19059_Stork Rotary_Env Sampling Letter Report with Lab Results_09.17.2020

September 17, 2020

Mr. Graham M. Andres, P.E., P. Eng.
No Bull Properties, LLC
326 Tryon Road
Raleigh, North Carolina 27603

Re: Letter Report of Environmental Sampling
3201 Rotary Drive
Charlotte, Mecklenburg County, North Carolina
TEP Project No. 246684

Dear Mr. Andres:
On August 13, 2020 Tower Engineering Professionals (TEP) visited the above referenced site (the subject
property) to collect soil and groundwater samples as part of a potential commercial real-estate
transaction. TEP generally collected soil samples in areas of proposed future development for parking
areas/laydown yards. Groundwater samples were collected from existing on-site monitoring wells. It is
TEPs understanding that the monitoring wells are associated with historical groundwater investigations
associated with solvent contamination (PCE); the subject property is a known brownfield. All samples
were analyzed for volatile organic compounds (VOCs) and Resources Conservation and Recovery (RCRA)
metals.
Groundwater samples MW-101 and MW-102 were collected from existing flush-mounted groundwater
wells located in a cleared, grassy area on the northern portion of the subject property. No VOCs were
detected in MW-102; however, barium was detected at a concentration of 80.4 ug/L, which is below the
NC 2L Groundwater Standard of 700 ug/L. PCE was detected at a concentration of 20.5 ug/L in MW-101,
which is above the NC 2L Groundwater Standard of 0.7 ug/L. Barium was also detected in MW-101 at a
concentration of 59.8, which is below the NC 2L Groundwater Standard of 700.
Soil samples HA-1 (2-4), HA-2 (0-2), and HA-3 (0-2) were collected using hand auger methods from a
wooded area on the northern portion of the subject property. This area is planned to be utilized for future
parking/laydown yard. Soil samples HA-4 (3-4) and HA-5 (3-4) were collected using hand auger methods
from a cleared grassy area on the southern portion of the subject property where a potential septic drain
field is presumably located. All soil sample results were below NC Preliminary Soil Remediation Goals
(PSRG) – Protection of Groundwater Standards and/or natural background levels, with the exception of
HA-1 (2-4) which detected chromium at a concentration of 68.6 mg/kg, which is below the NC Soil
Hazardous Waste Limit of 100 mg/kg; this soil can be disposed in a Subtitle D Landfill.

REPORT LIMITATIONS
These services have been performed in accordance with generally accepted environmental and
hydrogeological practices. No other warranty, expressed or implied, is made. As with any subsurface
investigation, actual conditions exist only at the precise locations from which samples were taken.
Certain inferences are based on the results of sampling and related testing to form a professional
opinion of conditions in areas beyond those from which samples were taken. Our conclusions and
recommendations are based upon information provided to us by others, our sampling and testing
results and our site observations. We have not verified the completeness or accuracy of the information
provided by others, unless otherwise noted. Our observations are based upon conditions readily visible
at the subject property at the time of our site visits.
TEP by virtue of providing the services described in this report, does not assume the responsibility of the
person(s) in charge of the subject property, or otherwise undertake responsibility for reporting to any
local, state or federal public agencies any conditions at the subject property that may present a potential
danger to public health, safety or the environment. In areas that require notification of local, state, or
federal public agencies as required by law, it is the Client or subject property owner's responsibility to so
notify.
If you have any questions/comments or require further information, please do not hesitate to contact
the undersigned at [phone].

Respectfully submitted,
Tower Engineering Professionals

Clint E. Sorrell, P.G.
Environmental Project Manager

Attachments: Result Tables
Soil and Groundwater Sampling Locations

VOCSBoring IDDate SampledStatic Water Level (ft) Tetrachloroethylene (PCE) Arsenic Barium Cadmium Chromium Lead Selenium SilverMercury12/31/2013 26.2729NA NA NA NA NA NA NA NA8/13/202023.220.5ND 59.8 ND ND ND ND ND ND12/31/201924.57NDNA NA NA NA NA NA NA NA8/13/202020.1NDND 80.4 ND ND ND ND ND ND0.710 700 2 10 15 20 20 1NotesND: Not Detected NA: Not Analyzed Results reported in ug/LBold: Exceeds NC Groundwater StandardBoring ID (depth')Date Sampledp‐Isopropyltoluene Tetrachloroethylene (PCE) Arsenic Barium Cadmium Chromium Lead Selenium SilverMercuryHA‐1 (2‐4)NDND2.9 54.3 ND68.64.8 0.96 ND 0.015HA‐2 (0‐2)26.4 ug/kgND2.4 54.6 ND 6.2 2.8 ND ND 0.0097HA‐3 (0‐2)NDND5 93.9 ND 37.2 3.6 ND ND 0.035HA‐4 (3‐4)NDND2.3 13.5 ND 4.4 2.5 ND ND 0.039HA‐5 (3‐4)4.1 55.8 ND ND 6.8 ND ND 0.012NSE173 47,000200 6.5 800 1,200 1,200 9.7NSE0.0063 5.8 580 3 3.8 250 2.1 3.4 1NSE82 0.68 3,100 14 0.31 250 78 78 2.3Notes:Results reported in mg/kg unless otherwise statedNSE ‐ No Standard ExistsND: Not Detected Bold: Exceeds NCDENR‐DWQ Natural Background LevelsMW‐101MW‐102NC Groundwater StandardRCRA MetalsGroundwater Sampling Results Soil Sampling ResultsVOCSRCRA Metals8/13/2020NC Preliminary Soil Remedation Goals (INDUSTRIAL)NC Preliminary Soil Remediaiton Goals (PROTECTION OF GW)NC Preliminary Soil Remedation Goals (RESIDENTIAL)NCDENR ‐ DWQ Groundwater Section Mooresville Region Metals Study (NATURAL BACKGROUND LEVELS)NSENSENSE NSE 0‐0.160‐23 4.1‐420 0.54‐4.9 2.0‐56 7.2‐50
TEP Sampling Locations
400 ft
N➤➤N
© 2020 Google
© 2020 Google
© 2020 Google
#=CL#
August 24, 2020
LIMS USE: FR - CLINT SORRELL
LIMS OBJECT ID: 92490828
92490828
Project:
Pace Project No.:
RE:
Clint Sorrell
Tower Engineering Professionals, Inc
326 Tryon Road
Raleigh, NC 27603
Rotary Drive
Dear Clint Sorrell:
Enclosed are the analytical results for sample(s) received by the laboratory on August 14, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Amanda Payne
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 41
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92490828
Rotary Drive
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 41
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92490828
Rotary Drive
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92490828001 MW-101 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-ASOO
EPA 8260D 71 PASI-CCL
92490828002 MW-102 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-ASOO
EPA 8260D 71 PASI-CCL
92490828003 HA-1 (2-4)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
92490828004 HA-2 (0-2)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
92490828005 HA-3 (0-2)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
92490828006 HA-4 (3-4)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
92490828007 HA-5 (3-4)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:MW-101 Lab ID:92490828001 Collected:08/13/20 12:20 Received:08/14/20 08:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 08/18/20 21:01 7440-38-208/18/20 02:1110.0 1
Barium 59.8 ug/L 08/18/20 21:01 7440-39-308/18/20 02:115.0 1
Cadmium ND ug/L 08/18/20 21:01 7440-43-908/18/20 02:111.0 1
Chromium ND ug/L 08/18/20 21:01 7440-47-308/18/20 02:115.0 1
Lead ND ug/L 08/18/20 21:01 7439-92-108/18/20 02:115.0 1
Selenium ND ug/L 08/18/20 21:01 7782-49-208/18/20 02:1110.0 1
Silver ND ug/L 08/18/20 21:01 7440-22-408/18/20 02:115.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 08/18/20 12:25 7439-97-608/17/20 17:190.20 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
Acetone ND ug/L 08/21/20 05:24 67-64-125.0 1
Benzene ND ug/L 08/21/20 05:24 71-43-25.0 1
Bromobenzene ND ug/L 08/21/20 05:24 108-86-15.0 1
Bromochloromethane ND ug/L 08/21/20 05:24 74-97-55.0 1
Bromodichloromethane ND ug/L 08/21/20 05:24 75-27-45.0 1
Bromoform ND ug/L 08/21/20 05:24 75-25-25.0 1
Bromomethane ND ug/L 08/21/20 05:24 74-83-9 IK10.0 1
2-Butanone (MEK)ND ug/L 08/21/20 05:24 78-93-3 IK10.0 1
tert-Butyl Alcohol ND ug/L 08/21/20 05:24 75-65-01001
n-Butylbenzene ND ug/L 08/21/20 05:24 104-51-85.0 1
sec-Butylbenzene ND ug/L 08/21/20 05:24 135-98-85.0 1
tert-Butylbenzene ND ug/L 08/21/20 05:24 98-06-65.0 1
Carbon tetrachloride ND ug/L 08/21/20 05:24 56-23-55.0 1
Chlorobenzene ND ug/L 08/21/20 05:24 108-90-75.0 1
Chloroethane ND ug/L 08/21/20 05:24 75-00-3 v210.0 1
Chloroform ND ug/L 08/21/20 05:24 67-66-35.0 1
Chloromethane ND ug/L 08/21/20 05:24 74-87-35.0 1
2-Chlorotoluene ND ug/L 08/21/20 05:24 95-49-85.0 1
4-Chlorotoluene ND ug/L 08/21/20 05:24 106-43-45.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/21/20 05:24 96-12-85.0 1
Dibromochloromethane ND ug/L 08/21/20 05:24 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/21/20 05:24 106-93-45.0 1
Dibromomethane ND ug/L 08/21/20 05:24 74-95-35.0 1
1,2-Dichlorobenzene ND ug/L 08/21/20 05:24 95-50-15.0 1
1,3-Dichlorobenzene ND ug/L 08/21/20 05:24 541-73-15.0 1
1,4-Dichlorobenzene ND ug/L 08/21/20 05:24 106-46-75.0 1
Dichlorodifluoromethane ND ug/L 08/21/20 05:24 75-71-8 v25.0 1
1,1-Dichloroethane ND ug/L 08/21/20 05:24 75-34-35.0 1
1,2-Dichloroethane ND ug/L 08/21/20 05:24 107-06-25.0 1
1,2-Dichloroethene (Total)ND ug/L 08/21/20 05:24 540-59-05.0 1
