6002_Mecklenburg_HolbrooksRoad_MSWLF_March2021GW_FID1575220_20210405

�ENR USE ONLY: I I ❑Paper Report ❑Electronic Data - Email CD
NC DENR
Division of Waste Management - Solid Waste
loaded: Yes / No
Doc/Event #:
Environmental Monitoring
Reaortina Form
Notice: This
form and
any
information attached
to it are "Public Records"
as defined
in NC
General Statute 132-1. As such, these documents are
available for
inspection
and
examination by any
person upon request (NC
General Statute 132-6),
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzvmski, P.G.
E-mail: [e-mail]
name:
Holbrooks Road Landfill
Address:
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Permit # (.0500 or .1600) October 20-24, 2006)
.0500 March 9-10, 2021,
March 25, 2021
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring Q Detection Monitoring ❑ Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells Q
Groundwater monitoring data from private water supply wells
Leachate monitoring data
Surface water monitoring data ❑
Notification attached?
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 26 surface water standard or NC S01id Waste GA and
preliminary analysis of the cause and significance of any concentration.
FRI Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G. _ Project Manager 980-314-3855
�Hrea �oae� i eiepnone rvumper
Affix NC Licensed/ Professional Geologist Seal
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

MECKLENBURU COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
Apri15, 2021
Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Holbroolcs Road Landfill Permit 60-02
Semi-annual WQ Monitoring
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Holbrooks Road Landfill March 9-10, 2021 in accordance with the approved sample and
analysis plan dated March 27, 2003. This report details the results of that monitoring
event. Laboratory analytical data, field -measured data table of values exceeding 2L
standards is contained on the electronic data deliverable submittal.
Samples were collected from eleven (11) monitoring wells (HRW-7, HRW-8, HRW-9R,
H19C%.W-10, HRW-11 R, HRW-13, HRW-10, HRW- 18. HRW-19, HRW-20 and Ells. W-21)
and three (3) surface -water sampling locations (HRSW-2, HRSW-3 and HRSW4).
Samples were analyzed for metals and volatile organic compounds ("VOCs") listed in
Appendix I of 40 CFR Part 258.54 "Detection monitoring program". Samples were also
analyzed for 1,4-Dioxane as required as of July 1, 2018. Field measurements of
temperature, pH, and specific conductivity were made at each sampling location using a
calibrated instrument. Additionally, measurements of dissolved oxygen were made at
each surface -water sampling location.
The electronic data deliverable package containing the monitoring data is labeled to
reflect the units used for reporting. Surface water standards listed are the water quality
standards established for freshwater classification for aquatic life as outlined in 15A
NCAC 2B "Classification and Water Quality Standards Applicable to Surface Waters of
North Carolina". Groundwater standards li
Nsted are the standards outlined in 15A NCAC
2L "Classification of Water Quality Standards applicable to the Groundwaters of North
Carolina". If the sample is reported in parts per billion, then the standard is also reported
in parts per billion.
PEOPLE •PRIDE PROGRESS •PARTNERSHIP
2145 Suttle Ave •Charlotte, North Carolina 28208 • [phone] Fax [phone]
www.wipeoutwaste. com

Page 2
Surface -water samples:
Barium was detected in all 3 stream sampling locations. The following table summarizes
the metals detections for the surface water sampling locations.
Sample Location
Barium
u /1
HRSW-2 upstream
32.7
HRSW-4 mid -stream
31.2
HRSW-3 downstream
32.8
No VOCs were detected in any of the samples collected from the three surface -water
sampling locations (HRSW-2, HRSW4 and HRSW-3). All field -measured parameters
were within the established regulatory limits. The following table summarizes field -
measured parameters for surface water samples,
Sample Location
Temp.
°C
pH
S.U.
Specific Conductivity
ms/cm
Dissolved Oxygen
mg/l
HRSW-2 upstream
10.1
7.1
0.221
16.97
HRSW4 mid -stream
9.6
7.3
0.224
16.53
HRSW-3 downstream
9.3
7.2
0.239
16.31
Groundwater samples:
Vanadium and cobalt were detected in various wells above the 21 standard. The
following table summarizes metals detection for groundwater samples.
WeIIID
As
ug/l
Ba
ug/l
Be
ug/1
Cd
ug/1
Cr
ug/l
Co
ug/l
Cu
ug/1
Pb
ug/1
Ni
ug/1
Se
ug/1
Vn
ug/1
Zn
ug/1
HRW-7
-----
132
-----
1.4
-----
-----
-----
-----
-----
-----
-----
-----
HRW-8
-----
77.6
-----
-----
6.7
-----
11.1
7.5
-----
-----
20.8
-----
HRW-9R
-----
354
-----
-----
8.7
15.0
48.8
-----
7.9
-----
33.4
16.6
HRW40
-----
102
-----
-----
-----
-----
-----
-----
6.9
-----
-----
-----
HRW-11R
-----
299
-----
-----
5A
15.1
6.3
-----
35.9
-----
-----
-----
HRW4 3
------
159
-----
-----
15.8
-----
23.8
10.3
11.0
-----
25.0
24.6
HRW46
-----
115
-----
-----
-----
-----
9.8
5.4
-----
-----
13.0
-----
HRW-18
-----
329
-----
-----
-----
-----
-----
-----
8.4
-----
-----
-----
HRW49-----
82.1
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-20
-----
112
-----
-----
-----
-----
-----
5.0
-----
-----
-----
-----
HRW-21
-----
65.2
-----
-----
-----
-----
-----
5.4
-----
-----
-----
-----
2L Std.
10
700
4
2
10
1
1,000
15
100
20
0.3
1,000
Note: Results shown in bold exceed the 2L standard.

Page 3
VOCs were detected in six monitoring wells; HRW-7, HRW-9R, HRW40, HRW41R,
HRW48 and HRW-20. The following table summarizes VOC detections.
Well ID
Volatile Constituent
Concentration
2L Standard
u /1
u /1
cis- 1,2-Dichloroethene
2.4
70
HRW-7
Trichloroethene
1.8
3
HRW-9R
Chlorobenzene
1.6
50
Chloroethane
1.3
3000
1,2-Dichlorobenzene
2.6
20
1,4-Dichlorobenzene
3.3
6
1,1-Dichloroethane
26.7
6
1,2-Dichloroethane
2.1
094
cis- 1,2-Dichloroethane
59.1
70
1,2-Dichloropropane
2.1
096
Trichloroethene
1.4
3
Vinyl Chloride
695
0.03
1,4-Dioxane
13.4
3
HRW-10
1,4-Dioxane
4.5
3
HRW41R
Chlorobenzene
6.7
50
1,4-Dichlorobenzene
1.4
6
1,4-Dioxane
122
3
Benzene
1.7
1
HRW48
Chlorobenzene
6.0
50
Chloroethane
L5
3000
1,1-Dichloroethane
26.7
6
cis-1,2-Dichloroethane
1.8
70
1,2-Dichloropropane
491
0.6
1,4-Dichlorobenzene
6.6
6
Vinyl Chloride
1194
0.03
1,4-Dioxane
9.3
3
HRW-20
1,1-Dichloroethane
5.6
6
Note: Results shown in bold exceed the 2L standard.
Measurements of pH were more acidic than the 2L standard range of 6.5 to 8.5 standard
units at HRW-7, HRW-8, HRW-9R, HRW-11R, HRW-13 and HRW-16. Field -
measured parameters for groundwater samples are summarized in the following table.

Sample Location
Temp. °C
PH
Specific Conductivity ms/cm
HRW-7
17.5
6.2
0.624
HRW-8
11.0
6.3
0.059
HRW-9R
15.1
6.3
1.108
HRW-10
12.1
6.7
0.507
HRW-11R
13.6
6.4
1.895
HRW43
11.8
5.9
0.327
HRW46
11.0
5.6
0.087
HRW4 8
15.9
6.7
L 184
HRW49
13.2
6.8
0.327
HRW-20
15.0
6.5
0.357
HRW-21
15.0
7.0
0.485
Note: Results shown in bold are outside of the 2L standard range of 6.5 - 8.5 S.U.
Please call me at [phone] if you have any questions regarding this report.
Project Manager
Solid Waste Services

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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 18, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on March 09, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92526479001 HRW7
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92526479002 HRW19
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92526479003 HRW20
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92526479004 HRW21
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92526479005 HRW18
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92526479006 Trip Blank
EPA 8260D
CL
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW7 Lab ID: 92526479001 Collected: 03/09/21 11:35 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:37
7440-38-2
Barium
132
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:37
7440-41-7
Cadmium
1.4
ug/L
1.0
1
03/16/21 18:33
03/17/2123:37
7440-43-9
Chromium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7440-48-4
Copper
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7440-50-8
Lead
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7439-92-1
Nickel
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:37
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:37
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:37
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:37
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/2109:42
03/17/2122:13
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 10:37
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 10:37
107-13-1
Benzene
ND
ug/L
1.0
1
03/11/21 10:37
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 10:37
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 10:37
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 10:37
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 10:37
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 10:37
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 10:37
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 10:37
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/11/21 10:37
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/11/21 10:37
75-00-3
Chloroform
ND
ug/L
5.0
1
03/11/21 10:37
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 10:37
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 10:37
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 10:37
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 10:37
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 10:37
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 10:37
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 10:37
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 10:37
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/11/21 10:37
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 10:37
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW7 Lab ID: 92526479001 Collected: 03/09/21 11:35 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:37
75-35-4
cis-1,2-Dichloroethene
2.4
ug/L
1.0
1
03/11/21 10:37
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:37
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:37
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:37
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:37
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/11/21 10:37
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/11/21 10:37
591-78-6
lodomethane
ND
ug/L
20.0
1
03/11/21 10:37
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/11/21 10:37
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/11/21 10:37
108-10-1
Styrene
ND
ug/L
1.0
1
03/11/21 10:37
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 10:37
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 10:37
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/11/21 10:37
127-18-4
Toluene
ND
ug/L
1.0
1
03/11/21 10:37
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/11/21 10:37
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/11/21 10:37
79-00-5
Trichloroethene
1.8
ug/L
1.0
1
03/11/21 10:37
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/11/21 10:37
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/11/21 10:37
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/11/21 10:37
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/11/21 10:37
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/11/21 10:37
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/11/21 10:37
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/11/21 10:37
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
03/11/21 10:37
460-00-4
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
03/11/21 10:37
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
03/11/21 10:37
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/09/21 17:59
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
82
%
70-130
1
03/09/21 17:59
17060-07-0
Toluene-d8(S)
90
%
66-133
1
03/09/21 17:59
2037-26-5
Date: 03/18/2021 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW19 Lab ID: 92526479002 Collected: 03/09/21 10:30 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:40
7440-38-2
Barium
82.1
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:40
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:40
7440-43-9
Chromium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7440-48-4
Copper
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7440-50-8
Lead
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7439-92-1
Nickel
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:40
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:40
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:40
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:40
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/2109:42
03/17/2122:37
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 10:55
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 10:55
107-13-1
Benzene
ND
ug/L
1.0
1
03/11/21 10:55
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 10:55
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 10:55
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 10:55
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 10:55
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 10:55
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 10:55
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 10:55
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/11/21 10:55
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/11/21 10:55
75-00-3
Chloroform
ND
ug/L
5.0
1
03/11/21 10:55
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 10:55
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 10:55
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 10:55
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 10:55
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 10:55
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 10:55
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 10:55
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 10:55
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/11/21 10:55
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 10:55
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW19 Lab ID: 92526479002 Collected: 03/09/21 10:30 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:55
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:55
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:55
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:55
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:55
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:55
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/11/21 10:55
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/11/21 10:55
591-78-6
lodomethane
ND
ug/L
20.0
1
03/11/21 10:55
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/11/21 10:55
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/11/21 10:55
108-10-1
Styrene
ND
ug/L
1.0
1
03/11/21 10:55
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 10:55
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 10:55
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/11/21 10:55
127-18-4
Toluene
ND
ug/L
1.0
1
03/11/21 10:55
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/11/21 10:55
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/11/21 10:55
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/11/21 10:55
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/11/21 10:55
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/11/21 10:55
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/11/21 10:55
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/11/21 10:55
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/11/21 10:55
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/11/21 10:55
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/11/21 10:55
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
03/11/21 10:55
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
03/11/21 10:55
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
03/11/21 10:55
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/09/21 18:18
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
83
%
70-130
1
03/09/21 18:18
17060-07-0
Toluene-d8 (S)
91
%
66-133
1
03/09/21 18:18
2037-26-5
Date: 03/18/2021 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW20 Lab ID: 92526479003 Collected: 03/09/21 10:50 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:43
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:43
7440-38-2
Barium
112
ug/L
5.0
1
03/16/2118:33
03/17/2123:43
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:43
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:43
7440-43-9
Chromium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:43
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:43
7440-48-4
Copper
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:43
7440-50-8
Lead
5.0
ug/L
5.0
1
03/16/21 18:33
03/17/2123:43
7439-92-1
Nickel
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:43
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:43
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:43
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:43
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:43
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:43
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/2109:42
03/17/2122:40
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 11:13
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 11:13
107-13-1
Benzene
ND
ug/L
1.0
1
03/11/21 11:13
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 11:13
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 11:13
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 11:13
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 11:13
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 11:13
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 11:13
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 11:13
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/11/21 11:13
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/11/21 11:13
75-00-3
Chloroform
ND
ug/L
5.0
1
03/11/21 11:13
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 11:13
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 11:13
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 11:13
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 11:13
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 11:13
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 11:13
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 11:13
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 11:13
110-57-6
1,1-Dichloroethane
5.6
ug/L
1.0
1
03/11/21 11:13
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 11:13
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW20 Lab ID: 92526479003 Collected: 03/09/21 10:50 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/11/21 11:13
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 11:13
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 11:13
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/11/21 11:13
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 11:13
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 11:13
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/11/21 11:13
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/11/21 11:13
591-78-6
lodomethane
ND
ug/L
20.0
1
03/11/21 11:13
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/11/21 11:13
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/11/21 11:13
108-10-1
Styrene
ND
ug/L
1.0
1
03/11/21 11:13
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 11:13
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 11:13
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/11/21 11:13
127-18-4
Toluene
ND
ug/L
1.0
1
03/11/21 11:13
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/11/21 11:13
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/11/21 11:13
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/11/21 11:13
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/11/21 11:13
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/11/21 11:13
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/11/21 11:13
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/11/21 11:13
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/11/21 11:13
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/11/21 11:13
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/11/21 11:13
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
03/11/21 11:13
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
03/11/21 11:13
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
03/11/21 11:13
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/09/21 18:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
80
%
70-130
1
03/09/21 18:37
17060-07-0
Toluene-d8 (S)
89
%
66-133
1
03/09/21 18:37
2037-26-5
Date: 03/18/2021 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW21 Lab ID: 92526479004 Collected: 03/09/21 10:00 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:47
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:47
7440-38-2
Barium
65.2
ug/L
5.0
1
03/16/2118:33
03/17/2123:47
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:47
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:47
7440-43-9
Chromium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:47
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:47
7440-48-4
Copper
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:47
7440-50-8
Lead
5.4
ug/L
5.0
1
03/16/21 18:33
03/17/2123:47
7439-92-1
Nickel
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:47
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:47
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:47
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:47
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:47
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:47
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/2109:42
03/17/2122:43
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 11:31
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 11:31
107-13-1
Benzene
ND
ug/L
1.0
1
03/11/21 11:31
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 11:31
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 11:31
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 11:31
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 11:31
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 11:31
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 11:31
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 11:31
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/11/21 11:31
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/11/21 11:31
75-00-3
Chloroform
ND
ug/L
5.0
1
03/11/21 11:31
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 11:31
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 11:31
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 11:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 11:31
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 11:31
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 11:31
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 11:31
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 11:31
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/11/21 11:31
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 11:31
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW21 Lab ID: 92526479004 Collected: 03/09/21 10:00 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 03/18/2021 04:38 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98
%
102
%
99
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
80 %
90 %
1.0
1
03/11/21 11:31
75-35-4
1.0
1
03/11/21 11:31
156-59-2
1.0
1
03/11/21 11:31
156-60-5
1.0
1
03/11/21 11:31
78-87-5
1.0
1
03/11/21 11:31
10061-01-5
1.0
1
03/11/21 11:31
10061-02-6
1.0
1
03/11/21 11:31
100-41-4
5.0
1
03/11/21 11:31
591-78-6
20.0
1
03/11/21 11:31
74-88-4
5.0
1
03/11/21 11:31
75-09-2
5.0
1
03/11/21 11:31
108-10-1
1.0
1
03/11/21 11:31
100-42-5
1.0
1
03/11/21 11:31
630-20-6
1.0
1
03/11/21 11:31
79-34-5
1.0
1
03/11/21 11:31
127-18-4
1.0
1
03/11/21 11:31
108-88-3
1.0
1
03/11/21 11:31
71-55-6
1.0
1
03/11/21 11:31
79-00-5
1.0
1
03/11/21 11:31
79-01-6
1.0
1
03/11/21 11:31
75-69-4
1.0
1
03/11/21 11:31
96-18-4
2.0
1
03/11/21 11:31
108-05-4
1.0
1
03/11/21 11:31
75-01-4
1.0
1
03/11/21 11:31
1330-20-7
2.0
1
03/11/21 11:31
179601-23-1
1.0
1
03/11/21 11:31
95-47-6
70-130 1
70-130 1
70-130 1
70-130 1
66-133 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
03/11/21 11:31 460-00-4
03/11/21 11:31 17060-07-0
03/11/21 11:31 2037-26-5
03/09/21 18:56 17060-07-0
03/09/21 18:56 2037-26-5
Page 11 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW18 Lab ID: 92526479005 Collected: 03/09/21 11:15 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:50
7440-38-2
Barium
329
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:50
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:50
7440-43-9
Chromium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7440-48-4
Copper
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7440-50-8
Lead
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7439-92-1
Nickel
8.4
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:50
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:50
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:50
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:50
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/2109:42
03/17/2122:47
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 11:49
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 11:49
107-13-1
Benzene
1.7
ug/L
1.0
1
03/11/21 11:49
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 11:49
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 11:49
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 11:49
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 11:49
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 11:49
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 11:49
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 11:49
56-23-5
Chlorobenzene
6.0
ug/L
1.0
1
03/11/21 11:49
108-90-7
Chloroethane
1.5
ug/L
1.0
1
03/11/21 11:49
75-00-3
Chloroform
ND
ug/L
5.0
1
03/11/21 11:49
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 11:49
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 11:49
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 11:49
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 11:49
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 11:49
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 11:49
95-50-1
1,4-Dichlorobenzene
6.6
ug/L
1.0
1
03/11/21 11:49
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 11:49
110-57-6
1,1-Dichloroethane
26.7
ug/L
1.0
1
03/11/21 11:49
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 11:49
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: HRW18 Lab ID: 92526479005 Collected: 03/09/21 11:15 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 03/18/2021 04:38 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
1.8
ug/L
ND
ug/L
4.1
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
11.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100
%
103
%
100
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
9.3 ug/L
83 %
89 %
1.0
1
03/11/21 11:49
75-35-4
1.0
1
03/11/21 11:49
156-59-2
1.0
1
03/11/21 11:49
156-60-5
1.0
1
03/11/21 11:49
78-87-5
1.0
1
03/11/21 11:49
10061-01-5
1.0
1
03/11/21 11:49
10061-02-6
1.0
1
03/11/21 11:49
100-41-4
5.0
1
03/11/21 11:49
591-78-6
20.0
1
03/11/21 11:49
74-88-4
5.0
1
03/11/21 11:49
75-09-2
5.0
1
03/11/21 11:49
108-10-1
1.0
1
03/11/21 11:49
100-42-5
1.0
1
03/11/21 11:49
630-20-6
1.0
1
03/11/21 11:49
79-34-5
1.0
1
03/11/21 11:49
127-18-4
1.0
1
03/11/21 11:49
108-88-3
1.0
1
03/11/21 11:49
71-55-6
1.0
1
03/11/21 11:49
79-00-5
1.0
1
03/11/21 11:49
79-01-6
1.0
1
03/11/21 11:49
75-69-4
1.0
1
03/11/21 11:49
96-18-4
2.0
1
03/11/21 11:49
108-05-4
1.0
1
03/11/21 11:49
75-01-4
1.0
1
03/11/21 11:49
1330-20-7
2.0
1
03/11/21 11:49
179601-23-1
1.0
1
03/11/21 11:49
95-47-6
70-130 1
70-130 1
70-130 1
70-130 1
66-133 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
03/11/21 11:49 460-00-4
03/11/21 11:49 17060-07-0
03/11/21 11:49 2037-26-5
11191LIRypi1 `Pi ELL' = PaS4 N
03/09/21 19:34 17060-07-0
03/09/21 19:34 2037-26-5
Page 13 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: Trip Blank Lab ID: 92526479006 Collected: 03/09/21 08:50 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 09:06
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 09:06
107-13-1
Benzene
ND
ug/L
1.0
1
03/11/21 09:06
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 09:06
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 09:06
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 09:06
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 09:06
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 09:06
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 09:06
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 09:06
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/11/21 09:06
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/11/21 09:06
75-00-3 v2
Chloroform
ND
ug/L
5.0
1
03/11/21 09:06
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 09:06
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 09:06
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 09:06
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 09:06
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 09:06
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 09:06
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 09:06
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 09:06
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/11/21 09:06
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 09:06
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/11/21 09:06
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 09:06
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 09:06
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/11/21 09:06
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 09:06
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 09:06
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/11/21 09:06
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/11/21 09:06
591-78-6
lodomethane
ND
ug/L
20.0
1
03/11/21 09:06
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/11/21 09:06
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/11/21 09:06
108-10-1
Styrene
ND
ug/L
1.0
1
03/11/21 09:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 09:06
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 09:06
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/11/21 09:06
127-18-4
Toluene
ND
ug/L
1.0
1
03/11/21 09:06
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/11/21 09:06
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/11/21 09:06
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/11/21 09:06
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/11/21 09:06
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/11/21 09:06
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/11/21 09:06
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/11/21 09:06
75-01-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM
without
the written consent of Pace Analytical Services, LLC.
Page 14 of 28

