/L 03/21/91 -- -- -- ND -- -- -- -- -- -- ND -- ND 12 10 -- -- -- -- -- ND EPA MCL = 100 ug/L ug/L 03/10/92 ND ND ND ND ND -- -- ND ug/L 04/20/95 -- -- -- ND -- -- -- -- -- -- -- -- -- -- -- ND ND 12 7 -- ND ug/L 06/27/95 -- -- ND ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- -- ND ND ND NO -- ND ug/L 03/28/96 -- -- -- ND -- -- -- -- -- -- -- -- ND ND -- ND ND NO NO -- ND ug/L 10/29/96 ND ND ND ND ND NO ND ND ug/L 04/08/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/30/98 ND ND ND ND ND NO ND ND ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/21/99 ND ND ND ND ND NO ND ND ug/L 03/14/00 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/18/02 ND ND ND ND ND NO ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/09/03 20 ND ND ND ND 11 ND ND ug/L 10/13/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/26/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND 19 ND ND ug/L 10/25/04 ND ND ND ND ND NO ND ND ug/L 04/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/28/06 -- -- -- ND -- ND -- -- -- -- ND -- ND ND NO ND ND ND NO ND ND ug/L 10/09/06 -- -- -- ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 04/24/07 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/30/07 10 ND ND 2.4 J ND ND NO ND ND ND NO ND 2.8 J ug/L 04/23/08 -- -- 10 ND -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 10/06/08 10 ND ND NO ND ND NO ND ND ND NO ND NO ug/L 04/13/09 -- -- 10 ND -- ND -- -- -- -- NO -- ND ND NO ND 1.1 J ND NO ND ND ug/L 10/15/09 -- -- 10 ND -- ND -- -- -- -- NO -- ND ND 1.02 J ND ND ND NO ND ND ug/L 04/26/10 10 ND ND NO ND ND NO ND ND ND NO ND NO ug/L 10/19/10 -- -- 10 5.84 J -- ND -- -- -- -- 3.07 J -- NO ND NO ND ND ND NO ND NO ug/L 04/18/11 -- -- 10 ND -- ND -- -- -- -- 1.02 J -- 1.90 J ND NO ND ND ND NO ND NO ug/L 10/10/11 10 ND ND NO NO ND NO ND ND ND NO Dry NO ug/L 04/17/12 -- -- 10 3.10 J -- ND -- -- -- -- NO -- NO ND NO ND ND NO 2.25 J Dry ND ug/L 10/09/12 10 1.65 J ND 3.37 J ND ND NO ND ND ND NO Dry NO ug/L 04/15/13 10 ND ND NO ND ND NO 2.64 B ND ND NO Dry NO ug/L 09/30/13 -- -- 10 ND -- ND -- -- -- -- 2.25 J -- ND ND NO ND ND NO NO Dry ND ug/L 04/16/14 10 ND ND 1.88 J NO ND NO ND ND ND NO Dry NO ug/L 10/15/14 1.4 10 Dry ND 5.71 J 1.83 J ND NO ND ND ND NO Dry NO ug/L 04/15/15 1.4 -- 10 ND -- ND -- -- -- -- NO -- NO ND 1.64 J ND ND NO NO Dry ND ug/L 10/07/15 1.4 10 ND ND 2.97 J ND ND NO ND ND ND NO ND NO ug/L 04/11/16 1.4 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO ND ND NO NO 4.36 J ND ug/L 11/30/16 1.4 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO ND ND NO NO 1.42 J ND ug/L 04/11/17 1.4 10 ND ND 2.22 J ND ND NO ND ND ND NO ND NO ug/L 12/12/17 1.4 -- 10 ND -- ND -- -- -- -- 1.88 J -- ND ND NO ND ND NO NO NO ND ug/L 06/20/18 1.4 -- 10 ND NO ND -- -- -- -- 1.55 J ND ND ND NO ND ND NO NO ND -- ug/L 11/27/18 1.4 10 -- ND NO ND NO ND ND ND NO ND ND ND NO ND NO ug/L 04/02/19 1.4 10 -- ND NO ND -- -- -- -- NO ND ND ND NO ND ND NO NO ND ND ug/L 11/19/19 1.4 10 ND NO ND NO ND NO ND ND ND NO ND ND ND NO ND NO ug/L 04/07/20 1.4 10 ND NO ND NO ND NO 3.46 J 3.68 J ND ND ND NO ND ug/L 10/13/20 1.4 10 ND NO ND NO ND NO 1.59 J NO ND NO ND ND ND NO ND ND ND NO ND ug/L 1 04/13/21 1 1.4 10 -- ND NO NO ND ND NO NO NO ND NO ND NS NS NS ND ND ND NO ND NS Z:\Sharetl\SME\Ops\ENV r,j s\2030Y35&O0 3A Moore Co My ROWne LFG& WQ Monkaing\Task 01-S--Annual Waled Quality F 2020-2021\W-Ing_Dx--Sphng 2021 Even02020-10 WOMR Tables Fob App-,.- Page 4 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A &Det.etcted Monitoring n ituent/Parameter Cobalt NC 2L IMAC = 1 ug/L Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L API 06/20/18 11/27/18 04/02/19 11/19/19 04/07/20 10/13/20 04/13/21 1.4 1.4 1.4 1.4 1.4 1.4 1.4 PQL -- 10 10 10 10 10 10 SWSL 10 -- -- -- -- -- MW-JI1111r� ND ND ND ND ND ND ND 2.13 2.03 2.55 ND ND 1.49 1.63 J J J J J ND ND 1.51 1.43 Active :D Monitoring MW-14 ND ND ND ND 1.50 J J J ND Wells MW-17S -- -- ND ND ND ND MW-17D -- -- ND ND 1.48 J ND IMME&W-4 -- -- -- ND ND ND -- -- -- -- ND ND ND NO NO NO NO NO NO MW-A"SANO ND ND 1.63 J ND ND ND ND -- -- -- -- -- NS Closed MW-2 -- -- -- -- -- NS MSW Monitoring MW-3 -- -- -- -- -- NS Wells & MW-6 ND -- -- -- -- ANR MNA Performance A. ND -- -- -- -- ANR Monitoring aw. 8 -- -- -- -- -- ANR Wells -- -- -- -- -- ANR �W -- -- -- -- -- ANR -- -- -- -- -- NS Copper ug/L -- -- --ND -- -- -- -- -- -- ND -- 10 NO NO -- -- -- -- -- NO NC 2L=1000 ug/L ug/L 03/21/91 -- -- -- ND -- -- -- -- -- -- NO -- 14 12 NO -- -- -- -- -- NO EPA MCL = 1300 ug/L ug/L 03/10/92 -- -- -- ND -- -- -- -- -- -- NO -- ND 110 NO -- -- -- -- -- NO ug/L 04/20/95 ND -- ND ND 14 11 NO ug/L 06/27/95 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- NO ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- -- ND ND NO NO -- NO ug/L 03/28/96 ND ND NO ND ND ND NO NO ug/L 10/29/96 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/08/97 ND ND ND ND ND NO ND NO ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/30/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/27/99 ND ND ND ND ND NO ND NO ug/L 10/21/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 03/14/00 NO ug/L 04/19/00 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 10/17/00 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/10/01 ND ND ND ND ND NO ND NO ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND NO ug/L 04/18/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND NO ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/09/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/13/03 ND ND ND ND ND NO ND NO ug/L 04/26/04 ND ND ND ND ND NO ND NO ug/L 10/25/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/04/05 ND ND ND ND ND NO ND NO ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/30/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/23/08 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 1.6 -- 10 2.28 B NO ND -- -- -- -- 5.70 B ND -- -- -- ND ND -- -- -- -- ug/L 11/27/18 1.6 10 -- ND NO ND 3.17 B ND ug/L 04/02/19 1.6 10 ND NO ND -- 3.37 J ND ug/L 11/19/19 1.6 10 -- ND NO ND NO 2.96 J -- -- 1.76 J ND -- -- -- -- -- -- -- -- -- ug/L 04/07/20 1.6 10 ND NO ND NO ND NO -- 1.75 J ND ug/L 10/13/20 1.6 10 ND NO ND NO 3.26 J NO 2.97 J 1.99 2.03 J 3.81 J ND ug/L 04/13/21 1.6 10 -- ND NO 1.97 J NO 3.37 J NO ND NO ND NO ND NS NS NS ANR ANR ANR ANR ANR NS Z:\Sh,re\SME\Ops\ENV rojed 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waler Qualgy F 2020-2021\W-Ing_Dx--Spring-1Even02020-10 WOMR Tables For App-,.- Page 5 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Sa Active :D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter Lead Units ug/L a 5 PWO -- PQL -- SWSL -- MW-J����� 16 -- MW-14 -- MW-11 7S -- MW-17D ���IW-4 -- -- -- 14 MW-11SR -- MW-1 7 MW-2 29 MW-3 6 MW-6 -- MW-7 -- MW-8 -- M�F_ -- -- PW 11 ND NC 2L = 15 ug/L ug/L 03/21/91 -- -- -- ND -- -- -- -- -- -- ND -- ND ND ND -- -- -- -- -- ND EPA MCL = 15 ug/L* ug/L 03/10/92 14 25 10 39 12 -- -- -- ND ug/L 04/20/95 -- -- -- ND -- -- -- -- -- -- -- -- -- -- -- 7 ND 18 16 -- ND ug/L 06/27/95 -- -- -- ND ug/L 09/22/95 ND ND ND ND ND NO ND ug/L 03/28/96 -- -- -- ND -- -- -- -- -- -- -- -- ND ND -- NO ND NO NO -- ND ug/L 10/29/96 ND ND ND ND ND NO ND 39 ug/L 04/08/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO ND NO NO ND 34 ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND 70 ug/L 04/30/98 ND ND ND ND ND NO ND 42 ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND 26 ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO 13 166 ug/L 10/21/99 ND ND ND ND ND NO ND 135 ug/L 03/14/00 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 ND ND ND ND ND NO ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO ND NO NO 10 14 ug/L 10/11/01 ND ND ND ND NO NO ND ND ug/L 04/18/02 ND ND ND ND ND NO ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND ND ug/L 04/09/03 10 ND ND 13 ND NO 19 ND ug/L 10/13/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND 11 ug/L 04/26/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND ND ug/L 10/25/04 ND ND ND ND ND NO ND ND ug/L 04/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO 12 NO 14 ND 16 ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- NO 11 NO NO ND 17 ug/L 04/28/06 ND ND ND ND ND NO ND ND ND NO 13 18 ug/L 10/09/06 -- -- -- ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 04/24/07 ND ND NO ND ND NO ND ND ND NO ND NO ug/L 10/30/07 10 ND 3.9 J NO ND ND NO 4.6 J 5.2 J 6.5 J 2.6 J 2.5 J 6.8 J ug/L 04/23/08 -- -- 10 ND -- NO -- -- -- -- NO -- ND ND NO NO ND ND NO NO 15.8 ug/L 10/06/08 10 ND ND 9.4 J ND ND NO 2.9 J 4.9 J ND NO 2.2 J 13.4 ug/L 04/13/09 -- -- 10 ND -- 6.3 J -- -- -- -- NO -- ND 2.1 J 2.3 J 5.4 J 5.2 J 6.5 J 6.4 J 5.5 J 10.4 ug/L 10/15/09 -- -- 10 ND -- NO -- -- -- -- NO -- ND ND NO NO 3.90 J NO NO 2.27 J 3.37 J ug/L 04/26/10 10 ND 3.82 J NO ND 2.47 J NO 3.17 J 4.54 J 3.95 J 3.09 J 3.89 J 2.18 J ug/L 10/19/10 -- -- 10 4.34 J -- 2.07 J -- -- -- -- 3.45 J -- ND ND NO NO ND 1.92 J NO NO 8.93 J ug/L 04/18/11 -- -- 10 ND -- 5.09 J -- -- -- -- 2.00 J -- ND ND NO 5.57 J 5.07 J 6.87 J NO 5.19 J 19.0 ug/L 10/10/11 10 ND ND NO ND ND NO ND ND ND NO Dry NO ug/L 04/17/12 -- -- 10 ND -- NO -- -- -- -- 2.26 J -- ND ND NO NO 4.08 J ND NO Dry 16.6 ug/L 10/09/12 10 ND 3.49 J 2.51 J ND ND NO 3.89 J 2.89 J ND NO Dry 20.6 ug/L 04/15/13 10 ND ND 2.11 J ND ND NO ND ND ND NO Dry 20.4 ug/L 09/30/13 10 ND 4.05 J 2.75 J ND ND NO 6.67 J 5.81 J 5.32 J 3.31 J Dry 37.3 ug/L 04/16/14 10 ND 4.17 J 3.06 J ND ND NO 5.24 J 7.02 J 4.95 J 2.83 J Dry 60.5 ug/L 10/15/14 2.1 10 Dry ND NO ND ND NO ND NO ND NO Dry 18.3 ug/L 04/15/15 2.1 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO ND NO ND NO Dry 26.2 ug/L 10/07/15 2.1 10 ND ND 4.58 J 3.55 J ND NO 3.21 J 4.36 J ND 5.90 J 6.76 J 22.2 ug/L 04/11/16 2.1 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO NO ND NO 4.87 J 21.0 ug/L 11/30/16 3.1 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO NO 11.5 ug/L 04/11/17 3.1 10 ND ND 4.48 J ND ND NO ND NO ND NO ND 36.0 ug/L 12/12/17 3.1 -- 10 ND -- 7.48 J -- -- -- -- NO -- ND ND NO 7.80 J ND 3.33 J NO 5.91 J 15.6 ug/L 06/20/18 3.1 -- 10 ND NO ND -- -- -- -- NO ND ND ND NO NO ND ND NO ND -- ug/L 11/27/18 3.1 10 -- ND 3.42 J ND NO ND ND ND NO ND NO ND NO ND 23.7 ug/L 04/02/19 3.1 10 -- ND NO ND -- -- -- -- NO ND ND ND NO NO ND ND NO 23.8 22.4 ug/L 11/19/19 3.1 10 ND NO ND NO ND NO ND ND ND NO ND NO ND NO ND 26.3 ug/L 04/07/20 3.1 10 ND NO ND NO ND NO NO ND ND NO ND NO ND -- ug/L 10/13/20 3.1 10 -- ND 6.92 4.49 J NO 11.2 NO NO 7.49 ND NO ND ND NO NO 9.32 J 10.9 9.86 6.58 J 9.94 J 11.4 ug/L 04/13/21 3.1 10 ND 8.39 J 9.88 J NO 7 J 3.98 J ND NO 7.9 JI 5.15 J 11.5 NS NS NS 4.25 J 4.39 J 13.9 10.9 13 NS Z:\Sh,re\SME\Ops\ENV r,j s\2030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waled Qualgy F 2020-2021\W-Ing_Dx--Sphng-1Even02020-10 WOMR Tables Fob App-,.- Page 6 of 30 TABLE5A Record of Groundwater Monitoring Water Quality Monitoring Report, Moore County Landfill, NC Solid Aberdeen, Moore County, North S&ME Project No. 4358-20-043A WDetected Monitoring 'e n.t'ituent/Parameter a Mercury Results October Waste Permit Carolina Units ug/L (Detected 2020 Monitoring No. 63-01 apdo 03/05/90 Constituents) Event PQL SWSL MW-5dj U.b Active C&D Monitoring MW-14 Wells MW-11 7S MW-17D W-4 MW-11SR IM6 ND MW-2 0.5 Closed MSW Monitoring MW-3 ND Wells & MNA MW-6 Performance MW-7 Monitoring Wells MW-8 MW-9 ��Kjl �F- PW-I ND NC 2L = 1 ug/L ug/L 03/21/91 0.6 0.6 0.8 2.4 0.6 ND EPA MCL = 2 ug/L ug/L 03/10/92 0.7 1.1 ND 6 1.3 -- -- NO ug/L 04/20195 ND -- -- -- NO ND 1.2 0.3 NO ug/L 06/27/95 -- -- NO ug/L 09/22/95 ND ND ND ND ND NO NO ug/L 03/28196 ND ND ND NO ND NO NO ND ug/L 10/29/96 ND ND ND ND ND NO ND NO ug/L 04/08197 ND ND NO ND NO NO ND ND ug/L 10/29197 ND ND NO ND ND NO ND ND ug/L 04/30/98 ND ND ND ND ND NO ND NO ug/L 10/14198 ND ND NO ND ND NO ND NO ug/L 04/27199 ND ND NO ND ND NO ND NO ug/L 10/21/99 ND ND ND ND ND NO ND NO ug/L 03/14100 ND ug/L 04/19/00 ND ND ND ND ND NO ND NO ug/L 10/17/00 ND ND ND ND ND NO ND NO ug/L 04/10/01 ND ND NO ND NO NO ND ND ug/L 10/11/01 ND ND ND ND ND NO ND NO ug/L 04/18/02 ND ND ND ND ND NO ND NO ug/L 10/08/02 ND ND NO ND NO NO ND ND ug/L 04/09/03 ND ND 1.01 ND ND NO ND NO ug/L 10/13/03 ND ND NO ND NO NO ND NO ug/L 04/26104 ND ND NO ND ND NO ND NO ug/L 10/25/04 ND ND ND ND ND NO ND NO ug/L 04/04105 ND ND NO ND ND NO ND NO ug/L 10/04105 ND ND NO ND ND NO ND NO ug/L 04/28/06 ND ND ND NO ND NO ND ND ND NO ND NO ug/L 10/09106 ND ND NO NO NO NO NO ND ND NO ND ND ug/L 04/24/07 ND ND NO NO ND NO ND ND ND NO ND NO ug/L 10/30/07 0.2 0.17 J 0.12 J 0.24 0.21 0.16 J NO ND ND 0.17 J NO ND NO ug/L 04/23108 0.2 ND ND NO NO ND NO NO ND ND NO ND ND ug/L 10/06/08 0.2 ND ND NO NO ND 0.21 ND ND ND NO ND NO ug/L 04/13109 0.2 ND ND NO NO ND NO NO ND ND NO ND ND ug/L 10/15109 0.2 ND ND NO 0.0952 J ND NO NO ND ND NO ND ND ug/L 04/26/10 0.2 ND ND NO NO ND NO ND ND ND NO ND NO ug/L 10/19/10 0.2 ND ND NO NO ND NO NO ND ND NO ND NO ug/L 04/18/11 0.2 ND ND NO NO ND NO NO ND ND NO ND NO ug/L 10/10/11 0.2 ND ND NO 0.478 ND NO ND ND ND NO Dry NO ug/L 04/17/12 0.2 ND ND NO 0.175 J ND NO NO ND NO NO Dry ND ug/L 10/09/12 0.2 ND ND NO NO ND NO ND ND ND NO Dry NO ug/L 04/15/13 0.2 ND ND NO NO ND NO ND ND ND NO Dry NO ug/L 09/30/13 0.2 ND ND NO ND ND NO NO ND NO NO Dry ND ug/L 04/16/14 0.2 ND ND NO ND ND NO ND ND ND NO Dry NO ug/L 10/15/14 0.17 0.2 Dry ND NO ND ND NO ND ND ND NO Dry NO ug/L 04/15/15 0.17 0.2 ND ND 0.0261 J ND ND NO 0.0796 J ND ND NO Dry ND ug/L 10/07/15 0.17 0.2 ND ND NO ND ND NO 0.197 J ND ND NO 0.201 NO ug/L 04/11/16 0.17 0.2 ND ND NO ND ND NO NO 0.274 ND NO 0.219 ND ug/L 11/30/16 0.17 0.2 ND ND NO ND ND NO NO ND ND NO NO ND ug/L 04/11/17 0.17 0.2 ND ND NO ND ND NO ND ND ND NO ND NO ug/L 12/12/17 0.10 0.2 ND 0.0990 J NO 0.103 J ND NO NO ND ND 0.118 J 0.111 J ND ug/L 06/20/18 0.15 0.2 ND NO ND NO ND NO ND NO NO ND ND NO ND ug/L 11/27/18 0.15 0.2 -- 0.281 NO ND NO ND ND ND NO ND 0.338 ND 0.187 J ND NO ug/L 04/02/19 0.15 0.2 ND NO ND NO ND ND ND NO NO ND NO NO ND NO ug/L 11/19/19 0.15 0.2 ND NO ND ND ND NO ND ND ND NO ND ND ND NO ND NO ug/L 04/07/20 0.15 0.2 ND NO ND ND ND NO NO ND ND ND ND NO ND ug/L 10/13/20 0.15 0.2 ND NO NO NO ND ND ND NO ND NO ND ND NO NO NO ND ND NO ND ug/L 04/13/21 0.15 0.2 -- ND NO ND NO ND ND ND NO ND 0.476 ND NS NS NS ND NO ND NO ND NS Nickel Total ug/L 06/20/18 2.2 -- 50 4.03 B 3.14 B ND 2.30 B ND NO ND NC 2L = 100 ug/L ug/L 11/27/18 2.2 10 -- ND NO ND NO ND ug/L 04/02/19 2.2 10 ND NO ND NO ND ug/L 11/19/19 2.2 10 ND NO ND NO ND NO ND ug/L 04/07/20 2.2 10 ND NO ND NO ND ND NO ND ug/L 10/13/20 2.2 10 ND NO ND NO ND NO ND ND ND NO ND ANR ANR ANR ANR ANR ANR ANR ANR ND ug/L 04/13/21 2.2 10 ND NO NO NO NO NO ND ND ND NO ND NS NS NS ANR ANR ANR ANR ANR NS Z:\Sh,re\SME\Op,\ENV r,jed 020Y35&O3A - Co M R-, LFG & WQ M-g\-k 01 - S-- ... I - Q,,Ilty F 2020-2021 W-Iffig --- Spd,g -1 -020-10 WQMR T,- For App-,.