23067_Blythe Isenhour_BARpt_20200406

Via Email

April 6, 2020

NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Ms. Jordan Thompson

Re: Brownfields Assessment Report
Blythe Isenhour
4920 Old Pineville Road
Charlotte, North Carolina
Brownfields Project No. 23067-19-060
H&H Project No. BOU-014

Dear Ms. Thompson:

On behalf of Boulevard at 4920 Old Pineville, LLC, enclosed please find a copy of the
Brownfields Assessment Report prepared for the Blythe Isenhour Brownfields property located
in Charlotte, Mecklenburg County.

Should you have questions or need additional information, please do not hesitate to contact us at
[phone].

Sincerely,
Hart & Hickman, PC
Haley Martin, PG Ralph McGee, PG
Assistant Project Geologist Project Manager

Enclosure:

cc: Mr. Chris Branch, Boulevard Real Estate Advisors (Via Email)
Mr. Michael Bender, Boulevard Real Estate Advisors (Via Email)
Ms. Amanda Kitchen Short, McGuireWoods (Via Email)
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Brownfields Assessment Report
Blythe Isenhour
4920 Old Pineville Road
Charlotte, North Carolina
Brownfields Project No. 23067-19-060
H&H Job No. BOU-014

Table of Contents

1.0 Introduction .............................................................................................................................1 
1.1 Background ............................................................................................................................1 
1.2 Previous Assessment Activities .............................................................................................2 
2.0 Brownfields Assessment Activities ........................................................................................6 
3.0 Receptor Survey ......................................................................................................................8 
4.0 Soil Assessment Activities .....................................................................................................11 
4.1 Soil Sampling Methodologies .............................................................................................11 
4.2 Soil Sampling Analytical Results ........................................................................................13 
5.0 Groundwater Assessment Activities ....................................................................................15 
5.1 Groundwater Sampling Activities .......................................................................................15 
5.2 Groundwater Sample Analytical Results .............................................................................17 
6.0 Soil Gas Assessment Activities .............................................................................................19 
6.1 Soil Gas Sampling Activities ...............................................................................................19 
6.2 Soil Gas Sample Analytical Results ....................................................................................21 
6.3 Vapor Intrusion Evaluation .................................................................................................21 
7.0 Quality Assurance – Quality Control ..................................................................................23 
7.1 Trip Blank ............................................................................................................................23 
7.2 Laboratory Duplicates .........................................................................................................23 
8.0 Summary and Conclusions ..................................................................................................25 

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List of Tables

Table 1 Summary of Soil Analytical Data
Table 2 Summary of Well Construction and Groundwater Elevation Data
Table 3 Summary of Groundwater Analytical Data
Table 4 Summary of Soil Gas Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Receptor Survey Map
Figure 4 Sample Location Map
Figure 5 Shallow Groundwater Hydraulic Gradient Map

List of Appendices

Appendix A Brownfields Receptor Survey Form
Appendix B Boring Logs & Well Construction Records
Appendix C Laboratory Analytical Reports
Appendix D Groundwater Sampling Forms
Appendix E DEQ Risk Calculators

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Brownfields Assessment Report
Blythe Isenhour
4920 Old Pineville Road
Charlotte, North Carolina
Brownfields Project No. 23067-19-060
H&H Job No. BOU-014

1.0 Introduction

On behalf of Boulevard at 4920 Old Pineville, LLC (Prospective Developer or PD), Hart &
Hickman, PC (H&H) has prepared this report to document assessment activities recently
completed at the Blythe Isenhour Brownfields property (Brownfields Project No. 23067-19-060)
located at 4920 Old Pineville Road in Charlotte, Mecklenburg County, North Carolina (Site).
The Site consists of one parcel (Parcel Identification No. 16907609) totaling approximately 1.67
acres of land located in a primarily industrial and commercial area of lower South End Charlotte.
A Site location map is provided as Figure 1, and the Site and surrounding area are shown in
Figure 2.

The Site is developed with an approximate 1,800 square foot (sq ft) office building and an
approximate 3,900 sq ft warehouse building. Proposed redevelopment of the Brownfields
property includes razing the existing Site buildings and construction of a high-density residential
townhome community with associated parking areas and access roads.

1.1 Background

Historically, the Site primarily consisted of land used for agricultural purposes as early as the
1930s and remained undeveloped land until the current office and warehouse buildings were
constructed in the early 1960s. Following construction of the on-Site buildings, the Site was
occupied by a general contractor business from the 1960s until the 1990s. In the late 1990s to
early 2000s, the Site was occupied by an environmental emergency response and remediation
contractor (Four Seasons Environmental). During that time, the Site was improved with a
concrete secondary containment system for above ground storage tanks (ASTs) located in the
south-central portion of the Site and a curbed concrete pad was constructed in the central portion
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of the Site (Figure 2). In the mid-2000s, an abandoned railcar was staged in the northeastern
portion of the Site and remains near the northern Site boundary. The Site has been occupied by
Heartwood Tree Services since 2003. Heartwood Tree Service operations include fleet vehicle,
tree service equipment, and materials staging, fleet vehicle fueling, administrative offices, and
tree clearing debris processing activities.

1.2 Previous Assessment Activities

H&H has completed review of available environmental reports documenting assessments
previously completed at the Site. A brief summary of each assessment is provided below and
locations of applicable previously collected environmental samples are shown in Figure 3.

1990 UST Closure Activities
On April 27, 1990, one 3,000-gallon gasoline underground storage tank (UST) was removed
from the Site. The UST was located in the eastern portion of the Site adjacent to the storage
building (Figure 2). Upon removal of the UST from the basin, soil samples were collected from
the sidewalls and base of the excavation for analysis of total petroleum hydrocarbons as diesel-
range organics (TPH-DRO) and TPH as gasoline-range organics (TPH-GRO). Analytical results
of the closure soil samples indicated that no compounds were detected above the laboratory
reporting limits. UST removal activities and initial abatement assessment results are
documented in the Limited Site Assessment Report prepared by Aquaterra, Inc. and dated July 9,
1990.

Following the 3000-gallon UST removal, DEQ requested collection of soil samples for
laboratory analysis below the associated dispenser and product lines. In September and October
2003, soil samples were collected and submitted for analysis of TPH-GRO. Laboratory
analytical results indicated that no compounds were detected at concentrations above the
laboratory reporting limits in the dispenser island and product line soil samples collected. The
sampling activities are documented in two letters completed by Froehling & Robertson, Inc.
dated October 6, 2003 and October 28, 2003. Based on results of the additional soil sampling
activities, the North Carolina Department of Environmental Quality (DEQ) UST Section issued a
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No Further Action (NFA) letter for the 3000-gallon UST closure on October 29, 2003.

2001 Spill Incident
In February 2001, a tank overturned at the Site and released approximately 4,000-gallons of used
oil and water onto the ground surface west of a curbed concrete pad located in the central portion
of the Site (Figure 2). According to a Soil Cleanup Report prepared by MACTEC and dated
June 20, 2003, soil samples identified as 1, 2, and 3 (Figure 3) were collected in May 2003 for
laboratory analysis of TPH as oil and grease from areas impacted by the spill. Laboratory
analytical results indicated that compound concentrations were detected above the DEQ
screening criteria at the time of 250 milligrams per kilogram (mg/kg). Based on the soil sample
analytical results, approximately 1,564-tons of impacted soil was excavated in the western
portion of the Site and transported to the BFI Landfill located in Concord, North Carolina.
Following excavation activities, thirteen confirmation soil samples were collected and analyzed
for TPH as oil and grease to confirm impacts were adequately removed. Analytical results
indicated that no compounds were detected at concentrations above the DEQ screening criteria in
the thirteen confirmation soil samples.

July 2003 Phase I ESA
In July 2003, MACTEC performed Phase I Environmental Site Assessment (ESA) activities at
the Site. Results of the Phase I ESA identified staining near the ASTS located in the south-
central portion of the Site as an environmental concern. The ESA report also indicated that Four
Seasons Environmental staged fluids recovered from hazardous material spills and storage tanks
in the central portion of the Site. The recovered fluids were stored and mixed with sawdust for
solidifying on a curbed concrete pad located in the central portion of the Site.