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
Sample: Trip Blank
Parameters
Lab ID: 92526479006 Collected: 03/09/21 08:50
Results Units Report Limit DF
Received: 03/09/21 14:18 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
03/11/21 09:06
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
03/11/21 09:06
179601-23-1
o-Xylene
ND ug/L
1.0
1
03/11/21 09:06
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
03/11/21 09:06
460-00-4
1,2-Dichloroethane-d4 (S)
104 %
70-130
1
03/11/21 09:06
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
03/11/21 09:06
2037-26-5
Date: 03/18/2021 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 28

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
QC Batch: 606946 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92526479001, 92526479002, 92526479003, 92526479004, 92526479005
METHOD BLANK: 3197719 Matrix: Water
Associated Lab Samples: 92526479001, 92526479002, 92526479003, 92526479004, 92526479005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
03/17/2122:32
Arsenic
ug/L
ND
10.0
03/17/2122:32
Barium
ug/L
ND
5.0
03/17/2122:32
Beryllium
ug/L
ND
1.0
03/17/2122:32
Cadmium
ug/L
ND
1.0
03/17/2122:32
Chromium
ug/L
ND
5.0
03/17/2122:32
Cobalt
ug/L
ND
5.0
03/17/2122:32
Copper
ug/L
ND
5.0
03/17/2122:32
Lead
ug/L
ND
5.0
03/17/2122:32
Nickel
ug/L
ND
5.0
03/17/2122:32
Selenium
ug/L
ND
10.0
03/17/2122:32
Silver
ug/L
ND
5.0
03/17/2122:32
Thallium
ug/L
ND
10.0
03/17/2122:32
Vanadium
ug/L
ND
5.0
03/17/2122:32
Zinc
ug/L
ND
10.0
03/17/2122:32
LABORATORY CONTROL SAMPLE:
Parameter
3197720
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
504
101
80-120
Arsenic
ug/L
500
491
98
80-120
Barium
ug/L
500
498
100
80-120
Beryllium
ug/L
500
498
100
80-120
Cadmium
ug/L
500
495
99
80-120
Chromium
ug/L
500
489
98
80-120
Cobalt
ug/L
500
479
96
80-120
Copper
ug/L
500
512
102
80-120
Lead
ug/L
500
487
97
80-120
Nickel
ug/L
500
492
98
80-120
Selenium
ug/L
500
490
98
80-120
Silver
ug/L
250
252
101
80-120
Thallium
ug/L
500
486
97
80-120
Vanadium
ug/L
500
480
96
80-120
Zinc
ug/L
500
478
96
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92526479
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3197721
3197722
MS
MSD
92526090001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
499
502
99
100
75-125
1
Arsenic
ug/L
ND
500
500
493
506
99
101
75-125
3
Barium
ug/L
17.5
500
500
505
508
98
98
75-125
1
Beryllium
ug/L
ND
500
500
492
494
98
99
75-125
0
Cadmium
ug/L
1.6
500
500
500
506
100
101
75-125
1
Chromium
ug/L
ND
500
500
485
489
97
98
75-125
1
Cobalt
ug/L
ND
500
500
472
477
94
95
75-125
1
Copper
ug/L
21.6
500
500
524
531
101
102
75-125
1
Lead
ug/L
ND
500
500
478
480
95
96
75-125
0
Nickel
ug/L
7.5
500
500
490
495
96
97
75-125
1
Selenium
ug/L
ND
500
500
519
524
104
105
75-125
1
Silver
ug/L
ND
250
250
247
249
98
99
75-125
1
Thallium
ug/L
ND
500
500
473
484
94
96
75-125
2
Vanadium
ug/L
ND
500
500
477
484
95
97
75-125
1
Zinc
ug/L
358
500
500
826
832
94
95
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
QC Batch: 607128 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92526479001, 92526479002, 92526479003, 92526479004, 92526479005
METHOD BLANK: 3198549 Matrix: Water
Associated Lab Samples: 92526479001, 92526479002, 92526479003, 92526479004, 92526479005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Thallium ug/L ND 1.0 03/17/2121:56
LABORATORY CONTROL SAMPLE:
3198550
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Thallium
ug/L
10
10.3
103
80-120
LABORATORY CONTROL SAMPLE:
3198551
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Thallium
ug/L
10
10.5
105
80-120
LABORATORY CONTROL SAMPLE: 3198552
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.3 103 80-120
LABORATORY CONTROL SAMPLE: 3198553
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.6 106 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3198554 3198555
MS MSD
92526479001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.9 10.6 109 106 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
QC Batch: 605602 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526479001, 92526479002, 92526479003, 92526479004, 92526479005, 92526479006
METHOD BLANK: 3190534 Matrix: Water
Associated Lab Samples: 92526479001, 92526479002, 92526479003, 92526479004, 92526479005, 92526479006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1,1-Trichloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1,2-Trichloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1-Dichloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1-Dichloroethene
ug/L
ND
1.0
03/11/21 02:09
1,2,3-Trichloropropane
ug/L
ND
1.0
03/11/21 02:09
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
03/11/21 02:09
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/11/21 02:09
1,2-Dichlorobenzene
ug/L
ND
1.0
03/11/21 02:09
1,2-Dichloroethane
ug/L
ND
1.0
03/11/21 02:09
1,2-Dichloropropane
ug/L
ND
1.0
03/11/21 02:09
1,4-Dichlorobenzene
ug/L
ND
1.0
03/11/21 02:09
2-Butanone (MEK)
ug/L
ND
5.0
03/11/21 02:09
2-Hexanone
ug/L
ND
5.0
03/11/21 02:09
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/11/21 02:09
Acetone
ug/L
ND
25.0
03/11/21 02:09
Acrylonitrile
ug/L
ND
10.0
03/11/21 02:09
Benzene
ug/L
ND
1.0
03/11/21 02:09
Bromochloromethane
ug/L
ND
1.0
03/11/21 02:09
Bromodichloromethane
ug/L
ND
1.0
03/11/21 02:09
Bromoform
ug/L
ND
1.0
03/11/21 02:09
Bromomethane
ug/L
ND
2.0
03/11/21 02:09
Carbon disulfide
ug/L
ND
2.0
03/11/21 02:09
Carbon tetrachloride
ug/L
ND
1.0
03/11/21 02:09
Chlorobenzene
ug/L
ND
1.0
03/11/21 02:09
Chloroethane
ug/L
ND
1.0
03/11/21 02:09
Chloroform
ug/L
ND
5.0
03/11/21 02:09
Chloromethane
ug/L
ND
1.0
03/11/21 02:09
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/11/21 02:09
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/11/21 02:09
Dibromochloromethane
ug/L
ND
1.0
03/11/21 02:09
Dibromomethane
ug/L
ND
1.0
03/11/21 02:09
Ethylbenzene
ug/L
ND
1.0
03/11/21 02:09
lodomethane
ug/L
ND
20.0
03/11/21 02:09
m&p-Xylene
ug/L
ND
2.0
03/11/21 02:09
Methylene Chloride
ug/L
ND
5.0
03/11/21 02:09
o-Xylene
ug/L
ND
1.0
03/11/21 02:09
Styrene
ug/L
ND
1.0
03/11/21 02:09
Tetrachloroethene
ug/L
ND
1.0
03/11/21 02:09
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
METHOD BLANK: 3190534 Matrix: Water
Associated Lab Samples: 92526479001, 92526479002, 92526479003, 92526479004, 92526479005, 92526479006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
03/11/21 02:09
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/11/21 02:09
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/11/21 02:09
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/11/21 02:09
Trichloroethene
ug/L
ND
1.0
03/11/21 02:09
Trichlorofluoromethane
ug/L
ND
1.0
03/11/21 02:09
Vinyl acetate
ug/L
ND
2.0
03/11/21 02:09
Vinyl chloride
ug/L
ND
1.0
03/11/21 02:09
Xylene (Total)
ug/L
ND
1.0
03/11/21 02:09
1,2-Dichloroethane-d4 (S)
%
101
70-130
03/11/21 02:09
4-Bromofluorobenzene (S)
%
98
70-130
03/11/21 02:09
Toluene-d8 (S)
%
98
70-130
03/11/21 02:09
LABORATORY CONTROL SAMPLE:
Parameter
3190535
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.8
100
70-130
1,1,1-Trichloroethane
ug/L
50
48.8
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.5
99
70-130
1,1-Dichloroethane
ug/L
50
49.6
99
70-130
1,1-Dichloroethene
ug/L
50
48.8
98
70-132
1,2,3-Trichloropropane
ug/L
50
49.3
99
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.3
101
70-132
1,2-Dibromoethane (EDB)
ug/L
50
48.9
98
70-130
1,2-Dichlorobenzene
ug/L
50
50.8
102
70-130
1,2-Dichloroethane
ug/L
50
49.6
99
70-130
1,2-Dichloropropane
ug/L
50
49.4
99
70-130
1,4-Dichlorobenzene
ug/L
50
49.0
98
70-130
2-Butanone (MEK)
ug/L
100
98.1
98
70-133
2-Hexanone
ug/L
100
101
101
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
102
102
70-144
Acrylonitrile
ug/L
250
246
98
70-130
Benzene
ug/L
50
47.0
94
70-130
Bromochloromethane
ug/L
50
51.9
104
70-130
Bromodichloromethane
ug/L
50
48.9
98
70-130
Bromoform
ug/L
50
50.0
100
70-131
Bromomethane
ug/L
50
50.5
101
30-177
Carbon disulfide
ug/L
50
49.9
100
70-133
Carbon tetrachloride
ug/L
50
49.0
98
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
40.8
82
46-131 v2
Chloroform
ug/L
50
50.0
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
LABORATORY CONTROL SAMPLE:
3190535
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Chloromethane
ug/L
50
43.9
88
49-130
cis-1,2-Dichloroethene
ug/L
50
47.8
96
70-130
cis-1,3-Dichloropropene
ug/L
50
50.6
101
70-130
Dibromochloromethane
ug/L
50
51.1
102
70-130
Dibromomethane
ug/L
50
50.5
101
70-130
Ethylbenzene
ug/L
50
47.9
96
70-130
lodomethane
ug/L
100
121
121
47-140
m&p-Xylene
ug/L
100
95.7
96
70-130
Methylene Chloride
ug/L
50
51.2
102
68-130
o-Xylene
ug/L
50
48.4
97
70-130
Styrene
ug/L
50
49.5
99
70-130
Tetrachloroethene
ug/L
50
46.0
92
70-130
Toluene
ug/L
50
48.2
96
70-130
trans-1,2-Dichloroethene
ug/L
50
50.2
100
70-130
trans- 1,3-Dichloropropene
ug/L
50
50.5
101
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
59.4
119
25-200
Trichloroethene
ug/L
50
47.9
96
70-130
Trichlorofluoromethane
ug/L
50
47.5
95
61-130
Vinyl acetate
ug/L
100
112
112
70-140
Vinyl chloride
ug/L
50
47.2
94
59-142
Xylene (Total)
ug/L
150
144
96
70-130
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3190536
3190537
MS
MSD
92525449005
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
100
100
104
116
104
116
70-135
11
1,1,1-Trichloroethane
ug/L
528
100
100
643
635
115
107
70-148
1
1,1,2,2-Tetrachloroethane
ug/L
ND
100
100
97.3
115
97
115
70-131
17
1,1,2-Trichloroethane
ug/L
2.7J
100
100
103
118
100
115
70-136
14
1,1-Dichloroethane
ug/L
413
100
100
520
525
107
113
70-147
1
1,1-Dichloroethene
ug/L
52.6
100
100
165
176
112
124
70-158
7
1,2,3-Trichloropropane
ug/L
ND
100
100
100
110
100
110
67-137
10
1,2-Dibromo-3-chloropropane
ug/L
ND
100
100
98.5
112
98
112
69-136
13
1,2-Dibromoethane (EDB)
ug/L
ND
100
100
99.5
112
100
112
70-137
12
1,2-Dichlorobenzene
ug/L
ND
100
100
104
119
104
119
70-133
13
1,2-Dichloroethane
ug/L
ND
100
100
104
114
104
114
67-138
9
1,2-Dichloropropane
ug/L
ND
100
100
105
116
105
116
70-138
10
1,4-Dichlorobenzene
ug/L
ND
100
100
103
115
103
115
70-133
11
2-Butanone (MEK)
ug/L
ND
200
200
194
225
97
112
61-147
15
2-Hexanone
ug/L
ND
200
200
198
232
99
116
67-139
16
4-Methyl-2-pentanone (MIBK)
ug/L
ND
200
200
201
232
99
114
67-136
15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3190536
3190537
MS
MSD
92525449005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
200
200
208
242
104
121
55-159
15
Acrylonitrile
ug/L
ND
500
500
506
572
101
114
68-140
12
Benzene
ug/L
6.4
100
100
108
121
101
115
67-150
12
Bromochloromethane
ug/L
ND
100
100
107
121
107
121
70-146
12
Bromodichloromethane
ug/L
ND
100
100
99.5
111
99
111
70-138
11
Bromoform
ug/L
ND
100
100
90.4
103
90
103
57-138
13
Bromomethane
ug/L
ND
100
100
159
151
159
151
10-200
5
Carbon disulfide
ug/L
ND
100
100
102
114
102
114
70-152
11
Carbon tetrachloride
ug/L
ND
100
100
109
123
109
123
70-147
12
Chlorobenzene
ug/L
ND
100
100
102
115
102
115
70-137
12
Chloroethane
ug/L
ND
100
100
103
120
103
120
51-166
15
Chloroform
ug/L
7.8J
100
100
115
124
107
117
70-144
8
Chloromethane
ug/L
ND
100
100
97.4
106
97
106
24-161
8
cis-1,2-Dichloroethene
ug/L
666
100
100
770
768
104
102
67-148
0
cis-1,3-Dichloropropene
ug/L
ND
100
100
102
115
102
115
70-142
13
Dibromochloromethane
ug/L
ND
100
100
98.4
112
98
112
68-138
13
Dibromomethane
ug/L
ND
100
100
103
115
103
115
70-134
11
Ethylbenzene
ug/L
11.1
100
100
114
126
103
115
68-143
10
lodomethane
ug/L
ND
200
200
121
179
61
89
20-161
38 R1
m&p-Xylene
ug/L
12.3
200
200
218
242
103
115
53-157
11
Methylene Chloride
ug/L
ND
100
100
113
124
106
117
64-148
9
o-Xylene
ug/L
23.3
100
100
126
136
103
113
68-143
8
Styrene
ug/L
ND
100
100
104
117
104
117
70-136
12
Tetrachloroethene
ug/L
23.6
100
100
124
135
101
111
70-139
8
Toluene
ug/L
19.6
100
100
121
134
102
115
47-157
10
trans-1,2-Dichloroethene
ug/L
ND
100
100
110
122
110
122
70-149
11
trans- 1,3-Dichloropropene
ug/L
ND
100
100
99.5
113
99
113
70-138
13
trans-1,4-Dichloro-2-butene
ug/L
ND
100
100
105
122
105
122
31-145
15
Trichloroethene
ug/L
633
100
100
754
744
120
110
70-149
1
Trichlorofluoromethane
ug/L
ND
100
100
112
125
112
125
61-154
11
Vinyl acetate
ug/L
ND
200
200
222
252
111
126
48-156
13
Vinyl chloride
ug/L
ND
100
100
99.7
114
100
114
55-172
14
Xylene (Total)
ug/L
35.5
300
300
344
379
103
114
66-145
10
1,2-Dichloroethane-d4 (S)
%
102
102
70-130
4-Bromofluorobenzene (S)
%
101
101
70-130
Toluene-d8(S)
%
100
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
QC Batch: 605277 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526479001, 92526479002, 92526479003, 92526479004, 92526479005
METHOD BLANK: 3188671
Matrix:
Water
Associated Lab Samples:
92526479001, 92526479002, 92526479003, 92526479004, 92526479005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
03/09/21 13:34
1,2-Dichloroethane-d4 (S)
%
81
70-130
03/09/21 13:34
Toluene-d8 (S)
%
91
66-133
03/09/21 13:34
LABORATORY CONTROL SAMPLE: 3188672
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 21.6 108 70-130
1,2-Dichloroethane-d4 (S) % 83 70-130
Toluene-d8 (S) % 90 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3188673
3188674
MS
MSD
92526059009 Spike
Spike MS MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 117 40
40 153 161 92
111
64-141 5
1,2-Dichloroethane-d4 (S)
%
83
82
70-130
Toluene-d8(S)
%
91
90
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526479
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
R1 RPD value was outside control limits.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:38 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92526479
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92526479001
HRW7
EPA 3010A
606946
EPA6010D
607036
92526479002
HRW19
EPA 3010A
606946
EPA6010D
607036
92526479003
HRW20
EPA 3010A
606946
EPA6010D
607036
92526479004
HRW21
EPA 3010A
606946
EPA6010D
607036
92526479005
HRW18
EPA 3010A
606946
EPA6010D
607036
92526479001
HRW7
EPA 3010A
607128
EPA 6020B
607180
92526479002
HRW19
EPA 3010A
607128
EPA 6020B
607180
92526479003
HRW20
EPA 3010A
607128
EPA 6020B
607180
92526479004
HRW21
EPA 3010A
607128
EPA 6020B
607180
92526479005
HRW18
EPA 3010A
607128
EPA 6020B
607180
92526479001
HRW7
EPA 8260D
605602
92526479002
HRW19
EPA 8260D
605602
92526479003
HRW20
EPA 8260D
605602
92526479004
HRW21
EPA 8260D
605602
92526479005
HRW18
EPA 8260D
605602
92526479006
Trip Blank
EPA 8260D
605602
92526479001
HRW7
EPA 8260D Mod.
605277
92526479002
HRW19
EPA 8260D Mod.
605277
92526479003
HRW20
EPA 8260D Mod.
605277
92526479004
HRW21
EPA 8260D Mod.
605277
92526479005
HRW18
EPA 8260D Mod.
605277
Date: 03/18/2021 04:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 28

