5002_JacksonCounty_MSWLF_March21GW_FID1586718_20210617

DENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No) Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Anchor QEA of North Carolina, PLLC
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Chuck Pippin Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Jackson County Municipal Solid US Highway 441 50-02 .1600 March 9-10, 2021
Waste Landfill Dillsboro, North Carolina 28725
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑ Detection Monitoring ❑X Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑X
Leachate monitoring data ❑
Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify) Natural Attenuation Parameters
Other(specifv
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Chuck Pippin, P.G. Project Manager
Facility Represen_taFive� Title
06/09/2021
Date
231 Haywood Street Asheville, North Carolina 28801
Facility Representative Address
P-1649
NC PE Firm License Number (if applicable effective May 1, 2009)
828-281-3350
(Area Code) Telephone Number
Affix NC Licensed/ Professional Geologist Seal
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June 2021 ANCHOR
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 QEA `'"'
Spring 2021
Semiannual Water Quality Monitoring Report
Prepared for Jackson County Solid Waste Department

June 2021
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Spring 2021
Semiannual Water Quality Monitoring Report
Prepared for
Jackson County Solid Waste Department
401 Grindstaff Cove Road
Sylva, North Carolina 28779
Chuck PW PG
Project Geologist
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
A60-9-71 --
Melanie Kemp
Staff Scientist
Project Number: C01480-01.02
\\Athena\Asheville\Projects\Jackson County\Reports - Groundwater\2021\01_Spring 2021\Text\5002_Jackson County_SemiannuaI Water Quality
Report -Spring 2021.docx

TABLE OF CONTENTS
1 Introduction....................................................................................................................1
2 Semiannual Monitoring................................................................................................2
2.1 Groundwater, Surface Water, Domestic Well, and Leachate Sampling.......................................2
2.1.1 Monitoring Well Purging and Sampling Methods..............................................................2
2.1.2 Surface Water Sampling Methods...........................................................................................3
2.1.3 Leachate Sampling Methods.....................................................................................................3
2.1.4 Domestic Well Sampling Methods..........................................................................................4
2.2 Sample Handling, Documentation, and Analysis...............................................................................4
3 Findings..........................................................................................................................6
3.1
Groundwater.................................................................................................................................................6
3.1.1 Field Parameters............................................................................................................................7
3.1.2 Appendix I Metals (Total)...........................................................................................................7
3.1.3 Appendix I Metals (Dissolved)...................................................................................................8
3.1.4 Appendix I VOCs and 1,4-Dioxane..........................................................................................8
3.1.5 Natural Attenuation Parameters...............................................................................................9
3.2
Surface Water................................................................................................................................................9
3.2.1 Field Parameters............................................................................................................................9
3.2.2 Appendix I Metals.......................................................................................................................10
3.2.3 Appendix I VOCs and 1,4-Dioxane........................................................................................10
3.3
Leachate........................................................................................................................................................10
3.4
Domestic Well.............................................................................................................................................11
3.4.1 Field Parameters..........................................................................................................................11
3.4.2 VOCs...............................................................................................................................................11
3.5
Groundwater Flow Directions.................................................................................................................11
4 Summary.......................................................................................................................12
4.1 Groundwater Quality................................................................................................................................12
4.1.1 Appendix I Metals.......................................................................................................................12
4.1.2 Appendix I Volatile Organic Compounds and 1,4-Dioxane...........................................12
4.1.3 Field Parameters and Other Constituents............................................................................12
4.2 Surface Water Quality...............................................................................................................................13
4.3 Leachate Quality.........................................................................................................................................13
4.4 Domestic Well Water Quality.................................................................................................................13
Spring 2021 Semiannual
Water Quality Monitoring Report i June 2021

5 Future Activities............................................................................................................14
6 References.....................................................................................................................15
TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Well Construction Details and Corresponding Elevations
Table 3 Analytical Summary
Table 4 Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in
the Leachate Sample (LT-01)
FIGURES
Figure 1 Site Location Map
Figure 2 Site Layout Map
Figure 3 Generalized Groundwater Flow Direction
Figure 4 Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-01)
Figure 5 Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-01)
Figure 6 Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time (Monitoring Well
M W-05 R)
Figure 7
Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-05R)
Figure 8
Hydrograph and Vinyl Chloride Concentration vs. Time
(Monitoring Well MW-05R)
Figure 9
Hydrograph and 1,4-Dioxane Concentration vs. Time (Monitoring Well MW-07)
Figure 10
Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-07)
APPENDICES
Appendix A Well Sampling Logs, and Equipment Documentation and Instrument Calibration
Data Sheets
Appendix B Reports of Laboratory Analysis, Chain -of -Custody Documentation,
and Certificates of Analysis
Spring 2021 Semiannual
Water Quality Monitoring Report ii June 2021

ABBREVIATIONS
pg/L micrograms per liter
pmhos/cm micromhos per centimeter
AM Analytical Method
bgs below ground surface
BOD biochemical oxygen demand
CAE Corrective Action Evaluation Report
CAP Corrective Action Plan
CFR Code of Federal Regulations
COD chemical oxygen demand
DENR North Carolina Department of Environment and Natural Resources
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
DWM Division of Waste Management
EPA U.S. Environmental Protection Agency
IMAC interim maximum allowable concentration
MDL method detection limit
mg/L milligrams per liter
MNA monitored natural attenuation
MSWLF Municipal Solid Waste Landfill
mV millivolts
NCAC North Carolina Administrative Code
NTU nephelometric turbidity unit
ORP oxidation reduction potential
PWR partially weathered rock
SC specific conductivity
Site Closed Municipal Solid Waste Landfill, approximately 0.75 mile west of Dillsboro,
North Carolina, on the northeast side of Old Dillsboro Road (Old U.S. Highway 74)
SM Standard Method
SU standard unit
SWS Solid Waste Section
TOC total organic carbon
TWSA Tuckasegee Water & Sewer Authority
VOC volatile organic compound
Waypoint Waypoint Analytical Laboratories
Spring 2021 Semiannual
Water Quality Monitoring Report iii June 2021

1 Introduction
The Jackson County Solid Waste Department maintains a closed Municipal Solid Waste Landfill (the
Site) approximately 0.75 mile west of Dillsboro, North Carolina, on the northeast side of
Old Dillsboro Road (Old U.S. Highway 74; Figure 1). Water quality monitoring at the landfill is
governed by the North Carolina Department of Environmental Quality (DEQ), Division of Waste
Management (DWM), Solid Waste Section (SWS), under Permit No. 50-02 issued to Jackson County.
The landfill permit requires semiannual monitoring of groundwater and surface water quality.
Since October 2007, when Anchor QEA of North Carolina, PLLC, began performing water quality
monitoring events at the Site, groundwater quality monitoring has indicated persistent low-level
concentrations of constituents that exceed groundwater quality standards. In response to the
continued exceedances of the analyzed constituents, an Assessment of Corrective Measures was
submitted to the North Carolina Department of Environment and Natural Resources (DENR; now the
DEQ) on September 7, 2010 (Altamont 2010). A Corrective Action Plan (CAP; Altamont 2011) was
implemented upon approval by the DENR, as recorded in the September 1, 2011 letter regarding
"Approval of the County's Corrective Action Plan" (DENR 2011). The implemented remedy includes the
extraction of leachate through dedicated submersible pumps installed within landfill gas extraction
wells and disposal of the leachate into the Tuckasegee Water & Sewer Authority (TWSA) collection
system. In addition to the leachate extraction, groundwater natural attenuation parameters are
monitored, and natural attenuation processes are evaluated. As discussed in the CAP, a corrective
action evaluation report is prepared every 5 years. The evaluation report analyzes the progress of the
approved corrective action remedy based on semiannual water quality monitoring data. The remedy
was implemented in a phased approach, with full implementation occurring on September 6, 2013. The
first Five -Year Corrective Action Evaluation Report (CAER), submitted by Altamont on October 31, 2016
(Altamont 2016), concluded that the current conditions of the monitored natural attenuation (MNA)
parameters and Site geochemical parameters allowforthe slow degradation of the select contaminants
identified in the CAER. The second CAER is scheduled to be submitted in fall 2021.
This report serves as the first semiannual water quality monitoring report for 2021. The report
provides an evaluation of groundwater and surface water quality. The water quality monitoring
network is presented in Figure 2. The generalized groundwater flow direction in the upper parts of
the underlying aquifer system is provided in Figure 3. In addition to groundwater and surface water
monitoring, this report includes analysis of the extracted leachate and one domestic water well. The
water samples collected from selected monitoring points during the spring sampling event were
analyzed for a range of parameters, as presented in Section 2.2 and Table 1. The spring 2021
sampling event was performed on March 9 and 10, 2021, and is being reported in accordance with
requirements stipulated in the DEQ Solid Waste Management Rules codified under Title 15A,
Subchapter 13B of the North Carolina Administrative Code (NCAC).
Spring 2021 Semiannual
Water Quality Monitoring Report 1 June 2021

2 Semiannual Monitoring
2.1 Groundwater, Surface Water, Domestic Well, and Leac hate
Sampling
The Site monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06, and MW-07), surface
water sample locations (SW-01 and SW-02), leachate sample location (LT-01), and domestic well
(DW-01) were sampled on March 9 and 10, 2021, by Anchor QEA. Static groundwater level
measurements and field parameter data are included on the sampling logs presented in Appendix A.
Field equipment calibration logs for the YSI Professional Plus Multiparameter Water Quality Meter
and the Hach 2100Q Turbidimeter are also provided in Appendix A. The full suite of groundwater
and surface water laboratory analytical results is presented in the laboratory analysis reports in
Appendix B.
Monitoring wells MW-01 and MW-06 are considered to be the Site's upgradient monitoring wells;
MW-03 and MW-05R are located in the midgradient portion of the Site; and MW-02, MW-04, and
MW-07 monitor downgradient portions of the Site. As summarized in Table 2, the total depths of the
monitoring wells range from 40 to 110 feet below ground surface (bgs). The geology of the screened
intervals of the monitoring wells is as follows:
• Saprolite': MW-04 and MW-05R
• Partially Weathered Rock (PWR)z: MW-03
• Bedrock3: MW-01, MW-02, MW-06, and MW-07
The locations of the monitoring wells, surface water samples, leachate, and domestic well sample
locations are shown in Figure 2.
2. 7.1 Monitoring Well Purging and Sampling Methods
Before the monitoring wells were sampled, the static water level was gauged in each well, and an
initial round of field parameters was measured (consisting of pH, specific conductivity [SC], dissolved
oxygen [DO], turbidity, temperature, and oxidation reduction potential [ORP]).
Anchor QEA personnel used either low -flow techniques or disposable bailers to purge the
monitoring wells and collect groundwater samples. The total depth, condition of the casing, and
groundwater recharge rate determined the purging and sample collection method employed at each
monitoring well.
Saprolite is the result of in -place weathering that produces soil -like material that retains relict features of the parent rock.
z PWR is generally found above the bedrock and is softer than bedrock, but not as soft as sap rolite.
'Bedrock is solid competent rock that underlies saprolite and partially weathered rock.
Spring 2021 Semiannual
Water Quality Monitoring Report 2 June 2021

Four of the monitoring wells (MW-03, MW-04, MW-06, and MW-07) were purged using low -flow
techniques in accordance with the procedures described by the U.S. Environmental Protection
Agency (EPA) in Low -Flow (Minimal Drawdown) Ground -Water Sampling Procedures (EPA 1996).
During purging, the field parameters (pH, SC, DO, ORP, turbidity, and temperature) were measured
and recorded approximately every 3 minutes. Well purging continued until these parameters had
generally stabilized for three consecutive readings. The required stabilization criteria are determined
by the EPA Region 4 Science and Ecosystem Support Division in Operating Procedure. Groundwater
Sampling (EPA 2017) and are summarized as follows:
• pH values within ±0.1 standard unit (SU)
• SC values within ±5%
• Temperature, DO, and turbidity values within ±10%
• ORP values within ±10 millivolts (mV)
Once the parameters had stabilized, a groundwater sample was collected by field personnel wearing
a new pair of nitrile gloves, using laboratory -supplied sample containers.
Because of their slow recharge rates, monitoring wells MW-01, MW-02, and MW-05R were purged
and sampled using disposable bailers. The wells were purged of three successive well volumes or
purged dry, whichever occurred first. Monitoring well MW-02 was purged dry on March 9 and
sampled on March 10, 2021, after the well had sufficient time to recharge. Monitoring well MW-05R
was purged dry in the morning on March 9 and sampled later that day after the well had sufficient
time to recharge. Monitoring well MW-01 was purged and sampled on March 10, 2021. A round of
field parameters was measured and recorded at the start of purging and after each consecutive well
volume had been purged.
Field parameter data are shown in the well sampling logs included in Appendix A.
2. 7.2 Surface Water Sampling Methods
Surface water samples SW-01 and SW-02 were collected on March 9, 2021, at designated locations
from the Tuckasegee River, which is adjacent to and southwest of the landfill (Figure 2). Sampling
location SW-01 is assumed to represent surface water quality upstream of the landfill, and sampling
location SW-02 is assumed to represent surface water quality downstream of the landfill. One round
of field parameters was measured and recorded at each surface water sampling location immediately
prior to collecting the sample (Appendix A). The surface water samples were collected in
laboratory -provided sample containers by a technician wearing a new pair of nitrile gloves.
2. 7.3 Leachate Sampling Methods
Dedicated bottom -loading air -powered pumps, air pressure lines, and a leachate force main
collection system are installed at the landfill. Pumps are installed in landfill gas extraction wells
Spring 2021 Semiannual
Water Quality Monitoring Report 3 June 2021

EW-1 R, EW-2R, EW-3R, EW-4, EW-5, EW-6, EW-7, EW-8, EW-9, and EW-10. The gas extraction well
locations are presented in Figure 2. The leachate is pumped from the wells into a flow equalization
tank, which is connected to the TWSA wastewater collection system.
The flow equalization tank is eastof the landfill, adjacentto the existing landfill gas flare. Agrab
sample of leachate (LT-01) was acquired on March 10, 2021, by collecting a sample as the leachate
entered the flow equalization tank. One round of field parameters was measured and recorded after
the sample was collected (Appendix A).
2. 7.4 Domestic Well Sampling Methods
The domestic well water sample (DW-01, owned by Mr. Frank Wilkie) was collected on
March 10, 2021, from an outside spigot at the residence located at 318 Joe Wilkey Road, bordering
the northern boundary of the landfill (Figure 2). The well was purged of 30 gallons prior to sample
collection. One round of field parameters was measured and recorded after the 30 gallons had been
purged. The domestic well water sample was collected in laboratory -provided sample containers by
field personnel wearing a new pair of nitrile gloves.
Attempts to sample the second domestic water well (DW-2, owned by Mr. Joshua Bulla at
138 Joe Wilkey Road) were unsuccessful because the owner could not be contacted.
2.2 Sample Handling, Documentation, and Analysis
It should be noted that during most semiannual sampling events atthe Jackson County Landfill,
water quality samples are submitted for Appendix I parameters only. A larger suite of Appendix II
parameters as noted below are analyzed during the fall sampling event only on a biannual basis.
Field parameters and additional observations pertaining to the Site sampling locations are provided
in the sampling logs (Appendix A). Following sample collection, each groundwater, surface water,
leachate, and domestic well water sample was immediately placed on ice in a sample cooler for
transport to Waypoint Analytical Laboratories (Waypoint), a North Carolina -certified laboratory in
Charlotte, North Carolina. The groundwater samples collected from the monitoring wells were
analyzed for the following parameters (Table 1):
• Appendix I metals, including mercury, using EPA Methods 6020B and 7470A
• Appendix I volatile organic compounds (VOCs), using EPA Method 8260D
• 1,4-Dioxane, using EPA Method 8260DSIM
• MNA parameters:
- Alkalinity, using Standard Method (SM) 2320B
- Biochemical oxygen demand (BOD; 5-day), using SM 5210B
- Volatile fatty acids, carbon dioxide, ethane, ethene, and methane, using Analytical
Method (AM) 20GAX
Spring 2021 Semiannual
Water Quality Monitoring Report 4 June 2021

- Hydrogen (only in MW-03, MW-04, MW-06, and MW-07), using AM20GAX
- Chemical oxygen demand (COD), using SM 5220D
- Chloride, nitrate, and sulfate, using EPA Method 9056A
- Ferrous iron, using SM 3500-Fe D
- Sulfide, using SM 4500-5 F
- Total organic carbon (TOC), using SM 9060A
- Nitrate as N, chloride, and sulfate, using EPA Methods 9056A
The surface water samples were analyzed for the following parameters:
• Appendix I metals, including mercury, using EPA Methods 6020B and 7470A
• Appendix I VOCs, using EPA Method 8260D
• 1,4-Dioxane, using EPA Method 8260DSIM
• Hardness, using SM2340C
The leachate sample was analyzed for the following parameters:
• Appendix I VOCs, using EPA Method 8260D
• 1,4-Dioxane, using EPA Method 8260DSIM
• Appendix I metals, using EPA Method 6020B
The domestic well sample was analyzed for the following parameters:
• VOCs, using EPA Method 524.2
Proper chain -of -custody documentation procedures were followed during collection and
transportation of each sample (Appendix B). Two trip blank samples for quality control/quality
assurance purposes were included in the sample coolers and analyzed for Appendix I VOCs when
applicable. The reports of the laboratory analyses are provided in Appendix B. Laboratory analyses
performed on the samples are summarized in Table 1.
Spring 2021 Semiannual
Water Quality Monitoring Report 5 June 2021

3 Findings
The field parameter data and laboratory analytical results for the groundwater samples (from
monitoring wells MW-01 through MW-07), surface water samples (SW-01 and SW-02), leachate
sample (LT-01), and domestic well sample (DW-01) collected at the landfill are included in
Appendices A and B. The results are also submitted separately to the DEQ DWM SWS in the
Electronic Data Deliverable format (DEQ 2020).
The laboratory analytical results were reported and appropriately qualified as follows:
• Non -Detections: Non -detections are values reported by the laboratory as less than the method
detection limits (MDLs).They are tabulated in Table 3 and flagged with a "U" qualifier. The MDLis
the minimum concentration of a substance that can be measured and reported by a laboratory
with 99% confidence that the constituent concentration is greater than zero.
• Estimated or "Y' Qualified: A "Y' qualifier is used by the laboratory for parameters that are
detected at estimated concentrations greater than the MDL but less than the laboratory's
method reporting limit. The method reporting limit is the minimum concentration of a target
analyte that can be accurately determined by the referenced method.
• Groundwater Quality Standard: Detected concentrations of constituents in groundwater
samples were compared to applicable North Carolina groundwater quality standards. For
most constituents, this standard is the 2L standard, defined in 15A NCAC 2L .0202. Detected
concentrations of analytes in groundwater with no established 2L standard were compared to
the interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]). For the purposes of this report, groundwater
standards were taken from the October 15, 2018 list published by the North Carolina SWS
(DEQ 2018b).
• 2B Standard: Detections of analytes in surface water samples were compared to the
surface -water quality standards 2B standards, defined in 15A NCAC 2B. Hardness -dependent
2B surface water standards were calculated using the average analyzed hardness value
(calculated from the upstream and downstream surface water sampling location results) via
the most stringent hardness -dependent metal calculation.
Table 3 summarizes detected concentrations of analytes that exceeded their respective 2L standard,
IMAC, or 2B standard.
3.1 Groundwater
Measured field parameters and analytical results for groundwater samples collected from the
monitoring wells during the spring 2021 sampling event are discussed in the following sections and
summarized in Table 3.
Spring 2021 Semiannual
Water Quality Monitoring Report 6 June 2021

3. 7. 7 Field Parameters
Field parameter measurements were obtained from all site monitoring wells (MW-01, MW-02,
MW-03, MW-04, MW-05R, MW-06, and MW-07). The pH readings ranged from 5.0 SU in MW-06 to
6.7 SU in MW-03. Of these monitoring wells, the pH values for MW-01, MW-02, MW-04, MW-06, and
MW-07 were less than the 2L standard pH range of 6.5 to 8.5 SU.
Turbidity ranged from 4.67 nephelometric turbidity units (NTU) in MW-04 to 225 NTU in MW-02.
Generally, the higher values were measured at the monitoring wells (MW-01, MW-02, and MW-05R)
that were purged and sampled using the bailer method (Section 2.1.1). The bailers were lowered
gently to minimize water column disturbance when the samples were collected.
Dissolved oxygen (DO) concentrations at the Site ranged from 0.84 milligram per liter (mg/L) in
monitoring well MW-05R to 6.83 mg/L in monitoring well MW-03. SC concentrations at the Site
ranged from 53.5 micromhos per centimeter (pmhos/cm) in monitoring well MW-06 to
802 pmhos/cm in monitoring well MW-07. ORP concentrations at the Site ranged from -129.9 mV in
monitoring well MW-05R to 351 mV in monitoring well MW-04. Groundwater standards are not
established for DO, SC, or ORP.
3. 7.2 Appendixl Metals (Total)
Twelve metals were detected in one or more of the monitoring well samples. Three of these metals
(chromium, cobalt, and vanadium) were detected at concentrations above their respective NC21-
and/or IMAC water quality standards in one or more of the groundwater samples. Chromium was
detected at a concentration that exceeded its 2L standard (10 microgram per liter [pg/L]) in
groundwater samples collected from MW-02, detected at a concentration of 19.8 pg/L. Cobaltwas
detected at a concentration that exceeded its 2L standard (1 pg/L) in groundwater samples collected
from MW-01, MW-02, MW-04, MW-05R, MW-06, and MW-07. Cobalt concentrations in these
samples ranged from an estimated 1.69 pg/L (MW-07) to 146 pg/L (MW-01). As noted in Section 2.1,
the monitoring well MW-01 is considered to represent upgradient conditions. The second
upgradientwell (MW-06) also showed an exceedance of cobalt (12.5 pg/L). Historically, cobalt has
been present at concentrations that exceed its applicable water quality standard in groundwater
samples from each of the seven monitoring wells. Additionally, vanadium was detected at
concentrations exceeding its 2L standard (0.3 pg/L) in samples collected from MW-02 (26 pg/L) and
MW-05R (6.37 pg/L).
These metals have historically been present at concentrations exceeding their water quality standard
in samples collected from multiple groundwater monitoring wells at the Site. However, the elevated
turbidity value (225 NTU) measured in the MW-02 sample may have affected the metal
concentrations reported here. During the spring 2020 sampling event, MW-02 showed a turbidity of
15.5 NTU with consistently lower concentrations of these metals (Anchor QEA 2020).
Spring 2021 Semiannual
Water Quality Monitoring Report 7 June 2021

3. 7.3 Appendixl Metals (Dissolved)
Laboratory -filtered analysis of Appendix II metals were performed for monitoring well samples
MW-05R because of their elevated turbidity readings (74.4 NTU) during sample collection. The
reported concentrations for the dissolved metals were consistently lower than the total unfiltered
metals analytical results in MW-05R, with no exceedances of the groundwater protection standards.
(Table 3).
3. 7.4 Appendixl VOCs and 7,4-Dioxane
Fifteen VOCs were detected in one or more of the monitoring wells (Table 3). Four of these VOCs
(1,4-dichlorobenzene; 1,4-dioxane; benzene; and vinyl chloride) were detected at concentrations that
exceeded their respective 2L standards in the groundwater samples collected from one or more
monitoring wells. Concentration -versus -time graphs (trend plots) were created for the monitoring wells
that have historically exhibited VOC concentrations that exceed the associated 2L standards (Figures 4
through 10).
The detected concentration of 1,4-dichlorobenzene exceeded its 2L standard (6 pg/L) in monitoring
wells MW-01 (9.33 pg/L) and MW-05R (6.05 pg/L). The historical 1,4-dichlorobenzene concentration
trend in MW-01 remains relatively stable (Figure 4). Historical 1,4-dichlorobenzene concentrations in
MW-05R have consistently fluctuated (Figure 6).
The detected concentrations of 1,4-dioxane exceeded its 2L standard (3 pg/L) in MW-07 (16.3 pg/L).
1,4-Dioxane was not detected in monitoring wells MW-01, MW-02, MW-03 or MW-06. 1,4-Dioxane
was detected under the 2L standard in MW-04 and MW-05R. A trend plot for 1,4-dioxane
concentrations in MW-07 show stable concentrations (Figure 7) since sampling for this compound,
beginning in October 2018.
Benzene was detected at concentrations that exceed its 2L standard of 1 pg/L in MW-01 (1.07 pg/L),
MW-05R (2.27 pg/L) and MW-07 (1.36 pg/L). Overall, historic benzene concentrations in monitoring
well MW-01 shows a generalized downward trend since April 2007 (Figure 5). Benzene
concentrations at MW-5R have fluctuated consistently since 2012 (Figure 7). Benzene concentrations
at MW-07 have been relatively stable since 2011 (Figure 10).
The concentration of vinyl chloride in the sample collected from one monitoring well, MW-05R
(2.33 pg/L), exceeded the compound's 2L standard (0.03 pg/L). A trend plot for vinyl chloride
concentrations in MW-05R shows consistently fluctuating concentrations (Figure 8).
A review of historical groundwater data indicates that the VOCs (1,4-dichlorobenzene; 1,4-dioxane,
benzene; and vinyl chloride) exhibiting concentrations that exceed the 2L standards during the
spring 2021 sampling event have been detected at relatively consistent concentrations for the past
several years. As described in Section 3.2.3, historical surface water samples from the
Spring 2021 Semiannual
Water Quality Monitoring Report 8 June 2021

Tuckasegee River, which may receive discharge from the saprolite groundwater -bearing zone, have
consistently shown no detections of these compounds, or other VOCs.
3. 7.5 Natural Attenuation Parameters
During this sampling event, the groundwater samples were analyzed for MNA parameters as
described in Section 2.2 (Table 1). The results of these analyses are summarized in Table 3. These
parameters were detected in one or more groundwater samples collected from the monitoring wells.
Many of these parameters do not have established groundwater standards. Of the parameters that
do have established groundwater standards (chloride and sulfate) there were no exceedances. An
in-depth analysis of the MNA parameters that apply to the Site's select contaminants was presented
in the first Five -Year CAER (Altamont 2016). The CAER concluded that the MNA data provide
evidence that reductive degradation and aerobic degradation are occurring in different portions of
the Site. The dataset of the MNA parameters collected from spring 2017 to spring 2021 will be used
in the second Five -Year CAER (scheduled for fall 2021) to evaluate the degradation processes at the
Site.
3.2 Surface Water
The following sections summarize the measured field parameters and analytical results associated
with the two surface water samples collected during the spring 2021 sampling event.
3.27 Field Parameters
The pH readings for the upstream (SW-01) and downstream (SW-02) surface water samples collected
during the spring 2021 sampling event were 7.6 and 6.6 SU, respectively. The pH readings for both
surface water samples were within the 2B standard range of 6.0 to 9.0 SU.
The turbidity values measured in SW-01 (12.2 NTU) and SW-02 (8.2 NTU) were less than the
2B standard, which is established at less than or equal to 50 NTU for the receiving water in streams
not designated as trout waters.
DO was measured at a concentration of 11.61 mg/L in SW-01 and 11.46 mg/L in SW-02. The
2B standard is established as greater than or equal to 6 mg/L; thus, each sample is within the
acceptable DO range.
SC concentrations in surface water samples SW-01 and SW-02 were recorded at 30.5 and
30.6 pmhos/cm, respectively. ORP values for SW-01 and SW-02 were 221.9 and 274.6 mV,
respectively. These concentrations of SC and ORP are consistent with historical data for both surface
water samples. 2B standards do not exist for these parameters.
Spring 2021 Semiannual
Water Quality Monitoring Report 9 June 2021

3.2.2 Appendix Metals
Six metals were detected in both surface water sampling locations. Of these metals, only one (lead)
was detected at a concentration that slightly exceeded its 2B standard of0.2 pg/L. Lead was detected
above the 2B standard in downstream location SW-2 at an estimated concentration of 0.652 pg/L.
These results are consistent with historical sample results that show that lead has been detected
above 213 standards in past sampling events at both the upstream and downstream sampling
locations.
3.2.3 Appendixl VOCs and 7,4-Dioxane
No VOCs were detected in either of the surface water sampling locations.
3.3 Leachate
Five metals (arsenic [2.9 pg/L], barium [360 pg/L], chromium [2.99 pg/L], cobalt [3.97 pg/L], and
nickel [23.6 pg/L]) were detected in the leachate sample (LT-01).
Six VOCs (1,4-dichlorobenzene [3.44 pg/L]; 1,4-dioxane [55.5 pg/L]; acetone [20.2 pg/L];
benzene [1.49 pg/L]; chlorobenzene [3.13 pg/L]; and tetrahydrofuran [82.9 pg/L]) were detected in
the leachate sample (LT-01).
On September 1, 2012, leachate extraction was initiated following installation of leachate extraction
pumps in the 10 landfill gas extraction wells at the Site (Figure 2). Due to a temporary malfunction
with the leachate flow meter between October 2017 and March 2018, there is a gap in the mass
removal calculations represented in Table 4. Therefore, the total volume of leachate removed since
September 2012 is not known. However, based on readings taken from the leachate totalizer during
the October 2020 monitoring events, approximately 98,790 gallons of leachate were discharged
through a permanent connection to the TWSA between March 19 and October 14, 2020.
During spring 2021 sampling, Anchor QEA personnel attempted to access the leachate totalizer, but
the access location was buried due to construction at the Jackson County Green Energy Park.
Updated mass removal calculations are not provided, but Anchor QEA will attempt to collect a
leachate totalizer reading during the next semiannual sampling event (Table 4).
In fall 2013, the active portion of the approved corrective action remedy was initiated. Based on the
leachate analytical results for the sample collected on October 14, 2020, Anchor QEA estimates that
approximately 0.17 pounds of VOCs was removed with the extracted leachate between the March
and October 2020 sampling events. Mass removal calculations, through October 2020, are included
in Table 4.
Spring 2021 Semiannual
Water Quality Monitoring Report 10 June 2021

3.4 Domestic Well
The following sections summarize measured field parameters and analytical results associated with
the domestic well water sample collected during the spring 2021 sampling event.
3.4. 7 Field Parameters
The pH reading for the domestic well sample (DW-01) was 6.5 SU, which is within the 2L standard
range of 6.5 to 8.5 SU.
Turbidity measured in DW-01 was 9.8 NTU. DO was measured at a concentration of 7.24 mg/L in
DW-01. SC and ORP values in DW-01 were recorded at 59.3 pmhos/cm and 157.5 mV, respectively.
These parameters do not have established water quality standards.
3.4.2 VOCs
No VOCs were detected at concentrations that exceeded their respective MDLs in the domestic well
water samples.
3.5 Groundwater Flow Directions
Groundwater levels in the saprolite, PWR, and bedrock are monitored atthe Site. Three of the
bedrock monitoring wells (MW-01, MW-02, and MW-06) are located in the northern and
northwestern portions of the Site (Figure 3; Table 2). The fourth bedrock monitoring well (MW-07) is
located southwest of the landfill (Figure 3). The fall 2020 water level data collected from these four
bedrock wells were used to determine the generalized bedrock groundwater flow direction, which is
to the southwest (Figure 3).
PWR monitoring well MW-03 and saprolite monitoring wells MW-04 and MW-05R (Figure 3) are
located in the south-central and southern parts of the landfill, respectively. The fall 2020 water level
data collected from monitoring wells MW-03, MW-04, and MW-05R (Table 2) indicate that
groundwater flow direction in the combined saprolite and PWR zones is generally to the south-
southwest, toward the Tuckasegee River (Figure 3).
Spring 2021 Semiannual
Water Quality Monitoring Report 11 June 2021

4 Summary
The first semiannual water quality monitoring event of 2021 for the Site was performed on March 9
and 10, 2021. Appendices A and B and Table 3 provide detailed analytical results and field data
summarizing the groundwater, surface water, and leachate quality at the landfill.
4.1 Groundwater Quality
4. 7.1 Appendix) Metals
Three metals (chromium, cobalt, and vanadium) were detected at concentrations that exceeded their
associated groundwater quality standards in one or more of the monitoring wells (Table 3). Cadmium
concentrations exceeded its 2L standard in MW-02. Cobalt concentrations exceeded its 2L standard
in all of the collected groundwater samples excluding MW-03 but including the upgradient
monitoring wells, MW-01 and MW-06. These results are consistent with historical data. Vanadium
exceeded its 2L concentration MW-02 and MW-05R.
The results for groundwater samples from MW-05R, submitted for dissolved filtered metals, shows
significantly lower metals concentrations than the total unfiltered samples, indicating turbidity
directly affects metal concentrations in these wells.
4.7.2 Appendixl Volatile Organic Compounds and 1,4-Dioxane
Four VOCs (1,4-dichlorobenzene; benzene; vinyl chloride; and 1,4-dioxane) were detected at
concentrations that exceeded their respective 2L standards (Table 3) in one or more monitoring
wells, including 1,4-dichlorobenzene and benzene, in the upgradient monitoring well MW-01. Trend
plots for samples from monitoring wells that had VOC concentrations that exceeded their
2L standards (Figures 4 through 10) show relatively stable concentrations with time.
4. 7.3 Field Parameters and Other Constituents
Five of the seven samples collected from the monitoring wells had pH readings outside of the
2L standard range (6.5 to 8.5 SU). These results are consistent with historical data and are
characteristic of the natural groundwater quality of the region. Turbidity readings ranged from
4.67 NTU (MW-04) to 225 NTU (MW-02).
Natural attenuation parameters (alkalinity, BOD, COD, chloride, cyanide, nitrate as N, sulfate, sulfide,
TOC, ferrous iron, hydrogen, methane, acetic acid, formic acid, lactic acid, propionic acid, and carbon
dioxide) were detected at various concentrations in groundwater samples collected from one or
more of the monitoring wells. Natural attenuation parameters are being monitored to fulfill CAP
requirements; further evaluation of these parameters will be performed in the second Five -Year CAER
(scheduled for fall 2021).
Spring 2021 Semiannual
Water Quality Monitoring Report 12 June 2021

4.2 Surface Water Quality
One metal, lead, was detected at a concentration that exceeded its applicable 2B standard for surface
water during this monitoring event, in downstream location SW-02. Lead was detected in two of the
monitoring wells, not exceeding its 2L standard. These results are consistent with historical sample
results that show that lead has been detected above 2B standards in past sampling events at both
the upstream and downstream sampling locations. No VOCs were detected at concentrations that
exceeded the applicable surface water standards. Field parameters measured in both surface water
samples, including pH, turbidity, and DO, were within the 2B standards established for these
parameters. Based on these data, the groundwater migrating from the landfill toward the
Tuckasegee River does not appear to be impacting surface water quality with regard to metals and
VOCS.
4.3 Leachate Quality
The leachate sample (LT-01) was collected from the flow equalization tank and analyzed for
Appendix I VOCs and 1,4-dioxane. Six VOCs were detected in the leachate sample (Table 3). There
are no established water quality standards for leachate. 1,4-Dioxane was detected at 55.5 pg/L, which
is higher than the detected concentrations of the compound in the monitoring well groundwater
samples. This is the second sampling event where 1,4 dioxane was analyzed in the leachate.
4.4 Domestic Well Water Quality
No VOCs were detected at concentrations that exceeded their respective MDLs in the domestic well
water samples.
Spring 2021 Semiannual
Water Quality Monitoring Report 13 June 2021

5 Future Activities
Anchor QEA will continue to monitor the water quality on a semiannual basis at the Site. During
spring 2021, domestic well owners will be contacted, and groundwater samples will be collected
from domestic wells if permitted by the well owner, and if possible, based on well pump operability.
Domestic well samples will be analyzed for VOCs only. Samples will be collected from the monitoring
wells, surface water monitoring points, and leachate flow equalization tank during fall 2021 and
spring 2022. In addition to the MNA parameters that were added to the monitoring requirements as
part of the CAP, the analytical suites associated with the current and future sampling events are
outlined in the 2011 CAP (Altamont 2011) and the first Five -Year CAER (Altamont 2016). The
upcoming sampling event parameters are as follows:
Sampling Event
Analytical Suite
(not inclusive of natural attenuation parameters)
Appendixll VOCs (including 1,4-dioxane)
Fall 2021
Appendixll Metals
Sulfide
Appendix VOCs (including 1,4-dioxane)
Spring 2022
Appendix I Metals
Sulfide
The second Five -Year CAER is scheduled for fall 2021. This evaluation will include a detailed analysis
of the contaminant and MNA parameter trends to assess effectiveness of the MNA program. This
report will also include an evaluation of MW-01 and MW-06 as representative background wells at
the Site.
Spring 2021 Semiannual
Water Quality Monitoring Report 14 June 2021

6 References
Altamont (Altamont Environmental, Inc.), 2010. Assessment of Corrective Measures. Prepared for the
North Carolina Department of Environment and Natural Resources. September 7, 2010.
Altamont, 2011. Corrective Action Plan. Prepared for the North Carolina Department of Environment
and Natural Resources. June 30, 2011.
Altamont, 2016. Five -Year Corrective Action Evaluation Report. Prepared for the North Carolina
Department of Environmental Quality. October 31, 2016.
Anchor QEA, 2020. Spring 2020 Semiannual Water Quality Monitoring Report. Prepared for Jackson
County Solid Waste Department. June, 2020.
DENR (North Carolina Department of Environmental and Natural Resources), 2011. Letter to:
Altamont Environmental, Inc. Regarding: Approval of the County's Corrective Action Plan.
September 1, 2011.
DEQ (North Carolina Department of Environmental Quality), 2018a. Memorandum to: Solid Waste
Directors, Landfill Owners/Operators, and North Carolina Certified Laboratories. Regarding:
1,4-Dioxane Analysis, Solid Waste Section Limits, and Laboratory Analytical Methods.
May 29, 2018.
DEQ, 2018b. "Groundwater Protection Compliance Standards — Constituents List". Last modified
October 15, 2018. Available at:
https://edocs.deq.nc.gov/WasteManagement/0/edoc/1257181/SWS_EnviroMonitoring_Const
ituents_List. pdf?sea rchid=13f8efb 1-eel l-485a-b03f-718f2287b271
DEQ, 2020. Memorandum Re: New Electronic Data Deliverable (EDD) Format. July 20, 2020.
EPA (U.S. Environmental Protection Agency), 1996. Low -Flow (Minimal Drawdown) Ground -Water
Sampling Procedures. OSWER, EPA/540/5-95/504.
EPA, 2017. Science and Ecosystem Support Division. Operating Procedure. Groundwater Sampling.
April 26, 2017.
Spring 2021 Semiannual
Water Quality Monitoring Report 15 June 2021

Tables

Table 1
Summary of Laboratory Analyses Performed on Samples
Groundwater Samples
Location ID
Date
Collected
Sample ID
Appendix I
VOCs
1,4-Dioxane
Appendix I
Metals
Mercury
EPA 8260D
EPA 8260D
SIM
EPA 6020B
EPA 7470A
MW-01
03/10/2021
MW-01-20213010
X
X
X
X
MW-02
03/10/2021
MW-02-20210310
X
X
X
X
MW-03
03/09/2021
MW-03-20210309
X
X
X
X
MW-04
03/09/2021
MW-04-20210309
X
X
X
X
MW-05R
03/09/2021
MW-05R-20210309
X
X
X
X
MW-06
03/10/2021
MW-06-20210310
X
X
X
X
MW-07
03/09/2021
MW-07-20210309
X
X
X
X
Surface Water, Leachate, Domestic Well, and Quality Control Samples
Location ID
Date
Collected
Sample ID
Appendix I
VOCs
1,4-Dioxane
Appendix I
Metals
Mercury
Calcium,
Magnesium,
Hardness
VOCs
EPA 8260D
EPA 8260D
SIM
EPA 6020B
EPA 7470A
EPA 200.7
EPA 524.2
DW-01
03/10/2021
DW-01-20210310
X
LT-01
03/10/2021
LT-01-20210310
X
X
X
SW-01
03/09/2021
SW-01-20210309
X
X
X
X
X
SW-02
03/09/2021
SW-02-20210309
X
X
X
X
X
TB-01
03/09/2021
TB-202103090000
X
TB-02
03/10/2021
TB-202103100000
X
Groundwater and Surface Water Samples: Monitored Natural Attenuation Parameters
Location ID
Date
Collected
Sample ID
COD
BOD
Ferrous Iron
Total
Alkalinity
to pH 4.5
Nitrate
as N
Chloride
Sulfate
TOC
Sulfide
Volatile Fatty
Acids
Carbon
Dioxide
Ethane,
Ethene,
Methane
Dissolved
Hydrogen
SM 5220D
SM 5210B
SM 3500-Fe D
SM 2320B
EPA 9056A
SM 9060A
SM4500-S F
AM20GAX
MW-01
03/10/2021
MW-01-20213010
X
X
X
X
X
X
X
X
X
X
X
X
MW-02
03/10/2021
MW-02-20210310
X
X
X
X
X
X
X
X
X
X
X
X
MW-03
03/09/2021
MW-03-20210309
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-04
03/09/2021
MW-04-20210309
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-05R
03/09/2021
MW-05R-20210309
X
X
X
X
X
X
X
X
X
X
X
X
MW-06
03/10/2021
MW-06-20210310
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-07
03/09/2021
MW-07-20210309
X
X
X
X
X
X
X
X
X
X
X
X
X
Notes:
Appendix II constituents were analyzed per Title 40 Code of Federal Regulations, Part 258.
Blank cell: Analysis was not performed on that sample.
AM: Analytical Method
BOD: biochemical oxygen demand
COD: chemical oxygen demand
EPA: U.S. Environmental Protection Agency (method)
PCBs: Polychlorinated biphenyls
SIM: Selective Ion Monitoring
SM: Standard Method
SVOCs: Semi -volatile organic compounds
TB: Trip Blank
TOC: total organic carbon
VOC: volatile organic compound
Spring 2021 Semiannual Water Quality Monitoring Report Page 1 of 1
Jackson County Closed Municipal Solid Waste Landfill June 2021