Based on findings in the July 2003 Phase I ESA, MACTEC collected two soil samples for
laboratory analysis of TPH-GRO and TPH-DRO in the area of staining observed near the ASTs.
Laboratory analytical results indicated the presence of TPH-DRO and TPH-GRO concentrations
in soil sample B-1 (Figure 3) above the DEQ screening criteria at the time. Based on the
detected TPH-DRO and TPH-GRO concentrations, MACTEC recommended the stained areas be
excavated to a depth of approximately 4 feet below ground surface (ft bgs). MACTECs findings
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are documented in the Report of Regulatory File Review, Soil Sampling and Analysis report
dated August 12, 2003. No documentation for removal of the impacted soil reported by
MACTEC was available for review.

October 2019 Phase I ESA
In October 2019, H&H conducted Phase I ESA activities at the Site. The results of the Phase I
ESA identified the following potential environmental concerns in connection with the Site:
 Based on review of available information, H&H was unable to obtain documentation
confirming soil impacts in the area of the ASTs, identified by MACTEC in July 2003,
were remediated to levels below DEQ screening criteria. As such, reported soil impacts
in the area of the on-Site ASTs identified by MACTEC were identified as an
environmental concern.

 H&H observed a curbed concrete pad located in the central portion of the Site used for
staging various Heartwood Tree Service equipment and materials. According to
information provided in the July 2003 MACTEC Phase I ESA report, the concrete pad
was formerly used by Four Seasons Environmental for solidification of waste fluids
recovered during responses to hazardous waste spills and from USTs prior to closure
activities. During Site reconnaissance, the concrete pad appeared to be in good condition
with no obvious evidence of drains, sumps, or significant staining or cracks. The
historical use of the concrete pad located in the central portion of the Site for
solidification of waste fluids was identified as a potential environmental concern.

 Although the 2001 tanker spill discussed above was reportedly remediated to levels
below DEQ screening criteria, the potential for residual impacts to the Site was identified
as a potential environmental concern.

 The property located adjacent to the south and topographically cross-gradient of the Site
is identified as the Old Pineville Road Brownfields Property (BPN 10061-06-060, see
Figure 2). According to a review of available information, ECS conducted Phase II ESA
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sampling activities at the south adjacent property in March 2007. Results of Phase II
ESA activities did not identify compounds at concentrations exceeding the DEQ
screening criteria in sediment, surface water, soil, or groundwater. The potential for
impact to the Site from an undocumented release on the adjacent Old Pineville Road
Brownfields property was identified as a potential environmental concern.

In addition to the above, the Site is located in an area of Charlotte historically developed for
industrial and commercial uses. Multiple release incidents are reported on nearby off-Site
properties in available environmental databases. Additionally, properties located in the
immediate Site area have historically included automotive repair operations, a chemical
manufacturing facility, and refinery that likely used certain petroleum products and/or
chlorinated solvents. The potential for impact to the Site from potential undocumented releases
on nearby off-Site properties was identified as a potential environmental concern.

To address potential environmental concerns associated with historical on-Site and nearby
off-Site operations, the PD entered the Site into the DEQ Brownfields Program Redevelopment
Now option and received eligibility in a letter dated January 13, 2020. As part of the
Brownfields process, a kick-off/data gap meeting with PD, legal counsel for the PD, DEQ
Brownfields personnel, and H&H was held on January 23, 2020 to discuss prior Site history,
proposed redevelopment plans, data gaps, and the proposed schedule for completing the
Brownfields agreement. To address DEQ Brownfields concerns and requests for Site assessment
activities, H&H prepared a Brownfields Assessment Work Plan (Work Plan) for DEQ review
and approval. The Work Plan received DEQ-approval in an email dated February 14, 2020.

Brownfields assessment activities described herein were completed to further evaluate the
potential for impacts at the Site for the protection of future Site workers and occupants. To
further evaluate for potential impacts at the Site, H&H completed soil, groundwater, and soil gas
assessment activities. In addition, H&H collected background soil samples to establish Site-
specific ranges for naturally occurring metals. H&H also conducted receptor survey activities in
the area surrounding the Site as part of the assessment. A summary of Brownfields assessment
activities conducted in accordance with the Work Plan is provided in the following sections.
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2.0 Brownfields Assessment Activities

In March 2020, H&H completed Brownfields assessment activities including soil, groundwater,
and soil gas sampling activities at the Site to evaluate subsurface conditions for potential impacts
associated with historical on-Site and nearby off-Site operations. In addition, receptor survey
activities were completed to obtain information about land use, water supply, basements,
underground utilities, drains, and surface water bodies in the vicinity of the Site.

As part of the assessment activities, soil and groundwater samples were collected in the area of
the on-Site AST containment area and former chemical storage and solidification pad. H&H
also completed groundwater assessment activities along the western (downgradient), southern
(cross-gradient) and eastern (upgradient) Site boundaries. To address the potential for structural
vapor intrusion into proposed townhome buildings, H&H completed exterior soil gas assessment
activities within the footprint of proposed townhome buildings.

Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator,
to mark subsurface utilities at the Site. H&H also contracted with a private utility locator to
mark utilities which were not identified by the public locator. The private utility locator also
utilized ground penetrating radar (GPR) survey techniques to identify and mark utilities.

H&H directed the drilling contractor to hand clear each boring to a depth of approximately 5 ft
bgs to further screen the boring locations for the presence of subsurface utilities. In accordance
with Mecklenburg County rules, H&H obtained a Subsurface Investigation Permit (SIP) from
Mecklenburg County (SIP No. 70002730) prior to temporary monitoring well installation and
sampling.

The assessment activities were performed in general accordance with the DEQ Inactive
Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated Sites
(Guidelines) dated January 2020, the DEQ Division of Waste Management (DWM) Vapor
Intrusion Guidance (VI Guidance) dated March 2018, most recent versions of the U.S.
Environmental Protection Agency (EPA) Region IV Science and Ecosystem Support Division
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(SESD) Field Branches Quality System and Technical Procedures guidance, and the DEQ-
approved Work Plan. A summary of receptor survey results is provided in Section 3.0; details of
the soil assessment activities are provided in Section 4.0; details of the groundwater assessment
activities are provided in Section 5.0; details of the soil gas assessment activities are provided in
Section 6.0; quality assurance and quality control measures are provided in Section 7.0; and
summary and conclusions based on results of the assessment activities are provided in Section
8.0.
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3.0 Receptor Survey

On March 2, 2020, H&H conducted receptor survey activities at the Site and nearby area.
Receptor survey activities included an intensive pedestrian and vehicular survey for possible
potable water supply wells, springs, and surface water intakes used as a source of water within a
1,500 ft radius of the Site in accordance with the DEQ Brownfields approved Work Plan. H&H
also utilized the online Mecklenburg County Well Information System and DEQ Source Water
Assessment Program (SWAP) to identify potential potable water sources for properties located
within a 1,500 ft radius of the Site. In addition, H&H identified the locations of main
underground and aboveground utilities, and land use and zoning in the area of the Site using
available Mecklenburg County online resources. A receptor survey map is provided as Figure 3
and a copy of the completed DEQ Brownfields Property Receptor Survey form is provided as
Appendix A. Results of the receptor survey activities are summarized below.

Zoning
The Site is zoned Commercial Center Transit Oriented Development (TOD-CC). The adjacent
properties located to the north, west, and south of the Site are also zoned TOD-CC. Adjacent
properties to the east and southeast, across Old Pineville Road, are zoned Shopping Center
District (B-1SCD) and general industrial (I-2).