1,1-Dichloroethene ND ug/L 08/21/20 05:24 75-35-45.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:MW-101 Lab ID:92490828001 Collected:08/13/20 12:20 Received:08/14/20 08:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
cis-1,2-Dichloroethene ND ug/L 08/21/20 05:24 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/L 08/21/20 05:24 156-60-55.0 1
1,2-Dichloropropane ND ug/L 08/21/20 05:24 78-87-55.0 1
1,3-Dichloropropane ND ug/L 08/21/20 05:24 142-28-95.0 1
2,2-Dichloropropane ND ug/L 08/21/20 05:24 594-20-75.0 1
1,1-Dichloropropene ND ug/L 08/21/20 05:24 563-58-65.0 1
cis-1,3-Dichloropropene ND ug/L 08/21/20 05:24 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/L 08/21/20 05:24 10061-02-65.0 1
Diisopropyl ether ND ug/L 08/21/20 05:24 108-20-35.0 1
Ethylbenzene ND ug/L 08/21/20 05:24 100-41-45.0 1
Hexachloro-1,3-butadiene ND ug/L 08/21/20 05:24 87-68-35.0 1
2-Hexanone ND ug/L 08/21/20 05:24 591-78-610.0 1
Isopropylbenzene (Cumene)ND ug/L 08/21/20 05:24 98-82-85.0 1
p-Isopropyltoluene ND ug/L 08/21/20 05:24 99-87-65.0 1
Methylene Chloride ND ug/L 08/21/20 05:24 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/21/20 05:24 108-10-110.0 1
Methyl-tert-butyl ether ND ug/L 08/21/20 05:24 1634-04-45.0 1
Naphthalene ND ug/L 08/21/20 05:24 91-20-35.0 1
n-Propylbenzene ND ug/L 08/21/20 05:24 103-65-15.0 1
Styrene ND ug/L 08/21/20 05:24 100-42-55.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/21/20 05:24 630-20-65.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/21/20 05:24 79-34-55.0 1
Tetrachloroethene 20.5 ug/L 08/21/20 05:24 127-18-45.0 1
Toluene ND ug/L 08/21/20 05:24 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/L 08/21/20 05:24 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/L 08/21/20 05:24 120-82-15.0 1
1,1,1-Trichloroethane ND ug/L 08/21/20 05:24 71-55-65.0 1
1,1,2-Trichloroethane ND ug/L 08/21/20 05:24 79-00-55.0 1
Trichloroethene ND ug/L 08/21/20 05:24 79-01-65.0 1
Trichlorofluoromethane ND ug/L 08/21/20 05:24 75-69-410.0 1
1,2,3-Trichloropropane ND ug/L 08/21/20 05:24 96-18-45.0 1
1,2,4-Trimethylbenzene ND ug/L 08/21/20 05:24 95-63-65.0 1
1,3,5-Trimethylbenzene ND ug/L 08/21/20 05:24 108-67-85.0 1
Vinyl acetate ND ug/L 08/21/20 05:24 108-05-4 IK10.0 1
Vinyl chloride ND ug/L 08/21/20 05:24 75-01-45.0 1
m&p-Xylene ND ug/L 08/21/20 05:24 179601-23-110.0 1
o-Xylene ND ug/L 08/21/20 05:24 95-47-65.0 1
Surrogates
4-Bromofluorobenzene (S)101 %08/21/20 05:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)84 %08/21/20 05:24 17060-07-070-130 1
Toluene-d8 (S)105 %08/21/20 05:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:MW-102 Lab ID:92490828002 Collected:08/13/20 12:30 Received:08/14/20 08:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 08/18/20 21:14 7440-38-208/18/20 02:1110.0 1
Barium 80.4 ug/L 08/18/20 21:14 7440-39-308/18/20 02:115.0 1
Cadmium ND ug/L 08/18/20 21:14 7440-43-908/18/20 02:111.0 1
Chromium ND ug/L 08/18/20 21:14 7440-47-308/18/20 02:115.0 1
Lead ND ug/L 08/18/20 21:14 7439-92-108/18/20 02:115.0 1
Selenium ND ug/L 08/18/20 21:14 7782-49-208/18/20 02:1110.0 1
Silver ND ug/L 08/18/20 21:14 7440-22-408/18/20 02:115.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 08/18/20 12:28 7439-97-608/17/20 17:190.20 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
Acetone ND ug/L 08/21/20 05:43 67-64-125.0 1
Benzene ND ug/L 08/21/20 05:43 71-43-25.0 1
Bromobenzene ND ug/L 08/21/20 05:43 108-86-15.0 1
Bromochloromethane ND ug/L 08/21/20 05:43 74-97-55.0 1
Bromodichloromethane ND ug/L 08/21/20 05:43 75-27-45.0 1
Bromoform ND ug/L 08/21/20 05:43 75-25-25.0 1
Bromomethane ND ug/L 08/21/20 05:43 74-83-9 IK10.0 1
2-Butanone (MEK)ND ug/L 08/21/20 05:43 78-93-3 IK10.0 1
tert-Butyl Alcohol ND ug/L 08/21/20 05:43 75-65-01001
n-Butylbenzene ND ug/L 08/21/20 05:43 104-51-85.0 1
sec-Butylbenzene ND ug/L 08/21/20 05:43 135-98-85.0 1
tert-Butylbenzene ND ug/L 08/21/20 05:43 98-06-65.0 1
Carbon tetrachloride ND ug/L 08/21/20 05:43 56-23-55.0 1
Chlorobenzene ND ug/L 08/21/20 05:43 108-90-75.0 1
Chloroethane ND ug/L 08/21/20 05:43 75-00-3 v210.0 1
Chloroform ND ug/L 08/21/20 05:43 67-66-35.0 1
Chloromethane ND ug/L 08/21/20 05:43 74-87-35.0 1
2-Chlorotoluene ND ug/L 08/21/20 05:43 95-49-85.0 1
4-Chlorotoluene ND ug/L 08/21/20 05:43 106-43-45.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/21/20 05:43 96-12-85.0 1
Dibromochloromethane ND ug/L 08/21/20 05:43 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/21/20 05:43 106-93-45.0 1
Dibromomethane ND ug/L 08/21/20 05:43 74-95-35.0 1
1,2-Dichlorobenzene ND ug/L 08/21/20 05:43 95-50-15.0 1
1,3-Dichlorobenzene ND ug/L 08/21/20 05:43 541-73-15.0 1
1,4-Dichlorobenzene ND ug/L 08/21/20 05:43 106-46-75.0 1
Dichlorodifluoromethane ND ug/L 08/21/20 05:43 75-71-8 v25.0 1
1,1-Dichloroethane ND ug/L 08/21/20 05:43 75-34-35.0 1
1,2-Dichloroethane ND ug/L 08/21/20 05:43 107-06-25.0 1
1,2-Dichloroethene (Total)ND ug/L 08/21/20 05:43 540-59-05.0 1
1,1-Dichloroethene ND ug/L 08/21/20 05:43 75-35-45.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:MW-102 Lab ID:92490828002 Collected:08/13/20 12:30 Received:08/14/20 08:01 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
cis-1,2-Dichloroethene ND ug/L 08/21/20 05:43 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/L 08/21/20 05:43 156-60-55.0 1
1,2-Dichloropropane ND ug/L 08/21/20 05:43 78-87-55.0 1
1,3-Dichloropropane ND ug/L 08/21/20 05:43 142-28-95.0 1
2,2-Dichloropropane ND ug/L 08/21/20 05:43 594-20-75.0 1
1,1-Dichloropropene ND ug/L 08/21/20 05:43 563-58-65.0 1
cis-1,3-Dichloropropene ND ug/L 08/21/20 05:43 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/L 08/21/20 05:43 10061-02-65.0 1
Diisopropyl ether ND ug/L 08/21/20 05:43 108-20-35.0 1
Ethylbenzene ND ug/L 08/21/20 05:43 100-41-45.0 1
Hexachloro-1,3-butadiene ND ug/L 08/21/20 05:43 87-68-35.0 1
2-Hexanone ND ug/L 08/21/20 05:43 591-78-610.0 1
Isopropylbenzene (Cumene)ND ug/L 08/21/20 05:43 98-82-85.0 1
p-Isopropyltoluene ND ug/L 08/21/20 05:43 99-87-65.0 1
Methylene Chloride ND ug/L 08/21/20 05:43 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/21/20 05:43 108-10-110.0 1
Methyl-tert-butyl ether ND ug/L 08/21/20 05:43 1634-04-45.0 1
Naphthalene ND ug/L 08/21/20 05:43 91-20-35.0 1
n-Propylbenzene ND ug/L 08/21/20 05:43 103-65-15.0 1
Styrene ND ug/L 08/21/20 05:43 100-42-55.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/21/20 05:43 630-20-65.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/21/20 05:43 79-34-55.0 1
Tetrachloroethene ND ug/L 08/21/20 05:43 127-18-45.0 1
Toluene ND ug/L 08/21/20 05:43 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/L 08/21/20 05:43 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/L 08/21/20 05:43 120-82-15.0 1
1,1,1-Trichloroethane ND ug/L 08/21/20 05:43 71-55-65.0 1
1,1,2-Trichloroethane ND ug/L 08/21/20 05:43 79-00-55.0 1
Trichloroethene ND ug/L 08/21/20 05:43 79-01-65.0 1
Trichlorofluoromethane ND ug/L 08/21/20 05:43 75-69-410.0 1
1,2,3-Trichloropropane ND ug/L 08/21/20 05:43 96-18-45.0 1
1,2,4-Trimethylbenzene ND ug/L 08/21/20 05:43 95-63-65.0 1
1,3,5-Trimethylbenzene ND ug/L 08/21/20 05:43 108-67-85.0 1
Vinyl acetate ND ug/L 08/21/20 05:43 108-05-4 IK10.0 1
Vinyl chloride ND ug/L 08/21/20 05:43 75-01-45.0 1
m&p-Xylene ND ug/L 08/21/20 05:43 179601-23-110.0 1
o-Xylene ND ug/L 08/21/20 05:43 95-47-65.0 1
Surrogates
4-Bromofluorobenzene (S)100 %08/21/20 05:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %08/21/20 05:43 17060-07-070-130 1
Toluene-d8 (S)104 %08/21/20 05:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-1 (2-4)Lab ID:92490828003 Collected:08/13/20 13:15 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.9 mg/kg 08/17/20 22:47 7440-38-208/17/20 07:510.87 1
Barium 54.3 mg/kg 08/17/20 22:47 7440-39-308/17/20 07:510.43 1
Cadmium ND mg/kg 08/17/20 22:47 7440-43-908/17/20 07:510.087 1
Chromium 68.6 mg/kg 08/17/20 22:47 7440-47-308/17/20 07:510.43 1
Lead 4.8 mg/kg 08/17/20 22:47 7439-92-108/17/20 07:510.43 1
Selenium 0.96 mg/kg 08/17/20 22:47 7782-49-208/17/20 07:510.87 1
Silver ND mg/kg 08/17/20 22:47 7440-22-408/17/20 07:510.43 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.015 mg/kg 08/17/20 15:18 7439-97-608/17/20 10:210.0057 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/20 17:56 67-64-108/19/20 12:261971
Benzene ND ug/kg 08/19/20 17:56 71-43-208/19/20 12:269.8 1
Bromobenzene ND ug/kg 08/19/20 17:56 108-86-108/19/20 12:269.8 1
Bromochloromethane ND ug/kg 08/19/20 17:56 74-97-5 IK08/19/20 12:269.8 1
Bromodichloromethane ND ug/kg 08/19/20 17:56 75-27-408/19/20 12:269.8 1
Bromoform ND ug/kg 08/19/20 17:56 75-25-208/19/20 12:269.8 1
Bromomethane ND ug/kg 08/19/20 17:56 74-83-9 v108/19/20 12:2619.7 1
2-Butanone (MEK)ND ug/kg 08/19/20 17:56 78-93-308/19/20 12:261971
n-Butylbenzene ND ug/kg 08/19/20 17:56 104-51-808/19/20 12:269.8 1
sec-Butylbenzene ND ug/kg 08/19/20 17:56 135-98-808/19/20 12:269.8 1
tert-Butylbenzene ND ug/kg 08/19/20 17:56 98-06-608/19/20 12:269.8 1
Carbon tetrachloride ND ug/kg 08/19/20 17:56 56-23-508/19/20 12:269.8 1
Chlorobenzene ND ug/kg 08/19/20 17:56 108-90-708/19/20 12:269.8 1
Chloroethane ND ug/kg 08/19/20 17:56 75-00-308/19/20 12:2619.7 1
Chloroform ND ug/kg 08/19/20 17:56 67-66-308/19/20 12:269.8 1
Chloromethane ND ug/kg 08/19/20 17:56 74-87-308/19/20 12:2619.7 1
2-Chlorotoluene ND ug/kg 08/19/20 17:56 95-49-808/19/20 12:269.8 1
