8603_Surry_Elkin_MSWLF_CDLF_Dec20GW_20210603

NC DENR
Division of Waste Management - Solid Waste
loaded: Yes / No) Doc/Event #:
Environmental Monitoring
Reoortina Form
Notice:
This
form and any
information attached
to
it are "Public Records"
as defined in NC
General Statute 132-1, As such, these documents are
available for
inspection and
examination by any
person upon request (NC
General Statute 132-6),
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 136 .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity.submitting data (laboratory, consultant, facility owner):
,Municipal Engineering Services Co., PA
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Jonathan Pfohl Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Surry County Closed C&D and Landfill Road off Joe Mill Lane (SR 1121) 86-03 .1600 December 21-22, 2020
Closed MSW Landfill -Elkin Elkin, NC 28621
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑X Detection Monitoring ❑X Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
Leachate monitoring data El
water monitoring data
Notification attached?
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
No. No groundwater or surface water standards were exceeded.
�< Yes, a nocation of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
rl Yes, a -notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, 1 have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levelsand a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that th
,ere
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Benjamin Clawson, P.E. Senior Project Manager [phone]
Facility Representative Name (P�t) Title (Area Code) Telephone Number
Signature
P.O. Box 97, Garner, NC 27529
Facility Representative Address
C-0281
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
3
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Date
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Affix NC Licensed/ Professional Geologist Seal
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Semi -Annual Water Quality Monitoring Report
December 2020
Prepared for
Surry County Closed C&D and Closed Landfill
Elkin, North Carolina
Permit No. 86-03
Prepared by
Municipal Engineering Services Company, P.A.
P.O. BOX 97
a SEAL-
• 0 r701#10
iN
V ♦ '
Benjamin Clawson, P.E.
Senior Project Manager
bclawsonr�mesco.com
Garner, North Carolina
MESCO Project Number: G20031.0
Nr1�1IVEC1��►6� �N�IIF•1��RIhJ
f66 SHIOWA91H DklVt, WANNtroo NO 27529 • PHtiN€i 919=772J53931
��.•��// Pit]. box :J4% CCtlH[, NC 2A607 ' PHONE: tlZ6��'�°17�fi
LICENSE NHMMM CM0291
Jonathan Pfohl
Environmental Specialist
jpfohigmesco.com

Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi -Annual Water Quality Monitoring Report for an event performed at the Surry County closed construction and
demolition (C&D) and closed unlined municipal solid waste landfill (MSWLF) located in Elkin NC (SWS Permit
No. 86-03) on December 21-22, 2020. The site is located at the end of Landfill Road off Joe Mill Lane (SR 1121),
Elkin, Surry County, North Carolina. The site location topographic map is depicted as Sheet 1.
NCDEQ Solid Waste Rule NCDEQ Solid Waste Rules 15ANCAC13B.1630 through .1637 require that Surry
County provide this monitoring report to the SWS on a semi-annual basis. In general accordance with 15A NCAC
1313.16320), the SWS Environmental Monitoring Report Form and SWS memorandums this report contains
sampling procedures, field and laboratory results, groundwater characterization and a brief discussion of the
findings. Detection tables, a potentiometric map, field parameters and the laboratory analytical reports with quality
assurance/quality control data and chains -of -custody (COC) are also included in this report.
Laboratory analytical results indicate that volatile organic compound(s) (VOC) were found above their reporting
limit and respective North Carolina Groundwater Standard in groundwater samples collected from 4 wells. Surface
water point SW-1 contained cadmium above its NC 2B Surface water Standard.
Background
Prior to operating as a C&D landfill the site operated as an unlined sanitary MSWLF that consisted of two units.
The first area was closed prior to October 1991 with a 24 inch final soil cover. The second area was closed with a
cohesive cap of 18 inches of soil with a minimum permeability of less than 1 x 10-5 cm/sec, and 18 inches of
erosive layer prior to December 31, 1998 in accordance with the Transition Plan. C&D was placed on top of the
cohesive capped MSW unit until 2008. The transfer station that operated at the landfill closed around June 2010
and the site has remained vacant since.
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available
since 1994. The landfill has been in assessment monitoring since 1997 in response to detections of VOCs. The
SWS approved a modification to the assessment monitoring program on October 15, 2014 (DIN:21983) which
entails a subset of wells to be sampled for Appendix II parameters once every three years which was performed
during this event.
Sampling Locations
The groundwater monitoring network includes 12 locations; nine downgradient monitoring wells (MW-2, MW-3,
MW-3A, MW-4, MW-5, MW-6, MW-7S, MW-7D and MW-8), a background monitoring well (MW-1) and two
downstream surface water points (SW-1, SW-2). All locations were sampled during this event. Water monitoring
locations are depicted on Sheet 2. A summary detailing the construction of the water monitoring wells is
presented on Table 1.

Sampling Procedures
Sampling was conducted utilizing portable methodologies outlined in the NCDENR SWS guidance document Solid
Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008. The function
and integrity of all monitoring locations were visually evaluated as documented on Table 2. The depth to water in
each well was electronically gaged prior to purging to quantify the static water level elevation. Bailing or
submersible pumping was utilized to purge the wells a minimum of three times the volume of standing water in the
well or until dry. Surface water samples were dipped from the surface of Snow Creek at previously designated
locations. Stabilized field parameters were recorded during purging. Samples were then placed into laboratory -
prepared, pre -preserved containers. Samples were kept on ice and transported to a NC -certified laboratory under
proper chain of custody (C-O-C) protocol within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters recorded during purging included pH, specific conductance, temperature, hardness and
turbidity. A summary of the field parameter data is presented in Table 3 and field data sheets are in Appendix A.
In general field parameter results remain consistent with previously reported events.
Laboratory Results
Pace Analytical Laboratories (PACE) (NC Cert. #12 & 40) performed the laboratory analysis. Pace reported that
their procedures conformed to the most current, applicable TNI/NELAC standards and the their Quality Assurance
Manual, where applicable, unless otherwise noted in the body of the laboratory report.
Groundwater samples were tested for constituents listed in 40 CFR 258 Appendix II and 1,4-dioxane. Surface water
samples were analyzed for parameters listed in 40 CFR 258 Appendix I and 1,4-dioxane. A sampling and analysis
table summarizing the locations, targeted constituents and methods is presented as Table 4. Laboratory results and
C-O-Cs are presented in Appendix B.
Water samples were analyzed to the laboratory -established Method Detection Limits (MDL) and any value between
the MDL and laboratory -established Reporting Limit (RL) is qualified by the laboratory as with a "J" which
indicates an estimated concentration. "J-qualified" concentrations are considered non -quantifiable and discretion
should be made prior to making decisions based on a value that the laboratory considers an estimate. Table 5
summarizes constituents detected in groundwater samples compared to Interim Maximum Allowable
Concentrations (IMAC) and North Carolina Groundwater Standards (2L) which are recognized by the NC SWS as
groundwater compliance Standards. Although not applicable for regulatory compliance purposes the detections are
also compared to the Maximum Contaminant Level (MCL) commonly referenced as the Federal Primary "Drinking
Water Standard". Table 6 lists the constituents detected in surface water samples compared to the current version
of the Division of Water Quality Surface Water Quality Tables.
2

Groundwater Samples Above Standards
Metals
One or two total recoverable metals were detected above their respective NC 2L/IMAC value in samples collected
from six wells as summarized below.
Metals Detected Above Standards
Arsenic
Cadmium
Cobalt
2L/IMAC
10
2
1
MW-1
MW-2
159
6.8
MW-3
2.1
MW-3A
16.4
MW-6
26.1
ug/L
VOCs
Benzene was detected in sample MW-2 (1.9 ug/L) and MW-3 (1.5 ug/L) which is above its NC 2L Standard (1
ug/L). 1,4-dioxane was also found in sample MW-2 at 173 ug/L which is above the NC 2L Standard (3 ug/L).
Surface Water Samples Above Standards
Total cadmium was detected at 1.8 ug/L in surface water sample SW-1. After applying a conversion factor the
dissolved phase is 1.76 ug/L which is above its calculated NC 2B Surface water Standard (1.23 ug/L).
Groundwater Characterization
A single -day potentiometric map constructed from groundwater levels collected during this event is presented as
Sheet 2. Groundwater flow rates and directions were calculated and are included in Table 7. Groundwater flows
generally southwest, towards the Snow Creek discharge feature. Groundwater average linear velocity rates
calculated from modified Darcy's equation indicate flow rates ranged from approximately 90 ft/yr (MW5) to 290
ft/yr (MW-4).
Findings
All constituents remain within their respective historically identified range except for arsenic in sample MW-2.
The reduction in VOC concentrations over time and distance from the landfill and the prevalence of biodegradation
byproducts indicate natural attenuation is occurring and groundwater quality is expected to continue to improve.
Cadmium was elevated in surface water sample SW-1 which is inconsistent with historical results (4 detections
over past 46 events). Cadmium was not detected in surface water sample SW-2 collected further downstream.
A low "j-qualified" concentration of sulfide in sample MW-2 was the only constituent detected which is not listed
in 40 CFR Appendix I.
Closing
Semi-annual water quality assessment monitoring is planned to be performed again in June 2021. Notwithstanding
any changes samples will be tested for Appendix II parameters in the winter of 2023.
3

Sheets

Topographic Map with Site Location
Surry County Closed MSW/C&D Landfill - Elkin
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ROAD CLASSIFICATION
QUADRANGLE LEGEND Primary highway, Light -duty road, hard or
hard surface ..... _.............. improved surface........ --
Secondary highway,
= 2�00� hard surface Unimproved road --_-- 1
Interstate Route C3 U. S. Route 0 State Route
Landfill Road (Off Joe Mill Ln SR 1121)
Elkin, NC 28621
Lat:36-17-49.4007
Long:-80-46-20.6499
Northing:931704.33
Easting:1477683.95
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NOTES:
1. TOPOGRAPHIC CONTOURS FROM NC ONEMAP (11-2013)
2. WELL LOCATIONS PLOTTED WITH ELEVATIONS EXTRAPOLATED
FROM AERIAL PHOTOGPAHY INSPECTION
3. PARCEL BOUNDARY FROM NC ONEMAP (10/2018)
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Tables

Table 1
Groundwater Monitoring Well Construction Table
December 21-22, 2020
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length
Geology of Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
Latitude
Longitude
(inches)
(ft bgs)
(ft bgs)
(ft)
(ft amsl)
(ft amsl)
(ft amsl)
(ft btoc)
MW-1
11/28/89
4
80
70
10
Soil
1042
1041
991
50.63
36.29711
-80.77236
MW-2
11/08/89
4
79
69
10
Soil
948
947
895
53.45
36.29572
-80.77620
MW-3
11/28/89
4
63
53
10
Soil
932
931
884
48.27
36.29362
-80.77646
MW-3A
09/16/94
2
40
24
16
Fractured Rock
927
924
896
30.38
36.29457
-80.77675
MW-4
09/15/94
2
29
13
16
Fractured Rock
933
929
922
10.23
36.29379
-80.77528
MW-5
09/15/94
2
31
16
15
Fractured Rock
949
845
939
9.72
36.29450
-80.77456
MW-6
09/15/94
2
66
51
15
Fractured Rock
1005
1002
960
44.51
36.29780
-80.77270
MW-7S
06/05/01
2
24
9
15
Fractured Rock
901
889
891
10.47
36.29407
-80.77730
MW-7D
06/05/01
2
90
80
10
Fractured Rock
901
889
887
14.17
36.29407
-80.77730
MW-8
06/04/01
1 2
1 67
52
15
Fractured Rock
1015
1013
978
37.18
36.29739
1 -80.77246
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Slurry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 2
Field Observations of Monitoring Locations
December 21-22, 2020
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears to
be Effective
Comments
MW-1
Yes
Yes
Yes
Yes
Yes
Yes
4" Diameter.
MW-2
Yes
Yes
Yes
Yes
Yes
Yes
4" Diameter. Slow Recharge. Strong odor
MW-3
Yes
Yes
Yes
Yes
Yes
Yes
4" Diameter. Slow Recharge. Purge water odor
MW-3A
Yes
Yes
Yes
Yes
Yes
Unknown
Concrete pad covered with soi. Purge water odor
MW-4
Yes
Yes
Yes
Yes
Yes
Yes
MW-5
Yes
Yes
Yes
Yes
Yes
Unknown
Concrete pad covered with soil.
MW-6
Yes
Yes
Yes
Yes
Yes
Yes
Trees across path
MW-7S
Yes
Yes
Yes
Yes
Yes
Yes
MW-71)
Yes
Yes
Yes
Yes
Yes
Yes
pH elevated likely grout intrusion
MW-8
Yes
Yes
Yes
Yes
Yes
Yes
Purge water odor
SW-1
Yes
-
-
-
-
Moderate gage & high flow
SW-2
Yes
-
-
-
-
Moderate gage & high flow
Any unusual field conditions, observations, or events:
Facility no longer in operation or occupied since transfer station closed in - June 2010.
Vehicle access improved by County since last event.
Slurry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 3
Field Parameter Data Summary
December 21-22, 2020
Depth to
Water
Water
Elevation*
TOC
Elevation*
Temp.
pH
Specific
Conductance
Hardness
Turbidity of
Metals Sample
Parameter
ft (btoc)
ft (amsl)
ft (amsl)
C
SU
umhos/cm
mg/L
NTU
MW-1
50.63
991
1042.00
15.3
7.48
73
--
0.94
MW-2
53.45
895
948.00
14.8
7.11
1815
--
52.6
MW-3
48.27
884
932.00
14.1
7.35
191
--
14.1
MW-3A
30.38
896
926.50
14.7
7.63
665
--
1.90
MW-4
10.23
922
932.50
13.4
7.61
40
--
3.91
MW-5
9.72
939
948.50
14.1
7.86
59
--
8.35
MW-6
44.51
960
1004.50
13.4
7.03
330
--
5.92
MW-7S
10.47
891
901.01
14.9
7.93
194
--
0.85
MW-7D
14.17
887
900.95
14.9
7.06
372
--
2.15
MW-8
37.18
978
1014.87
14.2
7.07
146
--
16.5
Minimum
9.72
884
900.95
13.4
7.03
40
--
0.85
Average
30.90
924
955.08
14.4
7.4
389
--
10.7
Maximum
53.45
991
1042.00
15.3
7.93
1815
--
52.6
SW-1
-
-
-
6.6
8.32
64
40
11.9
SW-2
-
-
-
6.8
8.01
62
40
10.4
Minimum
-
-
-
6.6
8.01
62
40
10.4
Average
-
-
-
-
6.7
8.17
63
40
11.2
Maximum
-
-
6.8
8.32
64
40
11.9
NOTES:
= Elevation extrapolated from photo inspected LIDAR released in 2007 by NCDOT (Not Surveyed).
btoc = below top of casing
amsl = above mean sea level
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 4
Sampling and Analysis Summary
December 21-22, 2020
App. I
Other
App. II
Field Parameters
m
U
a
O
O
O
U
co
�
Q
•C
O-0
-0
(c
2)
N
O
N
CU
m
T
U
O
(6
O
�
c6
O
U
U
=
N
-
N
>
O
N
9
O
7
N
M
O
=
>
F-
F->
a-
M:
a-
cn
F-
U)
F-=
U
Q
F-
0
0
0
0
r
0
r-
m
Q
0
U)
o
O
O
O
Co
�_
—
Q
N
O
,1-
O
N
00
O
(0
N
00
O
(0
O
CY)
O
00
LO
�
O
00
N
00
O
0)
V
00
N
N
N
0)
ww
a
a
a
s
a
a
a
Y
w
w
w
w
w
w
w
w
w
-0ca
co
ca
M
M
ca
co
M
70-0-0-0
a�
a�
a�
a�
70
m
J
J
co
J
J
J
J
J
J
co
J
J
LL
LL
LL
LL
LL
MW-1
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-2
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-3
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-3A
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-4
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-5
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-6
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-7S
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-7D
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-8
x
x
x
x
x
x
x
x
x
x
x
x
x
SW-1
x
x
x
x
x
x
x
x
SW-2
x
x
x
x
x
x
x
x
App I & II = Lists from current 40 CFR 258
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 5
Groundwater Sample Detections
December 22, 2020
Parameter Name
MDL
RL
2L Standard
MCL
MW-1
MW-2
MW-3
MW-3A
MW-4
MW-5
MW-6
MW-7D
MW-7S
MW-8
IMAC Value*
BG
S
S
S
S
S
S
S
S
S
Metals Tar
eted 40CFR 258 Appendix I
Antimony, total
3
5
1
6
4.2 J
Arsenic, total
4.7
10
10
10
159 (L)
Barium, total
3.5
5
700
2000
29
320
65.8
312
23.2
21.1
93.7
10.7
75.8
42.8
Cadmium, total
0.4
1
2
5
0.74 J
1.6
2.1 (L)
1.4
1.4
1.2
0.98 J
0.47 J
0.99 J
Cobalt, total
3.6
5
1
NE
6.8 (L)
16.4 (L)
26.1 (L)
4.1 J
Nickel, total
3.5
5
100
NE
4.2 J
29.7
21.5
8.8
Zinc, total
1 9.5
1 10
1000
NE
16.3
VOCs Tar eted 40CFR 258 Appendix I & 1 4-Dioxane
1,1-Dichloroethane
0.27
1
6
NE
0.37J
1,2,4-Trichlorobenzene
0.22
1
70
7
1.2
1,2-Dichlorobenzene
0.29
1
20
NE
3.6
1.9
2.1
0.57 J
1,2-Dichloroethane
0.34
1
0.4
5
0.46 J
1,2-Dichloropropane
0.19
1
0.6
5
0.41 J
1,4-Dichlorobenzene
0.26
1
6
75
4.6
2.9
2.6
3.4
0.97 J
1,4-Dioxane
56.2
150
3
NE
173 (L)
Acetone
6.2
25
6000
NE
17.2 J
Benzene
0.15
1
1
5
1.9 (L)
1.5 (L)
0.28 J
0.69 J
0.57 J
Chlorobenzene
0.23
1
50
100
4.1
0.57 J
1.6
9.1
0.56 J
cis-1,2-Dichloroethene
0.29
1
70
70
6.7
4.4
2.7
0.37 J
1.4
4
Toluene
0.24
1
600
1000
0.48 J
Trichloroethene
0.22
1
3
5
0.66 J
0.5 J
Targeted
40CFR
258 A endix
II
Sulfide 50 100 NE
Notes:
Units ug/L unless shown otherwise, Blank cells means not detected above MDL, NE means not established.
BG= Background Well Sample, S = Seminal Well Sample
Bold Above RL and Established 21-/IMAC
Above Established Federal MCL Drinking Water Std. (NOT a regulatory compliance Standard)
U= Well Upgradient, D = Well Downgradient
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
RL = Reporting Limit defined by Pace laboratory as "The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix."
2L Standard and IMAC Values recognized by the NC SWS as regulatory groundater Standards.
2L = NC 2L Groundater Standard 15A NCAC 02L .0202
IMAC = Interim Maximum Allowable Concentration
MCL = Maximum Contaminant Level for drinking water established by the USEPA.
J = "J-qualified". Defined by the lab as "estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
(L) Preliminary source is believed to be anthropogenic with Landfill Gas Wor leachate as suspected transport mechanism.
A definitive source of the detections was not determined as part of this report.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 6
Surface Water Sample Detections
December 22, 2020
Parameter Name
MDL
RL
NC 2B
STD
EPA 2
NRWQC
NC 3
ISTV
MCL4
SWA
SW-2
Downstream
Downstream
Targeted 40CFR 258 Appendix I & 1 4-Dioxane
Barium, total
0.03
1
NE
NE
200,000
2000
20
19.6
Cadmium, total
0.4
1
NE
NE
NE
5
1.8
Cadmium, dissolved"
0.21
1.76
Hardness
Hardness 20,000 NE NE NE NE NE 40,000 40,000
Notes:
Units ug/L unless indicated otherwise, Blank cells means Not Detected, NE means Not Established
J = "J-qualified" by lab and defined as estimated concentration above the adusted method detection limit and below the adusted reporting limit.
Bold Above Applicable Established 2B Std.
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
RL = Reporting Limit defined by Pace laboratory as "The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte
in a specific matrix."
Receivina surface water is Snow Creek 02-62-15) Class C
1 NC 2B STD = North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters. Presumed NC SWS adopted the numerical Standard for regulatory compliance purposes
2B Standard for cadmium is in the dissolved form and is determined via a calculation (below) for acute that is dependent upon hardness.
Cadmium 2B Standard calculation (chronic):WER*[(1.101672-[In hardness](0.041838))*eA(0.7998[In hardness]-4.4451)]
*Total to dissolved conversion factor for Cadmium is 0.98 = (1.136672-[In hardness](0.041838))
2 EPA NRWQC = EPA Nationally Recommended Water Quality Criteria for Aquatic Life & Human Health.
Nationally Recommended Water Quality Criteria for which NC does not have a Water Quality Standard for one or more uses.
s NC ISTV= North Carolina In -Stream Target Value. Established per language in 15A NCAC 02B .0202 & .0208. Contact DW R staff for further information.
NC PV for barium from fresh and salt water All waters (Class C & SC) for fish consumption.
4 MCL= Maximum Contaminant Level. Federal "Primary Drinking Water Standard". Shown for comparison purposes only. Not applicable for regulatory compliance purposes.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 7
Hydrologic Properties at Monitoring Locations
December 21, 2020
Monitoring
Well
Hydraulic
Conductivity
(cm/second)
Effective
Porosity
N
Hydraulic
Gradient
(feet/feet)
Groundwater
Average Linear
Velocity Rate
(feet/year)
Flow
Direction
Depth to
Groundwater
(ft btoc)
Groundwater
Potentiometric
Elevation*
(ft amsl)
Screened Interval
Lithology
MW-1
9.90E-05
5
0.240
492
N37W
50.63
991
Clay
MW-2
2.00E-05
5
na
na
na
53.45
895**
Clay
MW-3
5.00E-05
5
na
na
na
48.27
884**
Clay
Minimum
2.00E-05
5
0.240
492
-
48.27
884
-
Average
5.63E-05
5
0.240
492
-
50.78
923
-
Maximum
9.90E-05
5
0.240
492
-
53.45
991
-
MW-3A
2.50E-05
5
0.190
99
S60W
30.38
896
Fractured Rock
MW-4
4.20E-04
5
0.033
290
S66W
10.23
922
Fractured Rock
MW-5
2.70E-04
5
0.016
90
N75W
9.72
939
Fractured Rock
MW-6
1.20E-04
5
0.063
155
N10W
44.51
960
Fractured Rock
MW-7S
2.30E-04
5
0.048
227
S78W
10.47
891
Fractured Rock
MW-7D
na
na
na
na
na
14.17
887**
Fractured Rock
MW-8
2.40E-05
5
0.300
149
N25W
37.18
978
Fractured Rock
Minimum
2.40E-05
5
0.016
90
-
9.72
896
-
Average
1.82E-04
5
0.108
168
-
22.38
925
-
Maximum
4.20E-04
1 5
1 0.300
290
1-
44.51
1 939
1-
NOTE: Effective porosity data obtained from GAI Consultants' January 1995 Groundwater Sampling Report.
Hydraulic conductivity values from MW-7S and MW-8 derived from slug tests performed by Joyce Engineering on July 25, 2001.
Values for MW-1 through MW-6 obtained from GAI consultants' January 1995 Groundwater Sampling Report.
Hydrologic gradient calculated from groundwater elevations recorded December 21, 2020.
Wells screened in both the upper bedrock & unconfined aquifer utilized for flow directions/gradients.
= Datum used to determine elevation extrapolated from photo inspected LIDAR released 2007 by NCDOT (Not Surveyed).
* = Denotes wells with depressed potentiometric head. Therefore, flow directions and rates not calculable.
Average Linear Velocity Rate (Q) is defined by modified Darcy's equation:
where _ K A
Q ne dl
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Appendix A
Field Sampling Parameter Data Sheet(s)

. r
�l fiA kllw� /�� 1 �'�� l kl uv I �,
.,� � wn �
Project: Surry Co Closed MSWLF &Closed C&[) I_F, Elkin Samplers: _ Page_1—of-1
� : � � ��
Sampling
Parameters
Water
Quality
Parameters
Monitoring
Purge
Purge
Sample
Sample
De th to
p
Water
Lab
Volume
Sampl
oes
Dry
Total
Depth
Totai
CO2
DO
Tem p'
Specific
TDS
�'
:o
Hard -
Point
Date
Time
Date
Time
Parameters
to be
purged
e Type
Durin
Measured
Depth
(mg/I)
(i7tg/L)
ORP
pH
©
Cond,
(mg/L)
�
Hess
(BTOP)
(Gal)
�
as
Expected
(us/cm
�
(mg/L)
�,�
�(%�
Static
analyzed for
e
ex acted
MW-1
�.�
9,���
�d-i'�"
����
I(�)
�? �
��v=r'
�
80
�r
d ✓
�a
MW-2
�) �
r � �I
I(5)
� u
;:,;
�`
79
�'f �'
' 4,`'
� � �_
�; r �
MW-3
�- � �
� � � �.
I(I)
;'F�
;
80
'�, �.
! �! )
�/ �
@ `f r
1
�..�
_
40
,�'�a
f � ,
� l
���
�„�
t � � `�
t-i �
� : �[ .
MW-4
� � ; i �
L �. �.�
I(0)
i �`
( �
�`��'
29
MW-5
j " � b
�?.
I(0)
� f
��
'.-�
31
`p,u�=
!, t
`-
�,3�
MW-6
)7 �3��'
`��;JI
I(3)
��`
;�
�`,`
46
��S<^����,�
_
��?
C� ,�
->��`'
�,�
MW-7S
�"�. ;8/
�_� �
I(6)
��
�� i�
24
� °a, �
,n
�7, `") `
Z ' �`'
_� � �
� r �
MW-7D
__
�' ; L
l �i , Z �
I(0)
Q �
''Si-t 4�
�.
90
�
� �, �
� �-
� l
MW-8
�
` ��
� ��, f �
I(4)
�
'�` >
',r
67
� ;t
�
<J .
� '''f. �
" `� �
B �
�
` -
— -
I(0)
-
i � . n
-
-
-
�-
Mtn rya �.,.
� , � i
�j �'
�'� ,��._._
j t.�,�. �
S W-2
-
�
{
SS B=Stainless Steel Baler,
D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly l'urbid, C=Clear
NR=No Reading Attempted, NS=No Sample Obtained

Appendix B
Laboratory Analysis Reports
Chains of Custody

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 06, 2021
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 22, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Steven R. Gandy, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
r
e
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 118

laneAnalytical
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21LA 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92513376001
MW-1
Water
12/22/2010:43
12/22/20 15:20
92513376002
MW-2
Water
12/22/20 08:36
12/22/20 15:20
92513376003
MW-3
Water
12/22/20 09:55
12/22/20 15:20
92513376004
MW-3A
Water
12/22/20 08:49
12/22/20 15:20
92513376005
MW-4
Water
12/22/2010:18
12/22/20 15:20
92513376006
MW-5
Water
12/22/2010:36
12/22/20 15:20
92513376007
MW-6
Water
12/22/2010:50
12/22/20 15:20
92513376008
MW-7S
Water
12/22/20 09:03
12/22/20 15:20
92513376009
MW-7D
Water
12/22/20 09:07
12/22/20 15:20
92513376010
MW-8
Water
12/22/2010:58
12/22/20 15:20
92513376011
SW-1
Water
12/22/20 09:12
12/22/20 15:20
92513376012
SW-2
Water
12/22/20 09:19
12/22/20 15:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
SURRY CLOSED LF ELKIN
92513376
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92513376001
MW-1
EPA 8151
MTJ
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376002
MW-2
EPA 8151
MTJ
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376003
MW-3
EPA 8151
MTJ
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376004
MW-3A
EPA 8151
MTJ
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 118