Municipal Water Availability
Municipal water supplied by the City of Charlotte is available to the Site and surrounding area.
H&H did not identify sources of public drinking water within 1,500 ft of the Site based on the
review of information available on Mecklenburg County Well Information System maps, DEQ
SWAP, and the Annual Water Quality Report published by the City of Charlotte. The City of
Charlotte obtains raw water from Lake Norman and Mountain Island Lake which are located
approximately 12 miles north of the Site at Mountain Island Lake’s closest point.

H&H reviewed the service area map published by Mecklenburg County which indicated that
municipal water is available to the Site and the surrounding area within a 1,500 ft radius of the
Site. Additionally, H&H observed municipal water meters for the Site and surrounding
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properties during receptor survey reconnaissance activities.

Water Supply Wells
H&H conducted a pedestrian and vehicular survey of properties within a 1,500 ft radius of the
Site to identify potential water supply wells. H&H also utilized Mecklenburg County Well
Information System maps and a DEQ SWAP geographic information system map to identify
potential potable water supply wells located within a 1,500 ft radius of the Site. According to the
Mecklenburg County Well Information System map there is one private drinking water supply
well within the 500 ft to 1,000 ft radius of the Site. Two private water supply wells are located
within the 1,000 ft to 1,500 ft radius of the Site. The approximate locations of the water supply
wells identified during receptor survey activities are shown in Figure 3. The property addresses
associated with each identified water supply well are provided in the DEQ Brownfields Property
Receptor Survey form (Appendix A).

Surface Water Bodies
No surface water bodies were identified on the Site. A stormwater drainage feature is reportedly
located in the western portion of the south adjacent property. An unnamed tributary of Kings
Branch is located approximately 400 ft west of the Site at its closest point (Figure 3). Based on
the North Carolina DEQ classification system, Irwin Creek is a Class C surface water body. A
Class C surface water body is defined as “waters protected for uses such as secondary recreation,
fishing, wildlife, fish consumption, aquatic life including propagation, survival and maintenance
of biological integrity, and agriculture. Secondary recreation includes wading, boating, and other
uses involving human body contact with water where such activities take place in an infrequent,
unorganized, or incidental manner”. Kings Branch is located approximately 6,000 ft southwest
of the Site and flows southwest through Mecklenburg County and discharges into Sugar Creek
approximately 4.5 miles southwest of the Site.

Subsurface Structures
H&H contacted North Carolina 811, the public utility locator, to mark subsurface utilities located
on the Site and conducted a visual reconnaissance in the Site area to identify potential subsurface
structures within 100 ft of the subject Site. H&H observed evidence of subsurface utilities
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including sanitary sewer, storm sewer, municipal water, natural gas, electrical, and fiber adjacent
to the Site and nearby adjacent properties. Over-head electrical lines were observed near the
eastern Site boundary along Old Pineville Road. H&H did not observe structures with potential
basements within a 1,000 ft radius of the Site during visual reconnaissance. Approximate
locations of subsurface and overhead utilities located in the immediate vicinity of the Site are
shown in Figure 3.
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4.0 Soil Assessment Activities

On March 3 and 4, 2020, H&H teamed with Innovative Environmental Technologies (IET) to
advance soil borings at the Site in the area of the former waste storage and solidification pad
located in the central portion of the Site, and in the vicinity of the AST secondary containment
system located in the south-central portion of the Site. H&H collected two (2) composite soil
samples and two (2) grab samples for laboratory analysis from seven (7) soil borings to evaluate
the potential for impacts. In addition, two (2) background soil samples were collected for
laboratory analysis to establish Site-specific background concentrations for naturally occurring
metals. Soil boring locations are depicted on Figure 4.

Soil borings were advanced at the Site using decontaminated stainless steel hand augers or a
track-mounted drill rig capable in utilizing direct push technology (DPT) drilling techniques.
Continuous soil samples were collected from the center of the hand auger bucket or from acetate
lined macrocore DPT sleeves at each boring. Soil samples were logged for lithologic
description, observed for obvious evidence of staining and unusual odors, and field screened for
the presence of volatile organic vapors using a calibrated photoionization detector (PID). Based
on field screening results, H&H collected an additional soil sample for laboratory analysis from
soil gas monitoring point boring for SGP-5 advanced in the south-central portion of the Site near
a storage shed (Figure 4). Boring logs including lithologic descriptions and field screening
results for each soil boring are provided in Appendix B.

Details of the soil sampling activities and results are provided in the following sections.

4.1 Soil Sampling Methodologies

Former Waste Storage and Solidification Pad
IET utilized a decontaminated stainless-steel hand auger to advance four (4) soil borings (SB-1A
through SB-1D) at a depth of approximately 3 ft bgs adjacent to each side of the concrete pad
located in the central portion of the Site (Figure 4). During boring advancement, aliquot soil
samples were collected at one-foot intervals from each boring. Field screening results did not
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identify evidence of potential impact in the soil samples. As such, aliquot soil samples were
collected from the depth interval interpreted to be below the base of the concrete pad (2 to 3 ft
bgs). The soil sample aliquots collected from each soil boring were combined and homogenized
to form a composite soil sample (COMP-1). In addition, one grab soil sample was collected
from an undisturbed portion of the 2-3 ft soil sample aliquot collected from the SB-1A soil
boring advanced topographically downgradient of the former waste storage and solidification
pad.

AST Containment Basin
Three (3) soil borings (SB-2A through SB-2C) were advanced to a depth of approximately 3 ft
bgs adjacent to each side of the AST containment basin located in the south-central portion of the
Site (Figure 4). During boring advancement, aliquot soil samples were collected at one-foot
intervals from each boring. Field screening results did not identify evidence of potential impact
in the soil samples. Similar to the area of the concrete pad, aliquot soil samples were collected
from the depth interval interpreted to be below the base of the AST secondary containment
system (2 to 3 ft bgs). The soil sample aliquots collected from each soil boring were combined
and homogenized to form a composite soil sample (COMP-2). In addition, one grab soil sample
was collected from an undisturbed portion of the 2-3 ft soil sample aliquot collected from the
SB-2A soil boring advanced topographically downgradient of the AST secondary containment
system.

South-Central Storage Building
Soil boring SGP-5 was advanced for installation of a soil gas sampling point in the south-central
portion of the Site near the existing storage shed (Figure 4). During boring advancement, aliquot
soil samples were collected at two-foot intervals from the SGP-5 soil boring for field screening.
Field screening results indicated PID readings up to ranging approximately 750 parts per million
(ppm). Based on field screening results, H&H collected a grab soil sample for laboratory
analysis from the 2-4 ft depth interval where the highest PID reading was observed to evaluate
the potential for impacts in the area of the storage shed.

Soil samples selected for laboratory analysis in each evaluation area were collected directly into
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laboratory supplied glassware, labeled with the sample identification, date, time, and requested
analysis and placed in a laboratory supplied cooler with ice. The soil samples were delivered to
Pace Analytical (Pace) under standard chain of custody protocols. The composite soil samples
were submitted for analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270
and Resource Conservation and Recovery Act (RCRA) metals plus hexavalent chromium by
EPA Methods 6020/7471/7199. The grab soil samples sample were submitted for analysis of
volatile organic compounds (VOCs) by EPA Method 8260. In addition, the SB-1A grab soil
sample collected downgradient to the concrete pad was submitted for analysis of polychlorinated
biphenyls (PCBs) by EPA Method 8082. The SGP-5 grab soil sample was submitted for
laboratory analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA
metals plus hexavalent chromium by EPA Methods 6020/7471/7199.

In addition to the soil samples described above, H&H also collected two (2) shallow background
soil samples to establish Site-specific background concentrations for naturally occurring metals.
Soil sample locations (denoted by BG nomenclature) are depicted on Figure 4. Background soil
sample BG-1 was collected from 1-3 ft bgs in the eastern portion of the Site and background soil
sample BG-2 was collected from 1-3 ft bgs in the western portion of the Site. Background soil
samples were submitted for laboratory analysis of RCRA metals plus hexavalent chromium by
EPA Methods 6020/7471/7199.