4-Chlorotoluene ND ug/kg 08/19/20 17:56 106-43-408/19/20 12:269.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/20 17:56 96-12-808/19/20 12:269.8 1
Dibromochloromethane ND ug/kg 08/19/20 17:56 124-48-108/19/20 12:269.8 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/20 17:56 106-93-408/19/20 12:269.8 1
Dibromomethane ND ug/kg 08/19/20 17:56 74-95-308/19/20 12:269.8 1
1,2-Dichlorobenzene ND ug/kg 08/19/20 17:56 95-50-108/19/20 12:269.8 1
1,3-Dichlorobenzene ND ug/kg 08/19/20 17:56 541-73-108/19/20 12:269.8 1
1,4-Dichlorobenzene ND ug/kg 08/19/20 17:56 106-46-708/19/20 12:269.8 1
Dichlorodifluoromethane ND ug/kg 08/19/20 17:56 75-71-808/19/20 12:2619.7 1
1,1-Dichloroethane ND ug/kg 08/19/20 17:56 75-34-308/19/20 12:269.8 1
1,2-Dichloroethane ND ug/kg 08/19/20 17:56 107-06-208/19/20 12:269.8 1
1,1-Dichloroethene ND ug/kg 08/19/20 17:56 75-35-408/19/20 12:269.8 1
cis-1,2-Dichloroethene ND ug/kg 08/19/20 17:56 156-59-208/19/20 12:269.8 1
trans-1,2-Dichloroethene ND ug/kg 08/19/20 17:56 156-60-508/19/20 12:269.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-1 (2-4)Lab ID:92490828003 Collected:08/13/20 13:15 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/19/20 17:56 78-87-508/19/20 12:269.8 1
1,3-Dichloropropane ND ug/kg 08/19/20 17:56 142-28-908/19/20 12:269.8 1
2,2-Dichloropropane ND ug/kg 08/19/20 17:56 594-20-708/19/20 12:269.8 1
1,1-Dichloropropene ND ug/kg 08/19/20 17:56 563-58-608/19/20 12:269.8 1
cis-1,3-Dichloropropene ND ug/kg 08/19/20 17:56 10061-01-508/19/20 12:269.8 1
trans-1,3-Dichloropropene ND ug/kg 08/19/20 17:56 10061-02-608/19/20 12:269.8 1
Diisopropyl ether ND ug/kg 08/19/20 17:56 108-20-308/19/20 12:269.8 1
Ethylbenzene ND ug/kg 08/19/20 17:56 100-41-408/19/20 12:269.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/20 17:56 87-68-308/19/20 12:269.8 1
2-Hexanone ND ug/kg 08/19/20 17:56 591-78-608/19/20 12:2698.3 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/20 17:56 98-82-808/19/20 12:269.8 1
p-Isopropyltoluene ND ug/kg 08/19/20 17:56 99-87-608/19/20 12:269.8 1
Methylene Chloride ND ug/kg 08/19/20 17:56 75-09-208/19/20 12:2639.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/20 17:56 108-10-108/19/20 12:2698.3 1
Methyl-tert-butyl ether ND ug/kg 08/19/20 17:56 1634-04-408/19/20 12:269.8 1
Naphthalene ND ug/kg 08/19/20 17:56 91-20-308/19/20 12:269.8 1
n-Propylbenzene ND ug/kg 08/19/20 17:56 103-65-108/19/20 12:269.8 1
Styrene ND ug/kg 08/19/20 17:56 100-42-508/19/20 12:269.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/20 17:56 630-20-608/19/20 12:269.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/20 17:56 79-34-508/19/20 12:269.8 1
Tetrachloroethene ND ug/kg 08/19/20 17:56 127-18-408/19/20 12:269.8 1
Toluene ND ug/kg 08/19/20 17:56 108-88-308/19/20 12:269.8 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/20 17:56 87-61-608/19/20 12:269.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/20 17:56 120-82-108/19/20 12:269.8 1
1,1,1-Trichloroethane ND ug/kg 08/19/20 17:56 71-55-608/19/20 12:269.8 1
1,1,2-Trichloroethane ND ug/kg 08/19/20 17:56 79-00-508/19/20 12:269.8 1
Trichloroethene ND ug/kg 08/19/20 17:56 79-01-608/19/20 12:269.8 1
Trichlorofluoromethane ND ug/kg 08/19/20 17:56 75-69-408/19/20 12:269.8 1
1,2,3-Trichloropropane ND ug/kg 08/19/20 17:56 96-18-408/19/20 12:269.8 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/20 17:56 95-63-608/19/20 12:269.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/20 17:56 108-67-808/19/20 12:269.8 1
Vinyl acetate ND ug/kg 08/19/20 17:56 108-05-408/19/20 12:2698.3 1
Vinyl chloride ND ug/kg 08/19/20 17:56 75-01-408/19/20 12:2619.7 1
Xylene (Total)ND ug/kg 08/19/20 17:56 1330-20-708/19/20 12:2619.7 1
m&p-Xylene ND ug/kg 08/19/20 17:56 179601-23-108/19/20 12:2619.7 1
o-Xylene ND ug/kg 08/19/20 17:56 95-47-608/19/20 12:269.8 1
Surrogates
Toluene-d8 (S)99 %08/19/20 17:56 2037-26-508/19/20 12:2670-130 1
4-Bromofluorobenzene (S)100 %08/19/20 17:56 460-00-408/19/20 12:2670-130 1
1,2-Dichloroethane-d4 (S)95 %08/19/20 17:56 17060-07-008/19/20 12:2670-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.1 %08/17/20 16:000.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-2 (0-2)Lab ID:92490828004 Collected:08/13/20 13:20 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.4 mg/kg 08/17/20 22:50 7440-38-208/17/20 07:510.78 1
Barium 54.6 mg/kg 08/17/20 22:50 7440-39-308/17/20 07:510.39 1
Cadmium ND mg/kg 08/17/20 22:50 7440-43-908/17/20 07:510.078 1
Chromium 6.2 mg/kg 08/17/20 22:50 7440-47-308/17/20 07:510.39 1
Lead 2.8 mg/kg 08/17/20 22:50 7439-92-108/17/20 07:510.39 1
Selenium ND mg/kg 08/17/20 22:50 7782-49-208/17/20 07:510.78 1
Silver ND mg/kg 08/17/20 22:50 7440-22-408/17/20 07:510.39 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.0097 mg/kg 08/17/20 15:25 7439-97-608/17/20 10:210.0053 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/20 18:15 67-64-108/19/20 12:261991
Benzene ND ug/kg 08/19/20 18:15 71-43-208/19/20 12:26101
Bromobenzene ND ug/kg 08/19/20 18:15 108-86-108/19/20 12:26101
Bromochloromethane ND ug/kg 08/19/20 18:15 74-97-5 IK08/19/20 12:26101
Bromodichloromethane ND ug/kg 08/19/20 18:15 75-27-408/19/20 12:26101
Bromoform ND ug/kg 08/19/20 18:15 75-25-208/19/20 12:26101
Bromomethane ND ug/kg 08/19/20 18:15 74-83-9 v108/19/20 12:2619.9 1
2-Butanone (MEK)ND ug/kg 08/19/20 18:15 78-93-308/19/20 12:261991
n-Butylbenzene ND ug/kg 08/19/20 18:15 104-51-808/19/20 12:26101
sec-Butylbenzene ND ug/kg 08/19/20 18:15 135-98-808/19/20 12:26101
tert-Butylbenzene ND ug/kg 08/19/20 18:15 98-06-608/19/20 12:26101
Carbon tetrachloride ND ug/kg 08/19/20 18:15 56-23-508/19/20 12:26101
Chlorobenzene ND ug/kg 08/19/20 18:15 108-90-708/19/20 12:26101
Chloroethane ND ug/kg 08/19/20 18:15 75-00-308/19/20 12:2619.9 1
Chloroform ND ug/kg 08/19/20 18:15 67-66-308/19/20 12:26101
Chloromethane ND ug/kg 08/19/20 18:15 74-87-308/19/20 12:2619.9 1
2-Chlorotoluene ND ug/kg 08/19/20 18:15 95-49-808/19/20 12:26101
4-Chlorotoluene ND ug/kg 08/19/20 18:15 106-43-408/19/20 12:26101
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/20 18:15 96-12-808/19/20 12:26101
Dibromochloromethane ND ug/kg 08/19/20 18:15 124-48-108/19/20 12:26101
1,2-Dibromoethane (EDB)ND ug/kg 08/19/20 18:15 106-93-408/19/20 12:26101
Dibromomethane ND ug/kg 08/19/20 18:15 74-95-308/19/20 12:26101
1,2-Dichlorobenzene ND ug/kg 08/19/20 18:15 95-50-108/19/20 12:26101
1,3-Dichlorobenzene ND ug/kg 08/19/20 18:15 541-73-108/19/20 12:26101
1,4-Dichlorobenzene ND ug/kg 08/19/20 18:15 106-46-708/19/20 12:26101
Dichlorodifluoromethane ND ug/kg 08/19/20 18:15 75-71-808/19/20 12:2619.9 1
1,1-Dichloroethane ND ug/kg 08/19/20 18:15 75-34-308/19/20 12:26101
1,2-Dichloroethane ND ug/kg 08/19/20 18:15 107-06-208/19/20 12:26101
1,1-Dichloroethene ND ug/kg 08/19/20 18:15 75-35-408/19/20 12:26101
cis-1,2-Dichloroethene ND ug/kg 08/19/20 18:15 156-59-208/19/20 12:26101
trans-1,2-Dichloroethene ND ug/kg 08/19/20 18:15 156-60-508/19/20 12:26101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-2 (0-2)Lab ID:92490828004 Collected:08/13/20 13:20 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/19/20 18:15 78-87-508/19/20 12:26101
1,3-Dichloropropane ND ug/kg 08/19/20 18:15 142-28-908/19/20 12:26101
2,2-Dichloropropane ND ug/kg 08/19/20 18:15 594-20-708/19/20 12:26101
1,1-Dichloropropene ND ug/kg 08/19/20 18:15 563-58-608/19/20 12:26101
cis-1,3-Dichloropropene ND ug/kg 08/19/20 18:15 10061-01-508/19/20 12:26101
trans-1,3-Dichloropropene ND ug/kg 08/19/20 18:15 10061-02-608/19/20 12:26101
Diisopropyl ether ND ug/kg 08/19/20 18:15 108-20-308/19/20 12:26101
Ethylbenzene ND ug/kg 08/19/20 18:15 100-41-408/19/20 12:26101
Hexachloro-1,3-butadiene ND ug/kg 08/19/20 18:15 87-68-308/19/20 12:26101
2-Hexanone ND ug/kg 08/19/20 18:15 591-78-608/19/20 12:2699.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/20 18:15 98-82-808/19/20 12:26101
p-Isopropyltoluene 26.4 ug/kg 08/19/20 18:15 99-87-608/19/20 12:26101
Methylene Chloride ND ug/kg 08/19/20 18:15 75-09-208/19/20 12:2639.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/20 18:15 108-10-108/19/20 12:2699.5 1
Methyl-tert-butyl ether ND ug/kg 08/19/20 18:15 1634-04-408/19/20 12:26101
Naphthalene ND ug/kg 08/19/20 18:15 91-20-308/19/20 12:26101
n-Propylbenzene ND ug/kg 08/19/20 18:15 103-65-108/19/20 12:26101
Styrene ND ug/kg 08/19/20 18:15 100-42-508/19/20 12:26101
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/20 18:15 630-20-608/19/20 12:26101
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/20 18:15 79-34-508/19/20 12:26101
Tetrachloroethene ND ug/kg 08/19/20 18:15 127-18-408/19/20 12:26101
Toluene ND ug/kg 08/19/20 18:15 108-88-308/19/20 12:26101
1,2,3-Trichlorobenzene ND ug/kg 08/19/20 18:15 87-61-608/19/20 12:26101
1,2,4-Trichlorobenzene ND ug/kg 08/19/20 18:15 120-82-108/19/20 12:26101
1,1,1-Trichloroethane ND ug/kg 08/19/20 18:15 71-55-608/19/20 12:26101
1,1,2-Trichloroethane ND ug/kg 08/19/20 18:15 79-00-508/19/20 12:26101
Trichloroethene ND ug/kg 08/19/20 18:15 79-01-608/19/20 12:26101
Trichlorofluoromethane ND ug/kg 08/19/20 18:15 75-69-408/19/20 12:26101
1,2,3-Trichloropropane ND ug/kg 08/19/20 18:15 96-18-408/19/20 12:26101
1,2,4-Trimethylbenzene ND ug/kg 08/19/20 18:15 95-63-608/19/20 12:26101
1,3,5-Trimethylbenzene ND ug/kg 08/19/20 18:15 108-67-808/19/20 12:26101