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9800 Kincey Ave. Suite 100
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[phone]
SAMPLE ANALYTE COUNT
Project:
SURRY CLOSED LF ELKIN
Pace Project No.:
92513376
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376005
MW-4
EPA 8151
MTJ
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376006
MW-5
EPA 8151
MTJ
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376007
MW-6
EPA 8151
MTJ
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601 OD
IDS, RDT
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376008
MW-7S
EPA 8151
TAB
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601 OD
IDS, RDT
15
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376009
MW-71)
EPA 8151
TAB
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601 OD
IDS, RDT
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376010
MW-8
EPA 8151
TAB
5
PAN
EPA 8081 B
SEM
21
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8270E
PKS
111
PASI-C
EPA 8260D
BSH
66
PASI-C
SM 4500-S2D-2011
NAL
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92513376011
SW-1
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8260D
BSH
66
PASI-C
92513376012
SW-2
EPA 601OD
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8260D
BSH
66
PASI-C
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-1
Lab ID:
92513376001
Collected:
12/22/20 10:43
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/24/20 18:58
12/28/20 20:43
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/24/20 18:58
12/28/20 20:43
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/24/20 18:58
12/28/20 20:43
93-76-5
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/24/20 18:58
12/28/20 20:43
93-72-1
Surrogates
2,4-DCAA (S)
69.8
%
14.0-158
1
12/24/20 18:58
12/28/20 20:43
19719-28-9
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 09:48
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 09:48
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 09:48
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 09:48
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 09:48
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 09:48
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 09:48
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 09:48
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 09:48
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 09:48
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 09:48
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 09:48
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 09:48
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 09:48
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 09:48
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 09:48
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 09:48
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 09:48
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 09:48
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
86
%
10-184
1
12/28/20 20:12
12/31/20 09:48
877-09-8
Decachlorobiphenyl (S)
101
%
10-154
1
12/28/20 20:12
12/31/20 09:48
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 3510C
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 15:54
12674-11-2 R1
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 15:54
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 15:54
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 15:54
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 15:54
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 15:54
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 15:54
11096-82-5 R1
Surrogates
Decachlorobiphenyl (S)
98
%
10-181
1
12/28/20 20:12
12/30/20 15:54
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MWA Lab ID: 92513376001 Collected: 12/22/20 10:43 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:05
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:05
7440-38-2
Barium
29.0
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:05
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:05
7440-41-7
Cadmium
0.74.1
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:05
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:05
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:05
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:05
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:05
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:05
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:05
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:05
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:05
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:05
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:05
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/2011:24
12/31/2019:28
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:10 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 11:37
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 11:37
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 11:37
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 11:37
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 11:37
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 11:37
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 11:37
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 11:37
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 11:37
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 11:37
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 11:37
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 11:37
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 11:37
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 11:37
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 11:37
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 11:37
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 11:37
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 8 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-1 Lab ID: 92513376001 Collected: 12/22/20 10:43 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 11:37
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 11:37
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 11:37
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 11:37
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 11:37
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 11:37
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 11:37
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 11:37
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 11:37
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 11:37
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 11:37
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 11:37
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 11:37
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 11:37
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 11:37
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 11:37
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 11:37
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 11:37
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 11:37
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 11:37
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 11:37
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 11:37
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 11:37
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 11:37
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 11:37
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 11:37
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 11:37
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 11:37
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 11:37
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 11:37
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 11:37
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 11:37
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 11:37
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 11:37
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 11:37
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 11:37
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 11:37
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 11:37
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 11:37
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 11:37
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 11:37
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
IH
L2
L2
v1
IL
IH,v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-1 Lab ID: 92513376001 Collected: 12/22/20 10:43 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 11:37
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 11:37
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 11:37
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 11:37
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 11:37
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 11:37
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 11:37
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 11:37
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 11:37
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 11:37
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 11:37
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 11:37
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 11:37
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 11:37
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 11:37
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 11:37
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 11:37
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 11:37
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 11:37
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 11:37
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 11:37
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 11:37
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 11:37
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 11:37
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 11:37
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 11:37
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 11:37
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 11:37
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 11:37
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 11:37
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 11:37
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 11:37
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 11:37
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 11:37
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 11:37
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 11:37
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 11:37
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 11:37
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 11:37
99-35-4
45
%
10-144
1
12/28/20 08:59
12/29/20 11:37
4165-60-0
16
%
10-130
1
12/28/20 08:59
12/29/20 11:37
321-60-8
116
%
34-163
1
12/28/20 08:59
12/29/20 11:37
1718-51-0
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
IH
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-1 Lab ID: 92513376001 Collected: 12/22/20 10:43 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
9
%
10-130
1
12/28/20 08:59 12/29/20 11:37
13127-88-3 SO
15
%
10-130
1
12/28/20 08:59 12/29/20 11:37
367-12-4
23
%
10-144
1
12/28/20 08:59 12/29/20 11:37
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 03:07
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 03:07
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 03:07
107-02-8 IH,v2
ND
ug/L
10.0
0.90
1
12/24/20 03:07
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 03:07
107-05-1
ND
ug/L
1.0
0.15
1
12/24/20 03:07
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 03:07
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 03:07
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 03:07
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 03:07
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 03:07
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 03:07
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 03:07
56-23-5
ND
ug/L
1.0
0.23
1
12/24/20 03:07
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 03:07
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 03:07
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 03:07
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 03:07
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 03:07
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 03:07
74-95-3
ND
ug/L
1.0
0.29
1
12/24/20 03:07
95-50-1
ND
ug/L
1.0
0.26
1
12/24/20 03:07
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 03:07
110-57-6 IH
ND
ug/L
1.0
0.23
1
12/24/20 03:07
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 03:07
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 03:07
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 03:07
75-35-4
ND
ug/L
1.0
0.29
1
12/24/20 03:07
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 03:07
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 03:07
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 03:07
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 03:07
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 03:07
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 03:07
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 03:07
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 03:07
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 03:07
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 03:07
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MWA Lab ID: 92513376001 Collected: 12/22/20 10:43 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 03:07
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 03:07
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 03:07
74-88-4
ND
ug/L
100
66.4
1
12/24/20 03:07
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 03:07
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 03:07
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 03:07
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 03:07
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 03:07
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 03:07
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 03:07
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 03:07
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 03:07
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 03:07
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 03:07
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 03:07
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 03:07
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 03:07
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 03:07
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 03:07
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 03:07
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 03:07
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 03:07
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 03:07
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 03:07
1330-20-7
99
%
70-130
1
12/24/20 03:07
460-00-4
95
%
70-130
1
12/24/20 03:07
17060-07-0
100
%
70-130
1
12/24/20 03:07
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100 50.0 1 12/28/2013:45 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 03:32 12/29/20 22:45 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-2
Lab ID:
92513376002
Collected:
12/22/20 08:36
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/24/20 18:58
12/28/20 20:57
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/24/20 18:58
12/28/20 20:57
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/24/20 18:58
12/28/20 20:57
93-76-5
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/24/20 18:58
12/28/20 20:57
93-72-1
Surrogates
2,4-DCAA (S)
444
%
14.0-158
1
12/24/20 18:58
12/28/20 20:57
19719-28-9 ST
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 10:22
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 10:22
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 10:22
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 10:22
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 10:22
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 10:22
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 10:22
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 10:22
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 10:22
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 10:22
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 10:22
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 10:22
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 10:22
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 10:22
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 10:22
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 10:22
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 10:22
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 10:22
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 10:22
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
36
%
10-184
1
12/28/20 20:12
12/31/20 10:22
877-09-8
Decachlorobiphenyl (S)
87
%
10-154
1
12/28/20 20:12
12/31/20 10:22
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 3510C
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 16:28
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 16:28
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 16:28
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 16:28
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 16:28
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 16:28
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 16:28
11096-82-5
Surrogates
Decachlorobiphenyl (S)
82
%
10-181
1
12/28/20 20:12
12/30/20 16:28
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-2 Lab ID: 92513376002 Collected: 12/22/20 08:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
4.2J
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:08
7440-36-0
Arsenic
159
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:08
7440-38-2
Barium
320
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:08
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:08
7440-41-7
Cadmium
1.6
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:08
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:08
7440-47-3
Cobalt
6.8
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:08
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:08
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:08
7439-92-1
Nickel
4.2J
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:08
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:08
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:08
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:08
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:08
7440-62-2
Zinc
16.3
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:08
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/2011:24
12/31/2019:56
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:17 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 15:52
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:52
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 15:52
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 15:52
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:52
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:52
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 15:52
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:52
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:52
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 15:52
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:52
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 15:52
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 15:52
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 15:52
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 15:52
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:52
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:52
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 14 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-2 Lab ID: 92513376002 Collected: 12/22/20 08:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:52
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:52
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:52
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:52
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:52
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:52
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 15:52
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:52
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:52
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 15:52
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:52
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 15:52
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:52
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:52
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:52
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 15:52
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 15:52
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 15:52
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:52
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:52
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 15:52
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:52
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 15:52
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 15:52
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 15:52
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 15:52
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:52
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:52
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:52
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:52
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:52
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 15:52
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 15:52
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:52
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:52
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 15:52
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 15:52
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 15:52
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 15:52
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 15:52
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:52
91-57-6
REPORT OF LABORATORY ANALYSIS
R1
R1
M1,R1
IL
IH
M1
M1
IH
R1
L2,M0
L2,M0
v1
IL,R1
IH,M1,
v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-2 Lab ID: 92513376002 Collected: 12/22/20 08:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Methyl parathion
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
298-00-0
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:52
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:52
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 15:52
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 15:52
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 15:52
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 15:52
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 15:52
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 15:52
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:52
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:52
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 15:52
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:52
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:52
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 15:52
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 15:52
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:52
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 15:52
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 15:52
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:52
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 15:52
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:52
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 15:52
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:52
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 15:52
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:52
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:52
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:52
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 15:52
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 15:52
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:52
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:52
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 15:52
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 15:52
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 15:52
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:52
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:52
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:52
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:52
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 15:52
99-35-4
81
%
10-144
1
12/28/20 08:59
12/29/20 15:52
4165-60-0
61
%
10-130
1
12/28/20 08:59
12/29/20 15:52
321-60-8
REPORT OF LABORATORY ANALYSIS
R1
M1
v2,v3
v2,v3
v2,v3
v1
M1
v1
R1
R1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 118

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-2 Lab ID: 92513376002 Collected: 12/22/20 08:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Date: 01/06/2021 05:06 PM
109
%
34-163
1
12/28/20 08:59
12/29/20 15:52
1718-51-0
17
%
10-130
1
12/28/20 08:59
12/29/20 15:52
13127-88-3
25
%
10-130
1
12/28/20 08:59
12/29/20 15:52
367-12-4
39
%
10-144
1
12/28/20 08:59
12/29/20 15:52
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
17.2J
ug/L
25.0
6.2
1
12/24/20 03:25
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 03:25
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 03:25
107-02-8
ND
ug/L
10.0
0.90
1
12/24/20 03:25
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 03:25
107-05-1
1.9
ug/L
1.0
0.15
1
12/24/20 03:25
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 03:25
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 03:25
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 03:25
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 03:25
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 03:25
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 03:25
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 03:25
56-23-5
4.1
ug/L
1.0
0.23
1
12/24/20 03:25
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 03:25
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 03:25
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 03:25
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 03:25
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 03:25
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 03:25
74-95-3
3.6
ug/L
1.0
0.29
1
12/24/20 03:25
95-50-1
4.6
ug/L
1.0
0.26
1
12/24/20 03:25
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 03:25
110-57-6
ND
ug/L
1.0
0.23
1
12/24/20 03:25
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 03:25
75-34-3
0.46J
ug/L
1.0
0.34
1
12/24/20 03:25
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 03:25
75-35-4
ND
ug/L
1.0
0.29
1
12/24/20 03:25
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 03:25
156-60-5
0.41J
ug/L
1.0
0.19
1
12/24/20 03:25
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 03:25
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 03:25
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 03:25
563-58-6
N D
ug/L
1.0
0.30
1
12/24/20 03:25
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 03:25
10061-02-6
173
ug/L
150
56.2
1
12/24/20 03:25
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 03:25
100-41-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH.v2
Page 17 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-2 Lab ID: 92513376002 Collected: 12/22/20 08:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.51
1
12/24/20 03:25
97-63-2
ND
ug/L
1.0
0.44
1
12/24/20 03:25
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 03:25
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 03:25
74-88-4
ND
ug/L
100
66.4
1
12/24/20 03:25
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 03:25
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 03:25
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 03:25
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 03:25
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 03:25
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 03:25
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 03:25
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 03:25
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 03:25
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 03:25
127-18-4
0.48J
ug/L
1.0
0.24
1
12/24/20 03:25
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 03:25
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 03:25
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 03:25
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 03:25
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 03:25
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 03:25
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 03:25
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 03:25
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 03:25
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 03:25
1330-20-7
99
%
70-130
1
12/24/20 03:25
460-00-4
95
%
70-130
1
12/24/20 03:25
17060-07-0
99
%
70-130
1
12/24/20 03:25
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
97.8J ug/L 100 50.0 1 12/28/2013:46 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 03:32 12/29/20 22:46 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3
Lab ID:
92513376003
Collected:
12/22/20 09:55
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/24/20 18:58
12/28/20 21:12
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/24/20 18:58
12/28/20 21:12
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/24/20 18:58
12/28/20 21:12
93-76-5
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/24/20 18:58
12/28/20 21:12
93-72-1
Surrogates
2,4-DCAA (S)
65.8
%
14.0-158
1
12/24/20 18:58
12/28/20 21:12
19719-28-9
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 10:33
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 10:33
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 10:33
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 10:33
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 10:33
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 10:33
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 10:33
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 10:33
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 10:33
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 10:33
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 10:33
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 10:33
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 10:33
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 10:33
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 10:33
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 10:33
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 10:33
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 10:33
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 10:33
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
64
%
10-184
1
12/28/20 20:12
12/31/20 10:33
877-09-8
Decachlorobiphenyl (S)
93
%
10-154
1
12/28/20 20:12
12/31/20 10:33
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 3510C
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 16:39
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 16:39
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 16:39
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 16:39
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 16:39
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 16:39
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 16:39
11096-82-5
Surrogates
Decachlorobiphenyl (S)
88
%
10-181
1
12/28/20 20:12
12/30/20 16:39
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3 Lab ID: 92513376003 Collected: 12/22/20 09:55 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:12
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:12
7440-38-2
Barium
65.8
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:12
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:12
7440-41-7
Cadmium
2.1
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:12
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:12
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:12
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:12
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:12
7439-92-1
Nickel
29.7
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:12
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:12
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:12
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:12
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:12
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:12
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/20 11:24
12/31/20 20:00
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:19 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 12:28
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:28
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 12:28
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 12:28
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 12:28
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:28
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 12:28
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:28
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 12:28
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 12:28
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 12:28
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 12:28
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 12:28
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 12:28
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 12:28
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 12:28
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:28
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 20 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3 Lab ID: 92513376003 Collected: 12/22/20 09:55 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 12:28
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 12:28
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:28
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 12:28
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 12:28
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 12:28
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 12:28
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:28
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 12:28
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 12:28
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:28
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 12:28
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 12:28
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 12:28
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 12:28
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 12:28
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 12:28
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 12:28
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 12:28
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 12:28
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 12:28
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 12:28
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 12:28
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 12:28
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 12:28
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 12:28
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 12:28
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 12:28
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 12:28
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 12:28
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:28
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 12:28
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 12:28
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 12:28
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 12:28
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 12:28
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 12:28
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 12:28
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 12:28
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 12:28
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:28
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
IH
L2
L2
v1
IL
IH,v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3 Lab ID: 92513376003 Collected: 12/22/20 09:55 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:28
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 12:28
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 12:28
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 12:28
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 12:28
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 12:28
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 12:28
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 12:28
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:28
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:28
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 12:28
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 12:28
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:28
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 12:28
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 12:28
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 12:28
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 12:28
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 12:28
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 12:28
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 12:28
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 12:28
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 12:28
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 12:28
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 12:28
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:28
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:28
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:28
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 12:28
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 12:28
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 12:28
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 12:28
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 12:28
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 12:28
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 12:28
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 12:28
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:28
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:28
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 12:28
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 12:28
99-35-4
54
%
10-144
1
12/28/20 08:59
12/29/20 12:28
4165-60-0
17
%
10-130
1
12/28/20 08:59
12/29/20 12:28
321-60-8
133
%
34-163
1
12/28/20 08:59
12/29/20 12:28
1718-51-0
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
v1
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Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 118

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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3 Lab ID: 92513376003 Collected: 12/22/20 09:55 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
9
%
10-130
1
12/28/20 08:59 12/29/20 12:28
13127-88-3 SO
13
%
10-130
1
12/28/20 08:59 12/29/20 12:28
367-12-4
19
%
10-144
1
12/28/20 08:59 12/29/20 12:28
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 03:43
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 03:43
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 03:43
107-02-8 IH,v2
ND
ug/L
10.0
0.90
1
12/24/20 03:43
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 03:43
107-05-1
1.5
ug/L
1.0
0.15
1
12/24/20 03:43
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 03:43
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 03:43
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 03:43
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 03:43
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 03:43
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 03:43
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 03:43
56-23-5
0.57J
ug/L
1.0
0.23
1
12/24/20 03:43
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 03:43
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 03:43
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 03:43
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 03:43
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 03:43
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 03:43
74-95-3
ND
ug/L
1.0
0.29
1
12/24/20 03:43
95-50-1
2.9
ug/L
1.0
0.26
1
12/24/20 03:43
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 03:43
110-57-6 IH
ND
ug/L
1.0
0.23
1
12/24/20 03:43
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 03:43
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 03:43
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 03:43
75-35-4
6.7
ug/L
1.0
0.29
1
12/24/20 03:43
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 03:43
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 03:43
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 03:43
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 03:43
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 03:43
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 03:43
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 03:43
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 03:43
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 03:43
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 03:43
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3 Lab ID: 92513376003 Collected: 12/22/20 09:55 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 03:43
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 03:43
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 03:43
74-88-4
ND
ug/L
100
66.4
1
12/24/20 03:43
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 03:43
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 03:43
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 03:43
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 03:43
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 03:43
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 03:43
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 03:43
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 03:43
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 03:43
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 03:43
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 03:43
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 03:43
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 03:43
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 03:43
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 03:43
79-00-5
0.66J
ug/L
1.0
0.22
1
12/24/20 03:43
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 03:43
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 03:43
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 03:43
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 03:43
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 03:43
1330-20-7
98
%
70-130
1
12/24/20 03:43
460-00-4
96
%
70-130
1
12/24/20 03:43
17060-07-0
99
%
70-130
1
12/24/20 03:43
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100 50.0 1 12/28/2013:46 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 03:32 12/29/20 22:47 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 24 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3A
Lab ID:
92513376004
Collected:
12/22/20 08:49
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/24/20 18:58
12/28/20 21:26
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/24/20 18:58
12/28/20 21:26
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/24/20 18:58
12/28/20 21:26
93-76-5
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/24/20 18:58
12/28/20 21:26
93-72-1
Surrogates
2,4-DCAA (S)
54.6
%
14.0-158
1
12/24/20 18:58
12/28/20 21:26
19719-28-9
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 10:45
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 10:45
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 10:45
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 10:45
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 10:45
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 10:45
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 10:45
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 10:45
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 10:45
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 10:45
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 10:45
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 10:45
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 10:45
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 10:45
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 10:45
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 10:45
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 10:45
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 10:45
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 10:45
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
53
%
10-184
1
12/28/20 20:12
12/31/20 10:45
877-09-8
Decachlorobiphenyl (S)
107
%
10-154
1
12/28/20 20:12
12/31/20 10:45
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 3510C
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 16:51
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 16:51
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 16:51
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 16:51
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 16:51
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 16:51
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 16:51
11096-82-5
Surrogates
Decachlorobiphenyl (S)
103
%
10-181
1
12/28/20 20:12
12/30/20 16:51
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3A Lab ID: 92513376004 Collected: 12/22/20 08:49 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:15
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:15
7440-38-2
Barium
312
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:15
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:15
7440-41-7
Cadmium
1.4
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:15
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:15
7440-47-3
Cobalt
16.4
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:15
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:15
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:15
7439-92-1
Nickel
21.5
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:15
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:15
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:15
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:15
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:15
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:15
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/20 11:24
12/31/20 20:04
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:22 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 12:54
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:54
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 12:54
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 12:54
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 12:54
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:54
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 12:54
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:54
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 12:54
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 12:54
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 12:54
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 12:54
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 12:54
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 12:54
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 12:54
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 12:54
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:54
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 26 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3A Lab ID: 92513376004 Collected: 12/22/20 08:49 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 12:54
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 12:54
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:54
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 12:54
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 12:54
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 12:54
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 12:54
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:54
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 12:54
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 12:54
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:54
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 12:54
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 12:54
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 12:54
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 12:54
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 12:54
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 12:54
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 12:54
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 12:54
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 12:54
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 12:54
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 12:54
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 12:54
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 12:54
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 12:54
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 12:54
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 12:54
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 12:54
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 12:54
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 12:54
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:54
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 12:54
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 12:54
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 12:54
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 12:54
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 12:54
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 12:54
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 12:54
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 12:54
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 12:54
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:54
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
IH
L2
L2
v1
IL
IH,v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3A Lab ID: 92513376004 Collected: 12/22/20 08:49 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:54
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 12:54
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 12:54
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 12:54
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 12:54
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 12:54
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 12:54
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 12:54
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:54
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:54
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 12:54
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 12:54
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:54
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 12:54
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 12:54
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 12:54
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 12:54
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 12:54
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 12:54
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 12:54
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 12:54
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 12:54
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 12:54
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 12:54
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 12:54
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 12:54
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:54
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 12:54
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 12:54
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 12:54
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 12:54
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 12:54
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 12:54
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 12:54
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 12:54
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 12:54
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 12:54
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 12:54
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 12:54
99-35-4
84
%
10-144
1
12/28/20 08:59
12/29/20 12:54
4165-60-0
59
%
10-130
1
12/28/20 08:59
12/29/20 12:54
321-60-8
131
%
34-163
1
12/28/20 08:59
12/29/20 12:54
1718-51-0
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3A Lab ID: 92513376004 Collected: 12/22/20 08:49 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
16
%
10-130
1
12/28/20 08:59 12/29/20 12:54
13127-88-3
25
%
10-130
1
12/28/20 08:59 12/29/20 12:54
367-12-4
37
%
10-144
1
12/28/20 08:59 12/29/20 12:54
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 04:01
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 04:01
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 04:01
107-02-8
ND
ug/L
10.0
0.90
1
12/24/20 04:01
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 04:01
107-05-1
0.28J
ug/L
1.0
0.15
1
12/24/20 04:01
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 04:01
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 04:01
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 04:01
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 04:01
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 04:01
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 04:01
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 04:01
56-23-5
1.6
ug/L
1.0
0.23
1
12/24/20 04:01
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 04:01
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 04:01
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 04:01
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 04:01
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 04:01
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 04:01
74-95-3
1.9
ug/L
1.0
0.29
1
12/24/20 04:01
95-50-1
2.6
ug/L
1.0
0.26
1
12/24/20 04:01
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 04:01
110-57-6
ND
ug/L
1.0
0.23
1
12/24/20 04:01
75-71-8
0.37J
ug/L
1.0
0.27
1
12/24/20 04:01
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 04:01
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 04:01
75-35-4
4.4
ug/L
1.0
0.29
1
12/24/20 04:01
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 04:01
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 04:01
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 04:01
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 04:01
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 04:01
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 04:01
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 04:01
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 04:01
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 04:01
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 04:01
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,v2
IH
Page 29 of 118

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-3A Lab ID: 92513376004 Collected: 12/22/20 08:49 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 04:01
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 04:01
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 04:01
74-88-4
ND
ug/L
100
66.4
1
12/24/20 04:01
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 04:01
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 04:01
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 04:01
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 04:01
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 04:01
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 04:01
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 04:01
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 04:01
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 04:01
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 04:01
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 04:01
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 04:01
87-61-6
1.2
ug/L
1.0
0.22
1
12/24/20 04:01
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 04:01
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 04:01
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 04:01
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 04:01
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 04:01
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 04:01
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 04:01
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 04:01
1330-20-7
98
%
70-130
1
12/24/20 04:01
460-00-4
95
%
70-130
1
12/24/20 04:01
17060-07-0
100
%
70-130
1
12/24/20 04:01
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100 50.0 1 12/28/2013:47 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 03:32 12/29/20 22:50 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-4
Lab ID:
92513376005
Collected:
12/22/20 10:18
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/24/20 18:58
12/28/20 21:41
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/24/20 18:58
12/28/20 21:41
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/24/20 18:58
12/28/20 21:41
93-76-5
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/24/20 18:58
12/28/20 21:41
93-72-1
Surrogates
2,4-DCAA (S)
74.2
%
14.0-158
1
12/24/20 18:58
12/28/20 21:41
19719-28-9
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 10:56
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 10:56
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 10:56
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 10:56
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 10:56
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 10:56
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 10:56
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 10:56
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 10:56
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 10:56
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 10:56
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 10:56
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 10:56
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 10:56
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 10:56
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 10:56
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 10:56
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 10:56
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 10:56
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
69
%
10-184
1
12/28/20 20:12
12/31/20 10:56
877-09-8
Decachlorobiphenyl (S)
104
%
10-154
1
12/28/20 20:12
12/31/20 10:56
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 3510C
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 17:02
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 17:02
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 17:02
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 17:02
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 17:02
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 17:02
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 17:02
11096-82-5
Surrogates
Decachlorobiphenyl (S)
99
%
10-181
1
12/28/20 20:12
12/30/20 17:02
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 118