Following sampling activities, the soil borings were properly abandoned and the surfaces were
repaired similar to pre-drilling conditions. Additionally, the soil sample locations were estimated
using a hand-held global positioning system (GPS) unit.

4.2 Soil Sampling Analytical Results

A tabular summary of the soil sample analytical results is presented in Table 1 and the laboratory
analytical reports and chain of custody records are provided in Appendix C. The laboratory
analytical results were compared to the most recent versions of the DEQ IHSB Residential and
Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated December 2019. In
addition to the PSRGs, metals results were compared to published concentrations for naturally
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occurring metals in North Carolina soil as well as Site-specific background levels established by
soil samples BG-1 and BG-2.

Laboratory analytical results indicate that several petroleum-related compounds were detected at
concentrations above laboratory method detection limits in the SGP-5 soil sample collected in
the area of south-central storage shed. No organic compounds were detected at concentration
above the DEQ IHSB Residential PSRGs in the SGP-5 soil sample. Aside from trace levels of
acetone (a common laboratory introduced contaminant), no other organic compounds (including
PCBs) were detected at concentrations above the laboratory method detection limits in soil
samples collected in the remaining evaluation areas.

As expected, several metals were detected at concentrations above laboratory method detection
limits in the background soil samples collected at the Site. Metal concentrations detected in the
soil samples are consistent with both published and Site-specific background levels. Based on
results of Brownfields soil assessment activities, metal concentrations detected in soil samples
collected at the Site appear to be naturally occurring.
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5.0 Groundwater Assessment Activities

On March 3, 2020, H&H provided oversight during installation of four (4) temporary
groundwater monitoring wells (TMW-1 through TMW-4) at the Site. Groundwater samples
were collected for laboratory analysis from each temporary monitoring well to evaluate
subsurface conditions for potential impacts. Locations of the temporary monitoring wells are
depicted on Figure 4, and were installed in the following locations:
 topographically downgradient of the former waste solidification pad (TMW-1);
 topographically upgradient near the eastern Site boundary (TMW-2);
 topographically cross-gradient to the former Queen City Boiler facility (TMW-3); and
 topographically downgradient area near the western Site boundary (TMW-4). 
Details of the groundwater sampling activities and results are provided in the following sections.

5.1 Groundwater Sampling Activities

The temporary monitoring well borings were advanced using the track-mounted DPT drill rig to
advance soil borings until sufficient groundwater was encountered. Continuous soil samples
were collected from the temporary monitoring well borings and logged for lithologic description,
observed for obvious evidence of staining and unusual odors, and field screened for the presence
of volatile organic vapors using a calibrated PID. Field screening results did not indicate the
likely presence of impacts in soil collected from the temporary monitoring well borings.

Temporary monitoring wells were constructed of 1-inch diameter PVC with 10 to 15 ft of
pre-packed well screen set to bracket the water table and 1-inch diameter PVC well casing to the
ground surface. Temporary monitoring wells were installed to depths ranging from
approximately 13 to 25 ft bgs. A filter sand pack was installed from the bottom of each
temporary well boring to approximately 2 ft above each well screen, and a hydrated bentonite
seal was then installed above the filter sand pack. Due to shallow groundwater encountered in
the western portion of the Site, temporary well TMW-4 was constructed with filter sand pack
from the bottom of the boring to approximately one foot above the well screen, and a 2 ft
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hydrated bentonite was then installed above the filter sand pack. A summary of well
construction and groundwater elevation information is provided in Table 2. Temporary
monitoring well boring logs with well construction details and driller provided well records are
provided in Appendix B.

Upon completion of temporary monitoring well installation activities, the wells were allowed to
equilibrate to static conditions and a decontaminated electronic water level indicator was used to
measure the depth to the water table relative to the ground surface and the tops of the well
casings. Groundwater was measured at depths ranging from approximately 5 ft bgs in the
western portion of the Site to approximately 15 ft bgs in the eastern portion of the Site. Once
groundwater measurements had been collected, each temporary well was developed by removing
a minimum of 3 to 5 well volumes and field parameters stabilized (pH ± 0.1 Standard Units [SU]
and specific conductivity varied no more than 5%).

After development, a groundwater sample was collected for laboratory analysis from each
temporary monitoring well utilizing low flow/low stress purging techniques using a peristaltic
pump and dedicated polyethylene tubing. The intake point of the pump tubing was placed in the
approximate mid-portion of the screened interval of the well and groundwater was removed at a
rate no greater than 200 milliliters per minute. H&H utilized water quality meters to collect
measurements of pH, temperature, dissolved oxygen, oxidation reduction potential, turbidity, and
specific conductivity during the purging process. Purging was considered complete when field
parameters stabilized (pH ± 0.1 SU, conductivity varied no more than 5% and turbidity was near
or less than 10 Nephelometric Turbidity Units [NTUs]). Groundwater sampling forms
completed by sampling personnel are provided in Appendix D.

Once groundwater parameters stabilized, groundwater samples for VOC analysis were collected
directly into laboratory supplied sample containers using the “soda straw” method to minimize
volatile loss through the peristaltic pump head. Groundwater samples submitted for remaining
analyses were collected directly into laboratory supplied glassware directly from the sample
tubing discharge. The sample containers were labeled with the sample identification, date, time,
and requested analysis, and placed in a laboratory supplied cooler with ice. The samples were
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delivered to Pace under standard chain of custody protocols for analysis of VOCs by EPA
Method 8260, SVOCs by EPA Method 8270, and RCRA metals by EPA Method 6020/7471.

Following sample collection, H&H surveyed the top of casing (TOC) and ground surface
elevations for each temporary monitoring well relative to an on-Site datum. The surveyed TOC
elevations and the measured depths to groundwater were used to calculate groundwater
elevations for each temporary monitoring well. Based on the calculated groundwater elevations,
groundwater flow direction was estimated to be toward the west in the western portion of the Site
and to the east in the eastern portion of the Site. A shallow groundwater hydraulic gradient map
is provided as Figure 5.

Upon completion of the groundwater assessment activities, each temporary monitoring well
location was estimated using a hand-held GPS unit. The temporary monitoring wells were
properly abandoned and the surfaces were repaired similar to pre-drilling conditions.

5.2 Groundwater Sample Analytical Results

A tabular summary of the groundwater sample laboratory analytical results is presented in
Table 3. Copies of the laboratory analytical report and chain of custody records are provided in
Appendix C. Groundwater data were compared to the DEQ 15A NCAC 02L .0202 Groundwater
Standards (2L Standards) dated April 2013 and the DEQ DWM Residential and Non-Residential
Vapor Intrusion Groundwater Screening Levels (GWSLs) dated February 2018. Summary of the
groundwater assessment results is provided below.

Laboratory analytical results indicate that toluene (up to 1.7 microgram per liter [µg/L]) was
detected at concentrations above laboratory method detection limits, but below the 2L Standard
and DEQ DWM GWSLs in the TMW-2 and TMW-3 groundwater samples collected in
upgradient and cross-gradient portions of the Site (Figure 4). No other organic compounds were
detected at concentrations above the laboratory reporting limits in the remaining groundwater
samples collected at the Site.
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Low levels of several metals including arsenic (up to 0.646 J µg/L), barium (up to 94.0 µg/L),
cadmium (0.173 J µg/L), and selenium (up to 0.410 µg/L) were detected at concentrations above
the laboratory method detection limits, but below the 2L Standards in groundwater samples
collected at the Site. Note that the J-flag designation (J) indicates the compound was detected at
a concentration above the laboratory method detection limit, but below the laboratory reporting
limit resulting in the laboratory analyst estimating the concentration.

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6.0 Soil Gas Assessment Activities

On March 5 and March 9, 2020, H&H completed soil gas assessment activities at the Site to
evaluate the potential for structural vapor intrusion into proposed townhome buildings. As part
of the soil gas assessment activities, seven (7) temporary soil gas monitoring points (SGP-1
through SGP-7) were installed within the footprints of proposed residential townhome buildings.
The soil gas sample locations are shown in Figure 4. Details of the assessment activities and
results are provided in the following sections.