- Page 7 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active :D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells nil Detected Monitoring &n'.t'ituent/Parameter Selenium Units ug/L won 04/28/06 -- PQL -- SWSL -- MW-5dJ01111"M ND -- MW-14 ND MW-11 7S -- MW-17D -- ���IW-4 -- -- ND MW-11SRIVI -- ND MW-2 ND MW-3 NO MW-6 ND MiL ND MW-8 ND MW-9�1 NO ND PW-I ND NC 2L = 20 ug/L ug/L 10/09/06 -- -- -- ND -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO ND ND EPA MCL = 50 ug/L ug/L 04/24/07 -- ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/30/07 -- -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 04/23/08 10 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/06/08 10 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/13/09 -- -- 10 ND -- 6.4 B -- -- -- -- NO -- ND ND NO 4.7 B 13.9 B ND 14.6 B 15.2 B ND ug/L 10/15/09 10 ND ND NO ND ND NO ND ND 1.02 B 2.47 B ND ND ug/L 04/26/10 -- -- 10 ND -- 1.35 J -- -- -- -- NO -- ND ND NO 1.17 J 1.18 J ND NO 3.22 J ND ug/L 10/19/10 -- -- 10 ND -- ND -- -- -- -- NO -- ND 2.48 J 1.09 J 0.919 J 2.88 J 1.30 J 4.50 J 1.49 J ND ug/L 04/18/11 10 ND ND 4.90 J ND ND NO ND ND ND NO ND ND ug/L 10/10/11 -- -- 10 ND -- ND -- -- -- -- NO -- ND ND 2.71 J NO ND ND NO Dry ND ug/L 04/17/12 -- -- 10 ND - 5.54 (ND) J -- 2.86 (ND) J -- ND ND NO 4.55 (ND) J ND ND NO Dry ND ug/L 10/09/12 10 ND ND NO ND ND NO ND ND ND 12.4 Dry ND ug/L 04/15/13 -- -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO Dry ND ug/L 09/30/13 10 ND ND NO ND ND NO ND ND NO NO Dry ND ug/L 04/16/14 10 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/15/14 5.0 -- 10 Dry -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO Dry ND ug/L 04/15/15 5.0 10 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/07/15 5.0 10 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/11/16 5.0 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO ND ND ug/L 11/30/16 6.2 10 ND ND NO ND ND NO ND ND ND NO NO ND ug/L 04/11/17 6.2 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO ND ND ug/L 12/12/17 6.2 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO NO ND ug/L 06/20/18 6.2 -- 10 ND NO ND NO ND ND ND NO ND ND ND NO ND ug/L 11/27/18 6.2 10 -- ND NO ND -- -- -- -- NO ND ND ND NO NO ND ND NO ND ND ug/L 04/02/19 6.2 10 -- ND NO ND -- -- -- -- NO ND ND ND NO NO ND ND NO ND ND ug/L 11/19/19 6.2 10 ND NO ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 04/07/20 6.2 10 -- ND NO ND NO ND NO -- NO ND NS NS NS NO ND ND NO ND -- ug/L 10/13/20 6.2 10 ND NO ND NO ND NO ND ND ND NO ND NO ND NO ND ND ND NO ND ug/L 04/13/21 6.2 10 -- ND NO ND NO ND NO ND ND ND NO ND NS NS NS ND ND ND NO ND NS Silver ug/L 04/28/06 -- -- -- ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND NC 2L = 20 ug/L ug/L 10/09/06 ND ND NO ND ND NO ND ND ND NO ND NO EPA MCL = 100 ug/L" ug/L 04/24/07 -- -- -- ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 10/30/07 -- -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 04/23/08 10 2.8 B ND NO ND ND NO ND ND ND NO ND NO ug/L 10/06/08 -- -- 10 ND -- NO -- -- -- -- NO -- ND ND NO NO ND ND 4.6 B ND NO ug/L 04/13/09 -- -- 10 ND -- NO -- -- -- -- NO -- ND ND NO NO ND ND NO ND NO ug/L 10/15/09 10 ND ND NO ND ND NO ND ND ND 3.03 J ND NO ug/L 04/26/10 -- -- 10 ND -- 5.35 J -- -- -- -- NO -- ND ND NO 3.86 J 5.70 J 5.29 J 5.55 J 2.17 J ND ug/L 10/19/10 10 ND ND NO ND ND NO ND NO ND NO ND NO ug/L 04/18/11 10 ND 5.35 J NO ND ND NO 5.13 J NO ND 5.64 J 1.95 J NO ug/L 10/10/11 -- -- 10 ND -- NO -- -- -- -- NO -- ND ND NO NO 9.37 J ND NO Dry ND ug/L 04/17/12 10 ND ND NO ND ND NO ND NO ND NO Dry NO ug/L 10/09/12 10 ND ND NO ND ND NO ND 2.66 J ND 2.43 J Dry NO ug/L 04/15/13 -- -- 10 ND -- 2.19 J -- -- -- -- NO -- ND ND NO NO NO ND NO Dry ND ug/L 09/30/13 10 ND 4.10 J NO ND ND NO 4.63 J 5.55 J 4.09 J 2.61 J Dry NO ug/L 04/16/14 -- -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO NO ND NO Dry ND ug/L 10/15/14 1.9 -- 10 Dry -- ND -- -- -- -- NO -- ND ND NO NO NO ND NO Dry ND ug/L 04/15/15 1.9 10 ND ND NO ND ND NO ND NO ND NO Dry NO ug/L 10/07/15 1.9 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND NO ug/L 04/11/16 1.9 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND NO ug/L 11/30/16 1.9 10 ND ND NO ND ND NO ND ND ND NO ND NO ug/L 04/11/17 1.9 -- 10 ND -- ND -- -- -- -- NO -- ND ND NO NO 1.92 J ND NO ND ND ug/L 12/12/17 1.9 10 ND ND NO ND ND NO ND ND 2.43 B NO ND NO ug/L 06/20/18 1.9 -- 10 ND NO ND NO ND ND ND NO ND ND ND NO ND ug/L 11/27/18 1.9 10 -- ND NO ND -- -- -- -- NO ND ND ND NO NO ND ND NO ND ND ug/L 04/02/19 1.9 10 ND NO ND NO ND ND ND NO ND NO ND NO ND NO ug/L 11/19/19 1.9 10 -- ND NO ND ND ND -- -- NO ND ND ND NO NO ND ND NO ND NO ug/L 04/07/20 1.9 10 -- ND NO ND ND ND NO -- NO ND NS NS NS NO ND ND NO ND NS ug/L 10/13/20 1.9 10 ND NO ND NO ND ND ND NO ND NO ND ND ND NO ND NO ND NO ND NO ug/L 04/13/21 1.9 10 -- ND NO NO NO NO ND ND NO ND NO ND NS NS NS NO ND NO NO ND NS Z:\Sh,re\SME\Ops\ENVrojed 030Y35&O0 3AMo Co My R,u,,LFGBWGMon,g\TBSk01-Seml-Annual Wafer Quality FY 2020-2021\W-Ing_Dxu-Spbng2021 Even02020-10WOMRTabI For App-,.- Page 8of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SS:ME Project No. 4358-20-043A &De,.e,,cted Monitoring n ituent/Parameter Vanadium Total NC 2L IMAC = 0.3 ug/L Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L 06/20/18 11/27/18 04/02/19 11/19/19 04/07/20 10/13/20 04/13/21 1.4 1.4 1.4 1.4 1.4 1.4 1.4 PQL -- 10 10 10 10 10 10 SWSL 25 -- -- -- -- -- MW-5 ND ND ND ND ND ND ND 2.86 1.65 1.65 NO NO 1.70 NO J J J J 2.15 ND NO ND Active :D Monitoring MW-14 3.60 1.95 1.65 ND 1.55 4.83 ND Wells MW-1 7S J -- J -- J ND J ND J ND ND MW-17D -- -- ND 2.02 ND ND MEME&W-4 -- -- -- J ND 2.34 J ND -- -- -- -- ND ND ND NO NO 1.92 NO NO NO MMW-AlSW 3.39 J 2.90 J 2.46 J J ND ND 2.32 J ND -- -- -- -- ANR NS Closed MW-2 -- -- -- -- ANR NS MSW Monitoring MW-3 -- -- -- -- ANR NS Wells MW-6 4.40 -- -- -- ANR ANR & MNA Performance MW-7 J 3.09 -- -- -- ANR ANR Monitoring MW-8 J -- -- -- -- ANR ANR Wells M�w -- -- -- -- ANR ANR -- -- -- -- ANR ANR -- -- -- -- ANR NS Zinc ug/L -- -- --34-- -- -- -- -- -- -- 43 79 11 -- -- -- -- ND NC 2L = 1000 ug/L ug/L 03/21/91 -- -- -- NO -- -- -- -- -- -- NO -- 24 24 NO -- -- -- -- -- NO EPA MCL = 5000 ug/L ug/L 03/10/92 -- -- -- 30 -- -- -- -- -- -- 31 -- 40 31 21 -- -- -- -- -- NO ug/L 04/20/95 35 -- -- -- -- 47 60 49 51 NO ug/L 06/27/95 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- NO ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- -- ND ND ND NO -- NO ug/L 03/28/96 ND ND NO ND ND ND NO NO ug/L 10/29/96 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/08/97 ND ND ND ND ND NO ND NO ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/30/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/27/99 ND ND ND ND ND NO ND NO ug/L 10/21/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 03/14/00 NO ug/L 04/19/00 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 10/17/00 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/10/01 ND ND ND ND ND NO ND NO ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND NO ug/L 04/18/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND NO ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/09/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/13/03 ND ND ND ND ND NO ND NO ug/L 04/26/04 ND ND ND ND ND NO ND NO ug/L 10/25/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/04/05 ND ND ND ND ND NO ND NO ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/30/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/23/08 -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 4.4 -- 10 ND NO NO -- -- -- -- NO ND -- -- -- ND ND -- -- -- -- ug/L 11/27/18 4.4 10 -- ND NO ND NO ND ug/L 04/02/19 4.4 10 ND NO ND NO ND ug/L 11/19/19 4.4 10 -- ND NO 5.24 J NO ND -- -- 22.6 ND -- -- -- -- -- -- -- -- -- ug/L 04/07/20 4.4 10 ND 27.7 ND NO ND NO NO ND ug/L 10/13/20 4.4 10 ND NO 455 NO 4.83 J NO ND NO ND NO ND ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 04/13/21 4.4 10 -- ND NO NO NO NO NO ND NO ND NO ND NS NS NS ANR ANR ANR ANR ANR NS Z:\Sh,re\SME\Ops\ENV,,]d 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waled QualgyF 2020-2021\W-Ing_Dx--Sphng-1Even02020-10 WOMR Tables Fob App-,.- Page 9 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Sa Active :D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells ��Kjl Detected Monitoring Constituent/Parameter Iron Units ug/L a 03/05/90 Poe -- PQL -- SWSL -- MW-5dj����� 1469 -- MW-14 -- MW-11 7S -- MW-17D ���RW-4 -- -- -- 419 MW1-- -11SR I= -- 239 MW-2 1110 MW-3 394 MW-6 -- MW-7 -- MW-8 -- M�F- -- -- PW-1 ND NC 2L = 300 ug/L ug/L 03/21/91 -- -- -- 7800 -- -- -- -- -- -- 700 -- 2510 17000 6500 -- -- -- -- -- ND EPA MCL = 300 ug/L ug/L 03/10/92 213 463 90 3110 323 -- -- -- -- ND ug/L 04/20/95 -- -- -- 186 -- -- -- -- -- -- -- -- -- -- -- 1340 9600 51200 71500 -- ND ug/L 06/27/95 - -- -- -- -- ND ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- -- ND ND ND NO -- ND ug/L 03/28/96 -- -- -- ND -- -- -- -- -- -- -- -- ND ND -- ND ND NO NO -- ND ug/L 10/29/96 ND ND ND ND ND NO ND ND ug/L 04/08/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/30/98 ND ND ND ND ND NO ND ND ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/21/99 ND ND ND ND ND NO ND ND ug/L 03/14/00 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/18/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/09/03 ND ND ND ND ND NO ND ND ug/L 10/13/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/26/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/25/04 ND ND ND ND ND NO NO ND ug/L 04/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/30/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/23/08 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 22 -- 300 72.9 J 83,700 135,000 1,790 144,000 ug/L 11/27/18 22 50 -- ND 88,300 142,000 -- -- -- -- 417 141,000 -- -- -- -- -- -- -- -- -- ug/L 04/02/19 22 50 -- ND 82,700 134,000 -- -- -- -- 440 129,000 -- -- -- -- -- -- -- -- -- ug/L 11/19/19 22 50 ND 75,900 152,000 38,400 181 -- 15,500 101'000 ug/L 04/07/20 22 50 -- ND 52,300 141,000 2,670 448 111,000 -- 2,510 101,000 -- -- -- -- -- -- -- -- -- ug/L 10/13/20 22 50 -- ND 83,800 66,200 7,600 139,000 14,400 2,500 103,000 ND 397 119,000 ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 1 04/13/21 22 50 ND 94,700 78,700 8,000 45,900 9,390 1,470 131,000 60,400 1 19,300 123,000 NS NS NS ANR ANR ANR ANR ANR NS Z:\Sharetl\SME\Ops\ENV ,o]ed 030Y35&O0 3A Moore Co My ROWne LFG& WG Monilaing\Task 01-S--Annual Wale, Oualgy F 2020-2021\W-Ing_Dx--Sphng 2021 Even02020-10 WOMR Tables Fo, App-,.- Page 10 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active :D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells WDetected Monitoring n.t'ituent/Parameter a Manganese Units ug/L :MR 03/05/90 -- PQL -- SWSL -- MW-J����� ND -- MW-14 -- MW-11 7S -- MW-17D -- -- -- W-4 ND MW-11SR -- MW-1 31 MW-2 ND MW-3 ND MW-6 -- MW-7 -- MW-8 -- M� -- -- PW 11 F ND NC 2L = 50 ug/L ug/L 03/21/91 -- -- -- 20 -- -- -- -- -- -- 14 -- 50 50 13 -- -- -- -- -- ND EPA MCL = 50 ug/L ug/L 03/10/92 ND ND 47 32 ND -- -- -- -- ND ug/L 04/20/95 -- -- -- ND -- -- -- -- -- -- -- -- -- -- -- 23 23 1020 173 -- ND ug/L 06/27/95 -- -- -- -- ND ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- -- ND ND ND NO -- ND ug/L 03/28/96 -- -- -- ND -- -- -- -- -- -- -- -- ND ND -- ND ND NO NO -- ND ug/L 10/29/96 ND ND ND ND ND NO ND ND ug/L 04/08/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/30/98 ND ND ND ND ND NO ND ND ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/21/99 ND ND ND ND ND NO ND ND ug/L 03/14/00 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/18/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/09/03 ND ND ND ND ND NO ND ND ug/L 10/13/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/26/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/25/04 ND ND ND ND ND NO NO ND ug/L 04/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/30/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/23/08 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 1.5 -- 50 ND 200 186 40.2 J 346 ug/L 11/27/18 1.5 10 -- 1.73 J 203 185 -- -- -- -- 103 384 -- -- -- -- -- -- -- -- -- ug/L 04/02/19 1.5 10 -- 3.52 J 190 174 -- -- -- -- 185 443 -- -- -- -- -- -- -- -- -- ug/L 11/19/19 1.5 10 2.68 J 191 212 114 2.71 J -- 131 248 ug/L 04/07/20 1.5 10 1.59 J 166 229 99.6 8.4 J 228 53 258 ug/L 10/13/20 1.5 10 -- 2.85 J 180 569 123 183 164 47.8 227 ND 11.0 294 ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 1 04/13/21 1.5 1 10 1 1 4.80 JI 178 683 150 68 104 37.3 241 229 327 372 NS NS NS ANR ANR ANR ANR ANR I NS Z:\Sh,re\SME\Ops\ENV,,]d 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waled QualgyF 2020-2021\W-Ing_Dx--Sphng-1Even02020-10 WOMR Tables Fob App—,.