Sample Condition Upon Receipttxunl -re. 1u
aceAnalytrcal Document No.'. Issuing Authority:
F-CAR-CS-D33-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville 5 Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Sample Condition Client Name: WO# • 92526479
Upon Receipt --- ----....-—....... _- _ - — project 9
Courier; []Fed Ex ❑UPS uSPS Client II III II III I I III I� III
❑ Commercial ❑Pace []Other: 92526478
Custody Seal Present? ❑Yes ao Seals intact? []Yes RfNo
t)ateflnitlalsPerson Examining Contents; 3- Z1 SG
Packing Material: []Bubble Wrap []Bubble Bags ]None ❑ Other Biological Tissue frozen?
[:]Yes []No RN/A
Thermometer; 1 Inlet ❑Blue []None
IR Gun ID: 67 Type of Ice:
75— Correction Factor:
Cooler Temp: I Add/Subtract (°C) O.00C Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°Cl: cl has begun
USDA Regulated Soil (ON/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
i—iyac astir, including Hawaii and Puerto Rico)? ❑Yes []No
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (<72 hr.)?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COO
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5.6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
JoYes
❑No
❑N/A
S.
9YYes
❑No
[]N/A
6.
es
❑No
❑N/A
[Yes
❑Na _
[]N/A
7
❑Yes ❑No 10N/A 8.
)Yes []No ❑N/A 9.
❑Yes JgNo []N/A
10-
❑Yes
®No
❑N/A
11.
❑Yes
❑No
®NiA
Lot ID of sp}it containers:
CLIENT NOTIFICATION/RESOLUTION
Project Manager SCURF Review:
Date:
Field Data Required? ❑Yes [:]No
Project Manager SRF Review:
Date:
Page 26 of 28

Document Name: Document Revised: October 28, 2020
2
F sample Condition Upon Receipt(SCUR) Page 2 of 2
aceAnaWica! Document No.: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas quality Office
*Check mark top half of box if pH and/or clechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DR0/8015 (water) DOC, LLHg
*"Bottom half of box is to list number of bottles
Project # '
W4#:92526479
PM: MWB Due Dale: 03/23/21
CLIENT: 92—MECK CO
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot It
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 27 of 28

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noi 3 b Tsl
o n
n < o
v
c ° r
a
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Lo
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c
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T
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° n 2
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#
3 O
_
(
M
MATRIX CODE (see valid Codes to left)
m b
m 33 m
_
i
SAMPLE TYPE (G=GRA9 C=CO6M1P)
x
o n o
M1
N
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m
C7
41
=
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..
j
n
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• •
�-•
SAMPLE TEmp AT COLLECTION
N r^
A
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CONTAINERSA
v TJMmz�-,.
N
m
m
H2SO4
3
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HNO3
w
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NaOH
°
w
C
G7
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Na25203
n
�+G
�
Methanol
-r
m
a
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m
Analyses Pest
YliJ
a
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x Metals by 601016020
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x x x
x 5260
Q
m M
n
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1
a
m
CL (/1
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a
c 0
�+ 0
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N
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m
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'
v
TEMP
in
C
Residual Chlorine (YIN)
a c
� m
z o
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Received
on
>
n D
Ice
O
a
(YIN)
m
(�,
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Gy
��
�.3
n
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]
rN
?
(YIN)
Page 28 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 22, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on March 09, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92526471001 HRW10
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92526471002 HRW11R
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92526471003 HRW13
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Sample: HRW10 Lab ID: 92526471001 Collected: 03/09/21 13:35 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:27
7440-38-2
Barium
102
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:27
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/2118:33
03/17/2123:27
7440-43-9
Chromium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7440-48-4
Copper
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7440-50-8
Lead
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7439-92-1
Nickel
6.9
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:27
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:27
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/16/2118:33
03/17/2123:27
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/2118:33
03/17/2123:27
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/21 01:47
03/19/2107:09
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 09:42
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 09:42
107-13-1
Benzene
ND
ug/L
1.0
1
03/11/21 09:42
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 09:42
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 09:42
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 09:42
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 09:42
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 09:42
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 09:42
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 09:42
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/11/21 09:42
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/11/21 09:42
75-00-3
Chloroform
ND
ug/L
5.0
1
03/11/21 09:42
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 09:42
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 09:42
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 09:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 09:42
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 09:42
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 09:42
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 09:42
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 09:42
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/11/21 09:42
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 09:42
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Sample: HRW10 Lab ID: 92526471001 Collected: 03/09/21 13:35 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/11/21 09:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 09:42
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 09:42
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/11/21 09:42
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 09:42
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 09:42
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/11/21 09:42
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/11/21 09:42
591-78-6
lodomethane
ND
ug/L
20.0
1
03/11/21 09:42
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/11/21 09:42
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/11/21 09:42
108-10-1
Styrene
ND
ug/L
1.0
1
03/11/21 09:42
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 09:42
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 09:42
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/11/21 09:42
127-18-4
Toluene
ND
ug/L
1.0
1
03/11/21 09:42
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/11/21 09:42
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/11/21 09:42
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/11/21 09:42
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/11/21 09:42
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/11/21 09:42
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/11/21 09:42
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/11/21 09:42
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/11/21 09:42
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/11/21 09:42
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/11/21 09:42
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
03/11/21 09:42
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
03/11/21 09:42
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
03/11/21 09:42
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
4.5
ug/L
2.0
1
03/09/21 19:53
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
84
%
70-130
1
03/09/21 19:53
17060-07-0
Toluene-d8(S)
89
%
66-133
1
03/09/21 19:53
2037-26-5
Date: 03/22/2021 05:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Sample: HRW11R
Lab ID: 92526471002
Collected:
03/09/21
12:50
Received: 03/09/21 14:18 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
5.1
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:31
7440-38-2
Barium
299
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/21 18:33
03/17/2123:31
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/21 18:33
03/17/2123:31
7440-43-9
Chromium
5.4
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7440-47-3
Cobalt
15.1
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7440-48-4
Copper
6.3
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7440-50-8
Lead
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7439-92-1
Nickel
35.9
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:31
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:31
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:31
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:31
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND
ug/L
2.0
2
03/17/21 01:47
03/19/2107:13
7440-28-0 D3
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 10:01
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 10:01
107-13-1
Benzene
ND
ug/L
1.0
1
03/11/21 10:01
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 10:01
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 10:01
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 10:01
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 10:01
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 10:01
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 10:01
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 10:01
56-23-5
Chlorobenzene
6.7
ug/L
1.0
1
03/11/21 10:01
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/11/21 10:01
75-00-3 v2
Chloroform
ND
ug/L
5.0
1
03/11/21 10:01
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 10:01
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 10:01
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 10:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 10:01
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 10:01
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 10:01
95-50-1
1,4-Dichlorobenzene
1.4
ug/L
1.0
1
03/11/21 10:01
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 10:01
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/11/21 10:01
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 10:01
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 03/22/2021 05:55 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 6 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Sample: HRW11R Lab ID: 92526471002 Collected: 03/09/21 12:50 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:01
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:01
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:01
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:01
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/11/21 10:01
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/11/21 10:01
591-78-6
lodomethane
ND
ug/L
20.0
1
03/11/21 10:01
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/11/21 10:01
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/11/21 10:01
108-10-1
Styrene
ND
ug/L
1.0
1
03/11/21 10:01
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 10:01
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 10:01
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/11/21 10:01
127-18-4
Toluene
ND
ug/L
1.0
1
03/11/21 10:01
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/11/21 10:01
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/11/21 10:01
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/11/21 10:01
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/11/21 10:01
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/11/21 10:01
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/11/21 10:01
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/11/21 10:01
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/11/21 10:01
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/11/21 10:01
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/11/21 10:01
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
03/11/21 10:01
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
03/11/21 10:01
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
03/11/21 10:01
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
122
ug/L
5.0
2.5
03/09/21 20:12
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
83
%
70-130
2.5
03/09/21 20:12
17060-07-0
Toluene-d8 (S)
90
%
66-133
2.5
03/09/21 20:12
2037-26-5
Date: 03/22/2021 05:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Sample: HRW13 Lab ID: 92526471003 Collected: 03/09/21 13:10 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:34
7440-38-2
Barium
159
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/21 18:33
03/17/2123:34
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/21 18:33
03/17/2123:34
7440-43-9
Chromium
15.8
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7440-48-4
Copper
23.8
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7440-50-8
Lead
10.3
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7439-92-1
Nickel
11.0
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:34
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:34
7440-28-0
Vanadium
25.0
ug/L
5.0
1
03/16/21 18:33
03/17/2123:34
7440-62-2
Zinc
24.6
ug/L
10.0
1
03/16/21 18:33
03/17/2123:34
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/21 01:47
03/19/2107:16
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/11/21 10:19
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/11/21 10:19
107-13-1
Benzene
ND
ug/L
1.0
1
03/11/21 10:19
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/11/21 10:19
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/11/21 10:19
75-27-4
Bromoform
ND
ug/L
1.0
1
03/11/21 10:19
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/11/21 10:19
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/11/21 10:19
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/11/21 10:19
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/11/21 10:19
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/11/21 10:19
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/11/21 10:19
75-00-3
Chloroform
ND
ug/L
5.0
1
03/11/21 10:19
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/11/21 10:19
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/11/21 10:19
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/11/21 10:19
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/11/21 10:19
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/11/21 10:19
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 10:19
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/11/21 10:19
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/11/21 10:19
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/11/21 10:19
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/11/21 10:19
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
Sample: HRW13 Lab ID: 92526471003 Collected: 03/09/21 13:10 Received: 03/09/21 14:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/11/21 10:19
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:19
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:19
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/11/21 10:19
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/11/21 10:19
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/11/21 10:19
591-78-6
lodomethane
ND
ug/L
20.0
1
03/11/21 10:19
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/11/21 10:19
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/11/21 10:19
108-10-1
Styrene
ND
ug/L
1.0
1
03/11/21 10:19
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 10:19
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/11/21 10:19
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/11/21 10:19
127-18-4
Toluene
ND
ug/L
1.0
1
03/11/21 10:19
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/11/21 10:19
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/11/21 10:19
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/11/21 10:19
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/11/21 10:19
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/11/21 10:19
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/11/21 10:19
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/11/21 10:19
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/11/21 10:19
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/11/21 10:19
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/11/21 10:19
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
03/11/21 10:19
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
03/11/21 10:19
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
03/11/21 10:19
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/09/21 19:15
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
82
%
70-130
1
03/09/21 19:15
17060-07-0
Toluene-d8 (S)
89
%
66-133
1
03/09/21 19:15
2037-26-5
Date: 03/22/2021 05:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
QC Batch: 606946 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92526471001, 92526471002, 92526471003
METHOD BLANK: 3197719 Matrix: Water
Associated Lab Samples: 92526471001, 92526471002, 92526471003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
03/17/2122:32
10.0
03/17/2122:32
5.0
03/17/2122:32
1.0
03/17/2122:32
1.0
03/17/2122:32
5.0
03/17/2122:32
5.0
03/17/2122:32
5.0
03/17/2122:32
5.0
03/17/2122:32
5.0
03/17/2122:32
10.0
03/17/2122:32
5.0
03/17/2122:32
10.0
03/17/2122:32
5.0
03/17/2122:32
10.0
03/17/2122:32
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3197720
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
504
101
80-120
Arsenic
ug/L
500
491
98
80-120
Barium
ug/L
500
498
100
80-120
Beryllium
ug/L
500
498
100
80-120
Cadmium
ug/L
500
495
99
80-120
Chromium
ug/L
500
489
98
80-120
Cobalt
ug/L
500
479
96
80-120
Copper
ug/L
500
512
102
80-120
Lead
ug/L
500
487
97
80-120
Nickel
ug/L
500
492
98
80-120
Selenium
ug/L
500
490
98
80-120
Silver
ug/L
250
252
101
80-120
Thallium
ug/L
500
486
97
80-120
Vanadium
ug/L
500
480
96
80-120
Zinc
ug/L
500
478
96
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92526471
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3197721
3197722
MS
MSD
92526090001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
499
502
99
100
75-125
1
Arsenic
ug/L
ND
500
500
493
506
99
101
75-125
3
Barium
ug/L
17.5
500
500
505
508
98
98
75-125
1
Beryllium
ug/L
ND
500
500
492
494
98
99
75-125
0
Cadmium
ug/L
1.6
500
500
500
506
100
101
75-125
1
Chromium
ug/L
ND
500
500
485
489
97
98
75-125
1
Cobalt
ug/L
ND
500
500
472
477
94
95
75-125
1
Copper
ug/L
21.6
500
500
524
531
101
102
75-125
1
Lead
ug/L
ND
500
500
478
480
95
96
75-125
0
Nickel
ug/L
7.5
500
500
490
495
96
97
75-125
1
Selenium
ug/L
ND
500
500
519
524
104
105
75-125
1
Silver
ug/L
ND
250
250
247
249
98
99
75-125
1
Thallium
ug/L
ND
500
500
473
484
94
96
75-125
2
Vanadium
ug/L
ND
500
500
477
484
95
97
75-125
1
Zinc
ug/L
358
500
500
826
832
94
95
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
QC Batch: 607053 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92526471001, 92526471002, 92526471003
METHOD BLANK: 3198359
Matrix:
Water
Associated Lab Samples: 92526471001, 92526471002, 92526471003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
03/19/2115:25
LABORATORY CONTROL SAMPLE:
3198360
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
9.6
96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3198361 3198362
MS MSD
92526916001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 11.0 10.7 110 107 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
QC Batch: 605602 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526471001, 92526471002, 92526471003
METHOD BLANK: 3190534 Matrix:
Associated Lab Samples: 92526471001, 92526471002, 92526471003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1,1-Trichloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1,2-Trichloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1-Dichloroethane
ug/L
ND
1.0
03/11/21 02:09
1,1-Dichloroethene
ug/L
ND
1.0
03/11/21 02:09
1,2,3-Trichloropropane
ug/L
ND
1.0
03/11/21 02:09
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
03/11/21 02:09
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/11/21 02:09
1,2-Dichlorobenzene
ug/L
ND
1.0
03/11/21 02:09
1,2-Dichloroethane
ug/L
ND
1.0
03/11/21 02:09
1,2-Dichloropropane
ug/L
ND
1.0
03/11/21 02:09
1,4-Dichlorobenzene
ug/L
ND
1.0
03/11/21 02:09
2-Butanone (MEK)
ug/L
ND
5.0
03/11/21 02:09
2-Hexanone
ug/L
ND
5.0
03/11/21 02:09
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/11/21 02:09
Acetone
ug/L
ND
25.0
03/11/21 02:09
Acrylonitrile
ug/L
ND
10.0
03/11/21 02:09
Benzene
ug/L
ND
1.0
03/11/21 02:09
Bromochloromethane
ug/L
ND
1.0
03/11/21 02:09
Bromodichloromethane
ug/L
ND
1.0
03/11/21 02:09
Bromoform
ug/L
ND
1.0
03/11/21 02:09
Bromomethane
ug/L
ND
2.0
03/11/21 02:09
Carbon disulfide
ug/L
ND
2.0
03/11/21 02:09
Carbon tetrachloride
ug/L
ND
1.0
03/11/21 02:09
Chlorobenzene
ug/L
ND
1.0
03/11/21 02:09
Chloroethane
ug/L
ND
1.0
03/11/21 02:09
Chloroform
ug/L
ND
5.0
03/11/21 02:09
Chloromethane
ug/L
ND
1.0
03/11/21 02:09
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/11/21 02:09
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/11/21 02:09
Dibromochloromethane
ug/L
ND
1.0
03/11/21 02:09
Dibromomethane
ug/L
ND
1.0
03/11/21 02:09
Ethylbenzene
ug/L
ND
1.0
03/11/21 02:09
lodomethane
ug/L
ND
20.0
03/11/21 02:09
m&p-Xylene
ug/L
ND
2.0
03/11/21 02:09
Methylene Chloride
ug/L
ND
5.0
03/11/21 02:09
o-Xylene
ug/L
ND
1.0
03/11/21 02:09
Styrene
ug/L
ND
1.0
03/11/21 02:09
Tetrachloroethene
ug/L
ND
1.0
03/11/21 02:09
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 22