6.1 Soil Gas Sampling Activities

Under the direction of H&H, IET advanced seven (7) soil borings to depths ranging from 5 ft bgs
to 12 ft bgs for installation of temporary exterior soil gas sampling points in areas of the Site that
will be redeveloped with residential townhome buildings. Temporary exterior soil gas
monitoring point borings were installed to varying depths depending on the measured depth to
groundwater in the nearest temporary monitoring well.

The initial 5 ft of each soil boring was advanced using a stainless-steel hand auger to clear for
subsurface utilities. Beyond the initial 5 ft bgs, the soil borings were advanced using DPT
drilling methods. Continuous soil samples were collected from the soil gas sampling point
borings and logged for lithologic description, observed for obvious evidence of staining and
unusual odors, and field screened for the presence of volatile organic vapors using a calibrated
PID. As discussed in Section 4.1 above, elevated PID readings were observed in soil samples
collected from the SGP-5 soil boring. Field screening results did not indicate obvious evidence
of potential impacts in other soil gas sampling point borings.

Once at depth, a six-inch stainless-steel vapor implant screen point fitted with ¼-inch diameter
Teflon® tubing was installed at the base of each borehole. Filter sand was then placed from the
base of the boring to approximately 6 inches above the top of the stainless-steel screen. The
sampling points were completed by placing hydrated bentonite from the top of the filter sand to
the ground surface. The soil gas boring logs including lithologic descriptions, field screening
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results, and soil gas sampling point construction details are provided in Appendix B.

A laboratory-supplied 1-liter stainless steel Summa sample canister was connected to an in-line
flow controller with a vacuum gauge that was subsequently connected to the Teflon® sample
tubing at each sampling point using a brass nut and ferrule assembly to form an air-tight seal.
The airflow regulator was pre-set by the laboratory to regulate the vapor intake rate to
approximately 100 milliliters per minute.

Prior to sample collection, a leak check was conducted at the soil gas sampling points by
constructing a shroud around the sample train and flooding the air within the shroud with helium
gas. Helium concentrations inside the shroud were measured using a helium gas detector and
maintained at concentrations of approximately 15% to 30%. Using a syringe and three-way
valve, the sand filter pack, the vapor implant screen, and Teflon tubing were purged of
approximately three sample volumes. Following purging, a sample was collected from the
sample tubing outside the shroud into a Tedlar® bag and analyzed using the helium gas detector
to ensure that helium concentrations were less than 10% of the helium concentrations in the
shroud. Each soil gas sampling point passed the helium leak check criteria.

Following a successful leak check, the intake valve on the canister was fully opened to begin
collection of the soil gas sample. Vacuum readings on the Summa canister were recorded prior
to and following the approximate ten-minute sampling period to ensure adequate sample volume
was collected. A vacuum was maintained within each summa canister at the conclusion of the
sampling event per laboratory standard operating procedures.

After sample collection, the Summa canister valve was closed prior to the regulator being
disconnected from the canister and the Summa canisters were then placed in laboratory supplied
shipping containers, properly labeled, and shipped under standard chain-of-custody protocols to
ConTest Analytical Laboratory for analysis of VOCs by EPA Method TO-15. Upon receipt of
the samples, the laboratory recorded the final received vacuum pressure for each Summa
canister.
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Following sampling, the soil gas sampling points were estimated using a GPS unit, and were
properly abandoned. The surfaces were repaired similar to pre-drilling conditions.

6.2 Soil Gas Sample Analytical Results

A tabular summary of the soil gas sample analytical results is provided as Table 4. The
laboratory analytical report and chain of custody records are provided in Appendix C. The
analytical results were compared to DEQ DWM Residential and Non-Residential Vapor
Intrusion Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) dated February 2018.

Laboratory analytical results for the soil gas samples indicate the presence of several compounds
at concentrations above the laboratory method detection limits in each sample. Petroleum-
related compounds 1,2,4-trimethylbenzene (4,200 microgram per cubic meter [µg/m3]) and
1,3,5-trimethylbenzene (3,700 µg/m3) were detected in soil gas sample SGP-5 at concentrations
exceeding the Residential SGSL of 420 µg/m3. In addition, naphthalene (220 µg/m3) was
detected in soil gas point SGP-3 at a concentration exceeding the Residential SGSL of 21 µg/m3.
No other compounds were detected at concentrations above the Residential SGSLs in the
remaining soil gas sample and no compounds were detected at concentrations exceeding the
Non-Residential SGSLs.

6.3 Vapor Intrusion Evaluation

The DEQ DWM Vapor Intrusion SGSLs used for comparison to the laboratory analytical results
are conservative and based upon a cumulative lifetime incremental carcinogenic risk (LICR) of
1 x 10-5 for potential carcinogenic effects and a cumulative hazard quotient (HQ) of 0.2 for
potential non-carcinogenic effects. Vapor intrusion mitigation or additional assessment is not
typically warranted if the calculated cumulative LICR is less than 1 x 10-4 and a calculated
cumulative Hazard Index (HI) is less than 1.0.

H&H utilized the DEQ Risk Calculator (December 2019) assuming a residential land use
scenario to further evaluate potential cumulative risks for the soil gas to indoor air vapor
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intrusion pathway for the proposed townhome development. H&H calculated the cumulative
risks using the highest concentration of any compound detected in any soil gas sample collected
at the Site to model the potential for vapor intrusion under a hypothetical “worst-case” scenario.

Risk calculator results indicate that under a hypothetical worst-case scenario for the soil gas to
indoor air vapor intrusion pathway for residential use, the cumulative LICR is 9.6 x 10-5 and the
cumulative HI is 6.5. Risk calculator results for the soil gas to indoor air vapor intrusion
pathway for a resident indicate that the cumulative non-carcinogenic risk is greater than 1.
Copies of the completed risk calculators are provided in Appendix E.

Review of the soil gas analytical data in comparison to the residential risk calculator results
indicates that the cumulative HI value is primarily driven by the naphthalene,
1,2,4-trimethylbenzene, and 1,3,5-trimethylbenzene concentrations detected in soil gas samples
SGP-3 and SGP-5.

Typically, petroleum releases do not represent a significant vapor intrusion concern unless
compound concentrations are detected at levels consistent with the presence of free phase
product. Groundwater assessment results did not identify petroleum-related compound
concentrations at elevated levels consistent with free product in groundwater samples collected at
the Site. In addition, compound concentrations detected in soil gas samples collected across the
Site do not support the presence of free product in the subsurface and did not identify evidence
of widespread impacts.

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7.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools
were decontaminated prior to use at each boring or sampling location or following exposure to
soil or groundwater. Field QA/QC samples were analyzed along with the investigative samples
to determine potential variability introduced in sampling, handling, shipping, and analysis. One
trip blank was submitted for analysis of VOCs by EPA Method 8260. In addition, H&H
collected duplicate soil, groundwater, and soil gas samples to evaluate the ability of the laboratory
to reproduce sample results. Duplicate samples were submitted to the laboratory for the same
analysis as the corresponding parent sample.

7.1 Trip Blank

The trip blank was prepared by the laboratory and consisted of certified-clean sample containers
filled with analyte-free water. The trip blank accompanied the empty laboratory sample
containers to the Site, remained within the sample cooler during sampling, and traveled back to
the laboratory with field samples. The purpose of a trip blank is to evaluate sample handling
conditions and the potential for external contaminants to compromise investigative samples
during transit. A trip blank accompanied the field groundwater samples. Laboratory analytical
results of the trip blank did not indicate the presence of compounds at concentrations above the
laboratory method detection limits (Appendix C).

7.2 Laboratory Duplicates

Duplicate samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. Duplicate soil and groundwater
samples were collected directly into individual laboratory supplied sample containers using
sampling methodologies described in previous sections. The duplicate soil gas sample was
collected concurrently with the parent sample using a laboratory supplied T-fitting which allows
for collection of two soil gas samples from one soil gas sampling point simultaneously. The
samples were analyzed for the same parameters as the parent samples, and the analytical results
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were compared with those of the parent sample. The analytical results of the parent sample and
the duplicate sample were used to evaluate the cumulative precision of the analytical method,
sample matrix, and sample collection techniques.