lceAnalyircal
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-4 Lab ID: 92513376005 Collected: 12/22/20 10:18 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:18
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:18
7440-38-2
Barium
23.2
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:18
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:18
7440-41-7
Cadmium
1.4
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:18
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:18
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:18
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:18
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:18
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:18
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:18
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:18
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:18
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:18
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:18
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/20 11:24
12/31/20 20:08
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:24 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 13:19
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:19
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 13:19
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 13:19
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 13:19
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:19
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 13:19
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:19
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 13:19
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 13:19
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 13:19
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 13:19
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 13:19
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 13:19
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 13:19
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 13:19
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:19
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 32 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-4 Lab ID: 92513376005 Collected: 12/22/20 10:18 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 13:19
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 13:19
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:19
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 13:19
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 13:19
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 13:19
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 13:19
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:19
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 13:19
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 13:19
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:19
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 13:19
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 13:19
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 13:19
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 13:19
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 13:19
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 13:19
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 13:19
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 13:19
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 13:19
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 13:19
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 13:19
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 13:19
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 13:19
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 13:19
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 13:19
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 13:19
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 13:19
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 13:19
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 13:19
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:19
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 13:19
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 13:19
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 13:19
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 13:19
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 13:19
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 13:19
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 13:19
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 13:19
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 13:19
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:19
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
IH
L2
L2
v1
IL
IH,v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-4 Lab ID: 92513376005 Collected: 12/22/20 10:18 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:19
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 13:19
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 13:19
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 13:19
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 13:19
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 13:19
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 13:19
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 13:19
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:19
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:19
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 13:19
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 13:19
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:19
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 13:19
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 13:19
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 13:19
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 13:19
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 13:19
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 13:19
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 13:19
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 13:19
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 13:19
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 13:19
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 13:19
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:19
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:19
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:19
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 13:19
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 13:19
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 13:19
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 13:19
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 13:19
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 13:19
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 13:19
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 13:19
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:19
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:19
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 13:19
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 13:19
99-35-4
73
%
10-144
1
12/28/20 08:59
12/29/20 13:19
4165-60-0
49
%
10-130
1
12/28/20 08:59
12/29/20 13:19
321-60-8
133
%
34-163
1
12/28/20 08:59
12/29/20 13:19
1718-51-0
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-4 Lab ID: 92513376005 Collected: 12/22/20 10:18 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
14
%
10-130
1
12/28/20 08:59 12/29/20 13:19
13127-88-3
19
%
10-130
1
12/28/20 08:59 12/29/20 13:19
367-12-4
24
%
10-144
1
12/28/20 08:59 12/29/20 13:19
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 04:19
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 04:19
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 04:19
107-02-8
ND
ug/L
10.0
0.90
1
12/24/20 04:19
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 04:19
107-05-1
ND
ug/L
1.0
0.15
1
12/24/20 04:19
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 04:19
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 04:19
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 04:19
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 04:19
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 04:19
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 04:19
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 04:19
56-23-5
ND
ug/L
1.0
0.23
1
12/24/20 04:19
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 04:19
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 04:19
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 04:19
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 04:19
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 04:19
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 04:19
74-95-3
ND
ug/L
1.0
0.29
1
12/24/20 04:19
95-50-1
ND
ug/L
1.0
0.26
1
12/24/20 04:19
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 04:19
110-57-6
ND
ug/L
1.0
0.23
1
12/24/20 04:19
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 04:19
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 04:19
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 04:19
75-35-4
ND
ug/L
1.0
0.29
1
12/24/20 04:19
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 04:19
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 04:19
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 04:19
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 04:19
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 04:19
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 04:19
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 04:19
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 04:19
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 04:19
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 04:19
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,v2
IH
Page 35 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-4 Lab ID: 92513376005 Collected: 12/22/20 10:18 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 04:19
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 04:19
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 04:19
74-88-4
ND
ug/L
100
66.4
1
12/24/20 04:19
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 04:19
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 04:19
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 04:19
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 04:19
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 04:19
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 04:19
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 04:19
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 04:19
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 04:19
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 04:19
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 04:19
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 04:19
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 04:19
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 04:19
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 04:19
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 04:19
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 04:19
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 04:19
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 04:19
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 04:19
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 04:19
1330-20-7
98
%
70-130
1
12/24/20 04:19
460-00-4
96
%
70-130
1
12/24/20 04:19
17060-07-0
99
%
70-130
1
12/24/20 04:19
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100 50.0 1 12/28/2013:47 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 03:32 12/29/20 22:51 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 36 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-5
Lab ID:
92513376006
Collected:
12/22/20 10:36
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/24/20 18:58
12/28/20 21:55
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/24/20 18:58
12/28/20 21:55
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/24/20 18:58
12/28/20 21:55
93-76-5
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/24/20 18:58
12/28/20 21:55
93-72-1
Surrogates
2,4-DCAA (S)
72.4
%
14.0-158
1
12/24/20 18:58
12/28/20 21:55
19719-28-9
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 06:57
12/28/20 11:40
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 06:57
12/28/20 11:40
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 06:57
12/28/20 11:40
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 06:57
12/28/20 11:40
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 06:57
12/28/20 11:40
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 06:57
12/28/20 11:40
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 06:57
12/28/20 11:40
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 06:57
12/28/20 11:40
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 06:57
12/28/20 11:40
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 06:57
12/28/20 11:40
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 06:57
12/28/20 11:40
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 06:57
12/28/20 11:40
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 06:57
12/28/20 11:40
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 06:57
12/28/20 11:40
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 06:57
12/28/20 11:40
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 06:57
12/28/20 11:40
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 06:57
12/28/20 11:40
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 06:57
12/28/20 11:40
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 06:57
12/28/20 11:40
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
72
%
10-184
1
12/28/20 06:57
12/28/20 11:40
877-09-8
Decachlorobiphenyl (S)
125
%
10-154
1
12/28/20 06:57
12/28/20 11:40
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 3510C
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 17:13
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 17:13
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 17:13
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 17:13
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 17:13
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 17:13
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 17:13
11096-82-5
Surrogates
Decachlorobiphenyl (S)
76
%
10-181
1
12/28/20 20:12
12/30/20 17:13
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 37 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-5 Lab ID: 92513376006 Collected: 12/22/20 10:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:22
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:22
7440-38-2
Barium
21.1
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:22
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:22
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:22
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:22
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:22
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:22
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:22
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:22
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:22
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:22
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:22
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:22
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:22
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/20 11:24
12/31/20 20:12
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:26 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 13:45
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:45
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 13:45
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 13:45
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 13:45
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:45
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 13:45
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:45
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 13:45
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 13:45
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 13:45
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 13:45
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 13:45
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 13:45
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 13:45
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 13:45
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:45
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 38 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-5 Lab ID: 92513376006 Collected: 12/22/20 10:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 13:45
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 13:45
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:45
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 13:45
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 13:45
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 13:45
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 13:45
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:45
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 13:45
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 13:45
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:45
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 13:45
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 13:45
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 13:45
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 13:45
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 13:45
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 13:45
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 13:45
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 13:45
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 13:45
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 13:45
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 13:45
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 13:45
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 13:45
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 13:45
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 13:45
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 13:45
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 13:45
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 13:45
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 13:45
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:45
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 13:45
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 13:45
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 13:45
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 13:45
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 13:45
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 13:45
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 13:45
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 13:45
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 13:45
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:45
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
IH
L2
L2
v1
IL
IH,v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-5 Lab ID: 92513376006 Collected: 12/22/20 10:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:45
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 13:45
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 13:45
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 13:45
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 13:45
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 13:45
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 13:45
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 13:45
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:45
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:45
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 13:45
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 13:45
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:45
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 13:45
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 13:45
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 13:45
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 13:45
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 13:45
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 13:45
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 13:45
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 13:45
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 13:45
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 13:45
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 13:45
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 13:45
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 13:45
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:45
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 13:45
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 13:45
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 13:45
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 13:45
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 13:45
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 13:45
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 13:45
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 13:45
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 13:45
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 13:45
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 13:45
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 13:45
99-35-4
40
%
10-144
1
12/28/20 08:59
12/29/20 13:45
4165-60-0
11
%
10-130
1
12/28/20 08:59
12/29/20 13:45
321-60-8
109
%
34-163
1
12/28/20 08:59
12/29/20 13:45
1718-51-0
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-5 Lab ID: 92513376006 Collected: 12/22/20 10:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
7
%
10-130
1
12/28/20 08:59 12/29/20 13:45
13127-88-3 SO
11
%
10-130
1
12/28/20 08:59 12/29/20 13:45
367-12-4
17
%
10-144
1
12/28/20 08:59 12/29/20 13:45
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 02:48
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 02:48
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 02:48
107-02-8 IH
ND
ug/L
10.0
0.90
1
12/24/20 02:48
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 02:48
107-05-1
ND
ug/L
1.0
0.15
1
12/24/20 02:48
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 02:48
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 02:48
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 02:48
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 02:48
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 02:48
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 02:48
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 02:48
56-23-5
ND
ug/L
1.0
0.23
1
12/24/20 02:48
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 02:48
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 02:48
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 02:48
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 02:48
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 02:48
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 02:48
74-95-3
ND
ug/L
1.0
0.29
1
12/24/20 02:48
95-50-1
ND
ug/L
1.0
0.26
1
12/24/20 02:48
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 02:48
110-57-6 IH
ND
ug/L
1.0
0.23
1
12/24/20 02:48
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 02:48
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 02:48
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 02:48
75-35-4
ND
ug/L
1.0
0.29
1
12/24/20 02:48
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 02:48
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 02:48
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 02:48
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 02:48
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 02:48
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 02:48
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 02:48
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 02:48
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 02:48
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 02:48
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 41 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-5 Lab ID: 92513376006 Collected: 12/22/20 10:36 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 02:48
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 02:48
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 02:48
74-88-4
ND
ug/L
100
66.4
1
12/24/20 02:48
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 02:48
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 02:48
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 02:48
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 02:48
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 02:48
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 02:48
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 02:48
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 02:48
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 02:48
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 02:48
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 02:48
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 02:48
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 02:48
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 02:48
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 02:48
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 02:48
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 02:48
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 02:48
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 02:48
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 02:48
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 02:48
1330-20-7
99
%
70-130
1
12/24/20 02:48
460-00-4
96
%
70-130
1
12/24/20 02:48
17060-07-0
100
%
70-130
1
12/24/20 02:48
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100 50.0 1 12/28/2013:48 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 03:32 12/29/20 22:52 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 42 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-6
Lab ID:
92513376007
Collected:
12/22/20 10:50
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/24/20 18:58
12/28/20 22:10
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/24/20 18:58
12/28/20 22:10
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/24/20 18:58
12/28/20 22:10
93-76-5
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/24/20 18:58
12/28/20 22:10
93-72-1
Surrogates
2,4-DCAA (S)
344
%
14.0-158
1
12/24/20 18:58
12/28/20 22:10
19719-28-9 ST
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 3510C
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 11:07
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 11:07
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 11:07
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 11:07
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 11:07
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 11:07
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 11:07
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 11:07
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 11:07
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 11:07
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 11:07
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 11:07
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 11:07
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 11:07
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 11:07
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 11:07
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 11:07
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 11:07
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 11:07
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
46
%
10-184
1
12/28/20 20:12
12/31/20 11:07
877-09-8
Decachlorobiphenyl (S)
72
%
10-154
1
12/28/20 20:12
12/31/20 11:07
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 3510C
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 17:25
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 17:25
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 17:25
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 17:25
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 17:25
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 17:25
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 17:25
11096-82-5
Surrogates
Decachlorobiphenyl (S)
68
%
10-181
1
12/28/20 20:12
12/30/20 17:25
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 43 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-6 Lab ID: 92513376007 Collected: 12/22/20 10:50 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
12/30/2013:40
01/01/2115:53
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/30/2013:40
01/01/2115:53
7440-38-2
Barium
93.7
ug/L
5.0
3.5
1
12/30/2013:40
01/01/2115:53
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
12/30/2013:40
01/01/2115:53
7440-41-7
Cadmium
1.2
ug/L
1.0
0.40
1
12/30/2013:40
01/01/2115:53
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
12/30/2013:40
01/01/2115:53
7440-47-3
Cobalt
26.1
ug/L
5.0
3.6
1
12/30/2013:40
01/01/2115:53
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
12/30/2013:40
01/03/2118:13
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
12/30/2013:40
01/01/2115:53
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
12/30/2013:40
01/01/2115:53
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/30/2013:40
01/01/2115:53
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/30/2013:40
01/01/2115:53
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
12/30/20 13:40
01 /01 /21 15:53
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
12/30/2013:40
01/01/2115:53
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
12/30/2013:40
01/01/2115:53
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/20 11:24
12/31/20 20:16
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:29 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 14:10
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 14:10
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 14:10
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 14:10
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 14:10
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 14:10
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 14:10
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 14:10
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 14:10
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 14:10
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 14:10
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 14:10
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 14:10
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 14:10
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 14:10
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 14:10
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 14:10
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 44 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-6 Lab ID: 92513376007 Collected: 12/22/20 10:50 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 14:10
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 14:10
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 14:10
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 14:10
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 14:10
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 14:10
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 14:10
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 14:10
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 14:10
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 14:10
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 14:10
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 14:10
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 14:10
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 14:10
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 14:10
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 14:10
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 14:10
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 14:10
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 14:10
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 14:10
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 14:10
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 14:10
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 14:10
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 14:10
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 14:10
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 14:10
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 14:10
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 14:10
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 14:10
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 14:10
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 14:10
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 14:10
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 14:10
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 14:10
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 14:10
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 14:10
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 14:10
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 14:10
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 14:10
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 14:10
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 14:10
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
IH
L2
L2
v1
IL
IH,v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-6 Lab ID: 92513376007 Collected: 12/22/20 10:50 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 14:10
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 14:10
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 14:10
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 14:10
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 14:10
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 14:10
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 14:10
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 14:10
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 14:10
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 14:10
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 14:10
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 14:10
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 14:10
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 14:10
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 14:10
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 14:10
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 14:10
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 14:10
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 14:10
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 14:10
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 14:10
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 14:10
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 14:10
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 14:10
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 14:10
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 14:10
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 14:10
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 14:10
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 14:10
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 14:10
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 14:10
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 14:10
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 14:10
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 14:10
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 14:10
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 14:10
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 14:10
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 14:10
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 14:10
99-35-4
81
%
10-144
1
12/28/20 08:59
12/29/20 14:10
4165-60-0
57
%
10-130
1
12/28/20 08:59
12/29/20 14:10
321-60-8
140
%
34-163
1
12/28/20 08:59
12/29/20 14:10
1718-51-0
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-6 Lab ID: 92513376007 Collected: 12/22/20 10:50 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
14
%
10-130
1
12/28/20 08:59 12/29/20 14:10
13127-88-3
24
%
10-130
1
12/28/20 08:59 12/29/20 14:10
367-12-4
33
%
10-144
1
12/28/20 08:59 12/29/20 14:10
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 04:38
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 04:38
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 04:38
107-02-8
ND
ug/L
10.0
0.90
1
12/24/20 04:38
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 04:38
107-05-1
0.69J
ug/L
1.0
0.15
1
12/24/20 04:38
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 04:38
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 04:38
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 04:38
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 04:38
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 04:38
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 04:38
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 04:38
56-23-5
9.1
ug/L
1.0
0.23
1
12/24/20 04:38
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 04:38
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 04:38
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 04:38
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 04:38
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 04:38
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 04:38
74-95-3
2.1
ug/L
1.0
0.29
1
12/24/20 04:38
95-50-1
3.4
ug/L
1.0
0.26
1
12/24/20 04:38
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 04:38
110-57-6
ND
ug/L
1.0
0.23
1
12/24/20 04:38
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 04:38
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 04:38
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 04:38
75-35-4
2.7
ug/L
1.0
0.29
1
12/24/20 04:38
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 04:38
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 04:38
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 04:38
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 04:38
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 04:38
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 04:38
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 04:38
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 04:38
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 04:38
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 04:38
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,v2
IH
Page 47 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-6 Lab ID: 92513376007 Collected: 12/22/20 10:50 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 04:38
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 04:38
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 04:38
74-88-4
ND
ug/L
100
66.4
1
12/24/20 04:38
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 04:38
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 04:38
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 04:38
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 04:38
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 04:38
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 04:38
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 04:38
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 04:38
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 04:38
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 04:38
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 04:38
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 04:38
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 04:38
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 04:38
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 04:38
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 04:38
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 04:38
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 04:38
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 04:38
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 04:38
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 04:38
1330-20-7
99
%
70-130
1
12/24/20 04:38
460-00-4
96
%
70-130
1
12/24/20 04:38
17060-07-0
99
%
70-130
1
12/24/20 04:38
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100 50.0 1 12/28/2013:48 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 03:32 12/29/20 22:53 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 48 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-7S
Lab ID:
92513376008
Collected:
12/22/20 09:03
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/29/20 07:38
12/31/20 18:25
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/29/20 07:38
12/31/20 18:25
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/29/20 07:38
12/31/20 18:25
93-76-5 LO
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/29/20 07:38
12/31/20 18:25
93-72-1
Surrogates
2,4-DCAA (S)
96.8
%
14.0-158
1
12/29/20 07:38
12/31/20 18:25
19719-28-9
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 351 OC
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 11:19
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 11:19
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 11:19
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 11:19
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 11:19
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 11:19
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 11:19
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 11:19
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 11:19
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 11:19
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 11:19
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 11:19
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 11:19
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 11:19
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 11:19
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 11:19
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 11:19
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 11:19
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 11:19
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
46
%
10-184
1
12/28/20 20:12
12/31/20 11:19
877-09-8
Decachlorobiphenyl (S)
89
%
10-154
1
12/28/20 20:12
12/31/20 11:19
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 351 OC
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 17:36
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 17:36
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 17:36
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 17:36
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 17:36
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 17:36
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 17:36
11096-82-5
Surrogates
Decachlorobiphenyl (S)
84
%
10-181
1
12/28/20 20:12
12/30/20 17:36
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 49 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-7S Lab ID: 92513376008 Collected: 12/22/20 09:03 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
12/30/2013:40
01/01/2115:56
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/30/2013:40
01/01/2115:56
7440-38-2
Barium
75.8
ug/L
5.0
3.5
1
12/30/2013:40
01/01/2115:56
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
12/30/2013:40
01/01/2115:56
7440-41-7
Cadmium
0.47J
ug/L
1.0
0.40
1
12/30/2013:40
01/01/2115:56
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
12/30/2013:40
01/01/2115:56
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
12/30/2013:40
01/01/2115:56
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
12/30/2013:40
01/03/2118:16
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
12/30/2013:40
01/01/2115:56
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
12/30/2013:40
01/01/2115:56
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/30/2013:40
01/01/2115:56
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/30/2013:40
01/01/2115:56
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
12/30/20 13:40
01 /01 /21 15:56
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
12/30/2013:40
01/01/2115:56
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
12/30/2013:40
01/01/2115:56
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/2011:24
12/31/2018:00
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:31 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
83-32-9
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
208-96-8
ND
ug/L
10.0
1.5
1
12/29/20 20:55
12/30/20 12:02
98-86-2
ND
ug/L
10.0
1.9
1
12/29/20 20:55
12/30/20 12:02
53-96-3
ND
ug/L
10.0
4.2
1
12/29/20 20:55
12/30/20 12:02
92-67-1
ND
ug/L
10.0
2.3
1
12/29/20 20:55
12/30/20 12:02
120-12-7
ND
ug/L
10.0
2.7
1
12/29/20 20:55
12/30/20 12:02
56-55-3
ND
ug/L
10.0
2.8
1
12/29/20 20:55
12/30/20 12:02
50-32-8
ND
ug/L
10.0
2.6
1
12/29/20 20:55
12/30/20 12:02
205-99-2
ND
ug/L
10.0
2.8
1
12/29/20 20:55
12/30/20 12:02
191-24-2
ND
ug/L
10.0
2.7
1
12/29/20 20:55
12/30/20 12:02
207-08-9
ND
ug/L
20.0
2.9
1
12/29/20 20:55
12/30/20 12:02
100-51-6
ND
ug/L
10.0
1.8
1
12/29/20 20:55
12/30/20 12:02
101-55-3
ND
ug/L
10.0
3.1
1
12/29/20 20:55
12/30/20 12:02
85-68-7
ND
ug/L
10.0
3.3
1
12/29/20 20:55
12/30/20 12:02
59-50-7
ND
ug/L
20.0
3.6
1
12/29/20 20:55
12/30/20 12:02
106-47-8
ND
ug/L
10.0
3.6
1
12/29/20 20:55
12/30/20 12:02
510-15-6
ND
ug/L
10.0
1.8
1
12/29/20 20:55
12/30/20 12:02
111-91-1
ND
ug/L
10.0
1.9
1
12/29/20 20:55
12/30/20 12:02
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 50 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-7S Lab ID: 92513376008 Collected: 12/22/20 09:03 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/29/20 20:55
12/30/20 12:02
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/29/20 20:55
12/30/20 12:02
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/29/20 20:55
12/30/20 12:02
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/29/20 20:55
12/30/20 12:02
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/29/20 20:55
12/30/20 12:02
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/29/20 20:55
12/30/20 12:02
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/29/20 20:55
12/30/20 12:02
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/29/20 20:55
12/30/20 12:02
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/29/20 20:55
12/30/20 12:02
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/29/20 20:55
12/30/20 12:02
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/29/20 20:55
12/30/20 12:02
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/29/20 20:55
12/30/20 12:02
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/29/20 20:55
12/30/20 12:02
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/29/20 20:55
12/30/20 12:02
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/29/20 20:55
12/30/20 12:02
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/29/20 20:55
12/30/20 12:02
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/29/20 20:55
12/30/20 12:02
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/29/20 20:55
12/30/20 12:02
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/29/20 20:55
12/30/20 12:02
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/29/20 20:55
12/30/20 12:02
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/29/20 20:55
12/30/20 12:02
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/29/20 20:55
12/30/20 12:02
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/29/20 20:55
12/30/20 12:02
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/29/20 20:55
12/30/20 12:02
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/29/20 20:55
12/30/20 12:02
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/29/20 20:55
12/30/20 12:02
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/29/20 20:55
12/30/20 12:02
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/29/20 20:55
12/30/20 12:02
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/29/20 20:55
12/30/20 12:02
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/29/20 20:55
12/30/20 12:02
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/29/20 20:55
12/30/20 12:02
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/29/20 20:55
12/30/20 12:02
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/29/20 20:55
12/30/20 12:02
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/29/20 20:55
12/30/20 12:02
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/29/20 20:55
12/30/20 12:02
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/29/20 20:55
12/30/20 12:02
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/29/20 20:55
12/30/20 12:02
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/29/20 20:55
12/30/20 12:02
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/29/20 20:55
12/30/20 12:02
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/29/20 20:55
12/30/20 12:02
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/29/20 20:55
12/30/20 12:02
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
v1
IH
IL
IH,v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-7S Lab ID: 92513376008 Collected: 12/22/20 09:03 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/29/20 20:55
12/30/20 12:02
95-48-7
ND
ug/L
10.0
1.2
1
12/29/20 20:55
12/30/20 12:02
15831-10-4
ND
ug/L
5.0
4.6
1
12/29/20 20:55
12/30/20 12:02
134-32-7
ND
ug/L
10.0
6.1
1
12/29/20 20:55
12/30/20 12:02
91-59-8
ND
ug/L
5.0
2.4
1
12/29/20 20:55
12/30/20 12:02
130-15-4
ND
ug/L
20.0
3.0
1
12/29/20 20:55
12/30/20 12:02
88-74-4
ND
ug/L
20.0
3.8
1
12/29/20 20:55
12/30/20 12:02
99-09-2
ND
ug/L
20.0
5.1
1
12/29/20 20:55
12/30/20 12:02
100-01-6
ND
ug/L
10.0
1.9
1
12/29/20 20:55
12/30/20 12:02
98-95-3
ND
ug/L
10.0
1.4
1
12/29/20 20:55
12/30/20 12:02
88-75-5
ND
ug/L
50.0
6.6
1
12/29/20 20:55
12/30/20 12:02
100-02-7
ND
ug/L
10.0
2.4
1
12/29/20 20:55
12/30/20 12:02
99-55-8
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
55-18-5
ND
ug/L
10.0
1.9
1
12/29/20 20:55
12/30/20 12:02
62-75-9
ND
ug/L
10.0
6.2
1
12/29/20 20:55
12/30/20 12:02
924-16-3
ND
ug/L
10.0
1.3
1
12/29/20 20:55
12/30/20 12:02
621-64-7
ND
ug/L
10.0
3.0
1
12/29/20 20:55
12/30/20 12:02
86-30-6
ND
ug/L
10.0
3.3
1
12/29/20 20:55
12/30/20 12:02
10595-95-6
ND
ug/L
10.0
2.6
1
12/29/20 20:55
12/30/20 12:02
100-75-4
ND
ug/L
10.0
2.1
1
12/29/20 20:55
12/30/20 12:02
930-55-2
ND
ug/L
10.0
3.5
1
12/29/20 20:55
12/30/20 12:02
126-68-1
ND
ug/L
10.0
1.2
1
12/29/20 20:55
12/30/20 12:02
108-60-1
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
56-38-2
ND
ug/L
10.0
4.4
1
12/29/20 20:55
12/30/20 12:02
608-93-5
ND
ug/L
10.0
2.4
1
12/29/20 20:55
12/30/20 12:02
82-68-8
ND
ug/L
20.0
3.8
1
12/29/20 20:55
12/30/20 12:02
87-86-5
ND
ug/L
10.0
1.9
1
12/29/20 20:55
12/30/20 12:02
62-44-2
ND
ug/L
10.0
2.0
1
12/29/20 20:55
12/30/20 12:02
85-01-8
ND
ug/L
10.0
1.4
1
12/29/20 20:55
12/30/20 12:02
108-95-2
ND
ug/L
10.0
10.0
1
12/29/20 20:55
12/30/20 12:02
106-50-3
ND
ug/L
10.0
3.8
1
12/29/20 20:55
12/30/20 12:02
298-02-2
ND
ug/L
10.0
2.4
1
12/29/20 20:55
12/30/20 12:02
23950-58-5
ND
ug/L
10.0
2.2
1
12/29/20 20:55
12/30/20 12:02
129-00-0
ND
ug/L
10.0
3.2
1
12/29/20 20:55
12/30/20 12:02
94-59-7
ND
ug/L
10.0
4.6
1
12/29/20 20:55
12/30/20 12:02
95-94-3
ND
ug/L
10.0
1.5
1
12/29/20 20:55
12/30/20 12:02
58-90-2
ND
ug/L
10.0
1.8
1
12/29/20 20:55
12/30/20 12:02
297-97-2
ND
ug/L
10.0
2.8
1
12/29/20 20:55
12/30/20 12:02
95-53-4
ND
ug/L
10.0
1.4
1
12/29/20 20:55
12/30/20 12:02
95-95-4
ND
ug/L
10.0
1.6
1
12/29/20 20:55
12/30/20 12:02
88-06-2
ND
ug/L
10.0
5.3
1
12/29/20 20:55
12/30/20 12:02
99-35-4
86
%
10-144
1
12/29/20 20:55
12/30/20 12:02
4165-60-0
62
%
10-130
1
12/29/20 20:55
12/30/20 12:02
321-60-8
148
%
34-163
1
12/29/20 20:55
12/30/20 12:02
1718-51-0
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-7S Lab ID: 92513376008 Collected: 12/22/20 09:03 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
19
%
10-130
1
12/29/20 20:55 12/30/20 12:02
13127-88-3
19
%
10-130
1
12/29/20 20:55 12/30/20 12:02
367-12-4
31
%
10-144
1
12/29/20 20:55 12/30/20 12:02
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 04:56
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 04:56
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 04:56
107-02-8
ND
ug/L
10.0
0.90
1
12/24/20 04:56
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 04:56
107-05-1
ND
ug/L
1.0
0.15
1
12/24/20 04:56
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 04:56
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 04:56
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 04:56
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 04:56
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 04:56
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 04:56
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 04:56
56-23-5
ND
ug/L
1.0
0.23
1
12/24/20 04:56
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 04:56
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 04:56
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 04:56
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 04:56
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 04:56
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 04:56
74-95-3
ND
ug/L
1.0
0.29
1
12/24/20 04:56
95-50-1
ND
ug/L
1.0
0.26
1
12/24/20 04:56
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 04:56
110-57-6
ND
ug/L
1.0
0.23
1
12/24/20 04:56
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 04:56
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 04:56
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 04:56
75-35-4
1.4
ug/L
1.0
0.29
1
12/24/20 04:56
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 04:56
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 04:56
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 04:56
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 04:56
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 04:56
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 04:56
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 04:56
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 04:56
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 04:56
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 04:56
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,v2
IH
Page 53 of 118

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-7S Lab ID: 92513376008 Collected: 12/22/20 09:03 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 04:56
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 04:56
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 04:56
74-88-4
ND
ug/L
100
66.4
1
12/24/20 04:56
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 04:56
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 04:56
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 04:56
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 04:56
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 04:56
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 04:56
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 04:56
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 04:56
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 04:56
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 04:56
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 04:56
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 04:56
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 04:56
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 04:56
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 04:56
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 04:56
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 04:56
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 04:56
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 04:56
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 04:56
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 04:56
1330-20-7
96
%
70-130
1
12/24/20 04:56
460-00-4
96
%
70-130
1
12/24/20 04:56
17060-07-0
99
%
70-130
1
12/24/20 04:56
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100 50.0 1 12/28/2013:52 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 03:32 12/29/20 22:54 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 54 of 118

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-71)
Lab ID:
92513376009
Collected:
12/22/20 09:07
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/29/20 07:38
12/31/20 18:39
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/29/20 07:38
12/31/20 18:39
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/29/20 07:38
12/31/20 18:39
93-76-5 LO
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/29/20 07:38
12/31/20 18:39
93-72-1
Surrogates
2,4-DCAA (S)
95.8
%
14.0-158
1
12/29/20 07:38
12/31/20 18:39
19719-28-9
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 351 OC
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 11:30
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 11:30
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 11:30
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 11:30
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 11:30
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 11:30
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 11:30
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 11:30
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 11:30
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 11:30
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 11:30
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 11:30
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 11:30
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 11:30
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 11:30
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 11:30
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 11:30
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 11:30
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 11:30
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
55
%
10-184
1
12/28/20 20:12
12/31/20 11:30
877-09-8
Decachlorobiphenyl (S)
81
%
10-154
1
12/28/20 20:12
12/31/20 11:30
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 351 OC
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 17:59
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 17:59
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 17:59
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 17:59
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 17:59
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 17:59
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 17:59
11096-82-5
Surrogates
Decachlorobiphenyl (S)
75
%
10-181
1
12/28/20 20:12
12/30/20 17:59
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 55 of 118

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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-7D Lab ID: 92513376009 Collected: 12/22/20 09:07 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
12/30/2013:40
01/01/2115:59
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/30/2013:40
01/01/2115:59
7440-38-2
Barium
10.7
ug/L
5.0
3.5
1
12/30/2013:40
01/01/2115:59
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
12/30/2013:40
01/01/2115:59
7440-41-7
Cadmium
0.98J
ug/L
1.0
0.40
1
12/30/2013:40
01/01/2115:59
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
12/30/2013:40
01/01/2115:59
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
12/30/2013:40
01/01/2115:59
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
12/30/2013:40
01/03/2118:20
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
12/30/2013:40
01/01/2115:59
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
12/30/2013:40
01/01/2115:59
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/30/2013:40
01/01/2115:59
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/30/2013:40
01/01/2115:59
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
12/30/20 13:40
01 /01 /21 15:59
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
12/30/2013:40
01/01/2115:59
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
12/30/2013:40
01/01/2115:59
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/2011:24
12/31/2018:28
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:34 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 15:01
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:01
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 15:01
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 15:01
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:01
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:01
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 15:01
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:01
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:01
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 15:01
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:01
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 15:01
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 15:01
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 15:01
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 15:01
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:01
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:01
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 56 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-71) Lab ID: 92513376009 Collected: 12/22/20 09:07 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:01
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:01
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:01
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:01
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:01
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:01
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 15:01
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:01
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:01
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 15:01
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:01
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 15:01
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:01
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:01
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:01
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 15:01
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 15:01
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 15:01
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:01
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:01
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 15:01
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:01
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 15:01
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 15:01
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 15:01
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 15:01
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:01
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:01
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:01
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:01
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:01
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 15:01
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 15:01
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:01
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:01
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 15:01
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 15:01
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 15:01
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 15:01
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 15:01
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:01
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
IH
L2
L2
v1
IL
IH,v1
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Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-71) Lab ID: 92513376009 Collected: 12/22/20 09:07 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:01
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:01
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 15:01
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 15:01
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 15:01
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 15:01
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 15:01
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 15:01
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:01
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:01
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 15:01
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:01
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:01
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 15:01
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 15:01
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:01
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 15:01
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 15:01
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:01
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 15:01
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:01
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 15:01
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:01
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 15:01
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:01
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:01
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:01
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 15:01
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 15:01
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:01
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:01
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 15:01
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 15:01
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 15:01
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:01
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:01
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:01
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:01
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 15:01
99-35-4
52
%
10-144
1
12/28/20 08:59
12/29/20 15:01
4165-60-0
16
%
10-130
1
12/28/20 08:59
12/29/20 15:01
321-60-8
126
%
34-163
1
12/28/20 08:59
12/29/20 15:01
1718-51-0
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-71) Lab ID: 92513376009 Collected: 12/22/20 09:07 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
9
%
10-130
1
12/28/20 08:59 12/29/20 15:01
13127-88-3 SO
16
%
10-130
1
12/28/20 08:59 12/29/20 15:01
367-12-4
25
%
10-144
1
12/28/20 08:59 12/29/20 15:01
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 05:14
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 05:14
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 05:14
107-02-8 IH,v2
ND
ug/L
10.0
0.90
1
12/24/20 05:14
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 05:14
107-05-1
ND
ug/L
1.0
0.15
1
12/24/20 05:14
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 05:14
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 05:14
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 05:14
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 05:14
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 05:14
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 05:14
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 05:14
56-23-5
ND
ug/L
1.0
0.23
1
12/24/20 05:14
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 05:14
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 05:14
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 05:14
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 05:14
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 05:14
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 05:14
74-95-3
ND
ug/L
1.0
0.29
1
12/24/20 05:14
95-50-1
ND
ug/L
1.0
0.26
1
12/24/20 05:14
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 05:14
110-57-6 IH
ND
ug/L
1.0
0.23
1
12/24/20 05:14
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 05:14
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 05:14
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 05:14
75-35-4
0.37J
ug/L
1.0
0.29
1
12/24/20 05:14
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 05:14
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 05:14
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 05:14
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 05:14
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 05:14
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 05:14
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 05:14
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 05:14
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 05:14
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 05:14
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 59 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-7D Lab ID: 92513376009 Collected: 12/22/20 09:07 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 05:14
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 05:14
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 05:14
74-88-4
ND
ug/L
100
66.4
1
12/24/20 05:14
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 05:14
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 05:14
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 05:14
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 05:14
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 05:14
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 05:14
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 05:14
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 05:14
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 05:14
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 05:14
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 05:14
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 05:14
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 05:14
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 05:14
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 05:14
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 05:14
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 05:14
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 05:14
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 05:14
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 05:14
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 05:14
1330-20-7
98
%
70-130
1
12/24/20 05:14
460-00-4
95
%
70-130
1
12/24/20 05:14
17060-07-0
99
%
70-130
1
12/24/20 05:14
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services
-Asheville
ND
ug/L
100
50.0
1
12/28/2013:53
18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 01:56 12/29/20 22:56 57-12-5 M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 60 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-8
Lab ID:
92513376010
Collected:
12/22/20 10:58
Received: 12/22/20 15:20 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Chlorinated Herb. (GC) 8151
Analytical
Method: EPA8151
Preparation
Method: 8151A
Pace National
- Mt. Juliet
2,4-D
ND
ug/L
2.00
0.547
1
12/29/20 07:38
12/31/20 18:54
94-75-7
Dinoseb
ND
ug/L
2.00
0.250
1
12/29/20 07:38
12/31/20 18:54
88-85-7
2,4,5-T
ND
ug/L
2.00
0.258
1
12/29/20 07:38
12/31/20 18:54
93-76-5 LO
2,4,5-TP (Silvex)
ND
ug/L
2.00
0.335
1
12/29/20 07:38
12/31/20 18:54
93-72-1
Surrogates
2,4-DCAA (S)
94.5
%
14.0-158
1
12/29/20 07:38
12/31/20 18:54
19719-28-9
8081 OC Pesticides RVE
Analytical
Method: EPA 8081
B Preparation Method: EPA 351 OC
Pace Analytical
Services
- Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/28/20 20:12
12/31/20 11:42
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/28/20 20:12
12/31/20 11:42
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/28/20 20:12
12/31/20 11:42
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/28/20 20:12
12/31/20 11:42
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/28/20 20:12
12/31/20 11:42
58-89-9
Chlordane (Technical)
ND
ug/L
0.20
0.14
1
12/28/20 20:12
12/31/20 11:42
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/28/20 20:12
12/31/20 11:42
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/28/20 20:12
12/31/20 11:42
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/28/20 20:12
12/31/20 11:42
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/28/20 20:12
12/31/20 11:42
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/28/20 20:12
12/31/20 11:42
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/28/20 20:12
12/31/20 11:42
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/28/20 20:12
12/31/20 11:42
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/28/20 20:12
12/31/20 11:42
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/28/20 20:12
12/31/20 11:42
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/28/20 20:12
12/31/20 11:42
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12/28/20 20:12
12/31/20 11:42
1024-57-3
Methoxychlor
ND
ug/L
0.15
0.033
1
12/28/20 20:12
12/31/20 11:42
72-43-5
Toxaphene
ND
ug/L
0.20
0.19
1
12/28/20 20:12
12/31/20 11:42
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
42
%
10-184
1
12/28/20 20:12
12/31/20 11:42
877-09-8
Decachlorobiphenyl (S)
76
%
10-154
1
12/28/20 20:12
12/31/20 11:42
2051-24-3
8082 GCS PCB RVE
Analytical
Method: EPA 8082A
Preparation Method:
EPA 351 OC
Pace Analytical
Services
- Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/28/20 20:12
12/30/20 18:10
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/28/20 20:12
12/30/20 18:10
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/28/20 20:12
12/30/20 18:10
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/28/20 20:12
12/30/20 18:10
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/28/20 20:12
12/30/20 18:10
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/28/20 20:12
12/30/20 18:10
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/28/20 20:12
12/30/20 18:10
11096-82-5
Surrogates
Decachlorobiphenyl (S)
74
%
10-181
1
12/28/20 20:12
12/30/20 18:10
2051-24-3
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 61 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-8 Lab ID: 92513376010 Collected: 12/22/20 10:58 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:25
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:25
7440-38-2
Barium
42.8
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:25
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:25
7440-41-7
Cadmium
0.991
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:25
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:25
7440-47-3
Cobalt
4.1J
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:25
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:25
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:25
7439-92-1
Nickel
8.8
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:25
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:25
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:25
7440-22-4
Tin
N D
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:25
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:25
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:25
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/2011:24
12/31/2018:32
7440-28-0
7470 Mercury
Mercury
8270E APP9 RV
Acenaphthene
Acenaphthylene
Acetophenone
2-Acetylaminofluorene
4-Aminobiphenyl
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
4-Chloroaniline
Chlorobenzilate
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:36 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
83-32-9
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
208-96-8
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 15:26
98-86-2
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:26
53-96-3
ND
ug/L
10.0
4.2
1
12/28/20 08:59
12/29/20 15:26
92-67-1
ND
ug/L
10.0
2.3
1
12/28/20 08:59
12/29/20 15:26
120-12-7
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:26
56-55-3
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:26
50-32-8
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 15:26
205-99-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:26
191-24-2
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:26
207-08-9
ND
ug/L
20.0
2.9
1
12/28/20 08:59
12/29/20 15:26
100-51-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:26
101-55-3
ND
ug/L
10.0
3.1
1
12/28/20 08:59
12/29/20 15:26
85-68-7
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 15:26
59-50-7
ND
ug/L
20.0
3.6
1
12/28/20 08:59
12/29/20 15:26
106-47-8
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 15:26
510-15-6
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:26
111-91-1
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:26
111-44-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 62 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-8 Lab ID: 92513376010 Collected: 12/22/20 10:58 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
2-Chloronaphthalene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:26
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:26
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
7005-72-3
Chrysene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:26
218-01-9
Diallate
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:26
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:26
53-70-3
Dibenzofuran
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:26
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
20.0
8.1
1
12/28/20 08:59
12/29/20 15:26
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:26
120-83-2
2,6-Dichlorophenol
ND
ug/L
10.0
2.7
1
12/28/20 08:59
12/29/20 15:26
87-65-0
Diethylphthalate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
84-66-2
Dimethoate
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
5.0
3.3
1
12/28/20 08:59
12/29/20 15:26
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:26
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
25.0
23.5
1
12/28/20 08:59
12/29/20 15:26
119-93-7
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:26
105-67-9
Dimethylphthalate
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:26
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:26
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
3.4
1
12/28/20 08:59
12/29/20 15:26
534-52-1
1,3-Dinitrobenzene
ND
ug/L
10.0
3.7
1
12/28/20 08:59
12/29/20 15:26
99-65-0
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/28/20 08:59
12/29/20 15:26
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:26
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:26
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
3.9
1
12/28/20 08:59
12/29/20 15:26
117-84-0
Diphenylamine
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:26
122-39-4
Disulfoton
ND
ug/L
10.0
6.0
1
12/28/20 08:59
12/29/20 15:26
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
3.7
1
12/28/20 08:59
12/29/20 15:26
117-81-7
Ethyl methanesulfonate
ND
ug/L
20.0
2.8
1
12/28/20 08:59
12/29/20 15:26
62-50-0
Famphur
ND
ug/L
10.0
5.7
1
12/28/20 08:59
12/29/20 15:26
52-85-7
Fluoranthene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:26
206-44-0
Fluorene
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:26
86-73-7
Hexachlorobenzene
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:26
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:26
77-47-4
Hexachloroethane
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:26
67-72-1
Hexachloropropene
ND
ug/L
10.0
5.5
1
12/28/20 08:59
12/29/20 15:26
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
2.9
1
12/28/20 08:59
12/29/20 15:26
193-39-5
Isodrin
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:26
465-73-6
Isophorone
ND
ug/L
10.0
1.7
1
12/28/20 08:59
12/29/20 15:26
78-59-1
Isosafrole
ND
ug/L
10.0
3.6
1
12/28/20 08:59
12/29/20 15:26
120-58-1
Kepone
ND
ug/L
10.0
8.2
1
12/28/20 08:59
12/29/20 15:26
143-50-0
Methapyrilene
ND
ug/L
50.0
27.2
1
12/28/20 08:59
12/29/20 15:26
91-80-5
3-Methylcholanthrene
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 15:26
56-49-5
Methyl methanesulfonate
ND
ug/L
5.0
3.0
1
12/28/20 08:59
12/29/20 15:26
66-27-3
2-Methylnaphthalene
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:26
91-57-6
Methyl parathion
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
298-00-0
REPORT OF LABORATORY ANALYSIS
IL
IH
IH
L2
L2
v1
IL
IH,v1
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 63 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-8 Lab ID: 92513376010 Collected: 12/22/20 10:58 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
1-Naphthalenamine
2-Naphthalenamine
1,4-Naphthoquinone
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:26
95-48-7
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:26
15831-10-4
ND
ug/L
5.0
4.6
1
12/28/20 08:59
12/29/20 15:26
134-32-7
ND
ug/L
10.0
6.1
1
12/28/20 08:59
12/29/20 15:26
91-59-8
ND
ug/L
5.0
2.4
1
12/28/20 08:59
12/29/20 15:26
130-15-4
ND
ug/L
20.0
3.0
1
12/28/20 08:59
12/29/20 15:26
88-74-4
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 15:26
99-09-2
ND
ug/L
20.0
5.1
1
12/28/20 08:59
12/29/20 15:26
100-01-6
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:26
98-95-3
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:26
88-75-5
ND
ug/L
50.0
6.6
1
12/28/20 08:59
12/29/20 15:26
100-02-7
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:26
99-55-8
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
55-18-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:26
62-75-9
ND
ug/L
10.0
6.2
1
12/28/20 08:59
12/29/20 15:26
924-16-3
ND
ug/L
10.0
1.3
1
12/28/20 08:59
12/29/20 15:26
621-64-7
ND
ug/L
10.0
3.0
1
12/28/20 08:59
12/29/20 15:26
86-30-6
ND
ug/L
10.0
3.3
1
12/28/20 08:59
12/29/20 15:26
10595-95-6
ND
ug/L
10.0
2.6
1
12/28/20 08:59
12/29/20 15:26
100-75-4
ND
ug/L
10.0
2.1
1
12/28/20 08:59
12/29/20 15:26
930-55-2
ND
ug/L
10.0
3.5
1
12/28/20 08:59
12/29/20 15:26
126-68-1
ND
ug/L
10.0
1.2
1
12/28/20 08:59
12/29/20 15:26
108-60-1
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
56-38-2
ND
ug/L
10.0
4.4
1
12/28/20 08:59
12/29/20 15:26
608-93-5
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:26
82-68-8
ND
ug/L
20.0
3.8
1
12/28/20 08:59
12/29/20 15:26
87-86-5
ND
ug/L
10.0
1.9
1
12/28/20 08:59
12/29/20 15:26
62-44-2
ND
ug/L
10.0
2.0
1
12/28/20 08:59
12/29/20 15:26
85-01-8
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:26
108-95-2
ND
ug/L
10.0
10.0
1
12/28/20 08:59
12/29/20 15:26
106-50-3
ND
ug/L
10.0
3.8
1
12/28/20 08:59
12/29/20 15:26
298-02-2
ND
ug/L
10.0
2.4
1
12/28/20 08:59
12/29/20 15:26
23950-58-5
ND
ug/L
10.0
2.2
1
12/28/20 08:59
12/29/20 15:26
129-00-0
ND
ug/L
10.0
3.2
1
12/28/20 08:59
12/29/20 15:26
94-59-7
ND
ug/L
10.0
4.6
1
12/28/20 08:59
12/29/20 15:26
95-94-3
ND
ug/L
10.0
1.5
1
12/28/20 08:59
12/29/20 15:26
58-90-2
ND
ug/L
10.0
1.8
1
12/28/20 08:59
12/29/20 15:26
297-97-2
ND
ug/L
10.0
2.8
1
12/28/20 08:59
12/29/20 15:26
95-53-4
ND
ug/L
10.0
1.4
1
12/28/20 08:59
12/29/20 15:26
95-95-4
ND
ug/L
10.0
1.6
1
12/28/20 08:59
12/29/20 15:26
88-06-2
ND
ug/L
10.0
5.3
1
12/28/20 08:59
12/29/20 15:26
99-35-4
68
%
10-144
1
12/28/20 08:59
12/29/20 15:26
4165-60-0
40
%
10-130
1
12/28/20 08:59
12/29/20 15:26
321-60-8
125
%
34-163
1
12/28/20 08:59
12/29/20 15:26
1718-51-0
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
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Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 64 of 118