— Page 11 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Sa Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter Acetone Units ug/L a 03/05/90 PWO PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 M�F_ PW 11 NC 2L = 6000 ug/L ug/L 03/21/91 ND ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 NO ND NO ND ug/L 09/22/95 ND ND ND ND NO ND NO ND NO ND ug/L 03/28196 ND ND ND ND NO NO ND NO NO ND ug/L 10/29/96 ND ND ND NO ND NO ND ND ug/L 04/08197 ND ND NO ND NO NO ND ND ug/L 10/29197 ND ND NO ND NO NO ND ND ug/L 04/30/98 ND ND ND NO ND NO ND ND ug/L 10/14198 ND ND NO ND 3085 NO ND ND ug/L 04/27199 ND ND NO 541 ND NO ND ND ug/L 10/21/99 ND ND 335 390 108 NO ND ND ug/L 03/14100 ND ND ND ND NO NO NO ND ND NO ND ND ug/L 04/19/00 ND ND ND NO 728 NO 139 ND ug/L 10/17/00 ND ND ND NO ND NO ND ND ug/L 04/10/01 ND ND 185 NO 2628 NO ND ND ug/L 10/11/01 ND ND ND NO ND NO ND ND ug/L 04/18/02 ND ND 129 NO ND NO ND ND ug/L 10/08/02 ND ND 422 110 ND NO ND ND ug/L 04/09/03 ND ND ND 192 119 NO ND ND ug/L 10/13/03 ND ND 125 113 361 NO ND ND ug/L 04/26104 ND ND NO NO ND NO ND ND ug/L 10/25/04 ND ND ND NO ND NO ND ND ug/L 04/04105 ND ND NO 1400 123 NO ND ND ug/L 10/04105 ND ND NO NO ND NO ND ND ug/L 04/28/06 ND ND ND ND ND NO ND NO ND NO ND ND ug/L 10/09106 ND ND NO ND ND NO NO NO NO NO ND ND ug/L 04/24/07 ND ND NO ND ND NO ND 138 ND NO ND ND ug/L 10/30/07 100 ND 4.8 J NO ND ND NO 380 60 16 7.7 5.6 ND ug/L 04/23108 100 ND ND 5.7 J ND ND NO 420 120 220 10 J ND ND ug/L 10/06/08 100 ND 7.6 B NO ND ND NO 1100 160 56 J 20 B 210 ND ug/L 04/13109 100 ND ND NO ND ND NO 48 J 240 160 NO 45 J ND ug/L 10/15109 100 ND ND NO ND ND NO NO 78 J NO NO NO ND ug/L 04/26/10 100 ND ND NO ND ND NO 80 J 25 J 77 J 8.9 J 140 ND ug/L 10/19/10 100 ND ND NO ND ND NO 180 1700 ND NO 170 ND ug/L 04/18/11 100 ND ND NO ND ND NO 29 J 36 J ND 36 J NO ND ug/L 10/10/11 100 ND ND NO ND ND NO 15 J -- ND 5.0 J Dry ND ug/L 04/17/12 100 ND ND NO ND ND NO 10 J 56 J 12 J 18 J Dry ND ug/L 10/09/12 100 ND ND NO ND ND NO ND 290 ND 13 J Dry ND ug/L 04/15/13 100 ND ND NO ND ND NO 150 88 J 73 J 12 J Dry ND ug/L 09/30/13 100 ND ND NO ND ND NO 94 J 24 J 9.8 J 5.5 J Dry ND ug/L 04/16/14 100 ND ND NO ND ND NO 280 36 J 6.3 J 15 J Dry ND ug/L 10/15/14 1.2 100 Dry ND NO ND ND NO 16 J 110 6.6 J 12 J Dry ND ug/L 04/15/15 1.2 100 ND ND NO ND ND NO 210 110 16 J 7.0 J Dry ND ug/L 10/07/15 1.2 100 ND ND NO ND ND NO 130 200 6.4 J 2.6 J 98 J ND ug/L 04/11/16 1.2 100 ND ND NO ND ND NO 290 110 NO 55 J 300 ND ug/L 11/30/16 10 100 ND ND NO ND ND NO 46 J 10 J NO 19 J 980 ND ug/L 04/11/17 10 100 ND ND NO ND ND NO ND 20 J ND NO 880 ND ug/L 12/12/17 10 100 ND ND NO ND ND NO NO NO NO 11 J 20 J ND ug/L 06/20/18 10 -- 100 ND NO ND NO ND ND ND NO 20 B 19 B 11 B 20 B ND ND ug/L 11/27/18 10 20 -- ND NO ND NO ND ND ND NO 28 190 56 57 ND ND ug/L 04/02/19 10 20 ND NO ND NO ND ND ND NO 12 J 490 21 NO ND ND ug/L 11/19/19 10 20 ND NO ND ND ND NO ND ND ND NO ND 12 J ND NO 190 NO ug/L 04/07/20 10 20 ND NO ND ND ND NO NO ND NS NS NS 26 59 ND 17 J ND NS ug/L 10/13/20 10 20 ND NO NO NO ND ND ND NO ND NO ND ND NO NO NO 490 D ND NO NO NO ug/L 04/13/21 10 20 ND NO ND NO 120 ND ND 11 J 22 NO 10 NS NS NS 46 75 ND NO ND NS Z:\Sh,re\SME\Op,\ENV r,jed 020Y35&O3A — Co M R—, LFG & WQ M—g\—k 01 - S-- ... I — Q,,Ilty F 2020-2021 W-Iffig --- Spd,g —1 —020-10 WQMR T,— For App—,.— Page 12 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells JWetected Monitoring SCuent/Parameter Benzene Units ug/L apmo 03/05/90 PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 lw�l PW-I NC 2L = 1 ug/L ug/L 03/21/91 ND EPA MCL = 5 ug/L ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 ND 3.2 8.8 9.8 ND ug/L 09/22/95 ND ND ND ND ND ND ND 6 6 ND ug/L 03/28196 ND ND ND 59 ND 5 6 -- ND ug/L 10/29/96 ND ND ND ND ND 6 9 ND ug/L 04/08197 ND ND ND ND ND 6 7 ND ug/L 10/29197 ND ND 5 ND ND 6.5 11 ND ug/L 04/30/98 ND ND ND 6.6 ND 6.4 11 ND ug/L 10/14198 ND ND ND ND ND NO 8.5 ND ug/L 04/27199 ND 5.3 ND ND ND 6.2 10 ND ug/L 10/21/99 ND ND -- ND ND ND NO 11 ND ug/L 03/14100 ND ND ND ND 3 ND 3 ND ND 4 11 ND ug/L 04/19/00 ND ND -- ND ND ND NO 7.6 ND ug/L 10/17/00 ND ND ND ND 5 5.2 9.2 ND ug/L 04/10/01 ND ND ND ND ND 5.1 9.6 ND ug/L 10/11/01 ND ND ND ND ND NO 8 ND ug/L 04/18/02 ND ND ND ND 5 NO ND ND ug/L 10/08/02 ND ND ND ND ND NO ND ND ug/L 04/09/03 ND ND ND ND ND NO 6.8 ND ug/L 10/13/03 ND ND ND ND ND NO 8.9 ND ug/L 04/26104 ND ND ND ND ND NO 8.4 ND ug/L 10/25/04 ND ND ND ND ND NO 6.8 ND ug/L 04/04105 ND ND ND ND ND NO 7.9 ND ug/L 10/04105 ND ND ND ND ND NO 6.5 ND ug/L 04/28/06 ND ND ND ND ND NO ND ND ND NO 6.6 ND ug/L 10/09106 ND ND NO ND NO NO ND ND ND NO 5.5 ND ug/L 04/24/07 ND ND NO ND ND NO ND ND 4.1 3.5 3.3 ND ug/L 10/30/07 1 ND 2.2 NO ND 1.2 NO 3.0 1.5 2.7 3.2 4.2 ND ug/L 04/23108 1 ND 2.5 NO ND 0.92 J NO ND 2.8 0.84 J 4.0 ND ND ug/L 10/06/08 1 ND ND NO ND 0.97 J NO ND 2.1 2.2 2.5 6.4 ND ug/L 04/13109 1 ND 2.3 NO ND NO NO 2.6 ND 3.1 3.4 5.9 ND ug/L 10/15109 1 ND 2.2 0.40 J 1.1 1.4 NO 3.4 1.3 2.9 3.5 4.0 ND ug/L 04/26/10 1 ND 2.5 NO ND 1.1 NO 2.2 2.4 3.1 3.6 5.2 ND ug/L 10/19/10 1 ND 2.3 NO ND 1.0 NO 3.1 ND 3.0 3.6 4.6 ND ug/L 04/18/11 1 ND ND NO ND NO NO ND 0.80 J 3.9 NO 4.1 ND ug/L 10/10/11 1 ND 2.2 NO NO 1.0 NO 3.4 -- 3.4 3.5 Dry ND ug/L 04/17/12 1 ND 2.3 NO 0.81 J 1.0 NO 3.6 1.2 4.3 3.9 Dry ND ug/L 10/09/12 1 ND 2.0 NO 0.69 J 1.2 NO 2.2 2.2 3.6 4.0 Dry ND ug/L 04/15/13 1 ND 2.1 NO NO 0.74 J NO 2.4 1.1 3.6 4.2 Dry ND ug/L 09/30/13 1 ND 2.1 NO ND 0.50 J NO 2.2 2.7 2.4 3.4 Dry ND ug/L 04/16/14 1 ND 2.0 NO ND 0.67 J NO 2.9 1.8 2.8 3.3 Dry ND ug/L 10/15/14 0.15 1 Dry 1.9 NO ND 0.81 J NO 2.8 1.6 3.9 3.4 Dry ND ug/L 04/15/15 0.15 1 ND 1.2 NO ND 0.81 J NO 1.5 0.69 J 1.9 2.9 Dry ND ug/L 10/07/15 0.15 1 ND 2.4 NO ND 0.80 J NO 3.9 1.6 3.1 3.9 6.3 ND ug/L 04/11/16 0.15 1 ND 2.2 NO ND 0.54 J NO 2.0 0.64 J 3.5 3.8 2.8 ND ug/L 11/30/16 0.15 1 ND 2.0 NO ND 0.45 J NO 2.6 1.4 2.9 2.9 3.6 ND ug/L 04/11/17 0.15 1 ND 2.2 NO ND 1.2 NO 2.9 ND 3.9 4.1 3.4 ND ug/L 12/12/17 0.15 1 ND -- 1.4 NO -- 0.87 J 0.60 J NO 2.4 1.1 2.7 3.5 4.4 ND ug/L 06/20/18 0.15 1 ND 1.2 1.6 NO 2.4 ND 1.0 NO 2.5 1.1 3.3 3.4 1.1 ND ug/L 11/27/18 0.15 1 -- ND 2.0 2.0 NO 2.8 ND ND NO 3.3 0.75 J 2.3 3.6 1.5 ND ug/L 04/02/19 0.15 1 ND 2.1 1.6 NO 2.7 ND 0.50 J NO 3.4 1.1 J 2.7 3.4 1.8 ND ug/L 11/19/19 0.15 1 ND 1.6 2.3 ND ND -- NO 2.8 0.48 J 0.97 J NO 3.7 1.6 2.9 3.8 5.7 ND (Verification Event) ug/L 01/08/20 0.57 1 -- -- -- -- -- -- -- -- -- 1.5 NO ug/L 04/07/20 0.15 1 ND 1.6 1.7 ND ND 1.6 ND 3.1 1.4 ND 2.5 3.6 1.5 NO (Verification Event) ug/L 06/05/20 0.15 1 -- 1.2 NS NS NS -- -- -- NS ug/L 10/13120 0.15 1 ND 1.9 ND ND 2.2 ND ND 0.99 J ND ND 3.2 ND 0.54 J NO 2.5 ND 2.8 4.0 1.2 NO ug/L 04/13121 0.15 1 ND 2.1 ND ND ND ND ND 1.2 ND ND 2.7 NS NS NS 2.6 1 3.2 3.2 0.8 JI NS Z:\Sh,retl\SME\Op,\ENV r,jed 020Y35&O3A - Co M R-, LFG & WQ M-g\-k 01 - S-- ... I - Q,,Ilty F 2020-2021 W-Iffig --- Spd,g -1 -020-10 WQMR T,- For App-,.- Page 13 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells KDetected Monitoring e 0 .tc.t'..`mtJParameter Chlorobenzene Units ug/L apmo 03/05/90 PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 lw�l PW-I NC 2L = 50 ug/L ug/L 03/21/91 ND EPA IVICL = 100 ug/L ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 ND NO ND 6.5 ND ug/L 09/22/95 ND ND ND ND NO ND NO ND 6 ND ug/L 03/28196 ND ND ND NO ND NO NO ND ug/L 10/29/96 ND ND ND NO ND NO ND ND ug/L 04/08197 ND ND NO ND NO NO ND ND ug/L 10/29197 ND ND NO ND NO 7.5 ND ND ug/L 04/30/98 ND ND ND NO ND 5.4 ND ND ug/L 10/14/98 ND ND ND NO ND 5.1 ND ND ug/L 04/27/99 ND ND ND NO ND 6.1 ND ND ug/L 10/21/99 ND ND -- ND NO ND 7.1 ND ND ug/L 03/14100 ND ND ND ND 3 NO NO ND NO 6 ND ND ug/L 04/19100 ND ND -- NO ND NO 5.5 ND ND ug/L 10/17/00 ND ND ND NO ND 12 ND ND ug/L 04/10/01 ND ND NO ND NO 7.3 ND ND ug/L 10/11/01 ND ND NO ND NO 13 ND ND ug/L 04/18/02 ND ND ND NO ND 10.5 ND ND ug/L 10/08/02 ND ND NO NO NO 8.6 ND ND ug/L 04/09/03 ND ND ND NO ND 8.6 ND ND ug/L 10/13/03 ND ND ND NO ND 10.8 ND ND ug/L 04/26104 ND ND NO NO NO 10.9 ND ND ug/L 10/25/04 ND ND ND NO ND 11.9 NO ND ug/L 04/04105 ND ND NO NO NO 9 ND ND ug/L 10/04105 ND ND NO NO NO 9.1 ND ND ug/L 04/28/06 ND ND ND ND ND NO ND NO ND 7.8 ND ND ug/L 10/09106 ND NO NO ND NO NO NO NO ND NO ND ND ug/L 04/24107 ND NO NO ND 3.2 NO NO NO ND 9.1 ND ND ug/L 10/30/07 3 ND 3.0 NO ND 4.0 NO 0.93 J 0.98 J 2.4 J 9.2 0.48 J ND ug/L 04/23108 3 ND 2.7 J NO ND 2.5 J NO NO 0.45 J ND 9.9 ND ND ug/L 10/06/08 3 ND 2.1 J NO ND 2.6 J NO ND 0.93 J ND 9.0 ND ND ug/L 04/13/09 3 ND 2.9 J NO ND 3.4 NO 0.71 J NO 1.1 J 11 ND ND ug/L 10/15109 3 ND 3.2 NO 8.4 3.8 NO 1.2 J 1.0 J 2.9 J 11 0.57 J ND ug/L 04/26/10 3 ND 3.2 NO NO 2.7 J NO 0.81 J 0.61 J 1.0 J 11 ND ND ug/L 10/19/10 3 ND 3.0 NO NO 3.1 NO 0.99 J NO 1.5 J 10 ND ND ug/L 04/18/11 3 ND 3.2 NO NO 2.6 J NO NO 0.81 J 2.7 J 7.8 NO ND ug/L 10/10/11 3 ND 3.9 NO 6.7 3.0 NO 1.6 J -- 3.6 9.6 Dry ND ug/L 04/17/12 3 ND 3.6 NO 6.3 2.8 J NO 1.4 J 0.86 J 2.3 J 12 Dry ND ug/L 10/09/12 3 ND 3.5 NO 5.6 3.1 NO 1.3 J 1.4 J 2.5 J 11 Dry ND ug/L 04/15/13 3 ND 3.1 NO NO 1.9 J NO 1.1 J 0.41 J 1.1 J 10 Dry ND ug/L 09/30/13 3 ND 2.5 J NO ND 1.2 J NO 1.2 J 1.0 J 0.64 J 9.2 Dry ND ug/L 04/16/14 3 ND 3.3 NO ND 1.8 J NO 1.2 J 0.75 J 0.74 J 9.1 Dry ND ug/L 10/15/14 0.17 3 Dry 2.6 J NO 1.6 J 2.1 J NO 0.96 J 1.4 J 3.1 10 Dry ND ug/L 04/15/15 0.17 3 ND 2.7 J NO ND 2.1 J NO 0.69 J ND 1.1 J 10 Dry ND ug/L 10/07/15 0.17 3 ND 2.6 J NO ND 2.3 J NO 1.2 J 1.8 J 3.6 9.9 0.64 J ND ug/L 04/11/16 0.17 3 ND 2.6 J NO ND 1.2 J NO 0.74 J ND 2.1 J 10 ND ND ug/L 11/30/16 0.17 3 ND 2.3 J NO ND 1.4 J NO 1.0 J 1.4 J 3.1 8.4 ND ND ug/L 04/11/17 0.17 3 ND 2.6 J NO NO 3.3 NO 1.4 J ND 4.6 12 ND ND ug/L 12/12/17 0.17 3 ND -- 1.2 J NO -- 7.1 2.1 J NO NO 1.4 J 4.0 10 0.62 J ND ug/L 06/20/18 0.17 3 ND 0.62 J 2.9 J NO 1.3 J NO 2.8 J NO 1.8 J 0.93 J 2.8 J 10 0.40 J ND ug/L 11/27/18 0.17 1 -- ND 0.97 J 3.5 NO 1.0 NO 0.90 J NO 1.6 0.46 J 0.91 J 7.4 ND ND ug/L 04/02/19 0.17 1 ND 1.2 3.4 NO 1.0 NO 1.3 NO 1.4 ND 1.2 9.3 0.44 J ND ug/L 11/19/19 0.17 1 ND 0.90 J 5.1 NO ND -- NO 1.3 3.7 2.6 NO 1.9 4.1 6.1 11 0.91 J ND ug/L 04/07/20 0.17 1 ND NO 5.3 NO ND 1.2 NO 1.6 NS NS NS 1.2 ND 1.9 9.6 ND NS ug/L 10/13/20 0.17 1 ND NO NO NO 5.8 NO ND 0.88 J ND NO 1.9 NO 1.2 NO 1.6 ND 4.3 8.9 ND NO ug/L 04/13/21 0.17 1 ND 1.3 ND NO 1.5 NO ND 0.91 J ND 0.53 J 1.6 NS NS NS 1.5 0.9 J 3.8 10.0 ND NS Z:\Sh,retl\SME\Op,\ENV r,jed 020Y35&O3A - Co M R-, LFG & WQ M-g\-k 01 - S-- ... I - Q,,Ilty F 2020-2021 W-Iffig --- Spd,g -1 -020-10 WQMR T,- For App-,.- Page 14 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells &Detected Monitoring e n'stituent/Parameter Chloroethane Units ug/L apmo 03/05/90 PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 MW-9 PW-I NC 2L = 3000 ug/L ug/L 03/21/91 ND ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 13.3 4.2 6.6 8.5 ND ug/L 09/22/95 ND ND ND ND NO 12 14 ND NO ND ug/L 03/28196 ND ND NO 23 14 NO NO ND ug/L 10/29/96 ND ND ND ND ND NO ND ND ug/L 04/08197 ND ND 23 ND ND NO ND ND ug/L 10/29197 ND ND 17 ND ND NO ND ND ug/L 04/30/98 ND ND 19 ND ND NO ND ND ug/L 10/14198 ND ND 16 ND ND NO ND ND ug/L 04/27199 ND ND 15 ND ND NO ND ND ug/L 10/21/99 ND ND 11 ND ND NO ND ND ug/L 03/14100 ND ND ND ND ND NO 6 ND NO NO 2 ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 ND ND ND ND ND NO ND ND ug/L 04/10/01 ND ND NO ND NO NO ND ND ug/L 10/11/01 ND ND ND ND ND NO ND ND ug/L 04/18/02 ND ND ND ND ND NO ND ND ug/L 10/08/02 ND ND NO ND NO NO ND ND ug/L 04/09/03 ND ND ND ND ND NO ND ND ug/L 10/13/03 ND ND NO ND NO NO ND ND ug/L 04/26104 ND ND NO ND ND NO ND ND ug/L 10/25/04 ND ND ND ND ND NO ND ND ug/L 04/04105 ND ND NO ND ND NO ND ND ug/L 10/04105 ND ND NO ND ND NO ND ND ug/L 04/28/06 ND ND ND ND ND NO ND ND NO NO ND ND ug/L 10/09106 ND ND NO ND ND NO NO ND NO NO ND ND ug/L 04/24/07 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/30/07 10 ND ND NO ND ND NO 1.3 J ND ND NO ND ND ug/L 04/23108 10 ND ND NO ND ND NO NO ND NO NO ND ND ug/L 10/06/08 10 ND 1.2 J NO ND ND NO 4.8 J 0.55 J 0.78 J 1.3 J 2.5 J ND ug/L 04/13109 10 ND ND NO ND ND NO NO ND 1.1 J NO ND ND ug/L 10/15109 10 ND ND NO ND ND NO NO ND ND NO ND ND ug/L 04/26/10 10 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/19/10 10 ND ND NO ND ND NO NO ND ND NO ND ND ug/L 04/18/11 10 ND ND NO ND ND NO NO ND ND NO ND ND ug/L 10/10/11 10 ND ND NO ND ND NO ND ND NO Dry ND ug/L 04/17/12 10 ND ND NO ND ND NO NO ND 0.54 J NO Dry ND ug/L 10/09/12 10 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/13 10 ND 0.65 J NO ND ND NO ND ND 0.79 J NO Dry ND ug/L 09/30/13 10 ND ND NO ND ND NO NO ND ND NO Dry ND ug/L 04/16/14 10 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/15/14 0.23 10 Dry ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/15 0.23 10 ND ND NO ND ND NO NO ND ND NO Dry ND ug/L 10/07/15 0.23 10 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/11/16 0.23 10 ND ND NO ND ND NO NO ND ND NO ND ND ug/L 11/30/16 0.23 10 ND ND NO ND ND NO NO ND NO NO ND ND ug/L 04/11/17 0.23 10 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 12/12/17 0.23 10 ND ND NO ND ND NO NO ND NO NO 0.65 J ND ug/L 06/20/18 0.23 10 ND NO ND NO ND ND ND NO NO ND NO NO ND ND ug/L 11/27/18 0.23 1 -- ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 04/02/19 0.23 1 ND NO ND NO ND ND ND NO NO ND NO NO ND ND ug/L 11/19/19 0.23 1 ND NO ND ND ND NO ND ND ND NO ND ND ND NO ND NO ug/L 04/07/20 0.23 1 ND NO ND ND ND NO NO ND NS NS NS ND ND ND NO ND NS ug/L 10/13/20 0.23 1 ND NO NO ND ND ND ND NO ND NO ND ND NO NO NO ND ND NO ND NO ug/L 04/13/21 0.23 1 ND NO ND NO ND ND ND NO ND NO ND NS NS NS ND ND ND NO ND NS Z:\Sh,retl\SME\Op,\ENV r,jed 020Y35&O3A — Co M R—, LFG & WQ M—g\—k 01 - S-- ... I — Q,,Ilty F 2020-2021 W-Iffig --- Spd,g —1 —020-10 WQMR T,— For App—,.