leAnalyiical
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QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
METHOD BLANK: 3190534 Matrix:
Associated Lab Samples: 92526471001, 92526471002, 92526471003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
03/11/21 02:09
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/11/21 02:09
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/11/21 02:09
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/11/21 02:09
Trichloroethene
ug/L
ND
1.0
03/11/21 02:09
Trichlorofluoromethane
ug/L
ND
1.0
03/11/21 02:09
Vinyl acetate
ug/L
ND
2.0
03/11/21 02:09
Vinyl chloride
ug/L
ND
1.0
03/11/21 02:09
Xylene (Total)
ug/L
ND
1.0
03/11/21 02:09
1,2-Dichloroethane-d4 (S)
%
101
70-130
03/11/21 02:09
4-Bromofluorobenzene (S)
%
98
70-130
03/11/21 02:09
Toluene-d8 (S)
%
98
70-130
03/11/21 02:09
LABORATORY CONTROL SAMPLE:
Parameter
3190535
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.8
100
70-130
1,1,1-Trichloroethane
ug/L
50
48.8
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.5
99
70-130
1,1-Dichloroethane
ug/L
50
49.6
99
70-130
1,1-Dichloroethene
ug/L
50
48.8
98
70-132
1,2,3-Trichloropropane
ug/L
50
49.3
99
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.3
101
70-132
1,2-Dibromoethane (EDB)
ug/L
50
48.9
98
70-130
1,2-Dichlorobenzene
ug/L
50
50.8
102
70-130
1,2-Dichloroethane
ug/L
50
49.6
99
70-130
1,2-Dichloropropane
ug/L
50
49.4
99
70-130
1,4-Dichlorobenzene
ug/L
50
49.0
98
70-130
2-Butanone (MEK)
ug/L
100
98.1
98
70-133
2-Hexanone
ug/L
100
101
101
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
102
102
70-144
Acrylonitrile
ug/L
250
246
98
70-130
Benzene
ug/L
50
47.0
94
70-130
Bromochloromethane
ug/L
50
51.9
104
70-130
Bromodichloromethane
ug/L
50
48.9
98
70-130
Bromoform
ug/L
50
50.0
100
70-131
Bromomethane
ug/L
50
50.5
101
30-177
Carbon disulfide
ug/L
50
49.9
100
70-133
Carbon tetrachloride
ug/L
50
49.0
98
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
40.8
82
46-131 v2
Chloroform
ug/L
50
50.0
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
LABORATORY CONTROL SAMPLE:
3190535
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Chloromethane
ug/L
50
43.9
88
49-130
cis-1,2-Dichloroethene
ug/L
50
47.8
96
70-130
cis-1,3-Dichloropropene
ug/L
50
50.6
101
70-130
Dibromochloromethane
ug/L
50
51.1
102
70-130
Dibromomethane
ug/L
50
50.5
101
70-130
Ethylbenzene
ug/L
50
47.9
96
70-130
lodomethane
ug/L
100
121
121
47-140
m&p-Xylene
ug/L
100
95.7
96
70-130
Methylene Chloride
ug/L
50
51.2
102
68-130
o-Xylene
ug/L
50
48.4
97
70-130
Styrene
ug/L
50
49.5
99
70-130
Tetrachloroethene
ug/L
50
46.0
92
70-130
Toluene
ug/L
50
48.2
96
70-130
trans-1,2-Dichloroethene
ug/L
50
50.2
100
70-130
trans- 1,3-Dichloropropene
ug/L
50
50.5
101
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
59.4
119
25-200
Trichloroethene
ug/L
50
47.9
96
70-130
Trichlorofluoromethane
ug/L
50
47.5
95
61-130
Vinyl acetate
ug/L
100
112
112
70-140
Vinyl chloride
ug/L
50
47.2
94
59-142
Xylene (Total)
ug/L
150
144
96
70-130
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3190536
3190537
MS
MSD
92525449005
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
100
100
104
116
104
116
70-135
11
1,1,1-Trichloroethane
ug/L
528
100
100
643
635
115
107
70-148
1
1,1,2,2-Tetrachloroethane
ug/L
ND
100
100
97.3
115
97
115
70-131
17
1,1,2-Trichloroethane
ug/L
2.7J
100
100
103
118
100
115
70-136
14
1,1-Dichloroethane
ug/L
413
100
100
520
525
107
113
70-147
1
1,1-Dichloroethene
ug/L
52.6
100
100
165
176
112
124
70-158
7
1,2,3-Trichloropropane
ug/L
ND
100
100
100
110
100
110
67-137
10
1,2-Dibromo-3-chloropropane
ug/L
ND
100
100
98.5
112
98
112
69-136
13
1,2-Dibromoethane (EDB)
ug/L
ND
100
100
99.5
112
100
112
70-137
12
1,2-Dichlorobenzene
ug/L
ND
100
100
104
119
104
119
70-133
13
1,2-Dichloroethane
ug/L
ND
100
100
104
114
104
114
67-138
9
1,2-Dichloropropane
ug/L
ND
100
100
105
116
105
116
70-138
10
1,4-Dichlorobenzene
ug/L
ND
100
100
103
115
103
115
70-133
11
2-Butanone (MEK)
ug/L
ND
200
200
194
225
97
112
61-147
15
2-Hexanone
ug/L
ND
200
200
198
232
99
116
67-139
16
4-Methyl-2-pentanone (MIBK)
ug/L
ND
200
200
201
232
99
114
67-136
15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 22

leAnalyiical
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[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3190536
3190537
MS
MSD
92525449005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
200
200
208
242
104
121
55-159
15
Acrylonitrile
ug/L
ND
500
500
506
572
101
114
68-140
12
Benzene
ug/L
6.4
100
100
108
121
101
115
67-150
12
Bromochloromethane
ug/L
ND
100
100
107
121
107
121
70-146
12
Bromodichloromethane
ug/L
ND
100
100
99.5
111
99
111
70-138
11
Bromoform
ug/L
ND
100
100
90.4
103
90
103
57-138
13
Bromomethane
ug/L
ND
100
100
159
151
159
151
10-200
5
Carbon disulfide
ug/L
ND
100
100
102
114
102
114
70-152
11
Carbon tetrachloride
ug/L
ND
100
100
109
123
109
123
70-147
12
Chlorobenzene
ug/L
ND
100
100
102
115
102
115
70-137
12
Chloroethane
ug/L
ND
100
100
103
120
103
120
51-166
15
Chloroform
ug/L
7.8J
100
100
115
124
107
117
70-144
8
Chloromethane
ug/L
ND
100
100
97.4
106
97
106
24-161
8
cis-1,2-Dichloroethene
ug/L
666
100
100
770
768
104
102
67-148
0
cis-1,3-Dichloropropene
ug/L
ND
100
100
102
115
102
115
70-142
13
Dibromochloromethane
ug/L
ND
100
100
98.4
112
98
112
68-138
13
Dibromomethane
ug/L
ND
100
100
103
115
103
115
70-134
11
Ethylbenzene
ug/L
11.1
100
100
114
126
103
115
68-143
10
lodomethane
ug/L
ND
200
200
121
179
61
89
20-161
38 R1
m&p-Xylene
ug/L
12.3
200
200
218
242
103
115
53-157
11
Methylene Chloride
ug/L
ND
100
100
113
124
106
117
64-148
9
o-Xylene
ug/L
23.3
100
100
126
136
103
113
68-143
8
Styrene
ug/L
ND
100
100
104
117
104
117
70-136
12
Tetrachloroethene
ug/L
23.6
100
100
124
135
101
111
70-139
8
Toluene
ug/L
19.6
100
100
121
134
102
115
47-157
10
trans-1,2-Dichloroethene
ug/L
ND
100
100
110
122
110
122
70-149
11
trans- 1,3-Dichloropropene
ug/L
ND
100
100
99.5
113
99
113
70-138
13
trans-1,4-Dichloro-2-butene
ug/L
ND
100
100
105
122
105
122
31-145
15
Trichloroethene
ug/L
633
100
100
754
744
120
110
70-149
1
Trichlorofluoromethane
ug/L
ND
100
100
112
125
112
125
61-154
11
Vinyl acetate
ug/L
ND
200
200
222
252
111
126
48-156
13
Vinyl chloride
ug/L
ND
100
100
99.7
114
100
114
55-172
14
Xylene (Total)
ug/L
35.5
300
300
344
379
103
114
66-145
10
1,2-Dichloroethane-d4 (S)
%
102
102
70-130
4-Bromofluorobenzene (S)
%
101
101
70-130
Toluene-d8(S)
%
100
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
QC Batch: 605277 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526471001, 92526471002, 92526471003
METHOD BLANK: 3188671
Matrix:
Water
Associated Lab Samples:
92526471001, 92526471002, 92526471003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
03/09/21 13:34
1,2-Dichloroethane-d4 (S)
%
81
70-130
03/09/21 13:34
Toluene-d8 (S)
%
91
66-133
03/09/21 13:34
LABORATORY CONTROL SAMPLE: 3188672
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 21.6 108 70-130
1,2-Dichloroethane-d4 (S) % 83 70-130
Toluene-d8 (S) % 90 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3188673
3188674
MS
MSD
92526059009 Spike
Spike MS MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 117 40
40 153 161 92
111
64-141 5
1,2-Dichloroethane-d4 (S)
%
83
82
70-130
Toluene-d8(S)
%
91
90
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 22

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[phone]
QUALIFIERS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526471
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
R1 RPD value was outside control limits.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
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Date: 03/22/2021 05:55 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92526471
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92526471001
HRW10
EPA 3010A
606946
EPA6010D
607036
92526471002
HRW11R
EPA 3010A
606946
EPA6010D
607036
92526471003
HRW13
EPA 3010A
606946
EPA6010D
607036
92526471001
HRW10
EPA 3010A
607053
EPA6020B
607080
92526471002
HRW11R
EPA 3010A
607053
EPA 6020B
607080
92526471003
HRW13
EPA 3010A
607053
EPA6020B
607080
92526471001
HRW10
EPA 8260D
605602
92526471002
HRW11R
EPA 8260D
605602
92526471003
HRW13
EPA 8260D
605602
92526471001
HRW10
EPA 8260D Mod.
605277
92526471002
HRW11R
EPA 8260D Mod.
605277
92526471003
HRW13
EPA 8260D Mod.
605277
Date: 03/22/2021 05:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 22

M Sample Condition Upon Recei
I�PaceAnalytical Document No.
F-CAR-05-033-Rev.07
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Condition Client Name:Upon W0## : 92526471
Receipt `{-�_ ; PL o } � t #
Courier: [-]Fed Ex ❑UPS -❑USPS J&Client
❑ Commercial []Pace ❑other. 92526471 I 1 1 1
Custody Seal Present? ❑Yes ®No Seals Intact? []yes M.No
Date/Initials Person Examining Contents: 3 Z( SU
Packing Material: []Bubble Wrap ❑Bubble Bags 4None ❑ Other Biological Tissue frozen?
Thermometer: QWet ❑Blue ❑None ❑Yes []No QN/A
� IR Gun ID: 7 TI�1 Type of lee:
r Correction Factor:
Cooler Temp: l Add/Subtract ('C) O,O°C Temp shcuId be above freezing to 6'C
❑samples out of temp criteria. Samples an ice, cooling process
Cooler Temp Corrected ('C): -. r1 has begun
USDA Regulated Soil (Q' N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source [internationally,
I —Iv,,. r lhl , inrhirlina Hawaii and Puerto Ricol? nYes []No
Comments/Discrepancy:
Chain of Custody Present?
❑x Yes
❑No
[I N/A
1.
Samples Arrived within Bold Time?
nYes
[:]No
❑N/A
2.
Short Hold Time Analysis (02 hr.i?
❑Yes
ONO
[]NIA
3,
Rush Turn Around Timie, }
A
4.
SufficientVofume?
`❑Yes
❑No
❑N/A
5.
Co rrect C onta ine rs Used?
Yes
❑No
❑N/A
6.
-Pace Containers used?
9yes
(-]NO
❑N/A
Containers intact?
lives
❑No
❑N/A
7.
Dissolved analysis: Samples field Filtered?
[-)Yes❑No
ON/A
8.
Sample Labels Match COC?
j Iyes
[-]No
[]N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
10.
Headspace in VOA Vials (>S-6mml? ❑Yes Ef No ❑N/A
Trip Blank Present?
❑Yes
MNo
❑N/A
11.
Trip Blank Custody Seals Present?
[Dyes
❑No
QN/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Project Manager SCURF Review:
Lot ID of split contalners:
Date:
Field Data Required? ❑Yes [-]No
Project Manager SRF Review:
Date:
Page 20 of 22

nI Sample Condition Upon Receiipt(SCUR) Page 2 of 2
aceAnelytical Document No.. Issuing Authority:
F-CAR-05-033-Rev•07 Pace Carolinas quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, UHg
"Bottom half of box is to list number of bottles
Project # �0#:92526471
PM: MWB Due Date: 03/23/21
CLIENT: 92—MECK CO
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Page 21 of 22

