1101_Buncombe_MSWLF_Oct20GW_FID1578480_20210505

DEN
R USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Bunnell-Lammons Engineering
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Andrew W. Alexander
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
2726 Riverside Drive, Woodfin, NC, 1101-MSWLF October 26-30, 2020
Old Buncombe County Landfill 28804 1979 .1600
Environmental Status: (Check all that apply)
Initial/Background Monitoring Detection Monitoring 0 Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells El
Leachate monitoring data El
water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
El Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Andrew W. Alexander, PG RSM Consulting Hydrogeologist 864-288-1265
Facility Representative Name (Print) Title (Area Code) Telephone Number
�� w a• �E,o•,....=a•d,a ®e,•o.owm, 5/5/2021
Signature Date
6004 Ponders Court, Greenville, SC, 29615
Facility Representative Address
C-284 & C-1538
NC PE Firm License Number (if applicable effective May 1, 2009)
Affix NC Licensed/ Professional Geologist Seal
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1' JGE NSF%
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Revised 6/2009

REPORT OF WATER QUALITY
SAMPLING AND ANALYSIS
2nd SEMI-ANNUAL
EVENT 2020
OLD BUNCOMBE COUNTY LANDFILL
WOODFIN, NORTH CAROLINA
DWM Permit Number 1101-MSWLF-1979
DWR UIC Permit No. WI0100353
Prepared For:
Buncombe County, North Carolina
BLE Project Number J20-14175-04
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BLE North Carolina Business Licenses C-284 & C-1538
IM 13UNNELL
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ENGiNEER1NG
6004 Panders Court I Greenville, 5C 29615
t, 864.288.1265 A. 864,286.43,90 w fnft]@blecorwom
RLECORP.COM

� LAMM[]N5
ENGINEERING
April 27, 2021
Buncombe County Solid Waste Department
81 Panther Branch Road
Alexander, North Carolina 28701
Attention: Ms. Kristy Smith
Subject: Report of Water Quality Sampling and Analysis
2" Semi -Annual Event 2020
Old Buncombe County Landfill
Woodfin, North Carolina
DWM Permit Number 1101-MSWLF-1979
DWR UIC Permit No. W10100353
BLE Project Number J20-14175-04
Dear Ms. Smith:
Pursuant to Buncombe County authorization of Bunnell-Lammons Engineering, Inc. (BLE) Proposal Number
J20-14175-04, dated July 30, 2020, BLE has prepared this report of the groundwater and surface water
sampling and laboratory analysis for the 2' semi-annual sampling event of 2020 at the Old Buncombe County
Landfill. Consistent with the North Carolina Division of Waste Management (DWM) — Solid Waste Section
(SWS) and the North Carolina Division of Water Resources (DWR) approved monitoring program, sampling
and analysis was conducted twice in 2020. This report contains the information required by both the DWM
and DWR to document the sampling and analysis activities for the 2' semi-annual sampling event of 2020 in
the State's permanent project record.
Sincerely,
BUNNELL LAMMONs ENGINEERING INC.
Ril . Blais, .LT.
Staff Hydrogeologist
cc: Ms. Jaclynne Drummond — DWM-ARO
Mr. Andrew Moore, P.G. — DWR-ARO
Mr. Michael Rogers, P.G. — DWR-CO
At/
Andrew W. Alex der, P.G., RSM
Senior Hydrogeologist
Registered, NC #1475
Ilblegvlsvrllsolidwasteprojectslbuncombe county closed lf, ncU,1175-04 fall 2020 semi repor6repor4old bclf I101-mswlf--1979 2020 2nd semi-
annua114175-04.docx
6004 Ponders Court, Greenville, SC 29615 ( H!54.28B.1265 a B64.288.4430 045info@hleMrp com
6LECORP.COM

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Old Buncombe County Landfill -- Woodfin, North Carolina April 27, 2021
Report of Groundwater Sampling and Analysis — 2,d Semi -Annual Event 2020 BLE Project No. J20-14175-04
TABLE OF CONTENTS
1.0 PROJECT INFORMATION........................................................................................................1
2.0 FIELD ACTIVITIES, SAMPLING, AND ANALYSIS.............................................................1
3.0 GROUNDWATER FLOW........................................................................................................... 2
4.0 RESULTS....................................................................................................................................... 2
4.1 Groundwater.................................................................................................................................... 2
4.2 Surface Water.................................................................................................................................. 3
4.3 Geochemical Parameters for Monitored Natural Attenuation......................................................... 4
5.0 CONCLUSIONS AND RECOMMENDATIONS....................................................................... 4
6.0 QUALIFICATIONS OF REPORT.............................................................................................. 4
7.0 CLOSING.......................................................................................................................................4
Tables
Table 1
SWS Approved Groundwater Sampling and Analysis Matrix
Table 2
SWS Approved Surface Water Sampling and Analysis Matrix
Table 3
Well Construction and Monitoring Well Data
Table 4
Groundwater VOCs
Table 5
Groundwater Field Parameters and Total Metals
Table 6
Groundwater Appendix II Pesticides
Table 7
Surface Water VOCs
Table 8
Surface Water Field Parameters and Total Metals
Table 9
Groundwater Transects for Remedial Monitoring
Table 10
Groundwater Geochemical Parameters for MNA
Figures
Figure 1
Site Location Map
Figure 2
Groundwater Elevation Contour Map — October 26-30, 2020
Appendices
Appendix A Field Sampling Logs — Pace Analytical Services, LLC.
Appendix B Laboratory Analytical Data — Pace Analytical Services, LLC.
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Old Buncombe County Landfill -- Woodfin, North Carolina April 27, 2021
Report of Groundwater Sampling and Analysis — 2,d Semi -Annual Event 2020 BLE Project No. J20-14175-04
1.0 PROJECT INFORMATION
Buncombe County provides post -closure care for the Pre -Subtitle D MSWLF (unlined) located at 2726
Riverside Drive, Woodfin, North Carolina (Figure 1). The county operated the facility as a municipal solid
waste (MSW), industrial solid waste (ISW), and construction and demolition (C&D) landfill. The landfill is
separated into four (4) separate waste areas labeled A through D. Waste areas A, B, and C stopped receiving
waste before October 9, 1991 and waste area D stopped receiving waste on September 27, 1997.
Groundwater and surface water monitoring is performed at the site in accordance with a DWM approved
Corrective Action Plan (CAP) dated September 3, 2014 [DIN 21838 (SCS Engineers File No 09204072.06)]
and a DWM approved Request for Reduction of MNA Parameters dated November 30, 2016 [DIN 27144
(SCS Engineers File No 09204072.14)]. The facility requires semi-annual groundwater and surface water
monitoring and reporting in accordance with the CAP, et seq. Prior to the second semi-annual sampling event
of 2020, BLE submitted on behalf of Buncombe County the DWM approved Report of 1, 4-Dioxane Sampling
and Analysis November 2018 to April 2020 dated September 1, 2020 [FID 145059] which updated the
facilities approved groundwater and surface water matrix.
As part of the correction action at the facility, Buncombe County applied for, and was granted a permit for
subsurface injection of materials for enhanced bioremediation of VOCs in groundwater. The Underground
Injection Control (UIC) Permit (No WI0100353) was transmitted by the DWR on September 11, 2015. The
permit issue date was September 15, 2015. The permit was renewed on September 21, 2020 and expires on
August 31, 2025 (effective dates).
The UIC permit requires groundwater monitoring and reporting. We understand that this semi-annual
monitoring report prepared as part of the DWM approved sampling and analysis matrix is sufficient to meet
the monitoring requirements of the UIC permit.
The active groundwater monitoring network for the Closed Buncombe County Landfill consists of one (1)
upgradient (background) well and twenty-three (23) downgradient (compliance, performance, and sentinel)
wells. There are a total of fourteen (14) additional wells that are considering inactive for sampling purposes
and are used for collecting water levels only (Table 1).
Five (5) active surface water monitoring locations have been established for the facility to monitor surface
water quality. The existing surface water locations consist of one (1) upstream (background) location and
four (4) downstream (compliance) locations. Five (5) inactive surface water monitoring locations have
been established but are not sampled (Table 2).
2.0 FIELD ACTIVITIES, SAMPLING, AND ANALYSIS
Groundwater and surface water samples were collected for the 2t'd semi-annual sampling event by personnel
from Pace Analytical Services, LLC. (Pace) of Asheville, North Carolina between October 26-30, 2020.
Groundwater samples were collected from twenty-two (22) of the twenty-four (24) active groundwater
monitoring well locations located on the site (Table 1). Additionally, the five (5) surface water locations were
sampled during the event (Table 2).
The groundwater and surface water samples were delivered to Pace Analytical Services, LLC. (Pace) of
Columbia, South Carolina and analyzed in the laboratory per the approved monitoring plan. The field
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Old Buncombe County Landfill -- Woodfin, North Carolina April 27, 2021
Report of Groundwater Sampling and Analysis — 2,d Semi -Annual Event 2020 BLE Project No. J20-14175-04
parameters of dissolved oxygen, pH, redox potential, specific conductance, turbidity, and temperature were
measured in the field by Pace. A copy of the Pace field sampling logs is included in Appendix A. A copy of
the laboratory analytical data is included in Appendix B.
3.0 GROUNDWATER FLOW
The water level data collected during the groundwater sampling event on October 26-30, 2020 is presented
in Table 3. A groundwater elevation contour map is presented as Figure 2 which includes generalized
groundwater flow directions.
4.0 RESULTS
4.1 Groundwater
The results of the groundwater field and laboratory analyses are summarized on Tables 4, 5 and 6 and the
laboratory analytical data is included in Appendix B.
VOC detections during the current sampling event included:
• Acetone (14 wells);
• Benzene (8 wells);
• Carbon Disulfide (7 wells);
• Chlorobenzene (14 wells);
• Chloroethane (10 wells);
• 1,2-Dichlorobenzene (1,2 DCB) (5 wells);
• 1,4-Dichlorobenzene (1,4 DCB) (16 wells);
• 1, 1 -Dichlorethane (1,1 DCA) (14 wells);
• 1,2-Dichlorethane (1,2 DCA) (3 wells);
• cis-1,2-Dichloroethene (cis-DCE) (12 wells);
• Ethylbenzene (1 well);
• Iodomethane (1 well);
• 2-Butanone (2 wells);
• Toluene (1 well);
• Trichloroethene (2 wells);
• Vinyl chloride (11 wells);
• Total Xylenes (4 wells);
• 1,4-Dioxane (14 wells);
• 4-Chloro-3-methyl phenol (1 well);
• Diethyl phthalate (1 well); and
• Naphthalene (1 well).
Total metal detections during the current sampling event included:
• total barium (22 wells);
• total cadmium (4 wells);
• total chromium (3 wells);
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Old Buncombe County Landfill -- Woodfin, North Carolina April 27, 2021
Report of Groundwater Sampling and Analysis — 2,d Semi -Annual Event 2020 BLE Project No. J20-14175-04
• total cobalt (8 wells);
• total copper (6 wells);
• total lead (4 wells);
• total nickel (16 wells);
• total selenium (4 wells); and
• total zinc (I I wells).
Total pesticide detections during the current sampling event included:
• beta-BHC (2 wells);
• endosulfan II (2 wells); and
• endrin aldehyde (1 well).
Please refer to Tables 4, 5, and 6 for a summary of which groundwater constituents exceed North Carolina
Groundwater Quality Standards (NC2L) maximum contaminant levels' (MCLs).
Field parameters measured in the groundwater included dissolved oxygen, pH, redox potential, specific
conductance, turbidity, and temperature.
4.2 Surface Water
The results of the surface water field and laboratory analyses are summarized on Tables 7 and 8 and the
laboratory analytical data is included in Appendix B.
VOC detections during the current sampling event included:
• Acetone (1 location); and
• 1,4-Dioxane (1 location).
Total metal detections during the current sampling event included:
• total antimony (1 location);
• total barium (all locations);
• total copper (1 location);
• total lead (3 locations);
• total nickel (2 locations); and
• total zinc (2 locations).
Field parameters measured in the surface water included dissolved oxygen, pH, redox potential, specific
conductance, turbidity, and temperature. Please refer to Table 7 and 8 for a summary of which surface water
constituents and field parameters exceeded their established North Carolina Surface Water Quality Standards
(NC2B)2 standard limits.
' North Carolina Department of Environmental Quality, Classifications of Water Quality Standards, Section 15A NCAC 2L.202, July 24,2020.
2 North Carolina Department of Environmental Quality, Surface Waters and Wetlands Standards, Section 15A NCAC 02B workbook dated June
10, 2019.
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Old Buncombe County Landfill -- Woodfin, North Carolina April 27, 2021
Report of Groundwater Sampling and Analysis — 2,d Semi -Annual Event 2020 BLE Project No. J20-14175-04
4.3 Geochemical Parameters for Monitored Natural Attenuation
Buncombe County selected Monitored Natural Attenuation (MNA), Institutional Controls (restrictive cover;
a.k.a. landfill cap), and In Situ Enhanced Bioremediation and Bioaugmentation as the groundwater remedies
for the facility. The selected remedies are in progress. A series of transects along groundwater flow paths were
identified in the CAP, et. Seq, which includes groundwater monitoring wells selected for remedial monitoring.
A summary table which identifies each transect (1 through 5) and associated monitoring wells is included as
Table 9. Sampling for specific geochemical parameters to evaluate remedial performance was performed
during the 2nd semi-annual event of 2020. Those results are summarized on Table 10 and the laboratory
analytical data is included in Appendix B.
A corrective action evaluation report (CAER) will be submitted by BLE on behalf of Buncombe County later
in 2021.
5.0 CONCLUSIONS AND RECOMMENDATIONS
Semi-annual assessment monitoring was performed during the 2nd semi-annual event of 2020 in general
accordance with the approved CAP and monitoring plan. Detected constituents which exceed their respective
groundwater and surface water standards are identified on the summary tables.
We recommend that semi-annual sampling continue in accordance the approved CAP and monitoring plan.
6.0 QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those normally employed
in hydrogeological and environmental assessments of this type. Our evaluation of site conditions has been
based on our understanding of the site and project information and the data provided to BLE.
This report has been prepared on behalf of and exclusively for the use of Buncombe County, North Carolina.
This report and the findings contained herein shall not, in whole or in part, be used or relied upon by any other
parry (excluding the DWM and DWR) without BLE's prior written consent.
7.0 CLOSING
We appreciate the opportunity to be of service to Buncombe County, North Carolina. Please contact us at
[phone] if you have any questions or comments.
4 of 4

Tables

Table 1
SWS Approved Groundwater Sampling and Analysis Matrix
Closed Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Standard Semi -Annual Laboratory Parameters
Standard Semi -Annual Field Parameters
Semi -Annual Geochemical Parameters for MNA
Monitoring Well
Well Status
Transect
Number
Appendix I VOCs
(EPA 8260B)
1,4-dioxane
(EPA 8260 SIM)
Appendix H
Full List
(Various Methods)
Appendix I
Metals
WL
Turb
Temp
pH ORP DO SC
.alkalinity
DH
VIA
TOC BOD
COD
Chloride
CO2
Fee
NO3
MEE
SO4
Sulfide
DPL-1
Active
5
Y Y
O
Y
Y
Y
Y
Y
Y
Y Y
DPL-2
Injection
4
MW-A
Inactive
-
Y
MW-B
Active
2
Y
Y
-
Y
Y
Y
Y
Y
Y
Y
Y
MW-2
Active
-
Y
O
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-3
Active
3
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-4
Active
4
Y
Y
-
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-4A
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-5
Active
5
Y
Y
O
Y
Y
Y
Y
Y
Y
Y
Y
MW-6
Active
5
Y
Y
O
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-6-192
Active
5
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-7
Active
-
Y
*Y*
Y
Y
Y
Y
Y
Y
Y
Y
MW-8
Inactive
Y
MW-9
Abandoned
MW-10
Abandoned
MW-12-10
Inactive
Y
MW-12-25
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-13-10
Inactive
Y
MW-13-35
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-13-132
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-14
Inactive
Y
MW-15
Active
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-16
Abandoned
MW-17
Abandoned
MW-17-60
Active
2
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-17-137
Active
2
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-17-310
Active
-
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-18-3
Inactive
-
Y
MW-18-78
Active
5
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-19-4
Inactive
Y
MW-19-75
Active
4
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-19-110
Active
4
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-20-3
Inactive
-
Y
MW-20-32
Inactive
Y
MW-21-4
Inactive
-
Y
MW-21-21
Active
3
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-21-94
Active
3
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-22-78
Inactive
-
Y
MW-22-143
Inactive
Y
MW-23-119
Inactive
Y
MW-23-186
Inactive
-
Y
MW-24-45
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
MW-24-160
Active
1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Notes:
Typical Events: April (Spring) and October (Fall)
O = October (Fall) Only
VOCs = Volatile Organic Compounds
Y = Yes *remove if 1,4-dioxane not detected in the Fall 2020 event*
SWS Approved Matrix on September 1, 2020
BOD = Biologic Oxygen Demand
COD = Chemical Oxygen Demand
40 CFR Part 258 Appendix I - Constituents for Detection Monitoring (Organics and Inorganics)
40 CFR Part 258 Appendix II - Constituents for Assessment Monitoring (Full List)
WL = Water Level
ORP = Oxidation Reduction Potential
DO = Dissolved Oxygen
SC = Specific Conductance
DH = Dissolved Hydrogen
VFA = Volatile Fatty Acids
TOC = Total Organic Carbon
Fe' = Iron II
NO3 = Nitrate
MEE = Methme/Ethene/Ethane
SO4 = Sulfate
CO2 = Carbon Dioxide
GW Approved Matrix Tl of Approved 2020-09-01 Closed BCLF GW and SW Matrix for Fall 2020.xlsx
Prepared By: AWA
Checked By: TJD

Table 2
SWS Approved Surface Water Sampling and Analysis Matrix
Closed Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Standard Semi -Annual
Laboratory Parameters
Standard Semi -Annual Field Parameters
Surface
Water
Location
Location
Status
Appendix I VOCs
(EPA 8260B)
1,4-dioxane
(EPA 8260 SIM)
Appendix I
Metals
Turb
Temp
pH
ORP
DO
SC
SW-1
Active
Y
-
Y
Y
Y
Y
Y
Y
Y
SW-2
Active
Y
-
Y
Y
Y
Y
Y
Y
Y
SW-2A
Active
Y
Y
Y
Y
Y
Y
Y
Y
Y
SW-3
Active
Y
Y
Y
Y
Y
Y
Y
Y
Y
SW-4
Active
Y
Y
Y
Y
Y
Y
Y
Y
Y
SW-5
Inactive
-
-
-
-
-
-
-
-
-
SW-6
Inactive
-
-
-
-
-
-
-
-
-
SW-7
Inactive
-
-
-
-
-
-
-
-
-
SW-8
Inactive
-
-
-
-
-
-
-
-
-
SW-9
1 Inactive
-
-
-
-
I -
I -
I -
I -
I -
Notes:
Typical Events: April (Spring) and October (Fall)
VOCs = Volatile Organic Compounds
Y=Yes
40 CFR Part 258 Appendix I - Constituents for Detection Monitoring (Organics and Inorganics)
SWS Approved Matrix on September 1, 2020
SW Approved Matrix T2 of Approved 2020-09-01 Closed BCLF GW and SW Matrix for Fall 2020.xlsx
ORP = Oxidation Reduction Potential
DO = Dissolved Oxygen
SC = Specific Conductance
Prepared By: AWA
Checked By: TJD

Table 3
Well Construction and Monitoring Well Data
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Monitoring
Point
Northing'
Easting1
TOC
Elevation
(ft)'
GS Elevation
(ft)'
Depth to GW (ft)
Oct. 26-30, 2020
Groundwater
Elevation (ft)
Well
Depth (ft)'
Screen Depth
(below GS)'
Geology Monitored'
Well
Status/Purpose
DPL-1
714,361.2
928,456.1
2040.73
2038.23
Dry
Dry
65
55 65
Bedrock
Compliance
DPL-2
714,508.1
928,812.6
2112.15
2109.65
A
A
97
87 97
Bedrock
Injection
MW-A
714,654.47
931,068.90
2063.37
2061.90
1.08
2062.29
33
1 23 33
Bedrock
DNA
MW-B
713,635.93
930,421.08
1960.86
1960.30
4.05
1956.81
15
5 15
Bedrock
Compliance
MW-2
715,052.9
930,063.8
2205.33
2203.40
107.50
2097.83
175
145 - 175
Bedrock
Background
MW-3
713,790.10
929,814.44
1991.15
1989.90
66.08
1925.07
90
60 90
Bedrock
Compliance
MW-4
714,177.83
928,875.09
2014.27
2013.60
72.04
1942.23
75
55 75
Bedrock
Performance
MW-4A
713,351.70
931,195.02
2083.10
2082.50
67.53
2015.57
77
67 77
Bedrock
Compliance
MW-5
714,620.07
928,174.58
2019.73
2019.00
49.57
1970.16
80
70 80
Bedrock
Compliance
MW-6
715,103.13
928,152.69
2002.08
2000.30
0.20
2001.88
40
1 30 40
Bedrock
Performance
MW-6-192
715,146.34
928,113.86
2009.02
2006.73
25.71
1983.31
192
182 - 192
Bedrock
Compliance
MW-7
715,604.13
930,534.81
2108.86
2107.70
22.75
2086.11
29
14 29
Saprolite
Compliance
MW-8
716,107.98
930,308.94
2079.02
2077.20
25.23
2053.79
38
23 38
Saprolite
DNA
MW-9
716,024.04
928,619.48
2061.59
2060.00
A
A
29
14 29
Saprolite
DNA
MW-10
716,086.5
929,060.5
2049.67
2047.40
A
A
19
9 19
Saprolite
DNA
MW-12-10
DNA
DNA
2028.03
2024.94
Dry
Dry
8
1 4 8
Saprolite
DNA
MW-12-25
713,258.9
931,353.0
2029.98
2026.36
8.17
2021.81
26
16 26
Bedrock
Compliance
MW-13-10
713,000.2
931,279.7
2012.26
2009.85
3.78
2008.48
10
4 10
Saprolite
DNA
MW-13-35
713,023.1
931,236.9
2017.68
2014.13
6.68
2011.00
35
25 35
Bedrock
Compliance
MW-13-132
712,997.8
931,274.0
2012.89
2009.58
21.60
1991.29
132
122 - 132
Bedrock
Performance
MW-14
716,348.1
930,124.0
2053.46
2049.61
7.67
2045.79
55
40 55
Bedrock
DNA
MW-15
716,995.2
929,509.6
2028.08
2024.08
5.33
2022.75
72
1 62 72
Bedrock
Compliance
MW-16
716,170.0
929,107.2
2048.13
2045.13
A
A
94
84 94
Bedrock
DNA
MW-17
DNA
DNA
DNA
DNA
A
A
DNA
DNA - DNA
DNA
DNA
MW-17-60
713,339.0
930,205.8
1922.97
1920.35
21.98
1900.99
60
50 60
Bedrock
Compliance
MW-17-137
713,329.8
930,199.1
1921.73
1919.24
21.24
1900.49
137
127 - 137
Bedrock
Compliance
MW-17-310
713,302.4
930,207.9
DNA
1918.00
0.00
DNA
310
300 - 310
Bedrock
Compliance
MW-18-3
714,130.9
927,843.0
1895.62
1892.62
Dry
Dry
3
1 3
Flood Plain
DNA
MW-18-78
714,131.1
927,848.7
1894.62
1891.62
6.47
1888.15
78
68 78
Bedrock
Sentinel
MW-19-4
713,953.9
928,939.4
1902.27
1898.97
Dry
Dry
4
2 4
Flood Plain
DNA
MW-19-75
713,948.7
928,950.0
1900.72
1898.02
9.60
1891.12
75
65 75
Bedrock
Compliance
MW-19-110
713,951.7
928,942.4
1901.43
1898.53
10.04
1891.39
110
100 - 110
Bedrock
Sentinel
MW-20-3
713,865.0
929,310.2
1898.90
1895.90
Dry
Dry
3
1 2 3
Flood Plain
DNA
MW-20-32
713,879.0
929,332.7
1899.57
1896.67
6.02
1893.55
32
22 32
Bedrock
DNA
MW-21-4
713,810.5
929,567.5
1900.33
1896.73
6.19
1894.14
4
2 4
Flood Plain
DNA
MW-21-21
713,826.6
929,581.7
1900.49
1897.49
5.70
1894.79
21
11 21
Bedrock
Performance
MW-21-94
713,829.5
929,577.5
1901.06
1897.76
7.78
1893.28
94
84 94
Bedrock
Sentinel
MW-22-78
716,370.39
930,380.26
2068.13
2065.92
24.50
2043.63
79
69 79
Bedrock
DNA
MW-22-143
716,306.96
930,320.49
2068.34
2066.17
44.19
2024.15
148
1 138 - 148
Bedrock
DNA
MW-23-119
716,014.05
930,476.24
2076.61
2074.37
42.08
2034.53
120
110 - 120
Bedrock
DNA
MW-23-186
716,004.53
930,480.42
2076.43
2074.29
52.20
2024.23
186
176 - 186
Bedrock
DNA
MW-24-45
711,372.03
930,963.22
1 1932.07
1929.82
1 Dry
I Dry
45
35 45
Bedrock
I Compliance
MW-24-160
1711,435.811931,042.731
1933.24
1 1930.93
1 94.48
1 1838.76
160
150 - 160
Bedrock
I Sentinel
- Data from Table 1, Well Construction Summary, from Old Buncombe County Landfill Corrective Action Plan, by SCS Engineers, Dated September 3, 2014.
2 - Water levels were collected for these wells but no accurate survey data is available.
TOC - Top of Casing.
GS - Ground Surface.
DNA - Data Not Available
A - Abandoned
14175-04 GW Tables.xlsx Prepared By: RLB
Table 3 Oct 2020 Checked By: TJD

Table 4
Groundwater VOCs
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Sampled by
Pace Anal tical Services, LLC. October 26-30, 2020
TEST
UNITS
MRL
MDL
MCL
NM-B
MW-2
NM-3
MW-4
MW-4A
NM-5
MW-6
MW-6-192
MW-7 NM-12-25
AM-13-35
MW-13-132
MW-15
MW-17-60
MW-17-137
MW-17-310
MW-18-78
MW-19-75
MW-19-110
MW-21-21
MW-21-94 MW-24-45
MW-24-160
DPI-1
Acetone
µgfl
20
5.0
6,000
5.11
<5.0
7.6 J
6.7 J
<5.0
5.3 J
8.4 J
<5.0
16 J
<5.0
<5.0
<5.0
191
6.9 J
7.2 J
<5.0
9.0 J
6.6 J
5.7 J
7.0 J
7.1 J
Dry
<5.0
Dry
Acrylonitrile
µg/l
20
0.80
NE
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
<0.80
Dry
<0.80
Dry
Benzene
µgd
1.0
0.40
1.0
<0.40
<0.40
0.78 J
0.41J
2.8
<0.40
0.87 J
<0.40
EF 1.7
<0.40
1 1.7
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
1.8
<0.40
Dry
<0.40
Dry
Bromochloromethane
119/1
1.0
0.40
NE
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Bromodichloromethane
µgfl
1.0
0.40
0.6
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Bromoform
µgd
1.0
0.40
4.0
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Carbon Disulfide
µgfl
1.0
0.40
700
<0.40
<0.40
<0.40
0.42 J
<0.40
<0.40
0.84 J
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
1.9
0.77 J
1.1
0.60 J
1.6
Dry
<0.40
Dry
Bromomethane (Methylbromide)
99/1
2.0
0.40
10.0 (1)
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Carbon tetrachloride
99/1
1.0
0.40
0.3
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Chlorobenzene (mono)
99/1
1.0
0.40
50
1.2
<0.40
3.6
4.3
13
7.1
8.8
1.3
9.9
<0.40
6.8
<0.40
<0.40
<0.40
<0.40
<0.40
3.3
4.8
0.55 J
13
1.2
Dry
<0.40
Dry
Chloroethane
99/1
2.0
0.40
3,000
0.60 J
<0.40
2.6
1.9 J
<0.40
0.92 J
3.7
0.75 J
3.7
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
0.70 J
<0.40
0.81 J
<0.40
2.5
Dry
<0.40
Dry
Chloroform
µgfl
1.0
0.40
70
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Chloromethane (Methylchloride)
µg/l
1.0
0.50
3.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
Dry
<0.50
Dry
Dibromochloromethane
µg/l
1.0
0.40
0.4
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,2-Dibromo-3-chloropropane; DBCP
µg9
1.0
0.40
0.04
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,2-Dibromoethane; Ethylene dibromide
µg/1
1.0
0.40 0.02
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Dibromomethane
µgd
1.0
0.40 70.0 (1)
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,2-Dichlorobenzene
µgd
1.0
0.40 20.0
<0.40
<0.40
0.77 J
0.56 J
3.5
<0.40
<0.40
<0.40
<0.40
<0.40
4.1
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
2.7
<0.40
Dry
<0.40
Dry
1,4-Dichlorobenzene
µgd
1.0
0.40
6.0
1.9
<0.40
F 6.5
5.5
1 32
4.7
3.7
0.61 J
3.9
<0.40
17
0.78 J
<0.40
<0.40
0.47 J
<0.40
2.5
4.2
0.64 J
12
1.6
Dry
<0.40
Dry
trans-1,4-Dichloro-2-butene
µgfl
2.0
0.50
NE
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
Dry
<0.50
Dry
1,1-Dichloroethane
99/1
1.0
0.40
6.0
1.7
<0.40
1.7
<0.40
0.64 J
2.0
0.66 J
2.7
<0.40
<0.40
0.73 J
<0.40
0.68 J
0.65 J
<0.40
0.94 J
0.58 J
<0.40
2.5
0.82 J
Dry
<0.40
Dry
1,2-Dichloroethane
µgfl
1.0
0.40
0.4
<0.40
<0.40
<0.40
0.41 J
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
0.54 J
0.48 J
Dry
<0.40
Dry
l,l-Dichloroethene (-ethylene)
µg/l
1.0
0.40
350
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
cis-1,2-Dichloroethene (-ethylene)
µgfl
1.0
0.40
70
21
<0.40
0.84 J
16
<0.40
<0.40
0.49 J
<0.40
25
<0.40
2.9
4.4
<0.40
1.0
<0.40
<0.40
0.85 J
<0.40
0.61 J
5.2
2.4
Dry
<0.40
Dry
trans-1,2-Dichloroethene (-ylene)
µgfl
1.0
0.40
100
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,2-Dichloropropane
µgo
1.0
0.40
0.6
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
cis-1,3-Dichloropropene (-propylene)
µgfl
1.0
0.40
0.4
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
naps-1,3-Dichloropropene (-propylene)
µgfl
1.0
0.40
0.4
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Ethylbenzene
µgd
1.0
0.40 600
<0.40
<0.40
<0.40
<0.40
1.5
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
2-Hexanone
µgfl
10.0
2.0 40.0 (i)
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
Dry
Iodomethane
µgfl
5.0
0.40 NE
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
0.45 J
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Dichloromethane (Methylene chloride)
µgll
1.0
0.40
5.0
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
2-Butanone (Methyl ethyl ketone)
µgd
10.0
2.0
4000
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
2.3 J
<2.0
<2.0
<2.0
<2.0
5.3 J
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
Dry
4-Methyl-2-Pentanone
µgfl
10.0
2.0
NE
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
Dry
Styrene
µg/l
1.0
0.41
70.0
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
Dry
<0.41
Dry
1, 1, 1,2-Tetrachloroethane
99/1
1.0
0.40
1.0 (i)
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,1,2,2-Tetrwhloroethane
99/1
1.0
0.40
0.2
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Tenachloroethene (-ethylene)
µgfl
1.0
0.40
0.7
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Toluene
µg/l
1.0
0.40
600
<0.40
<0.40
<0.40
<0.40
1.2
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,1,1-Trlchloroethane
99/1
1.0
0.40
200
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,1,2-Trichloroethane
µg/i
1.0
0.40
.6 (i)
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Trichloroethene (-ethylene)
µg9
1.0
0.40
3.0
<0.40
<0.40
<0.40
0.64 J
<0.40
<0.40
<0.40
<0.40
0.77 J
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Trichlorofluoromethane
µgfl
1.0
0.40
2,000
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,2,3-Trichloropropane
µg/l
1.0
0.40
0.005
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
Vinyl acetate
µg/l
5.0
1.2 88.0 (i)
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
Dry
<1.2
Dry
Vinyl chloride
µg/l
1.0
0.40
0.03
10
<0.40
0.79 J
3
0.51 J
<0.40
0.44 J
<0.40
<0.40
<0.40
0.53 J
1.6
<0.40
<0.40
0.54 J
<0.40
<0.40
<0.40
2.3
1.1
Dry
<0.40
Dry
Total Xylenes
µgfl
1.0
0.40
500
<0.40
<0.40
0.82 J
<0.40
3.2
<0.40
<0.40
<0.40
0.57 J
<0.40
10.40
<0.40
<0.40
<0.40
0.50 J
<0.40
<0.40
<0.40
<0.40
<0.40
<0.40
Dry
<0.40
Dry
1,4-Dioxane
3.0
1.0 3.0
36
NT
97
22
20
31
<1.0
NT
NT
NT
NT
23
34
NT
45
34
52
1 46
Dry
NT
4-Chloro-3-methyl phenol
µgR
4.0
0.50 NE
NT
<0.50
NT
NT
NT
<0.50
1.7 J
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT NT
NT
Dry
Diethyl phthalate
µg/1
4.0
0.50
6000
NT
<0.50
NT
NT
NT
<0.50
2.5 J
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
Naphthalene
µgR
0.80
0.20
1 6.0
NT
<0.20
NT
NT
NT
<0.20
0.78 J
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
Other A . H Volatile Organic Compounds VOC's
Various
VarjouslVariouslVanousl
NT
ND
I NT
NT
I NT
ND
ND
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
Notes:
1. MCL= Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Updated July 24, 2020
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated April 6, 2018
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. MRL = Method Reporting Limit
7. MDL = Minimum Detection Limit
8. NT=Not Tested
9. "J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
14175-04 GW Tables.xlsx
Table 4 VOC Oct 2020
Prepared By: RLB
Checked By: TJD

Table 5
Groundwater Field Parameters and Total Metals
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Sampled by Pace Analytical Services, LLC. October 26-30, 2020.
TEST
UNITS
MRL
MDL
MCL
MW-B
MW-2
MW-3
MW-4 MW-4A MW-5
MW-6 MW-6-192
MW-7
MW-12-25 MW-13-35
MW-13-132
MW-15
MW-17-60
MW-17-137
MW-17-310
MW-18-78 MW-19-75
MW-19-110
MW-21-21
MW-21-94
MW-24-45
MW-24-160
DPL-1
pH
S.U.
>6.5; <8.5
6.3
6.0
6.4
6.2
1 6.2
6.3
6.2 6.3
5.6
6.3
5.5
7.1
12.5
6.9
7.3
8.2
6.3
6.2
7.4
6.3
6.6
Dry
7.4
Dry
Specific Conductance
mmhos/cm
NE
692
128.1
1413
983
548.1
1368
1496 458.6
279.3
548.7
350.2
368.6
7744
584
831
143.5
983
1285
458.0
1373
886
Dry
210.4
Dry
Temperature
°C
NE
20.5
20.1
17.6
18.2
17.9
15.0
22.6
17.6
11.6
16.5
15.8
17.9
17.6
24.5
19.5
21.7
17.4
16.2
19.0
16.4
16.1
Dry
19.3
Dry
Turbidity
NTU
NE
14.5
9.4
2.3
1.1
1.0
3.2
5.4
2.2
14.1
5.4
7.5
5.1
8.1
5.1
7.9
12.0
0.6
1.3
0.8
1.6
0.7
Dry
26.3
Dry
Dissolved Oxygen (DO)
mg/L
NE
0.2
1.8
0.4
0.4
2.7
0.4
0.4
0.6
0.3
1.5
0.5
0.6
5.3
0.5
2.7
0.2
0.3
0.5
0.3
0.4
0.6
Dry
0.5
Dry
Redox
mV
NE
-52.6
94.1
-55.0
-19.0
-40.0
-16.8
-47.1
-33.5
60.1
101.0
68.6
-127.4
-87.8
-105.7
-65.8
-8.1
-54.8
-7.2
-128.5
40.6
-63.9
Dry
-41.4
Dry
Total Antimony (Sb)
µg/1
2.0
0.5
1.0 (i)
<0.50
0.55 J
<0.50
<0.50
0.79 J
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
0.58 J
<0.50
<0.50
<0.50
Dry
0.52 J
Dry
Total Arsenic (As)
µg/1
2.0
1.3
10.0
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
1 <1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
Dry
<1.3
Dry
Total Barium (11a)
µg/I
5.0
1.3
700
170
20
230
530
540
140
nn[mom
59
230
55
180
42
210
20
24
3.1 J
68
130
9.8
110
47
Dry
38
Dry
Total Beryllium (Be)
µg/I
0.4
0.15
4.0 (i)
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
Dry
<0.15
Dry
Total Cadmium (Cd)
µg/I
0.5
0.13
2.0
<0.13
<0.13
<0.13
0.63
0.17 J
<0.13
<0.13
<0.13
0.72
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
Dry
0.19 J
Dry
Total Chromium (Cr)
µg/I
5.0
1.3
10.0
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
12 J
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
1.3 J
<1.3
Dry
1.3 J
Dry
Total Cobalt (Co)
µg/1
5.0
1.3
1.0 (i)
<1.3
<1.3
12
3
33
11
<1.3
<1.3
190
<1.3
lr]t.4 J
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
3.8 J
<5.0
<1.3
Dry
<1.3
Dry
Total Copper (Cu)
µg/]
5.0
1.3
1000
<1.3
1.8 J
<1.3
<1.3
1.6 J
<1.3
1.9 J
<1.3
9.5
1.5 J
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
Dry
3.9 J
Dry
Total Lead (Pb)
µg/]
1.0
0.25
15.0
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
0.48 J
<0.25
<0.25
<0.25
1.1
<0.25
<0.25
0.37 J
<0.25
<0.25
<0.25
<0.25
<0.25
Dry
2.0
Dry
Total Mercury (Hg)
µg/I
0.20
0.091
1.0
NT
<0.091
NT
NT
NT
<0.091
<0.091
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Total Nickel (Ni)
µg/I
5.0
1.3
100.0
<1.3
2.5 J
31
90
12
19
9.8
1.7 J
64
17
4.8 J
<1.3
<1.3
<1.3
<1.3
<1.3
6.2
25
3.4 J
4.7 J
7.7
Dry
3.6 J
Dry
Total Selenium (Se)
µg/1
5.0
1.3
20.0
<1.3
<1.3
1.8 J
<1.3
<1.3
1.5 J
1.3 J
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
1.3 J
<1.3
<1.3
<1.3
Dry
<1.3
Dry
Total Silver (Ag)
µg/1
1.0
0.25
20.0
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
Dry
<0.25
Dry
Total Thallium (Tl)
µg/1
0.5
0.15
0.2 (i)
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
Dry
<0.15
Dry
Total Tin
µg/I
20
5.0
2000 (i)
NT
<5.0
NT
NT
NT
<5.0
<5.0
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Total Vanadium (V)
µg/I
5.0
2.5
0.3 (i)
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
Dry
<2.5
Dry
Total Zinc (Zn)
µg/I
10
2.5
1000.0
<2.5
10
<2.5
17
2.9 J
<2.5
<2.5
3.9 J
13
13
5.8 J
3.8 J
<2.5
<2.5
<2.5
4.6 J
<2.5
2.6 J
<2.5
<2.5
<2.5
Dry
16
Dry
Notes:
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Updated July 24, 2020
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated April 6, 2018
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. MRL = Method Reporting Limit
7. MDL = Minimum Detection Limit
8. NT -Not Tested
9. "J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
14175-04 GW Tables.xlsx
Table 5 Metals Oct 2020
Prepared By: RLB
Checked By: TJD

Table 6
Groundwater Appendix II Pesticides
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Sampled by Pace Environmental Services on October 26-30, 2020
COMPOUND
Method
UNITS
MRL
MDL
MCL
MW-B
MW-2
MW-3
MW-4
MW-4A
MW-5
MW-6
MW-6-
192
MW-7
MW-12-
25
MW-13-
35
MW-13-
132
MW-15
MW-17-
60
MW-17-
137
MW-17-
310
MW-18-
78
MW-19-
75
MW-19-
110
MW-21-
21
MW-21-
94
MW-24-
45
MW-24-
160
DPL-1
Aldrin
EPA 8081B
µg/1
0.040
0.020
0.002 (i)
NT
<0.020
NT
NT
NT
<0.020
<0.020
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
gamma-BHC (Lindane)
EPA 8081B
µg/1
0.040
0.017
0.03
NT
<0.017
NT
NT
NT
<0.017
<0.017
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
alpha-BHC
EPA 8081B
µg/1
0.040
0.015
0.02
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
beta-BHC
EPA 8081B
µg/l
0.040
0.015
0.02
NT
<0.015
NT
NT
NT
0.032 J
0.025 J
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
delta-BHC
EPA 8081B
µg/l
0.040
0.015
0.02
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
cis -Chlordane
EPA 8081B
µg/1
0.040
0.015
NE
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
trans -Chlordane
EPA 8081B
µg/1
0.040
0.015
NE
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
4,4'-DDD
EPA 8081B
µg/1
0.040
0.015
0.1
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
4,4'-DDE
EPA 8081B
µg/l
0.040
0.020
0.1 (i)
NT
<0.020
NT
NT
NT
<0.020
<0.020
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
4,4'-DDT
EPA 8081B
µg/l
0.040
0.020
0.1
NT
<0.020
NT
NT
NT
<0.020
<0.020
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Dieldrin
EPA 8081B
µg/1
0.040
0.015
0.002
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
EndosulfanI
EPA 8081B
µg/1
0.040
0.015
NE
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Endosulfan H
EPA 8081B
µg/1
0.040
0.015
NE
NT
<0.015
NT
NT
NT
0.14
0.042
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Endosulfan sulfate
EPA 8081B
µg/l
0.040
0.015
40 (i
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Endrin
EPA 8081B
µg/l
0.040
0.015
NE
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Endrin aldehyde
EPA 8081B
µg/1
0.040
0.015
NE
NT
<0.015
NT
NT
NT
<0.015
0.020 J
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Endrin keytone
EPA 8081B
µg/1
0.040
0.015
NE
NT
<0.015
NT
NT
NT
<0.015
<0.015
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Total Endrin
EPA 8081B
µg/1
-
-
2
NT
ND
NT
NT
NT
ND
0.020 J
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Heptachlor
EPA 8081B
µg/l
0.040
0.021
0.008
NT
<0.021
NT
NT
NT
<0.021
<0.021
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Heptachlor epoxide
EPA 8081B
µg/l
0.040
0.016
0.004
NT
<0.016
NT
NT
NT
<0.016
<0.016
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Methoxychlor
EPA 8081B
µg/1
0.16
0.021
40
NT
<0.021
NT
NT
NT
<0.021
<0.021
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Toxaphene
EPA 8081B
µg/1
0.040
0.30
0.03
NT
<0.30
NT
NT
NT
<0.30
<0.30
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Dry
NT
Dry
Notes:
1. MCL - Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Updated July 24, 2020
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated April 6, 2018
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. MRL = Method Reporting Limit
7. MDL = Minimum Detection Limit
8. NT = Not Tested
9. "J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
14175-04 GW Tables.xlsx
Table 6 Pest Oct 2020
Prepared by: RLB
Checked by: TJD

Table 7
Surface Water VOCs
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Sampled by Pace Analytical
Services, LLC. October
26, 2020
TEST
UNITS
MRL
MDL
NC2B
SW-1
SW-2
SW-2A
SW-3
SW4
Acetone
µg/I
20
5.0
2,000
<5.0
<5.0
<5.0
5.3 J
<5.0
Acrylonitrile
µg/I
20
0.80
420.0
<0.8
<0.8
<0.8
<0.8
<0.8
Benzene
µg/I
1.0
0.40
51.0
<0.4
<0.4
<0.4
<0.4
<0.4
Bromochloromethane
µg/I
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Bromodichloromethane
µg/I
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Bromoform
µg/I
1.0
0.40
120
<0.4
<0.4
<0.4
<0.4
<0.4
Carbon Disulfide
µg/l
1.0
0.40
100
<0.4
<0.4
<0.4
<0.4
<0.4
Bromomethane (Methylbromide)
µg/1
2.0
0.40
0.04
<0.4
<0.4
<0.4
<0.4
<0.4
Carbon tetrachloride
µg/1
1.0
0.40
1.6
<0.4
<0.4
<0.4
<0.4
<0.4
Chlorobenzene (mono)
µg/l
1.0
0.40
800
<0.4
<0.4
<0.4
<0.4
<0.4
Chloroethane
µg/l
2.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Chloroform
µg/1
1.0
0.40
2,000
<0.4
<0.4
<0.4
<0.4
<0.4
Chloromethane (Methylchloride)
µg/l
1.0
0.50
96.0
<0.5
<0.5
<0.5
<0.5
<0.5
Dibromochloromethane
µg/l
1.0
0.40
21
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dibromo-3-chloropropane; DBCP
µg/1
1.0
0.40
0.13
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dibromoethane; Ethylene dibromide
µg/1
1.0
0.40
0.1
<0.4
<0.4
<0.4
<0.4
<0.4
Dibromomethane
µg/l
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichlorobenzene
µg/I
1.0
0.40
3,000
<0.4
<0.4
<0.4
<0.4
<0.4
1,4-Dichlorobenzene
µg/I
1.0
0.40
900
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,4-Dichloro-2butene
µg/l
2.0
0.50
NE
<0.5
<0.5
<0.5
<0.5
<0.5
1,1-Dichloroethane
µg/l
1.0
0.40
100
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichloroethane
µg/I
1.0
0.40
650
<0.4
<0.4
<0.4
<0.4
<0.4
1, 1 -Dichloroethene (-ethylene)
µg/I
1.0
0.40
20,000
<0.4
<0.4
<0.4
<0.4
<0.4
cis-1,2-Dichloroethene (-ethylene)
µg/I
1.0
0.40
720
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,2-Dichloroethene (-ylene)
µg/I
1.0
0.40
4,000
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichloropropane
µg/I
1.0
0.40
31.0
<0.4
<0.4
<0.4
<0.4
<0.4
cis-1,3-Dichloropropene (-propylene)
µg/I
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,3-Dichloropropene (-propylene)
µg/I
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Ethylbenzene
µg/I
1.0
0.40
97
<0.4
<0.4
<0.4
<0.4
<0.4
2-Hex anone
µg/I
10
2.0
NE
<2.0
<2.0
<2.0
<2.0
<2.0
Iodomethane
µg/I
5.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
Dichloromethane (Methylene chloride)
µM
1.0
0.40
1,000
<0.4
<0.4
<0.4
<0.4
<0.4
2-Butanone (Methyl ethyl ketone)
µg/1
10
2.0
26,000
<2.0
<2.0
<2.0
<2.0
<2.0
4-Methyl-2-Pentanone
µg/1
10
2.0
26,000
<2.0
<2.0
<2.0
<2.0
<2.0
Styrene
µg/l
1.0
0.41
NE
<0.4
<0.4
<0.4
<0.4
<0.4
1, 1, 1,2-Tetrachloroethane
µg/l
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
1,1,2,2-Tetrachloroethane
µg/1
1.0
0.40
4.0
<0.4
<0.4
<0.4
<0.4
<0.4
Tetrachloroethene (-ethylene)
µg/l
1.0
0.40
3.3
<0.4
<0.4
<0.4
<0.4
<0.4
Toluene
µg/1
1.0
0.40
11.0
<0.4
<0.4
<0.4
<0.4
<0.4
1,1,1-Trichloroethane
µg/1
1.0
0.40
200,000
<0.4
<0.4
<0.4
<0.4
<0.4
1,1,2-Trichloroethane
µg/1
1.0
0.40
8.9
<0.4
<0.4
<0.4
<0.4
<0.4
Trichloroethene (-ethylene)
µg/l
1.0
0.40
30.0
<0.4
<0.4
<0.4
<0.4
<0.4
Trichlorofluoromethane
µg/l
1.0
0.40
67,000
<0.4
<0.4
<0.4
<0.4
<0.4
1,2,3-Trichloropropane
µg/l
1.0
0.40
0.001
<0.4
<0.4
<0.4
<0.4
<0.4
Vinyl acetate
µg/l
5.0
1.2
NE
<1.2
<1.2
<1.2
<1.2
<1.2
Vinyl chloride
µg/l
1.0
0.40
2.4
<0.4
<0.4
<0.4
<0.4
<0.4
Total Xylenes
µg/l
1.0
0.40
670
<0.4
<0.4
<0.4
<0.4
<0.4
1,4-dioxane
µg/1
3.0
1.0
80.0
NT
NT
12
<1.0
<1.0
Notes:
NC213 = North Carolina Surface Water Standards for Class B freshwater under Title 15A Subchapter 213.
per NC DWR Surface Water Quality Standards, Criteria, & In -Stream Target Values (Workbook Dated 6-10-2019)
NE = Not Established; North Carolina has not established a MCL
NT = Not Tested
MRL = Method Reporting Limit
MDL = Minimum Detection Limit
"J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
Shaded cells indicated exceedances of NC213 Surface Water Standards
14175-04 SW Tables.xlsx Prepared By: RLB
Table 7 SW VOC (10-26-20) Checked By: TJD