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-8 Lab ID: 92513376010 Collected: 12/22/20 10:58 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Date: 01/06/2021 05:06 PM
13
%
10-130
1
12/28/20 08:59 12/29/20 15:26
13127-88-3
21
%
10-130
1
12/28/20 08:59 12/29/20 15:26
367-12-4
28
%
10-144
1
12/28/20 08:59 12/29/20 15:26
118-79-6
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
ND
ug/L
25.0
6.2
1
12/24/20 05:32
67-64-1
ND
ug/L
50.0
30.4
1
12/24/20 05:32
75-05-8
ND
ug/L
10.0
2.7
1
12/24/20 05:32
107-02-8
ND
ug/L
10.0
0.90
1
12/24/20 05:32
107-13-1
ND
ug/L
2.0
0.28
1
12/24/20 05:32
107-05-1
0.57J
ug/L
1.0
0.15
1
12/24/20 05:32
71-43-2
ND
ug/L
1.0
0.34
1
12/24/20 05:32
74-97-5
ND
ug/L
1.0
0.26
1
12/24/20 05:32
75-27-4
ND
ug/L
1.0
0.62
1
12/24/20 05:32
75-25-2
ND
ug/L
2.0
0.62
1
12/24/20 05:32
74-83-9
ND
ug/L
5.0
3.3
1
12/24/20 05:32
78-93-3
ND
ug/L
2.0
0.40
1
12/24/20 05:32
75-15-0
ND
ug/L
1.0
0.22
1
12/24/20 05:32
56-23-5
0.56J
ug/L
1.0
0.23
1
12/24/20 05:32
108-90-7
ND
ug/L
1.0
0.49
1
12/24/20 05:32
75-00-3
ND
ug/L
5.0
2.3
1
12/24/20 05:32
67-66-3
ND
ug/L
1.0
0.39
1
12/24/20 05:32
74-87-3
ND
ug/L
5.0
1.7
1
12/24/20 05:32
126-99-8
ND
ug/L
1.0
0.41
1
12/24/20 05:32
124-48-1
ND
ug/L
1.0
0.46
1
12/24/20 05:32
74-95-3
0.57J
ug/L
1.0
0.29
1
12/24/20 05:32
95-50-1
0.97J
ug/L
1.0
0.26
1
12/24/20 05:32
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 05:32
110-57-6
ND
ug/L
1.0
0.23
1
12/24/20 05:32
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 05:32
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 05:32
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 05:32
75-35-4
4.0
ug/L
1.0
0.29
1
12/24/20 05:32
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 05:32
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 05:32
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 05:32
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 05:32
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 05:32
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 05:32
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 05:32
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 05:32
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 05:32
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 05:32
97-63-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,v2
IH
Page 65 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: MW-8 Lab ID: 92513376010 Collected: 12/22/20 10:58 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
450OCNE Cyanide, Total
Cyanide
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.44
1
12/24/20 05:32
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 05:32
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 05:32
74-88-4
ND
ug/L
100
66.4
1
12/24/20 05:32
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 05:32
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 05:32
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 05:32
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 05:32
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 05:32
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 05:32
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 05:32
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 05:32
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 05:32
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 05:32
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 05:32
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 05:32
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 05:32
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 05:32
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 05:32
79-00-5
0.501
ug/L
1.0
0.22
1
12/24/20 05:32
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 05:32
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 05:32
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 05:32
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 05:32
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 05:32
1330-20-7
98
%
70-130
1
12/24/20 05:32
460-00-4
97
%
70-130
1
12/24/20 05:32
17060-07-0
100
%
70-130
1
12/24/20 05:32
2037-26-5
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100 50.0 1 12/28/2013:53 18496-25-8
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND ug/L 8.0 6.0 1 12/29/20 01:56 12/29/20 23:01 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 66 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: SW-1 Lab ID: 92513376011 Collected: 12/22/20 09:12 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:28
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:28
7440-38-2
Barium
20.0
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:28
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:28
7440-41-7
Cadmium
1.8
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:28
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:28
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:28
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:28
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:28
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:28
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:28
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:28
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:28
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:28
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:28
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/2011:24
12/31/2018:36
7440-28-0
7470 Mercury
Mercury
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2018:38 7439-97-6
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
ND
ug/L
50.0
ND
ug/L
10.0
ND
ug/L
10.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
6.2
1
12/24/20 02:12
67-64-1
30.4
1
12/24/20 02:12
75-05-8
2.7
1
12/24/20 02:12
107-02-8
0.90
1
12/24/20 02:12
107-13-1
0.28
1
12/24/20 02:12
107-05-1
0.15
1
12/24/20 02:12
71-43-2
0.34
1
12/24/20 02:12
74-97-5
0.26
1
12/24/20 02:12
75-27-4
0.62
1
12/24/20 02:12
75-25-2
0.62
1
12/24/20 02:12
74-83-9
3.3
1
12/24/20 02:12
78-93-3
0.40
1
12/24/20 02:12
75-15-0
0.22
1
12/24/20 02:12
56-23-5
0.23
1
12/24/20 02:12
108-90-7
0.49
1
12/24/20 02:12
75-00-3
2.3
1
12/24/20 02:12
67-66-3
0.39
1
12/24/20 02:12
74-87-3
1.7
1
12/24/20 02:12
126-99-8
0.41
1
12/24/20 02:12
124-48-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,v2
Page 67 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: SW-1 Lab ID: 92513376011 Collected: 12/22/20 09:12 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrach loroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.46
1
12/24/20 02:12
74-95-3
ND
ug/L
1.0
0.29
1
12/24/20 02:12
95-50-1
ND
ug/L
1.0
0.26
1
12/24/20 02:12
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 02:12
110-57-6 IH
ND
ug/L
1.0
0.23
1
12/24/20 02:12
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 02:12
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 02:12
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 02:12
75-35-4
ND
ug/L
1.0
0.29
1
12/24/20 02:12
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 02:12
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 02:12
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 02:12
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 02:12
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 02:12
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 02:12
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 02:12
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 02:12
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 02:12
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 02:12
97-63-2
ND
ug/L
1.0
0.44
1
12/24/20 02:12
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 02:12
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 02:12
74-88-4
ND
ug/L
100
66.4
1
12/24/20 02:12
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 02:12
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 02:12
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 02:12
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 02:12
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 02:12
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 02:12
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 02:12
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 02:12
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 02:12
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 02:12
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 02:12
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 02:12
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 02:12
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 02:12
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 02:12
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 02:12
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 02:12
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 02:12
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 02:12
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 02:12
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 02:12
1330-20-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 68 of 118

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[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: SW-1
Parameters
Lab ID: 92513376011 Collected:
Report
Results Units Limit
12/22/20 09:12
MDL DF
Received: 12/22/20 15:20 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Surrogates
4-Bromofluorobenzene (S)
98 % 70-130
1
12/24/20 02:12
460-00-4
1,2-Dichloroethane-d4 (S)
95 % 70-130
1
12/24/20 02:12
17060-07-0
Toluene-d8(S)
99 % 70-130
1
12/24/20 02:12
2037-26-5
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 69 of 118

lceAnalyircal
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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: SW-2 Lab ID: 92513376012 Collected: 12/22/20 09:19 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
01/05/2101:00
01/05/2115:38
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:38
7440-38-2
Barium
19.6
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:38
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
01/05/2101:00
01/05/2115:38
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
01/05/2101:00
01/05/2115:38
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
01/05/2101:00
01/05/2115:38
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
01/05/2101:00
01/05/2115:38
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
01/05/2101:00
01/05/2115:38
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
01/05/2101:00
01/05/2115:38
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
01/05/2101:00
01/05/2115:38
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
01/05/2101:00
01/05/2115:38
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
01/05/2101:00
01/05/2115:38
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
01 /05/21 01:00
01 /05/21 15:38
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
01/05/2101:00
01/05/2115:38
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
01/05/2101:00
01/05/2115:38
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/28/2011:24
12/31/2018:40
7440-28-0
7470 Mercury
Mercury
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/29/2013:15 12/29/2017:32 7439-97-6
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
ND
ug/L
50.0
ND
ug/L
10.0
ND
ug/L
10.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
6.2
1
12/24/20 02:30
67-64-1
30.4
1
12/24/20 02:30
75-05-8
2.7
1
12/24/20 02:30
107-02-8
0.90
1
12/24/20 02:30
107-13-1
0.28
1
12/24/20 02:30
107-05-1
0.15
1
12/24/20 02:30
71-43-2
0.34
1
12/24/20 02:30
74-97-5
0.26
1
12/24/20 02:30
75-27-4
0.62
1
12/24/20 02:30
75-25-2
0.62
1
12/24/20 02:30
74-83-9
3.3
1
12/24/20 02:30
78-93-3
0.40
1
12/24/20 02:30
75-15-0
0.22
1
12/24/20 02:30
56-23-5
0.23
1
12/24/20 02:30
108-90-7
0.49
1
12/24/20 02:30
75-00-3
2.3
1
12/24/20 02:30
67-66-3
0.39
1
12/24/20 02:30
74-87-3
1.7
1
12/24/20 02:30
126-99-8
0.41
1
12/24/20 02:30
124-48-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,v2
Page 70 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: SW-2 Lab ID: 92513376012 Collected: 12/22/20 09:19 Received: 12/22/20 15:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrach loroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Date: 01/06/2021 05:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.46
1
12/24/20 02:30
74-95-3
ND
ug/L
1.0
0.29
1
12/24/20 02:30
95-50-1
ND
ug/L
1.0
0.26
1
12/24/20 02:30
106-46-7
ND
ug/L
1.0
0.54
1
12/24/20 02:30
110-57-6 IH
ND
ug/L
1.0
0.23
1
12/24/20 02:30
75-71-8
ND
ug/L
1.0
0.27
1
12/24/20 02:30
75-34-3
ND
ug/L
1.0
0.34
1
12/24/20 02:30
107-06-2
ND
ug/L
1.0
0.24
1
12/24/20 02:30
75-35-4
ND
ug/L
1.0
0.29
1
12/24/20 02:30
156-59-2
ND
ug/L
1.0
0.25
1
12/24/20 02:30
156-60-5
ND
ug/L
1.0
0.19
1
12/24/20 02:30
78-87-5
ND
ug/L
1.0
0.16
1
12/24/20 02:30
142-28-9
ND
ug/L
1.0
0.27
1
12/24/20 02:30
594-20-7
ND
ug/L
1.0
0.21
1
12/24/20 02:30
563-58-6
ND
ug/L
1.0
0.30
1
12/24/20 02:30
10061-01-5
ND
ug/L
1.0
0.31
1
12/24/20 02:30
10061-02-6
ND
ug/L
150
56.2
1
12/24/20 02:30
123-91-1
ND
ug/L
1.0
0.26
1
12/24/20 02:30
100-41-4
ND
ug/L
1.0
0.51
1
12/24/20 02:30
97-63-2
ND
ug/L
1.0
0.44
1
12/24/20 02:30
87-68-3
ND
ug/L
5.0
0.57
1
12/24/20 02:30
591-78-6
ND
ug/L
20.0
12.5
1
12/24/20 02:30
74-88-4
ND
ug/L
100
66.4
1
12/24/20 02:30
78-83-1
ND
ug/L
10.0
1.9
1
12/24/20 02:30
126-98-7
ND
ug/L
5.0
3.7
1
12/24/20 02:30
75-09-2
ND
ug/L
2.0
0.46
1
12/24/20 02:30
80-62-6
ND
ug/L
5.0
4.5
1
12/24/20 02:30
108-10-1
ND
ug/L
1.0
0.35
1
12/24/20 02:30
91-20-3
ND
ug/L
20.0
1.8
1
12/24/20 02:30
107-12-0
ND
ug/L
1.0
0.27
1
12/24/20 02:30
100-42-5
ND
ug/L
1.0
0.34
1
12/24/20 02:30
630-20-6
ND
ug/L
1.0
0.22
1
12/24/20 02:30
79-34-5
ND
ug/L
1.0
0.16
1
12/24/20 02:30
127-18-4
ND
ug/L
1.0
0.24
1
12/24/20 02:30
108-88-3
ND
ug/L
1.0
0.34
1
12/24/20 02:30
87-61-6
ND
ug/L
1.0
0.22
1
12/24/20 02:30
120-82-1
ND
ug/L
1.0
0.18
1
12/24/20 02:30
71-55-6
ND
ug/L
1.0
0.24
1
12/24/20 02:30
79-00-5
ND
ug/L
1.0
0.22
1
12/24/20 02:30
79-01-6
ND
ug/L
1.0
0.31
1
12/24/20 02:30
75-69-4
ND
ug/L
1.0
0.35
1
12/24/20 02:30
96-18-4
ND
ug/L
2.0
1.4
1
12/24/20 02:30
108-05-4
ND
ug/L
1.0
0.24
1
12/24/20 02:30
75-01-4
ND
ug/L
1.0
0.63
1
12/24/20 02:30
1330-20-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 71 of 118

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
Sample: SW-2
Parameters
Lab ID: 92513376012 Collected:
Report
Results Units Limit
12/22/20 09:19
MDL DF
Received: 12/22/20 15:20 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Surrogates
4-Bromofluorobenzene (S)
98 % 70-130
1
12/24/20 02:30
460-00-4
1,2-Dichloroethane-d4 (S)
95 % 70-130
1
12/24/20 02:30
17060-07-0
Toluene-d8(S)
99 % 70-130
1
12/24/20 02:30
2037-26-5
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 72 of 118

lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 1597441 Analysis Method: EPA 8151
QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007
METHOD BLANK: R3607925-1
Matrix:
Water
Associated Lab Samples:
92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
2,4-D
ug/L
ND
2.00
0.547
12/28/20 16:36
Dinoseb
ug/L
ND
2.00
0.250
12/28/20 16:36
2,4,5-T
ug/L
ND
2.00
0.258
12/28/20 16:36
2,4,5-TP (Silvex)
ug/L
ND
2.00
0.335
12/28/20 16:36
2,4-DCAA (S)
%
73.2
14.0-158
12/28/20 16:36
LABORATORY CONTROL SAMPLE & LCSD:
R3607925-2
R3607925-3
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
2,4-D
ug/L
5.00
4.28
4.21
85.6
84.2
50.0-120
1.65
20 P9
Dinoseb
ug/L
5.00
3.18
3.29
63.6
65.8
36.0-134
3.40
20
2,4,5-T
ug/L
5.00
5.32
5.23
106
105
54.0-120
1.71
20
2,4,5-TP (Silvex)
ug/L
5.00
4.80
4.73
96.0
94.6
50.0-125
1.47
20
2,4-DCAA (S)
%
79.2
78.8
14.0-158
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 73 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 1598360 Analysis Method: EPA 8151
QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92513376008, 92513376009, 92513376010
METHOD BLANK: R3608713-1
Matrix:
Water
Associated Lab Samples:
92513376008, 92513376009, 92513376010
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
2,4-D
ug/L
ND
2.00
0.547
12/31/20 08:43
Dinoseb
ug/L
ND
2.00
0.250
12/31/20 08:43
2,4,5-T
ug/L
ND
2.00
0.258
12/31/20 08:43
2,4,5-TP (Silvex)
ug/L
ND
2.00
0.335
12/31/20 08:43
2,4-DCAA (S)
%
93.6
14.0-158
12/31/20 08:43
LABORATORY CONTROL SAMPLE & LCSD:
R3608713-2
R3608713-3
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
2,4-D
ug/L
5.00
5.16
5.37
103
107
50.0-120
3.99
20 P9
Dinoseb
ug/L
5.00
4.25
4.51
85.0
90.2
36.0-134
5.94
20 P9
2,4,5-T
ug/L
5.00
5.96
6.26
119
125
54.0-120
4.91
20 LO,P9
2,4,5-TP (Silvex)
ug/L
5.00
5.97
6.24
119
125
50.0-125
4.42
20 P9
2,4-DCAA (S)
%
103
106
14.0-158
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 74 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589768 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008,92513376009,92513376010,92513376011,92513376012
METHOD BLANK: 3114665 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008,92513376009,92513376010,92513376011,92513376012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Mercury ug/L ND 0.20 0.12 12/29/2017:49
LABORATORY CONTROL SAMPLE: 3114666
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 106 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3114667 3114668
MS MSD
92513205001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L 0.35 2.5 2.5 2.6 2.7 91 94 75-125 3 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 75 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 590033 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376007, 92513376008, 92513376009
METHOD BLANK: 3115778 Matrix:
Associated Lab Samples: 92513376007, 92513376008, 92513376009
Blank
Parameter Units Result
Water
Reporting
Limit
Antimony
ug/L
ND
5.0
Arsenic
ug/L
ND
10.0
Barium
ug/L
ND
5.0
Beryllium
ug/L
ND
1.0
Cadmium
ug/L
ND
1.0
Chromium
ug/L
ND
5.0
Cobalt
ug/L
ND
5.0
Copper
ug/L
ND
5.0
Lead
ug/L
ND
5.0
Nickel
ug/L
ND
5.0
Selenium
ug/L
ND
10.0
Silver
ug/L
ND
5.0
Tin
ug/L
ND
5.0
Vanadium
ug/L
ND
5.0
Zinc
ug/L
ND
10.0
MDL Analyzed
3.0
01/01/21 14:54
4.7
01/01/21 14:54
3.5
01/01/21 14:54
0.70
01/01/21 14:54
0.40
01/01/21 14:54
3.7
01/01/21 14:54
3.6
01/01/21 14:54
4.3
01/01/21 14:54
4.5
01/01/21 14:54
3.5
01/01/21 14:54
4.7
01/01/21 14:54
2.5
01/01/21 14:54
4.7
01/01/21 14:54
3.9
01/01/21 14:54
9.5
01/01/21 14:54
LABORATORY CONTROL SAMPLE:
Parameter
3115779
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
510
102
80-120
Arsenic
ug/L
500
502
100
80-120
Barium
ug/L
500
490
98
80-120
Beryllium
ug/L
500
495
99
80-120
Cadmium
ug/L
500
492
98
80-120
Chromium
ug/L
500
479
96
80-120
Cobalt
ug/L
500
487
97
80-120
Copper
ug/L
500
476
95
80-120
Lead
ug/L
500
485
97
80-120
Nickel
ug/L
500
499
100
80-120
Selenium
ug/L
500
507
101
80-120
Silver
ug/L
250
247
99
80-120
Tin
ug/L
500
477
95
80-120
Vanadium
ug/L
500
502
100
80-120
Zinc
ug/L
500
503
101
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 76 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
SURRY CLOSED LF ELKIN
92513376
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3115780
3115781
MS
MSD
92510340001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
551
550
109
109
75-125
0
20
Arsenic
ug/L
ND
500
500
556
551
111
110
75-125
1
20
Barium
ug/L
21.7
500
500
523
522
100
100
75-125
0
20
Beryllium
ug/L
ND
500
500
511
512
102
102
75-125
0
20
Cadmium
ug/L
ND
500
500
524
522
105
104
75-125
0
20
Chromium
ug/L
8.4
500
500
488
490
96
96
75-125
0
20
Cobalt
ug/L
ND
500
500
488
484
97
97
75-125
1
20
Copper
ug/L
8.0
500
500
504
506
99
99
75-125
0
20
Lead
ug/L
ND
500
500
486
483
97
96
75-125
1
20
Nickel
ug/L
15.0
500
500
510
507
99
98
75-125
1
20
Selenium
ug/L
ND
500
500
460
455
92
91
75-125
1
20
Silver
ug/L
ND
250
250
260
260
104
104
75-125
0
20
Tin
ug/L
ND
500
500
484
482
97
96
75-125
0
20
Vanadium
ug/L
ND
500
500
527
529
105
105
75-125
0
20
Zinc
ug/L
118
500
500
632
631
103
103
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 77 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 590554 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376010,
92513376011,92513376012
METHOD BLANK: 3118022 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376010,
92513376011,92513376012
Parameter
Units
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Lead
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Tin
ug/L
Vanadium
ug/L
Zinc
ug/L
Blank
Result
Reporting
Limit
MDL
Analyzed Qualifiers
ND
5.0
3.0
01/05/2113:43
ND
10.0
4.7
01/05/2113:43
ND
5.0
3.5
01/05/2113:43
ND
1.0
0.70
01/05/2113:43
ND
1.0
0.40
01/05/2113:43
ND
5.0
3.7
01/05/2113:43
ND
5.0
3.6
01/05/2113:43
ND
5.0
4.3
01/05/2113:43
ND
5.0
4.5
01/05/2113:43
ND
5.0
3.5
01/05/2113:43
ND
10.0
4.7
01/05/2113:43
ND
5.0
2.5
01/05/2113:43
ND
5.0
4.7
01/05/2113:43
ND
5.0
3.9
01/05/2113:43
ND
10.0
9.5
01/05/2113:43
LABORATORY CONTROL SAMPLE:
Parameter
3118023
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
472
94
80-120
Arsenic
ug/L
500
459
92
80-120
Barium
ug/L
500
482
96
80-120
Beryllium
ug/L
500
471
94
80-120
Cadmium
ug/L
500
470
94
80-120
Chromium
ug/L
500
473
95
80-120
Cobalt
ug/L
500
475
95
80-120
Copper
ug/L
500
483
97
80-120
Lead
ug/L
500
464
93
80-120
Nickel
ug/L
500
473
95
80-120
Selenium
ug/L
500
462
92
80-120
Silver
ug/L
250
235
94
80-120
Tin
ug/L
500
471
94
80-120
Vanadium
ug/L
500
478
96
80-120
Zinc
ug/L
500
466
93
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 78 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
SURRY CLOSED LF ELKIN
92513376
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3118024
3118025
MS
MSD
92513201001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
490
486
98
97
75-125
1
20
Arsenic
ug/L
ND
500
500
483
466
97
93
75-125
4
20
Barium
ug/L
27.7
500
500
523
515
99
97
75-125
2
20
Beryllium
ug/L
ND
500
500
494
488
99
98
75-125
1
20
Cadmium
ug/L
ND
500
500
484
480
97
96
75-125
1
20
Chromium
ug/L
ND
500
500
486
480
97
96
75-125
1
20
Cobalt
ug/L
ND
500
500
486
486
97
97
75-125
0
20
Copper
ug/L
ND
500
500
493
485
98
97
75-125
2
20
Lead
ug/L
ND
500
500
479
475
96
95
75-125
1
20
Nickel
ug/L
ND
500
500
486
479
97
96
75-125
1
20
Selenium
ug/L
ND
500
500
493
488
99
98
75-125
1
20
Silver
ug/L
ND
250
250
244
240
97
96
75-125
1
20
Tin
ug/L
ND
500
500
483
477
97
95
75-125
1
20
Vanadium
ug/L
ND
500
500
493
486
98
97
75-125
1
20
Zinc
ug/L
ND
500
500
483
476
96
95
75-125
2
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 79 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589513 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007
METHOD BLANK: 3113790 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.10 0.050 12/31/2019:20
LABORATORY CONTROL SAMPLE: 3113791
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.7 107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3113792 3113793
MS MSD
92513376001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 10.6 10.7 106 107 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 80 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589514 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376008, 92513376009, 92513376010, 92513376011, 92513376012
METHOD BLANK: 3113794 Matrix: Water
Associated Lab Samples: 92513376008, 92513376009, 92513376010, 92513376011, 92513376012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.10 0.050 12/31/2017:52
LABORATORY CONTROL SAMPLE: 3113795
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.5 105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3113796 3113797
MS MSD
92513376008 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 10.7 10.7 107 107 75-125 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 81 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589025 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008,92513376009,92513376010,92513376011,92513376012
METHOD BLANK: 3111733 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008,92513376009,92513376010,92513376011,92513376012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
12/24/20 01:36
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
12/24/20 01:36
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
12/24/20 01:36
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
12/24/20 01:36
1,1-Dichloroethane
ug/L
ND
1.0
0.27
12/24/20 01:36
1,1-Dichloroethene
ug/L
ND
1.0
0.24
12/24/20 01:36
1,1-Dichloropropene
ug/L
ND
1.0
0.21
12/24/20 01:36
1,2,3-Trichlorobenzene
ug/L
ND
1.0
0.34
12/24/20 01:36
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
12/24/20 01:36
1,2,4-Trichlorobenzene
ug/L
ND
1.0
0.22
12/24/20 01:36
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
12/24/20 01:36
1,2-Dichloroethane
ug/L
ND
1.0
0.34
12/24/20 01:36
1,2-Dichloropropane
ug/L
ND
1.0
0.19
12/24/20 01:36
1,3-Dichloropropane
ug/L
ND
1.0
0.16
12/24/20 01:36
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
12/24/20 01:36
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
12/24/20 01:36
2,2-Dichloropropane
ug/L
ND
1.0
0.27
12/24/20 01:36
2-Butanone (MEK)
ug/L
ND
5.0
3.3
12/24/20 01:36
2-Hexanone
ug/L
ND
5.0
0.57
12/24/20 01:36
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
12/24/20 01:36
Acetone
ug/L
ND
25.0
6.2
12/24/20 01:36
Acetonitrile
ug/L
ND
50.0
30.4
12/24/20 01:36
Acrolein
ug/L
ND
10.0
2.7
12/24/20 01:36
Acrylonitrile
ug/L
ND
10.0
0.90
12/24/20 01:36
Allyl chloride
ug/L
ND
2.0
0.28
12/24/20 01:36
Benzene
ug/L
ND
1.0
0.15
12/24/20 01:36
Bromochloromethane
ug/L
ND
1.0
0.34
12/24/20 01:36
Bromodichloromethane
ug/L
ND
1.0
0.26
12/24/20 01:36
Bromoform
ug/L
ND
1.0
0.62
12/24/20 01:36
Bromomethane
ug/L
ND
2.0
0.62
12/24/20 01:36
Carbon disulfide
ug/L
ND
2.0
0.40
12/24/20 01:36
Carbon tetrachloride
ug/L
ND
1.0
0.22
12/24/20 01:36
Chlorobenzene
ug/L
ND
1.0
0.23
12/24/20 01:36
Chloroethane
ug/L
ND
1.0
0.49
12/24/20 01:36
Chloroform
ug/L
ND
5.0
2.3
12/24/20 01:36
Chloromethane
ug/L
ND
1.0
0.39
12/24/20 01:36
Chloroprene
ug/L
ND
5.0
1.7
12/24/20 01:36
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
12/24/20 01:36
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
12/24/20 01:36
IH,v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 82 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
METHOD BLANK: 3111733 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008,92513376009,92513376010,92513376011,92513376012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Dibromochloromethane
ug/L
ND
1.0
0.41
12/24/20 01:36
Dibromomethane
ug/L
ND
1.0
0.46
12/24/20 01:36
Dichlorodifluoromethane
ug/L
ND
1.0
0.23
12/24/20 01:36
Ethyl methacrylate
ug/L
ND
1.0
0.51
12/24/20 01:36
Ethylbenzene
ug/L
ND
1.0
0.26
12/24/20 01:36
Hexachloro-1,3-butadiene
ug/L
ND
1.0
0.44
12/24/20 01:36
lodomethane
ug/L
ND
20.0
12.5
12/24/20 01:36
Isobutanol
ug/L
ND
100
66.4
12/24/20 01:36
Methacrylonitrile
ug/L
ND
10.0
1.9
12/24/20 01:36
Methyl methacrylate
ug/L
ND
2.0
0.46
12/24/20 01:36
Methylene Chloride
ug/L
ND
5.0
3.7
12/24/20 01:36
Naphthalene
ug/L
ND
1.0
0.35
12/24/20 01:36
Propionitrile
ug/L
ND
20.0
1.8
12/24/20 01:36
Styrene
ug/L
ND
1.0
0.27
12/24/20 01:36
Tetrachloroethene
ug/L
ND
1.0
0.16
12/24/20 01:36
Toluene
ug/L
ND
1.0
0.24
12/24/20 01:36
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
12/24/20 01:36
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
12/24/20 01:36
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
12/24/20 01:36 IH
Trichloroethene
ug/L
ND
1.0
0.22
12/24/20 01:36
Trichlorofluoromethane
ug/L
ND
1.0
0.31
12/24/20 01:36
Vinyl acetate
ug/L
ND
2.0
1.4
12/24/20 01:36
Vinyl chloride
ug/L
ND
1.0
0.24
12/24/20 01:36
Xylene (Total)
ug/L
ND
1.0
0.63
12/24/20 01:36
1,2-Dichloroethane-d4 (S)
%
95
70-130
12/24/20 01:36
4-Bromofluorobenzene (S)
%
99
70-130
12/24/20 01:36
Toluene-d8 (S)
%
100
70-130
12/24/20 01:36
LABORATORY CONTROL SAMPLE:
3111734
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
48.6
97
70-130
1,1,1-Trichloroethane
ug/L
50
45.6
91
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.7
97
70-130
1,1,2-Trichloroethane
ug/L
50
49.8
100
70-130
1,1-Dichloroethane
ug/L
50
45.9
92
70-130
1,1-Dichloroethene
ug/L
50
46.8
94
70-132
1,1-Dichloropropene
ug/L
50
45.7
91
70-131
1,2,3-Trichlorobenzene
ug/L
50
45.5
91
70-134
1,2,3-Trichloropropane
ug/L
50
49.4
99
70-130
1,2,4-Trichlorobenzene
ug/L
50
46.9
94
70-130
1,2-Dichlorobenzene
ug/L
50
47.9
96
70-130
1,2-Dichloroethane
ug/L
50
44.9
90
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 83 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE: 3111734
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,2-Dichloropropane
ug/L
50
48.6
97
70-130
1,3-Dichloropropane
ug/L
50
49.4
99
70-130
1,4-Dichlorobenzene
ug/L
50
47.6
95
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
1030
103
70-137
2,2-Dichloropropane
ug/L
50
42.5
85
70-130
2-Butanone (MEK)
ug/L
100
95.6
96
70-133
2-Hexanone
ug/L
100
94.5
94
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
96.9
97
70-130
Acetone
ug/L
100
88.4
88
70-144
Acetonitrile
ug/L
500
497
99
68-134
Acrolein
ug/L
250
313
125
32-2001H,v3
Acrylonitrile
ug/L
250
241
97
70-130
Allyl chloride
ug/L
50
45.4
91
70-134
Benzene
ug/L
50
46.3
93
70-130
Bromochloromethane
ug/L
50
48.7
97
70-130
Bromodichloromethane
ug/L
50
47.5
95
70-130
Bromoform
ug/L
50
49.5
99
70-131
Bromomethane
ug/L
50
45.9
92
30-177
Carbon disulfide
ug/L
50
46.6
93
70-133
Carbon tetrachloride
ug/L
50
46.7
93
70-130
Chlorobenzene
ug/L
50
47.7
95
70-130
Chloroethane
ug/L
50
52.8
106
46-131
Chloroform
ug/L
50
45.6
91
70-130
Chloromethane
ug/L
50
38.5
77
49-130
Chloroprene
ug/L
50
45.4
91
70-130
cis-1,2-Dichloroethene
ug/L
50
44.2
88
70-130
cis-1,3-Dichloropropene
ug/L
50
49.4
99
70-130
Dibromochloromethane
ug/L
50
50.9
102
70-130
Dibromomethane
ug/L
50
51.2
102
70-130
Dichlorodifluoromethane
ug/L
50
39.3
79
52-134
Ethyl methacrylate
ug/L
50
48.3
97
70-130
Ethylbenzene
ug/L
50
46.7
93
70-130
Hexachloro-1,3-butadiene
ug/L
50
43.2
86
70-131
lodomethane
ug/L
100
93.8
94
47-140
Isobutanol
ug/L
1000
891
89
62-136
Methacrylonitrile
ug/L
500
479
96
70-130
Methyl methacrylate
ug/L
50
47.1
94
70-130
Methylene Chloride
ug/L
50
43.0
86
68-130
Naphthalene
ug/L
50
46.6
93
70-133
Propionitrile
ug/L
500
483
97
70-130
Styrene
ug/L
50
47.2
94
70-130
Tetrachloroethene
ug/L
50
45.8
92
70-130
Toluene
ug/L
50
47.0
94
70-130
trans-1,2-Dichloroethene
ug/L
50
45.1
90
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.2
98
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
56.5
113
25-2001H
Trichloroethene
ug/L
50
48.1
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 84 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE:
3111734
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Trichlorofluoromethane
ug/L
50
47.3
95
61-130
Vinyl acetate
ug/L
100
107
107
70-140
Vinyl chloride
ug/L
50
39.5
79
59-142
Xylene (Total)
ug/L
150
141
94
70-130
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
3111736
92513376012
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.5
103
70-135
1,1,1-Trichloroethane
ug/L
ND
20
20.4
102
70-148
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20.7
103
70-131
1,1,2-Trichloroethane
ug/L
ND
20
20.6
103
70-136
1,1-Dichloroethane
ug/L
ND
20
20.1
100
70-147
1,1-Dichloroethene
ug/L
ND
20
20.5
102
70-158
1,1-Dichloropropene
ug/L
ND
20
19.4
97
70-149
1,2,3-Trichlorobenzene
ug/L
ND
20
17.6
88
68-140
1,2,3-Trichloropropane
ug/L
ND
20
20.7
103
67-137
1,2,4-Trichlorobenzene
ug/L
ND
20
17.5
87
70-139
1,2-Dichlorobenzene
ug/L
ND
20
19.7
99
70-133
1,2-Dichloroethane
ug/L
ND
20
18.6
93
67-138
1,2-Dichloropropane
ug/L
ND
20
20.7
104
70-138
1,3-Dichloropropane
ug/L
ND
20
20.8
104
70-136
1,4-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
471
118
69-146
2,2-Dichloropropane
ug/L
ND
20
14.8
74
52-155
2-Butanone (MEK)
ug/L
ND
40
45.0
112
61-147
2-Hexanone
ug/L
ND
40
42.2
106
67-139
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
41.7
104
67-136
Acetone
ug/L
ND
40
42.5
106
55-159
Acetonitrile
ug/L
ND
200
213
107
66-145
Acrolein
ug/L
ND
100
118
118
10-2001H
Acrylonitrile
ug/L
ND
100
107
107
68-140
AIIyl chloride
ug/L
ND
20
18.8
94
70-147
Benzene
ug/L
ND
20
20.0
100
67-150
Bromochloromethane
ug/L
ND
20
21.7
108
70-146
Bromodichloromethane
ug/L
ND
20
19.8
99
70-138
Bromoform
ug/L
ND
20
19.1
95
57-138
Bromomethane
ug/L
ND
20
13.4
67
10-200
Carbon disulfide
ug/L
ND
20
18.7
94
70-152
Carbon tetrachloride
ug/L
ND
20
20.1
100
70-147
Chlorobenzene
ug/L
ND
20
20.7
103
70-137
Chloroethane
ug/L
ND
20
22.7
114
51-166
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 85 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
MATRIX SPIKE SAMPLE:
Parameter
3111736
Units
92513376012
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Chloroform
ug/L
ND
20
20.1
101
70-144
Chloromethane
ug/L
ND
20
17.3
87
24-161
Chloroprene
ug/L
ND
20
20.0
100
70-143
cis-1,2-Dichloroethene
ug/L
ND
20
19.1
96
67-148
cis-1,3-Dichloropropene
ug/L
ND
20
18.8
94
70-142
Dibromochloromethane
ug/L
ND
20
20.3
101
68-138
Dibromomethane
ug/L
ND
20
22.0
110
70-134
Dichlorodifluoromethane
ug/L
ND
20
17.1
85
43-155
Ethyl methacrylate
ug/L
ND
20
19.8
99
70-137
Ethylbenzene
ug/L
ND
20
20.0
100
68-143
Hexachloro-1,3-butadiene
ug/L
ND
20
16.0
80
62-151
lodomethane
ug/L
ND
40
24.1
60
20-161
Isobutanol
ug/L
ND
400
386
97
44-145
Methacrylonitrile
ug/L
ND
200
202
101
67-139
Methyl methacrylate
ug/L
ND
20
20.3
101
70-130
Methylene Chloride
ug/L
ND
20
18.5
93
64-148
Naphthalene
ug/L
ND
20
19.4
97
57-150
Propionitrile
ug/L
ND
200
215
108
70-138
Styrene
ug/L
ND
20
20.0
100
70-136
Tetrachloroethene
ug/L
ND
20
19.5
97
70-139
Toluene
ug/L
ND
20
20.4
102
47-157
trans-1,2-Dichloroethene
ug/L
ND
20
18.7
93
70-149
trans- 1,3-Dichloropropene
ug/L
ND
20
18.3
92
70-138
trans-1,4-Dichloro-2-butene
ug/L
ND
20
17.4
87
31-1451H
Trichloroethene
ug/L
ND
20
20.5
102
70-149
Trichlorofluoromethane
ug/L
ND
20
19.8
99
61-154
Vinyl acetate
ug/L
ND
40
31.5
79
48-156
Vinyl chloride
ug/L
ND
20
17.2
86
55-172
Xylene (Total)
ug/L
ND
60
58.7
98
66-145
1,2-Dichloroethane-d4 (S)
%
89
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 3111735
92513376011
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,1-Dichloropropene
ug/L
ND
ND
30
1,2,3-Trichlorobenzene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 86 of 118

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
SAMPLE DUPLICATE: 3111735
Parameter
Units
92513376011
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,3-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
ND
30
2,2-Dichloropropane
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Acetonitrile
ug/L
ND
ND
30
Acrolein
ug/L
ND
ND
301H
Acrylonitrile
ug/L
ND
ND
30
Allyl chloride
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromochloromethane
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
Bromomethane
ug/L
ND
ND
30
Carbon disulfide
ug/L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
ND
ND
30
Chloroethane
ug/L
ND
ND
30
Chloroform
ug/L
ND
ND
30
Chloromethane
ug/L
ND
ND
30
Chloroprene
ug/L
ND
ND
30
cis-1,2-Dichloroethene
ug/L
ND
ND
30
cis-1,3-Dichloropropene
ug/L
ND
ND
30
Dibromochloromethane
ug/L
ND
ND
30
Dibromomethane
ug/L
ND
ND
30
Dichlorodifluoromethane
ug/L
ND
ND
30
Ethyl methacrylate
ug/L
ND
ND
30
Ethylbenzene
ug/L
ND
ND
30
Hexachloro-1,3-butadiene
ug/L
ND
ND
30
lodomethane
ug/L
ND
ND
30
Isobutanol
ug/L
ND
ND
30
Methacrylonitrile
ug/L
ND
ND
30
Methyl methacrylate
ug/L
ND
ND
30
Methylene Chloride
ug/L
ND
ND
30
Naphthalene
ug/L
ND
ND
30
Propionitrile
ug/L
ND
ND
30
Styrene
ug/L
ND
ND
30
Tetrachloroethene
ug/L
ND
ND
30
Toluene
ug/L
ND
ND
30
trans-1,2-Dichloroethene
ug/L
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 87 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
SAMPLE DUPLICATE: 3111735
Parameter
trans- 1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
QUALITY CONTROL DATA
Units
92513376011
Result
Dup
Result
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
%
95
96
%
98
99
%
99
98
Max
RPD RPD Qualifiers
30
30 I H
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 88 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589473 Analysis Method: EPA 8081 B
QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513376006
METHOD BLANK: 3113649
Associated Lab Samples: 92513376006
Parameter
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
beta-BHC
Chlordane (Technical)
delta-BHC
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Matrix: Water
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
ug/L
ND
0.050
0.0069
12/28/20 12:26
ug/L
ND
0.050
0.0064
12/28/20 12:26
ug/L
ND
0.050
0.018
12/28/20 12:26
ug/L
ND
0.050
0.022
12/28/20 12:26
ug/L
ND
0.050
0.019
12/28/20 12:26
ug/L
ND
0.050
0.014
12/28/20 12:26
ug/L
ND
0.20
0.14
12/28/20 12:26
ug/L
ND
0.050
0.020
12/28/20 12:26
ug/L
ND
0.050
0.0073
12/28/20 12:26
ug/L
ND
0.050
0.0094
12/28/20 12:26
ug/L
ND
0.050
0.0065
12/28/20 12:26
ug/L
ND
0.050
0.0091
12/28/20 12:26
ug/L
ND
0.050
0.0089
12/28/20 12:26
ug/L
ND
0.050
0.013
12/28/20 12:26
ug/L
ND
0.050
0.012
12/28/20 12:26
ug/L
ND
0.050
0.016
12/28/20 12:26
ug/L
ND
0.050
0.0097
12/28/20 12:26
ug/L
ND
0.15
0.033
12/28/20 12:26
ug/L
ND
0.20
0.19
12/28/20 12:26
%
127
10-154
12/28/20 12:26
%
64
10-184
12/28/20 12:26
LABORATORY CONTROL SAMPLE: 3113650
Qualifiers
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
0.25
0.31
125
45-158
4,4'-DDE
ug/L
0.25
0.27
108
37-141
4,4'-DDT
ug/L
0.25
0.31
124
52-160
Aldrin
ug/L
0.25
0.13
52
10-130
alpha-BHC
ug/L
0.25
0.28
113
37-139
beta-BHC
ug/L
0.25
0.34
138
39-176
delta-BHC
ug/L
0.25
0.27
110
39-144
Dieldrin
ug/L
0.25
0.31
124
40-149
Endosulfan I
ug/L
0.25
0.31
122
44-145
Endosulfan II
ug/L
0.25
0.31
123
47-153
Endosulfan sulfate
ug/L
0.25
0.31
125
48-159
Endrin
ug/L
0.25
0.33
132
41-155
Endrin aldehyde
ug/L
0.25
0.28
114
45-146
gamma-BHC (Lindane)
ug/L
0.25
0.27
109
42-146
Results presented on
this page are in the units
indicated by the "Units"
column except
where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 89 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE:
3113650
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Heptachlor
ug/L
0.25
0.19
76
23-135
Heptachlor epoxide
ug/L
0.25
0.28
111
39-142
Methoxychlor
ug/L
0.75
0.95
127
55-173
Decachlorobiphenyl (S)
%
125
10-154
Tetrachloro-m-xylene (S)
%
52
10-184
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3113651
3113652
MS
MSD
92513376006
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
4,4'-DDD
ug/L
ND
0.25
0.25
0.30
0.29
118
116
36-169
2
30
4,4'-DDE
ug/L
ND
0.25
0.25
0.24
0.25
94
102
31-154
7
30
4,4'-DDT
ug/L
ND
0.25
0.25
0.27
0.27
107
108
23-187
1
30
Aldrin
ug/L
ND
0.25
0.25
0.20
0.20
78
79
10-141
2
30
alpha-BHC
ug/L
ND
0.25
0.25
0.28
0.23
113
91
25-151
22
30
beta-BHC
ug/L
ND
0.25
0.25
0.37
0.33
147
133
30-188
10
30
delta-BHC
ug/L
ND
0.25
0.25
0.29
0.27
115
106
32-157
8
30
Dieldrin
ug/L
ND
0.25
0.25
0.29
0.29
117
116
24-165
1
30
Endosulfan I
ug/L
ND
0.25
0.25
0.28
0.27
114
109
19-168
5
30
Endosulfan II
ug/L
ND
0.25
0.25
0.31
0.29
124
118
27-176
5
30
Endosulfan sulfate
ug/L
ND
0.25
0.25
0.32
0.30
128
118
31-174
8
30
Endrin
ug/L
ND
0.25
0.25
0.32
0.30
127
121
23-171
5
30
Endrin aldehyde
ug/L
ND
0.25
0.25
0.28
0.27
112
106
16-177
5
30
gamma-BHC (Lindane)
ug/L
ND
0.25
0.25
0.28
0.26
112
104
29-157
8
30
Heptachlor
ug/L
ND
0.25
0.25
0.26
0.25
104
100
11-149
4
30
Heptachlor epoxide
ug/L
ND
0.25
0.25
0.26
0.26
103
105
21-157
2
30
Methoxychlor
ug/L
ND
0.75
0.75
0.87
0.86
116
115
33-193
1
30
Decachlorobiphenyl (S)
%
96
117
10-154
Tetrachloro-m-xylene (S)
%
74
67
10-184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 90 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589664 Analysis Method: EPA 8081 B
QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376007, 92513376008,
92513376009,92513376010
METHOD BLANK: 3114378 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376007, 92513376008,
92513376009,92513376010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
4,4'-DDD
ug/L
ND
0.050
0.0069
12/31/20 12:04
4,4'-DDE
ug/L
ND
0.050
0.0064
12/31/20 12:04
4,4'-DDT
ug/L
ND
0.050
0.018
12/31/20 12:04
Aldrin
ug/L
ND
0.050
0.022
12/31/20 12:04
alpha-BHC
ug/L
ND
0.050
0.019
12/31/20 12:04
beta-BHC
ug/L
ND
0.050
0.014
12/31/20 12:04
Chlordane (Technical)
ug/L
ND
0.20
0.14
12/31/20 12:04
delta-BHC
ug/L
ND
0.050
0.020
12/31/20 12:04
Dieldrin
ug/L
ND
0.050
0.0073
12/31/20 12:04
Endosulfan I
ug/L
ND
0.050
0.0094
12/31/20 12:04
Endosulfan II
ug/L
ND
0.050
0.0065
12/31/20 12:04
Endosulfan sulfate
ug/L
ND
0.050
0.0091
12/31/20 12:04
Endrin
ug/L
ND
0.050
0.0089
12/31/20 12:04
Endrin aldehyde
ug/L
ND
0.050
0.013
12/31/20 12:04
gamma-BHC (Lindane)
ug/L
ND
0.050
0.012
12/31/20 12:04
Heptachlor
ug/L
ND
0.050
0.016
12/31/20 12:04
Heptachlor epoxide
ug/L
ND
0.050
0.0097
12/31/20 12:04
Methoxychlor
ug/L
ND
0.15
0.033
12/31/20 12:04
Toxaphene
ug/L
ND
0.20
0.19
12/31/20 12:04
Decachlorobiphenyl (S)
%
64
10-154
12/31/20 12:04
Tetrachloro-m-xylene (S)
%
36
10-184
12/31/20 12:04
LABORATORY CONTROL SAMPLE:
Parameter
3114379
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
0.25
0.24
95
45-158
4,4'-DDE
ug/L
0.25
0.24
95
37-141
4,4'-DDT
ug/L
0.25
0.17
68
52-160
Aldrin
ug/L
0.25
0.15
59
10-130
alpha-BHC
ug/L
0.25
0.18
73
37-139
beta-BHC
ug/L
0.25
0.22
86
39-176
delta-BHC
ug/L
0.25
0.22
88
39-144
Dieldrin
ug/L
0.25
0.23
91
40-149
Endosulfan I
ug/L
0.25
0.23
93
44-145
Endosulfan II
ug/L
0.25
0.23
94
47-153
Endosulfan sulfate
ug/L
0.25
0.24
96
48-159
Endrin
ug/L
0.25
0.23
90
41-155
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 91 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE:
3114379
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Endrin aldehyde
ug/L
0.25
0.21
84
45-146
gamma-BHC (Lindane)
ug/L
0.25
0.18
74
42-146
Heptachlor
ug/L
0.25
0.15
61
23-135
Heptachlor epoxide
ug/L
0.25
0.23
90
39-142
Methoxychlor
ug/L
0.75
0.66
88
55-173
Decachlorobiphenyl (S)
%
127
10-154
Tetrachloro-m-xylene (S)
%
77
10-184
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3114380
MS
92513376001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3114381
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
4,4'-DDD
ug/L
ND
0.5
0.5
0.72
0.64
144
128
36-169
12
30
4,4'-DDE
ug/L
ND
0.5
0.5
0.72
0.63
144
125
31-154
14
30
4,4'-DDT
ug/L
ND
0.5
0.5
0.52
0.47
104
95
23-187
10
30
Aldrin
ug/L
ND
0.5
0.5
0.49
0.45
98
91
10-141
7
30
alpha-BHC
ug/L
ND
0.5
0.5
0.56
0.52
112
105
25-151
7
30
beta-BHC
ug/L
ND
0.5
0.5
0.69
0.61
138
123
30-188
12
30
delta-BHC
ug/L
ND
0.5
0.5
0.67
0.62
134
123
32-157
8
30
Dieldrin
ug/L
ND
0.5
0.5
0.70
0.64
140
128
24-165
9
30
Endosulfan I
ug/L
ND
0.5
0.5
0.69
0.64
138
127
19-168
8
30
Endosulfan II
ug/L
ND
0.5
0.5
0.70
0.65
140
130
27-176
8
30
Endosulfan sulfate
ug/L
ND
0.5
0.5
0.71
0.67
143
133
31-174
7
30
Endrin
ug/L
ND
0.5
0.5
0.68
0.63
136
126
23-171
8
30
Endrin aldehyde
ug/L
ND
0.5
0.5
0.62
0.58
125
115
16-177
8
30
gamma-BHC (Lindane)
ug/L
ND
0.5
0.5
0.60
0.53
120
105
29-157
13
30
Heptachlor
ug/L
ND
0.5
0.5
0.49
0.48
99
95
11-149
4
30
Heptachlor epoxide
ug/L
ND
0.5
0.5
0.67
0.56
134
113
21-157
17
30
Methoxychlor
ug/L
ND
1.5
1.5
1.9
1.8
129
117
33-193
10
30
Decachlorobiphenyl (S)
%
158
147
10-154
SO
Tetrachloro-m-xylene (S)
%
104
87
10-184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 92 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589665 Analysis Method: EPA 8082A
QC Batch Method: EPA 3510C Analysis Description: 8082 GCS PCB
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008,92513376009,92513376010
METHOD BLANK: 3114382
Matrix:
Water
Associated Lab Samples:
92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008,92513376009,92513376010
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
0.22
12/30/20 19:18
PCB-1221 (Aroclor 1221)
ug/L
ND
0.50
0.32
12/30/20 19:18
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
0.21
12/30/20 19:18
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
0.44
12/30/20 19:18
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
0.34
12/30/20 19:18
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
0.24
12/30/20 19:18
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
0.30
12/30/20 19:18
Decachlorobiphenyl (S)
%
59
10-181
12/30/20 19:18
LABORATORY CONTROL SAMPLE: 3114383
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
PCB-1016 (Aroclor 1016) ug/L 5 3.9 78 41-137
PCB-1260 (Aroclor 1260) ug/L 5 4.4 88 42-156
Decachlorobiphenyl (S) % 113 10-181
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3114384
3114385
MS
MSD
92513376001 Spike
Spike MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
PCB-1016 (Aroclor 1016)
ug/L
ND 10
10 7.8
5.4
78
54
22-145
36 30 R1
PCB-1260 (Aroclor 1260)
ug/L
ND 10
10 8.5
6.0
85
60
10-167
34 30 R1
Decachlorobiphenyl (S)
%
98
70
10-181
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 93 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589474 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water APP9 RV MSSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376009,92513376010
METHOD BLANK: 3113653
Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376009,92513376010
Parameter
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
1,2,4,5-Tetrachlorobenzene
ug/L
ND
10.0
4.6
12/29/20 10:21
1,3,5-Trinitrobenzene
ug/L
ND
10.0
5.3
12/29/20 10:21
1,3-Dinitrobenzene
ug/L
ND
10.0
3.7
12/29/20 10:21
1,4-Naphthoquinone
ug/L
ND
5.0
2.4
12/29/20 10:21
1-Naphthalenamine
ug/L
ND
5.0
4.6
12/29/20 10:21
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
1.2
12/29/20 10:21
2,3,4,6-Tetrachlorophenol
ug/L
ND
10.0
1.5
12/29/20 10:21
2,4,5-Trichlorophenol
ug/L
ND
10.0
1.4
12/29/20 10:21
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.6
12/29/20 10:21
2,4-Dichlorophenol
ug/L
ND
10.0
1.4
12/29/20 10:21
2,4-Dimethylphenol
ug/L
ND
10.0
1.7
12/29/20 10:21
2,4-Dinitrophenol
ug/L
ND
50.0
26.0
12/29/20 10:21
2,4-Dinitrotoluene
ug/L
ND
10.0
1.6
12/29/20 10:21
2,6-Dichlorophenol
ug/L
ND
10.0
2.7
12/29/20 10:21
2,6-Dinitrotoluene
ug/L
ND
10.0
1.7
12/29/20 10:21
2-Acetylaminofluorene
ug/L
ND
10.0
1.9
12/29/20 10:21
2-Chloronaphthalene
ug/L
ND
10.0
1.7
12/29/20 10:21
2-Chlorophenol
ug/L
ND
10.0
1.2
12/29/20 10:21
2-Methylnaphthalene
ug/L
ND
10.0
1.9
12/29/20 10:21
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
1.9
12/29/20 10:21
2-Naphthalenamine
ug/L
ND
10.0
6.1
12/29/20 10:21
2-Nitroaniline
ug/L
ND
20.0
3.0
12/29/20 10:21
2-Nitrophenol
ug/L
ND
10.0
1.4
12/29/20 10:21
3&4-Methylphenol (m&p Cresol)
ug/L
ND
10.0
1.2
12/29/20 10:21
3,3'-Dichlorobenzidine
ug/L
ND
20.0
8.1
12/29/20 10:21
3,3'-Dimethylbenzidine
ug/L
ND
25.0
23.5
12/29/20 10:21
3-Methylcholanthrene
ug/L
ND
10.0
5.3
12/29/20 10:21
3-Nitroaniline
ug/L
ND
20.0
3.8
12/29/20 10:21
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
3.4
12/29/20 10:21
4-Aminobiphenyl
ug/L
ND
10.0
4.2
12/29/20 10:21
4-Bromophenylphenyl ether
ug/L
ND
10.0
1.8
12/29/20 10:21
4-Chloro-3-methyl phenol
ug/L
ND
10.0
3.3
12/29/20 10:21
4-Chloroaniline
ug/L
ND
20.0
3.6
12/29/20 10:21
4-Chlorophenylphenyl ether
ug/L
ND
10.0
2.0
12/29/20 10:21
4-Nitroaniline
ug/L
ND
20.0
5.1
12/29/20 10:21
4-Nitrophenol
ug/L
ND
50.0
6.6
12/29/20 10:21
5-Nitro-o-toluidine
ug/L
ND
10.0
2.4
12/29/20 10:21
7,12-Dimethylbenz(a)anthracene
ug/L
ND
10.0
2.8
12/29/20 10:21
Acenaphthene
ug/L
ND
10.0
2.0
12/29/20 10:21
v1
IH
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 94 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
METHOD BLANK: 3113653 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376009,92513376010
Parameter
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
Acenaphthylene
ug/L
ND
10.0
2.0
12/29/20 10:21
Acetophenone
ug/L
ND
10.0
1.5
12/29/20 10:21
Anthracene
ug/L
ND
10.0
2.3
12/29/20 10:21
Benzo(a)anthracene
ug/L
ND
10.0
2.7
12/29/20 10:21
Benzo(a)pyrene
ug/L
ND
10.0
2.8
12/29/20 10:21
Benzo(b)fluoranthene
ug/L
ND
10.0
2.6
12/29/20 10:21
Benzo(g,h,i)perylene
ug/L
ND
10.0
2.8
12/29/20 10:21
Benzo(k)fluoranthene
ug/L
ND
10.0
2.7
12/29/20 10:21
Benzyl alcohol
ug/L
ND
20.0
2.9
12/29/20 10:21
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
1.8
12/29/20 10:21
bis(2-Chloroethyl) ether
ug/L
ND
10.0
1.9
12/29/20 10:21
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
3.7
12/29/20 10:21
Butylbenzylphthalate
ug/L
ND
10.0
3.1
12/29/20 10:21
Chlorobenzilate
ug/L
ND
10.0
3.6
12/29/20 10:21
Chrysene
ug/L
ND
10.0
2.8
12/29/20 10:21
Di-n-butylphthalate
ug/L
ND
10.0
2.2
12/29/20 10:21
Di-n-octylphthalate
ug/L
ND
10.0
3.9
12/29/20 10:21
Diallate
ug/L
ND
10.0
2.7
12/29/20 10:21
Dibenz(a,h)anthracene
ug/L
ND
10.0
3.0
12/29/20 10:21
Dibenzofuran
ug/L
ND
10.0
2.1
12/29/20 10:21
Diethylphthalate
ug/L
ND
10.0
2.0
12/29/20 10:21
Dimethoate
ug/L
ND
10.0
2.0
12/29/20 10:21
Dimethylphthalate
ug/L
ND
10.0
2.1
12/29/20 10:21
Diphenylamine
ug/L
ND
10.0
3.0
12/29/20 10:21
Disulfoton
ug/L
ND
10.0
6.0
12/29/20 10:21
Ethyl methanesulfonate
ug/L
ND
20.0
2.8
12/29/20 10:21
Famphur
ug/L
ND
10.0
5.7
12/29/20 10:21
Fluoranthene
ug/L
ND
10.0
2.2
12/29/20 10:21
Fluorene
ug/L
ND
10.0
2.1
12/29/20 10:21
Hexachlorobenzene
ug/L
ND
10.0
2.2
12/29/20 10:21
Hexachlorocyclopentadiene
ug/L
ND
10.0
1.6
12/29/20 10:21
Hexachloroethane
ug/L
ND
10.0
1.4
12/29/20 10:21
Hexachloropropene
ug/L
ND
10.0
5.5
12/29/20 10:21
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
2.9
12/29/20 10:21
Isodrin
ug/L
ND
10.0
3.0
12/29/20 10:21
Isophorone
ug/L
ND
10.0
1.7
12/29/20 10:21
Isosafrole
ug/L
ND
10.0
3.6
12/29/20 10:21
Kepone
ug/L
ND
10.0
8.2
12/29/20 10:21
Methapyrilene
ug/L
ND
50.0
27.2
12/29/20 10:21
Methyl methanesulfonate
ug/L
ND
5.0
3.0
12/29/20 10:21
Methyl parathion
ug/L
ND
10.0
2.0
12/29/20 10:21
N-Nitroso-di-n-butylamine
ug/L
ND
10.0
6.2
12/29/20 10:21
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
1.3
12/29/20 10:21
N-Nitrosodiethylamine
ug/L
ND
10.0
2.0
12/29/20 10:21
N-Nitrosodimethylamine
ug/L
ND
10.0
1.9
12/29/20 10:21
Qualifiers
v1
IH
v1
IL
IH,v1
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 95 of 118