Table 2
Well Construction Details and Corresponding Elevations
Stick Up
Depth to
Depth to
Elevation of
Ground
(feet
Depth To
Approximate
Approximate
Top of
Bottom of
Top Elevation
Bottom of
Surface
TOC
above
Total Well
Water
Depth to
Top of Bedrock
Screened
Screened
of Screened
Screened
Geology of
Source of Well
Elevation
Elevation
ground
Depth
(feet below
Groundwater
Bedrock
Elevation
Interval
Interval
Interval
Interval
Screened
Construction
Facility Permit
Well ID
Date Drilled
(feet)
(feet)
surface)
(feet bgs)
TOC)
Elevation (feet)
(feet bgs)
(feet)
(feet bgs)
(feet bgs)
(feet)
(feet)
Interval
Information
MW-01
04/23/1992
2,169.40
2,171.42
2.0
110.5
94.19
2,077.23
83.0
2,086.40
95.0
110.0
2,074.40
2,059.40
Bedrock
MW-02
04/22/1992
2,013.15
2,015.38
2.3
60.7
36.55
1,978.83
13.0
2,000.15
45.0
60.0
1,968.15
1,953.15
Bedrock
Partially
S&ME, Inc.
MW-03
04/21/1992
2,044.16
2,045.53
1.3
65.5
40.10
2,005.43
57.0
1,987.16
48.5
63.5
1,995.66
1,980.66
Weathered Rock
50-02
MW-04
04/21/1992
1,978.68
1,980.77
2.0
43.0
24.85
1,955.92
NA
NA
25.0
40.0
1,953.68
1,938.68
Saprolite
MW-05R
01/26/2012
2,027.98
2,030.95
2.8
54.0
43.97
1,986.98
NA
NA
44.0
54.0
1,983.98
1,973.98
Saprolite
MW-06
03/23/2004
2,136.58
2,139.57
3.0
94.0
75.20
2,064.37
47.6
2,088.98
84.6
94.6
2,051.98
2,041.98
Bedrock
Altamont
Environmental, Inc.
MW-07
07/30/2010
1,978.71
1,981.29
2.6
95.0
29.02
1,952.27
44.0
1,935.00
70.0
95.0
1,908.71
1,883.71
Bedrock
Notes:
Elevations associated with wells MW-01, MW-02, MW-03, MW-04, and MW-06 are measured relative to mean sea level and are based on surveying completed by Davenport & Associates, Inc.
Elevations associated with wells MW-05R and MW-07 are measured relative to horizontal North American Datum 83 and are based on surveying completed by Wes Cole Land Surveying, PA.
Depth to water was measured on March 9 and 10, 2021.
Depth to bedrock and screened interval for MW-01 through MW-04 was taken from S&ME, Inc., boring logs completed April 21 through 23, 1992.
Depth to bedrock and screened interval for MW-06 was taken from an Altamont Environmental, Inc., boring log completed March 23, 2004.
Depth to bedrock and screened interval for MW-07 was taken from an Altamont Environmental, Inc., boring log completed July 30, 2010.
nanth to hcrlrnrlr and cr-ncrl intcn-I fnr t\A\A/-()FP %A-C tnL-n from an Alt-nnt F-firnnmental Inr hnrinn Inn rmmnlctcrl Ianiinn/ ''M M19
Monitoring well MW-05 was abandoned on January 26, 2012, by NYEG Drilling, LLC. Monitoring well MW-05R was installed by NYEG Drilling, LLC, on January 26, 2012, as a replacement to MW-05.
Monitoring well MW-05R was surveyed by Wes Cole Land Surveying, PA, on September 28, 2012.
bgs: below ground surface
NA: not applicable
TOC: top of casing
Spring 2021 Semiannual Water Quality Monitoring Report Page 1 of 1
Jackson County Closed Municipal Solid Waste Landfill June 2021

Table 3
Analytical Summary
Domestic Well
Sample
Leachate
Sample
Monitoring Well Samples
Surface Water Samples
QC Samples
Location ID
DW-01
LT-01
MW-01
MW-02
MW-03
MW-04
MW-OSR
MW-06
MW-07
SW-01
SW-02
FielcIQC
FieIdQC
Sample ID
DW-01-
20210310
LT-01-
20210310
MW-01-
20210310
MW-02-
20210310
MW-03-
20210309
MW-04-
20210309
MW-OSR-
20210309
MW-06-
20210310
MW-07-
20210309
SW-01-
20210309
SW-02-
20210309
TB-
202103090000
TB -
202103100000
Sample Date
3/10/2021
3/10/2021
3/10/2021
3/10/2021
3/9/2021
3/9/2021
3/9/2021
3/10/2021
3/9/2021
3/9/2021
3/9/2021
3/9/2021
3/10/2021
Sample Type
N
N
N
N
N
N
N
N
N
N
N
TB
TB
Matrix
WG
WG
WG
WG
WG
WG
WG
WG
WG
WS
WS
WQ
WQ
X
730117.7
730041.8
729526.4
728841.4
729285.1
729406
729649.3
729170.4
729395.8
729383.4
728409
Y
618143.8
617628.1
618129.2
617869.4
617628.9
617105.4
617259.7
618177.5
617118.8
616840.8
618322.7
Method
NC21.
NC2L
IMAC
NC213
Conventional Parameters
Water Level Depth (ft)
Field Measure
--
94.19
36.SS
40.1
24.85
43.97
75.2
29.02
--
--
Temperature (field) (°C)
Field Measure
15.2
16.7
18.2
17.6
16.3
14.4
19
15.2
15.2
7.7
8.2
pH (field) (SU)
Field Measure/SM4500
6.5-8.5
6.0-9.0
6.S
6.9
5.8
6.0
6.7
5.4
6.6
5.0
5.7
7.6
6.6
Turbidity (field) (NTU)
Field Measure
<_50
9.8
20.5
8.47
225
8.76
4.67
74.4
5.91
5.39
12.2
8.2
Dissolved oxygen (field)
Field Measure
>_6
7.24
6.46
2.56
6.23
6.83
6.49
0.84
1.42
1.79
11.61
11.46
Specific Conductivity (field) (µmhos/cm)
Field Measure
59.3
3776
218.8
188.2
376
537.5
685
53.5
802
30.5
30.6
ORP (mV)
Field Measure
157.5
-55.7
-11.3
137.9
197.1
351
-129.9
262.4
147.5
221.9
274.6
Hardness as Ca and Mg (mg/L)
SM2340C
--
--
--
--
--
--
--
--
10.2
8.5
Monitored Natural Attenuation Results
Alkalinity, Total (µg/L)
SM2320B
20000
99
47
140
80
222
22
256
--
--
Biochemical oxygen demand (mg/L)
SM5210B
2 U
4
2 U
2
12
2 U
2
Chemical oxygen demand (mg/L)
SM5220C
11 U
11 U
11 U
11 U
65
11 U
12 J
Chloride (mg/L)
SW9056A
250
230
1.11
19.1
16.8
33
51.7
0.35 U
82.5
Nitrate as nitrogen (mg/L)
SW9056A
0.045 U
0.355
3.59
3.57
0.078 J
0.045 U
0.045 U
Sulfate (mg/L)
SW9056
250
0.56 U
110.4
3.77
123
0.56 U
0.56 U
27.3
Sulfide (mg/L)
SM4500S2F
0.83 U
0.83 U
29.7
44.8
0.83 U
39.6
36.2
Total organic carbon (mg/L)
SM5310B
1.14
4.96
2.43
1.6
4.36
0.5 U
2.89
Ferrous iron (µg/L)
SM3500FEB
1000
38900
50 U
50 U
50 U
50 U
50 U
190 J
Ethane (µg/L)
AM20GAX
0.075 U
0.075 U
0.075 U
0.075 U
0.57 J
0.075 U
0.21 J
Ethene (µg/L)
AM20GAX
0.12 U
0.12 U
0.12 U
0.12 U
0.6 J
0.24 J
0.2 J
Hydrogen (nM)
EPA RSK-175
--
I--
190
19
--
22
9.2
Methane (µg/L)
AM20GAX
1700
4.3 J
3.1 J
300
2300
25
470
Acetic acid (mg/L)
AM23G
5000
0.15 J
0.39 J
0.14 J
0.13 J
1.2 U
0.13 J
0.12 U
Butyric Acid (mg/L)
AM23G
0.058 U
0.12 U
0.058 U
0.073 J
0.58 U
0.058 U
0.21 J
Formic acid (mg/L)
AM23G
7.6
13
6.9
6.9
74
6.6
7.5
Carbon dioxide (µg/L)
AM20GAX
108000
29600
8310
92900
1460
150000
1 133000
--
--
Appendix I Metals, Total (µg/L)
Arsenic
SW6020
10
10
2.9
0.17 U
2.57
0.255 J
0.17 U
0.629 J
0.17 U
0.17 U
0.17 U
0.17 U
Barium
SW6020
700
21000
360
109
116
130
68.3
135
46.8
405
13.8
22.7
Beryllium
SW6020
4
0.19U
0.19U
0.19U
0.19U
0.19U
0.307J
0.19U
0.19U
0.19U
0.19U
Cadmium
SW6020
2
*0.07
0.16 U
0.16 U
0.16 U
0.16 U
0.257 J
0.218 J
0.16 U
0.16 U
0.76 U
0.76 U
Chromium
SW6020
10
*10.64
2.99
0.79 U
19.8
0.823 J
0.79 U
5.83
0.79 U
0.79 U
0.79 U
3.06
Cobalt
SW6020
1
3.97
146
125.1
0.738 J
1.97 J
13.6
12.5
1.69 J
0.52 U
0.646 J
Copper
SW6020
1000
*1.18
3.8 U
3.8 U
18.8
3.8 U
3.8 U
11.1
3.8 U
3.8 U
3.8 U
3.8 U
Lead
SW6020
15
*0.18
0.26 U
0.26 U
4.66
0.26 U
0.26 U
2.34
0.26 U
0.26 U
0.26 U
0.652 J
Nickel
SW6020
100
*7.00
23.6
16
14.5
0.858 J
0.861 J
5.92
4.19
6.67
0.51 U
1.92 J
Selenium
SW6020
20
5
0.74 U
0.74 U
9.01
0.74 U
0.74 U
2.04 J
0.74 U
0.74 U
0.74 U
0.74 U
Vanadium
SW6020
0.3
7.3 U
7.3 U
26
7.3 U
7.3 U
6.37
7.3 U
7.3 U
1.3 U
3.03 J
Zinc
SW6020
1000
*15.73
6.9 U
23.9
81.6
6.9 U
6.9 U
34.6
6.9 U
6.9 U
6.9 U
6.9 U
Spring 2021 Semiannual Water Quality Monitoring Report Page 1 of 3
Jackson County Closed Municipal Solid Waste Landfill June 2021

Table 3
Analytical Summary
Domestic Well
Sample
Leachate
Sample
Monitoring Well Samples
Surface Water Samples
QC Samples
Location ID
DW-01
LT-01
MW-01
MW-02
MW-03
MW-04
MW-05R
MW-06
MW-07
SW-01
SW-02
FieldQC
FieIdQC
Sample ID
DW-01-
20210310
LT-01-
20210310
MW-01-
20210310
MW-02-
20210310
MW-03-
20210309
MW-04-
20210309
MW-0511-
20210309
MW-06-
20210310
MW-07-
20210309
SW-01-
20210309
SW-02-
20210309
TB-
202103090000
TB -
202103100000
Sample Date
3/10/2021
3/10/2021
3/10/2021
3/10/2021
3/9/2021
3/9/2021
3/9/2021
3/10/2021
3/9/2021
3/9/2021
3/9/2021
3/9/2021
3/10/2021
Sample Type
N
N
N
N
N
N
N
N
N
N
N
TB
TB
Matrix
WG
WG
WG
WG
WG
WG
WG
WG
WG
WS
WS
WQ
WQ
X
730117.7
730041.8
729526.4
728841.4
729285.1
729406
729649.3
729170.4
729395.8
729383.4
728409
Y
618143.8
617628.1
618129.2
617869.4
617628.9
617105.4
617259.7
618177.5
617118.8
616840.8
618322.7
Method
NC21-
NC2L
IMAC
NC2B
Appendix I Metals, Dissolved (pg/L)
Barium SW6020
700
21000
56.1
Cobalt SW6020
1
8.59
Nickel SW6020
100
*4.30
1.6 J
Appendix I Volatile Organic Compounds (VOCs) and 1,4-Dioxane (Ng/L)
1,1-Dichloroethane SW8260D
6
100
--
0.083 U
2.62
0.083 U
0.083 U
0.083 U
0.083 U
0.907
0.083 U
0.083 U
0.083 U
0.083 U
0.083 U
1,2-Dichloroethene, cis- SW8260D
70
720
0.00050 U
0.056 U
3.82
0.056 U
0.056 U
0.494 J
1.06
0.781
2.22
0.056 U
0.056 U
0.056 U
0.056 U
1,4-Dioxane SW8260DSIM
3
--
55.5
0.139 U
0.139 U
0.139 U
2.16
2.87
0.139 U
0.139 U
0.139 U
--
--
2-Hexanone (Methyl butyl ketone) SW8260D
40
0.065 U
0.065 U
0.065 U
0.065 U
0.065 U
4.92 J
0.065 U
0.065 U
0.065 U
0.065 U
0.065 U
0.065 U
Acetone SW8260D
6000
2000
--
20.2
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
Benzene SW8260D
1
51
0.00050 U
1.49
1.07
1 0.048 U
0.048 U
0.236 J
0.048 U
0.048 U
0.048 U
0.048 U
0.048 U
Chlorobenzene SW8260D
50
140
0.00050 U
3.13
1.45
0.062 U
0.062 U
1.21
9.01
0.062 U
5.24
0.062 U
0.062 U
0.062 U
0.062 U
Chloroethane SW8260D
3000
--
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.481 J
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
m,p-Xylene SW8260D
500
550
0.12 U
0.12 U
0.12 U
0.289 J
0.12 U
0.12 U
0.12 U
0.342 J
0.12 U
0.12 U
0.12 U
0.12 U
Tetrahydrofuran SW8260D
--
82.9
1.1 U
1.1 U
1.1 U
1.1 U
4.9 J
1.1 U
2.96 J
1.1 U
1.1 U
1.1 U
1.1 U
Toluene SW8260D
600
0.36
0.00050 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.214 J
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
Total Xylene SW8260D
0.00050 U
0.500 U
0.500 U
0.500 U
0.289 J
0.044 U
0.044 U
0.500 U
0.342 J
0.044 U
0.044 U
0.044 U
0.500 U
Trichloroethene (TCE) SW8260D
3
30
0.00050 U
0.078 U
0.545
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
Vinyl chloride SW8260D
0.03
2.4
0.00050 U
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
2.33
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
1,2-Dichlorobenzene SW8260D
20
0.00050 U
0.076 U
0.076 U
0.076 U
0.076 U
0.076 U
0.264 J
0.076 U
0.36 J
0.076 U
0.076 U
0.076 U
0.076 U
1,4-Dichlorobenzene SW8260D
6
56
10.00050 U
3.44
9.33
0.05 U
0.05 U
1.53
6.05
1.04
5.46
0.05 U
0.05 U
0.05 U
0.05 U
Spring 2021 Semiannual Water Quality Monitoring Report Page 2 of 3
Jackson County Closed Municipal Solid Waste Landfill June 2021

Table 3
Analytical Summary
N otes:
'Detected concentration is greater than NC2L or NC2L IMAC standard
Detected concentration is greater than NC26 standard
Bold: Detected result
Italicized: Non -detected concentration is above one or more identified NC2L standard
*: 2B surface water standard calculated using average analyzed hardness value (calculated from the upstream and downstream sampling location results) via the most stringent hardness -dependent metal
calculation, per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards (last amended September 2017).
NC26: surface water standard per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B — Surface Water and Wetland Standards (last amended in September 2017),
or the standard obtained from the EPA Nationally Recommended Water Quality Criteria for Aquatic Life and Human Health.
NC2L: Subchapter 2L — Groundwater Classifications and Standards, Department of Environmental Quality (Amended April 1, 2013). Groundwater standard from North Carolina Administrative Code, Title 15A.
All nondetect results are reported at the method detection limit.
Appendix I: per 40 Code of Federal Regulations Part 258
Horizontal coordinate datum is NAD 1983 State Plane North Carolina FIPS 3200 (US Survey Feet).
--: not sampled
°C: degrees Celsius
Ng/L: micrograms per liter
pmhos/cm: micromhos per centimeter
ft:feet
GW: groundwater
IMAC: Interim Maximum Allowable Concentration. IMAC concentrations are listed in Appendix #1 of the 2L.
J: Estimated value
mg/L: milligrams per liter
mv: millivolts
N: normal environmental sample
NTU: nephelometric turbidity unit
ORP: oxidation-reduction potential
SU: standard unit
SW: surface water
TB: Trip Blank
U: Compound analyzed for, but not detected above minimum detection limit
WG: groundwater sample
WQ: water quality
11
Spring 2021 Semiannual Water Quality Monitoring Report Page 3 of 3
Jackson County Closed Municipal Solid Waste Landfill June 2021

Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the Leachate Sample (LT-01)
Sample Dates
Detected Volatile Organic
Compounds
Concentration
in LT-01
(mg/L)
Cumulative
Flow at Gauge
(gallons)
Differential
Flow
(gallons)
Mass
Removed
(pounds)
Estimated Cumulative
Mass Removed
(pounds)
Beginning
Ending
09/01/2012
10/25/2012
1,4-Dichlorobenzene
0.0034
11,500
11,500
0.00033
4-Methyl-2-pentanone (MIBK)
0.0021
J
0.00020
Acetone
0.0292
0.00280
Benzene
0.0021
0.00020
Chlorobenzene
0.0029
0.00028
cis-1,2-Dichloroethene
0.00063
J
0.00006
Dichlorodifluoro-methane
0.00093
J
0.00009
Ethylbenzene
0.0102
0.00098
Naphthalene
0.0069
0.00066
Styrene
0.00033
J
0.00003
Toluene
0.003
0.00029
X lene (Total)
10.0094
0.00090
Total
0.00682
0.00682
10/26/2012
04/11/2013
1,4-Dichlorobenzene
0.006
65,500
54,000
0.00270
Acetone
0.012
J
0.00540
Benzene
0.0011
0.00049
Carbon disulfide
0.0067
J
0.00301
Chlorobenzene
0.0024
J
0.00108
cis-1,2-Dichloroethene
0.00058
J
0.00026
Ethylbenzene
0.0083
0.00373
Toluene
0.00059
J
0.00027
X lene (Total)
0.0078
0.00351
Total
0.02045
0.02727
04/12/2013
10/08/2013
1,4-Dichlorobenzene
0.0055
114,737
1
49,237
0.00226
4-Meth I-2- entanone (MIBK)
0.0012
J
0.00049
Benzene
0.0020
0.00082
Chlorobenzene
0.0039
0.00160
cis-1,2-Dichloroethene
0.00080
J
0.00033
Ethylbenzene
10.0151
1
0.00619
Naphthalene
0.0184
0.00754
Toluene
0.0012__d
0.00049
Xylene (Total)
0.0090
0.00369
Total
0.02341
0.05068
10/09/2013
04/08/2014
1,4-Dichlorobenzene
0.0056
168,821
54,084
0.00252
Benzene
0.0018
0.00081
Chlorobenzene
0.0051
0.00230
cis-1,2-Dichloroethene
0.00049
J
0.00022
Ethylbenzene
0.0047
0.00212
Toluene
10.000411
J
0.00018
X lene (Total)
10.0021
1 J
0.00095
Total
0.00910
0.05978
04/08/2014
10/23/2014
1,4-Dichlorobenzene
0.0053
179,652
10,831
0.00048
Benzene
0.0014
0.00013
Chlorobenzene
0.003
0.00027
cis-1,2-Dichloroethene
0.00049
J
0.00004
Ethylbenzene
0.0027
0.00024
Toluene
10.000511
J
0.00005
X lene (Total)
10.0014
1 J
0.00013
Total
0.00133
0.06111
10/23/2014
04/21/2015
1,2,3-Trimethyl benzene
0.00062
219,965
40,313
0.00021
1,2,4-Trimethyl benzene
0.00076
0.00026
2-Chlorotoluene
0.00067
0.00022
1,4-Dichlorobenzene
0.0059
0.00198
Acetone
0.00790
0.00265
Benzene
0.0022
0.00074
Chlorobenzene
0.003
0.00101
Ethylbenzene
0.0056
0.00188
Isopropyl benzene
0.0013
0.00044
Methy Tert-butyl -Ether
0.0013
0.00044
Na thalene
0.024
0.00806
n-Propylbenzene
0.00088
0.00030
Tetra hyd rofu ra n
0.089
0.02988
Toluene
0.00054
J
0.00018
Vinyl Chloride
0.00038
J
0.00013
X lene (Total)
10.0030
J
0.00101
Total
0.04937
0.11048
04/21/2015
10/13/2015
1,4-Dichlorobenzene
0.00600
256,685
36,720
0.00183
2-Butanone
0.00960
J
0.00294
Benzene
0.00210
0.00064
Chlorobenzene
0.0040
0.00122
Ethylbenzene
0.00710
0.00217
m, -X lenes
0.0014
0.00043
Naphthalene
0.021
0.00642
o-Xylene
0.0017
0.00052
Tetrah drofuran
0.062
0.01896
Toluene
0.00058
J
0.00018
Total X lenes
10.0031
J
0.00095
Total
0.03626
0.14674
10/13/2015
04/05/2016
1,4-Dichlorobenzene
0.00590
315,663
58,978
0.00290
Benzene
0.00170
0.00083
Chlorobenzene
0.0038
0.00187
Ethylbenzene
0.00500
0.00246
m, -X lenes
0.0010
0.00049
o-X lene
10.0015
1
0.00074
Toluene
10.00063
J
0.00031
Total Xylenes
10.0025
J
0.00123
Total
0.01082
0.15756
04/05/2016 10/11/20161 No detected compounds. 331,010 15,347
0.00000
Total
0.00000
1 0.15756
Spring 2021 Semiannual Water Quality Monitoring Report Page 1 of 2
Jackson County Closed Municipal Solid Waste Landfill June 2021

Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the Leachate Sample (LT-01)
Sample Dates
Detected Volatile Organic
Compounds
Concentration
in LT-01
(mg/1-)
Cumulative
Flow at Gauge
(gallons)
Differential
Flow
(gallons)
Mass
Removed
(pounds)
Estimated Cumulative
Mass Removed
(pounds)
Beginning
Ending
10/11/2016
03/21/2017
1,4-Dichlorobenzene
0.0046
334,212
3,202
0.00012
Acetone
0.0094
J
1
0.00025
Benzene
0.0015
0.00004
Chlorobenzene
0.0043
0.00011
Eth (benzene
0.0014
0.00004
m, -X lenes
0.0006
J
0.00002
o-X lene
0.00092
1
0.00002
Tetrahydrofuran
0.066
0.00176
Total X lenes
0.0015
J
0.00004
Total
0.00241
0.1 S997
03/21/2017
10/11/2017
1,4-Dichlorobenzene
0.0041
364,760 30,548
0.00104
Acetone
0.0067
J
0.00170
Acetonitrile
0.008
J
Benzene
0.00061
0.00016
Chlorobenzene
0.0012
0.00031
Eth (benzene
0.00087
0.00022
Naphthalene
0.0012___H
0.00031
Tetrah drofuran
0.12
0.03053
Total
0.03630
0.19627
Issue with totalizer
between October 2017 and March 2018
03/21/2018
10/18/2018
1,4-Dichlorobenzene
0.0028
1,784,710 159,341
0.00372
Acetone
0.017
1
0.02256
Benzene
0.0012
0.00159
Chlorobenzene
0.0024
0.00318
Eth (benzene
0.0018
0.00239
m,p-Xylenes
10.00038
1 J
0.00050
Methylene Chloride
0.00034
J
0.00045
o-X lene
0.00060
0.00080
X lenes, Total
0.00098
J
0.00130
Total
0.04
0.23
10/18/2018
10/22/2019
1,4-Dichlorobenzene
0.0037
2,045,960 261,250
0.00805
Acetone
0.006
0.01305
Benzene
0.0017
0.00370
Chlorobenzene
0.0038
0.00827
Eth (benzene
0.0016
0.00348
o-X lene
0.00110
0.00239
Toluene
10.000391
J
0.00085
Xylenes, Total
10.0017
J
0.00370
Total
0.04
0.28
10/22/2019
03/18/2020
1,4-Dichlorobenzene
0.0056
2,139,992 94,032
0.00438
1,4-Dioxane
0.06
0.04697
Acetone
0.0064
0.00501
Benzene
0.0013
0.00102
Chlorobenzene
0.0032
0.00250
Eth (benzene
0.0027
0.00211
m, -X lenes
0.00089
J
0.00070
Methyl isobut I ketone
0.00079
J
0.00062
o-X lene
0.00120
0.00094
Toluene
0.00070
0.00055
Total
0.06
0.34
03/18/2020
10/14/2020
1,2-Dichloroethene, cis-
0.00029
J
2,238,782 98,790
0.00024
1,3-Dichlorobenzene
0.00027
J
0.00022
1,4-Dichlorobenzene
0.0048
0.00395
1,4-Dioxane
0.058
0.04770
Acetone
0.011
0.00905
Acetonitrile (Ethanenitrile)
0.0047
J
0.00387
Benzene
0.0024
0.00197
Chlorobenzene
0.0044
0.00362
Chloroethane
0.00047
J
0.00039
Eth (benzene
0.0018
0.00148
m, -X lene
0.0017
0.00140
Naphthalene
0.013
0.01069
o-X lene
0.002
0.00164
Tetrah drofuran
0.094
0.07731
Toluene
0.00079
0.00065
Total X lene
0.0037
0.00304
Vin I chloride
10.00022
J
0.00018
Total
0.17
O.S 1
Totalizer buried during March 2021 sampling event
Notes:
1. No VOCs were detected in the leachate sample collected during the October 2016 sampling event.
Only detected volatile organic compounds (VOCs) in leachate sample LT-01 are included in the mass removal calculation.
Leachate extraction at the landfill was initiated on September 1, 2012.
Extraction volume measurements were recorded and provided by Jackson County staff.
Anchor QEA bases mass removal calculations on the assumption that the VOCs concentration in one sampling event is representative of leachate quality until the next sampling event occurs, and
that the leachate removal system has a 100% removal and treatment efficiency.
Due to a malfunction with the leachate totalizer, there is a gap in total volume calcuations between October 11, 2017 and March 21, 2018.
During March 2021 sampling, Anchor QEA observed that the leachate totalizer was covered and potentially destroyed due to construction happening at the Green Energy Center.
Represents the total flow between the LT-01 sample dates.
Estimated cumulative mass removed and treated is estimated based upon a conversion of milligrams to pounds and liters to gallons and the multiplication of the concentration by the differential
flow for the specified period.
mg/L: milligrams per liter
J: Indicates laboratory estimated concentration is above the adjusted method detection limit and below the adjusted reporting limit.
Spring 2021 Semiannual Water Quality Monitoring Report Page 2 of 2
Jackson County Closed Municipal Solid Waste Landfill June 2021

Figures

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LEGEND: SOURCES:
1. BaUSGS Topographic Maps Greens
® Site Parcel Boundary Creekk and Whittier 7.5-minute Quadrangles
2. Parcel: Jackson County GIS
0 2,000
Feet
Publish Date: 2021/03/24, 4:10 PM I User: alesueur
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)P, ANCHOR Figure 1
Q E A Site Location Map
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

-02
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LEGEND:
Monitoring Well — Road
Landfill Gas Extraction Well Elevation Contour (20-Foot Interval)
® Domestic Well Sample Location 0 Property Boundary
❑ Leachate Sample Location and
Flow Equalization Tank
Surface Water Sample Location
MW-03 +*
LT-01
MW-05R
MW-07 \ 04
NOTE:
Sample locations are approximate.
SOURCES:
Aerial Imagery: Esri Online Services
Contours, Roads, and Parcels: Jackson County GIs
Publish Date: 2021/03/24, 4:12 PM I User: alesueur
Filepath: \\orcas\gisVobs\JacksonCounty-NC-1480\Maps\2021\SpringWQ\AQ_Fig02-Jackson County-SpringWQ2021-SampleLocationMap.mxd
n
0 500
Feet
11
kZANCHOR Figure 2
QEA-- Site Layout Map
Anchor QEA of North Carolina, PLLC
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

LEGEND:
® Saprolite Monitoring Well — Stream
® PWR Monitoring Well — Road
® Bedrock Monitoring Well Elevation Contour (20-Foot Interval)
Property Boundary (2,005.43) Groundwater Elevation
(March 9 and 10, 2021)
immAi-nti
\ 2100
CONN
D1
3)/
27g0
2120 aG� c
O
ta\`��eGtOG�
t
Ge � feat
Q� dot
•MW-03 0
(2,005.43) N
2�AO 60
Z c
3
Cqt o Q
w°
MW-07
952.27).
�MW-04
(1,955.92)
WILKEY
218
•MW-05R
i
2020
(1,986.98)
NOTES:
1. Monitoring well locations are approximate.
2. Groundwater elevations and flow direction are updated on a semiannual basis following sample collection events
in March and October.
3. Groundwater flow direction is based on groundwater elevations from all Site monitoring wells. Direction is
calculated based on depth to water measured on March 9 and 10, 2021.
4. Last names of property owners are shown in parcels that border the landfill property.
5. PWR: partially weathered rock
6. Groundwater elevation in feet (North American Vertical Datum 1988)
Publish Date: 2021/03/24, 4:20 PM I User: alesueur
Filepath:\\orcas\gis\)obs\JacksonCounty_NC_1480\Maps\2021\SpringWQ\AQ_Fig03_JacksonCounty_SpringWQ2021_GroundwaterElevationMap.mxd
WILKEY
\0
PtR
WILKEY
0
N
/ y
WILKEY
2100
SOURCES:
1. Elevation contours, roads, and parcels: Jackson County GIS
2. Groundwater elevations: calculated from surveys
performed by Davenport & Associates, Inc. (MW-01, MW-02,
MW-03, MW-04, and MW-06) and Wes Cole Land Surveying,
PA (MW-05R and MW-07) 0
0 200
Feet
N
0
Z}�
ANCHOR Figure 3
QEA—`-�" Generalized Groundwater Flow Direction
Anchor QEA of North Carolina, PLLC
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

Figure 4
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-01)
20
in
,^ 16
J
p1
14
0
12
a,
v
C
Uo 10
a
a,
c 8
a
0
0 6
s
v
0
4
2
A
r I'- Co Co rn rn O O N
CD CD O O
N
m m
� � 2
2
2 2
r co 02 rn O
N
CDCD
N N
CD CD CD O CD CD O O O O
cV N N N N N N r\1 [V N N
O
N
O O
N N
O O O
N fV ["I
O
N
O O
N N
O O O O O O O
N N N N N r\I N
O O
N N
Q v Q v Q v Q v Q v Q
Q o a o Q o Q o Q o Q
v
o
�--
Q v
Q o
�--
Q v Q
Q o Q
}i
v
o
a--'
Q v
Q o
ra v ca v � v �
2 o 2 o 2 o 2
v ca
o
Notes:
1. NC 2L (2013) standard = 6 micrograms per liter (µg/L)
Sampling Date
p g
1,4-Dichlorobenzene
2. "J" indicates result is estimated by laboratory.
NC21- (2013) Standard
3. "<" indicates result is less than method detection limit.
4. Oct 2017 result reported in semivolatile organic compound list.
Groundwater Elevation
2080
2078
a1](i
v
2074 o
a
v
W
2072
�a
3
2070
0
l7
2064
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 June 2021

Figure 5
Hydrograph and Benzene Concentration vs. Time
(Monitoring Well MW-01)
12
10
J
= 8
0
a
a
N
G!
CO 4
2
U
r r 00 00 M 0') O O
O O O O O O —
N
N
m m
V Ln
Ln
�.O
Q0
—
�
—
r—
—
00
—
00
—
M M O O
— N N
N
O CD CD CD CD CDO CD CD CD
N N N N N N N N N N
CD
N
CDO
N
O O
N N N
CDO
N N
O
N
O
N
CD
N
CD
N
CD
N
O
N
CD
N
O O O O
N N N N
O
N
� v �
Q Q Q Q �.� Q �.�
0 0 0 0 Q 0 Q 0 Q 0
Q
Q
v
0
�
Q Q
Q 0 Q
�.� Q
0 Q
�.%
0
Q
Q
U
0
co
2
U
0
ca
v
0
ro U ro U
2 0 2 0
co
Notes:
1. NC 2L (2013) standard = 1 microgram per liter (µg/L)
Sampling
Date
0 Benzene
2. "J' indicates result is estimated by laboratory.
NC2L (2013) Standard
3. "<" indicates result is less than method detection limit.
+Groundwater Elevation
2080.00
2078.00
2076.00
2074.00
2072.00 c
.a
a
2070.00 W
a
M
3
2068.00 3
0
L
W
2066.00
2064.00
Spring 2021 Semiannual Water Quality Monitoring Report June 2021
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02

Figure 6
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-05R)
12
10
�,
O O O O O O O
N N N N N N N
+ + +
Notes: Q O Q O Q O Q
Constituent concentration after January 2012 was found in MW-05R.
Constituent concentration before January 2012 was found in MW-05.
Groundwater elevation in October 2011 was interpolated.
NC 2L (2013) standard = 6 micrograms per liter (µg/L)
"J" indicates result is estimated by laboratory
"<" indicates result is less than method detection limit
Oct 2017 result reported in semivolatile organic compound list
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
O O
O
O
O
O O
N N
N
N
N
N N
V Q
V
6
V
6 V
O Q
O
O
g O
Sampling Date
O O N
O O O O O
N N N N N
O O
fi 1,4-Dichlorobenzene
NC2L (2013) Standard
Groundwater Elevation
•::
INIT.
1984
a
0
1982 `U
a,
3
C
3
0
1980 t9
1978
1976
June 2021

Figure 7
Hydrograph and Benzene Concentration vs. Time
(Monitoring Well MW-0511)
3
2.5
1
0.5
O O O O O O O O O O O O O
N N N N N N N rQ N N N N N
Q V Q V Q V Q V Q V (Z V fu
Q O Q O Q O Q O Q O 2 O
Notes: Sampling Date
1. NC 2L (2013) standard = 1 microgram per liter (µg/L)
2. "<" indicates result is less than method detection limit.
0O d, O O
N N N
O O O O O O
N N N N N N
v c`o U a v ro
0 0 g 0 g
Benzene
NC2L (2013) Standard
0 Groundwater Elevation
.;e
1987
1985
0
1983 a,
W
L
d
to
1981
C
3
0
0
1979
1977
1975
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
June 2021

Figure 8
Hydrograph and Vinyl Chloride Concentration vs. Time
(Monitoring Well MW-0511)
4
3.5
3
0.5
0
N
N
M
rv2
Ii
�
Ln
l2
l2
I�
r` W
O
O
O
O
O
O
O
O
O
O
O
O O
N
N
N
N
N
N
N
N
N
N
N
N N
Q
U
Q
U
Q
U
Q
U
Q
U
(6
U (6
Q
O
Q
O
Q
O
Q
O
Q
O
O 2
Notes: Sampling Date
1. NC 2L (2013) standard = 0.03 microgram per liter (µg/L)
2. "J" indicates result is estimated by laboratory.
3. "<" indicates result is less than method detection limit.
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
c0 6� 61 O O
N N N
O O O O O O
N N N N N rV
}J L U
V (6 V (6 V (6
O O g O
IIIIIIIIIIIIIIIIIIIIIIIIIIIIVinyl Chloride
NC2L (2013) Standard
0 Groundwater Elevation
1988
•:.
1984
1980
W
1978
1976
June 2021

Figure 9
Hydrograph and 1,4-Dioxane Concentration vs. Time
(Monitoring Well MW-07)
30
25
20
0
m rn o
N
O O O O
N N N N
V (6 V M
O g O g
Notes: Sampling Date
1. NC 2L (2018) standard = 3 micrograms per liter (µg/L)
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
0
N N
O O
N N
V (6
0 g
1,4-Dioxane
NC2L (2018) Standard
0 Groundwater Elevation
1953
1952
1951
a�
a�
O
1950 -
_a
W
L
1949
3
c
O
1948 C7
1947
1946
June 2021

Figure 10
Hydrograph and Benzene Concentration vs. Time
(Monitoring Well MW-07)
2
flu
1.6
J
01.4
0
1.2
L
a
= 1
0
u
a
0.8
N
_
G!
m
1:
1A
0.2
I
N N M M L2 L2 l2 12 r r` W
O O O O O O O O O O O O O O O
N N N N N N N N N N N N N N N
Q V Q U Q U Q U Q V Q V (�6 V c6
Q O Q O Q O Q O Q O Q O O g
Notes: Sampling Date
1. NC 2L (2013) standard = 1 microgram per liter (µg/L)
2. "<" indicates result is less than method detection limit.
Spring 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
O
O
cV
O
O
O
O
O
O
N
N
N
N
N
N
u
O
o
g
v
O
ai
v
O
cE
2!
O
Benzene
NC2L (2013)
Standard
6
Groundwater
Elevation
1953
1952
1952
0
1951
a
W
L
1950
�a
_
1950 c
0
1949
1949
1948
June 2021

AppendixA
Well Sampling Logs, and Equipment
Documentation and Instrument
Calibration Data Sheets

ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Well Sampling Log
Well ID: MW-01
Project Name:
Jackson County Landfill
Date:
ii
3 lb
Project Number.
C01480-01.02
Weather.
!�
Project Location:
Dillsboro, NC
Facility ID or Permit # (if applicable):
50-02
Sample Collector(s):
M- ken, p PV
f? ,q Sample ID (on COC):
MW-01- 24)1 �3w
Well Diameter.
2
in Sample Time:
031
Screen Interval:
N/A
ft bgs
Measuring Point:
TOC
Well Depth (WD):
110.5 ft TOC
Well Type:
KStick Up ❑Flush Mount
Water Level in Feet (WL):
4 "1 ft TOC
Comments: rAtUcWJ .e_v)eALength of Water Column (LWC):
4 , ft; (WD - WL)
`
l One Casing Volume:
0 gallons; (LWC x WCV)
�. Three Casing Volumes:
gallons
/�.
Actual Volume Purged:
n gallons
Tagged Bottom:
, L. ft at (time):
�3 asing o mes:
al
Well Casing Volumes (WCV)
1" = 0.04 Gal/Ft I 2" 0.16 GA-" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft
8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method:
IV Dis Bailer-Teflo Dedicated Pump Whale Pump Grundfos
Other.
Sample Method:
B er- Bailer -Teflon Dedicated Pump Whale Pump Grundfos
Other.
Oxidation
Dissolved
Specific
pH (S.U.)
Reduction
Gallons
Temperature
Oxygen
Conductivity
report to 0.1
Potential
Turbidity
Reading
Time
Purged
VQ
(mg/L)
(pmhos/cm)
S.U.
(mv)
(NTU)
Comments
1
l2/5
.,
/.C,-f
/ .C.-
20,2
.foe
22
5
17. a_
•
2/0-2
E. 0
-� / /.
3
/
!
r�
-7.
30
7-.)
5
6
7
8
9
10
Sampling Container
Number of Containers Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
_
a iA J
( 0
_
Other
Protective Casing:
Pad: Lock: Vegetation:_CLLV Access:
Sample Analysts
ame
Signature:
Date: �]
Name _ t
Notes: L,/ t
1: Stabilization (3 successi �eadis,inutes apart): within +/- 70% DO and turbidity +/- 3%Conductivity +/- 0.1 pH unit; +/- 70 mV(or ORP
from EPA - Low -Flow (Mini aGroundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are o be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
pmhos/cm: micromhos per centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
ft: feet
in: inches
bgs: below ground surface
TOC: top of casing
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 0 G-2011
pH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR.
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Well Sampling Log
Well ID- MW,-02
Project Name:
Jackson County Landfill
Date: " d ,.( 71
Project Number.
C01480-01.02
Weather:
op�p f>
Project Location:
Dillsboro, NC
Facility ID or Permit # (if applicable):
50-02
Sample Collector(s):�i
Sample ID (on COC):
MW-02-
Well Diameter.
2
in Sample Time: _L �
Screen Interval:
N/A
ft bgs
Measuring Point:
TOC
Well Depth (WD):
60.7 ft TOC
Well Type:
KStick Up ❑Flush Mount
Water Level in Feet (WL):
1 4, S ft TOC
Comments:
Length of Water Column (LWQ:
"Z bft q — ft; (WD - WL)
One Casing Volume: 3 , gallons; (LWC x WCV)
Three Casing Volumes:
gallons
Actual Volume Purged:
�/ gallons
Tagged Bottom: �, ft at (time): - Th= r'acinn VOIu
Itr v�
Well Casing Volumes (WCV)
1" = 0.04 Gal/Ft
2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft
8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method:
Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos
Other:
Sample Method:
Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos
Other.
Oxidation
Dissolved
Specific
pH (S.U.)
Reduction
Gallons
Temperature
Oxygen
Conductivity
report to 0.1
Potential
Turbidity
Reading
Time
Purged
VQ
(mg/L)
(pmhos/cm)
S.U.
(m1)
(NTU)
Comments
1
3
3,
5
2
7 ou
3
4
5
J,23
'A I L
6, Q
6
7
8
9
10
Sampling Container
Number of containers
Requested Analysis
500 mL Plastic
250 mL Plastic]
125 mL Plastic
40 mL Glass
oucz
1 L Glass
Other
Protective Casing:
Pad: Lock: W Vegetation: Access:
Sample Analysts
Signature:
Sample
Analysts
Date:
Name: _ _
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity,' +/- 3% Conductivity, +/- 0.1 pH unit +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
pmhos/cm: micromhos per centimeter
mg/L: milligrams per liter
mV: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
ft: feet
in: inches
bgs: below ground surface
TOC: top of casing
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
QEA `
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
v-Flow Sampling Log
Well ID: MW-03
Project Name:
Project Number:
Project Location:
Sample Collector(s):
Well Diameter:
Screen Interval:
Well Depth (as constructed):
Depth to Water:
Measuring Point:
Depth of Pump Intake:
Pump Used (circle):
Comments:
Jackson County Landfill Date: ���%1
C01480-01.02 Weather: C( e�-
Dillsboro, NC Facility ID or Permit # (if applicable): 50-02
M 4 Sample ID (on COC): MW-03- 24 0 3 6
2 in Arrive at Well: t 3 15—
48.5-63.5 ft bgs Start Time: 1130
65.5 ft bgs Sample Time:
ql V ft Leave Well: �] �
TOC Well Type: XSti k Up ❑Flush Mount
50 ft Tagged Bottom: a, ft at (time): �4-35
Peristaltic Bladder Other (describe): Purge Rate: 350 pk
start miCrosee� Total Volume Purged:
stop microseep: Pump Speed:
Time
DTW (feet)
Temperature (°C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (m1)
Turbidity (INTO)
3 3 0
A` - 15-,q
1-7
T76
c;�d I. t
13,1
t
t576
-7, 7 3
3'71. C)
9
13
7.61
177.6
C,, Y
I
13 3y
D
,s6,
13 L/,X
a 5
?'
uLf. gI
qvL_13
lei
r
Sample Analyst Signature:
Sample Analyst
Name:`
Date:
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity,, +/- 0.1 pH unit; +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
5. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
'C: degrees Celsius S.U.: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches
DO: SM 4500 0 G-2011
mV: millivolt bgs: below ground surface
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOC: top of casing
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
V, QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
j-Flow Sampling Log
iWell
ID: MW-04
Project Name:
Project Number:
Project Location:
Sample Collector(s):
Well Diameter:
Screen Interval:
Well Depth (as constructed):
Depth to Water:
Measuring Point:
Depth of Pump Intake:
Pump Used (circle):
Comments:
Jackson County Landfill
C01480-01.02
Dillsboro, NC
A K/A L
2
25 - 40
43
y
TOC
35
Peristaltic Bladder
Start IIIICfOSe@
Stop micrOSe@X}:
Date: 3 /9 / a 1
Weather. Clew 3TIJ= St. -)I
Facility ID or Permit # (if applicable): 50-02
Sample ID (on COC): MW-04-
in Arrive at Well:
ft bgs StartTime: (j 3
ft bgs Sample Time: Atl 0
ft Leave We] I: K�
Well Type: NStick Up ❑Flush Mount
ft Tagged Bottom: 49L,3 ft at (time):
Other (describe): Purge Rate:
Total Volume Purged:
Pump Speed:
ii
10q_'_�_
t-(o),.,
Time
DTW (feet)
Temperature ("C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (mN)
Turbidity (NTU)
0431
25,3
Q..
3
117i.
IC-1'-lk
.2"';
%3q
Z IT, C)
_?•33
Sl;.a
ilLI
o x
SI i
11-113L
.tc3T-i
(3U. 6
.-,&-13
7,9
�t yy
`173Q.
?3O)C
lat.f
(6
0 1571
ZS", 15
t -1. 3
6.00
7 1
C,1-14t
L -7
S. I
N L-
Z S, a
'-1, 3
G. t-t
I'/ 3
S 1-y 8: S"
3 48
i OC/Q)
G.IT
53'7
3
351,U
Lt. 07
Sample Analyst Signature:
Lz�
Sample Analyst
Name:
Date:
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity,' +/- 0.1 pH unit, +/- 70 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
5. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
°C: degrees Celsius S.U.: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches
DO: SM 4500 0 G-2011
mV: millivolt bgs: below ground surface
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOC: top of casing
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Well Sampling Log
well ID:
/ '.- �.+,,At
Project Name: �� Q'Uyl
�� Date: 3
Project Number: CO (q " � � _ �
Weather:
Project Location: P 4Sb6yo � Nc1
Facility ID or Permit # (if applicable): J
Sample Collector(s): , �
Sample lD (on COQ:
Well Diameter:
in Sample Time: ,rj0-V
Screen Interval: N�
ft bgs
Measuring Point: Q G
Well Depth (WD): ft TOC
Well Type: ick Up ❑Flush Mount
Water Level in Feet (WL): 41 A? ft TOC
Comments:
Length of Water Column (LWQ: �_ ?j ft; (WD - WL)
One Casing Volume: C gallons; (LWC x WCV)
Three Casing Volumes: gallons
Actual Volume Purged:^� gallons
Tagged Bottom: ft at (time):
f � (� in VV11
Well Casing Volumes (WCV)
1" = 0.04 GaVFt = 0 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1A7 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other:
Sample Method: Bailer -Di Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other:
Oxidation
Dissolved
Specific
pH (S.U.)
Reduction
Gallons
Temperature
Oxygen
Conductivity
report to 0.1
Potential
Turbidity
Reading
Time
Purged
VQ
(mg/L)
(pmhos/cm)
S.U.
(m1)
(NTU)
Comments
1
.
(7
lD .
2
a
3
— j
3
4
l5671
L0
D,
5
6
7
8
9
10
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
VOW) I
125 mL Plastic
40 mL Glass
1 L Glass
Other
Protective Casing: Pad; Lo[k Vegetation: Access:
Sample Analysts
Signature:
'el
niamp e
Analysts r.� > Date:
me:
Notes: '
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity, +/- 0.7 pH unit,' +/- 70 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
S.U.: standard units
pmhos/cm: micromhos per centimeter
ft: feet
mg/L: milligrams per liter
in: inches
mv: millivolt
bgs: below ground surface
NTU: nephelometric turbidity units
TOC: top of casing
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
a -Flow Sampling Log
Well ID: MW-06
Project Name: Jackson County Landfill
Project Number. C01480-01.02
Project Location: Dillsboro, NC
Sample Collector(s): A. p4 t 1)77/1
Well Diameter. 2
Screen Interval: 84-94
Well Depth (as constructed): 94
Depth to Water: 4 5 3V
Measuring Point: TOC
Depth of Pump Intake: 91
Pump Used (circle): Peristaltic Bladder
Comments: start microseep:: f 1 :3 p
stop microseep: / 15 6
Date: N A
Weather.
Facility ID or Permit # (if applicable): 50-02
Sample ID (on COC): MW-06- D3 It?
in Arrive at Well: o 31
ft bgs Start Time: /0-5
ft bgs Sample Time: f{ i Ito
ft Leave Well:
Well Type: AStick Up ❑Flush Mount
ft Tagged Bottom: ft at (time):
Other (describe): Purge Rate: �r.
sr
Total Volume Purged:
Pump Speed:
Time
DTW (feet)
Temperature ("C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
PH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (m1)
Turbidity (NTU)
rr
75.3 C
S.2
i'
a•
131
.25
1.2.
r
r 'µ
.)
-2 -3
4.2-c
?3
:k
5.
.2 .2.
I 7
"7r. 3E
I.k7-
•SSJ
-fir
-
l!
C .�$
S.I
r
I /3
24, 3 5
13
02
• 1
1/I
r
15.2
f.4.2
5
�i•
..
Sample Analyst Signature:
Sample Analystp^
Name:
, ,
�/V Y`iJ
Date:
O t
Notes: f
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity,' +/- 0.7 pH unit +/- 70 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
5. 1 pmho/cm = 1 PS/cm
Abbreviations:
Method Reference.
°C: degrees Celsius S.U.: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches
DO: SM 4500 O G-2011
mv: millivolt bgs: below ground surface
PH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOC: top of casing
Turbidity: SM 2130 B-2011
Page 1 of 1