— Page 15 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active :D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells nil rameter 1,2-Dichloro5-en z-en e Units ug/L JPM 04/24/07 -- -- -- MW-5dJ01111"M ND -- -- MW-14 -- ND MW-11 7S -- MW-17D ,A��IW-4 -- -- -- ND MW-11SRIVI -- ND MW-2 ND MW-3 NO MW-6 ND MiL ND MW-8 ND MW-9�1 NO ND PW-I ND NC 2L = 20 ug/L ug/L 04/28/07 -- -- -- ND -- -- -- NO -- -- -- -- NO -- ND NO NO ND ND ND NO ND ND EPA MCL = 600 ug/L ug/L 10/09/07 -- ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/30/07 -- -- 5 ND -- -- -- 2.7 J -- -- -- -- NO -- ND 0.75 J NO ND ND 0.81 J 0.61 J ND ND ug/L 04/23/08 5 ND 2.1 J NO ND 0.43 J NO ND ND ND 0.69 J ND ND ug/L 10/06/08 5 ND 1.5 J NO ND 0.42 J NO ND ND ND 0.64 J ND ND ug/L 04/13/09 -- -- 5 ND -- -- -- 2.3 J -- -- -- -- NO -- ND 0.64 J NO ND ND ND 0.73 J ND ND ug/L 10/15/09 5 ND 2.2 J NO 0.62 J 0.67 J NO ND ND 0.81 J 0.69 J ND ND ug/L 04/26/10 -- -- 5 ND -- -- -- 2.0 J -- -- -- -- NO -- ND 0.50 J NO ND ND ND 0.82 J ND ND ug/L 10/19/10 -- -- 5 ND -- -- -- 2.1 J -- -- -- -- NO -- NO 0.53 J NO ND ND ND 0.88 J NO ND ug/L 04/18/11 5 ND 2.0 J NO NO 0.43 J NO ND NO 0.51 J 0.67 J ND ND ug/L 10/10/11 -- -- 5 ND -- -- -- 1.9 J -- -- -- -- NO -- 0.47 J 0.49 J NO ND -- 0.86 J 0.49 J Dry ND ug/L 04/17/12 -- -- 5 ND -- -- -- 2.0 J -- -- -- -- NO -- 0.49 J 0.64 J NO ND NO ND 0.66 J Dry ND ug/L 10/09/12 5 ND 2.0 J NO NO 0.49 J NO ND NO 0.48 J 0.76 J Dry ND ug/L 04/15/13 -- -- 5 ND -- -- -- 1.7 J -- -- -- -- NO -- NO ND NO ND NO ND 0.65 J Dry ND ug/L 09/30/13 5 ND 1.2 J NO ND ND NO ND NO ND 0.72 J Dry ND ug/L 04/16/14 5 ND 1.7 J NO ND ND NO ND NO ND 0.68 J Dry ND ug/L 10/15/14 0.19 -- 5 Dry -- -- -- 1.3 J -- -- -- -- NO -- ND ND NO ND NO 0.59 J 0.58 J Dry ND ug/L 04/15/15 0.19 5 ND 1.4 J NO ND ND NO ND NO ND 0.51 J Dry ND ug/L 10/07/15 0.19 5 ND 1.1 J NO ND 0.42 J NO ND NO 0.65 J NO ND ND ug/L 04/11/16 0.19 -- 5 ND -- -- -- 1.0 J -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 11/30/16 0.19 5 ND 0.92 J NO ND ND NO ND ND ND NO NO ND ug/L 04/11/17 0.19 -- 5 ND -- -- -- 0.94 J -- -- -- -- NO -- ND ND NO ND ND 0.57 J NO ND ND ug/L 12/12/17 0.19 -- 5 ND -- -- -- 0.82 J -- -- -- -- NO -- 0.44 J ND NO ND ND 0.59 J NO NO ND ug/L 06/20/18 0.19 5 ND NO ND NO ND ND ND NO ND NO ND NO ND ND ug/L 11/27/18 0.19 1 -- ND NO -- -- 1.1 -- -- -- -- NO ND ND ND NO ND ND ND NO ND ND ug/L 04/02/19 0.19 1 -- ND NO -- -- 1.1 -- -- -- -- NO ND ND ND NO ND NO ND NO ND ND ug/L 11/19/19 0.19 1 ND NO 1.8 NO ND -- NO ND ND ND NO ND 0.49 J 0.84 J 0.41 J ND ND ug/L 04/07/20 0.19 1 -- ND NO -- -- 1.3 NO ND 0.55 J -- NO ND NS NS NS ND NO ND NO ND NS ug/L 10/13/20 0.19 1 ND NO ND NO 1.6 NO ND 0.52 J ND NO ND NO ND NO ND NO 0.54 J NO NO ug/L 04/13/21 0.19 1 ND 0.51 J ND NO ND NO ND 0.55 J ND NO ND NS NS NS ND NO ND NO ND NS Z:\Sharetl\SME\Ops\ENV r,j s\2030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waled Quality F 2020-2021\W-Ing_Dx--Sphng-1Even02020-10 WOMR Tables Fob App-,.- Page 16 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A . Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Moniton ng .......... rameter 1777i FF 737 5 -en z -en e Units ug/L apmo 03/05/90 PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 lw�l PW-I NC 2L = 6 ug/L ug/L 03/21/91 ND EPA IVICL = 75 ug/L ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 ND 3.3 2 7.4 ND ug/L 09/22/95 ND ND ND ND NO ND NO ND NO ND ug/L 03/28196 ND ND ND NO ND ND NO ND ug/L 10/29/96 ND ND ND NO ND NO ND ND ug/L 04/08197 ND 6 NO ND NO 7 6 ND ug/L 10/29197 ND 7.8 NO ND NO 7 6.1 ND ug/L 04/30/98 ND ND ND NO ND 7.1 ND ND ug/L 10/14198 ND 9.7 NO ND NO 5.2 ND ND ug/L 04/27199 ND 8.7 NO ND NO 5.9 5.6 ND ug/L 10/21/99 ND ND -- ND NO ND NO 21 ND ug/L 03/14100 ND 2 ND ND 3 NO NO ND NO 4 ND ND ug/L 04/19/00 ND 7.5 -- ND NO ND NO 6.4 ND ug/L 10/17/00 ND 9.5 ND NO ND 10 6.3 ND ug/L 04/10/01 ND 6.7 NO NO NO 5.1 5.9 ND ug/L 10/11/01 ND ND ND NO ND 5.6 8.3 ND ug/L 04/18/02 ND ND ND NO ND 5.9 ND ND ug/L 10/08/02 ND ND NO ND NO 5.7 ND ND ug/L 04/09/03 ND ND ND NO ND 5.3 7.5 ND ug/L 10/13/03 ND ND NO ND NO 5.8 7.8 ND ug/L 04/26104 ND 5.1 NO ND NO 5.9 6.9 ND ug/L 10/25/04 ND ND ND NO ND NO ND ND ug/L 04/04105 ND ND NO ND ND NO 6.1 ND ug/L 10/04105 ND ND NO NO ND NO 6.6 ND ug/L 04/28/06 ND ND ND ND ND NO ND NO ND NO 6.8 ND ug/L 10/09106 ND ND NO ND ND NO NO NO ND NO 6 ND ug/L 04/24/07 ND 5.3 NO ND ND NO ND NO ND 3.5 5.7 ND ug/L 10/30/07 1 ND 5.7 NO ND 1.9 NO 2.0 0.49 J 4.0 3.0 3.3 ND ug/L 04/23108 1 ND 5.5 NO ND 1.8 NO NO NO ND 4.2 NO ND ug/L 10/06/08 1 ND 4.9 NO ND ND NO ND 1.5 ND 3.6 5.8 ND ug/L 04/13109 1 ND 6.9 NO ND 2.3 NO 1.6 NO 0.97 J 4.2 5.9 ND ug/L 10/15109 1 ND 5.5 NO ND 2.6 NO 3.4 1.6 4.1 3.7 5.3 ND ug/L 04/26/10 1 ND 6.0 NO ND 2.0 NO 1.8 1.2 0.67 J 3.9 4.9 ND ug/L 10/19/10 1 ND 4.2 NO ND NO NO NO NO 1.8 3.9 5.3 ND ug/L 04/18/11 1 ND 5.0 NO ND 1.5 NO 1.7 0.92 J 3.0 3.0 5.4 ND ug/L 10/10/11 1 ND 5.1 NO 0.82 J ND NO 4.0 -- 4.1 3.1 Dry ND ug/L 04/17/12 1 ND 5.2 NO ND 2.2 NO 4.3 1.1 2.6 4.0 Dry ND ug/L 10/09/12 1 ND 5.1 NO NO ND NO 3.7 1.8 3.3 4.9 Dry ND ug/L 04/15/13 1 ND 4.7 NO NO 1.9 NO 3.2 0.74 J 1.1 3.9 Dry ND ug/L 09/30/13 1 ND 4.4 NO ND ND NO 3.0 1.4 0.41 J 3.9 Dry ND ug/L 04/16/14 1 ND 4.7 NO ND ND NO 3.1 0.83 J 0.60 J 3.7 Dry ND ug/L 10/15/14 0.19 1 Dry 4.0 NO ND ND NO 2.4 1.6 4.1 3.3 Dry ND ug/L 04/15/15 0.19 1 ND 4.0 0.45 J ND ND NO 1.2 0.58 J 0.72 J 3.4 Dry ND ug/L 10/07/15 0.19 1 ND 3.9 NO ND ND NO 2.3 1.4 5.4 3.3 7.8 ND ug/L 04/11/16 0.19 1 ND 4.8 NO ND ND NO 1.4 NO 2.3 3.1 5.4 ND ug/L 11/30/16 0.19 1 ND 3.5 NO ND NO NO 1.9 1.3 3.5 2.5 4.8 ND ug/L 04/11/17 0.19 1 ND 4.4 NO ND 1.7 NO 2.8 0.63 J 6.1 3.6 5.0 ND ug/L 12/12/17 0.19 1 ND -- 2.7 NO -- 0.97 J 1.2 NO 2.4 1.3 4.6 2.7 5.1 ND ug/L 06/20/18 0.19 1 ND 1.7 4.3 NO 2.8 NO 1.9 NO 2.9 0.72 J 3.4 2.6 0.89 J ND ug/L 11/27/18 0.19 1 -- ND 2.1 4.2 NO 2.3 NO 0.53 J NO 2.6 NO 1.2 2.7 0.89 J ND ug/L 04/02/19 0.19 1 ND 2.9 4.2 NO 2.6 NO 0.74 J NO 2.0 NO 1.2 2.6 1.3 ND ug/L 11/19/19 0.19 1 ND 2.0 5.6 ND ND -- 0.46 J 2.9 0.45 J 1.2 NO 2.3 3.0 6.2 2.9 5.8 NO ug/L 04/07/20 0.19 1 ND 2.1 5.1 ND ND 2.1 NO 2.9 NS NS NS 1.3 NO 2.5 2.6 0.92 J NS ug/L 10/13/20 0.19 1 ND 2.6 NO NO 5.1 ND ND 1.8 ND NO 3.1 NO 0.59 J NO 1.7 NO 5.3 3.1 0.73 J NO ug/L 04/13/21 0.19 1 ND 3.1 ND NO ND ND ND 2.0 ND NO 2.4 NS NS NS 1.6 0.81 J 3.1 2.7 ND NS Z:\Sh,retl\SME\Op,\ENV r,jed 020Y35&O3A - Co M R-, LFG & WQ M-g\-k 01 - S-- ... I - Q,,Ilty F 2020-2021 W-Iffig --- Spd,g -1 -020-10 WQMR T,- For App-,.- Page 17 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A . Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Moniton ng .......... rameter 1779-c F 7or -oe-t F7a Fn -e Units ug/L apmo 03/05/90 PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 lw�l PW-I NC 2L = 6 ug/L ug/L 03/21/91 ND ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 7.9 9.3 13.4 9.6 ND ug/L 09/22/95 ND ND ND 9 NO 18 10 19 12 ND ug/L 03/28196 ND ND 11 ND 14 ND 10 -- ND ug/L 10/29/96 ND ND 70 7 ND 7 80 ND ug/L 04/08197 ND 14 74 5 ND 6 72 ND ug/L 10/29197 ND 12 64 6.2 8.3 7.5 72 ND ug/L 04/30/98 ND ND 45 8.1 ND 5.3 60 ND ug/L 10/14198 ND 8.4 50 ND ND NO 46 ND ug/L 04/27199 ND 9.7 37 ND ND 5.6 39 ND ug/L 10/21/99 ND ND -- 12 ND ND NO 24 ND ug/L 03/14100 ND ND ND ND 4 ND 12 ND ND NO 20 ND ug/L 04/19/00 ND 5.9 -- 19 ND ND NO 23 ND ug/L 10/17/00 ND ND 909 ND ND NO 24 ND ug/L 04/10/01 ND 5.5 9.2 ND ND NO 23 ND ug/L 10/11/01 ND ND 16 ND 6 NO 22 ND ug/L 04/18/02 ND ND 5.5 ND ND NO ND ND ug/L 10/08/02 ND ND 5.7 ND ND NO ND ND ug/L 04/09/03 ND ND ND ND ND NO 9.5 ND ug/L 10/13/03 ND ND NO ND NO NO 11.7 ND ug/L 04/26104 ND ND NO ND ND NO 10.7 ND ug/L 10/25/04 ND ND ND ND ND NO 8.5 ND ug/L 04/04105 ND ND NO ND ND NO 11.5 ND ug/L 10/04105 ND ND NO ND ND NO 10.7 ND ug/L 04/28/06 ND ND ND ND ND NO ND ND ND NO 10.1 ND ug/L 10/09106 ND ND NO ND ND NO NO ND ND NO 17.7 ND ug/L 04/24/07 ND ND NO ND ND NO ND ND ND NO 5.9 ND ug/L 10/30/07 5 ND 1.0 J 0.69 J ND 1.1 J NO 1.4 J 0.38 J 4.3 J 0.51 J 3.6 J ND ug/L 04/23108 5 ND 1.2 J NO ND 0.84 J NO NO 0.76 J ND 0.87 J 1.0 J ND ug/L 10/06/08 5 ND 1.2 J NO ND 0.61 J NO ND ND ND 0.83 J 7.4 ND ug/L 04/13109 5 ND 0.79 J NO ND 0.77 J NO 0.67 J ND 0.65 J 0.74 J 4.7 J ND ug/L 10/15109 5 ND 0.71 J 0.78 J ND 0.76 J NO 1.1 J ND 1.2 J 0.45 J 2.4 J ND ug/L 04/26/10 5 ND 0.64 J NO ND 0.56 J NO 0.51 J ND 0.86 J 0.49 J 2.8 J ND ug/L 10/19/10 5 ND 0.68 J NO ND 0.59 J NO 0.75 J ND 0.74 J 0.59 J 2.7 J ND ug/L 04/18/11 5 ND 0.69 J NO ND 0.47 J NO 0.51 J ND 1.0 J 0.50 J 2.0 J ND ug/L 10/10/11 5 ND 0.78 J 0.42 J ND 0.53 J NO 0.91 J -- 1.0 J 0.45 J Dry ND ug/L 04/17/12 5 ND 0.66 J NO ND 0.51 J NO 0.87 J ND 1.0 J 0.40 J Dry ND ug/L 10/09/12 5 ND 0.58 J NO ND 0.64 J NO 0.46 J ND 0.75 J 0.55 J Dry ND ug/L 04/15/13 5 ND 0.49 J NO ND ND NO 0.53 J ND 0.85 J 0.45 J Dry ND ug/L 09/30/13 5 ND ND NO ND ND NO 0.49 J 0.42 J ND NO Dry ND ug/L 04/16/14 5 ND ND NO ND ND NO 0.53 J ND 0.45 J 0.42 J Dry ND ug/L 10/15/14 0.13 5 Dry ND NO ND ND NO 0.50 J ND 0.87 J NO Dry ND ug/L 04/15/15 0.13 5 ND NO NO ND ND NO NO ND NO NO Dry ND ug/L 10/07/15 0.13 5 ND 0.73 J NO ND ND NO 0.58 J ND 0.62 J NO 1.1 J ND ug/L 04/11/16 0.13 5 ND 0.66 J NO ND ND NO NO ND 0.61 J NO 0.90 J ND ug/L 11/30/16 0.13 5 ND 0.59 J NO ND ND NO NO ND 0.70 J NO 0.77 J ND ug/L 04/11/17 0.13 5 ND 0.61 J NO ND 0.44 J NO ND ND 1.1 J NO ND ND ug/L 12/12/17 0.13 5 ND NO NO ND ND NO NO ND 0.46 J NO 0.66 J ND ug/L 06/20/18 0.13 5 ND NO NO NO ND ND ND NO NO ND 0.49 J NO ND ND ug/L 11/27/18 0.13 1 -- ND 0.64 J 0.50 J NO ND ND ND NO ND ND ND NO ND ND ug/L 04/02/19 0.13 1 ND NO ND NO ND ND ND NO NO ND NO NO ND ND ug/L 11/19/19 0.13 1 ND NO ND ND ND NO ND ND ND NO ND ND ND NO 0.93 J NO ug/L 04/07/20 0.13 1 ND NO ND ND ND NO NO ND NS NS NS ND ND ND NO ND NS ug/L 10/13/20 0.13 1 ND 0.43 J ND NO ND ND ND NO ND NO ND ND ND NO ND ND 0.56 J NO ND NO ug/L 1 04/13121 1 0.13 1 ND NO NO ND ND ND ND NO ND NO ND NS NS NS NO ND 0.56 J NO ND NS Z:\Sh,re\SME\Op,\ENV r,jed 020Y35&O3A - Co M R-, LFG & WQ M-g\-k 01 - S-- ... I - Q,,Ilty F 2020-2021 W-Iffig --- Spd,g -1 -020-10 WQMR T,- For App-,.- Page 18 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active :D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells nil Detected Monitoring 1,2-Dichloroethane ug/L 10/30/07 -- PQL -- SWSL 1 ND -- -- -- ND -- -- -- -- ND -- ND ND NO NO ND ND NO ND ND NC 2L = 0.4 ug/L ug/L 04/23/08 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO ND ND EPA MCL = 5 ug/L ug/L 10/06/08 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/13/09 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 10/15/09 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/26/10 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/19/10 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 04/18/11 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/10/11 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO -- ND NO Dry ND ug/L 04/17/12 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO Dry ND ug/L 10/09/12 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/13 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO Dry ND ug/L 09/30/13 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO Dry ND ug/L 04/16/14 1 ND ND NO ND 1.4 NO ND ND ND NO Dry ND ug/L 10/15/14 0.21 -- 1 Dry -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO Dry ND ug/L 04/15/15 0.21 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/07/15 0.21 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/11/16 0.21 -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO ND ND ug/L 11/30/16 0.21 1 ND ND NO ND ND NO ND ND ND NO NO ND ug/L 04/11/17 0.21 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 12/12/17 0.21 -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO ND ND ug/L 06/20/18 0.21 -- 1 ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 11/27/18 0.21 1 -- ND NO -- -- ND -- -- -- -- NO ND ND ND NO NO ND NO NO ND ND ug/L 04/02/19 0.21 1 -- ND NO -- -- ND -- -- -- -- NO ND ND ND NO NO ND ND NO ND ND ug/L 11/19/19 0.21 1 ND NO ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 04/07/20 0.21 1 -- ND NO NO NO ND NO ND NO ND NO ND NS NS NS NO ND ND NO ND NS ug/L 10/13/20 0.21 1 -- ND NO NO NO NO NO ND NO NO NO ND NO ND NO NO ND ND NO ND NO u /L 04/13/21 0.21 1 ND NO ND NO ND NO ND NO ND NO ND NS NS NS ND ND ND NO ND NS cis-1,2-Dichloroethene ug/L 04/28/06 -- -- -- ND -- -- -- 16.3 -- -- -- -- NO -- NO 6.4 NO 19.6 ND ND NO 18.4 NO NC 2L = 70 ug/L ug/L 10/09/06 ND 17.3 NO ND 5.1 NO 14.3 9.5 ND 9.3 19.4 NO EPA MCL = 70 ug/L ug/L 04/24/07 -- ND 19.3 NO ND ND NO 15.3 ND ND NO 7.3 NO ug/L 10/30/07 -- -- 5 ND -- -- -- 20 -- -- -- -- 4.4 J -- ND 5.1 0.35 J 14 6.4 3.0 J 1.6 J 17 ND ug/L 04/23/08 5 ND 20 NO ND 3.0 J NO 3.8 J 3.1 J ND 2.2 J 3.2 J NO ug/L 10/06/08 -- -- 5 ND -- -- -- 14 -- -- -- -- NO -- ND 