Table 8
Surface Water Field Parameters and Total Metals
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Sam led b Pace Anal tical Services, LLC. October
26, 2020.
TEST
UNITS
MRL
MDL
NC211
SW-1
SW-2
SW-2A
SW-3
SW-4
pH
S.U. (on -site)
<6.0; >9.0
6.9
7.8
7.7
6.4
7.5
Specific Conductance
µmhos/cm (on -site)
NE
57.2
404.0
414.2
60.4
59.7
Temperature
°C (on -site)
29.0
19.0
21.2
19.7
19.7
20.0
Turbidity
NTU (on -site)
50.0
22.0
5.7
7.9
20.5
22.4
Hardness
mg/L
10
2.0
NE
NT
NT
NT
NT
NT
Dissolved Oxygen
mg/L
-
-
<5.0
5.9
4.4
6.4
6.1
Redox
mV
-
NE
110.0
61.9
63.6
130.4
14.8
Total Antimony (Sb)
1g/1
2.0
0.50
640
<2.0
<2.0
0.58 J
<2.0
<2.0
Total Arsenic (As)
µg/l
2.0
1.3
10.0
<2.0
<2.0
<2.0
<2.0
<2.0
Total Barium (Ba)
µg/1
5.0
1.3
21,000
16
31
29
16
15
Total Beryllium (Be)
µg/1
0.40
0.15
65.0
<0.4
<0.4
<0.4
<0.4
<0.4
Total Cadmium (Cd)
µg/1
0.50
0.13
0.82
<0.5
<0.5
<0.5
<0.5
<0.5
Total Chromium (Cr)
µg/1
5.0
1.3
183.07
<5.0
<5.0
<5.0
<5.0
<5.0
Total Cobalt (Co)
µg/l
5.0
1.3
4.0
<5.0
<5.0
<5.0
<5.0
<5.0
Total Copper (Cu)
11g/1
5.0
1.3
3.64
1.5 J
<5.0
<5.0
<5.0
<5.0
Total Lead (Pb)
11g/1
1.0
0.25
13.88
0.80 J
<1.0
<1.0
0.58 J
0.53 J
Total Mercury (Hg)
µgd
NT
NT
0.012
NT
NT
NT
NT
NT
Total Nickel (Ni)
µg/1
5.0
1.3
144.92
<5.0
1.4 J
1.3 J
<5.0
<5.0
Total Selenium (Se)
µg/l
5.0
1.3
5.0
<5.0
<5.0
<5.0
<5.0
<5.0
Total Silver (Ag)
µg/1
1.0
0.25
0.3
<1.0
<1.0
<1.0
<1.0
<1.0
Total Thallium (Tl)
µg/1
0.5
0.15
2
<0.5
<0.5
<0.5
<0.5
<0.5
Total Vanadium (V)
1g/1
5.0
2.5
NE
<5.0
<5.0
<5.0
<5.0
<5.0
Total Zinc (Zn)
µg/1
10
2.5
3621
3.9 J
<10.0
<10.0
<10.0
4.4 J
Notes:
NC213 = North Carolina Surface Water Standards for Class B freshwater under Title 15A Subchapter 213. MRL = Method Reporting Limit
per NC DWR Surface Water Quality Standards, Criteria, & In -Stream Target Values (Workbook Dated 6-10-2019) MDL = Minimum Detection Limit
An assumed hardness of 25 mg/L was utilized to calculate an acute standard for metals highlighted in green. NT = Not Tested
NE = Not Established; North Carolina has not established a standard DNA = Data Not Available
"J"-flagged data (i.e., values estimated between the MDL and the MRL) are presented on this spreadsheet.
Shaded cells indicated exceedances of NC213 Surface Water Standards
14175-04 SW Tables.xlsx Prepared By: RLB
Table 8 SW Metals (10-26-20) Checked By: TJD

Table 9
Groundwater Transects for Remedial Monitoring
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Transect 1
I Transect 2
Transect 3
Transect 4
I Transect 5
MW-4A
MW-B
MW-3
DPL-2 (AB)
MW-6
MW-12-25
MW-17-60
MW-21-21
MW-4
MW-6-192
MW-13-35
MW-17-137
MW-21-194
MW-19-75
MW-5
MW-13-132
MW-19-110
DPL-1
MW-24-45
MW-18-78
MW-24-160
Bold - MNA Performance Well
AB - Abandonded
14175-04 GW Tables.xlsx
Table 9 Transect Numbers

Table 10
Groundwater Geochemical Parameters for MNA
Old Buncombe County Landfill
Woodfin, North Carolina
Permit No. 1101-MSWLF-1979
BLE Project Number J20-14175-04
Sampled by Pace Analytical Services, LLC. October 26-30, 2020.
TEST
UNITS
MPL
MDL
MCL
MW-B
MW-2
MW-3
MW4
MW4A
NM-5
MW-6 MW-6-192
MW-7
MW-12-25
MW-13-35
MW-13-132
MW-15
MW-17-60
MW-17-137
MW-17-310
MW-18-78
MW-19-75
MW-19-110
MW-21-21
MW-21-94
MW-24-45
MW-24-160
DPL-1
Dissolved Hydrogen (DH)
nM
1.9
0.49
NE
NT
5.4
NT
4.6
NT
NT
20
NT
NT
NT
NT
6.0
NT
NT
NT
NT
6.6
1.4 J
3.6
2.7
5.3
Dry
10
Dry
Lactic Acid
m9/1
0.50
0.053
NE
NT
<0.053
NT
<0.053
NT
NT
<0.053
NT
NT
NT
NT
<0.053
NT
NT
NT
NT
<0.053
<0.053
<0.053
<0.053
<0.053
Dry
0.058 J
Dry
Acetic Acid
m9/1
0.50
0.120
5.0 (i)
NT
0.41 J
NT
4.0 J
NT
NT
4.1 J
NT
NT
NT
NT
4.0 J
NT
NT
NT
NT
4.0 J
3.9 J
0.44 J
3.7 J
0.79 J
Dry
0.42 J
Dry
Propionic Acid
mg/1
0.50
0.053
NE
NT
<0.053
NT
<0.053
NT
NT
<0.053
NT
NT
NT
NT
<0.053
NT
NT
NT
NT
<0.053
<0.053
<0.053
<0.053
<0.053
Dry
<0.053
Dry
Formic Acid
mg/l
0.50
0.055
NE
NT
5.0
NT
48
NT
NT
45
NT
NT
NT
NT
44
NT
NT
NT
NT
4.6
44
4.8
44
9.5
Dry
4.8
Dry
Butyric Acid
mg/1
0.50
0.058
NE
NT
<0.058
NT
<0.058
NT
NT
<0.058
NT
NT
NT
NT
<0.058
NT
NT
NT
NT
<0.058
<0.058
<0.058
<0.058
<0.058
Dry
<0.058
Dry
Pymvic Acid
mg/I
0.50
0.060
NE
NT
<0.06
NT
<0.060
NT
NT
<0.060
NT
NT
NT
NT
<0.060
NT
NT
NT
NT
<0.060
<0.060
<0.060
<0.060
<0.060
Dry
<0.06
Dry
i-Pentanoic Acid
m9/1
0.50
0.061
NE
NT
<0.061
NT
<0.061
NT
NT
<0.061
NT
NT
NT
NT
<0.061
NT
NT
NT
NT
<0.061
<0.061
<0.061
<0.061
<0.061
Dry
<0.061
Dry
Pentanoic Acid
mg/J
0.50
0.056
NE
NT
<0.056
NT
<0.056
NT
NT
<0.056
NT
NT
NT
NT
<0.056
NT
NT
NT
NT
<0.056
<0.056
<0.056
<0.056
<0.056
Dry
<0.056
Dry
i-Hexanoic Acid
mgA
0.50
0.056
NE
NT
<0.056
NT
<0.056
NT
NT
<0.056
NT
NT
NT
NT
<0.056
NT
NT
NT
NT
<0.056
<0.056
<0.056
<0.056
<0.056
Dry
<0.056
Dry
Hexanoic Acid
mg/1
0.50
0.058
NE
NT
0.076 J
NT
0.67 J
NT
NT
<0.058
NT
NT
NT
NT
<0.058
NT
NT
NT
NT
<0.058
<0.058
<0.058
0.58 J
<0.058
Dry
0.058 J
Dry
Methane
ugli
5.0
2.5
NE
NT
7.7
NT
720
NT
NT
4,700
NT
NT
NT
NT
1,400
NT
NT
NT
NT
1,700
480
400
11900
21000
Dry
27
Dry
Ethane
ugfl
1.0
0.075
NE
NT
<0.075
NT
0.47 J
NT
NT
0.92 J
NT
NT
NT
NT
<0.075
NT
NT
NT
NT
1.1
0.67 J
<0.075
1.1
1.5
Dry
<0.075
Dry
Ethene
ug/I
1.0
0.12
NE
NT
<0.12
NT
0.46 J
NT
NT
0.3 J
NT
NT
NT
NT
1.8
NT
NT
NT
NT
1.3
0.46 J
<0.12
0.75 J
0.33 J
Dry
0.34 J
Dry
Carbon Dioxide (CO2)
m9/1
0.9
0.127
NE
NT
30
NT
177
NT
NT
197
NT
NT
NT
NT
281
NT
NT
NT
NT
83.2
141
3.93
165
55.9
Dry
1.43
Dry
Alkalinity
m9/1
20
20
NE
NT
60
NT
420
NT
NT
560
NT
NT
NT
NT
150
NT
NT
NT
NT
300
410
170
640
310
Dry
64
Dry
Sulfide
m9l1
1.0
0.99
NE
NT
<0.99
NT
1.3
NT
NT
<0.99
NT
NT
NT
NT
<0.99
NT
NT
NT
NT
1.2
<1.0
<1.0
1.6
<1.0
Dry
<0.99
Dry
Biological Oxygen Demand (BOD)
m9/1 2.0
0.18
NE
NT
<0.18
NT
2.2
NT
NT
10
NT
NT
NT
NT
3.6
NT
NT
NT
NT
3.9
2.8
2.4
3.2
2.1
Dry
2.0
Dry
Sulfate
m9/1 1.0
0.2
250
NT
4.1
NT
21
NT
NT
0.78 J
NT
NT
NT
NT
7.2
NT
NT
NT
NT
1.2
11
9.7
13
2.2
Dry
27
Dry
Nitrate
m9/1 0.10
0.025
10
NT
0.028
NT
<0.025
NT
NT
<0.025
NT
NT
NT
NT
<0.025
NT
NT
NT
NT
<0.025
<0.025
<0.025
<0.025
<0.025
Dry
<0.025
Dry
Chloride
m9/1 1.0
0.2
250
NT
2.1
NT
57
NT
NT
140
NT
NT
NT
NT
4.7
NT
NT
NT
NT
140
160
39
86
89
Dry
6.4
Dry
Chemical Oxygen Demand (COD)
m9/1 20
20
NE
NT
<20.0
NT
21
NT
NT
39
NT
NT
NT
NT
<20.0
NT
NT
NT
NT
28
45
<20.0
38
21
Dry
<20.0
Dry
Total Organic Carbon (TOC)
m9/1 1.0
1.0
NE
NT
<1.0
NT
5.9
NT
NT
11
NT
NT
NT
NT
<1.0
NT
NT
NT
NT
8.0
14
2.2
12
7.1
Dry
1.1
Dry
Iron II (field measured)
u t
NE
2,500
ND
NT
6,000
NT
2,500
3,000
3,000
3,000
ND
1,000
7,000
ND
2,000
3,000
ND
3,000
2,000
2,500
7,000
2,000
Dry
1,500
Dry
Notes
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Updated July 24, 2020
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated April 6, 2018
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. MRL = Method Reporting Limit
7. MDL = Minimum Detection Limit
8. NT = Not Tested
9. "J"-flagged data (i.e., values estimated between the MDL and the MRL) me presented on this spreadsheet.
10. ND = Not Detected
14175-04 GW Tables.xlsx
Table 10 MNA Oct 2020
Prepared By: RLB
Checked By: TJD

Figures

r O
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25
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$ C' IOLivette-Cem� fq 70
ry. n ec>
00 3
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Old
Macedonia
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Gem. f {(�, 251 N Akp
UpLB�N:pR
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23 I
0 1 b OODFIiN r0
N 0
0
m,
Q)
REFERENCES:
Mour USGS TOPOGRAPHIC MAP, 7.5
2000 1000 0 2000 4000 r MINUTE SERIES, WEAVERVILLE AND
LEICESTER. NC. QUADRANGLE 2019
APPROXIMATE SCALE IN FEET ;� ,
DRAWN' KLW DATE: 12-29-20 BUNNELL FIGURE
IM
M LAMMONS SITE LOCATION MAP
CHECKED: TJD CAD: BCOLF04—SLM M ENGINEERING CLOSED BUNCOMBE COUNTY LANDFILL
6004 Ponders Court, Greenville, SC 29615 WOODFIN, NORTH CAROLINA 1
APPROVED: AWA JOB NO: J20-14175-04 Phone: [phone] Fax: [phone]

250 125 0 250 500
APPROXIMATE SCALE IN FEET
I o0 ff
0
I q ,
LAN,
ACTIVE
MONITORING
WELLS
INACTIVE
MONITORINC
WELLS
�BANDONE[
IONITORINC
WELLS
ACTIVE
SURFACE
WATER
SAMPLING
LOCATIONS
INACTIVE
SURFACE
WATER
SAMPLING
LOCATIONS
MW-2
MW-8
MW-9
SW-1
SW-5
MW-3
MW-12-10
MW-10
SW-2
SW-6
MW-4
MW-13-10
MW-16
SW-2A
SW-7
MW-4A
MW-14
MW-17
SW-3
SW-8
MW-5
MW-18-3
DPL-2
SW-4
SW-9
MW-6
MW-19-4
MW-6-192
MW-20-3
MW-7
MW-20-32
MW-12-25
MW-21-4
MW-13-35
MW-22-78
MW-13-132
MW-22-143
MW-15
MW-23-119
MW-17-60
MW-23-186
MW-17-137
MW-A
MW-17-310
MW-18-78
MW-19-75
MW-19-110
M W-21-21
M W-21-94
M W-24-45
M W-24-160
DPL-1
M W-B
NOTE: ACTIVE SAMPLING MONITORING WELLS AND SURFACE LOCATIONS ARE TO BE
SAMPLED AND TESTED TWICE ANNUALLY. INACTIVE MONITORING WELLS ARE TO BE
CHECKED FOR DEPTH TO GROUNDWATER ONLY.
*WATER LEVEL IS DEEP AND NOT USED FOR CONTOURING PURPOSES.
** WATER LEVELS COLLECTED BUT NO VERIFIABLE SURVEY DATA COLLECTED
FOR GROUNDWATER ELEVATION CONTOURING PURPOSES.
NM -NOT MEASURED
1 r- n r- n 1 r1
MW-2® ACTIVE GROUNDWATER MONITORING WELL
MW-8(p INACTIVE GROUNDWATER MONITORING WELL
MW-8 & ABANDONED GROUNDWATER MONITORING WELL
SW-1- ACTIVE SURFACE WATER MONITORING LOCATION
SW-54 INACTIVE SURFACE WATER MONITORING LOCATION
PROPERTY BOUNDARY
SURFACE WATER
POTENTIOMETRIC CONTOUR
GROUNDWATER FLOW DIRECTION
200 100 0 200 400
APPROXIMATE SCALE IN FEET
REVISIONS
No. DESCRIPTION BY
DRAWN: RLB
CHECKED: TJD
APPROVED: AWA
)ATE: 12-7-20
,AD FILE: BCOLF-04WTM
JOB NO: J20-14175-04
BUNNELL
� LAMMONS
ENGINEERING
6004 Ponders Court, Greenville, SC 29615
Phone: [phone] Fax: [phone]
GROUNDWATER ELEVATION CONTOUR MAP — OCTOBER 26-30, 2020
OLD BUNCOMBE COUNTY LANDFILL
WOODFIN, NORTH CAROLINA
FIGURE NO.
2

APPENDIX A
FIELD SAMPLING LOGS
PACE ANALYTICAL SERVICES, LLC.

Document Name: Field data Sheet
Date Issued: March 8, 2019
e+lk7li4kal y
Page: I of a
suing Authority:
cfice tersviEle Quality,
�`
Document Numbim F-CAR-FLD-001-re�.03
Office
Field Data Sheet
Client: SL-F _Location:
A 1,a-vrI(sip •�s� Project #: u nr'R[y�4�c C�. ld Z
Name and Affiliation (Sampler(s)QT)7 - PCx ck !� nrt�c. t Field Data Sheet Review:
Name -and Affiliation (Inspector): M)A
Date; By:
Well Information
Well ID: -. 1-9-7-7
Well Locked: rE� / NO / Flushmount) '
Well Diameter:
Construction: (V�/SteeI/Stainless Steel)
Total WellDepth: G ft
Multi Factor; 0, � 3 [(Radius/12)2 x 3.14 x 7.481
d
Static Water Level: t-'i�- ft
Casing Volume: j 1 gallons.
Height of Water Column! ' 13 it
Cal. 3 Volumes: `�'a gallons
Pump Intake: • QQ ft
Purge Information
Date Purged: C7 . / L ./ .
Start : 1 9 5- _ Finish: � Purge Rate- ;)4
Purging Method: PWLIsVCJ4_VC.
�Total.Volume'Purged: oQ (gauons/(Td/L)
}
Sampling Infolnformation
Date Collected: l n / )�
Time Collected: 1320 (am/(
Sampling Equipment Used: R-rTs6%t"t ?u&f Instrument ID: YSrpm�Iw. i Qa(1 MtGcc1I4'W 3�y
13attIe Type I'reservatin AnalyVsis Required
vex% to i
�o Z I, H _D ou�nQ
N
Mti1A
Field Measurements/Observations
Sample Temp (°C): 1-4 • Time: )LQ Turbidity (ntu); Q • Timer I3 _
Diss Oxy (mg/L): n '�
Time:
Fe 2+ mg/L: . O
Time:
Specific Cond. (uS): �75 3
Time: 13
Res. C! (mg/L)/(µg/L):
�Time:.
Sample pH (s.u.): L '3
Time: _ 13310 .
Odor:Na
Time:
ReDox (m.V): TM St-e •
Time: 3-DO
Appearance: Qeo
Time: I
ReDox (EH value):YSI ProPlus +200mV }'u 5 A ^
Other:
Time:
General/Weather Observations:.
cloudy/rainy) Temp.r}_�)- (°F) Wind a (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
CC)
Diss Oxy.
(mg/L)
Spec.
f S) •
PH (s.u.)
ReDox
(m.V)
Turbidity
(ntu)
Volume
removed
(gallons
Water
level (ft)
Other
I
26o
6,3
to
1
L Q
6:3
r
au
b� 3LA�—
i3
ti-- .
b. 3
� g,4
a .
S a
, ��
----�

Document Name:
Field Data Sheet
Document Number.
F-CAR-FLD-001.rev.03
Client: FS L-
Location: v, 4 � /-) C—
Project: 5V,nC- 01 J.L1�7
well ID: M kj - 111 1� _
Reviewed Date and By:
Stabilization Test
Document Issued: March 8, 2019
Page aof
Issueing Authority:
Pace Huntersville Quality Office
E 1...62-5
I 2a.Z
a
4
1 Amity
Time
Temp.Spec.
r •
Cond.
r.Waterlevel
Turbidity
.
•
Purged
(1,C)
(ntu)
circle on
�����■��
�®_r�■��
ram■
ram■

Document Nen►e: Field data Sheet
Date Issued: March 8, 2019
1 of a
aceArWyWai'
—Page:
Issuing Authority: Pace Huntersville Quality.
Document Numbor: F-CAR-FLD-001-eev.03
Office
Field Data Sheet
Name and Affiliation (Sampler(s):_ ']- kce A A al „g,(
Name and Affiliation (Inspector): N 1 A
Well Information
Well ID: M t-J - J S 11
Well Diameter:
Total Well Depth: 3 ' S . ft
Static Water Level: i o 0 • it
Height of Water Column: l Q3 •y � ft
Well Locked:
#: cc- Q i d LC
:ld Data Sheet Review:
Date: 11- 0 3 - 2 ° By:
'/ NO / Flushmotlnt )
Consttuction: (ik/Steel/Stainless Steel)
Multi Factor": Q ° 1 (73 r(Radius/12)2 x 3.14 is 7.48].
Casing Volume: i b ."S' gallons.
Cal. 3 Volumes: 670- 6 1 gallons
Pump Intake: 1(0,00 . ft
Purge Inforiation
Date Purged: 10 / a6 ./ Start: �5—) O Finish: 6 Q IL Purge Rate: a H 0 m L`�
Purging Method:_ 2�Totdi Volume Purged: i SL 0 Q (gallons/is)
Sampling Information
Date Collected:_LQ—j2L./ o.) Q Time Collected: L�, t ® (am/em
Sampling Equipment Used: Lf-c -6 9 s(1 c_p4c6p^Instrument ID: Y5 T �c-n3e �
Bottle Type Preservatign Analysis Required
Field Measuretnerits/Observations
Sample Ternp CC): -Time: Turbidity (ntu): 0 Time, ) 6 r O
Digs Oxy (mg/L): Ci,3 Time: 14 i LFe2+mg/ L: , Time:- 16 t o
Specific Cond. (uS): 4SY , :•,Time: 116�—Res. Ci (mg/Ly(µg/L): Time:
Sample pH (s.u.): '� ,t-� _ Time: 1 I.O Odor:
ReDox (mV): 8, Time: 16_ l Q Appearance: _ C4190-c— Time: ( 6 / 0
ReDox (EH value):YSI ProPlus +200mV Other: Time:
General/Weather Observations: .
sun4/cloudy/rainy) Temp.'Ll (°F) Wind 3 (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
CC)
Digs Oxy.
(mg/L)
Spec.
5)
PH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/
Water
level (ft)
Other
a.
��.
6
s
-7- •
1j0
i1,�
Ans—
Li
1 �.
7, L
6, L
��
�)4 00-�--
l�a�
titi .
-b
-a ,,:,I
1 S 35-
1
t-1W
V., 1
1-722
1

s
Document Name:
Field Data Sheet
Document Number.
F-CAR-FLD-001.rev.43
Client: LE --
Location: F�QnA ( (.e I --
Project: �l f�Cnrn iT ti a LE -
Well lb: (VY�J --121 - 114
Reviewed Date and By: �� 3 "a0 CV
Stabilization Test
Document issued: March 8, 2019
Page _Nf oL
issueing Authority,
Pace Huntexsvitle Quality Office
1.1.6,25
"s
13, 6770E
A
a�
;6,
1.6
g.,5
0�L4
Time•Cond.
7d!
Spec.
Turbidity
�
Water level
P u r g e
circle one
�■�o����
pro

Document Name: Field date Sheet
Date Issued: March 8, 2019
as&Arwlj feaf'
Page: 1 of _
Document Numbtr: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality
Office -
Field Data Sheet
Ltv
Name and Affiliation (Sampler(s): Field Data Sheet Review:
Name and Affiliation (inspector):
Well Information Date: G
Well ID: . M .L-J -. al - 54 Well Locked: t i / NO / Flushmount )
Well Diameter: " Construction: 'V /Steel/Stainless Steel)
Total Well Depth; . CH ,1 °l ft
Static Water Level:.*`a ft
Height of Water ColumnA •k k ft
Multi Factor*: Q • 1 b3 [*(Radius/12)2 x 3.14 x 7.481
Casing Volume: 14. gallons.
Cal. 3 Volumes: a a gallons
Pump Intake: ft
By:
old Lr
Purge Information
Date Purged: 9 4 Start :Q'� 1 7— Finish: 0'19 Q Purge Rate: a can L
Purging Method: 7C c, s �k -k ;?sc�np —Total Volume Purged: Lj Q 4 (gallons/e/L)
Sainuliniz Information
Date Collected: 9 Q /2a/ �. . Time Collected:99W�- (apm) '
Sampling Equipment Used: 1--C . A 6'�, 41 pi" trument ID: V5 f4- Oa4lA rc a^a7 Qw rr 30-�.9
Bottle 'Type Freservatibn Analyysis Required
J4C.4 i�cAu15
Apo 1-- 4- 1� �l�a 0 ,,.y
Field Measurements( Observ_tations
Sample Temp (aq: Tine: CUi 14 Turbidity (ntu): Q Timer ()Cj"�
Dias Oxy (ing/L):_ Q1 Time: Fe 2+ mg/L: a . Q Time: Q)C'k -f=
--------Specific--Cond:=(-aS): `�2- -_ - -T-ime-Qq--t Z- Res. Cl (mg/L)/(µg/L): ---- -T=ime:. =- - -- - - - --
Sample pH (s.u.): , Time: Q�1 -f - Odor: Lard ,0 Time: Or l
ReDox (mV):_ �� �{ Time: OGLi T- Appearance:. Ciecg' Time: 0r-1-4�
ReDox (EH value):YSI ProPlus +200mV ) ti Other: Time: —
General/Weather Observations:
(sunny lou /rainy) Temp-5-7 _{°F) Wind 3 (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
( q
Diss Oxy.
(mg/L)
Spec.
{ )
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/�nlsj/
Ll
Water
level (ft)
Other
I6.1
115
"Rs-3
(,,
P I 1 1.
q 3
1t '. �
1
b.
-H
_-5
10230 11
L. o
.WS-, 9
s,
a g o
.�
Q9Lio 16 11 Cl•6 33'� b.b - 6s.3 1, 0 Ll000 HBO —�--

y, aceArelyPca!"
t
Document Name: Field data Sheet
Document [Number: F-CAR-FLD-001-rev.03
Field Data Sheet
Name and Affiliation (Sampler(s);_RM 6 ?-(L
Name and Affiliation (Inspector): N (IV
Well Information
WeIIID: Mw-2l-11
Well Diameter: 2 : n
Total Well Depth: 13 •� fk
Static Water Level: s. 7 9 it
Height of Water Column: 17.9 1 ft
Well Locked:
Construction:
Date issued: March 8, 2014
Page: 1 of _I
ig Authority: Pace Hunterwille Quality.
Office -
#: BanL. CO. 01J L1=
1d Data Sheet Review:
Date: 1113 By:
/ Flushmount )
Steel)
Multi Factor*:? �.14 3 r(Radius/12)2 x 3.14 x 7,48].
Casing Volume: Z • Q rJ gallons
Cal. 3 VoIuines: " 8.7 gallons
Pump Intake: 2. �t
Purge Information
Date Purged: tO. / 17 ./ In Start: 0.4(0 Finish 0Q Purge Rate: 80,41ii`" 1
Purging Method: - P Qr-; 14% 14, 'c Ptt m P Total Volume Purged: 6 o0 (gallon mis L)
Sampling Information
Date Collected: 1. 0. Time Collected: 0135 (am m}
Sampling Equipment Used: PE -%Sf-b• f *1'4 Pu 'A P Instrument ID: Y f1 S 6 q f rpW 6o Q 3
Bottle Type Preservation Analysis Required
N A
Field Measur merit Observii tions
Sample Temp (°C): f b• 'l Time: n0►35 Turbidity (ntu): 1 • 6 Timer_ OS 35
Digs Oxy (mg/L): y Time: I Fe 2+ mg/L: "7•0 Timer 1104, on 1%/4/ ZD
- Sgecific�ond_( S): ..-�..373 ...----=Time: Res. Q (mg/LY(µg/L):
b 3 . _Time: Odar: T rp --- -—__
Sample pH (s.u.): n_ .,.,. Time; `� 9 3 5
ReDox (mV): 4 • 6 Time: Appearance: _ 4164-- e' Time:
ReDox (EH value):YSI ProPlus +200mV I S q • i{ Other: Time:
General/Weather Observations_
(sunn cloud rainy) Temp. j_(°F) Wind 4 S (mph)
Sampler Signature:__ _ R y a- It S 1/014 Date:i L � � Z 7 / Z rD
Stabilization Test
Time
Temp.
Diss Oxy.
Spy'
pH (s.u.)
ReDox
Turbidity
Volume
removed
Water
Other
Purged
(oq
(mg/L)
(US)
(mV)
(ntu)
(gallons
level (ft)
IS .
•�
LA
1 53
6 , 3
- 3 •S
'z , 4
y 0!)
5,s
,9
16.4
�
1353
b-�3
33.�.
z,L\
A00
0ILo
ib.
0.1o137.
6.3
_36,
4,7
too.
5,q i
_9a 25
•4
0•
1i7
b.3
3y.2
1,8
izoo
5,q5
DOOO
16
3.3
6,_2
I 4.
1.$
1604
5.�7

s
Document Nerve: Field data Sheet
Elate Issued: March 8, 2019
Page: 1 of I
ace,rrafyEical
Documentl�Eumlrer; F-CAR-FLl?-001-�ev.03
Issuing Authority: Pace Huntersville Quality.
1.
�
, Office .
Field Data Sheet
#: &aa ww �a- o I d L (--
Name a:nd Affiliation (Sampler(s): A-T�- - ?acn A-aa(P Field Data Sheet Review: .
Name and Affiliation (Inspector): . 01A __-
Well Information Date: CI' o3'"�b By: �/
Well ID: M tJ - I Q Well Locked: / NO / Flushmount )
Well Diameter: �" Construction: (1V9/Steel/Stainless Steel)
Total Well Depth: I-S ,Q.A ._-.._ft
Static Water Level: LA • 6 Q ft
Height of Water Column: b ya ft
Multi Factor: Q�163 l•(ltadiue/12]2x 9.14 x 7.48]
Casing Volume: gallons.
Cal. 3 Volumes: 33 gallons
Pump Intake:
Purge Information
bate Purged:-16-_/ / 1,Q Start : PLAO Finish: Q 4, Purge Rate: a t-f Q t',' LIcrylal
Purging Method:_ - Fe- a:tS ()(- o Total Volume Purged: LAY00 (gallons/L)
Sampling Information
Date Collected: 1 Cl /)}/ -�)-o Time Collected: JI Q S
Sampling Equipment Used:- i��cts {HL v��nR_InstrumentID: greWi�,30;�,
Bottle Type Preservation Analysis Required
A.nAx "focj, "y ats
1-1 VT13xgLlk
nn hJ
Field Measurements Observations
Sample Temp (DC): Time: () Turbidity (ntu): 3 Timer i I n S�
Diss Oxy (mg/L): Time: I QS— .Fe 2+ mg/L: _ C) ime: f 1 L)
S ecific Cond.- uS A- �-_ Time: QL— Res. Cl (mg/L)/(µg/L): =--=Time.. --
Sample pH (s.u.): _-�' `3� Time: 1,, 0, Odor: Time: I
ReDox (mV): - a Time: I N SAppearance:. Q-eo Time: i f Q C
ReDox (BH value):YSI ProPlus +200mV I q'a-,2 Other: Time: --
General/Weather Observations:
(sunny/ oud rainy) Temp.57 (°F) Wind � (mph)
Sampler Signature
Stabilization Test
10
Time
Purged
Temp.
Cq
Diss Oxy.
(mg/L)
Spec.ReDox
E S)
PH (s.u.)
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/
Water
level (ft)
Other
23
- s
'�,-4 o
6
i a3
b.
�3j
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� I Q
1 .
0-�
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- b•

Document NamDate Issued: March 8, 2014e: Field data Sheet Page: 1 of _�
C8r7l1r]ljEACaI s Issuing Authority: Pace Huntersvilli
f .Document Number: F-CAR-FLD-00I-rev.03 Office
Field Data Sheet -
Client: BL f Location: _ A_i wet, ! (e,,c h! C Project #: 13411. Cg . old $- C
Name and Affiliation (Sampler(s):_ FM P6t t e
Name and Affiliation (Inspector): N /
Well Information
Well ID: M w - 3
Well Diameter: -4 t n
Total Well Depth: $ 7 , —ft
Static Water Level: b ..0 S ft
Height of Water Column: fg�_ft
Well Locked:
Construction:
Data Sheet Review;
Date: (ti;ICON
/ Flushm.ount )
tainless Steel)
Multi Factor*: 0, 1 6 3 ['(Radius/12)2 x 3.14 x 7.48]
Casing Volume: 3 ' 14 gallons.
Cal. 3 Volumes: '� Z q gallons
Pump Intake: ' $ 3 ft
Purge Information
Date Purged: to / Z'7./ . 2ej Start Finish: Finish: 11 5.. Purge Rate:--La-or-1S�f++i
Purging Method: g 1'`dd f e' N eA l' Total Volume'Purged: '7 0 Q0 (gallo /m1s L)
Sampling Information
Date Collected: io. /g_7/ Z Q Time Collected: y 20p (am prn)
Sampling Equipment Used:_a_l�J �e,(' P Lk rA P. Instrument ID:`f 4Z 0_56 D _/ZPuv6d
Bottle Type
1'reservati6n
Analysis Required
N(- APr.
1,r H - Di4)eISA'Q
Field Measuremerits/Observations
Sample Temp (°C): ! 7 • ` Time: 11 C) +7 Turbidity (ntu). Z • 3 Time Z 00
Diss Oxy (mg/L): Time; A Fe 2+ mg/L;
_ S _ecific-Cond.- uS • �43 Time: Res. C1 m L L —"r1'ime:.
Sample pH (s.u.): 6 • Time: Odor: 0 -
ReDox (mV): S 5 . Q Time: Appearance: 4-1 ear - Time: `
ReDox (EH value):YS1 ProPlus +200mV 145.0 Other: Time:
General/Weather Observations:
cloudy/rainy) Temp. (°F) Wind a - 5 (mph)
Sampler Signature: o-n b &- Date: 7 / Z 0
Stabilization Test
Time
Temp.
Digs Oxy.
Spec'
•
PH (s.u.)
ReDox
Turbidity
Volume
removed
Water
Other
Purged
( q
(mg/L)
t S)
(mV)
(ntu)
(gallo mis
level (ft)
0
10
b 4
- b.5
5.1
So
1 b. 2
otke
1 -$
o.•7
llko
IA
-4b.5
5. q
50Q
6b Al
.
11 S
l
0.
T%05
-o. 5
ki .3
1Djc3
6.71
�1 So 11J.5
►
-5"k 6
2,
ISO
6 . 7.
1 5
7
j.
A,
141.5 .
&,.
-54.6 12,
ZD JXj
6 1..3

Document Name: Field data Sheet
Date Issued: March 8, 2019
Page: l of—(
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority:: Pace Huntersville Quality,
Office .
Field Data Sheet
Name and Affiliation (Sampler(s): Wt- Rha- AnalAca'
Name and Affiliation (Inspector):_ ii i A
Well Information
ti L Project #:� a� a rnh� Cc�- 4 id LS
Field Data Sheet Review:
Date: 11- 01 " Z u By: ,r S
Well ID: �Yl I^ 1 - _ Well Locked: M / NO / Flushmount )
Well Diameter: �� Construction: PV /Steel/Stainless Steel)
Total Well Depth: T) , oQ ft Multi Factor*: Q_ y L 3 r(Radius/12)2 x 3.14 x 7.481
Static Water Level: 4 ` . --it Casing Volume: 6 gallons.
Height of Water Column:] �' ft Cal. 3 Volumes: gallons
Pump Intake: -'T-3 •S­'�' ft
Purge Information_
Date Purged: Start: 12aO Finish: I cSL7 Purge Rate: r��-lmsn
Purging Method: F) l al d,e r �z o rna ^Total Volume Purged: 6 M Q (gallons/ L)
Sampling Information
Date Collected:. 1Q_/ / .aM- .n Time Collected:_1 '� J (=4�
Sampling Equipment Used: Sh a d dw-strument iD:
Bottle Type Preservation Analysis Required
A p Z JQb i-(ftktr
- AUK
+ (, Ll 'D4bua-e- -
Field Measurernents/Observ_ations
Sample Temp (°C): i Q Time: Turbidity (ntu): _ j • - Time:'. a ^
Digs Oxy (ing/ L): Q '� -Time: Fe 2+ mg/ L: S Time:. l
-- Specific C-ond:(u5): - - - - T=Time: 1 5 Res. Cl (mg/L)/(µg/L): - TTime: - - -- - - -- ---
Sample pH (s.u.): 6 Time: ti -,'LSE-- Odor: Lc­n j o l L Time: i a�
ReDox (rxtV): Time: 1 Appearance: _ L_ S e er' —Time:
ReDox (EH value):YSI ProPlus +200mV 1-1ta Other: -- Time:
General/Weather Observations:
unn oudy/rainy) Temp-' 3 (°F) Wind t (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.Dins
(oq
O
(mg/)
Spec.
Cond.
pH (s.u.)
ReDox
(mV)
Turbidityremoved
(ntu)
Volume
(gallons/ 11 s
Water
level (ft)
Other
a�
l5 I
�•
l39
L
ti
1,.
1000Q
13ael�4
t
1� .0
1 0.6
1,
3 t a
q •3 .
W
S�
LA, Ck
S Ono
1a5 4 1� a n f 3�S U,;3 -t6.6 3 5 b000 53.6`t

Document Name: Field data Sheet
Date Issued: March 8, 2019
aCe Afj81j4ea('
Pa e: 1 of?
Document P+lumb2r: F-CAR-FLD-Ol7l-rev.p3
Issuing Authority: Pace Huntersville Quality,
t
Office .
Field Data Sheet
Clienf: B LIE Location: A 5 Mey;1 re, NL Project #: $ttn� G�. atz L
Name and Affiliation (Sampler(s). R A 13 N c ¢ . Field Data Sheet Review:
Name and Affiliation (Inspector): N /A
Well Information Date: �, 3 I By.
Well ID: . M W WellLocked: <YE5 NO / Flushmount) `
Well Diameter: Construction: PVC Steel/Stainless Steel)
Total Well Depth: 7 6 .7 5
Static Water Level: 7 2 0 y it
Height of Water Column: 1427 ft
Purge Information
Multi Factor*: O. l [*(Radius/12)2 x 3.14 x 7.481
7
Casing Volume: `7 gallons
Cal. 3 Volumes: 2.3 ( gallons
Pump Intake: "' 7 5 ft
Date Purged. I /
"2' /
.2 O Start: 1.3 CQ Finish: 1330
Purge Rate:
i do _ __►1 S / ^� • �1
Purging Method: Did
roOLbse
ID —Lie.- ?A.-r Total Volume Purged:
3000
(gallons mis L)
Sampling Information
Date Collected:—! 0. /32/ 19 Time Collected: 131 ( pm)
Sampling Equipment Used: 0' 1 Po sap Ie 0 u Instruent I1•
Bottle Type
Field Measurernents/Observations
Preservatimn
Analysis Required
MN A
C A
Sample Tentip (°C): • 1 Time: 3 Turbidity (ntu): ( Time: 1335
Digs Oxy (Mg/L): Q H Time: Fe 2+ mg/L: rg•Q T ne;. — rl I 4 n t114 /20
K 2�—
Specific--C-ond. (uS)------- Time: Res. Cl (mg/L)/(pg/L): �T=ime;. - - --- --- - -
Sample pH (s.u.): �. 2 _ Time: Odor: N n� Time: 13 3 5
ReDox (mV): °1 . d Time: Appearance: _ �- le �`r Timer i
ReDox (EH value):YSI P.roPlus +200rnV i l •4 Other: Time.
General/Weather Observations:
-- - -- -- �Wcloudy/rainy) Temp. 70 (OF) Wind �" 5 (mph)
Sampler Signature: R n 8 o 5 Date: 14 Z
Stabilization Test
Time
Purged
Temp.
a
(C)
Digs Oxy.
{mg/L)
Spec'
Cond.
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons rnls
Water
level (ft)
Other
(US)
L
13o
16 ,I
2 ,e
a i 3
2
-16. 7
LA
SQ9
31 o
1'3 . rA
LA
alb
_15-7
2 . z
1000
13t 5
I
1.0
q001A
6.
..I4A
1 .
iSoO
13 z�
13•4
0. 6
6 .Z
15. 11

Document Issued: March 8, 2019
Document Name:
Field Data Sited
Page
Document Number:
F-CAR-FLD-001.rev,03
Issueing Authority:
Face Huntersvitle Quality Office
Client:
Location:
Project:
well lb: W—
Stkbilization Test
Time
Temp-
Diss Oxy-
Spec.
Ems U'r
—~----
1.27
Turbidity
Volume Removed
Water level
circle one

Document Name: Field data Sheet
Date Issued: March 8, 2019
aceAwl3ftaTy
Pa e: 1 of
Document [`lumber: F-CAR-FLD-001-rev.03
issuing Authority: race Huntersviiie Quality-
Office
Field Data Sheet
C_
Name and Affiliation (Sampler(s): 3W, - -Rac z A-na U,�,( Field Data Sheet Review:
Name and Affiliation (Inspector): N)
©
Well Information Date; 11 - 2a
Well ID: (Y)LJ -. _ _-� Well Lacked; (OYES / NO / Flushmount )
Well Diameter: a Construction: (' /SteeI/Stainless Steel)
Total Well Depth: W - � 0 ft
Static Water Level: 0 .'3-Q it
Height of Water Column: �1Oft
Multi Facto?: C? • 1103 C(Radius/12)2 x 3.14 x 7.48].
Casing Volume: G .7 5,� gallons.
Cal. 3 Volumes: 0�0 a �� gallons
Pump Intake: 3 �i • QQ ft
Purge Information
Date Purged: 14 / j::� Start:_( L'IQ _Finish: )`1 Purge Rate: 1
Q)dE LP
Purging Method: e n S �,et l 1-i C 7 Lm4 Total Volume Purged: _ .1 i✓ 9 O (gallons/ t>�s L)
Salrtpling information
Date Collected:_1 D/_�W a-Q Time Collected: ` � (am
Sampling Equipment Used:_ _ fit?�,5l [c _ VLlnstrument ID: 5..� Q�nnL., S# n�iO� fY1��snrOwd'`34i
Bottle Type Preservafi6n Analysis Required
Field Measuremerit Obsery tions
Sample Temp (OC): Time:I L�'-JS_ � Turbidity (ntu): ', , �j �� Time: � `"I `l
Dias Oxy (mg/L): .L4 Time: '--i LIc_Fe 2t mg/L: - O Time:. 1 Ll `-t (�
--Specific--Cond:-(--u — _L - T-ime: `1"[ Res. Cl{mg/L)/(ug/L) a` - T=ime:. - �"`- ---- - ----- - - -
Sarnple pH (s.u.): 6 oZ Time: I `-I `I S- Odor: Lc_nd Ft 1 Time:i-
ReDox (mV): -- `'� _ Time: l '-I Appearance: Time:
ReDox (1H value):YSI ProPlus +200rttV L 5�-.) Other: Time:
General/Weather Observations:
unny cloudy/rainy) Temp.(°F) Wind�_(mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(oq
Diss Oxy.
(mg/L)
Spec'
Cond.
S •
PH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons
L
Water
level (ft)
Other
II
�s
t u1
I
-tip.
t_-} 1
5-, 3 Q�—_

C9.'Vk?fJleal$
Document Iderne: Field data Sheet
Date Issued: March 8, 2019
Page: 1 of_i
Document [dumber: F-CAR-FLD-001-rev.03
issuing Authority: Pace Huntersville Quality.
Office
Field Data Sheet
Name and Affiliation (Sampler(s): _ E- Q��c - Anal—f-I ov,� Field Data Sheet Review:
Name and Affiliation (Inspector): rvI
Well Information Date:1 l
Well ID: �Yl,� - 6 - i `� a Well Locked: (YM / NO / Flushmount )
Well Diameter: 4 Consttuction: &V /Steel/Stainless Steel)
Total Well Depth; ) q .l 5� ft Multi Factor*: 71 [(Radius/ 12)2 x 3.14 x 7.48]
Static Water Level:- it Casing Volume: a�� Q gallons
Height of Water Colurnn; L b6 - it Cal. 3 Volumes: gallons
Pump Intake; 17q • Qn ft
a 104 I- P
By: 0
Purge Information
Date Purged: 10 / `a - ./ -,)-0a Start: 1400 Finish:, Purge Rate: CY I (1
Purging Method: P"c TotalVolume'Purged: -)-QDQ (gallons/(E�L)
Sampling Information
Date Collected:j;//. OHO Time Collected: ��a�" (am/bm)\
Sampling equipment Used:f o5ha L-\A i Instrument ID:_ ,l S� cm" n�lf o fk /C n (rcxt P-L-) tp'3c }
Bottle Type Preservatl6n Analysis Required
A f1 o T (Ylc 1-al',; t:v M!
Field Measur tnen Observations
Sample Temp (°C): Time: Turbidity (ntu). Time:.
Digs Oxy (mg/L): C� �'b Time: Fe 2+ mg/L: 3 >0 Time:. 1(o
Time:. ((, �5�_ Res. Cl m L L---T-ime:. ----Specific--Coed: (uS): �-i�-� � � _ _ - _ _ _ ... ( g/ }/(ug/ )' - �- - - -- - ---- - _ -
Sample pH (s.u.): Time: ] l3� ��. Odor: 5u l C-t/<- _Time: ) 6'Yt�
ReDox (mV): 33 ' _ Time: 16 Appearance: _� � .0 Time:_
ReDox (EH value):YSI ProPlus +200mV 1 .5 Other: Time:
General/Weather Observations:.
- (unn /cloudy/rainy) Temp.113 (°F) Wind 3 (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(°C)
Diss Choy.
(mg/L)
Spec'
� S) .
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/ fq/
Water
level (ft)
Other
4
g,
�-
? .
-C),
6 .Lf
M! o
[.0
3
0
4.
1 o)
a- �-3.
6aa 1
Mt
0,6
451263
-13,S-
'a,
-20. 0

Document Name: Field data Sheet
Date Issued: MarctiL8, 2019
r aceAWfyffcal4 . Page: I of 1
Document Number: F-CAR-FLD-001-rev.03 Issuing Authority: Pace Huntersville Quality.
Office
Field Data Sheet Old
Client: B L 6 —Location: A Skcy; c Ip . to c Project #: 84 A 4 . L P
Name and Affiliation (Sampler(s): �'� 8 QQ/,Q. Field Data Sheet Review:
Name- and Affiliation (Inspector): jar A
Well Information Date: 11 3 ap�-0 By:
Well 11): L Well Locked: YES NO / Flushmount } '
Well Diameter. ? ;A Construction: (PVC/ eel/Stainiess Steel)
Total Well Depth: 6 -O 5 -it Multi Factor`: 0, ! b ? r(Radius/12)2 x 3.14 x 7.481
Static Water Level: (7 S ft Casing Volume: 0. 11 gallons
Height of Water CoIumn: 0.7 ft Cal. 3 Volumes: , 4. 7 3 gallons
Pump Intake: N A ft
Purge Information
Date Purged: '�j1��-- Start: Finish:-- Purge Rate:
Purging Method: TotalVolume'Purged: (gallons/cols/L)
Sampling Information
Date Collected: Time Collected: Tam/pm)
Sampling Equipment Used: T! Instrument ID:
Bottle Type Preservation Analysis Required
Field Measurements/Observations
Dins Oxy (mg/L):
Sample pH (s.u.):
ReDox
Time: Turbidity (ntu):
Fe 2+ mg/L: 1 Time:
—.._ s. (mg/L)/(K$/L):---
Odor: Time:
Time: Appearance:
ReStx� _(EH vaIue):YSI ProPlus +200mV Other: Time:
GeneraVWeather Observations: T n ,cr,i iuj Iry 1 a M8 of -wg49f P-o f-54 u.b,'fi Uc4 i sn +e,2 + /
(sunny c oud rainy) Temp.6-5--(°F) Wind O— � (mph)
Sampler Signature: -/ 8-5 - Date: to P
Stabilization Test
Time
Pu ed
Temp.
(°C)
Diss Oxy.
(mg/L)
Spy'
(US)
pH (s,u.)
ReDox
(MV)
Turbidity
(ntu)
Volume
removed
(gallons/mIs/
Water
ley
r
r�

p�
Document Name: Field data Sheet
Date Issued: Marc 8, 2019
eAnafyfrcal'
Page: 1 of
Document Numb& F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersvfile Quality
IIII
Office
Field Data Sheet
L
Name and Affiliation (Sampler(s): -VA—Z - Pace A nctf h (A
Name and Affiliation {Inspector): .
Well Information
Well ID: M lJ
Well Diameter: V�
Total Well Depth; of ft
Static Water Level:
Height of Water Column: I • S 1 it
Well Locked:
#:.SL-l(-nmbe o-Old LF-
:ld Data Sheet Review:
Date: Jj - 0 3 By:
/ NO / Flushmount )
Construction: (' /Steel/Stainless Steel)
Multi Factor*: (},10 r(Radius/12)2 x 3.ta X 7.as1
Casing Volume: S - �J- gallons
Cal. 3 Volumes: gallons
Pump Intake: It
Purge Information
Date Purged. 10 T / .aQ-r) 0 Start: Finish: Oq Q Q.. Purge Rate: 1 `i M 0 M 1 A
Purging Method:^ ,) L n,-_Total Volume Purged: 1 g Q O (gallons/@/L)
Sampling; Information
Date Collected:. i () . /-M/_ {Cl l Time Collected: (A N- (qFypm)
Sampling Equipment Used:�er�5�e,,�,4 �(- _Instrument ID: YSzi cn PCQ4 m Q Y� IM C(bTQW430�L�
Bottle Type Preservation Analysis Required
VQC
Z (,0s
Field Measurements/Observations
Sample Temp (°C): i Time: Ci�t�1 Turbidity (ntu): Timer QSC Q S7
DiSs Oxy (mg/L):. ......: Time: OFe 2+ mg/ Q Time: nGn
----Specific-Gored (uS).— 'a. ----Time: nq0Res, -Cl-(mg/L}/(µg/L): -- Time:,
Sample pH (s.u.): _, Time: Odor: N—h Time: 09 C�C—_.
ReDox (mV): Time: Appearance: 1 ee r Time: _ 4 ci O C
ReDox (EH value):YSI ProPlus +200=V a-h 2S ,6 Other: `- Time:
General/Weather
Sampler Signature
Stabilization Test
(sunny/cloudy/
Q
ph)
Time
Purged
Temp.
(°C)
Dtss Oxy.
(mg/L}
Cone.
tub) '
PH (s.u.}
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/ Is
Water
level (ft)
Other
15 '
a I
(A&,
6 ,
g .3 0
F Q,W
d e ce.Sed.
�a
I Ni-
rnrn�
a SS•

Document Name: Field data Sheet
Date Issued: March 8, 2019
C8 Analjdlcal a
-Pa : 1 of
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality.
�.
Office .
Field Data Sheet
A58io_cur .u,
Name and Affiliation (Sampler(s): Are 6 f U f
Name and Affiliation (Inspector): H /A
Well Information
Well ID: . Mwf - L3 ( 2 Well Locked:
Well Diameter: 2 ( n Construction:
Total Well Depth: _ ft
Static Water Level: Z ti. 6 `o ft
Height of Water Column: 112,AJ ft
Project #: old L F
rld Data Sheet Review:
Date: 1 �7l
By:
f NO / Flushmount }
eel/Stainless Steel)
Multi Factor: 3 ["Radius/12)2 x 3.14 x 7.48].
Casing Volume: l 2 gallons.
Cal. 3 Volumes: g 6 gallons
Pump Intake: — 13 ft
Purge Information
Date Purged. to / / .2o . Start: q _9 ; Finish: Q a3 Purge Rate: l aQ 0 1 A'
Purging Method:_rQ r r 5'fs"It -( Total Volume'Purged: 1A 1 00 (gallo /mis )
Sampling Information
Date Collected:_/W/ Z Time Collected:) 4 (am m)
Sampling Equipment Used: P r i dal } � to rip Instrument iD: 'V 05 b
Bottle Type
Field. Measurements/Observations
Preservati6n
Analysis Required
tANA
Sample Temp (°C): 17 a Time: OR y 0 Turbidity (ntu): 5 Time: Dol 4 0
Digs Oxy (mg/L): 0 Time: Fe 2t mg/L: �� ^Q Time: 11 IND on t M/ 4/ 2�
i V 4 /20
--S ecific-Cond (uS) -. a �.�i --Time: --.. Res. Cl (mg/L)/(µg/L):
Times .
Sample pH (s. u.): -7 • Time: Odor: 7.. t 0A f 5 a t r-tt' Time: O q u 0
ReDox (mV): 1 27_ Time: Appearance: Time:
ReDox (EH value):YSI ProPlus +200MV 7 2 . b Other: Time:
General/Weather Observations:.5 %,^f /G ox :d , 2e S- OS -tBr L OA k -C- �' ' f h +_ r
_ (sunny/cloudy rain Temp.-_(°F) Wind 4" 5 (mph)
Sampler Signature: R y 4n _9 Na5 Date: 10/ 2 a /Z 0
Stabilization Test
Time
Temp.Digs
Ox
Spec.
Cond.
pH (s,%)
ReDox
Turbidity
Volume
reinoved
Water
Other
Purged
( q
(mg/L)
(US)
(mV)
(ntu)
(gallon,m e
level (ft)
360
1 -7.4
-34.3
2
5,,9
z2,2-0
Dw�
ll�.l
2.L
3bb.-A
7
-Sw.
►ti.�
50-0
27,2Q
5o^titS��.
og5�
Ib•5
I .7i
552-6
-ka-lk
300
7-2.3
Ogoo
1 .q
0,96,
501.
7, t
I.3
13o0
�2.4
� 30
1 Vig
1 4.1
4 "
7.
ZI.3
1 5.6
17,00
22.5

s
Client: Q LE
Location: A 4%,ev; t f e-
Project: ut r, L CO. O 1
well lb: jA vl— 13 -- 13 Z
Reviewed Date and By: 3
Stabilization Test
Document Name:
Field Data Sheet
Document Number:
F-CAR-FLD-001.rev.03
Document Issued: March 8, 2019
Page 2 of 2
issueing Authority:
Pace I-iuntersvi& Quality Office
0.04138
1
G 3
,13. 3.6.
Spec.NOW
Cond.
Turbidity
(gallons Is/
_ , level
■ram
®�sr���

Document Name: Field data Sheet
Date Issued: March 8, 2014
taAnaliNca q
Page: 1 of I
Document Number. F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality,
Office .
Field Data Sheet
A 5 k2 vt t(/ � AJ G Project #:. 5umro e co • n LT --
Name and Affiliation (Sampler(s}:_ �5 �� �-� n� {e ��ret Field Data Sheet Review:
Name and Affiliation (Inspector): .✓y p Z�
Date:)
Well Information
Well ID: - k a- Well Lacked: ( / NO / Flushmotint )
Well Diameter: 2 k Construction: (EV�/Steel/Stainless Steel)
Total Well Depth: 4 ft
Static Water Level: it
Height of Water Column: , r ft
Multi Factor": % i 9 3 r(Radius/12)2 x 3.14 is 7.48]
Casing Volume: -3:93 gallons
Cal. 3 Volumes: ')� .�� _ gallons
Pump Intake: ' 9 , 2Q ¢t
By: 3A5
Purge lnforination
Date Purged-J-Q-/ 11 Start: - Q00Ltd Finish: I L) o S- Purge Rate: gQ fi't`o
Purging Method:_ �,IvR ___:rotaI Volume Purged: 1 570 (gallons mis L)
Sampling Infoxmation
Date CoUected: [j Time Collected: 19 10 aIi /pm)
Sampling Equipment Used: R L., Instrument 1D: YSr D nc� o).uS O-�"iJ6
Bottle Type Preservatid n Analysis Required
o
Field Measur tnera Observations
Sample Temp (°C): I b 'S Time:_ I Cl 1 Q Turbidity (ntu): Timer 1 a 1.0
Digs Oxy (mg/L): 1. S Time: c 10 Fe 2+ mg/L: N17 Timer^ I [] f. C
Specific-Cond (-uS) S-3 Time Res. Cl (mg/L)/(µg/L): Time:.
Sample pH (s.u.): _ t, 3 Time: I n 11 n Odor: ry Time: to 10
ReDox (mV): i �) 1, Q Tim e:.1q 1 0 Appearance: C i Time: (a to
ReDox (EH value):YSI ProPlus +200mV ''54 1 , C1 Other: Time: r'
General/4Meather Observations:
(sunny/cloudy/ (ain Temp.(°F) Wind -_(mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(°C)
Diss Oxy.
(m$/L)
Spec.
Cond.
(US)
PH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/ is
Water
level (ft)
Other
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1
Document Name: Field data Sheet
Document Number: F-CAR-FLD-001-tev.03
Field Data Sheet
Issuing
.d: March 8, 2019
e: 10�—. f1�
Pace Huntersvill,
Office
Name and Affiliation (Sampler(s): ?, M $ Po.c e,. F
Name and Affiliation (Inspector): 13 f A,
Well Information
Well ID: M t+V - 4 A Well Locked: ( YES
Well Diameter: "Z '1 Construction: (PVC
Total Well Depth. % 7. 0 O ft
Static Water Level: 0.5 3 it
Height of Water Column: Q,_ '7 it
#: go, 4 . CO. c td L P
Data Sheet Review:
Date: 1113 ��,0m By:
/ Flushmount )
tainless Steel)
Multi Factor*: (7 3 ['(Radius/12)2 x 3.14 x 7.481
Casing Volume: I "s y . gallons.
Cal. 3 Volumes: 4 . & 3 gallons
Pump Intake: 7 5 ft
Purge Information
Date Purged: 10 / 'LS ./ 10 Start: 11`00, Finish: 11 O Purge Rate: 1201"1"'r1
Purging Method: 6 Io. 1 rice- ?,, Total Volume'Purged: 3 000 {gallon
Sampling lefftmation
Date Collected:._Ao. 7 Time Collected: It 3 S {am m)
Sampling Equipment Used: 131ad ter -Pk M V _ Instrument ID: Y�f OS TP tv OQ
Bottle ''Type Preservation Analysis Required
NCApp. T
Field Measurements/Observations
Sample Teinp (°C): 17 q Time:
Digs Oxy (mg/L): 2 7 Time:
Specific Cond. (uS):--_. J LI0 � . �— Tim- e:
Sample pH (s.u.): 'Z
• � Time:
ReDox (mV): L•l • `� Time:
ReDox (EH value):YSI ProPlus +200mV_
General/Weather Observations: .
(135 Turbidity (ntu): 1-0. Time: 3 5
Fe 2+ mg/L: Time:.
Res. Cl-_--
Odor: 6+ t0hq 3: d-. n Time: 113 5
Appearance: L t Q- r - Time:
b 0. Other: Time:
(sunny/cloud
Sampler Signature: R y dL ix _ g y & 5 Date: O / 2 $ l27
Stabilization Test
Wind " 5 (mph)
Spec'
Volume
Time
Temp.
Diss Oxy.
Co)
pH {s.u.)
ReDox
Turbidity
removed
Water
Other
Purged
(°C)
(mg/L)
(mV)
(ntu)
(gallons mIs
level (ft)
2,1
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Document Name:
Ar / Field Data Slieet
Document Number,
F-CAR-FLD-001',rev.03
Client: 0 LC
Location: A" hem: lie., N C
IB,t(,( Co. j0 I cl 1. F
Project:
10 2S 2.0
Weil 0: /4 w-q A
Reviewed Date and By:
stabilization Test
Time Temp. Diss Oxy. Spec,
C
Purged (00 (mg/L) ond.
I I (us)
Document Issued: March 8,2019
rageZof Z
issueing Authority,
Pace Huntersville Quality Office
O.A.G91
0-1,60.0
4
0.65
2.6100
Turbidity Volume Removed Water level
pH (S.U.) ReDOX (MV) (ntu) (gallonse,
I I I circle one
1125 117. q 1 2. -7 1547(7 1 -250,0 l -owl,
kk310 I 17.q 1 2. ik 1 300.0 1 1
Other

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�
Document Name: Field data Sheet
Date issued: March 8, 2014Pa e: 1 of
.
Document Number: F-CAR-FLD-QOl-rev.o3
issuing Authority: Pace Huntersviiie Quality,
, Office .
Field Data Sheet
Client- Lf
Location: A 5 WA/j b(2 JProject #: .
Name and Affiliation
,QnF��ce.,i Field Data Sheet Review:
Name and Affiliation (inspector): n
14
Date: ~ ��'- �� By:
Well Information
Well1D:.
Well Locked: Yp, / NO / Flushmount) '
Well Diameter: a "
Construction: (iM/SteeI/Stainless Steel)
Total Well Depth:. _) b �-� —ft
Multi Factor: Q j 6 3 . [*(Radius/12)2 x 3.14 x 7,48]
n
Static Water Level: (Lt•LAI ft
Casing Volume: I 1,03 gallons.
Height of Water Column: � - ft
Cal, 3 Volumes: Cq °j gallons
Pump Intake:
Purge Inforinati'on
Date Purged: I D / 53 /Q
f
Start : _ �.a _ Finish: )� Purge Rate:r�
Purging Method: ... tg d d_& 7,
rnn. Total Volume'Purged: (gallons/X (L)
Sampling Information
Date Collected:. 1__/,Z/ 'A-ozl;n Time Collected:-- I�__ (am/M
Sampling Equipment Used:_Met et d 1�c Instr-urnent1D:__Y<r
Bottle Type Preservation Analysis Required
A ,n n L \ici(,-+- 'MR [ n l�
rm N
Field MeasurementsjObservations
Sample Temp (°C): 1 3 Time: 13 w 5 Turbidity (ntu): .3 Tim& 13 ti t�
Diss Oxy (mg/L): Time: Fe 2+ mg/L: 1 ' S Time: �' +
S ecific_Cond._ uS. M-Oi L `--� Time•- - - Res. C1 m L L . Time;..
Sample pH (s.u.); # w Time: I -, LK . Odor: - S -0 Cc.C'" Tithe: 13ti,4`
ReDox (mV): _ _ -- ' -t l • 4 - _ Time: ]"ice r Appearance: S)t�i4 •, d twL, Time: 13•-t�
ReDox (F.H value):YSI ProPlus +200nnA - 5�3 . 4� Other: Time.
General/Weather Observations:_ . 50" p('e de -J/ �L'b I A ;�' .
Sampler Signature
Stabilization Test
/cloudy/o� Temp. Y ff) Wind 3(mph)
.te: ) Q 2tQ�) n ^
Time
Purged
Temp.
(°C)
Diss Oxy.
(mg/L)
Spec'
Con )
pH (s.u,)
ReDox
(m.V)
Turbidity
(ntu)
q ume
removed
(gallons/
L
Water
level (ft)
der
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De,3 7
`rt
Jl
S
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Document Name:
Field Data Sheet
Document Number;
F-CAR-FLD-OM,rev.03
Client.• L E
Location:-. As�v Vi I L"'UC
Project: E-A r,( c" M- � fl J_ LP
Well I b:
Reviewed Date and By: zo
Stabilization Test
Document Issued: March 8, 2019
Page ;W ?_
Issueing AadioritY;
Face Huntersvitle Quality Office
weit oiamEU-1
NitUtip-licabein Facbor'
GAON
2
0-1.63-0
4
0,65,30
6
A6.8.0
•Spec.
Cond.
Turbidity
(gallons/V�L)
Water level
(u 5)
(ntu)
circle one
(ft)
mom
0
SIMI
M,
ml
IMP

Document Name: Field data Sheet
Date Issued: March 8, 2019
acer'Irlydlcal'
Page: 1 of
Document Numb4m P-CAR-FLD-001-rev.03
Issuing Authority; Pace f3untersville Quality-
,
Office -
Field Data Sheet
L
Name and Affiliation (Sampler(s): _TTZ --{7ac L Araa,luk-,-a,�
Name and Affiliation (Inspector): N 1 A
Well Information
Weil lD:
Well Diameter:
Total Well Depth: 75 3cft
Static Water Level: S_'7 ft
Height of Water Colurmal `i-' ft
#: -. 0I J V
Data Sheet Review:
Date: i i • 03 - �-o By: 30
WellLocked: / NO / Flushmount )
Consttuction: Steel/Stainless Steel)
Multi Factor*: Q -1:3 [*(Radius/ 12)2 z 3.14 x 7.481.
Casing Volume: gallons
Cal. 3 Volumes: y , -gallons
Pump Intake: 123, S C ft
_Purge Information _
Date Purged: 1 / a$ ./ ao Start: ` 1� Finish: 1 S'-1 Q Purge Rate. —I Oa rrk i Mtn
Purging Method:_ pi rt5h��1 i ` TTotal Volu-me'Purged: -10 (gallons/ l /L)
Sainvlin¢ Information
Date Collected jQ /M/ Time Collected: 1 S_•-- 'J (am/Cm)
Sampling Equipment Used: IhstrumentID: flao6 I�/1cLcClrQw�3o j
Bottle Type Preservati6n Analysis Required
A tzLii f.QL5
Field Measuremerits/Observations
Sample Temp (°C): `� Time: IS-4 4 Turbidity (ntu): $ ' t Time:' -
Digs Oxy (mg/L): Time: IS Q C Fe 2t mg/L: Nb Time:
1-1T4 Res. Cl m L L Tizxte:- ,- — --Specific- Cand u5 ��4— -----T-ime: -- ----
P ( )
Sample pH (s.u.): Time: 1 s`'dS~ Odor:. njD
ReDox (mV): Time: Appearance: G2 �e cr Time:
ReDox (EH value):YS1 ProPlus +200mV 11 Other: - — Time:
GeneraMeatherObservations:
.1�'..fIFa�1o4�re�-
(sunny/c udy/ iny) Temp. ff) Wind (mph)
Sampler Signature:_
Stabilization Test
Time
Purged
Temp.DiSs
( q
O
(mg/
Spec.
C Sd.
(US)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
remove
(gallons Is/
Water
level (ft)
Other
I-1• I
'777N
I
13 .S
Soo
i$
-�
1ti
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2006
X -o

Document Name: Field data Sheet
Date Issued: March 8, 2019
Pa e: 1 of
iceAnaIWeal'
Document Number. F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality.
Office .
Field Data Sheet
Client: `6LE „Location: AJC PYoject
Name Ymd Affiliation (Sampler(s): 111-Bx2,-q-n-NCO(! Field Data Sheet Review:
Name and Affiliation (Inspector): j j A --- Date: 11- 0 3 By: %5
Well Information
Well ID: C8 w - .a Li Well Locked: (7L� / NO / Flushmount) '
Well Diameter: �y� Construction: ('V /Steel/Stainless Steel)
Total Well Depth: Lk-T . Li ( -it
Static Water Level: ` -q .11 it
Height of Water Column: Q � a ft
Purge Information
Multi Factor':_ r(Radius/12)2 x 3.14 x -48)
Casing Volume: 0.0 f gallons.
Cal, 3 Volumes: gallons
Pump Intake: . ft
Date Purged: �- / / .` Start: Finish: Purge Rate: -
Purging Method: J Tot'dlVolume'Purged: (gallons/mis/L)
Sampling Information '
Date Collected: / `--/ Time Collected: s (am/pm)
Sampling Equipment Used: Instrument ID:
Bottle Type
Field Measur ments Observations
Pre-servatibn
Sam Tem (°C): Time: Turbidity (ntu):
Diss Oxy (mg/L): Fe 2+ mg/L:_
-- ----- -Specific--C-=ond (uS). - - ---Time
Sample pH (s.u.):
ReDox (mV): ,
Time: Appearance:
value):YSI ProPlus +200mV Other:
General/Weather
Sampler Signature
Stabilization Test
v
(sunny/cloud rainy
Analysis Required
Time:
Time:
Time:
Time:
mow, M..,
f -
f f
NO.-
10
Tf
removed
0

�� aceAfV1j1flC`?l y
Document Name: Field data Sheet
Date Issued: March 8, 2019Pa e: 1 of �
Document Number: F-CAR-FLD-001-[ev.03
issuing Authority: Pace fiuntersville Qualify.
Office .
Field Data Sheet
Chem. Location:. 4 l(.p, AJ4L Project #&U rnV?,a Co 01d L F
Name and Affiliation (Sampler(s): :�Y T7Z- - PLA � Q. A, on f Ca. Field Data Sheet Review:
Name and Affiliation (Inspector): Date: i 1 ' � `�
Well Information By:
Well ID: N) w -5 Well Lacked: Y / / NO / Flushmount )
Well Diameter: a " Construction: (VC/Steel/Stainless Steel)
Total Well Depth: IIL40 ft Multi Factor*; f r(Radius/12)2 x 3.14 x 7.48]
Static Water Level:. 4 ' ` ft Casing Volume: 3 S gallons.
Height of Water Column: ('�o 3Q ft Cal. 3 Volumes: a • y V gallons
Pump Intake: a 1 Q ft
Purge Information
Date Purged:I a. /. CA . /)�QtZ Start: (J jL3.: Finish:_ Purge Rate: n L tY m
Purging Method: P,�,rfb�a4iC. �-nTotalVolume'Purged: ``i"o (gallons/(&DL)
Sampling Information
Date CoIIected: I n Time Collected: oq H' m pm}
Sampling Equipment Used: - Pe mil)-et iAC: _ :_Instrument TD:"(S-r- n 1 u 5 �k n �, i Ms u��t•�� jc)}�
Bottle ''Type Preservation Analysis Required
r
L _0,oxcrip_
Field Measurements/Observations
Sample Temp (°C): Time: Cif Turbidity (ntu): 4 1 Timer oS �tm
Digs Oxy (rrtg/L): Q , Time;Gt�-I Fe 2+mg/ L:- ,Time: omits tIZ—
Specific Cond. (uS): VI-Q, .. Time: 99 tiRes. Cl (mg/ L)/(µg/L): Time: ,
Sample pH (s.u.): ,3 Time: C� C) `tip_ Odor: Time: "4.—
ReDox (mV): _ - 75.). f Time: a ' `,l Appearance: 0 ecf Time; c,Rg r
ReDox (EH value):YSI ProPlus +200xnV Other: — Time:
General/V1leather Observations: �'l���( —6 . wf
(sunny/cloudy/ ail) Temp. (°F)
Sampler Signature
Stabilization Test
Ph)
Time
Purged
Temp,
(°C)
Diss Oxy.
(mg/L)
Spec.
{u5)
pH {s.u.)
ReDox
(mV)
Turbidity
(ntu)
o ume
removed
{gallons/ is
Water
level (ft)
Other
la
1,
�
. a
� a,
aoo
,,
ao ,'b
l00
R., Ck
O.
o,m
a l
o ,3
6ci Ll

ZaAnalyticaf
Client: G LE
Location: A Ska U,
Document Name:
Field Data Sheet
Document Number:
F-CAR-FLD-00I.rev.03
Project: a Cc1CQ . alA L�
Well ID:
Reviewed Date and By: 23
Stabilization Test
Document issued: March 8,2019
Page )Of '-)—
Issucing Aadiority;
Pace Huntersville Quality Office
...........
�W all
tipltcaki,= Facboe IW
WNW,
1.2
0.09V15
1.,625
01,1080
0.5-673-
4
0.65:30
1.4680
•
Spec.
Cond.
Turbidity
(gallons mls L)•
Water level
(US)
circle one
I . "IF
01. "11I.E.
W.
I "IF

Document Name: Field data Sheet
Date Issued: March 9, 2019Pa e: 1 of
ace�lyff�al"
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersvilie Quality,
�.
Office
Field Data Sheet
&6,A ((ag it�C Project #: Co o (d LP
Name and Affiliation (Sampler(s): = — ?a ca_. !4 n a.L iY co` Field Data Sheet Review:
Name and Affiliation (Inspector): ti
Date: '11- 4`I By:
Well Information
Well. ID: tVl. Li WeU.Locked: "S / NO / Flushmount )
Well Diameter: a n Consttuction: (I V�/Steel/Stainless Steel)
Total Well Depth: . H 0 __ft Multi Factor*: 4 3 r(Radius/12)2 x 3.14 x 7.481. a
Static Water Level: L .• 0 S ft Casing Volume: S gallons.
Height of Water Column: lQ _"3 ft Cal. 3 Volumes: .t-t gallons
Pump Intake: ti 4 ft
Purge Information
Date Purged: 1(2t / X? / ')-Q Q Start: - [t�5_ Finish. Purge Rate: --A &LL-luo
Purging Method: 17u viR Total Volume Purged: � oo (gallons/ 1o/L)
Sampling Information
Date Collected:. `��'$' �_=/ Time. Collected: (am/pm)
Sampling Equipment Used: Instrument 1D: _ sr� QLAc W a La�M_ rccdrP to t*-30-�,- j
Bottle Type Preservation Analysis Required
Field Measurements/Observations
Time: Turbidity (ntu):
Dias Oxy (irtg/L).
Fe 2+
- Specific Cond. (uS)
Time: Rest
Sample pH (s.u.):.
Odor
S
Time:
L): Time:
ReDox (mV): Time: Appearance: T1'i
ReDo alue):YSI ProPlus +200mV Other: Time:
General/Weather
Wind —(mph)
Sampler Signature
Stabilization Teat
Time
Purged
Temp.
( q
Diss Oxy.
(mg/L)
Spec'
Con) '
PH (s,u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/1F /
Water
level (ft)
Other
►ia
-
D�_4
1
-ax\
3
oo
4.'213
1 ou
Crc d.
L
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1,.,,
Document Name:
Field Data Sheet
Document Number:
F-CAR-FLD-001.rev.03
Client:
Location: . A-C"V r 4
Proj ect; BSA. (�c n r,,,l bz Cg . (A I A L
Well lb: —(Y " 6
Reviewed Date and By:
Stabilization Test
Document Issued;- March 8, 2019
Pag4of - -
issueing Authority:
Pace Huntersville Quality Office
A
1.46.8.0
Time•Spec. Turbidity Water level
Purged Cond. (ntu) (gallons/(Ps L) (ft) I
(US) circle one
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Document Name: Field data Sheet
Date Issued: March 8, 2019AnaPa
J C@l�1 s
e: 1 of
Document Number. F-CAR-Fi D-001-rev.fl3
Issuing Authority: Pace Huntersville Quality-
t
Office
Field Data Sheet
Name and Affiliation (Sampler(s):�,IR - -Ra Lv Aca- ��
Name and Affiliation (Inspector):_ . ns i A
Well Information
Well ID; ice?"� �- ti 3 Well Locked:
Well Diameter: . �_ V�
Total Well Depth: ft
Static Water Level: a 1 a ` t ft
Height of Water Column: 1 q� it
#:_Fci cocvilae CQ-n1d Lr
1d Data Sheet Review:
Date: ]J - ('3 --7,0 By: V' 'r
NO / Flushmount )
Construction: (1�/Steel/Stainless Steel)
Multi Factor*: 0. I A 3 r (Radius/12)2x 3.14 x 7.491
Casing Volume: 1 'q, 9 gallons
Cal. 3 Volumes: 6' 6 gallons
Pump Intake- 3� 5� ft
Purge Information
Date Purged: 10 2210 Start: ) S) 15 Finish I o L4 a Purge Rate: 270 nas--�
Purging Method: Rl (19h1tr "sc= f _Total VoIurne Purged: W 000 (gallons/�/L)
Sampling Information
Date Collected; f Q /a 1/gip Time Collected: j �1 ! �� (FYpm)
Sampling Equipment Used. 1 as r C,* Instrument ID:
Bottle Type Preservatimn Analysis Required
Field Measuretnents/Observations
Sample Temp (°C): .) fl - Time. j CMS' Turbidity (ntu): � • i Time:' 0
Digs Oxy (mg/L), �-'•� _ Time: _S-Q-LI - Fe 2+ mg/L:
Specific- Cond. (uS): -- Time:. ) n Y fi Res. C1(mg/L)/(µg/L):
Sample pH (s.u.): 3 '3, Time: Odor: Time:
ReDox (mV): _— �S Time: 0 1--1 Appearance: U. Par- Time: 10
ReDox (EH value):YSI ProPlus +200mV t"3t-1 . Other: °J Time: `—
General/Weather Observations:_Paq cg¢ r ye
(sunny/ ou /rainy) Temp. (°F) Wind ---(mph)
Sampler Signature: Date:
Stabilization Test
Spec.
Volume
Time
Temp.
Diss Oxy.
pH (s.u.)
ReDox
Turbidity
removed
Water
Other
Purged
(OC)
(mg/L)
(US)Cond
(mV)
(ntu)
(gallons/ tI /
level (ft)
W,L
-31
1-1).
1 a �
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Document Name:
Field Data Sheet
Document Number:
F-CAR-FLD-001,rev.03
Client: S -L, 7:!-
Location, 45,)rnr k �V-
Project: C-nr,CQ- C) ( Ct t, F
Well ID: L-i c2)q-
Document - Issued: Mardi 8,2019
Page ?lf?—
Issueing Authority;
Face Huntersville Quality Office
1.2
0.0-915
1.625
0.1-630
4
.0,:65W
Reviewed Date
Stabilization
and By:
Test
Temp.
('C)
Ct
ReDox (mV)
" 1
7—
11
75p e c.
CO nd.
Cond.
(us)
(LL S)I
Time
Purged
Turbidity
NOWNF—
(gallons/fEWL) �
circle one
.
Water level
(ft)

Document Name: Field data Sheet
Dare Issued: March 8, 2019
@i:er4l7F1fyFfCa1 z
Page: 1 of
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace HuntersvilTe Quality.
_.
t
Office -
Field Data Sheet
0
#: vf,cgc CO, ala L"--
Name and Affiliation (Sampler(s):_%� - c_-e A -c%2, Isere( Field Data Sheet Review:
Name and Affiliation (Inspector):. "I A Date: 03 - Z.a By:
Well Information
Well ID: M '- Well. Locked: {(Y / NO / Flushmount )
Well Diameter: a Construction: (I �`C` /Steel/Stainless Steel)
Total Well Depth: �Q-00 ft
Static Water Level::
Height of Water Column: S ft
Multi Far tor*: Q ,1 G 3 r(Radius/ 12)2 x 3.14 x 7.481
Casing Volume: �, .-�-O gallons.
Cal. 3 Volumes: J S - gallons
Pump Intake: 5T VO ft
Purge Information
Date Purged: K) / 19 . / D 0 Start: 1.1 Finish: Purge Rate: �
Purging Method: Ca i7,., rn�-_ Total Volume Purged: , � � Q � �1
{gallons/ Is L)
Sampling Information
Date Collected: Cl /2v'aa-1)p Time Collected: -)�
Sampling Equipment Used: _ De -A; -Cad ea 7 _Instrument ID:_ YSs n �r, n In, s n ,� 4lY4rrt 7°I P� ? �?
Bottle Type
Preservati6n
Analysis Required
4-F- V Cl S �---&
Field Measurements Observations
Sample Temp (°C): Tune. 0,-i O Turbidity (ntu): i Time: h-L- 0
Digs Oxy (mg/L): ; Time: 0 Fe 2+ mg/L: Q Timer
--- Specific Cond.-(pS): -S S- Time: l O _ Res.
Sample pH (s.u.): Time: Odor: �Jb Time: l
ReDox (mV): _ 5 _ Time: 1 �� 1 �l _ Appearance: - Q e.c<-- Time: _ I 4 n
ReDox (EH value):YSI ProPlus +200mV S1M . Other: Time: \ )-!IQ
General/Weather Observations:_,QM )nIA,Ca a-etss�,,l��U
(an ne (e ( tiny/c ou /rainy) Temp.-�(°F) Wind f (mph)
Sampler Signature: Date:. )Q���� f1
Stabilization.Test
Time
Purged
Temp.
(oq
Dtss Oxy.
(mg/L)
Spec'
(S)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/�rils�
L
Water
level (ft)
Other
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1
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Client:
-J 01---
Location: . A �Ze A -)(-
Document Name:
Field Data Sheet
Document Number:
F-CAR-FLD-001.rev,03
Project: . oU L
Well ID: M W 12 - 6 O
Reviewed Date and By:
Stabilization Test
Document Issued: March S, 2019
Page ) OQ—
Issueing Authority,
Pace HuntersvWe Quality Office
t
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4
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Document Flame: Field data Sheet
Date Issued: March 8, 2019
page: 2-
aceAlnalyfIcal z
1 of
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality.
--
Office .
Field Data Sheet "
Client: 1�, ✓<� _! `Location: �v vdi¢. a_C PYoject #;J�v.n a-,r,- Re Gc). 01 d LLF
Name and Affiliation (Sampler(s): ~ ?4c.e . A-ny�Fs cel Field Data Sheet Review:
Name- and Affiliation (Inspector):
Well Infvrrnation Date: ��, 03��© By: W}
Well ID; M +,� Well Locked: 5'TI/ NO / Flushmount) '
Well Diameter:
Total Well Depth:
Static Water Level: O.,C)Oft
Height of Water Column: « it
Construction: ('�/Steel/ Stainless Steel)
Multi Factor*: 0 �l 63 [*(Radius/12)2 x 3.14 x 7.48].
Casing Volume: gallons.
Cal. 3 Volumes;" -gallons
Pump Intake: ft
I.urge Information
Date Purged: I_/ _ 9 . / IM A Start: Finish: I Purge Rate: ! n 0 r n L l r)
Purging Method; ` e ci s�n;1 k � c �u-nn o ,_Total Volume' Purged: i0 O (gallons/�L)
Saftling Information
Date Collected:. ! n // a�o�g Time Collected: 1 S 3C1 (am
Sampling Equipment Used: 2P S lbc ,_Instrument ID: Y 5r (f
Bottle Type
Field Measuretnerits/Observations
Preservatf�n
Analysis Required
Sample Tetap (°C): Time: S-') - Turbidity (ntu): 0 Timer i S'3cl
Dias Oxy (ing/L): Q a Time: 1 .0 Fe 2+ mg/L: �i �_ - - Time:.
--------SpecificCond.-(uS) 4 � --Time:- -�5_3o Res. Cl--
Sample pH (s.u.): Time:16L Odor: !,,JD Time:
:YY& l0WO
ReDox (mV): —rid. `�' Time: 1 Appearance: Time: I S"- Q�
ReDox (EH vaIue):YSI ProPlus +200mV 1 CA � c\ Other: __- Time:
General/Weather
R {Cy/r(u /rainy) Temp.(°F) Wind I � (mph)
Sampler Signature: Date:
Stabilization Test
Time
Purged
Temp.
CC)
Diss Oxy.
(mg/L)
Spec.
(S)
pH (s.u:)
ReDox
(mv)
Turbidity
(nta)
Volume
removed
(gallons/�
Water
level (ft)
Other
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Document Name:
Field Data Sheet
Document Number:
F-CAR-FLD-001.rev.03
Client: 16 0-1
Location:
Project: B L,_Il LCl av�h n L P ---
Well ID: M VJ - I7T---
Reviewed Date and By:
Stabilization Test
11`a�`�-° N fl5
Document Issued: March S, 2019
Page�-of�
Issueing Authority:
Pace Huntersville Quality Office
1_.625
GAGED
fi.
-IA6&a
Turbidity
Water level
circle one
IMF ms
i
iI
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Document Name: Field data Sheet
Date Issued: March 8, 2019
ca rrrifs�ieaf
PaLe: 1 of_?,
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality.
r
Office .
Clienf: 9L.V-7 _ Location: k. t.c.., V ,. Project #: c c(1 s��C�. C) i J `P
Name and Affiliation (Sampler(s): �J�--- Li 0- A cAL It W Field Data Sheet Review:
Name and Affiliation (Inspector): A _^ c
Well Information Date: 1I - O �_O By:cV
Well ID: (\,o (r! Well Locked: ( / NO / Flushmount) '
Well Diameter: �� Construction: (P C/Steel/Stainless Steel)
Total Well Depth: \ft Multi Factor'`; 0 1 0 3 ['(Radius/12)2 x 3.14 x 7.481
Static Water Level: ( Cl _• '�_Q ft Casing Volume: 1 16H gallons.
Height of Water Column: bS a� ft Cal. 3 Volumes: j • "i -gallons
Pump Intake: '+0-Cl ft
Purge Information
Date Purged: 10 'a`! / ;�Q StartFinish: tiro n[� Purge Rate: )`10 L1d`^"}
Purging Method: 112dbr ^Tot al Volume'Purged: �� (gallons /L)
Sampling Information
Date Collected: i /`% q--c1 Time Collected:__1ll c)CK (am/gmj
Sampling Equipment Used: 13t R J &a_f nou,^InstrunLent ID: VSY r), a5 ti�0�n�� IwCcrr y
Bottle 'Type PreservatU)n Analysis Required
Lea NA
Field. Measurements/Observations
Sample Teglp (OC): Turbidity (ntu): Time i 7n
Dias Oxy (mg/"L): 1. Time: Fe 2+ mg/L: Time.,. \ -�-nC'
----Specific-Cond. (uS): 4--7.....,....--Time: , ._. _10Res. CL(mg/LY(µg/L): j: .-Time:.
Sample PH (s.u.): - 6, O Time: � Odor: N [ Time: �n
ReDox (mV): '-C - � Time: AD:05-': Appearance: _ G 1 t. c�, { Timm:
ReDox (EH vaIue):YSI ProPlus +200m.V 19 `- - Other: — Time:
General/Weather Observations:
nM /cloudy/rainy) Temp. `(°F) Wind g (rnph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(pC)
Diss Ozy.
(mg/L)
Spec.
t S)
pH {s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
reinoved
(gallons/ n�/
L
Water
level (ft)
der
vg
C1 ,
a,&
.----
1�.Q
i
1� r�
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--�% Document Mane:
-act Analytica14 Field Data Sheet
Document Number;
F-CAR-PLD-001.zev-03
Client: IR L IF —
Location:
Project: 0, LP
Well 10: M L'i -
'Reviewed Date and BY:
Stabilization Test
Document issued: Mardi 8, 2019
Page�If�--
Issueing Authority:
Pace Huntersville Quality Office
If Ve .1-1. Di am tr-r
Fact=A
1-625
A
1.46W
Time Temp. Diss Oxy, Spec. Turbidity L Volume Removed Water level
Purged Cond. pH (S.u.) ReDox (mv) (n1u) (gallon I!n Is/L) (ft) other
(00 (mg/L) circle one
(us) I
0

ical y
Document Name: Field data Sheet
Date Issued: March 8; 2019
Page: e: 1 of
Document Number: F-CAR-FLD-001-rev.03
Issuing Authors: Pace Huntersville Quality.
r.s aCeAMIJ1
s
Office
Field Data Sheet '
Clienf: R� _ Location: AS1�y f (o., /NC Project #: 13unco Ax-L, Q I eA LC -
Name and Affiliation (Sampler(s):_ !" - J1 c2- A,�c, Nkc L(
Name and Affiliation (Inspector): M A
Well Information
Well]:D: . ry).W •--'IWeU Locked:
Well Diameter: __ `a µ
s.35
Total Well Depthe -it
Static Water Level: olal•5 it
Height of Water Column:-1 L 4 ft
Purge Information
Construction:
Id Data Sheet Review:
Date: 11 - O3 - 7-0 By:
/ NO / Flushmount )
Steel)
Multi Factor: 010 r(Radius/ 12)2 x 3.14 x -481
Casing Volume: G � 4 3 gallons
Cal. 3 Volumes: 4111 gallons
Pump Intake: a 3 � 01 f t
Date Purged:_ ID / 3 a / . -1021C.1 Start: U L-iS' Finish: Purge Rate: j 0 Q rO U M�`N
Purging Method: (.tiAzr�rw Total Volume Purged: 3 7 0 (gallons�L)
Sampling Information
Date Collected: - k Q /.h/ �-q-Cl Time Collected: j n � ai /pm)
Sampling Equipment Used:_ B3 ck.Jd-Re o Instrument ID: YS�.� Canf a Y � rn�e cut wtt-3a }�
Bottle Type
Field Measurements/Observations
Preservadin
Analysis Required
A V'r-y0 ry- t
I p -Lt �,-\ [IKcn�
Sample Temp (°C): l- l Time: 10 S—C) Turbidity (ntu): )4. ` Time:' 10 �-Q _
Dias Oxy (1ng/L): Time: E O '�-D_Fe 2+ mg/L:_ S. Q Time 1 0 �-C,
Specific Cond. (uS): Time:�.ClCl Res. Cl (mg/L)/(µg/L): — Time:.
Sample pH (s.u.): _` Time: i 02) Odor:
ReDox (mV): 4 ) Time: Q'7� Appearance: _ C-)z (' Time: l c) �-G
ReDox (l3H value):YSI ProPlus +200mVOther: Time:
GeneraVWeather Observations:.
(sunny cloud /rainy) Tesnp.LiY (7) Wind17- (mph)
Sampler Signature
Stabilization Test
Spec'
Volume
Time
Temp.
Diss Oxy.
.
pH (s.u.)
ReDox
Turbidity
removed
Water
Other
Purged
(C)
(mg/L)
� S)
(mV)
(ntu)
(gallons/� e
level (ft)
L
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13 A
100
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i
Client: c LEI
Location: A 6,1
Document Name:
Field Data Sheet
Document Number:
F-CAR-FLD-001.rev.03
Project: M)QL G - (�)� d LJ
WOO: M W.
Reviewed Date and By:
Stabilization Test
Document Issued: March 8, 2019
Page Pof -�-
Issueing Authority:
Pace Huntersvllle Quality Office
J 1.625
i
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Document Name: Field data Sheet
Date Issued: March 8, 2019
CeArzfj4kat'
Pa e: 1 of
Document Number: F-CAR-FLD-001-rev.03
Iss'ng Authority: Pace Huntersville Quality
Office .
Field Data Sheet
As 4 a V% 1(a, j (_ Project #: *JTUn en rya ac. C (o• oj6t LP
Name and Affiliation (5ampler(s): - PE�u- �4nal� k-c ceJ.l Field Data Sheet Review:
Name and Affiliation (Inspector):. .&21 A
Well Information Date: f 1 C� 3 " °l� By:
Well ID: . SW -DA et;
Well Diameter: 1 -
Total Well Depth: Et
Static Water Level: ft
Height of Water Column: ft
Multi Factor*: [*(Radius/ 12)2 x 3.14 x 7.481
Casing Volume: gallons.
Cal. 3 Volumes: gallons
Pump Intake: ft
Purge Information
Date Purged: / � ./ —start: Finish: � Purge Rate:
Purging Method: Total Volume'Purged: (gallons/mis/L)
Sampling Information
Date Collected: l 0 / L/ 00 Time Collected: } (a pm
Sampling Equipment Used: �Z2 t C _ Instrument ID:"y%ynp (,L4-Y 4L M0 f yl icOWL-i0 3
Bottle 'Type Preservation Analysis Required
Z vaCr
Field Measuretnerits/Observations
Sample Temp (°C): l�l �� Time: `� a4 Turbidity(ntu): Time:
Dins Oxy (mg/L): L—k Time: } `"i �.0 Fe 2+ mg/L: Time:
Specific Cond. (uS): L 4 -_;L Time:
� �
Res. Cl (mg/L)/(µg/L):
Time:. r
Sample pH (s.u.): _ q • 1 _ Time:
Odor: N
Time:.
ReDox (mV): 63, Time:
1'"� Q
Appearance: C. -ear
Time: ) `'t -0
ReDox (EH value):YSI ProPlus +2OOmV ab�a
Other:
Time:
General/Weather Observations: . i�l'S CooS'r 35 °�j�l S.a n►I _ ��� ��
, 615 `w_J
R
^_unn cloudy/rainy) Temp. T3
(°F) Wind (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(oq
Diss Oxy.
(mg/L)
Spy'
� S) .
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
o ume
removed
(gallons/mis/
Water
'level (ft)
Other

Document Name: Field data Sheet
Date Issued: March 8, 2019
page: 1 of _(
aceAnalyffeaT•
Issuing Authority: Pace Huntersville Quality.
Document Number: F-CAR-Fi D-001-rev.03
Office .
Field Data Sheet
F
Name and Affiliation (Sarapler(s) 17c, ,A h.c l,.l ea,t
Field Data Sheet Review:
Name and Affiliation (Inspector):
. LAA
p
Date: It - � 3 ' � By.
Well Information
Well ID: . S.J --�L-
urtt)
Well Diameter:--
ss Steel)
Total Well Depth:
ft Multi Factor; �
r(Radius/12)2 x 3.14 x 7.48]
Static Water Level:
ft Casing Volume:
w gallons
Height of Water Column: .r
ft Cal. 3 Volumes:
gallons
Pump Intake:
ft
Purge I iformati'on
Date Purged:
Start: "- Finish:
Purge Rate:
Purging Method:_
__ - Total Volume Purged: (gallons/mis/ L)
Smnyling Information
Date Collected: { % /._;)6./ -o-o o Time Collected: ) �i'`4 O (am/ m
Sampling Equipment Used: v-s,h Instrument ID: y <.c p co a(
Bottle Type Preservation Analysis Required
Field Measurements/Observations
Sample Temp (oq: cl 1 � c�- Time:_ I ­Jk G Turbidity (ntu): � ��-Time:, H�-A
Diss Oxy (mg/ L): Li 3 Time: N `--A Q) Fe 2+ mg/ L: ►.lid - --Time: f "L1Q.'
Specific Cond. (uS): a Oy • Q Time: 1 L1L-i0 Res. Cl (mg/L)/(µg/L): = Time:.
Sample pH (s.u.): %1.2 Time: Li c--t- Odor: _ , t2 Time: 1 `--4 -t 0
ReDox (mV): 6 Time: ( L- ``id Appearance: Time: )L_' <)
ReDox (EH value):YSI ProPlus +200mV� 1 �-1 Other: Time:
Generai/Weather Observations:.A S ° 3"t . �fj t ti' Nj _
suriny c oudy/rainy) Tempe(°F) Wind (mph)
Sampler Signature
Stabilization Test
Spec
To fume
�350

Document Name: Field data Sheet
Date Issued: March 8, 2019
ceAnali4icaly
pave: lot_{
Document Number. F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersviiie Quality.
i
Office .
Field Data Sheet
1E Z.f:---
Name and Affiliation (Sampler(s):_ �M -
URVIVES
�... t
Data Sheet Review:
Name and Affiliation (Inspector): N 1 Pr
Date: f ! - 03' �a
Well Information
Well ID: SW - L4 WeYI- g �+�F}usl>movTtt
Well Diameter:
Total Well Depth: ft
Static Water Level: r' ft
Height of Water Column: ft
Purge Information
C n: ee P---
Multi Factor'. � [*(Radius/12)2x 3.14 x 7.48].
Casing Volume: gallons.
Cal. 3 Volumes: gallons
Pump Intake: t
By:5
Date Purged: _ / / `- Start : Finish: Purge Rate:
Purging Method: Total Volume Purged: (gallons/mis/L)
Sampling Infos oration
Date Collected:. 10. /26 20,)0Time Collected:_ k-4-00 (am DULY
Sampling Equipment Used: Instruritent ID:_ V 5�- am Liz s *k 0: a 6 Msc-MTe 3o5"j
Bottle Type Preservatl�n Analysis Required
_r 1-el�
VnC
Field Measurements/Observations
Sample Temp (°C): Time: \3�QO : _ Turbidity (ntu): �Q' 4 Time: 17- . .
Diss Oxy (mg/L): lr,...S ---Time: E-�00 Fe 2+ mg/L: �Jb ,Time:
Specific Cond. (u5): Time: jQ0 Res. Cl (mg/L)/(µg/L): Time:.
Sarnple pH (s.u.): ` Time: i QO . Odor: N Time: )a
ReDox (mV): LA X ' Time: I aCD Appearance-&&IL,r.IcLOL •—
Time: ) Q
-V-�
ReDox (EH value):YSI ProPlus +200inV 11 LA T Other: -- Time:
General/Weather Observations:. -, PS _ma'] 5-• at . L- 3<- 'j 71 3L 3-AL4 I k/
urin cloudy/rainy) Temp.aD- (7) Wind_�)- —(mph)
v
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(oC)
Digs Oxy.
(mg/L)
Spy
tus) •
pH (s,u,)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallorts/mis/
Water
level (ft)
Other

Document Name: Field data Sheet
Date Issued: March B, 2019
aceAWIYUCW
Page: 1 of _f
Document Number: F-CAR-FLD401-rev.03
issuing Authority: Pace Huntersville Quality.
s
Office -
Field Data Sheet
L94
Name and Affiliation (Sampler(s):_ `TT-Z ­ aEtLL-sa�s-c kA
Name -and Affiliation (Inspector): A
Well Information
Data Sheet Review:
Date: / i - 0 3 By: �5
Well ID: ..� Gt1e1LT cked S_/�O f Fluslu ount
Well Diameter: _.
Total Well Depth: —r ft
Static Water Level: ` _ it
Height of Water Column: ft
9
Multi Factor*: � r(Radius/ 12)2 x 3.14 x 7.481.
Casing Volume: — gallons.
Cal, 3 Volumes: l gallons
Pump Intake: `—' ft
Purge Information
Ia"b
Date Purged: Start : Finish Purge Rate:
Purging Method: �- Tot -Al Volume Purged: (gallons/cols/L)
Sampling Information
Date Collected:.k 0 Time Collected: 3 (am pm
Sampling Equipment Used: &fib Instrument ID: YSt Q m .ple., s t a[t b�Nl� ter p�
Bottle Type Preservatiin Analysis Required
,o
voc_
Field Measurements/Observations
Sample Temp (°C): Time: Turbidity (ntu): _r)-4 �� Timer )
Digs Oxy (mg/L): 6 i- � Time: Fe 2+ mg/L: Nn __ Time: �—
Specific Cond. (-6): _ Time: Res. C1 (mg/L)/(wg/L): — Time:.
Sample pH (s.u.): Time: 1C Odor: . _ / Time:
ReDox (mV): j!2i . Time: Appearance: Si In c(,�.. Time:
ReDox (EH value):YSI Pror-lus +200mV 330 , t--( Other: Time:
General/Weather Observations:
sunny, ou y/rainy) Temp:_3(OF) Wind'� —(mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
Cq
Digs Oxy.
(mg/L)
Spec'
(u5) Cond.
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
o urm
removed
(gallons/mis/
Water
level (ft)
Other
iOL
6 .
.&o.4
6 . L4,
l 3 Q,-1
t

Document Name: Field data Sheet
Date Issued: March 8, 2019
Page: 1 of!
ace�inuleafy
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersviile Quality,
Office .
#: &nc6.r1llze C. 0 1 d LP
Name and Affiliation {Sampler(s): nc��'k CA,
! Field Data Sheet Review:
Name and Affiliation (Inspector): _- N
Date:
Well Information
Well ID: ) W - __ Weg4zocked.
Well Diameter: Co
el)
Total Well Depth: ft Multi Factor:
� [ (Radius/12)2 x 3.14 is 7.481.
Static Water ]revel: � ft Casing Volume:
� gallons.
Height of Water Column: ft Cal. 3 Volumes:
_ gallons
Pump Intake:
ft
By:
Purge Information
Date Purged: / r / Start : Finish: L Purge Rate: `—
Purging Method: Total Volume'Purged: (gallons/mis/L)
Samvline Information
Date Collected:.) 0 . /,)_6/ n7 n Time Collected: «ate {am/�
Sampling Equipment Used: Instrument ID: �S - rnn_ Q oi, /na so-rp" 0 39-9i
Bottle Type Preservati6n Analysis Required
.g n ( V'O C
Field Measurements/Observations
Sample Temp (°C): I 1 Time. C1 Turbidity (ntu): 4 Time: -
Digs Oxy (mg/L): Time: i QCFe 2+ mg/L:, ND _Time: lnr'
Specific Cond. (uS): S2 Time: i'S aC_ Res. Cl (mg/L)/(ltg/L): � Time:.
Sample pH (s.u.): 6 `�- Time: S ' Q! Odor: 0 Time: P
ReDox (mV): 4 0 � O _ Time: 13 2'_ Appearance: C c Time: ) 7o
ReDox (EH value):YSI ProPlus +200mV 3 0 Other: Time:
General/Weather Observations: a 5•tt.1 a' /U3 S, ' til
unny loudy airy) Temp Wind�(I
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(°C)
Digs Oxy.
(mg/L)
Spec'
(us)
pH {s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/mis/
Wager
level (ft)
Other

i
Document Revised: August 4, 2011
I
j
,-3
Document Name:":. -
for Fled Monitoring
Page 1 of 7:
1
i
Report Form
Issuing Authorities: �•.
j
ocumenNo.:
Dt
F-Al<L-F-004-rev.00
Pace Asheville Quality Office
Pace Analytical Services, Inc
- �I
Report Form for Field Monitoring
hi
6✓/'G
CO I.,or/ CTI✓� G/c
Location
W2tE'C
Sample Samplz ID
Level (FT)
Pj{ (u -t5)
Tcmp ('C)
SpecifiQ
C ductivity
(uhmos
Turgidity-
(NTV} SAG
EOTR12Pt5
.
Cate
Time
A
1,0
_
(o-xb
;
(oLO
0.16
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c✓
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lolb
c✓-li
4- i<Oe
i
I

APPENDIX B
LABORATORY ANALYTICAL DATA -
PACE ANALYTICAL SERVICES, LLC.