Duplicate sample laboratory analytical results for each sample media are presented in the
summary tables (Table 1, Table 3, and Table 4). Review of the duplicate sample results in
comparison to the parent sample results for each media sampled indicates that there was no
significant variability and confirm adequate sampling and laboratory reproducibility.
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8.0 Summary and Conclusions

H&H completed Brownfields assessment activities at the Blythe Isenhour Brownfields property
located in Charlotte, North Carolina. The assessment activities were conducted in accordance
with the DEQ Brownfields approved Work Plan dated February 7, 2020. Brownfields
assessment activities included collection of soil, groundwater, and soil gas for laboratory analysis
to further evaluate potential risks associated with the Site and to assist in management of Site
media during proposed redevelopment activities. In addition, H&H conducted a receptor survey
to assess potential on-Site and off-Site receptors in the nearby area. A brief summary of the
Brownfields assessment activities is provided below.

 The results of the receptor survey identified the presence of three possible private water
supply wells located on properties within 1,500 ft southwest and northwest of the Site.
However, no impacts were identified in groundwater samples collected during
Brownfields assessment activities. No perennial surface water bodies were identified on
the Site or adjacent properties, and no structures with basements were identified in the
vicinity of the Site.

 Results of soil assessment activities completed in the vicinity of the former concrete
chemical storage and solidification pad, AST secondary containment area, and storage
shed did not identify organic compounds at concentrations above the DEQ IHSB
Residential PSRGs. Metal concentrations detected in soil samples collected at the Site
are consistent with published and established naturally occurring levels.

 Results of groundwater assessment activities completed in upgradient, cross-gradient, and
downgradient portions of the Site did not identify compounds at concentrations above the
DEQ 2L Standards or the DEQ DWM Vapor Intrusion GWSLs.

 Results of soil gas assessment activities completed within the footprints of proposed
residential townhomes identified petroleum-related compounds at concentrations above
the DEQ DWM Residential Vapor Intrusion SGSLs in samples collected in central
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portions of the Site. Risk calculator results using compound concentrations detected in
the soil gas samples indicate that the calculated cumulative non-carcinogenic HI exceeds
1. However, the elevated HI value is primarily driven by the petroleum-related
compound concentrations detected in the soil gas samples collected in the central portion
of the Site. As noted above, no groundwater impacts were identified at the Site including
samples collected in hydraulically downgradient areas at the Site. Therefore, compound
concentrations that exceed the acceptable vapor intrusion risk levels are petroleum-
related and appear to be present in soil at a limited extent.

In summary, results of soil assessment activities completed at the Site indicate that there is no
evidence of significant impacts in the areas of the former concrete chemical storage and
solidification pad or AST secondary containment system. Field screening results identified
evidence of potential soil impacts in the area of a storage shed located in the south-central
portions of the Site. However, no compounds were detected at concentrations above the DEQ
IHSB PSRGs. Based on the result of Brownfields soil assessment activities, soil at the Site can
be managed in accordance with a DEQ Brownfields approved Environmental Management Plan
(EMP).

Results of groundwater assessment activities indicate that no impacts were identified at
concentrations above the DEQ groundwater quality or vapor intrusion screening criteria. In the
unlikely event groundwater is encountered during future redevelopment activities, it can easily
be managed in accordance with a DEQ Brownfields approved EMP.

Hypothetical worst-case scenario risk calculator results for the soil gas to indoor air vapor
intrusion pathways exceed acceptable risk levels for residential use due to petroleum-related
compound concentrations detected in limited areas located in central portions of the Site. The
PD plans to install vapor mitigation systems for each of the proposed townhome buildings.
Based on review of the laboratory analytical data, risk evaluation results, and the limited extent
of petroleum-related impacts, potential structural vapor intrusion can be managed through
installation of passive vapor mitigation measures.