2.8 J NO 5.1 5.8 ND 2.5 J 12 ND ug/L 04/13/09 -- -- 5 ND -- -- -- 14 -- -- -- -- NO -- ND 3.7 J NO 6.1 ND ND 2.9 J 12 ND ug/L 10/15/09 5 ND 17 6.2 1.9 J 4.6 J 0.41 J 15 5.1 5.0 1.8 J 16 NO ug/L 04/26/10 -- -- 5 ND -- -- -- 13 -- -- -- -- 0.60 J -- ND 2.8 J 0.43 J 7.5 3.2 J ND 2.3 J 7.2 NO ug/L 10/19/10 -- -- 5 ND -- -- -- 13 -- -- -- -- NO -- ND 3.0 J NO 8.4 ND ND 2.8 J 10 NO ug/L 04/18/11 5 ND 12 NO ND 2.8 J NO 6.8 3.4 J ND 1.9 J 11 NO ug/L 10/10/11 -- -- 5 ND -- -- -- 12 -- -- -- -- 3.0 J -- 1.5 J 2.6 J NO 13 -- 2.8 J 1.6 J Dry ND ug/L 04/17/12 5 ND 11 1.8 J 1.4 J 2.2 J 0.39 J 16 2.8 J ND 1.6 J Dry NO ug/L 10/09/12 5 ND 7.0 NO 1.5 J 2.5 J NO 9.1 3.2 J ND 2.0 J Dry NO ug/L 04/15/13 -- -- 5 ND -- -- -- 7.3 -- -- -- -- NO -- ND 1.7 J NO 11 1.2 J ND 1.7 J Dry ND ug/L 09/30/13 5 ND 4.0 J NO ND 1.2 J NO 5.6 2.7 J ND 1.7 J Dry NO ug/L 04/16/14 5 ND 6.7 NO ND 1.6 J NO 6.8 1.6 J ND 2.1 J Dry NO ug/L 10/15/14 0.15 -- 5 Dry -- -- -- 5.3 -- -- -- -- 0.43 J -- 0.70 J 1.9 J NO 4.3 J 2.5 J ND 1.2 J Dry ND ug/L 04/15/15 0.15 5 ND 3.4 J 3.1 J ND 2.0 J NO 1.6 J 0.47 J ND 0.89 J Dry NO ug/L 10/07/15 0.15 -- 5 ND -- -- -- 4.3 J -- -- -- -- NO -- ND 1.7 J NO 2.6 J 2.7 J ND 0.69 J 1.5 J ND ug/L 04/11/16 0.15 -- 5 ND -- -- -- 3.1 J -- -- -- -- 1.0 J -- ND 0.88 J NO 2.0 J 0.49 J 0.50 J 0.85 J 0.42 J ND ug/L 11/30/16 0.15 5 ND 3.6 J 0.58 J ND 0.68 J NO 2.0 J 2.1 J 0.52 J 0.63 J 0.53 J NO ug/L 04/11/17 0.15 -- 5 ND -- -- -- 3.0 J -- -- -- -- NO -- ND 1.9 B NO 2.5 B NO 0.66 B 0.60 B NO NO ug/L 12/12/17 0.15 -- 5 ND -- -- -- 2.2 J -- -- -- -- NO -- 1.1 J 0.81 J NO 0.68 J 1.8 J 2.0 J 0.84 J 1.0 J NO ug/L 06/20/18 0.15 5 ND 2.6 J 3.0 J NO 1.6 J NO 1.2 J NO 4.4 J 1.0 J ND 0.54 J 1.9 J NO ug/L 11/27/18 0.15 1 -- ND 3.6 -- -- 3.0 -- -- -- -- 0.80 J 1.8 NO ND NO 3.3 0.64 J NO 1.0 1.6 NO ug/L 04/02/19 0.15 1 ND 3.3 2.3 NO 1.1 NO 0.44 J NO 1.3 ND ND 1.3 2.5 NO ug/L 11/19/19 0.15 1 ND 2.4 3.9 1.8 ND -- 1.5 1.1 0.72 J 0.84 J NO 1.5 2.0 ND 0.43 J 0.76 J NO ug/L 04/07/20 0.15 1 -- ND NO -- -- NO ND ND 3.9 -- NO ND -- -- -- 1.9 ND ND NO 2.1 NS ug/L 10/13/20 0.15 1 ND 3.0 ND 0.96 J 1.7 ND ND 3.8 ND NO 1.7 NO ND NO 3.1 7.8 0.43 J 0.74 J 1.6 NO ug/L 04/13/21 0.15 1 -- ND 3.0 NO NO NO ND ND 2.9 1.5 1.9 1.2 NS NS NS 1.2 0.61 J 0.71 J 1.2 2.5 NS Z:\Sharetl\SME\Ops\ENV ,,] s\2030Y35&O0 3A Moore Co My ROWne LFG& WQ Monkaing\Task 01-S--Annual Waled Quality F 2020-2021\W-Ing_Dx--Sphng 2021 Even02020-10 WOMR Tables Fob App-,.- Page 19 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells KDetected Monitoring e 0 .tc.t'..`mtJParameter Ethylbenzene Units ug/L apmo 03/05/90 PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 M� PW 11 NC 2L = 600 ug/L ug/L 03/21/91 ND EPA IVICL = 700 ug/L ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 ND ND ND NO ND ug/L 09/22/95 ND ND ND ND ND ND ND ND NO ND ug/L 03/28196 ND ND ND ND ND NO NO ND ug/L 10/29/96 ND ND ND ND ND NO ND ND ug/L 04/08197 ND ND ND ND ND NO ND ND ug/L 10/29197 ND ND ND ND NO NO 9.4 ND ug/L 04/30/98 ND ND ND ND ND NO ND ND ug/L 10/14198 ND ND ND ND NO NO ND ND ug/L 04/27199 ND ND ND ND NO NO ND ND ug/L 10/21/99 ND ND ND ND ND NO ND ND ug/L 03/14100 ND ND ND ND ND ND ND ND NO NO ND ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 ND ND ND ND ND NO ND ND ug/L 04/10/01 ND ND ND ND NO NO ND ND ug/L 10/11/01 ND ND ND ND ND NO ND ND ug/L 04/18/02 ND ND ND ND ND NO ND ND ug/L 10/08/02 ND ND ND ND NO NO ND ND ug/L 04/09/03 ND ND ND ND ND NO ND ND ug/L 10/13/03 ND ND ND ND NO NO ND ND ug/L 04/26104 ND ND ND ND ND NO ND ND ug/L 10/25/04 ND ND ND ND ND NO ND ND ug/L 04/04105 ND ND ND ND ND NO ND ND ug/L 10/04105 ND ND ND ND ND NO ND ND ug/L 04/28/06 ND ND ND ND ND NO ND ND ND NO ND ND ug/L 10/09106 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/24/07 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/30/07 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/23108 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/06/08 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/13109 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/15109 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/26/10 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/19/10 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/18/11 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/10/11 1 ND ND NO ND ND NO ND ND NO Dry ND ug/L 04/17/12 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/09/12 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/13 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 09/30/13 1 ND ND NO ND ND NO ND ND NO NO Dry ND ug/L 04/16/14 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/15/14 0.13 1 Dry ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/15 0.13 1 ND ND NO ND ND NO ND ND NO NO Dry ND ug/L 10/07/15 0.13 1 ND 0.62 J NO ND ND NO 0.66 J ND ND NO ND ND ug/L 04/11/16 0.13 1 ND ND NO ND ND NO ND ND NO NO ND ND ug/L 11/30/16 0.13 1 ND 0.48 J NO ND ND NO ND ND ND NO ND ND ug/L 04/11/17 0.13 1 ND ND NO ND ND NO ND ND ND NO ND ug/L 12/12/17 0.13 1 ND 0.48 J NO ND ND NO ND ND ND NO NO ND ug/L 06/20/18 0.13 1 ND NO 0.41 J NO ND ND ND NO ND ND NO NO ND ND ug/L 11/27/18 0.13 1 -- ND NO 0.46 J NO ND ND ND NO ND ND ND NO ND ND ug/L 04/02/19 0.13 1 ND NO NO NO ND ND ND NO ND ND NO NO ND ND ug/L 11/19/19 0.13 1 ND NO 0.58 J ND ND NO ND ND ND NO ND ND ND NO ND NO ug/L 04/07/20 0.13 1 ND NO ND ND ND NO NO ND NS NS NS ND ND ND NO ND NS ug/L 10/13/20 0.13 1 ND NO NO NO 0.67 J ND ND NO ND NO ND ND NO NO ND ND ND NO ND NO ug/L 04/13/21 0.13 1 ND NO ND NO ND ND ND NO ND NO ND NS NS NS ND ND ND NO ND NS Z:\Sh,re\SME\Op,\ENV r,jed 020Y35&O3A — Co M R—, LFG & WQ M—g\—k 01 - S-- ... I — Q,,Ilty F 2020-2021 W-Iffig --- Spd,g —1 —020-10 WQMR T,— For App—,.— Page 20 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells KDetected Monitoring e 0 .tc.t'..`mtJParameter Chloromethane Units ug/L apmo 03/05/90 PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 lw�l PW-I NC 2L = 3 ug/L ug/L 03/21/91 ND ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 ND ND ND NO ND ug/L 09/22/95 ND ND ND ND NO ND ND ND NO ND ug/L 03/28196 ND ND ND ND ND ND NO ND ug/L 10/29/96 ND ND ND ND NO ND ug/L 04/08/97 ND ND ND NO NO ND ug/L 10/29/97 ND ND ND ND 26 NO ND ND ug/L 04/30/98 ND 40 ND ND ND NO ND ND ug/L 10/14/98 ND 32 ND ND ND NO ND ND ug/L 04/27/99 ND ND ND ND ND NO ND ND ug/L 10/21/99 ND ND ND ND ND NO ND ND ug/L 03/14/00 ND ND ND ND ND NO ND ND ND NO ND ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 ND ND ND ND ND NO ND ND ug/L 04/10/01 ND ND ND ND ND NO ND ND ug/L 10/11/01 ND ND ND ND ND NO ND ND ug/L 04/18/02 ND ND ND ND ND NO ND ND ug/L 10/08/02 ND ND ND ND ND NO ND ND ug/L 04/09/03 ND ND ND ND ND NO ND ND ug/L 10/13/03 ND ND ND ND ND NO ND ND ug/L 04/26/04 ND ND ND ND ND NO ND ND ug/L 10/25/04 ND ND ND ND ND NO ND ND ug/L 04/04/05 ND ND ND ND ND NO ND ND ug/L 10/04/05 ND ND ND ND ND NO ND ND ug/L 04/28/06 ND ND ND ND ND NO ND ND ND NO ND ND ug/L 10/09/06 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/24/07 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/30/07 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/23/08 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/06/08 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/13/09 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/15/09 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/26/10 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 10/19/10 1 ND ND NO ND ND 0.67 J ND ND ND NO ND ND ug/L 04/18/11 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 10/10/11 1 ND ND NO NO ND NO ND ND NO Dry ND ug/L 04/17/12 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 10/09/12 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 04/15/13 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 09/30/13 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 04/16/14 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 10/15/14 0.13 1 Dry ND NO NO ND NO ND ND ND NO Dry ND ug/L 04/15/15 0.13 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 10/07/15 0.13 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 04/11/16 0.13 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 11/30/16 0.13 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 04/11/17 0.13 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 12/12/17 0.13 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 06/20/18 0.13 1 ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 11/27/18 0.13 1 -- ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 04/02/19 0.13 1 ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 11/19/19 0.13 1 ND NO ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 04/07/20 0.13 1 ND NO ND NO ND NO NO ND NS NS NS ND ND ND NO ND NS ug/L 10/13/20 0.13 1 ND NO ND NO ND NO ND NO ND NO ND ND ND NO ND ND ND NO ND NO ug/L 04/13/21 0.13 1 ND NO ND NO ND NO ND NO ND NO ND NS NS NS ND ND ND NO ND NS Z:\Sh,re\SME\Op,\ENV r,js\2020Y35&O3A — Co M R—, LFG & WQ M—g\—k 01 - S-- ... I — Q,,Ilty F 2020-2021 W-Iffig --- Spd,g —1 —020-10 WQMR T,— - App—,.— Page 21 of 30 TABLE5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells elected Monitoring nst; Methylene chloride Units ug/L apmo 03/05/90 PQL SWSL MW-J����� MW-14 MW-11 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 M�I PW 11 NC 2L = 5 ug/L ug/L 03/21/91 ND EPA MCL = 5 ug/L ug/L 03/10/92 ND ug/L 04/20195 ND ug/L 06/27/95 ND NO ND NO ND ug/L 09/22/95 ND ND ND ND ND 40 NO ND NO ND ug/L 03/28196 ND ND ND 15 ND NO NO ND ug/L 10/29/96 ND ND ND NO ND NO ND ND ug/L 04/08197 ND ND ND ND NO NO ND ND ug/L 10/29197 ND ND ND ND NO NO ND ND ug/L 04/30/98 ND ND ND NO ND NO ND ND ug/L 10/14198 ND ND ND ND NO NO ND ND ug/L 04/27199 ND ND ND ND NO NO ND ND ug/L 10/21/99 ND ND ND NO ND NO ND ND ug/L 03/14100 ND ND ND ND ND ND ND ND NO NO ND ND ug/L 04/19/00 ND ND ND NO ND NO ND ND ug/L 10/17/00 ND ND ND NO ND NO ND ND ug/L 04/10/01 ND ND ND NO NO NO ND ND ug/L 10/11/01 ND ND ND NO ND NO ND ND ug/L 04/18/02 ND ND ND NO ND NO ND ND ug/L 10/08/02 ND ND ND ND NO NO ND ND ug/L 04/09/03 ND ND ND NO ND NO ND ND ug/L 10/13/03 ND ND ND ND NO NO ND ND ug/L 04/26104 ND ND ND ND NO NO ND ND ug/L 10/25/04 ND ND ND NO ND NO ND ND ug/L 04/04105 ND ND ND ND NO NO ND ND ug/L 10/04105 ND ND ND NO NO NO ND ND ug/L 04/28/06 ND ND ND ND ND NO ND NO ND NO ND ND ug/L 10/09106 ND ND NO ND ND NO ND NO NO NO ND ND ug/L 04/24/07 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 10/30/07 1 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 04/23108 1 ND ND NO ND ND NO ND NO NO NO ND ND ug/L 10/06/08 1 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 04/13109 1 ND ND NO ND ND NO ND NO NO NO ND ND ug/L 10/15109 1 ND ND NO ND ND NO ND NO NO NO ND ND ug/L 04/26/10 1 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 10/19/10 1 ND ND NO ND ND NO ND NO NO NO ND ND ug/L 04/18/11 1 ND ND NO ND ND NO ND NO NO NO ND ND ug/L 10/10/11 1 ND ND NO ND ND NO ND ND NO Dry ND ug/L 04/17/12 1 ND ND NO ND ND NO ND NO NO NO Dry ND ug/L 10/09/12 1 ND ND NO ND ND NO ND NO ND NO Dry ND ug/L 04/15/13 1 ND ND NO ND ND NO ND NO ND NO Dry ND ug/L 09/30/13 1 ND ND NO ND ND NO ND ND NO NO Dry ND ug/L 04/16/14 1 ND ND NO ND ND NO ND NO ND NO Dry ND ug/L 10/15/14 0.23 1 Dry ND NO ND ND NO ND NO ND NO Dry ND ug/L 04/15/15 0.23 1 ND ND NO ND ND NO ND ND NO NO Dry ND ug/L 10/07/15 0.23 1 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 04/11/16 0.23 1 ND ND NO ND ND NO ND ND NO NO ND ND ug/L 11/30/16 0.23 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/11/17 0.23 1 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 12/12/17 0.23 1 ND ND NO ND ND NO ND ND ND NO NO ND ug/L 06/20/18 0.23 1 ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 11/27/18 0.23 1 -- ND NO ND NO ND ND ND NO ND NO ND NO ND ND ug/L 04/02/19 0.23 1 ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 11/19/19 0.23 1 ND NO ND ND ND NO ND ND ND NO ND 0.64 J ND NO ND NO ug/L 04/07/20 0.23 1 ND NO ND ND ND NO NO ND NS NS NS ND NO ND NO ND NS ug/L 10/13/20 0.23 1 ND NO NO ND ND ND ND NO ND NO ND ND NO NO ND ND ND NO ND NO ug/L 04/13/21 0.23 1 ND NO ND NO ND ND ND NO ND NO ND NS NS NS ND NO ND NO ND NS Z:\Sh,re\SME\Op,\ENV r,jed 020Y35&O3A — Co M R—, LFG & WQ M—g\—k 01 - S-- ... I — Q,,Ilty F 2020-2021 W-Iffig --- Spd,g —1 —020-10 WQMR T,— For App—,.— Page 22 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Detected Monitoring PQL :D Monitoring Wells '�.