0
aceAnalytical
Report of Analysis
Bunnell-Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Attention: Andy Alexander
Project Name: Closed Buncombe County Landfill Monitoring Wells
Project Number: J20-14175-04
Lot Number:VJ27055
Date Completed:11/18/2020
NO N � � J N N �
11 /19/2020 3:58 PM
Approved and released by:
Project Manager II: Lucas Odom
pCCgF�
24r�A
lkiA
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 253

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Bunnell-Lammons Engineering, Inc.
Lot Number: VJ27055
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Nitrate
The method blank, as well as the continuing calibration blank, for analytical batch 71726 contained
analyte nitrate greater than the acceptance criteria. The associated sample, VJ27055-002, did not
contain detections for the target analyte; therefore, re -extraction and/or re -analysis of sample was not
performed.
Reanalysis of the following Nitrate samples was performed outside of the analytical holding time:
VJ27055-001, VJ27055-003, VJ27055-004, VJ27055-005, VJ27055-008, VJ27055-009. The samples
were reanalyzed out of hold due to matrix interference in the first run. The data has been reported.
The following samples were analyzed outside of analytical holding time because the sample was logged
in with greater than 50% of the holding time expired: VJ27055-012, VJ27055-015 .
The following samples were diluted due to the nature of the sample matrix: VJ27055-001, VJ27055-003,
VJ27055-004, VJ27055-005, VJ27055-008, VJ27055-009. The LOQ has been elevated to reflect the
dilution.
Sample -021 was put in for a run 2 due to instrumentation error: the nitrate peak eluted out later than the
expected retention times during run 1. The results from run 2 eluted out as expected and are confirming
of the run 1 results. Since the results are confirming and run 1 was analyzed within the hold time, run 1
will be reported.
BOD
The seed correction factor was above the method range of 0.6 to 1.0. No corrective action is required as
the BOD calculation accounts for variances in the SCF. Associated samples have been qualified with a 7
The results of the three GGA check samples associated with the batch averaged 235.5 mg/L which is
higher than the method required range of 198±30.5 mg/L. The affected data has been flagged with a 2.
The method blank result was higher than the method -required limit of 0.20mg/L. Associated samples
have been qualified with a 4.
Samples VJ27055-012 and VJ27055-015 were prepared just hours outside of the hold time. Data is not
likely impacted. Additionally, BOD values are in line with reported COD values demonstrating accuracy.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 253

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Metals by ICP-MS
Due to sample matrix effect on the internal standard (ISTD), a dilution was required for sample VJ27055-
016. The LOQ has been adjusted accordingly.
VOCs by GC/MS
The laboratory control sample (LCS) for analytical batch 72211 exceeded acceptance criteria for Acetone.
This analytes is biased high but not detected in the samples affected.
Due to the large number of spiked analytes, there is a high probability that one or more analytes will
recover outside acceptance limits. The laboratory's SOP allows for 10% of analytes to recover marginally
outside criteria. Acetone recovered marginally outside LCS/LCSD criteria in batch 72367.
SVOCS by GUMS
One surrogate recovery for the following samples was outside of acceptance limits: VJ27055-007,
VJ27055-009. Another extraction was not performed outside of the analytical hold time.
The method blank associated with batch 72150 yielded a "J" value detection for Butyl Benzyl Phthalate.
No corrective action is required as this is an estimated value recovered below the LOQ.
Pesticides by GC
Sample -009 has been qualified with a "P" for beta-BHC and Endosulfan II as the relative percent
difference between the two GC columns exceeds method criteria. Per SOP, the lesser of the two values
has been reported.
Subcontracted Samples
The analysis for VFA, Dissolved Hydrogen, MEE, and CO2 has been performed by Pace Gulf Coast
Laboratories. This data has been ammended to this report following sample receipt information.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 253

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: VJ27055
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
MW-18-78
Aqueous
10/26/20201320
10/27/2020
002
MW-19-110
Aqueous
10/26/20201610
10/27/2020
003
MW-21-94
Aqueous
10/27/2020 0945
10/28/2020
004
MW-21-21
Aqueous
10/27/2020 0935
10/28/2020
005
MW-19-75
Aqueous
10/27/20201105
10/28/2020
006
MW-3
Aqueous
10/27/20201200
10/28/2020
007
MW-5
Aqueous
10/27/20201255
10/28/2020
008
MW-4
Aqueous
10/27/20201335
10/28/2020
009
MW-6
Aqueous
10/27/20201445
10/28/2020
010
MW-6-192
Aqueous
10/27/20201625
10/28/2020
011
MW-13-35
Aqueous
10/28/2020 0905
10/30/2020
012
MW-13-132
Aqueous
10/28/2020 0940
10/30/2020
013
MW-12-25
Aqueous
10/28/20201010
10/30/2020
014
MW-4A
Aqueous
10/28/20201135
10/30/2020
015
MW-24-160
Aqueous
10/28/20201345
10/30/2020
016
MW-15
Aqueous
10/28/20201545
10/30/2020
017
MW-B
Aqueous
10/29/2020 0945
10/30/2020
018
MW-17-137
Aqueous
10/29/20201045
10/30/2020
019
MW-17-60
Aqueous
10/29/20201240
10/30/2020
020
MW-17-310
Aqueous
10/29/20201530
10/30/2020
021
MW-2
Aqueous
10/29/20201705
10/30/2020
022
MW-7
Aqueous
10/30/20201050
11/02/2020
(22 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 253

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: VJ27055
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
MW-18-78
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
300
mg CaCO3/L
16
001
MW-18-78
Aqueous
BOD, 5 day
SM 521013-
3.9
7
mg/L
16
001
MW-18-78
Aqueous
Chloride
9056A
140
mg/L
16
001
MW-18-78
Aqueous
COD
SM 5220D-
28
mg/L
16
001
MW-18-78
Aqueous
Sulfate
9056A
1.2
mg/L
16
001
MW-18-78
Aqueous
Sulfide
SM 4500-S2 F-
1.2
mg/L
16
001
MW-18-78
Aqueous
TOC
SM 5310C-
8.0
mg/L
16
001
MW-18-78
Aqueous
1,4-Dioxane
8260D (SIM)
45
ug/L
16
001
MW-18-78
Aqueous
Acetone
8260D
9.0
J
ug/L
16
001
MW-18-78
Aqueous
Carbon disulfide
8260D
1.9
ug/L
17
001
MW-18-78
Aqueous
Chlorobenzene
8260D
3.3
ug/L
17
001
MW-18-78
Aqueous
Chloroethane
8260D
0.70
J
ug/L
17
001
MW-18-78
Aqueous
1,4-Dichlorobenzene
8260D
2.5
ug/L
17
001
MW-18-78
Aqueous
1, 1 -Dichloroethane
8260D
0.94
J
ug/L
17
001
MW-18-78
Aqueous
cis- 1,2-Dichloroethene
8260D
0.85
J
ug/L
17
001
MW-18-78
Aqueous
Vinyl chloride
8260D
0.68
J
ug/L
17
001
MW-18-78
Aqueous
Barium
6020B
68
ug/L
18
001
MW-18-78
Aqueous
Nickel
6020B
6.2
ug/L
18
002
MW-19-110
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
170
mg CaCO3/1-
19
002
MW-19-110
Aqueous
BOD, 5 day
SM 521013-
2.4
7
mg/L
19
002
MW-19-110
Aqueous
Chloride
9056A
39
mg/L
19
002
MW-19-110
Aqueous
Sulfate
9056A
9.7
mg/L
19
002
MW-19-110
Aqueous
TOC
SM 5310C-
2.2
mg/L
19
002
MW-19-110
Aqueous
1,4-Dioxane
8260D (SIM)
34
ug/L
19
002
MW-19-110
Aqueous
Acetone
8260D
5.7
J
ug/L
19
002
MW-19-110
Aqueous
Carbon disulfide
8260D
1.1
ug/L
20
002
MW-19-110
Aqueous
Chlorobenzene
8260D
0.55
J
ug/L
20
002
MW-19-110
Aqueous
Chloroethane
8260D
0.81
J
ug/L
20
002
MW-19-110
Aqueous
1,4-Dichlorobenzene
8260D
0.64
J
ug/L
20
002
MW-19-110
Aqueous
cis-1,2-Dichloroethene
8260D
0.61
J
ug/L
20
002
MW-19-110
Aqueous
Barium
6020B
9.8
ug/L
21
002
MW-19-110
Aqueous
Nickel
6020B
3.4
J
ug/L
21
003
MW-21-94
Aqueous
Alkalinity @ pH 4.5 su
SM 2320B-
310
mg CaCO3/1-
22
003
MW-21-94
Aqueous
BOD, 5 day
SM 521013-
2.1
27
mg/L
22
003
MW-21-94
Aqueous
Chloride
9056A
89
mg/L
22
003
MW-21-94
Aqueous
COD
SM 5220D-
21
mg/L
22
003
MW-21-94
Aqueous
Sulfate
9056A
2.2
mg/L
22
003
MW-21-94
Aqueous
TOC
SM 5310C-
7.1
mg/L
22
003
MW-21-94
Aqueous
1,4-Dioxane
8260D (SIM)
46
ug/L
22
003
MW-21-94
Aqueous
Acetone
8260D
7.1
J
ug/L
22
003
MW-21-94
Aqueous
Carbon disulfide
8260D
1.6
ug/L
23
003
MW-21-94
Aqueous
Chlorobenzene
8260D
1.2
ug/L
23
003
MW-21-94
Aqueous
Chloroethane
8260D
2.5
ug/L
23
003
MW-21-94
Aqueous
1,4-Dichlorobenzene
8260D
1.6
ug/L
23
003
MW-21-94
Aqueous
1,1-Dichloroethane
8260D
0.82
J
ug/L
23
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 253

Detection Summary (Continued)
Lot Number: VJ27055
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
003
MW-21-94
Aqueous
1,2-Dichloroethane
8260D
0.48
J
ug/L
23
003
MW-21-94
Aqueous
cis- 1,2-Dichloroethene
8260D
2.4
ug/L
23
003
MW-21-94
Aqueous
Vinyl chloride
8260D
1.1
ug/L
23
003
MW-21-94
Aqueous
Barium
6020B
47
ug/L
24
003
MW-21-94
Aqueous
Nickel
6020B
7.7
ug/L
24
004
MW-21-21
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
640
mg CaCO3/1-
25
004
MW-21-21
Aqueous
BOD, 5 day
SM 5210B-
3.2
27
mg/L
25
004
MW-21-21
Aqueous
Chloride
9056A
86
mg/L
25
004
MW-21-21
Aqueous
COD
SM 5220D-
38
mg/L
25
004
MW-21-21
Aqueous
Sulfate
9056A
13
mg/L
25
004
MW-21-21
Aqueous
Sulfide
SM 4500-S2 F-
1.6
mg/L
25
004
MW-21-21
Aqueous
TOC
SM 5310C-
12
mg/L
25
004
MW-21-21
Aqueous
1,4-Dioxane
8260D (SIM)
52
ug/L
25
004
MW-21-21
Aqueous
Acetone
8260D
7.0
J
ug/L
25
004
MW-21-21
Aqueous
Benzene
8260D
1.8
ug/L
25
004
MW-21-21
Aqueous
Carbon disulfide
8260D
0.60
J
ug/L
26
004
MW-21-21
Aqueous
Chlorobenzene
8260D
13
ug/L
26
004
MW-21-21
Aqueous
1,2-Dichlorobenzene
8260D
2.7
ug/L
26
004
MW-21-21
Aqueous
1,4-Dichlorobenzene
8260D
12
ug/L
26
004
MW-21-21
Aqueous
1,1-Dichloroethane
8260D
2.5
ug/L
26
004
MW-21-21
Aqueous
1,2-Dichloroethane
8260D
0.54
J
ug/L
26
004
MW-21-21
Aqueous
cis- 1,2-Dichloroethene
8260D
5.2
ug/L
26
004
MW-21-21
Aqueous
Vinyl chloride
8260D
2.3
ug/L
26
004
MW-21-21
Aqueous
Barium
6020B
110
ug/L
27
004
MW-21-21
Aqueous
Chromium
6020B
1.3
J
ug/L
27
004
MW-21-21
Aqueous
Cobalt
6020B
9.3
ug/L
27
004
MW-21-21
Aqueous
Nickel
6020B
4.7
J
ug/L
27
005
MW-19-75
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
410
mg CaCO3/1-
28
005
MW-19-75
Aqueous
BOD, 5 day
SM 521013-
2.8
27
mg/L
28
005
MW-19-75
Aqueous
Chloride
9056A
160
mg/L
28
005
MW-19-75
Aqueous
COD
SM 5220D-
45
mg/L
28
005
MW-19-75
Aqueous
Sulfate
9056A
11
mg/L
28
005
MW-19-75
Aqueous
TOC
SM 5310C-
14
mg/L
28
005
MW-19-75
Aqueous
1,4-Dioxane
8260D (SIM)
93
ug/L
28
005
MW-19-75
Aqueous
Acetone
8260D
6.6
J
ug/L
28
005
MW-19-75
Aqueous
Carbon disulfide
8260D
0.77
J
ug/L
29
005
MW-19-75
Aqueous
Chlorobenzene
8260D
4.8
ug/L
29
005
MW-19-75
Aqueous
1,4-Dichlorobenzene
8260D
4.2
ug/L
29
005
MW-19-75
Aqueous
1, 1 -Dichloroethane
8260D
0.58
J
ug/L
29
005
MW-19-75
Aqueous
Antimony
6020B
0.58
J
ug/L
30
005
MW-19-75
Aqueous
Barium
6020B
130
ug/L
30
005
MW-19-75
Aqueous
Cobalt
6020B
3.8
J
ug/L
30
005
MW-19-75
Aqueous
Nickel
6020B
25
ug/L
30
005
MW-19-75
Aqueous
Selenium
6020B
1.3
J
ug/L
30
005
MW-19-75
Aqueous
Zinc
6020B
2.6
J
ug/L
30
006
MW-3
Aqueous
1,4-Dioxane
8260D (SIM)
97
ug/L
31
006
MW-3
Aqueous
Acetone
8260D
7.6
J
ug/L
31
006
MW-3
Aqueous
Benzene
8260D
0.78
J
ug/L
31
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 253

Detection Summary (Continued)
Lot Number: VJ27055
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
006
MW-3
Aqueous
Chlorobenzene
8260D
3.6
ug/L
31
006
MW-3
Aqueous
Chloroethane
8260D
2.6
ug/L
31
006
MW-3
Aqueous
1,2-Dichlorobenzene
8260D
0.77
J
ug/L
31
006
MW-3
Aqueous
1,4-Dichlorobenzene
8260D
6.5
ug/L
31
006
MW-3
Aqueous
1,1-Dichloroethane
8260D
1.7
ug/L
31
006
MW-3
Aqueous
cis- 1,2-Dichloroethene
8260D
0.84
J
ug/L
31
006
MW-3
Aqueous
Vinyl chloride
8260D
0.79
J
ug/L
32
006
MW-3
Aqueous
Xylenes (total)
8260D
0.82
J
ug/L
32
006
MW-3
Aqueous
Barium
6020B
230
ug/L
32
006
MW-3
Aqueous
Cobalt
6020B
12
ug/L
32
006
MW-3
Aqueous
Nickel
6020B
31
ug/L
32
006
MW-3
Aqueous
Selenium
6020B
1.8
J
ug/L
33
007
MW-5
Aqueous
1,4-Dioxane
8260D (SIM)
67
ug/L
34
007
MW-5
Aqueous
Acetone
8260D
5.3
J
ug/L
34
007
MW-5
Aqueous
Chlorobenzene
8260D
7.1
ug/L
34
007
MW-5
Aqueous
Chloroethane
8260D
0.92
J
ug/L
34
007
MW-5
Aqueous
1,4-Dichlorobenzene
8260D
4.7
ug/L
34
007
MW-5
Aqueous
1,1-Dichloroethane
8260D
0.64
J
ug/L
34
007
MW-5
Aqueous
1,4-Dichlorobenzene
8270E
1.6
J
ug/L
36
007
MW-5
Aqueous
beta-BHC
8081B
0.032
J
ug/L
39
007
MW-5
Aqueous
Endosulfan II
8081B
0.14
ug/L
40
007
MW-5
Aqueous
Barium
6020B
140
ug/L
40
007
MW-5
Aqueous
Cobalt
6020B
11
ug/L
40
007
MW-5
Aqueous
Nickel
6020B
19
ug/L
41
007
MW-5
Aqueous
Selenium
6020B
1.5
J
ug/L
41
008
MW-4
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
420
mg CaCO3/1-
42
008
MW-4
Aqueous
BOD, 5 day
SM 521013-
2.2
27
mg/L
42
008
MW-4
Aqueous
Chloride
9056A
57
mg/L
42
008
MW-4
Aqueous
COD
SM 5220D-
21
mg/L
42
008
MW-4
Aqueous
Sulfate
9056A
21
mg/L
42
008
MW-4
Aqueous
Sulfide
SM 4500-S2 F-
1.3
mg/L
42
008
MW-4
Aqueous
TOC
SM 5310C-
5.9
mg/L
42
008
MW-4
Aqueous
1,4-Dioxane
8260D (SIM)
22
ug/L
42
008
MW-4
Aqueous
Acetone
8260D
6.7
J
ug/L
42
008
MW-4
Aqueous
Benzene
8260D
0.41
J
ug/L
42
008
MW-4
Aqueous
Carbon disulfide
8260D
0.42
J
ug/L
43
008
MW-4
Aqueous
Chlorobenzene
8260D
4.3
ug/L
43
008
MW-4
Aqueous
Chloroethane
8260D
1.9
J
ug/L
43
008
MW-4
Aqueous
1,2-Dichlorobenzene
8260D
0.56
J
ug/L
43
008
MW-4
Aqueous
1,4-Dichlorobenzene
8260D
5.5
ug/L
43
008
MW-4
Aqueous
1,1-Dichloroethane
8260D
7.4
ug/L
43
008
MW-4
Aqueous
1,2-Dichloroethane
8260D
0.41
J
ug/L
43
008
MW-4
Aqueous
cis- 1,2-Dichloroethene
8260D
16
ug/L
43
008
MW-4
Aqueous
Trichloroethene
8260D
0.64
J
ug/L
43
008
MW-4
Aqueous
Vinyl chloride
8260D
3.0
ug/L
43
008
MW-4
Aqueous
Barium
6020B
530
ug/L
44
008
MW-4
Aqueous
Cadmium
6020B
0.63
ug/L
44
008
MW-4
Aqueous
Cobalt
6020B
73
ug/L
44
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 7 of 253

Detection Summary (Continued)
Lot Number: VJ27055
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
008
MW-4
Aqueous
Nickel
6020B
90
ug/L
44
008
MW-4
Aqueous
Zinc
6020B
17
ug/L
44
009
MW-6
Aqueous
Alkalinity @ pH 4.5 su
SM 2320B-
560
mg CaCO3/1-
45
009
MW-6
Aqueous
BOD, 5 day
SM 521013-
10
27
mg/L
45
009
MW-6
Aqueous
Chloride
9056A
140
mg/L
45
009
MW-6
Aqueous
COD
SM 5220D-
39
mg/L
45
009
MW-6
Aqueous
Sulfate
9056A
0.78
J
mg/L
45
009
MW-6
Aqueous
TOC
SM 5310C-
11
mg/L
45
009
MW-6
Aqueous
1,4-Dioxane
8260D (SIM)
31
ug/L
45
009
MW-6
Aqueous
Acetone
8260D
8.4
J
ug/L
45
009
MW-6
Aqueous
Benzene
8260D
0.87
J
ug/L
45
009
MW-6
Aqueous
Carbon disulfide
8260D
0.84
J
ug/L
46
009
MW-6
Aqueous
Chlorobenzene
8260D
8.8
ug/L
46
009
MW-6
Aqueous
Chloroethane
8260D
3.7
ug/L
46
009
MW-6
Aqueous
1,4-Dichlorobenzene
8260D
3.7
ug/L
46
009
MW-6
Aqueous
1,1-Dichloroethane
8260D
2.0
ug/L
46
009
MW-6
Aqueous
cis- 1,2-Dichloroethene
8260D
0.49
J
ug/L
46
009
MW-6
Aqueous
Vinyl chloride
8260D
0.44
J
ug/L
47
009
MW-6
Aqueous
4-Chloro-3-methyl phenol
8270E
1.7
J
ug/L
48
009
MW-6
Aqueous
1,4-Dichlorobenzene
8270E
1.3
J
ug/L
48
009
MW-6
Aqueous
Diethylphthalate
8270E
2.5
J
ug/L
48
009
MW-6
Aqueous
Naphthalene
8270E
0.78
J
ug/L
49
009
MW-6
Aqueous
beta-BHC
8081B
0.025
JP
ug/L
51
009
MW-6
Aqueous
Endosulfan II
8081B
0.042
P
ug/L
51
009
MW-6
Aqueous
Endrin aldehyde
8081B
0.020
J
ug/L
51
009
MW-6
Aqueous
Barium
6020B
1400
ug/L
52
009
MW-6
Aqueous
Copper
6020B
1.9
J
ug/L
52
009
MW-6
Aqueous
Nickel
6020B
9.8
ug/L
52
009
MW-6
Aqueous
Selenium
6020B
1.3
J
ug/L
52
010
MW-6-192
Aqueous
1,4-Dioxane
8260D (SIM)
8.5
ug/L
53
010
MW-6-192
Aqueous
Chlorobenzene
8260D
1.3
ug/L
53
010
MW-6-192
Aqueous
Chloroethane
8260D
0.75
J
ug/L
53
010
MW-6-192
Aqueous
1,4-Dichlorobenzene
8260D
0.61
J
ug/L
53
010
MW-6-192
Aqueous
1,1-Dichloroethane
8260D
0.66
J
ug/L
53
010
MW-6-192
Aqueous
Barium
6020B
59
ug/L
54
010
MW-6-192
Aqueous
Nickel
6020B
1.7
J
ug/L
54
010
MW-6-192
Aqueous
Zinc
6020B
3.9
J
ug/L
55
011
MW-13-35
Aqueous
Benzene
8260D
1.7
ug/L
56
011
MW-13-35
Aqueous
Chlorobenzene
8260D
6.8
ug/L
56
011
MW-13-35
Aqueous
1,2-Dichlorobenzene
8260D
4.1
ug/L
56
011
MW-13-35
Aqueous
1,4-Dichlorobenzene
8260D
17
ug/L
56
011
MW-13-35
Aqueous
cis- 1,2-Dichloroethene
8260D
2.9
ug/L
56
011
MW-13-35
Aqueous
Vinyl chloride
8260D
0.53
J
ug/L
57
011
MW-13-35
Aqueous
Barium
6020B
180
ug/L
57
011
MW-13-35
Aqueous
Cobalt
6020B
1.4
J
ug/L
57
011
MW-13-35
Aqueous
Nickel
6020B
4.8
J
ug/L
57
011
MW-13-35
Aqueous
Zinc
6020B
5.8
J
ug/L
57
012
MW-13-132
Aqueous
Alkalinity @ pH 4.5 su
SM 2320B-
150
mg CaCO3/1-
58
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 253

Detection Summary (Continued)
Lot Number: VJ27055
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
012
MW-13-132
Aqueous
BOD, 5 day
SM 521013-
3.6
H47
mg/L
58
012
MW-13-132
Aqueous
Chloride
9056A
4.7
mg/L
58
012
MW-13-132
Aqueous
Sulfate
9056A
7.2
mg/L
58
012
MW-13-132
Aqueous
Benzene
8260D
1.4
ug/L
58
012
MW-13-132
Aqueous
1,4-Dichlorobenzene
8260D
0.78
J
ug/L
59
012
MW-13-132
Aqueous
1, 1 -Dichloroethane
8260D
0.73
J
ug/L
59
012
MW-13-132
Aqueous
cis- 1,2-Dichloroethene
8260D
4.4
ug/L
59
012
MW-13-132
Aqueous
Vinyl chloride
8260D
1.6
ug/L
59
012
MW-13-132
Aqueous
Barium
6020B
42
ug/L
60
012
MW-13-132
Aqueous
Zinc
6020B
3.8
J
ug/L
60
013
MW-12-25
Aqueous
Barium
6020B
55
ug/L
62
013
MW-12-25
Aqueous
Copper
6020B
1.5
J
ug/L
62
013
MW-12-25
Aqueous
Nickel
6020B
17
ug/L
62
013
MW-12-25
Aqueous
Zinc
6020B
13
ug/L
62
014
MW-4A
Aqueous
1,4-Dioxane
8260D (SIM)
20
ug/L
63
014
MW-4A
Aqueous
Benzene
8260D
2.8
ug/L
63
014
MW-4A
Aqueous
Chlorobenzene
8260D
13
ug/L
63
014
MW-4A
Aqueous
1,2-Dichlorobenzene
8260D
3.5
ug/L
63
014
MW-4A
Aqueous
1,4-Dichlorobenzene
8260D
32
ug/L
63
014
MW-4A
Aqueous
Ethylbenzene
8260D
1.5
ug/L
64
014
MW-4A
Aqueous
Toluene
8260D
1.2
ug/L
64
014
MW-4A
Aqueous
Vinyl chloride
8260D
0.51
J
ug/L
64
014
MW-4A
Aqueous
Xylenes (total)
8260D
3.2
ug/L
64
014
MW-4A
Aqueous
Antimony
6020B
0.79
J
ug/L
64
014
MW-4A
Aqueous
Barium
6020B
540
ug/L
64
014
MW-4A
Aqueous
Cadmium
6020B
0.17
J
ug/L
64
014
MW-4A
Aqueous
Cobalt
6020B
33
ug/L
64
014
MW-4A
Aqueous
Copper
6020B
1.6
J
ug/L
64
014
MW-4A
Aqueous
Nickel
6020B
12
ug/L
65
014
MW-4A
Aqueous
Zinc
6020B
2.9
J
ug/L
65
015
MW-24-160
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
64
mg CaCO3/1-
66
015
MW-24-160
Aqueous
BOD, 5 day
SM 521013-
2.0
H47
mg/L
66
015
MW-24-160
Aqueous
Chloride
9056A
6.4
mg/L
66
015
MW-24-160
Aqueous
Sulfate
9056A
27
mg/L
66
015
MW-24-160
Aqueous
TOC
SM 5310C-
1.1
mg/L
66
015
MW-24-160
Aqueous
Antimony
6020B
0.52
J
ug/L
68
015
MW-24-160
Aqueous
Barium
6020B
38
ug/L
68
015
MW-24-160
Aqueous
Cadmium
6020B
0.19
J
ug/L
68
015
MW-24-160
Aqueous
Chromium
6020B
1.3
J
ug/L
68
015
MW-24-160
Aqueous
Copper
6020B
3.9
J
ug/L
68
015
MW-24-160
Aqueous
Lead
6020B
2.0
ug/L
68
015
MW-24-160
Aqueous
Nickel
6020B
3.6
J
ug/L
68
015
MW-24-160
Aqueous
Zinc
6020B
16
ug/L
68
016
MW-15
Aqueous
Acetone
8260D
19
J
ug/L
69
016
MW-15
Aqueous
Barium
6020B
210
ug/L
70
016
MW-15
Aqueous
Chromium
6020B
12
J
ug/L
70
016
MW-15
Aqueous
Lead
6020B
1.1
ug/L
70
017
MW-B
Aqueous
1,4-Dioxane
8260D (SIM)
36
ug/L
71
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 253

Detection Summary (Continued)
Lot Number: VJ27055
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
017
MW-B
Aqueous
Acetone
8260D
5.1
J
ug/L
71
017
MW-B
Aqueous
Chlorobenzene
8260D
1.2
ug/L
71
017
MW-B
Aqueous
Chloroethane
8260D
0.60
J
ug/L
71
017
MW-B
Aqueous
1,4-Dichlorobenzene
8260D
1.9
ug/L
71
017
MW-B
Aqueous
1,1-Dichloroethane
8260D
1.7
ug/L
71
017
MW-B
Aqueous
cis- 1,2-Dichloroethene
8260D
21
ug/L
71
017
MW-B
Aqueous
Vinyl chloride
8260D
10
ug/L
72
017
MW-B
Aqueous
Barium
6020B
170
ug/L
72
018
MW-17-137
Aqueous
1,4-Dioxane
8260D (SIM)
34
ug/L
74
018
MW-17-137
Aqueous
Acetone
8260D
7.2
J
ug/L
74
018
MW-17-137
Aqueous
1,4-Dichlorobenzene
8260D
0.47
J
ug/L
74
018
MW-17-137
Aqueous
1, 1 -Dichloroethane
8260D
0.65
J
ug/L
74
018
MW-17-137
Aqueous
Vinyl chloride
8260D
0.54
J
ug/L
75
018
MW-17-137
Aqueous
Xylenes (total)
8260D
0.50
J
ug/L
75
018
MW-17-137
Aqueous
Barium
6020B
24
ug/L
75
019
MW-17-60
Aqueous
1,4-Dioxane
8260D (SIM)
23
ug/L
77
019
MW-17-60
Aqueous
Acetone
8260D
6.9
J
ug/L
77
019
MW-17-60
Aqueous
2-Butanone (MEK)
8260D
5.3
J
ug/L
77
019
MW-17-60
Aqueous
1, 1 -Dichloroethane
8260D
0.68
J
ug/L
77
019
MW-17-60
Aqueous
cis- 1,2-Dichloroethene
8260D
1.0
ug/L
77
019
MW-17-60
Aqueous
Barium
6020B
20
ug/L
78
020
MW-17-310
Aqueous
Barium
6020B
3.1
J
ug/L
81
020
MW-17-310
Aqueous
Lead
6020B
0.37
J
ug/L
81
020
MW-17-310
Aqueous
Zinc
6020B
4.6
J
ug/L
81
021
MW-2
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
60
mg CaCO3/1-
82
021
MW-2
Aqueous
Chloride
9056A
2.1
mg/L
82
021
MW-2
Aqueous
Nitrate - N
9056A
0.028
mg/L
82
021
MW-2
Aqueous
Sulfate
9056A
4.1
mg/L
82
021
MW-2
Aqueous
Antimony
6020B
0.55
J
ug/L
89
021
MW-2
Aqueous
Barium
6020B
20
ug/L
89
021
MW-2
Aqueous
Copper
6020B
1.8
J
ug/L
89
021
MW-2
Aqueous
Nickel
6020B
2.5
J
ug/L
89
021
MW-2
Aqueous
Zinc
6020B
10
ug/L
89
022
MW-7
Aqueous
Acetone
8260D
16
J
ug/L
90
022
MW-7
Aqueous
Benzene
8260D
1.7
ug/L
90
022
MW-7
Aqueous
2-Butanone (MEK)
8260D
2.3
J
ug/L
90
022
MW-7
Aqueous
Chlorobenzene
8260D
9.9
ug/L
90
022
MW-7
Aqueous
Chloroethane
8260D
3.7
ug/L
90
022
MW-7
Aqueous
1,4-Dichlorobenzene
8260D
3.9
ug/L
90
022
MW-7
Aqueous
1,1-Dichloroethane
8260D
2.7
ug/L
90
022
MW-7
Aqueous
cis-1,2-Dichloroethene
8260D
25
ug/L
90
022
MW-7
Aqueous
Methyl iodide (lodomethane)
8260D
0.45
J
ug/L
91
022
MW-7
Aqueous
Trichloroethene
8260D
0.77
J
ug/L
91
022
MW-7
Aqueous
Xylenes (total)
8260D
0.57
J
ug/L
91
022
MW-7
Aqueous
Barium
6020B
230
ug/L
91
022
MW-7
Aqueous
Cadmium
6020B
0.72
ug/L
91
022
MW-7
Aqueous
Cobalt
6020B
190
ug/L
91
022
MW-7
Aqueous
Copper
6020B
9.5
ug/L
91
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 253