Anchor QEA of North Carolina, PLLC
231 Haywood Street
ANCHOR
QEA
Asheville, North Carolina 28801
,f-Flow Sampling Log
Well ID: MW-07
Project Name: Jackson County Landfill
Project Number. C01480-01.02
Project Location: Dillsboro, NC
Sample Collector(s): ��
Well Diameter. 2
Screen Interval: 70 - 95
Well Depth (as constructed): 95
Depth to Water. 6 _
Measuring Point: TOC
Depth of Pump Intake: 85
Pump Used (circle): Peristaltic Bladder
Comments: Start 111icroSeep: 1�11
Stop microSeep: 1,9 bil
Date: � � lz� f�
Weather: C�i�i%F SCE' r
Facility ID or Permit # (if applicable): 50-02
Sample ID (on COQ: MW-07- �3
in Arrive at Well:
ft bgs Start Time:
ft bgs Sample Time: ( a
ft Leave Well:
Well Type: 1;51(Ick Up oFlush Mount
ft Tagged Bottom: ft at (time):
Other (describe): Purge Rate: 3 C'd ✓"L ,t,,
Total Volume Purged:
_ _ _ _ Pump Speed: �t
Time
DTW (feet)
Temperature (°C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(Ftmhos/cm)
pH (S.U.)
report to 0.1 S U.
Oxidation
Reduction
Poterttial (mV)
Turbidity (NTU)
'7 CIr
2af.G
1U
3 r, � �-
ab
? 11
s .
l �r�. 5-
1
IN
K00
s. �(
1L-11Y. I%
IT.
800
Sr -7
1 `1 S,
f 3
�0C
r t.a
a. 66
1
st-4C)
r411.a
r
i t 10
0 e
I'T.
. 3�
r0
5,1.E
1 K 9' e/
i t
tT-, r
,0
t
�
1k9r 3
ip
5-
t.
t � c
�Da
l/
11EC
'�—r
(Uq
111r, 4 21
1. Pel
f
S. d
'VE e
7.'-I
Sample Analyst Signature:
Sample Analyst
Name:
Date: 3
Notes
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity,, +/- 3% Conductivity,' +/- 0.7 pH unlZ +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
5. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
"C: degrees Celsius S.U.: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches
DO: SM 4500 O G-2011
mV: millivolt bgs: below ground surface
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOC: top of casing
Turbidity: SM 2130 B-2011
1 b pql zs - V. ►ter
Page 1 of 1

,� ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Surface Water Sampling Log
Location ID: SW.-01
Project Name: Jackson County Landfill
3 j
Date: ?1
Project Number:
C01480-01.02
Weather: wmW1/i♦ �j DIt
Project Location:
Dillsboro, NC
Facility ID or Permit # (if applicable): 50-02
Sample Collector(s):
nV-
Sample ID (on COQ SW-01- U-24050q
Comments:
Upstream of landfill
Sample Method (circle
Grab
Syringe
Pump
Bailer-Disp. Other:
one):
Specific
Oxidation
Temperature
Dissolved
Conductivity
pHl (S.U.)
Reduction
Turbidity
Time
VC)
Oxygen (mg/L)
(pmhos/cm)
reportto t7.1 S.U.
Potential (mV)
(NTU)
Comments
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
l 2JA0S
1 L Glass
l
Other
Vegetation: LnL��
Sample Analyst Signature:
Analyst
Name:
Access: �v
Date: 7I q 1
Notes:
1. Documentation errors are to -e crossed out with a sinale line, so the oriainal text is still legible, followed by the staff members initials and date
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
Method Reference:
°C: degrees Celsius
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter
DO: SM 4500 O G-2011
mv: millivolt
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units
Turbiditv: SM 2130 B-2011
S.U.: standard units
Page 1 of 1

kZANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Surface Water Sampling Log
Location ID: SW-02
Project Name: Jackson County Landfill
Project Number: C01480-01.02
Project Location: Dillsboro, NC
Sample Collector(s): _ �[�
Comments: Downstream of landfill
Date: 3
Weather: Q5
Facility ID or Permit* (if applicable): 50-02
Sample ID (on COC): SW-02- ?DAd30
Sample Method (circle
one):
Grab
Syringe
Pump
Bailer-Disp. Other:
Time
Temperature
VC)
Dissolved
Oxygen (mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S. U.
Oxidation
Reduction
Potential (mV)
Turbidity
(NTU)
Comments
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
Other
Vegetation:
Access: vA 6etd -- 6,a"" _
Sample Analyst ,,,
Sample Analyst Signature: Name: 1 w`�""" lQ Date: J a jj 1
NMec-
1. Documentation errors are to be crossed out with a sinale line. so the oriainal text is still leaible. followed by the staff members initials and date
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
Method Reference:
°C: degrees Celsius
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter
DO: SM 4500 0 G-2011
mv: millivolt
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units
Turbiditv: SM 2130 B-2011
S.U.: standard units
Page 1 of 1

Anchor QEA of North Carolina, PLLC
231 Haywood Street
tSZANCHOR
QEA
Asheville, North Carolina 28801
npling Log - Grab
Location ID: LT-01
Project Name:
Jackson County Landfill
Date:
3 10b (i
Project Number.
C01480-01.02
Weather.
q(mwVjc
Project Location:
Dillsboro, NC
Facility ID or Permit # (if applicable):
50-02
Sample Collector(s):
(—
Sample ID (on COC):
LT-01--G3��
Comments:
1
Sample Method (circle one):
Grab
Syringe
Pump Bailer-Disp. Other:
Dissolved
Specific
Oxidation
Temperature
Oxygen
Conductivity
pH (S.U.)
Reduction
Turbidity
Tirmme�/�/
(m'Vg�fy/�L))
(Nmhos/cm)
report to 0.1 S.U.
Potential (mV)
(NVA,TU)
Comments
1((n°C)�tX'
Sampling Container
Number of Containers Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glassy;
[j S
Glass
er
Vegetation:
Access:
Sample Analyst
Sample Analyst Signature: Name: AC Date: /,/-X - -
Notes:
1. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
pmhos/cm: micromhos per centimeter
mg/L milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
npling Log - Grab
Location ID: DW-01
Asheville, North Carolina 28801
Project Name:
Project Number.
Project Location:
Sample Collector(s):
Comments:
Jackson County Landfill Date:
C01480-01.02 Weather:
Dillsboro, INC Facility ID or Permit # (if applicable):
c_i Sample ID (on COC):
Purged 30 gallons prior to sampling. Wilkey residence.
3 10
_ e4- / V 1
50-02 xJ'
DW 01- �1 0
Sample Method (circle one):
Grab
Syringe
Pump
Bailer-Disp. Other:
Time
Temperature
(°C
Dissolved
Oxygen
(mg/L)I
Specific
Conductivity
(pmhhos/cm)
pH (S.U.)
reporttto O.I S.U.
Oxidation
Reduction
Pottennttiall(mV)
Turbidity
(NTU)
Comments
vt�
15.172
JI•3
wiL
/-JiaC
Q i S0
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
1
V (h
125 mL Plastic
40 mL Glass
'Glass
2r
Vegetation: Access:
Sample Analyst zz
Sample Analyst Signature: Name: �(,� Date: �J I I b
Notes: %—.
1. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
pmhos/cm: micromhos per centimeter
mg/L: milligrams per liter
mV: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
pH: SM 4500-H' B-2011
Turbidity. SM 2130 B-2011
Page 1 of 1

ANCHOR
.�, QEA
Equipment Documentation and Instrument Calibration Data Sheet
Project Name: Jackson County Landfill Analyst Conducting Calibration:
Project Number: C01480-01.02 Date of Calibration:
Project Location: Dillsboro, NC Date of Field Measurements:
Facility ID or Permit # (if applicable): 50-02
EQUIPMENT DOCUMENTATION
or meters used to take measurements:
Select Turbidimeter- Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPV1 (s/n 200601045)
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Instrument Readings
Instrument Readings
(Hach 2100Q)
(HF Scfentffic MicroTPUQ
Cal Sid Information
10 NTU
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Lot #
ID D
ration Date•
i
(,l
It 123
Cal (NTU):
Cal (NT
,
Cal (NTU):
Cal (NTU):
Cal (NTU):
Cal (NTU): r
Time: Old ✓
Time: y _ -If
Time:
Time:
Time:
Ime:
Calibration
"Pre -Analysis
Result (NTU):
Time:
"Pre -Analysis
Result (N
Time:
Verification:
Check (10 NTU):
a,
lA p
Check (10 NTU):
*Post -Analysis
ResuI (NTU):
Time*
"Post -Analysis
Result (NTU):
Time:
Check (10 NTU):
Check (I TU)-
YSI Professional Plus Multiparameter Meter (s/n 186101802)
Cal Std Information
Instrument Readings
Lot #
Date
Date
Opened
Dissolved Oxygen
Initial(%):(%):�j
�`
Cal (%):
1-4
mmHg: j)
Temperature (°C):
Time: /��L/�
�"t,
(% saturation)
0 /
o� (ip
�b
t 2
DO (Site #2,
Initial %)!
�SI
Tem to (°C):0tif
Time
�i
applicable)*
QC** Check: DO
Time:
Result (%):
Time:
Result (%):
Time:
Result I%):
H 7 S.U.
Initial:/ 4
b
p HmV:
3
Cal (S.U.):
p HmV:
'-
Time:
report to 0.1 S. U.
• D
•
.01a
`t7
pH4S.U-
Initial: r r 0
J�
pHm1(:l�'
1{F/,
CaI(S.U.):
pHmV: MLO-
Time
loivu�r
report to C.7 S.U.
U
Ji
Initial:
pHmV:�
Cal (Si .L
pHmV1 �.�
� Time:
report to 0.1 S.U.
Y o ,
QC** PH 7 S.U.
Time: NaResult
S.U.)
Ti
Result (S.U.
Time:
Result (S.UJ:
o t
report to 0.1 S. U.
a46
r
Spec. Cond.
P
Initial:
:
Cal (pmhos/cm):
Tim�e::1
a%
1,000 mhos/cm
�D
Recov -
QC** Spec. Cond.
Time:
id
Time:
Result (pmhos/cm):
Time:
Result (pmhos/cm):o��s
�31�1,000
mhos/cm
V
% Recov -
ORP 200 mV
Initial: j
"1,
Cal: 0
Temperature (°q:
t,
Time:
`
1.'�
V
I
V
Analyst Signature: Analyst Name: Date: Q 1
L� j
Not 6, 12/20/20, K
1. Instruments shall be calibrated in accordance with the manufacturer's operation manual.
2 Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. *When performing DO analyses at multiple sample sites (i.e. project/facility locations), the DO probe must be calibrated at each sample site prior to analysis.
5. QC Acceptatle Ranges: PH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
6. ** QC check must be performed prior to sampling and following completion of sampling, at a minimum. CIC checks must be performed with calibration standard from a separate Iota« as the initial QC.
7. % Recovery = (Value Obtained, pmhos/cm + True Value, pmhos/cm) x 100
B. NC Field Laboratory Certificate Number 5445
9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity.
11. 1 pmho/cm = 1 pS/cm
Abbreviations Method Reference:
pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units Temperature: SM 2550 B-2010
*C: degrees Celsius ORP: oxidation reduction potential Specific conductivity. EPA Method 120.1, Rev. 1982
DO: dissolved oxygen s/n: serial number DO: SM 4500 0 G-2011
mg/L• milligrams per liter S.U.: standard units PH: SM 4500-H' B-2011
mV: millivolt Spec. Cond.: Specific Conductivity Turbidity SM 2130 B-2011
Page 1 of 1

R. ANCHOR
Equipment Documentation and Instrument Calibration Data Sheet _
Project Name: Jackson County Landfill Analyst Conducting Calibration:
Project Number. C01480-01.02 Date of Calibration:1 r
Project Location: Dillsboro, NC Date of Field Measurements:
Facility ID or Permit # (if applicable): 50-02
EQUIPMENT DOCUMENTATION
Rental sample analysis equipment or meters used to take measurements:
u ment Type Brand Serial Number Date of Use Rental Company
Select Turbidimeter. Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Instrument Readings
Instrument Readings
(Hach 2100Q)
(HF Scientific MicroTPW)
Cal Std Information
10 NTU
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Lot
EiRiration Date*
Cal (NTU):'
�� VV
Cal (NTU):
Cal (N
Cal (NTU):
Cal (NTU):
Cal i r1W_
Time:
Time:
Time:
Time:
Time:
Time:
Calibration
'Pre -Analysis
Result (NTU),
Time: //
*Pre -Analysis
Resul' U):
Time:
Verification:
Check (10 NTU):
Check 00 NTU):
*Post -Analysis
Result (NTU):
Time:
*Post- s
Result (NTU):
Time:
Check (10 NTU):
Q ,la�
(10 NTU):
YSI Professional Plus MuMparameter Meter (s/n 18B101802)
Cal Std Information
Instrument Readings
Date
Lot #
O coed
Exp. Date
Dissolved Oxygen
Initial (%):
Cal M:
mmHg:
Temperature (oQ:
Time:
(% saturation)
• a
1 V
DO (Site #2,
Initial ( %
Cal %
�Qo*©
m
Ti
my
ifa licable *
13
QC** Check: DO
Time:
Result (%):
Time:
Result (%):
Time:
Result (%):
PH 7 S.U.
Initial:
pHmV:
Cal (S.U.):
pHmV:
Tim :.
otw
'r
report to 0.1 S.U.
r
({(/ •
ld✓VJ
I� .
pH 4 S.U.
Initial:
pHmV:i
+ ►
Cal (S.U.: T
4,V
pHmV:
Time:
!(
report to0.7S.U.
I
✓0
PH 10 S.U.
Initial-
pHmV:
Cal (S.U.):
pHmV:
Time: %/jj
kD
0(a��/
report to 0.1 S.U.
,
— 1 D``Gp?� ,
s
6Llel-
QC** pH 7 S.U.
Time: GG
Result S.U.)r:�
D
Time:
��
Result S.
Time:
Result (S.U.):
lY1
0-
re•,ort to 0.1 S.U.
J
r
Spec. Cond.
Inill:o
Cal (pmhos/cm):
Time:
1,000 mhos/cm
% Recove =
QC** Spec. Cond.
Time:
Result (umhos/cm):
Time::
Result (umhosQ/cm):
Time:
Result (umhos/cm):
O —\"
1
1,000 pmhos/cm
l
Recovery=
ORP 200 mV
Initial:
Cal: �D
Temperature4pQ,
• , O
Time:l �y�
6 l� —L
10Ts
Falyst Signature:__,Analyst Name: NN`"66 Date:
U f,
Notes:
Revision 6, 12/20/20, MAK
Zccrdance
1. Instruments shall be calib with the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. When performing DO analyses at multiple sample sites (i.e. project/facility locations), the DO probe
must be calibrated at each sample site prior to analysis.
5. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If Qc readings are out of range, the instrument needs to be recalibrated.
6. " QC check must be performed prior to sampling and following completion of sampling, at a minimum.
QC checks must be performed with calibration standard from a separate lot # as the initial QC.
7. % Recovery = (Value Obtained, pmhos/cm = True Value, pmhos/cm) x 100
8. NC Field Laboratory Certificate Number 5445
9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity.
11. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units
Temperature: SM 2550 B-2010
'C: degrees Celsius ORP: oxidation reduction potential
Specific conductivity. EPA Method 120.1, Rev. 1982
DO: dissolved oxygen s/n: serial number
DO: SM 4500 O G-2011
mg/L: milligrams per liter S.U.: standard units
pH: SM 4500-H' B-2011
mv: millivolt Spec. Cond.: Specific Conductivity
Turbidity. SM 2130 B-2011
Page 1 of 1

Appendix
Reports of Laboratory Analysis,
Chain -of -Custody Documentation,
and Certificates of Analysis

Waypointo
ANALYTICAL
3/31 /2021
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville, NC, 28801
Ref: Analytical Testing
Lab Report Number: 21-069-0019
Client Project Description: Jackson County LF
Site: 58-02
Project Number: 58-02
Dear Chuck Pippin:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/10/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a ---I
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 67

0
Waypoint.
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2021
North Carolina
State Program
402
12/31/2021
South Carolina
State Program
99012
07/31/2021
South Carolina
State Program
99012
12/31/2020
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2022
Arkansas
State Program
88-0650
02/07/2022
California
State Program
2904
06/30/2021
Florida
State Program
- NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program
- NELAP
200078
10/10/2021
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2021
Louisiana
State Program
- NELAP
LA037
12/31/2021
Louisiana
State Program
- NELAP
04015
06/30/2021
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2021
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21-A ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
09/30/2021
Virginia
State Program
00106
06/30/2021
Virginia
State Program
- NELAP
460181
09/14/2021
Page 1 of 1 00016/21-069-0019
Page 2 of 67

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 21-069-0019
Client Project Description: Jackson County LF
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
94374
MW-03-20210309
Aqueous
03/09/2021
13:48
03/10/2021
08:30
94374
MW-03-20210309
Aqueous
03/09/2021
13:48
03/10/2021
08:30
531OC-2011
WP MTN
94375
MW-04-20210309
Aqueous
03/09/2021
10:00
03/10/2021
08:30
94375
MW-04-20210309
Aqueous
03/09/2021
10:00
03/10/2021
08:30
531OC-2011
WP MTN
94376
MW-05R-20210309
Aqueous
03/09/2021
15:00
03/10/2021
08:30
94376
MW-05R-20210309
Aqueous
03/09/2021
15:00
03/10/2021
08:30
531OC-2011
WP MTN
94377
MW-07-20210309
Aqueous
03/09/2021
11:22
03/10/2021
08:30
94377
MW-07-20210309
Aqueous
03/09/2021
11:22
03/10/2021
08:30
531OC-2011
WP MTN
94378
SW-01-20210309
Aqueous
03/09/2021
12:42
03/10/2021
08:30
94379
SW-02-20210309
Aqueous
03/09/2021
13:04
03/10/2021
08:30
94380
TB-202103090000
Aqueous
03/09/2021
12:00
03/10/2021
08:30
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 67

Waypoint.(2)
ANALYTICAL
Project: Jackson County LF
Report Number: 21-069-0019
Client Sample ID Lab Sample ID
Method Parameters
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Summary of Detected
Result Units Report Limit Analyzed
MW-03-20210309
V 94374
2320B-2011
Alkalinity (as CaCO3)
140000
pq/L
800
03/19/2021
13:40
2340C-2011
Hardness
162000
Ng/L
1140
03/18/2021
11:20
4500S2F-2011
Sulfide
29700
pq/L
830
03/15/202111:30
5310C-2011
TOC
2.43
mg/L
0.567
03/13/202102:06
6020B
Arsenic
0.255
pq/L
0.170
03/15/202118:29
6020B
Barium
130
Ng/L
0.810
03/15/202118:29
6020B
Chromium
0.823
pq/L
0.790
03/15/202118:29
6020B
Cobalt
0.738
pg/L
0.520
03/15/202118:29
6020B
Nickel
0.858
pq/L
0.510
03/15/202118:29
8260D
m,p-Xylene
0.289
pg/L
0.120
03/13/202116:22
8260D
Xylene (Total)
0.289
pq/L
0.044
03/13/2021
16:22
9056A
Chloride
16800
pg/L
350
03/10/202117:11
9056A
Nitrate (NO3-N)
3590
pq/L
45.0
03/10/2021
17:11
9056A
Sulfate
3770
Ng/L
560
03/10/202117:11
MW-04-20210309
V 94375
2320B-2011
Alkalinity (as CaCO3)
80000
pq/L
800
03/19/2021
13:40
2340C-2011
Hardness
189000
Ng/L
1140
03/18/2021
11:20
4500S2F-2011
Sulfide
44800
pq/L
830
03/15/202111:30
5210B-2011
Biochemical Oxygen Demand (5-day)
2000
Ng/L
2000
03/10/2021
11:06
5310C-2011
TOC
1.60
mg/L
0.567
03/13/202103:22
6020B
Barium
68.3
Ng/L
0.810
03/15/202118:36
6020B
Cadmium
0.257
pq/L
0.160
03/15/202118:36
6020B
Cobalt
1.97
Ng/L
0.520
03/15/202118:36
6020B
Nickel
0.861
pq/L
0.510
03/15/202118:36
8260D
Benzene
0.236
Ng/L
0.048
03/13/202116:56
8260D
Chlorobenzene
1.21
pq/L
0.062
03/13/202116:56
8260D
1,4-Dichlorobenzene
1.53
Ng/L
0.050
03/13/202116:56
8260D
cis-1,2-Dichloroethene
0.494
pq/L
0.056
03/13/202116:56
8260D
SIM
1,4-Dioxane
2.16
Ng/L
0.139
03/11/2021
17:01
9056A
Chloride
33000
pq/L
350
03/10/202117:27
9056A
Nitrate (NO3-N)
3570
Ng/L
45.0
03/10/2021
17:27
9056A
Sulfate
123000
pq/L
560
03/10/202117:27
MW-05R-20210309
V 94376
2320B-2011
Alkalinity (as CaCO3)
222000
Ng/L
800
03/19/2021
13:40
2340C-2011
Hardness
162000
pq/L
1140
03/18/2021
11:20
5210B-2011
Biochemical Oxygen Demand (5-day)
12000
Ng/L
2000
03/10/2021
11:06
Qualifiers
0
I
0
Page 4 of 67

Waypoint. (2)
449 Springbrook
Rd, Charlotte, NC
28217
Main 704.529.6364
ANALYTICAL
www.waypointana lyti ca I som
Summary of Detected Analytes
Project:
Jackson County LF
Report Number: 21-069-0019
Client Sample ID Lab Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
MW-OSR-20210309
V 94376
5220D-2011
COD (Chemical Oxygen Demand)
65000
pq/L
11000
03/16/2021 11:30
5310C-2011
TOC
4.36
mg/L
0.567
03/13/202104:38
6020B
Arsenic
0.629
pq/L
0.170
03/15/202118:55
J
6020B
Barium
135
Ng/L
0.810
03/15/202118:55
6020B
Dissolved Barium
56.1
uq/L
0.810
03/13/2021 00:34
6020B
Beryllium
0.307
Ng/L
0.190
03/15/202118:55
J
6020B
Cadmium
0.218
uq/L
0.160
03/15/202118:55
J
6020B
Chromium
5.83
pg/L
0.790
03/15/202118:55
6020B
Cobalt
13.6
uq/L
0.520
03/15/202118:55
6020B
Dissolved Cobalt
8.59
pg/L
0.520
03/13/2021 00:34
6020B
Copper
11.1
pq/L
3.80
03/15/202118:55
6020B
Lead
2.34
Ng/L
0.260
03/15/202118:55
6020B
Dissolved Nickel
1.60
pq/L
0.510
03/13/2021 00:34
J
6020B
Nickel
5.92
pg/L
0.510
03/15/202118:55
6020B
Selenium
2.04
uq/L
0.740
03/15/202118:55
J
6020B
Vanadium
6.37
Ng/L
1.30
03/15/202118:55
6020B
Zinc
34.6
pq/L
6.90
03/15/202118:55
8260D
Benzene
2.27
pg/L
0.048
03/13/202117:30
8260D
Chlorobenzene
9.01
uq/L
0.062
03/13/202117:30
8260D
Chloroethane
0.481
Ng/L
0.220
03/13/202117:30
J
8260D
1,2-Dichlorobenzene
0.264
uq/L
0.076
03/13/202117:30
J
8260D
1,4-Dichlorobenzene
6.05
Ng/L
0.050
03/13/202117:30
8260D
cis-1,2-Dichloroethene
1.06
uq/L
0.056
03/13/202117:30
8260D
2-Hexanone
4.92
Ng/L
0.065
03/13/202117:30
J
8260D
Tetrahydrofuran
4.90
uq/L
1.10
03/13/202117:30
J
8260D
Toluene
0.214
Ng/L
0.044
03/13/202117:30
J
8260D
Vinyl Chloride
2.33
uq/L
0.097
03/13/2021 17:30
8260D SIM
1,4-Dioxane
2.87
Ng/L
0.139
03/11/2021 17:26
9056A
Chloride
51700
uq/L
350
03/10/202117:43
9056A
Nitrate (NO3-N)
78.0
Ng/L
45.0
03/10/2021 17:43
JB
MW-07-20210309 V 94377
2320B-2011
Alkalinity (as CaCO3)
256000
pq/L
800
03/19/2021 13:40
2340C-2011
Hardness
342000
Ng/L
1140
03/18/2021 11:20
4500S2F-2011
Sulfide
36200
uq/L
830
03/15/202111:30
5210B-2011
Biochemical Oxygen Demand (5-day)
2000
Ng/L
2000
03/10/2021 11:06
5220D-2011
COD (Chemical Oxygen Demand)
12000
pq/L
11000
03/16/2021 11:30
J
Page 5 of 67

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: Jackson County LF
Report Number: 21-069-0019
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
MW-07-20210309
V 94377
5310C-2011
TOC
6020B
Barium
6020B
Cobalt
6020B
Nickel
8260D
Benzene
8260D
Chlorobenzene
8260D
1,2-Dichlorobenzene
8260D
1,4-Dichlorobenzene
8260D
cis-1,2-Dichloroethene
8260D
Tetra hyd rofu ra n
8260D
m, p-Xylene
8260D
Xylene (Total)
8260D SIM
1,4-Dioxane
9056A
Chloride
9056A
Sulfate
SM-3500-Fe-B
Ferrous Iron
SW-01-20210309
V 94378
2340C-2011
Hardness
6020B
Barium
SW-02-20210309
V 94379
2340C-2011
Hardness
6020B
Barium
6020B
Chromium
6020B
Cobalt
6020B
Lead
6020B
Nickel
6020B
Vanadium
2.89
mg/1-
0.567
03/13/202105:16
405
Ng/L
0.810
03/15/202119:02
1.69
pq/L
0.520
03/15/202119:02
1
6.67
pq/L
0.510
03/15/202119:02
1.36
pq/L
0.048
03/13/202118:04
5.24
pq/L
0.062
03/13/202118:04
0.360
pq/L
0.076
03/13/202118:04
1
5.46
pq/L
0.050
03/13/202118:04
2.22
pq/L
0.056
03/13/202118:04
2.96
pq/L
1.10
03/13/202118:04
1
0.342
pq/L
0.120
03/13/202118:04
1
0.342
pq/L
0.044
03/13/202118:04
1
16.3
pq/L
0.139
03/11/202117:52
82500
pg/L
350
03/10/202117:58
27300
pq/L
560
03/10/2021
17:58
190
Ng/L
50.0
03/12/202112:15
1
10200
pq/L
1140
03/18/2021
11:20
13.8
Ng/L
0.810
03/13/202101:00
8500
pq/L
570
03/18/2021
11:20
22.7
Ng/L
0.810
03/13/202101:46
3.06
pq/L
0.790
03/13/202101:46
0.646
pq/L
0.520
03/13/202101:46
1
0.652
pq/L
0.260
03/13/202101:46
1
1.92
pg/L
0.510
03/13/202101:46
1
3.03
pq/L
1.30
03/13/202101:46
1
Page 6 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
REPORT OF ANAL YSIS
Lab No : 94374
Matrix: Aqueous
Sample ID: MW-03-20210309
Sampled:
3/9/2021 13:48
Ferrous Iron
<50.0
Ng/L
50.0
200
1
03/12/21 12:15
ENM
Hardness
162000
ug/L
1140
10000
1
03/18/21 11:20
SLS
1,4-Dioxane
<0.139
Ng/L
0.139
2.00
1
03/11/21 16:36
TBL
Surrogate:4-Bromofluorobenzene
107
Limits:70-130%
1 03/11/2116:36 TBL
V1584
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
140000
ug/L
800
5000
1
03/19/21 13:40
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
<2000
Ng/L
2000
2000
1
03/10/21 11:06
SLS
521OB-2011
Chloride
16800
ug/L
350
1000
1
03/10/2117:11
NMB
9056A
COD (Chemical Oxygen Demand)
<11000
Ng/L
11000
50000
1
03/16/21 11:30
SLS
5220D-2011
Nitrate (NO3-N)
3590
ug/L
45.0
200
1
03/10/21 17:11
NMB
9056A
TOC
2.43
mg/L
0.567
1.00
1
03/13/2102:06
DDB
531OC-2011
Sulfate
3770
ug/L
560
2000
1
03/10/2117:11
NMB
9056A
Sulfide
29700
Ng/L
830
2000
1
03/15/2111:30
ENM
4500S2F-2011
Antimony
<0.490
ug/L
0.490
2.00
1
03/15/2118:29
MMR
6020B
Arsenic
0.2553
Ng/L
0.170
1.00
1
03/15/2118:29
MMR
6020E
Barium
130
ug/L
0.810
10.0
1
03/15/2118:29
MMR
6020B
Beryllium
<0.190
Ng/L
0.190
1.00
1
03/15/2118:29
MMR
6020E
Cadmium
<0.160
ug/L
0.160
1.00
1
03/15/2118:29
MMR
6020B
Chromium
0.8233
Ng/L
0.790
2.00
1
03/15/2118:29
MMR
6020E
Cobalt
0.738J
ug/L
0.520
2.00
1
03/15/2118:29
MMR
6020B
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
L
Limit Exceeded
MQL Method Quantitation Limit
Page 7 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94374 Matrix: Aqueous
Sample ID: MW-03-20210309 Sampled: 3/9/2021 13:48
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Copper
<3.80
N9/L
3.80
10.0
1
03/15/2118:29
MMR
6020B
Lead
<0.260
u9/L
0.260
1.00
1
03/15/2118:29
MMR
6020B
Mercury (Total)
<0.0300
Ng/L
0.0300
0.200
1
03/16/21 13:23
EDV
7470A
Nickel
0.858J
ug/L
0.510
3.00
1
03/15/2118:29
MMR
6020B
Selenium
<0.740
Ng/L
0.740
5.00
1
03/15/2118:29
MMR
6020E
Silver
<0.110
u9/L
0.110
1.00
1
03/15/2118:29
MMR
6020B
Thallium
<0.570
Ng/L
0.570
2.00
1
03/15/2118:29
MMR
6020B
Vanadium
<1.30
u9/L
1.30
5.00
1
03/15/2118:29
MMR
6020B
Zinc
<6.90
N9/L
6.90
20.0
1
03/15/2118:29
MMR
6020B
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
MQL Method Quantitation Limit
DF Dilution Factor
L Limit Exceeded
Page 8 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
REPORT OF ANAL YSIS
Lab No : 94374 Matrix: Aqueous
Sample ID: MW-03-20210309 Sampled: 3/9/2021 13:48
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.310
Ng/L
0.310
5.00
1
03/13/21 16:22
JLB
V1702
Acrylonitrile
<0.200
pg/L
0.200
20.0
1
03/13/21 16:22
JLB
V1702
Benzene
<0.048
Ng/L
0.048
0.500
1
03/13/21 16:22
JLB
V1702
Bromochloromethane
<0.140
pg/L
0.140
0.500
1
03/13/21 16:22
JLB
V1702
Bromodichloromethane
<0.062
Ng/L
0.062
0.500
1
03/13/21 16:22
JLB
V1702
Bromoform
<0.040
ug/L
0.040
1.00
1
03/13/21 16:22
JLB
V1702
Bromomethane
<0.180
Ng/L
0.180
1.00
1
03/13/21 16:22
JLB
V1702
Carbon Disulfide
<0.075
pg/L
0.075
5.00
1
03/13/21 16:22
JLB
V1702
Carbon Tetrachloride
<0.110
Ng/L
0.110
0.500
1
03/13/21 16:22
JLB
V1702
Chlorobenzene
<0.062
pg/L
0.062
0.500
1
03/13/21 16:22
JLB
V1702
Chlorodibromomethane
<0.081
Ng/L
0.081
0.500
1
03/13/21 16:22
JLB
V1702
Chloroethane
<0.220
pg/L
0.220
0.500
1
03/13/21 16:22
JLB
V1702
Chloroform
<0.076
Ng/L
0.076
0.500
1
03/13/21 16:22
JLB
V1702
Chloromethane
<0.079
pg/L
0.079
0.500
1
03/13/21 16:22
JLB
V1702
Di -Isopropyl Ether(DIPE)
<0.960
Ng/L
0.960
5.00
1
03/13/21 16:22
JLB
V1702
1,2-Dibromo-3-Chloropropane
<0.170
pg/L
0.170
2.00
1
03/13/21 16:22
JLB
V1702
1,2-Dibromoethane
<0.051
Ng/L
0.051
0.500
1
03/13/21 16:22
JLB
V1702
Dibromomethane
<0.065
pg/L
0.065
0.500
1
03/13/21 16:22
JLB
V1702
trans-1,4-Dichloro-2-butene
<0.120
Ng/L
0.120
10.0
1
03/13/21 16:22
JLB
V1702
1,2-Dichlorobenzene
<0.076
pg/L
0.076
0.500
1
03/13/21 16:22
JLB
V1702
1,4-Dichlorobenzene
<0.050
Ng/L
0.050
0.500
1
03/13/21 16:22
JLB
V1702
Dichlorodifluoromethane
<0.110
pg/L
0.110
5.00
1
03/13/21 16:22
JLB
V1702
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 9 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
REPORT OF ANAL YSIS
Lab No : 94374 Matrix: Aqueous
Sample ID: MW-03-20210309 Sampled: 3/9/2021 13:48
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,1-Dichloroethane
<0.083
N9/L
0.083
0.500
1
03/13/21 16:22
JLB
V1702
1,2-Dichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 16:22
JLB
V1702
1,1-Dichloroethene
<0.083
N9/L
0.083
0.500
1
03/13/21 16:22
JLB
V1702
cis- 1,2-Dich loroethene
<0.056
u9/L
0.056
0.500
1
03/13/21 16:22
JLB
V1702
trans-1,2-Dichloroethene
<0.094
N9/L
0.094
0.500
1
03/13/21 16:22
JLB
V1702
1,2-Dichloropropane
<0.110
u9/L
0.110
0.500
1
03/13/21 16:22
JLB
V1702
cis- 1,3-Dich loropropene
<0.079
N9/L
0.079
0.500
1
03/13/21 16:22
JLB
V1702
trans-1,3-Dichloropropene
<0.070
u9/L
0.070
0.500
1
03/13/21 16:22
JLB
V1702
1,4-Dioxane
<14.0
N9/L
14.0
150
1
03/13/21 16:22
JLB
V1702
Ethylbenzene
<0.061
u9/L
0.061
0.500
1
03/13/21 16:22
JLB
V1702
2-Hexanone
<0.065
N9/L
0.065
5.00
1
03/13/21 16:22
JLB
V1702
Methyl Ethyl Ketone (MEK)
<0.240
ug/L
0.240
5.00
1
03/13/21 16:22
JLB
V1702
4-Methyl-2-Pentanone
<1.00
N9/L
1.00
5.00
1
03/13/21 16:22
JLB
V1702
Methylene Chloride
<0.083
ug/L
0.083
1.00
1
03/13/21 16:22
JLB
V1702
Styrene
<0.047
N9/L
0.047
0.500
1
03/13/21 16:22
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.110
pg/L
0.110
0.500
1
03/13/21 16:22
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.036
N9/L
0.036
0.500
1
03/13/21 16:22
JLB
V1702
Tetrachloroethene
<0.098
pg/L
0.098
0.500
1
03/13/21 16:22
JLB
V1702
Tetrahydrofuran
<1.10
N9/L
1.10
10.0
1
03/13/21 16:22
JLB
V1702
Toluene
<0.044
u9/L
0.044
0.500
1
03/13/21 16:22
JLB
V1702
1,1,1-Trichloroethane
<0.061
N9/L
0.061
0.500
1
03/13/21 16:22
JLB
V1702
1,1,2-Trichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 16:22
JLB
V1702
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 10 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94374 Matrix: Aqueous
Sample ID: MW-03-20210309 Sampled: 3/9/2021 13:48
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Trichloroethene
<0.078
Ng/L
0.078 0.500
1
03/13/21 16:22 JLB
V1702
Trichlorofluoromethane
<0.062
ug/L
0.062 0.500
1
03/13/21 16:22 JLB
V1702
1,2,3-Trichloropropane
<0.140
Ng/L
0.140 1.00
1
03/13/21 16:22 JLB
V1702
Vinyl Acetate
<0.060
ug/L
0.060 2.00
1
03/13/21 16:22 JLB
V1702
Vinyl Chloride
<0.097
Ng/L
0.097 0.500
1
03/13/21 16:22 JLB
V1702
o-Xylene
<0.044
ug/L
0.044 0.500
1
03/13/21 16:22 JLB
V1702
m,p-Xylene
0.2893
Ng/L
0.120 1.00
1
03/13/21 16:22 JLB
V1702
Xylene (Total)
0.2893
ug/L
0.044 0.500
1
03/13/21 16:22
V1702
Surrogate:4-Bromofluorobenzene
95.6
Limits:80-124%
1 03/13/21 16:22 JLB
V1702
Surrogate: Dibromofluoromethane
114
Limits: 75-129%
1 03/13/21 16:22 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
111
Limits: 63-136%
1 03/13/21 16:22 JLB
V1702
Surrogate: Toluene-d8
100
Limits: 77-123%
1 03/13/21 16:22 JLB
V1702
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 11 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
REPORT OF ANAL YSIS
Lab No : 94375
Matrix: Aqueous
Sample ID: MW-04-20210309
Sampled:
3/9/2021 10:00
Ferrous Iron
<50.0
Ng/L
50.0
200
1
03/12/21 12:15
ENM
Hardness
189000
u9/L
1140
10000
1
03/18/21 11:20
SLS
1,4-Dioxane
2.16
Ng/L
0.139
2.00
1
03/11/21 17:01
TBL
Surrogate:4-Bromofluorobenzene
99.2
Limits:70-130%
1 03/11/2117:01 TBL
V1584
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
80000
u9/L
800
5000
1
03/19/21 13:40
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
2000
Ng/L
2000
2000
1
03/10/21 11:06
SLS
521OB-2011
Chloride
33000
u9/L
350
1000
1
03/10/2117:27
NMB
9056A
COD (Chemical Oxygen Demand)
<11000
Ng/L
11000
50000
1
03/16/21 11:30
SLS
5220D-2011
Nitrate (NO3-N)
3570
u9/L
45.0
200
1
03/10/21 17:27
NMB
9056A
TOC
1.60
mg/L
0.567
1.00
1
03/13/2103:22
DDB
531OC-2011
Sulfate
123000
u9/L
560
2000
1
03/10/2117:27
NMB
9056A
Sulfide
44800
Ng/L
830
2000
1
03/15/2111:30
ENM
4500S2F-2011
Antimony
<0.490
u9/L
0.490
2.00
1
03/15/2118:36
MMR
6020B
Arsenic
<0.170
Ng/L
0.170
1.00
1
03/15/2118:36
MMR
6020E
Barium
68.3
u9/L
0.810
10.0
1
03/15/2118:36
MMR
6020B
Beryllium
<0.190
Ng/L
0.190
1.00
1
03/15/2118:36
MMR
6020E
Cadmium
0.2571
u9/L
0.160
1.00
1
03/15/2118:36
MMR
6020B
Chromium
<0.790
Ng/L
0.790
2.00
1
03/15/2118:36
MMR
6020E
Cobalt
1.97J
u9/L
0.520
2.00
1
03/15/2118:36
MMR
6020B
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
L
Limit Exceeded
MQL Method Quantitation Limit
Page 12 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94375 Matrix: Aqueous
Sample ID: MW-04-20210309 Sampled: 3/9/2021 10:00
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Copper
<3.80
N9/L
3.80
10.0
1
03/15/2118:36
MMR
6020B
Lead
<0.260
u9/L
0.260
1.00
1
03/15/2118:36
MMR
6020B
Mercury (Total)
<0.0300
N9/L
0.0300
0.200
1
03/16/21 13:42
EDV
7470A
Nickel
0.861 J
ug/L
0.510
3.00
1
03/15/21 18:36
MMR
6020B
Selenium
<0.740
N9/L
0.740
5.00
1
03/15/2118:36
MMR
6020E
Silver
<0.110
u9/L
0.110
1.00
1
03/15/2118:36
MMR
6020B
Thallium
<0.570
N9/L
0.570
2.00
1
03/15/2118:36
MMR
6020B
Vanadium
<1.30
u9/L
1.30
5.00
1
03/15/2118:36
MMR
6020B
Zinc
<6.90
N9/L
6.90
20.0
1
03/15/2118:36
MMR
6020B
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
MQL Method Quantitation Limit
DF Dilution Factor
L Limit Exceeded
Page 13 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
REPORT OF ANAL YSIS
Lab No : 94375 Matrix: Aqueous
Sample ID: MW-04-20210309 Sampled: 3/9/2021 10:00
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Acetone
<0.310
Ng/L
0.310
5.00
1
03/13/21 16:56
JLB
V1702
Acrylonitrile
<0.200
ug/L
0.200
20.0
1
03/13/21 16:56
JLB
V1702
Benzene
0.2363
Ng/L
0.048
0.500
1
03/13/21 16:56
JLB
V1702
Bromochloromethane
<0.140
ug/L
0.140
0.500
1
03/13/21 16:56
JLB
V1702
Bromodichloromethane
<0.062
Ng/L
0.062
0.500
1
03/13/21 16:56
JLB
V1702
Bromoform
<0.040
ug/L
0.040
1.00
1
03/13/21 16:56
JLB
V1702
Bromomethane
<0.180
Ng/L
0.180
1.00
1
03/13/21 16:56
JLB
V1702
Carbon Disulfide
<0.075
ug/L
0.075
5.00
1
03/13/21 16:56
JLB
V1702
Carbon Tetrachloride
<0.110
Ng/L
0.110
0.500
1
03/13/21 16:56
JLB
V1702
Chlorobenzene
1.21
ug/L
0.062
0.500
1
03/13/21 16:56
JLB
V1702
Chlorodibromomethane
<0.081
Ng/L
0.081
0.500
1
03/13/21 16:56
JLB
V1702
Chloroethane
<0.220
ug/L
0.220
0.500
1
03/13/21 16:56
JLB
V1702
Chloroform
<0.076
Ng/L
0.076
0.500
1
03/13/21 16:56
JLB
V1702
Chloromethane
<0.079
ug/L
0.079
0.500
1
03/13/21 16:56
JLB
V1702
Di -Isopropyl Ether(DIPE)
<0.960
Ng/L
0.960
5.00
1
03/13/21 16:56
JLB
V1702
1,2-Dibromo-3-Chloropropane
<0.170
ug/L
0.170
2.00
1
03/13/21 16:56
JLB
V1702
1,2-Dibromoethane
<0.051
Ng/L
0.051
0.500
1
03/13/21 16:56
JLB
V1702
Dibromomethane
<0.065
pg/L
0.065
0.500
1
03/13/21 16:56
JLB
V1702
trans-1,4-Dichloro-2-butene
<0.120
Ng/L
0.120
10.0
1
03/13/21 16:56
JLB
V1702
1,2-Dichlorobenzene
<0.076
pg/L
0.076
0.500
1
03/13/21 16:56
JLB
V1702
1,4-Dichlorobenzene
1.53
Ng/L
0.050
0.500
1
03/13/21 16:56
JLB
V1702
Dichlorodifluoromethane
<0.110
pg/L
0.110
5.00
1
03/13/21 16:56
JLB
V1702
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 14 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
REPORT OF ANAL YSIS
Lab No : 94375 Matrix: Aqueous
Sample ID: MW-04-20210309 Sampled: 3/9/2021 10:00
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,1-Dichloroethane
<0.083
N9/L
0.083
0.500
1
03/13/21 16:56
JLB
V1702
1,2-Dichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 16:56
JLB
V1702
1,1-Dichloroethene
<0.083
N9/L
0.083
0.500
1
03/13/21 16:56
JLB
V1702
cis- 1,2-Dich loroethene
0.494J
u9/L
0.056
0.500
1
03/13/21 16:56
JLB
V1702
trans-1,2-Dichloroethene
<0.094
N9/L
0.094
0.500
1
03/13/21 16:56
JLB
V1702
1,2-Dichloropropane
<0.110
u9/L
0.110
0.500
1
03/13/21 16:56
JLB
V1702
cis- 1,3-Dich loropropene
<0.079
N9/L
0.079
0.500
1
03/13/21 16:56
JLB
V1702
trans-1,3-Dichloropropene
<0.070
u9/L
0.070
0.500
1
03/13/21 16:56
JLB
V1702
1,4-Dioxane
<14.0
N9/L
14.0
150
1
03/13/21 16:56
JLB
V1702
Ethylbenzene
<0.061
u9/L
0.061
0.500
1
03/13/21 16:56
JLB
V1702
2-Hexanone
<0.065
N9/L
0.065
5.00
1
03/13/21 16:56
JLB
V1702
Methyl Ethyl Ketone (MEK)
<0.240
ug/L
0.240
5.00
1
03/13/21 16:56
JLB
V1702
4-Methyl-2-Pentanone
<1.00
N9/L
1.00
5.00
1
03/13/21 16:56
JLB
V1702
Methylene Chloride
<0.083
ug/L
0.083
1.00
1
03/13/21 16:56
JLB
V1702
Styrene
<0.047
N9/L
0.047
0.500
1
03/13/21 16:56
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.110
pg/L
0.110
0.500
1
03/13/21 16:56
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.036
N9/L
0.036
0.500
1
03/13/21 16:56
JLB
V1702
Tetrachloroethene
<0.098
pg/L
0.098
0.500
1
03/13/21 16:56
JLB
V1702
Tetrahydrofuran
<1.10
N9/L
1.10
10.0
1
03/13/21 16:56
JLB
V1702
Toluene
<0.044
u9/L
0.044
0.500
1
03/13/21 16:56
JLB
V1702
1,1,1-Trichloroethane
<0.061
N9/L
0.061
0.500
1
03/13/21 16:56
JLB
V1702
1,1,2-Trichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 16:56
JLB
V1702
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 15 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94375 Matrix: Aqueous
Sample ID: MW-04-20210309 Sampled: 3/9/2021 10:00
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Trichloroethene
<0.078
Ng/L
0.078 0.500
1
03/13/21 16:56 JLB
V1702
Trichlorofluoromethane
<0.062
ug/L
0.062 0.500
1
03/13/21 16:56 JLB
V1702
1,2,3-Trichloropropane
<0.140
Ng/L
0.140 1.00
1
03/13/21 16:56 JLB
V1702
Vinyl Acetate
<0.060
ug/L
0.060 2.00
1
03/13/21 16:56 JLB
V1702
Vinyl Chloride
<0.097
Ng/L
0.097 0.500
1
03/13/21 16:56 JLB
V1702
o-Xylene
<0.044
ug/L
0.044 0.500
1
03/13/21 16:56 JLB
V1702
m,p-Xylene
<0.120
Ng/L
0.120 1.00
1
03/13/21 16:56 JLB
V1702
Xylene (Total)
<0.044
ug/L
0.044 0.500
1
03/13/21 16:56
V1702
Surrogate:4-Bromofluorobenzene
95.4
Limits:80-124%
1 03/13/21 16:56 JLB
V1702
Surrogate: Dibromofluoromethane
110
Limits: 75-129%
1 03/13/21 16:56 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
106
Limits: 63-136%
1 03/13/21 16:56 JLB
V1702
Surrogate: Toluene-d8
97.2
Limits: 77-123%
1 03/13/21 16:56 JLB
V1702
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 16 of 67