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
METHOD BLANK: 3113653 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376009,92513376010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
12/29/20 10:21
N-Nitrosomethylethylamine
ug/L
ND
10.0
3.3
12/29/20 10:21
N-Nitrosopiperidine
ug/L
ND
10.0
2.6
12/29/20 10:21
N-Nitrosopyrrolidine
ug/L
ND
10.0
2.1
12/29/20 10:21 v2
Nitrobenzene
ug/L
ND
10.0
1.9
12/29/20 10:21
O,O,O-Triethylphosphorothioate
ug/L
ND
10.0
3.5
12/29/20 10:21
O-Toluidine
ug/L
ND
10.0
2.8
12/29/20 10:21
P-Dimethylaminoazobenzene
ug/L
ND
5.0
3.3
12/29/20 10:21 IL
p-Phenylenediamine
ug/L
ND
10.0
10.0
12/29/20 10:21
Parathion (Ethyl parathion)
ug/L
ND
10.0
2.0
12/29/20 10:21
Pentachlorobenzene
ug/L
ND
10.0
4.4
12/29/20 10:21
Pentachloronitrobenzene
ug/L
ND
10.0
2.4
12/29/20 10:21
Pentachlorophenol
ug/L
ND
20.0
3.8
12/29/20 10:21
Phenacetin
ug/L
ND
10.0
1.9
12/29/20 10:21
Phenanthrene
ug/L
ND
10.0
2.0
12/29/20 10:21
Phenol
ug/L
ND
10.0
1.4
12/29/20 10:21
Phorate
ug/L
ND
10.0
3.8
12/29/20 10:21 v1
Pronamide
ug/L
ND
10.0
2.4
12/29/20 10:21
Pyrene
ug/L
ND
10.0
2.2
12/29/20 10:21
Safrole
ug/L
ND
10.0
3.2
12/29/20 10:21
Thionazin
ug/L
ND
10.0
1.8
12/29/20 10:21
2,4,6-Tribromophenol (S)
%
31
10-144
12/29/20 10:21
2-Fluorobiphenyl (S)
%
55
10-130
12/29/20 10:21
2-Fluorophenol (S)
%
24
10-130
12/29/20 10:21
Nitrobenzene-d5 (S)
%
78
10-144
12/29/20 10:21
Phenol-d6 (S)
%
14
10-130
12/29/20 10:21
Terphenyl-d14 (S)
%
128
34-163
12/29/20 10:21
LABORATORY CONTROL SAMPLE:
Parameter
3113654
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4,5-Tetrachlorobenzene
ug/L
50
23.1
46
17-130
1,3,5-Trinitrobenzene
ug/L
50
60.9
122
44-200
1,3-Dinitrobenzene
ug/L
50
46.8
94
39-159
1,4-Naphthoquinone
ug/L
50
34.4
69
10-159
1-Naphthalenamine
ug/L
50
42.7
85
10-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
41.1
82
28-130 v1
2,3,4,6-Tetrachlorophenol
ug/L
50
44.2
88
10-200
2,4,5-Trichlorophenol
ug/L
50
45.7
91
35-130
2,4,6-Trichlorophenol
ug/L
50
41.8
84
31-130
2,4-DichIorophenol
ug/L
50
39.2
78
35-130
2,4-Dimethylphenol
ug/L
50
43.9
88
34-130
2,4-Dinitrophenol
ug/L
250
165
66
10-153
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 96 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE:
Parameter
3113654
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4-Dinitrotoluene
ug/L
50
53.5
107
37-136
2,6-Dichlorophenol
ug/L
50
40.1
80
31-139
2,6-Dinitrotoluene
ug/L
50
53.2
106
33-136
2-Acetylaminofluorene
ug/L
50
45.7
91
19-181
2-Chloronaphthalene
ug/L
50
32.6
65
26-130
2-Chlorophenol
ug/L
50
37.6
75
37-130
2-Methylnaphthalene
ug/L
50
23.5
47
29-130
2-Methylphenol(o-Cresol)
ug/L
50
34.4
69
35-130
2-Naphthalenamine
ug/L
50
41.3
83
10-136
2-Nitroaniline
ug/L
100
91.0
91
37-130
2-Nitrophenol
ug/L
50
40.5
81
32-130
3&4-Methyl phenol (m&p Cresol)
ug/L
50
35.9
72
34-130
3,3'-Dichlorobenzidine
ug/L
100
103
103
34-136
3,3'-Dimethylbenzidine
ug/L
100
184
184
10-2001H
3-Methylcholanthrene
ug/L
50
47.4
95
39-190
3-Nitroaniline
ug/L
100
97.1
97
37-138
4,6-Dinitro-2-methyl phenol
ug/L
100
91.7
92
21-157
4-Aminobiphenyl
ug/L
50
50.2
100
17-137
4-Bromophenylphenyl ether
ug/L
50
45.2
90
38-130
4-ChIoro-3-methyl phenol
ug/L
100
82.2
82
37-130
4-Chloroaniline
ug/L
100
79.6
80
38-130
4-Chlorophenylphenyl ether
ug/L
50
41.3
83
33-130
4-Nitroaniline
ug/L
100
105
105
42-137
4-Nitrophenol
ug/L
250
131
53
10-130
5-Nitro-o-toluidine
ug/L
50
47.2
94
39-170 v3
7,12-Dimethylbenz(a)anthracene
ug/L
50
44.1
88
33-139
Acenaphthene
ug/L
50
39.3
79
33-130
Acenaphthylene
ug/L
50
40.4
81
35-130
Acetophenone
ug/L
50
37.9
76
36-130
Anthracene
ug/L
50
43.2
86
48-130
Benzo(a)anthracene
ug/L
50
50.9
102
48-137
Benzo(a)pyrene
ug/L
50
54.0
108
49-138
Benzo(b)fluoranthene
ug/L
50
57.4
115
52-138
Benzo(g,h,i)perylene
ug/L
50
56.8
114
48-140 v1
Benzo(k)fluoranthene
ug/L
50
54.5
109
48-139
Benzyl alcohol
ug/L
100
64.9
65
35-130
bis(2-Chloroethoxy)methane
ug/L
50
39.7
79
34-130
bis(2-Chloroethyl) ether
ug/L
50
40.6
81
36-130
bis(2-Ethylhexyl)phthalate
ug/L
50
55.6
111
32-165
Butylbenzylphthalate
ug/L
50
61.9
124
34-161
Chlorobenzilate
ug/L
50
43.1
86
43-176
Chrysene
ug/L
50
51.0
102
47-131
Di-n-butylphthalate
ug/L
50
52.6
105
39-144
Di-n-octylphthalate
ug/L
50
56.1
112
30-170
Diallate
ug/L
50
44.0
88
33-143
Dibenz(a,h)anthracene
ug/L
50
56.1
112
49-138
Dibenzofuran
ug/L
50
43.4
87
33-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 97 of 118

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE:
Parameter
3113654
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Diethylphthalate
ug/L
50
51.7
103
38-131
Dimethoate
ug/L
50
46.5
93
46-173
Dimethylphthalate
ug/L
50
48.1
96
37-130
Diphenylamine
ug/L
50
48.7
97
35-135
Disulfoton
ug/L
50
38.0
76
34-139
Ethyl methanesulfonate
ug/L
50
34.6
69
33-133
Famphur
ug/L
100
69.1
69
10-1301H
Fluoranthene
ug/L
50
49.6
99
46-137
Fluorene
ug/L
50
43.6
87
37-130
Hexachlorobenzene
ug/L
50
45.1
90
38-130
Hexachlorocyclopentadiene
ug/L
50
8.3J
17
10-130
Hexachloroethane
ug/L
50
4.9J
10
14-130 L2
Hexachloropropene
ug/L
50
ND
9
10-130 L2
Indeno(1,2,3-cd)pyrene
ug/L
50
57.0
114
41-130 v1
Isodrin
ug/L
50
48.4
97
36-139
Isophorone
ug/L
50
41.0
82
33-130
Isosafrole
ug/L
50
34.6
69
22-130
Kepone
ug/L
100
56.1
56
10-130IL
Methapyrilene
ug/L
50
83.7
167
10-1731H,v1
Methyl methanesulfonate
ug/L
50
29.6
59
33-130
Methyl parathion
ug/L
50
53.2
106
39-200
N-Nitroso-di-n-butylamine
ug/L
50
27.2
54
22-130 v3
N-Nitroso-di-n-propylamine
ug/L
50
41.1
82
36-130
N-Nitrosodiethylamine
ug/L
50
35.1
70
23-136
N-Nitrosodimethylamine
ug/L
50
30.6
61
34-130
N-Nitrosodiphenylamine
ug/L
50
48.7
97
37-130
N-Nitrosomethylethylamine
ug/L
50
34.4
69
18-137
N-Nitrosopiperidine
ug/L
50
39.4
79
25-142
N-Nitrosopyrrolidine
ug/L
50
34.4
69
24-146 v3
Nitrobenzene
ug/L
50
40.8
82
36-130
O,O,O-Triethylphosphorothioate
ug/L
50
34.0
68
29-130
O-Toluidine
ug/L
50
36.9
74
27-132
P-Dimethylaminoazobenzene
ug/L
50
20.1
40
17-130IL
p-Phenylenediamine
ug/L
ND
Parathion (Ethyl parathion)
ug/L
50
49.5
99
32-200
Pentachlorobenzene
ug/L
50
38.6
77
27-130
Pentachloronitrobenzene
ug/L
50
56.9
114
47-164
Pentachlorophenol
ug/L
100
82.4
82
23-149
Phenacetin
ug/L
50
44.0
88
44-181
Phenanthrene
ug/L
50
47.7
95
44-130
Phenol
ug/L
50
22.4
45
18-130
Phorate
ug/L
50
60.9
122
18-183 v1
Pronamide
ug/L
50
49.3
99
45-163
Pyrene
ug/L
50
50.0
100
47-134
Safrole
ug/L
50
28.9
58
27-130
Thionazin
ug/L
50
43.5
87
36-162
2,4,6-Tribromophenol (S)
%
40
10-144
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 98 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE:
3113654
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
2-Fluorobiphenyl (S)
%
60
10-130
2-Fluorophenol(S)
%
26
10-130
Nitrobenzene-d5 (S)
%
80
10-144
Phenol-d6 (S)
%
19
10-130
Terphenyl-d14 (S)
%
111
34-163
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3113655
3113656
MS
MSD
92513376002
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
1,2,4,5-Tetrachlorobenzene
ug/L
ND
50
50
28.5
25.2
57
50
10-130
12
30
1,3,5-Trinitrobenzene
ug/L
ND
50
50
56.9
65.8
114
132
50-200
14
30
1,3-Dinitrobenzene
ug/L
ND
50
50
45.8
52.2
92
104
43-161
13
30
1,4-Naphthoquinone
ug/L
ND
50
50
29.0
35.9
58
72
10-184
21
30
1-Naphthalenamine
ug/L
ND
50
50
42.3
54.5
85
109
10-130
25
30
2,2'-Oxybis(1-
ug/L
ND
50
50
35.3
40.5
71
81
12-142
14
30 v1
chloropropane)
2,3,4,6-Tetrachlorophenol
ug/L
ND
50
50
7.1J
31.2
14
62
10-198
30
2,4,5-Trichlorophenol
ug/L
ND
50
50
21.5
44.5
43
89
10-143
70
30 R1
2,4,6-Trichlorophenol
ug/L
ND
50
50
11.6
36.5
23
73
10-147
104
30 R1
2,4-Dichlorophenol
ug/L
ND
50
50
25.4
42.6
51
85
10-138
51
30 R1
2,4-Dimethylphenol
ug/L
ND
50
50
45.7
50.1
91
100
25-130
9
30
2,4-Dinitrophenol
ug/L
ND
250
250
ND
ND
5
10
10-165
30 M1
2,4-Dinitrotoluene
ug/L
ND
50
50
49.1
59.1
98
118
29-148
18
30
2,6-Dichlorophenol
ug/L
ND
50
50
13.7
39.4
27
79
33-139
97
30 M1,R1
2,6-Dinitrotoluene
ug/L
ND
50
50
52.1
58.7
104
117
26-146
12
30
2-Acetylam inofl uorene
ug/L
ND
50
50
44.6
49.9
89
100
27-172
11
30
2-Chloronaphthalene
ug/L
ND
50
50
37.5
35.8
75
72
11-130
5
30
2-Chlorophenol
ug/L
ND
50
50
23.0
39.5
46
79
10-133
53
30 R1
2-Methyl naphthalene
ug/L
ND
50
50
30.8
26.3
62
53
13-130
16
30
2-Methyl phenol(o-Cresol)
ug/L
ND
50
50
36.7
41.2
73
82
20-130
12
30
2-Naphthalenamine
ug/L
ND
50
50
35.9
41.3
72
83
10-135
14
30
2-Nitroaniline
ug/L
ND
100
100
89.7
103
90
103
24-136
14
30
2-Nitrophenol
ug/L
ND
50
50
20.0
43.3
40
87
10-153
73
30 R1
3&4-Methylphenol(m&p
ug/L
ND
50
50
38.2
45.0
76
90
16-130
16
30
Cresol)
3,3'-Dichlorobenzidine
ug/L
ND
100
100
91.1
103
91
103
10-153
13
30
3,3'-Dimethylbenzidine
ug/L
ND
100
100
134
150
134
150
10-200
12
30 IH
3-Methylcholanthrene
ug/L
ND
50
50
46.9
54.6
94
109
53-181
15
30
3-Nitroaniline
ug/L
ND
100
100
95.4
112
95
112
22-151
16
30
4,6-Dinitro-2-methylphenol
ug/L
ND
100
100
9AJ
45.1
9
45
10-180
30 M1
4-Aminobiphenyl
ug/L
ND
50
50
43.6
55.8
87
112
10-139
25
30
4-Bromophenylphenyl ether
ug/L
ND
50
50
46.0
50.5
92
101
25-130
9
30
4-Chloro-3-methylphenol
ug/L
ND
100
100
86.0
101
86
101
25-133
16
30
4-Chloroaniline
ug/L
ND
100
100
78.4
88.3
78
88
14-132
12
30
4-Chlorophenylphenyl ether
ug/L
ND
50
50
40.8
45.7
82
91
19-130
11
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 99 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3113655
3113656
MS
MSD
92513376002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
4-Nitroaniline
ug/L
ND
100
100
98.5
112
99
112
29-150
13
30
4-Nitrophenol
ug/L
ND
250
250
16.3J
75.6
7
30
10-130
30 M1
5-Nitro-o-toluidine
ug/L
ND
50
50
44.9
54.7
90
109
48-163
20
30 v3
7,12-
ug/L
ND
50
50
43.6
51.0
87
102
40-140
16
30
Dimethylbenz(a)anthracene
Acenaphthene
ug/L
ND
50
50
40.7
43.1
81
86
16-130
6
30
Acenaphthylene
ug/L
ND
50
50
41.9
44.3
84
89
15-137
6
30
Acetophenone
ug/L
ND
50
50
35.6
41.0
71
82
28-130
14
30
Anthracene
ug/L
ND
50
50
42.6
48.5
85
97
37-136
13
30
Benzo(a)anth race ne
ug/L
ND
50
50
49.5
55.8
99
112
40-145
12
30
Benzo(a)pyrene
ug/L
ND
50
50
51.3
57.9
103
116
41-146
12
30
Benzo(b)fluoranthene
ug/L
ND
50
50
54.7
62.5
109
125
39-151
13
30
Benzo(g,h,i)perylene
ug/L
ND
50
50
53.2
59.6
106
119
40-147
11
30 v1
Benzo(k)fluoranthene
ug/L
ND
50
50
53.2
59.0
106
118
40-146
10
30
Benzyl alcohol
ug/L
ND
100
100
74.5
83.2
74
83
25-130
11
30
bis(2-
ug/L
ND
50
50
38.3
41.7
77
83
23-130
8
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
ug/L
ND
50
50
35.5
42.0
71
84
25-130
17
30
bis(2- Ethyl hexyl)phthalate
ug/L
ND
50
50
54.8
61.7
110
123
28-166
12
30
Butylbenzylphthalate
ug/L
ND
50
50
61.9
68.4
124
137
33-165
10
30
Chlorobenzilate
ug/L
ND
50
50
43.8
52.2
88
104
55-170
18
30
Chrysene
ug/L
ND
50
50
48.9
55.1
98
110
38-141
12
30
Di-n-butylphthalate
ug/L
ND
50
50
51.7
58.5
103
117
32-153
12
30
Di-n-octylphthalate
ug/L
ND
50
50
56.1
63.4
112
127
30-175
12
30
Diallate
ug/L
ND
50
50
43.8
50.8
88
102
39-141
15
30
Dibenz(a,h)anthracene
ug/L
ND
50
50
51.7
59.0
103
118
39-148
13
30
Dibenzofuran
ug/L
ND
50
50
43.8
47.4
88
95
20-130
8
30
Diethylphthalate
ug/L
ND
50
50
50.5
56.7
98
110
28-142
11
30
Dimethoate
ug/L
ND
50
50
45.7
52.5
91
105
57-167
14
30
Dimethylphthalate
ug/L
ND
50
50
46.4
52.6
93
105
26-136
13
30
Diphenylamine
ug/L
ND
50
50
49.3
54.6
99
109
38-132
10
30
Disulfoton
ug/L
ND
50
50
39.1
45.5
78
91
40-140
15
30
Ethyl methanesulfonate
ug/L
ND
50
50
34.2
42.2
68
84
38-134
21
30
Famphur
ug/L
ND
100
100
35.8
28.7
36
29
10-130
22
30 IH
Fluoranthene
ug/L
ND
50
50
48.0
54.0
96
108
39-143
12
30
Fluorene
ug/L
ND
50
50
43.1
48.3
86
97
24-132
11
30
Hexachlorobenzene
ug/L
ND
50
50
43.6
49.2
87
98
29-130
12
30
Hexachlorocyclopentadiene
ug/L
ND
50
50
17.6
11.0
35
22
10-130
46
30 R1
Hexachloroethane
ug/L
ND
50
50
3.1 J
4.1 J
6
8
10-130
30 MO
Hexachloropropene
ug/L
ND
50
50
8.5J
ND
17
8
10-130
30 MO
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
52.9
59.4
106
119
39-148
12
30 v1
Isodrin
ug/L
ND
50
50
47.1
54.6
94
109
45-138
15
30
Isophorone
ug/L
ND
50
50
41.7
46.8
83
94
23-130
11
30
Isosafrole
ug/L
ND
50
50
34.7
39.5
69
79
25-130
13
30
Kepone
ug/L
ND
100
100
21.1
35.4
21
35
10-130
50
30 IL,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 100 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3113655
3113656
MS
MSD
92513376002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Methapyrilene
ug/L
ND
50
50
85.4
105
171
209
10-181
20
30 IH,M1,
v1
Methyl methanesulfonate
ug/L
ND
50
50
31.2
38.4
62
77
31-130
21
30
Methyl parathion
ug/L
ND
50
50
51.4
60.2
103
120
53-197
16
30
N-Nitroso-di-n-butylamine
ug/L
ND
50
50
27.3
33.0
55
66
28-130
19
30 v3
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
41.0
46.8
82
94
25-130
13
30
N-Nitrosodiethylamine
ug/L
ND
50
50
32.4
43.2
65
86
29-132
29
30
N-Nitrosodimethylamine
ug/L
ND
50
50
33.6
36.3
67
73
22-130
8
30
N-Nitrosodiphenylamine
ug/L
ND
50
50
49.3
54.6
99
109
26-134
10
30
N-Nitrosomethylethylamine
ug/L
ND
50
50
36.1
42.9
72
86
24-133
17
30
N-Nitrosopiperidine
ug/L
ND
50
50
39.1
46.3
78
93
29-141
17
30
N-Nitrosopyrrolidine
ug/L
ND
50
50
37.8
45.7
76
91
29-140
19
30 v3
Nitrobenzene
ug/L
ND
50
50
37.2
40.8
74
82
25-130
9
30
0,0,0-
ug/L
ND
50
50
29.6
38.2
59
76
30-130
25
30
Triethylphosphorothioate
O-Toluidine
ug/L
ND
50
50
33.0
43.5
66
87
27-130
27
30
P-
ug/L
ND
50
50
20.7
24.1
41
48
20-130
15
30 IL
Dimethylaminoazobenzene
p-Phenylenediamine
ug/L
ND
ND
ND
30
Parathion (Ethyl parathion)
ug/L
ND
50
50
50.4
59.3
101
119
48-200
16
30
Pentachlorobenzene
ug/L
ND
50
50
37.9
42.5
76
85
23-130
11
30
Pentachloronitrobenzene
ug/L
ND
50
50
50.1
60.6
100
121
57-159
19
30
Pentachlorophenol
ug/L
ND
100
100
9.11
41.7
9
42
10-175
30 M1
Phenacetin
ug/L
ND
50
50
47.0
57.1
94
114
57-179
19
30
Phenanthrene
ug/L
ND
50
50
47.1
52.3
94
105
36-133
11
30
Phenol
ug/L
ND
50
50
23.1
30.3
46
61
10-130
27
30
Phorate
ug/L
ND
50
50
59.9
69.3
120
139
21-192
15
30 v1
Pronamide
ug/L
ND
50
50
49.8
58.0
100
116
55-162
15
30
Pyrene
ug/L
ND
50
50
50.4
56.9
101
114
40-143
12
30
Safrole
ug/L
ND
50
50
31.0
35.4
62
71
25-130
13
30
Thionazin
ug/L
ND
50
50
43.4
49.5
87
99
50-157
13
30
2,4,6-Tribromophenol (S)
%
14
36
10-144
2-Fluorobiphenyl (S)
%
45
68
10-130
2-Fluorophenol (S)
%
10
29
10-130
Nitrobenzene-d5 (S)
%
68
90
10-144
Phenol-d6 (S)
%
18
28
10-130
Terphenyl-d14 (S)
%
109
124
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 101 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589909 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water APP9 RV MSSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513376008
METHOD BLANK: 3115374
Associated Lab Samples: 92513376008
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
1,2,4,5-Tetrachlorobenzene
ug/L
ND
10.0
4.6
12/30/20 10:47
1,3,5-Trinitrobenzene
ug/L
ND
10.0
5.3
12/30/20 10:47 v1
1,3-Dinitrobenzene
ug/L
ND
10.0
3.7
12/30/20 10:47
1,4-Naphthoquinone
ug/L
ND
5.0
2.4
12/30/20 10:47
1-Naphthalenamine
ug/L
ND
5.0
4.6
12/30/20 10:47
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
1.2
12/30/20 10:47 v1
2,3,4,6-Tetrachlorophenol
ug/L
ND
10.0
1.5
12/30/20 10:47
2,4,5-Trichlorophenol
ug/L
ND
10.0
1.4
12/30/20 10:47
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.6
12/30/20 10:47
2,4-Dichlorophenol
ug/L
ND
10.0
1.4
12/30/20 10:47
2,4-Dimethylphenol
ug/L
ND
10.0
1.7
12/30/20 10:47
2,4-Dinitrophenol
ug/L
ND
50.0
26.0
12/30/20 10:47
2,4-Dinitrotoluene
ug/L
ND
10.0
1.6
12/30/20 10:47
2,6-Dichlorophenol
ug/L
ND
10.0
2.7
12/30/20 10:47
2,6-Dinitrotoluene
ug/L
ND
10.0
1.7
12/30/20 10:47
2-Acetylaminofluorene
ug/L
ND
10.0
1.9
12/30/20 10:47
2-Chloronaphthalene
ug/L
ND
10.0
1.7
12/30/20 10:47
2-Chlorophenol
ug/L
ND
10.0
1.2
12/30/20 10:47
2-Methylnaphthalene
ug/L
ND
10.0
1.9
12/30/20 10:47
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
1.9
12/30/20 10:47
2-Naphthalenamine
ug/L
ND
10.0
6.1
12/30/20 10:47
2-Nitroaniline
ug/L
ND
20.0
3.0
12/30/20 10:47
2-Nitrophenol
ug/L
ND
10.0
1.4
12/30/20 10:47
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
1.2
12/30/20 10:47
3,3'-Dichlorobenzidine
ug/L
ND
20.0
8.1
12/30/20 10:47
3,3'-Dimethylbenzidine
ug/L
ND
25.0
23.5
12/30/20 10:47 IH
3-Methylcholanthrene
ug/L
ND
10.0
5.3
12/30/20 10:47
3-Nitroaniline
ug/L
ND
20.0
3.8
12/30/20 10:47
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
3.4
12/30/20 10:47
4-Aminobiphenyl
ug/L
ND
10.0
4.2
12/30/20 10:47
4-Bromophenylphenyl ether
ug/L
ND
10.0
1.8
12/30/20 10:47
4-ChIoro-3-methyl phenol
ug/L
ND
10.0
3.3
12/30/20 10:47
4-Chloroaniline
ug/L
ND
20.0
3.6
12/30/20 10:47
4-Chlorophenylphenyl ether
ug/L
ND
10.0
2.0
12/30/20 10:47
4-Nitroaniline
ug/L
ND
20.0
5.1
12/30/20 10:47
4-Nitrophenol
ug/L
ND
50.0
6.6
12/30/20 10:47
5-Nitro-o-toluidine
ug/L
ND
10.0
2.4
12/30/20 10:47
7,12-Dimethylbenz(a)anthracene
ug/L
ND
10.0
2.8
12/30/20 10:47
Acenaphthene
ug/L
ND
10.0
2.0
12/30/20 10:47
Acenaphthylene
ug/L
ND
10.0
2.0
12/30/20 10:47
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 102 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
METHOD BLANK: 3115374
Associated Lab Samples: 92513376008
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Acetophenone
ug/L
ND
10.0
1.5
12/30/20 10:47
Anthracene
ug/L
ND
10.0
2.3
12/30/20 10:47
Benzo(a)anthracene
ug/L
ND
10.0
2.7
12/30/20 10:47
Benzo(a)pyrene
ug/L
ND
10.0
2.8
12/30/20 10:47
Benzo(b)fluoranthene
ug/L
ND
10.0
2.6
12/30/20 10:47
Benzo(g,h,i)perylene
ug/L
ND
10.0
2.8
12/30/20 10:47
Benzo(k)fluoranthene
ug/L
ND
10.0
2.7
12/30/20 10:47
Benzyl alcohol
ug/L
ND
20.0
2.9
12/30/20 10:47
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
1.8
12/30/20 10:47
bis(2-Chloroethyl) ether
ug/L
ND
10.0
1.9
12/30/20 10:47
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
3.7
12/30/20 10:47
Butylbenzylphthalate
ug/L
ND
10.0
3.1
12/30/20 10:47
Chlorobenzilate
ug/L
ND
10.0
3.6
12/30/20 10:47
Chrysene
ug/L
ND
10.0
2.8
12/30/20 10:47
Di-n-butylphthalate
ug/L
ND
10.0
2.2
12/30/20 10:47
Di-n-octylphthalate
ug/L
ND
10.0
3.9
12/30/20 10:47
Diallate
ug/L
ND
10.0
2.7
12/30/20 10:47
Dibenz(a,h)anthracene
ug/L
ND
10.0
3.0
12/30/20 10:47
Dibenzofuran
ug/L
ND
10.0
2.1
12/30/20 10:47
Diethylphthalate
ug/L
ND
10.0
2.0
12/30/20 10:47
Dimethoate
ug/L
ND
10.0
2.0
12/30/20 10:47
Dimethylphthalate
ug/L
ND
10.0
2.1
12/30/20 10:47
Diphenylamine
ug/L
ND
10.0
3.0
12/30/20 10:47
Disulfoton
ug/L
ND
10.0
6.0
12/30/20 10:47
Ethyl methanesulfonate
ug/L
ND
20.0
2.8
12/30/20 10:47
Famphur
ug/L
ND
10.0
5.7
12/30/20 10:47
Fluoranthene
ug/L
ND
10.0
2.2
12/30/20 10:47
Fluorene
ug/L
ND
10.0
2.1
12/30/20 10:47
Hexachlorobenzene
ug/L
ND
10.0
2.2
12/30/20 10:47
Hexachlorocyclopentadiene
ug/L
ND
10.0
1.6
12/30/20 10:47
Hexachloroethane
ug/L
ND
10.0
1.4
12/30/20 10:47
Hexachloropropene
ug/L
ND
10.0
5.5
12/30/20 10:47
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
2.9
12/30/20 10:47
Isodrin
ug/L
ND
10.0
3.0
12/30/20 10:47
Isophorone
ug/L
ND
10.0
1.7
12/30/20 10:47
Isosafrole
ug/L
ND
10.0
3.6
12/30/20 10:47
Kepone
ug/L
ND
10.0
8.2
12/30/20 10:47
Methapyrilene
ug/L
ND
50.0
27.2
12/30/20 10:47
Methyl methanesulfonate
ug/L
ND
5.0
3.0
12/30/20 10:47
Methyl parathion
ug/L
ND
10.0
2.0
12/30/20 10:47
N-Nitroso-di-n-butylamine
ug/L
ND
10.0
6.2
12/30/20 10:47
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
1.3
12/30/20 10:47
N-Nitrosodiethylamine
ug/L
ND
10.0
2.0
12/30/20 10:47
N-Nitrosodimethylamine
ug/L
ND
10.0
1.9
12/30/20 10:47
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
12/30/20 10:47
Qualifiers
v1
v1
IH
IL
IH,v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 103 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
METHOD BLANK: 3115374
Matrix:
Water
Associated Lab Samples: 92513376008
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Qualifiers
N-Nitrosomethylethylamine
ug/L
ND
10.0
3.3
12/30/20 10:47
N-Nitrosopiperidine
ug/L
ND
10.0
2.6
12/30/20 10:47
N-Nitrosopyrrolidine
ug/L
ND
10.0
2.1
12/30/20 10:47
Nitrobenzene
ug/L
ND
10.0
1.9
12/30/20 10:47
O,O,O-Triethylphosphorothioate
ug/L
ND
10.0
3.5
12/30/20 10:47
O-Toluidine
ug/L
ND
10.0
2.8
12/30/20 10:47
P-Dimethylaminoazobenzene
ug/L
ND
5.0
3.3
12/30/20 10:47
IL
p-Phenylenediamine
ug/L
ND
10.0
10.0
12/30/20 10:47
Parathion (Ethyl parathion)
ug/L
ND
10.0
2.0
12/30/20 10:47
Pentachlorobenzene
ug/L
ND
10.0
4.4
12/30/20 10:47
Pentachloronitrobenzene
ug/L
ND
10.0
2.4
12/30/20 10:47
Pentachlorophenol
ug/L
ND
20.0
3.8
12/30/20 10:47
Phenacetin
ug/L
ND
10.0
1.9
12/30/20 10:47
Phenanthrene
ug/L
ND
10.0
2.0
12/30/20 10:47
Phenol
ug/L
ND
10.0
1.4
12/30/20 10:47
Phorate
ug/L
ND
10.0
3.8
12/30/20 10:47
v1
Pronamide
ug/L
ND
10.0
2.4
12/30/20 10:47
Pyrene
ug/L
ND
10.0
2.2
12/30/20 10:47
Safrole
ug/L
ND
10.0
3.2
12/30/20 10:47
Thionazin
ug/L
ND
10.0
1.8
12/30/20 10:47
2,4,6-Tribromophenol (S)
%
34
10-144
12/30/20 10:47
2-Fluorobiphenyl (S)
%
60
10-130
12/30/20 10:47
2-Fluorophenol (S)
%
26
10-130
12/30/20 10:47
Nitrobenzene-d5 (S)
%
79
10-144
12/30/20 10:47
Phenol-d6 (S)
%
17
10-130
12/30/20 10:47
Terphenyl-d14 (S)
%
143
34-163
12/30/20 10:47
LABORATORY CONTROL SAMPLE & LCSD:
3115375
3115376
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD
RPD Qualifiers
1,2,4,5-Tetrachlorobenzene
ug/L
50
25.1
34.2
50
68
17-130
31
30 R1
1,3,5-Trinitrobenzene
ug/L
50
57.7
65.3
115
131
44-200
12
30 v1
1,3-Dinitrobenzene
ug/L
50
44.2
50.1
88
100
39-159
13
30
1,4-Naphthoquinone
ug/L
50
29.9
37.7
60
75
10-159
23
30
1-Naphthalenamine
ug/L
50
35.5
43.1
71
86
10-130
19
30
2,2'-Oxybis(1-chloropropane)
ug/L
50
30.1
36.6
60
73
28-130
20
30 v1
2,3,4,6-Tetrachlorophenol
ug/L
50
38.3
43.6
77
87
10-200
13
30
2,4,5-Trichlorophenol
ug/L
50
37.7
41.8
75
84
35-130
10
30
2,4,6-Trichlorophenol
ug/L
50
34.3
41.0
69
82
31-130
18
30
2,4-Dichlorophenol
ug/L
50
29.7
37.0
59
74
35-130
22
30
2,4-Dimethylphenol
ug/L
50
32.5
41.1
65
82
34-130
23
30
2,4-Dinitrophenol
ug/L
250
182
212
73
85
10-153
15
30
2,4-Dinitrotoluene
ug/L
50
44.5
49.7
89
99
37-136
11
30
2,6-Dichlorophenol
ug/L
50
33.2
41.6
66
83
31-139
23
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 104 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE & LCSD:
3115375
3115376
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
2,6-Dinitrotoluene
ug/L
50
44.6
50.5
89
101
33-136
12
30
2-Acetylaminofluorene
ug/L
50
44.9
51.9
90
104
19-181
15
30
2-Chloronaphthalene
ug/L
50
30.1
38.0
60
76
26-130
23
30
2-Chlorophenol
ug/L
50
26.6
34.8
53
70
37-130
27
30
2-Methylnaphthalene
ug/L
50
25.8
33.1
52
66
29-130
25
30
2-Methylphenol(o-Cresol)
ug/L
50
24.9
31.7
50
63
35-130
24
30
2-Naphthalenamine
ug/L
50
40.5
41.0
81
82
10-136
1
30
2-Nitroaniline
ug/L
100
74.9
85.1
75
85
37-130
13
30
2-Nitrophenol
ug/L
50
29.7
39.0
59
78
32-130
27
30
3&4-Methyl phenol (m&p Cresol)
ug/L
50
26.7
34.2
53
68
34-130
24
30
3,3'-Dichlorobenzidine
ug/L
100
85.0
91.9
85
92
34-136
8
30
3,3'-Dimethylbenzidine
ug/L
100
126
173
126
173
10-200
31
30 IH,R1
3-Methylcholanthrene
ug/L
50
46.7
49.6
93
99
39-190
6
30
3-Nitroaniline
ug/L
100
83.1
90.9
83
91
37-138
9
30
4,6-Dinitro-2-methyl phenol
ug/L
100
81.6
94.9
82
95
21-157
15
30
4-Aminobiphenyl
ug/L
50
31.0
41.1
62
82
17-137
28
30
4-Bromophenylphenyl ether
ug/L
50
39.5
45.0
79
90
38-130
13
30
4-Chloro-3-methylphenol
ug/L
100
71.0
80.8
71
81
37-130
13
30
4-Chloroaniline
ug/L
100
59.8
71.8
60
72
38-130
18
30
4-Chlorophenylphenyl ether
ug/L
50
34.9
40.0
70
80
33-130
13
30
4-Nitroaniline
ug/L
100
83.5
88.8
83
89
42-137
6
30
4-Nitrophenol
ug/L
250
128
133
51
53
10-130
4
30
5-Nitro-o-toluidine
ug/L
50
45.3
48.4
91
97
39-170
7
30
7,12-Dimethylbenz(a)anthracene
ug/L
50
42.1
46.5
84
93
33-139
10
30
Acenaphthene
ug/L
50
33.9
40.0
68
80
33-130
17
30
Acenaphthylene
ug/L
50
34.1
41.1
68
82
35-130
19
30
Acetophenone
ug/L
50
27.3
33.6
55
67
36-130
21
30
Anthracene
ug/L
50
36.7
41.2
73
82
48-130
12
30
Benzo(a)anthracene
ug/L
50
42.5
46.4
85
93
48-137
9
30
Benzo(a)pyrene
ug/L
50
43.2
46.9
86
94
49-138
8
30
Benzo(b)fluoranthene
ug/L
50
46.5
49.9
93
100
52-138
7
30
Benzo(g,h,i)perylene
ug/L
50
45.8
46.7
92
93
48-140
2
30
Benzo(k)fluoranthene
ug/L
50
44.1
48.1
88
96
48-139
9
30
Benzyl alcohol
ug/L
100
48.9
63.6
49
64
35-130
26
30
bis(2-Chloroethoxy)methane
ug/L
50
28.4
36.6
57
73
34-130
25
30
bis(2-Chloroethyl) ether
ug/L
50
28.6
35.5
57
71
36-130
22
30
bis(2-Ethylhexyl)phthalate
ug/L
50
49.4
54.0
99
108
32-165
9
30
Butylbenzylphthalate
ug/L
50
52.2
58.0
104
116
34-161
10
30 v1
Chlorobenzilate
ug/L
50
43.1
49.5
86
99
43-176
14
30
Chrysene
ug/L
50
42.1
45.4
84
91
47-131
8
30
Di-n-butylphthalate
ug/L
50
45.0
50.1
90
100
39-144
11
30
Di-n-octylphthalate
ug/L
50
48.6
53.7
97
107
30-170
10
30 v1
Diallate
ug/L
50
41.9
48.7
84
97
33-143
15
30
Dibenz(a,h)anthracene
ug/L
50
44.1
45.8
88
92
49-138
4
30
Dibenzofuran
ug/L
50
36.5
42.3
73
85
33-130
15
30
Diethylphthalate
ug/L
50
43.2
48.3
86
97
38-131
11
30
Dimethoate
ug/L
50
46.6
51.9
93
104
46-173
11
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 105 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE & LCSD:
3115375
3115376
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Dimethylphthalate
ug/L
50
40.9
45.3
82
91
37-130
10
30
Diphenylamine
ug/L
50
41.4
47.9
83
96
35-135
15
30
Disulfoton
ug/L
50
36.5
42.9
73
86
34-139
16
30
Ethyl methanesulfonate
ug/L
50
27.0
35.0
54
70
33-133
26
30
Famphur
ug/L
100
87.3
79.8
87
80
10-130
9
30 IH
Fluoranthene
ug/L
50
40.1
43.7
80
87
46-137
9
30
Fluorene
ug/L
50
37.3
42.4
75
85
37-130
13
30
Hexachlorobenzene
ug/L
50
37.8
43.7
76
87
38-130
14
30
Hexachlorocyclopentadiene
ug/L
50
17.2
26.0
34
52
10-130
41
30 R1
Hexachloroethane
ug/L
50
7.7J
11.3
15
23
14-130
30
Hexachloropropene
ug/L
50
13.4
20.8
27
42
10-130
43
30 R1
Indeno(1,2,3-cd)pyrene
ug/L
50
45.6
47.7
91
95
41-130
4
30
Isodrin
ug/L
50
45.3
51.1
91
102
36-139
12
30
Isophorone
ug/L
50
30.7
38.2
61
76
33-130
22
30
Isosafrole
ug/L
50
31.0
38.8
62
78
22-130
22
30
Kepone
ug/L
100
61.0
64.9
61
65
10-130
6
30 IL
Methapyrilene
ug/L
50
ND
ND
15
43
10-173
30 IH,v1
Methyl methanesulfonate
ug/L
50
24.6
31.5
49
63
33-130
25
30
Methyl parathion
ug/L
50
50.8
58.7
102
117
39-200
15
30
N-Nitroso-di-n-butylamine
ug/L
50
23.4
28.9
47
58
22-130
21
30
N-Nitroso-di-n-propylamine
ug/L
50
29.9
37.5
60
75
36-130
23
30
N-Nitrosodiethylamine
ug/L
50
27.3
35.3
55
71
23-136
25
30
N-Nitrosodimethylamine
ug/L
50
23.3
29.1
47
58
34-130
22
30
N-Nitrosodiphenylamine
ug/L
50
41.4
47.9
83
96
37-130
15
30
N-Nitrosomethylethylamine
ug/L
50
26.1
35.0
52
70
18-137
29
30
N-Nitrosopiperidine
ug/L
50
32.1
40.5
64
81
25-142
23
30
N-Nitrosopyrrolidine
ug/L
50
29.2
37.8
58
76
24-146
26
30
Nitrobenzene
ug/L
50
29.2
36.2
58
72
36-130
22
30
O,O,O-Triethylphosphorothioate
ug/L
50
28.2
36.4
56
73
29-130
25
30
O-Toluidine
ug/L
50
27.9
36.6
56
73
27-132
27
30
P-Dimethylaminoazobenzene
ug/L
50
20.1
23.0
40
46
17-130
14
30 IL
p-Phenylenediamine
ug/L
ND
ND
30
Parathion (Ethyl parathion)
ug/L
50
49.4
55.6
99
111
32-200
12
30
Pentachlorobenzene
ug/L
50
35.6
42.8
71
86
27-130
18
30
Pentachloronitrobenzene
ug/L
50
53.3
60.2
107
120
47-164
12
30
Pentachlorophenol
ug/L
100
70.9
83.6
71
84
23-149
16
30
Phenacetin
ug/L
50
43.5
50.2
87
100
44-181
14
30
Phenanthrene
ug/L
50
39.8
44.9
80
90
44-130
12
30
Phenol
ug/L
50
16.6
21.9
33
44
18-130
28
30
Phorate
ug/L
50
58.4
67.6
117
135
18-183
15
30 v1
Pronamide
ug/L
50
46.8
53.2
94
106
45-163
13
30
Pyrene
ug/L
50
42.9
48.6
86
97
47-134
13
30
Safrole
ug/L
50
27.9
35.5
56
71
27-130
24
30
Thionazin
ug/L
50
42.0
46.3
84
93
36-162
10
30
2,4,6-Tribromophenol (S)
%
38
44
10-144
2-Fluorobiphenyl (S)
%
55
73
10-130
2-Fluorophenol(S)
%
19
25
10-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 106 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
LABORATORY CONTROL SAMPLE & LCSD:
3115375
3115376
Spike
LCS LCSD LCS LCSD
% Rec Max
Parameter
Units Conc.
Result Result % Rec % Rec
Limits RPD RPD Qualifiers
Nitrobenzene-d5 (S)
%
58 71
10-144
Phenol-d6 (S)
%
15 19
10-130
Terphenyl-d14 (S)
%
99 112
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 107 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589498 Analysis Method: SM 4500-S2D-2011
QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007
METHOD BLANK: 3113740 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Sulfide ug/L ND 100 50.0 12/28/2013:29
LABORATORY CONTROL SAMPLE: 3113741
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide ug/L 500 529 106 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3113742 3113743
MS MSD
92513214001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfide ug/L ND 500 500 564 565 109 109 80-120 0 10 H1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3113744 3113745
MS MSD
92513214002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfide ug/L ND 500 500 538 537 105 105 80-120 0 10 H1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 108 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589500 Analysis Method: SM 4500-S2D-2011
QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376008, 92513376009, 92513376010
METHOD BLANK: 3113746 Matrix: Water
Associated Lab Samples: 92513376008, 92513376009, 92513376010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Sulfide ug/L ND 100 50.0 12/28/2013:51
LABORATORY CONTROL SAMPLE: 3113747
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide ug/L 500 474 95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3113748 3113749
MS MSD
92513376008 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfide ug/L ND 500 500 480 480 94 94 80-120 0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 109 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589660 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008
METHOD BLANK: 3114361 Matrix: Water
Associated Lab Samples: 92513376001, 92513376002, 92513376003, 92513376004, 92513376005, 92513376006, 92513376007,
92513376008
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide ug/L ND 8.0 6.0 12/29/20 21:45
LABORATORY CONTROL SAMPLE: 3114362
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide ug/L 100 94.7 95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3114363 3114364
MS MSD
92512927003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide ug/L ND 100 100 74.8 56.7 73 55 80-120 28 10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3114386 3114387
MS MSD
92513198002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide ug/L ND 100 100 77.2 21.1 76 19 80-120 114 10 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 110 of 118