Detection Summary (Continued)
Lot Number: VJ27055
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
022 MW-7
Aqueous
Lead
6020B
0.48 J
ug/L
91
022 MW-7
Aqueous
Nickel
6020B
64
ug/L
91
022 MW-7
Aqueous
Zinc
6020B
13
ug/L
92
(288 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-001
Description: MW-18-78 Matrix: Aqueous
Date Sampled:10/26/2020 1320
)ate Received:10/27/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 10/28/2020 1823 AAB
71525
1
(BOD, 5 day) SM 521OB-2011
1 11/01/2020 1456 MOM
10/27/2020 1754
13659
1
(Chloride) 9056A
1 10/28/2020 1009 AMR
71727
1
(COD) SM 5220D-2011
1 11/03/2020 2244 SRB
72159
2
(Nitrate - N) 9056A
5 10/30/2020 1612 AMR
71940
1
(Sulfate) 9056A
1 10/28/2020 1009 AMR
71729
1
(Sulfide) SM 4500-S2 F-2011
1 10/30/2020 2119 SRB
71842
1
(TOC) SM 531 OC-2011
1 10/29/2020 2111 DMA
71682
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
300
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
3.9 7
2.0
0.18
mg/L
1
Chloride
9056A
140
1.0
0.20
mg/L
1
COD
SM 5220D-2011
28
20
20
mg/L
1
Nitrate - N
9056A
ND H
0.10
0.025
mg/L
2
Sulfate
9056A
1.2
1.0
0.20
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
1.2
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
8.0
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/02/2020 1631 BWS
71945
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
45
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
94 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201047 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
9.0 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-001
Description: MW-18-78 Matrix: Aqueous
Date Sampled:10/26/2020 1320
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201047 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
1.9
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
3.3
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
0.70 J
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
2.5
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
0.94 J
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
0.85 J
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
0.68 J
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-001
Description: MW-18-78 Matrix: Aqueous
Date Sampled:10/26/2020 1320
Date Received:10/27/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
93 70-130
1,2-Dichloroethane-d4
90 70-130
Toluene-d8
90 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2020 1853 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
68
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
6.2
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
Footnote(s): 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-002
Description: MW-19-110 Matrix: Aqueous
Date Sampled:10/26/2020 1610
)ate Received:10/27/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 10/28/2020 1829 AAB
71525
1
(BOD, 5 day) SM 521OB-2011
1 11/01/2020 1456 MOM
10/27/2020 1754 13659
1
(Chloride) 9056A
1 10/28/2020 1028 AMR
71727
1
(COD) SM 5220D-2011
1 11/03/2020 2245 SRB
72159
1
(Nitrate - N) 9056A
1 10/28/2020 1028 AMR
71726
1
(Sulfate) 9056A
1 10/28/2020 1028 AMR
71729
1
(Sulfide) SM 4500-S2 F-2011
1 10/30/2020 2119 SRB
71842
1
(TOC) SM 531 OC-2011
1 10/29/2020 2124 DMA
71682
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
170
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
2.4 7
2.0
0.18
mg/L
1
Chloride
9056A
39
1.0
0.20
mg/L
1
COD
SM 5220D-2011
ND
20
20
mg/L
1
Nitrate - N
9056A
ND
0.020
0.0050
mg/L
1
Sulfate
9056A
9.7
1.0
0.20
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
2.2
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/02/2020 1655 BWS
71945
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
34
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
94 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201110 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
5.7 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-002
Description: MW-19-110 Matrix: Aqueous
Date Sampled:10/26/2020 1610
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201110 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
1.1
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
0.55 J
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
0.81 J
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
0.64 J
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
0.61 J
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-002
Description: MW-19-110 Matrix: Aqueous
Date Sampled:10/26/2020 1610
Date Received:10/27/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
101 70-130
1,2-Dichloroethane-d4
95 70-130
Toluene-d8
95 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2020 1901 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
9.8
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
3.4 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
Footnote(s): 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-003
Description: MW-21-94 Matrix: Aqueous
Date Sampled:10/27/2020 0945
)ate Received: 10/28/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 10/28/2020 1837 AAB
71525
1
(BOD, 5 day) SM 521OB-2011
1 11/02/2020 1523 MOM
10/28/2020 1722
13660
1
(Chloride) 9056A
1 10/28/2020 2053 AMR
71732
1
(COD) SM 5220D-2011
1 11/03/2020 2247 SRB
72159
2
(Nitrate - N) 9056A
5 10/30/2020 1650 AMR
71940
1
(Sulfate) 9056A
1 10/28/2020 2053 AMR
71733
1
(Sulfide) SM 4500-S2 F-2011
1 10/30/2020 2119 SRB
71842
1
(TOC) SM 531 OC-2011
1 10/29/2020 2137 DMA
71682
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
310
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
2.1 27
2.0
0.18
mg/L
1
Chloride
9056A
89
1.0
0.20
mg/L
1
COD
SM 5220D-2011
21
20
20
mg/L
1
Nitrate - N
9056A
ND H
0.10
0.025
mg/L
2
Sulfate
9056A
2.2
1.0
0.20
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
7.1
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1244 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
46
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
94 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201133 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
7.1 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-003
Description: MW-21-94 Matrix: Aqueous
Date Sampled:10/27/2020 0945
Date Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201133 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
1.6
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
1.2
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
2.5
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
1.6
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
0.82 J
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
0.48 J
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
2.4
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
1.1
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-003
Description: MW-21-94 Matrix: Aqueous
Date Sampled:10/27/2020 0945
Date Received:10/28/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
103 70-130
1,2-Dichloroethane-d4
94 70-130
Toluene-d8
98 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2020 1923 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
47
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
7.7
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
Footnote(s): 2-G:G Higher than valid range 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-004
Description: MW-21-21 Matrix: Aqueous
Date Sampled:10/27/2020 0935
)ate Received: 10/28/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 10/28/2020 1846 AAB
71525
1
(BOD, 5 day) SM 521OB-2011
1 11/02/2020 1523 MOM
10/28/2020 1722
13660
1
(Chloride) 9056A
1 10/28/2020 2150 AMR
71732
1
(COD) SM 5220D-2011
1 11/03/2020 2247 SRB
72159
2
(Nitrate - N) 9056A
5 10/30/2020 1728 AMR
71940
1
(Sulfate) 9056A
1 10/28/2020 2150 AMR
71733
1
(Sulfide) SM 4500-S2 F-2011
1 10/30/2020 2119 SRB
71842
1
(TOC) SM 531 OC-2011
1 10/29/2020 2151 DMA
71682
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
640
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
3.2 27
2.0
0.18
mg/L
1
Chloride
9056A
86
1.0
0.20
mg/L
1
COD
SM 5220D-2011
38
20
20
mg/L
1
Nitrate - N
9056A
ND H
0.10
0.025
mg/L
2
Sulfate
9056A
13
1.0
0.20
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
1.6
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
12
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1309 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
52
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
96 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201155 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
7.0 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
1.8
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-004
Description: MW-21-21 Matrix: Aqueous
Date Sampled:10/27/2020 0935
Date Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201155 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
0.60 J
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
13
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
2.7
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
12
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
2.5
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
0.54 J
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
5.2
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
2.3
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-004
Description: MW-21-21 Matrix: Aqueous
Date Sampled:10/27/2020 0935
Date Received:10/28/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
98 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
93 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2020 1930 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
110
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
1.3 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
9.3
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
4.7 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
Footnote(s): 2-G:G Higher than valid range 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-005
Description: MW-19-75 Matrix: Aqueous
Date Sampled:10/27/2020 1105
)ate Received: 10/28/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 10/28/2020 1854 AAB
71525
1
(BOD, 5 day) SM 521OB-2011
1 11/02/2020 1523 MOM
10/28/2020 1722
13660
1
(Chloride) 9056A
1 10/28/2020 2209 AMR
71732
1
(COD) SM 5220D-2011
1 11/03/2020 2247 SRB
72159
2
(Nitrate - N) 9056A
5 10/30/2020 1806 AMR
71940
1
(Sulfate) 9056A
1 10/28/2020 2209 AMR
71733
1
(Sulfide) SM 4500-S2 F-2011
1 10/30/2020 2119 SRB
71842
1
(TOC) SM 531 OC-2011
1 10/29/2020 2204 DMA
71682
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
410
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
2.8 27
2.0
0.18
mg/L
1
Chloride
9056A
160
1.0
0.20
mg/L
1
COD
SM 5220D-2011
45
20
20
mg/L
1
Nitrate - N
9056A
ND H
0.10
0.025
mg/L
2
Sulfate
9056A
11
1.0
0.20
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
14
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1334 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
93
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
95 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201217 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
6.6 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-005
Description: MW-19-75 Matrix: Aqueous
Date Sampled:10/27/2020 1105
Date Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201217 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
0.77 J
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
4.8
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
4.2
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
0.58 J
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-005
Description: MW-19-75 Matrix: Aqueous
Date Sampled:10/27/2020 1105
Date Received:10/28/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
99 70-130
1,2-Dichloroethane-d4
91 70-130
Toluene-d8
97 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep
Date
Batch
1 3005A
6020B 1 11/02/2020 2008 BPK
10/30/2020
1549 71571
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
0.58
J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
130
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
3.8
J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
25
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
1.3
J
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
2.6
J
10
2.5
ug/L
1
Footnote(s): 2-G:G Higher than valid range 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-006
Description: MW-3 Matrix: Aqueous
Date Sampled:10/27/2020 1200
Date Received:10/28/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1358 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
97
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
94 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201240 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
7.6 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
0.78 J
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
3.6
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
2.6
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
0.77 J
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
6.5
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
1.7
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
0.84 J
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-006
Description: MW-3 Matrix: Aqueous
Date Sampled:10/27/2020 1200
Date Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201240 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.79 J
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
0.82 J
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
102 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
94 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2020 2015 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
230
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
12
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
31
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-006
Description: MW-3 Matrix: Aqueous
Date Sampled:10/27/2020 1200
Date Received:10/28/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2020 2015 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
1.8 J
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-007
Description: MW-5 Matrix: Aqueous
Date Sampled:10/27/2020 1255
Date Received:10/28/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1423 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
67
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
92 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201302 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
5.3 J
20
5.0
ug/L
1
Acetonitrile
75-05-8 8260D
ND
50
15
ug/L
1
Acrolein
107-02-8 8260D
ND
20
4.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
2-Chloro-1,3-Butadiene (Chloroprene) 126-99-8 8260D
ND
5.0
1.0
ug/L
1
Chlorobenzene
108-90-7 8260D
7.1
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
0.92 J
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
3-Chloropropene (Allyl chloride)
107-05-1 8260D
ND
5.0
1.0
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
4.7
1.0
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8 8260D
ND
2.0
0.60
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
0.64 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-007
Description: MW-5 Matrix: Aqueous
Date Sampled:10/27/2020 1255
)ate Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201302 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1
1,3-Dichloropropane
142-28-9
8260D
ND
1.0
0.40
ug/L
1
2,2-Dichloropropane
594-20-7
8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloropropene
563-58-6
8260D
ND
2.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethyl methacrylate
97-63-2
8260D
ND
5.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isobutyl alcohol
78-83-1
8260D
ND
50
12
ug/L
1
Methacrylonitrile
126-98-7
8260D
ND
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
Methyl methacrylate
80-62-6
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Propionitrile (Ethyl cyanide)
107-12-0
8260D
ND
20
4.0
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
94 70-130
Toluene-d8
95 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-007
Description: MW-5 Matrix: Aqueous
Date Sampled:10/27/2020 1255
Date Received:10/28/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1603 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
2-Acetylaminofluorene
53-96-3
8270E
ND
8.0
1.7
ug/L
4-Aminobiphenyl
92-67-1
8270E
ND
8.0
1.1
ug/L
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
Benzyl alcohol
100-51-6
8270E
ND
4.0
0.30
ug/L
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
Chlorobenzilate
510-15-6
8270E
ND
10
1.6
ug/L
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
cis-Diallate
17708-57-5
8270E
ND
8.0
1.9
ug/L
trans-Diallate
17708-58-6
8270E
ND
8.0
1.9
ug/L
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8270E
ND
4.0
0.50
ug/L
1,3-Dichlorobenzene
541-73-1
8270E
ND
4.0
0.50
ug/L
1,4-Dichlorobenzene
106-46-7
8270E
1.6 J
4.0
0.60
ug/L
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
2,6-Dichlorophenol
87-65-0
8270E
ND
4.0
1.6
ug/L
0,0-Diethyl-0-2-pyrazinyl (Thionazin)
297-97-2
8270E
ND
4.0
0.90
ug/L
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
Dimethoate
60-51-5
8270E
ND
8.0
2.8
ug/L
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
p-(Dimethylamino)azobenzene
60-11-7
8270E
ND
10
0.53
ug/L
3,3'-Dimethylbenzidine
119-93-7
8270E
ND
16
10
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-007
Description: MW-5 Matrix: Aqueous
Date Sampled:10/27/2020 1255
Date Received:10/28/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1603 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
7,12-Dimethylbenzo(a)anthracene
57-97-6
8270E
ND
4.0
1.1
ug/L
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1,3-Dinitrobenzene
99-65-0
8270E
ND
16
13
ug/L
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
Ethyl methanesulfonate
62-50-0
8270E
ND
5.0
0.70
ug/L
Ethyl parathion
56-38-2
8270E
ND
16
2.8
ug/L
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
Famphur
52-85-7
8270E
ND
16
13
ug/L
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
Hexachloropropene
1888-71-7
8270E
ND
8.0
0.80
ug/L
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
Isodrin
465-73-6
8270E
ND
4.0
0.70
ug/L
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
Isosafrole
120-58-1
8270E
ND
4.0
1.1
ug/L
Methapyrilene
91-80-5
8270E
ND
16
8.8
ug/L
Methyl methanesulfonate
66-27-3
8270E
ND
4.0
0.50
ug/L
Methyl parathion
298-00-0
8270E
ND
16
2.0
ug/L
3-Methylcholanthrene
56-49-5
8270E
ND
8.0
5.0
ug/L
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1,4-Naphthoquinone
130-15-4
8270E
ND
8.0
0.40
ug/L
1-Naphthylamine
134-32-7
8270E
ND
8.0
0.030
ug/L
2-Naphthylamine
91-59-8
8270E
ND
8.0
0.14
ug/L
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
5-Nitro-o-toluidine
99-55-8
8270E
ND
8.0
2.2
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-007
Description: MW-5 Matrix: Aqueous
Date Sampled:10/27/2020 1255
Date Received:10/28/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1603 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
N-Nitroso-di-butylamine
924-16-3
8270E
ND
4.0
1.1
ug/L
N-Nitrosodiethylamine
55-18-5
8270E
ND
4.0
0.80
ug/L
N-Nitrosodimethylamine
62-75-9
8270E
ND
4.0
0.50
ug/L
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
N-Nitrosomethylethylamine
10595-95-6
8270E
ND
5.0
1.8
ug/L
N-Nitrosopiperidine
100-75-4
8270E
ND
4.0
1.4
ug/L
N-Nitrosopyrrolidine
930-55-2
8270E
ND
4.0
2.1
ug/L
Pentachlorobenzene
608-93-5
8270E
ND
4.0
0.70
ug/L
Pentachloronitrobenzene
82-68-8
8270E
ND
16
2.6
ug/L
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
Phenacetin
62-44-2
8270E
ND
4.0
3.4
ug/L
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
p-Phenylenediamine
106-50-3
8270E
ND
40
11
ug/L
Phorate
298-02-2
8270E
ND
4.0
3.6
ug/L
Pronamide
23950-58-5
8270E
ND
8.0
3.0
ug/L
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
Safrole
94-59-7
8270E
ND
5.0
0.90
ug/L
Sulfotepp
3689-24-5
8270E
ND
8.0
0.60
ug/L
1,2,4,5-Tetrachlorobenzene
95-94-3
8270E
ND
4.0
0.90
ug/L
2,3,4,6-Tetrachlorophenol
58-90-2
8270E
ND
8.0
0.80
ug/L
o-Toluidine
95-53-4
8270E
ND
4.0
0.90
ug/L
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
4.0
0.50
ug/L
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
0,0,0-Triethylphosphorothioate
126-68-1
8270E
ND
4.0
1.3
ug/L
1,3,5-Trinitrobenzene
99-35-4
8270E
ND
16
13
ug/L
Surrogate
Run 1
Q % Recovery
Acceptance
Limits
2-Fluorobiphenyl
57
37-129
2-Fluorophenol
N 20
24-127
Nitrobenzene-d5
61
38-127
Phenol-d5
34
28-128
Terphenyl-d14
81
10-148
2,4,6-Tribromophenol
60
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-007
Description: MW-5 Matrix: Aqueous
Date Sampled:10/27/2020 1255
Date Received:10/28/2020
Herbicides by GC
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 8151A
8151A
1 10/30/2020 1928 JJG
10/29/2020 2037 71691
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
2,4,5-T
93-76-5 8151A
ND
0.50
0.13
ug/L
1
2,4-D
94-75-7 8151A
ND
2.0
0.50
ug/L
1
Dinoseb
88-85-7 8151A
ND
1.0
0.50
ug/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.50
0.13
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
86 50-112
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
3665A 8082A
1 11/05/2020 1309 NCM
11/03/2020 2330 72148
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1221
11104-28-2 8082A
ND
0.40
0.25
ug/L
1
Aroclor 1232
11141-16-5 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1242
53469-21-9 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1248
12672-29-6 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1254
11097-69-1 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1260
11096-82-5 8082A
ND
0.40
0.15
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
81 10-133
Tetrachloro-m-xylene
82 31-122
Organochlorine
Pesticides by GC
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8081 B
1 11 /06/2020 1106 DAL1
11 /03/2020 2330 72139
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aldrin
309-00-2 8081B
ND
0.040
0.020
ug/L
1
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.040
0.017
ug/L
1
alpha-BHC
319-84-6 8081B
ND
0.040
0.015
ug/L
1
beta-BHC
319-85-7 8081B
0.032 J
0.040
0.015
ug/L
1
delta-BHC
319-86-8 8081B
ND
0.040
0.015
ug/L
1
cis -Chlordane
5103-71-9 8081B
ND
0.040
0.015
ug/L
1
trans -Chlordane
5103-74-2 8081B
ND
0.040
0.015
ug/L
1
4,4'-DDD
72-54-8 8081B
ND
0.040
0.015
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result
< LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-007
Description: MW-5 Matrix: Aqueous
Date Sampled:10/27/2020 1255
Date Received:10/28/2020
Organochlorine
Pesticides by GC
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8081B
1 11/06/20201106 DAL1
11/03/20202330 72139
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
4,4'-DDE
72-55-9 8081B
ND
0.040
0.020
ug/L
1
4,4'-DDT
50-29-3 8081B
ND
0.040
0.020
ug/L
1
Dieldrin
60-57-1 8081B
ND
0.040
0.015
ug/L
1
Endosulfan 1
959-98-8 8081B
ND
0.040
0.015
ug/L
1
Endosulfan II
33213-65-9 8081B
0.14
0.040
0.015
ug/L
1
Endosulfan sulfate
1031-07-8 8081B
ND
0.040
0.015
ug/L
1
Endrin
72-20-8 8081B
ND
0.040
0.015
ug/L
1
Endrin aldehyde
7421-93-4 8081B
ND
0.040
0.015
ug/L
1
Endrin ketone
53494-70-5 8081B
ND
0.040
0.015
ug/L
1
Heptachlor
76-44-8 8081B
ND
0.040
0.021
ug/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.040
0.016
ug/L
1
Methoxychlor
72-43-5 8081B
ND
0.16
0.021
ug/L
1
Toxaphene
8001-35-2 8081B
ND
0.40
0.30
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery
Limits
Decachlorobiphenyl
66 20-122
Tetrachloro-m-xylene
64 46-119
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/13/2020 0848 JAB2
11/13/2020 0552 73376
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7470A
ND
0.00020
0.000091
mg/L
1
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2020 2023 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
140
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
11
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection
Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 36 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-007
Description: MW-5 Matrix: Aqueous
Date Sampled:10/27/2020 1255
Date Received:10/28/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2020 2023 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
19
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
1.5 J
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Tin
7440-31-5 6020B
ND
20
5.0
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 37 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-008
Description: MW-4 Matrix: Aqueous
Date Sampled:10/27/2020 1335
)ate Received:10/28/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 10/31/2020 1449 AAB
72118
1
(BOD, 5 day) SM 521OB-2011
1 11/02/2020 1523 MOM
10/28/2020 1722
13660
1
(Chloride) 9056A
1 10/30/2020 1553 AMR
71943
1
(COD) SM 5220D-2011
1 11/03/2020 2247 SRB
72159
2
(Nitrate - N) 9056A
5 11/03/2020 2004 AMR
72216
1
(Sulfate) 9056A
1 10/30/2020 1553 AMR
71944
1
(Sulfide) SM 4500-S2 F-2011
1 10/30/2020 2119 SRB
71842
1
(TOC) SM 531 OC-2011
1 10/29/2020 2217 DMA
71682
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
420
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
2.2 27
2.0
0.18
mg/L
1
Chloride
9056A
57
1.0
0.25
mg/L
1
COD
SM 5220D-2011
21
20
20
mg/L
1
Nitrate - N
9056A
ND H
0.10
0.025
mg/L
2
Sulfate
9056A
21
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
1.3
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
5.9
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1448 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
22
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
94 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201324 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
6.7 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
0.41 J
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 38 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-008
Description: MW-4 Matrix: Aqueous
Date Sampled:10/27/2020 1335
Date Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201324 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
0.42
J 1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
4.3
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
1.9
J 2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
0.56
J 1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
5.5
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
7.4
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
0.41
J 1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
16
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
0.64
J 1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
3.0
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-008
Description: MW-4 Matrix: Aqueous
Date Sampled:10/27/2020 1335
Date Received:10/28/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
100 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
96 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2020 2030 BPK
10/30/2020 1549 71571
2 3005A
6020B 10 11/03/2020 1837 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
530
50
13
ug/L
2
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.63
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
73
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
90
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
17
10
2.5
ug/L
1
Footnote(s): 2-G:G Higher than valid range 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-009
Description: MW-6 Matrix: Aqueous
Date Sampled:10/27/2020 1445
)ate Received: 10/28/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 10/28/2020 1902 AAB
71525
1
(BOD, 5 day) SM 521OB-2011
1 11/02/2020 1523 MOM
10/28/2020 1722
13660
1
(Chloride) 9056A
1 10/29/2020 0003 AMR
71732
1
(COD) SM 5220D-2011
1 11/03/2020 2247 SRB
72159
2
(Nitrate - N) 9056A
5 10/30/2020 1844 AMR
71940
1
(Sulfate) 9056A
1 10/29/2020 0003 AMR
71733
1
(Sulfide) SM 4500-S2 F-2011
1 10/30/2020 2119 SRB
71842
1
(TOC) SM 531 OC-2011
1 10/29/2020 2230 DMA
71682
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
560
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
10 27
2.0
0.18
mg/L
1
Chloride
9056A
140
1.0
0.20
mg/L
1
COD
SM 5220D-2011
39
20
20
mg/L
1
Nitrate - N
9056A
ND H
0.10
0.025
mg/L
2
Sulfate
9056A
0.78 J
1.0
0.20
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
11
1.0
1.0
mg/L
1
Volatile Organic Compounds by GC/MS (SIM
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1512 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
31
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
93 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201347 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
8.4 J
20
5.0
ug/L
1
Acetonitrile
75-05-8 8260D
ND
50
15
ug/L
1
Acrolein
107-02-8 8260D
ND
20
4.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
0.87 J
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-009
Description: MW-6 Matrix: Aqueous
Date Sampled:10/27/2020 1445
Date Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201347 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
0.84 J
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
2-Chloro-1,3-Butadiene (Chloroprene)
126-99-8
8260D
ND
5.0
1.0
ug/L
Chlorobenzene
108-90-7
8260D
8.8
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
3.7
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
3-Chloropropene (Allyl chloride)
107-05-1
8260D
ND
5.0
1.0
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,3-Dichlorobenzene
541-73-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
3.7
1.0
0.40
ug/L
Dichlorodifluoromethane
75-71-8
8260D
ND
2.0
0.60
ug/L
1,1-Dichloroethane
75-34-3
8260D
2.0
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
0.49 J
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1,3-Dichloropropane
142-28-9
8260D
ND
1.0
0.40
ug/L
2,2-Dichloropropane
594-20-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloropropene
563-58-6
8260D
ND
2.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethyl methacrylate
97-63-2
8260D
ND
5.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Isobutyl alcohol
78-83-1
8260D
ND
50
12
ug/L
Methacrylonitrile
126-98-7
8260D
ND
5.0
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
Methyl methacrylate
80-62-6
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 42 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-009
Description: MW-6 Matrix: Aqueous
Date Sampled:10/27/2020 1445
Date Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201347 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Propionitrile (Ethyl cyanide)
107-12-0
8260D
ND
20
4.0
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
0.44 J
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
103
70-130
1,2-Dichloroethane-d4
90
70-130
Toluene-d8
93
70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 11/13/2020 1628 SCD
11/03/2020 1919 72150
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9 8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8 8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2 8270E
ND
4.0
0.50
ug/L
1
2-Acetylaminofluorene
53-96-3 8270E
ND
8.0
1.7
ug/L
1
4-Aminobiphenyl
92-67-1 8270E
ND
8.0
1.1
ug/L
1
Anthracene
120-12-7 8270E
ND
0.80
0.20
ug/L
1
Benzo(a)anthracene
56-55-3 8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8 8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2 8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2 8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9 8270E
ND
0.80
0.20
ug/L
1
Benzyl alcohol
100-51-6 8270E
ND
4.0
0.30
ug/L
1
4-Bromophenyl phenyl ether
101-55-3 8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7 8270E
ND
4.0
0.50
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-009
Description: MW-6 Matrix: Aqueous
Date Sampled:10/27/2020 1445
Date Received:10/28/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1628 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
4-Chloro-3-methyl phenol
59-50-7
8270E
1.7 J
4.0
0.50
ug/L
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
Chlorobenzilate
510-15-6
8270E
ND
10
1.6
ug/L
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
cis-Diallate
17708-57-5
8270E
ND
8.0
1.9
ug/L
trans-Diallate
17708-58-6
8270E
ND
8.0
1.9
ug/L
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8270E
ND
4.0
0.50
ug/L
1,3-Dichlorobenzene
541-73-1
8270E
ND
4.0
0.50
ug/L
1,4-Dichlorobenzene
106-46-7
8270E
1.3 J
4.0
0.60
ug/L
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
2,6-Dichlorophenol
87-65-0
8270E
ND
4.0
1.6
ug/L
0,0-Diethyl-0-2-pyrazinyl (Thionazin)
297-97-2
8270E
ND
4.0
0.90
ug/L
Diethylphthalate
84-66-2
8270E
2.5 J
4.0
0.50
ug/L
Dimethoate
60-51-5
8270E
ND
8.0
2.8
ug/L
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
p-(Dimethylamino)azobenzene
60-11-7
8270E
ND
10
0.53
ug/L
3,3'-Dimethylbenzidine
119-93-7
8270E
ND
16
10
ug/L
7,12-Dimethylbenzo(a)anthracene
57-97-6
8270E
ND
4.0
1.1
ug/L
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1,3-Dinitrobenzene
99-65-0
8270E
ND
16
13
ug/L
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
Ethyl methanesulfonate
62-50-0
8270E
ND
5.0
0.70
ug/L
Ethyl parathion
56-38-2
8270E
ND
16
2.8
ug/L
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
Famphur
52-85-7
8270E
ND
16
13
ug/L
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 44 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-009
Description: MW-6 Matrix: Aqueous
Date Sampled:10/27/2020 1445
Date Received:10/28/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1628 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
Hexachloropropene
1888-71-7
8270E
ND
8.0
0.80
ug/L
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
Isodrin
465-73-6
8270E
ND
4.0
0.70
ug/L
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
Isosafrole
120-58-1
8270E
ND
4.0
1.1
ug/L
Methapyrilene
91-80-5
8270E
ND
16
8.8
ug/L
Methyl methanesulfonate
66-27-3
8270E
ND
4.0
0.50
ug/L
Methyl parathion
298-00-0
8270E
ND
16
2.0
ug/L
3-Methylcholanthrene
56-49-5
8270E
ND
8.0
5.0
ug/L
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
Naphthalene
91-20-3
8270E
0.78 J
0.80
0.20
ug/L
1,4-Naphthoquinone
130-15-4
8270E
ND
8.0
0.40
ug/L
1-Naphthylamine
134-32-7
8270E
ND
8.0
0.030
ug/L
2-Naphthylamine
91-59-8
8270E
ND
8.0
0.14
ug/L
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
5-Nitro-o-toluidine
99-55-8
8270E
ND
8.0
2.2
ug/L
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
N-Nitroso-di-butylamine
924-16-3
8270E
ND
4.0
1.1
ug/L
N-Nitrosodiethylamine
55-18-5
8270E
ND
4.0
0.80
ug/L
N-Nitrosodimethylamine
62-75-9
8270E
ND
4.0
0.50
ug/L
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
N-Nitrosomethylethylamine
10595-95-6
8270E
ND
5.0
1.8
ug/L
N-Nitrosopiperidine
100-75-4
8270E
ND
4.0
1.4
ug/L
N-Nitrosopyrrolidine
930-55-2
8270E
ND
4.0
2.1
ug/L
Pentachlorobenzene
608-93-5
8270E
ND
4.0
0.70
ug/L
Pentachloronitrobenzene
82-68-8
8270E
ND
16
2.6
ug/L
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
Phenacetin
62-44-2
8270E
ND
4.0
3.4
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-009
Description: MW-6 Matrix: Aqueous
Date Sampled:10/27/2020 1445
Date Received:10/28/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1628 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
p-Phenylenediamine
106-50-3
8270E
ND
40
11
ug/L
Phorate
298-02-2
8270E
ND
4.0
3.6
ug/L
Pronamide
23950-58-5
8270E
ND
8.0
3.0
ug/L
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
Safrole
94-59-7
8270E
ND
5.0
0.90
ug/L
Sulfotepp
3689-24-5
8270E
ND
8.0
0.60
ug/L
1,2,4,5-Tetrachlorobenzene
95-94-3
8270E
ND
4.0
0.90
ug/L
2,3,4,6-Tetrachlorophenol
58-90-2
8270E
ND
8.0
0.80
ug/L
o-Toluidine
95-53-4
8270E
ND
4.0
0.90
ug/L
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
4.0
0.50
ug/L
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
0,0,0-Triethylphosphorothioate
126-68-1
8270E
ND
4.0
1.3
ug/L
1,3,5-Trinitrobenzene
99-35-4
8270E
ND
16
13
ug/L
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
63
37-129
2-Fluorophenol
N 13
24-127
Nitrobenzene-d5
68
38-127
Phenol-d5
29
28-128
Terphenyl-d14
85
10-148
2,4,6-Tribromophenol
41
35-144
Herbicides by GC
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 8151A
8151A 1 10/30/2020 2037 JJG
10/29/2020 2037
71691
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
2,4,5-T
93-76-5 8151A
ND
0.50
0.13
ug/L
1
2,4-D
94-75-7 8151A
ND
2.0
0.50
ug/L
1
Dinoseb
88-85-7 8151A
ND
1.0
0.50
ug/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.50
0.13
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
84 50-112
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 46 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-009
Description: MW-6 Matrix: Aqueous
Date Sampled:10/27/2020 1445
Date Received:10/28/2020
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
3665A 8082A
1 11/05/2020 1349 NCM
11/03/2020 2330 72148
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1221
11104-28-2 8082A
ND
0.40
0.25
ug/L
1
Aroclor 1232
11141-16-5 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1242
53469-21-9 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1248
12672-29-6 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1254
11097-69-1 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1260
11096-82-5 8082A
ND
0.40
0.15
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery
Limits
Decachlorobiphenyl
59 10-133
Tetrachloro-m-xylene
82 31-122
Organochlorine
Pesticides by GC
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8081B
1 11/06/20201121 DAL1
11/03/20202330 72139
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aldrin
309-00-2 8081B
ND
0.040
0.020
ug/L
1
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.040
0.017
ug/L
1
alpha-BHC
319-84-6 8081B
ND
0.040
0.015
ug/L
1
beta-BHC
319-85-7 8081B
0.025 JP
0.040
0.015
ug/L
1
delta-BHC
319-86-8 8081B
ND
0.040
0.015
ug/L
1
cis -Chlordane
5103-71-9 8081B
ND
0.040
0.015
ug/L
1
trans -Chlordane
5103-74-2 8081B
ND
0.040
0.015
ug/L
1
4,4'-DDD
72-54-8 8081B
ND
0.040
0.015
ug/L
1
4,4'-DDE
72-55-9 8081B
ND
0.040
0.020
ug/L
1
4,4'-DDT
50-29-3 8081B
ND
0.040
0.020
ug/L
1
Dieldrin
60-57-1 8081B
ND
0.040
0.015
ug/L
1
Endosulfan 1
959-98-8 8081B
ND
0.040
0.015
ug/L
1
Endosulfan II
33213-65-9 8081B
0.042 P
0.040
0.015
ug/L
1
Endosulfan sulfate
1031-07-8 8081B
ND
0.040
0.015
ug/L
1
Endrin
72-20-8 8081B
ND
0.040
0.015
ug/L
1
Endrin aldehyde
7421-93-4 8081B
0.020 J
0.040
0.015
ug/L
1
Endrin ketone
53494-70-5 8081B
ND
0.040
0.015
ug/L
1
Heptachlor
76-44-8 8081B
ND
0.040
0.021
ug/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.040
0.016
ug/L
1
Methoxychlor
72-43-5 8081B
ND
0.16
0.021
ug/L
1
Toxaphene
8001-35-2 8081B
ND
0.40
0.30
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result
< LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 47 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-009
Description: MW-6 Matrix: Aqueous
Date Sampled:10/27/2020 1445
Date Received:10/28/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
46 20-122
Tetrachloro-m-xylene
60 46-119
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/13/2020 0856 JAB2
11/13/2020 0552 73376
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7470A
ND
0.00020
0.000091
mg/L
1
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2020 2052 BPK
10/30/2020 1549
71571
2 3005A
6020B
10 11/03/2020 1845 BPK
10/30/2020 1549
71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
1400
50
13
ug/L
2
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.9 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
9.8
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
1.3 J
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Tin
7440-31-5 6020B
ND
20
5.0
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
Footnote(s): 2-G:G Higher than valid range 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 48 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-010
Description: MW-6-192 Matrix: Aqueous
Date Sampled:10/27/2020 1625
Date Received:10/28/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1537 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
8.5
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
94 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/05/20201409 TML
72367
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
1.3
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
0.75 J
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
0.61 J
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
0.66 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 49 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-010
Description: MW-6-192 Matrix: Aqueous
Date Sampled:10/27/2020 1625
Date Received:10/28/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/05/20201409 TML 72367
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
93 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2020 2100 BPK
10/30/2020 1549 71571
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
59
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
1.7 J
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 50 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-010
Description: MW-6-192 Matrix: Aqueous
Date Sampled:10/27/2020 1625
Date Received:10/28/2020
ICP-MS Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 11/02/2020 2100 BPK 10/30/2020 1549 71571
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Selenium
7782-49-2
Silver
7440-22-4
Thallium
7440-28-0
Vanadium
7440-62-2
Zinc
7440-66-6
6020B
ND
5.0
1.3
ug/L 1
6020B
ND
1.0
0.25
ug/L 1
6020B
ND
0.50
0.15
ug/L 1
6020B
ND
5.0
2.5
ug/L 1
6020B
3.9 J
10
2.5
ug/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 51 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-011
Description: MW-13-35 Matrix: Aqueous
Date Sampled:10/28/2020 0905
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201452 TML 72210
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
1.7
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
6.8
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
4.1
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
17
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1, 1 -Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
2.9
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 52 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-011
Description: MW-13-35 Matrix: Aqueous
Date Sampled:10/28/2020 0905
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201452 TML
72210
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
0.53 J
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
94 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
99 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0044 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
180
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
1.4 J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
4.8 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
5.8 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 53 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-012
Description: MW-13-132 Matrix: Aqueous
Date Sampled:10/28/2020 0940
Date Received:10/30/2020
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 10/31/2020 1511 AAB
72118
1 (BOD, 5 day) SM 521OB-2011
1 11/04/2020 1939 MOM
10/30/2020 2204
13666
1 (Chloride) 9056A
1 10/31/2020 1427 AMR
71951
1 (COD) SM 5220D-2011
1 11/03/2020 2248 SRB
72159
1 (Nitrate - N) 9056A
1 10/31/2020 1427 AMR
71949
1 (Sulfate) 9056A
1 10/31/2020 1427 AMR
71950
1 (Sulfide) SM 4500-S2 F-2011
1 11/04/2020 1552 SRB
72315
1 (TOC) SM 531OC-2011
1 11/02/2020 1414 DMA
71953
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
150
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
3.6 H47
2.0
0.18
mg/L
1
Chloride
9056A
4.7
1.0
0.25
mg/L
1
COD
SM 5220D-2011
ND
20
20
mg/L
1
Nitrate - N
9056A
ND H
0.020
0.0050
mg/L
1
Sulfate
9056A
7.2
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
ND
1.0
1.0
mg/L
1
Volatile Organic Compounds
by GUMS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 11/04/20201515 TML
72210
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
1.4
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL
= Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J =
Estimated result
< LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 54 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-012
Description: MW-13-132 Matrix: Aqueous
Date Sampled:10/28/2020 0940
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201515 TML 72210
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
0.78 J
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
0.73 J
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
4.4
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
1.6
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
94
70-130
1,2-Dichloroethane-d4
91
70-130
Toluene-d8
101
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 3005A
6020B
1 11/04/2020 0052 BPK 11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method Result Q
LOQ DL Units Run
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 55 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-012
Description: MW-13-132 Matrix: Aqueous
Date Sampled:10/28/2020 0940
Date Received:10/30/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0052 BPK
11/03/2020 0936
71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
42
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
3.8 J
10
2.5
ug/L
1
Footnote(s): 4-Blank depletion > 0.20 mg/L 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 56 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-013
Description: MW-12-25 Matrix: Aqueous
Date Sampled:10/28/2020 1010
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201538 TML 72210
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 57 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-013
Description: MW-12-25 Matrix: Aqueous
Date Sampled:10/28/2020 1010
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201538 TML
72210
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
94 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
102 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0059 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
55
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.5 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
17
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
13
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 58 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-014
Description: MW-4A Matrix: Aqueous
Date Sampled:10/28/2020 1135
Date Received:10/30/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1602 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
20
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
92 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201602 TML
72210
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
2.8
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
13
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
3.5
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
32
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 59 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-014
Description: MW-4A Matrix: Aqueous
Date Sampled:10/28/2020 1135
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201602 TML 72210
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
1.5
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
1.2
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.51 J
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
3.2
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
101 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/04/2020 0137 BPK
11/03/2020 0936 71919
2 3005A
6020B
10 11/04/2020 1513 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
0.79 J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
540
50
13
ug/L
2
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.17 J
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
33
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.6 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 60 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-014
Description: MW-4A Matrix: Aqueous
Date Sampled:10/28/2020 1135
Date Received:10/30/2020
ICP-MS Metals
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3005A
6020B
1
11/04/2020 0137 BPK
11/03/2020 0936 71919
2
3005A
6020B
10
11/04/2020 1513 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel
7440-02-0
Selenium
7782-49-2
Silver
7440-22-4
Thallium
7440-28-0
Vanadium
7440-62-2
Zinc
7440-66-6
6020B
12
5.0
1.3
ug/L 1
6020B
ND
5.0
1.3
ug/L 1
6020B
ND
1.0
0.25
ug/L 1
6020B
ND
0.50
0.15
ug/L 1
6020B
ND
5.0
2.5
ug/L 1
6020B
2.9 J
10
2.5
ug/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 61 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-015
Description: MW-24-160 Matrix: Aqueous
Date Sampled:10/28/2020 1345
Date Received:10/30/2020
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 10/31/2020 1517 AAB
72118
1 (BOD, 5 day) SM 521OB-2011
1 11/04/2020 1939 MOM
10/30/2020 2204
13666
1 (Chloride) 9056A
1 10/31/2020 1446 AMR
71951
1 (COD) SM 5220D-2011
1 11/03/2020 2248 SRB
72159
1 (Nitrate - N) 9056A
1 10/31/2020 1446 AMR
71949
1 (Sulfate) 9056A
1 10/31/2020 1446 AMR
71950
1 (Sulfide) SM 4500-S2 F-2011
1 11/04/2020 1552 SRB
72315
1 (TOC) SM 531OC-2011
1 11/02/2020 1428 DMA
71953
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
64
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
2.0 H47
2.0
0.18
mg/L
1
Chloride
9056A
6.4
1.0
0.25
mg/L
1
COD
SM 5220D-2011
ND
20
20
mg/L
1
Nitrate - N
9056A
ND H
0.020
0.0050
mg/L
1
Sulfate
9056A
27
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
1.1
1.0
1.0
mg/L
1
Volatile Organic Compounds
by GUMS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 11/04/20201625 TML
72210
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL
= Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J =
Estimated result
< LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 62 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-015
Description: MW-24-160 Matrix: Aqueous
Date Sampled:10/28/2020 1345
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201625 TML 72210
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
95
70-130
1,2-Dichloroethane-d4
92
70-130
Toluene-d8
102
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 3005A
6020B
1 11/04/2020 0144 BPK 11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method Result Q
LOQ DL Units Run
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 63 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-015
Description: MW-24-160 Matrix: Aqueous
Date Sampled:10/28/2020 1345
Date Received:10/30/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep
Date
Batch
1 3005A
6020B 1 11/04/2020 0144 BPK
11/03/2020
0936
71919
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
0.52
J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
38
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.19
J
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
1.3
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
3.9
J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
2.0
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
3.6
J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
16
10
2.5
ug/L
1
Footnote(s): 4-Blank depletion > 0.20 mg/L 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 64 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-016
Description: MW-15 Matrix: Aqueous
Date Sampled:10/28/2020 1545
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201023 TML 72211
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
19 J
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 65 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-016
Description: MW-15 Matrix: Aqueous
Date Sampled:10/28/2020 1545
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201023 TML
72211
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
107 70-130
1,2-Dichloroethane-d4
95 70-130
Toluene-d8
97 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0152 BPK
11/03/2020 0936 71919
2 3005A
6020B 5 11/04/2020 1520 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
10
6.3
ug/L
2
Barium
7440-39-3 6020B
210
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
2.0
0.75
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
12 J
25
6.3
ug/L
2
Cobalt
7440-48-4 6020B
ND
25
6.3
ug/L
2
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
1.1
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
25
6.3
ug/L
2
Selenium
7782-49-2 6020B
ND
25
6.3
ug/L
2
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
25
13
ug/L
2
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 66 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-017
Description: MW-B Matrix: Aqueous
Date Sampled:10/29/2020 0945
Date Received:10/30/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1626 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
36
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
93 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201045 TML
72211
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
5.1 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
1.2
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
0.60 J
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
1.9
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
1.7
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
21
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 67 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-017
Description: MW-B Matrix: Aqueous
Date Sampled:10/29/2020 0945
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201045 TML 72211
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
10
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
100 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
97 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/04/2020 0214 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
170
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 68 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-017
Description: MW-B Matrix: Aqueous
Date Sampled:10/29/2020 0945
Date Received:10/30/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0214 BPK
11/03/2020 0936
71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 69 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-018
Description: MW-17-137 Matrix: Aqueous
Date Sampled:10/29/2020 1045
Date Received:10/30/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1651 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
34
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
93 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201108 TML
72211
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
7.2 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
0.47 J
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
0.65 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 70 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-018
Description: MW-17-137 Matrix: Aqueous
Date Sampled:10/29/2020 1045
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201108 TML 72211
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.54 J
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
0.50 J
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
98 70-130
1,2-Dichloroethane-d4
95 70-130
Toluene-d8
95 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/04/2020 0221 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
24
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 71 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-018
Description: MW-17-137 Matrix: Aqueous
Date Sampled:10/29/2020 1045
Date Received:10/30/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0221 BPK
11/03/2020 0936
71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 72 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-019
Description: MW-17-60 Matrix: Aqueous
Date Sampled:10/29/2020 1240
Date Received:10/30/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2020 1715 BWS
72081
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
23
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
93 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201130 TML
72211
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
6.9 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
5.3 J
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
0.68 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
1.0
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 73 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-019
Description: MW-17-60 Matrix: Aqueous
Date Sampled:10/29/2020 1240
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201130 TML 72211
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
101 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
94 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/04/2020 0229 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
20
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 74 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-019
Description: MW-17-60 Matrix: Aqueous
Date Sampled:10/29/2020 1240
Date Received:10/30/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0229 BPK
11/03/2020 0936
71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 75 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-020
Description: MW-17-310 Matrix: Aqueous
Date Sampled:10/29/2020 1530
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201152 TML 72211
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 76 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-020
Description: MW-17-310 Matrix: Aqueous
Date Sampled:10/29/2020 1530
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201152 TML
72211
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
93 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0237 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
3.1 J
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.37 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
4.6 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 77 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-021
Description: MW-2 Matrix: Aqueous
Date Sampled:10/29/2020 1705
Date Received:10/30/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 10/31/2020 1523 AAB
72118
1
(BOD, 5 day) SM 521OB-2011
1 11/04/2020 1939 MOM
10/30/2020 2204
13666
1
(Chloride) 9056A
1 10/31/2020 1331 AMR
71951
1
(COD) SM 5220D-2011
1 11/03/2020 2248 SRB
72159
1
(Nitrate - N) 9056A
1 10/31/2020 1331 AMR
71949
1
(Sulfate) 9056A
1 10/31/2020 1331 AMR
71950
1
(Sulfide) SM 4500-S2 F-2011
1 11/04/2020 1552 SRB
72315
1
(TOC) SM 531OC-2011
1 11/02/2020 1440 DMA
71953
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 232OB-2011
60
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521OB-2011
ND 47
2.0
0.18
mg/L
1
Chloride
9056A
2.1
1.0
0.25
mg/L
1
COD
SM 5220D-2011
ND
20
20
mg/L
1
Nitrate - N
9056A
0.028
0.020
0.0050
mg/L
1
Sulfate
9056A
4.1
1.0
0.25
mg/L
1
Sulfide
18496-25-8 SM 4500-S2 F-2
ND
1.0
0.99
mg/L
1
TOC
SM 531OC-2011
ND
1.0
1.0
mg/L
1
Volatile Organic Compounds
by GUMS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/04/20201215 TML
72211
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acetonitrile
75-05-8 8260D
ND
50
15
ug/L
1
Acrolein
107-02-8 8260D
ND
20
4.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl
bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
2-Chloro-1,3-Butadiene
(Chloroprene)
126-99-8 8260D
ND
5.0
1.0
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl
chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
3-Chloropropene (Allyl chloride)
107-05-1 8260D
ND
5.0
1.0
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL
= Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J =
Estimated result
< LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 78 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-021
Description: MW-2 Matrix: Aqueous
Date Sampled:10/29/2020 1705
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201215 TML 72211
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,3-Dichlorobenzene
541-73-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
Dichlorodifluoromethane
75-71-8
8260D
ND
2.0
0.60
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1,3-Dichloropropane
142-28-9
8260D
ND
1.0
0.40
ug/L
2,2-Dichloropropane
594-20-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloropropene
563-58-6
8260D
ND
2.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethyl methacrylate
97-63-2
8260D
ND
5.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Isobutyl alcohol
78-83-1
8260D
ND
50
12
ug/L
Methacrylonitrile
126-98-7
8260D
ND
5.0
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
Methyl methacrylate
80-62-6
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Propionitrile (Ethyl cyanide)
107-12-0
8260D
ND
20
4.0
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 79 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-021
Description: MW-2 Matrix: Aqueous
Date Sampled:10/29/2020 1705
Date Received:10/30/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201215 TML
72211
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
105 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
96 70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E 1 11/13/2020 1653 SCD
11/03/2020 1919 72150
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9 8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8 8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2 8270E
ND
4.0
0.50
ug/L
1
2-Acetylaminofluorene
53-96-3 8270E
ND
8.0
1.7
ug/L
1
4-Aminobiphenyl
92-67-1 8270E
ND
8.0
1.1
ug/L
1
Anthracene
120-12-7 8270E
ND
0.80
0.20
ug/L
1
Benzo(a)anthracene
56-55-3 8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8 8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2 8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2 8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9 8270E
ND
0.80
0.20
ug/L
1
Benzyl alcohol
100-51-6 8270E
ND
4.0
0.30
ug/L
1
4-Bromophenyl phenyl ether
101-55-3 8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7 8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1 8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7 8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8 8270E
ND
8.0
0.50
ug/L
1
Chlorobenzilate
510-15-6 8270E
ND
10
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1 8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4 8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7 8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8 8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3 8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9 8270E
ND
0.80
0.20
ug/L
1
cis-Diallate
17708-57-5 8270E
ND
8.0
1.9
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 80 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-021
Description: MW-2 Matrix: Aqueous
Date Sampled:10/29/2020 1705
Date Received:10/30/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1653 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans-Diallate
17708-58-6
8270E
ND
8.0
1.9
ug/L
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8270E
ND
4.0
0.50
ug/L
1,3-Dichlorobenzene
541-73-1
8270E
ND
4.0
0.50
ug/L
1,4-Dichlorobenzene
106-46-7
8270E
ND
4.0
0.60
ug/L
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
2,6-Dichlorophenol
87-65-0
8270E
ND
4.0
1.6
ug/L
0,0-Diethyl-0-2-pyrazinyl (Thionazin)
297-97-2
8270E
ND
4.0
0.90
ug/L
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
Dimethoate
60-51-5
8270E
ND
8.0
2.8
ug/L
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
p-(Dimethylamino)azobenzene
60-11-7
8270E
ND
10
0.53
ug/L
3,3'-Dimethylbenzidine
119-93-7
8270E
ND
16
10
ug/L
7,12-Dimethylbenzo(a)anthracene
57-97-6
8270E
ND
4.0
1.1
ug/L
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1,3-Dinitrobenzene
99-65-0
8270E
ND
16
13
ug/L
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
Ethyl methanesulfonate
62-50-0
8270E
ND
5.0
0.70
ug/L
Ethyl parathion
56-38-2
8270E
ND
16
2.8
ug/L
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
Famphur
52-85-7
8270E
ND
16
13
ug/L
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
Hexachloropropene
1888-71-7
8270E
ND
8.0
0.80
ug/L
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
Isodrin
465-73-6
8270E
ND
4.0
0.70
ug/L
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
Isosafrole
120-58-1
8270E
ND
4.0
1.1
ug/L
Methapyrilene
91-80-5
8270E
ND
16
8.8
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 81 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-021
Description: MW-2 Matrix: Aqueous
Date Sampled:10/29/2020 1705
Date Received:10/30/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1653 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Methyl methanesulfonate
66-27-3
8270E
ND
4.0
0.50
ug/L
Methyl parathion
298-00-0
8270E
ND
16
2.0
ug/L
3-Methylcholanthrene
56-49-5
8270E
ND
8.0
5.0
ug/L
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1,4-Naphthoquinone
130-15-4
8270E
ND
8.0
0.40
ug/L
1-Naphthylamine
134-32-7
8270E
ND
8.0
0.030
ug/L
2-Naphthylamine
91-59-8
8270E
ND
8.0
0.14
ug/L
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
5-Nitro-o-toluidine
99-55-8
8270E
ND
8.0
2.2
ug/L
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
N-Nitroso-di-butylamine
924-16-3
8270E
ND
4.0
1.1
ug/L
N-Nitrosodiethylamine
55-18-5
8270E
ND
4.0
0.80
ug/L
N-Nitrosodimethylamine
62-75-9
8270E
ND
4.0
0.50
ug/L
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
N-Nitrosomethylethylamine
10595-95-6
8270E
ND
5.0
1.8
ug/L
N-Nitrosopiperidine
100-75-4
8270E
ND
4.0
1.4
ug/L
N-Nitrosopyrrolidine
930-55-2
8270E
ND
4.0
2.1
ug/L
Pentachlorobenzene
608-93-5
8270E
ND
4.0
0.70
ug/L
Pentachloronitrobenzene
82-68-8
8270E
ND
16
2.6
ug/L
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
Phenacetin
62-44-2
8270E
ND
4.0
3.4
ug/L
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
p-Phenylenediamine
106-50-3
8270E
ND
40
11
ug/L
Phorate
298-02-2
8270E
ND
4.0
3.6
ug/L
Pronamide
23950-58-5
8270E
ND
8.0
3.0
ug/L
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
Safrole
94-59-7
8270E
ND
5.0
0.90
ug/L
Sulfotepp
3689-24-5
8270E
ND
8.0
0.60
ug/L
1,2,4,5-Tetrachlorobenzene
95-94-3
8270E
ND
4.0
0.90
ug/L
2,3,4,6-Tetrachlorophenol
58-90-2
8270E
ND
8.0
0.80
ug/L
o-Toluidine
95-53-4
8270E
ND
4.0
0.90
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 82 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-021
Description: MW-2 Matrix: Aqueous
Date Sampled:10/29/2020 1705
Date Received:10/30/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 11/13/2020 1653 SCD 11/03/2020 1919 72150
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
4.0
0.50
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
0,0,0-Triethylphosphorothioate
126-68-1
8270E
ND
4.0
1.3
ug/L
1
1,3,5-Trinitrobenzene
99-35-4
8270E
ND
16
13
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
62 37-129
2-Fluorophenol
31 24-127
Nitrobenzene-d5
65 38-127
Phenol-d5
42 28-128
Terphenyl-d14
78 10-148
2,4,6-Tribromophenol
80 35-144
Herbicides by GC
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 8151A 8151A 1 11/05/2020 1556 JJG 11/04/2020 1924 72317
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2,4,5-T
93-76-5
8151A
ND
0.50
0.13
ug/L
1
2,4-D
94-75-7
8151A
ND
2.0
0.50
ug/L
1
Dinoseb
88-85-7
8151A
ND
1.0
0.50
ug/L
1
2,4,5-TP (Silvex)
93-72-1
8151A
ND
0.50
0.13
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
72 50-112
PCBs by GC
Run Prep Method
Cleanup
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
3665A
8082A
1 11/05/2020 1402 NCM
11/03/2020 2330 72148
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1221
11104-28-2 8082A
ND
0.40
0.25
ug/L
1
Aroclor 1232
11141-16-5 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1242
53469-21-9 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1248
12672-29-6 8082A
ND
0.40
0.15
ug/L
1
Aroclor 1254
11097-69-1 8082A
ND
0.40
0.15
ug/L
1
LOQ = Limit of Quantitation
B =
Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 83 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-021
Description: MW-2 Matrix: Aqueous
Date Sampled:10/29/2020 1705
Date Received:10/30/2020
PCBs by GC
Run Prep Method Cleanup
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C 3665A
8082A
1 11/05/2020 1402 NCM
11/03/2020 2330 72148
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aroclor 1260
11096-82-5 8082A
ND
0.40
0.15
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
94 10-133
Tetrachloro-m-xylene
79 31-122
Organochlorine
Pesticides by GC
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8081 B
1 11/05/2020 2004 DAL1
11/03/2020 2330 72139
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aldrin
309-00-2 8081B
ND
0.040
0.020
ug/L
1
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.040
0.017
ug/L
1
alpha-BHC
319-84-6 8081B
ND
0.040
0.015
ug/L
1
beta-BHC
319-85-7 8081B
ND
0.040
0.015
ug/L
1
delta-BHC
319-86-8 8081B
ND
0.040
0.015
ug/L
1
cis -Chlordane
5103-71-9 8081B
ND
0.040
0.015
ug/L
1
trans -Chlordane
5103-74-2 8081B
ND
0.040
0.015
ug/L
1
4,4'-DDD
72-54-8 8081B
ND
0.040
0.015
ug/L
1
4,4'-DDE
72-55-9 8081B
ND
0.040
0.020
ug/L
1
4,4'-DDT
50-29-3 8081B
ND
0.040
0.020
ug/L
1
Dieldrin
60-57-1 8081B
ND
0.040
0.015
ug/L
1
Endosulfan 1
959-98-8 8081B
ND
0.040
0.015
ug/L
1
Endosulfan 11
33213-65-9 8081B
ND
0.040
0.015
ug/L
1
Endosulfan sulfate
1031-07-8 8081B
ND
0.040
0.015
ug/L
1
Endrin
72-20-8 8081B
ND
0.040
0.015
ug/L
1
Endrin aldehyde
7421-93-4 8081B
ND
0.040
0.015
ug/L
1
Endrin ketone
53494-70-5 8081B
ND
0.040
0.015
ug/L
1
Heptachlor
76-44-8 8081B
ND
0.040
0.021
ug/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.040
0.016
ug/L
1
Methoxychlor
72-43-5 8081B
ND
0.16
0.021
ug/L
1
Toxaphene
8001-35-2 8081B
ND
0.40
0.30
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
82 20-122
Tetrachloro-m-xylene
66 46-119
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 84 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-021
Description: MW-2 Matrix: Aqueous
Date Sampled:10/29/2020 1705
Date Received:10/30/2020
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/13/2020 0858 JAB2
11/13/2020 0552 73376
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7470A
ND
0.00020
0.000091
mg/L
1
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/04/2020 0244 BPK
11/03/2020 0936 71919
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
0.55 J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
20
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.8 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
2.5 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Tin
7440-31-5 6020B
ND
20
5.0
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
10
10
2.5
ug/L
1
Footnote(s): 4-Blank depletion > 0.20 mg/L 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 85 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-022
Description: MW-7 Matrix: Aqueous
Date Sampled:10/30/2020 1050
Date Received: 11 /02/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
2 5030B
8260D (SIM) 1 11/04/2020 2315 DJG
72318
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
2
Run 2 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
96 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201237 TML
72211
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
16 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
1.7
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
2.3 J
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
9.9
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
3.7
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
3.9
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
2.7
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
25
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 86 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-022
Description: MW-7 Matrix: Aqueous
Date Sampled:10/30/2020 1050
Date Received: 11 /02/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201237 TML 72211
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
0.45 J
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.77 J
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
0.57 J
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
101 70-130
1,2-Dichloroethane-d4
91 70-130
Toluene-d8
95 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/04/2020 0536 BPK
11/03/2020 0936 72039
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
230
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.72
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
190
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
9.5
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.48 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
64
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 87 of 253

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: VJ27055-022
Description: MW-7 Matrix: Aqueous
Date Sampled:10/30/2020 1050
Date Received: 11 /02/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/04/2020 0536 BPK
11/03/2020 0936
72039
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
13
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 88 of 253

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 89 of 253

Inorganic non-metals - LCS
Sample ID: VQ71525-002 Matrix: Aqueous
Batch: 71525
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg CaCO3/L) (mg CaCO3/L) Q Dil % Rec Limit Analysis Date
Alkalinity @ pH 4.5 su 100 96 1 96 90-110 10/28/2020 1816
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 90 of 253

Inorganic non-metals - MB
Sample ID: VQ71682-001 Matrix: Aqueous
Batch: 71682
Analytical Method: SM 531 OC-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
TOC ND 1 1.0 1.0 mg/L 10/29/20201833
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 91 of 253

Inorganic non-metals - LCS
Sample ID: VQ71682-002 Matrix: Aqueous
Batch: 71682
Analytical Method: SM 531 OC-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TOC 20 20 1 99 90-110 10/29/20201846
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 92 of 253

Inorganic non-metals - MB
Sample ID: VQ71726-001 Matrix: Aqueous
Batch: 71726
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Nitrate - N 0.012 J 1 0.020 0.0050 mg/L 10/28/2020 0912
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 93 of 253

Inorganic non-metals - LCS
Sample ID: VQ71726-002 Matrix: Aqueous
Batch: 71726
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.80 0.83 1 104 80-120 10/28/2020 0950
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 94 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-0O2MS Matrix: Aqueous
Batch: 71726
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N ND 0.40 0.37 1 93 80-120 10/28/2020 1047
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 95 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-0O2MD Matrix: Aqueous
Batch: 71726
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Nitrate - N ND 0.40 0.38 1 95 2.7 80-120 20 10/28/2020 1106
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 96 of 253

Inorganic non-metals - MB
Sample ID: VQ71727-001 Matrix: Aqueous
Batch: 71727
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride ND 1 1.0 0.20 mg/L 10/28/2020 0912
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 97 of 253

Inorganic non-metals - LCS
Sample ID: VQ71727-002 Matrix: Aqueous
Batch: 71727
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 21 1 103 80-120 10/28/2020 0950
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 98 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-0O2MS Matrix: Aqueous
Batch: 71727
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 39 10 49 1 100 80-120 10/28/20201047
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 99 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-0O2MD Matrix: Aqueous
Batch: 71727
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Chloride 39 10 49 1 103 0.62 80-120 20 10/28/20201106
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 100 of 253

Inorganic non-metals - MB
Sample ID: VQ71729-001 Matrix: Aqueous
Batch: 71729
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate ND 1 1.0 0.20 mg/L 10/28/2020 0912
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 101 of 253

Inorganic non-metals - LCS
Sample ID: VQ71729-002 Matrix: Aqueous
Batch: 71729
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 21 1 102 80-120 10/28/2020 0950
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 102 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-0O2MS Matrix: Aqueous
Batch: 71729
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 9.7 10 19 1 95 80-120 10/28/20201047
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 103 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-0O2MD Matrix: Aqueous
Batch: 71729
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 9.7 10 20 1 98 1.6 80-120 20 10/28/20201106
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 104 of 253

Inorganic non-metals - MB
Sample ID: VQ71732-001 Matrix: Aqueous
Batch: 71732
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride ND 1 1.0 0.20 mg/L 10/28/20201610
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 105 of 253

Inorganic non-metals - LCS
Sample ID: VQ71732-002 Matrix: Aqueous
Batch: 71732
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 19 1 96 80-120 10/28/20201647
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 106 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-003MS Matrix: Aqueous
Batch: 71732
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 89 10 98 1 91 80-120 10/28/2020 2112
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 107 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-003MD Matrix: Aqueous
Batch: 71732
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Chloride 89 10 99 1 96 0.51 80-120 20 10/28/2020 2131
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 108 of 253

Inorganic non-metals - MB
Sample ID: VQ71733-001 Matrix: Aqueous
Batch: 71733
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate ND 1 1.0 0.20 mg/L 10/28/20201610
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 109 of 253

Inorganic non-metals - LCS
Sample ID: VQ71733-002 Matrix: Aqueous
Batch: 71733
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 19 1 93 80-120 10/28/20201647
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 110 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-003MS Matrix: Aqueous
Batch: 71733
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 2.2 10 11 1 85 80-120 10/28/2020 2112
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 111 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-003MD Matrix: Aqueous
Batch: 71733
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 2.2 10 11 1 83 1.9 80-120 20 10/28/2020 2131
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 112 of 253

Inorganic non-metals - MB
Sample ID: VQ71842-001 Matrix: Aqueous
Batch: 71842
Analytical Method: SM 4500-S2 F-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfide ND 1 1.0 0.99 mg/L 10/30/2020 2119
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 113 of 253

Inorganic non-metals - LCS
Sample ID: VQ71842-002 Matrix: Aqueous
Batch: 71842
Analytical Method: SM 4500-S2 F-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfide 10 9.6 1 96 80-120 10/30/2020 2119
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 114 of 253

Inorganic non-metals - LCSD
Sample ID: VQ71842-003 Matrix: Aqueous
Batch: 71842
Analytical Method: SM 4500-S2 F-2011
Spike
Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfide 10 9.6 1 96 0.00 80-120 20 10/30/2020 2119
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 115 of 253

Inorganic non-metals - MB
Sample ID: VQ71940-001 Matrix: Aqueous
Batch: 71940
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Nitrate - N ND 1 0.020 0.0050 mg/L 10/30/2020 1254
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 116 of 253

Inorganic non-metals - LCS
Sample ID: VQ71940-002 Matrix: Aqueous
Batch: 71940
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.80 0.78 1 98 80-120 10/30/2020 1341
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 117 of 253

Inorganic non-metals - MB
Sample ID: VQ71943-001 Matrix: Aqueous
Batch: 71943
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride ND 1 1.0 0.25 mg/L 10/30/20201254
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 118 of 253

Inorganic non-metals - LCS
Sample ID: VQ71943-002 Matrix: Aqueous
Batch: 71943
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 19 1 97 80-120 10/30/20201341
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 119 of 253

Inorganic non-metals - MB
Sample ID: VQ71944-001 Matrix: Aqueous
Batch: 71944
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate ND 1 1.0 0.25 mg/L 10/30/20201254
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 120 of 253

Inorganic non-metals - LCS
Sample ID: VQ71944-002 Matrix: Aqueous
Batch: 71944
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 19 1 95 80-120 10/30/20201341
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 121 of 253

Inorganic non-metals - MB
Sample ID: VQ71949-001 Matrix: Aqueous
Batch: 71949
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Nitrate - N ND 1 0.020 0.0050 mg/L 10/31/2020 1037
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 122 of 253

Inorganic non-metals - LCS
Sample ID: VQ71949-002 Matrix: Aqueous
Batch: 71949
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.80 0.76 1 96 80-120 10/31/2020 1115
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 123 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-021 MS Matrix: Aqueous
Batch: 71949
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.028 0.40 0.37 1 85 80-120 10/31/2020 1349
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 124 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-021MD Matrix: Aqueous
Batch: 71949
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Nitrate - N 0.028 0.40 0.37 1 87 1.3 80-120 20 10/31/2020 1408
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 125 of 253

Inorganic non-metals - MB
Sample ID: VQ71950-001 Matrix: Aqueous
Batch: 71950
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate ND 1 1.0 0.25 mg/L 10/31/20201037
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 126 of 253

Inorganic non-metals - LCS
Sample ID: VQ71950-002 Matrix: Aqueous
Batch: 71950
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 19 1 94 80-120 10/31/20201115
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 127 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-021 MS Matrix: Aqueous
Batch: 71950
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 4.1 10 11 N 1 70 80-120 10/31/20201349
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 128 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-021MD Matrix: Aqueous
Batch: 71950
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 4.1 10 11 N 1 70 0.25 80-120 20 10/31/20201408
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 129 of 253

Inorganic non-metals - MB
Sample ID: VQ71951-001 Matrix: Aqueous
Batch: 71951
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride ND 1 1.0 0.25 mg/L 10/31/20201037
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 130 of 253

Inorganic non-metals - LCS
Sample ID: VQ71951-002 Matrix: Aqueous
Batch: 71951
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 19 1 96 80-120 10/31/20201115
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 131 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-021 MS Matrix: Aqueous
Batch: 71951
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 2.1 10 11 1 92 80-120 10/31/20201349
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 132 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-021MD Matrix: Aqueous
Batch: 71951
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Chloride 2.1 10 11 1 92 0.62 80-120 20 10/31/20201408
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 133 of 253

Inorganic non-metals - MB
Sample ID: VQ71953-001 Matrix: Aqueous
Batch: 71953
Analytical Method: SM 531 OC-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
TOC ND 1 1.0 1.0 mg/L 11102120201348
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 134 of 253

Inorganic non-metals - LCS
Sample ID: VQ71953-002 Matrix: Aqueous
Batch: 71953
Analytical Method: SM 531 OC-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TOC 20 19 1 97 90-110 11102120201401
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 135 of 253

Inorganic non-metals - MS
Sample ID: VJ27055-021 MS Matrix: Aqueous
Batch: 71953
Analytical Method: SM 531 OC-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TOC ND 50 49 1 98 70-130 11102120201454
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 136 of 253

Inorganic non-metals - MSD
Sample ID: VJ27055-021MD Matrix: Aqueous
Batch: 71953
Analytical Method: SM 531 OC-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
TOC ND 50 49 1 98 0.35 70-130 20 11102120201507
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 137 of 253

Inorganic non-metals - LCS
Sample ID: VQ72118-002 Matrix: Aqueous
Batch: 72118
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg CaCO3/L) (mg CaCO3/L) Q Dil % Rec Limit Analysis Date
Alkalinity @ pH 4.5 su 100 97 1 97 90-110 10/31/2020 1405
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 138 of 253

Inorganic non-metals - Duplicate
Sample ID: VJ27055-008DU Matrix: Aqueous
Batch: 72118
Analytical Method: SM 2320B-2011
Sample
Amount Result % RPD
Parameter (mg CaCO3/L) (mg CaCO3/L) 0 Dil % RPD Limit Analysis Date
Alkalinity @ pH 4.5 su 420 430 1 1.4 20 10/31/2020 1505
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 139 of 253

Inorganic non-metals - MB
Sample ID: VQ72159-001 Matrix: Aqueous
Batch: 72159
Analytical Method: SM 5220D-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
COD ND 1 20 20 mg/L 11/03/2020 2243
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 140 of 253

Inorganic non-metals - LCS
Sample ID: VQ72159-002 Matrix: Aqueous
Batch: 72159
Analytical Method: SM 5220D-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
COD 40 39 1 98 95-105 11/03/2020 2243
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 141 of 253

Inorganic non-metals - MB
Sample ID: VQ72216-001 Matrix: Aqueous
Batch: 72216
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Nitrate - N ND 1 0.020 0.0050 mg/L 11/03/2020 1655
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 142 of 253

Inorganic non-metals - LCS
Sample ID: VQ72216-002 Matrix: Aqueous
Batch: 72216
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.80 0.79 1 98 80-120 11/03/2020 1733
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 143 of 253

Inorganic non-metals - MB
Sample ID: VQ72315-001 Matrix: Aqueous
Batch: 72315
Analytical Method: SM 4500-S2 F-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfide ND 1 1.0 0.99 mg/L 11/04/20201552
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 144 of 253

Inorganic non-metals - LCS
Sample ID: VQ72315-002 Matrix: Aqueous
Batch: 72315
Analytical Method: SM 4500-S2 F-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfide 5.0 5.1 1 102 80-120 11/04/20201552
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 145 of 253

Inorganic non-metals - LCSD
Sample ID: VQ72315-003 Matrix: Aqueous
Batch: 72315
Analytical Method: SM 4500-S2 F-2011
Spike
Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfide 5.0 5.0 1 100 2.0 80-120 20 11/04/20201552
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 146 of 253

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: VQ71945-001 Matrix: Aqueous
Batch: 71945 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11102120201010
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
95 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 147 of 253

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: VQ71945-002 Matrix: Aqueous
Batch: 71945 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 52 1 105 70-130 11/02/2020 0910
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
109 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 148 of 253

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: VQ72081-001 Matrix: Aqueous
Batch:72081 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11/03/2020 0941
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
96 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 149 of 253