- = Closed MSW Monitoring Wells & MNA Performance Monitoring Wells nil &o.n.tituent/Parameter 2-Butanone Units ug/L 10/30/07 -- -- 100 MW-JI1111r� ND -- -- -- MW-14 ND MW-11 7S -- MW-17D -- ���§W-4 -- -- ND MW-11SRIVI -- ND MW-2 ND MW-3 NO MW-6 ND MiL ND MW-8 ND MW-9�1 NO ND PW-I ND NC 2L = 4000 ug/L ug/L 04/23/08 -- -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO 4.8 J 2.8 J NO ND ND ug/L 10/06/08 100 ND ND NO ND ND NO 17 J 14 J ND NO ND ND ug/L 04/13/09 -- -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO NO ND NO ND ND ug/L 10/15/09 100 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 04/26/10 100 ND ND NO ND ND NO ND NO ND 6.8 J ND ND ug/L 10/19/10 -- -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO 3.8 J NO NO NO ND ND ug/L 04/18/11 100 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 10/10/11 -- -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO -- NO NO Dry ND ug/L 04/17/12 -- -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO NO ND NO Dry ND ug/L 10/09/12 100 ND ND NO ND ND NO ND NO ND NO Dry ND ug/L 04/15/13 -- -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO NO ND NO Dry ND ug/L 09/30/13 -- -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO 2.6 J NO ND NO Dry ND ug/L 04/16/14 100 ND ND NO ND ND NO 2.4 J 1.3 J ND 13 J Dry ND ug/L 10/15/14 1.3 -- 100 Dry -- -- -- ND -- -- -- -- NO -- ND ND NO NO NO ND NO Dry ND ug/L 04/15/15 1.3 100 ND ND NO ND ND NO ND NO ND NO Dry ND ug/L 10/07/15 1.3 100 ND ND NO ND ND NO ND NO ND NO ND ND ug/L 04/11/16 1.3 -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO 28 J 7.0 J ND 4.2 J ND ND ug/L 11/30/16 1.3 100 ND ND NO ND ND NO 1.4 J NO ND NO 6.4 J ND ug/L 04/11/17 1.3 100 ND ND NO ND ND NO ND NO ND NO 24 J ND ug/L 12/12/17 1.3 -- 100 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO NO NO NO NO ND ug/L 06/20/18 1.3 -- 100 ND NO ND NO ND ND ND NO ND NO ND NO ND ug/L 11/27/18 1.3 5 -- ND NO -- -- ND -- -- -- -- NO ND ND ND NO NO NO NO NO NO ND ug/L 04/02/19 1.3 5 -- ND NO -- -- ND -- -- -- -- NO ND ND ND NO NO 21 NO NO ND ND ug/L 11/19/19 1.3 5 ND NO ND NO ND NO ND ND ND NO ND NO ND NO 5.7 ND ug/L 04/07/20 1.3 5 -- ND NO -- -- ND NO ND NO -- NO ND NS NS NS NO NO ND NO ND NS ug/L 10/13/20 1.3 5 -- ND NO NO NO ND NO ND NO NO NO ND ND ND NO NO NO ND NO NO NO ug/L 04/13/21 1.3 5 ND NO ND NO ND NO ND NO ND NO ND NS NS NS ND NO ND NO ND NS Naphthalene ug/L 03/05/90 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- NO NC 2L = 6 ug/L ug/L 03/21/91 NO ug/L 03/10/92 NO ug/L 04/20/95 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 06/27/95 ND ND ND ND 2.5 ND NO ug/L 09/22/95 -- -- -- ND -- -- -- ND -- -- -- -- ND -- ND NO ND ND ND NO NO ND ND ug/L 03/28/96 -- -- -- ND -- -- -- ND -- -- -- -- -- -- ND NO -- ND ND NO NO ND ND ug/L 10/29/96 ND ND ND ND ND NO ND NO ug/L 04/08/97 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 10/29/97 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/30/98 ND ND ND ND ND NO ND NO ug/L 10/14/98 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/27/99 ND ND ND ND ND NO ND NO ug/L 10/21/99 ND ND ND ND ND NO ND NO ug/L 03/14/00 -- -- -- ND -- -- -- ND -- -- -- -- ND -- ND ND ND ND ND NO NO ND ND ug/L 04/19/00 ND ND ND ND ND NO ND NO ug/L 10/17/00 ND ND ND ND ND NO ND NO ug/L 04/10/01 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/11/01 ND ND ND ND ND NO ND NO ug/L 04/18/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/08/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 04/09/03 ND ND ND ND ND NO ND NO ug/L 10/13/03 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND NO ug/L 04/26/04 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND NO ug/L 10/25/04 ND ND ND ND ND NO ND NO ug/L 04/04/05 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND ND ug/L 10/04/05 ND ND ND ND ND NO ND NO ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 0.11 -- 10 ND ND -- -- 0.65 J -- -- -- -- ND 0.58 J -- -- -- ND ND -- -- -- -- ug/L 11/27/18 0.11 1 -- ND -- -- -- ND -- -- -- -- -- ND -- -- -- -- -- -- -- -- -- ug/L 04/02/19 0.11 1 ND 0.40 J ND ug/L 11/19/19 0.11 1 -- ND -- -- -- NO -- -- -- -- -- ND -- -- -- -- -- -- -- -- -- ug/L 04/07/20 0.11 1 -- ND -- -- -- 0.42 J -- -- -- -- -- ND -- -- -- -- -- -- -- -- -- ug/L 10/13/20 0.11 1 ND ND ND NO 0.49 J NO ND ND ND ND NO NO ANR ug/L 04/13/21 0.11 1 -- ND ND NO NO NO NO NO ND ND -- ND NS NS NS ANR ANR ANR ANR ANR NS Z:\Sh,re\SME\Ops\ENV rojed 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waler Qualgy F 202-021\-Ing_Dxumen5 Spring 2.1 Even02020-10 WOMR Tables For Appentll.A. Page 23 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Detected Monitoring Sa Active :D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Constituent /Parameter Tetrachloroethene Units ug/L 03/05/90 -- PQL -- SWSL -- MW-J����� -- -- MW-14 -- -- -- MW-11 7S -- MW-17D -- -- -- -- MW-11SR -- MW-1 -- MW-2 -- MW-3 -- MW-6 -- MW-7 -- MW-8 -- MW-9�611 -- -- ND NC 2L = 0.7 ug/L ug/L 03/21/91 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND EPA MCL = 5 ug/L ug/L 03/10/92 ND ug/L 04/20/95 ND ug/L 06/27/95 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 8.4 3.2 ND NO -- ND ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- ND ND ND ND ND ND NO -- ND ug/L 03/28/96 ND ND ND 12 ND ND NO -- ND ug/L 10/29/96 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO 6 ND ug/L 04/08/97 ND ND ND ND ND NO 8 ND ug/L 10/29/97 ND ND 9.2 ND ND NO 9.1 ND ug/L 04/30/98 ND ND ND ND ND NO 8.2 ND ug/L 10/14/98 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO 5 ND ug/L 04/27/99 ND ND ND ND ND NO ND ND ug/L 10/21/99 ND ND ND ND ND NO 7.6 ND ug/L 03/14/00 ND ND ND ND ND ND ND ND ND NO 3 ND ug/L 04/19/00 ND ND ND ND ND NO ND ND ug/L 10/17/00 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/10/01 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- 8.1 ND ND NO ND ND ug/L 10/11/01 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/18/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/08/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/09/03 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND ND ug/L 10/13/03 ND ND ND ND ND NO ND ND ug/L 04/26/04 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/25/04 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/04/05 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/04/05 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/28/06 -- -- -- ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 10/09/06 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 04/24/07 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 10/30/07 1 ND 0.52 J 0.35 J NO ND NO ND ND ND NO 0.38 J ND ug/L 04/23/08 -- -- 1 ND -- -- -- 0.40 J -- -- -- -- NO -- NO ND NO NO ND ND NO NO ND ug/L 10/06/08 1 ND ND NO NO ND NO ND ND ND NO 0.49 J ND ug/L 04/13/09 1 ND 0.44 J NO NO ND NO ND ND ND NO 0.49 J ND ug/L 10/15/09 1 ND ND NO ND ND NO ND ND ND NO 0.50 J ND ug/L 04/26/10 1 ND ND NO ND ND NO ND ND ND NO 0.47 J ND ug/L 10/19/10 1 ND ND NO ND ND NO ND ND ND NO 0.52 J ND ug/L 04/18/11 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO NO ND ug/L 10/10/11 1 ND ND NO NO ND NO ND ND NO Dry ND ug/L 04/17/12 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 10/09/12 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 04/15/13 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- NO ND NO NO ND ND NO Dry ND ug/L 09/30/13 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/16/14 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 10/15/14 0.17 1 Dry ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/15 0.17 1 ND ND NO ND NO NO ND ND ND NO Dry ND ug/L 10/07/15 0.17 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/11/16 0.17 -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO ND ND ug/L 11/30/16 0.17 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/11/17 0.17 -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 12/12/17 0.17 -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO ND ND ND NO ND ND ug/L 06/20/18 0.17 -- 1 ND NO -- -- ND -- -- -- -- NO ND ND ND NO NO ND ND NO ND ND ug/L 11/27/18 0.17 1 -- ND NO ND NO ND ND ND NO ND ND ND NO ND NO ug/L 04/02/19 0.17 1 ND NO ND NO ND ND ND NO ND ND ND NO ND NO ug/L 11/19/19 0.17 1 ND NO ND ND ND NO ND ND ND NO ND ND ND NO ND NO ug/L 04/07/20 0.17 1 ND NO ND ND ND ND NO ND NS NS NS ND ND ND NO ND NS ug/L 10/13/20 0.17 1 ND NO ND NO ND ND ND ND ND NO ND ND ND NO ND ND ND NO ND NO u /L 04/13/21 0.17 1 ND NO NO NO ND ND ND ND ND NO ND NS NS NS NO ND ND NO ND NS Z:\Sh,re\SME\Ops\ENV r,j s\2030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waled Qualgy F 2020-2021\W-Ing_Dx--Sphng-1Even02020-10 WOMR Tables Fob App-,.- Page 24 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SSME Project No. 4358-20-043A Detected Monitoring Sa Active :D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Constituent/Parameter Toluene Units ug/L a 03/05/90 M -- PQL -- SWSL -- MW-J����� -- -- MW-14 -- -- -- MW-11 7S -- MW-17D -- -- -- -- MW-11SR -- MW-1 -- MW-2 -- MW-3 -- MW-6 -- MW-7 -- MW-8 -- MW-9�611 -- -- ND NC 2L = 600 ug/L ug/L 03/21/91 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND EPA MCL = 1000 ug/L ug/L 03/10/92 ND ug/L 04/20/95 ND ug/L 06/27/95 ND ND ND NO ND ug/L 09/22/95 ND ND ND ND NO ND ND ND NO ND ug/L 03/28/96 ND ND ND ND ND ND NO ND ug/L 10/29/96 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND NO NO ND ND ug/L 04/08/97 ND ND ND ND ND NO ND ND ug/L 10/29/97 ND ND ND ND ND NO ND ND ug/L 04/30/98 ND ND ND ND ND NO 15 ND ug/L 10/14/98 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND ND ug/L 04/27/99 ND ND ND ND ND NO ND ND ug/L 10/21/99 ND ND -- ND ND ND NO ND ND ug/L 03/14/00 ND ND 2 ND ND NO ND ND ND NO ND ND ug/L 04/19/00 ND ND -- ND ND ND NO ND ND ug/L 10/17/00 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/10/01 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND ND ug/L 10/11/01 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/18/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/08/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/09/03 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND ND ug/L 10/13/03 ND ND ND ND ND NO ND ND ug/L 04/26/04 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/25/04 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/04/05 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/04/05 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/28/06 -- -- -- ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 10/09/06 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 04/24/07 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 10/30/07 1 ND 0.31 J NO NO ND NO ND ND ND NO ND ND ug/L 04/23/08 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 10/06/08 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 04/13/09 1 ND 0.53 J NO NO ND NO ND ND ND NO ND ND ug/L 10/15/09 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 04/26/10 -- -- 1 ND -- -- -- 0.47 J -- -- -- -- NO -- NO ND NO NO ND ND NO ND ND ug/L 10/19/10 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 04/18/11 -- -- 1 ND -- -- -- NO -- -- -- -- NO -- NO ND NO NO ND ND NO NO ND ug/L 10/10/11 1 ND ND NO NO ND NO ND ND NO Dry ND ug/L 04/17/12 -- -- 1 ND -- -- -- 0.47 J -- -- -- -- NO -- NO ND NO NO ND ND NO Dry ND ug/L 10/09/12 1 ND 0.43 J NO NO ND NO ND 0.44 J ND NO Dry ND ug/L 04/15/13 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- NO ND NO NO ND ND NO Dry ND ug/L 09/30/13 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 04/16/14 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 10/15/14 0.14 1 Dry ND NO NO ND NO ND ND 0.59 J NO Dry ND ug/L 04/15/15 0.14 1 ND ND NO NO ND NO ND ND ND NO Dry ND ug/L 10/07/15 0.14 1 ND ND NO NO ND NO ND ND 0.56 J NO ND ND ug/L 04/11/16 0.14 1 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 11/30/16 0.14 1 ND ND NO ND ND NO 0.48 J ND 0.60 J NO ND ND ug/L 04/11/17 0.14 -- 1 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND 1.0 B NO ND ND ug/L 12/12/17 0.14 1 ND ND NO ND ND NO ND ND 0.64 J NO 0.44 J ND ug/L 06/20/18 0.14 -- 1 ND NO -- -- ND -- -- -- -- NO ND ND ND NO NO ND NO NO ND ND ug/L 11/27/18 0.14 1 -- ND NO ND NO ND ND ND NO ND ND 0.48 J NO ND ND ug/L 04/02/19 0.14 1 -- ND NO -- -- ND -- -- -- -- NO ND ND ND NO NO ND ND NO ND ND ug/L 11/19/19 0.14 1 ND NO ND NO ND NO ND ND ND NO ND ND 0.48 J NO 0.43 J ND ug/L 04/07/20 0.14 1 ND NO ND NO ND NO NO ND NS NS NS ND ND 0.40 J NO ND NS ug/L 10/13/20 0.14 1 ND NO ND NO 0.48 J NO ND NO ND NO ND ND ND NO 0.40 J ND 0.51 J 0.43 J ND NO u /L 04/13/21 0.14 1 ND NO ND NO 0.48 J NO ND NO ND NO ND NS NS NS ND ND ND NO ND NS Z:\Sh,re\SME\Ops\ENV r,j s\2030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waled Qualgy F 2020-2021\W-Ing_Dx--Sphng-1Even02020-10 WOMR Tables Fob App-,.