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Page 22 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 18, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on March 10, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92526789001 HRW8
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92526789002 HRW9R
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92526789003 HRW16
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92526789004 Trip Blank
EPA 8260D
CL
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Sample: HRW8 Lab ID: 92526789001 Collected: 03/10/21 11:50 Received: 03/10/21 13:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:53
7440-38-2
Barium
77.6
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/21 18:33
03/17/2123:53
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/21 18:33
03/17/2123:53
7440-43-9
Chromium
6.7
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7440-48-4
Copper
11.1
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7440-50-8
Lead
7.5
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7439-92-1
Nickel
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:53
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:53
7440-28-0
Vanadium
20.8
ug/L
5.0
1
03/16/21 18:33
03/17/2123:53
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:53
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/2109:42
03/17/2122:50
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/16/21 21:23
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/16/21 21:23
107-13-1
Benzene
ND
ug/L
1.0
1
03/16/21 21:23
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/16/21 21:23
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/16/21 21:23
75-27-4
Bromoform
ND
ug/L
1.0
1
03/16/21 21:23
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/16/21 21:23
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
03/16/21 21:23
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/16/21 21:23
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/16/21 21:23
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/16/21 21:23
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/16/21 21:23
75-00-3
Chloroform
ND
ug/L
5.0
1
03/16/21 21:23
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/16/21 21:23
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/16/21 21:23
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/16/21 21:23
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/16/21 21:23
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/16/21 21:23
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/16/21 21:23
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/16/21 21:23
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/16/21 21:23
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/16/21 21:23
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/16/21 21:23
107-06-2
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Sample: HRW8
Lab ID: 92526789001 Collected:
03/10/21
11:50
Received: 03/10/21 13:45 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/16/21 21:23
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/16/21 21:23
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/16/21 21:23
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/16/21 21:23
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/16/21 21:23
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/16/21 21:23
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/16/21 21:23
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/16/21 21:23
591-78-6
lodomethane
ND
ug/L
20.0
1
03/16/21 21:23
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
1
03/16/21 21:23
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/16/21 21:23
108-10-1
Styrene
ND
ug/L
1.0
1
03/16/21 21:23
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/16/21 21:23
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/16/21 21:23
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/16/21 21:23
127-18-4
Toluene
ND
ug/L
1.0
1
03/16/21 21:23
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/16/21 21:23
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/16/21 21:23
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/16/21 21:23
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/16/21 21:23
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/16/21 21:23
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/16/21 21:23
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/16/21 21:23
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/16/21 21:23
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/16/21 21:23
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/16/21 21:23
95-47-6
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
03/16/21 21:23
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
03/16/21 21:23
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
03/16/21 21:23
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/11/21 11:02
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
76
%
70-130
1
03/11/21 11:02
17060-07-0
Toluene-d8 (S)
90
%
66-133
1
03/11/21 11:02
2037-26-5
Date: 03/18/2021 04:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Sample: HRW9R
Lab ID: 92526789002 Collected:
03/10/21
11:30
Received: 03/10/21 13:45 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:56
7440-38-2
Barium
354
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/21 18:33
03/17/2123:56
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/21 18:33
03/17/2123:56
7440-43-9
Chromium
8.7
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7440-47-3
Cobalt
15.0
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7440-48-4
Copper
48.8
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7440-50-8
Lead
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7439-92-1
Nickel
7.9
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:56
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/21 18:33
03/17/2123:56
7440-28-0
Vanadium
33.4
ug/L
5.0
1
03/16/21 18:33
03/17/2123:56
7440-62-2
Zinc
16.6
ug/L
10.0
1
03/16/21 18:33
03/17/2123:56
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/2109:42
03/17/2122:54
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/12/21 18:56
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/12/21 18:56
107-13-1
Benzene
ND
ug/L
1.0
1
03/12/21 18:56
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/12/21 18:56
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/12/21 18:56
75-27-4
Bromoform
ND
ug/L
1.0
1
03/12/21 18:56
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/12/21 18:56
74-83-9 IK,v2
2-Butanone (MEK)
ND
ug/L
5.0
1
03/12/21 18:56
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/12/21 18:56
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/12/21 18:56
56-23-5
Chlorobenzene
1.6
ug/L
1.0
1
03/12/21 18:56
108-90-7
Chloroethane
1.3
ug/L
1.0
1
03/12/21 18:56
75-00-3
Chloroform
ND
ug/L
5.0
1
03/12/21 18:56
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/12/21 18:56
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/12/21 18:56
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/12/21 18:56
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/12/21 18:56
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/12/21 18:56
74-95-3
1,2-Dichlorobenzene
2.6
ug/L
1.0
1
03/12/21 18:56
95-50-1
1,4-Dichlorobenzene
3.3
ug/L
1.0
1
03/12/21 18:56
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/12/21 18:56
110-57-6
1,1-Dichloroethane
26.7
ug/L
1.0
1
03/12/21 18:56
75-34-3
1,2-Dichloroethane
2.1
ug/L
1.0
1
03/12/21 18:56
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Sample: HRW9R Lab ID: 92526789002 Collected: 03/10/21 11:30 Received: 03/10/21 13:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/12/21 18:56
75-35-4
cis-1,2-Dichloroethene
59.1
ug/L
1.0
1
03/12/21 18:56
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 18:56
156-60-5
1,2-Dichloropropene
2.1
ug/L
1.0
1
03/12/21 18:56
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 18:56
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 18:56
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/12/21 18:56
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/12/21 18:56
591-78-6
lodomethane
ND
ug/L
20.0
1
03/12/21 18:56
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/12/21 18:56
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/12/21 18:56
108-10-1
Styrene
ND
ug/L
1.0
1
03/12/21 18:56
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 18:56
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 18:56
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/12/21 18:56
127-18-4
Toluene
ND
ug/L
1.0
1
03/12/21 18:56
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/12/21 18:56
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/12/21 18:56
79-00-5
Trichloroethene
1.4
ug/L
1.0
1
03/12/21 18:56
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/12/21 18:56
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/12/21 18:56
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/12/21 18:56
108-05-4
Vinyl chloride
6.5
ug/L
1.0
1
03/12/21 18:56
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/12/21 18:56
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/12/21 18:56
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/12/21 18:56
95-47-6
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
03/12/21 18:56
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
03/12/21 18:56
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
03/12/21 18:56
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
13.4
ug/L
2.0
1
03/11/21 12:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
03/11/21 12:37
17060-07-0
Toluene-d8 (S)
89
%
66-133
1
03/11/21 12:37
2037-26-5
Date: 03/18/2021 04:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Sample: HRW16
Lab ID: 92526789003 Collected:
03/10/21
11:10
Received: 03/10/21 13:45 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/16/21 18:33
03/18/2100:06
7440-38-2
Barium
115
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/16/21 18:33
03/18/2100:06
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/16/21 18:33
03/18/2100:06
7440-43-9
Chromium
ND
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7440-48-4
Copper
9.8
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7440-50-8
Lead
5.4
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7439-92-1
Nickel
ND
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7440-02-0
Selenium
ND
ug/L
10.0
1
03/16/21 18:33
03/18/2100:06
7782-49-2
Silver
ND
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7440-22-4
Thallium
ND
ug/L
10.0
1
03/16/21 18:33
03/18/2100:06
7440-28-0
Vanadium
13.0
ug/L
5.0
1
03/16/21 18:33
03/18/2100:06
7440-62-2
Zinc
ND
ug/L
10.0
1
03/16/21 18:33
03/18/2100:06
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/2109:42
03/17/2122:57
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/12/21 18:38
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/12/21 18:38
107-13-1
Benzene
ND
ug/L
1.0
1
03/12/21 18:38
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/12/21 18:38
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/12/21 18:38
75-27-4
Bromoform
ND
ug/L
1.0
1
03/12/21 18:38
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/12/21 18:38
74-83-9 IK,v2
2-Butanone (MEK)
ND
ug/L
5.0
1
03/12/21 18:38
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/12/21 18:38
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/12/21 18:38
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/12/21 18:38
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/12/21 18:38
75-00-3
Chloroform
ND
ug/L
5.0
1
03/12/21 18:38
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/12/21 18:38
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/12/21 18:38
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/12/21 18:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/12/21 18:38
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/12/21 18:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 18:38
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 18:38
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/12/21 18:38
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/12/21 18:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/12/21 18:38
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Sample: HRW16 Lab ID: 92526789003 Collected: 03/10/21 11:10 Received: 03/10/21 13:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/12/21 18:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 18:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 18:38
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/12/21 18:38
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 18:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 18:38
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/12/21 18:38
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/12/21 18:38
591-78-6
lodomethane
ND
ug/L
20.0
1
03/12/21 18:38
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/12/21 18:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/12/21 18:38
108-10-1
Styrene
ND
ug/L
1.0
1
03/12/21 18:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 18:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 18:38
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/12/21 18:38
127-18-4
Toluene
ND
ug/L
1.0
1
03/12/21 18:38
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/12/21 18:38
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/12/21 18:38
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/12/21 18:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/12/21 18:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/12/21 18:38
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/12/21 18:38
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/12/21 18:38
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/12/21 18:38
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/12/21 18:38
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/12/21 18:38
95-47-6
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
03/12/21 18:38
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
03/12/21 18:38
17060-07-0
Toluene-d8 (S)
108
%
70-130
1
03/12/21 18:38
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/11/21 11:21
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
80
%
70-130
1
03/11/21 11:21
17060-07-0
Toluene-d8 (S)
91
%
66-133
1
03/11/21 11:21
2037-26-5
Date: 03/18/2021 04:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Sample: Trip Blank
Lab ID: 92526789004 Collected:
03/10/21
09:15
Received: 03/10/21 13:45 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/12/21 13:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/12/21 13:50
107-13-1
Benzene
ND
ug/L
1.0
1
03/12/21 13:50
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/12/21 13:50
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/12/21 13:50
75-27-4
Bromoform
ND
ug/L
1.0
1
03/12/21 13:50
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/12/21 13:50
74-83-9 IK,v2
2-Butanone (MEK)
ND
ug/L
5.0
1
03/12/21 13:50
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/12/21 13:50
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/12/21 13:50
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/12/21 13:50
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/12/21 13:50
75-00-3
Chloroform
ND
ug/L
5.0
1
03/12/21 13:50
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/12/21 13:50
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/12/21 13:50
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/12/21 13:50
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/12/21 13:50
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/12/21 13:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 13:50
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 13:50
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/12/21 13:50
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/12/21 13:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/12/21 13:50
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/12/21 13:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 13:50
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 13:50
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/12/21 13:50
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 13:50
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 13:50
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/12/21 13:50
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/12/21 13:50
591-78-6
lodomethane
ND
ug/L
20.0
1
03/12/21 13:50
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/12/21 13:50
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/12/21 13:50
108-10-1
Styrene
ND
ug/L
1.0
1
03/12/21 13:50
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 13:50
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 13:50
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/12/21 13:50
127-18-4
Toluene
ND
ug/L
1.0
1
03/12/21 13:50
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/12/21 13:50
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/12/21 13:50
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/12/21 13:50
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/12/21 13:50
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/12/21 13:50
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/12/21 13:50
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/12/21 13:50
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 28

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ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
Sample: Trip Blank
Parameters
Lab ID: 92526789004 Collected: 03/10/21 09:15
Results Units Report Limit DF
Received: 03/10/21 13:45 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
03/12/21 13:50
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
03/12/21 13:50
179601-23-1
o-Xylene
ND ug/L
1.0
1
03/12/21 13:50
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101 %
70-130
1
03/12/21 13:50
460-00-4
1,2-Dichloroethane-d4 (S)
96 %
70-130
1
03/12/21 13:50
17060-07-0
Toluene-d8 (S)
106 %
70-130
1
03/12/21 13:50
2037-26-5
Date: 03/18/2021 04:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 28