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: VQ72081-002 Matrix: Aqueous
Batch:72081 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 47 1 93 70-130 11/03/2020 0841
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
101 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 150 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72210-001 Matrix: Aqueous
Batch: 72210 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/04/2020 0912
Acrylonitrile
ND
1
20
0.80
ug/L
11/04/2020 0912
Benzene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Bromoform
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/04/2020 0912
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/04/2020 0912
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Chloroethane
ND
1
2.0
0.40
ug/L
11/04/2020 0912
Chloroform
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/04/2020 0912
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/04/2020 0912
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/04/2020 0912
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
2-Hexanone
ND
1
10
2.0
ug/L
11/04/2020 0912
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/04/2020 0912
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/04/2020 0912
Methylene chloride
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Styrene
ND
1
1.0
0.41
ug/L
11/04/2020 0912
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Toluene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Trichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 0912
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 151 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72210-001 Matrix: Aqueous
Batch: 72210 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/04/2020 0912
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/04/2020 0912
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 103 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 152 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72210-002
Matrix: Aqueous
Batch: 72210
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
84
1
84
60-140
11/04/2020 0745
Acrylonitrile
100
81
1
81
70-130
11/04/2020 0745
Benzene
50
49
1
99
70-130
11/04/2020 0745
Bromochloromethane
50
48
1
96
70-130
11/04/2020 0745
Bromodichloromethane
50
48
1
97
70-130
11/04/2020 0745
Bromoform
50
53
1
106
70-130
11/04/2020 0745
Bromomethane (Methyl bromide)
50
50
1
99
70-130
11/04/2020 0745
2-Butanone (MEK)
100
91
1
91
70-130
11/04/2020 0745
Carbon disulfide
50
47
1
94
70-130
11/04/2020 0745
Carbon tetrachloride
50
49
1
97
70-130
11/04/2020 0745
Chlorobenzene
50
53
1
106
70-130
11/04/2020 0745
Chloroethane
50
47
1
94
70-130
11/04/2020 0745
Chloroform
50
46
1
92
70-130
11/04/2020 0745
Chloromethane (Methyl chloride)
50
48
1
97
60-140
11/04/2020 0745
1,2-Dibromo-3-chloropropane (DBCP)
50
42
1
83
70-130
11/04/2020 0745
Dibromochloromethane
50
51
1
102
70-130
11/04/2020 0745
1,2-Dibromoethane (EDB)
50
52
1
104
70-130
11/04/2020 0745
Dibromomethane (Methylene bromide)
50
50
1
100
70-130
11/04/2020 0745
trans- 1,4-Dichloro-2-butene
50
53
1
106
70-130
11/04/2020 0745
1,2-Dichlorobenzene
50
51
1
101
70-130
11/04/2020 0745
1,4-Dichlorobenzene
50
52
1
104
70-130
11/04/2020 0745
1,1-Dichloroethane
50
47
1
95
70-130
11/04/2020 0745
1,2-Dichloroethane
50
50
1
101
70-130
11/04/2020 0745
1,1-Dichloroethene
50
47
1
95
70-130
11/04/2020 0745
cis- 1,2-Dichloroethene
50
47
1
94
70-130
11/04/2020 0745
trans- 1,2-Dichloroethene
50
47
1
93
70-130
11/04/2020 0745
1,2-Dichloropropane
50
49
1
97
70-130
11/04/2020 0745
cis- 1,3-Dichloropropene
50
50
1
100
70-130
11/04/2020 0745
trans- 1,3-Dichloropropene
50
52
1
105
70-130
11/04/2020 0745
Ethylbenzene
50
53
1
106
70-130
11/04/2020 0745
2-Hexanone
100
100
1
104
70-130
11/04/2020 0745
Methyl iodide (lodomethane)
50
49
1
97
70-130
11/04/2020 0745
4-Methyl-2-pentanone
100
100
1
101
70-130
11/04/2020 0745
Methylene chloride
50
45
1
90
70-130
11/04/2020 0745
Styrene
50
53
1
105
70-130
11/04/2020 0745
1,1,1,2-Tetrachloroethane
50
53
1
106
70-130
11/04/2020 0745
1,1,2,2-Tetrachloroethane
50
50
1
101
70-130
11/04/2020 0745
Tetrachloroethene
50
57
1
113
70-130
11/04/2020 0745
Toluene
50
52
1
105
70-130
11/04/2020 0745
1,1,1-Trichloroethane
50
48
1
96
70-130
11/04/2020 0745
1,1,2-Trichloroethane
50
51
1
102
70-130
11/04/2020 0745
Trichloroethene
50
52
1
103
70-130
11/04/2020 0745
Trichlorofluoromethane
50
50
1
100
70-130
11/04/2020 0745
1,2,3-Trichloropropane
50
52
1
104
70-130
11/04/2020 0745
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 153 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72210-002
Matrix: Aqueous
Batch: 72210
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
52
1 104
60-140
11/04/2020 0745
Vinyl chloride
50
51
1 102
70-130
11/04/2020 0745
Xylenes (total)
100
110
1 107
70-130
11/04/2020 0745
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 154 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72211-001 Matrix: Aqueous
Batch:72211 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/04/2020 0922
Acrylonitrile
ND
1
20
0.80
ug/L
11/04/2020 0922
Benzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Bromoform
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/04/2020 0922
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/04/2020 0922
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Chloroethane
ND
1
2.0
0.40
ug/L
11/04/2020 0922
Chloroform
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/04/2020 0922
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/04/2020 0922
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/04/2020 0922
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
2-Hexanone
ND
1
10
2.0
ug/L
11/04/2020 0922
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/04/2020 0922
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/04/2020 0922
Methylene chloride
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Styrene
ND
1
1.0
0.41
ug/L
11/04/2020 0922
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Toluene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Trichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 155 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72211-001 Matrix: Aqueous
Batch:72211 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/04/2020 0922
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 90 70-130
Toluene-d8 95 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 156 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72211-002
Matrix: Aqueous
Batch:72211
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
150
N 1
152
60-140
11/04/2020 0754
Acrylonitrile
100
130
1
129
70-130
11/04/2020 0754
Benzene
50
47
1
94
70-130
11/04/2020 0754
Bromochloromethane
50
49
1
99
70-130
11/04/2020 0754
Bromodichloromethane
50
48
1
96
70-130
11/04/2020 0754
Bromoform
50
51
1
102
70-130
11/04/2020 0754
Bromomethane (Methyl bromide)
50
52
1
104
70-130
11/04/2020 0754
2-Butanone (MEK)
100
110
1
114
70-130
11/04/2020 0754
Carbon disulfide
50
49
1
98
70-130
11/04/2020 0754
Carbon tetrachloride
50
53
1
106
70-130
11/04/2020 0754
Chlorobenzene
50
50
1
100
70-130
11/04/2020 0754
Chloroethane
50
51
1
101
70-130
11/04/2020 0754
Chloroform
50
47
1
94
70-130
11/04/2020 0754
Chloromethane (Methyl chloride)
50
59
1
119
60-140
11/04/2020 0754
1,2-Dibromo-3-chloropropane (DBCP)
50
48
1
97
70-130
11/04/2020 0754
Dibromochloromethane
50
52
1
104
70-130
11/04/2020 0754
1,2-Dibromoethane (EDB)
50
52
1
104
70-130
11/04/2020 0754
Dibromomethane (Methylene bromide)
50
49
1
99
70-130
11/04/2020 0754
trans- 1,4-Dichloro-2-butene
50
60
1
120
70-130
11/04/2020 0754
1,2-Dichlorobenzene
50
49
1
97
70-130
11/04/2020 0754
1,4-Dichlorobenzene
50
50
1
101
70-130
11/04/2020 0754
1,1-Dichloroethane
50
49
1
98
70-130
11/04/2020 0754
1,2-Dichloroethane
50
48
1
96
70-130
11/04/2020 0754
1,1-Dichloroethene
50
47
1
94
70-130
11/04/2020 0754
cis- 1,2-Dichloroethene
50
47
1
94
70-130
11/04/2020 0754
trans- 1,2-Dichloroethene
50
49
1
98
70-130
11/04/2020 0754
1,2-Dichloropropane
50
49
1
98
70-130
11/04/2020 0754
cis- 1,3-Dichloropropene
50
51
1
101
70-130
11/04/2020 0754
trans- 1,3-Dichloropropene
50
54
1
107
70-130
11/04/2020 0754
Ethylbenzene
50
53
1
106
70-130
11/04/2020 0754
2-Hexanone
100
110
1
110
70-130
11/04/2020 0754
Methyl iodide (lodomethane)
50
48
1
96
70-130
11/04/2020 0754
4-Methyl-2-pentanone
100
110
1
110
70-130
11/04/2020 0754
Methylene chloride
50
47
1
93
70-130
11/04/2020 0754
Styrene
50
50
1
100
70-130
11/04/2020 0754
1,1,1,2-Tetrachloroethane
50
53
1
106
70-130
11/04/2020 0754
1,1,2,2-Tetrachloroethane
50
54
1
109
70-130
11/04/2020 0754
Tetrachloroethene
50
53
1
107
70-130
11/04/2020 0754
Toluene
50
51
1
103
70-130
11/04/2020 0754
1,1,1-Trichloroethane
50
49
1
98
70-130
11/04/2020 0754
1,1,2-Trichloroethane
50
52
1
104
70-130
11/04/2020 0754
Trichloroethene
50
47
1
94
70-130
11/04/2020 0754
Trichlorofluoromethane
50
55
1
110
70-130
11/04/2020 0754
1,2,3-Trichloropropane
50
53
1
106
70-130
11/04/2020 0754
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 157 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72211-002
Matrix: Aqueous
Batch:72211
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
54
1 109
60-140
11/04/2020 0754
Vinyl chloride
50
55
1 110
70-130
11/04/2020 0754
Xylenes (total)
100
100
1 104
70-130
11/04/2020 0754
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 91 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 158 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72211-001 Matrix: Aqueous
Batch:72211 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/04/2020 0922
Acetonitrile
ND
1
50
15
ug/L
11/04/2020 0922
Acrolein
ND
1
20
4.0
ug/L
11/04/2020 0922
Acrylonitrile
ND
1
20
0.80
ug/L
11/04/2020 0922
Benzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Bromoform
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/04/2020 0922
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/04/2020 0922
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/04/2020 0922
2-Chloro-1,3-Butadiene (Chloroprene)
ND
1
5.0
1.0
ug/L
11/04/2020 0922
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Chloroethane
ND
1
2.0
0.40
ug/L
11/04/2020 0922
Chloroform
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/04/2020 0922
3-Chloropropene (Allyl chloride)
ND
1
5.0
1.0
ug/L
11/04/2020 0922
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/04/2020 0922
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/04/2020 0922
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,3-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Dichlorodifluoromethane
ND
1
2.0
0.60
ug/L
11/04/2020 0922
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,3-Dichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
2,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1-Dichloropropene
ND
1
2.0
0.40
ug/L
11/04/2020 0922
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Ethyl methacrylate
ND
1
5.0
0.40
ug/L
11/04/2020 0922
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
2-Hexanone
ND
1
10
2.0
ug/L
11/04/2020 0922
Isobutyl alcohol
ND
1
50
12
ug/L
11/04/2020 0922
Methacrylonitrile
ND
1
5.0
2.0
ug/L
11/04/2020 0922
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/04/2020 0922
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 159 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72211-001 Matrix: Aqueous
Batch:72211 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Methyl methacrylate
ND
1
5.0
0.40
ug/L
11/04/2020 0922
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/04/2020 0922
Methylene chloride
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Propionitrile (Ethyl cyanide)
ND
1
20
4.0
ug/L
11/04/2020 0922
Styrene
ND
1
1.0
0.41
ug/L
11/04/2020 0922
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Toluene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Trichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/04/2020 0922
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/04/2020 0922
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 90 70-130
Toluene-d8 95 70-130
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 160 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72211-002
Matrix: Aqueous
Batch:72211
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
150
N 1
152
60-140
11/04/2020 0754
Acetonitrile
500
640
1
128
60-140
11/04/2020 0754
Acrolein
500
660
1
133
60-140
11/04/2020 0754
Acrylonitrile
100
130
1
129
70-130
11/04/2020 0754
Benzene
50
47
1
94
70-130
11/04/2020 0754
Bromochloromethane
50
49
1
99
70-130
11/04/2020 0754
Bromodichloromethane
50
48
1
96
70-130
11/04/2020 0754
Bromoform
50
51
1
102
70-130
11/04/2020 0754
Bromomethane (Methyl bromide)
50
52
1
104
70-130
11/04/2020 0754
2-Butanone (MEK)
100
110
1
114
70-130
11/04/2020 0754
Carbon disulfide
50
49
1
98
70-130
11/04/2020 0754
Carbon tetrachloride
50
53
1
106
70-130
11/04/2020 0754
2-Chloro-1,3-Butadiene (Chloroprene)
50
52
1
103
70-130
11/04/2020 0754
Chlorobenzene
50
50
1
100
70-130
11/04/2020 0754
Chloroethane
50
51
1
101
70-130
11/04/2020 0754
Chloroform
50
47
1
94
70-130
11/04/2020 0754
Chloromethane (Methyl chloride)
50
59
1
119
60-140
11/04/2020 0754
3-Chloropropene (Allyl chloride)
50
49
1
98
70-130
11/04/2020 0754
1,2-Dibromo-3-chloropropane (DBCP)
50
48
1
97
70-130
11/04/2020 0754
Dibromochloromethane
50
52
1
104
70-130
11/04/2020 0754
1,2-Dibromoethane (EDB)
50
52
1
104
70-130
11/04/2020 0754
Dibromomethane (Methylene bromide)
50
49
1
99
70-130
11/04/2020 0754
trans- 1,4-Dichloro-2-butene
50
60
1
120
70-130
11/04/2020 0754
1,2-Dichlorobenzene
50
49
1
97
70-130
11/04/2020 0754
1,3-Dichlorobenzene
50
54
1
107
70-130
11/04/2020 0754
1,4-Dichlorobenzene
50
50
1
101
70-130
11/04/2020 0754
Dichlorodifluoromethane
50
50
1
99
60-140
11/04/2020 0754
1,1-Dichloroethane
50
49
1
98
70-130
11/04/2020 0754
1,2-Dichloroethane
50
48
1
96
70-130
11/04/2020 0754
1,1-Dichloroethene
50
47
1
94
70-130
11/04/2020 0754
cis- 1,2-Dichloroethene
50
47
1
94
70-130
11/04/2020 0754
trans- 1,2-Dichloroethene
50
49
1
98
70-130
11/04/2020 0754
1,2-Dichloropropane
50
49
1
98
70-130
11/04/2020 0754
1,3-Dichloropropane
50
52
1
104
70-130
11/04/2020 0754
2,2-Dichloropropane
50
53
1
106
70-130
11/04/2020 0754
1,1-Dichloropropene
50
48
1
97
70-130
11/04/2020 0754
cis- 1,3-Dichloropropene
50
51
1
101
70-130
11/04/2020 0754
trans- 1,3-Dichloropropene
50
54
1
107
70-130
11/04/2020 0754
Ethyl methacrylate
50
55
1
110
70-130
11/04/2020 0754
Ethylbenzene
50
53
1
106
70-130
11/04/2020 0754
2-Hexanone
100
110
1
110
70-130
11/04/2020 0754
Isobutyl alcohol
500
640
1
127
60-140
11/04/2020 0754
Methacrylonitrile
250
280
1
114
70-130
11/04/2020 0754
Methyl iodide (lodomethane)
50
48
1
96
70-130
11/04/2020 0754
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 161 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72211-002
Matrix: Aqueous
Batch:72211
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Methyl methacrylate
50
52
1
104
70-130
11/04/2020 0754
4-Methyl-2-pentanone
100
110
1
110
70-130
11/04/2020 0754
Methylene chloride
50
47
1
93
70-130
11/04/2020 0754
Propionitrile (Ethyl cyanide)
500
590
1
118
70-130
11/04/2020 0754
Styrene
50
50
1
100
70-130
11/04/2020 0754
1,1,1,2-Tetrachloroethane
50
53
1
106
70-130
11/04/2020 0754
1,1,2,2-Tetrachloroethane
50
54
1
109
70-130
11/04/2020 0754
Tetrachloroethene
50
53
1
107
70-130
11/04/2020 0754
Toluene
50
51
1
103
70-130
11/04/2020 0754
1,1,1-Trichloroethane
50
49
1
98
70-130
11/04/2020 0754
1,1,2-Trichloroethane
50
52
1
104
70-130
11/04/2020 0754
Trichloroethene
50
47
1
94
70-130
11/04/2020 0754
Trichlorofluoromethane
50
55
1
110
70-130
11/04/2020 0754
1,2,3-Trichloropropane
50
53
1
106
70-130
11/04/2020 0754
Vinyl acetate
50
54
1
109
60-140
11/04/2020 0754
Vinyl chloride
50
55
1
110
70-130
11/04/2020 0754
Xylenes (total)
100
100
1
104
70-130
11/04/2020 0754
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 91 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 162 of 253

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: VQ72318-001 Matrix: Aqueous
Batch: 72318 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11/04/2020 2141
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
96 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 163 of 253

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: VQ72318-002 Matrix: Aqueous
Batch: 72318 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 48 1 96 70-130 11/04/2020 2038
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
102 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 164 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72367-001 Matrix: Aqueous
Batch:72367 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/05/2020 0950
Acrylonitrile
ND
1
20
0.80
ug/L
11/05/2020 0950
Benzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Bromoform
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/05/2020 0950
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/05/2020 0950
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Chloroethane
ND
1
2.0
0.40
ug/L
11/05/2020 0950
Chloroform
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/05/2020 0950
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/05/2020 0950
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/05/2020 0950
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
2-Hexanone
ND
1
10
2.0
ug/L
11/05/2020 0950
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/05/2020 0950
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/05/2020 0950
Methylene chloride
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Styrene
ND
1
1.0
0.41
ug/L
11/05/2020 0950
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Toluene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Trichloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 165 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72367-001 Matrix: Aqueous
Batch:72367 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/05/2020 0950
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 95 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 166 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72367-002
Matrix: Aqueous
Batch:72367
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
150
N 1
147
60-140
11/05/2020 0831
Acrylonitrile
100
120
1
121
70-130
11/05/2020 0831
Benzene
50
43
1
86
70-130
11/05/2020 0831
Bromochloromethane
50
46
1
92
70-130
11/05/2020 0831
Bromodichloromethane
50
45
1
89
70-130
11/05/2020 0831
Bromoform
50
48
1
96
70-130
11/05/2020 0831
Bromomethane (Methyl bromide)
50
50
1
99
70-130
11/05/2020 0831
2-Butanone (MEK)
100
110
1
106
70-130
11/05/2020 0831
Carbon disulfide
50
41
1
83
70-130
11/05/2020 0831
Carbon tetrachloride
50
49
1
98
70-130
11/05/2020 0831
Chlorobenzene
50
48
1
95
70-130
11/05/2020 0831
Chloroethane
50
48
1
96
70-130
11/05/2020 0831
Chloroform
50
44
1
88
70-130
11/05/2020 0831
Chloromethane (Methyl chloride)
50
58
1
117
60-140
11/05/2020 0831
1,2-Dibromo-3-chloropropane (DBCP)
50
42
1
83
70-130
11/05/2020 0831
Dibromochloromethane
50
50
1
99
70-130
11/05/2020 0831
1,2-Dibromoethane (EDB)
50
48
1
96
70-130
11/05/2020 0831
Dibromomethane (Methylene bromide)
50
45
1
90
70-130
11/05/2020 0831
trans- 1,4-Dichloro-2-butene
50
57
1
114
70-130
11/05/2020 0831
1,2-Dichlorobenzene
50
46
1
91
70-130
11/05/2020 0831
1,4-Dichlorobenzene
50
47
1
94
70-130
11/05/2020 0831
1,1-Dichloroethane
50
45
1
90
70-130
11/05/2020 0831
1,2-Dichloroethane
50
45
1
90
70-130
11/05/2020 0831
1,1-Dichloroethene
50
42
1
84
70-130
11/05/2020 0831
cis- 1,2-Dichloroethene
50
44
1
89
70-130
11/05/2020 0831
trans- 1,2-Dichloroethene
50
44
1
88
70-130
11/05/2020 0831
1,2-Dichloropropane
50
46
1
93
70-130
11/05/2020 0831
cis- 1,3-Dichloropropene
50
47
1
94
70-130
11/05/2020 0831
trans- 1,3-Dichloropropene
50
50
1
99
70-130
11/05/2020 0831
Ethylbenzene
50
47
1
95
70-130
11/05/2020 0831
2-Hexanone
100
100
1
101
70-130
11/05/2020 0831
Methyl iodide (lodomethane)
50
43
1
85
70-130
11/05/2020 0831
4-Methyl-2-pentanone
100
100
1
104
70-130
11/05/2020 0831
Methylene chloride
50
42
1
84
70-130
11/05/2020 0831
Styrene
50
49
1
97
70-130
11/05/2020 0831
1,1,1,2-Tetrachloroethane
50
49
1
98
70-130
11/05/2020 0831
1,1,2,2-Tetrachloroethane
50
54
1
108
70-130
11/05/2020 0831
Tetrachloroethene
50
48
1
97
70-130
11/05/2020 0831
Toluene
50
47
1
93
70-130
11/05/2020 0831
1,1,1-Trichloroethane
50
44
1
89
70-130
11/05/2020 0831
1,1,2-Trichloroethane
50
48
1
96
70-130
11/05/2020 0831
Trichloroethene
50
43
1
86
70-130
11/05/2020 0831
Trichlorofluoromethane
50
52
1
104
70-130
11/05/2020 0831
1,2,3-Trichloropropane
50
51
1
101
70-130
11/05/2020 0831
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 167 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72367-002
Matrix: Aqueous
Batch:72367
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
49
1 98
60-140
11/05/2020 0831
Vinyl chloride
50
53
1 105
70-130
11/05/2020 0831
Xylenes (total)
100
96
1 96
70-130
11/05/2020 0831
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 94 70-130
1,2-Dichloroethane-d4 89 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 168 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72367-001 Matrix: Aqueous
Batch:72367 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/05/2020 0950
Acetonitrile
ND
1
50
15
ug/L
11/05/2020 0950
Acrolein
ND
1
20
4.0
ug/L
11/05/2020 0950
Acrylonitrile
ND
1
20
0.80
ug/L
11/05/2020 0950
Benzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Bromoform
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/05/2020 0950
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/05/2020 0950
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/05/2020 0950
2-Chloro-1,3-Butadiene (Chloroprene)
ND
1
5.0
1.0
ug/L
11/05/2020 0950
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Chloroethane
ND
1
2.0
0.40
ug/L
11/05/2020 0950
Chloroform
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/05/2020 0950
3-Chloropropene (Allyl chloride)
ND
1
5.0
1.0
ug/L
11/05/2020 0950
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/05/2020 0950
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/05/2020 0950
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,3-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Dichlorodifluoromethane
ND
1
2.0
0.60
ug/L
11/05/2020 0950
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,3-Dichloropropane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
2,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1-Dichloropropene
ND
1
2.0
0.40
ug/L
11/05/2020 0950
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Ethyl methacrylate
ND
1
5.0
0.40
ug/L
11/05/2020 0950
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
2-Hexanone
ND
1
10
2.0
ug/L
11/05/2020 0950
Isobutyl alcohol
ND
1
50
12
ug/L
11/05/2020 0950
Methacrylonitrile
ND
1
5.0
2.0
ug/L
11/05/2020 0950
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/05/2020 0950
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 169 of 253

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72367-001 Matrix: Aqueous
Batch:72367 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Methyl methacrylate
ND
1
5.0
0.40
ug/L
11/05/2020 0950
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/05/2020 0950
Methylene chloride
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Propionitrile (Ethyl cyanide)
ND
1
20
4.0
ug/L
11/05/2020 0950
Styrene
ND
1
1.0
0.41
ug/L
11/05/2020 0950
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Toluene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Trichloroethene
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/05/2020 0950
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/05/2020 0950
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 95 70-130
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 170 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72367-002
Matrix: Aqueous
Batch:72367
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
150
N 1
147
60-140
11/05/2020 0831
Acetonitrile
500
590
1
118
60-140
11/05/2020 0831
Acrolein
500
670
1
134
60-140
11/05/2020 0831
Acrylonitrile
100
120
1
121
70-130
11/05/2020 0831
Benzene
50
43
1
86
70-130
11/05/2020 0831
Bromochloromethane
50
46
1
92
70-130
11/05/2020 0831
Bromodichloromethane
50
45
1
89
70-130
11/05/2020 0831
Bromoform
50
48
1
96
70-130
11/05/2020 0831
Bromomethane (Methyl bromide)
50
50
1
99
70-130
11/05/2020 0831
2-Butanone (MEK)
100
110
1
106
70-130
11/05/2020 0831
Carbon disulfide
50
41
1
83
70-130
11/05/2020 0831
Carbon tetrachloride
50
49
1
98
70-130
11/05/2020 0831
2-Chloro-1,3-Butadiene (Chloroprene)
50
46
1
92
70-130
11/05/2020 0831
Chlorobenzene
50
48
1
95
70-130
11/05/2020 0831
Chloroethane
50
48
1
96
70-130
11/05/2020 0831
Chloroform
50
44
1
88
70-130
11/05/2020 0831
Chloromethane (Methyl chloride)
50
58
1
117
60-140
11/05/2020 0831
3-Chloropropene (Allyl chloride)
50
45
1
90
70-130
11/05/2020 0831
1,2-Dibromo-3-chloropropane (DBCP)
50
42
1
83
70-130
11/05/2020 0831
Dibromochloromethane
50
50
1
99
70-130
11/05/2020 0831
1,2-Dibromoethane (EDB)
50
48
1
96
70-130
11/05/2020 0831
Dibromomethane (Methylene bromide)
50
45
1
90
70-130
11/05/2020 0831
trans- 1,4-Dichloro-2-butene
50
57
1
114
70-130
11/05/2020 0831
1,2-Dichlorobenzene
50
46
1
91
70-130
11/05/2020 0831
1,3-Dichlorobenzene
50
51
1
103
70-130
11/05/2020 0831
1,4-Dichlorobenzene
50
47
1
94
70-130
11/05/2020 0831
Dichlorodifluoromethane
50
43
1
86
60-140
11/05/2020 0831
1,1-Dichloroethane
50
45
1
90
70-130
11/05/2020 0831
1,2-Dichloroethane
50
45
1
90
70-130
11/05/2020 0831
1,1-Dichloroethene
50
42
1
84
70-130
11/05/2020 0831
cis- 1,2-Dichloroethene
50
44
1
89
70-130
11/05/2020 0831
trans- 1,2-Dichloroethene
50
44
1
88
70-130
11/05/2020 0831
1,2-Dichloropropane
50
46
1
93
70-130
11/05/2020 0831
1,3-Dichloropropane
50
48
1
96
70-130
11/05/2020 0831
2,2-Dichloropropane
50
47
1
94
70-130
11/05/2020 0831
1,1-Dichloropropene
50
44
1
88
70-130
11/05/2020 0831
cis- 1,3-Dichloropropene
50
47
1
94
70-130
11/05/2020 0831
trans- 1,3-Dichloropropene
50
50
1
99
70-130
11/05/2020 0831
Ethyl methacrylate
50
49
1
98
70-130
11/05/2020 0831
Ethylbenzene
50
47
1
95
70-130
11/05/2020 0831
2-Hexanone
100
100
1
101
70-130
11/05/2020 0831
Isobutyl alcohol
500
620
1
124
60-140
11/05/2020 0831
Methacrylonitrile
250
270
1
106
70-130
11/05/2020 0831
Methyl iodide (lodomethane)
50
43
1
85
70-130
11/05/2020 0831
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 171 of 253

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72367-002
Matrix: Aqueous
Batch:72367
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Methyl methacrylate
50
50
1
101
70-130
11/05/2020 0831
4-Methyl-2-pentanone
100
100
1
104
70-130
11/05/2020 0831
Methylene chloride
50
42
1
84
70-130
11/05/2020 0831
Propionitrile (Ethyl cyanide)
500
550
1
110
70-130
11/05/2020 0831
Styrene
50
49
1
97
70-130
11/05/2020 0831
1,1,1,2-Tetrachloroethane
50
49
1
98
70-130
11/05/2020 0831
1,1,2,2-Tetrachloroethane
50
54
1
108
70-130
11/05/2020 0831
Tetrachloroethene
50
48
1
97
70-130
11/05/2020 0831
Toluene
50
47
1
93
70-130
11/05/2020 0831
1,1,1-Trichloroethane
50
44
1
89
70-130
11/05/2020 0831
1,1,2-Trichloroethane
50
48
1
96
70-130
11/05/2020 0831
Trichloroethene
50
43
1
86
70-130
11/05/2020 0831
Trichlorofluoromethane
50
52
1
104
70-130
11/05/2020 0831
1,2,3-Trichloropropane
50
51
1
101
70-130
11/05/2020 0831
Vinyl acetate
50
49
1
98
60-140
11/05/2020 0831
Vinyl chloride
50
53
1
105
70-130
11/05/2020 0831
Xylenes (total)
100
96
1
96
70-130
11/05/2020 0831
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 94 70-130
1,2-Dichloroethane-d4 89 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 172 of 253

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ72150-001 Matrix: Aqueous
Batch: 72150 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 11/03/2020 1919
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Acenaphthylene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Acetophenone
ND
1
4.0
0.50
ug/L
11/13/2020 1334
2-Acetylaminofluorene
ND
1
8.0
1.7
ug/L
11/13/2020 1334
4-Aminobiphenyl
ND
1
8.0
1.1
ug/L
11/13/2020 1334
Anthracene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Benzo(a)anthracene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Benzo(a)pyrene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Benzo(g,h,i)perylene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Benzyl alcohol
ND
1
4.0
0.30
ug/L
11/13/2020 1334
4-Bromophenyl phenyl ether
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Butyl benzyl phthalate
1.1 J
1
4.0
0.50
ug/L
11/13/2020 1334
bis (2-Chloro-1-methylethyl) ether
ND
1
4.0
0.50
ug/L
11/13/2020 1334
4-Chloro-3-methyl phenol
ND
1
4.0
0.50
ug/L
11/13/2020 1334
4-Chloroaniline
ND
1
8.0
0.50
ug/L
11/13/2020 1334
Chlorobenzilate
ND
1
10
1.6
ug/L
11/13/2020 1334
bis(2-Chloroethoxy)methane
ND
1
4.0
0.50
ug/L
11/13/2020 1334
bis(2-Chloroethyl)ether
ND
1
4.0
0.50
ug/L
11/13/2020 1334
2-Chloronaphthalene
ND
1
4.0
0.50
ug/L
11/13/2020 1334
2-Chlorophenol
ND
1
4.0
0.50
ug/L
11/13/2020 1334
4-Chlorophenyl phenyl ether
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Chrysene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
cis-Diallate
ND
1
8.0
1.9
ug/L
11/13/2020 1334
trans-Diallate
ND
1
8.0
1.9
ug/L
11/13/2020 1334
Dibenzo(a,h)anthracene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Dibenzofuran
ND
1
4.0
0.50
ug/L
11/13/2020 1334
1,2-Dichlorobenzene
ND
1
4.0
0.50
ug/L
11/13/2020 1334
1,3-Dichlorobenzene
ND
1
4.0
0.50
ug/L
11/13/2020 1334
1,4-Dichlorobenzene
ND
1
4.0
0.60
ug/L
11/13/2020 1334
3,3'-Dichlorobenzidine
ND
1
4.0
1.8
ug/L
11/13/2020 1334
2,4-Dichlorophenol
ND
1
8.0
1.0
ug/L
11/13/2020 1334
2,6-Dichlorophenol
ND
1
4.0
1.6
ug/L
11/13/2020 1334
0,0-Diethyl-0-2-pyrazinyl (Thionazin)
ND
1
4.0
0.90
ug/L
11/13/2020 1334
Diethylphthalate
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Dimethoate
ND
1
8.0
2.8
ug/L
11/13/2020 1334
Dimethyl phthalate
ND
1
4.0
0.50
ug/L
11/13/2020 1334
p-(Dimethylamino)azobenzene
ND
1
10
0.53
ug/L
11/13/2020 1334
3,3'-Dimethylbenzidine
ND
1
16
10
ug/L
11/13/2020 1334
7,12-Dimethylbenzo(a)anthracene
ND
1
4.0
1.1
ug/L
11/13/2020 1334
2,4-Dimethylphenol
ND
1
4.0
1.0
ug/L
11/13/2020 1334
Di-n-butyl phthalate
ND
1
4.0
0.50
ug/L
11/13/2020 1334
4,6-Dinitro-2-methyl phenol
ND
1
20
1.0
ug/L
11/13/2020 1334
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 173 of 253

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ72150-001 Matrix: Aqueous
Batch: 72150 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 11/03/2020 1919
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
1,3-Dinitrobenzene
ND
1
16
13
ug/L
11/13/2020 1334
2,4-Dinitrophenol
ND
1
20
1.0
ug/L
11/13/2020 1334
2,4-Dinitrotoluene
ND
1
8.0
0.50
ug/L
11/13/2020 1334
2,6-Dinitrotoluene
ND
1
8.0
0.50
ug/L
11/13/2020 1334
Di-n-octylphthalate
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Ethyl methanesulfonate
ND
1
5.0
0.70
ug/L
11/13/2020 1334
Ethyl parathion
ND
1
16
2.8
ug/L
11/13/2020 1334
bis(2-Ethylhexyl)phthalate
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Famphur
ND
1
16
13
ug/L
11/13/2020 1334
Fluoranthene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Fluorene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Hexachlorobenzene
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Hexachlorobutadiene
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Hexachlorocyclopentadiene
ND
1
20
2.0
ug/L
11/13/2020 1334
Hexachloroethane
ND
1
4.0
1.0
ug/L
11/13/2020 1334
Hexachloropropene
ND
1
8.0
0.80
ug/L
11/13/2020 1334
Indeno(1,2,3-c,d)pyrene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
Isodrin
ND
1
4.0
0.70
ug/L
11/13/2020 1334
Isophorone
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Isosafrole
ND
1
4.0
1.1
ug/L
11/13/2020 1334
Methapyrilene
ND
1
16
8.8
ug/L
11/13/2020 1334
Methyl methanesulfonate
ND
1
4.0
0.50
ug/L
11/13/2020 1334
Methyl parathion
ND
1
16
2.0
ug/L
11/13/2020 1334
3-Methylcholanthrene
ND
1
8.0
5.0
ug/L
11/13/2020 1334
2-Methyl naphthalene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
2-Methylphenol
ND
1
4.0
1.0
ug/L
11/13/2020 1334
3+4-Methylphenol
ND
1
4.0
1.5
ug/L
11/13/2020 1334
Naphthalene
ND
1
0.80
0.20
ug/L
11/13/2020 1334
1,4-Naphthoquinone
ND
1
8.0
0.40
ug/L
11/13/2020 1334
1-Naphthylamine
ND
1
8.0
0.030
ug/L
11/13/2020 1334
2-Naphthylamine
ND
1
8.0
0.14
ug/L
11/13/2020 1334
2-Nitroaniline
ND
1
8.0
0.50
ug/L
11/13/2020 1334
3-Nitroaniline
ND
1
8.0
1.0
ug/L
11/13/2020 1334
4-Nitroaniline
ND
1
8.0
1.5
ug/L
11/13/2020 1334
Nitrobenzene
ND
1
4.0
1.5
ug/L
11/13/2020 1334
5-Nitro-o-toluidine
ND
1
8.0
2.2
ug/L
11/13/2020 1334
2-Nitrophenol
ND
1
4.0
1.0
ug/L
11/13/2020 1334
4-Nitrophenol
ND
1
20
2.0
ug/L
11/13/2020 1334
N-Nitroso-di-butylamine
ND
1
4.0
1.1
ug/L
11/13/2020 1334
N-Nitrosodiethylamine
ND
1
4.0
0.80
ug/L
11/13/2020 1334
N-Nitrosodimethylamine
ND
1
4.0
0.50
ug/L
11/13/2020 1334
N-Nitrosodi-n-propylamine
ND
1
4.0
0.50
ug/L
11/13/2020 1334
N-Nitrosodiphenylamine (Diphenylamine) ND
1
4.0
0.50
ug/L
11/13/2020 1334
N-Nitrosomethylethylamine
ND
1
5.0
1.8
ug/L
11/13/2020 1334
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 174 of 253

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ72150-001 Matrix: Aqueous
Batch: 72150 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 11/03/2020 1919
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
N-Nitrosopiperidine
ND
1
4.0
1.4
ug/L
11/13/20201334
N-Nitrosopyrrolidine
ND
1
4.0
2.1
ug/L
11/13/20201334
Pentachlorobenzene
ND
1
4.0
0.70
ug/L
11/13/20201334
Pentachloronitrobenzene
ND
1
16
2.6
ug/L
11/13/20201334
Pentachlorophenol
ND
1
20
2.0
ug/L
11/13/20201334
Phenacetin
ND
1
4.0
3.4
ug/L
11/13/20201334
Phenanthrene
ND
1
0.80
0.20
ug/L
11/13/20201334
Phenol
ND
1
4.0
0.50
ug/L
11/13/20201334
p-Phenylenediamine
ND
1
40
11
ug/L
11/13/20201334
Phorate
ND
1
4.0
3.6
ug/L
11/13/20201334
Pronamide
ND
1
8.0
3.0
ug/L
11/13/20201334
Pyrene
ND
1
0.80
0.20
ug/L
11/13/20201334
Safrole
ND
1
5.0
0.90
ug/L
11/13/20201334
Sulfotepp
ND
1
8.0
0.60
ug/L
11/13/20201334
1,2,4,5-Tetrachlorobenzene
ND
1
4.0
0.90
ug/L
11/13/20201334
2,3,4,6-Tetrachlorophenol
ND
1
8.0
0.80
ug/L
11/13/20201334
o-Toluidine
ND
1
4.0
0.90
ug/L
11/13/20201334
1,2,4-Trichlorobenzene
ND
1
4.0
0.50
ug/L
11/13/20201334
2,4,5-Trichlorophenol
ND
1
4.0
0.50
ug/L
11/13/20201334
2,4,6-Trichlorophenol
ND
1
4.0
0.50
ug/L
11/13/20201334
0,0,0-Triethylphosphorothioate
ND
1
4.0
1.3
ug/L
11/13/20201334
1,3,5-Trinitrobenzene
ND
1
16
13
ug/L
11/13/20201334
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
71
37-129
2-Fluorophenol
49
24-127
Nitrobenzene-d5
79
38-127
Phenol-d5 64 28-128
Terphenyl-d 14 81 10-148
2,4,6-Tribromophenol 84 35-144
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 175 of 253

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72150-002
Matrix: Aqueous
Batch: 72150
Prep Method:
3520C
Analytical Method: 8270E
Prep Date: 11/03/2020 1919
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
40
31
1
77
30-122
11/13/2020 1359
Acenaphthylene
40
31
1
79
30-130
11/13/2020 1359
Acetophenone
40
36
1
91
30-130
11/13/2020 1359
Anthracene
40
33
1
82
30-123
11/13/2020 1359
Benzo(a)anthracene
40
32
1
79
40-125
11/13/2020 1359
Benzo(a)pyrene
40
34
1
85
40-128
11/13/2020 1359
Benzo(b)fluoranthene
40
35
1
87
30-130
11/13/2020 1359
Benzo(g,h,i)perylene
40
37
1
93
30-130
11/13/2020 1359
Benzo(k)fluoranthene
40
37
1
92
30-130
11/13/2020 1359
4-Bromophenyl phenyl ether
40
34
1
84
30-124
11/13/2020 1359
Butyl benzyl phthalate
40
33
1
82
30-130
11/13/2020 1359
bis (2-Chloro-1-methylethyl) ether
40
34
1
85
30-130
11/13/2020 1359
4-Chloro-3-methyl phenol
40
32
1
81
30-115
11/13/2020 1359
4-Chloroaniline
40
41
1
103
12-157
11/13/2020 1359
bis(2-Chloroethoxy)methane
40
30
1
76
30-130
11/13/2020 1359
bis(2-Chloroethyl)ether
40
36
1
91
30-130
11/13/2020 1359
2-Chloronaphthalene
40
31
1
77
30-130
11/13/2020 1359
2-Chlorophenol
40
30
1
76
30-130
11/13/2020 1359
4-Chlorophenyl phenyl ether
40
30
1
76
30-121
11/13/2020 1359
Chrysene
40
31
1
78
30-130
11/13/2020 1359
Dibenzo(a,h)anthracene
40
37
1
94
30-130
11/13/2020 1359
Dibenzofuran
40
30
1
76
30-118
11/13/2020 1359
1,2-Dichlorobenzene
40
31
1
78
30-130
11/13/2020 1359
1,3-Dichlorobenzene
40
31
1
78
30-130
11/13/2020 1359
1,4-Dichlorobenzene
40
31
1
78
30-130
11/13/2020 1359
3,3'-Dichlorobenzidine
40
30
1
74
10-126
11/13/2020 1359
2,4-Dichlorophenol
40
32
1
81
30-121
11/13/2020 1359
Diethylphthalate
40
30
1
76
40-125
11/13/2020 1359
Dimethyl phthalate
40
30
1
76
40-127
11/13/2020 1359
2,4-Dimethylphenol
40
36
1
91
20-125
11/13/2020 1359
Di-n-butyl phthalate
40
32
1
81
30-130
11/13/2020 1359
4,6-Dinitro-2-methyl phenol
40
38
1
95
30-130
11/13/2020 1359
2,4-Dinitrophenol
80
69
1
86
11-126
11/13/2020 1359
2,4-Dinitrotoluene
40
32
1
80
30-130
11/13/2020 1359
2,6-Dinitrotoluene
40
32
1
81
30-130
11/13/2020 1359
Di-n-octylphthalate
40
36
1
90
30-130
11/13/2020 1359
bis(2-Ethylhexyl)phthalate
40
33
1
82
30-130
11/13/2020 1359
Fluoranthene
40
31
1
76
40-128
11/13/2020 1359
Fluorene
40
30
1
74
30-124
11/13/2020 1359
Hexachlorobenzene
40
34
1
84
30-125
11/13/2020 1359
Hexachlorobutadiene
40
32
1
81
24-110
11/13/2020 1359
Hexachlorocyclopentadiene
200
170
1
85
22-122
11/13/2020 1359
Hexachloroethane
40
31
1
77
30-130
11/13/2020 1359
Indeno(1,2,3-c,d)pyrene
40
34
1
86
30-130
11/13/2020 1359
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 176 of 253

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72150-002
Matrix: Aqueous
Batch: 72150
Prep Method:
3520C
Analytical Method: 8270E
Prep Date: 11/03/2020 1919
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Isophorone
40
37
1
92
30-130
11/13/20201359
2-Methyl naphthalene
40
32
1
79
40-132
11/13/20201359
2-Methylphenol
40
36
1
90
30-130
11/13/20201359
3+4-Methylphenol
40
38
1
95
30-130
11/13/20201359
Naphthalene
40
31
1
79
30-130
11/13/20201359
2-Nitroaniline
40
40
1
101
30-130
11 /13/2020 1359
3-Nitroaniline
40
33
1
83
30-130
11/13/20201359
4-Nitroaniline
40
40
1
100
30-135
11/13/20201359
Nitrobenzene
40
36
1
89
30-130
11/13/20201359
2-Nitrophenol
40
33
1
83
30-130
11/13/20201359
4-Nitrophenol
80
59
1
74
30-130
11/13/20201359
N-Nitrosodimethylamine
40
31
1
78
30-130
11/13/20201359
N-Nitrosodi-n-propylamine
40
39
1
98
30-130
11/13/20201359
N-Nitrosodiphenylamine (Diphenylamine) 40
34
1
84
30-123
11/13/2020 1359
Pentachlorophenol
80
74
1
92
30-130
11/13/20201359
Phenanthrene
40
31
1
78
40-123
11/13/20201359
Phenol
40
29
1
72
30-130
11/13/20201359
Pyrene
40
33
1
84
40-126
11/13/20201359
2,4,5-Trichlorophenol
40
29
1
74
30-123
11/13/20201359
2,4,6-Trichlorophenol
40
33
1
83
30-125
11/13/20201359
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
77
37-129
2-Fluorophenol
65
24-127
Nitrobenzene-d5
87
38-127
Phenol-d5 76 28-128
Terphenyl-d 14 81 10-148
2,4,6-Tribromophenol 92 35-144
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 177 of 253

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: VJ27055-021 MS
Matrix: Aqueous
Batch: 72150
Prep Method: 3520C
Analytical Method: 8270E
Prep Date: 11/03/2020 1919
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
ND
80
48
1
60
30-122
11/13/2020 1718
Acenaphthylene
ND
80
50
1
63
30-130
11/13/2020 1718
Acetophenone
ND
80
64
1
80
30-130
11/13/2020 1718
Anthracene
ND
80
53
1
67
30-123
11/13/2020 1718
Benzo(a)anthracene
ND
80
51
1
64
40-125
11/13/2020 1718
Benzo(a)pyrene
ND
80
56
1
70
40-128
11/13/2020 1718
Benzo(b)fluoranthene
ND
80
59
1
74
30-130
11/13/2020 1718
Benzo(g,h,i)perylene
ND
80
63
1
79
30-130
11/13/2020 1718
Benzo(k)fluoranthene
ND
80
61
1
77
30-130
11/13/2020 1718
4-Bromophenyl phenyl ether
ND
80
54
1
67
30-124
11/13/2020 1718
Butyl benzyl phthalate
ND
80
52
1
65
30-130
11/13/2020 1718
bis (2-Chloro-1-methylethyl) ether
ND
80
59
1
74
30-130
11/13/2020 1718
4-Chloro-3-methyl phenol
ND
80
52
1
65
30-115
11/13/2020 1718
4-Chloroaniline
ND
80
51
1
64
10-130
11/13/2020 1718
bis(2-Chloroethoxy)methane
ND
80
48
1
60
30-130
11/13/2020 1718
bis(2-Chloroethyl)ether
ND
80
63
1
78
30-130
11/13/2020 1718
2-Chloronaphthalene
ND
80
47
1
58
30-130
11/13/2020 1718
2-Chlorophenol
ND
80
49
1
61
30-130
11/13/2020 1718
4-Chlorophenyl phenyl ether
ND
80
48
1
60
30-121
11/13/2020 1718
Chrysene
ND
80
53
1
66
30-130
11/13/2020 1718
Dibenzo(a,h)anthracene
ND
80
63
1
79
30-130
11/13/2020 1718
Dibenzofuran
ND
80
47
1
59
30-118
11/13/2020 1718
1,2-Dichlorobenzene
ND
80
46
1
58
30-130
11/13/2020 1718
1,3-Dichlorobenzene
ND
80
43
1
54
30-130
11/13/2020 1718
1,4-Dichlorobenzene
ND
80
45
1
56
30-130
11/13/2020 1718
3,3'-Dichlorobenzidine
ND
80
53
1
67
10-126
11/13/2020 1718
2,4-Dichlorophenol
ND
80
51
1
64
30-121
11/13/2020 1718
Diethylphthalate
ND
80
50
1
62
40-125
11/13/2020 1718
Dimethyl phthalate
ND
80
49
1
62
40-127
11/13/2020 1718
2,4-Dimethylphenol
ND
80
58
1
72
20-125
11/13/2020 1718
Di-n-butyl phthalate
ND
80
54
1
68
30-130
11/13/2020 1718
4,6-Dinitro-2-methyl phenol
ND
80
62
1
77
30-130
11/13/2020 1718
2,4-Dinitrophenol
ND
160
110
1
68
30-130
11/13/2020 1718
2,4-Dinitrotoluene
ND
80
51
1
64
30-130
11/13/2020 1718
2,6-Dinitrotoluene
ND
80
52
1
65
30-130
11/13/2020 1718
Di-n-octylphthalate
ND
80
60
1
75
30-130
11/13/2020 1718
bis(2-Ethylhexyl)phthalate
ND
80
51
N 1
64
70-131
11/13/2020 1718
Fluoranthene
ND
80
53
1
66
40-128
11/13/2020 1718
Fluorene
ND
80
46
1
58
30-124
11/13/2020 1718
Hexachlorobenzene
ND
80
56
1
70
30-125
11/13/2020 1718
Hexachlorobutadiene
ND
80
45
1
56
24-110
11/13/2020 1718
Hexachlorocyclopentadiene
ND
400
240
1
61
22-122
11/13/2020 1718
Hexachloroethane
ND
80
43
1
54
30-130
11/13/2020 1718
Indeno(1,2,3-c,d)pyrene
ND
80
58
1
72
30-130
11/13/2020 1718
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 178 of 253

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: VJ27055-021 MS
Matrix: Aqueous
Batch: 72150
Prep Method: 3520C
Analytical Method: 8270E
Prep Date: 11/03/2020 1919
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Isophorone
ND
80
58
1
73
30-130
11/13/20201718
2-Methyl naphthalene
ND
80
47
1
59
40-132
11/13/20201718
2-Methylphenol
ND
80
63
1
79
30-130
11/13/20201718
3+4-Methylphenol
ND
80
69
1
87
30-130
11/13/20201718
Naphthalene
ND
80
46
1
58
30-130
11/13/20201718
2-Nitroaniline
ND
80
62
1
78
30-130
11/13/20201718
3-Nitroaniline
ND
80
51
1
64
30-130
11/13/20201718
4-Nitroaniline
ND
80
53
1
66
30-135
11/13/20201718
Nitrobenzene
ND
80
55
1
68
30-130
11/13/20201718
2-Nitrophenol
ND
80
51
1
64
30-130
11/13/20201718
4-Nitrophenol
ND
160
87
1
54
30-130
11/13/20201718
N-Nitrosodimethylamine
ND
80
51
1
64
30-130
11/13/20201718
N-Nitrosodi-n-propylamine
ND
80
70
1
88
30-130
11/13/20201718
N-Nitrosodiphenylamine (Diphenylamine)
ND
80
54
1
68
30-123
11/13/2020 1718
Pentachlorophenol
ND
160
120
1
75
30-130
11/13/20201718
Phenanthrene
ND
80
51
1
64
40-123
11/13/20201718
Phenol
ND
80
47
1
59
30-130
11/13/20201718
Pyrene
ND
80
55
1
69
40-126
11/13/20201718
2,4,5-Trichlorophenol
ND
80
48
1
60
30-123
11/13/20201718
2,4,6-Trichlorophenol
ND
80
53
1
66
30-125
11/13/20201718
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
60
37-129
2-Fluorophenol
39
24-127
Nitrobenzene-d5
66
38-127
Phenol-d5 62 28-128
Terphenyl-d 14 68 10-148
2,4,6-Tribromophenol 74 35-144
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 179 of 253

Semivolatile Organic Compounds by GC/MS - MSD
Sample ID: VJ27055-021MD
Matrix: Aqueous
Batch: 72150
Prep Method:
3520C
Analytical Method: 8270E
Prep Date: 11/03/2020 1919
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Acenaphthene
ND
80
58
1
72
19
30-122
40
11/13/2020 1743
Acenaphthylene
ND
80
59
1
73
16
30-130
40
11/13/2020 1743
Acetophenone
ND
80
76
1
95
17
30-130
40
11/13/2020 1743
Anthracene
ND
80
62
1
77
15
30-123
40
11/13/2020 1743
Benzo(a)anthracene
ND
80
59
1
74
14
40-125
40
11/13/2020 1743
Benzo(a)pyrene
ND
80
64
1
80
13
40-128
40
11/13/2020 1743
Benzo(b)fluoranthene
ND
80
66
1
82
11
30-130
40
11/13/2020 1743
Benzo(g,h,i)perylene
ND
80
71
1
88
12
30-130
40
11/13/2020 1743
Benzo(k)fluoranthene
ND
80
68
1
85
11
30-130
40
11/13/2020 1743
4-Bromophenyl phenyl ether
ND
80
61
1
76
13
30-124
40
11/13/2020 1743
Butyl benzyl phthalate
ND
80
60
1
75
15
30-130
40
11/13/2020 1743
bis (2-Chloro-1-methylethyl) ether
ND
80
69
1
87
16
30-130
40
11/13/2020 1743
4-Chloro-3-methyl phenol
ND
80
62
1
77
17
30-115
40
11/13/2020 1743
4-Chloroaniline
ND
80
61
1
77
18
10-130
40
11/13/2020 1743
bis(2-Chloroethoxy)methane
ND
80
58
1
73
20
30-130
40
11/13/2020 1743
bis(2-Chloroethyl)ether
ND
80
76
1
95
19
30-130
40
11/13/2020 1743
2-Chloronaphthalene
ND
80
56
1
70
18
30-130
40
11/13/2020 1743
2-Chlorophenol
ND
80
60
1
75
20
30-130
40
11/13/2020 1743
4-Chlorophenyl phenyl ether
ND
80
56
1
70
16
30-121
40
11/13/2020 1743
Chrysene
ND
80
60
1
75
13
30-130
40
11/13/2020 1743
Dibenzo(a,h)anthracene
ND
80
71
1
89
11
30-130
40
11/13/2020 1743
Dibenzofuran
ND
80
56
1
70
17
30-118
40
11/13/2020 1743
1,2-Dichlorobenzene
ND
80
59
1
73
24
30-130
40
11/13/2020 1743
1,3-Dichlorobenzene
ND
80
55
1
68
24
30-130
40
11/13/2020 1743
1,4-Dichlorobenzene
ND
80
56
1
70
23
30-130
40
11/13/2020 1743
3,3'-Dichlorobenzidine
ND
80
63
1
79
16
10-126
40
11/13/2020 1743
2,4-Dichlorophenol
ND
80
61
1
77
18
30-121
40
11/13/2020 1743
Diethylphthalate
ND
80
59
1
74
18
40-125
40
11/13/2020 1743
Dimethyl phthalate
ND
80
58
1
73
17
40-127
40
11/13/2020 1743
2,4-Dimethylphenol
ND
80
64
1
80
10
20-125
40
11/13/2020 1743
Di-n-butyl phthalate
ND
80
63
1
79
15
30-130
40
11/13/2020 1743
4,6-Dinitro-2-methyl phenol
ND
80
70
1
87
12
30-130
40
11/13/2020 1743
2,4-Dinitrophenol
ND
160
120
1
77
12
30-130
40
11/13/2020 1743
2,4-Dinitrotoluene
ND
80
61
1
76
17
30-130
40
11/13/2020 1743
2,6-Dinitrotoluene
ND
80
62
1
78
18
30-130
40
11/13/2020 1743
Di-n-octylphthalate
ND
80
67
1
83
11
30-130
40
11/13/2020 1743
bis(2-Ethylhexyl)phthalate
ND
80
58
1
73
13
70-131
40
11/13/2020 1743
Fluoranthene
ND
80
61
1
77
15
40-128
40
11/13/2020 1743
Fluorene
ND
80
55
1
68
17
30-124
40
11/13/2020 1743
Hexachlorobenzene
ND
80
63
1
79
12
30-125
40
11/13/2020 1743
Hexachlorobutadiene
ND
80
56
1
70
22
24-110
40
11/13/2020 1743
Hexachlorocyclopentadiene
ND
400
300
1
74
19
22-122
40
11/13/2020 1743
Hexachloroethane
ND
80
55
1
69
25
30-130
40
11/13/2020 1743
Indeno(1,2,3-c,d)pyrene
ND
80
64
1
80
11
30-130
40
11/13/2020 1743
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 180 of 253