Vinyl acetate ND ug/kg 08/19/20 18:15 108-05-408/19/20 12:2699.5 1
Vinyl chloride ND ug/kg 08/19/20 18:15 75-01-408/19/20 12:2619.9 1
Xylene (Total)ND ug/kg 08/19/20 18:15 1330-20-708/19/20 12:2619.9 1
m&p-Xylene ND ug/kg 08/19/20 18:15 179601-23-108/19/20 12:2619.9 1
o-Xylene ND ug/kg 08/19/20 18:15 95-47-608/19/20 12:26101
Surrogates
Toluene-d8 (S)100 %08/19/20 18:15 2037-26-508/19/20 12:2670-130 1
4-Bromofluorobenzene (S)99 %08/19/20 18:15 460-00-408/19/20 12:2670-130 1
1,2-Dichloroethane-d4 (S)96 %08/19/20 18:15 17060-07-008/19/20 12:2670-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.1 %08/17/20 16:000.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-3 (0-2)Lab ID:92490828005 Collected:08/13/20 13:30 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 5.0 mg/kg 08/17/20 22:53 7440-38-208/17/20 07:511.3 1
Barium 93.9 mg/kg 08/17/20 22:53 7440-39-308/17/20 07:510.63 1
Cadmium ND mg/kg 08/17/20 22:53 7440-43-908/17/20 07:510.13 1
Chromium 37.2 mg/kg 08/17/20 22:53 7440-47-308/17/20 07:510.63 1
Lead 3.6 mg/kg 08/17/20 22:53 7439-92-108/17/20 07:510.63 1
Selenium ND mg/kg 08/17/20 22:53 7782-49-208/17/20 07:511.3 1
Silver ND mg/kg 08/17/20 22:53 7440-22-408/17/20 07:510.63 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.035 mg/kg 08/17/20 15:27 7439-97-608/17/20 10:210.0077 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/20 18:33 67-64-108/19/20 12:262761
Benzene ND ug/kg 08/19/20 18:33 71-43-208/19/20 12:2613.8 1
Bromobenzene ND ug/kg 08/19/20 18:33 108-86-108/19/20 12:2613.8 1
Bromochloromethane ND ug/kg 08/19/20 18:33 74-97-5 IK08/19/20 12:2613.8 1
Bromodichloromethane ND ug/kg 08/19/20 18:33 75-27-408/19/20 12:2613.8 1
Bromoform ND ug/kg 08/19/20 18:33 75-25-208/19/20 12:2613.8 1
Bromomethane ND ug/kg 08/19/20 18:33 74-83-9 v108/19/20 12:2627.6 1
2-Butanone (MEK)ND ug/kg 08/19/20 18:33 78-93-308/19/20 12:262761
n-Butylbenzene ND ug/kg 08/19/20 18:33 104-51-808/19/20 12:2613.8 1
sec-Butylbenzene ND ug/kg 08/19/20 18:33 135-98-808/19/20 12:2613.8 1
tert-Butylbenzene ND ug/kg 08/19/20 18:33 98-06-608/19/20 12:2613.8 1
Carbon tetrachloride ND ug/kg 08/19/20 18:33 56-23-508/19/20 12:2613.8 1
Chlorobenzene ND ug/kg 08/19/20 18:33 108-90-708/19/20 12:2613.8 1
Chloroethane ND ug/kg 08/19/20 18:33 75-00-308/19/20 12:2627.6 1
Chloroform ND ug/kg 08/19/20 18:33 67-66-308/19/20 12:2613.8 1
Chloromethane ND ug/kg 08/19/20 18:33 74-87-308/19/20 12:2627.6 1
2-Chlorotoluene ND ug/kg 08/19/20 18:33 95-49-808/19/20 12:2613.8 1
4-Chlorotoluene ND ug/kg 08/19/20 18:33 106-43-408/19/20 12:2613.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/20 18:33 96-12-808/19/20 12:2613.8 1
Dibromochloromethane ND ug/kg 08/19/20 18:33 124-48-108/19/20 12:2613.8 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/20 18:33 106-93-408/19/20 12:2613.8 1
Dibromomethane ND ug/kg 08/19/20 18:33 74-95-308/19/20 12:2613.8 1
1,2-Dichlorobenzene ND ug/kg 08/19/20 18:33 95-50-108/19/20 12:2613.8 1
1,3-Dichlorobenzene ND ug/kg 08/19/20 18:33 541-73-108/19/20 12:2613.8 1
1,4-Dichlorobenzene ND ug/kg 08/19/20 18:33 106-46-708/19/20 12:2613.8 1
Dichlorodifluoromethane ND ug/kg 08/19/20 18:33 75-71-808/19/20 12:2627.6 1
1,1-Dichloroethane ND ug/kg 08/19/20 18:33 75-34-308/19/20 12:2613.8 1
1,2-Dichloroethane ND ug/kg 08/19/20 18:33 107-06-208/19/20 12:2613.8 1
1,1-Dichloroethene ND ug/kg 08/19/20 18:33 75-35-408/19/20 12:2613.8 1
cis-1,2-Dichloroethene ND ug/kg 08/19/20 18:33 156-59-208/19/20 12:2613.8 1
trans-1,2-Dichloroethene ND ug/kg 08/19/20 18:33 156-60-508/19/20 12:2613.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-3 (0-2)Lab ID:92490828005 Collected:08/13/20 13:30 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/19/20 18:33 78-87-508/19/20 12:2613.8 1
1,3-Dichloropropane ND ug/kg 08/19/20 18:33 142-28-908/19/20 12:2613.8 1
2,2-Dichloropropane ND ug/kg 08/19/20 18:33 594-20-708/19/20 12:2613.8 1
1,1-Dichloropropene ND ug/kg 08/19/20 18:33 563-58-608/19/20 12:2613.8 1
cis-1,3-Dichloropropene ND ug/kg 08/19/20 18:33 10061-01-508/19/20 12:2613.8 1
trans-1,3-Dichloropropene ND ug/kg 08/19/20 18:33 10061-02-608/19/20 12:2613.8 1
Diisopropyl ether ND ug/kg 08/19/20 18:33 108-20-308/19/20 12:2613.8 1
Ethylbenzene ND ug/kg 08/19/20 18:33 100-41-408/19/20 12:2613.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/20 18:33 87-68-308/19/20 12:2613.8 1
2-Hexanone ND ug/kg 08/19/20 18:33 591-78-608/19/20 12:261381
Isopropylbenzene (Cumene)ND ug/kg 08/19/20 18:33 98-82-808/19/20 12:2613.8 1
p-Isopropyltoluene ND ug/kg 08/19/20 18:33 99-87-608/19/20 12:2613.8 1
Methylene Chloride ND ug/kg 08/19/20 18:33 75-09-208/19/20 12:2655.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/20 18:33 108-10-108/19/20 12:261381
Methyl-tert-butyl ether ND ug/kg 08/19/20 18:33 1634-04-408/19/20 12:2613.8 1
Naphthalene ND ug/kg 08/19/20 18:33 91-20-308/19/20 12:2613.8 1
n-Propylbenzene ND ug/kg 08/19/20 18:33 103-65-108/19/20 12:2613.8 1
Styrene ND ug/kg 08/19/20 18:33 100-42-508/19/20 12:2613.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/20 18:33 630-20-608/19/20 12:2613.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/20 18:33 79-34-508/19/20 12:2613.8 1
Tetrachloroethene ND ug/kg 08/19/20 18:33 127-18-408/19/20 12:2613.8 1
Toluene ND ug/kg 08/19/20 18:33 108-88-308/19/20 12:2613.8 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/20 18:33 87-61-608/19/20 12:2613.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/20 18:33 120-82-108/19/20 12:2613.8 1
1,1,1-Trichloroethane ND ug/kg 08/19/20 18:33 71-55-608/19/20 12:2613.8 1
1,1,2-Trichloroethane ND ug/kg 08/19/20 18:33 79-00-508/19/20 12:2613.8 1
Trichloroethene ND ug/kg 08/19/20 18:33 79-01-608/19/20 12:2613.8 1
Trichlorofluoromethane ND ug/kg 08/19/20 18:33 75-69-408/19/20 12:2613.8 1
1,2,3-Trichloropropane ND ug/kg 08/19/20 18:33 96-18-408/19/20 12:2613.8 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/20 18:33 95-63-608/19/20 12:2613.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/20 18:33 108-67-808/19/20 12:2613.8 1
Vinyl acetate ND ug/kg 08/19/20 18:33 108-05-408/19/20 12:261381
Vinyl chloride ND ug/kg 08/19/20 18:33 75-01-408/19/20 12:2627.6 1
Xylene (Total)ND ug/kg 08/19/20 18:33 1330-20-708/19/20 12:2627.6 1
m&p-Xylene ND ug/kg 08/19/20 18:33 179601-23-108/19/20 12:2627.6 1
o-Xylene ND ug/kg 08/19/20 18:33 95-47-608/19/20 12:2613.8 1
Surrogates
Toluene-d8 (S)100 %08/19/20 18:33 2037-26-508/19/20 12:2670-130 1
4-Bromofluorobenzene (S)101 %08/19/20 18:33 460-00-408/19/20 12:2670-130 1
1,2-Dichloroethane-d4 (S)98 %08/19/20 18:33 17060-07-008/19/20 12:2670-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.0 %08/17/20 16:000.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-4 (3-4)Lab ID:92490828006 Collected:08/13/20 13:40 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.3 mg/kg 08/17/20 22:56 7440-38-208/17/20 07:510.83 1
Barium 13.5 mg/kg 08/17/20 22:56 7440-39-308/17/20 07:510.42 1
Cadmium ND mg/kg 08/17/20 22:56 7440-43-908/17/20 07:510.083 1
Chromium 4.4 mg/kg 08/17/20 22:56 7440-47-308/17/20 07:510.42 1
Lead 2.5 mg/kg 08/17/20 22:56 7439-92-108/17/20 07:510.42 1
Selenium ND mg/kg 08/17/20 22:56 7782-49-208/17/20 07:510.83 1
Silver ND mg/kg 08/17/20 22:56 7440-22-408/17/20 07:510.42 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.039 mg/kg 08/17/20 15:35 7439-97-608/17/20 10:210.0067 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/20 18:51 67-64-108/19/20 12:261951
Benzene ND ug/kg 08/19/20 18:51 71-43-208/19/20 12:269.8 1
Bromobenzene ND ug/kg 08/19/20 18:51 108-86-108/19/20 12:269.8 1
Bromochloromethane ND ug/kg 08/19/20 18:51 74-97-5 IK08/19/20 12:269.8 1
Bromodichloromethane ND ug/kg 08/19/20 18:51 75-27-408/19/20 12:269.8 1
Bromoform ND ug/kg 08/19/20 18:51 75-25-208/19/20 12:269.8 1
Bromomethane ND ug/kg 08/19/20 18:51 74-83-9 v108/19/20 12:2619.5 1
2-Butanone (MEK)ND ug/kg 08/19/20 18:51 78-93-308/19/20 12:261951
n-Butylbenzene ND ug/kg 08/19/20 18:51 104-51-808/19/20 12:269.8 1
sec-Butylbenzene ND ug/kg 08/19/20 18:51 135-98-808/19/20 12:269.8 1
tert-Butylbenzene ND ug/kg 08/19/20 18:51 98-06-608/19/20 12:269.8 1
Carbon tetrachloride ND ug/kg 08/19/20 18:51 56-23-508/19/20 12:269.8 1
Chlorobenzene ND ug/kg 08/19/20 18:51 108-90-708/19/20 12:269.8 1
Chloroethane ND ug/kg 08/19/20 18:51 75-00-308/19/20 12:2619.5 1
Chloroform ND ug/kg 08/19/20 18:51 67-66-308/19/20 12:269.8 1
Chloromethane ND ug/kg 08/19/20 18:51 74-87-308/19/20 12:2619.5 1
2-Chlorotoluene ND ug/kg 08/19/20 18:51 95-49-808/19/20 12:269.8 1
4-Chlorotoluene ND ug/kg 08/19/20 18:51 106-43-408/19/20 12:269.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/20 18:51 96-12-808/19/20 12:269.8 1
Dibromochloromethane ND ug/kg 08/19/20 18:51 124-48-108/19/20 12:269.8 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/20 18:51 106-93-408/19/20 12:269.8 1
Dibromomethane ND ug/kg 08/19/20 18:51 74-95-308/19/20 12:269.8 1
1,2-Dichlorobenzene ND ug/kg 08/19/20 18:51 95-50-108/19/20 12:269.8 1
1,3-Dichlorobenzene ND ug/kg 08/19/20 18:51 541-73-108/19/20 12:269.8 1
1,4-Dichlorobenzene ND ug/kg 08/19/20 18:51 106-46-708/19/20 12:269.8 1
Dichlorodifluoromethane ND ug/kg 08/19/20 18:51 75-71-808/19/20 12:2619.5 1
1,1-Dichloroethane ND ug/kg 08/19/20 18:51 75-34-308/19/20 12:269.8 1
1,2-Dichloroethane ND ug/kg 08/19/20 18:51 107-06-208/19/20 12:269.8 1
1,1-Dichloroethene ND ug/kg 08/19/20 18:51 75-35-408/19/20 12:269.8 1