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
QC Batch: 606946 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92526789001, 92526789002, 92526789003
METHOD BLANK: 3197719 Matrix: Water
Associated Lab Samples: 92526789001, 92526789002, 92526789003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
03/17/2122:32
10.0
03/17/2122:32
5.0
03/17/2122:32
1.0
03/17/2122:32
1.0
03/17/2122:32
5.0
03/17/2122:32
5.0
03/17/2122:32
5.0
03/17/2122:32
5.0
03/17/2122:32
5.0
03/17/2122:32
10.0
03/17/2122:32
5.0
03/17/2122:32
10.0
03/17/2122:32
5.0
03/17/2122:32
10.0
03/17/2122:32
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3197720
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
504
101
80-120
Arsenic
ug/L
500
491
98
80-120
Barium
ug/L
500
498
100
80-120
Beryllium
ug/L
500
498
100
80-120
Cadmium
ug/L
500
495
99
80-120
Chromium
ug/L
500
489
98
80-120
Cobalt
ug/L
500
479
96
80-120
Copper
ug/L
500
512
102
80-120
Lead
ug/L
500
487
97
80-120
Nickel
ug/L
500
492
98
80-120
Selenium
ug/L
500
490
98
80-120
Silver
ug/L
250
252
101
80-120
Thallium
ug/L
500
486
97
80-120
Vanadium
ug/L
500
480
96
80-120
Zinc
ug/L
500
478
96
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92526789
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3197721
3197722
MS
MSD
92526090001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
499
502
99
100
75-125
1
Arsenic
ug/L
ND
500
500
493
506
99
101
75-125
3
Barium
ug/L
17.5
500
500
505
508
98
98
75-125
1
Beryllium
ug/L
ND
500
500
492
494
98
99
75-125
0
Cadmium
ug/L
1.6
500
500
500
506
100
101
75-125
1
Chromium
ug/L
ND
500
500
485
489
97
98
75-125
1
Cobalt
ug/L
ND
500
500
472
477
94
95
75-125
1
Copper
ug/L
21.6
500
500
524
531
101
102
75-125
1
Lead
ug/L
ND
500
500
478
480
95
96
75-125
0
Nickel
ug/L
7.5
500
500
490
495
96
97
75-125
1
Selenium
ug/L
ND
500
500
519
524
104
105
75-125
1
Silver
ug/L
ND
250
250
247
249
98
99
75-125
1
Thallium
ug/L
ND
500
500
473
484
94
96
75-125
2
Vanadium
ug/L
ND
500
500
477
484
95
97
75-125
1
Zinc
ug/L
358
500
500
826
832
94
95
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
QC Batch: 607128 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92526789001, 92526789002, 92526789003
METHOD BLANK: 3198549 Matrix: Water
Associated Lab Samples: 92526789001, 92526789002, 92526789003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Thallium ug/L ND 1.0 03/17/2121:56
LABORATORY CONTROL SAMPLE:
3198550
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Thallium
ug/L
10
10.3
103
80-120
LABORATORY CONTROL SAMPLE:
3198551
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Thallium
ug/L
10
10.5
105
80-120
LABORATORY CONTROL SAMPLE: 3198552
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.3 103 80-120
LABORATORY CONTROL SAMPLE: 3198553
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.6 106 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3198554 3198555
MS MSD
92526479001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.9 10.6 109 106 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
QC Batch: 606051 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526789002, 92526789003, 92526789004
METHOD BLANK: 3193053 Matrix:
Associated Lab Samples: 92526789002, 92526789003, 92526789004
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1,1-Trichloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1,2-Trichloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1-Dichloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1-Dichloroethene
ug/L
ND
1.0
03/12/21 12:56
1,2,3-Trichloropropane
ug/L
ND
1.0
03/12/21 12:56
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
03/12/21 12:56
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/12/21 12:56
1,2-Dichlorobenzene
ug/L
ND
1.0
03/12/21 12:56
1,2-Dichloroethane
ug/L
ND
1.0
03/12/21 12:56
1,2-Dichloropropane
ug/L
ND
1.0
03/12/21 12:56
1,4-Dichlorobenzene
ug/L
ND
1.0
03/12/21 12:56
2-Butanone (MEK)
ug/L
ND
5.0
03/12/21 12:56
2-Hexanone
ug/L
ND
5.0
03/12/21 12:56
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/12/21 12:56
Acetone
ug/L
ND
25.0
03/12/21 12:56
Acrylonitrile
ug/L
ND
10.0
03/12/21 12:56
Benzene
ug/L
ND
1.0
03/12/21 12:56
Bromochloromethane
ug/L
ND
1.0
03/12/21 12:56
Bromodichloromethane
ug/L
ND
1.0
03/12/21 12:56
Bromoform
ug/L
ND
1.0
03/12/21 12:56
Bromomethane
ug/L
ND
2.0
03/12/21 12:56 IK,v2
Carbon disulfide
ug/L
ND
2.0
03/12/21 12:56
Carbon tetrachloride
ug/L
ND
1.0
03/12/21 12:56
Chlorobenzene
ug/L
ND
1.0
03/12/21 12:56
Chloroethane
ug/L
ND
1.0
03/12/21 12:56
Chloroform
ug/L
ND
5.0
03/12/21 12:56
Chloromethane
ug/L
ND
1.0
03/12/21 12:56 v2
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/12/21 12:56
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/12/21 12:56
Dibromochloromethane
ug/L
ND
1.0
03/12/21 12:56
Dibromomethane
ug/L
ND
1.0
03/12/21 12:56
Ethylbenzene
ug/L
ND
1.0
03/12/21 12:56
lodomethane
ug/L
ND
20.0
03/12/21 12:56
m&p-Xylene
ug/L
ND
2.0
03/12/21 12:56
Methylene Chloride
ug/L
ND
5.0
03/12/21 12:56
o-Xylene
ug/L
ND
1.0
03/12/21 12:56
Styrene
ug/L
ND
1.0
03/12/21 12:56
Tetrachloroethene
ug/L
ND
1.0
03/12/21 12:56
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
METHOD BLANK: 3193053 Matrix:
Associated Lab Samples: 92526789002, 92526789003, 92526789004
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
03/12/21 12:56
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/12/21 12:56
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/12/21 12:56
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/12/21 12:56
Trichloroethene
ug/L
ND
1.0
03/12/21 12:56
Trichlorofluoromethane
ug/L
ND
1.0
03/12/21 12:56
Vinyl acetate
ug/L
ND
2.0
03/12/21 12:56
Vinyl chloride
ug/L
ND
1.0
03/12/21 12:56
Xylene (Total)
ug/L
ND
1.0
03/12/21 12:56
1,2-Dichloroethane-d4 (S)
%
96
70-130
03/12/21 12:56
4-Bromofluorobenzene (S)
%
102
70-130
03/12/21 12:56
Toluene-d8 (S)
%
107
70-130
03/12/21 12:56
LABORATORY CONTROL SAMPLE: 3193054
Qualifiers
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.3
107
70-130
1,1,1-Trichloroethane
ug/L
50
44.7
89
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
52.1
104
70-130
1,1-Dichloroethane
ug/L
50
45.5
91
70-130
1,1-Dichloroethene
ug/L
50
47.8
96
70-132
1,2,3-Trichloropropane
ug/L
50
49.8
100
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.0
108
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.6
105
70-130
1,2-Dichlorobenzene
ug/L
50
49.4
99
70-130
1,2-Dichloroethane
ug/L
50
45.8
92
70-130
1,2-Dichloropropane
ug/L
50
51.1
102
70-130
1,4-Dichlorobenzene
ug/L
50
48.9
98
70-130
2-Butanone (MEK)
ug/L
100
110
110
70-133
2-Hexanone
ug/L
100
105
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
97.0
97
70-144
Acrylonitrile
ug/L
250
222
89
70-130
Benzene
ug/L
50
47.9
96
70-130
Bromochloromethane
ug/L
50
44.2
88
70-130
Bromodichloromethane
ug/L
50
47.0
94
70-130
Bromoform
ug/L
50
52.8
106
70-131
Bromomethane
ug/L
50
41.2
82
30-177lK,v2
Carbon disulfide
ug/L
50
45.1
90
70-133
Carbon tetrachloride
ug/L
50
46.3
93
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
39.2
78
46-131
Chloroform
ug/L
50
45.1
90
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
LABORATORY CONTROL SAMPLE:
Parameter
3193054
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
39.6
cis-1,2-Dichloroethene
ug/L
50
44.0
cis-1,3-Dichloropropene
ug/L
50
54.2
Dibromochloromethane
ug/L
50
53.4
Dibromomethane
ug/L
50
47.1
Ethylbenzene
ug/L
50
48.7
lodomethane
ug/L
100
102
m&p-Xylene
ug/L
100
96.8
Methylene Chloride
ug/L
50
43.5
o-Xylene
ug/L
50
48.7
Styrene
ug/L
50
49.7
Tetrachloroethene
ug/L
50
47.2
Toluene
ug/L
50
46.4
trans-1,2-Dichloroethene
ug/L
50
44.6
trans- 1,3-Dichloropropene
ug/L
50
53.2
trans-1,4-Dichloro-2-butene
ug/L
50
51.1
Trichloroethene
ug/L
50
49.2
Trichlorofluoromethane
ug/L
50
42.6
Vinyl acetate
ug/L
100
122
Vinyl chloride
ug/L
50
40.6
Xylene (Total)
ug/L
150
146
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
79
49-130 v2
88
70-130
108
70-130
107
70-130
94
70-130
97
70-130
102
47-140
97
70-130
87
68-130
97
70-130
99
70-130
94
70-130
93
70-130
89
70-130
106
70-130
102
25-200
98
70-130
85
61-130
122
70-140
81
59-142
97
70-130
95
70-130
98
70-130
96
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3193055
MS
92527185003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3193056
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.8
23.5
104
118
70-135
12
1,1,1-Trichloroethane
ug/L
ND
20
20
21.3
22.4
106
112
70-148
5
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.0
23.1
100
116
70-131
14
1,1,2-Trichloroethane
ug/L
ND
20
20
21.8
23.5
109
118
70-136
8
1,1-Dichloroethane
ug/L
ND
20
20
20.7
21.4
103
107
70-147
3
1,1-Dichloroethene
ug/L
ND
20
20
22.0
23.0
110
115
70-158
5
1,2,3-Trichloropropane
ug/L
ND
20
20
19.8
22.1
99
110
67-137
11
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.6
21.8
103
109
69-136
6
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
23.5
107
118
70-137
9
1,2-Dichlorobenzene
ug/L
ND
20
20
20.9
22.3
104
112
70-133
7
1,2-Dichloroethane
ug/L
ND
20
20
20.5
21.6
103
108
67-138
5
1,2-Dichloropropane
ug/L
ND
20
20
21.8
23.8
109
119
70-138
9
1,4-Dichlorobenzene
ug/L
ND
20
20
20.9
22.4
104
112
70-133
7
2-Butanone (MEK)
ug/L
ND
40
40
44.6
49.4
112
124
61-147
10
2-Hexanone
ug/L
ND
40
40
40.6
45.5
102
114
67-139
11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
39.8
44.4
100
111
67-136
11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3193055
MS
92527185003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3193056
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
43.8
47.4
110
119
55-159
8
Acrylonitrile
ug/L
ND
100
100
99.3
106
99
106
68-140
7
Benzene
ug/L
ND
20
20
20.8
22.4
104
112
67-150
7
Bromochloromethane
ug/L
ND
20
20
21.1
22.4
106
112
70-146
6
Bromodichloromethane
ug/L
ND
20
20
20.7
22.3
104
112
70-138
7
Bromoform
ug/L
ND
20
20
20.8
22.7
104
114
57-138
9
Bromomethane
ug/L
ND
20
20
21.4
22.6
107
113
10-200
51K
Carbon disulfide
ug/L
ND
20
20
21.9
22.5
109
112
70-152
3
Carbon tetrachloride
ug/L
ND
20
20
21.8
22.8
109
114
70-147
5
Chlorobenzene
ug/L
ND
20
20
21.4
22.8
107
114
70-137
6
Chloroethane
ug/L
ND
20
20
20.2
20.4
101
102
51-166
1
Chloroform
ug/L
ND
20
20
20.2
21.7
101
108
70-144
7
Chloromethane
ug/L
ND
20
20
19.2
20.2
96
101
24-161
5
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
20.9
101
105
67-148
4
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.7
24.4
113
122
70-142
7
Dibromochloromethane
ug/L
ND
20
20
22.2
24.0
111
120
68-138
8
Dibromomethane
ug/L
ND
20
20
21.1
22.8
106
114
70-134
8
Ethylbenzene
ug/L
ND
20
20
21.4
22.8
107
114
68-143
6
lodomethane
ug/L
ND
40
40
40.2
42.5
101
106
20-161
6
m&p-Xylene
ug/L
ND
40
40
42.7
45.5
107
114
53-157
6
Methylene Chloride
ug/L
ND
20
20
19.4
20.1
97
100
64-148
3
o-Xylene
ug/L
ND
20
20
21.8
22.7
109
114
68-143
4
Styrene
ug/L
ND
20
20
21.9
23.1
109
115
70-136
6
Tetrachloroethene
ug/L
ND
20
20
20.7
22.1
104
110
70-139
6
Toluene
ug/L
ND
20
20
20.9
22.1
104
111
47-157
6
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.4
21.6
102
108
70-149
5
trans- 1,3-Dichloropropene
ug/L
ND
20
20
22.1
24.1
110
120
70-138
9
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
20.3
23.0
102
115
31-145
12
Trichloroethene
ug/L
ND
20
20
22.0
23.4
110
117
70-149
6
Trichlorofluoromethane
ug/L
ND
20
20
20.4
21.1
102
106
61-154
3
Vinyl acetate
ug/L
ND
40
40
45.7
50.5
114
126
48-156
10
Vinyl chloride
ug/L
ND
20
20
18.7
19.4
93
97
55-172
4
Xylene (Total)
ug/L
ND
60
60
64.5
68.2
107
114
66-145
6
1,2-Dichloroethane-d4 (S)
%
99
97
70-130
4-Bromofluorobenzene (S)
%
104
103
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
QC Batch: 606852 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526789001
METHOD BLANK: 3197122
Associated Lab Samples: 92526789001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/16/21 16:36
1,1,1-Trichloroethane
ug/L
ND
1.0
03/16/21 16:36
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/16/21 16:36
1,1,2-Trichloroethane
ug/L
ND
1.0
03/16/21 16:36
1,1-Dichloroethane
ug/L
ND
1.0
03/16/21 16:36
1,1-Dichloroethene
ug/L
ND
1.0
03/16/21 16:36
1,2,3-Trichloropropane
ug/L
ND
1.0
03/16/21 16:36
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
03/16/21 16:36
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/16/21 16:36
1,2-Dichlorobenzene
ug/L
ND
1.0
03/16/21 16:36
1,2-Dichloroethane
ug/L
ND
1.0
03/16/21 16:36
1,2-Dichloropropane
ug/L
ND
1.0
03/16/21 16:36
1,4-Dichlorobenzene
ug/L
ND
1.0
03/16/21 16:36
2-Butanone (MEK)
ug/L
ND
5.0
03/16/21 16:36
2-Hexanone
ug/L
ND
5.0
03/16/21 16:36
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/16/21 16:36
Acetone
ug/L
ND
25.0
03/16/21 16:36
Acrylonitrile
ug/L
ND
10.0
03/16/21 16:36
Benzene
ug/L
ND
1.0
03/16/21 16:36
Bromochloromethane
ug/L
ND
1.0
03/16/21 16:36
Bromodichloromethane
ug/L
ND
1.0
03/16/21 16:36
Bromoform
ug/L
ND
1.0
03/16/21 16:36
Bromomethane
ug/L
ND
2.0
03/16/21 16:36 IK
Carbon disulfide
ug/L
ND
2.0
03/16/21 16:36
Carbon tetrachloride
ug/L
ND
1.0
03/16/21 16:36
Chlorobenzene
ug/L
ND
1.0
03/16/21 16:36
Chloroethane
ug/L
ND
1.0
03/16/21 16:36
Chloroform
ug/L
ND
5.0
03/16/21 16:36
Chloromethane
ug/L
ND
1.0
03/16/21 16:36
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/16/21 16:36
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/16/21 16:36
Dibromochloromethane
ug/L
ND
1.0
03/16/21 16:36
Dibromomethane
ug/L
ND
1.0
03/16/21 16:36
Ethylbenzene
ug/L
ND
1.0
03/16/21 16:36
lodomethane
ug/L
ND
20.0
03/16/21 16:36 v2
m&p-Xylene
ug/L
ND
2.0
03/16/21 16:36
Methylene Chloride
ug/L
ND
5.0
03/16/21 16:36
o-Xylene
ug/L
ND
1.0
03/16/21 16:36
Styrene
ug/L
ND
1.0
03/16/21 16:36
Tetrachloroethene
ug/L
ND
1.0
03/16/21 16:36
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
METHOD BLANK: 3197122
Associated Lab Samples: 92526789001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
03/16/21 16:36
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/16/21 16:36
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/16/21 16:36
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/16/21 16:36
Trichloroethene
ug/L
ND
1.0
03/16/21 16:36
Trichlorofluoromethane
ug/L
ND
1.0
03/16/21 16:36
Vinyl acetate
ug/L
ND
2.0
03/16/21 16:36
Vinyl chloride
ug/L
ND
1.0
03/16/21 16:36
Xylene (Total)
ug/L
ND
1.0
03/16/21 16:36
1,2-Dichloroethane-d4 (S)
%
93
70-130
03/16/21 16:36
4-Bromofluorobenzene (S)
%
103
70-130
03/16/21 16:36
Toluene-d8 (S)
%
107
70-130
03/16/21 16:36
LABORATORY CONTROL SAMPLE:
Parameter
3197123
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
51.8
104
70-130
1,1,1-Trichloroethane
ug/L
50
44.0
88
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.0
96
70-130
1,1,2-Trichloroethane
ug/L
50
50.9
102
70-130
1,1-Dichloroethane
ug/L
50
43.5
87
70-130
1,1-Dichloroethene
ug/L
50
46.0
92
70-132
1,2,3-Trichloropropane
ug/L
50
47.3
95
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
48.8
98
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.7
101
70-130
1,2-Dichlorobenzene
ug/L
50
48.6
97
70-130
1,2-Dichloroethane
ug/L
50
44.7
89
70-130
1,2-Dichloropropane
ug/L
50
48.2
96
70-130
1,4-Dichlorobenzene
ug/L
50
48.3
97
70-130
2-Butanone (MEK)
ug/L
100
102
102
70-133
2-Hexanone
ug/L
100
93.0
93
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
94.1
94
70-130
Acetone
ug/L
100
101
101
70-144
Acrylonitrile
ug/L
250
214
86
70-130
Benzene
ug/L
50
46.1
92
70-130
Bromochloromethane
ug/L
50
46.0
92
70-130
Bromodichloromethane
ug/L
50
46.0
92
70-130
Bromoform
ug/L
50
50.8
102
70-131
Bromomethane
ug/L
50
47.9
96
30-177lK
Carbon disulfide
ug/L
50
45.5
91
70-133
Carbon tetrachloride
ug/L
50
45.6
91
70-130
Chlorobenzene
ug/L
50
47.4
95
70-130
Chloroethane
ug/L
50
40.4
81
46-131
Chloroform
ug/L
50
43.5
87
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
LABORATORY CONTROL SAMPLE:
Parameter
3197123
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
44.7
89
49-130
42.8
86
70-130
52.8
106
70-130
52.6
105
70-130
46.5
93
70-130
47.3
95
70-130
85.8
86
47-140 v2
95.5
96
70-130
43.1
86
68-130
48.6
97
70-130
49.5
99
70-130
47.1
94
70-130
45.5
91
70-130
43.7
87
70-130
51.7
103
70-130
54.6
109
25-200
48.1
96
70-130
41.5
83
61-130
115
115
70-140
41.2
82
59-142
144
96
70-130
94
70-130
99
70-130
97
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3197124
MS
92526789001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3197125
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.6
21.7
108
108
70-135
0
1,1,1-Trichloroethane
ug/L
ND
20
20
21.6
22.1
108
111
70-148
2
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.9
19.3
100
97
70-131
3
1,1,2-Trichloroethane
ug/L
ND
20
20
21.8
21.1
109
105
70-136
3
1,1-Dichloroethane
ug/L
ND
20
20
20.4
21.2
102
106
70-147
4
1,1-Dichloroethene
ug/L
ND
20
20
20.2
20.9
101
104
70-158
4
1,2,3-Trichloropropane
ug/L
ND
20
20
19.9
19.3
99
96
67-137
3
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.8
21.6
109
108
69-136
1
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.7
21.6
109
108
70-137
1
1,2-Dichlorobenzene
ug/L
ND
20
20
21.9
21.8
110
109
70-133
1
1,2-Dichloroethane
ug/L
ND
20
20
21.3
20.9
106
105
67-138
2
1,2-Dichloropropane
ug/L
ND
20
20
21.2
21.0
106
105
70-138
1
1,4-Dichlorobenzene
ug/L
ND
20
20
21.8
21.5
109
107
70-133
2
2-Butanone (MEK)
ug/L
ND
40
40
40.9
40.4
102
101
61-147
1
2-Hexanone
ug/L
ND
40
40
38.9
38.0
97
95
67-139
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
37.1
36.8
93
92
67-136
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3197124
MS
92526789001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3197125
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
42.1
43.1
105
108
55-159
2
Acrylonitrile
ug/L
ND
100
100
99.3
101
99
101
68-140
1
Benzene
ug/L
ND
20
20
20.8
21.6
104
108
67-150
4
Bromochloromethane
ug/L
ND
20
20
22.1
22.5
110
113
70-146
2
Bromodichloromethane
ug/L
ND
20
20
20.1
19.7
100
98
70-138
2
Bromoform
ug/L
ND
20
20
21.0
21.1
105
105
57-138
0
Bromomethane
ug/L
ND
20
20
27.0
26.1
135
130
10-200
4
Carbon disulfide
ug/L
ND
20
20
20.3
21.4
102
107
70-152
5
Carbon tetrachloride
ug/L
ND
20
20
22.0
22.8
110
114
70-147
4
Chlorobenzene
ug/L
ND
20
20
21.9
21.8
109
109
70-137
0
Chloroethane
ug/L
ND
20
20
17.8
17.2
89
86
51-166
4
Chloroform
ug/L
ND
20
20
21.2
21.5
106
108
70-144
1
Chloromethane
ug/L
ND
20
20
16.0
16.5
80
83
24-161
3 v2
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.5
21.0
102
105
67-148
2
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.3
20.5
101
102
70-142
1
Dibromochloromethane
ug/L
ND
20
20
22.2
22.3
111
112
68-138
0
Dibromomethane
ug/L
ND
20
20
23.4
23.3
117
116
70-134
1
Ethylbenzene
ug/L
ND
20
20
21.5
21.1
108
106
68-143
2
lodomethane
ug/L
ND
40
40
35.4
36.2
88
91
20-161
2
m&p-Xylene
ug/L
ND
40
40
43.4
42.9
108
107
53-157
1
Methylene Chloride
ug/L
ND
20
20
18.7
19.4
94
97
64-148
3
o-Xylene
ug/L
ND
20
20
21.4
20.9
107
105
68-143
2
Styrene
ug/L
ND
20
20
22.2
22.0
111
110
70-136
1
Tetrachloroethene
ug/L
ND
20
20
22.3
22.5
111
113
70-139
1
Toluene
ug/L
ND
20
20
20.6
21.2
103
106
47-157
3
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.2
21.4
101
107
70-149
6
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.2
20.5
101
103
70-138
1
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
22.6
21.6
113
108
31-145
4 v1
Trichloroethene
ug/L
ND
20
20
23.3
22.9
116
114
70-149
2
Trichlorofluoromethane
ug/L
ND
20
20
19.0
18.1
95
91
61-154
5
Vinyl acetate
ug/L
ND
40
40
42.3
43.5
106
109
48-156
3
Vinyl chloride
ug/L
ND
20
20
17.4
17.9
87
89
55-172
3
Xylene (Total)
ug/L
ND
60
60
64.8
63.8
108
106
66-145
2
1,2-Dichloroethane-d4 (S)
%
95
91
70-130
4-Bromofluorobenzene (S)
%
101
99
70-130
Toluene-d8(S)
%
94
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
QC Batch: 605885 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526789001, 92526789002, 92526789003
METHOD BLANK: 3191963
Matrix:
Water
Associated Lab Samples:
92526789001, 92526789002, 92526789003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
03/11/21 10:44
1,2-Dichloroethane-d4 (S)
%
83
70-130
03/11/21 10:44
Toluene-d8 (S)
%
91
66-133
03/11/21 10:44
LABORATORY CONTROL SAMPLE: 3191964
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 21.2 106 70-130
1,2-Dichloroethane-d4 (S) % 79 70-130
Toluene-d8 (S) % 88 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3191965
3191966
MS
MSD
92526789001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 22.1
20.8 111
104
64-141 6
1,2-Dichloroethane-d4 (S)
%
83
82
70-130
Toluene-d8(S)
%
92
92
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 28