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-069-0019
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County LF
Information :
REPORT OF ANAL YSIS
Report Date : 03/31/2021
Received : 03/10/2021
Lab No : 94376
Matrix: Aqueous
Sample ID: MW-05R-20210309
Sampled:
3/9/2021 15:00
Ferrous Iron
<50.0
Ng/L
50.0
200
1
03/12/21 12:15
ENM
Hardness
162000
ug/L
1140
10000
1
03/18/21 11:20
SLS
1,4-Dioxane
2.87
Ng/L
0.139
2.00
1
03/11/21 17:26
TBL
Surrogate:4-Bromofluorobenzene
94.4
Limits:70-130%
1 03/11/2117:26 TBL
V1584
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
222000
ug/L
800
5000
1
03/19/21 13:40
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
12000
Ng/L
2000
2000
1
03/10/21 11:06
SLS
521OB-2011
Chloride
51700
ug/L
350
1000
1
03/10/2117:43
NMB
9056A
COD (Chemical Oxygen Demand)
65000
Ng/L
11000
50000
1
03/16/21 11:30
SLS
5220D-2011
Nitrate (NO3-N)
78.OJB
ug/L
45.0
200
1
03/10/21 17:43
NMB
9056A
TOC
4.36
mg/L
0.567
1.00
1
03/13/2104:38
DDB
531OC-2011
Sulfate
<560
ug/L
560
2000
1
03/10/2117:43
NMB
9056A
Sulfide
<830
Ng/L
830
2000
1
03/15/2111:30
ENM
4500S2F-2011
Antimony
<0.490
ug/L
0.490
2.00
1
03/15/2118:55
MMR
6020B
Dissolved Antimony
<0.490
Ng/L
0.490
2.00
1
03/13/21 00:34
MMR
6020E
Arsenic
0.629J
ug/L
0.170
1.00
1
03/15/2118:55
MMR
6020B
Dissolved Arsenic
<0.170
Ng/L
0.170
1.00
1
03/13/21 00:34
MMR
6020E
Barium
135
ug/L
0.810
10.0
1
03/15/2118:55
MMR
6020B
Dissolved Barium
56.1
Ng/L
0.810
10.0
1
03/13/21 00:34
MMR
6020E
Beryllium
0.3073
ug/L
0.190
1.00
1
03/15/2118:55
MMR
6020B
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
L
Limit Exceeded
MQL Method Quantitation Limit
Page 17 of 67

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County LF
Information :
Report Date : 03/31/2021
Received : 03/10/2021
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94376 Matrix: Aqueous
Sample ID: MW-05R-20210309 Sampled: 3/9/2021 15:00
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Dissolved Beryllium
<0.190
Ng/L
0.190
1.00
1
03/13/21 00:34
MMR
6020E
Cadmium
0.218J
ug/L
0.160
1.00
1
03/15/2118:55
MMR
6020B
Dissolved Cadmium
<0.160
Ng/L
0.160
1.00
1
03/13/21 00:34
MMR
6020E
Chromium
5.83
ug/L
0.790
2.00
1
03/15/2118:55
MMR
6020B
Dissolved Chromium
<0.790
Ng/L
0.790
2.00
1
03/13/21 00:34
MMR
6020E
Cobalt
13.6
ug/L
0.520
2.00
1
03/15/2118:55
MMR
6020B
Dissolved Cobalt
8.59
Ng/L
0.520
2.00
1
03/13/21 00:34
MMR
6020E
Copper
11.1
u9/L
3.80
10.0
1
03/15/2118:55
MMR
6020B
Dissolved Copper
<3.80
Ng/L
3.80
10.0
1
03/13/21 00:34
MMR
6020B
Lead
2.34
ug/L
0.260
1.00
1
03/15/2118:55
MMR
6020B
Dissolved Lead
<0.260
Ng/L
0.260
1.00
1
03/13/21 00:34
MMR
6020E
Mercury (Total)
<0.0300
ug/L
0.0300
0.200
1
03/16/21 13:46
EDV
7470A
Dissolved Mercury
<0.0300
Ng/L
0.0300
0.200
1
03/15/21 15:11
EDV
7470A
Dissolved Nickel
1.60J
ug/L
0.510
3.00
1
03/13/21 00:34
MMR
6020B
Nickel
5.92
Ng/L
0.510
3.00
1
03/15/2118:55
MMR
6020E
Selenium
2.04J
ug/L
0.740
5.00
1
03/15/2118:55
MMR
6020B
Dissolved Selenium
<0.740
Ng/L
0.740
5.00
1
03/13/21 00:34
MMR
6020E
Silver
<0.110
ug/L
0.110
1.00
1
03/15/2118:55
MMR
6020B
Dissolved Silver
<0.110
Ng/L
0.110
1.00
1
03/13/21 00:34
MMR
6020E
Thallium
<0.570
ug/L
0.570
2.00
1
03/15/2118:55
MMR
6020B
Dissolved Thallium
<0.570
Ng/L
0.570
2.00
1
03/13/21 00:34
MMR
6020E
Vanadium
6.37
ug/L
1.30
5.00
1
03/15/2118:55
MMR
6020B
Dissolved Vanadium
<1.30
Ng/L
1.30
5.00
1
03/13/21 00:34
MMR
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
L
Limit Exceeded
MQL
Method Quantitation Limit
Page 18 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94376 Matrix: Aqueous
Sample ID: MW-05R-20210309 Sampled: 3/9/2021 15:00
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Zinc 34.6 Ng/L 6.90 20.0
Dissolved Zinc <6.90 ug/L 6.90 20.0
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
MQL Method Quantitation Limit
1 03/15/2118:55 MMR 6020E
1 03/13/2100:34 MMR 6020B
DF Dilution Factor
L Limit Exceeded
Page 19 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94376
Matrix: Aqueous
Sample ID: MW-05R-20210309
Sampled:
3/9/2021 15:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.310
N9/L
0.310
5.00
1
03/13/21 17:30
JLB
V1702
Acrylonitrile
<0.200
u9/L
0.200
20.0
1
03/13/21 17:30
JLB
V1702
Benzene
2.27
N9/L
0.048
0.500
1
03/13/21 17:30
JLB
V1702
Bromochloromethane
<0.140
u9/L
0.140
0.500
1
03/13/21 17:30
JLB
V1702
Bromodichloromethane
<0.062
N9/L
0.062
0.500
1
03/13/21 17:30
JLB
V1702
Bromoform
<0.040
u9/L
0.040
1.00
1
03/13/21 17:30
JLB
V1702
Bromomethane
<0.180
N9/L
0.180
1.00
1
03/13/21 17:30
JLB
V1702
Carbon Disulfide
<0.075
u9/L
0.075
5.00
1
03/13/21 17:30
JLB
V1702
Carbon Tetrachloride
<0.110
N9/L
0.110
0.500
1
03/13/21 17:30
JLB
V1702
Chlorobenzene
9.01
u9/L
0.062
0.500
1
03/13/21 17:30
JLB
V1702
Chlorodibromomethane
<0.081
N9/L
0.081
0.500
1
03/13/21 17:30
JLB
V1702
Chloroethane
0.4813
u9/L
0.220
0.500
1
03/13/21 17:30
JLB
V1702
Chloroform
<0.076
N9/L
0.076
0.500
1
03/13/21 17:30
JLB
V1702
Chloromethane
<0.079
ug/L
0.079
0.500
1
03/13/21 17:30
JLB
V1702
Di -Isopropyl Ether(DIPE)
<0.960
N9/L
0.960
5.00
1
03/13/21 17:30
JLB
V1702
1,2-Dibromo-3-Chloropropane
<0.170
ug/L
0.170
2.00
1
03/13/21 17:30
JLB
V1702
1,2-Dibromoethane
<0.051
N9/L
0.051
0.500
1
03/13/21 17:30
JLB
V1702
Dibromomethane
<0.065
pg/L
0.065
0.500
1
03/13/21 17:30
JLB
V1702
trans-1,4-Dichloro-2-butene
<0.120
N9/L
0.120
10.0
1
03/13/21 17:30
JLB
V1702
1,2-Dichlorobenzene
0.2643
pg/L
0.076
0.500
1
03/13/21 17:30
JLB
V1702
1,4-Dichlorobenzene
6.05
N9/L
0.050
0.500
1
03/13/21 17:30
JLB
V1702
Dichlorodifluoromethane
<0.110
pg/L
0.110
5.00
1
03/13/21 17:30
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 20 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94376
Matrix: Aqueous
Sample ID: MW-05R-20210309
Sampled:
3/9/2021 15:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,1-Dichloroethane
<0.083
N9/L
0.083
0.500
1
03/13/21 17:30
JLB
V1702
1,2-Dichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 17:30
JLB
V1702
1,1-Dichloroethene
<0.083
N9/L
0.083
0.500
1
03/13/21 17:30
JLB
V1702
cis- 1,2-Dich loroethene
1.06
u9/L
0.056
0.500
1
03/13/21 17:30
JLB
V1702
trans-1,2-Dichloroethene
<0.094
N9/L
0.094
0.500
1
03/13/21 17:30
JLB
V1702
1,2-Dichloropropane
<0.110
u9/L
0.110
0.500
1
03/13/21 17:30
JLB
V1702
cis- 1,3-Dich loropropene
<0.079
N9/L
0.079
0.500
1
03/13/21 17:30
JLB
V1702
trans-1,3-Dichloropropene
<0.070
u9/L
0.070
0.500
1
03/13/21 17:30
JLB
V1702
1,4-Dioxane
<14.0
N9/L
14.0
150
1
03/13/21 17:30
JLB
V1702
Ethylbenzene
<0.061
u9/L
0.061
0.500
1
03/13/21 17:30
JLB
V1702
2-Hexanone
4.923
N9/L
0.065
5.00
1
03/13/21 17:30
JLB
V1702
Methyl Ethyl Ketone (MEK)
<0.240
u9/L
0.240
5.00
1
03/13/21 17:30
JLB
V1702
4-Methyl-2-Pentanone
<1.00
N9/L
1.00
5.00
1
03/13/21 17:30
JLB
V1702
Methylene Chloride
<0.083
ug/L
0.083
1.00
1
03/13/21 17:30
JLB
V1702
Styrene
<0.047
N9/L
0.047
0.500
1
03/13/21 17:30
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.110
ug/L
0.110
0.500
1
03/13/21 17:30
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.036
N9/L
0.036
0.500
1
03/13/21 17:30
JLB
V1702
Tetrachloroethene
<0.098
pg/L
0.098
0.500
1
03/13/21 17:30
JLB
V1702
Tetrahydrofuran
4.903
N9/L
1.10
10.0
1
03/13/21 17:30
JLB
V1702
Toluene
0.2143
u9/L
0.044
0.500
1
03/13/21 17:30
JLB
V1702
1,1,1-Trichloroethane
<0.061
N9/L
0.061
0.500
1
03/13/21 17:30
JLB
V1702
1,1,2-Trichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 17:30
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 21 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
Lab No : 94376
Sample ID: MW-05R-20210309
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 3/9/2021 15:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Trichloroethene
<0.078
Ng/L
0.078
0.500
1
03/13/21 17:30 JLB
V1702
Trichlorofluoromethane
<0.062
ug/L
0.062
0.500
1
03/13/21 17:30 JLB
V1702
1,2,3-Trichloropropane
<0.140
Ng/L
0.140
1.00
1
03/13/21 17:30 JLB
V1702
Vinyl Acetate
<0.060
ug/L
0.060
2.00
1
03/13/21 17:30 JLB
V1702
Vinyl Chloride
2.33
Ng/L
0.097
0.500
1
03/13/21 17:30 JLB
V1702
o-Xylene
<0.044
ug/L
0.044
0.500
1
03/13/21 17:30 JLB
V1702
m,p-Xylene
<0.120
Ng/L
0.120
1.00
1
03/13/21 17:30 JLB
V1702
Xylene (Total)
<0.044
ug/L
0.044
0.500
1
03/13/21 17:30
V1702
Surrogate:4-Bromofluorobenzene
96.0
Limits:80-124%
1 03/13/21 17:30 JLB
V1702
Surrogate: Dibromofluoromethane
108
Limits:
75-129%
1 03/13/21 17:30 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
105
Limits:
63-136%
1 03/13/21 17:30 JLB
V1702
Surrogate: Toluene-d8
98.8
Limits:
77-123%
1 03/13/21 17:30 JLB
V1702
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 22 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
REPORT OF ANAL YSIS
Lab No : 94377
Matrix: Aqueous
Sample ID: MW-07-20210309
Sampled:
3/9/2021 11:22
Ferrous Iron
1903
Ng/L
50.0
200
1
03/12/21 12:15
ENM
Hardness
342000
ug/L
1140
10000
1
03/18/21 11:20
SLS
1,4-Dioxane
16.3
Ng/L
0.139
2.00
1
03/11/21 17:52
TBL
Surrogate:4-Bromofluorobenzene
106
Limits:70-130%
1 03/11/2117:52 TBL
V1584
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
256000
ug/L
800
5000
1
03/19/21 13:40
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
2000
Ng/L
2000
2000
1
03/10/21 11:06
SLS
521OB-2011
Chloride
82500
ug/L
350
1000
1
03/10/2117:58
NMB
9056A
COD (Chemical Oxygen Demand)
120003
Ng/L
11000
50000
1
03/16/21 11:30
SLS
5220D-2011
Nitrate (NO3-N)
<45.0
ug/L
45.0
200
1
03/10/21 17:58
NMB
9056A
TOC
2.89
mg/L
0.567
1.00
1
03/13/2105:16
DDB
531OC-2011
Sulfate
27300
ug/L
560
2000
1
03/10/2117:58
NMB
9056A
Sulfide
36200
Ng/L
830
2000
1
03/15/2111:30
ENM
4500S2F-2011
Antimony
<0.490
ug/L
0.490
2.00
1
03/15/2119:02
MMR
6020B
Arsenic
<0.170
Ng/L
0.170
1.00
1
03/15/2119:02
MMR
6020E
Barium
405
ug/L
0.810
10.0
1
03/15/2119:02
MMR
6020B
Beryllium
<0.190
Ng/L
0.190
1.00
1
03/15/2119:02
MMR
6020E
Cadmium
<0.160
ug/L
0.160
1.00
1
03/15/2119:02
MMR
6020B
Chromium
<0.790
Ng/L
0.790
2.00
1
03/15/2119:02
MMR
6020E
Cobalt
1.69J
ug/L
0.520
2.00
1
03/15/2119:02
MMR
6020B
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
L
Limit Exceeded
MQL Method Quantitation Limit
Page 23 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94377 Matrix: Aqueous
Sample ID: MW-07-20210309 Sampled: 3/9/2021 11:22
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Copper
<3.80
N9/L
3.80
10.0
1
03/15/2119:02
MMR
6020B
Lead
<0.260
u9/L
0.260
1.00
1
03/15/2119:02
MMR
6020B
Mercury (Total)
<0.0300
Ng/L
0.0300
0.200
1
03/16/21 13:58
EDV
7470A
Nickel
6.67
u9/L
0.510
3.00
1
03/15/2119:02
MMR
6020B
Selenium
<0.740
Ng/L
0.740
5.00
1
03/15/2119:02
MMR
6020E
Silver
<0.110
u9/L
0.110
1.00
1
03/15/2119:02
MMR
6020B
Thallium
<0.570
Ng/L
0.570
2.00
1
03/15/2119:02
MMR
6020B
Vanadium
<1.30
u9/L
1.30
5.00
1
03/15/2119:02
MMR
6020B
Zinc
<6.90
N9/L
6.90
20.0
1
03/15/2119:02
MMR
6020B
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
MQL Method Quantitation Limit
DF Dilution Factor
L Limit Exceeded
Page 24 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94377
Matrix: Aqueous
Sample ID: MW-07-20210309
Sampled:
3/9/2021 11:22
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.310
N9/L
0.310
5.00
1
03/13/21 18:04
JLB
V1702
Acrylonitrile
<0.200
u9/L
0.200
20.0
1
03/13/21 18:04
JLB
V1702
Benzene
1.36
N9/L
0.048
0.500
1
03/13/21 18:04
JLB
V1702
Bromochloromethane
<0.140
u9/L
0.140
0.500
1
03/13/21 18:04
JLB
V1702
Bromodichloromethane
<0.062
N9/L
0.062
0.500
1
03/13/21 18:04
JLB
V1702
Bromoform
<0.040
u9/L
0.040
1.00
1
03/13/21 18:04
JLB
V1702
Bromomethane
<0.180
N9/L
0.180
1.00
1
03/13/21 18:04
JLB
V1702
Carbon Disulfide
<0.075
u9/L
0.075
5.00
1
03/13/21 18:04
JLB
V1702
Carbon Tetrachloride
<0.110
N9/L
0.110
0.500
1
03/13/21 18:04
JLB
V1702
Chlorobenzene
5.24
u9/L
0.062
0.500
1
03/13/21 18:04
JLB
V1702
Chlorodibromomethane
<0.081
N9/L
0.081
0.500
1
03/13/21 18:04
JLB
V1702
Chloroethane
<0.220
u9/L
0.220
0.500
1
03/13/21 18:04
JLB
V1702
Chloroform
<0.076
N9/L
0.076
0.500
1
03/13/21 18:04
JLB
V1702
Chloromethane
<0.079
ug/L
0.079
0.500
1
03/13/21 18:04
JLB
V1702
Di -Isopropyl Ether(DIPE)
<0.960
N9/L
0.960
5.00
1
03/13/21 18:04
JLB
V1702
1,2-Dibromo-3-Chloropropane
<0.170
ug/L
0.170
2.00
1
03/13/21 18:04
JLB
V1702
1,2-Dibromoethane
<0.051
N9/L
0.051
0.500
1
03/13/21 18:04
JLB
V1702
Dibromomethane
<0.065
pg/L
0.065
0.500
1
03/13/21 18:04
JLB
V1702
trans-1,4-Dichloro-2-butene
<0.120
N9/L
0.120
10.0
1
03/13/21 18:04
JLB
V1702
1,2-Dichlorobenzene
0.3603
pg/L
0.076
0.500
1
03/13/21 18:04
JLB
V1702
1,4-Dichlorobenzene
5.46
N9/L
0.050
0.500
1
03/13/21 18:04
JLB
V1702
Dichlorodifluoromethane
<0.110
pg/L
0.110
5.00
1
03/13/21 18:04
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 25 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94377
Matrix: Aqueous
Sample ID: MW-07-20210309
Sampled:
3/9/2021 11:22
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,1-Dichloroethane
<0.083
N9/L
0.083
0.500
1
03/13/21 18:04
JLB
V1702
1,2-Dichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 18:04
JLB
V1702
1,1-Dichloroethene
<0.083
N9/L
0.083
0.500
1
03/13/21 18:04
JLB
V1702
cis- 1,2-Dich loroethene
2.22
u9/L
0.056
0.500
1
03/13/21 18:04
JLB
V1702
trans-1,2-Dichloroethene
<0.094
N9/L
0.094
0.500
1
03/13/21 18:04
JLB
V1702
1,2-Dichloropropane
<0.110
u9/L
0.110
0.500
1
03/13/21 18:04
JLB
V1702
cis- 1,3-Dich loropropene
<0.079
N9/L
0.079
0.500
1
03/13/21 18:04
JLB
V1702
trans-1,3-Dichloropropene
<0.070
u9/L
0.070
0.500
1
03/13/21 18:04
JLB
V1702
1,4-Dioxane
<14.0
N9/L
14.0
150
1
03/13/21 18:04
JLB
V1702
Ethylbenzene
<0.061
u9/L
0.061
0.500
1
03/13/21 18:04
JLB
V1702
2-Hexanone
<0.065
N9/L
0.065
5.00
1
03/13/21 18:04
JLB
V1702
Methyl Ethyl Ketone (MEK)
<0.240
ug/L
0.240
5.00
1
03/13/21 18:04
JLB
V1702
4-Methyl-2-Pentanone
<1.00
N9/L
1.00
5.00
1
03/13/21 18:04
JLB
V1702
Methylene Chloride
<0.083
ug/L
0.083
1.00
1
03/13/21 18:04
JLB
V1702
Styrene
<0.047
N9/L
0.047
0.500
1
03/13/21 18:04
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.110
pg/L
0.110
0.500
1
03/13/21 18:04
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.036
N9/L
0.036
0.500
1
03/13/21 18:04
JLB
V1702
Tetrachloroethene
<0.098
pg/L
0.098
0.500
1
03/13/21 18:04
JLB
V1702
Tetrahydrofuran
2.963
N9/L
1.10
10.0
1
03/13/21 18:04
JLB
V1702
Toluene
<0.044
u9/L
0.044
0.500
1
03/13/21 18:04
JLB
V1702
1,1,1-Trichloroethane
<0.061
N9/L
0.061
0.500
1
03/13/21 18:04
JLB
V1702
1,1,2-Trichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 18:04
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 26 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
Lab No : 94377
Sample ID: MW-07-20210309
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 3/9/2021 11:22
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Trichloroethene
<0.078
Ng/L
0.078
0.500
1
03/13/21 18:04 JLB
V1702
Trichlorofluoromethane
<0.062
ug/L
0.062
0.500
1
03/13/21 18:04 JLB
V1702
1,2,3-Trichloropropane
<0.140
Ng/L
0.140
1.00
1
03/13/21 18:04 JLB
V1702
Vinyl Acetate
<0.060
ug/L
0.060
2.00
1
03/13/21 18:04 JLB
V1702
Vinyl Chloride
<0.097
Ng/L
0.097
0.500
1
03/13/21 18:04 JLB
V1702
o-Xylene
<0.044
ug/L
0.044
0.500
1
03/13/21 18:04 JLB
V1702
m,p-Xylene
0.3423
Ng/L
0.120
1.00
1
03/13/21 18:04 JLB
V1702
Xylene (Total)
0.3423
ug/L
0.044
0.500
1
03/13/21 18:04
V1702
Surrogate:4-Bromofluorobenzene
95.2
Limits:80-124%
1 03/13/21 18:04 JLB
V1702
Surrogate: Dibromofluoromethane
106
Limits:
75-129%
1 03/13/21 18:04 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
104
Limits:
63-136%
1 03/13/21 18:04 JLB
V1702
Surrogate: Toluene-d8
101
Limits:
77-123%
1 03/13/21 18:04 JLB
V1702
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 27 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94378 Matrix: Aqueous
Sample ID: SW-01-20210309 Sampled: 3/9/2021 12:42
Hardness 10200 Ng/L
1,4-Dioxane <0.139 ug/L
Surrogate: 4-Bromofluorobenzene 111
Test Results Units
1140 10000
1 03/18/21 11:20 SLS
0.139 2.00
1 03/11/21 18:17 TBL
Limits:70-130%
1 03/11/2118:17 TBL V1584
MDL MQL
DF Date / Time By Analytical
Analyzed Method
Antimony
<0.490
Ng/L
0.490
2.00
1
03/13/2101:00
MMR
6020E
Arsenic
<0.170
ug/L
0.170
1.00
1
03/13/2101:00
MMR
6020B
Barium
13.8
Ng/L
0.810
10.0
1
03/13/2101:00
MMR
6020E
Beryllium
<0.190
ug/L
0.190
1.00
1
03/13/2101:00
MMR
6020B
Cadmium
<0.160
Ng/L
0.160
1.00
1
03/13/2101:00
MMR
6020E
Chromium
<0.790
ug/L
0.790
2.00
1
03/13/2101:00
MMR
6020B
Cobalt
<0.520
Ng/L
0.520
2.00
1
03/13/2101:00
MMR
6020E
Copper
<3.80
ug/L
3.80
10.0
1
03/13/2101:00
MMR
6020B
Lead
<0.260
Ng/L
0.260
1.00
1
03/13/2101:00
MMR
6020E
Mercury (Total)
<0.0300
ug/L
0.0300
0.200
1
03/16/21 14:01
EDV
7470A
Nickel
<0.510
Ng/L
0.510
3.00
1
03/13/2101:00
MMR
6020E
Selenium
<0.740
ug/L
0.740
5.00
1
03/13/2101:00
MMR
6020B
Silver
<0.110
Ng/L
0.110
1.00
1
03/13/2101:00
MMR
6020E
Thallium
<0.570
ug/L
0.570
2.00
1
03/13/2101:00
MMR
6020B
Vanadium
<1.30
Ng/L
1.30
5.00
1
03/13/2101:00
MMR
6020B
Zinc
<6.90
ug/L
6.90
20.0
1
03/13/2101:00
MMR
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
L
Limit Exceeded
MQL
Method Quantitation Limit
Page 28 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94378
Matrix: Aqueous
Sample ID: SW-01-20210309
Sampled:
3/9/2021 12:42
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.310
N9/L
0.310
5.00
1
03/13/21 18:39
JLB
V1702
Acrylonitrile
<0.200
u9/L
0.200
20.0
1
03/13/21 18:39
JLB
V1702
Benzene
<0.048
N9/L
0.048
0.500
1
03/13/21 18:39
JLB
V1702
Bromochloromethane
<0.140
u9/L
0.140
0.500
1
03/13/21 18:39
JLB
V1702
Bromodichloromethane
<0.062
N9/L
0.062
0.500
1
03/13/21 18:39
JLB
V1702
Bromoform
<0.040
u9/L
0.040
1.00
1
03/13/21 18:39
JLB
V1702
Bromomethane
<0.180
N9/L
0.180
1.00
1
03/13/21 18:39
JLB
V1702
Carbon Disulfide
<0.075
u9/L
0.075
5.00
1
03/13/21 18:39
JLB
V1702
Carbon Tetrachloride
<0.110
N9/L
0.110
0.500
1
03/13/21 18:39
JLB
V1702
Chlorobenzene
<0.062
u9/L
0.062
0.500
1
03/13/21 18:39
JLB
V1702
Chlorodibromomethane
<0.081
N9/L
0.081
0.500
1
03/13/21 18:39
JLB
V1702
Chloroethane
<0.220
ug/L
0.220
0.500
1
03/13/21 18:39
JLB
V1702
Chloroform
<0.076
N9/L
0.076
0.500
1
03/13/21 18:39
JLB
V1702
Chloromethane
<0.079
ug/L
0.079
0.500
1
03/13/21 18:39
JLB
V1702
Di -Isopropyl Ether(DIPE)
<0.960
N9/L
0.960
5.00
1
03/13/21 18:39
JLB
V1702
1,2-Dibromo-3-Chloropropane
<0.170
pg/L
0.170
2.00
1
03/13/21 18:39
JLB
V1702
1,2-Dibromoethane
<0.051
N9/L
0.051
0.500
1
03/13/21 18:39
JLB
V1702
Dibromomethane
<0.065
pg/L
0.065
0.500
1
03/13/21 18:39
JLB
V1702
trans-1,4-Dichloro-2-butene
<0.120
N9/L
0.120
10.0
1
03/13/21 18:39
JLB
V1702
1,2-Dichlorobenzene
<0.076
pg/L
0.076
0.500
1
03/13/21 18:39
JLB
V1702
1,4-Dichlorobenzene
<0.050
N9/L
0.050
0.500
1
03/13/21 18:39
JLB
V1702
Dichlorodifluoromethane
<0.110
pg/L
0.110
5.00
1
03/13/21 18:39
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 29 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94378
Matrix: Aqueous
Sample ID: SW-01-20210309
Sampled:
3/9/2021 12:42
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,1-Dichloroethane
<0.083
Ng/L
0.083
0.500
1
03/13/21 18:39
JLB
V1702
1,2-Dichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 18:39
JLB
V1702
1,1-Dichloroethene
<0.083
N9/L
0.083
0.500
1
03/13/21 18:39
JLB
V1702
cis- 1,2-Dich loroethene
<0.056
u9/L
0.056
0.500
1
03/13/21 18:39
JLB
V1702
trans-1,2-Dichloroethene
<0.094
N9/L
0.094
0.500
1
03/13/21 18:39
JLB
V1702
1,2-Dichloropropane
<0.110
u9/L
0.110
0.500
1
03/13/21 18:39
JLB
V1702
cis- 1,3-Dich loropropene
<0.079
N9/L
0.079
0.500
1
03/13/21 18:39
JLB
V1702
trans-1,3-Dichloropropene
<0.070
u9/L
0.070
0.500
1
03/13/21 18:39
JLB
V1702
1,4-Dioxane
<14.0
N9/L
14.0
150
1
03/13/21 18:39
JLB
V1702
Ethylbenzene
<0.061
u9/L
0.061
0.500
1
03/13/21 18:39
JLB
V1702
2-Hexanone
<0.065
N9/L
0.065
5.00
1
03/13/21 18:39
JLB
V1702
Methyl Ethyl Ketone (MEK)
<0.240
ug/L
0.240
5.00
1
03/13/21 18:39
JLB
V1702
4-Methyl-2-Pentanone
<1.00
N9/L
1.00
5.00
1
03/13/21 18:39
JLB
V1702
Methylene Chloride
<0.083
ug/L
0.083
1.00
1
03/13/21 18:39
JLB
V1702
Styrene
<0.047
N9/L
0.047
0.500
1
03/13/21 18:39
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.110
pg/L
0.110
0.500
1
03/13/21 18:39
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.036
N9/L
0.036
0.500
1
03/13/21 18:39
JLB
V1702
Tetrachloroethene
<0.098
pg/L
0.098
0.500
1
03/13/21 18:39
JLB
V1702
Tetrahydrofuran
<1.10
N9/L
1.10
10.0
1
03/13/21 18:39
JLB
V1702
Toluene
<0.044
u9/L
0.044
0.500
1
03/13/21 18:39
JLB
V1702
1,1,1-Trichloroethane
<0.061
N9/L
0.061
0.500
1
03/13/21 18:39
JLB
V1702
1,1,2-Trichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 18:39
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 30 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
Lab No : 94378
Sample ID: SW-01-20210309
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 3/9/2021 12:42
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Trichloroethene
<0.078
Ng/L
0.078
0.500
1
03/13/21 18:39 JLB
V1702
Trichlorofluoromethane
<0.062
ug/L
0.062
0.500
1
03/13/21 18:39 JLB
V1702
1,2,3-Trichloropropane
<0.140
Ng/L
0.140
1.00
1
03/13/21 18:39 JLB
V1702
Vinyl Acetate
<0.060
ug/L
0.060
2.00
1
03/13/21 18:39 JLB
V1702
Vinyl Chloride
<0.097
Ng/L
0.097
0.500
1
03/13/21 18:39 JLB
V1702
o-Xylene
<0.044
ug/L
0.044
0.500
1
03/13/21 18:39 JLB
V1702
m,p-Xylene
<0.120
Ng/L
0.120
1.00
1
03/13/21 18:39 JLB
V1702
Xylene (Total)
<0.044
ug/L
0.044
0.500
1
03/13/21 18:39
V1702
Surrogate:4-Bromofluorobenzene
95.0
Limits:80-124%
1 03/13/21 18:39 JLB
V1702
Surrogate: Dibromofluoromethane
113
Limits:
75-129%
1 03/13/21 18:39 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
112
Limits:
63-136%
1 03/13/21 18:39 JLB
V1702
Surrogate: Toluene-d8
98.6
Limits:
77-123%
1 03/13/21 18:39 JLB
V1702
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 31 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94379 Matrix: Aqueous
Sample ID: SW-02-20210309 Sampled: 3/9/2021 13:04
Hardness 8500 Ng/L
1,4-Dioxane <0.139 ug/L
Surrogate: 4-Bromofluorobenzene 103
Test Results Units
570 5000
1 03/18/21 11:20 SLS
0.139 2.00
1 03/11/21 18:42 TBL
Limits:70-130%
1 03/11/2118:42 TBL V1584
MDL MQL
DF Date / Time By Analytical
Analyzed Method
Antimony
<0.490
Ng/L
0.490
2.00
1
03/13/2101:46
MMR
6020E
Arsenic
<0.170
ug/L
0.170
1.00
1
03/13/2101:46
MMR
6020B
Barium
22.7
Ng/L
0.810
10.0
1
03/13/2101:46
MMR
6020E
Beryllium
<0.190
ug/L
0.190
1.00
1
03/13/2101:46
MMR
6020B
Cadmium
<0.160
Ng/L
0.160
1.00
1
03/13/2101:46
MMR
6020E
Chromium
3.06
ug/L
0.790
2.00
1
03/13/2101:46
MMR
6020B
Cobalt
0.6463
Ng/L
0.520
2.00
1
03/13/2101:46
MMR
6020E
Copper
<3.80
ug/L
3.80
10.0
1
03/13/2101:46
MMR
6020B
Lead
0.6523
Ng/L
0.260
1.00
1
03/13/2101:46
MMR
6020E
Mercury (Total)
<0.0300
ug/L
0.0300
0.200
1
03/16/21 14:05
EDV
7470A
Nickel
1.923
Ng/L
0.510
3.00
1
03/13/2101:46
MMR
6020E
Selenium
<0.740
ug/L
0.740
5.00
1
03/13/2101:46
MMR
6020B
Silver
<0.110
Ng/L
0.110
1.00
1
03/13/2101:46
MMR
6020E
Thallium
<0.570
ug/L
0.570
2.00
1
03/13/2101:46
MMR
6020B
Vanadium
3.033
Ng/L
1.30
5.00
1
03/13/2101:46
MMR
6020E
Zinc
<6.90
ug/L
6.90
20.0
1
03/13/2101:46
MMR
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
L
Limit Exceeded
MQL
Method Quantitation Limit
Page 32 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94379
Matrix: Aqueous
Sample ID: SW-02-20210309
Sampled:
3/9/2021 13:04
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.310
N9/L
0.310
5.00
1
03/13/21 19:13
JLB
V1702
Acrylonitrile
<0.200
u9/L
0.200
20.0
1
03/13/21 19:13
JLB
V1702
Benzene
<0.048
N9/L
0.048
0.500
1
03/13/21 19:13
JLB
V1702
Bromochloromethane
<0.140
u9/L
0.140
0.500
1
03/13/21 19:13
JLB
V1702
Bromodichloromethane
<0.062
N9/L
0.062
0.500
1
03/13/21 19:13
JLB
V1702
Bromoform
<0.040
u9/L
0.040
1.00
1
03/13/21 19:13
JLB
V1702
Bromomethane
<0.180
N9/L
0.180
1.00
1
03/13/21 19:13
JLB
V1702
Carbon Disulfide
<0.075
u9/L
0.075
5.00
1
03/13/21 19:13
JLB
V1702
Carbon Tetrachloride
<0.110
N9/L
0.110
0.500
1
03/13/21 19:13
JLB
V1702
Chlorobenzene
<0.062
u9/L
0.062
0.500
1
03/13/21 19:13
JLB
V1702
Chlorodibromomethane
<0.081
N9/L
0.081
0.500
1
03/13/21 19:13
JLB
V1702
Chloroethane
<0.220
ug/L
0.220
0.500
1
03/13/21 19:13
JLB
V1702
Chloroform
<0.076
N9/L
0.076
0.500
1
03/13/21 19:13
JLB
V1702
Chloromethane
<0.079
ug/L
0.079
0.500
1
03/13/21 19:13
JLB
V1702
Di -Isopropyl Ether(DIPE)
<0.960
N9/L
0.960
5.00
1
03/13/21 19:13
JLB
V1702
1,2-Dibromo-3-Chloropropane
<0.170
pg/L
0.170
2.00
1
03/13/21 19:13
JLB
V1702
1,2-Dibromoethane
<0.051
N9/L
0.051
0.500
1
03/13/21 19:13
JLB
V1702
Dibromomethane
<0.065
pg/L
0.065
0.500
1
03/13/21 19:13
JLB
V1702
trans-1,4-Dichloro-2-butene
<0.120
N9/L
0.120
10.0
1
03/13/21 19:13
JLB
V1702
1,2-Dichlorobenzene
<0.076
pg/L
0.076
0.500
1
03/13/21 19:13
JLB
V1702
1,4-Dichlorobenzene
<0.050
N9/L
0.050
0.500
1
03/13/21 19:13
JLB
V1702
Dichlorodifluoromethane
<0.110
pg/L
0.110
5.00
1
03/13/21 19:13
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 33 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94379
Matrix: Aqueous
Sample ID: SW-02-20210309
Sampled:
3/9/2021 13:04
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,1-Dichloroethane
<0.083
N9/L
0.083
0.500
1
03/13/21 19:13
JLB
V1702
1,2-Dichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 19:13
JLB
V1702
1,1-Dichloroethene
<0.083
N9/L
0.083
0.500
1
03/13/21 19:13
JLB
V1702
cis- 1,2-Dich loroethene
<0.056
u9/L
0.056
0.500
1
03/13/21 19:13
JLB
V1702
trans-1,2-Dichloroethene
<0.094
N9/L
0.094
0.500
1
03/13/21 19:13
JLB
V1702
1,2-Dichloropropane
<0.110
u9/L
0.110
0.500
1
03/13/21 19:13
JLB
V1702
cis- 1,3-Dich loropropene
<0.079
N9/L
0.079
0.500
1
03/13/21 19:13
JLB
V1702
trans-1,3-Dichloropropene
<0.070
u9/L
0.070
0.500
1
03/13/21 19:13
JLB
V1702
1,4-Dioxane
<14.0
N9/L
14.0
150
1
03/13/21 19:13
JLB
V1702
Ethylbenzene
<0.061
u9/L
0.061
0.500
1
03/13/21 19:13
JLB
V1702
2-Hexanone
<0.065
N9/L
0.065
5.00
1
03/13/21 19:13
JLB
V1702
Methyl Ethyl Ketone (MEK)
<0.240
ug/L
0.240
5.00
1
03/13/21 19:13
JLB
V1702
4-Methyl-2-Pentanone
<1.00
N9/L
1.00
5.00
1
03/13/21 19:13
JLB
V1702
Methylene Chloride
<0.083
ug/L
0.083
1.00
1
03/13/21 19:13
JLB
V1702
Styrene
<0.047
N9/L
0.047
0.500
1
03/13/21 19:13
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.110
pg/L
0.110
0.500
1
03/13/21 19:13
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.036
N9/L
0.036
0.500
1
03/13/21 19:13
JLB
V1702
Tetrachloroethene
<0.098
pg/L
0.098
0.500
1
03/13/21 19:13
JLB
V1702
Tetrahydrofuran
<1.10
N9/L
1.10
10.0
1
03/13/21 19:13
JLB
V1702
Toluene
<0.044
u9/L
0.044
0.500
1
03/13/21 19:13
JLB
V1702
1,1,1-Trichloroethane
<0.061
N9/L
0.061
0.500
1
03/13/21 19:13
JLB
V1702
1,1,2-Trichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 19:13
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 34 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
Lab No : 94379
Sample ID: SW-02-20210309
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 3/9/2021 13:04
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Trichloroethene
<0.078
Ng/L
0.078
0.500
1
03/13/21 19:13 JLB
V1702
Trichlorofluoromethane
<0.062
ug/L
0.062
0.500
1
03/13/21 19:13 JLB
V1702
1,2,3-Trichloropropane
<0.140
Ng/L
0.140
1.00
1
03/13/21 19:13 JLB
V1702
Vinyl Acetate
<0.060
ug/L
0.060
2.00
1
03/13/21 19:13 JLB
V1702
Vinyl Chloride
<0.097
Ng/L
0.097
0.500
1
03/13/21 19:13 JLB
V1702
o-Xylene
<0.044
ug/L
0.044
0.500
1
03/13/21 19:13 JLB
V1702
m,p-Xylene
<0.120
Ng/L
0.120
1.00
1
03/13/21 19:13 JLB
V1702
Xylene (Total)
<0.044
ug/L
0.044
0.500
1
03/13/21 19:13
V1702
Surrogate:4-Bromofluorobenzene
95.0
Limits:80-124%
1 03/13/21 19:13 JLB
V1702
Surrogate: Dibromofluoromethane
114
Limits:
75-129%
1 03/13/21 19:13 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
110
Limits:
63-136%
1 03/13/21 19:13 JLB
V1702
Surrogate: Toluene-d8
101
Limits:
77-123%
1 03/13/21 19:13 JLB
V1702
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 35 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94380
Matrix: Aqueous
Sample ID : TB-202103090000
Sampled:
3/9/2021 12:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.310
N9/L
0.310
5.00
1
03/13/21 15:14
JLB
V1702
Acrylonitrile
<0.200
u9/L
0.200
20.0
1
03/13/21 15:14
JLB
V1702
Benzene
<0.048
N9/L
0.048
0.500
1
03/13/21 15:14
JLB
V1702
Bromochloromethane
<0.140
u9/L
0.140
0.500
1
03/13/21 15:14
JLB
V1702
Bromodichloromethane
<0.062
N9/L
0.062
0.500
1
03/13/21 15:14
JLB
V1702
Bromoform
<0.040
u9/L
0.040
1.00
1
03/13/21 15:14
JLB
V1702
Bromomethane
<0.180
N9/L
0.180
1.00
1
03/13/21 15:14
JLB
V1702
Carbon Disulfide
<0.075
u9/L
0.075
5.00
1
03/13/21 15:14
JLB
V1702
Carbon Tetrachloride
<0.110
N9/L
0.110
0.500
1
03/13/21 15:14
JLB
V1702
Chlorobenzene
<0.062
u9/L
0.062
0.500
1
03/13/21 15:14
JLB
V1702
Chlorodibromomethane
<0.081
N9/L
0.081
0.500
1
03/13/21 15:14
JLB
V1702
Chloroethane
<0.220
ug/L
0.220
0.500
1
03/13/21 15:14
JLB
V1702
Chloroform
<0.076
N9/L
0.076
0.500
1
03/13/21 15:14
JLB
V1702
Chloromethane
<0.079
ug/L
0.079
0.500
1
03/13/21 15:14
JLB
V1702
Di -Isopropyl Ether(DIPE)
<0.960
N9/L
0.960
5.00
1
03/13/21 15:14
JLB
V1702
1,2-Dibromo-3-Chloropropane
<0.170
pg/L
0.170
2.00
1
03/13/21 15:14
JLB
V1702
1,2-Dibromoethane
<0.051
N9/L
0.051
0.500
1
03/13/21 15:14
JLB
V1702
Dibromomethane
<0.065
pg/L
0.065
0.500
1
03/13/21 15:14
JLB
V1702
trans-1,4-Dichloro-2-butene
<0.120
N9/L
0.120
10.0
1
03/13/21 15:14
JLB
V1702
1,2-Dichlorobenzene
<0.076
pg/L
0.076
0.500
1
03/13/21 15:14
JLB
V1702
1,4-Dichlorobenzene
<0.050
N9/L
0.050
0.500
1
03/13/21 15:14
JLB
V1702
Dichlorodifluoromethane
<0.110
pg/L
0.110
5.00
1
03/13/21 15:14
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 36 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019 REPOR T OF A NA L YSIS
Lab No : 94380
Matrix: Aqueous
Sample ID : TB-202103090000
Sampled:
3/9/2021 12:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,1-Dichloroethane
<0.083
N9/L
0.083
0.500
1
03/13/21 15:14
JLB
V1702
1,2-Dichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 15:14
JLB
V1702
1,1-Dichloroethene
<0.083
N9/L
0.083
0.500
1
03/13/21 15:14
JLB
V1702
cis- 1,2-Dich loroethene
<0.056
u9/L
0.056
0.500
1
03/13/21 15:14
JLB
V1702
trans-1,2-Dichloroethene
<0.094
N9/L
0.094
0.500
1
03/13/21 15:14
JLB
V1702
1,2-Dichloropropane
<0.110
u9/L
0.110
0.500
1
03/13/21 15:14
JLB
V1702
cis- 1,3-Dich loropropene
<0.079
N9/L
0.079
0.500
1
03/13/21 15:14
JLB
V1702
trans-1,3-Dichloropropene
<0.070
u9/L
0.070
0.500
1
03/13/21 15:14
JLB
V1702
1,4-Dioxane
<14.0
N9/L
14.0
150
1
03/13/21 15:14
JLB
V1702
Ethylbenzene
<0.061
u9/L
0.061
0.500
1
03/13/21 15:14
JLB
V1702
2-Hexanone
<0.065
N9/L
0.065
5.00
1
03/13/21 15:14
JLB
V1702
Methyl Ethyl Ketone (MEK)
<0.240
ug/L
0.240
5.00
1
03/13/21 15:14
JLB
V1702
4-Methyl-2-Pentanone
<1.00
N9/L
1.00
5.00
1
03/13/21 15:14
JLB
V1702
Methylene Chloride
<0.083
ug/L
0.083
1.00
1
03/13/21 15:14
JLB
V1702
Styrene
<0.047
N9/L
0.047
0.500
1
03/13/21 15:14
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.110
pg/L
0.110
0.500
1
03/13/21 15:14
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.036
N9/L
0.036
0.500
1
03/13/21 15:14
JLB
V1702
Tetrachloroethene
<0.098
pg/L
0.098
0.500
1
03/13/21 15:14
JLB
V1702
Tetrahydrofuran
<1.10
N9/L
1.10
10.0
1
03/13/21 15:14
JLB
V1702
Toluene
<0.044
u9/L
0.044
0.500
1
03/13/21 15:14
JLB
V1702
1,1,1-Trichloroethane
<0.061
N9/L
0.061
0.500
1
03/13/21 15:14
JLB
V1702
1,1,2-Trichloroethane
<0.066
u9/L
0.066
0.500
1
03/13/21 15:14
JLB
V1702
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation
Limit
Page 37 of 67