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
QC Batch: 589661 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92513376009, 92513376010
METHOD BLANK: 3114367 Matrix: Water
Associated Lab Samples: 92513376009, 92513376010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide ug/L ND 8.0 6.0 12/29/20 22:55
LABORATORY CONTROL SAMPLE: 3114368
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide ug/L 100 104 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3114369 3114370
MS MSD
92513376009 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide ug/L ND 100 100 ND 89.7 6 90 80-120 10 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC.
Page 111 of 118

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALIFIERS
Project: SURRY CLOSED LF ELKIN
Pace Project No.: 92513376
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P9 RPD between the primary and confirmatory analysis exceeded 40%.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
ST Surrogate recovery was above laboratory control limits. Results may be biased high.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 112 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SURRY CLOSED LF ELKIN
92513376
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92513376001
MW-1
8151A
1597441
EPA8151
1597441
92513376002
MW-2
8151A
1597441
EPA8151
1597441
92513376003
MW-3
8151A
1597441
EPA8151
1597441
92513376004
MW-3A
8151A
1597441
EPA8151
1597441
92513376005
MW-4
8151A
1597441
EPA8151
1597441
92513376006
MW-5
8151A
1597441
EPA8151
1597441
92513376007
MW-6
8151A
1597441
EPA8151
1597441
92513376008
MW-7S
8151A
1598360
EPA8151
1598360
92513376009
MW-7D
8151A
1598360
EPA8151
1598360
92513376010
MW-8
8151A
1598360
EPA8151
1598360
92513376001
MW-1
EPA 3510C
589664
EPA 8081 B
589980
92513376002
MW-2
EPA 3510C
589664
EPA 8081 B
589980
92513376003
MW-3
EPA 3510C
589664
EPA 8081 B
589980
92513376004
MW-3A
EPA 3510C
589664
EPA 8081 B
589980
92513376005
MW-4
EPA 3510C
589664
EPA 8081 B
589980
92513376006
MW-5
EPA 3510C
589473
EPA 8081 B
589477
92513376007
MW-6
EPA 3510C
589664
EPA 8081 B
589980
92513376008
MW-7S
EPA 3510C
589664
EPA 8081 B
589980
92513376009
MW-7D
EPA 3510C
589664
EPA 8081 B
589980
92513376010
MW-8
EPA 3510C
589664
EPA 8081 B
589980
92513376001
MW-1
EPA 3510C
589665
EPA 8082A
589983
92513376002
MW-2
EPA 3510C
589665
EPA 8082A
589983
92513376003
MW-3
EPA 3510C
589665
EPA 8082A
589983
92513376004
MW-3A
EPA 3510C
589665
EPA 8082A
589983
92513376005
MW-4
EPA 3510C
589665
EPA 8082A
589983
92513376006
MW-5
EPA 3510C
589665
EPA 8082A
589983
92513376007
MW-6
EPA 3510C
589665
EPA 8082A
589983
92513376008
MW-7S
EPA 3510C
589665
EPA 8082A
589983
92513376009
MW-7D
EPA 3510C
589665
EPA 8082A
589983
92513376010
MW-8
EPA 3510C
589665
EPA 8082A
589983
92513376001
MW-1
EPA 3010A
590554
EPA 6010D
590598
92513376002
MW-2
EPA 3010A
590554
EPA 6010D
590598
92513376003
MW-3
EPA 3010A
590554
EPA 6010D
590598
92513376004
MW-3A
EPA 3010A
590554
EPA 6010D
590598
92513376005
MW-4
EPA 3010A
590554
EPA 6010D
590598
92513376006
MW-5
EPA 3010A
590554
EPA 6010D
590598
92513376007
MW-6
EPA 3010A
590033
EPA 6010D
590109
92513376008
MW-7S
EPA 3010A
590033
EPA 6010D
590109
92513376009
MW-7D
EPA 3010A
590033
EPA 6010D
590109
92513376010
MW-8
EPA 3010A
590554
EPA 6010D
590598
92513376011
SW-1
EPA 3010A
590554
EPA 6010D
590598
92513376012
SW-2
EPA 3010A
590554
EPA 6010D
590598
92513376001
MW-1
EPA 3010A
589513
EPA 6020B
589556
92513376002
MW-2
EPA 3010A
589513
EPA 6020B
589556
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 01 /06/2021
05:06 PM
without the written consent of Pace Analytical Services, LLC.
Page 113 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SURRY CLOSED LF ELKIN
92513376
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92513376003
MW-3
EPA 3010A
589513
EPA 6020B
589556
92513376004
MW-3A
EPA 3010A
589513
EPA 6020B
589556
92513376005
MW-4
EPA 3010A
589513
EPA 6020B
589556
92513376006
MW-5
EPA 3010A
589513
EPA 6020B
589556
92513376007
MW-6
EPA 3010A
589513
EPA 6020B
589556
92513376008
MW-7S
EPA 3010A
589514
EPA 6020B
589557
92513376009
MW-7D
EPA 3010A
589514
EPA 6020B
589557
92513376010
MW-8
EPA 3010A
589514
EPA 6020B
589557
92513376011
SW-1
EPA 3010A
589514
EPA 6020B
589557
92513376012
SW-2
EPA 3010A
589514
EPA 6020B
589557
92513376001
MW-1
EPA 7470A
589768
EPA 7470A
589837
92513376002
MW-2
EPA 7470A
589768
EPA 7470A
589837
92513376003
MW-3
EPA 7470A
589768
EPA 7470A
589837
92513376004
MW-3A
EPA 7470A
589768
EPA 7470A
589837
92513376005
MW-4
EPA 7470A
589768
EPA 7470A
589837
92513376006
MW-5
EPA 7470A
589768
EPA 7470A
589837
92513376007
MW-6
EPA 7470A
589768
EPA 7470A
589837
92513376008
MW-7S
EPA 7470A
589768
EPA 7470A
589837
92513376009
MW-7D
EPA 7470A
589768
EPA 7470A
589837
92513376010
MW-8
EPA 7470A
589768
EPA 7470A
589837
92513376011
SW-1
EPA 7470A
589768
EPA 7470A
589837
92513376012
SW-2
EPA 7470A
589768
EPA 7470A
589837
92513376001
MW-1
EPA 3510C
589474
EPA 8270E
589694
92513376002
MW-2
EPA 3510C
589474
EPA 8270E
589694
92513376003
MW-3
EPA 3510C
589474
EPA 8270E
589694
92513376004
MW-3A
EPA 3510C
589474
EPA 8270E
589694
92513376005
MW-4
EPA 3510C
589474
EPA 8270E
589694
92513376006
MW-5
EPA 3510C
589474
EPA 8270E
589694
92513376007
MW-6
EPA 3510C
589474
EPA 8270E
589694
92513376008
MW-7S
EPA 3510C
589909
EPA 8270E
590000
92513376009
MW-7D
EPA 3510C
589474
EPA 8270E
589694
92513376010
MW-8
EPA 3510C
589474
EPA 8270E
589694
92513376001
MW-1
EPA 8260D
589025
92513376002
MW-2
EPA 8260D
589025
92513376003
MW-3
EPA 8260D
589025
92513376004
MW-3A
EPA 8260D
589025
92513376005
MW-4
EPA 8260D
589025
92513376006
MW-5
EPA 8260D
589025
92513376007
MW-6
EPA 8260D
589025
92513376008
MW-7S
EPA 8260D
589025
92513376009
MW-7D
EPA 8260D
589025
92513376010
MW-8
EPA 8260D
589025
92513376011
SW-1
EPA 8260D
589025
92513376012
SW-2
EPA 8260D
589025
92513376001
MW-1
SM 4500-S2D-2011
589498
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2021
05:06 PM
without the written consent of Pace Analytical Services, LLC.
Page 114 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SURRY CLOSED LF ELKIN
92513376
Analytical
Lab ID
Sample ID
QC
Batch Method
QC Batch
Analytical Method
Batch
92513376002
MW-2
SM
4500-S2D-2011
589498
92513376003
MW-3
SM
4500-S2D-2011
589498
92513376004
MW-3A
SM
4500-S2D-2011
589498
92513376005
MW-4
SM
4500-S2D-2011
589498
92513376006
MW-5
SM
4500-S2D-2011
589498
92513376007
MW-6
SM
4500-S2D-2011
589498
92513376008
MW-7S
SM
4500-S2D-2011
589500
92513376009
MW-7D
SM
4500-S2D-2011
589500
92513376010
MW-8
SM
4500-S2D-2011
589500
92513376001
MW-1
SM
4500-CN-E-2011
589660
SM
4500-CN-E-2011
589679
92513376002
MW-2
SM
4500-CN-E-2011
589660
SM
4500-CN-E-2011
589679
92513376003
MW-3
SM
4500-CN-E-2011
589660
SM
4500-CN-E-2011
589679
92513376004
MW-3A
SM
4500-CN-E-2011
589660
SM
4500-CN-E-2011
589679
92513376005
MW-4
SM
4500-CN-E-2011
589660
SM
4500-CN-E-2011
589679
92513376006
MW-5
SM
4500-CN-E-2011
589660
SM
4500-CN-E-2011
589679
92513376007
MW-6
SM
4500-CN-E-2011
589660
SM
4500-CN-E-2011
589679
92513376008
MW-7S
SM
4500-CN-E-2011
589660
SM
4500-CN-E-2011
589679
92513376009
MW-7D
SM
4500-CN-E-2011
589661
SM
4500-CN-E-2011
589680
92513376010
MW-8
SM
4500-CN-E-2011
589661
SM
4500-CN-E-2011
589680
Date: 01/06/2021 05:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 115 of 118

Document Name:
Document Revised: October 28, 2020
Analytical }
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [�. Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Condition —1 CII t Name: ' WO# : 92513376
—UponReceipt !Project 4:
�1 ba
9L46 f !1iI 11iI I Il+
Courier: ❑Fed Exv ❑UPS ❑LISPS [Client ❑ Commercial ❑Pace ❑Other: + II I I I
92513376
� , AI�, L
Custody Seal Present? ❑���'Yes W Seals Intact? ❑Yes �lo
Date/Initials Person Examining Contents; _
1
Packing Material: C3ubbleWrap C36ubbleBags ❑None ❑ Other Biological Tissue Frozen? � YC
Thermometer: ❑Yes []No [XA
[�+ta [:]Blue❑None
IR Gun ID: 92TO64 Type of Ice:
1 r rection Factor:
Cooler Temp: ip J d dd/Subtract (°C) . -0.1 Temp should be above freezing to 6°C
7— U 2 3 []Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (*Cl: ( 7 hasbegun
U50A Regulated Soil (t .N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
FlYes rlNn includine Hawaii and Puerto Ricol? FIYes MNn
Comments/Discrepancy:
Chain of Custody Present?
hYes
❑No
[]N/A
1.
Samples Arrived within Hold Time?
yes
❑No
N/A
2.
Short Hold Time Analysis (02 hr.)?
❑Yes
o
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
J! No
❑NIA
4.
Sufficient Volume?
- Yes
No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
C9yes
Yes
❑No
❑No
❑N/A
❑N/A
6•
Containers Intact?
Yes
[:]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
UqJA
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Ef�es
[:]No
❑N/A
9•
Headspace in VOA Vials (>5-6mm)?
❑Yes
[jto
❑NJA
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
[—]Yes
❑Yes
tQKO
No
❑N/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Date/Time:
Lot ID of split containers:
Date:
Field Data Required? ❑Yes ❑No
Project Manager SRF Review:
Date:
Page 116 of 118

Document Name:
sample condition Upon Recei
��;aceAnaWicai Document No.:
f-CAR-Cs-033-Rev.07
*Check mark tap half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Document Revised: October 28, 2020
t(sCUR) Page 2 of 2
Issuing Authority:
Pace Carolinas Quality Office
Project P W4# ; 92513376
PM; AMB Due Date: ol/07/21
CLIENT: 92-Municipal
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Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot 4
adjusted I added
Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sentto the North Carolina DEHNR Certification Office 0,e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 117 of 118

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Page 118 of 118

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 31, 2020
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry Blanks
Pace Project No.: 92512025
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 15, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Steven R. Gandy, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
r
e
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 24

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Surry Blanks
Pace Project No.: 92512025
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 24

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Surry Blanks
Pace Project No.: 92512025
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92512025001
92512025002
EB
FIB
Water
Water
12/11/2016:00
12/11/2016:05
12/15/2011:40
12/15/2011:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 24

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Surry Blanks
Pace Project No.: 92512025
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92512025001 EB
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 8260D
CL
65
PASI-C
92512025002 FIB
EPA 8260D
CL
65
PASI-C
SM 4500-CN-E-2011
CJL
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 24

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92512025
Sample: EB Lab ID: 92512025001 Collected: 12/11/20 16:00 Received: 12/15/20 11:40 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
12/16/20 12:00
12/30/20 21:34
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/16/20 12:00
12/30/20 21:34
7440-38-2
Barium
ND
ug/L
5.0
3.5
1
12/16/20 12:00
12/30/20 21:34
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
12/16/20 12:00
12/30/20 21:34
7440-41-7
Cadmium
0.42J
ug/L
1.0
0.40
1
12/16/20 12:00
12/30/20 21:34
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
12/16/20 12:00
12/30/20 21:34
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
12/16/20 12:00
12/30/20 21:34
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
12/16/20 12:00
12/30/20 21:34
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
12/16/20 12:00
12/30/20 21:34
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
12/16/20 12:00
12/30/20 21:34
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/16/20 12:00
12/30/20 21:34
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/16/20 12:00
12/30/20 21:34
7440-22-4
Tin
ND
ug/L
5.0
4.7
1
12/16/20 12:00
12/30/20 21:34
7440-31-5
Vanadium
ND
ug/L
5.0
3.9
1
12/16/20 12:00
12/30/20 21:34
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
12/16/20 12:00
12/30/20 21:34
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation
Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
12/18/20 02:42
12/30/20 04:16
7440-28-0
7470 Mercury
Mercury
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Date: 12/31 /2020 08:59 AM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
ND ug/L 0.20 0.12 1 12/16/2012:20 12/18/2019:04 7439-97-6
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
ND
ug/L
50.0
ND
ug/L
10.0
ND
ug/L
10.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
6.2
1
12/22/20 16:06
67-64-1
30.4
1
12/22/20 16:06
75-05-8
2.7
1
12/22/20 16:06
107-02-8
0.90
1
12/22/20 16:06
107-13-1
0.28
1
12/22/20 16:06
107-05-1
0.15
1
12/22/20 16:06
71-43-2
0.34
1
12/22/20 16:06
74-97-5
0.26
1
12/22/20 16:06
75-27-4
0.62
1
12/22/20 16:06
75-25-2
0.62
1
12/22/20 16:06
74-83-9
3.3
1
12/22/20 16:06
78-93-3
0.40
1
12/22/20 16:06
75-15-0
0.22
1
12/22/20 16:06
56-23-5
0.23
1
12/22/20 16:06
108-90-7
0.49
1
12/22/20 16:06
75-00-3
2.3
1
12/22/20 16:06
67-66-3
0.39
1
12/22/20 16:06
74-87-3
1.7
1
12/22/20 16:06
126-99-8
0.41
1
12/22/20 16:06
124-48-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IK
Page 5 of 24