- Page 25 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SSME Project No. 4358-20-043A Active :D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells &Detected Monitoring eth'..'mmdParameter Trichloroethene Units ug/L 03/05/90 -- PQL -- SWSL -- MW-5 -- -- MW-14 -- -- -- MW-11 7S -- MW-17D -- -- -- -- MW-11SR -- MW-1 -- MW-2 -- MW-3 -- MW-6 -- MW-7 -- MW-8 -- MW-9�611 -- -- ND NC 2L = 3 ug/L ug/L 03/21/91 ND EPA MCL = 5 ug/L ug/L 03/10/92 ND ug/L 04/20/95 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 06/27/95 3.6 ND ND NO ND ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- ND ND NO ND ND NO NO -- ND ug/L 03/28/96 ND ND ND 6.4 ND ND NO -- ND ug/L 10/29/96 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO 5 ND ug/L 04/08/97 ND ND ND ND ND NO ND ND ug/L 10/29/97 ND ND ND ND ND NO 5.9 ND ug/L 04/30/98 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO 5.4 ND ug/L 10/14/98 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/27/99 ND ND ND ND ND NO ND ND ug/L 10/21/99 ND ND ND ND ND NO ND ND ug/L 03/14/00 ND ND ND ND ND NO ND ND ND NO 3 ND ug/L 04/19/00 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/17/00 ND ND ND ND ND NO ND ND ug/L 04/10/01 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- 5.2 ND ND NO ND ND ug/L 10/11/01 ND ND ND ND ND NO ND ND ug/L 04/18/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/08/02 ND ND ND ND ND NO ND ND ug/L 04/09/03 ND ND ND ND ND NO ND ND ug/L 10/13/03 ND ND ND ND ND NO ND ND ug/L 04/26/04 ND ND ND ND ND NO ND ND ug/L 10/25/04 ND ND ND ND ND NO ND ND ug/L 04/04/05 ND ND ND ND ND NO ND ND ug/L 10/04/05 ND ND ND ND ND NO ND ND ug/L 04/28/06 -- -- -- ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 10/09/06 ND ND NO ND ND NO ND ND ND NO ND ND ug/L 04/24/07 -- -- -- ND -- -- -- NO -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 10/30/07 1 ND 1.5 J 0.40 J ND 0.30 J NO ND ND 0.31 J NO 0.46 J ND ug/L 04/23/08 -- -- 1 ND -- -- -- 1.0 -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 10/06/08 1 ND 0.76 J NO ND ND NO ND ND ND NO 0.46 J ND ug/L 04/13/09 -- -- 1 ND -- -- -- 1.0 -- -- -- -- NO -- ND ND NO NO ND ND NO 0.74 J ND ug/L 10/15/09 1 ND 0.97 J 0.51 J 0.64 J ND NO ND ND 0.44 J NO 0.50 J ND ug/L 04/26/10 1 ND 0.85 J NO NO ND NO ND NO ND NO 0.50 J ND ug/L 10/19/10 1 ND 0.59 J NO NO ND NO ND NO ND NO 0.42 J ND ug/L 04/18/11 1 ND ND NO NO ND NO ND NO ND NO ND ND ug/L 10/10/11 1 ND 0.77 J NO ND ND NO ND ND NO Dry ND ug/L 04/17/12 1 ND 0.50 J NO ND ND NO ND ND ND NO Dry ND ug/L 10/09/12 1 ND 0.54 J NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/13 -- -- 1 ND -- -- -- NO -- -- -- -- NO -- ND ND NO NO ND ND NO Dry ND ug/L 09/30/13 1 ND ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/16/14 -- -- 1 ND -- -- -- 0.41 J -- -- -- -- NO -- ND ND NO NO ND ND NO Dry ND ug/L 10/15/14 0.15 1 Dry ND NO ND ND NO ND ND ND NO Dry ND ug/L 04/15/15 0.15 -- 1 ND -- -- -- 0.50 J -- -- -- -- NO -- NO ND NO NO ND ND NO Dry ND ug/L 10/07/15 0.15 1 ND ND NO NO ND NO ND ND ND NO 0.53 J ND ug/L 04/11/16 0.15 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 11/30/16 0.15 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 04/11/17 0.15 1 ND ND NO NO 0.95 J NO ND ND ND NO ND ND ug/L 12/12/17 0.15 1 ND ND NO NO ND NO ND ND ND NO ND ND ug/L 06/20/18 0.15 1 ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 11/27/18 0.15 1 -- ND NO ND NO ND ND ND NO ND ND ND NO ND ND ug/L 04/02/19 0.15 1 -- ND NO -- -- ND -- -- -- -- NO ND ND ND NO NO ND ND NO ND ND ug/L 11/19/19 0.15 1 ND NO ND NO ND NO ND ND ND NO ND NO ND NO ND ND ug/L 04/07/20 0.15 1 -- ND NO -- -- ND NO ND NO -- NO NO NS NS NS NO ND ND NO ND NS ug/L 10/13/20 0.15 1 ND NO ND NO ND NO ND NO ND NO ND ND ND NO ND NO ND NO ND NO ug/L 04/13/21 0.15 1 ND NO ND NO ND NO ND NO ND NO ND NS NS NS NO ND ND NO ND NS Z:\Sh,re\SME\Ops\ENV rojed 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waler Qualgy F 2020-2021\W-Ing_Dx--Spring-1Even02020-10 WOMR Tables For App-,.- Page 26 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SSME Project No. 4358-20-043A Active :D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells &Detected Monitoring eth'..ummdParameter Vinyl chloride Units ug/L 03/05/90 -- PQL -- SWSL -- MW-5 -- -- MW-14 -- -- -- MW-11 7S -- MW-17D -- -- -- -- MW-11SR -- MW-1 -- MW-2 -- MW-3 -- MW-6 -- MW-7 -- MW-8 -- MW-9�611 -- -- ND NC 2L = 0.03 ug/L ug/L 03/21/91 ND EPA MCL = 2 ug/L ug/L 03/10/92 ND ug/L 04/20/95 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 06/27/95 5.3 9.4 40.3 15.9 ND ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- ND ND NO NO ND 45 20 -- ND ug/L 03/28/96 ND ND 13 ND ND 12 NO ND ug/L 10/29/96 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND ND ug/L 04/08/97 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/29/97 ND ND ND ND ND NO ND ND ug/L 04/30/98 ND ND ND 10 ND NO ND ND ug/L 10/14/98 ND 35 ND ND ND NO ND ND ug/L 04/27/99 ND 58 18 ND ND NO ND ND ug/L 10/21/99 -- -- -- ND -- -- -- 28 -- -- -- -- -- -- -- -- -- 21 ND ND NO 17 ND ug/L 03/14/00 -- -- -- ND -- -- -- 16 -- -- -- -- ND -- ND 8 ND 15 5 4 NO 9 ND ug/L 04/19/00 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- 25 21 ND NO 11 ND ug/L 10/17/00 -- -- -- ND -- -- -- 40 -- -- -- -- -- -- -- -- -- 14 ND 28 13 ND ND ug/L 04/10/01 -- -- -- ND -- -- -- 35 -- -- -- -- -- -- -- -- -- 25 16 ND 11 16 ND ug/L 10/11/01 ND 12 15 12 28 NO ND ND ug/L 04/18/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- 13 10.8 17.7 NO ND ND ug/L 10/08/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 04/09/03 -- -- -- ND -- -- -- 18.5 -- -- -- -- -- -- -- -- -- ND ND ND NO NO ND ug/L 10/13/03 -- -- -- ND -- -- -- 12.5 -- -- -- -- -- -- -- -- -- ND ND ND 11.4 ND ND ug/L 04/26/04 ND 15.9 ND ND 19.4 NO ND ND ug/L 10/25/04 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND 13.3 NO ND ND ug/L 04/04/05 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND ND ug/L 10/04/05 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- 11.7 ND 12.8 NO ND ND ug/L 04/28/06 -- -- -- ND -- -- -- 12.8 -- -- -- -- NO -- ND ND NO 14.2 ND ND NO ND ND ug/L 10/09/06 ND ND NO ND ND NO ND ND 12.4 NO ND ND ug/L 04/24/07 -- -- -- ND -- -- -- 7.6 -- -- -- -- NO -- ND ND NO ND ND ND -- ND ND ug/L 10/30/07 1 ND 2.8 0.30 J ND 2.7 NO 3.6 ND 4.2 1.2 ND ND ug/L 04/23/08 -- -- 1 ND -- -- -- 5.1 -- -- -- -- NO -- ND 1.4 NO ND 3.0 ND 1.8 ND ND ug/L 10/06/08 1 ND 5.8 NO ND 1.2 NO 3.4 J 2.1 ND 1.9 3.9 ND ug/L 04/13/09 -- -- 1 ND -- -- -- 5.4 -- -- -- -- NO -- ND 1.6 NO 1.3 ND 0.67 J 1.7 3.0 ND ug/L 10/15/09 -- -- 1 ND -- -- -- 3.5 -- -- -- -- 0.62 J -- 0.92 J 2.1 NO 4.0 ND 5.3 1.1 ND ND ug/L 04/26/10 -- -- 1 ND -- -- -- 5.4 -- -- -- -- NO -- ND 1.9 NO 2.0 2.4 0.81 J 1.6 2.4 ND ug/L 10/19/10 -- -- 1 ND -- -- -- ND -- -- -- -- NO -- ND 1.3 NO ND ND 0.53 J ND 2.1 ND ug/L 04/18/11 1 ND 2.8 NO ND 0.91 J NO 0.78 J 0.90 J 1.0 0.71 J 2.2 ND ug/L 10/10/11 1 ND 3.1 NO ND 0.86 J NO 2.8 -- 3.7 1.2 Dry ND ug/L 04/17/12 1 ND 3.7 NO 0.39 J 0.79 J NO 2.0 1.5 ND 1.1 Dry ND ug/L 10/09/12 1 ND 2.6 NO ND 1.3 NO 2.0 2.0 ND 1.4 Dry ND ug/L 04/15/13 -- -- 1 ND -- -- -- 3.5 -- -- -- -- NO -- ND 0.61 J NO 2.6 1.5 ND 1.1 Dry ND ug/L 09/30/13 1 ND 2.3 NO ND ND NO 3.1 1.4 ND 0.85 J Dry ND ug/L 04/16/14 -- -- 1 ND -- -- -- 3.1 -- -- -- -- NO -- ND ND NO 1.7 1.8 ND 1.3 Dry ND ug/L 10/15/14 0.32 1 Dry 2.3 NO ND 0.62 J NO 2.2 1.5 0.57 J 0.55 J Dry ND ug/L 04/15/15 0.32 -- 1 ND -- -- -- 1.8 -- -- -- -- NO -- NO 0.72 J NO 0.78 J ND ND NO Dry ND ug/L 10/07/15 0.32 1 ND 3.4 NO NO 0.61 J NO 2.7 1.5 ND 0.51 J 1.2 ND ug/L 04/11/16 0.32 1 ND 3.3 NO NO ND NO 0.72 J 0.71 J 0.48 J 0.42 J NO ND ug/L 11/30/16 0.32 1 ND 2.5 NO NO ND NO 1.3 1.1 0.64 J NO 0.48 J ND ug/L 04/11/17 0.32 1 ND 1.9 NO NO ND NO 1.4 0.45 J 0.65 J NO NO ND ug/L 12/12/17 0.32 1 ND -- 2.0 NO -- NO ND NO 1.5 1.1 0.99 J NO 0.47 J ND ug/L 06/20/18 0.32 1 ND 2.2 2.7 NO 1.9 ND ND NO 2.1 2.1 ND NO ND ND ug/L 11/27/18 0.32 1 -- ND 1.8 2.3 NO 2.3 ND ND NO 1.9 1.1 ND NO 0.50 J ND ug/L 04/02/19 0.32 1 -- ND 2.1 -- -- 1.4 -- -- -- -- NO 2.1 ND ND NO NO 2.4 ND NO NO ND ug/L 11/19/19 0.32 1 ND 1.3 2.5 NO ND -- NO 2.0 ND ND NO 1.3 1.3 ND NO 0.74 J ND ug/L 04/07/20 0.32 1 -- ND 1.3 -- -- 1.3 NO ND 1.8 -- NO 2.0 NS NS NS NO 0.89 J ND NO NO NS (Verification Event) ug/L 06/05/20 0.32 1 ND ANR ANR ANR ANR ANR ANR 1.1 ANR ANR ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 10/13/20 0.32 1 -- ND 1.8 NO NO 2.3 0.79 J ND 1.9 ND NO 2.4 ND ND NO 1.1 5.4 ND NO 1.1 NO ug/L 04/13/21 0.32 1 ND 2.2 0.86 J NO 0.85 J NO ND 1.6 0.6 il 0.5 J 1.8 NS NS NS 1.2 2.2 ND NO ND NS Z:\Sh,re\SME\Ops\ENV rojed 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waler Quality F 2020-2021\W-Ing_Dx--Spring-1Even02020-10 WOMR Tables For App-,.- Page 27 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SSME Project No. 4358-20-043A Sa Active :D Monitoring Wells ...... Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent �R,, /Parameter Xylenes (Total) Units ug/L 03/05/90 -- PQL -- SWSL -- MW-5dj����� -- -- -- -- MW-14 -- MW-11 7S -- MW-17D -- -- -- -- MW-11SR -- MW-1 -- MW-2 -- MW-3 -- MW-6 -- MW-7 -- MW-8 -- MW-q�p -- -- ND NC 2L = 500 ug/L ug/L 03/21/91 NO EPA MCL = 10000 ug/L ug/L 03/10/92 NO ug/L 04/20/95 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ND ug/L 06/27/95 ND ND 4.7 4.3 NO ug/L 09/22/95 -- -- -- ND -- -- -- -- -- -- -- -- ND -- ND ND NO NO ND NO NO -- ND ug/L 03/28/96 ND ND ND ND ND ND NO NO ug/L 10/29/96 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND NO NO ND NO ug/L 04/08/97 ND ND ND ND ND NO ND NO ug/L 10/29/97 ND ND 10.2 ND ND NO ND NO ug/L 04/30/98 ND ND ND ND ND NO 18 NO ug/L 10/14/98 ND ND ND ND ND NO ND NO ug/L 04/27/99 ND ND ND ND ND NO ND NO ug/L 10/21/99 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 03/14/00 ND ND ND ND ND NO ND ND ND NO ND NO ug/L 04/19/00 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND NO ug/L 10/17/00 ND ND ND ND ND NO ND NO ug/L 04/10/01 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND NO ug/L 10/11/01 ND ND ND ND ND NO ND NO ug/L 04/18/02 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- NO ND ND NO ND NO ug/L 10/08/02 ND ND ND ND ND NO ND NO ug/L 04/09/03 ND ND ND ND ND NO ND NO ug/L 10/13/03 ND ND ND ND ND NO ND NO ug/L 04/26/04 ND ND ND ND ND NO ND NO ug/L 10/25/04 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/04/05 ND ND ND ND ND NO ND NO ug/L 10/04/05 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND NO ND NO ug/L 04/28/06 -- -- -- ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND NO ug/L 10/09/06 ND ND NO ND ND NO ND ND ND NO ND NO ug/L 04/24/07 -- -- -- ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND NO ug/L 10/30/07 5 ND 0.52 J NO ND ND NO 0.34 J ND 4.4 J 0.44 J ND NO ug/L 04/23/08 -- -- 5 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND ND NO ND ND ug/L 10/06/08 5 ND ND NO ND ND NO ND ND ND NO 5.4 NO ug/L 04/13/09 -- -- 5 ND -- -- -- 0.47 J -- -- -- -- NO -- ND ND NO NO ND ND 0.41 J 0.98 J NO ug/L 10/15/09 5 ND 0.51 J NO ND ND NO ND ND 0.46 J 0.45 J ND NO ug/L 04/26/10 5 ND 0.52 J NO ND ND NO ND ND ND NO 1.3 J NO ug/L 10/19/10 5 ND 0.48 J NO ND ND NO ND ND 0.47 J 0.41 J ND NO ug/L 04/18/11 5 ND ND NO ND ND NO ND ND ND NO ND NO ug/L 10/10/11 5 ND ND NO ND ND NO ND ND NO Dry NO ug/L 04/17/12 5 ND 0.56 J NO ND ND NO ND ND ND NO Dry NO ug/L 10/09/12 5 ND 0.45 J NO ND ND NO ND ND ND NO Dry NO ug/L 04/15/13 -- -- 5 ND -- -- -- NO -- -- -- -- NO -- ND ND NO NO ND ND NO Dry NO ug/L 09/30/13 5 ND ND NO ND ND NO ND ND ND NO Dry NO ug/L 04/16/14 -- -- 5 ND -- -- -- ND -- -- -- -- NO -- ND ND NO NO ND NO NO Dry NO ug/L 10/15/14 0.45 5 Dry ND NO ND ND NO ND ND 0.60 J NO Dry NO ug/L 04/15/15 0.45 -- 5 ND -- -- -- ND -- -- -- -- NO -- NO ND NO NO ND ND NO Dry ND ug/L 10/07/15 0.45 5 ND ND NO NO ND NO ND ND 0.93 J NO ND NO ug/L 04/11/16 0.45 5 ND ND NO NO ND NO ND ND ND NO ND NO ug/L 11/30/16 0.45 5 ND ND NO NO ND NO ND ND 0.61 J NO ND NO ug/L 04/11/17 0.45 5 ND ND NO NO ND NO ND ND 1.3 B NO ND NO ug/L 12/12/17 0.45 5 ND ND NO NO ND NO ND ND 1.2 J NO ND NO ug/L 06/20/18 0.45 5 ND NO ND NO ND NO ND NO ND ND 0.99 J NO ND NO ug/L 11/27/18 0.45 3 -- ND NO ND NO ND NO ND NO ND ND ND NO ND NO ug/L 04/02/19 0.45 3 ND NO ND NO ND NO ND NO ND ND ND 0.45 J ND NO ug/L 11/19/19 0.45 3 ND NO ND NO ND NO ND NO ND NO ND ND 2.2 J NO ND NO ug/L 04/07/20 0.45 3 ND NO 0.48 J NO ND NO NO ND NS NS NS ND ND 0.7 J NO ND NS ug/L 10/13/20 0.45 3 ND NO ND NO 0.49 J NO ND NO ND NO ND NO ND NO ND 2.2 0.46 J ND NO ug/L 04/13/21 0.45 3 ND NO ND NO ND NO ND NO ND NO ND NS NS NS ND ND ND NO ND NS 1,4-Dioxane ug/L 11/27/18 1.2 2.0 ND 5.6 15 2.8 7.3 NO 7.8 NO 2.9 4.6 6.3 39 ND NO NC 2L= 3.0 ug/L ug/L 04/02/19 1.2 2.0 ND 4.8 11 -- -- 2.0 8.4 ND 7.5 NO 1.6 J 4.0 7.2 23 ND NO ug/L 11/19/19 0.8 2.0 ND 3.9 15 1.6 J 5.2 2.0 4.8 2.3 14 1.1 J 1.4 J 10 39 22 ND NO ug/L 04/07/20 0.8 2.0 ND 5.9 -- -- 15 3.0 8.5 11 -- 2.2 4.3 NS NS NS 2.5 1 J 16 29 ND NS ug/L 10/13/20 0.8 2.0 ND 4.4 3.4 2.5 14 2.3 6.8 10 2.8 1.3 5.4 ND 9.7 1.0 J 2.0 6.9 29 25 ND NO ug/L 04/13/21 0.8 2.0 ND 5.3 3.8 3.4 5 0.9 J 10.0 15 7.9 5.3 7.0 NS NS NS 1.7 3.9 22 30 2.2 NS etra y ro uran 0.53 1.0 -- ND -- -- 1.8 -- -- -- -- NO 5.5 -- -- -- -- -- -- -- -- -- ug 7/18 0.53 1.0-- ND NO ND NO ND -- -- -- ug/L 04/02/19 0.53 1.0-- ND NO ND NO 15 -- -- -- ug/L 11/19/19 0.53 1.0-- ND NO ND NO ND NO ND -- -- -- ug/L 10/13/20 0.53 1.0 ND 2.4 ND NO 3.3 NO ND -- 5.8 ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 04/13/21 0.53 1.0 ND NO ND NO ND NO ND ND ND 8.6 7.5 NS NS NS ANR ANR ANR ANR ANR NS Z:\Sh,re\SME\Ops\ENV rojed 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waler Qualgy F 2020-2021\W-Ing_Dx--Spring-1Even02020-10 WOMR Tables For App-,.