Table 1Summary of Soil Analytical DataBlythe IsenhourCharlotte, North CarolinaH&H Job No. BOU-014Evaluation AreaStorage ShedSample IDCOMP-1 SB-1A COMP-2 SB-2A SB-DUP SGP-5 BG-1 BG-2Date3/4/2020 3/4/2020 3/4/2020 3/4/2020 3/3/2020 3/3/2020Depth (ft bgs)2-3 2-3 2-3 2-4 0-3 0-3Sample Type4-point Grab 3-point GrabRange MeanUnitsPCBs (8082)NA ALL BDL NA NA NA NA NA NA -- -- -- --VOCs (8260B)AcetoneNA0.0166 JNA0.0782 J 0.0144 J 0.0592 JNA NA12,000 140,000-- --n-ButylbenzeneNA <0.0027 NA <0.0029 <0.00280.0488NA NA780 12,000-- --sec-Butylbenzene NA <0.002 NA <0.0022 <0.00210.0739NA NA1,600 23,000-- --EthylbenzeneNA <0.001 NA <0.0011 <0.00100.0015 JNA NA6.1 27-- --Isopropylbenzene (Cumene)NA <0.0014 NA <0.0015 <0.00140.0674NA NA410 2,100-- --p-Isopropyltoluene NA <0.0023 NA <0.0025 <0.00240.143NA NANE NE-- --4-Methyl-2-pentanone (MIBK)NA <0.0036 NA <0.0038 <0.00360.156NA NA7,000 30,000-- --Naphthalene NA <0.0041 NA <0.0043 <0.00420.0131NA NA4.1 18-- --n-PropylbenzeneNA <0.0016 NA <0.0017 <0.00160.163NA NA780 5,100-- --1,2,4-TrimethylbenzeneNA <0.0019 NA <0.0020 <0.001918.3NA NA63 370-- --1,3,5-TrimethylbenzeneNA <0.0016 NA <0.0017 <0.00167.0NA NA56 320-- --SVOCs (8270D)Naphthalene<0.0986 NA <0.0992 NA NA0.110 JNA NA4.1 18-- --Metals (6020/7471/7196A)Arsenic 2.46NA3.19NA NA1.73 3.676.47 0.68 3.0 1.0 - 18 4.8Barium 116NA30.6NA NA7.81 48.616.8 3,100 47,000 50 - 1,000 356Cadmium<0.110 NA <0.101 NA NA <0.109 <0.104<0.10314 200 1.0 - 10 4.3Chromium (total) 32.1NA31.4NA NA25.1 47.4122 NE NE 7.0 - 300 65Hexavalent Chromium<0.349 NA <0.321 NA NA <0.3480.415 J0.584 J 0.31 6.5 NS NSTrivalent Chromium 32.1NA31.4NA NA25.1 47.0121.4 23,000 350,000 NS NSLead 7.93NA11.0NA NA7.34 15.16.44 400 800 ND - 50 16Mercury 0.0585NA0.0675NA NA0.0478 0.08420.139 2.3 9.7 0.03 - 0.52 0.121Selenium 0.818NA0.523 JNA NA0.581 J 0.9880.673 78 1,200 <0.1 - 0.8 0.42Silver<0.212 NA <0.195 NA NA <0.211 <0.202<0.20078 1,200 ND - 5.0 NSNotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) dated December 20192) Range & mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils.Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.Aside from metals, only those compounds detected in at least one sample are shown in the table above; refer to the analytical report.ft bgs = feet below ground surface; COMP = Composite; SB = Soil Boring; SGP = Soil Gas Point boring; AST = Aboveground Storage Tank; BG = BackgroundVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; PCBs = Polychlorinated biphenylsNE = Not Established; NS= Not Specified; NA = Not Analyzed; -- = Not Applicable; BDL = Below Laboratory Method Detection Limits; ND = Not DetectedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. CompositeConcrete Storage Pad AST Containment Area Background mg/kg3/4/20202-3GrabRegional Background Metals in Soil (2)Residential PSRGs (1)Industrial/ Commercial PSRGs (1)S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Assessment\Report\Tables\Blythe Isenhour_Tables 3-19-02.xlsx4/1/2020Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Well Construction and Groundwater Elevation DataBlythe Isenhour Charlotte, North CarolinaH&H Project No. BOU-014Well IDTOC Elevation (ft)Total Depth (ft below TOC)Screen Length (ft)Static Depth to Groundwater (ft below TOC)Groundwater Elevation (ft below TOC)TMW-1 93.20 16.50 15 7.70 85.50TMW-2 100.00 24.00 15 15.10 84.90TMW-3 102.13 24.00 15 15.10 87.03TMW-4 89.29 13.00 10 5.61 83.68Notes:Depth to groundwater measurements collected on March 4, 2020.Elevations were surveyed by H&H relative to an arbitrary datum of 100 ft at TMW-2.TMW = temporary monitoring well; TOC = top of casing; ft = feetS:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Assessment\Report\Tables\Blythe Isenhour_Tables 3-19-024/3/2020Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3Summary of Groundwater Analytical DataBlythe IsenhourCharlotte, North CarolinaH&H Job No. BOU-014Sample LocationBackground Cross-Gradient DowngradientSample IDTMW-2 TMW-3 TMW-4Date1/22/2019 1/22/2019 1/22/2019UnitsVOCs (8260B)Toluene<0.24 <0.240.28 J 1.7<0.24600 3,800 16,000SVOCs (8270D)Metals (6010D/7470A)Arsenic0.646 J <0.250 <0.2500.317 J<0.25010-- --Barium52.8 53.4 94.0 29.1 11.5700-- --Cadmium<0.160 <0.1600.173 J<0.160 <0.1602-- --Total Chromium1.12 J 1.12 J 0.861 J 2.32 0.635 J10-- --Lead<0.240 <0.240 <0.240 <0.240 <0.24015-- --Mercury<0.0490 <0.0490<0.0490<0.0490<0.04901 0.18 0.75Selenium0.410 J<0.3800.393 J<0.380 <0.38020-- --Silver<0.310 <0.310 <0.310 <0.310 <0.31020-- --Notes:1) NC Department of Environmental Quality (DEQ) 15A North Carolina Administrative Code 02L.0202 Groundwater Quality Standard (2L Standard) dated April 20132) DEQ Division of Waste Management (DWM) Vapor Intrusion Groundwater Screening Levels (GWSLs) dated February 2018Concentrations are reported in micrograms per liter (μg/L).Concentrations are reported to the laboratory method detection limits. Laboratory analytical methods are shown in parentheses.Aside from metals, only those compounds detected in at least one sample are shown in the table above.TMW = Temporary Monitoring Well; DUP = Duplicate; VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic CompoundsBDL = Below Laboratory Method Detection Limits; -- = Not ApplicableJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.-- --Concrete Storage Pad2L Standard (1)Residential GWSLs (2)Non-Residential GWSLs (2)µg/LTMW-1/TMW-DUP1/22/2019All BDL All BDL All BDL All BDL All BDL --S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Assessment\Report\Tables\Blythe Isenhour_Tables 3-19-02.xlsx4/1/2020Table 3 (Page 1 of 1)Hart & Hickman, PC
Table 4Summary of Soil Gas Analytical DataBlythe IsenhourCharlotte, North CarolinaH&H Job No. BOU-014Sample LocationSample IDSGP-1 SGP-2 SGP-3 SGP-4 SGP-5 SGP-6Date3/5/2020 3/5/2020 3/5/2020 3/9/2020 3/9/2020 3/9/2020Depth (ft bgs)55105812UnitsVOCs (TO-15)Acetone<6.663 31 25<66 <6.624 24220,000 2,700,000Benzene1.2 3.1 2.7 0.37 J 31 4.0 3.3 3.3120 1,6001,3-Butadiene<0.32 <0.32 <0.32 <0.32 <3.2 <0.329.4 9.414 1802-Butanone (MEK)8.7 J 6.1 J 5.4 J 8.0 J<113.1 J 3.9 J 4.0 J35,000 440,000Carbon Disulfide<0.43 <0.437.1<0.43 <4.3110 7.5 7.44,900 61,000Chloroform0.64 J 1.0<0.36 <0.36 <3.6 <0.36 <0.36 <0.3641 530Cyclohexane6.5<0.495.8 11 79 12<0.49 <0.4942,000 530,000Dichlorodifluoromethane (Freon 12)<0.431.8 1.6<0.43 <4.3 <0.431.7 1.8700 8,800Ethanol180 59 57 140<6735 30 26NE NEEthyl Acetate<0.54 <0.54 <0.5469<5.4 <0.54 <0.54 <0.54490 6,100Ethylbenzene2.7 7.0 9.9 1.5 370 5.7 4.7 4.6370 4,9004-Ethyltoluene1.1<0.6063 2.4 1,500<0.601.3 1.3NE NEHeptane41 67 79<0.48230 460 84 842,800 35,000Hexane4.7 J<1.2 <1.2 <1.2 <1227 J<1.28.5 J4,900 61,000Isopropanol<0.90 <0.908.0 J 14 J<9.0 <0.90 <0.90 <0.901,400 18,000Methylene Chloride3.7 J<0.844.0 J<0.84 <8.4 <0.84 <0.84 <0.844,200 53,0004-Methyl-2-pentanone (MIBK)<0.43 <0.43 <0.432.7<4.3 <0.43 <0.43 <0.4321,000 260,000Naphthalene<0.80 <0.80220 V-055.1 V-05<8.00.84 J, V-05<0.80 <0.8021 260Propene<0.64 <0.644.8 J<0.64 <6.4100 110 110NE NETetrachloroethylene1.8 3.9 2.0<0.75 <7.5140 1.8 4.1280 3,500Toluene16 47 52 2.6 55 53 35 3635,000 440,000Trichlorofluoromethane (Freon 11)<0.851.1 J 1.1 J 1.5 J<8.546 2.2 J 2.3 JNE NE1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)<1.2 <1.2 <1.22.2 J<123.2 J<1.2 <1.235,000 440,0001,2,4-Trimethylbenzene3.3 6.6 360 7.54,200<0.634.6<0.63420 5,3001,3,5-Trimethylbenzene1.0 1.9 150 5.93,700<0.621.3 1.2420 5,300m&p-Xylene9.7 26 29 4.3 470 17 17 17700 8,800o-Xylene3.0 8.4 13 2.1 360 4.2 5.7 5.4700 8,800Notes:1) NC Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Vapor Intrusion Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) (February 2018) Compound concentrations are reported in micrograms per cubic meter (μg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.Only those compounds detected in at least one sample are shown in the table above.Bold indicates concentration exceeds Residential SGSL.VOCs = volatile organic compounds; ft bgs= feet below ground surface; NE = Not EstablishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. V-05 = Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.µg/m3Residential SGSLs (1)Non-Residential SGSLs (1)Northern Townhome Footprint Southern Townhome FootprintSGP-7 / SG-DUP123/5/2020Eastern Townhome FootprintS:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Assessment\Report\Tables\Blythe Isenhour_Tables 3-19-02.xlsx4/1/2020Table 4 (Page 1 of 1)Hart & Hickman, PC
SITE LOCATION MAP
BLYTHE ISENHOUR
4920 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
2-4-20 0
1BOU-014
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
7.5 MINUTE SERIES (TOPOGRAPHIC)
2923 S. Tryon Street, Suite 100Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
CHARLOTTE WEST, NORTH CAROLINA 1996
SITE
REVISION NO. 0
JOB NO. BOU-014
DATE: 2-5-20
FIGURE NO. 2
BLYTHE ISENHOUR
4920 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
LYNX LIGHT RAIL
POLE-MOUNTED TRANSFORMER
MONITORING WELL LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 GeologyOLD PINEVILLE ROADSOUTH BOULEVARDSPRINGBRO
O
K