Semivolatile Organic Compounds by GC/MS - MSD
Sample ID: VJ27055-021MD
Matrix: Aqueous
Batch: 72150
Prep Method:
3520C
Analytical Method: 8270E
Prep Date: 11/03/2020 1919
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Isophorone
ND
80
72
1
90
21
30-130
40
11/13/20201743
2-Methyl naphthalene
ND
80
58
1
73
21
40-132
40
11/13/20201743
2-Methylphenol
ND
80
73
1
91
15
30-130
40
11/13/20201743
3+4-Methylphenol
ND
80
79
1
98
13
30-130
40
11/13/20201743
Naphthalene
ND
80
57
1
71
21
30-130
40
11/13/20201743
2-Nitroaniline
ND
80
74
1
93
18
30-130
40
11/13/20201743
3-Nitroaniline
ND
80
62
1
77
19
30-130
40
11/13/20201743
4-Nitroaniline
ND
80
73
1
91
32
30-135
40
11/13/20201743
Nitrobenzene
ND
80
68
1
84
21
30-130
40
11/13/20201743
2-Nitrophenol
ND
80
63
1
79
21
30-130
40
11/13/20201743
4-Nitrophenol
ND
160
110
1
68
22
30-130
40
11/13/20201743
N-Nitrosodimethylamine
ND
80
61
1
76
17
30-130
40
11/13/20201743
N-Nitrosodi-n-propylamine
ND
80
83
1
104
17
30-130
40
11/13/20201743
N-Nitrosodiphenylamine (Diphenylamine)
ND
80
63
1
79
16
30-123
40
11/13/2020 1743
Pentachlorophenol
ND
160
140
1
87
15
30-130
40
11/13/20201743
Phenanthrene
ND
80
59
1
73
14
40-123
40
11/13/20201743
Phenol
ND
80
56
1
70
18
30-130
40
11/13/20201743
Pyrene
ND
80
64
1
80
15
40-126
40
11/13/20201743
2,4,5-Trichlorophenol
ND
80
57
1
72
17
30-123
40
11/13/20201743
2,4,6-Trichlorophenol
ND
80
64
1
80
19
30-125
40
11/13/20201743
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
70
37-129
2-Fluorophenol
45
24-127
Nitrobenzene-d5
80
38-127
Phenol-d5 72 28-128
Terphenyl-d 14 77 10-148
2,4,6-Tribromophenol 84 35-144
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 181 of 253

Herbicides by GC - MB
Sample ID: VQ71691-001 Matrix: Aqueous
Batch:71691 Prep Method: 8151A
Analytical Method: 8151A Prep Date: 10/29/2020 2037
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
2,4,5-T
ND
1
0.50
0.13
ug/L
10/30/20201842
2,4-D
ND
1
2.0
0.50
ug/L
10/30/20201842
Dinoseb
ND
1
1.0
0.50
ug/L
10/30/20201842
2,4,5-TP (Silvex)
ND
1
0.50
0.13
ug/L
10/30/2020 1842
Surrogate
DCAA
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
87 50-112
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 182 of 253

Herbicides by GC - LCS
Sample ID: VQ71691-002
Matrix: Aqueous
Batch:71691
Prep Method: 8151A
Analytical Method: 8151A
Prep Date: 10/29/2020 2037
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
2,4,5-T
5.0
4.2
1 84
70-130
10/30/20201905
2,4-D
5.0
4.7
1 94
70-130
10/30/20201905
Dinoseb
5.0
3.7
1 74
31-128
10/30/20201905
2,4,5-TP (Silvex)
5.0
4.6
1 92
70-130
10/30/2020 1905
Surrogate
DCAA
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
85 50-112
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 183 of 253

Herbicides by GC - MS
Sample ID: VJ27055-007MS
Matrix: Aqueous
Batch:71691
Prep Method: 8151A
Analytical Method: 8151A
Prep Date: 10/29/2020 2037
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
2,4,5-T
ND
10
8.5
1
85
70-130
10/30/20201951
2,4-D
ND
10
7.1
1
71
70-130
10/30/20201951
Dinoseb
ND
10
7.2
1
72
31-128
10/30/20201951
2,4,5-TP (Silvex)
ND
10
10
1
100
70-130
10/30/2020 1951
Surrogate
DCAA
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
90 50-112
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 184 of 253

Herbicides by GC - MSD
Sample ID: VJ27055-007MD
Matrix: Aqueous
Batch:71691
Prep Method: 8151A
Analytical Method: 8151A
Prep Date: 10/29/2020 2037
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil % Rec % RPD
Limit
Limit
Analysis Date
2,4,5-T
ND
10
6.9
N 1 69 20
70-130
40
10/30/2020 2014
2,4-D
ND
10
7.3
1 73 2.3
70-130
40
10/30/2020 2014
Dinoseb
ND
10
6.2
1 62 14
31-128
40
10/30/2020 2014
2,4,5-TP (Silvex)
ND
10
8.5
1 85 17
70-130
40
10/30/2020 2014
Surrogate
DCAA
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
82 50-112
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 185 of 253

Organochlorine Pesticides by GC - MB
Sample ID: VQ72139-001 Matrix: Aqueous
Batch: 72139 Prep Method: 3520C
Analytical Method: 8081B Prep Date: 11/03/2020 2330
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Aldrin
ND
1
0.040
0.020
ug/L
11/05/2020 1902
gamma-BHC (Lindane)
ND
1
0.040
0.017
ug/L
11/05/2020 1902
alpha-BHC
ND
1
0.040
0.015
ug/L
11/05/2020 1902
beta-BHC
ND
1
0.040
0.015
ug/L
11/05/2020 1902
delta-BHC
ND
1
0.040
0.015
ug/L
11/05/2020 1902
cis -Chlordane
ND
1
0.040
0.015
ug/L
11/05/2020 1902
trans -Chlordane
ND
1
0.040
0.015
ug/L
11/05/2020 1902
4,4'-DDD
ND
1
0.040
0.015
ug/L
11/05/2020 1902
4,4'-DDE
ND
1
0.040
0.020
ug/L
11/05/2020 1902
4,4'-DDT
ND
1
0.040
0.020
ug/L
11/05/2020 1902
Dieldrin
ND
1
0.040
0.015
ug/L
11/05/2020 1902
Endosulfan I
ND
1
0.040
0.015
ug/L
11/05/2020 1902
Endosulfan 11
ND
1
0.040
0.015
ug/L
11/05/2020 1902
Endosulfan sulfate
ND
1
0.040
0.015
ug/L
11/05/2020 1902
Endrin
ND
1
0.040
0.015
ug/L
11/05/2020 1902
Endrin aldehyde
ND
1
0.040
0.015
ug/L
11/05/2020 1902
Endrin ketone
ND
1
0.040
0.015
ug/L
11/05/2020 1902
Heptachlor
ND
1
0.040
0.021
ug/L
11/05/2020 1902
Heptachlor epoxide
ND
1
0.040
0.016
ug/L
11/05/2020 1902
Methoxychlor
ND
1
0.16
0.021
ug/L
11/05/2020 1902
Toxaphene
ND
1
0.40
0.30
ug/L
11/05/2020 1902
Surrogate Q % Rec Acceptance
Limit
Decachlorobiphenyl 91 20-122
Tetrachloro-m-xylene 73 46-119
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 186 of 253

Organochlorine Pesticides by GC - LCS
Sample ID: VQ72139-002
Matrix: Aqueous
Batch: 72139
Prep Method: 3520C
Analytical Method: 8081B
Prep Date: 11/03/2020 2330
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
Aldrin
0.80
0.69
1 86
70-130
11/05/2020 1917
gamma-BHC (Lindane)
0.80
0.71
1 89
70-130
11/05/2020 1917
alpha-BHC
0.80
0.61
1 76
70-130
11/05/2020 1917
beta-BHC
0.80
0.74
1 93
70-130
11/05/2020 1917
delta-BHC
0.80
0.78
1 98
70-130
11/05/2020 1917
cis -Chlordane
0.80
0.74
1 92
70-130
11/05/2020 1917
trans -Chlordane
0.80
0.75
1 94
70-130
11/05/2020 1917
4,4'-DDD
0.80
0.85
1 106
70-130
11/05/2020 1917
4,4'-DDE
0.80
0.76
1 96
70-130
11/05/2020 1917
4,4'-DDT
0.80
0.80
1 100
70-130
11/05/2020 1917
Dieldrin
0.80
0.81
1 101
70-130
11/05/2020 1917
Endosulfan 1
0.80
0.77
1 96
70-130
11/05/2020 1917
Endosulfan 11
0.80
0.71
1 89
70-130
11/05/2020 1917
Endosulfan sulfate
0.80
0.96
1 120
70-130
11/05/2020 1917
Endrin
0.80
0.74
1 92
70-130
11/05/2020 1917
Endrin aldehyde
0.80
0.76
1 96
70-130
11/05/2020 1917
Endrin ketone
0.80
0.85
1 106
70-130
11/05/2020 1917
Heptachlor
0.80
0.66
1 82
70-130
11/05/2020 1917
Heptachlor epoxide
0.80
0.74
1 93
70-130
11/05/2020 1917
Methoxychlor
0.80
0.76
1 95
70-130
11/05/2020 1917
Surrogate Q % Rec Acceptance
Limit
Decachlorobiphenyl 93 20-122
Tetrachloro-m-xylene 69 46-119
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 187 of 253

Organochlorine Pesticides by GC - MS
Sample ID: VJ27055-021 MS
Matrix: Aqueous
Batch: 72139
Prep Method: 3520C
Analytical Method: 8081B
Prep Date: 11/03/2020 2330
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Aldrin
ND
0.80
0.73
1
91
70-130
11/05/2020 2019
gamma-BHC (Lindane)
ND
0.80
0.76
1
95
70-130
11/05/2020 2019
alpha-BHC
ND
0.80
0.62
1
78
70-130
11/05/2020 2019
beta-BHC
ND
0.80
0.75
1
94
70-130
11/05/2020 2019
delta-BHC
ND
0.80
0.83
1
103
70-130
11/05/2020 2019
cis -Chlordane
ND
0.80
0.76
1
96
70-130
11/05/2020 2019
trans -Chlordane
ND
0.80
0.75
1
93
70-130
11/05/2020 2019
4,4'-DDD
ND
0.80
0.88
1
110
70-130
11/05/2020 2019
4,4'-DDE
ND
0.80
0.76
1
95
70-130
11/05/2020 2019
4,4'-DDT
ND
0.80
0.80
1
100
70-130
11/05/2020 2019
Dieldrin
ND
0.80
0.81
1
102
70-130
11/05/2020 2019
Endosulfan I
ND
0.80
0.77
1
96
70-130
11/05/2020 2019
Endosulfan 11
ND
0.80
0.74
1
92
70-130
11/05/2020 2019
Endosulfan sulfate
ND
0.80
0.97
1
122
70-130
11/05/2020 2019
Endrin
ND
0.80
0.73
1
92
70-130
11/05/2020 2019
Endrin aldehyde
ND
0.80
0.79
1
99
70-130
11/05/2020 2019
Endrin ketone
ND
0.80
0.84
1
106
70-130
11/05/2020 2019
Heptachlor
ND
0.80
0.67
1
84
70-130
11/05/2020 2019
Heptachlor epoxide
ND
0.80
0.75
1
93
70-130
11/05/2020 2019
Methoxychlor
ND
0.80
0.76
1
96
70-130
11/05/2020 2019
Surrogate Q % Rec Acceptance
Limit
Decachlorobiphenyl 77 20-122
Tetrachloro-m-xylene 71 46-119
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 188 of 253

Organochlorine Pesticides by GC - MSD
Sample ID: VJ27055-021MD
Matrix: Aqueous
Batch: 72139
Prep Method:
3520C
Analytical Method: 8081B
Prep Date: 11/03/2020 2330
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Aldrin
ND
0.80
0.71
1
88
3.1
70-130
30
11/05/2020 2035
gamma-BHC (Lindane)
ND
0.80
0.74
1
92
3.6
70-130
30
11/05/2020 2035
alpha-BHC
ND
0.80
0.64
1
80
2.5
70-130
30
11/05/2020 2035
beta-BHC
ND
0.80
0.77
1
96
2.2
70-130
30
11/05/2020 2035
delta-BHC
ND
0.80
0.83
1
103
0.12
70-130
30
11/05/2020 2035
cis -Chlordane
ND
0.80
0.76
1
94
1.1
70-130
30
11/05/2020 2035
trans -Chlordane
ND
0.80
0.76
1
95
1.8
70-130
30
11/05/2020 2035
4,4'-DDD
ND
0.80
0.88
1
110
0.079
70-130
30
11/05/2020 2035
4,4'-DDE
ND
0.80
0.76
1
95
0.30
70-130
30
11/05/2020 2035
4,4'-DDT
ND
0.80
0.81
1
102
1.4
70-130
30
11/05/2020 2035
Dieldrin
ND
0.80
0.83
1
103
1.6
70-130
30
11/05/2020 2035
Endosulfan I
ND
0.80
0.78
1
98
2.1
70-130
30
11/05/2020 2035
Endosulfan 11
ND
0.80
0.74
1
93
0.74
70-130
30
11/05/2020 2035
Endosulfan sulfate
ND
0.80
0.99
1
124
1.7
70-130
30
11/05/2020 2035
Endrin
ND
0.80
0.76
1
95
4.0
70-130
30
11/05/2020 2035
Endrin aldehyde
ND
0.80
0.80
1
100
1.4
70-130
30
11/05/2020 2035
Endrin ketone
ND
0.80
0.87
1
108
2.6
70-130
30
11/05/2020 2035
Heptachlor
ND
0.80
0.66
1
83
0.93
70-130
30
11/05/2020 2035
Heptachlor epoxide
ND
0.80
0.76
1
95
1.4
70-130
30
11/05/2020 2035
Methoxychlor
ND
0.80
0.77
1
97
1.0
70-130
30
11/05/2020 2035
Surrogate Q % Rec Acceptance
Limit
Decachlorobiphenyl 80 20-122
Tetrachloro-m-xylene 69 46-119
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 189 of 253

PCBs by GC - MB
Sample ID: VQ72148-001 Matrix: Aqueous
Batch:72148 Prep Method: 3520C Cleanup: 3665A
Analytical Method: 8082A Prep Date: 11/03/2020 2330
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Aroclor 1016
ND
1
0.40
0.15
ug/L
11/05/2020 1242
Aroclor 1221
ND
1
0.40
0.25
ug/L
11/05/2020 1242
Aroclor 1232
ND
1
0.40
0.15
ug/L
11/05/2020 1242
Aroclor 1242
ND
1
0.40
0.15
ug/L
11/05/2020 1242
Aroclor 1248
ND
1
0.40
0.15
ug/L
11/05/2020 1242
Aroclor 1254
ND
1
0.40
0.15
ug/L
11/05/2020 1242
Aroclor 1260
ND
1
0.40
0.15
ug/L
11/05/2020 1242
Acceptance
Surrogate
0
Q /o Rec
Limit
Decachlorobiphenyl 90 10-133
Tetrachloro-m-xylene 82 31-122
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 190 of 253

PCBs by GC - LCS
Sample ID: VQ72148-002
Matrix: Aqueous
Batch:72148
Prep Method: 3520C
Cleanup:
3665A
Analytical Method: 8082A
Prep Date: 11/03/2020 2330
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Aroclor 1016
4.0
3.6
1 90
70-130
11/05/2020 1256
Aroclor 1260
4.0
4.1
1 102
70-130
11/05/2020 1256
Surrogate
Q % Rec
Acceptance
Limit
Decachlorobiphenyl 100 10-133
Tetrachloro-m-xylene 87 31-122
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 191 of 253

PCBs by GC - MS
Sample ID: VJ27055-007MS
Matrix: Aqueous
Batch:72148
Prep Method: 3520C
Cleanup:
3665A
Analytical Method: 8082A
Prep Date: 11/03/2020 2330
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L) Q Dil % Rec
Limit
Analysis Date
Aroclor 1016
ND
4.0
3.6 1 89
70-130
11/05/2020 1322
Aroclor 1260
ND
4.0
4.3 1 107
70-130
11/05/2020 1322
Acceptance
Surrogate Q % Rec Limit
Decachlorobiphenyl 92 10-133
Tetrachloro-m-xylene 85 31-122
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 192 of 253

PCBs by GC - MSD
Sample ID: VJ27055-007MD
Matrix: Aqueous
Batch:72148
Prep Method: 3520C
Cleanup:
3665A
Analytical Method: 8082A
Prep Date: 11/03/2020 2330
Sample
Spike
Amount
Amount
Result
% Rec % RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil % Rec % RPD
Limit Limit
Analysis Date
Aroclor 1016
ND
4.0
3.2
1 80 11
70-130 20
11/05/2020 1336
Aroclor 1260
ND
4.0
3.8
1 96 11
70-130 20
11/05/2020 1336
Acceptance
Surrogate Q % Rec Limit
Decachlorobiphenyl 86 10-133
Tetrachloro-m-xylene 78 31-122
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 193 of 253

Herbicides by GC - MB
Sample ID: VQ72317-001 Matrix: Aqueous
Batch:72317 Prep Method: 8151A
Analytical Method: 8151A Prep Date: 11/04/2020 1924
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
2,4,5-T
ND
1
0.50
0.13
ug/L
11/05/20201447
2,4-D
ND
1
2.0
0.50
ug/L
11/05/20201447
Dinoseb
ND
1
1.0
0.50
ug/L
11/05/20201447
2,4,5-TP (Silvex)
ND
1
0.50
0.13
ug/L
11/05/2020 1447
Surrogate
DCAA
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
77 50-112
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 194 of 253

Herbicides by GC - LCS
Sample ID: VQ72317-002
Matrix: Aqueous
Batch:72317
Prep Method: 8151A
Analytical Method: 8151A
Prep Date: 11/04/2020 1924
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
2,4,5-T
5.0
3.8
1 76
70-130
11/05/20201510
2,4-D
5.0
4.1
1 81
70-130
11/05/20201510
Dinoseb
5.0
2.3
1 46
31-128
11/05/20201510
2,4,5-TP (Silvex)
5.0
4.1
1 81
70-130
11/05/2020 1510
Surrogate
DCAA
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
74 50-112
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 195 of 253

Herbicides by GC - MS
Sample ID: VJ27055-021 MS
Matrix: Aqueous
Batch:72317
Prep Method: 8151A
Analytical Method: 8151A
Prep Date: 11/04/2020 1924
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
2,4,5-T
ND
10
8.5
1
85
70-130
11/05/20201620
2,4-D
ND
10
8.5
1
85
70-130
11/05/20201620
Dinoseb
ND
10
3.5
1
35
31-128
11/05/20201620
2,4,5-TP (Silvex)
ND
10
8.6
1
86
70-130
11/05/2020 1620
Surrogate
DCAA
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
77 50-112
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 196 of 253

Herbicides by GC - MSD
Sample ID: VJ27055-021MD
Matrix: Aqueous
Batch:72317
Prep Method: 8151A
Analytical Method: 8151A
Prep Date: 11/04/2020 1924
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil % Rec % RPD
Limit
Limit
Analysis Date
2,4,5-T
ND
10
8.8
1 88 3.4
70-130
40
11/05/20201643
2,4-D
ND
10
9.4
1 94 9.8
70-130
40
11/05/20201643
Dinoseb
ND
10
7.4
+ 1 74 71
31-128
40
11/05/20201643
2,4,5-TP (Silvex)
ND
10
9.1
1 91 5.7
70-130
40
11/05/2020 1643
Surrogate
DCAA
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
80 50-112
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 197 of 253

ICP-MS Metals - MB
Sample ID: VQ71571-001 Matrix: Aqueous
Batch: 71571 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 10/30/2020 1549
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/02/20201838
Arsenic
ND
1
2.0
1.3
ug/L
11/02/20201838
Barium
ND
1
5.0
1.3
ug/L
11/02/20201838
Beryllium
ND
1
0.40
0.15
ug/L
11/02/20201838
Cadmium
ND
1
0.50
0.13
ug/L
11/02/20201838
Chromium
ND
1
5.0
1.3
ug/L
11/02/20201838
Cobalt
ND
1
5.0
1.3
ug/L
11/02/20201838
Copper
ND
1
5.0
1.3
ug/L
11/02/20201838
Lead
ND
1
1.0
0.25
ug/L
11/02/20201838
Nickel
ND
1
5.0
1.3
ug/L
11/02/20201838
Selenium
ND
1
5.0
1.3
ug/L
11/02/20201838
Silver
ND
1
1.0
0.25
ug/L
11/02/20201838
Thallium
ND
1
0.50
0.15
ug/L
11/02/20201838
Tin
ND
1
20
5.0
ug/L
11/02/20201838
Vanadium
ND
1
5.0
2.5
ug/L
11/02/20201838
Zinc
ND
1
10
2.5
ug/L
11/02/20201838
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 198 of 253

ICP-MS Metals - LCS
Sample ID: VQ71571-002
Matrix: Aqueous
Batch: 71571
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 10/30/2020 1549
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
Antimony
100
99
1 99
80-120
11/02/20201846
Arsenic
100
100
1 101
80-120
11 /02/2020 1846
Barium
100
96
1 96
80-120
11/02/20201846
Beryllium
100
99
1 99
80-120
11/02/20201846
Cadmium
100
100
1 100
80-120
11/02/20201846
Chromium
100
110
1 109
80-120
11/02/20201846
Cobalt
100
110
1 108
80-120
11/02/20201846
Copper
100
100
1 104
80-120
11/02/20201846
Lead
100
110
1 112
80-120
11/02/20201846
Nickel
100
110
1 107
80-120
11/02/20201846
Selenium
100
92
1 92
80-120
11/02/20201846
Silver
100
110
1 106
80-120
11/02/20201846
Thallium
100
110
1 112
80-120
11/02/20201846
Tin
100
100
1 100
80-120
11/02/20201846
Vanadium
100
110
1 107
80-120
11/02/20201846
Zinc
100
96
1 96
80-120
11/02/20201846
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 199 of 253

ICP-MS Metals - MS
Sample ID: VJ27055-0O4MS
Matrix: Aqueous
Batch: 71571
Prep Method: 3OO5A
Analytical Method: 6020B
Prep Date: 10/30/2020 1549
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
ND
100
100
1
103
70-130
11/02/20201938
Arsenic
ND
100
100
1
102
70-130
11/02/20201938
Barium
110
100
220
1
109
70-130
11/02/20201938
Beryllium
ND
100
100
1
103
70-130
11/02/20201938
Cadmium
ND
100
99
1
99
70-130
11/02/20201938
Chromium
1.3
100
100
1
100
70-130
11/02/20201938
Cobalt
9.3
100
110
1
102
70-130
11/02/20201938
Copper
ND
100
99
1
99
70-130
11/02/20201938
Lead
ND
100
100
1
100
70-130
11/02/20201938
Nickel
4.7
100
98
1
94
70-130
11/02/20201938
Selenium
ND
100
95
1
95
70-130
11/02/20201938
Silver
ND
100
97
1
97
70-130
11/02/20201938
Thallium
ND
100
99
1
99
70-130
11/02/20201938
Vanadium
ND
100
100
1
104
70-130
11/02/20201938
Zinc
ND
100
100
1
100
70-130
11/02/20201938
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 200 of 253

ICP-MS Metals - MSD
Sample ID: VJ27055-004MD
Matrix: Aqueous
Batch: 71571
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 10/30/2020 1549
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil % Rec % RPD
Limit
Limit
Analysis Date
Antimony
ND
100
100
1 104
0.89
70-130
20
11/02/20201945
Arsenic
ND
100
100
1 101
1.5
70-130
20
11/02/20201945
Barium
110
100
220
1 112
1.4
70-130
20
11/02/20201945
Beryllium
ND
100
100
1 103
0.65
70-130
20
11/02/20201945
Cadmium
ND
100
99
1 99
0.24
70-130
20
11/02/20201945
Chromium
1.3
100
100
1 99
0.48
70-130
20
11/02/20201945
Cobalt
9.3
100
110
1 102
0.087
70-130
20
11/02/20201945
Copper
ND
100
100
1 101
2.2
70-130
20
11/02/20201945
Lead
ND
100
100
1 100
0.43
70-130
20
11/02/20201945
Nickel
4.7
100
99
1 94
0.35
70-130
20
11/02/20201945
Selenium
ND
100
93
1 93
2.5
70-130
20
11/02/20201945
Silver
ND
100
99
1 99
1.6
70-130
20
11/02/20201945
Thallium
ND
100
100
1 100
0.82
70-130
20
11/02/20201945
Vanadium
ND
100
100
1 104
0.10
70-130
20
11/02/20201945
Zinc
ND
100
100
1 101
0.56
70-130
20
11/02/20201945
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 201 of 253

ICP-MS Metals - MB
Sample ID: VQ71919-001 Matrix: Aqueous
Batch: 71919 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/03/2020 0936
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/04/2020 0014
Arsenic
ND
1
2.0
1.3
ug/L
11/04/2020 0014
Barium
ND
1
5.0
1.3
ug/L
11/04/2020 0014
Beryllium
ND
1
0.40
0.15
ug/L
11/04/2020 0014
Cadmium
ND
1
0.50
0.13
ug/L
11/04/2020 0014
Chromium
ND
1
5.0
1.3
ug/L
11/04/2020 0014
Cobalt
ND
1
5.0
1.3
ug/L
11/04/2020 0014
Copper
ND
1
5.0
1.3
ug/L
11/04/2020 0014
Lead
ND
1
1.0
0.25
ug/L
11/04/2020 0014
Nickel
ND
1
5.0
1.3
ug/L
11/04/2020 0014
Selenium
ND
1
5.0
1.3
ug/L
11/04/2020 0014
Silver
ND
1
1.0
0.25
ug/L
11/04/2020 0014
Thallium
ND
1
0.50
0.15
ug/L
11/04/2020 0014
Tin
ND
1
20
5.0
ug/L
11/04/2020 0014
Vanadium
ND
1
5.0
2.5
ug/L
11/04/2020 0014
Zinc
ND
1
10
2.5
ug/L
11/04/2020 0014
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 202 of 253

ICP-MS Metals - LCS
Sample ID: VQ71919-002
Matrix: Aqueous
Batch: 71919
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 11/03/2020 0936
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
Antimony
100
100
1 101
80-120
11/04/2020 0022
Arsenic
100
99
1 99
80-120
11/04/2020 0022
Barium
100
95
1 95
80-120
11/04/2020 0022
Beryllium
100
96
1 96
80-120
11/04/2020 0022
Cadmium
100
100
1 100
80-120
11/04/2020 0022
Chromium
100
110
1 106
80-120
11/04/2020 0022
Cobalt
100
110
1 106
80-120
11/04/2020 0022
Copper
100
100
1 102
80-120
11/04/2020 0022
Lead
100
110
1 107
80-120
11/04/2020 0022
Nickel
100
100
1 105
80-120
11/04/2020 0022
Selenium
100
91
1 91
80-120
11/04/2020 0022
Silver
100
100
1 103
80-120
11/04/2020 0022
Thallium
100
110
1 109
80-120
11/04/2020 0022
Tin
100
99
1 99
80-120
11/04/2020 0022
Vanadium
100
100
1 102
80-120
11/04/2020 0022
Zinc
100
91
1 91
80-120
11/04/2020 0022
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 203 of 253

ICP-MS Metals - MS
Sample ID: VJ27055-013MS
Matrix: Aqueous
Batch: 71919
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 11/03/2020 0936
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
ND
100
110
1
106
70-130
11/04/2020 0107
Arsenic
ND
100
100
1
101
70-130
11/04/2020 0107
Barium
55
100
150
1
95
70-130
11/04/2020 0107
Beryllium
ND
100
98
1
98
70-130
11/04/2020 0107
Cadmium
ND
100
100
1
103
70-130
11/04/2020 0107
Chromium
ND
100
100
1
103
70-130
11/04/2020 0107
Cobalt
ND
100
100
1
100
70-130
11/04/2020 0107
Copper
1.5
100
98
1
97
70-130
11/04/2020 0107
Lead
ND
100
100
1
103
70-130
11/04/2020 0107
Nickel
17
100
110
1
95
70-130
11/04/2020 0107
Selenium
ND
100
97
1
97
70-130
11/04/2020 0107
Silver
ND
100
100
1
101
70-130
11/04/2020 0107
Thallium
ND
100
110
1
107
70-130
11/04/2020 0107
Vanadium
ND
100
100
1
104
70-130
11/04/2020 0107
Zinc
13
100
110
1
93
70-130
11/04/2020 0107
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 204 of 253

ICP-MS Metals - MSD
Sample ID: VJ27055-013MD
Matrix: Aqueous
Batch: 71919
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 11/03/2020 0936
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil % Rec % RPD
Limit
Limit
Analysis Date
Antimony
ND
100
110
1 108
1.9
70-130
20
11/04/2020 0114
Arsenic
ND
100
110
1 105
3.8
70-130
20
11/04/2020 0114
Barium
55
100
150
1 98
2.2
70-130
20
11/04/2020 0114
Beryllium
ND
100
100
1 101
2.8
70-130
20
11/04/2020 0114
Cadmium
ND
100
110
1 106
3.0
70-130
20
11/04/2020 0114
Chromium
ND
100
110
1 106
2.6
70-130
20
11/04/2020 0114
Cobalt
ND
100
100
1 102
2.1
70-130
20
11/04/2020 0114
Copper
1.5
100
100
1 99
2.0
70-130
20
11/04/2020 0114
Lead
ND
100
110
1 105
2.2
70-130
20
11/04/2020 0114
Nickel
17
100
110
1 98
2.8
70-130
20
11/04/2020 0114
Selenium
ND
100
100
1 100
3.0
70-130
20
11/04/2020 0114
Silver
ND
100
100
1 102
0.59
70-130
20
11/04/2020 0114
Thallium
ND
100
110
1 109
2.1
70-130
20
11/04/2020 0114
Vanadium
ND
100
110
1 106
2.0
70-130
20
11/04/2020 0114
Zinc
13
100
110
1 95
1.8
70-130
20
11/04/2020 0114
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 205 of 253

ICP-MS Metals - MB
Sample ID: VQ72039-001 Matrix: Aqueous
Batch: 72039 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/03/2020 0936
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/04/2020 0252
Arsenic
ND
1
2.0
1.3
ug/L
11/04/2020 0252
Barium
ND
1
5.0
1.3
ug/L
11/04/2020 0252
Beryllium
ND
1
0.40
0.15
ug/L
11/04/2020 0252
Cadmium
ND
1
0.50
0.13
ug/L
11/04/2020 0252
Chromium
ND
1
5.0
1.3
ug/L
11/04/2020 0252
Cobalt
ND
1
5.0
1.3
ug/L
11/04/2020 0252
Copper
ND
1
5.0
1.3
ug/L
11/04/2020 0252
Lead
ND
1
1.0
0.25
ug/L
11/04/2020 0252
Nickel
ND
1
5.0
1.3
ug/L
11/04/2020 0252
Selenium
ND
1
5.0
1.3
ug/L
11/04/2020 0252
Silver
ND
1
1.0
0.25
ug/L
11/04/2020 0252
Thallium
ND
1
0.50
0.15
ug/L
11/04/2020 0252
Vanadium
ND
1
5.0
2.5
ug/L
11/04/2020 0252
Zinc
ND
1
10
2.5
ug/L
11/04/2020 0252
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 206 of 253

ICP-MS Metals - LCS
Sample ID: VQ72039-002
Matrix: Aqueous
Batch: 72039
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 11/03/2020 0936
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
Antimony
100
100
1 103
80-120
11/04/2020 0259
Arsenic
100
110
1 106
80-120
11/04/2020 0259
Barium
100
97
1 97
80-120
11/04/2020 0259
Beryllium
100
100
1 100
80-120
11/04/2020 0259
Cadmium
100
100
1 102
80-120
11/04/2020 0259
Chromium
100
110
1 113
80-120
11/04/2020 0259
Cobalt
100
110
1 113
80-120
11/04/2020 0259
Copper
100
100
1 104
80-120
11/04/2020 0259
Lead
100
110
1 109
80-120
11/04/2020 0259
Nickel
100
110
1 112
80-120
11/04/2020 0259
Selenium
100
96
1 96
80-120
11/04/2020 0259
Silver
100
110
1 106
80-120
11/04/2020 0259
Thallium
100
110
1 110
80-120
11/04/2020 0259
Vanadium
100
110
1 110
80-120
11/04/2020 0259
Zinc
100
93
1 93
80-120
11/04/2020 0259
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 207 of 253

CVAA -MB
Sample ID: VQ73376-001 Matrix: Aqueous
Batch: 73376 Prep Method:
Analytical Method: 7470A Prep Date: 11/13/2020 0552
Parameter Result Q Dil LOQ DL Units Analysis Date
Mercury ND 1 0.00020 0.000091 mg/L 11/13/2020 0843
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 208 of 253

CVAA - LCS
Sample ID: VQ73376-002 Matrix: Aqueous
Batch: 73376 Prep Method:
Analytical Method: 7470A Prep Date: 11/13/2020 0552
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury 0.0020 0.0020 1 99 80-120 11/13/2020 0846
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 209 of 253

CVAA - MS
Sample ID: VJ27055-007MS Matrix: Aqueous
Batch: 73376 Prep Method:
Analytical Method: 7470A Prep Date: 11/13/2020 0552
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury ND 0.0020 0.0014 N 1 70 85-115 11/13/2020 0851
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 210 of 253

CVAA - MSD
Sample ID: VJ27055-007MD Matrix: Aqueous
Batch: 73376 Prep Method:
Analytical Method: 7470A Prep Date: 11/13/2020 0552
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Mercury ND 0.0020 0.0013 N 1 63 9.8 85-115 20 11/13/2020 0853
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 211 of 253

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 212 of 253

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SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage FoW Drive • 1�.'aal Golumbiar SC 29172
Talepr-one Nv. EM-7 1-07DD Fax No. £-791-91
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SamplesReCOIPt CheCklis# [SRCj (Mrt00'1SC-15) Revl4Sed!91'29f2D20
Issuir'g Authority. Pace ENV -'N�:OL PW.P- 1 of 3
Sample Receipt Chcclkfist (SRC
__
Clier.%' Coale: ?rts ectcd lryfdat�:
;means ofrcocipt_ JPacer Client U!'� FedEx Qth�T=-- _
Yes 'Teo 1. W" custody seals pnewAlt on the eoalcil".)
Yes 1hTo NA ':, If ustod; sca16 were pr:�enia were toe intact grid unbroken',
11-I Strip ID; rCl�l{)rine5trip 1D. T by:
ri ival #em eraturc on ei f en Corn3c to rarHtun; u}lou reC eii]t L„tiLiNd Snap -Cup [D
'fen0d; ❑Temp"tiirt- Blank ir-SA S6t#lcs IR C;r n LCY _ TR Gun Currecticm Fal.lnr= ¢C
Mothod Of coolants W-et Ice Lj lee Pn rks F Dr Ice El Nonc
3. if, terapc,'awrc 4f any coo for extxeded G.0°C vas Pmjcal- Manager Nbtitied'i
©Yet hlo NNA pM was Nutiflod by, phoslo email i fa-40-faoa (rirule uire).
_ lfct5 -No MAI 4, is the caramarcial courier's pL kMn slip attached to this roan? —
Ycs lwlo 5- Werzpropercustodypraoadures(relinqu=shedk,xeivad) tollowetP
Pes o 6. wL!re sample IE1s Jistcd r-n the COC? _
yes -Nol 17, Wem-5mrnple IDs Ustcd Un aJI sample. containers?
M'rfifesU No S. Was coll4Gl:on dam & time listed ou the C'OC?
Yes p{c ?- W,, coilectiocti date & time listed 4ri all sample crr.19dilers7 w
yrs No 10, laid all container labO irlbrmatlon (TT), dju., thm) agree wit the CQC?
Vex No 11, W-crc tests lei be pertotmed lister on the COO
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12- Did a1l.5Mrples arrive in thz proper cor+tttiners for caul, test aiLd�or in �rnxrd con ,tars
Yrs � ° (unhrokeri, lads oil, em)?
Yes u 13. WEis adequate sample volruM awaiLable't
Yes >tio 14. 'rr- all sam Ies race
wRhin Vt the holding time or dS hours, whic'nGwei comm first's
Yes Na 15. V4'ere any satuples catitalners rnissir.Evcxcxss eir�gr pnej samplrs Not liswd cm {:{MC?
16. For VOA and RS{-l7� suttrpim, ware huhbles pres4ut "pea -sire" 41,�'ar 61mi) in dixr toted
' No ) 4 _r any I Ff ate VOA via ls7
Y 35 Ala NA 17- ` m-e ,dl 17 kcXFncte+l $lnatrien: samples uecei 4,Vd $t a H of < 2?
1'es llo NA i$-'A ere all Cyanide samplri :exeived at a PJI > L2 acrid w1fid0 s rrrples *received Ot a H> W -
f9, lVerc at s�pplicable 7,fH3.rTKAf+cyautidelpheno1i625. I �598.3 �1.Sm L SKLmPles see If
[�y s ONu NA residuit[ uhla.ine
2Ci. Won- r:liert renm-'6cs''requests (i-c. t+egrrested dilutimns, MSi M51D desigrrafions,El
Yes MITactly Lra,raacribcd from the W i1lr.rt the cornmont sEction ;r, LI�i$`�
Yesl LI-Nal 121, Was the qu= number lister; m the ocimu w label? If Rs. Quni_ #
sample Preacr�atign (MusLhe winp!e:tod for ny sarnpl&(s) weorroctiy pdewrved or }siLh hea+tpaoe_j
samph>(S) were R=lved inaorrarll, poese wd ere ardjustad accardingl
in sample receiving with mL of r,i le one. H2904, : R� G3, H C L. MaOF using SR >'� _�..
Tulle off � ry3CrY�ilarr , If more, tihsm ono w�rv&Lkle is 11"d f1, pltiaa� ,DEClIC1 the �otTktt7Cuts bLjUW,
were Mt! i tied with hi INIA cs >6 MM in diameter.
amales(S vrcre rc c :4ed with 1'l l; ? CO m ug'i. (]; +a 4,�s no }grid McrC
%ijrrstedaccordinglyinsartlplumwiviagwith ypdiiimCkiosulfate(Naj&4q-,�wit Shealy iD:.. �-
4Jit baraode labe;s appl ied by:
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 214 of 253

PACE ANALYTICAL SERVICES, LLC
Samples Recialpt CheMirit (514 l 1Mf01)1RC-15) Re,rised:9}29{2020
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CIjg11_ t U,' — — Cooler Lirpec-" bti?dSL;�: AHED , V137055
a'Yes
d -No I, Were cust«dy s� k r.-M01tit wi Lhe,�aoler? N o ,J f cotody seals W15M rc;xul' werelhay it itac: and �,rthm�cn?
�fw:.x�� 43z TQs;ed b
�T�3 Strip ]d; _ L:ltforine $trip II]' — - _ y:
Driginal t6edpertu,ire upon rCccfpt I Daiv!c (CO11oCt0d) tempQraLure open raCeipl °o5olic Sslap itp Ill; N
2.d r2,8 0 NA eNA nC NA NA oC NA INN s,L
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_�. If temperature of anY cooler rxe�edea 6'03C, was Projt:ct Manulgcr Nc4itiod?
l'cs� PM was Nytif rd by-- phone i emai! 1 C"%�-Lc-face (sire:e ono),
YCS N10 1J.1 rl_ [r, the pgnuueWisl CDUnft's I}9Cian-Slip attached to Ms form?
J Y Na 5_ Were proper cusfAidy proced-,,res (rclinuuf9h$d'recciv A) fallavmd7 _
, Yts No 6. WCFO 36Ln P16IN listed on the Cam'?
Yes LjNa 7, Were saru IcTTIN listed oa al[ sampkcmitadners9
yrg EIND 8. 1VA5 of)llection datte d` iinl[ listed On t119 COO?
YEg Nn 9_ leas L!u1jecdon date & timc fisLed on all sample contariners7
yF�ti l]c 14_ Did all.Emmincr 1:1bef information CID. &W time} a,ree w'I 0w COC'r
Yes Isla l I_ Were tests to be Wroamed 1, qwd on the CDC?
12 Did all senmples arrlvo in the propCr {�x,,r;rautiers :xor each test widlur in Rom oondition
Y [� Na (LmbraM -M, lids on, tvLe-)?
Yet Flo 13.VaS adequate sampleLurn & 6vailablk?
J Yes No 14. %derc all sarnples eceived within Vithe boldits� tureardS Irout�, whiche�crcames first'
Yes l 0 15. Were 3uv sHrnpl t$ ;': �ttaincrs :n issinglcxoess (circle one} sainpl�s trot lis exi r,s i {]C"7
❑ ❑ 161 For VDA and R5K-175 kajrples, wer,- bubbles pnxerrt=�'psa-sine' ['}�"or 6=1 in diarrm�ter')
❑ Yes 'No NA in akly cf the VQA vi- als`t
1,7 yes No t44 l7. Were all MOlmetals,hnrtrient samplca received at a 11B cf < ??
,� Ytis No NA 1 S, Were ail tYMOU sainples rtceivpd at api. ` 12 and solfide sampkq reeeKed an i �I I -> 97
_ Vdeie a �pp13cab1c N H rTIL r}antdc+l�ISeno1161S,1f608- ( ft_irr.�rL} sampl tee of
KE]YES❑Nlo ❑ �` Clualakwirm V
211 NO QNl+ cnrl•cctly trum;cuibad from the COC info flip cor:tment oc=ion in LTMLS?
� No 2l_ Wt,s $u quote number Listed an Lim container [ahel7 if a, �Uo e
Sample peservation �,sk,usr be cexr.�leted for #tn}saiwplc(s) irtecrreCtLy I,r��rved ar rills Itieadsptlr.�.)
Sample{s3 A were rerAivcd inconvaly preserved —] were adjusted aceorcingl:
is Sample recei ,n wide ` uiL ofcirrle or•.c- 1-12SO4, I INU'3, VC1,?tiaOH usfaa tiR rk
TixlocofpreservationNA —. If morethat, orteprc.4jva_iveisneeded,-abasenOLDin1hecommentsbelou',
Salnple;sj — werere"iwed withhutbks>4mm indigMeCr.
Samnie%(s) WCM received with'1'Rr' > 0.5 mg,'L (1f #I9 is ran) and wera
a+�jtkSted aardingly in sample receiving vrltl; sadit;n_ diiasulfatc (N42S2t ) w;16 Shoal}' IQ: 1 A
a,^
SR barcodv JabY!R applied by: R # Datc; t0�27,�3{r20
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 215 of 253

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106 Vantage POirrt 1)fIV(. * VVP-9 : dumbla. SC 2917P
Ts. Whor* No, 803-791 $IQQ Fax NQ, 903-791-9111
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Client: L'F
h4eat1SUr7k%' pL_ Face 0101t UPS FelEx Othew 'r
No 1. Wuvc cumrxty smis present orn the cover?
No A 2. If Custody scats wal,c present, wt:cthcy iill act and unbroken?
w2 Chlorine 5trifI3; Tested by:
pe,'al.u. LIPOIt Lpy71Cell-d ! Deuived (CIU rcct temp-21-1t4Lle upon ,t�cipt %Solid Snap -Cup ID: _
E1 St17r:1):
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IssvIng Author:ty; Pace CNV - WCOL
Sample Receipt Checklist (SR '
Coale{Inspected 416atc: W JA 0-31�J Lat#:
:iA93d: ©'fCMpemtJ J31a6k gninSt Banes Jlt Crurr [D:: GL11t COrI";eLi4M :'actor- °{;
vrathod ofcoo larL' W43t Ice El Jce Packs D Ice ❑ None
LJ Yes
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NA 3, If to pInture of any cuolcr cxceedcl 6.0 C, wrly Projcrt M;ljl49er Notified?
PM was LN tii led by. p],cnc f email i face -to -farce (circle one).
Yes
No
_[' 'KA 4. [t tiles cammWtdl 9QUHGl''3 pac[cing shp aff5died to this font.?
Yes
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5, Were proper canto -0re6res 41-CJiriquisltedireceivedj fo]fowed''
cs
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6, Were Salk -[,IV IDS listed nn th-e COC? .
Yes
No
17. eresamp=e IDs listed on nll .3am le onutailurS7
1?cs
=Np
S. Was co'lecfic- date & ti n IhI-A on the C:OQ?
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9._ww collection dale & on't I.I& on a I I Sample c-ontainers?
] U. Did all container m
label otforation ([D, date, ticrc) agm,� wh 1:11 COC7
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s
No
IL Were lasts to be performed listed on .be C:DQ?
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11 Did all SFlmpies arrive in the proper containers fur wwh 1v3r3n[For in gccdcandi,inn
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(unbroken, lids or;,
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13. Was adec tra(c sample vollrrme avai lab le` _
14. Were all samples r�eceivud tvitl�' ' fw I;oldingtiu,c ur48 F_qurs, whichcwrctxncs fi;,1.
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P.s.
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-5`bE" (!4"ur Clara io diamrler)
{
in any of the VOA vials?
cs - r,%o A 7. We-evII DJtOee l misfnntricnt swuplrs r_r:eived at a H of { 29
Yes LLJJ 1N,6 A I H. Wern ull cyanide sanlplLs r2ceircd at a UH;- 12 811d sulfide samples naceived o a pH > 9?
❑ Yes ❑N0 A 1 ,Were all &pp tcabl%: NIT;{1'I4z.J+cy+a,rir[rlphen V625.I .3 (< U-1MW Samples fluresidnal rhlcn-ite? of
Q+ 20. %18m client rerawk&kquesrs (i.e. ,pquested dilulium, MSIMSD desigiati{rn�, rtc... j
t Ycs O NG NA corn fly tr7'r9cL7tS(,,d -rpllt tllE COO in-0 tl:e ceiainciiI section In LIlMS12
- 51hc quaLe ;-_L:in rr listed c:t jw container lab41'x
Sample Fremrvutiarl (MLIEt be crurlP.1Ned for any sa:npte(s) incorrectly presrLrvice or vi-Ah hradapace.)
Salnple(s) _ w(-,rc :-cccived lnmi-ectly prey rwtvl a 44'ere ;Ldj:..'steel accordingly
-in �alnple rareivinl; with mL of circle one: H2904, HNj Oq , I IC:1, Naf)H usin# SR # Un.
Tame of preservalior �S �. if morethaltl one preservRtive is needed, please Llate i„ the comments beJovi..
were received witli bubbly s }( lam in dJtm ter.
5nrnplcs(a} _ 'L were received wAlk TRC > U.3 mEfr, 19 is nu) and were
zu[j,lad accor€lingE; in sarnple rerclV3ng xi[a sodrum throsul1h[e (''laaaa) willtJtval}' 1D:
Sit barcode lubcla :appl;mry: gale-
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 217 of 253

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Sample Receipt Checklik (SRC)
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frlearr3 ofreceipl; !' Paao li-rtt UPS F IEx '(ltlier - -
Y cs N L` 1, Wore custucly wrLil� T res+'11t oil t1e to}E5'e - —
Yes Flo NA . Ircustud Y weals were presenlF WCra they jr fact rmcl unbrokeii?
PH StrapLD- Chlorine Strip1D; zo Ie;tCd -KM
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NO
V LN
4. Is the oom> icrcfal anuri-m-'s JMCki�& slily EitLLLC11ed to r},IN torn?
5, Were Pnvr.T custody ]A 2)ud ~res (relinquished, receivred) fol]owkd7
Y-m
Nu
or Yas
NEI
G, Were sainplo IDS iisted Cm the COC"
yes
❑No
-r', Vf_re sample [CPS lisw a,i a'] .:e-nple coittait> ? -
1
Yea
I Lj No
S_ Was colle*Liaia doic & dme liMd un dhe COC7
❑
Yes
Na
9- Was col Icction dale~ & time listed on v 1T sans le ccn1taincx57 -
ywd
; No
1431_ Did all coirtainer la he] infonhnatioE3 (ID, Llx,le, time ZCXtO with ttte CO'
J Ve_e
Na
11. we.- a tests to be prrfcxmcd iisted on th3 COC?
❑ Yes Li-Nn' 12, bid all Siunplcs give In the proper e(alf4incrs for eadi lest andlaa' iu goad eorLf_Von,
(Imbidon, Iids on, Ctr,j'?
Yci I JNQ 13. Ww; rxtlegnabe sample vnfume airailoblk7
Yes hie} 14. Ware all samples rowivcd witl=in V; tho holding time ❑r d$ l,aLos, wt,;ch2:var coihhes _irsL?
5f s No 15. Were anY sernrlcs containers mis3ingis [Lsircie one sanlplcs Not listed t)n jC.'+
`❑ yes No DNA 16. por VIDA. and RSK-175 3auipl&;, were bttbb'es pecWnL ="pea -size" (112'or 6rnri in di0mcicr)
ul any of IFr. VELA 1ria1$?
Ves LJNu NA I e-Wore all DR4fmotLalsrnutrien, Str:3ple5,+et-eivod ate p1l of< 2? - -�
Yes No JJNA l h. Wes' all iryanide sam I ns rUccivad at a PH x 12 anc su] f de Samples race iwod a# a i ] '
d❑Ycs [�Nn ONA 19. Were.Rllapplica aNH-1,xT1fCN.,-yanidJpl3rnoL i_].fi�3$_3 (t- .5m&'L)sainP streeof
residuyl &'rarine?
20_ %V�:rr c:Iirn# reala>rJ sAcquesis (i_e_ req im*d dilutiolhs, 1 &WL%D de l root cu
mTectly Iranscribed fmm the C oic fmp tho ualnniait svclian in LIM';?
es L40 r n
21. Vas the w)Lurn:-ier listed or Lhe coultaithcr labol'? It 'e-% UA. 0L
SarnplePiresurvHdon (blush hn completed foTany mmplf{s, incanwdyp.-0Ar.vcd or with 1Lavdspace.)
5rlmpte(s) 141, wcrc received incar11ectly p,uyyrvcd arc were ftdjt1sted accorairigly
'n sainpte rt=i v ing with NP _ onL of ciTcic� ono; I125O4, HNO3, I-1{:l,jNa() H tisbig 5R l; �
Time of lH cacrvatian NA if more than an t pilrwrvative it. needed, please n oto in tihe orrr merit below,
Sarr P1r*) u were r-coiled with bubbles>6 mrtl in diantiecer_
SsunplCs[s:i z wexe racslve %7t i TkC > a_G rngiL (1f*19 is.ry ) and were
djustad a=rdingly [is bwnpjw receivingVyi(h sodiutn Lhiu5ulfare (Ctia 5 3) with 51healy 13).r CIA
9R barcode labtIu applied by,, 1CeS data: IW304aw
C.I rTmn�htK I
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 219 of 253