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526789
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2021 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92526789
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92526789001
HRW8
EPA 3010A
606946
EPA 6010D
607036
92526789002
HRW9R
EPA 3010A
606946
EPA 6010D
607036
92526789003
HRW16
EPA 3010A
606946
EPA6010D
607036
92526789001
HRW8
EPA 3010A
607128
EPA 6020B
607180
92526789002
HRW9R
EPA 3010A
607128
EPA 6020B
607180
92526789003
HRW16
EPA 3010A
607128
EPA 6020B
607180
92526789001
HRW8
EPA 8260D
606852
92526789002
HRW9R
EPA 8260D
606051
92526789003
HRW16
EPA 8260D
606051
92526789004
Trip Blank
EPA 8260D
606051
92526789001
HRW8
EPA 8260D Mod.
605885
92526789002
HRW9R
EPA 8260D Mod.
605885
92526789003
HRW16
EPA 8260D Mod.
605885
Date: 03/18/2021 04:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 28

UUCURItnL rvoMc. �..,�w < •�• ���. ,
r Sample Condition Upon Receipt(SCUR) Page 1 of 2
�2ceAnalyfical Document No.: Issuing Authority:
F-CAR-CS-D33-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ iiuntersville [4 Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
Sample Condition Client Name: WO# 92526�00
89
Receipt---- Project #: •
Courier: ❑fed Ex ❑UPS ❑USPS J 5(lient
❑ Commercial ❑Pace ❑Other: 92526769
Custody Seal Present? Oyes S4 Seals Intact? []Yes Rlo
Date/Initials Person Examining Contents: LT
Packing Materlak []Bubble Wrap ❑Bubble Bags None ❑ Other
Thermometer: �� owet ❑Blue
�' IR Gun ID: q j-\ t.. Co t- Type of ice:
Correction Factor:
Cooler Temp: �- Add/Subtract {°C) 0.0*12
Cooler Temp Corrected (°C):
USDA Regulated Soil�N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC {check maps)? Did samples originate From a foreign source (internationally,
❑Yes ❑No including Hawaii and Puerto Rico)? ❑Yes ❑No
Comments/Dlscrepancy,
Chain of Custody Present? 0yes []NO ❑N/A 1.
Samples Arrived within Hold Time? yes ❑No [-I N/A 2,
Short Hold Time Analysis (02 hr.)? [-]Yes o ❑NIA 3.
Mich Turn Arnund Tmg 7 o FJN4A 4.
Sufficient Volume? JkfYES []NO ❑NIA 5.
Correct Containers Used? es ❑No ❑N/A 6.
-Pace Containers Used? s ❑No ❑N/A
Containers Intact? rYes ❑Na ❑N/A 7.
Dissolved analysis: Samples field Filtered? ❑Yes No ❑N/A 8.
Sample Labels Match COC? ves ❑No []NIA 9.
-includes Date/T-ime/ID/Analysis Matrix: ;FI k
Headspace in VOA Vials (>5-6mm)? ❑Yes b6o ❑N/A 10.
Trip Blank Present? Ayes ❑No ❑N/A 11.
Trip Blank Custody Seals Present? ❑eyes Rio ❑N/A
Biological Tissue Frozen?
Des❑No �N/A
❑None
Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on ice, cooling process
hasbegun
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Oyes ❑No
CLIENT NOTIFICATION/RESOLUTION
parson rnntartnrl• Date/Time:
Project Manager SCURF Review:
Lot ID of split containers:
Date:
Project Manager SRF Review:
Date:
Page 26 of 28

Sample Condition Upon Recei,
aceAnaVical; Document No.:
F-CAR-CS-033-Rev.07
Page 2 of 2
Issuing Authority:
Pace Carolinas quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DR0/8015 (water) DOC, LLI•Ig
"Bottom half of box is to list number of bottles
Project a WO# ; 92526789
PM: MW$ Due late: 03/24/2.1
CLIENT: 92—MECK CO
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Sample ID
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Lot p
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Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy or tine loan win lie 5e111L tv tine rvunn Lyruunu U-1— — L-60% - I --
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 27 of 28

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Page 28 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 22, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on March 10, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92526797001 HRSW2
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92526797002 HRSW3
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92526797003 HRSW4
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Sample: HRSW2
Lab ID: 92526797001 Collected:
03/10/21
10:45
Received: 03/10/21 13:45 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:39
7440-38-2
Barium
32.7
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/17/2101:53
03/18/2120:39
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/17/2101:53
03/18/2120:39
7440-43-9
Chromium
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7440-48-4
Copper
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7440-50-8
Lead
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7439-92-1
Nickel
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7440-02-0
Selenium
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:39
7782-49-2
Silver
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7440-22-4
Thallium
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:39
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:39
7440-62-2
Zinc
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:39
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/21 01:47
03/19/2107:20
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/12/21 18:02
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/12/21 18:02
107-13-1
Benzene
ND
ug/L
1.0
1
03/12/21 18:02
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/12/21 18:02
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/12/21 18:02
75-27-4
Bromoform
ND
ug/L
1.0
1
03/12/21 18:02
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/12/21 18:02
74-83-9 IK,v2
2-Butanone (MEK)
ND
ug/L
5.0
1
03/12/21 18:02
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/12/21 18:02
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/12/21 18:02
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/12/21 18:02
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/12/21 18:02
75-00-3
Chloroform
ND
ug/L
5.0
1
03/12/21 18:02
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/12/21 18:02
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/12/21 18:02
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/12/21 18:02
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/12/21 18:02
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/12/21 18:02
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 18:02
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 18:02
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/12/21 18:02
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/12/21 18:02
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/12/21 18:02
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Sample: HRSW2 Lab ID: 92526797001 Collected: 03/10/21 10:45 Received: 03/10/21 13:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/12/21 18:02
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 18:02
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 18:02
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/12/21 18:02
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 18:02
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 18:02
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/12/21 18:02
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/12/21 18:02
591-78-6
lodomethane
ND
ug/L
20.0
1
03/12/21 18:02
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/12/21 18:02
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/12/21 18:02
108-10-1
Styrene
ND
ug/L
1.0
1
03/12/21 18:02
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 18:02
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 18:02
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/12/21 18:02
127-18-4
Toluene
ND
ug/L
1.0
1
03/12/21 18:02
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/12/21 18:02
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/12/21 18:02
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/12/21 18:02
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/12/21 18:02
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/12/21 18:02
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/12/21 18:02
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/12/21 18:02
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/12/21 18:02
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/12/21 18:02
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/12/21 18:02
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
03/12/21 18:02
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
03/12/21 18:02
17060-07-0
Toluene-d8 (S)
108
%
70-130
1
03/12/21 18:02
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/11/21 11:40
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
78
%
70-130
1
03/11/21 11:40
17060-07-0
Toluene-d8 (S)
90
%
66-133
1
03/11/21 11:40
2037-26-5
Date: 03/22/2021 05:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Sample: HRSW3
Lab ID: 92526797002 Collected:
03/10/21
09:50
Received: 03/10/21 13:45 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:43
7440-38-2
Barium
32.8
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/17/2101:53
03/18/2120:43
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/17/2101:53
03/18/2120:43
7440-43-9
Chromium
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7440-48-4
Copper
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7440-50-8
Lead
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7439-92-1
Nickel
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7440-02-0
Selenium
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:43
7782-49-2
Silver
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7440-22-4
Thallium
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:43
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:43
7440-62-2
Zinc
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:43
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/21 01:47
03/19/2107:24
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/12/21 17:44
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/12/21 17:44
107-13-1
Benzene
ND
ug/L
1.0
1
03/12/21 17:44
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/12/21 17:44
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/12/21 17:44
75-27-4
Bromoform
ND
ug/L
1.0
1
03/12/21 17:44
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/12/21 17:44
74-83-9 IK,v2
2-Butanone (MEK)
ND
ug/L
5.0
1
03/12/21 17:44
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/12/21 17:44
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/12/21 17:44
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/12/21 17:44
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/12/21 17:44
75-00-3
Chloroform
ND
ug/L
5.0
1
03/12/21 17:44
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/12/21 17:44
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/12/21 17:44
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/12/21 17:44
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/12/21 17:44
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/12/21 17:44
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 17:44
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 17:44
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/12/21 17:44
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/12/21 17:44
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/12/21 17:44
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Sample: HRSW3 Lab ID: 92526797002 Collected: 03/10/21 09:50 Received: 03/10/21 13:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/12/21 17:44
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 17:44
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 17:44
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/12/21 17:44
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 17:44
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 17:44
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/12/21 17:44
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/12/21 17:44
591-78-6
lodomethane
ND
ug/L
20.0
1
03/12/21 17:44
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/12/21 17:44
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/12/21 17:44
108-10-1
Styrene
ND
ug/L
1.0
1
03/12/21 17:44
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 17:44
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 17:44
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/12/21 17:44
127-18-4
Toluene
ND
ug/L
1.0
1
03/12/21 17:44
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/12/21 17:44
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/12/21 17:44
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/12/21 17:44
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/12/21 17:44
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/12/21 17:44
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/12/21 17:44
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/12/21 17:44
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/12/21 17:44
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/12/21 17:44
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/12/21 17:44
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
03/12/21 17:44
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
03/12/21 17:44
17060-07-0
Toluene-d8 (S)
107
%
70-130
1
03/12/21 17:44
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/11/21 11:59
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
81
%
70-130
1
03/11/21 11:59
17060-07-0
Toluene-d8 (S)
90
%
66-133
1
03/11/21 11:59
2037-26-5
Date: 03/22/2021 05:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Sample: HRSW4
Lab ID: 92526797003 Collected:
03/10/21
10:20
Received: 03/10/21 13:45 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:46
7440-38-2
Barium
31.2
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/17/2101:53
03/18/2120:46
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/17/2101:53
03/18/2120:46
7440-43-9
Chromium
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7440-48-4
Copper
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7440-50-8
Lead
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7439-92-1
Nickel
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7440-02-0
Selenium
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:46
7782-49-2
Silver
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7440-22-4
Thallium
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:46
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/17/2101:53
03/18/2120:46
7440-62-2
Zinc
ND
ug/L
10.0
1
03/17/2101:53
03/18/2120:46
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
1.0
1
03/17/21 01:47
03/19/2107:28
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
03/12/21 17:26
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/12/21 17:26
107-13-1
Benzene
ND
ug/L
1.0
1
03/12/21 17:26
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/12/21 17:26
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/12/21 17:26
75-27-4
Bromoform
ND
ug/L
1.0
1
03/12/21 17:26
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/12/21 17:26
74-83-9 IK,v2
2-Butanone (MEK)
ND
ug/L
5.0
1
03/12/21 17:26
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/12/21 17:26
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/12/21 17:26
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/12/21 17:26
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/12/21 17:26
75-00-3
Chloroform
ND
ug/L
5.0
1
03/12/21 17:26
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/12/21 17:26
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
03/12/21 17:26
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/12/21 17:26
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/12/21 17:26
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/12/21 17:26
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 17:26
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/12/21 17:26
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/12/21 17:26
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/12/21 17:26
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/12/21 17:26
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 22