cis-1,2-Dichloroethene ND ug/kg 08/19/20 18:51 156-59-208/19/20 12:269.8 1
trans-1,2-Dichloroethene ND ug/kg 08/19/20 18:51 156-60-508/19/20 12:269.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-4 (3-4)Lab ID:92490828006 Collected:08/13/20 13:40 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/19/20 18:51 78-87-508/19/20 12:269.8 1
1,3-Dichloropropane ND ug/kg 08/19/20 18:51 142-28-908/19/20 12:269.8 1
2,2-Dichloropropane ND ug/kg 08/19/20 18:51 594-20-708/19/20 12:269.8 1
1,1-Dichloropropene ND ug/kg 08/19/20 18:51 563-58-608/19/20 12:269.8 1
cis-1,3-Dichloropropene ND ug/kg 08/19/20 18:51 10061-01-508/19/20 12:269.8 1
trans-1,3-Dichloropropene ND ug/kg 08/19/20 18:51 10061-02-608/19/20 12:269.8 1
Diisopropyl ether ND ug/kg 08/19/20 18:51 108-20-308/19/20 12:269.8 1
Ethylbenzene ND ug/kg 08/19/20 18:51 100-41-408/19/20 12:269.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/20 18:51 87-68-308/19/20 12:269.8 1
2-Hexanone ND ug/kg 08/19/20 18:51 591-78-608/19/20 12:2697.6 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/20 18:51 98-82-808/19/20 12:269.8 1
p-Isopropyltoluene ND ug/kg 08/19/20 18:51 99-87-608/19/20 12:269.8 1
Methylene Chloride ND ug/kg 08/19/20 18:51 75-09-208/19/20 12:2639.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/20 18:51 108-10-108/19/20 12:2697.6 1
Methyl-tert-butyl ether ND ug/kg 08/19/20 18:51 1634-04-408/19/20 12:269.8 1
Naphthalene ND ug/kg 08/19/20 18:51 91-20-308/19/20 12:269.8 1
n-Propylbenzene ND ug/kg 08/19/20 18:51 103-65-108/19/20 12:269.8 1
Styrene ND ug/kg 08/19/20 18:51 100-42-508/19/20 12:269.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/20 18:51 630-20-608/19/20 12:269.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/20 18:51 79-34-508/19/20 12:269.8 1
Tetrachloroethene ND ug/kg 08/19/20 18:51 127-18-408/19/20 12:269.8 1
Toluene ND ug/kg 08/19/20 18:51 108-88-308/19/20 12:269.8 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/20 18:51 87-61-608/19/20 12:269.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/20 18:51 120-82-108/19/20 12:269.8 1
1,1,1-Trichloroethane ND ug/kg 08/19/20 18:51 71-55-608/19/20 12:269.8 1
1,1,2-Trichloroethane ND ug/kg 08/19/20 18:51 79-00-508/19/20 12:269.8 1
Trichloroethene ND ug/kg 08/19/20 18:51 79-01-608/19/20 12:269.8 1
Trichlorofluoromethane ND ug/kg 08/19/20 18:51 75-69-408/19/20 12:269.8 1
1,2,3-Trichloropropane ND ug/kg 08/19/20 18:51 96-18-408/19/20 12:269.8 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/20 18:51 95-63-608/19/20 12:269.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/20 18:51 108-67-808/19/20 12:269.8 1
Vinyl acetate ND ug/kg 08/19/20 18:51 108-05-408/19/20 12:2697.6 1
Vinyl chloride ND ug/kg 08/19/20 18:51 75-01-408/19/20 12:2619.5 1
Xylene (Total)ND ug/kg 08/19/20 18:51 1330-20-708/19/20 12:2619.5 1
m&p-Xylene ND ug/kg 08/19/20 18:51 179601-23-108/19/20 12:2619.5 1
o-Xylene ND ug/kg 08/19/20 18:51 95-47-608/19/20 12:269.8 1
Surrogates
Toluene-d8 (S)99 %08/19/20 18:51 2037-26-508/19/20 12:2670-130 1
4-Bromofluorobenzene (S)100 %08/19/20 18:51 460-00-408/19/20 12:2670-130 1
1,2-Dichloroethane-d4 (S)93 %08/19/20 18:51 17060-07-008/19/20 12:2670-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.2 %08/17/20 16:000.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-5 (3-4)Lab ID:92490828007 Collected:08/13/20 13:50 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 4.1 mg/kg 08/17/20 23:06 7440-38-208/17/20 07:511.0 1
Barium 55.8 mg/kg 08/17/20 23:06 7440-39-308/17/20 07:510.51 1
Cadmium ND mg/kg 08/17/20 23:06 7440-43-908/17/20 07:510.10 1
Chromium ND mg/kg 08/17/20 23:06 7440-47-308/17/20 07:510.51 1
Lead 6.8 mg/kg 08/17/20 23:06 7439-92-108/17/20 07:510.51 1
Selenium ND mg/kg 08/17/20 23:06 7782-49-208/17/20 07:511.0 1
Silver ND mg/kg 08/17/20 23:06 7440-22-408/17/20 07:510.51 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.012 mg/kg 08/17/20 15:37 7439-97-608/17/20 10:210.0064 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/20 19:10 67-64-108/19/20 12:262311
Benzene ND ug/kg 08/19/20 19:10 71-43-208/19/20 12:2611.5 1
Bromobenzene ND ug/kg 08/19/20 19:10 108-86-108/19/20 12:2611.5 1
Bromochloromethane ND ug/kg 08/19/20 19:10 74-97-5 IK08/19/20 12:2611.5 1
Bromodichloromethane ND ug/kg 08/19/20 19:10 75-27-408/19/20 12:2611.5 1
Bromoform ND ug/kg 08/19/20 19:10 75-25-208/19/20 12:2611.5 1
Bromomethane ND ug/kg 08/19/20 19:10 74-83-9 v108/19/20 12:2623.1 1
2-Butanone (MEK)ND ug/kg 08/19/20 19:10 78-93-308/19/20 12:262311
n-Butylbenzene ND ug/kg 08/19/20 19:10 104-51-808/19/20 12:2611.5 1
sec-Butylbenzene ND ug/kg 08/19/20 19:10 135-98-808/19/20 12:2611.5 1
tert-Butylbenzene ND ug/kg 08/19/20 19:10 98-06-608/19/20 12:2611.5 1
Carbon tetrachloride ND ug/kg 08/19/20 19:10 56-23-508/19/20 12:2611.5 1
Chlorobenzene ND ug/kg 08/19/20 19:10 108-90-708/19/20 12:2611.5 1
Chloroethane ND ug/kg 08/19/20 19:10 75-00-308/19/20 12:2623.1 1
Chloroform ND ug/kg 08/19/20 19:10 67-66-308/19/20 12:2611.5 1
Chloromethane ND ug/kg 08/19/20 19:10 74-87-308/19/20 12:2623.1 1
2-Chlorotoluene ND ug/kg 08/19/20 19:10 95-49-808/19/20 12:2611.5 1
4-Chlorotoluene ND ug/kg 08/19/20 19:10 106-43-408/19/20 12:2611.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/20 19:10 96-12-808/19/20 12:2611.5 1
Dibromochloromethane ND ug/kg 08/19/20 19:10 124-48-108/19/20 12:2611.5 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/20 19:10 106-93-408/19/20 12:2611.5 1
Dibromomethane ND ug/kg 08/19/20 19:10 74-95-308/19/20 12:2611.5 1
1,2-Dichlorobenzene ND ug/kg 08/19/20 19:10 95-50-108/19/20 12:2611.5 1
1,3-Dichlorobenzene ND ug/kg 08/19/20 19:10 541-73-108/19/20 12:2611.5 1
1,4-Dichlorobenzene ND ug/kg 08/19/20 19:10 106-46-708/19/20 12:2611.5 1
Dichlorodifluoromethane ND ug/kg 08/19/20 19:10 75-71-808/19/20 12:2623.1 1
1,1-Dichloroethane ND ug/kg 08/19/20 19:10 75-34-308/19/20 12:2611.5 1
1,2-Dichloroethane ND ug/kg 08/19/20 19:10 107-06-208/19/20 12:2611.5 1
1,1-Dichloroethene ND ug/kg 08/19/20 19:10 75-35-408/19/20 12:2611.5 1
cis-1,2-Dichloroethene ND ug/kg 08/19/20 19:10 156-59-208/19/20 12:2611.5 1
trans-1,2-Dichloroethene ND ug/kg 08/19/20 19:10 156-60-508/19/20 12:2611.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92490828
Rotary Drive
Sample:HA-5 (3-4)Lab ID:92490828007 Collected:08/13/20 13:50 Received:08/14/20 08:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/19/20 19:10 78-87-508/19/20 12:2611.5 1
1,3-Dichloropropane ND ug/kg 08/19/20 19:10 142-28-908/19/20 12:2611.5 1
2,2-Dichloropropane ND ug/kg 08/19/20 19:10 594-20-708/19/20 12:2611.5 1
1,1-Dichloropropene ND ug/kg 08/19/20 19:10 563-58-608/19/20 12:2611.5 1
cis-1,3-Dichloropropene ND ug/kg 08/19/20 19:10 10061-01-508/19/20 12:2611.5 1
trans-1,3-Dichloropropene ND ug/kg 08/19/20 19:10 10061-02-608/19/20 12:2611.5 1
Diisopropyl ether ND ug/kg 08/19/20 19:10 108-20-308/19/20 12:2611.5 1
Ethylbenzene ND ug/kg 08/19/20 19:10 100-41-408/19/20 12:2611.5 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/20 19:10 87-68-308/19/20 12:2611.5 1
2-Hexanone ND ug/kg 08/19/20 19:10 591-78-608/19/20 12:261151
Isopropylbenzene (Cumene)ND ug/kg 08/19/20 19:10 98-82-808/19/20 12:2611.5 1
p-Isopropyltoluene ND ug/kg 08/19/20 19:10 99-87-608/19/20 12:2611.5 1
Methylene Chloride ND ug/kg 08/19/20 19:10 75-09-208/19/20 12:2646.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/20 19:10 108-10-108/19/20 12:261151
Methyl-tert-butyl ether ND ug/kg 08/19/20 19:10 1634-04-408/19/20 12:2611.5 1
Naphthalene ND ug/kg 08/19/20 19:10 91-20-308/19/20 12:2611.5 1
n-Propylbenzene ND ug/kg 08/19/20 19:10 103-65-108/19/20 12:2611.5 1
Styrene ND ug/kg 08/19/20 19:10 100-42-508/19/20 12:2611.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/20 19:10 630-20-608/19/20 12:2611.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/20 19:10 79-34-508/19/20 12:2611.5 1
Tetrachloroethene ND ug/kg 08/19/20 19:10 127-18-408/19/20 12:2611.5 1
Toluene ND ug/kg 08/19/20 19:10 108-88-308/19/20 12:2611.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/20 19:10 87-61-608/19/20 12:2611.5 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/20 19:10 120-82-108/19/20 12:2611.5 1
1,1,1-Trichloroethane ND ug/kg 08/19/20 19:10 71-55-608/19/20 12:2611.5 1
1,1,2-Trichloroethane ND ug/kg 08/19/20 19:10 79-00-508/19/20 12:2611.5 1
Trichloroethene ND ug/kg 08/19/20 19:10 79-01-608/19/20 12:2611.5 1
Trichlorofluoromethane ND ug/kg 08/19/20 19:10 75-69-408/19/20 12:2611.5 1
1,2,3-Trichloropropane ND ug/kg 08/19/20 19:10 96-18-408/19/20 12:2611.5 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/20 19:10 95-63-608/19/20 12:2611.5 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/20 19:10 108-67-808/19/20 12:2611.5 1
Vinyl acetate ND ug/kg 08/19/20 19:10 108-05-408/19/20 12:261151
Vinyl chloride ND ug/kg 08/19/20 19:10 75-01-408/19/20 12:2623.1 1
Xylene (Total)ND ug/kg 08/19/20 19:10 1330-20-708/19/20 12:2623.1 1
m&p-Xylene ND ug/kg 08/19/20 19:10 179601-23-108/19/20 12:2623.1 1
o-Xylene ND ug/kg 08/19/20 19:10 95-47-608/19/20 12:2611.5 1
Surrogates
Toluene-d8 (S)100 %08/19/20 19:10 2037-26-508/19/20 12:2670-130 1
4-Bromofluorobenzene (S)101 %08/19/20 19:10 460-00-408/19/20 12:2670-130 1
1,2-Dichloroethane-d4 (S)97 %08/19/20 19:10 17060-07-008/19/20 12:2670-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.9 %08/17/20 16:000.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