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippin Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/10/2021
Asheville , NC 28801
Report Number : 21-069-0019
Lab No : 94380
Sample ID : TB-202103090000
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 3/9/2021 12:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Trichloroethene
<0.078
Ng/L
0.078
0.500
1
03/13/21 15:14 JLB
V1702
Trichlorofluoromethane
<0.062
ug/L
0.062
0.500
1
03/13/21 15:14 JLB
V1702
1,2,3-Trichloropropane
<0.140
Ng/L
0.140
1.00
1
03/13/21 15:14 JLB
V1702
Vinyl Acetate
<0.060
ug/L
0.060
2.00
1
03/13/21 15:14 JLB
V1702
Vinyl Chloride
<0.097
Ng/L
0.097
0.500
1
03/13/21 15:14 JLB
V1702
o-Xylene
<0.044
ug/L
0.044
0.500
1
03/13/21 15:14 JLB
V1702
m,p-Xylene
<0.120
Ng/L
0.120
1.00
1
03/13/21 15:14 JLB
V1702
Xylene (Total)
<0.044
ug/L
0.044
0.500
1
03/13/21 15:14
V1702
Surrogate:4-Bromofluorobenzene
94.6
Limits:80-124%
1 03/13/21 15:14 JLB
V1702
Surrogate: Dibromofluoromethane
106
Limits:
75-129%
1 03/13/21 15:14 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
104
Limits:
63-136%
1 03/13/21 15:14 JLB
V1702
Surrogate: Toluene-d8
100
Limits:
77-123%
1 03/13/21 15:14 JLB
V1702
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 38 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Analytical Batch:
V1945
Analysis Method:
2320B-2011
Analysis Description:
Alkalinity
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
94374, 94375, 94376, 94377
Blank MDL
MQL
Analyzed
Parameter
Units Result
Alkalinity (as CaCO3)
pg/L <800 800
5000
03/19/21 13:40
Laboratory Control Sample LCS
Spike
LCS
LCS %Rec % Rec
Parameter
Units Conc.
Result
Limits
Alkalinity (as CaCO3)
pg/L 250000
247000
99.0 90-110
Duplicate
V 94507-DUP
Result DUP
RPD Max RPD
Analyzed
Parameter
Units Result
Alkalinity (as CaCO3)
pg/L 126000 128000
1.5 20
03/19/21 13:40
Date: 03/31/2021 12:59 PM Page 1 of 27
Page 39 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Analytical Batch:
V1864
Analysis Method:
2340C-2011
Analysis Description:
Total Hardness
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
94374, 94375, 94376, 94377, 94378, 94379
Blank MDL
MQL
Analyzed
Parameter
Units Result
Hardness
pg/L <570 570
5000
03/18/21 11:20
Laboratory Control Sample LCS
Spike
LCS
LCS %Rec % Rec
Parameter
Units Conc.
Result
Limits
Hardness
pg/L 50000
51000
102 90-110
Duplicate
V 94374-DUP
Result DUP
RPD Max RPD
Analyzed
Parameter
Units Result
Hardness
pg/L 162000 158000
2.5 20
03/18/21 11:20
Date: 03/31/2021 12:59 PM Page 2 of 27
Page 40 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Analytical Batch: V1747
Analysis Method: 4500S2F-2011
Analysis Description: Sulfide
Lab Reagent Blank LRB Matrix: AQU
Associated Lab Samples: 94374, 94375, 94376, 94377
Blank MDL MQL Analyzed
Parameter Units Result
Sulfide pg/L <830 830 2000 03/15/2111:30
Laboratory Control Sample LCS
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Sulfide
pg/L 10000 7200
72.0 70-122
Date: 03/31/2021 12:59 PM Page 3 of 27
Page 41 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Analytical Batch: V1753
Analysis Method: 5210B-2011
Analysis Description: Biochemical Oxygen Demand (BOD)
Glucose-Glutamic Acid GGA
Result Range Analyzed
Parameter Units
Biochemical Oxygen Demand (5-day) Ng/L 215 167.5-228.E 03/10/21 11:06
Duplicate V 94135-DUP
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Biochemical Oxygen Demand (5-day) Ng/L 2000 2000 0.0 30 03/10/21 11:06
Date: 03/31/2021 12:59 PM Page 4 of 27
Page 42 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Analytical Batch: V1722
Analysis Method: 5220D-2011
Analysis Description: Chemical Oxygen Demand (COD)
Lab Reagent Blank LRB
Matrix: AQU
Associated Lab Samples: 94374, 94375, 94376, 94377
Blank MDL
MQL
Analyzed
Parameter Units Result
COD (Chemical Oxygen Demand) pg/L <11000 11000
50000
03/16/21 11:30
Laboratory Control Sample LCS
Spike
LCS
LCS %Rec
% Rec
Parameter Units Conc.
Result
Limits
COD (Chemical Oxygen Demand) pg/L 500000
499000
100
90-110
Matrix Spike & Matrix Spike Duplicate V 94374-MS V 94374-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter Units Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
COD (Chemical Oxygen Demand) pg/L <11000 500000
500000 503000
485000 101
97.0 80-120 3.6 20
Date: 03/31/2021 12:59 PM Page 5 of 27
Page 43 of 67

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality
Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Prep:
L541168
QC Analytical Batch(es): L541422
QC Prep Batch Method:
5310C-2011
Analysis Method:
5310C-2011
Analysis Description:
Total Organic Carbon
Lab Reagent Blank
LRB-L541168
Matrix: AQU
Associated Lab Samples:
94374, 94375
Blank MDL
MQL
Analyzed
Parameter
Units
Result
TOC
mg/L
<0.567 0.567
1.00
03/12/2112:11
Laboratory Control Sample
LCS-L541168
Spike
LCS
LCS %Rec % Rec
Parameter
Units
Conc.
Result
Limits
TOC
mg/L
5.00
4.46
89.0 85-115
Duplicate
V 94374-DUP-L541168
Result DUP
RPD Max RPD
Analyzed
Parameter
Units
Result
TOC
mg/L
2.43 2.42
0.4 20.0
03/13/2102:44
Matrix Spike
V 94375-MS-L541168
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
TOC
mg/L
1.60 5.26
6.55
94.0 70-130
Date: 03/31/2021 12:59 PM Page 6 of 27
Page 44 of 67

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality
Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Prep:
L541248
QC Analytical Batch(es): L541422
QC Prep Batch Method:
5310C-2011
Analysis Method:
5310C-2011
Analysis Description:
Total Organic Carbon
Lab Reagent Blank
LRB-L541248
Matrix: AQU
Associated Lab Samples:
94376, 94377
Blank MDL
MQL
Analyzed
Parameter
Units
Result
TOC
mg/L
<0.567 0.567
1.00
03/12/2122:56
Laboratory Control Sample
LCS-L541248
Spike
LCS
LCS %Rec % Rec
Parameter
Units
Conc.
Result
Limits
TOC
mg/L
5.00
4.56
91.0 85-115
Duplicate
L 88298-DUP-L541248
Result DUP
RPD Max RPD
Analyzed
Parameter
Units
Result
TOC
mg/L
< 1.00 <1.00
0.0 20.0
03/13/21 11:37
Matrix Spike
L 88299-MS-L541248
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
TOC
mg/L
0.756 5.26
5.45
104 70-130
Date: 03/31/2021 12:59 PM Page 7 of 27
Page 45 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep:
V1589
QC Analytical Batch(es): V1669,V1737
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Lab Reagent Blank
LRB-V1589
Matrix: AQU
Associated Lab Samples:
94374, 94375, 94376, 94377
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Antimony
pg/L
<0.490
0.490
2.00
03/13/2102:45
Arsenic
pg/L
<0.170
0.170
1.00
03/13/2102:45
Barium
pg/L
<0.810
0.810
10.0
03/13/2102:45
Beryllium
pg/L
<0.190
0.190
1.00
03/13/2102:45
Cadmium
pg/L
<0.160
0.160
1.00
03/13/2102:45
Chromium
pg/L
<0.790
0.790
2.00
03/13/2102:45
Cobalt
pg/L
<0.520
0.520
2.00
03/13/2102:45
Copper
pg/L
<3.80
3.80
10.0
03/13/2102:45
Lead
pg/L
<0.260
0.260
1.00
03/13/2102:45
Nickel
pg/L
<0.510
0.510
3.00
03/13/2102:45
Selenium
pg/L
<0.740
0.740
5.00
03/13/2102:45
Silver
pg/L
<0.110
0.110
1.00
03/13/2102:45
Thallium
pg/L
<0.570
0.570
2.00
03/13/2102:45
Vanadium
pg/L
<1.30
1.30
5.00
03/13/2102:45
Zinc
pg/L
<6.90
6.90
20.0
03/13/2102:45
Laboratory Control Sample LCS-V1589
Spike
Parameter Units Conc.
LCS LCS %Rec % Rec
Result Limits
Antimony
pg/L
100
107
107
80-120
Arsenic
pg/L
100
96.9
97.0
80-120
Barium
pg/L
100
95.9
96.0
80-120
Beryllium
pg/L
100
110
110
80-120
Cadmium
pg/L
100
101
101
80-120
Chromium
pg/L
100
101
101
80-120
Cobalt
pg/L
100
104
104
80-120
Copper
pg/L
100
104
104
80-120
Date: 03/31/2021 12:59 PM Page 8 of 27
Page 46 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1589 QC Analytical Batch(es): V1669,V1737
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V1589
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Lead
pg/L
100
100
100
80-120
Nickel
pg/L
100
106
106
80-120
Selenium
pg/L
100
104
104
80-120
Silver
pg/L
100
101
101
80-120
Thallium
pg/L
100
97.6
98.0
80-120
Vanadium
pg/L
100
100
100
80-120
Zinc
pg/L
100
104
104
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 94364-MS-V1589
MS Spike
Result Conc.
V 94364-MSD-V1589
MSD MS Result
Spike
Conc.
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Antimony
pg/L
< 4.90
100
100
103
104
103
104
75-125
0.9
20.0
Arsenic
pg/L
< 1.70
100
100
98.6
95.5
99.0
96.0
75-125
3.1
20.0
Barium
pg/L
28.3
100
100
121
130
121
130*
75-125
7.1
20.0
Beryllium
pg/L
< 1.90
100
100
101
107
101
107
75-125
5.7
20.0
Cadmium
pg/L
< 1.60
100
100
101
99.3
101
99.0
75-125
1.6
20.0
Chromium
pg/L
< 7.90
100
100
105
103
105
103
75-125
1.9
20.0
Cobalt
pg/L
< 5.20
100
100
105
103
105
103
75-125
1.9
20.0
Copper
pg/L
< 38.0
100
100
106
103
106
103
75-125
2.8
20.0
Lead
pg/L
7.16
100
100
108
108
108
108
75-125
0.0
20.0
Nickel
pg/L
< 5.10
100
100
107
107
107
107
75-125
0.0
20.0
Selenium
pg/L
< 7.40
100
100
82.3
93.7
82.0
94.0
75-125
12.9
20.0
Silver
pg/L
< 1.10
100
100
103
102
103
102
75-125
0.9
20.0
Thallium
pg/L
< 5.70
100
100
95.9
96.6
96.0
97.0
75-125
0.7
20.0
Vanadium
pg/L
< 13.0
100
100
97.6
101
98.0
101
75-125
3.4
20.0
Zinc
pg/L
< 69.0
100
100
172
174
0.0*
0.0*
75-125
0.0
20.0
* QC Fail Date: 03/31/2021 12:59 PM Page 9 of 27
Page 47 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1589
QC Prep Batch Method: 3005A
Post Digestion Spike V 94364-PDS-V1589
Parameter
Units
PDS
Result
Antimony
pg/L
50.7
Arsenic
pg/L
46.2
Barium
Ng/L
59.5
Beryllium
Ng/L
50.0
Cadmium
pg/L
47.6
Chromium
pg/L
48.9
Cobalt
pg/L
49.0
Copper
pg/L
49.3
Lead
pg/L
49.6
Nickel
pg/L
47.6
Selenium
pg/L
47.2
Silver
pg/L
48.7
Thallium
pg/L
47.5
Vanadium
pg/L
48.7
Zinc
pg/L
64.2
QC Analytical Batch(es): V1669,V1737
Analysis Method: 6020B
Analysis Description: Metals Analyses
o/a
Recovery
101
92.0
119
100
95.0
98.0
98.0
99.0
99.0
95.0
94.0
97.0
95.0
97.0
128*
Analyzed
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
03/15/21 18:10
* QC Fail Date: 03/31/2021 12:59 PM Page 10 of 27
Page 48 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1591 QC Analytical Batch(es): V1669
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Lab Reagent Blank LRB-V1591 Matrix: AQU
Associated Lab Samples: 94378, 94379
Parameter
Units
Blank
Result
MDL
MQL
Analyzed
Antimony
pg/L
<0.490
0.490
2.00
03/13/2100:41
Arsenic
pg/L
<0.170
0.170
1.00
03/13/2100:41
Barium
pg/L
<0.810
0.810
10.0
03/13/2100:41
Beryllium
pg/L
<0.190
0.190
1.00
03/13/2100:41
Cadmium
pg/L
<0.160
0.160
1.00
03/13/2100:41
Chromium
pg/L
<0.790
0.790
2.00
03/13/2100:41
Cobalt
pg/L
<0.520
0.520
2.00
03/13/2100:41
Copper
pg/L
<3.80
3.80
10.0
03/13/2100:41
Lead
pg/L
<0.260
0.260
1.00
03/13/2100:41
Nickel
pg/L
<0.510
0.510
3.00
03/13/2100:41
Selenium
pg/L
<0.740
0.740
5.00
03/13/2100:41
Silver
pg/L
<0.110
0.110
1.00
03/13/2100:41
Thallium
pg/L
<0.570
0.570
2.00
03/13/2100:41
Vanadium
pg/L
<1.30
1.30
5.00
03/13/2100:41
Zinc
pg/L
<6.90
6.90
20.0
03/13/2100:41
Laboratory Control Sample LCS-V1591
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
pg/L
100
108
pg/L
100
97.9
pg/L
100
99.7
pg/L
100
102
pg/L
100
101
pg/L
100
102
pg/L
100
104
pg/L
100
104
Date: 03/31/2021 12:59 PM
Page 49 of 67
108
98.0
100
102
101
102
104
104
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
Page 11 of 27

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1591 QC Analytical Batch(es): V1669
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V1591
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Lead
pg/L
100
102
102
80-120
Nickel
pg/L
100
105
105
80-120
Selenium
pg/L
100
95.3
95.0
80-120
Silver
pg/L
100
102
102
80-120
Thallium
pg/L
100
98.5
99.0
80-120
Vanadium
pg/L
100
103
103
80-120
Zinc
pg/L
100
102
102
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 94378-MS-V1591
MS Spike
Result Conc.
V 94378-MSD-V1591
MSD MS Result
Spike
Conc.
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Antimony
pg/L
< 0.490
100
100
107
106
107
106
75-125
0.9
20.0
Arsenic
pg/L
< 0.170
100
100
97.7
95.2
98.0
95.0
75-125
2.5
20.0
Barium
pg/L
13.8
100
100
115
114
101
100
75-125
0.8
20.0
Beryllium
pg/L
< 0.190
100
100
105
104
105
104
75-125
0.9
20.0
Cadmium
pg/L
< 0.160
100
100
100
102
100
102
75-125
1.9
20.0
Chromium
pg/L
< 0.790
100
100
102
103
102
103
75-125
0.9
20.0
Cobalt
pg/L
< 0.520
100
100
104
103
104
103
75-125
0.9
20.0
Copper
pg/L
< 3.80
100
100
105
104
105
104
75-125
0.9
20.0
Lead
pg/L
< 0.260
100
100
102
100
102
100
75-125
1.9
20.0
Nickel
pg/L
< 0.510
100
100
105
105
105
105
75-125
0.0
20.0
Selenium
pg/L
< 0.740
100
100
102
103
102
103
75-125
0.9
20.0
Silver
pg/L
< 0.110
100
100
103
101
103
101
75-125
1.9
20.0
Thallium
pg/L
< 0.570
100
100
101
97.8
101
98.0
75-125
3.2
20.0
Vanadium
pg/L
< 1.30
100
100
104
103
104
103
75-125
0.9
20.0
Zinc
pg/L
< 6.90
100
100
103
103
103
103
75-125
0.0
20.0
Date: 03/31/2021 12:59 PM Page 12 of 27
Page 50 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1591
QC Prep Batch Method: 3005A
Post Digestion Spike V 94378-PDS-V1591
Parameter
Units
PDS
Result
Antimony
pg/L
49.7
Arsenic
Ng/L
50.0
Barium
pg/L
55.1
Beryllium
pg/L
50.1
Cadmium
pg/L
48.7
Chromium
Ng/L
50.9
Cobalt
Ng/L
50.3
Copper
pg/L
51.4
Lead
pg/L
49.9
Nickel
pg/L
52.2
Selenium
pg/L
50.4
Silver
Ng/L
50.0
Thallium
pg/L
49.5
Vanadium
pg/L
51.1
Zinc
pg/L
50.4
QC Analytical Batch(es): V1669
Analysis Method: 6020B
Analysis Description: Metals Analyses
o/a
Recovery
99.0
100
97.0
100
97.0
102
101
103
100
104
101
100
99.0
102
101
Analyzed
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
Date: 03/31/2021 12:59 PM Page 13 of 27
Page 51 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1688 QC Analytical Batch(es): V1695
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Lab Reagent Blank LRB-V1688 Matrix: AQU
Associated Lab Samples: 94376
Parameter
Units
Blank
Result
MDL
MQL
Analyzed
Dissolved Antimony
pg/L
<0.490
0.490
2.00
03/12/21 21:45
Dissolved Arsenic
pg/L
<0.170
0.170
1.00
03/12/21 21:45
Dissolved Barium
pg/L
<0.810
0.810
10.0
03/12/21 21:45
Dissolved Beryllium
pg/L
<0.190
0.190
1.00
03/12/21 21:45
Dissolved Cadmium
pg/L
<0.160
0.160
1.00
03/12/21 21:45
Dissolved Chromium
pg/L
<0.790
0.790
2.00
03/12/21 21:45
Dissolved Cobalt
pg/L
<0.520
0.520
2.00
03/12/21 21:45
Dissolved Copper
pg/L
<3.80
3.80
10.0
03/12/21 21:45
Dissolved Lead
pg/L
<0.260
0.260
1.00
03/12/21 21:45
Dissolved Nickel
pg/L
<0.510
0.510
3.00
03/12/21 21:45
Dissolved Selenium
pg/L
<0.740
0.740
5.00
03/12/21 21:45
Dissolved Silver
pg/L
<0.110
0.110
1.00
03/12/21 21:45
Dissolved Thallium
pg/L
<0.570
0.570
2.00
03/12/21 21:45
Dissolved Vanadium
pg/L
<1.30
1.30
5.00
03/12/21 21:45
Dissolved Zinc
pg/L
<6.90
6.90
20.0
03/12/21 21:45
Laboratory Control Sample LCS-V1688
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Dissolved Antimony
pg/L
100
92.6
93.0
80-120
Dissolved Arsenic
pg/L
100
93.2
93.0
80-120
Dissolved Barium
pg/L
100
94.6
95.0
80-120
Dissolved Beryllium
pg/L
100
96.6
97.0
80-120
Dissolved Cadmium
pg/L
100
99.6
100
80-120
Dissolved Chromium
pg/L
100
98.6
99.0
80-120
Dissolved Cobalt
pg/L
100
96.3
96.0
80-120
Dissolved Copper
pg/L
100
96.5
97.0
80-120
Date: 03/31/2021 12:59 PM Page 14 of 27
Page 52 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1688 QC Analytical Batch(es): V1695
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V1688
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Dissolved Lead
pg/L
100
97.6
98.0
80-120
Dissolved Nickel
pg/L
100
98.2
98.0
80-120
Dissolved Selenium
pg/L
100
99.8
100
80-120
Dissolved Silver
pg/L
100
97.4
97.0
80-120
Dissolved Thallium
pg/L
100
98.5
99.0
80-120
Dissolved Vanadium
pg/L
100
98.3
98.0
80-120
Dissolved Zinc
pg/L
100
97.3
97.0
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 93965-V1633-MS-V1688
MS Spike MSD
Result Conc. Spike
Conc.
V 93965-V1633-MSD-V1688
MS Result MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Dissolved Antimony
pg/L
< 0.490
100
100
94.4
95.4
94.0
95.0
75-125
1.0
20.0
Dissolved Arsenic
pg/L
< 0.170
100
100
92.6
92.1
93.0
92.0
75-125
0.5
20.0
Dissolved Barium
pg/L
57.6
100
100
151
155
93.0
97.0
75-125
2.6
20.0
Dissolved Beryllium
pg/L
< 0.190
100
100
96.6
99.5
97.0
100
75-125
2.9
20.0
Dissolved Cadmium
pg/L
< 0.160
100
100
96.7
97.9
97.0
98.0
75-125
1.2
20.0
Dissolved Chromium
pg/L
< 0.790
100
100
96.6
97.5
97.0
98.0
75-125
0.9
20.0
Dissolved Cobalt
pg/L
< 0.520
100
100
96.6
98.0
97.0
98.0
75-125
1.4
20.0
Dissolved Copper
pg/L
< 3.80
100
100
98.6
99.2
99.0
99.0
75-125
0.6
20.0
Dissolved Lead
pg/L
< 0.260
100
100
97.3
96.0
97.0
96.0
75-125
1.3
20.0
Dissolved Nickel
pg/L
0.921
100
100
98.4
99.7
98.0
100
75-125
1.3
20.0
Dissolved Selenium
pg/L
< 0.740
100
100
93.6
98.0
94.0
98.0
75-125
4.5
20.0
Dissolved Silver
pg/L
< 0.110
100
100
96.3
97.7
96.0
98.0
75-125
1.4
20.0
Dissolved Thallium
pg/L
< 0.570
100
100
97.6
95.8
98.0
96.0
75-125
1.8
20.0
Dissolved Vanadium
pg/L
< 1.30
100
100
96.2
97.7
96.0
98.0
75-125
1.5
20.0
Dissolved Zinc
pg/L
< 6.90
100
100
100
100
100
100
75-125
0.0
20.0
Date: 03/31/2021 12:59 PM Page 15 of 27
Page 53 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1688 QC Analytical Batch(es): V1695
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Post Digestion Spike V 93965-V1633-PDS-V1688
Parameter
Units
PDS
Result
%
Recovery
Analyzed
Dissolved Antimony
pg/L
52.1
104
03/12/21 22:17
Dissolved Arsenic
pg/L
51.7
103
03/12/21 22:17
Dissolved Barium
pg/L
82.5
105
03/12/21 22:17
Dissolved Beryllium
pg/L
53.8
108
03/12/21 22:17
Dissolved Cadmium
pg/L
51.7
103
03/12/21 22:17
Dissolved Chromium
pg/L
51.2
102
03/12/21 22:17
Dissolved Cobalt
pg/L
51.3
103
03/12/21 22:17
Dissolved Copper
pg/L
52.3
105
03/12/21 22:17
Dissolved Lead
pg/L
51.1
102
03/12/21 22:17
Dissolved Nickel
pg/L
52.6
105
03/12/21 22:17
Dissolved Selenium
pg/L
49.5
99.0
03/12/21 22:17
Dissolved Silver
pg/L
51.4
103
03/12/21 22:17
Dissolved Thallium
pg/L
50.2
100
03/12/21 22:17
Dissolved Vanadium
pg/L
51.6
103
03/12/21 22:17
Dissolved Zinc
pg/L
52.4
105
03/12/21 22:17
Date: 03/31/2021 12:59 PM Page 16 of 27
Page 54 of 67

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1703
QC Analytical Batch(es): V1708
QC Prep Batch Method: 7470A
Analysis Method:
7470A
Analysis Description:
Total Aqueous Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V1703
Matrix: AQU
Associated Lab Samples: 94376
Blank MDL
MQL
Analyzed
Parameter Units
Result
Dissolved Mercury pg/L
0.000 0.000
0.200
03/15/21 13:22
Laboratory Control Sample
LCS-V1703
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Dissolved Mercury pg/L
9.38
9.09
97.0 80-120
Matrix Spike & Matrix Spike Duplicate
V 92809-V1666-MS-V1703 V 92809-V1666-MSD-V1703
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Dissolved Mercury pg/L
<0.0300 9.38
9.38 9.06
9.05 97.0 97.0 80-120 0.1 20
Date: 03/31/2021 12:59 PM Page 17 of 27
Page 55 of 67