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
Sample: HRSW4 Lab ID: 92526797003 Collected: 03/10/21 10:20 Received: 03/10/21 13:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
03/12/21 17:26
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 17:26
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/12/21 17:26
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
03/12/21 17:26
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 17:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/12/21 17:26
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/12/21 17:26
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/12/21 17:26
591-78-6
lodomethane
ND
ug/L
20.0
1
03/12/21 17:26
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/12/21 17:26
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/12/21 17:26
108-10-1
Styrene
ND
ug/L
1.0
1
03/12/21 17:26
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 17:26
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/12/21 17:26
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/12/21 17:26
127-18-4
Toluene
ND
ug/L
1.0
1
03/12/21 17:26
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/12/21 17:26
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/12/21 17:26
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/12/21 17:26
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/12/21 17:26
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/12/21 17:26
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/12/21 17:26
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/12/21 17:26
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/12/21 17:26
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/12/21 17:26
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/12/21 17:26
95-47-6
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
03/12/21 17:26
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
03/12/21 17:26
17060-07-0
Toluene-d8 (S)
107
%
70-130
1
03/12/21 17:26
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/11/21 12:18
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
79
%
70-130
1
03/11/21 12:18
17060-07-0
Toluene-d8 (S)
90
%
66-133
1
03/11/21 12:18
2037-26-5
Date: 03/22/2021 05:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
QC Batch: 607051 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92526797001, 92526797002, 92526797003
METHOD BLANK: 3198351 Matrix: Water
Associated Lab Samples: 92526797001, 92526797002, 92526797003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
03/18/2119:54
10.0
03/18/2119:54
5.0
03/18/2119:54
1.0
03/18/2119:54
1.0
03/18/2119:54
5.0
03/18/2119:54
5.0
03/18/2119:54
5.0
03/18/2119:54
5.0
03/18/2119:54
5.0
03/18/2119:54
10.0
03/18/2119:54
5.0
03/18/2119:54
10.0
03/18/2119:54
5.0
03/18/2119:54
10.0
03/18/2119:54
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3198352
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
511
102
80-120
Arsenic
ug/L
500
501
100
80-120
Barium
ug/L
500
499
100
80-120
Beryllium
ug/L
500
511
102
80-120
Cadmium
ug/L
500
513
103
80-120
Chromium
ug/L
500
516
103
80-120
Cobalt
ug/L
500
493
99
80-120
Copper
ug/L
500
524
105
80-120
Lead
ug/L
500
497
99
80-120
Nickel
ug/L
500
512
102
80-120
Selenium
ug/L
500
508
102
80-120
Silver
ug/L
250
253
101
80-120
Thallium
ug/L
500
505
101
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
503
101
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92526797
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3198353
3198354
MS
MSD
92524737001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
505
509
101
102
75-125
1
Arsenic
ug/L
ND
500
500
492
494
98
99
75-125
0
Barium
ug/L
57.9
500
500
537
536
96
96
75-125
0
Beryllium
ug/L
ND
500
500
490
492
98
98
75-125
0
Cadmium
ug/L
ND
500
500
507
510
101
102
75-125
1
Chromium
ug/L
ND
500
500
498
503
99
100
75-125
1
Cobalt
ug/L
6.1
500
500
485
488
96
96
75-125
1
Copper
ug/L
7.8
500
500
504
507
99
100
75-125
1
Lead
ug/L
ND
500
500
489
489
97
97
75-125
0
Nickel
ug/L
ND
500
500
500
503
99
100
75-125
1
Selenium
ug/L
ND
500
500
534
532
107
106
75-125
0
Silver
ug/L
ND
250
250
247
250
99
100
75-125
1
Thallium
ug/L
ND
500
500
486
487
97
97
75-125
0
Vanadium
ug/L
ND
500
500
474
478
95
96
75-125
1
Zinc
ug/L
33.4
500
500
532
534
100
100
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
QC Batch: 607053 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92526797001, 92526797002, 92526797003
METHOD BLANK: 3198359
Matrix:
Water
Associated Lab Samples: 92526797001, 92526797002, 92526797003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
03/19/2115:25
LABORATORY CONTROL SAMPLE:
3198360
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
9.6
96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3198361 3198362
MS MSD
92526916001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 11.0 10.7 110 107 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
QC Batch: 606051 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526797001, 92526797002, 92526797003
METHOD BLANK: 3193053 Matrix:
Associated Lab Samples: 92526797001, 92526797002, 92526797003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1,1-Trichloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1,2-Trichloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1-Dichloroethane
ug/L
ND
1.0
03/12/21 12:56
1,1-Dichloroethene
ug/L
ND
1.0
03/12/21 12:56
1,2,3-Trichloropropane
ug/L
ND
1.0
03/12/21 12:56
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
03/12/21 12:56
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/12/21 12:56
1,2-Dichlorobenzene
ug/L
ND
1.0
03/12/21 12:56
1,2-Dichloroethane
ug/L
ND
1.0
03/12/21 12:56
1,2-Dichloropropane
ug/L
ND
1.0
03/12/21 12:56
1,4-Dichlorobenzene
ug/L
ND
1.0
03/12/21 12:56
2-Butanone (MEK)
ug/L
ND
5.0
03/12/21 12:56
2-Hexanone
ug/L
ND
5.0
03/12/21 12:56
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/12/21 12:56
Acetone
ug/L
ND
25.0
03/12/21 12:56
Acrylonitrile
ug/L
ND
10.0
03/12/21 12:56
Benzene
ug/L
ND
1.0
03/12/21 12:56
Bromochloromethane
ug/L
ND
1.0
03/12/21 12:56
Bromodichloromethane
ug/L
ND
1.0
03/12/21 12:56
Bromoform
ug/L
ND
1.0
03/12/21 12:56
Bromomethane
ug/L
ND
2.0
03/12/21 12:56 IK,v2
Carbon disulfide
ug/L
ND
2.0
03/12/21 12:56
Carbon tetrachloride
ug/L
ND
1.0
03/12/21 12:56
Chlorobenzene
ug/L
ND
1.0
03/12/21 12:56
Chloroethane
ug/L
ND
1.0
03/12/21 12:56
Chloroform
ug/L
ND
5.0
03/12/21 12:56
Chloromethane
ug/L
ND
1.0
03/12/21 12:56 v2
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/12/21 12:56
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/12/21 12:56
Dibromochloromethane
ug/L
ND
1.0
03/12/21 12:56
Dibromomethane
ug/L
ND
1.0
03/12/21 12:56
Ethylbenzene
ug/L
ND
1.0
03/12/21 12:56
lodomethane
ug/L
ND
20.0
03/12/21 12:56
m&p-Xylene
ug/L
ND
2.0
03/12/21 12:56
Methylene Chloride
ug/L
ND
5.0
03/12/21 12:56
o-Xylene
ug/L
ND
1.0
03/12/21 12:56
Styrene
ug/L
ND
1.0
03/12/21 12:56
Tetrachloroethene
ug/L
ND
1.0
03/12/21 12:56
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
METHOD BLANK: 3193053 Matrix:
Associated Lab Samples: 92526797001, 92526797002, 92526797003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
03/12/21 12:56
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/12/21 12:56
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/12/21 12:56
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/12/21 12:56
Trichloroethene
ug/L
ND
1.0
03/12/21 12:56
Trichlorofluoromethane
ug/L
ND
1.0
03/12/21 12:56
Vinyl acetate
ug/L
ND
2.0
03/12/21 12:56
Vinyl chloride
ug/L
ND
1.0
03/12/21 12:56
Xylene (Total)
ug/L
ND
1.0
03/12/21 12:56
1,2-Dichloroethane-d4 (S)
%
96
70-130
03/12/21 12:56
4-Bromofluorobenzene (S)
%
102
70-130
03/12/21 12:56
Toluene-d8 (S)
%
107
70-130
03/12/21 12:56
LABORATORY CONTROL SAMPLE: 3193054
Qualifiers
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.3
107
70-130
1,1,1-Trichloroethane
ug/L
50
44.7
89
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
52.1
104
70-130
1,1-Dichloroethane
ug/L
50
45.5
91
70-130
1,1-Dichloroethene
ug/L
50
47.8
96
70-132
1,2,3-Trichloropropane
ug/L
50
49.8
100
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.0
108
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.6
105
70-130
1,2-Dichlorobenzene
ug/L
50
49.4
99
70-130
1,2-Dichloroethane
ug/L
50
45.8
92
70-130
1,2-Dichloropropane
ug/L
50
51.1
102
70-130
1,4-Dichlorobenzene
ug/L
50
48.9
98
70-130
2-Butanone (MEK)
ug/L
100
110
110
70-133
2-Hexanone
ug/L
100
105
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
97.0
97
70-144
Acrylonitrile
ug/L
250
222
89
70-130
Benzene
ug/L
50
47.9
96
70-130
Bromochloromethane
ug/L
50
44.2
88
70-130
Bromodichloromethane
ug/L
50
47.0
94
70-130
Bromoform
ug/L
50
52.8
106
70-131
Bromomethane
ug/L
50
41.2
82
30-177lK,v2
Carbon disulfide
ug/L
50
45.1
90
70-133
Carbon tetrachloride
ug/L
50
46.3
93
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
39.2
78
46-131
Chloroform
ug/L
50
45.1
90
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
LABORATORY CONTROL SAMPLE:
Parameter
3193054
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
39.6
cis-1,2-Dichloroethene
ug/L
50
44.0
cis-1,3-Dichloropropene
ug/L
50
54.2
Dibromochloromethane
ug/L
50
53.4
Dibromomethane
ug/L
50
47.1
Ethylbenzene
ug/L
50
48.7
lodomethane
ug/L
100
102
m&p-Xylene
ug/L
100
96.8
Methylene Chloride
ug/L
50
43.5
o-Xylene
ug/L
50
48.7
Styrene
ug/L
50
49.7
Tetrachloroethene
ug/L
50
47.2
Toluene
ug/L
50
46.4
trans-1,2-Dichloroethene
ug/L
50
44.6
trans- 1,3-Dichloropropene
ug/L
50
53.2
trans-1,4-Dichloro-2-butene
ug/L
50
51.1
Trichloroethene
ug/L
50
49.2
Trichlorofluoromethane
ug/L
50
42.6
Vinyl acetate
ug/L
100
122
Vinyl chloride
ug/L
50
40.6
Xylene (Total)
ug/L
150
146
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
79
49-130 v2
88
70-130
108
70-130
107
70-130
94
70-130
97
70-130
102
47-140
97
70-130
87
68-130
97
70-130
99
70-130
94
70-130
93
70-130
89
70-130
106
70-130
102
25-200
98
70-130
85
61-130
122
70-140
81
59-142
97
70-130
95
70-130
98
70-130
96
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3193055
MS
92527185003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3193056
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.8
23.5
104
118
70-135
12
1,1,1-Trichloroethane
ug/L
ND
20
20
21.3
22.4
106
112
70-148
5
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.0
23.1
100
116
70-131
14
1,1,2-Trichloroethane
ug/L
ND
20
20
21.8
23.5
109
118
70-136
8
1,1-Dichloroethane
ug/L
ND
20
20
20.7
21.4
103
107
70-147
3
1,1-Dichloroethene
ug/L
ND
20
20
22.0
23.0
110
115
70-158
5
1,2,3-Trichloropropane
ug/L
ND
20
20
19.8
22.1
99
110
67-137
11
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.6
21.8
103
109
69-136
6
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
23.5
107
118
70-137
9
1,2-Dichlorobenzene
ug/L
ND
20
20
20.9
22.3
104
112
70-133
7
1,2-Dichloroethane
ug/L
ND
20
20
20.5
21.6
103
108
67-138
5
1,2-Dichloropropane
ug/L
ND
20
20
21.8
23.8
109
119
70-138
9
1,4-Dichlorobenzene
ug/L
ND
20
20
20.9
22.4
104
112
70-133
7
2-Butanone (MEK)
ug/L
ND
40
40
44.6
49.4
112
124
61-147
10
2-Hexanone
ug/L
ND
40
40
40.6
45.5
102
114
67-139
11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
39.8
44.4
100
111
67-136
11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3193055
MS
92527185003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3193056
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
43.8
47.4
110
119
55-159
8
Acrylonitrile
ug/L
ND
100
100
99.3
106
99
106
68-140
7
Benzene
ug/L
ND
20
20
20.8
22.4
104
112
67-150
7
Bromochloromethane
ug/L
ND
20
20
21.1
22.4
106
112
70-146
6
Bromodichloromethane
ug/L
ND
20
20
20.7
22.3
104
112
70-138
7
Bromoform
ug/L
ND
20
20
20.8
22.7
104
114
57-138
9
Bromomethane
ug/L
ND
20
20
21.4
22.6
107
113
10-200
51K
Carbon disulfide
ug/L
ND
20
20
21.9
22.5
109
112
70-152
3
Carbon tetrachloride
ug/L
ND
20
20
21.8
22.8
109
114
70-147
5
Chlorobenzene
ug/L
ND
20
20
21.4
22.8
107
114
70-137
6
Chloroethane
ug/L
ND
20
20
20.2
20.4
101
102
51-166
1
Chloroform
ug/L
ND
20
20
20.2
21.7
101
108
70-144
7
Chloromethane
ug/L
ND
20
20
19.2
20.2
96
101
24-161
5
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
20.9
101
105
67-148
4
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.7
24.4
113
122
70-142
7
Dibromochloromethane
ug/L
ND
20
20
22.2
24.0
111
120
68-138
8
Dibromomethane
ug/L
ND
20
20
21.1
22.8
106
114
70-134
8
Ethylbenzene
ug/L
ND
20
20
21.4
22.8
107
114
68-143
6
lodomethane
ug/L
ND
40
40
40.2
42.5
101
106
20-161
6
m&p-Xylene
ug/L
ND
40
40
42.7
45.5
107
114
53-157
6
Methylene Chloride
ug/L
ND
20
20
19.4
20.1
97
100
64-148
3
o-Xylene
ug/L
ND
20
20
21.8
22.7
109
114
68-143
4
Styrene
ug/L
ND
20
20
21.9
23.1
109
115
70-136
6
Tetrachloroethene
ug/L
ND
20
20
20.7
22.1
104
110
70-139
6
Toluene
ug/L
ND
20
20
20.9
22.1
104
111
47-157
6
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.4
21.6
102
108
70-149
5
trans- 1,3-Dichloropropene
ug/L
ND
20
20
22.1
24.1
110
120
70-138
9
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
20.3
23.0
102
115
31-145
12
Trichloroethene
ug/L
ND
20
20
22.0
23.4
110
117
70-149
6
Trichlorofluoromethane
ug/L
ND
20
20
20.4
21.1
102
106
61-154
3
Vinyl acetate
ug/L
ND
40
40
45.7
50.5
114
126
48-156
10
Vinyl chloride
ug/L
ND
20
20
18.7
19.4
93
97
55-172
4
Xylene (Total)
ug/L
ND
60
60
64.5
68.2
107
114
66-145
6
1,2-Dichloroethane-d4 (S)
%
99
97
70-130
4-Bromofluorobenzene (S)
%
104
103
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
QC Batch: 605885 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92526797001, 92526797002, 92526797003
METHOD BLANK: 3191963
Matrix:
Water
Associated Lab Samples:
92526797001, 92526797002, 92526797003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
03/11/21 10:44
1,2-Dichloroethane-d4 (S)
%
83
70-130
03/11/21 10:44
Toluene-d8 (S)
%
91
66-133
03/11/21 10:44
LABORATORY CONTROL SAMPLE: 3191964
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 21.2 106 70-130
1,2-Dichloroethane-d4 (S) % 79 70-130
Toluene-d8 (S) % 88 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3191965
3191966
MS
MSD
92526789001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 22.1
20.8 111
104
64-141 6
1,2-Dichloroethane-d4 (S)
%
83
82
70-130
Toluene-d8(S)
%
92
92
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 22

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92526797
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/22/2021 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92526797
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92526797001
HRSW2
EPA 3010A
607051
EPA 6010D
607083
92526797002
HRSW3
EPA 3010A
607051
EPA 6010D
607083
92526797003
HRSW4
EPA 3010A
607051
EPA 6010D
607083
92526797001
HRSW2
EPA 3010A
607053
EPA 6020B
607080
92526797002
HRSW3
EPA 3010A
607053
EPA 6020B
607080
92526797003
HRSW4
EPA 3010A
607053
EPA 6020B
607080
92526797001
HRSW2
EPA 8260D
606051
92526797002
HRSW3
EPA 8260D
606051
92526797003
HRSW4
EPA 8260D
606051
92526797001
HRSW2
EPA 8260D Mod.
605885
92526797002
HRSW3
EPA 8260D Mod.
605885
92526797003
HRSW4
EPA 8260D Mod.
605885
Date: 03/22/2021 05:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 22

Document Name:
Document Revised: October 28, 2020
,� �ceAnalytical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[] Atlanta[] Kernersville❑
Sample Condition Client Name:Upon Receipt 925
llllll�ll 2679
Courier: ❑fed Ex ❑UP ❑USPS �lient I/VI/ ❑ Commercial ❑Pace ❑Other: 92526797 r f 1J
Custody Seal Present? ❑Yes N4 Seals Intact? []Yes [lo
` Date/Initials Person Examining Contents: V �.
Packing Materlak ❑Bubble Wrap ❑Bubble Bags None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes []No
Net []Blue ❑None
_RIR Gun ID: Type of Ice:
Correction Factor;
Cooler Temp: Add/Subtract i"Cj 0.0`C Temp should be above freezing to 6°C
❑Samples out of temp criteria. Sampleson ice, cooling process
Cooler Temp Corrected (°C): Q . i has begun
USDA Regulated Soil ,(ZN/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check mapsl? Did samples originate from a foreign source [internationally,
FlYes FNr, inrl—lin2 Hawaii and Puerto Rica]? nVes FINo
Comments/Discrepancy;
Chain of Custody Present?
Yes
ONO
[--]N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
❑N/A
Z.
es
a
es
Sufficient volume?
Yes
ONO
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
es
s
[:]No
ONO
N/A
❑N/A
G.
Containers Intact?
2TYes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
eN.
❑N/A
a.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Yes
❑No
❑N/A
9.
Headspace in VOA Vials 1>5.6mmi?
❑Yes
o
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Oyes
❑Yes
RNo
DNo
❑N/A
aNJA
11.
COMMENTS/5AMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Lot ID of Wit Containers:
Field Data Required? ❑Yes [:]No
Project Manager SCURF Review;
Date:
Project Manager SRF Review: Date: Page 20 of 22

Analytical'
Document Name:
Condition Upon Recei
Document No.:
F-CAR-CS-033-Rev.07
Document Revised: October 28, 2020
Page 2 of 2
Issuing Authority:
Pace Carolinas Qualitv Office
*Check mark top half of box if pH and/or dechlorination is Project Al ��� f 92526797
verified and within the acceptance range for preservation
samples. PM: MWB Due Date: 03/24/21
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 92-MECK CO
**Bottom half of box is to list number of bottles
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pH Adjustment Log for Preserved Samples
Sample Ill
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preseruatior
adjusted
Amount of Preservative
added
Lot 9
Out of hold. Incorrect preservative, out of temp, incorrect containers. I
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