560437
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92490828001, 92490828002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2973490
Associated Lab Samples:92490828001, 92490828002
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 08/18/20 12:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2973491LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2973492MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92490458001
2973493
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 103 75-12596 62.5ND 2.6 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
560293
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92490828003, 92490828004, 92490828005, 92490828006, 92490828007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2972728
Associated Lab Samples:92490828003, 92490828004, 92490828005, 92490828006, 92490828007
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0060 08/17/20 15:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2972729LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0850.083 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2972730MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92490828003
2972731
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg 0.071 91 75-125100 200.0820.015 0.080 0.097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
560292
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92490828003, 92490828004, 92490828005, 92490828006, 92490828007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2972724
Associated Lab Samples:92490828003, 92490828004, 92490828005, 92490828006, 92490828007
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 08/17/20 22:04
Barium mg/kg ND 0.50 08/17/20 22:04
Cadmium mg/kg ND 0.10 08/18/20 13:02
Chromium mg/kg ND 0.50 08/17/20 22:04
Lead mg/kg ND 0.50 08/17/20 22:04
Selenium mg/kg ND 1.0 08/17/20 22:04
Silver mg/kg ND 0.50 08/17/20 22:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2972725LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 48.650 97 80-120
Barium mg/kg 51.750 103 80-120
Cadmium mg/kg 47.650 95 80-120
Chromium mg/kg 50.150 100 80-120
Lead mg/kg 50.750 101 80-120
Selenium mg/kg 47.050 94 80-120
Silver mg/kg 24.525 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2972726MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92489924004
2972727
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg 45 81 75-12584 847.74.4 41.0 44.5
Barium mg/kg M1,R1456175-125160 3047.7112 139 188
Cadmium mg/kg 45 86 75-12587 747.70.11 38.9 41.8
Chromium mg/kg 45 86 75-12590 747.717.2 56.1 60.2
Lead mg/kg 45 78 75-12579 547.717.2 52.4 54.8
Selenium mg/kg 45 75 75-12576 647.7ND 34.0 36.1
Silver mg/kg 22.6 89 75-12589 623.9ND 20.0 21.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
560535
EPA 3010A
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92490828001, 92490828002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2973980
Associated Lab Samples:92490828001, 92490828002
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 08/18/20 20:54
Barium ug/L ND 5.0 08/18/20 20:54
Cadmium ug/L ND 1.0 08/18/20 20:54
Chromium ug/L ND 5.0 08/18/20 20:54
Lead ug/L ND 5.0 08/18/20 20:54
Selenium ug/L ND 10.0 08/18/20 20:54
Silver ug/L ND 5.0 08/18/20 20:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2973981LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 463500 93 80-120
Barium ug/L 475500 95 80-120
Cadmium ug/L 466500 93 80-120
Chromium ug/L 467500 93 80-120
Lead ug/L 470500 94 80-120
Selenium ug/L 470500 94 80-120
Silver ug/L 232250 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2973982MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92490828001
2973983
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 98 75-12595 3500ND492478
Barium ug/L 500 97 75-12597 050059.8 543 543
Cadmium ug/L 500 97 75-12597 1500ND487484
Chromium ug/L 500 96 75-12596 0500ND482481
Lead ug/L 500 94 75-12593 1500ND470466
Selenium ug/L 500 100 75-125100 1500ND499503
Silver ug/L 250 96 75-12595 1250ND241238
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
560975
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92490828003, 92490828004, 92490828005, 92490828006, 92490828007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2975812
Associated Lab Samples:92490828003, 92490828004, 92490828005, 92490828006, 92490828007
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/19/20 12:26
1,1,1-Trichloroethane ug/kg ND 5.0 08/19/20 12:26
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/19/20 12:26
1,1,2-Trichloroethane ug/kg ND 5.0 08/19/20 12:26
1,1-Dichloroethane ug/kg ND 5.0 08/19/20 12:26
1,1-Dichloroethene ug/kg ND 5.0 08/19/20 12:26
1,1-Dichloropropene ug/kg ND 5.0 08/19/20 12:26
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/19/20 12:26
1,2,3-Trichloropropane ug/kg ND 5.0 08/19/20 12:26
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/19/20 12:26
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/19/20 12:26
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/19/20 12:26
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/19/20 12:26
1,2-Dichlorobenzene ug/kg ND 5.0 08/19/20 12:26
1,2-Dichloroethane ug/kg ND 5.0 08/19/20 12:26
1,2-Dichloropropane ug/kg ND 5.0 08/19/20 12:26
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/19/20 12:26
1,3-Dichlorobenzene ug/kg ND 5.0 08/19/20 12:26
1,3-Dichloropropane ug/kg ND 5.0 08/19/20 12:26
1,4-Dichlorobenzene ug/kg ND 5.0 08/19/20 12:26
2,2-Dichloropropane ug/kg ND 5.0 08/19/20 12:26
2-Butanone (MEK)ug/kg ND 100 08/19/20 12:26
2-Chlorotoluene ug/kg ND 5.0 08/19/20 12:26
2-Hexanone ug/kg ND 50.0 08/19/20 12:26
4-Chlorotoluene ug/kg ND 5.0 08/19/20 12:26
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/19/20 12:26
Acetone ug/kg ND 100 08/19/20 12:26
Benzene ug/kg ND 5.0 08/19/20 12:26
Bromobenzene ug/kg ND 5.0 08/19/20 12:26
Bromochloromethane ug/kg ND 5.0 IK08/19/20 12:26
Bromodichloromethane ug/kg ND 5.0 08/19/20 12:26
Bromoform ug/kg ND 5.0 08/19/20 12:26
Bromomethane ug/kg ND 10.0 v108/19/20 12:26
Carbon tetrachloride ug/kg ND 5.0 08/19/20 12:26
Chlorobenzene ug/kg ND 5.0 08/19/20 12:26
Chloroethane ug/kg ND 10.0 08/19/20 12:26
Chloroform ug/kg ND 5.0 08/19/20 12:26
Chloromethane ug/kg ND 10.0 08/19/20 12:26
cis-1,2-Dichloroethene ug/kg ND 5.0 08/19/20 12:26
cis-1,3-Dichloropropene ug/kg ND 5.0 08/19/20 12:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2975812
Associated Lab Samples:92490828003, 92490828004, 92490828005, 92490828006, 92490828007
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 08/19/20 12:26
Dibromomethane ug/kg ND 5.0 08/19/20 12:26
Dichlorodifluoromethane ug/kg ND 10.0 08/19/20 12:26
Diisopropyl ether ug/kg ND 5.0 08/19/20 12:26
Ethylbenzene ug/kg ND 5.0 08/19/20 12:26
Hexachloro-1,3-butadiene ug/kg ND 5.0 08/19/20 12:26
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/19/20 12:26
m&p-Xylene ug/kg ND 10.0 08/19/20 12:26
Methyl-tert-butyl ether ug/kg ND 5.0 08/19/20 12:26
Methylene Chloride ug/kg ND 20.0 08/19/20 12:26
n-Butylbenzene ug/kg ND 5.0 08/19/20 12:26
n-Propylbenzene ug/kg ND 5.0 08/19/20 12:26
Naphthalene ug/kg ND 5.0 08/19/20 12:26
o-Xylene ug/kg ND 5.0 08/19/20 12:26
p-Isopropyltoluene ug/kg ND 5.0 08/19/20 12:26
sec-Butylbenzene ug/kg ND 5.0 08/19/20 12:26
Styrene ug/kg ND 5.0 08/19/20 12:26
tert-Butylbenzene ug/kg ND 5.0 08/19/20 12:26
Tetrachloroethene ug/kg ND 5.0 08/19/20 12:26
Toluene ug/kg ND 5.0 08/19/20 12:26
trans-1,2-Dichloroethene ug/kg ND 5.0 08/19/20 12:26
trans-1,3-Dichloropropene ug/kg ND 5.0 08/19/20 12:26
Trichloroethene ug/kg ND 5.0 08/19/20 12:26
Trichlorofluoromethane ug/kg ND 5.0 08/19/20 12:26
Vinyl acetate ug/kg ND 50.0 08/19/20 12:26
Vinyl chloride ug/kg ND 10.0 08/19/20 12:26
Xylene (Total)ug/kg ND 10.0 08/19/20 12:26
1,2-Dichloroethane-d4 (S)%105 70-132 08/19/20 12:26
4-Bromofluorobenzene (S)%99 70-130 08/19/20 12:26
Toluene-d8 (S)%100 70-130 08/19/20 12:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2975813LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13001250 104 70-130
1,1,1-Trichloroethane ug/kg 12701250 102 70-130
1,1,2,2-Tetrachloroethane ug/kg 12101250 97 55-130
1,1,2-Trichloroethane ug/kg 12201250 97 70-130
1,1-Dichloroethane ug/kg 12601250 101 68-130
1,1-Dichloroethene ug/kg 12701250 102 70-130
1,1-Dichloropropene ug/kg 12701250 101 70-130
1,2,3-Trichlorobenzene ug/kg 11801250 94 70-130
1,2,3-Trichloropropane ug/kg 11901250 96 70-130
1,2,4-Trichlorobenzene ug/kg 11601250 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2975813LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12101250 97 69-130
1,2-Dibromo-3-chloropropane ug/kg 12601250 100 57-141
1,2-Dibromoethane (EDB)ug/kg 12401250 99 70-130
1,2-Dichlorobenzene ug/kg 12001250 96 70-130
1,2-Dichloroethane ug/kg 10801250 86 70-130
1,2-Dichloropropane ug/kg 12601250 101 70-130
1,3,5-Trimethylbenzene ug/kg 12401250 100 70-130
1,3-Dichlorobenzene ug/kg 12101250 97 70-130
1,3-Dichloropropane ug/kg 12701250 102 70-130
1,4-Dichlorobenzene ug/kg 12001250 96 70-130
2,2-Dichloropropane ug/kg 11901250 95 70-130
2-Butanone (MEK)ug/kg 23202500 93 60-130
2-Chlorotoluene ug/kg 12701250 101 70-130
2-Hexanone ug/kg 23902500 95 70-132
4-Chlorotoluene ug/kg 12001250 96 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23202500 93 69-130
Acetone ug/kg 23302500 93 49-148