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1728
QC Analytical Batch(es): V1842
QC Prep Batch Method: 7470A
Analysis Method:
7470A
Analysis Description:
Total Aqueous Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V1728
Matrix: AQU
Associated Lab Samples: 94374, 94375, 94376, 94377, 94378, 94379
Blank MDL
MQL
Analyzed
Parameter Units
Result
Mercury (Total) pg/L
<0.0300 0.0300
0.200
03/16/21 13:16
Laboratory Control Sample
LCS-V1728
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Mercury (Total) pg/L
9.38
8.96
96.0 80-120
Matrix Spike & Matrix Spike Duplicate
V 94374-MS-V1728
V 94374-MSD-V1728
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Mercury (Total) pg/L
<0.0300 9.38
9.38 8.91
8.85 95.0 94.0 80-120 0.6 20
Post Digestion Spike
V 94374-PDS-V1728
PDS
%
Analyzed
Parameter Units
Result
Recovery
Mercury (Total) pg/L
4.39
94.0
03/16/21 13:35
Date: 03/31/2021 12:59 PM Page 18 of 27
Page 56 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Prep:
V1583
QC Analytical Batch(es): V1584
QC Prep Batch Method:
5030B
Analysis Method:
8260D SIM
Analysis Description:
Volatile Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-V1583
Matrix: AQU
Associated Lab Samples:
94374, 94375, 94376, 94377, 94378, 94379
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
1,4-Dioxane
pg/L
<0.139 0.139
2.00
03/11/2116:11
4-Bromofluorobenzene (S)
03/11/21 16:11
109
70-130
Laboratory Control Sample
LCS-V1583
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
1,4-Dioxane
pg/L
50.0
47.4
94.8
70-130
4-Bromofluorobenzene (S)
115
70-130
Matrix Spike & Matrix Spike Duplicate
V 94374-MS-V1583
V 94374-MSD-V1583
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD
Conc.
1,4-Dioxane
pg/L
< 0.139 50.0
50.0 50.4
51.3 101
103
70-130
4-Bromofluorobenzene (S)
108
107
70-130
Date: 03/31/2021 12:59 PM Page 19 of 27
Page 57 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1700
QC Prep Batch Method: 5030B
QC Analytical Batch(es): V1702
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V1700 Matrix: AQU
Associated Lab Samples: 94374, 94375, 94376, 94377, 94378, 94379, 94380
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
pg/L
<0.310
0.310
5.00
03/13/21 14:40
Acrylonitrile
pg/L
<0.200
0.200
20.0
03/13/21 14:40
Benzene
pg/L
<0.048
0.048
0.500
03/13/21 14:40
Bromochloromethane
pg/L
<0.140
0.140
0.500
03/13/21 14:40
Bromodichloromethane
pg/L
<0.062
0.062
0.500
03/13/21 14:40
Bromoform
pg/L
<0.040
0.040
1.00
03/13/21 14:40
Bromomethane
pg/L
<0.180
0.180
1.00
03/13/21 14:40
Carbon Disulfide
pg/L
<0.075
0.075
5.00
03/13/21 14:40
Carbon Tetrachloride
pg/L
<0.110
0.110
0.500
03/13/21 14:40
Chlorobenzene
pg/L
<0.062
0.062
0.500
03/13/21 14:40
Chlorodibromomethane
pg/L
<0.081
0.081
0.500
03/13/21 14:40
Chloroethane
pg/L
<0.220
0.220
0.500
03/13/21 14:40
Chloroform
pg/L
<0.076
0.076
0.500
03/13/21 14:40
Chloromethane
pg/L
<0.079
0.079
0.500
03/13/21 14:40
Di -Isopropyl Ether (DIPE)
pg/L
<0.960
0.960
5.00
03/13/21 14:40
1,2-Dibromo-3-Chloropropane
pg/L
<0.170
0.170
2.00
03/13/21 14:40
1,2-Dibromoethane
pg/L
<0.051
0.051
0.500
03/13/21 14:40
Dibromomethane
pg/L
<0.065
0.065
0.500
03/13/21 14:40
trans-1,4-Dichloro-2-butene
pg/L
<0.120
0.120
10.0
03/13/21 14:40
1,2-Dichlorobenzene
pg/L
<0.076
0.076
0.500
03/13/21 14:40
1,4-Dichlorobenzene
pg/L
<0.050
0.050
0.500
03/13/21 14:40
Dichlorodifluoromethane
pg/L
<0.110
0.110
5.00
03/13/21 14:40
1,1-Dichloroethane
pg/L
<0.083
0.083
0.500
03/13/21 14:40
1,2-Dichloroethane
pg/L
<0.066
0.066
0.500
03/13/21 14:40
1,1-Dichloroethene
pg/L
<0.083
0.083
0.500
03/13/21 14:40
cis-1,2-Dichloroethene
pg/L
<0.056
0.056
0.500
03/13/21 14:40
trans-1,2-Dichloroethene
pg/L
<0.094
0.094
0.500
03/13/21 14:40
Date:
03/31/2021 12:59 PM
Page 20 of 27
Page 58 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1700
QC Prep Batch Method: 5030B
QC Analytical Batch(es): V1702
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V1700 Matrix: AQU
Associated Lab Samples: 94374, 94375, 94376, 94377, 94378, 94379, 94380
Blank
MDL
MQL
Analyzed
% % Rec
Parameter
Units
Result
Recovery Limits
1,2-Dichloropropane
pg/L
<0.110
0.110
0.500
03/13/21 14:40
cis-1,3-Dichloropropene
pg/L
<0.079
0.079
0.500
03/13/21 14:40
trans-1,3-Dichloropropene
pg/L
<0.070
0.070
0.500
03/13/21 14:40
1,4-Dioxane
pg/L
<14.0
14.0
150
03/13/21 14:40
Ethylbenzene
pg/L
<0.061
0.061
0.500
03/13/21 14:40
2-Hexanone
pg/L
<0.065
0.065
5.00
03/13/21 14:40
Methyl Ethyl Ketone (MEK)
pg/L
<0.240
0.240
5.00
03/13/21 14:40
4-Methyl-2-Pentanone
pg/L
<1.00
1.00
5.00
03/13/21 14:40
Methylene Chloride
pg/L
<0.083
0.083
1.00
03/13/21 14:40
Styrene
pg/L
<0.047
0.047
0.500
03/13/21 14:40
1,1,1,2-Tetrachloroethane
pg/L
<0.110
0.110
0.500
03/13/21 14:40
1,1,2,2-Tetrachloroethane
pg/L
<0.036
0.036
0.500
03/13/21 14:40
Tetrachloroethene
pg/L
<0.098
0.098
0.500
03/13/21 14:40
Tetrahydrofuran
pg/L
<1.10
1.10
10.0
03/13/21 14:40
Toluene
pg/L
<0.044
0.044
0.500
03/13/21 14:40
1,1,1-Trichloroethane
pg/L
<0.061
0.061
0.500
03/13/21 14:40
1,1,2-Trichloroethane
pg/L
<0.066
0.066
0.500
03/13/21 14:40
Trichloroethene
pg/L
<0.078
0.078
0.500
03/13/21 14:40
Trichlorofluoromethane
pg/L
<0.062
0.062
0.500
03/13/21 14:40
1,2,3-Trichloropropane
pg/L
<0.140
0.140
1.00
03/13/21 14:40
Vinyl Acetate
pg/L
<0.060
0.060
2.00
03/13/21 14:40
Vinyl Chloride
pg/L
<0.097
0.097
0.500
03/13/21 14:40
o-Xylene
pg/L
<0.044
0.044
0.500
03/13/21 14:40
m,p-Xylene
pg/L
<0.120
0.120
1.00
03/13/21 14:40
4-Bromofluorobenzene (S)
03/13/21 14:40
92.6 80-124
Dibromofluoromethane (S)
03/13/21 14:40
109 75-129
1,2-Dichloroethane - d4 (S)
03/13/21 14:40
108 63-136
Date:
03/31/2021 12:59 PM
Page 21 of 27
Page 59 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Prep:
V1700
QC Analytical Batch(es): V1702
QC Prep Batch Method:
5030B
Analysis Method:
8260D
Analysis Description:
Volatile
Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V1700
Matrix: AQU
Associated Lab Samples:
94374, 94375, 94376, 94377, 94378, 94379, 94380
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Toluene-d8 (S)
03/13/21 14:40
100
77-123
Laboratory Control Sample
& LCSD
LCS-V1700 LCSD-V1700
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
a/o Rec
Limits
RPD
Max
RPD
Acetone
pg/L
40.0
42.6
44.8
107
112
40-166
5.0
20.0
Acrylonitrile
pg/L
40.0
42.1
41.2
105
103
81-127
2.1
20.0
Benzene
pg/L
20.0
22.3
21.2
112
106
77-128
5.0
20.0
Bromochloromethane
pg/L
20.0
22.8
22.5
114
113
78-135
1.3
20.0
Bromodichloromethane
pg/L
20.0
22.1
20.9
111
105
76-138
5.5
20.0
Bromoform
pg/L
20.0
19.8
20.1
99.0
101
71-135
1.5
20.0
Bromomethane
pg/L
20.0
20.1
18.5
101
92.5
41-168
8.2
20.0
Carbon Disulfide
pg/L
20.0
23.8
22.8
119
114
59-135
4.2
20.0
Carbon Tetrachloride
pg/L
20.0
21.3
19.9
107
99.5
72-142
6.7
20.0
Chlorobenzene
pg/L
20.0
21.0
20.5
105
103
78-119
2.4
20.0
Chlorodibromomethane
pg/L
20.0
19.7
19.9
98.5
99.5
75-134
1.0
20.0
Chloroethane
pg/L
20.0
23.3
21.7
117
109
57-142
7.1
20.0
Chloroform
pg/L
20.0
22.7
20.6
114
103
77-130
9.6
20.0
Chloromethane
pg/L
20.0
24.8
23.8
124
119
47-145
4.1
20.0
Di -Isopropyl Ether (DIPE)
pg/L
20.0
22.5
21.6
113
108
60-154
4.0
20.0
1,2-Dibromo-3-Chloropropane pg/L
20.0
18.3
17.9
91.5
89.5
63-134
2.2
20.0
1,2-Dibromoethane
pg/L
20.0
21.2
20.7
106
104
77-135
2.3
20.0
Dibromomethane
pg/L
20.0
22.7
21.8
114
109
76-138
4.0
20.0
trans-1,4-Dichloro-2-butene
pg/L
20.0
18.5
18.9
92.5
94.5
70-130
2.1
20.0
1,2-Dichlorobenzene
pg/L
20.0
20.7
20.2
104
101
78-128
2.4
20.0
1,4-Dichlorobenzene
pg/L
20.0
21.1
20.1
106
101
75-126
4.8
20.0
Date: 03/31/2021 12:59 PM Page 22 of 27
Page 60 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-069-0019
QC Prep: V1700 QC Analytical Batch(es): V1702
QC Prep Batch Method: 5030B Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V1700 LCSD-V1700
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Dichlorodifluoromethane
pg/L
20.0
25.7
23.6
129
118
28-163
8.5
20.0
1,1-Dichloroethane
pg/L
20.0
22.8
21.6
114
108
70-130
5.4
20.0
1,2-Dichloroethane
pg/L
20.0
21.9
20.5
110
103
68-131
6.6
20.0
1,1-Dichloroethene
pg/L
20.0
22.5
21.5
113
108
70-154
4.5
20.0
cis-1,2-Dichloroethene
pg/L
20.0
22.4
21.8
112
109
76-141
2.7
20.0
trans-1,2-Dichloroethene
pg/L
20.0
22.5
21.2
113
106
76-135
5.9
20.0
1,2-Dichloropropane
pg/L
20.0
22.7
21.9
114
110
77-130
3.5
20.0
cis-1,3-Dichloropropene
pg/L
20.0
20.3
19.6
102
98.0
65-140
3.5
20.0
trans-1,3-Dichloropropene
pg/L
20.0
19.3
18.2
96.5
91.0
67-140
5.8
20.0
1,4-Dioxane
pg/L
200
144
110
0.0*
0.0*
70-130
0.0
20.0
Ethylbenzene
pg/L
20.0
21.4
20.5
107
103
80-127
4.2
20.0
2-Hexanone
pg/L
20.0
18.9
18.8
94.5
94.0
64-137
0.5
20.0
Methyl Ethyl Ketone (MEK)
pg/L
20.0
19.1
19.6
95.5
98.0
71-134
2.5
20.0
4-Methyl-2-Pentanone
pg/L
20.0
20.8
20.2
104
101
69-134
2.9
20.0
Methylene Chloride
pg/L
20.0
23.9
23.2
120
116
73-131
2.9
20.0
Styrene
pg/L
20.0
21.1
20.6
106
103
78-129
2.3
20.0
1,1,1,2-Tetrachloroethane
pg/L
20.0
20.3
19.4
102
97.0
79-134
4.5
20.0
1,1,2,2-Tetrachloroethane
pg/L
20.0
21.9
21.2
110
106
62-127
3.2
20.0
Tetrachloroethene
pg/L
20.0
20.8
19.9
104
99.5
80-129
4.4
20.0
Tetrahydrofuran
pg/L
20.0
22.8
21.0
114
105
70-130
8.2
20.0
Toluene
pg/L
20.0
22.5
21.1
113
106
76-131
6.4
20.0
1,1,1-Trichloroethane
pg/L
20.0
21.1
19.8
106
99.0
75-135
6.3
20.0
1,1,2-Trichloroethane
pg/L
20.0
22.2
21.7
111
109
70-140
2.2
20.0
Trichloroethene
pg/L
20.0
20.6
19.3
103
96.5
77-133
6.5
20.0
Trichlorofluoromethane
pg/L
20.0
22.5
20.7
113
104
62-148
8.3
20.0
1,2,3-Trichloropropane
pg/L
20.0
20.8
20.5
104
103
71-127
1.4
20.0
* QC Fail Date: 03/31/2021 12:59 PM Page 23 of 27
Page 61 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Prep:
V1700
QC Analytical Batch(es): V1702
QC Prep Batch Method:
5030B
Analysis Method:
8260D
Analysis Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V1700 LCSD-V1700
Spike
LCS LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec
% Rec
Limits
RPD
Max
RPD
Vinyl Acetate
pg/L
20.0
16.1 15.1
80.5
75.5
34-167
6.4
20.0
Vinyl Chloride
pg/L
20.0
23.3 21.6
117
108
57-141
7.5
20.0
o-Xylene
pg/L
20.0
20.4 19.6
102
98.0
78-128
4.0
20.0
m,p-Xylene
pg/L
40.0
42.6 41.1
107
103
77-133
3.5
20.0
4-Bromofluorobenzene (S)
95.8
93.2
80-124
Dibromofluoromethane (S)
110
104
75-129
1,2-Dichloroethane - d4 (S)
107
104
63-136
Toluene-d8(S)
103
101
77-123
Date: 03/31/2021 12:59 PM Page 24 of 27
Page 62 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Prep:
V1571
QC Analytical Batch(es): V1597
QC Prep Batch Method:
SW-9056A (PREP)
Analysis Method:
9056A
Analysis Description:
Anions by Ion Chromatography
Lab Reagent Blank
LRB-V1571
Matrix: AQU
Associated Lab Samples:
94374, 94375, 94376, 94377
Blank MDL
MQL
Analyzed
Parameter
Units
Result
Chloride
pg/L
<350 350
1000
03/10/21 22:27
Nitrate (NO3-N)
pg/L
46.0 45.0
200
03/10/21 22:27
Sulfate
pg/L
<560 560
2000
03/10/21 22:27
Laboratory Control Sample
LCS-V1571
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Chloride
pg/L
40000
39000
98.0
90-110
Nitrate (NO3-N)
pg/L
4000
3840
96.0
90-110
Sulfate
pg/L
40000
41900
105
90-110
Matrix Spike & Matrix Spike Duplicate
V 94371-MS-V1571
V 94371-MSD-V1571
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD RPD
Conc.
Chloride
pg/L
23400 40000
40000 63000
62300 99.0
97.0
90-110 1.1 20
Matrix Spike & Matrix Spike Duplicate
V 94377-MS-V1571
V 94377-MSD-V1571
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD RPD
Conc.
Chloride
pg/L
82500 40000
40000 121000
122000 96.0
99.0
90-110 0.8 20
Nitrate (NO3-N)
pg/L
<45.0 4000
4000 3870
3910 97.0
98.0
90-110 1.0 20
Date: 03/31/2021 12:59 PM Page 25 of 27
Page 63 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Prep:
V1571
QC Analytical Batch(es): V1597
QC Prep Batch Method:
SW-9056A (PREP)
Analysis Method:
9056A
Analysis Description:
Anions
by Ion Chromatography
Matrix Spike & Matrix Spike
Duplicate
V 94371-MS-V1571
V 94371-MSD-V1571
MS Spike
MSD MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Nitrate(NO3-N)
pg/L
5560 4000
4000 9500
9520
99.0
99.0
90-110
0.2
20
Matrix Spike & Matrix Spike Duplicate
V 94377-MS-V1571
V 94377-MSD-V1571
MS Spike
MSD MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Sulfate
pg/L
27300 40000
40000 67700
67900
101
102
90-110
0.2
20
Matrix Spike & Matrix Spike
Duplicate
V 94371-MS-V1571
V 94371-MSD-V1571
MS Spike
MSD MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Sulfate
pg/L
12900 40000
40000 50900
50400
95.0
94.0
90-110
0.9
20
Date: 03/31/2021 12:59 PM Page 26 of 27
Page 64 of 67

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-069-0019
QC Analytical Batch:
V1600
Analysis Method:
SM-3500-Fe-13
Analysis Description:
Ferrous Iron
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
94374, 94375, 94376, 94377
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Ferrous Iron
pg/L
<50.0
50.0
200
03/12/21 12:15
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Ferrous Iron
pg/L
2000
2050
103
90-110
Matrix Spike & Matrix Spike Duplicate
V 94374-MS V 94374-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result
Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Ferrous Iron
pg/L
<50.0
2000
2000 1980
2000 99.0
100 80-120 1.0 20
Date: 03/31/2021 12:59 PM Page 27 of 27
Page 65 of 67

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01015
Customer Name: Anchor QEA of North Carolina, PLLC
Report Number: 21-069-0019
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
® Other :
Thermometer ID:
CK
IRT-15 1.00
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
2
Custody seals intact on shipping container/cooler?
0 Yes
0 No
I* Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
I* Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
® Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
* N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Talon J Yelton Date & Time: 03/10/2021 12:34:37
Page 66 of 67

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Page 67 of 67

Waypointo
ANALYTICAL
3/31 /2021
Anchor QEA of North Carolina, PLLC
Chuck Pippen
231 Haywood Street
Asheville, NC, 28801
Ref: Analytical Testing
Lab Report Number: 21-070-0007
Client Project Description: Jackson County LF
Site: 58-02
Project Number: 58-02
Dear Chuck Pippen:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/11/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a,j
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 58

0
Waypoint.
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2021
North Carolina
State Program
402
12/31/2021
South Carolina
State Program
99012
07/31/2021
South Carolina
State Program
99012
12/31/2020
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2022
Arkansas
State Program
88-0650
02/07/2022
California
State Program
2904
06/30/2021
Florida
State Program
- NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program
- NELAP
200078
10/10/2021
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2021
Louisiana
State Program
- NELAP
LA037
12/31/2021
Louisiana
State Program
- NELAP
04015
06/30/2021
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2021
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21-A ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
09/30/2021
Virginia
State Program
00106
06/30/2021
Virginia
State Program
- NELAP
460181
09/14/2021
Page 1 of 1 00016/21-070-0007
Page 2 of 58

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 21-070-0007
Client Project Description: Jackson County LF
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
94462
MW-01-20210310
Aqueous
03/10/2021
13:38
03/11/2021
09:35
94462
MW-01-20210310
Aqueous
03/10/2021
13:38
03/11/2021
09:35
531OC-2011 WP MTN
94463
MW-02-20210310
Aqueous
03/10/2021
14:15
03/11/2021
09:35
94463
MW-02-20210310
Aqueous
03/10/2021
14:15
03/11/2021
09:35
531OC-2011 WP MTN
94464
MW-06-20210310
Aqueous
03/10/2021
11:16
03/11/2021
09:35
94464
MW-06-20210310
Aqueous
03/10/2021
11:16
03/11/2021
09:35
531OC-2011 WP MTN
94465
LT-01-20210310
Aqueous
03/10/2021
13:50
03/11/2021
09:35
94466
DW-01-20210310
Aqueous
03/10/2021
14:55
03/11/2021
09:35
524.2
94467
TB-202103100000
Aqueous
03/10/2021
12:00
03/11/2021
09:35
: Pace Analytical - Huntersville, NC, Huntersville, NC
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 58

Waypoint.(2)
ANALYTICAL
Project: Jackson County LF
Report Number: 21-070-0007
Client Sample ID Lab Sample ID
Method Parameters
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Summary of Detected
Result Units Report Limit Analyzed
MW-01-20210310
V 94462
2320B-2011
Alkalinity (as CaCO3)
99000
pq/L
800
03/19/2021
13:40
2340C-2011
Hardness
48000
Ng/L
1140
03/18/2021
11:20
5310C-2011
TOC
1.14
mq/L
0.500
03/16/202123:49
6020B
Barium
109
Ng/L
0.810
03/13/202102:06
6020B
Cobalt
146
uq/L
0.520
03/13/202102:06
6020B
Nickel
16.0
Ng/L
0.510
03/13/202102:06
6020B
Zinc
23.9
uq/L
6.90
03/13/202102:06
8260D
Benzene
1.07
pq/L
0.048
03/13/202119:47
8260D
Chlorobenzene
1.45
uq/L
0.062
03/13/202119:47
8260D
1,4-Dichlorobenzene
9.33
pq/L
0.050
03/13/202119:47
8260D
1,1-Dichloroethane
2.62
pq/L
0.083
03/13/202119:47
8260D
cis-1,2-Dichloroethene
3.82
Ng/L
0.056
03/13/202119:47
8260D
Trichloroethene
0.545
pq/L
0.078
03/13/202119:47
9056A
Chloride
1110
Ng/L
350
03/11/202115:03
SM-3500-Fe-13
Ferrous Iron
38900
pq/L
1250
03/12/2021
12:15
MW-02-20210310
V 94463
2320B-2011
Alkalinity (as CaCO3)
47000
Ng/L
800
03/19/2021
13:40
2340C-2011
Hardness
69000
uq/L
1140
03/18/2021
11:20
5210B-2011
Biochemical Oxygen Demand (5-day)
4000
Ng/L
2000
03/11/2021
16:07
5310C-2011
TOC
4.96
mg/L
0.500
03/16/202116:50
6020B
Arsenic
2.57
Ng/L
0.170
03/13/202102:12
6020B
Barium
116
uq/L
0.810
03/13/202102:12
6020B
Chromium
19.8
Ng/L
0.790
03/13/202102:12
6020B
Cobalt
25.1
uq/L
0.520
03/13/202102:12
6020B
Copper
18.8
Ng/L
3.80
03/13/202102:12
6020B
Lead
4.66
uq/L
0.260
03/13/202102:12
6020B
Nickel
14.5
Ng/L
0.510
03/13/202102:12
6020B
Selenium
9.01
uq/L
0.740
03/13/202102:12
6020B
Vanadium
26.0
Ng/L
1.30
03/13/202102:12
6020B
Zinc
81.6
uq/L
6.90
03/13/202102:12
9056A
Chloride
19100
Ng/L
350
03/11/202115:19
9056A
Nitrate (NO3-N)
355
uq/L
45.0
03/11/2021
15:19
9056A
Sulfate
10400
pq/L
560
03/11/202115:19
MW-06-20210310
V 94464
2320B-2011
Alkalinity (as CaCO3)
22000
pq/L
800
03/19/2021
13:40
2340C-2011
Hardness
21000
Ng/L
1140
03/18/2021
11:20
Qualifiers
Page 4 of 58

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: Jackson County LF
Report Number: 21-070-0007
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
MW-06-20210310
V 94464
4500S2F-2011
Sulfide
6020B
Barium
6020B
Cobalt
6020B
Nickel
8260D
1,4-Dichlorobenzene
8260D
1,1-Dichloroethane
8260D
cis-1,2-Dichloroethene
LT-01-20210310
V 94465
6020B
Arsenic
6020B
Barium
6020B
Chromium
6020B
Cobalt
6020B
Nickel
8260D
Acetone
8260D
Benzene
8260D
Chlorobenzene
8260D
1,4-Dichlorobenzene
8260D
Tetra hyd rofu ra n
8260D SIM
1,4-Dioxane
39600
pq/L
830
03/15/2021
11:30
46.8
Ng/L
0.810
03/13/202102:19
12.5
uq/L
0.520
03/13/202102:19
4.19
Ng/L
0.510
03/13/202102:19
1.04
uq/L
0.050
03/13/202120:55
0.907
Ng/L
0.083
03/13/202120:55
0.781
pg/L
0.056
03/13/202120:55
2.90
Ng/L
0.170
03/13/202102:25
360
uq/L
0.810
03/13/202102:25
2.99
Ng/L
0.790
03/13/202102:25
3.97
uq/L
0.520
03/13/202102:25
23.6
Ng/L
0.510
03/13/202102:25
20.2
uq/L
0.310
03/13/202121:29
1.49
Ng/L
0.048
03/13/202121:29
3.13
uq/L
0.062
03/13/202121:29
3.44
Ng/L
0.050
03/13/202121:29
82.9
uq/L
1.10
03/13/202121:29
55.5
Ng/L
0.139
03/11/202120:23
Page 5 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
REPORT OF ANAL YSIS
Lab No : 94462
Matrix: Aqueous
Sample ID: MW-01-20210310
Sampled:
3/10/2021 13:38
Ferrous Iron
38900
Ng/L
1250
5000
1
03/12/21 12:15
ENM
Hardness
48000
ug/L
1140
10000
1
03/18/21 11:20
SLS
1,4-Dioxane
<2.00
Ng/L
0.139
2.00
1
03/11/21 19:07
TBL
Surrogate:4-Bromofluorobenzene
101
Limits:70-130%
1 03/11/2119:07 TBL
V1584
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
99000
ug/L
800
5000
1
03/19/21 13:40
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
<2000
Ng/L
2000
2000
1
03/11/21 16:07
ENM
521OB-2011
Chloride
1110
ug/L
350
1000
1
03/11/2115:03
NMB
9056A
COD (Chemical Oxygen Demand)
<50000
Ng/L
11000
50000
1
03/16/21 11:30
SLS
5220D-2011
Nitrate (NO3-N)
<200
ug/L
45.0
200
1
03/11/21 15:03
NMB
9056A
TOC
1.14
mg/L
0.500
1.00
1
03/16/2123:49
DDB
531OC-2011
Sulfate
<2000
ug/L
560
2000
1
03/11/2115:03
NMB
9056A
Sulfide
<2000
Ng/L
830
2000
1
03/15/2111:30
ENM
4500S2F-2011
Antimony
<2.00
ug/L
0.490
2.00
1
03/13/2102:06
MMR
6020B
Arsenic
<1.00
Ng/L
0.170
1.00
1
03/13/2102:06
MMR
6020B
Barium
109
ug/L
0.810
10.0
1
03/13/2102:06
MMR
6020B
Beryllium
<1.00
Ng/L
0.190
1.00
1
03/13/2102:06
MMR
6020B
Cadmium
<1.00
ug/L
0.160
1.00
1
03/13/2102:06
MMR
6020B
Chromium
<2.00
Ng/L
0.790
2.00
1
03/13/2102:06
MMR
6020B
Cobalt
146
ug/L
0.520
2.00
1
03/13/2102:06
MMR
6020B
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 6 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94462 Matrix: Aqueous
Sample ID: MW-01-20210310 Sampled: 3/10/2021 13:38
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Copper
<10.0
N9/L
3.80
10.0
1
03/13/2102:06
MMR
6020B
Lead
<1.00
u9/L
0.260
1.00
1
03/13/2102:06
MMR
6020B
Mercury (Total)
<0.200
Ng/L
0.0300
0.200
1
03/16/21 14:09
EDV
7470A
Nickel
16.0
u9/L
0.510
3.00
1
03/13/2102:06
MMR
6020B
Selenium
<5.00
N9/L
0.740
5.00
1
03/13/2102:06
MMR
6020B
Silver
<1.00
u9/L
0.110
1.00
1
03/13/2102:06
MMR
6020B
Thallium
<2.00
N9/L
0.570
2.00
1
03/13/2102:06
MMR
6020B
Vanadium
<5.00
u9/L
1.30
5.00
1
03/13/2102:06
MMR
6020B
Zinc
23.9
Ng/L
6.90
20.0
1
03/13/2102:06
MMR
6020E
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 7 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94462
Matrix: Aqueous
Sample ID: MW-01-20210310
Sampled:
3/10/2021
13:38
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<5.00
Ng/L
0.310
5.00
1
03/13/21 19:47
JLB
V1702
Acrylonitrile
<20.0
u9/L
0.200
20.0
1
03/13/21 19:47
JLB
V1702
Benzene
1.07
N9/L
0.048
0.500
1
03/13/21 19:47
JLB
V1702
Bromochloromethane
<0.500
u9/L
0.140
0.500
1
03/13/21 19:47
JLB
V1702
Bromodichloromethane
<0.500
N9/L
0.062
0.500
1
03/13/21 19:47
JLB
V1702
Bromoform
<1.00
u9/L
0.040
1.00
1
03/13/21 19:47
JLB
V1702
Bromomethane
<1.00
N9/L
0.180
1.00
1
03/13/21 19:47
JLB
V1702
Carbon Disulfide
<5.00
u9/L
0.075
5.00
1
03/13/21 19:47
JLB
V1702
Carbon Tetrachloride
<0.500
N9/L
0.110
0.500
1
03/13/21 19:47
JLB
V1702
Chlorobenzene
1.45
u9/L
0.062
0.500
1
03/13/21 19:47
JLB
V1702
Chlorodibromomethane
<0.500
N9/L
0.081
0.500
1
03/13/21 19:47
JLB
V1702
Chloroethane
<0.500
u9/L
0.220
0.500
1
03/13/21 19:47
JLB
V1702
Chloroform
<0.500
N9/L
0.076
0.500
1
03/13/21 19:47
JLB
V1702
Chloromethane
<0.500
u9/L
0.079
0.500
1
03/13/21 19:47
JLB
V1702
Di -Isopropyl Ether (DIPE)
<5.00
N9/L
0.960
5.00
1
03/13/21 19:47
JLB
V1702
1,2-Dibromo-3-Chloropropane
<2.00
u9/L
0.170
2.00
1
03/13/21 19:47
JLB
V1702
1,2-Dibromoethane
<0.500
N9/L
0.051
0.500
1
03/13/21 19:47
JLB
V1702
Dibromomethane
<0.500
pg/L
0.065
0.500
1
03/13/21 19:47
JLB
V1702
trans-1,4-Dichloro-2-butene
<10.0
N9/L
0.120
10.0
1
03/13/21 19:47
JLB
V1702
1,2-Dichlorobenzene
<0.500
pg/L
0.076
0.500
1
03/13/21 19:47
JLB
V1702
1,4-Dichlorobenzene
9.33
N9/L
0.050
0.500
1
03/13/21 19:47
JLB
V1702
Dichlorodifluoromethane
<5.00
pg/L
0.110
5.00
1
03/13/21 19:47
JLB
V1702
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 8 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94462
Matrix: Aqueous
Sample ID: MW-01-20210310
Sampled:
3/10/2021
13:38
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,1-Dichloroethane
2.62
Ng/L
0.083
0.500
1
03/13/21 19:47
JLB
V1702
1,2-Dichloroethane
<0.500
pg/L
0.066
0.500
1
03/13/21 19:47
JLB
V1702
1,1-Dichloroethene
<0.500
N9/L
0.083
0.500
1
03/13/21 19:47
JLB
V1702
cis- 1,2-Dich loroethene
3.82
p9/L
0.056
0.500
1
03/13/21 19:47
JLB
V1702
trans-1,2-Dichloroethene
<0.500
N9/L
0.094
0.500
1
03/13/21 19:47
JLB
V1702
1,2-Dichloropropane
<0.500
pg/L
0.110
0.500
1
03/13/21 19:47
JLB
V1702
cis- 1,3-Dich loropropene
<0.500
N9/L
0.079
0.500
1
03/13/21 19:47
JLB
V1702
trans-1,3-Dichloropropene
<0.500
pg/L
0.070
0.500
1
03/13/21 19:47
JLB
V1702
1,4-Dioxane
<150
N9/L
14.0
150
1
03/13/21 19:47
JLB
V1702
Ethylbenzene
<0.500
pg/L
0.061
0.500
1
03/13/21 19:47
JLB
V1702
2-Hexanone
<5.00
N9/L
0.065
5.00
1
03/13/21 19:47
JLB
V1702
Methyl Ethyl Ketone (MEK)
<5.00
pg/L
0.240
5.00
1
03/13/21 19:47
JLB
V1702
4-Methyl-2-Pentanone
<5.00
N9/L
1.00
5.00
1
03/13/21 19:47
JLB
V1702
Methylene Chloride
<1.00
pg/L
0.083
1.00
1
03/13/21 19:47
JLB
V1702
Styrene
<0.500
N9/L
0.047
0.500
1
03/13/21 19:47
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.500
pg/L
0.110
0.500
1
03/13/21 19:47
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.500
N9/L
0.036
0.500
1
03/13/21 19:47
JLB
V1702
Tetrachloroethene
<0.500
pg/L
0.098
0.500
1
03/13/21 19:47
JLB
V1702
Tetrahydrofuran
<10.0
N9/L
1.10
10.0
1
03/13/21 19:47
JLB
V1702
Toluene
<0.500
pg/L
0.044
0.500
1
03/13/21 19:47
JLB
V1702
1, 1, 1-Trichloroethane
<0.500
N9/L
0.061
0.500
1
03/13/21 19:47
JLB
V1702
1,1,2-Trichloroethane
<0.500
pg/L
0.066
0.500
1
03/13/21 19:47
JLB
V1702
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 9 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
Lab No : 94462
Sample ID: MW-01-20210310
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 3/10/2021 13:38
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Trichloroethene
0.545
Ng/L
0.078
0.500
1
03/13/21 19:47 JLB
V1702
Trichlorofluoromethane
<0.500
ug/L
0.062
0.500
1
03/13/21 19:47 JLB
V1702
1,2,3-Trichloropropane
<1.00
Ng/L
0.140
1.00
1
03/13/21 19:47 JLB
V1702
Vinyl Acetate
<2.00
ug/L
0.060
2.00
1
03/13/21 19:47 JLB
V1702
Vinyl Chloride
<0.500
Ng/L
0.097
0.500
1
03/13/21 19:47 JLB
V1702
o-Xylene
<0.500
ug/L
0.044
0.500
1
03/13/21 19:47 JLB
V1702
m,p-Xylene
<1.00
Ng/L
0.120
1.00
1
03/13/21 19:47 JLB
V1702
Xylene (Total)
<0.500
ug/L
0.500
1
03/13/21 19:47
V1702
Surrogate:4-Bromofluorobenzene
96.4
Limits:80-124%
1 03/13/21 19:47 JLB
V1702
Surrogate: Dibromofluoromethane
105
Limits:
75-129%
1 03/13/21 19:47 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
105
Limits:
63-136%
1 03/13/21 19:47 JLB
V1702
Surrogate: Toluene-d8
100
Limits:
77-123%
1 03/13/21 19:47 JLB
V1702
Qualifiers/ DF Dilution Factor J Estimated value
Definitions MQL Method Quantitation Limit
Page 10 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
REPORT OF ANAL YSIS
Lab No : 94463
Matrix: Aqueous
Sample ID: MW-02-20210310
Sampled:
3/10/2021 14:15
Ferrous Iron
<200
Ng/L
50.0
200
1
03/12/21 12:15
ENM
Hardness
69000
ug/L
1140
10000
1
03/18/21 11:20
SLS
1,4-Dioxane
<2.00
Ng/L
0.139
2.00
1
03/11/21 19:32
TBL
Surrogate:4-Bromofluorobenzene
105
Limits:70-130%
1 03/11/2119:32 TBL
V1584
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
47000
ug/L
800
5000
1
03/19/21 13:40
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
4000
Ng/L
2000
2000
1
03/11/21 16:07
ENM
521OB-2011
Chloride
19100
ug/L
350
1000
1
03/11/2115:19
NMB
9056A
COD (Chemical Oxygen Demand)
<50000
Ng/L
11000
50000
1
03/16/21 11:30
SLS
5220D-2011
Nitrate (NO3-N)
355
ug/L
45.0
200
1
03/11/21 15:19
NMB
9056A
TOC
4.96
mg/L
0.500
1.00
1
03/16/2116:50
DDB
531OC-2011
Sulfate
10400
ug/L
560
2000
1
03/11/2115:19
NMB
9056A
Sulfide
<2000
Ng/L
830
2000
1
03/15/2111:30
ENM
4500S2F-2011
Antimony
<2.00
ug/L
0.490
2.00
1
03/13/2102:12
MMR
6020B
Arsenic
2.57
Ng/L
0.170
1.00
1
03/13/2102:12
MMR
6020E
Barium
116
ug/L
0.810
10.0
1
03/13/2102:12
MMR
6020B
Beryllium
<1.00
Ng/L
0.190
1.00
1
03/13/2102:12
MMR
6020B
Cadmium
<1.00
ug/L
0.160
1.00
1
03/13/2102:12
MMR
6020B
Chromium
19.8
Ng/L
0.790
2.00
1
03/13/2102:12
MMR
6020E
Cobalt
25.1
ug/L
0.520
2.00
1
03/13/2102:12
MMR
6020B
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 11 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94463 Matrix: Aqueous
Sample ID: MW-02-20210310 Sampled: 3/10/2021 14:15
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Copper
18.8
Ng/L
3.80
10.0
1
03/13/2102:12
MMR
6020E
Lead
4.66
ug/L
0.260
1.00
1
03/13/2102:12
MMR
6020B
Mercury (Total)
<0.200
Ng/L
0.0300
0.200
1
03/16/21 14:41
EDV
7470A
Nickel
14.5
ug/L
0.510
3.00
1
03/13/2102:12
MMR
6020B
Selenium
9.01
Ng/L
0.740
5.00
1
03/13/2102:12
MMR
6020E
Silver
<1.00
ug/L
0.110
1.00
1
03/13/2102:12
MMR
6020B
Thallium
<2.00
N9/L
0.570
2.00
1
03/13/2102:12
MMR
6020B
Vanadium
26.0
u9/L
1.30
5.00
1
03/13/2102:12
MMR
6020B
Zinc
81.6
Ng/L
6.90
20.0
1
03/13/2102:12
MMR
6020E
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 12 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94463
Matrix: Aqueous
Sample ID: MW-02-20210310
Sampled:
3/10/2021
14:15
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<5.00
Ng/L
0.310
5.00
1
03/13/21 20:21
JLB
V1702
Acrylonitrile
<20.0
u9/L
0.200
20.0
1
03/13/21 20:21
JLB
V1702
Benzene
<0.500
N9/L
0.048
0.500
1
03/13/21 20:21
JLB
V1702
Bromochloromethane
<0.500
u9/L
0.140
0.500
1
03/13/21 20:21
JLB
V1702
Bromodichloromethane
<0.500
N9/L
0.062
0.500
1
03/13/21 20:21
JLB
V1702
Bromoform
<1.00
u9/L
0.040
1.00
1
03/13/21 20:21
JLB
V1702
Bromomethane
<1.00
N9/L
0.180
1.00
1
03/13/21 20:21
JLB
V1702
Carbon Disulfide
<5.00
u9/L
0.075
5.00
1
03/13/21 20:21
JLB
V1702
Carbon Tetrachloride
<0.500
N9/L
0.110
0.500
1
03/13/21 20:21
JLB
V1702
Chlorobenzene
<0.500
u9/L
0.062
0.500
1
03/13/21 20:21
JLB
V1702
Chlorodibromomethane
<0.500
N9/L
0.081
0.500
1
03/13/21 20:21
JLB
V1702
Chloroethane
<0.500
ug/L
0.220
0.500
1
03/13/21 20:21
JLB
V1702
Chloroform
<0.500
N9/L
0.076
0.500
1
03/13/21 20:21
JLB
V1702
Chloromethane
<0.500
ug/L
0.079
0.500
1
03/13/21 20:21
JLB
V1702
Di -Isopropyl Ether (DIPE)
<5.00
N9/L
0.960
5.00
1
03/13/21 20:21
JLB
V1702
1,2-Dibromo-3-Chloropropane
<2.00
pg/L
0.170
2.00
1
03/13/21 20:21
JLB
V1702
1,2-Dibromoethane
<0.500
N9/L
0.051
0.500
1
03/13/21 20:21
JLB
V1702
Dibromomethane
<0.500
pg/L
0.065
0.500
1
03/13/21 20:21
JLB
V1702
trans-1,4-Dichloro-2-butene
<10.0
N9/L
0.120
10.0
1
03/13/21 20:21
JLB
V1702
1,2-Dichlorobenzene
<0.500
pg/L
0.076
0.500
1
03/13/21 20:21
JLB
V1702
1,4-Dichlorobenzene
<0.500
N9/L
0.050
0.500
1
03/13/21 20:21
JLB
V1702
Dichlorodifluoromethane
<5.00
pg/L
0.110
5.00
1
03/13/21 20:21
JLB
V1702
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 13 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
REPORT OF ANAL YSIS
Lab No : 94463 Matrix: Aqueous
Sample ID: MW-02-20210310 Sampled: 3/10/2021 14:15
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,1-Dichloroethane
<0.500
N9/L
0.083
0.500
1
03/13/21 20:21
JLB
V1702
1,2-Dichloroethane
<0.500
u9/L
0.066
0.500
1
03/13/21 20:21
JLB
V1702
1,1-Dichloroethene
<0.500
N9/L
0.083
0.500
1
03/13/21 20:21
JLB
V1702
cis- 1,2-Dich loroethene
<0.500
u9/L
0.056
0.500
1
03/13/21 20:21
JLB
V1702
trans-1,2-Dichloroethene
<0.500
N9/L
0.094
0.500
1
03/13/21 20:21
JLB
V1702
1,2-Dichloropropane
<0.500
u9/L
0.110
0.500
1
03/13/21 20:21
JLB
V1702
cis- 1,3-Dich loropropene
<0.500
N9/L
0.079
0.500
1
03/13/21 20:21
JLB
V1702
trans-1,3-Dichloropropene
<0.500
u9/L
0.070
0.500
1
03/13/21 20:21
JLB
V1702
1,4-Dioxane
<150
N9/L
14.0
150
1
03/13/21 20:21
JLB
V1702
Ethylbenzene
<0.500
u9/L
0.061
0.500
1
03/13/21 20:21
JLB
V1702
2-Hexanone
<5.00
N9/L
0.065
5.00
1
03/13/21 20:21
JLB
V1702
Methyl Ethyl Ketone (MEK)
<5.00
ug/L
0.240
5.00
1
03/13/21 20:21
JLB
V1702
4-Methyl-2-Pentanone
<5.00
N9/L
1.00
5.00
1
03/13/21 20:21
JLB
V1702
Methylene Chloride
<1.00
u9/L
0.083
1.00
1
03/13/21 20:21
JLB
V1702
Styrene
<0.500
N9/L
0.047
0.500
1
03/13/21 20:21
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.500
ug/L
0.110
0.500
1
03/13/21 20:21
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.500
N9/L
0.036
0.500
1
03/13/21 20:21
JLB
V1702
Tetrachloroethene
<0.500
pg/L
0.098
0.500
1
03/13/21 20:21
JLB
V1702
Tetrahydrofuran
<10.0
N9/L
1.10
10.0
1
03/13/21 20:21
JLB
V1702
Toluene
<0.500
u9/L
0.044
0.500
1
03/13/21 20:21
JLB
V1702
1, 1, 1-Trichloroethane
<0.500
N9/L
0.061
0.500
1
03/13/21 20:21
JLB
V1702
1,1,2-Trichloroethane
<0.500
u9/L
0.066
0.500
1
03/13/21 20:21
JLB
V1702
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 14 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94463 Matrix: Aqueous
Sample ID: MW-02-20210310 Sampled: 3/10/2021 14:15
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Trichloroethene
<0.500
Ng/L
0.078 0.500
1
03/13/21 20:21 JLB
V1702
Trichlorofluoromethane
<0.500
ug/L
0.062 0.500
1
03/13/21 20:21 JLB
V1702
1,2,3-Trichloropropane
<1.00
Ng/L
0.140 1.00
1
03/13/21 20:21 JLB
V1702
Vinyl Acetate
<2.00
ug/L
0.060 2.00
1
03/13/21 20:21 JLB
V1702
Vinyl Chloride
<0.500
Ng/L
0.097 0.500
1
03/13/21 20:21 JLB
V1702
o-Xylene
<0.500
ug/L
0.044 0.500
1
03/13/21 20:21 JLB
V1702
m,p-Xylene
<1.00
Ng/L
0.120 1.00
1
03/13/21 20:21 JLB
V1702
Xylene (Total)
<0.500
ug/L
0.500
1
03/13/21 20:21
V1702
Surrogate:4-Bromofluorobenzene
96.6
Limits:80-124%
1 03/13/21 20:21 JLB
V1702
Surrogate: Dibromofluoromethane
106
Limits: 75-129%
1 03/13/21 20:21 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
107
Limits: 63-136%
1 03/13/21 20:21 JLB
V1702
Surrogate: Toluene-d8
101
Limits: 77-123%
1 03/13/21 20:21 JLB
V1702
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 15 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
REPORT OF ANAL YSIS
Lab No : 94464
Matrix: Aqueous
Sample ID: MW-06-20210310
Sampled:
3/10/2021 11:16
Ferrous Iron
<200
Ng/L
50.0
200
1
03/12/21 12:15
ENM
Hardness
21000
ug/L
1140
10000
1
03/18/21 11:20
SLS
1,4-Dioxane
<2.00
Ng/L
0.139
2.00
1
03/11/21 19:58
TBL
Surrogate:4-Bromofluorobenzene
99.8
Limits:70-130%
1 03/11/2119:58 TBL
V1584
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
22000
ug/L
800
5000
1
03/19/21 13:40
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
<2000
Ng/L
2000
2000
1
03/11/21 16:07
ENM
521OB-2011
Chloride
<1000
ug/L
350
1000
1
03/11/2114:16
NMB
9056A
COD (Chemical Oxygen Demand)
<50000
Ng/L
11000
50000
1
03/16/21 11:30
SLS
5220D-2011
Nitrate (NO3-N)
<200
ug/L
45.0
200
1
03/11/21 14:16
NMB
9056A
TOC
<1.00
mg/L
0.500
1.00
1
03/16/2117:28
DDB
531OC-2011
Sulfate
<2000
ug/L
560
2000
1
03/11/2114:16
NMB
9056A
Sulfide
39600
Ng/L
830
2000
1
03/15/2111:30
ENM
4500S2F-2011
Antimony
<2.00
ug/L
0.490
2.00
1
03/13/2102:19
MMR
6020B
Arsenic
<1.00
Ng/L
0.170
1.00
1
03/13/2102:19
MMR
6020B
Barium
46.8
ug/L
0.810
10.0
1
03/13/2102:19
MMR
6020B
Beryllium
<1.00
Ng/L
0.190
1.00
1
03/13/2102:19
MMR
6020B
Cadmium
<1.00
ug/L
0.160
1.00
1
03/13/2102:19
MMR
6020B
Chromium
<2.00
Ng/L
0.790
2.00
1
03/13/2102:19
MMR
6020B
Cobalt
12.5
ug/L
0.520
2.00
1
03/13/2102:19
MMR
6020B
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 16 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94464 Matrix: Aqueous
Sample ID: MW-06-20210310 Sampled: 3/10/2021 11:16
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Copper
<10.0
N9/L
3.80
10.0
1
03/13/2102:19
MMR
6020B
Lead
<1.00
u9/L
0.260
1.00
1
03/13/2102:19
MMR
6020B
Mercury (Total)
<0.200
Ng/L
0.0300
0.200
1
03/16/21 14:45
EDV
7470A
Nickel
4.19
u9/L
0.510
3.00
1
03/13/2102:19
MMR
6020B
Selenium
<5.00
N9/L
0.740
5.00
1
03/13/2102:19
MMR
6020B
Silver
<1.00
u9/L
0.110
1.00
1
03/13/2102:19
MMR
6020B
Thallium
<2.00
N9/L
0.570
2.00
1
03/13/2102:19
MMR
6020B
Vanadium
<5.00
u9/L
1.30
5.00
1
03/13/2102:19
MMR
6020B
Zinc
<20.0
N9/L
6.90
20.0
1
03/13/2102:19
MMR
6020B
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 17 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94464
Matrix: Aqueous
Sample ID: MW-06-20210310
Sampled:
3/10/2021
11:16
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<5.00
Ng/L
0.310
5.00
1
03/13/21 20:55
JLB
V1702
Acrylonitrile
<20.0
u9/L
0.200
20.0
1
03/13/21 20:55
JLB
V1702
Benzene
<0.500
N9/L
0.048
0.500
1
03/13/21 20:55
JLB
V1702
Bromochloromethane
<0.500
u9/L
0.140
0.500
1
03/13/21 20:55
JLB
V1702
Bromodichloromethane
<0.500
N9/L
0.062
0.500
1
03/13/21 20:55
JLB
V1702
Bromoform
<1.00
u9/L
0.040
1.00
1
03/13/21 20:55
JLB
V1702
Bromomethane
<1.00
N9/L
0.180
1.00
1
03/13/21 20:55
JLB
V1702
Carbon Disulfide
<5.00
u9/L
0.075
5.00
1
03/13/21 20:55
JLB
V1702
Carbon Tetrachloride
<0.500
N9/L
0.110
0.500
1
03/13/21 20:55
JLB
V1702
Chlorobenzene
<0.500
u9/L
0.062
0.500
1
03/13/21 20:55
JLB
V1702
Chlorodibromomethane
<0.500
N9/L
0.081
0.500
1
03/13/21 20:55
JLB
V1702
Chloroethane
<0.500
ug/L
0.220
0.500
1
03/13/21 20:55
JLB
V1702
Chloroform
<0.500
N9/L
0.076
0.500
1
03/13/21 20:55
JLB
V1702
Chloromethane
<0.500
ug/L
0.079
0.500
1
03/13/21 20:55
JLB
V1702
Di -Isopropyl Ether (DIPE)
<5.00
N9/L
0.960
5.00
1
03/13/21 20:55
JLB
V1702
1,2-Dibromo-3-Chloropropane
<2.00
pg/L
0.170
2.00
1
03/13/21 20:55
JLB
V1702
1,2-Dibromoethane
<0.500
N9/L
0.051
0.500
1
03/13/21 20:55
JLB
V1702
Dibromomethane
<0.500
pg/L
0.065
0.500
1
03/13/21 20:55
JLB
V1702
trans-1,4-Dichloro-2-butene
<10.0
N9/L
0.120
10.0
1
03/13/21 20:55
JLB
V1702
1,2-Dichlorobenzene
<0.500
pg/L
0.076
0.500
1
03/13/21 20:55
JLB
V1702
1,4-Dichlorobenzene
1.04
N9/L
0.050
0.500
1
03/13/21 20:55
JLB
V1702
Dichlorodifluoromethane
<5.00
pg/L
0.110
5.00
1
03/13/21 20:55
JLB
V1702
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 18 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
REPORT OF ANAL YSIS
Lab No : 94464 Matrix: Aqueous
Sample ID: MW-06-20210310 Sampled: 3/10/2021 11:16
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,1-Dichloroethane
0.907
Ng/L
0.083
0.500
1
03/13/21 20:55
JLB
V1702
1,2-Dichloroethane
<0.500
u9/L
0.066
0.500
1
03/13/21 20:55
JLB
V1702
1,1-Dichloroethene
<0.500
N9/L
0.083
0.500
1
03/13/21 20:55
JLB
V1702
cis- 1,2-Dich loroethene
0.781
u9/L
0.056
0.500
1
03/13/21 20:55
JLB
V1702
trans-1,2-Dichloroethene
<0.500
N9/L
0.094
0.500
1
03/13/21 20:55
JLB
V1702
1,2-Dichloropropane
<0.500
u9/L
0.110
0.500
1
03/13/21 20:55
JLB
V1702
cis- 1,3-Dich loropropene
<0.500
N9/L
0.079
0.500
1
03/13/21 20:55
JLB
V1702
trans-1,3-Dichloropropene
<0.500
u9/L
0.070
0.500
1
03/13/21 20:55
JLB
V1702
1,4-Dioxane
<150
N9/L
14.0
150
1
03/13/21 20:55
JLB
V1702
Ethylbenzene
<0.500
u9/L
0.061
0.500
1
03/13/21 20:55
JLB
V1702
2-Hexanone
<5.00
N9/L
0.065
5.00
1
03/13/21 20:55
JLB
V1702
Methyl Ethyl Ketone (MEK)
<5.00
u9/L
0.240
5.00
1
03/13/21 20:55
JLB
V1702
4-Methyl-2-Pentanone
<5.00
N9/L
1.00
5.00
1
03/13/21 20:55
JLB
V1702
Methylene Chloride
<1.00
ug/L
0.083
1.00
1
03/13/21 20:55
JLB
V1702
Styrene
<0.500
N9/L
0.047
0.500
1
03/13/21 20:55
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.500
ug/L
0.110
0.500
1
03/13/21 20:55
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.500
N9/L
0.036
0.500
1
03/13/21 20:55
JLB
V1702
Tetrachloroethene
<0.500
ug/L
0.098
0.500
1
03/13/21 20:55
JLB
V1702
Tetrahydrofuran
<10.0
N9/L
1.10
10.0
1
03/13/21 20:55
JLB
V1702
Toluene
<0.500
u9/L
0.044
0.500
1
03/13/21 20:55
JLB
V1702
1, 1, 1-Trichloroethane
<0.500
N9/L
0.061
0.500
1
03/13/21 20:55
JLB
V1702
1,1,2-Trichloroethane
<0.500
u9/L
0.066
0.500
1
03/13/21 20:55
JLB
V1702
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 19 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
Lab No : 94464
Sample ID: MW-06-20210310
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 3/10/2021 11:16
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Trichloroethene
<0.500
Ng/L
0.078
0.500
1
03/13/21 20:55 JLB
V1702
Trichlorofluoromethane
<0.500
ug/L
0.062
0.500
1
03/13/21 20:55 JLB
V1702
1,2,3-Trichloropropane
<1.00
Ng/L
0.140
1.00
1
03/13/21 20:55 JLB
V1702
Vinyl Acetate
<2.00
ug/L
0.060
2.00
1
03/13/21 20:55 JLB
V1702
Vinyl Chloride
<0.500
Ng/L
0.097
0.500
1
03/13/21 20:55 JLB
V1702
o-Xylene
<0.500
ug/L
0.044
0.500
1
03/13/21 20:55 JLB
V1702
m,p-Xylene
<1.00
Ng/L
0.120
1.00
1
03/13/21 20:55 JLB
V1702
Xylene (Total)
<0.500
ug/L
0.500
1
03/13/21 20:55
V1702
Surrogate:4-Bromofluorobenzene
94.2
Limits:80-124%
1 03/13/21 20:55 JLB
V1702
Surrogate: Dibromofluoromethane
107
Limits:
75-129%
1 03/13/21 20:55 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
110
Limits:
63-136%
1 03/13/21 20:55 JLB
V1702
Surrogate: Toluene-d8
99.4
Limits:
77-123%
1 03/13/21 20:55 JLB
V1702
Qualifiers/ DF Dilution Factor J Estimated value
Definitions MQL Method Quantitation Limit
Page 20 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94465
Matrix: Aqueous
Sample ID : LT-01-20210310
Sampled: 3/10/2021 13:50
1,4-Dioxane
55.5
Ng/L
0.139
2.00
1
03/11/21 20:23 TBL
Surrogate:4-Bromofluorobenzene
110
Limits:70-130%
1 03/11/2120:23 TBL
V1584
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Method
Antimony
<2.00
ug/L
0.490
2.00
1
03/13/2102:25 MMR
6020B
Arsenic
2.90
Ng/L
0.170
1.00
1
03/13/2102:25 MMR
6020E
Barium
360
ug/L
0.810
10.0
1
03/13/2102:25 MMR
6020B
Beryllium
<1.00
Ng/L
0.190
1.00
1
03/13/2102:25 MMR
6020B
Cadmium
<1.00
ug/L
0.160
1.00
1
03/13/2102:25 MMR
6020B
Chromium
2.99
Ng/L
0.790
2.00
1
03/13/2102:25 MMR
6020E
Cobalt
3.97
ug/L
0.520
2.00
1
03/13/2102:25 MMR
6020B
Copper
<10.0
Ng/L
3.80
10.0
1
03/13/2102:25 MMR
6020B
Lead
<1.00
ug/L
0.260
1.00
1
03/13/2102:25 MMR
6020B
Nickel
23.6
Ng/L
0.510
3.00
1
03/13/2102:25 MMR
6020E
Selenium
<5.00
ug/L
0.740
5.00
1
03/13/2102:25 MMR
6020B
Silver
<1.00
Ng/L
0.110
1.00
1
03/13/2102:25 MMR
6020B
Thallium
<2.00
ug/L
0.570
2.00
1
03/13/2102:25 MMR
6020B
Vanadium
<5.00
Ng/L
1.30
5.00
1
03/13/2102:25 MMR
6020B
Zinc
<20.0
ug/L
6.90
20.0
1
03/13/2102:25 MMR
6020B
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 21 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94465
Matrix: Aqueous
Sample ID: LT-01-20210310
Sampled:
3/10/2021
13:50
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
20.2
Ng/L
0.310
5.00
1
03/13/21 21:29
JLB
V1702
Acrylonitrile
<20.0
u9/L
0.200
20.0
1
03/13/21 21:29
JLB
V1702
Benzene
1.49
N9/L
0.048
0.500
1
03/13/21 21:29
JLB
V1702
Bromochloromethane
<0.500
u9/L
0.140
0.500
1
03/13/21 21:29
JLB
V1702
Bromodichloromethane
<0.500
N9/L
0.062
0.500
1
03/13/21 21:29
JLB
V1702
Bromoform
<1.00
u9/L
0.040
1.00
1
03/13/21 21:29
JLB
V1702
Bromomethane
<1.00
N9/L
0.180
1.00
1
03/13/21 21:29
JLB
V1702
Carbon Disulfide
<5.00
u9/L
0.075
5.00
1
03/13/21 21:29
JLB
V1702
Carbon Tetrachloride
<0.500
N9/L
0.110
0.500
1
03/13/21 21:29
JLB
V1702
Chlorobenzene
3.13
u9/L
0.062
0.500
1
03/13/21 21:29
JLB
V1702
Chlorodibromomethane
<0.500
N9/L
0.081
0.500
1
03/13/21 21:29
JLB
V1702
Chloroethane
<0.500
u9/L
0.220
0.500
1
03/13/21 21:29
JLB
V1702
Chloroform
<0.500
N9/L
0.076
0.500
1
03/13/21 21:29
JLB
V1702
Chloromethane
<0.500
ug/L
0.079
0.500
1
03/13/21 21:29
JLB
V1702
Di -Isopropyl Ether (DIPE)
<5.00
N9/L
0.960
5.00
1
03/13/21 21:29
JLB
V1702
1,2-Dibromo-3-Chloropropane
<2.00
pg/L
0.170
2.00
1
03/13/21 21:29
JLB
V1702
1,2-Dibromoethane
<0.500
N9/L
0.051
0.500
1
03/13/21 21:29
JLB
V1702
Dibromomethane
<0.500
ug/L
0.065
0.500
1
03/13/21 21:29
JLB
V1702
trans-1,4-Dichloro-2-butene
<10.0
N9/L
0.120
10.0
1
03/13/21 21:29
JLB
V1702
1,2-Dichlorobenzene
<0.500
pg/L
0.076
0.500
1
03/13/21 21:29
JLB
V1702
1,4-Dichlorobenzene
3.44
N9/L
0.050
0.500
1
03/13/21 21:29
JLB
V1702
Dichlorodifluoromethane
<5.00
pg/L
0.110
5.00
1
03/13/21 21:29
JLB
V1702
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 22 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
REPORT OF ANAL YSIS
Lab No : 94465 Matrix: Aqueous
Sample ID: LT-01-20210310 Sampled: 3/10/2021 13:50
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,1-Dichloroethane
<0.500
N9/L
0.083
0.500
1
03/13/21 21:29
JLB
V1702
1,2-Dichloroethane
<0.500
u9/L
0.066
0.500
1
03/13/21 21:29
JLB
V1702
1,1-Dichloroethene
<0.500
N9/L
0.083
0.500
1
03/13/21 21:29
JLB
V1702
cis- 1,2-Dich loroethene
<0.500
u9/L
0.056
0.500
1
03/13/21 21:29
JLB
V1702
trans-1,2-Dichloroethene
<0.500
N9/L
0.094
0.500
1
03/13/21 21:29
JLB
V1702
1,2-Dichloropropane
<0.500
u9/L
0.110
0.500
1
03/13/21 21:29
JLB
V1702
cis- 1,3-Dich loropropene
<0.500
N9/L
0.079
0.500
1
03/13/21 21:29
JLB
V1702
trans-1,3-Dichloropropene
<0.500
u9/L
0.070
0.500
1
03/13/21 21:29
JLB
V1702
1,4-Dioxane
<150
N9/L
14.0
150
1
03/13/21 21:29
JLB
V1702
Ethylbenzene
<0.500
u9/L
0.061
0.500
1
03/13/21 21:29
JLB
V1702
2-Hexanone
<5.00
N9/L
0.065
5.00
1
03/13/21 21:29
JLB
V1702
Methyl Ethyl Ketone (MEK)
<5.00
u9/L
0.240
5.00
1
03/13/21 21:29
JLB
V1702
4-Methyl-2-Pentanone
<5.00
N9/L
1.00
5.00
1
03/13/21 21:29
JLB
V1702
Methylene Chloride
<1.00
u9/L
0.083
1.00
1
03/13/21 21:29
JLB
V1702
Styrene
<0.500
N9/L
0.047
0.500
1
03/13/21 21:29
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.500
u9/L
0.110
0.500
1
03/13/21 21:29
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.500
N9/L
0.036
0.500
1
03/13/21 21:29
JLB
V1702
Tetrachloroethene
<0.500
pg/L
0.098
0.500
1
03/13/21 21:29
JLB
V1702
Tetrahydrofuran
82.9
N9/L
1.10
10.0
1
03/13/21 21:29
JLB
V1702
Toluene
<0.500
u9/L
0.044
0.500
1
03/13/21 21:29
JLB
V1702
1, 1, 1-Trichloroethane
<0.500
N9/L
0.061
0.500
1
03/13/21 21:29
JLB
V1702
1,1,2-Trichloroethane
<0.500
u9/L
0.066
0.500
1
03/13/21 21:29
JLB
V1702
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 23 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94465 Matrix: Aqueous
Sample ID: LT-01-20210310 Sampled: 3/10/2021 13:50
Analytical Method: 8260D Prep Batch(es): V1700 03/13/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Trichloroethene
<0.500
Ng/L
0.078 0.500
1
03/13/21 21:29 JLB
V1702
Trichlorofluoromethane
<0.500
ug/L
0.062 0.500
1
03/13/21 21:29 JLB
V1702
1,2,3-Trichloropropane
<1.00
Ng/L
0.140 1.00
1
03/13/21 21:29 JLB
V1702
Vinyl Acetate
<2.00
ug/L
0.060 2.00
1
03/13/21 21:29 JLB
V1702
Vinyl Chloride
<0.500
Ng/L
0.097 0.500
1
03/13/21 21:29 JLB
V1702
o-Xylene
<0.500
ug/L
0.044 0.500
1
03/13/21 21:29 JLB
V1702
m,p-Xylene
<1.00
Ng/L
0.120 1.00
1
03/13/21 21:29 JLB
V1702
Xylene (Total)
<0.500
ug/L
0.500
1
03/13/21 21:29
V1702
Surrogate:4-Bromofluorobenzene
93.2
Limits:80-124%
1 03/13/21 21:29 JLB
V1702
Surrogate: Dibromofluoromethane
109
Limits: 75-129%
1 03/13/21 21:29 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
105
Limits: 63-136%
1 03/13/21 21:29 JLB
V1702
Surrogate: Toluene-d8
102
Limits: 77-123%
1 03/13/21 21:29 JLB
V1702
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 24 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94467
Matrix: Aqueous
Sample ID: TB-202103100000
Sampled:
3/10/2021
12:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<5.00
Ng/L
0.310
5.00
1
03/13/21 15:48
JLB
V1702
Acrylonitrile
<20.0
u9/L
0.200
20.0
1
03/13/21 15:48
JLB
V1702
Benzene
<0.500
N9/L
0.048
0.500
1
03/13/21 15:48
JLB
V1702
Bromochloromethane
<0.500
u9/L
0.140
0.500
1
03/13/21 15:48
JLB
V1702
Bromodichloromethane
<0.500
N9/L
0.062
0.500
1
03/13/21 15:48
JLB
V1702
Bromoform
<1.00
u9/L
0.040
1.00
1
03/13/21 15:48
JLB
V1702
Bromomethane
<1.00
N9/L
0.180
1.00
1
03/13/21 15:48
JLB
V1702
Carbon Disulfide
<5.00
u9/L
0.075
5.00
1
03/13/21 15:48
JLB
V1702
Carbon Tetrachloride
<0.500
N9/L
0.110
0.500
1
03/13/21 15:48
JLB
V1702
Chlorobenzene
<0.500
u9/L
0.062
0.500
1
03/13/21 15:48
JLB
V1702
Chlorodibromomethane
<0.500
N9/L
0.081
0.500
1
03/13/21 15:48
JLB
V1702
Chloroethane
<0.500
ug/L
0.220
0.500
1
03/13/21 15:48
JLB
V1702
Chloroform
<0.500
N9/L
0.076
0.500
1
03/13/21 15:48
JLB
V1702
Chloromethane
<0.500
ug/L
0.079
0.500
1
03/13/21 15:48
JLB
V1702
Di -Isopropyl Ether (DIPE)
<5.00
N9/L
0.960
5.00
1
03/13/21 15:48
JLB
V1702
1,2-Dibromo-3-Chloropropane
<2.00
pg/L
0.170
2.00
1
03/13/21 15:48
JLB
V1702
1,2-Dibromoethane
<0.500
N9/L
0.051
0.500
1
03/13/21 15:48
JLB
V1702
Dibromomethane
<0.500
pg/L
0.065
0.500
1
03/13/21 15:48
JLB
V1702
trans-1,4-Dichloro-2-butene
<10.0
N9/L
0.120
10.0
1
03/13/21 15:48
JLB
V1702
1,2-Dichlorobenzene
<0.500
pg/L
0.076
0.500
1
03/13/21 15:48
JLB
V1702
1,4-Dichlorobenzene
<0.500
N9/L
0.050
0.500
1
03/13/21 15:48
JLB
V1702
Dichlorodifluoromethane
<5.00
pg/L
0.110
5.00
1
03/13/21 15:48
JLB
V1702
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 25 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007 REPOR T OF A NA L YSIS
Lab No : 94467
Matrix: Aqueous
Sample ID: TB-202103100000
Sampled:
3/10/2021
12:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,1-Dichloroethane
<0.500
N9/L
0.083
0.500
1
03/13/21 15:48
JLB
V1702
1,2-Dichloroethane
<0.500
u9/L
0.066
0.500
1
03/13/21 15:48
JLB
V1702
1,1-Dichloroethene
<0.500
N9/L
0.083
0.500
1
03/13/21 15:48
JLB
V1702
cis- 1,2-Dich loroethene
<0.500
u9/L
0.056
0.500
1
03/13/21 15:48
JLB
V1702
trans-1,2-Dichloroethene
<0.500
N9/L
0.094
0.500
1
03/13/21 15:48
JLB
V1702
1,2-Dichloropropane
<0.500
u9/L
0.110
0.500
1
03/13/21 15:48
JLB
V1702
cis- 1,3-Dich loropropene
<0.500
N9/L
0.079
0.500
1
03/13/21 15:48
JLB
V1702
trans-1,3-Dichloropropene
<0.500
u9/L
0.070
0.500
1
03/13/21 15:48
JLB
V1702
1,4-Dioxane
<150
N9/L
14.0
150
1
03/13/21 15:48
JLB
V1702
Ethylbenzene
<0.500
u9/L
0.061
0.500
1
03/13/21 15:48
JLB
V1702
2-Hexanone
<5.00
N9/L
0.065
5.00
1
03/13/21 15:48
JLB
V1702
Methyl Ethyl Ketone (MEK)
<5.00
ug/L
0.240
5.00
1
03/13/21 15:48
JLB
V1702
4-Methyl-2-Pentanone
<5.00
N9/L
1.00
5.00
1
03/13/21 15:48
JLB
V1702
Methylene Chloride
<1.00
u9/L
0.083
1.00
1
03/13/21 15:48
JLB
V1702
Styrene
<0.500
N9/L
0.047
0.500
1
03/13/21 15:48
JLB
V1702
1,1,1,2-Tetrachloroethane
<0.500
ug/L
0.110
0.500
1
03/13/21 15:48
JLB
V1702
1,1,2,2-Tetrachloroethane
<0.500
N9/L
0.036
0.500
1
03/13/21 15:48
JLB
V1702
Tetrachloroethene
<0.500
pg/L
0.098
0.500
1
03/13/21 15:48
JLB
V1702
Tetrahydrofuran
<10.0
N9/L
1.10
10.0
1
03/13/21 15:48
JLB
V1702
Toluene
<0.500
u9/L
0.044
0.500
1
03/13/21 15:48
JLB
V1702
1, 1, 1-Trichloroethane
<0.500
N9/L
0.061
0.500
1
03/13/21 15:48
JLB
V1702
1,1,2-Trichloroethane
<0.500
u9/L
0.066
0.500
1
03/13/21 15:48
JLB
V1702
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 26 of 58