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92512025
Sample: EB Lab ID: 92512025001 Collected: 12/11/20 16:00 Received: 12/15/20 11:40 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propionitrile
Styrene
1,1,1,2-Tetrach loroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
Date: 12/31 /2020 08:59 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.46
1
12/22/2016:06
74-95-3
ND
ug/L
1.0
0.29
1
12/22/2016:06
95-50-1
ND
ug/L
1.0
0.22
1
12/22/2016:06
541-73-1
ND
ug/L
1.0
0.26
1
12/22/2016:06
106-46-7
ND
ug/L
1.0
0.54
1
12/22/2016:06
110-57-6 v1
ND
ug/L
1.0
0.23
1
12/22/2016:06
75-71-8
ND
ug/L
1.0
0.27
1
12/22/2016:06
75-34-3
ND
ug/L
1.0
0.34
1
12/22/2016:06
107-06-2
ND
ug/L
1.0
0.24
1
12/22/2016:06
75-35-4
ND
ug/L
1.0
0.29
1
12/22/2016:06
156-59-2
ND
ug/L
1.0
0.25
1
12/22/2016:06
156-60-5
ND
ug/L
1.0
0.19
1
12/22/2016:06
78-87-5
ND
ug/L
1.0
0.16
1
12/22/2016:06
142-28-9
ND
ug/L
1.0
0.27
1
12/22/2016:06
594-20-7
ND
ug/L
1.0
0.21
1
12/22/2016:06
563-58-6
ND
ug/L
1.0
0.30
1
12/22/20 16:06
10061-01-5
ND
ug/L
1.0
0.31
1
12/22/2016:06
10061-02-6
ND
ug/L
1.0
0.26
1
12/22/2016:06
100-41-4
ND
ug/L
1.0
0.51
1
12/22/2016:06
97-63-2
ND
ug/L
1.0
0.44
1
12/22/2016:06
87-68-3
ND
ug/L
5.0
0.57
1
12/22/2016:06
591-78-6
ND
ug/L
20.0
12.5
1
12/22/2016:06
74-88-4
ND
ug/L
100
66.4
1
12/22/2016:06
78-83-1
ND
ug/L
10.0
1.9
1
12/22/2016:06
126-98-7
ND
ug/L
5.0
3.7
1
12/22/2016:06
75-09-2
ND
ug/L
2.0
0.46
1
12/22/2016:06
80-62-6
ND
ug/L
5.0
4.5
1
12/22/2016:06
108-10-1
ND
ug/L
1.0
0.35
1
12/22/2016:06
91-20-3
ND
ug/L
20.0
1.8
1
12/22/2016:06
107-12-0
ND
ug/L
1.0
0.27
1
12/22/2016:06
100-42-5
ND
ug/L
1.0
0.34
1
12/22/2016:06
630-20-6
ND
ug/L
1.0
0.22
1
12/22/2016:06
79-34-5
ND
ug/L
1.0
0.16
1
12/22/2016:06
127-18-4
ND
ug/L
1.0
0.24
1
12/22/2016:06
108-88-3
ND
ug/L
1.0
0.22
1
12/22/2016:06
120-82-1
ND
ug/L
1.0
0.18
1
12/22/2016:06
71-55-6
ND
ug/L
1.0
0.24
1
12/22/2016:06
79-00-5
ND
ug/L
1.0
0.22
1
12/22/2016:06
79-01-6
ND
ug/L
1.0
0.31
1
12/22/2016:06
75-69-4
ND
ug/L
1.0
0.35
1
12/22/2016:06
96-18-4
ND
ug/L
2.0
1.4
1
12/22/2016:06
108-05-4
ND
ug/L
1.0
0.24
1
12/22/2016:06
75-01-4
ND
ug/L
1.0
0.63
1
12/22/2016:06
1330-20-7
100
%
70-130
1
12/22/2016:06
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 24

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92512025
Sample: EB
Lab ID: 92512025001 Collected:
12/11/20 16:00
Received: 12/15/20 11:40 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Surrogates
1,2-Dichloroethane-d4 (S)
104 % 70-130
1
12/22/20 16:06 17060-07-0
Toluene-d8 (S)
99 % 70-130
1
12/22/20 16:06 2037-26-5
Date: 12/31 /2020 08:59 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 24

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92512025
Sample: FIB Lab ID: 92512025002 Collected: 12/11/20 16:05 Received: 12/15/20 11:40 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
lodomethane
Isobutanol
Methacrylonitrile
Methylene Chloride
Methyl methacrylate
4-Methyl-2-pentanone (MIBK)
Date: 12/31 /2020 08:59 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
12/22/2016:24
67-64-1
ND
ug/L
50.0
30.4
1
12/22/2016:24
75-05-8
ND
ug/L
10.0
2.7
1
12/22/2016:24
107-02-8
ND
ug/L
10.0
0.90
1
12/22/2016:24
107-13-1
ND
ug/L
2.0
0.28
1
12/22/2016:24
107-05-1
ND
ug/L
1.0
0.15
1
12/22/2016:24
71-43-2
ND
ug/L
1.0
0.34
1
12/22/2016:24
74-97-5
ND
ug/L
1.0
0.26
1
12/22/2016:24
75-27-4
ND
ug/L
1.0
0.62
1
12/22/2016:24
75-25-2
ND
ug/L
2.0
0.62
1
12/22/2016:24
74-83-9
ND
ug/L
5.0
3.3
1
12/22/2016:24
78-93-3
ND
ug/L
2.0
0.40
1
12/22/2016:24
75-15-0
ND
ug/L
1.0
0.22
1
12/22/2016:24
56-23-5
ND
ug/L
1.0
0.23
1
12/22/2016:24
108-90-7
ND
ug/L
1.0
0.49
1
12/22/2016:24
75-00-3
ND
ug/L
5.0
2.3
1
12/22/2016:24
67-66-3
ND
ug/L
1.0
0.39
1
12/22/2016:24
74-87-3
ND
ug/L
5.0
1.7
1
12/22/2016:24
126-99-8
ND
ug/L
1.0
0.41
1
12/22/2016:24
124-48-1
ND
ug/L
1.0
0.46
1
12/22/2016:24
74-95-3
ND
ug/L
1.0
0.29
1
12/22/2016:24
95-50-1
ND
ug/L
1.0
0.26
1
12/22/2016:24
106-46-7
ND
ug/L
1.0
0.54
1
12/22/2016:24
110-57-6
ND
ug/L
1.0
0.23
1
12/22/2016:24
75-71-8
ND
ug/L
1.0
0.27
1
12/22/2016:24
75-34-3
ND
ug/L
1.0
0.34
1
12/22/2016:24
107-06-2
ND
ug/L
1.0
0.24
1
12/22/2016:24
75-35-4
ND
ug/L
1.0
0.29
1
12/22/2016:24
156-59-2
ND
ug/L
1.0
0.25
1
12/22/2016:24
156-60-5
ND
ug/L
1.0
0.19
1
12/22/2016:24
78-87-5
ND
ug/L
1.0
0.16
1
12/22/2016:24
142-28-9
ND
ug/L
1.0
0.27
1
12/22/2016:24
594-20-7
ND
ug/L
1.0
0.21
1
12/22/2016:24
563-58-6
ND
ug/L
1.0
0.30
1
12/22/20 16:24
10061-01-5
ND
ug/L
1.0
0.31
1
12/22/2016:24
10061-02-6
ND
ug/L
1.0
0.26
1
12/22/2016:24
100-41-4
ND
ug/L
1.0
0.51
1
12/22/2016:24
97-63-2
ND
ug/L
1.0
0.44
1
12/22/2016:24
87-68-3
ND
ug/L
5.0
0.57
1
12/22/2016:24
591-78-6
ND
ug/L
20.0
12.5
1
12/22/2016:24
74-88-4
ND
ug/L
100
66.4
1
12/22/2016:24
78-83-1
ND
ug/L
10.0
1.9
1
12/22/2016:24
126-98-7
ND
ug/L
5.0
3.7
1
12/22/2016:24
75-09-2
ND
ug/L
2.0
0.46
1
12/22/2016:24
80-62-6
ND
ug/L
5.0
4.5
1
12/22/2016:24
108-10-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 8 of 24

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92512025
Sample: FIB Lab ID: 92512025002 Collected: 12/11/20 16:05 Received: 12/15/20 11:40 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
Naphthalene
ND
ug/L
1.0
0.35
1
12/22/20 16:24
91-20-3
Propionitrile
ND
ug/L
20.0
1.8
1
12/22/20 16:24
107-12-0
Styrene
ND
ug/L
1.0
0.27
1
12/22/20 16:24
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/22/20 16:24
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/22/20 16:24
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/22/20 16:24
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/22/20 16:24
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
0.34
1
12/22/20 16:24
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
0.22
1
12/22/20 16:24
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/22/20 16:24
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/22/20 16:24
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/22/20 16:24
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/22/20 16:24
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/22/20 16:24
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/22/20 16:24
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/22/20 16:24
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/22/20 16:24
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/22/20 16:24
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
12/22/20 16:24
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/22/20 16:24
2037-26-5
4500CNE Cyanide, Total
Analytical Method: SM 4500-CN-E-2011
Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services
-Asheville
Cyanide
ND
ug/L
8.0
6.0
1
12/18/20 03:34 12/18/20 23:19
57-12-5
Date: 12/31 /2020 08:59 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
QC Batch: 587405 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92512025001
METHOD BLANK: 3104347
Matrix:
Water
Associated Lab Samples: 92512025001
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Mercury
ug/L
ND
0.20
0.12 12/18/2019:06
LABORATORY CONTROL SAMPLE:
3104348
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Mercury
ug/L
2.5
2.6 104
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3104349 3104350
MS MSD
92512025001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 3.0 2.7 114 106 75-125 7 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
QC Batch: 587397 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92512025001
METHOD BLANK: 3104314
Associated Lab Samples: 92512025001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
12/30/2019:57
Arsenic
ug/L
ND
10.0
4.7
12/30/2019:57
Barium
ug/L
ND
5.0
3.5
12/30/2019:57
Beryllium
ug/L
ND
1.0
0.70
12/30/2019:57
Cadmium
ug/L
ND
1.0
0.40
12/30/2019:57
Chromium
ug/L
ND
5.0
3.7
12/30/2019:57
Cobalt
ug/L
ND
5.0
3.6
12/30/2019:57
Copper
ug/L
ND
5.0
4.3
12/30/2019:57
Lead
ug/L
ND
5.0
4.5
12/30/2019:57
Nickel
ug/L
ND
5.0
3.5
12/30/2019:57
Selenium
ug/L
ND
10.0
4.7
12/30/2019:57
Silver
ug/L
ND
5.0
2.5
12/30/2019:57
Tin
ug/L
ND
5.0
4.7
12/30/2019:57
Vanadium
ug/L
ND
5.0
3.9
12/30/2019:57
Zinc
ug/L
ND
10.0
9.5
12/30/2019:57
LABORATORY CONTROL SAMPLE:
Parameter
3104315
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
491
98
80-120
Arsenic
ug/L
500
484
97
80-120
Barium
ug/L
500
502
100
80-120
Beryllium
ug/L
500
491
98
80-120
Cadmium
ug/L
500
481
96
80-120
Chromium
ug/L
500
474
95
80-120
Cobalt
ug/L
500
488
98
80-120
Copper
ug/L
500
494
99
80-120
Lead
ug/L
500
482
96
80-120
Nickel
ug/L
500
488
98
80-120
Selenium
ug/L
500
480
96
80-120
Silver
ug/L
250
239
95
80-120
Tin
ug/L
500
485
97
80-120
Vanadium
ug/L
500
476
95
80-120
Zinc
ug/L
500
465
93
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC.
Page 11 of 24

lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry Blanks
92512025
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3104316
3104317
MS
MSD
92511110014
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
509
506
102
101
75-125
1
20
Arsenic
ug/L
ND
500
500
507
508
101
102
75-125
0
20
Barium
ug/L
5.2
500
500
495
497
98
98
75-125
0
20
Beryllium
ug/L
ND
500
500
484
484
97
97
75-125
0
20
Cadmium
ug/L
4.0
500
500
503
501
100
99
75-125
0
20
Chromium
ug/L
ND
500
500
484
481
97
96
75-125
1
20
Cobalt
ug/L
ND
500
500
486
485
97
97
75-125
0
20
Copper
ug/L
ND
500
500
502
501
100
100
75-125
0
20
Lead
ug/L
ND
500
500
485
485
97
97
75-125
0
20
Nickel
ug/L
ND
500
500
490
488
98
97
75-125
1
20
Selenium
ug/L
ND
500
500
517
517
103
103
75-125
0
20
Silver
ug/L
ND
250
250
249
249
100
99
75-125
0
20
Tin
ug/L
ND
500
500
497
498
99
100
75-125
0
20
Vanadium
ug/L
ND
500
500
483
485
97
97
75-125
0
20
Zinc
ug/L
ND
500
500
476
476
95
95
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
QC Batch: 587824 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92512025001
METHOD BLANK: 3106303
Matrix:
Water
Associated Lab Samples: 92512025001
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Thallium
ug/L
ND
0.10
0.050 12/30/20 02:15
LABORATORY CONTROL SAMPLE:
3106304
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
10.1
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3106305 3106306
MS MSD
92511977001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 10.2 10.4 102 104 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
QC Batch: 588798 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92512025001, 92512025002
METHOD BLANK: 3110593
Matrix:
Water
Associated Lab Samples: 92512025001, 92512025002
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
12/22/20 14:54
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
12/22/20 14:54
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
12/22/20 14:54
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
12/22/20 14:54
1,1-Dichloroethane
ug/L
ND
1.0
0.27
12/22/20 14:54
1,1-Dichloroethene
ug/L
ND
1.0
0.24
12/22/20 14:54
1,1-Dichloropropene
ug/L
ND
1.0
0.21
12/22/20 14:54
1,2,3-Trichlorobenzene
ug/L
ND
1.0
0.34
12/22/20 14:54
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
12/22/20 14:54
1,2,4-Trichlorobenzene
ug/L
ND
1.0
0.22
12/22/20 14:54
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
12/22/20 14:54
1,2-Dichloroethane
ug/L
ND
1.0
0.34
12/22/20 14:54
1,2-Dichloropropane
ug/L
ND
1.0
0.19
12/22/20 14:54
1,3-Dichlorobenzene
ug/L
ND
1.0
0.22
12/22/20 14:54
1,3-Dichloropropane
ug/L
ND
1.0
0.16
12/22/20 14:54
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
12/22/20 14:54
2,2-Dichloropropane
ug/L
ND
1.0
0.27
12/22/20 14:54
2-Butanone (MEK)
ug/L
ND
5.0
3.3
12/22/20 14:54
2-Hexanone
ug/L
ND
5.0
0.57
12/22/20 14:54
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
12/22/20 14:54
Acetone
ug/L
ND
25.0
6.2
12/22/20 14:54
Acetonitrile
ug/L
ND
50.0
30.4
12/22/20 14:54
Acrolein
ug/L
ND
10.0
2.7
12/22/20 14:54
Acrylonitrile
ug/L
ND
10.0
0.90
12/22/20 14:54
Allyl chloride
ug/L
ND
2.0
0.28
12/22/20 14:54
Benzene
ug/L
ND
1.0
0.15
12/22/20 14:54
Bromochloromethane
ug/L
ND
1.0
0.34
12/22/20 14:54
Bromodichloromethane
ug/L
ND
1.0
0.26
12/22/20 14:54
Bromoform
ug/L
ND
1.0
0.62
12/22/20 14:54
Bromomethane
ug/L
ND
2.0
0.62
12/22/20 14:54 IK
Carbon disulfide
ug/L
ND
2.0
0.40
12/22/20 14:54
Carbon tetrachloride
ug/L
ND
1.0
0.22
12/22/20 14:54
Chlorobenzene
ug/L
ND
1.0
0.23
12/22/20 14:54
Chloroethane
ug/L
ND
1.0
0.49
12/22/20 14:54
Chloroform
ug/L
ND
5.0
2.3
12/22/20 14:54
Chloromethane
ug/L
ND
1.0
0.39
12/22/20 14:54
Chloroprene
ug/L
ND
5.0
1.7
12/22/20 14:54
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
12/22/20 14:54
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
12/22/20 14:54
Dibromochloromethane
ug/L
ND
1.0
0.41
12/22/20 14:54
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
METHOD BLANK: 3110593
Associated Lab Samples: 92512025001, 92512025002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Dibromomethane
ug/L
ND
1.0
0.46
12/22/20 14:54
Dichlorodifluoromethane
ug/L
ND
1.0
0.23
12/22/20 14:54
Ethyl methacrylate
ug/L
ND
1.0
0.51
12/22/20 14:54
Ethylbenzene
ug/L
ND
1.0
0.26
12/22/20 14:54
Hexachloro-1,3-butadiene
ug/L
ND
1.0
0.44
12/22/20 14:54
lodomethane
ug/L
ND
20.0
12.5
12/22/20 14:54
Isobutanol
ug/L
ND
100
66.4
12/22/20 14:54
Methacrylonitrile
ug/L
ND
10.0
1.9
12/22/20 14:54
Methyl methacrylate
ug/L
ND
2.0
0.46
12/22/20 14:54
Methylene Chloride
ug/L
ND
5.0
3.7
12/22/20 14:54
Naphthalene
ug/L
ND
1.0
0.35
12/22/20 14:54
Propionitrile
ug/L
ND
20.0
1.8
12/22/20 14:54
Styrene
ug/L
ND
1.0
0.27
12/22/20 14:54
Tetrachloroethene
ug/L
ND
1.0
0.16
12/22/20 14:54
Toluene
ug/L
ND
1.0
0.24
12/22/20 14:54
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
12/22/20 14:54
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
12/22/20 14:54
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
12/22/20 14:54
Trichloroethene
ug/L
ND
1.0
0.22
12/22/20 14:54
Trichlorofluoromethane
ug/L
ND
1.0
0.31
12/22/20 14:54
Vinyl acetate
ug/L
ND
2.0
1.4
12/22/20 14:54
Vinyl chloride
ug/L
ND
1.0
0.24
12/22/20 14:54
Xylene (Total)
ug/L
ND
1.0
0.63
12/22/20 14:54
1,2-Dichloroethane-d4 (S)
%
102
70-130
12/22/20 14:54
4-Bromofluorobenzene (S)
%
101
70-130
12/22/20 14:54
Toluene-d8 (S)
%
100
70-130
12/22/20 14:54
LABORATORY CONTROL SAMPLE:
Parameter
3110594
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
48.2
96
70-130
1,1,1-Trichloroethane
ug/L
50
47.4
95
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
46.5
93
70-130
1,1,2-Trichloroethane
ug/L
50
47.1
94
70-130
1,1-Dichloroethane
ug/L
50
46.1
92
70-130
1,1-Dichloroethene
ug/L
50
49.5
99
70-132
1,1-Dichloropropene
ug/L
50
45.2
90
70-131
1,2,3-Trichlorobenzene
ug/L
50
50.0
100
70-134
1,2,3-Trichloropropane
ug/L
50
47.0
94
70-130
1,2,4-Trichlorobenzene
ug/L
50
51.4
103
70-130
1,2-Dichlorobenzene
ug/L
50
47.8
96
70-130
1,2-Dichloroethane
ug/L
50
46.2
92
70-130
1,2-Dichloropropane
ug/L
50
48.1
96
70-130
1,3-Dichlorobenzene
ug/L
50
48.4
97
70-130
Qualifiers
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
LABORATORY CONTROL SAMPLE:
Parameter
3110594
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,3-Dichloropropane
ug/L
50
46.1
92
70-130
1,4-Dichlorobenzene
ug/L
50
47.3
95
70-130
2,2-Dichloropropane
ug/L
50
56.7
113
70-130
2-Butanone (MEK)
ug/L
100
94.6
95
70-133
2-Hexanone
ug/L
100
98.2
98
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
95.8
96
70-130
Acetone
ug/L
100
101
101
70-144
Acetonitrile
ug/L
500
489
98
68-134
Acrolein
ug/L
250
290
116
32-200
Acrylonitrile
ug/L
250
252
101
70-130
Allyl chloride
ug/L
50
46.8
94
70-134
Benzene
ug/L
50
46.6
93
70-130
Bromochloromethane
ug/L
50
53.1
106
70-130
Bromodichloromethane
ug/L
50
46.5
93
70-130
Bromoform
ug/L
50
47.1
94
70-131
Bromomethane
ug/L
50
53.7
107
30-177IK
Carbon disulfide
ug/L
50
47.6
95
70-133
Carbon tetrachloride
ug/L
50
47.7
95
70-130
Chlorobenzene
ug/L
50
45.2
90
70-130
Chloroethane
ug/L
50
42.0
84
46-131
Chloroform
ug/L
50
48.1
96
70-130
Chloromethane
ug/L
50
44.1
88
49-130
Chloroprene
ug/L
50
47.1
94
70-130
cis-1,2-Dichloroethene
ug/L
50
45.7
91
70-130
cis-1,3-Dichloropropene
ug/L
50
51.6
103
70-130
Dibromochloromethane
ug/L
50
48.3
97
70-130
Dibromomethane
ug/L
50
47.5
95
70-130
Dichlorodifluoromethane
ug/L
50
41.8
84
52-134
Ethyl methacrylate
ug/L
50
45.5
91
70-130
Ethylbenzene
ug/L
50
43.9
88
70-130
Hexachloro-1,3-butadiene
ug/L
50
51.3
103
70-131
lodomethane
ug/L
100
101
101
47-140
Isobutanol
ug/L
1000
940
94
62-136
Methacrylonitrile
ug/L
500
476
95
70-130
Methyl methacrylate
ug/L
50
48.1
96
70-130
Methylene Chloride
ug/L
50
43.7
87
68-130
Naphthalene
ug/L
50
50.1
100
70-133
Propionitrile
ug/L
500
486
97
70-130
Styrene
ug/L
50
45.2
90
70-130
Tetrachloroethene
ug/L
50
44.7
89
70-130
Toluene
ug/L
50
47.3
95
70-130
trans-1,2-Dichloroethene
ug/L
50
46.4
93
70-130
trans- 1,3-Dichloropropene
ug/L
50
51.7
103
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
67.4
135
25-200 v1
Trichloroethene
ug/L
50
46.5
93
70-130
Trichlorofluoromethane
ug/L
50
44.1
88
61-130
Vinyl acetate
ug/L
100
109
109
70-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
LABORATORY CONTROL SAMPLE:
3110594
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Vinyl chloride
ug/L
50
41.2
82
59-142
Xylene (Total)
ug/L
150
136
91
70-130
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3110595
3110596
MS
MSD
92512962011
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
1, 1, 1,2-Tetrachloroethane
ug/L
ND
20
20
21.0
20.5
105
102
70-135
3
30
1,1,1-Trichloroethane
ug/L
ND
20
20
21.2
22.2
106
111
70-148
5
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.3
19.2
97
96
70-131
0
30
1,1,2-Trichloroethane
ug/L
ND
20
20
19.2
19.9
96
99
70-136
3
30
1,1-Dichloroethane
ug/L
ND
20
20
20.9
21.1
102
103
70-147
1
30
1,1-Dichloroethene
ug/L
ND
20
20
22.3
22.5
112
113
70-158
1
30
1,1-Dichloropropene
ug/L
ND
20
20
20.9
21.1
104
105
70-149
1
30
1,2,3-Trichlorobenzene
ug/L
ND
20
20
21.2
20.9
106
105
68-140
1
30
1,2,3-Trichloropropane
ug/L
ND
20
20
19.4
20.1
97
100
67-137
4
30
1,2,4-Trichlorobenzene
ug/L
ND
20
20
21.8
22.6
109
113
70-139
3
30
1,2-Dichlorobenzene
ug/L
ND
20
20
21.4
21.3
107
107
70-133
0
30
1,2-Dichloroethane
ug/L
ND
20
20
19.6
20.2
98
101
67-138
3
30
1,2-Dichloropropane
ug/L
ND
20
20
20.8
21.1
104
106
70-138
2
30
1,3-Dichlorobenzene
ug/L
ND
20
20
22.0
22.0
110
110
70-133
0
30
1,3-Dichloropropane
ug/L
ND
20
20
20.0
20.0
100
100
70-136
0
30
1,4-Dichlorobenzene
ug/L
ND
20
20
22.4
21.4
112
107
70-133
4
30
2,2-Dichloropropane
ug/L
ND
20
20
25.5
25.9
127
130
52-155
2
30
2-Butanone (MEK)
ug/L
ND
40
40
38.6
39.6
96
99
61-147
2
30
2-Hexanone
ug/L
ND
40
40
40.2
41.8
101
104
67-139
4
30
4-Methyl-2-pentanone
ug/L
ND
40
40
38.2
39.9
96
100
67-136
4
30
(MIBK)
Acetone
ug/L
ND
40
40
41.8
43.9
105
110
55-159
5
30
Acetonitrile
ug/L
ND
200
200
205
214
103
107
66-145
4
30
Acrolein
ug/L
ND
100
100
120
123
120
123
10-200
3
30
Acrylonitrile
ug/L
ND
100
100
104
110
104
110
68-140
6
30
Allyl chloride
ug/L
ND
20
20
20.6
20.6
103
103
70-147
0
30
Benzene
ug/L
ND
20
20
20.9
21.7
102
105
67-150
4
30
Bromochloromethane
ug/L
ND
20
20
21.3
22.6
107
113
70-146
6
30
Bromodichloromethane
ug/L
ND
20
20
19.4
19.6
97
98
70-138
1
30
Bromoform
ug/L
ND
20
20
18.9
19.1
95
95
57-138
1
30
Bromomethane
ug/L
ND
20
20
21.6
23.3
108
117
10-200
8
30 IK,v2
Carbon disulfide
ug/L
ND
20
20
21.6
22.4
108
112
70-152
4
30
Carbon tetrachloride
ug/L
ND
20
20
21.5
22.0
107
110
70-147
3
30
Chlorobenzene
ug/L
ND
20
20
20.9
20.6
103
102
70-137
1
30
Chloroethane
ug/L
ND
20
20
20.0
18.6
100
93
51-166
7
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3110595
3110596
MS
MSD
92512962011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Chloroform
ug/L
ND
20
20
20.9
21.8
105
109
70-144
4
30
Chloromethane
ug/L
ND
20
20
17.1
17.3
85
87
24-161
2
30
Chloroprene
ug/L
ND
20
20
21.3
21.7
106
109
70-143
2
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.9
21.1
102
103
67-148
1
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.5
21.2
107
106
70-142
1
30
Dibromochloromethane
ug/L
ND
20
20
20.9
20.7
105
104
68-138
1
30
Dibromomethane
ug/L
ND
20
20
19.5
20.1
98
101
70-134
3
30
Dichlorodifluoromethane
ug/L
ND
20
20
18.0
18.1
90
90
43-155
0
30
Ethyl methacrylate
ug/L
ND
20
20
20.4
20.0
102
100
70-137
2
30
Ethylbenzene
ug/L
ND
20
20
19.7
19.9
99
99
68-143
1
30
Hexachloro-1,3-butadiene
ug/L
ND
20
20
22.5
23.5
112
117
62-151
4
30
lodomethane
ug/L
ND
40
40
42.1
42.7
105
107
20-161
1
30
Isobutanol
ug/L
ND
400
400
392
425
98
106
44-145
8
30
Methacrylonitrile
ug/L
ND
200
200
199
210
99
105
67-139
5
30
Methyl methacrylate
ug/L
ND
20
20
20.3
21.0
101
105
70-130
4
30
Methylene Chloride
ug/L
ND
20
20
19.7
20.2
99
101
64-148
2
30
Naphthalene
ug/L
ND
20
20
20.6
21.3
103
107
57-150
3
30
Propionitrile
ug/L
ND
200
200
200
206
100
103
70-138
3
30
Styrene
ug/L
ND
20
20
19.4
19.6
97
98
70-136
1
30
Tetrachloroethene
ug/L
ND
20
20
19.9
20.1
99
101
70-139
1
30
Toluene
ug/L
ND
20
20
20.6
20.8
103
104
47-157
1
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.7
21.3
103
107
70-149
3
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
20.3
21.3
102
107
70-138
5
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
20.4
20.9
102
104
31-145
3
30
Trichloroethene
ug/L
ND
20
20
20.9
20.6
105
103
70-149
1
30
Trichlorofluoromethane
ug/L
ND
20
20
20.0
21.1
100
106
61-154
5
30
Vinyl acetate
ug/L
ND
40
40
44.8
45.6
112
114
48-156
2
30
Vinyl chloride
ug/L
ND
20
20
18.3
19.3
91
97
55-172
6
30
Xylene (Total)
ug/L
ND
60
60
61.2
61.8
102
103
66-145
1
30
1,2-Dichloroethane-d4 (S)
%
104
105
70-130
4-Bromofluorobenzene (S)
%
100
99
70-130
Toluene-d8 (S)
%
98
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 24

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92512025
QC Batch: 587642 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92512025002
METHOD BLANK: 3105658
Matrix:
Water
Associated Lab Samples: 92512025002
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Cyanide
ug/L
ND
8.0
6.0 12/18/20 23:07
LABORATORY CONTROL SAMPLE:
3105659
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Cyanide
ug/L
100
100 100
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105698 3105699
MS MSD
92511983001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide ug/L ND 100 100 55.2 66.2 55 66 80-120 18 10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105700 3105701
MS MSD
92512330001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide ug/L ND 100 100 79.2 74.3 76 71 80-120 6 10 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 24

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALIFIERS
Project: Surry Blanks
Pace Project No.: 92512025
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2020 08:59 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 24

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Surry Blanks
92512025
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92512025001
EB
EPA 3010A
587397
EPA 6010D
587444
92512025001
EB
EPA 3010A
587824
EPA 6020B
588032
92512025001
EB
EPA 7470A
587405
EPA 7470A
587454
92512025001
EB
EPA 8260D
588798
92512025002
FB
EPA 8260D
588798
92512025002
FB
SM 4500-CN-E-2011
587642
SM 4500-CN-E-2011
588051
Date: 12/31 /2020 08:59 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 24

Document Name:
Document Revised: October 28, 2020
,111 �,aceAnaVical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.07
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [,�fl Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample. ° Client Name: WQ# : 92512D25
Upon Receipt Project �:
1Y�'r l fk I
Courier:Commercial &ce
dx UPS ether: ❑Client ������ ��� �I��I�f �" ���
❑ 92512026 111
Custody Seal Present? []Yes [ONo Seals Intact? []Yes ®No
Date/Initials Person Examining Contents: 1,41 (0 U=T�o
Packing Material:
Thermometer:
'Pr IR Gun ID:
❑Bubble Wrap ZBubble Bags ❑None ❑ other
92TO64 Type of ice: [7Wet ❑Blue ❑None
Biological Tissue Frozen?
[-]Yes [:]No ®N/A
Correction Factor:
Cooler Temp: r Add/Subtract (°C} -0.1 Temp should be above freezing to 6°C
r I ❑Samples out of temp criteria. Samples on ice, cooling process
Eseler % III, Eetreciedl"El. F�q harecgen
USDA Regulated Soli (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
❑Yes [-]No including Hawaii and Puerto Ricol? ❑Yes [:]NO
Comments/Discrepancy:
Chain of Custody Present?
es
❑No
[-]N/A
1.
Samples Arrived within Hold Time?
gVes
❑No
N/A
2.
Short Hold Time Analysis (02 hr,)7
❑Yes
NNO
❑NIA
3.
Hush Turn Around Time Requested?
❑Yes
%a
❑N/A
4.
Sufficient Volume?
19yes
DNO
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Yes
Yes
❑No
❑No
❑N/A
N/A
6,
Containers Intact?
Yes
[:]No
[-]N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑Na
N/A
8,
Sample Labels Match CDC?
-Includes Date/Time/ID/Analysis Matrix:
[ Ekes
[]NO
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
PNo
❑Na
❑N/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Date/Time:
Lot ID of split containers:
Date:
Field Data Required? ❑Yes [:]No
Project Manager SRF Review:
Date:
Page 22 of 24

Document Name:
Sample Condition Upon Recei
Document Revised: October 28, 2020
CUR) I Page 2 of 2
��aceAaatyticat'
Document No.:
F-CAR-CS-033-Rey.07
*Check mark top half of box if pH and/or dechiorination is Project #
verified and within the acceptance range for preservation
samples,
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 {water) DOC, LLHg
**Bottom half of box is to fist number of bottles
Issuing Authority:
onrn Carolinas Quality Office
V0-# -' �92512025
PM' AMB Due Date: 12/30/20
CLIENT: 92-Municipal
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt pate preservation adjusted Time preservation Amount of Preservative tot d
adjusted I added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DPHNR Certification Office ii.e,
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 23 of 24

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