Benzene ug/kg 12101250 97 70-130
Bromobenzene ug/kg 12301250 99 70-130
Bromochloromethane ug/kg 1220 IK12509770-130
Bromodichloromethane ug/kg 11701250 93 70-130
Bromoform ug/kg 13001250 104 68-136
Bromomethane ug/kg 1370 v1125010960-140
Carbon tetrachloride ug/kg 13301250 106 70-130
Chlorobenzene ug/kg 12301250 98 70-130
Chloroethane ug/kg 12201250 98 51-147
Chloroform ug/kg 12401250 99 70-130
Chloromethane ug/kg 9361250 75 48-130
cis-1,2-Dichloroethene ug/kg 12201250 97 70-130
cis-1,3-Dichloropropene ug/kg 12801250 102 70-130
Dibromochloromethane ug/kg 13001250 104 70-130
Dibromomethane ug/kg 12801250 102 70-130
Dichlorodifluoromethane ug/kg 10801250 86 49-130
Diisopropyl ether ug/kg 11601250 93 66-130
Ethylbenzene ug/kg 11801250 94 70-130
Hexachloro-1,3-butadiene ug/kg 11501250 92 70-130
Isopropylbenzene (Cumene)ug/kg 12601250 101 70-130
m&p-Xylene ug/kg 25202500 101 70-130
Methyl-tert-butyl ether ug/kg 12201250 97 70-130
Methylene Chloride ug/kg 10801250 86 50-137
n-Butylbenzene ug/kg 12101250 97 70-130
n-Propylbenzene ug/kg 12301250 98 70-130
Naphthalene ug/kg 12401250 99 70-131
o-Xylene ug/kg 12401250 99 70-130
p-Isopropyltoluene ug/kg 12001250 96 70-130
sec-Butylbenzene ug/kg 12201250 98 70-130
Styrene ug/kg 13501250 108 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2975813LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 11901250 96 69-130
Tetrachloroethene ug/kg 12801250 102 56-130
Toluene ug/kg 12001250 96 70-130
trans-1,2-Dichloroethene ug/kg 12601250 101 70-130
trans-1,3-Dichloropropene ug/kg 12101250 97 70-130
Trichloroethene ug/kg 12601250 101 70-141
Trichlorofluoromethane ug/kg 12801250 102 67-130
Vinyl acetate ug/kg 24302500 97 10-136
Vinyl chloride ug/kg 11201250 89 67-130
Xylene (Total)ug/kg 37603750 100 70-130
1,2-Dichloroethane-d4 (S)%92 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2975815MATRIX SPIKE SAMPLE:
MSSpike
Result
92490539002
1,1,1,2-Tetrachloroethane ug/kg 706 M152713452-133ND
1,1,1-Trichloroethane ug/kg 618527 117 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 585527 111 39-150ND
1,1,2-Trichloroethane ug/kg 692527 131 48-140ND
1,1-Dichloroethane ug/kg 539527 102 46-135ND
1,1-Dichloroethene ug/kg 368527 70 38-149ND
1,1-Dichloropropene ug/kg 621527 118 41-140ND
1,2,3-Trichlorobenzene ug/kg 464527 88 10-158ND
1,2,3-Trichloropropane ug/kg 529527 100 33-157ND
1,2,4-Trichlorobenzene ug/kg 547527 104 10-155ND
1,2,4-Trimethylbenzene ug/kg 574527 109 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 470527 89 33-158ND
1,2-Dibromoethane (EDB)ug/kg 558527 106 40-136ND
1,2-Dichlorobenzene ug/kg 584527 111 27-146ND
1,2-Dichloroethane ug/kg 561527 106 49-140ND
1,2-Dichloropropane ug/kg 617527 117 44-143ND
1,3,5-Trimethylbenzene ug/kg 602527 114 40-144ND
1,3-Dichlorobenzene ug/kg 597527 113 33-140ND
1,3-Dichloropropane ug/kg 572527 109 47-147ND
1,4-Dichlorobenzene ug/kg 572527 109 35-139ND
2,2-Dichloropropane ug/kg 419527 79 41-140ND
2-Butanone (MEK)ug/kg 8521050 81 10-181ND
2-Chlorotoluene ug/kg 598527 113 38-147ND
2-Hexanone ug/kg 5171050 49 18-169ND
4-Chlorotoluene ug/kg 572527 108 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 10301050 98 16-175ND
Acetone ug/kg 5531050 52 10-200ND
Benzene ug/kg 601527 114 46-136ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2975815MATRIX SPIKE SAMPLE:
MSSpike
Result
92490539002
Bromobenzene ug/kg 592527 112 38-149ND
Bromochloromethane ug/kg 588 IK52711244-142ND
Bromodichloromethane ug/kg 570527 108 41-140ND
Bromoform ug/kg 574527 109 34-145ND
Bromomethane ug/kg 983 M1,v152718614-162ND
Carbon tetrachloride ug/kg 652527 124 44-141ND
Chlorobenzene ug/kg 584527 111 39-141ND
Chloroethane ug/kg 219527 42 10-182ND
Chloroform ug/kg 577527 110 45-140ND
Chloromethane ug/kg 539527 101 19-149ND
cis-1,2-Dichloroethene ug/kg 586527 111 38-150ND
cis-1,3-Dichloropropene ug/kg 586527 111 30-144ND
Dibromochloromethane ug/kg 615527 117 36-145ND
Dibromomethane ug/kg 607527 115 41-145ND
Dichlorodifluoromethane ug/kg 526527 100 16-146ND
Diisopropyl ether ug/kg 539527 102 41-143ND
Ethylbenzene ug/kg 564527 107 35-144ND
Hexachloro-1,3-butadiene ug/kg 566527 107 10-160ND
Isopropylbenzene (Cumene)ug/kg 611527 116 30-152ND
m&p-Xylene ug/kg 12001050 114 33-145ND
Methyl-tert-butyl ether ug/kg 573527 109 49-140ND
Methylene Chloride ug/kg 496527 94 10-174ND
n-Butylbenzene ug/kg 583527 111 10-160ND
n-Propylbenzene ug/kg 604527 115 24-159ND
Naphthalene ug/kg 397527 75 10-171ND
o-Xylene ug/kg 579527 110 31-150ND
p-Isopropyltoluene ug/kg 592527 112 21-154ND
sec-Butylbenzene ug/kg 604527 115 19-159ND
Styrene ug/kg 631527 120 15-152ND
tert-Butylbenzene ug/kg 626527 119 31-141ND
Tetrachloroethene ug/kg 618527 117 19-141ND
Toluene ug/kg 586527 110 31-146ND
trans-1,2-Dichloroethene ug/kg 607527 115 28-157ND
trans-1,3-Dichloropropene ug/kg 547527 104 25-146ND
Trichloroethene ug/kg 697527 132 34-149ND
Trichlorofluoromethane ug/kg 178527 34 10-167ND
Vinyl acetate ug/kg 9731050 92 10-200ND
Vinyl chloride ug/kg 555527 105 36-155ND
Xylene (Total)ug/kg 17801580 112 29-148ND
1,2-Dichloroethane-d4 (S)%111 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92490539001
2975814SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg ND IKND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND v1ND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg 9.8JND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92490539001
2975814SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 5.1JND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%9498
4-Bromofluorobenzene (S)%102101
Toluene-d8 (S)%99100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
561291
EPA 8260D
EPA 8260D
8260D MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92490828001, 92490828002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2977364
Associated Lab Samples:92490828001, 92490828002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 08/20/20 22:46
1,1,1-Trichloroethane ug/L ND 5.0 08/20/20 22:46
1,1,2,2-Tetrachloroethane ug/L ND 5.0 08/20/20 22:46
1,1,2-Trichloroethane ug/L ND 5.0 08/20/20 22:46
1,1-Dichloroethane ug/L ND 5.0 08/20/20 22:46
1,1-Dichloroethene ug/L ND 5.0 08/20/20 22:46
1,1-Dichloropropene ug/L ND 5.0 08/20/20 22:46
1,2,3-Trichlorobenzene ug/L ND 5.0 08/20/20 22:46
1,2,3-Trichloropropane ug/L ND 5.0 08/20/20 22:46
1,2,4-Trichlorobenzene ug/L ND 5.0 08/20/20 22:46
1,2,4-Trimethylbenzene ug/L ND 5.0 08/20/20 22:46
1,2-Dibromo-3-chloropropane ug/L ND 5.0 08/20/20 22:46
1,2-Dibromoethane (EDB)ug/L ND 5.0 08/20/20 22:46
1,2-Dichlorobenzene ug/L ND 5.0 08/20/20 22:46
1,2-Dichloroethane ug/L ND 5.0 08/20/20 22:46
1,2-Dichloroethene (Total)ug/L ND 5.0 08/20/20 22:46
1,2-Dichloropropane ug/L ND 5.0 08/20/20 22:46
1,3,5-Trimethylbenzene ug/L ND 5.0 08/20/20 22:46
1,3-Dichlorobenzene ug/L ND 5.0 08/20/20 22:46
1,3-Dichloropropane ug/L ND 5.0 08/20/20 22:46
1,4-Dichlorobenzene ug/L ND 5.0 08/20/20 22:46
2,2-Dichloropropane ug/L ND 5.0 08/20/20 22:46
2-Butanone (MEK)ug/L ND 10.0 IK08/20/20 22:46
2-Chlorotoluene ug/L ND 5.0 08/20/20 22:46
2-Hexanone ug/L ND 10.0 08/20/20 22:46
4-Chlorotoluene ug/L ND 5.0 08/20/20 22:46
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 08/20/20 22:46
Acetone ug/L ND 25.0 08/20/20 22:46
Benzene ug/L ND 5.0 08/20/20 22:46
Bromobenzene ug/L ND 5.0 08/20/20 22:46
Bromochloromethane ug/L ND 5.0 08/20/20 22:46
Bromodichloromethane ug/L ND 5.0 08/20/20 22:46
Bromoform ug/L ND 5.0 08/20/20 22:46
Bromomethane ug/L ND 10.0 IK08/20/20 22:46
Carbon tetrachloride ug/L ND 5.0 08/20/20 22:46
Chlorobenzene ug/L ND 5.0 08/20/20 22:46
Chloroethane ug/L ND 10.0 v208/20/20 22:46
Chloroform ug/L ND 5.0 08/20/20 22:46
Chloromethane ug/L ND 5.0 08/20/20 22:46
cis-1,2-Dichloroethene ug/L ND 5.0 08/20/20 22:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2977364
Associated Lab Samples:92490828001, 92490828002
Matrix:Water
Analyzed
cis-1,3-Dichloropropene ug/L ND 5.0 08/20/20 22:46
Dibromochloromethane ug/L ND 5.0 08/20/20 22:46
Dibromomethane ug/L ND 5.0 08/20/20 22:46
Dichlorodifluoromethane ug/L ND 5.0 v208/20/20 22:46
Diisopropyl ether ug/L ND 5.0 08/20/20 22:46
Ethylbenzene ug/L ND 5.0 08/20/20 22:46
Hexachloro-1,3-butadiene ug/L ND 5.0 08/20/20 22:46
Isopropylbenzene (Cumene)ug/L ND 5.0 08/20/20 22:46
m&p-Xylene ug/L ND 10.0 08/20/20 22:46
Methyl-tert-butyl ether ug/L ND 5.0 08/20/20 22:46
Methylene Chloride ug/L ND 5.0 08/20/20 22:46
n-Butylbenzene ug/L ND 5.0 08/20/20 22:46
n-Propylbenzene ug/L ND 5.0 08/20/20 22:46
Naphthalene ug/L ND 5.0 08/20/20 22:46
o-Xylene ug/L ND 5.0 08/20/20 22:46
p-Isopropyltoluene ug/L ND 5.0 08/20/20 22:46
sec-Butylbenzene ug/L ND 5.0 08/20/20 22:46
Styrene ug/L ND 5.0 08/20/20 22:46
tert-Butyl Alcohol ug/L ND 100 08/20/20 22:46
tert-Butylbenzene ug/L ND 5.0 08/20/20 22:46
Tetrachloroethene ug/L ND 5.0 08/20/20 22:46
Toluene ug/L ND 5.0 08/20/20 22:46
trans-1,2-Dichloroethene ug/L ND 5.0 08/20/20 22:46
trans-1,3-Dichloropropene ug/L ND 5.0 08/20/20 22:46
Trichloroethene ug/L ND 5.0 08/20/20 22:46
Trichlorofluoromethane ug/L ND 10.0 08/20/20 22:46
Vinyl acetate ug/L ND 10.0 IK08/20/20 22:46
Vinyl chloride ug/L ND 5.0 08/20/20 22:46
1,2-Dichloroethane-d4 (S)%84 70-130 08/20/20 22:46
4-Bromofluorobenzene (S)%98 70-130 08/20/20 22:46
Toluene-d8 (S)%104 70-130 08/20/20 22:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2977365LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.450 105 70-130