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County LF
Chuck Pippen Report Date : 03/31/2021
231 Haywood Street Information : Received : 03/11/2021
Asheville , NC 28801
Report Number : 21-070-0007
Lab No : 94467
Sample ID: TB-202103100000
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 3/10/2021 12:00
Analytical Method: 8260D
Prep Batch(es):
V1700
03/13/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
Trichloroethene
<0.500
Ng/L
0.078
0.500
1
03/13/21 15:48 JLB
V1702
Trichlorofluoromethane
<0.500
ug/L
0.062
0.500
1
03/13/21 15:48 JLB
V1702
1,2,3-Trichloropropane
<1.00
Ng/L
0.140
1.00
1
03/13/21 15:48 JLB
V1702
Vinyl Acetate
<2.00
ug/L
0.060
2.00
1
03/13/21 15:48 JLB
V1702
Vinyl Chloride
<0.500
Ng/L
0.097
0.500
1
03/13/21 15:48 JLB
V1702
o-Xylene
<0.500
ug/L
0.044
0.500
1
03/13/21 15:48 JLB
V1702
m,p-Xylene
<1.00
Ng/L
0.120
1.00
1
03/13/21 15:48 JLB
V1702
Xylene (Total)
<0.500
ug/L
0.500
1
03/13/21 15:48
V1702
Surrogate:4-Bromofluorobenzene
95.4
Limits:80-124%
1 03/13/21 15:48 JLB
V1702
Surrogate: Dibromofluoromethane
110
Limits:
75-129%
1 03/13/21 15:48 JLB
V1702
Surrogate: 1,2-Dichloroethane - d4
109
Limits:
63-136%
1 03/13/21 15:48 JLB
V1702
Surrogate: Toluene-d8
101
Limits:
77-123%
1 03/13/21 15:48 JLB
V1702
Qualifiers/ DF Dilution Factor J Estimated value
Definitions MQL Method Quantitation Limit
Page 27 of 58

lacioAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 23, 2021
Robbi A. Jones
Prism Laboratories, Inc.
P.O. Box 240543
Charlotte, NC 28224
RE: Project: DW-01-20210310
Pace Project No.: 92527377
Dear Robbi Jones:
Enclosed are the analytical results for sample(s) received by the laboratory on March 12, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring for
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Angela Overcash, Prism
. V C.
_ REPORT OF LABORATORY ANALYSIS
I This report shall not be reproduced, except in full,
B ;
without the written consent of Pace Analytical Services, LLC.
Page 28 of 58
Page 1 of 11

a�
_ ;a'ceAnalyfica(
++ www.pacelabs.com
I
Project: DW-01-20210310
Pace Project No.: 92527377
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Arizona Certification# AZ0819
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 29 of 58
Page 2 of 11

lacioAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: DW-01-20210310
Pace Project No.: 92527377
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92527377001 DW-01-20210310 EPA524.2 JLR 24 PASI-O
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 11
Page 30 of 58

Pace Analytical Services, LLC
a
aceAnalytical 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
++ www.pacelabs.com [phone]
I
ANALYTICAL RESULTS
Project: DW-01-20210310
Pace Project No.: 92527377
Sample: DW-01-20210310 Lab ID: 92527377001 Collected: 03/10/21 14:55 Received: 03/12/21 10:00 Matrix: Drinking Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV
Analytical Method: EPA 524.2
Pace Analytical
Services - Ormond
Beach
Benzene
ND
mg/L
0.00050
1
03/20/21 02:49
71-43-2
Carbon tetrachloride
ND
mg/L
0.00050
1
03/20/21 02:49
56-23-5
Chlorobenzene
ND
mg/L
0.00050
1
03/20/21 02:49
108-90-7
1,2-Dichlorobenzene
ND
mg/L
0.00050
1
03/20/21 02:49
95-50-1
1,4-Dichlorobenzene
ND
mg/L
0.00050
1
03/20/21 02:49
106-46-7
1,2-Dichloroethane
ND
mg/L
0.00050
1
03/20/21 02:49
107-06-2
1,1-Dichloroethene
ND
mg/L
0.00050
1
03/20/21 02:49
75-35-4
cis-1,2-Dichloroethene
ND
mg/L
0.00050
1
03/20/21 02:49
156-59-2
trans-1,2-Dichloroethene
ND
mg/L
0.00050
1
03/20/21 02:49
156-60-5
1,2-Dichloropropane
ND
mg/L
0.00050
1
03/20/21 02:49
78-87-5
Ethylbenzene
ND
mg/L
0.00050
1
03/20/21 02:49
100-41-4
Methylene Chloride
ND
mg/L
0.0010
1
03/20/21 02:49
75-09-2
Styrene
ND
mg/L
0.00050
1
03/20/21 02:49
100-42-5
Tetrachloroethene
ND
mg/L
0.00050
1
03/20/21 02:49
127-18-4
Toluene
ND
mg/L
0.00050
1
03/20/21 02:49
108-88-3
1,2,4-Trichlorobenzene
ND
mg/L
0.00050
1
03/20/21 02:49
120-82-1
1,1,1-Trichloroethane
ND
mg/L
0.00050
1
03/20/21 02:49
71-55-6
1,1,2-Trichloroethane
ND
mg/L
0.00050
1
03/20/21 02:49
79-00-5
Trichloroethene
ND
mg/L
0.00050
1
03/20/21 02:49
79-01-6
Vinyl chloride
ND
mg/L
0.00050
1
03/20/21 02:49
75-01-4
Xylene (Total)
ND
mg/L
0.0010
1
03/20/21 02:49
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
03/20/21 02:49
460-00-4
Toluene-d8 (S)
99
%
70-130
1
03/20/21 02:49
2037-26-5
1,2-Dichlorobenzene-d4 (S)
104
%
70-130
1
03/20/21 02:49
2199-69-1
Date: 03/23/2021 07:58 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 11
Page 31 of 58

lacioAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: DW-01-20210310
Pace Project No.: 92527377
QC Batch: 714402 Analysis Method: EPA 524.2
QC Batch Method: EPA 524.2 Analysis Description: 524.2 MSV
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92527377001
METHOD BLANK: 3894684
Associated Lab Samples: 92527377001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
mg/L
ND
0.00050
03/20/21 00:15
1,1,2-Trichloroethane
mg/L
ND
0.00050
03/20/21 00:15
1,1-Dichloroethene
mg/L
ND
0.00050
03/20/21 00:15
1,2,4-Trichlorobenzene
mg/L
ND
0.00050
03/20/21 00:15
1,2-Dichlorobenzene
mg/L
ND
0.00050
03/20/21 00:15
1,2-Dichloroethane
mg/L
ND
0.00050
03/20/21 00:15
1,2-Dichloropropane
mg/L
ND
0.00050
03/20/21 00:15
1,4-Dichlorobenzene
mg/L
ND
0.00050
03/20/21 00:15
Benzene
mg/L
ND
0.00050
03/20/21 00:15
Carbon tetrachloride
mg/L
ND
0.00050
03/20/21 00:15
Chlorobenzene
mg/L
ND
0.00050
03/20/21 00:15
cis-1,2-Dichloroethene
mg/L
ND
0.00050
03/20/21 00:15
Ethylbenzene
mg/L
ND
0.00050
03/20/21 00:15
Methylene Chloride
mg/L
ND
0.0010
03/20/21 00:15
Styrene
mg/L
ND
0.00050
03/20/21 00:15
Tetrachloroethene
mg/L
ND
0.00050
03/20/21 00:15
Toluene
mg/L
ND
0.00050
03/20/21 00:15
trans- 1 2- Dich loroethene
mg/L
ND
0.00050
03/20/21 00:15
Trichloroethene
mg/L
ND
0.00050
03/20/21 00:15
Vinyl chloride
mg/L
ND
0.00050
03/20/21 00:15
Xylene (Total)
mg/L
ND
0.0010
03/20/21 00:15
1,2-Dichlorobenzene-d4 (S)
%
103
70-130
03/20/21 00:15
4-Bromofluorobenzene (S)
%
98
70-130
03/20/21 00:15
Toluene-d8 (S)
%
98
70-130
03/20/21 00:15
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
3894685
Units
Spike
Conc.
3894686
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,1,1-Trichloroethane
mg/L
0.04
0.039
0.037
96
92
70-130
4
20
1,1,2-Trichloroethane
mg/L
0.04
0.038
0.038
96
95
70-130
0
20
1,1-Dichloroethene
mg/L
0.04
0.040
0.040
100
101
70-130
1
20
1,2,4-Trichlorobenzene
mg/L
0.04
0.040
0.040
99
101
70-130
2
20
1,2-Dichlorobenzene
mg/L
0.04
0.036
0.035
91
89
70-130
2
20
1,2-Dichloroethane
mg/L
0.04
0.039
0.038
97
95
70-130
2
20
1,2-Dichloropropane
mg/L
0.04
0.037
0.036
92
91
70-130
1
20
1,4-Dichlorobenzene
mg/L
0.04
0.037
0.036
92
91
70-130
1
20
Benzene
mg/L
0.04
0.039
0.038
97
94
70-130
3
20
Carbon tetrachloride
mg/L
0.04
0.040
0.039
99
97
70-130
2
20
Chlorobenzene
mg/L
0.04
0.038
0.037
95
93
70-130
1
20
Results presented on this page are in the units indicated by the "Units"
column except where an alternate unit is
presented to the right of the
result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2021 07:58 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 11
Page 32 of 58

lacioAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: DW-01-20210310
Pace Project No.: 92527377
LABORATORY CONTROL SAMPLE & LCSD:
3894685
3894686
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
cis-1,2-Dichloroethene
mg/L
0.04
0.038
0.039
95
97
70-130
1
20
Ethylbenzene
mg/L
0.04
0.039
0.038
98
96
70-130
2
20
Methylene Chloride
mg/L
0.04
0.040
0.040
99
100
70-130
1
20
Styrene
mg/L
0.04
0.040
0.040
101
99
70-130
1
20
Tetrachloroethene
mg/L
0.04
0.040
0.039
101
99
70-130
3
20
Toluene
mg/L
0.04
0.039
0.038
97
95
70-130
2
20
trans- 1 2- Dich loroethene
mg/L
0.04
0.039
0.039
96
99
70-130
2
20
Trichloroethene
mg/L
0.04
0.040
0.039
99
97
70-130
2
20
Vinyl chloride
mg/L
0.04
0.035
0.035
87
87
70-130
0
20
Xylene (Total)
mg/L
0.12
0.12
0.12
102
100
70-130
2
20
1,2-Dichlorobenzene-d4 (S)
%
100
98
70-130
4-Bromofluorobenzene (S)
%
103
103
70-130
Toluene-d8 (S)
%
101
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2021 07:58 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 11
Page 33 of 58

a�
_ ;a'ceAnalyfica(
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: DW-01-20210310
Pace Project No.: 92527377
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/23/2021 07:58 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 11
Page 34 of 58

lacioAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DW-01-20210310
Pace Project No.: 92527377
Lab ID Sample ID
92527377001 DW-01-20210310
Date: 03/23/2021 07:58 AM
QC Batch Method QC Batch Analytical Method
EPA 524.2 714402
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 8 of 11
Page 35 of 58

aCi'Sample Condition Upon Recelpt(SCUR) Yvy~ y Page 1 of 2
AnaWical' Document No.: Issuing Authority:
F-CAR-CS-033-Rev,07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanlcsville❑ Atlanta[] Kernersville❑
Sample odr Client Name:- Upon Receipt WQ# : 92527377
Courier: Fed Ex i Project ❑UPS USPS ❑Client 1111111111111111111111
❑ Commercial space ❑Other:
92527377
Custody Seal Present? 0Yes No Seals intact? Yes No
Date/Initials Person Examining Contents: � 3 2-zl
Packing Material: []Bubble Wrap ❑Bubble Bags None ❑ Other Biological Tissue Frozen?
I� /A
Thermometgr: r Wet [—]Blue ❑ []Yeses []No None �`
iR Gun ID:
Type of Ice:
c[ Correction Factor;
Cooler Temp: Add/Subtract;°C) 0.0'C Temp should be above freezing to 6°C
C7 ❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C): 7 . has begun
USDA Regulated Soil (� N/A, water sample)
Did samples originate in quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
IFlYes IINo including Hawaii and Puerto Ricol? FlYes nNo
Comments/Discrepancy:
Chain of Custody Present?
ZYeS
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
❑Na
[]N/A
2.
Short Hold Time Analysis (e72 hr.)?
❑Yes
ImNo
❑NIA
3.
Rush Turn Around Time Requested?
YE
N
N A
4.
Sufficient Volume?
Yes
[:)No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
0Yes
%yes
[]No
❑No
[]N/A
❑NIA
6.
Containers Intact?
MYes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
NfN/A
8.
Sample Labels Match COC?
-Includes Oate�me/ID/Analysis Matrix:
]Yes
V _ �//
❑Na
❑N/A
9.
Headspace in VOA vials P5.6mm)?
❑Yes
No
ON/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
UNo
❑No
[�N/A
JONM
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Project Manager SCURF Review: Date:
Field Data Required? [—]Yes []No
Project Manager SRF Review:
Page 36 of 58
Date:
Page 9 of 11

1�aceAnaVical `
i
Condition Upon Recei
Document No.:
F-CAR-CS-033-Rev.07
2 of 2
issuing Authority:
Pace Cnrnlinac 011mlifir nffi,.
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) OOC, LLHg
**Bottom half of box is to list number of bottles
Project i WO# ; 92527377 -
PM: MWB Due Date: 03/19/21
CLIENT: 92-Prism
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PH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservatlan adjusted
Time preservation
Amount of Preservative
Lot p
adjusted
added
(heflalges thaFe -iRGF%1;RM4v
a4-w -
co—P103gro tnrnples-a rang of this form will bPtpnrtn thp North CarnlinaLDEMR rLrtifocation QfficL�
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 37 of 58
Page 10 of 11

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Page 38 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-070-0007
QC Analytical Batch:
V1945
Analysis Method:
2320B-2011
Analysis Description:
Alkalinity
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
94462, 94463, 94464
Blank MDL
MQL
Analyzed
Parameter
Units Result
Alkalinity (as CaCO3)
pg/L <800 800
5000
03/19/21 13:40
Laboratory Control Sample LCS
Spike
LCS
LCS %Rec % Rec
Parameter
Units Conc.
Result
Limits
Alkalinity (as CaCO3)
pg/L 250000
247000
99.0 90-110
Duplicate
V 94507-DUP
Result DUP
RPD Max RPD
Analyzed
Parameter
Units Result
Alkalinity (as CaCO3)
pg/L 126000 128000
1.5 20
03/19/21 13:40
Date: 03/31/2021 02:40 PM Page 1 of 18
Page 39 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-070-0007
QC Analytical Batch:
V1864
Analysis Method:
2340C-2011
Analysis Description:
Total Hardness
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
94462, 94463, 94464
Blank MDL
MQL
Analyzed
Parameter
Units Result
Hardness
pg/L <570 570
5000
03/18/21 11:20
Laboratory Control Sample LCS
Spike
LCS
LCS %Rec % Rec
Parameter
Units Conc.
Result
Limits
Hardness
pg/L 50000
51000
102 90-110
Duplicate
V 94374-DUP
Result DUP
RPD Max RPD
Analyzed
Parameter
Units Result
Hardness
pg/L 162000 158000
2.5 20
03/18/21 11:20
Date: 03/31/2021 02:40 PM Page 2 of 18
Page 40 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Analytical Batch: V1747
Analysis Method: 4500S2F-2011
Analysis Description: Sulfide
Lab Reagent Blank LRB Matrix: AQU
Associated Lab Samples: 94462, 94463, 94464
Blank MDL MQL Analyzed
Parameter Units Result
Sulfide pg/L <830 830 2000 03/15/2111:30
Laboratory Control Sample LCS
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Sulfide
pg/L 10000 7200
72.0 70-122
Date: 03/31/2021 02:40 PM Page 3 of 18
Page 41 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Analytical Batch: V1691
Analysis Method: 5210B-2011
Analysis Description: Biochemical Oxygen Demand (BOD)
Glucose-Glutamic Acid GGA
Result Range Analyzed
Parameter Units
Biochemical Oxygen Demand (5-day) Ng/L 246* 167.5-228.` 03/11/21 16:07
Duplicate V 94439-DUP
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Biochemical Oxygen Demand (5-day) Ng/L <2000 <2000 0.0 30 03/11/21 16:07
* QC Fail Date: 03/31/2021 02:40 PM Page 4 of 18
Page 42 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Analytical Batch: V1722
Analysis Method: 5220D-2011
Analysis Description: Chemical Oxygen Demand (COD)
Lab Reagent Blank LRB
Matrix: AQU
Associated Lab Samples: 94462, 94463, 94464
Blank MDL
MQL
Analyzed
Parameter Units Result
COD (Chemical Oxygen Demand) pg/L <11000 11000
50000
03/16/21 11:30
Laboratory Control Sample LCS
Spike
LCS
LCS %Rec
% Rec
Parameter Units Conc.
Result
Limits
COD (Chemical Oxygen Demand) pg/L 500000
499000
100
90-110
Matrix Spike & Matrix Spike Duplicate V 94374-MS V 94374-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter Units Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
COD (Chemical Oxygen Demand) pg/L <11000 500000
500000 503000
485000 101
97.0 80-120 3.6 20
Date: 03/31/2021 02:40 PM Page 5 of 18
Page 43 of 58

• Charlotte, NC 28217
Waypoint, 449 Springbrook Rd, Ch
Main 704.529.6364
ANALYTICAL www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep:
L541751
QC Analytical Batch(es): L541995
QC Prep Batch Method:
5310C-2011
Analysis Method:
5310C-2011
Analysis Description:
Total Organic Carbon
Lab Reagent Blank
LRB-L541751
Matrix: AQU
Associated Lab Samples:
94462, 94463, 94464
Blank MDL
MQL
Analyzed
Parameter
Units
Result
TOC
mg/L
<0.500 0.500
1.00
03/16/2110:39
Laboratory Control Sample
LCS-L541751
Spike
LCS
LCS %Rec % Rec
Parameter
Units
Conc.
Result
Limits
TOC
mg/L
5.00
4.82
96.0 85-115
Duplicate
L 95234-DUP-L541751
Result DUP
RPD Max RPD
Analyzed
Parameter
Units
Result
TOC
mg/L
63.0 62.4
0.9 20.0
03/16/2121:54
Matrix Spike
V 94462-MS-L541751
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
TOC
mg/L
1.14 5.26
6.21
96.0 70-130
Date: 03/31/2021 02:40 PM Page 6 of 18
Page 44 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep:
V1591
QC Analytical Batch(es): V1669
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Lab Reagent Blank
LRB-V1591
Matrix: AQU
Associated Lab Samples:
94462, 94463, 94464, 94465
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Antimony
pg/L
<0.490
0.490
2.00
03/13/2100:41
Arsenic
pg/L
<0.170
0.170
1.00
03/13/2100:41
Barium
pg/L
<0.810
0.810
10.0
03/13/2100:41
Beryllium
pg/L
<0.190
0.190
1.00
03/13/2100:41
Cadmium
pg/L
<0.160
0.160
1.00
03/13/2100:41
Chromium
pg/L
<0.790
0.790
2.00
03/13/2100:41
Cobalt
pg/L
<0.520
0.520
2.00
03/13/2100:41
Copper
pg/L
<3.80
3.80
10.0
03/13/2100:41
Lead
pg/L
<0.260
0.260
1.00
03/13/2100:41
Nickel
pg/L
<0.510
0.510
3.00
03/13/2100:41
Selenium
pg/L
<0.740
0.740
5.00
03/13/2100:41
Silver
pg/L
<0.110
0.110
1.00
03/13/2100:41
Thallium
pg/L
<0.570
0.570
2.00
03/13/2100:41
Vanadium
pg/L
<1.30
1.30
5.00
03/13/2100:41
Zinc
pg/L
<6.90
6.90
20.0
03/13/2100:41
Laboratory Control Sample LCS-V1591
Spike
Parameter Units Conc.
LCS LCS %Rec % Rec
Result Limits
Antimony
pg/L
100
108
108
80-120
Arsenic
pg/L
100
97.9
98.0
80-120
Barium
pg/L
100
99.7
100
80-120
Beryllium
pg/L
100
102
102
80-120
Cadmium
pg/L
100
101
101
80-120
Chromium
pg/L
100
102
102
80-120
Cobalt
pg/L
100
104
104
80-120
Copper
pg/L
100
104
104
80-120
Date: 03/31/2021 02:40 PM Page 7 of 18
Page 45 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep: V1591 QC Analytical Batch(es): V1669
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V1591
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Lead
pg/L
100
102
102
80-120
Nickel
pg/L
100
105
105
80-120
Selenium
pg/L
100
95.3
95.0
80-120
Silver
pg/L
100
102
102
80-120
Thallium
pg/L
100
98.5
99.0
80-120
Vanadium
pg/L
100
103
103
80-120
Zinc
pg/L
100
102
102
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 94378-MS-V1591
MS Spike
Result Conc.
V 94378-MSD-V1591
MSD MS Result
Spike
Conc.
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Antimony
pg/L
< 0.490
100
100
107
106
107
106
75-125
0.9
20.0
Arsenic
pg/L
< 0.170
100
100
97.7
95.2
98.0
95.0
75-125
2.5
20.0
Barium
pg/L
13.8
100
100
115
114
101
100
75-125
0.8
20.0
Beryllium
pg/L
< 0.190
100
100
105
104
105
104
75-125
0.9
20.0
Cadmium
pg/L
< 0.160
100
100
100
102
100
102
75-125
1.9
20.0
Chromium
pg/L
< 0.790
100
100
102
103
102
103
75-125
0.9
20.0
Cobalt
pg/L
< 0.520
100
100
104
103
104
103
75-125
0.9
20.0
Copper
pg/L
< 3.80
100
100
105
104
105
104
75-125
0.9
20.0
Lead
pg/L
< 0.260
100
100
102
100
102
100
75-125
1.9
20.0
Nickel
pg/L
< 0.510
100
100
105
105
105
105
75-125
0.0
20.0
Selenium
pg/L
< 0.740
100
100
102
103
102
103
75-125
0.9
20.0
Silver
pg/L
< 0.110
100
100
103
101
103
101
75-125
1.9
20.0
Thallium
pg/L
< 0.570
100
100
101
97.8
101
98.0
75-125
3.2
20.0
Vanadium
pg/L
< 1.30
100
100
104
103
104
103
75-125
0.9
20.0
Zinc
pg/L
< 6.90
100
100
103
103
103
103
75-125
0.0
20.0
Date: 03/31/2021 02:40 PM Page 8 of 18
Page 46 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep: V1591
QC Prep Batch Method: 3005A
Post Digestion Spike V 94378-PDS-V1591
Parameter
Units
PDS
Result
Antimony
pg/L
49.7
Arsenic
Ng/L
50.0
Barium
pg/L
55.1
Beryllium
pg/L
50.1
Cadmium
pg/L
48.7
Chromium
Ng/L
50.9
Cobalt
Ng/L
50.3
Copper
pg/L
51.4
Lead
pg/L
49.9
Nickel
pg/L
52.2
Selenium
pg/L
50.4
Silver
Ng/L
50.0
Thallium
pg/L
49.5
Vanadium
pg/L
51.1
Zinc
pg/L
50.4
QC Analytical Batch(es): V1669
Analysis Method: 6020B
Analysis Description: Metals Analyses
0/0
Recovery
99.0
100
97.0
100
97.0
102
101
103
100
104
101
100
99.0
102
101
Analyzed
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
03/13/21 01:20
Date: 03/31/2021 02:40 PM Page 9 of 18
Page 47 of 58