- Page 28 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Constituent/Parameter Units PW Active :D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Sulfide mg/L in 04/11/17 MW-5dj����� ND MW-14 MW-11 7S MW-17D MW-18 NO M&W-4 0.35 J MW-11SRIVI ND MW-2 ND MW-3 NO MW-6 0.89 MJ6MMA-8 J 0.82 J MW MW-9�0 0.77 J 1.00 mg/L 12/12/17 ND -- 0.54 J 0.16 J ND ND NO 0.11 J 1.30 J 2.70 J 0.66 J mg/L 06/20/18 0.01 0.1 ND 0.38 J 0.50 J NO ND ND NO 0.13 J NO 2.70 J ND mg/L 11/27/18 0.01 0.1 ND 0.17 J -- -- -- -- -- 0.62 J -- NO -- ND ND NO 0.97 J 3.20 1.40 ND -- mg/L 04/02/19 0.01 0.1 ND 1.50 -- -- -- -- -- 0.46 J -- NO -- ND ND NO 0.65 J 0.57 J 1.70 0.21 J -- mg/L 04/07/20 ND 0.83 J 0.42 J 0.16 J 0.28 J 0.16 2.70 1.00 0.58 J mg/L 10/13/20 ND 0.22 J ND NO 0.12 NO ND 0.42 J ND ND 0.17 J ND ND NO 0.16 NO 0.78 J 1.40 0.27 J mg/L 04/13/21 ND 0.49 J ND NO 0.37 NO ND 0.30 J ND ND 1.10 NS NS NS 0.19 NO 1.10 1.60 0.35 J NS Chloride mg/L 04/11/17 ND -- -- -- -- -- -- 42 -- 43 -- NO 40 3.7 J 16 2.9 J 95 ND -- mg/L 12/12/17 2 J -- 47 31 9.9 54 4.1 J 20 14 92 ND mg/L 06/20/18 2.2 5.0 ND 6.9 44 34 ND 63 2.8 J 15 7.1 110 3.1 J mg/L 11/27/18 2.2 5.0 ND 3.9 J 42 20 ND 30 2.7 J 16 6.3 120 ND mg/L 04/02/19 2.2 5.0 ND 3.5 J 39 20 -- ND 29 3.8 J 13 5.0 94 ND mg/L 04/07/20 ND 8.4 -- -- 33 -- -- 56 -- -- 3.2 J -- -- -- 14 4.0 J 100 3.1 J mg/L 10/13/20 2.5 J 21 7.7 5.8 52 22 3.0 41 14 8.9 27 2.3 J 38 5.5 13 20 69 100 D 2.9 J mg/L 10/13/20 2.9 J 22 8.4 6.8 15 8.2 2.9 51 36 30 34 NS NS NS 13 10 50 99 D 3.1 J NS Nitrate as N mg/L 04/11/17 240 J -- -- -- -- -- -- 0.100 J -- 14 -- 0.950 J 0.180 J NO 0.077 J 0 J 0.140 J 0.180 J mg/L 12/12/17 550 J 0.130 J 0.280 J 0.600 J 1.100 J NO 0.140 J 0 J 0.120 J 0.160 J mg/L 06/20/18 0.025 450 J 0.120 J 6.000 J 0.840 J 1.700 J NO 0.140 J 0 J 0.170 J 0.140 J mg/L 11/27/18 0.025 410 0.170 4.400 1.200 0.050 J NO 0.130 0 0.200 0.240 mg/L 04/07/20 0.025 320 -- -- -- -- 0.089 J 0 J 0.090 J 0.076 J mg/L 10/13/20 380 J ANR ANR ANR ANR ANR ANR ANR ANR 2.300 J 90 J 0.850 0.130 NO 0.110 0 0.120 0.100 0.510 mg/L 04/13/21 1400 ANR ANR ANR ANR ANR ANR ANR ANR 0.220 ND NS NS NS ND 1 ND NO ND NS Nitrite as N mg/L 04/11/17 ND 19 J 0.030 J ND ND NO 0.033 J NO NO ND mg/L 12/12/17 ND NO NO ND ND NO ND NO NO ND mg/L 06/20/18 0.017 0.1 ND NO NO ND ND NO ND NO NO ND mg/L 11/27/18 0.017 0.1 ND NO NO ND ND NO 0.017 J NO NO ND mg/L 04/02/19 0.017 0.1 ND 27 J NO ND ND NO 0.098 J NO NO ND mg/L 04/07/20 ND -- -- -- -- -- -- -- -- -- -- -- -- -- NO ND NO 0.038 J -- mg/L 10/13/20 ND ANR ANR ANR ANR ANR ANR ANR ANR NO ND ND NO NO NO ND NO NO ND mg/L 04/13/21 ND ANR ANR ANR ANR ANR ANR ANR ANR NO ND NS NS NS NO ND NO NO NO NS Total Dissolved Solids mg/L 06/20/18 50 50 ND NO -- -- -- -- -- 180 -- 200 -- -- -- -- -- -- -- -- -- mg/L 11/27/18 50 50 ND NO -- -- -- -- -- 160 -- 110 -- -- -- -- -- -- -- -- -- mg/L 04/02/19 50 50 ND NO -- -- -- -- -- 270 -- 220 -- -- -- -- -- -- -- -- -- mg/L 04/07/20 ND 66 -- -- 420 -- -- 280 -- -- 290 mg/L 10/13/20 ND 250 96 50 240 350 200 430 160 150 550 m /I 04/13/21 10 10 ND 270 82 30 74 240 250 470 350 520 680 NS NS NS ANR ANR ANR ANR ANR NS Sulfate as SO4 mg/L 04/11/17 ND -- -- -- -- -- -- 14 J -- 98 J -- 9.3 J 10 J 8.7 J 14 J NO 3.5 J ND mg/L 12/12/17 ND 11 J 38 J 10.0 J 16 J 10 J 8.9 J NO NO 1.8 J mg/L 06/20/18 2.9 5.0 ND NO 9.8 J 22 J 8.6 J 13 J 9.1 J 7.3 J NO NO 3.1 J mg/L 11/27/18 2.9 5.0 ND NO -- -- -- -- -- 8.1 -- 29 -- 7.6 5.2 7.6 9.2 NO NO 1.1 -- mg/L 04/02/19 2.9 5.0 ND NO -- -- -- -- -- 9.2 -- 61 -- 8.2 4.5 J 7.9 1.6 NO NO 8.7 -- mg/L 04/07/20 2.9 5 ND NO -- -- 35 -- -- NO -- -- 38 -- -- -- 10 NO NO 9.7 -- mg/L 10/13/20 2.9 5 ND 13 16 9.1 7.1 99 35 7 12 32 ND 8.0 5.5 8.4 7.2 NO NO NO 7.2 mg/L 04/13/21 2.9 5 2900 12 18 10 19 20 33 45 23 110 14 NS NS NS 11 NO NO NO 6.8 NS Total Alkalinity as CaCO3 mg/L 04/11/17 ND -- -- -- -- -- -- 150 -- 470 -- NO 230 NO 200 110 920 110 -- mg/L 12/12/17 ND -- -- -- -- -- -- 170 -- 350 -- 49 290 D NO 260 110 1,000 130 mg/L 06/20/18 14 15 ND 87 170 94 NO 310 NO 250 150 1,100 85 mg/L 11/27/18 14 15 ND 81 130 41 NO 180 NO 240 160 890 90 mg/L 04/02/19 14 15 ND NO -- 120 20 -- NO 170 NO ND NO 710 40 mg/L 04/07/20 ND 51 -- 190 -- -- 140 -- -- 170 -- 210 110 740 83 mg/L 10/13/20 ND 220 49 NO 190 140 120 290 95 39 620 NO 180 NO 190 120 240 D 830 96 m /I 04/13/21 28 30 ND 260 34 21 42 24 160 320 D 200 D 260 730 D NS NS NS 240 300 230 D 760 110 NS Total Organic Carbon mg/L 04/11/17 ND -- -- -- -- -- -- 9.2 -- 43 -- 1 9.1 0.780 J 26 13 59 37 mg/L 12/12/17 ND -- -- -- -- -- -- 13 -- 27 -- 5 8.7 9.2 15 7.1 40 14 mg/L 06/20/18 0.34 1.0 ND -- -- -- -- -- -- 12 -- 11 -- 1.7 12 1.1 19 6.5 66 4.8 -- mg/L 11/27/18 0.34 1.0 470 J 15 9.3 2 7.8 1.0 25 6.0 68 3.3 mg/L 04/02/19 0.34 1.0 ND -- -- -- -- -- -- 12 -- 11 -- 1.1 6.2 0.95 J 56 9.4 42 43 -- mg/L 04/07/20 ND -- -- -- -- -- -- -- -- -- -- -- -- -- 26 17 32 1.7 -- mg/L 10/13/20 ND ANR ANR ANR ANR ANR ANR ANR ANR 11 22 0.9 J 30 21 21 37 2.6 mg/L 04/13/21 0.54 1 1000 ANR ANR ANR ANR ANR ANR ANR ANR 42 34 NS NS NS 57 26 18 34 2.5 NS Z:\Sh,re\SME\Ops\ENV rojed 030Y35&O0 3A Moore Co My ROWne LFG B WQ Monkaing\Task 01-S--Annual Waler Qualgy F 2020-2021\W-Ing_Dx--Spring-1Even02020-10 WOMR Tables For App-,.- Page 29 of 30 TABLE 5A Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Monitoring ituent/Parameter Units PQL SWSL Active :DClosed MSW Monitoring Wells & MNA Performance Monitoring Wells &Dut.eticted on & Nitrate/Nitrite as N mg/L ;Apo 04/11/17 MW-5 J111PO 240 MW-14 MW-11 7S 0.120 W-4 14.0 MW-11SR I= 0.950 MW-2 0.180 MW-3 NO -6 &. 0.110 MIJ 0.160 MW.8 MW_9 0.140 �w 0.180 mg/L 12/12/17 550 0.130 2.8 0.600 1.100 NO 0.140 0.140 0.120 0.160 mg/L 06/20/18 0.041 0.1 450 0.120 6.0 0.840 1.700 NO 0.140 0.110 0.170 0.140 mg/L 11/27/18 0.041 0.1 410 -- -- -- -- -- -- 0.170 -- 4.4 -- 1.200 0.050 J NO 0.150 0.200 0.200 0.240 -- mg/L 04/02/19 0.041 0.1 320 0.110 3.6 1.000 0.048 J NO 0.150 0.080 J 0.100 0.120 mg/L 04/07/20 0.041 0.1 320 0.089 J 0.095 J 0.099 J 0.110 mg/L 10/13/20 0.041 0.1 380 J ANR ANR ANR ANR ANR ANR ANR ANR 2.3 J 0.090 J 0.85 0.130 -- 0.110 0.200 0.120 0.100 0.510 mg/L 04/13/21 0.041 0.1 1400 1 ANR ANR ANR ANR ANR ANR ANR ANR 0 NO NS NS NS NO 0.650 NO NO NO NS Ethane mg/L 04/11/17 NO -- -- -- -- -- -- NO -- NO -- ND NO NO NO NO NO NO -- mg/L 12/12/17 ND NO NO ND ND NO ND NO NO ND mg/L 06/20/18 0.0013 0.002 ND NO NO ND ND NO ND NO NO ND mg/L 11/27/18 0.0013 0.002 ND NO NO ND ND NO ND NO NO ND mg/L 04/02/19 0.0013 0.002 ND NO NO ND ND NO ND NO NO ND mg/L 04/07/20 ND ND NO NO ND mg/L 10/13/20 ND ANR ANR ANR ANR ANR ANR ANR ANR NO ND ND NO NO ND NO ND mg/L 04/13/21 0.0051 0.006 ND ANR ANR ANR ANR ANR ANR ANR ANR NO ND NS NS NS NO NO NO NO ND NS Ethene mg/L 04/11/17 ND -- -- -- -- -- -- NO -- NO -- ND NO NO NO NO NO ND -- mg/L 12/12/17 ND -- -- -- -- -- -- NO -- NO -- ND NO NO NO NO NO ND mg/L 06/20/18 0.0015 0.003 ND -- -- -- -- -- -- NO -- NO -- ND NO NO NO NO NO ND -- mg/L 11/27/18 0.0015 0.003 ND -- -- -- -- -- -- NO -- NO -- ND ND NO NO ND NO ND -- mg/L 04/02/19 0.0015 0.003 ND -- -- -- -- -- -- NO -- NO -- ND NO NO NO NO NO ND -- mg/L 04/07/20 ND -- -- -- -- -- -- -- -- -- -- -- -- -- NO NO NO ND -- mg/L 10/13/20 ND ANR ANR ANR ANR ANR ANR ANR ANR NO ND NO NO ND NO ND NO ND mg/L 04/13/21 0.0051 0.006 ND ANR ANR ANR ANR ANR ANR ANR ANR NO ND NS NS NS ND NO ND NO ND NS Methane mg/L 04/11/17 496 J 5.06 0.372 0.636 J 0.099 NO 6.05 1.56 5.90 5.10 mg/L 12/12/17 567 J 1.67 0.879 0.264 0.012 NO 1.79 1.62 2.34 3.58 mg/L 06/20/18 0.45 1.00 ND 3.10 0.154 NO 0.041 NO 1.45 2.97 2.35 0.40 mg/L 11/27/18 0.45 1.00 ND 1.06 0.948 NO 0.019 NO 3.84 4.02 5.64 0.96 mg/L 04/02/19 0.45 1.00 ND 3.60 0.039 0.566 J 0.055 NO 4.06 5.93 5.04 2.08 mg/L 04/07/20 ND -- -- -- -- -- -- -- -- -- -- -- -- -- 2.16 1.94 0.67 1.36 -- mg/L 10/13/20 ND ANR ANR ANR ANR ANR ANR ANR ANR NO 4.46 NO -- NO 3.68 6.150 5.68 D 3.20 mg/L 04/13/21 0.084 0.105 NO ANR ANR ANR ANR ANR ANR ANR ANR 0.323 3.28 NS NS NS 12.4 5.91 D 6.370 D NO 1.64 NS Carbon dioxide mg/L 04/07/20 17.2 51 55.7 499 288 451 365 mg/L 10/13/20 21.6 ANR ANR ANR ANR ANR ANR ANR ANR -- 573 55.7 5.24 47.5 429 D 406 D 462 J 729 D 425 mg/L 04/13/21 62.1 75.0 28.1 ANR ANR ANR ANR ANR ANR ANR ANR 217 D 423 NS NS NS ND 373 D 126 NO 242 NS 2,4-D 2C u /L 06/20/18 0.27 ND NO NO ND ND ND NO Dinoseb 2C u /L 06/20/18 0.32 ND NO ND NO ND NO ND 2,4,5-TP (Silvex) ug/L 06/20/18 0.44 ND 0.49 J -- -- -- -- ND NO ND -- -- -- -- NO ND -- -- -- -- Notes: 1.) ug/L = Micrograms per liter 2.) ND = Not detected at the stated reporting limit 3.) NM = Not measured 4.) J = Estimated concentration reported below Solid Waste Section Limit 5.) -- = No data available 6.) Blanks = Field, trip, and method blanks 7.) Reanalysis = Reanalysis result in parenthesis next to the original result (e.g., reanalysis was performed for arsenic in January 2017) 8.) Dissolved = Dissolved sample in brackets [e.g. a dissolved sample was analyzed for MW-9 for the Febuary 2017 verification event] 9.) Bold = Concentration above the current NC 2L Groundwater Standard or NC 2L IMAC Groundwater Standard 10.) Shaded and Bold = Concentration above the current NC 2L Groundwater Standard or NC 2L IMAC Groundwater Standard and EPA MCL 11.) EPA MCL = US Environmental Protection Agency Maximum Contaminant Level 12.) SWS GSP = Solid Waste Section Groundwater Protection Standard 13.) SWS Reporting Limit = NCPQL or lab -specific reporting limit prior to October 2007 and NCSWSL starting in October 2007 and ending June 1, 2018 14.) = EPA MCL is an action level 15.)"= EPA MCL is a secondary standard 16.) Historical data prior to 10/30/07 provided by HDR Engineering of the Carolinas, Inc. Data 10/30/07 to 6/30/2020 Provided by Golder 17.) Samples collected using low -flow purge and sample techniques. 18.) The following dilutions were noted for the April 2020 event: Chloride & Sulfate 2x @ MW-17S, 4x @ MW-18, 5x @ MW-5, 10x @ MW-14, 50x @ MW-9; Nitrate as N, Nitrate/Nitrite as N 10x @ MW-4; Total Alkalinity as CaCO3 2x @ MW-6, MW-7, MW-8, MW-14, 5x @ MW-11 SR, MW-11 DR, MW-18, 10x @ MW-9; Antimony, Selenium, Thallium 2x @ MW-4, MW-5, MW-11SR, MW-11 DR, MW-13S, MW-13D, MW-14, MV 19.) PQL = Practical quantitation limit - lab specific limit 20.) MDL = Method Detection Limit 21.) SWSL = Solid Waste Section Reporting Limits (historic) 22.) The Blake Well not sampled in June 2018 and April 2020 as the power was out at the residence and no sample could be obtained. Z:\Sh,re\SME\Ops\ENV rojed 030Y35&O0 3A Moore Co My R-,LFG&WG Monitaing\Task 01- Seml-AnnueI Waler Oualgy F 2020-2021\W-Ing_Dxum Spring 2021 Even02020-10 WOMR Tables For Appentllx.- Page 30 of 30 Appendix IV - Time vs Concentration Charts 12.0 11.5 11.0 10.5 10.0 9.5 9.0 8.5 8.0 7.5 J on 7.0 7 c 6.5 0 +� 6.0 L 5.5 v U 0 5.0 U 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 Benzene Concentrations Over Time - MSW Landfill Wells w r, r, oo M M o o .4 c4 c4 M M 'zT 'zT M LD kD r, r, oo M M o O N ti c.i c» ro -zt -zt un tp Lo r, r, oo oo rn o o N 01 M Ol M (n 0) O O O O O O O O O O O O O O O O O -1 ci ci rl -i ci ci ci ci ci ci ci ci ci ci ci ci N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ (D 0 0 0 0 ci ci ci ci 0 0 0 0 (D 0 0 (D 0 0 0 0 0 (D 0 (D (D 0 0 ci 0 ci ci ci (D 0 0 CD 0 0 0 (D ci 0 \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ O CD N n N C) V r-q tD r-i0 oo m O C) N n N (D a .--I l0 C) o0 co O CD N n N 0 V r-q tD C) oo m O In N rl-a N C) a i--I O N O O O O i--I O O O O N O i--� O O O O N O O O O i--I O N O O O O i--I O O O O N O N O O O O Sampling Dates MW-6 MW-7 MW-8 MW-9 MW-15R Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Spring 2021 Event\2020-10 Table for 2L Exceedance Charts.xlsx 5.0 4.5 4.0 3.5 3.0 on c v 2.0 1.5 1.0 0.5 0.0 Benzene Concentrations Over Time - C&D Landfill Wells LD n n 00 M M O O . 4 N N M M 'zT 'zT M LD l0 n n 00 M M O O N N N M M 'zT � Ln tD LD n n 00 00 Q1 O O N Ql M Ol M Ol O O O O O O O O CD CD CD CD CD CD O O -1 ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ri ci ci ci ci \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ O C) N n N O V r-q tD 0 00 0 O C) N n N C3 a r-i-4 l0 CD 00 CO O a N n N 0 V r-q tD C) 00 0 O In N a N O a i--I O N O O O O i--I O O O O N O i--� O O O O N O O O O i--I O N O O O O i--I O O O O N O N O O O O Sampling Dates MW-11DR MW-11SR MW-13SR MW-14 Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Spring 2021 Event\2020-10 Table for 2L Exceedance Charts.xlsx 30.0 25.0 20.0 J bb 7 C C O +� 15.0 L U U C O U 10.0 IM, nn Vinyl Chloride Concentrations Over Time - MSW Landfill Wells LD n n 00 M M O O N N N M M -zT -zT UI l0 LD n n 00 M M O O c-I c-i N M M Ln l0 LO n n 00 00 M O O N Ol Ol Ol Ql Ol Ql O O O O O O O O O O O O O O O O O .--I a --I a --I a --I ci ci ci ci a-i a --I a --I a --I i-I ci ci ci ci N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci c-I ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci a-i a --I c-I ci ci ci ci a-i a --I ci ri ci ci ci ci ci ci c-I ci \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ O o N o N O o r-I o o 00 o O o N o N o o .--I o o 00 m O o N n N O V .--I o o 00 o O o N o N o o N O i--� O O O O N O O O O i--I O N O O O O i--� O O O O N O a --I O O O O a --I O O O O i--I O N O O O O Sampling Dates MW-6 MW-7 MW-8 MW-9 MW-15R Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Spring 2021 Event\2020-10 Table for 2L Exceedance Charts.xlsx 60.0 50.0 40.0 J OA 7 C C 0 % 30.0 L C: U C 0 U 20.0 10.0 0.0 Vinyl Chloride Concentrations Over Time - C&D Landfill Wells lD n n 00 M M O O .--I N N M M u1 lD l0 n n 00 M M O O r-I r-I N M M -zT -zT M lD l0 n n 00 W 01 O O rI 01 Ol Ol Ol Ol Ol O O O O O O O O O O O O O O O O O .-i c-I r-I a --I c-I c-I c-I ci ci ci ci ci ci c-I a --I r-I e-I N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ri ci ci ci ci \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ O C) N n N C) V ci lD r-i0 00 M O C) N n N C3 a -4 l0 CD 00 co O C) N n N 0 V ci lD C) 00 M O In N n N C) � rl O C-I O O O O c-I O O O O C-I O i--I O O O O c-I O O O O c-I O C-I O O O O c-I O O O O C-I O c-I O O O O Sampling Dates MW-11DR MW-11SR MW-13SR MW-14 Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Spring 2021 Event\2020-10 Table for 2L Exceedance Charts.xlsx 1,4-Dioxane Concentrations Over Time - MSW Landfill Wells 39.0 34.0 `:111, 24.0 Own c c 0 0 19.0 c (U U C 0 U 14.0 9.0 4.0 -1.0 00 O) °1 rn rn rn rn 0 0 0 0 0 0 ti ci ci ci ci ci ci ci N N N N N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O O \ \ \ \ \ \ \ \ \ \ \ \ \ \ � o 0 0 0 0 o 0 0 0 0 o Sampling Dates N N O 0 m in 0 0 MW-6 MW-7 MW-8 MW-9 MW-15R MW-2 Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Spring 2021 Event\2020-10 Table for 2L Exceedance Charts.xlsx 16.0 15.0 14.0 13.0 12.0 11.0 10.0 J 9.0 0 +� 8.0 L u 7.0 c 0 v 6.0 5.0 4.0 3.0 2.0 1.0 0.0 00 ci O O N 1,4-Dioxane Concentrations Over Time - C&D Landfill Wells 00 rn rn M rn rn rn O O O O O O N a --I c-I c-I c-I ci ci ci N N N N N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ a --I ci ci ci ci ci ci ci ci c-I c-I ci ci ci O O O O O O O O O O O O O O \ \ \ N 0 00 \ O \ \ \ \ \ \ \ N C) l0 00 N N V l0 000 O N N a-i O O O O O O O O N a --I O Sampling Dates N N \ \ ci ci O O MW-11DR MW-11SR MW-13SR MW-14 Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Spring 2021 Event\2020-10 Table for 2L Exceedance Charts.xlsx