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aceAna lytical
Deliver To
LELAP CERTIFICATE NUMBER: 01955
DOD-ELAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
PERFORMED BY
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 11/17/2020
Report Y 210110317
�1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i III
Project Buncombe
Lucas Odom
Pace Analytical Services South Carolina
106 Vantage Point Drive
West Columbia, SC 29172
803 791 9700
L*
PJLA
wAting
WD ELAP
Additional Recipients
NONE
ISO
17025
I
Pace Gulf Coast Report#: 220110317 Page 1 of 33
Page 221 of 253

Report#: 220110317
ZeAnaly�ica!®
Project ID: Buncombe Report Date: 11/17/2020
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
Pace Gulf Coast Report 220110317
Pace Gulf Coast Report#: 220110317 Page 2 of 33
Page 222 of 253

acReport#:
6Anaoical
r Project ID:
220110317
Buncombe
Certifications
Report Date: 11/17/2020
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Pace Gulf Coast Report#: 220110317 Page 3 of 33
Page 223 of 253

Report#: 220110317
ZeAnalyfica!®
Project ID: Buncombe Report Date: 11/17/2020
Case Narrative
Client: Pace Analytical Services South Carolina Report: 220110317
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
VOLATILES GAS CHROMATOGRAPHY
In the AM20GAX analysis for all analytical batches, Methane was detected at a concentration > 1/2 the LOQ in the method blank.
This is probable laboratory contamination.
Pace Gulf Coast Report#: 220110317 Page 4 of 33
Page 224 of 253

Report#: 220110317
ZeAnalytical®
Project ID: Buncombe Report Date: 11/17/2020
Sample Summary
LAB ID Client ID Matrix Collect Date/Time Receive Date/Time
22011031701
MW-18-78
Water
10/26/202013:20
11/03/2020 10:02
22011031702
MW-19-110
Water
10/26/202016:10
11/03/2020 10:02
22011031703
MW-21-94
Water
10/27/2020 09:45
11/03/2020 10:02
22011031704
MW-21-21
Water
10/27/2020 09:35
11/03/2020 10:02
22011031705
MW-19-75
Water
10/27/202011:05
11/03/2020 10:02
22011031706
MW-4
Water
10/27/202013:35
11/03/2020 10:02
22011031707
MW-6
Water
10/27/202014:45
11/03/2020 10:02
22011031708
MW-13-132
Water
10/28/2020 09:40
11/03/2020 10:02
22011031709
MW-24-160
Water
10/28/202013:45
11/03/2020 10:02
22011031710
MW-2
Water
10/29/202017:05
11/03/2020 10:02
22011031711
MW-18-78
Bubble
Strip
10/26/2020 13:20
11/03/2020 10:02
22011031712
MW-19-110
Bubble
Strip
10/26/2020 16:10
11/03/2020 10:02
22011031713
MW-21-94
Bubble
Strip
10/27/2020 09:45
11/03/2020 10:02
22011031714
MW-21-21
Bubble
Strip
10/27/2020 09:35
11/03/2020 10:02
22011031715
MW-19-75
Bubble
Strip
10/27/2020 11:05
11/03/2020 10:02
22011031716
MW-4
Bubble
Strip
10/27/2020 13:35
11/03/2020 10:02
22011031717
MW-6
Bubble
Strip
10/27/2020 14:45
11/03/2020 10:02
22011031718
MW-13-132
Bubble
Strip
10/28/2020 09:40
11/03/2020 10:02
22011031719
MW-24-160
Bubble
Strip
10/28/2020 13:45
11/03/2020 10:02
22011031720
MW-2
Bubble
Strip
10/29/2020 17:05
11/03/2020 10:02
Pace Gulf Coast Report#: 220110317 Page 5 of 33
Page 225 of 253

Report#: 220110317
ZeAnaly�ical®
Project ID: Buncombe Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/26/2020 13:20 LAB ID 22011031701
MW-18-78
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS# Parameter
Result
DL
LOQ
Units
124-38-9 Carbon Dioxide
83200
2540
18000
ug/L
AM23G
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
4.OJ
1.2
5.0
mg/L
64-18-6 Formic Acid
46
0.55
5.0
mg/L
AM20GAX
CAS# Parameter
Result
DL
LOQ
Units
74-84-0 Ethane
1.1
0.075
1.0
ug/L
74-85-1 Ethene
1.3
0.12
1.0
ug/L
74-82-8 Methane
1700
2.5
5.0
ug/L
Collect Date 10/26/2020 16:10 LAB ID 22011031702
MW-19-110
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS#
Parameter
124-38-9
Carbon Dioxide
AM23G
CAS#
Parameter
64-19-7
Acetic Acid
64-18-6
Formic Acid
Result
DL
LOQ
Units
3930
127
900
ug/L
Result
DL
LOQ
Units
0.44J
0.12
0.50
mg/L
4.8
0.055
0.50
mg/L
Pace Gulf Coast Report#: 220110317 Page 6 of 33
Page 226 of 253

aceAnaly�ical®
r
Report#: 220110317
Project ID: Buncombe
Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/26/2020 16:10 LAB ID 22011031702
MW-19-110
Receive Date 11/03/2020 10:02 Matrix Water
AM20GAX
CAS# Parameter Result DL LOQ Units
74-82-8 Methane 400 2.5 5.0 ug/L
Collect Date 10/27/2020 09:45 LAB ID 22011031703
MW-21-94
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS# Parameter
Result
DL
LOQ
Units
124-38-9 Carbon Dioxide
55900
635
4500
ug/L
AM23G
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
0.79J
0.25
1.0
mg/L
64-18-6 Formic Acid
9.5
0.11
1.0
mg/L
AM20GAX
CAS# Parameter
Result
DL
LOQ
Units
74-84-0 Ethane
1.5
0.075
1.0
ug/L
74-85-1 Ethene
0.33J
0.12
1.0
ug/L
74-82-8 Methane
2000
2.5
5.0
ug/L
Collect Date 10/27/2020 09:35 LAB ID 22011031704
MW-21-21
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS# Parameter
124-38-9 Carbon Dioxide
Result
DL
LOQ
Units
165000
1270
9000
ug/L
Pace Gulf Coast Report#: 220110317 Page 7 of 33
Page 227 of 253

Report#: 220110317
ZeAnaly�ical®
Project ID: Buncombe Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/27/2020 09:35 LAB ID 22011031704
MW-21-21
Receive Date 11/03/2020 10:02 Matrix Water
AM23G
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
3.7J
1.2
5.0
mg/L
64-18-6
Formic Acid
44
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58J
0.58
5.0
mg/L
AM20GAX
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
1.1
0.075
1.0
ug/L
74-85-1
Ethene
0.75J
0.12
1.0
ug/L
74-82-8
Methane
1900
2.5
5.0
ug/L
Collect Date 10/27/2020 11:05 LAB ID 22011031705
MW-19-75
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS#
Parameter
124-38-9
Carbon Dioxide
AM23G
CAS#
Parameter
64-19-7
Acetic Acid
64-18-6
Formic Acid
AM20GAX
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
141000
1270
9000
ug/L
Result
DL
LOQ
Units
3.9J
1.2
5.0
mg/L
44
0.55
5.0
mg/L
Result
DL
LOQ
Units
0.67J
0.075
1.0
ug/L
0.46J
0.12
1.0
ug/L
480
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 8 of 33
Page 228 of 253

Report#: 220110317
ZeAnaly�ical®
Project ID: Buncombe Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/27/2020 13:35 LAB ID 22011031706
M W-4
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS# Parameter
Result
DL
LOQ
Units
124-38-9 Carbon Dioxide
177000
2540
18000
ug/L
AM23G
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
4.OJ
1.2
5.0
mg/L
64-18-6 Formic Acid
48
0.55
5.0
mg/L
142-62-1 Hexanoic Acid
0.67J
0.58
5.0
mg/L
AM20GAX
CAS# Parameter
Result
DL
LOQ
Units
74-84-0 Ethane
0.47J
0.075
1.0
ug/L
74-85-1 Ethene
0.46J
0.12
1.0
ug/L
74-82-8 Methane
720
2.5
5.0
ug/L
Collect Date 10/27/2020 14:45 LAB ID 22011031707
MW-6
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS#
Parameter
124-38-9
Carbon Dioxide
AM23G
CAS#
Parameter
64-19-7
Acetic Acid
64-18-6
Formic Acid
AM20GAX
CAS#
Parameter
74-84-0
Ethane
Result
DL
LOQ
Units
197000
2540
18000
ug/L
Result
DL
LOQ
Units
4.1J
1.2
5.0
mg/L
45
0.55
5.0
mg/L
Result
DL
LOQ
Units
0.92J
0.075
1.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 9 of 33
Page 229 of 253

Report#: 220110317
ZeAnaly�ical®
Project ID: Buncombe Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/27/2020 14:45 LAB ID 22011031707
MW-6
Receive Date 11/03/2020 10:02 Matrix Water
AM20GAX (Continued)
CAS# Parameter
Result DL LOQ Units
74-85-1 Ethene
0.30J 0.12 1.0 ug/L
74-82-8 Methane
4700 2.5 5.0 ug/L
Collect Date 10/28/2020 09:40 LAB ID 22011031708
MW-13-132
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS# Parameter
Result
DL
LOQ
Units
124-38-9 Carbon Dioxide
28100
2540
18000
ug/L
AM23G
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
4.OJ
1.2
5.0
mg/L
64-18-6 Formic Acid
44
0.55
5.0
mg/L
AM20GAX
CAS# Parameter
Result
DL
LOQ
Units
74-85-1 Ethene
1.8
0.12
1.0
ug/L
74-82-8 Methane
1400
2.5
5.0
ug/L
Collect Date 10/28/2020 13:45 LAB ID 22011031709
MW-24-160
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 1430 127 900 ug/L
Pace Gulf Coast Report#: 220110317 Page 10 of 33
Page 230 of 253

Report#: 220110317
ZeAnaly�ical®
Project ID: Buncombe Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/28/2020 13:45 LAB ID 22011031709
MW-24-160
Receive Date 11/03/2020 10:02 Matrix Water
AM23G
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.42J
0.12
0.50
mg/L
64-18-6
Formic Acid
4.8
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.060J
0.058
0.50
mg/L
50-21-5
Lactic Acid
0.0581
0.053
0.50
mg/L
AM20GAX
CAS#
Parameter
Result
DL
LOQ
Units
74-85-1
Ethene
0.34J
0.12
1.0
ug/L
74-82-8
Methane
27
2.5
5.0
ug/L
Collect Date 10/29/2020 17:05 LAB ID 22011031710
M W-2
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
CAS#
Parameter
124-38-9
Carbon Dioxide
AM23G
CAS#
Parameter
64-19-7
Acetic Acid
64-18-6
Formic Acid
142-62-1
Hexanoic Acid
AM20GAX
CAS#
Parameter
74-82-8
Methane
Result
DL
LOQ
Units
30000
635
4500
ug/L
Result
DL
LOQ
Units
0.41 J
0.12
0.50
mg/L
5.0
0.055
0.50
mg/L
0.076J
0.058
0.50
mg/L
Result
DL
LOQ
Units
7.7
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 11 of 33
Page 231 of 253

aceAnaly�ica!®
r
Report#: 220110317
Project ID: Buncombe
Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/26/2020 13:20 LAB ID 22011031711
MW-18-78
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 6.6 0.49 1.9 nM
Collect Date 10/26/2020 16:10 LAB ID 22011031712
MW-19-110
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 3.6 0.49 1.9 nM
Collect Date 10/27/2020 09:45 LAB ID 22011031713
MW-21-94
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 5.3 0.98 3.8 nM
Collect Date 10/27/2020 09:35 LAB ID 22011031714
MW-21-21
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
2.7
0.49
1.9
nM
Pace Gulf Coast Report#: 220110317 Page 12 of 33
Page 232 of 253

aceAnaly�ica!®
r
Report#: 220110317
Project ID: Buncombe
Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/27/2020 11:05 LAB ID 22011031715
MW-19-75
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 1.4.1 0.49 1.9 nM
Collect Date 10/27/2020 13:35 LAB ID 22011031716
M W-4
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 4.6 0.49 1.9 nM
Collect Date 10/27/2020 14:45 LAB ID 22011031717
MW-6
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 20 0.49 1.9 nM
Collect Date 10/28/2020 09:40 LAB ID 22011031718
MW-13-132
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
6.0
0.49
1.9
nM
Pace Gulf Coast Report#: 220110317 Page 13 of 33
Page 233 of 253

aceAnaly�ica!®
r
Report#: 220110317
Project ID: Buncombe
Report Date: 11/17/2020
Summary of Compounds Detected
Collect Date 10/28/2020 13:45 LAB ID 22011031719
MW-24-160
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 10 0.49 1.9 nM
Collect Date 10/29/2020 17:05 LAB ID 22011031720
M W-2
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
5.4
0.49
1.9
n M
Pace Gulf Coast Report#: 220110317 Page 14 of 33
Page 234 of 253

Report#: 220110317
ZeAnaly�ical®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/26/2020 13:20 LAB ID 22011031701
MW-18-78
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 11/09/202012:33 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 83200 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 11/09/2020 21:55 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
4.OJ
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
46
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.561-1
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.561-1
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.53U
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.60U
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/09/202015:14 JCK2 696457
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
1.1
0.075
1.0
ug/L
1.3
0.12
1.0
ug/L
1700
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 15 of 33
Page 235 of 253

Report#: 220110317
ZeAnaly�lca!®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/26/2020 16:10 LAB ID 22011031702
MW-19-110
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/09/202012:43 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 3930 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/09/2020 22:48 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.44J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
4.8
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.0581J
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.0561J
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.0531.1
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.0601.1
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/09/202015:25 JCK2 696457
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.0751.1
0.075
1.0
ug/L
0.12U
0.12
1.0
ug/L
400
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 16 of 33
Page 236 of 253

Report#: 220110317
ZeAnaly�lca!®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/27/2020 09:45 LAB ID 22011031703
MW-21-94
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 5 11/09/202012:53 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 55900 635 4500 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 2 11/09/2020 23:41 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.79J
0.25
1.0
mg/L
107-92-6
Butyric Acid
0.12U
0.12
1.0
mg/L
64-18-6
Formic Acid
9.5
0.11
1.0
mg/L
142-62-1
Hexanoic Acid
0.12U
0.12
1.0
mg/L
646-07-1
i-Hexanoic Acid
0.11 U
0.11
1.0
mg/L
503-74-2
i-Pentanoic Acid
0.121-1
0.12
1.0
mg/L
50-21-5
Lactic Acid
0.11 U
0.11
1.0
mg/L
109-52-4
Pentanoic Acid
0.11 U
0.11
1.0
mg/L
79-09-4
Propionic Acid
0.11 U
0.11
1.0
mg/L
127-17-3
Pyruvic Acid
0.121-1
0.12
1.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/11/2020 00:08 JCK2 696614
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
1.5
0.075
1.0
ug/L
0.33J
0.12
1.0
ug/L
2000
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 17 of 33
Page 237 of 253

Report#: 220110317
ZeAnaly�lca!®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/27/2020 09:35 LAB ID 22011031704
MW-21-21
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 11/09/202012:59 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 165000 1270 9000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 11/10/2020 00:35 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
3.7J
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
44
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58J
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.531-1
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.601-1
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/11/2020 00:21 JCK2 696614
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
1.1
0.075
1.0
ug/L
0.75J
0.12
1.0
ug/L
1900
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 18 of 33
Page 238 of 253

Report#: 220110317
ZeAnaly�lca!®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/27/2020 11:05 LAB ID 22011031705
MW-19-75
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 11/09/202013:20 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 141000 1270 9000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 11/10/2020 01:28 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
3.9J
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
44
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.531-1
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.601-1
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/11/2020 00:32 JCK2 696614
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.67J
0.075
1.0
ug/L
0.46J
0.12
1.0
ug/L
480
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 19 of 33
Page 239 of 253

Report#: 220110317
ZeAnaly�lca!®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/27/2020 13:35 LAB ID 22011031706
M W-4
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 11/09/202013:31 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 177000 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 11/10/2020 02:22 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
4.OJ
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
48
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.67J
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.531-1
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.601-1
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/11/2020 00:44 JCK2 696614
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.47J
0.075
1.0
ug/L
0.46J
0.12
1.0
ug/L
720
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 20 of 33
Page 240 of 253

Report#: 220110317
ZeAnaly�lca!®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/27/2020 14:45 LAB ID 22011031707
MW-6
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 11/09/202014:03 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 197000 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 11/10/2020 05:02 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
4.1J
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
45
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.531-1
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.601-1
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/11/2020 00:56 JCK2 696614
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.92J
0.075
1.0
ug/L
0.30J
0.12
1.0
ug/L
4700
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 21 of 33
Page 241 of 253

Report#: 220110317
ZeAnaly�lcal®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/28/2020 09:40 LAB ID 22011031708
MW-13-132
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 11/09/202014:13 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 28100 2540 18000 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 10 11/10/2020 05:55 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
4.OJ
1.2
5.0
mg/L
107-92-6
Butyric Acid
0.58U
0.58
5.0
mg/L
64-18-6
Formic Acid
44
0.55
5.0
mg/L
142-62-1
Hexanoic Acid
0.58U
0.58
5.0
mg/L
646-07-1
i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2
i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5
Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4
Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4
Propionic Acid
0.531-1
0.53
5.0
mg/L
127-17-3
Pyruvic Acid
0.601-1
0.60
5.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/11/202013:37 JCK2 697047
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.0751.1
0.075
1.0
ug/L
1.8
0.12
1.0
ug/L
1400
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 22 of 33
Page 242 of 253

Report#: 220110317
ZeAnaly�lcal®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/28/2020 13:45 LAB ID 22011031709
MW-24-160
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/09/202014:23 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 1430 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/10/2020 06:49 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.42J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
4.8
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.060J
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.0581
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.0561J
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/11/202013:49 JCK2 697047
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.075U
0.075
1.0
ug/L
0.34J
0.12
1.0
ug/L
27
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 23 of 33
Page 243 of 253

Report#: 220110317
ZeAnaly�lca!®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/29/2020 17:05 LAB ID 22011031710
M W-2
Receive Date 11/03/2020 10:02 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 5 11/09/202014:39 BMR 696814
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 30000 635 4500 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/10/2020 07:42 MOS 696861
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.41J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
5.0
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.076J
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.0561J
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.0561J
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.0531.1
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.0601.1
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/11/202016:18 JCK2 697047
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.0751.1
0.075
1.0
ug/L
0.12U
0.12
1.0
ug/L
7.7
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220110317 Page 24 of 33
Page 244 of 253

aceAnaly�ica!®
r
Report#: 220110317
Project ID: Buncombe
Sample Results
Report Date: 11/17/2020
Collect Date 10/26/2020 13:20 LAB ID 22011031711
MW-18-78
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202010:33 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ
6.6 0.49 1.9
Collect Date 10/26/2020 16:10 LAB ID 22011031712
MW-19-110
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202010:45 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ
3.6 0.49 1.9
Collect Date 10/27/2020 09:45 LAB ID 22011031713
MW-21-94
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 2 11/07/202012:35 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
5.3
0.98
3.8
nM
Pace Gulf Coast Report#: 220110317 Page 25 of 33
Page 245 of 253

aceAnaly�ica!®
r
Report#: 220110317
Project ID: Buncombe
Sample Results
Report Date: 11/17/2020
Collect Date 10/27/2020 09:35 LAB ID 22011031714
MW-21-21
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202011:10 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ
2.7 0.49 1.9
Collect Date 10/27/2020 11:05 LAB ID 22011031715
MW-19-75
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202011:22 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ
1.4.1 0.49 1.9
Collect Date 10/27/2020 13:35 LAB ID 22011031716
M W-4
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202011:34 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
4.6
0.49
1.9
nM
Pace Gulf Coast Report#: 220110317 Page 26 of 33
Page 246 of 253

aceAnaly�ica!®
r
Report#: 220110317
Project ID: Buncombe
Sample Results
Report Date: 11/17/2020
Collect Date 10/27/2020 14:45 LAB ID 22011031717
MW-6
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202011:46 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ
20 0.49 1.9
Collect Date 10/28/2020 09:40 LAB ID 22011031718
MW-13-132
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202011:58 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ
6.0 0.49 1.9
Collect Date 10/28/2020 13:45 LAB ID 22011031719
MW-24-160
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202012:10 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
10
0.49
1.9
nM
Pace Gulf Coast Report#: 220110317 Page 27 of 33
Page 247 of 253

Report#: 220110317
ZeAnaly�ica!®
Project ID: Buncombe Report Date: 11/17/2020
Sample Results
Collect Date 10/29/2020 17:05 LAB ID 22011031720
M W-2
Receive Date 11/03/2020 10:02 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/202012:22 AWE 696773
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ Units
5.4 0.49 1.9 n M
Pace Gulf Coast Report#: 220110317 Page 28 of 33
Page 248 of 253

acReport#:
6Anaoical
Project ID:
220110317
Buncombe
GC Volatiles QC Summary
Report Date: 11/17/2020
Analytical Batch Client ID
MB696814
LCS696814
LCSD696814
696814 LAB ID
2108446
2108447
2108448
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
11/09/20 09:08
11/09/20 09:17
11/09/20 09:22
Matrix
Water
Water
Water
EPA RSK-175
Units
ug/L
Spike
Result
%R
I
I Control
Spike
Result
I
%R
I
RPD
RPD
Result
DLI
Added
Limits%R
1 Added
Limit
Carbon Dioxide 124-38-9
127U
127
8700
9990
115
38 - 147
8700
9330
107
7
40
Pace Gulf Coast Report#: 220110317 Page 29 of 33
Page 249 of 253

acReport#:
6Anaoical
Project ID:
220110317
Buncombe
General Chemistry QC Summary
Report Date: 11/17/2020
Analytical Batch Client ID
MB696861
LCS696861
LCSD696861
696861 LAB ID
2108728
2108729
2108730
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
11/09/20 17:28
11/09/20 16:34
11/10/20 03:15
Matrix
Water
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Acetic Acid
64-19-7
0.12U
0.12
2.0
2.0
100
70 - 130
2.0
2.0
100
0
20
Butyric Acid
107-92-6
0.058U
0.058
2.0
2.0
103
70 - 130
2.0
2.0
103
0
20
Formic Acid
64-18-6
0.055U
0.055
2.0
2.0
101
70 - 130
2.0
2.0
102
1
20
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
2.0
101
70 - 130
2.0
2.0
101
1
20
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
2.0
100
70 - 130
2.0
2.0
99
1
20
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
2.1
104
70 - 130
2.0
2.1
104
0
20
Lactic Acid
50-21-5
0.053U
0.053
2.0
2.0
99
70 - 130
2.0
2.0
99
0
20
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
2.0
98
70 - 130
2.0
2.0
98
0
20
Propionic Acid
79-09-4
0.053U
0.053
2.0
2.0
102
70 - 130
2.0
2.0
102
1
20
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
1.8
88
70 - 130
2.0
1.8
90
3
20
Pace Gulf Coast Report#: 220110317 Page 30 of 33
Page 250 of 253

acReport#:
6Anaoical
Project ID:
220110317
Buncombe
General Chromatography QC Summary
Report Date: 11/17/2020
Analytical Batch Client ID
MB696773
LCS696773
LCSD696773
696773 LAB ID
2108237
2108238
2108239
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
11/07/20 10:21
11/07/20 09:57
11/07/20 10:09
Matrix
AM20GAX
Units
nM
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Hydrogen 1333-74-0
0.49U
0.49
12
10
87
70 - 130
12
11194
8
20
Analytical Batch
Client ID
MB696457
LCS696457
LCSD696457
696457
LAB ID
2106231
2106232
2106233
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
11/09/20 11:25
11/09/20 10:49
11/09/20 11:01
Matrix
Water
Water
Water
AM20GAX
Units
ug/L
Spike
I Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Ethane
74-84-0
0.075U
0.075
100
96
95
70-130
100
81
80
18
20
Ethene
74-85-1
0.12U
0.12
140
130
93
70 - 130
140
110
80
16
20
Methane
74-82-8
4.7J
2.5
490
460
94
70-130
490
390
80
16
20
Analytical Batch
Client ID
MB696614
LCS696614
LCSD696614
696614
LAB ID
2107091
2107092
2107093
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
11/10/20 21:21
11/10/20 20:45
11/10/20 20:57
Matrix
Water
Water
Water
AM20GAX
Units
ug/L
Spike
I Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Ethane
74-84-0
0.075U
0.075
100
98
97
70 - 130
100
94
93
4
20
Ethene
74-85-1
0.23J
0.12
140
140
96
70 - 130
140
130
92
4
20
Methane
74-82-8
2.9,1
2.5
490
450
93
70-130
490
440
90
3
20
Analytical Batch
Client ID
MB697047
LCS697047
LCSD697047
697047
LAB ID
2109743
2109744
2109745
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
11/11/20 10:19
11/11/20 09:43
11/11/20 09:56
Matrix
Water
Water
Water
AM20GAX
Units
ug/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
i
LiT
Ethane
74-84-0
0.075U
0.075
100
95
94
70 - 130
100
82
81
15
Ethene
74-85-1
0.12U
0.12
140
130
92
70-130
140
110
80
14Methane
74-82-8
2.9J
2.5
490
410
84
70-130
490
350
72
16
Pace Gulf Coast Report#: 220110317 Page 31 of 33
Page 251 of 253

Client ID: Shealy Envir - PaceAnalyticalServices South Carolina
Shealy Environmental Services, Inc. SDG: 220110317
Chain -of 106 Vantage Point Drive I I I
F1-Of-CUStOdy Record — West Columbia, South Carolina 29172 PM: RWe
Telephone No. [phone] Fax No. (803) 791-
www.shealylab.com
Client Report to Contact Telephone No. / E-mail Quote No.
Pace Analytical - Columbia Lucas Odom 803-206-9537/[e-mail]
Address Sampler's Signature Analysis (Attach list if more space is needed) Page
106 Vantage Point Dr. 1 of 1
City State Zip Code X
West Columbia I SC 129172 Printed Name
Project Name Laboratory Lot Number
Closed Buncombe County Landfill Monitoring Wells
Project Number P.0 No. No of Containers b
Matrix
Y
0 0
Preservative Ty
De
m
o
cv
Remarks /Cooler I.D.
Sample ID / Description
(Containers for each sample maybe combined on one line)
Date
Time
0 Q
11
U
o o o'
o o Air
m p c° =
a rn O t) O
Z = m
Y Y
m a
co
=
vi
Q
O
V
L�l
¢ CO Z
4
N
= 2 Z
m
o
N
0
iL
>
Lu
MW-18-78
10/26/2020
1320
G
x
X
X
X
X
/ VJ27055-001 �I
MW-19-110
10/26/2020
1610
G
x
X
X
X
X
PLVJ27055-002 I L
MW-21-94
10/27/2020
945
G
x
X
X
X
X
L3VJ27055-003 I3
MW-21-21
10/27/2020
935
G
x
X
X
X
X
klllVJ27055-004
MW-19-75
10/27/2020
1105
G
x
X
X
X
X
VJ27055-005 15
MW-4
10/27/2020
1335
G
x
X
X
X
X
VJ27055-008 10
MW-6
10/27/2020
1445
G
x
X I
X
X
X
'I VJ27055-009 tj
MW-13-132
10/28/2020
940
G
x
X I
X
X
X
T VJ27055-012 I�
MW-24-160
10/28/2020
1345
G
x
X I
X
X
X
LL
7055-015 G�
MW-2 10/29/2020 1705
G x
X X X X
(0 VJ27055 021 vv
Turn Around Time Required (Prior lab approval required for a pedited TAT)
Sample Disposal
Possible Hazard Identification (List any known hazards in the remarks)
QC Requirements
X Standard Rush
-_
ElReturn to Client BDis(poossal by Lab
❑Non -Hazardous alammable ❑Skin Irritant DDS provided ❑Inknown
1. Relinquished by ^
t
Tt `
1. Received by
Date
Time
e
`
W
12.
2. Relinquished by f--. t
Timp
_
Received by 1,
r:
4. Relinquished by
10
Note: All samples are retained for four weeks from receipt 1 I B USE ONLY
unless other arrangements are made. I O� o � 3�k4 L0� eceived on Ice (Check) nY []4 E]ce Pack Receipt Temp °C
01
1 G%4 Document Number: ME0020W-01
Pace Gulf Coast Report#: 220110317 Page 32 of 33
Page 252 of 253

i'auaimiytn:s SAMPLE RECEIVING CHECKLIST IIIIIIIIIIVII
SAMPLE DELIVERY GROUP
220110317
CHECKLIST
YES
NO
Client PM RUUe
Transport Method
Samples received with proper thermal preservation?
*❑
❑
Shealy Envir - Pace Analytical
FEDDC
Services South Carolina
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
*❑
*❑
❑
❑
Profile Number
Received By
285031
N/bane, Dodie K
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
*❑
0
❑
❑
Line Item(s)
Receive Date(s)
1 - LHC and Perm gases VFA
11/03/20
2- Hydrogen
Preservative added to any containers?
❑
0
If received, was headspace for VOC water containers < 6mm?
0
❑
Samples collected in containers provided by Pace Gulf Coast?
0
❑
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer ID E26
Temp °C
None
None
166334646755
4.9
NOTES
Pevision 1.6
Page 1 of 1
Pace Gulf Coast Report#: 220110317
Page 253 of 253
Page 33 of 33

0
aceAnalytical
Report of Analysis
Bunnell-Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Attention: Andy Alexander
Project Name: Closed Buncombe County Landfill Surface Water
Project Number: J20-14175-04
Lot Number:VJ27054
Date Completed:11/05/2020
11 /06/2020 4:35 PM
Approved and released by:
Project Manager II: Lucas Odom
PCCRF�
24rA
SOA
/
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 37

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Bunnell-Lammons Engineering, Inc.
Lot Number: VJ27054
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
VOCs by GC/MS
The laboratory control sample (LCS) for analytical batch 72213 exceeded acceptance criteria for
Bromomethane, Chloroethane, Vinyl Chloride, and Chloromethane. These analytes were biased high but
were not detected in the samples affected.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 37

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: VJ27054
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
SW-2A
Aqueous
10/26/20201420
10/27/2020
002
SW-2
Aqueous
10/26/20201440
10/27/2020
003
SW-4
Aqueous
10/26/20201700
10/27/2020
004
SW-3
Aqueous
10/26/20201735
10/27/2020
005
SW-1
Aqueous
10/26/20201805
10/27/2020
006
Trip blank
Aqueous
10/26/2020
10/27/2020
(6 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 37

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: VJ27054
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
SW-2A
Aqueous
1,4-Dioxane
8260D (SIM)
12
ug/L
5
001
SW-2A
Aqueous
Antimony
6020B
0.58
J
ug/L
6
001
SW-2A
Aqueous
Barium
6020B
29
ug/L
6
001
SW-2A
Aqueous
Nickel
6020B
1.3
J
ug/L
6
002
SW-2
Aqueous
Barium
6020B
31
ug/L
9
002
SW-2
Aqueous
Nickel
6020B
1.4
J
ug/L
9
003
SW-4
Aqueous
Barium
6020B
15
ug/L
11
003
SW-4
Aqueous
Lead
6020B
0.53
J
ug/L
11
003
SW-4
Aqueous
Zinc
6020B
4.4
J
ug/L
12
004
SW-3
Aqueous
Acetone
8260D
5.3
J
ug/L
13
004
SW-3
Aqueous
Barium
6020B
16
ug/L
14
004
SW-3
Aqueous
Lead
6020B
0.58
J
ug/L
14
005
SW-1
Aqueous
Barium
6020B
16
ug/L
17
005
SW-1
Aqueous
Copper
6020B
1.5
J
ug/L
17
005
SW-1
Aqueous
Lead
6020B
0.80
J
ug/L
17
005
SW-1
Aqueous
Zinc
6020B
3.9
J
ug/L
17
(16 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-001
Description: SW-2A Matrix: Aqueous
Date Sampled:10/26/2020 1420
Date Received:10/27/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 10/31/2020 0626 DJG
71851
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
12
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
108 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201516 TML
72224
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-001
Description: SW-2A Matrix: Aqueous
Date Sampled:10/26/2020 1420
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201516 TML 72224
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
114 70-130
1,2-Dichloroethane-d4
119 70-130
Toluene-d8
121 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/03/2020 0221 BPK
10/30/2020 1549 71494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
0.58 J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
29
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
1.3 J
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-001
Description: SW-2A Matrix: Aqueous
Date Sampled:10/26/2020 1420
Date Received:10/27/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/03/2020 0221 BPK
10/30/2020 1549 71494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-002
Description: SW-2 Matrix: Aqueous
Date Sampled:10/26/2020 1440
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201541 TML 72224
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-002
Description: SW-2 Matrix: Aqueous
Date Sampled:10/26/2020 1440
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201541 TML
72224
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
116 70-130
1,2-Dichloroethane-d4
120 70-130
Toluene-d8
123 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/03/2020 0229 BPK
10/30/2020 1549 71494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
31
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
1.4 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-003
Description: SW-4 Matrix: Aqueous
Date Sampled:10/26/2020 1700
Date Received:10/27/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
2 5030B
8260D (SIM) 1 11/02/2020 1427 BWS
71945
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
2
Run 2 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
95 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201607 TML
72224
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-003
Description: SW-4 Matrix: Aqueous
Date Sampled:10/26/2020 1700
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201607 TML 72224
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
113 70-130
1,2-Dichloroethane-d4
119 70-130
Toluene-d8
118 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/03/2020 0236 BPK
10/30/2020 1549 71494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
15
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.53 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-003
Description: SW-4 Matrix: Aqueous
Date Sampled:10/26/2020 1700
Date Received:10/27/2020
ICP-MS Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 11/03/2020 0236 BPK 10/30/2020 1549 71494
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Selenium
7782-49-2
Silver
7440-22-4
Thallium
7440-28-0
Vanadium
7440-62-2
Zinc
7440-66-6
6020B
ND
5.0
1.3
ug/L 1
6020B
ND
1.0
0.25
ug/L 1
6020B
ND
0.50
0.15
ug/L 1
6020B
ND
5.0
2.5
ug/L 1
6020B
4.4 J
10
2.5
ug/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-004
Description: SW-3 Matrix: Aqueous
Date Sampled:10/26/2020 1735
Date Received:10/27/2020
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 10/31/2020 0715 DJG
71851
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
106 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201632 TML
72224
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
5.3 J
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-004
Description: SW-3 Matrix: Aqueous
Date Sampled:10/26/2020 1735
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201632 TML 72224
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
114 70-130
1,2-Dichloroethane-d4
117 70-130
Toluene-d8
120 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/03/2020 0243 BPK
10/30/2020 1549 71494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
16
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.58 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-004
Description: SW-3 Matrix: Aqueous
Date Sampled:10/26/2020 1735
Date Received:10/27/2020
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/03/2020 0243 BPK
10/30/2020 1549 71494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-005
Description: SW-1 Matrix: Aqueous
Date Sampled:10/26/2020 1805
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201657 TML 72224
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-005
Description: SW-1 Matrix: Aqueous
Date Sampled:10/26/2020 1805
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/04/20201657 TML
72224
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
115 70-130
1,2-Dichloroethane-d4
121 70-130
Toluene-d8
122 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/03/2020 0306 BPK
10/30/2020 1549 71494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
16
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.5 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.80 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
3.9 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-006
Description: Trip blank Matrix: Aqueous
Date Sampled:10/26/2020
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201105 TML 72213
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 37

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: VJ 27054-006
Description: Trip blank Matrix: Aqueous
Date Sampled:10/26/2020
Date Received:10/27/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/04/20201105 TML 72213
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
95 70-130
95 70-130
98 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 37

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 37

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: VQ71851-001 Matrix: Aqueous
Batch: 71851 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 10/30/2020 2310
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
103 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 37

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: VQ71851-002 Matrix: Aqueous
Batch: 71851 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 46 1 91 70-130 10/30/2020 2157
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
104 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 37

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: VQ71945-001 Matrix: Aqueous
Batch: 71945 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11102120201010
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
95 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 37

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: VQ71945-002
Matrix: Aqueous
Batch: 71945
Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
1,4-Dioxane
50
52
1 105 70-130 11/02/2020 0910
Surrogate
Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
109 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 37

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72213-001 Matrix: Aqueous
Batch: 72213 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/04/2020 1004
Acrylonitrile
ND
1
20
0.80
ug/L
11/04/2020 1004
Benzene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Bromoform
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/04/2020 1004
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/04/2020 1004
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Chloroethane
ND
1
2.0
0.40
ug/L
11/04/2020 1004
Chloroform
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/04/2020 1004
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/04/2020 1004
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/04/2020 1004
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
2-Hexanone
ND
1
10
2.0
ug/L
11/04/2020 1004
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/04/2020 1004
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/04/2020 1004
Methylene chloride
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Styrene
ND
1
1.0
0.41
ug/L
11/04/2020 1004
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Toluene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Trichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 1004
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 37

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72213-001 Matrix: Aqueous
Batch: 72213 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/04/2020 1004
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/04/2020 1004
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 98 70-130
Toluene-d8 100 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 37

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72213-002
Matrix:
Aqueous
Batch: 72213
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q
Dil
% Rec
Limit
Analysis Date
Acetone
100
120
1
117
60-140
11/04/2020 0853
Acrylonitrile
100
110
1
115
70-130
11/04/2020 0853
Benzene
50
53
1
107
70-130
11/04/2020 0853
Bromochloromethane
50
51
1
103
70-130
11/04/2020 0853
Bromodichloromethane
50
49
1
99
70-130
11/04/2020 0853
Bromoform
50
44
1
88
70-130
11/04/2020 0853
Bromomethane (Methyl bromide)
50
75
N
1
151
70-130
11/04/2020 0853
2-Butanone (MEK)
100
110
1
109
70-130
11/04/2020 0853
Carbon disulfide
50
53
1
106
70-130
11/04/2020 0853
Carbon tetrachloride
50
52
1
104
70-130
11/04/2020 0853
Chlorobenzene
50
53
1
105
70-130
11/04/2020 0853
Chloroethane
50
67
N
1
134
70-130
11/04/2020 0853
Chloroform
50
53
1
106
70-130
11/04/2020 0853
Chloromethane (Methyl chloride)
50
76
N
1
152
60-140
11/04/2020 0853
1,2-Dibromo-3-chloropropane (DBCP)
50
51
1
101
70-130
11/04/2020 0853
Dibromochloromethane
50
47
1
94
70-130
11/04/2020 0853
1,2-Dibromoethane (EDB)
50
51
1
101
70-130
11/04/2020 0853
Dibromomethane (Methylene bromide)
50
50
1
100
70-130
11/04/2020 0853
trans- 1,4-Dichloro-2-butene
50
52
1
104
70-130
11/04/2020 0853
1,2-Dichlorobenzene
50
55
1
110
70-130
11/04/2020 0853
1,4-Dichlorobenzene
50
54
1
108
70-130
11/04/2020 0853
1,1-Dichloroethane
50
55
1
111
70-130
11/04/2020 0853
1,2-Dichloroethane
50
50
1
101
70-130
11/04/2020 0853
1,1-Dichloroethene
50
56
1
112
70-130
11/04/2020 0853
cis- 1,2-Dichloroethene
50
54
1
107
70-130
11/04/2020 0853
trans- 1,2-Dichloroethene
50
54
1
108
70-130
11/04/2020 0853
1,2-Dichloropropane
50
51
1
103
70-130
11/04/2020 0853
cis- 1,3-Dichloropropene
50
50
1
100
70-130
11/04/2020 0853
trans- 1,3-Dichloropropene
50
49
1
98
70-130
11/04/2020 0853
Ethylbenzene
50
54
1
109
70-130
11/04/2020 0853
2-Hexanone
100
110
1
108
70-130
11/04/2020 0853
Methyl iodide (lodomethane)
50
52
1
103
70-130
11/04/2020 0853
4-Methyl-2-pentanone
100
110
1
105
70-130
11/04/2020 0853
Methylene chloride
50
53
1
105
70-130
11/04/2020 0853
Styrene
50
52
1
105
70-130
11/04/2020 0853
1,1,1,2-Tetrachloroethane
50
50
1
101
70-130
11/04/2020 0853
1,1,2,2-Tetrachloroethane
50
58
1
115
70-130
11/04/2020 0853
Tetrachloroethene
50
51
1
103
70-130
11/04/2020 0853
Toluene
50
53
1
106
70-130
11/04/2020 0853
1,1,1-Trichloroethane
50
53
1
106
70-130
11/04/2020 0853
1,1,2-Trichloroethane
50
52
1
104
70-130
11/04/2020 0853
Trichloroethene
50
49
1
99
70-130
11/04/2020 0853
Trichlorofluoromethane
50
61
1
121
70-130
11/04/2020 0853
1,2,3-Trichloropropane
50
55
1
109
70-130
11/04/2020 0853
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 37

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72213-002
Matrix:
Aqueous
Batch: 72213
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Vinyl acetate
50
50
1
101
60-140
11/04/2020 0853
Vinyl chloride
50
68 N
1
136
70-130
11/04/2020 0853
Xylenes (total)
100
110
1
107
70-130
11/04/2020 0853
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 101 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 37

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72224-001 Matrix: Aqueous
Batch: 72224 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/04/2020 1115
Acrylonitrile
ND
1
20
0.80
ug/L
11/04/2020 1115
Benzene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Bromoform
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/04/2020 1115
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/04/2020 1115
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Chloroethane
ND
1
2.0
0.40
ug/L
11/04/2020 1115
Chloroform
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/04/2020 1115
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/04/2020 1115
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/04/2020 1115
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
2-Hexanone
ND
1
10
2.0
ug/L
11/04/2020 1115
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/04/2020 1115
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/04/2020 1115
Methylene chloride
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Styrene
ND
1
1.0
0.41
ug/L
11/04/2020 1115
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Toluene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Trichloroethene
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/04/2020 1115
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 37

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ72224-001 Matrix: Aqueous
Batch: 72224 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/04/2020 1115
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/04/2020 1115
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 115 70-130
1,2-Dichloroethane-d4 116 70-130
Toluene-d8 120 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 37

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72224-002
Matrix:
Aqueous
Batch: 72224
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
120
1
119
60-140
11/04/2020 1025
Acrylonitrile
100
110
1
108
70-130
11/04/2020 1025
Benzene
50
50
1
100
70-130
11/04/2020 1025
Bromochloromethane
50
50
1
100
70-130
11/04/2020 1025
Bromodichloromethane
50
49
1
98
70-130
11/04/2020 1025
Bromoform
50
50
1
100
70-130
11/04/2020 1025
Bromomethane (Methyl bromide)
50
59
1
118
70-130
11/04/2020 1025
2-Butanone (MEK)
100
100
1
101
70-130
11/04/2020 1025
Carbon disulfide
50
48
1
97
70-130
11/04/2020 1025
Carbon tetrachloride
50
51
1
101
70-130
11/04/2020 1025
Chlorobenzene
50
49
1
99
70-130
11/04/2020 1025
Chloroethane
50
49
1
98
70-130
11/04/2020 1025
Chloroform
50
49
1
97
70-130
11/04/2020 1025
Chloromethane (Methyl chloride)
50
51
1
102
60-140
11/04/2020 1025
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
94
70-130
11/04/2020 1025
Dibromochloromethane
50
51
1
101
70-130
11/04/2020 1025
1,2-Dibromoethane (EDB)
50
48
1
95
70-130
11/04/2020 1025
Dibromomethane (Methylene bromide)
50
48
1
96
70-130
11/04/2020 1025
trans- 1,4-Dichloro-2-butene
50
48
1
97
70-130
11/04/2020 1025
1,2-Dichlorobenzene
50
48
1
96
70-130
11/04/2020 1025
1,4-Dichlorobenzene
50
47
1
93
70-130
11/04/2020 1025
1,1-Dichloroethane
50
50
1
100
70-130
11/04/2020 1025
1,2-Dichloroethane
50
50
1
100
70-130
11/04/2020 1025
1,1-Dichloroethene
50
52
1
103
70-130
11/04/2020 1025
cis- 1,2-Dichloroethene
50
50
1
100
70-130
11/04/2020 1025
trans- 1,2-Dichloroethene
50
49
1
99
70-130
11/04/2020 1025
1,2-Dichloropropane
50
49
1
99
70-130
11/04/2020 1025
cis- 1,3-Dichloropropene
50
48
1
97
70-130
11/04/2020 1025
trans- 1,3-Dichloropropene
50
48
1
96
70-130
11/04/2020 1025
Ethylbenzene
50
48
1
97
70-130
11/04/2020 1025
2-Hexanone
100
97
1
97
70-130
11/04/2020 1025
Methyl iodide (lodomethane)
50
49
1
99
70-130
11/04/2020 1025
4-Methyl-2-pentanone
100
100
1
104
70-130
11/04/2020 1025
Methylene chloride
50
49
1
98
70-130
11/04/2020 1025
Styrene
50
48
1
96
70-130
11/04/2020 1025
1,1,1,2-Tetrachloroethane
50
49
1
98
70-130
11/04/2020 1025
1,1,2,2-Tetrachloroethane
50
48
1
97
70-130
11/04/2020 1025
Tetrachloroethene
50
49
1
99
70-130
11/04/2020 1025
Toluene
50
50
1
99
70-130
11/04/2020 1025
1,1,1-Trichloroethane
50
49
1
97
70-130
11/04/2020 1025
1,1,2-Trichloroethane
50
50
1
99
70-130
11/04/2020 1025
Trichloroethene
50
49
1
98
70-130
11/04/2020 1025
Trichlorofluoromethane
50
50
1
100
70-130
11/04/2020 1025
1,2,3-Trichloropropane
50
47
1
94
70-130
11/04/2020 1025
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 37

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ72224-002
Matrix:
Aqueous
Batch: 72224
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Vinyl acetate
50
44
1
89
60-140
11/04/2020 1025
Vinyl chloride
50
56
1
112
70-130
11/04/2020 1025
Xylenes (total)
100
95
1
95
70-130
11/04/2020 1025
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 98 70-130
Toluene-d8 101 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 37

ICP-MS Metals - MB
Sample ID: VQ71494-001 Matrix: Aqueous
Batch: 71494 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 10/30/2020 1549
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/03/2020 0029
Arsenic
ND
1
2.0
1.3
ug/L
11/03/2020 0029
Barium
ND
1
5.0
1.3
ug/L
11/03/2020 0029
Beryllium
ND
1
0.40
0.15
ug/L
11/03/2020 0029
Cadmium
ND
1
0.50
0.13
ug/L
11/03/2020 0029
Chromium
ND
1
5.0
1.3
ug/L
11/03/2020 0029
Cobalt
ND
1
5.0
1.3
ug/L
11/03/2020 0029
Copper
ND
1
5.0
1.3
ug/L
11/03/2020 0029
Lead
ND
1
1.0
0.25
ug/L
11/03/2020 0029
Nickel
ND
1
5.0
1.3
ug/L
11/03/2020 0029
Selenium
ND
1
5.0
1.3
ug/L
11/03/2020 0029
Silver
ND
1
1.0
0.25
ug/L
11/03/2020 0029
Thallium
ND
1
0.50
0.15
ug/L
11/03/2020 0029
Vanadium
ND
1
5.0
2.5
ug/L
11/03/2020 0029
Zinc
ND
1
10
2.5
ug/L
11/03/2020 0029
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 37

ICP-MS Metals - LCS
Sample ID: VQ71494-002
Matrix:
Aqueous
Batch: 71494
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
10/30/2020 1549
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
99
1
99
80-120
11/03/2020 0036
Arsenic
100
100
1
101
80-120
11/03/2020 0036
Barium
100
95
1
95
80-120
11/03/2020 0036
Beryllium
100
100
1
103
80-120
11/03/2020 0036
Cadmium
100
100
1
100
80-120
11/03/2020 0036
Chromium
100
110
1
108
80-120
11/03/2020 0036
Cobalt
100
110
1
110
80-120
11/03/2020 0036
Copper
100
100
1
104
80-120
11/03/2020 0036
Lead
100
110
1
112
80-120
11/03/2020 0036
Nickel
100
110
1
108
80-120
11/03/2020 0036
Selenium
100
92
1
92
80-120
11/03/2020 0036
Silver
100
110
1
105
80-120
11/03/2020 0036
Thallium
100
110
1
112
80-120
11/03/2020 0036
Vanadium
100
110
1
107
80-120
11/03/2020 0036
Zinc
100
94
1
94
80-120
11/03/2020 0036
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 37

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 37

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0 YHsj ❑ N01 111. Did al. sample, arrive in the proper cbmailiers foT each test ondiu in goad oonditian
(untlaen, [ids on, v4c_)7
❑ yes QNo
13- Was adequate Earn le volrur-c uvr.ilst.b10
14, Were all ssLTnplvs received WIit1lIn '.A the ]told
12. Wicpe m. y samples co m a iners mi sing} •m- ,
NA 16- For VOA and RSV_-175 samples, were httbb
❑ I m arry ofthoVOAvials?
ngtimc or48 hours, whi0yw comes ftrst'T
(circle cute) senples Not 0sled on COG? —
=h Prts;<u[ {"pe2-sire" (!/2'ar 61nm in di am r)
{ Yes tNo Nth 17. Were all DRJC*trtH'.Vi"utriettt SM,plt5 MCEiVC( at a pl I o°< V
}(r s Tl a K Tv A 18. Wall Ill ,Hide s tmnl Gs received at n pH > l anti s� Ittde sasnp 6r s ri c :=ued at a p[ I $?
wue all appucableRlFi�1[[C7llcynnirk+Irnen�fllF'35.11608. (�O,Smg+IL)Samples NQof
r] Yes ❑ No ❑NA residual e�lurirpe?
20- Wcrc eEent rctcsafksfrequests (Le, requested d:lutinns, WN15D designatiot35. etc. -A
❑ Yes' ElNo. �-lA oorfewly tpnsari1:Md from th,3 OOC into t-ie comment section in LTMS?
Ly 0s1 ED No 1 91, leas tltc quote titnrbar listed an ale container labr±l? J f s, Qur,te'� "A
Sam& Frz9orvatian (Must be owipicied f❑r any sanrp]a(s) incorrectly preserved ar wi'h headspace.)
eanple(s) NA were reccivcd incorrectly preserved and w;,Tm adjusted accorci;
t sample race vhs wit.'t ' mL of Circle onus: MR04, I IN05, KC], NaOH µ�iiLL SR- it L4A
iiI12 of presctntlon NA Tf mare than o o pnrervative is needed, #Iciaw ante in die 4 OMMMIa below,
aetlal (s) NA wemr ceivedwith bubbles_}6 mm in ditsmdcr,
am ples(x) ter. —were received w lth TRC :- 0.5 mt & (lf # 19 is no) and ire:e
djusted in sampleTeC&Mng with soditlm thinSulJ'atti. Na,2%03) with Shealy IU. TA --
R hucoca Iabch appl: by, t[r s
jD
17i11�: I Ir1�7� rQU
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
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