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep: V1728
QC Analytical Batch(es): V1842
QC Prep Batch Method: 7470A
Analysis Method:
7470A
Analysis Description:
Total Aqueous Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V1728
Matrix: AQU
Associated Lab Samples: 94462, 94463, 94464
Blank MDL
MQL
Analyzed
Parameter Units
Result
Mercury (Total) pg/L
<0.0300 0.0300
0.200
03/16/21 13:16
Laboratory Control Sample
LCS-V1728
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Mercury (Total) pg/L
9.38
8.96
96.0 80-120
Matrix Spike & Matrix Spike Duplicate
V 94374-MS-V1728
V 94374-MSD-V1728
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Mercury (Total) pg/L
<0.0300 9.38
9.38 8.91
8.85 95.0 94.0 80-120 0.6 20
Post Digestion Spike
V 94374-PDS-V1728
PDS
%
Analyzed
Parameter Units
Result
Recovery
Mercury (Total) pg/L
4.39
94.0
03/16/21 13:35
Date: 03/31/2021 02:40 PM Page 10 of 18
Page 48 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-070-0007
QC Prep:
V1583
QC Analytical Batch(es): V1584
QC Prep Batch Method:
5030B
Analysis Method:
8260D SIM
Analysis Description:
Volatile Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-V1583
Matrix: AQU
Associated Lab Samples:
94462, 94463, 94464, 94465
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
1,4-Dioxane
pg/L
<0.139 0.139
2.00
03/11/2116:11
4-Bromofluorobenzene (S)
03/11/21 16:11
109
70-130
Laboratory Control Sample
LCS-V1583
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
1,4-Dioxane
pg/L
50.0
47.4
94.8
70-130
4-Bromofluorobenzene (S)
115
70-130
Matrix Spike & Matrix Spike Duplicate
V 94374-MS-V1583
V 94374-MSD-V1583
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD
Conc.
1,4-Dioxane
pg/L
< 0.139 50.0
50.0 50.4
51.3 101
103
70-130
4-Bromofluorobenzene (S)
108
107
70-130
Date: 03/31/2021 02:40 PM Page 11 of 18
Page 49 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep: V1700
QC Prep Batch Method: 5030B
Lab Reagent Blank LRB-V1700
Associated Lab Samples: 94462, 94463, 94464, 94465, 94467
QC Analytical Batch(es): V1702
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: AQU
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
pg/L
<0.310
0.310
5.00
03/13/21 14:40
Acrylonitrile
pg/L
<0.200
0.200
20.0
03/13/21 14:40
Benzene
pg/L
<0.048
0.048
0.500
03/13/21 14:40
Bromochloromethane
pg/L
<0.140
0.140
0.500
03/13/21 14:40
Bromodichloromethane
pg/L
<0.062
0.062
0.500
03/13/21 14:40
Bromoform
pg/L
<0.040
0.040
1.00
03/13/21 14:40
Bromomethane
pg/L
<0.180
0.180
1.00
03/13/21 14:40
Carbon Disulfide
pg/L
<0.075
0.075
5.00
03/13/21 14:40
Carbon Tetrachloride
pg/L
<0.110
0.110
0.500
03/13/21 14:40
Chlorobenzene
pg/L
<0.062
0.062
0.500
03/13/21 14:40
Chlorodibromomethane
pg/L
<0.081
0.081
0.500
03/13/21 14:40
Chloroethane
pg/L
<0.220
0.220
0.500
03/13/21 14:40
Chloroform
pg/L
<0.076
0.076
0.500
03/13/21 14:40
Chloromethane
pg/L
<0.079
0.079
0.500
03/13/21 14:40
Di -Isopropyl Ether (DIPE)
pg/L
<0.960
0.960
5.00
03/13/21 14:40
1,2-Dibromo-3-Chloropropane
pg/L
<0.170
0.170
2.00
03/13/21 14:40
1,2-Dibromoethane
pg/L
<0.051
0.051
0.500
03/13/21 14:40
Dibromomethane
pg/L
<0.065
0.065
0.500
03/13/21 14:40
trans-1,4-Dichloro-2-butene
pg/L
<0.120
0.120
10.0
03/13/21 14:40
1,2-Dichlorobenzene
pg/L
<0.076
0.076
0.500
03/13/21 14:40
1,4-Dichlorobenzene
pg/L
<0.050
0.050
0.500
03/13/21 14:40
Dichlorodifluoromethane
pg/L
<0.110
0.110
5.00
03/13/21 14:40
1,1-Dichloroethane
pg/L
<0.083
0.083
0.500
03/13/21 14:40
1,2-Dichloroethane
pg/L
<0.066
0.066
0.500
03/13/21 14:40
1,1-Dichloroethene
pg/L
<0.083
0.083
0.500
03/13/21 14:40
cis-1,2-Dichloroethene
pg/L
<0.056
0.056
0.500
03/13/21 14:40
trans-1,2-Dichloroethene
pg/L
<0.094
0.094
0.500
03/13/21 14:40
Date:
03/31/2021 02:40 PM
Page 12 of 18
Page 50 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep: V1700
QC Prep Batch Method: 5030B
Lab Reagent Blank LRB-V1700
Associated Lab Samples: 94462, 94463, 94464, 94465, 94467
QC Analytical Batch(es): V1702
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: AQU
Blank
MDL
MQL
Analyzed
% % Rec
Parameter
Units
Result
Recovery Limits
1,2-Dichloropropane
pg/L
<0.110
0.110
0.500
03/13/21 14:40
cis-1,3-Dichloropropene
pg/L
<0.079
0.079
0.500
03/13/21 14:40
trans-1,3-Dichloropropene
pg/L
<0.070
0.070
0.500
03/13/21 14:40
1,4-Dioxane
pg/L
<14.0
14.0
150
03/13/21 14:40
Ethylbenzene
pg/L
<0.061
0.061
0.500
03/13/21 14:40
2-Hexanone
pg/L
<0.065
0.065
5.00
03/13/21 14:40
Methyl Ethyl Ketone (MEK)
pg/L
<0.240
0.240
5.00
03/13/21 14:40
4-Methyl-2-Pentanone
pg/L
<1.00
1.00
5.00
03/13/21 14:40
Methylene Chloride
pg/L
<0.083
0.083
1.00
03/13/21 14:40
Styrene
pg/L
<0.047
0.047
0.500
03/13/21 14:40
1,1,1,2-Tetrachloroethane
pg/L
<0.110
0.110
0.500
03/13/21 14:40
1,1,2,2-Tetrachloroethane
pg/L
<0.036
0.036
0.500
03/13/21 14:40
Tetrachloroethene
pg/L
<0.098
0.098
0.500
03/13/21 14:40
Tetrahydrofuran
pg/L
<1.10
1.10
10.0
03/13/21 14:40
Toluene
pg/L
<0.044
0.044
0.500
03/13/21 14:40
1,1,1-Trichloroethane
pg/L
<0.061
0.061
0.500
03/13/21 14:40
1,1,2-Trichloroethane
pg/L
<0.066
0.066
0.500
03/13/21 14:40
Trichloroethene
pg/L
<0.078
0.078
0.500
03/13/21 14:40
Trichlorofluoromethane
pg/L
<0.062
0.062
0.500
03/13/21 14:40
1,2,3-Trichloropropane
pg/L
<0.140
0.140
1.00
03/13/21 14:40
Vinyl Acetate
pg/L
<0.060
0.060
2.00
03/13/21 14:40
Vinyl Chloride
pg/L
<0.097
0.097
0.500
03/13/21 14:40
o-Xylene
pg/L
<0.044
0.044
0.500
03/13/21 14:40
m,p-Xylene
pg/L
<0.120
0.120
1.00
03/13/21 14:40
4-Bromofluorobenzene (S)
03/13/21 14:40
92.6 80-124
Dibromofluoromethane (S)
03/13/21 14:40
109 75-129
1,2-Dichloroethane - d4 (S)
03/13/21 14:40
108 63-136
Date:
03/31/2021 02:40 PM
Page 13 of 18
Page 51 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-070-0007
QC Prep:
V1700
QC Analytical Batch(es): V1702
QC Prep Batch Method:
5030B
Analysis Method:
8260D
Analysis Description:
Volatile
Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V1700
Matrix: AQU
Associated Lab Samples:
94462, 94463, 94464, 94465, 94467
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Toluene-d8 (S)
03/13/21 14:40
100
77-123
Laboratory Control Sample
& LCSD
LCS-V1700 LCSD-V1700
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
a/o Rec
Limits
RPD
Max
RPD
Acetone
pg/L
40.0
42.6
44.8
107
112
40-166
5.0
20.0
Acrylonitrile
pg/L
40.0
42.1
41.2
105
103
81-127
2.1
20.0
Benzene
pg/L
20.0
22.3
21.2
112
106
77-128
5.0
20.0
Bromochloromethane
pg/L
20.0
22.8
22.5
114
113
78-135
1.3
20.0
Bromodichloromethane
pg/L
20.0
22.1
20.9
111
105
76-138
5.5
20.0
Bromoform
pg/L
20.0
19.8
20.1
99.0
101
71-135
1.5
20.0
Bromomethane
pg/L
20.0
20.1
18.5
101
92.5
41-168
8.2
20.0
Carbon Disulfide
pg/L
20.0
23.8
22.8
119
114
59-135
4.2
20.0
Carbon Tetrachloride
pg/L
20.0
21.3
19.9
107
99.5
72-142
6.7
20.0
Chlorobenzene
pg/L
20.0
21.0
20.5
105
103
78-119
2.4
20.0
Chlorodibromomethane
pg/L
20.0
19.7
19.9
98.5
99.5
75-134
1.0
20.0
Chloroethane
pg/L
20.0
23.3
21.7
117
109
57-142
7.1
20.0
Chloroform
pg/L
20.0
22.7
20.6
114
103
77-130
9.6
20.0
Chloromethane
pg/L
20.0
24.8
23.8
124
119
47-145
4.1
20.0
Di -Isopropyl Ether (DIPE)
pg/L
20.0
22.5
21.6
113
108
60-154
4.0
20.0
1,2-Dibromo-3-Chloropropane pg/L
20.0
18.3
17.9
91.5
89.5
63-134
2.2
20.0
1,2-Dibromoethane
pg/L
20.0
21.2
20.7
106
104
77-135
2.3
20.0
Dibromomethane
pg/L
20.0
22.7
21.8
114
109
76-138
4.0
20.0
trans-1,4-Dichloro-2-butene
pg/L
20.0
18.5
18.9
92.5
94.5
70-130
2.1
20.0
1,2-Dichlorobenzene
pg/L
20.0
20.7
20.2
104
101
78-128
2.4
20.0
1,4-Dichlorobenzene
pg/L
20.0
21.1
20.1
106
101
75-126
4.8
20.0
Date: 03/31/2021 02:40 PM Page 14 of 18
Page 52 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep: V1700 QC Analytical Batch(es): V1702
QC Prep Batch Method: 5030B Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V1700 LCSD-V1700
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Dichlorodifluoromethane
pg/L
20.0
25.7
23.6
129
118
28-163
8.5
20.0
1,1-Dichloroethane
pg/L
20.0
22.8
21.6
114
108
70-130
5.4
20.0
1,2-Dichloroethane
pg/L
20.0
21.9
20.5
110
103
68-131
6.6
20.0
1,1-Dichloroethene
pg/L
20.0
22.5
21.5
113
108
70-154
4.5
20.0
cis-1,2-Dichloroethene
pg/L
20.0
22.4
21.8
112
109
76-141
2.7
20.0
trans-1,2-Dichloroethene
pg/L
20.0
22.5
21.2
113
106
76-135
5.9
20.0
1,2-Dichloropropane
pg/L
20.0
22.7
21.9
114
110
77-130
3.5
20.0
cis-1,3-Dichloropropene
pg/L
20.0
20.3
19.6
102
98.0
65-140
3.5
20.0
trans-1,3-Dichloropropene
pg/L
20.0
19.3
18.2
96.5
91.0
67-140
5.8
20.0
1,4-Dioxane
pg/L
200
144
110
0.0*
0.0*
70-130
0.0
20.0
Ethylbenzene
pg/L
20.0
21.4
20.5
107
103
80-127
4.2
20.0
2-Hexanone
pg/L
20.0
18.9
18.8
94.5
94.0
64-137
0.5
20.0
Methyl Ethyl Ketone (MEK)
pg/L
20.0
19.1
19.6
95.5
98.0
71-134
2.5
20.0
4-Methyl-2-Pentanone
pg/L
20.0
20.8
20.2
104
101
69-134
2.9
20.0
Methylene Chloride
pg/L
20.0
23.9
23.2
120
116
73-131
2.9
20.0
Styrene
pg/L
20.0
21.1
20.6
106
103
78-129
2.3
20.0
1,1,1,2-Tetrachloroethane
pg/L
20.0
20.3
19.4
102
97.0
79-134
4.5
20.0
1,1,2,2-Tetrachloroethane
pg/L
20.0
21.9
21.2
110
106
62-127
3.2
20.0
Tetrachloroethene
pg/L
20.0
20.8
19.9
104
99.5
80-129
4.4
20.0
Tetrahydrofuran
pg/L
20.0
22.8
21.0
114
105
70-130
8.2
20.0
Toluene
pg/L
20.0
22.5
21.1
113
106
76-131
6.4
20.0
1,1,1-Trichloroethane
pg/L
20.0
21.1
19.8
106
99.0
75-135
6.3
20.0
1,1,2-Trichloroethane
pg/L
20.0
22.2
21.7
111
109
70-140
2.2
20.0
Trichloroethene
pg/L
20.0
20.6
19.3
103
96.5
77-133
6.5
20.0
Trichlorofluoromethane
pg/L
20.0
22.5
20.7
113
104
62-148
8.3
20.0
1,2,3-Trichloropropane
pg/L
20.0
20.8
20.5
104
103
71-127
1.4
20.0
* QC Fail Date: 03/31/2021 02:40 PM Page 15 of 18
Page 53 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-070-0007
QC Prep:
V1700
QC Analytical Batch(es): V1702
QC Prep Batch Method:
5030B
Analysis Method:
8260D
Analysis Description:
Volatile
Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V1700 LCSD-V1700
Spike
LCS LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec
% Rec
Limits
RPD
Max
RPD
Vinyl Acetate
pg/L
20.0
16.1 15.1
80.5
75.5
34-167
6.4
20.0
Vinyl Chloride
pg/L
20.0
23.3 21.6
117
108
57-141
7.5
20.0
o-Xylene
pg/L
20.0
20.4 19.6
102
98.0
78-128
4.0
20.0
m,p-Xylene
pg/L
40.0
42.6 41.1
107
103
77-133
3.5
20.0
4-Bromofluorobenzene (S)
95.8
93.2
80-124
Dibromofluoromethane (S)
110
104
75-129
1,2-Dichloroethane - d4 (S)
107
104
63-136
Toluene-d8(S)
103
101
77-123
Date: 03/31/2021 02:40 PM Page 16 of 18
Page 54 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County LF
Report No: 21-070-0007
QC Prep: V1610 QC Analytical Batch(es): V1613
QC Prep Batch Method: SW-9056A (PREP) Analysis Method: 9056A
Analysis Description: Anions by Ion Chromatography
Lab Reagent Blank LRB-V1610 Matrix: AQU
Associated Lab Samples: 94462, 94463, 94464
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Chloride
pg/L
<350
350
1000
03/11/21 13:44
Nitrate (NO3-N)
pg/L
<45.0
45.0
200
03/11/21 13:44
Sulfate
pg/L
<560
560
2000
03/11/21 13:44
Laboratory Control Sample
LCS-V1610
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Chloride
pg/L
40000
37400
94.0
90-110
Nitrate (NO3-N)
pg/L
4000
3610
90.0
90-110
Sulfate
pg/L
40000
38500
96.0
90-110
Matrix Spike & Matrix Spike Duplicate
V 94464-MS-V1610
V 94464-MSD-V1610
MS Spike
MSD
MS Result
MSD MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result %Rec
%Rec
Limits
RPD
RPD
Conc.
Chloride
pg/L
850
40000
40000
42000
41800 105
105
90-110
0.4
20
Nitrate(NO3-N)
pg/L
78.0
4000
4000
4070
4050 102
101
90-110
0.4
20
Sulfate
pg/L
1070
40000
40000
45500
45500 114*
114*
90-110
0.0
20
* QC Fail Date: 03/31/2021 02:40 PM Page 17 of 18
Page 55 of 58

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County LF
Report No:
21-070-0007
QC Analytical Batch:
V1600
Analysis Method:
SM-3500-Fe-13
Analysis Description:
Ferrous Iron
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
94462, 94463, 94464
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Ferrous Iron
pg/L
<50.0
50.0
200
03/12/21 12:15
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Ferrous Iron
pg/L
2000
2050
103
90-110
Matrix Spike & Matrix Spike Duplicate
V 94374-MS V 94374-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result
Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Ferrous Iron
pg/L
<50.0
2000
2000 1980
2000 99.0
100 80-120 1.0 20
Date: 03/31/2021 02:40 PM Page 18 of 18
Page 56 of 58

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01015
Customer Name: Anchor QEA of North Carolina, PLLC
Report Number: 21-070-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
® Other :
Thermometer ID:
CK
IRT-15 5.8C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
2
Custody seals intact on shipping container/cooler?
0 Yes
0 No
I* Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
I* Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
® Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
* N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Talon J Yelton Date & Time: 03/11/2021 12:40:34
Page 57 of 58

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Page 58 of 58

Waypointo
ANALYTICAL
3/31 /2021
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville, NC, 28801
Ref: Analytical Testing
Lab Report Number: 21-070-0010
Client Project Description: Jackson County Landfill
Site: 58-02
Project Number: 58-02
Dear Chuck Pippin:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/11/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a,j
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 24

Waypoint.0
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2021
North Carolina
State Program
402
12/31/2021
South Carolina
State Program
99012
07/31/2021
South Carolina
State Program
99012
12/31/2020
Page 1 of 1 00016/21-070-0010
Page 2 of 24

Sample Summary Table
Report Number:
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
Page 3 of 24

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Waypoint Analytical
ATTENTION
Angie Overcash
PROJECT
Anchor QEA of NC
LABORATORY REPORT
221031506
DATE
03/23/2021
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Pace Analytical Gulf Coast, 7979
Innovation Park Dr., Baton Rouge, LA 70820.
- Pace Gulf Coast is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab #
LA-01955, NELAP certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of Pace Guld Coast serving clients in the SC/NC/GA areas. All questions regarding this report
should be directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 221031506
Page 4 of 24
Page 1 of 19

aceAna lytical
LELAP CERTIFICATE NUMBER: 01955
DOD-ELAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
PERFORMED BY
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 03/23/2021
Report Y 211031506
�1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i III
Project Waypoint NC
Deliver To Additional Recipients
Ashley Amick Lab Reports, Access Analytical
Access Analytical Angela Martin, Access Analytical
15 Thames Valley Rd
Irmo, SC 29063
803-781-4243
PJLA
Testing
WD EU1P
V V
'I 7025
Lab Report#: 221031506
Page 5 of 24
Page 2 of 19

Report#: 221031506
Mayesal'
Project ID: Waypoint NC Report Date: 03/23/2021
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD OSM as specified in the contract if
applicable.
_� LQ,7e,—, �—
Authorized Signature
Pace Gulf Coast Report 221031506
Lab Report#: 221031506
Page 6 of 24
Page 3 of 19

Report#: 221031506
, accArut4ical _
Project ID: Waypoint NC Report Date: 03/23/2021
Certifications
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Lab Report#: 221031506
Page 7 of 24
Page 4 of 19

aceReport#: 221031506
Ar��lytical
Project ID: Waypoint NC Report Date: 03/23/2021
Case Narrative
Client: Access Analytical Report: 221031506
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
MISCELLANEOUS
Sample 22103150605 (MW-05R-20210309) was received with a minimal volume of sample.
Lab Report#: 221031506
Page 8 of 24
Page 5 of 19

aReport#: 221031506
. ceAr��lytical
Project ID: Waypoint NC Report Date: 03/23/2021
Sample Summary
LAB ID
Client ID
Matrix
Collect Date
22103150601
MW-01-20210310
Water
03/10/202113:38
22103150602
MW-02-20210310
Water
03/10/202114:15
22103150603
MW-03-20210309
Water
03/09/202113:48
22103150604
MW-04-20210309
Water
03/09/202110:00
22103150605
MW-05R-20210309
Water
03/09/202115:00
22103150606
MW-06-20210310
Water
03/10/202111:16
22103150607
MW-07-20210309
Water
03/09/202111:22
22103150608
MW-03-20210309
Bubble Strip
03/09/2021 13:48
22103150609
MW-04-20210309
Bubble Strip
03/09/2021 10:00
22103150610
MW-06-20210310
Bubble Strip
03/10/2021 11:16
22103150611
MW-07-20210309
Bubble Strip
03/10/2021 11:22
Receive Date
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
03/15/2021 10:45
Lab Report#: 221031506
Page 9 of 24
Page 6 of 19

a
. ceAr��lytical
Report#:
Project ID:
221031506
Waypoint NC
Report Date:
03/23/2021
Detect Summary
LAB ID
Client ID
Method
Parameter
Result
Units
22103150601
MW-01-20210310
AM23G
Acetic Acid
0.15J
mg/L
22103150601
MW-01-20210310
AM23G
Formic Acid
7.6
mg/L
22103150601
MW-01-20210310
AM20GAX
Methane
1700
ug/L
22103150601
MW-01-20210310
EPA RSK-175
Carbon Dioxide
108000
ug/L
22103150602
MW-02-20210310
AM23G
Acetic Acid
0.39J
mg/L
22103150602
MW-02-20210310
AM23G
Formic Acid
13
mg/L
22103150602
MW-02-20210310
AM20GAX
Methane
4.3J
ug/L
22103150602
MW-02-20210310
EPA RSK-175
Carbon Dioxide
29600
ug/L
22103150603
MW-03-20210309
AM23G
Acetic Acid
0.14J
mg/L
22103150603
MW-03-20210309
AM23G
Formic Acid
6.9
mg/L
22103150603
MW-03-20210309
AM20GAX
Methane
3.1 J
ug/L
22103150603
MW-03-20210309
EPA RSK-175
Carbon Dioxide
8310
ug/L
22103150604
MW-04-20210309
AM23G
Acetic Acid
0.13J
mg/L
22103150604
MW-04-20210309
AM23G
Formic Acid
6.9
mg/L
22103150604
MW-04-20210309
AM23G
Butyric Acid
0.073J
mg/L
22103150604
MW-04-20210309
AM20GAX
Methane
300
ug/L
22103150604
MW-04-20210309
EPA RSK-175
Carbon Dioxide
92900
ug/L
22103150605
MW-05R-20210309
AM23G
Formic Acid
74
mg/L
22103150605
MW-05R-20210309
AM20GAX
Methane
2300
ug/L
22103150605
MW-05R-20210309
AM20GAX
Ethane
0.57J
ug/L
22103150605
MW-05R-20210309
AM20GAX
Ethene
0.60J
ug/L
22103150605
MW-05R-20210309
EPA RSK-175
Carbon Dioxide
1460
ug/L
22103150606
MW-06-20210310
AM23G
Acetic Acid
0.13J
mg/L
22103150606
MW-06-20210310
AM23G
Formic Acid
6.6
mg/L
22103150606
MW-06-20210310
AM20GAX
Methane
25
ug/L
22103150606
MW-06-20210310
AM20GAX
Ethene
0.24J
ug/L
22103150606
MW-06-20210310
EPA RSK-175
Carbon Dioxide
150000
ug/L
22103150607
MW-07-20210309
AM23G
Formic Acid
7.5
mg/L
22103150607
MW-07-20210309
AM23G
Butyric Acid
0.21J
mg/L
22103150607
MW-07-20210309
AM20GAX
Methane
470
ug/L
22103150607
MW-07-20210309
AM20GAX
Ethane
0.21J
ug/L
22103150607
MW-07-20210309
AM20GAX
Ethene
0.20J
ug/L
22103150607
MW-07-20210309
EPA RSK-175
Carbon Dioxide
133000
ug/L
22103150608
MW-03-20210309
AM20GAX
Hydrogen
190
nM
22103150609
MW-04-20210309
AM20GAX
Hydrogen
19
nM
22103150610
MW-06-20210310
AM20GAX
Hydrogen
22
nM
22103150611
MW-07-20210309
AM20GAX
Hydrogen
9.2
nM
Lab Report#: 221031506
Page 10 of 24
Page 7 of 19

Report#: 221031506
aceAr�afytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
Sample Results
Collect Date 03/10/2021 13:38 LAB ID 22103150601
MW-01-20210310
Receive Date 03/15/2021 10:45 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 03/23/202114:19 JAR 706641
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 108000 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/22/202118:59 MOS 706530
CAS#
Parameter
Result
DL
LOQ
Units
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
64-19-7
Acetic Acid
0.151
0.12
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
64-18-6
Formic Acid
7.6
0.055
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
127-17-3
Pyruvic Acid
0.060LI
0.060
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/19/202115:33 JCK2 706424
CAS#
Parameter
Result
DL
LOQ
Units
74-82-8
Methane
1700
2.5
5.0
ug/L
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
Collect Date 03/10/2021 14:15 LAB ID 22103150602
MW-02-20210310
Receive Date 03/15/2021 10:45 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 03/23/202114:26 JAR 706641
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 29600 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 2 03/22/202121:39 MOS 706530
CAS# Parameter
50-21-5 Lactic Acid
64-19-7 Acetic Acid
Result DL LOQ Units
0.11 U 0.11 1.0 mg/L
0.39J 0.25 1.0 mg/L
Lab Report#: 221031506 Page 8 of 19
Page 11 of 24

Report#: 221031506
aceAr�afytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
Sample Results
Collect Date 03/10/2021 14:15 LAB ID 22103150602
MW-02-20210310
Receive Date 03/15/2021 10:45 Matrix Water
AM23G (Continued)
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 2 03/22/202121:39 MOS 706530
CAS#
Parameter
Result
DL
LOO
Units
79-09-4
Propionic Acid
0.11 U
0.11
1.0
mg/L
64-18-6
Formic Acid
13
0.11
1.0
mg/L
107-92-6
Butyric Acid
0.12U
0.12
1.0
mg/L
127-17-3
Pyruvic Acid
0.12U
0.12
1.0
mg/L
503-74-2
i-Pentanoic Acid
0.12U
0.12
1.0
mg/L
109-52-4
Pentanoic Acid
0.11 U
0.11
1.0
mg/L
646-07-1
i-Hexanoic Acid
0.11 U
0.11
1.0
mg/L
142-62-1
Hexanoic Acid
0.12U
0.12
1.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/19/202115:46 JCK2 706424
CAS#
Parameter
Result
DL
LOO
Units
74-82-8
Methane
4.3,1
2.5
5.0
ug/L
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
Collect Date 03/09/2021 13:48 LAB ID 22103150603
MW-03-20210309
Receive Date 03/15/2021 10:45 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/23/202114:39 JAR 706641
CAS# Parameter Result DL LOO Units
124-38-9 Carbon Dioxide 8310 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/22/202122:33 MOS 706530
CAS#
Parameter
50-21-5
Lactic Acid
64-19-7
Acetic Acid
79-09-4
Propionic Acid
64-18-6
Formic Acid
107-92-6
Butyric Acid
127-17-3
Pyruvic Acid
503-74-2
i-Pentanoic Acid
109-52-4
Pentanoic Acid
646-07-1
i-Hexanoic Acid
142-62-1
Hexanoic Acid
Result
DL
LOO
Units
0.053U
0.053
0.50
mg/L
0.14,1
0.12
0.50
mg/L
0.053U
0.053
0.50
mg/L
6.9
0.055
0.50
mg/L
0.058U
0.058
0.50
mg/L
0.060LI
0.060
0.50
mg/L
0.061 U
0.061
0.50
mg/L
0.056U
0.056
0.50
mg/L
0.056U
0.056
0.50
mg/L
0.058U
0.058
0.50
mg/L
Lab Report#: 221031506 Page 9 of 19
Page 12 of 24

Report#: 221031506
aceAr�afytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
Sample Results
Collect Date 03/09/2021 13:48 LAB ID 22103150603
MW-03-20210309
Receive Date 03/15/2021 10:45 Matrix Water
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/19/202115:57 JCK2 706424
CAS#
Parameter
Result
DL
LOQ
Units
74-82-8
Methane
3.1J
2.5
5.0
ug/L
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
Collect Date 03/09/2021 10:00 LAB ID 22103150604
MW-04-20210309
Receive Date 03/15/2021 10:45 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 03/23/202114:50 JAR 706641
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 92900 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/22/202123:26 MOS 706530
CAS#
Parameter
Result
DL
LOQ
Units
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
64-19-7
Acetic Acid
0.13,1
0.12
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
64-18-6
Formic Acid
6.9
0.055
0.50
mg/L
107-92-6
Butyric Acid
0.073J
0.058
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/19/202116:10 JCK2 706424
CAS#
Parameter
74-82-8
Methane
74-84-0
Ethane
74-85-1
Ethene
Result
DL
LOQ
Units
300
2.5
5.0
ug/L
0.075U
0.075
1.0
ug/L
0.12U
0.12
1.0
ug/L
Lab Report#: 221031506 Page 10 of 19
Page 13 of 24

Report#: 221031506
aceAr�afytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
Sample Results
Collect Date 03/09/2021 15:00 LAB ID 22103150605
M W-05 R-20210309
Receive Date 03/15/2021 10:45 Matrix Water
RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/23/202114:58 JAR 706641
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 1460 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 03/23/202100:20 MOS 706530
CAS#
Parameter
Result
DL
LOQ
Units
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
64-19-7
Acetic Acid
1.2U
1.2
5.0
mg/L
79-09-4
Propionic Acid
0.53U
0.53
5.0
mg/L
64-18-6
Formic Acid
74
0.55
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
127-17-3
Pyruvic Acid
0.60U
0.60
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/19/202116:22 JCK2 706424
Parameter
B Methane
D Ethane
1 Ethene
Result
DL
LOQ
Units
2300
2.5
5.0
ug/L
0.57,1
0.075
1.0
ug/L
0.60,1
0.12
1.0
ug/L
Collect Date 03/10/2021 11:16 LAB ID 22103150606
MW-06-20210310
Receive Date 03/15/2021 10:45 Matrix Water
RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 03/23/202115:14 JAR 706641
CAS# Parameter
124-38-9 Carbon Dioxide
AM23G
Result
DL
LOQ
Units
150000
2540
18000
ug/L
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/23/202101:13 MOS 706530
CAS#
Parameter
Result
DL
LOQ
Units
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
64-19-7
Acetic Acid
0.13,1
0.12
0.50
mg/L
Lab Report#: 221031506 Page 11 of 19
Page 14 of 24

Report#: 221031506
aceAr�afytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
Sample Results
Collect Date 03/10/2021 11:16 LAB ID 22103150606
MW-06-20210310
Receive Date 03/15/2021 10:45 Matrix Water
AM23G (Continued)
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/23/202101:13 MOS 706530
CAS#
Parameter
Result
DL
LOO
Units
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
64-18-6
Formic Acid
6.6
0.055
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/19/202116:34 JCK2 706424
CAS#
Parameter
Result
DL
LOO
Units
74-82-8
Methane
25
2.5
5.0
ug/L
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.24,1
0.12
1.0
ug/L
Collect Date 03/09/2021 11:22 LAB ID 22103150607
MW-07-20210309
Receive Date 03/15/2021 10:45 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 03/23/202115:10 JAR 706641
CAS# Parameter Result DL LOO Units
124-38-9 Carbon Dioxide 133000 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/23/202102:06 MOS 706530
CAS#
Parameter
50-21-5
Lactic Acid
64-19-7
Acetic Acid
79-09-4
Propionic Acid
64-18-6
Formic Acid
107-92-6
Butyric Acid
127-17-3
Pyruvic Acid
503-74-2
i-Pentanoic Acid
109-52-4
Pentanoic Acid
646-07-1
i-Hexanoic Acid
142-62-1
Hexanoic Acid
Result
DL
LOO
Units
0.053U
0.053
0.50
mg/L
0.12U
0.12
0.50
mg/L
0.053U
0.053
0.50
mg/L
7.5
0.055
0.50
mg/L
0.21 J
0.058
0.50
mg/L
0.060U
0.060
0.50
mg/L
0.061 U
0.061
0.50
mg/L
0.056U
0.056
0.50
mg/L
0.056U
0.056
0.50
mg/L
0.058U
0.058
0.50
mg/L
Lab Report#: 221031506 Page 12 of 19
Page 15 of 24

Report#: 221031506
aceAr�afytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
Sample Results
Collect Date 03/09/2021 11:22 LAB ID 22103150607
MW-07-20210309
Receive Date 03/15/2021 10:45 Matrix Water
JGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/19/202116:46 JCK2 706424
CAS#
Parameter
74-82-8
Methane
74-84-0
Ethane
74-85-1
Ethene
Result
DL
LOQ
Units
470
2.5
5.0
ug/L
0.21J
0.075
1.0
ug/L
0.20J
0.12
1.0
ug/L
Collect Date 03/09/2021 13:48 LAB ID 22103150608
MW-03-20210309
Receive Date 03/15/2021 10:45 Matrix Bubble Strip
JGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/16/202113:42 JCK2 706108
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 190 0.49 1.9 nM
Collect Date 03/09/2021 10:00 LAB ID 22103150609
MW-04-20210309
Receive Date 03/15/2021 10:45 Matrix Bubble Strip
JGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/16/202113:54 JCK2 706108
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 19 0.49 1.9 nM
Collect Date 03/10/2021 11:16 LAB ID 22103150610
MW-06-20210310
Receive Date 03/15/2021 10:45 Matrix Bubble Strip
JGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/16/202114:07 JCK2 706108
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
22
0.49
1.9
nM
Lab Report#: 221031506 Page 13 of 19
Page 16 of 24

Report#: 221031506
aceAr�afytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
Sample Results
Collect Date 03/10/2021 11:22 LAB ID 22103150611
MW-07-20210309
Receive Date 03/15/2021 10:45 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 03/16/202114:19 JCK2 706108
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOO
Units
9.2
0.49
1.9
nM
Lab Report#: 221031506 Page 14 of 19
Page 17 of 24

Report#: 221031506
aceArk�fytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
GC Volatiles QC Summary
Analytical Batch Client ID
MB706641
LCS706641
LCSD706641
706641 LAB ID
2159899
2159900
2159901
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
03/23/21 13:26
03/23/21 13:01
03/23/21 13:06
Matrix
Water
Water
Water
EPA RSK-175
Units
ug/L
Spike
I Result
%R
I
Control
I
Spike
Result
I
%R
I
RPD
I
RPD
Result
DLI
Added
Limits%R
Added
Limit
Carbon Dioxide 124-38-9
127U
127
8700
7650
88
38 - 147
8700
7440186
3
40
Lab Report#: 221031506
Page 18 of 24
Page 15 of 19

Report#: 221031506
aceArk�fytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
General Chemistry QC Summary
Analytical Batch Client ID
MB706530
LCS706530
LCSD706530
706530 LAB ID
2159385
2159386
2159387
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
03/22/21 20:46
03/22/21 19:53
03/23/21 03:53
Matrix
Water
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Lactic Acid
50-21-5
0.053U
0.053
2.0
2.0
101
70 - 130
2.0
2.0
101
0
20
Acetic Acid
64-19-7
0.12U
0.12
2.0
2.0
98
70 - 130
2.0
2.0
98
0
20
Propionic Acid
79-09-4
0.053U
0.053
2.0
1.9
95
70 - 130
2.0
1.9
94
1
20
Formic Acid
64-18-6
0.055U
0.055
2.0
1.8
91
70 - 130
2.0
1.8
90
1
20
Butyric Acid
107-92-6
0.058U
0.058
2.0
1.9
97
70 - 130
2.0
1.9
95
2
20
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
1.9
95
70 - 130
2.0
1.9
94
1
20
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
2.0
98
70 - 130
2.0
1.9
96
1
20
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
1.9
93
70 - 130
2.0
1.8
93
1
20
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
1.8
88
70 - 130
2.0
1.7
84
4
20
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
1.8
92
70 - 130
2.0
1.8
91
1
20
Lab Report#: 221031506
Page 19 of 24
Page 16 of 19

Report#: 221031506
aceArk�fytrcal
Project ID: Waypoint NC Report Date: 03/23/2021
General Chromatography QC Summary
Analytical Batch Client ID
MB706108
LCS706108
706108 LAB ID
2156920
2156921
Sample Type
MB
LCS
Prep Date
Analysis Date
03/16/21 11:34
03/16/21 12:25
Matrix
AM20GAX
Units
nM
Spike
I Result
%R
I
Control
I
Result
DL
Added
Limits%R
Hydrogen 1333-74-0
0.49U
1 0.49
121
14
11181
70 - 130
Analytical Batch
Client ID
MB706424
LCS706424
LCSD706424
706424
LAB ID
2158743
2158744
2158745
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
03/19/21 11:40
03/19/21 10:52
03/19/21 11:04
Matrix
Water
Water
Water
AM20GAX
Units
ug/L
Spike
I Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Methane
74-82-8
2.5J
2.5
490
490
99
70 - 130
490
500
102
2
20
Ethane
74 84 0
0.075U
0.075
100
110
105
70 130
100
110
107
2
20
Ethene
74-85-1
0.12U
0.12
140
150
106
70 - 130
140
150
108
1
20
Lab Report#: 221031506
Page 20 of 24
Page 17 of 19

CHAIN -OF -CUSTODY Analytical Request Document
LAB USE ONLY- Affix Wor
Pace/inalytrcal'
client ID:
4565 - Access Analytical
Chain -of-Custody is a LEGAL DOCUMENT- Complete all releventfield s
company:
Billing Information:
1
ALL SHAG .913G: 221031506
11111
lei ■
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1
Address: ' [
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Container Preservative Tj PM: Rwe
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Report To: �C '
Email To: Y [
•• preseroaItive Types: (1) nitric acid, [4 sulfuric acid, (3l hydrochloric
arid. I4J sodium hydroxide,[}) lint acetate,
Copy To:
Site Collection In/Address:, yl. l ! y�
11l hL�
(6) methanol, (7) sodium hisu Ifate, (9) sodium throsul fa M (9) hexane,
(C) ammonium hydroxide, (G) TSP, (U) Unpreserved, (0) Other____
(A) ascorbic acid, IHl ammonium surfa re,
Customer Project Name/Number:
' State: County/City: Time Zone Collected:
11GLG�S�1 [ 1 PT [ ] MT [ ] CT [ ] ET
Anal ses
Lah Profller'Line:
l,ab Sample Receipt Checklist:
Phone: gafUe(le[
Emai1:c-QF
Site/Famlity ID H: Co pliance Monitoring?
[ Yes
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Custody Seals PreSeDt:IlDtaCt Y N NA
custody Signatures present Y H NA
�
[ ]No
Collector signature Present Y N NA
Collected 13 y [print]:
purchase Order 9: DW PWS ID #:
gottlee intact Y H NA
correct Bottles r N NA
4uote 1l: It .JO] DW Location Code:
�i
Sufficient Volume Y N NA
Ca11ec I B si at
Turnaround Date Re uired: Immediately Packed on ice:
_ q
s'
Samples Received on lee Y N NA
VOA - Headspaco Acceptable Y N NA
USDA Regulated Soils Y N NA
es [ ]No
Sample Disposal: Rush: Field Filtered
Samples in Holding Tirne Y N NA
1`&ispose as appropriate [ )Re
{if a cable):
turn [ ] Same Day [ ] Next Day Yes WN❑
Residual Chlorine Present Y N NA
[ ]Archive'
[ ] Hold:
[ ]
( 1 2 Day [ 1 3 Day l 14 Day [ J 5 Day
Analysis:
�
Cl Strips:
Sample pH Acceptable Y N NA
Pa Strt.ptr%
IExpedlle Charges Appfy]
• Matrix Codes (Insert 1n Matrix box helow): Drinking Water [DW], Ground Water (G W), Wastewater (WW),
6
Sulfide Present Y N NA
Lead Acetate Strips:
Product ]P), Sall/Solid (SQ, Oil {01L), Wipe ]WP], Air {AR], Tissue (TS), Bioassay (B), Vapor (V), Other [OT1
y
Customer Sample ID
Comp/Collected (or Res tt f
Composite End
Matrix * Grab Composite
� sf
LAII i353 ONLY:
Lab SamPle # 1 Comments;
Start} CI Ctnos
Date Time Date Time
IuiNf-p L-3ta�in3 !
4
O�MW-43-?A7
❑ QC
J1
Roc)
�+ )(
W O -7b
A
� ��
tvv
5'
3'qC
D}'
j II I ff++ I++++II JJ++rrII++II
1 f ill�ll��Il
IIIIff ffJf I++ )jIIIIII 11++ jj (fIIIIII++++IIII++II IIJjj rr II llII
�f �il�l�llfll1i11f
ILL
mid A 03o
11 y
i!I! Illlll
Illll lff! 111 �11�1f a3° ;
�I }`
North
aort
Carolina, PLLC
"
Norih Camlina Landfills - SWS ID 13:14'08
Customer Remarks r' Special
Conditions Possible Hazards: Type of Ice Used: Wet Blue Dry None
I ---- H
SHORT HOLDS PAESENT(<72 hours): Y N N/A
Lab Sample Temperature Info:
■}rye
p �[j �ry `/� Peen Material Used:
C. ��'
LabTrackingM
2604868
Temp Blarik Received: Y N NA
Therm IDIt:
"' `— {/
`
U C7,[lCSx
Hadchem sampe[sj screened {�SDo Cpm }; Y N NA
Samples received via:
Cooler 1 Temp Upon Receipt:
Coo l er 1 Therm Corr. Factor:
oe
aC
FEDEX UPS Client Courier Pace Courier Cooler i Corrected Temp:oC
ReliMhby/c pa yi
ignature} Date/Time: Received by�Campany: ]Signature)
�
Oaterfime: MT1L LAB USE ONLY Comments:
10 � � f f11]
� � Lot r3 � Table it:
elinquished by/Company: {Signature) Date/Time: Receiv by'C mpany: (Signature)
Acctnum:
DatefTime:
!V �y
Vrdl
Template:
++ 1t[
TripBlank Received: Y N NA
HCL McOH TSP her
Rellnquis byr'C mpan
Ignaturej Date/Time: Recei ed by/Company, V-gnotuj
��1.�
Date e: pM;
Non Conformance{s]: Page:
l..r��
PB:
IYES ,r NO of:
--
`
2 1 I13 (-ZJ (0-' S W1.0 � .Y1 K[ Ad
Lab Report#: 221031506
Page 18 of 19
Page 21 of 24

)!2cennay+rca SAMPLE RECEIVING CHECKLIST IIIIIIIIIIII
SAMPLE DELIVERY GROUP
221031506
CHECKLIST
YES
NO
Client PM RWe
Transport Method
Samples received with proper thermal preservation?
*❑
❑
4565 - Access Analytical
F®DC
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
*❑
*❑
❑
❑
Profile Number
Received By
290404
N/bOune, Dodie K
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
*❑
0
❑
❑
Line Item(s)
Receive Date(s)
1 - Anchor
03/15/21
2- hydrogen
Preservative added to any containers?
❑
*❑
If received, was headspace for VOC water containers < 6mm?
*❑
❑
Samples collected in containers provided by Pace Gulf Coast?
0
❑
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer ID E26
Temp °C
None
None
173150123315
0.3
NOTES
Pevision 1.6
Page 1 of 1
Lab Report#: 221031506
Page 22 of 24
Page 19 of 19

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01015
Customer Name: Anchor QEA of North Carolina, PLLC
Report Number: 21-070-0010
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
® Other :
Thermometer ID:
CK
IRT-15 6.6C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
I* Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
I* Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
® Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
* N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Talon J Yelton Date & Time: 03/11/2021 13:17:16
Page 23 of 24

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