1,1,1-Trichloroethane ug/L 48.850 98 70-130
1,1,2,2-Tetrachloroethane ug/L 51.350 103 70-130
1,1,2-Trichloroethane ug/L 53.750 107 70-130
1,1-Dichloroethane ug/L 49.550 99 70-130
1,1-Dichloroethene ug/L 49.850 100 70-130
1,1-Dichloropropene ug/L 52.750 105 70-130
1,2,3-Trichlorobenzene ug/L 46.250 92 70-130
1,2,3-Trichloropropane ug/L 49.050 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2977365LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 47.450 95 70-130
1,2,4-Trimethylbenzene ug/L 48.950 98 70-131
1,2-Dibromo-3-chloropropane ug/L 52.750 105 70-130
1,2-Dibromoethane (EDB)ug/L 55.550 111 70-130
1,2-Dichlorobenzene ug/L 50.450 101 70-130
1,2-Dichloroethane ug/L 44.550 89 70-130
1,2-Dichloroethene (Total)ug/L 99.3
1,2-Dichloropropane ug/L 55.750 111 70-130
1,3,5-Trimethylbenzene ug/L 50.150 100 70-130
1,3-Dichlorobenzene ug/L 50.050 100 70-130
1,3-Dichloropropane ug/L 56.050 112 70-131
1,4-Dichlorobenzene ug/L 49.650 99 70-130
2,2-Dichloropropane ug/L 47.850 96 69-130
2-Butanone (MEK)ug/L 97.1 IK1009764-135
2-Chlorotoluene ug/L 50.150 100 70-130
2-Hexanone ug/L 102100 102 66-135
4-Chlorotoluene ug/L 48.850 98 70-130
4-Methyl-2-pentanone (MIBK)ug/L 104100 104 70-130
Acetone ug/L 102100 102 61-157
Benzene ug/L 50.950 102 70-130
Bromobenzene ug/L 49.250 98 70-130
Bromochloromethane ug/L 52.550 105 70-130
Bromodichloromethane ug/L 46.350 93 70-130
Bromoform ug/L 53.750 107 70-130
Bromomethane ug/L 48.4 IK509738-130
Carbon tetrachloride ug/L 48.250 96 70-130
Chlorobenzene ug/L 49.050 98 70-130
Chloroethane ug/L 39.1 v3507837-142
Chloroform ug/L 47.750 95 70-130
Chloromethane ug/L 42.950 86 48-130
cis-1,2-Dichloroethene ug/L 48.850 98 70-130
cis-1,3-Dichloropropene ug/L 57.950 116 70-130
Dibromochloromethane ug/L 54.050 108 70-130
Dibromomethane ug/L 52.950 106 70-130
Dichlorodifluoromethane ug/L 36.6 v3507353-134
Diisopropyl ether ug/L 54.650 109 70-135
Ethylbenzene ug/L 48.850 98 70-130
Hexachloro-1,3-butadiene ug/L 43.950 88 68-132
Isopropylbenzene (Cumene)ug/L 48.850 98 70-130
m&p-Xylene ug/L 95.9100 96 70-130
Methyl-tert-butyl ether ug/L 56.350 113 70-130
Methylene Chloride ug/L 49.150 98 67-132
n-Butylbenzene ug/L 46.750 93 70-132
n-Propylbenzene ug/L 49.050 98 70-130
Naphthalene ug/L 47.550 95 70-130
o-Xylene ug/L 49.850 100 70-130
p-Isopropyltoluene ug/L 48.450 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2977365LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/L 48.250 96 70-130
Styrene ug/L 52.950 106 70-130
tert-Butyl Alcohol ug/L 473500 95 64-135
tert-Butylbenzene ug/L 42.450 85 66-130
Tetrachloroethene ug/L 49.250 98 69-130
Toluene ug/L 48.350 97 70-130
trans-1,2-Dichloroethene ug/L 50.550 101 70-130
trans-1,3-Dichloropropene ug/L 55.050 110 70-130
Trichloroethene ug/L 52.650 105 70-130
Trichlorofluoromethane ug/L 40.550 81 63-130
Vinyl acetate ug/L 94.1 IK1009455-143
Vinyl chloride ug/L 44.650 89 70-131
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2979226MATRIX SPIKE SAMPLE:
MSSpike
Result
92490828002
1,1,1,2-Tetrachloroethane ug/L 23.320 117 73-134ND
1,1,1-Trichloroethane ug/L 23.520 118 82-143ND
1,1,2,2-Tetrachloroethane ug/L 20.320 101 70-136ND
1,1,2-Trichloroethane ug/L 22.520 112 70-135ND
1,1-Dichloroethane ug/L 21.220 106 70-139ND
1,1-Dichloroethene ug/L 24.620 123 70-154ND
1,1-Dichloropropene ug/L 22.020 110 70-149ND
1,2,3-Trichlorobenzene ug/L 17.320 87 70-135ND
1,2,3-Trichloropropane ug/L 20.620 103 71-137ND
1,2,4-Trichlorobenzene ug/L 17.920 90 73-140ND
1,2,4-Trimethylbenzene ug/L 21.520 108 71-142ND
1,2-Dibromo-3-chloropropane ug/L 20.020 100 65-134ND
1,2-Dibromoethane (EDB)ug/L 21.120 106 70-137ND
1,2-Dichlorobenzene ug/L 20.520 103 70-133ND
1,2-Dichloroethane ug/L 22.020 110 70-137ND
1,2-Dichloroethene (Total)ug/L 43.2ND
1,2-Dichloropropane ug/L 21.420 107 70-140ND
1,3,5-Trimethylbenzene ug/L 22.120 111 76-139ND
1,3-Dichlorobenzene ug/L 21.420 107 70-135ND
1,3-Dichloropropane ug/L 21.020 105 70-143ND
1,4-Dichlorobenzene ug/L 21.220 106 70-133ND
2,2-Dichloropropane ug/L 24.020 120 61-148ND
2-Butanone (MEK)ug/L 38.040 95 60-139ND
2-Chlorotoluene ug/L 21.920 109 70-144ND
2-Hexanone ug/L 39.240 98 65-138ND
4-Chlorotoluene ug/L 21.520 108 70-137ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2979226MATRIX SPIKE SAMPLE:
MSSpike
Result
92490828002
4-Methyl-2-pentanone (MIBK)ug/L 40.340 101 65-135ND
Acetone ug/L 40.640 101 60-148ND
Benzene ug/L 21.5 IK2010870-151ND
Bromobenzene ug/L 22.120 110 70-136ND
Bromochloromethane ug/L 21.920 109 70-141ND
Bromodichloromethane ug/L 22.220 111 70-138ND
Bromoform ug/L 22.820 114 63-130ND
Bromomethane ug/L 20.620 103 15-152ND
Carbon tetrachloride ug/L 26.020 130 70-143ND
Chlorobenzene ug/L 21.620 108 70-138ND
Chloroethane ug/L 21.020 105 52-163ND
Chloroform ug/L 21.520 108 70-139ND
Chloromethane ug/L 17.620 88 41-139ND
cis-1,2-Dichloroethene ug/L 21.020 105 70-141ND
cis-1,3-Dichloropropene ug/L 24.120 120 70-137ND
Dibromochloromethane ug/L 22.120 111 70-134ND
Dibromomethane ug/L 23.8 IK2011970-138ND
Dichlorodifluoromethane ug/L 20.020 100 47-155ND
Diisopropyl ether ug/L 20.120 100 63-144ND
Ethylbenzene ug/L 21.920 110 66-153ND
Hexachloro-1,3-butadiene ug/L 23.420 117 65-149ND
Isopropylbenzene (Cumene)ug/L 22.220 111 70-139ND
m&p-Xylene ug/L 43.940 110 69-152ND
Methyl-tert-butyl ether ug/L 21.520 108 54-156ND
Methylene Chloride ug/L 19.520 97 42-159ND
n-Butylbenzene ug/L 21.520 108 70-139ND
n-Propylbenzene ug/L 22.020 110 70-144ND
Naphthalene ug/L 16.320 82 61-148ND
o-Xylene ug/L 21.620 108 70-148ND
p-Isopropyltoluene ug/L 22.820 114 70-146ND
sec-Butylbenzene ug/L 22.620 113 70-141ND
Styrene ug/L 21.320 107 70-135ND
tert-Butyl Alcohol ug/L 219200 109 43-188ND
tert-Butylbenzene ug/L 19.420 97 70-130ND
Tetrachloroethene ug/L 20.920 105 59-143ND
Toluene ug/L 22.220 111 59-148ND
trans-1,2-Dichloroethene ug/L 22.120 111 70-146ND
trans-1,3-Dichloropropene ug/L 24.020 120 70-135ND
Trichloroethene ug/L 23.420 117 70-147ND
Trichlorofluoromethane ug/L 23.420 117 70-148ND
Vinyl acetate ug/L 45.440 114 49-151ND
Vinyl chloride ug/L 19.120 96 70-156ND
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92490828001
2979225SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2,4-Trimethylbenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloroethene (Total)ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3,5-Trimethylbenzene ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L ND IKND
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L ND IKND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92490828001
2979225SAMPLE DUPLICATE:
Isopropylbenzene (Cumene)ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
n-Butylbenzene ug/L NDND
n-Propylbenzene ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
sec-Butylbenzene ug/L NDND
Styrene ug/L NDND
tert-Butyl Alcohol ug/L NDND
tert-Butylbenzene ug/L NDND
Tetrachloroethene ug/L 20.4 120.5
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
1,2-Dichloroethane-d4 (S)%10284
4-Bromofluorobenzene (S)%97101
Toluene-d8 (S)%103105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92490828
Rotary Drive
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
560478
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92490828003, 92490828004, 92490828005, 92490828006, 92490828007
Parameter Units
Dup
Result QualifiersRPDResult
92490828003
2973683SAMPLE DUPLICATE:
Percent Moisture %11.0 810.1
Parameter Units
Dup
Result QualifiersRPDResult
92491123008
2973684SAMPLE DUPLICATE:
Percent Moisture %21.1 1019.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 41
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92490828
Rotary Drive
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 41
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92490828
Rotary Drive
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92490828003 560292 560443HA-1 (2-4)EPA 3050B EPA 6010D
92490828004 560292 560443HA-2 (0-2)EPA 3050B EPA 6010D
92490828005 560292 560443HA-3 (0-2)EPA 3050B EPA 6010D
92490828006 560292 560443HA-4 (3-4)EPA 3050B EPA 6010D
92490828007 560292 560443HA-5 (3-4)EPA 3050B EPA 6010D
92490828001 560535 560545MW-101 EPA 3010A EPA 6010D
92490828002 560535 560545MW-102 EPA 3010A EPA 6010D
92490828001 560437 560520MW-101 EPA 7470A EPA 7470A
92490828002 560437 560520MW-102 EPA 7470A EPA 7470A
92490828003 560293 560416HA-1 (2-4)EPA 7471B EPA 7471B
92490828004 560293 560416HA-2 (0-2)EPA 7471B EPA 7471B
92490828005 560293 560416HA-3 (0-2)EPA 7471B EPA 7471B
92490828006 560293 560416HA-4 (3-4)EPA 7471B EPA 7471B
92490828007 560293 560416HA-5 (3-4)EPA 7471B EPA 7471B
92490828003 560975 560985HA-1 (2-4)EPA 5035A/5030B EPA 8260D
92490828004 560975 560985HA-2 (0-2)EPA 5035A/5030B EPA 8260D
92490828005 560975 560985HA-3 (0-2)EPA 5035A/5030B EPA 8260D
92490828006 560975 560985HA-4 (3-4)EPA 5035A/5030B EPA 8260D
92490828007 560975 560985HA-5 (3-4)EPA 5035A/5030B EPA 8260D
92490828001 561291MW-101 EPA 8260D
92490828002 561291MW-102 EPA 8260D
92490828003 560478HA-1 (2-4)ASTM D2974-87
92490828004 560478HA-2 (0-2)ASTM D2974-87
92490828005 560478HA-3 (0-2)ASTM D2974-87
92490828006 560478HA-4 (3-4)ASTM D2974-87
92490828007 560478HA-5 (3-4)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/24/2020 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 41
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