R
O
A
D
SCHOLTZ R
O
A
D
ROUNDTREE

R
O
A
D
C & T REFINERY / CARGILL INC.
(4828 & 5000 SOUTH BLVD)
FORMER CATAWBA CHARLAB FACILITY
(5046 OLD PINEVILLE ROAD)
ROUNDTREE PLANTATION
GARDEN CENTER
(517 ROUNDTREE ROAD)
MW-12DMW-2
MW-4A
MW-6
MW-7
MW-1DMW-1
MW-2
MW-9
MW-8
MW-10
MW-5
MW-3
MW-11
MW-4
NOTES:
1.AERIAL IMAGERY PARCEL BOUNDARY DATA
OBTAINED FROM MECKLENBURG COUNTY GIS 2018.
2.MONITORING WELL LOCATIONS ESTIMATED BASED
ON ANNUAL GROUNDWATER MONITORING REPORT
PREPARED FOR THE CHARLAB FACILITY BY H&H
AND DATED MARCH 3, 2009.
COMMERCIAL RETAIL
COMMERCIAL
/

L
I
G
H
T

I
N
D
U
S
T
R
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L
ASTs AND SECONDARY CONTAMMENT AREA
TOTES, DRUMS, AND
5-GALLON BUCKETS OF
HYDRAULIC FLUID BIOCIDE STORAGE
PORTABLE GASOLINE
DISPENSER
OFFICE
BUILDING
WOOD DISPOSAL PILE
CONCRETE PAD: FORMER WASTE STORAGE AND SOLIDIFICATION AREA
RAILCAR/OFFICE
OLD PINEVILLE ROAD
BROWNFIELD PROPERTYFORMER QUEEN CITY BOILER
(4928 OLD PINEVILLE ROAD)
APPROXIMATE LOCATION
OF FORMER AST
COMMERCIAL
/

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T

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N
D
U
S
T
R
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A
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SELF STORAGE
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Figures\Site and Surround Map.dwg, 9/5/2019 5:16:11 PM, amckenzie
!U#
!U#
!U#
E WO
O
D
L
A
W
N

R
D
FURMAN PLGILMOREDRGRICE CTMURRAYHILLRDCONNECTINGRDOLD P
INEV
ILLE
RD
ROUNTREE RD
PLYMOUTH STSOUTHBVINWOOD DRNATIONS CROSSING RDBA
Y
L
O
R

D
R
LISSOM LN
MANH A S SETRDSPRINGBROOK RD
MINUET LN
S C H O LT Z R DCHASTAINAV
RECEPTOR SURVEY MAP
BLYTHE ISENHOUR4920 OLD PINEVILLE ROADCHARLOTTE, NORTH CAROLINA
REVISION NO: 0
FIGURE NO: 3
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
0 320 640
SCALE IN FEET
N
DATE: 3-24-20
JOB NO. BOU-014
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY LINE
SURFACE WATER FEATURE
BUSINESS/INDUSTRIAL ZONING
TRANSIT ORIENTED ZONING
RESIDENTIAL ZONING
O/H OVERHEAD UTILITY LINE
GAS GAS UTILITY LINE
W WATER LINE
SS SEWER UTILITY LINE
UE UNDERGROUND ELECTRIC
!U#PRIVATE WATER SUPPLY WELL
!U#PRIVATE IRRIGATION WATER SUPPLY WELL
!U#PRIVATE POTABLE WATER SUPPLY WELL
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY GIS, 2019.
2. ZONING AND BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS, 2020.
UE U E GASGASGASGASGASGASW W
UE UE UEUEUE
UE SSSSSSSSO/HO/HO/HO/HO/HO/H0 75 150
SCALE IN FEET
INSET A
SEE INSET A
UNNAMED TRIBUTARY OF KINGS BRANCH
UNNAMED TRIBUTARY OF LITTLE SUGAR CREEK
1,500 FT
REVISION NO. 0
JOB NO. BOU-014
DATE: 3-24-20
FIGURE NO. 4
BLYTHE ISENHOUR
4920 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
720
AST CONTAINMENT AREA OLD PINEVILLE ROADNOTES:
1.SOIL BORING B-1 WAS ADVANCED BY MACTEC IN
APRIL 2003.
2.SOIL BORINGS 1 THROUGH 3 WERE ADVANCED BY
MACTEC IN MAY 2003.
3.PARCEL BOUNDARIES OBTAINED FROM
MECKLENBURG COUNTY GIS 2019.
4.ELEVATION CONTOURS OBTAINED FROM
MECKLENBURG COUNTY LIDAR, 2012.
5.PROPOSED REDEVELOPMENT PLAN WAS PREPARED
BY BOHLER ENGINEERING NC, PLLC AND PROVIDED
BY THE PROSPECTIVE DEVELOPER.
6.FT. MSL = FEET ABOVE MEAN SEA LEVEL
AST = ABOVEGROUND STORAGE TANK
BPN = BROWNFIELDS PROJECT NUMBER
TMW-2/BG-1
SGP-6
SGP-3
SGP-5
SGP-2
SGP-1
SGP-4
TMW-4/BG-2
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
LYNX LIGHT RAIL
PARCEL BOUNDARY
2' ELEVATION CONTOURS (FT. MSL)
PROPOSED BUILDING FOOTPRINT
SOIL BORING (APRIL 2003)
POST-EXCAVATION SOIL BORING (MAY 2003)
TEMPORARY MONITORING WELL
CO-LOCATED TEMPORARY MONITORING
WELL AND SOIL BORING
ALIQUOT SOIL BORING LOCATION
TEMPORARY SOIL GAS MONITORING POINT
CO-LOCATED TEMPORARY SOIL GAS
MONITORING POINT AND SOIL BORING
B-1
B-1
1
1
2
3
COMP-2
TMW-1
SELF STORAGE FACILITY
(4914 OLD PINEVILLE ROAD)
CONCRETE PAD:
FORMER WASTE
STORAGE AND
SOLIFICATION AREA
722 7
2
4
7
2
6
728 726724718716714712720
SB-1D
SB-1C
SB-1B
COMP-1
SB-2A
SB-2B SB-2C TMW-3
SGP-7
SB-1A
OLD PINEVILLE ROAD
BROWNFIELDS PROPERTY
FORMER QUEEN CITY BOILER
BPN 10061-06-060
(4928 OLD PINEVILLE ROAD)S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Figures\Site and Surround Map.dwg, FIG.4, 3/31/2020 4:11:06 PM, sperry
REVISION NO. 0
JOB NO. BOU-014
DATE: 3-24-20
FIGURE NO. 5
BLYTHE ISENHOUR
4920 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
SHALLOW GROUNDWATER HYDRAULIC
GRADIENT MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
720
AST CONTAINMENT AREA OLD PINEVILLE ROADNOTES:
1.TOP OF TEMPORARY MONITORING WELL CASINGS
WERE SURVEYED BY H&H RELATIVE TO A DATUM
OF 100 FT. AT TMW-2.
2.DEPTH TO GROUNDWATER MEASUREMENTS WERE
COLLECTED ON MARCH 4, 2020.
3.FT. MSL. = FEET ABOVE MEAN SESA LEVEL
AST = ABOVEGROUND STORAGE TANK
BPN = BROWNFIELDS PROJECT NUMBER
SELF STORAGE FACILITY
(4914 OLD PINEVILLE ROAD)
OLD PINEVILLE ROAD
BROWNFIELDS PROPERTY
FORMER QUEEN CITY BOILER
BPN 10061-06-060
(4928 OLD PINEVILLE ROAD)
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
LYNX LIGHT RAIL
PARCEL BOUNDARY
2' ELEVATION CONTOURS (FT. MSL)
PROPOSED BUILDING FOOTPRINT
TEMPORARY MONITORING WELL
CO-LOCATED TEMPORARY MONITORING
WELL AND SOIL BORING
GROUNDWATER ELEVATION (FT.)
GROUNDWATER CONTOUR (FT.) (DASHED
WHERE INFERRED)
INFERRED DIRECTION OF GROUNDWATER
FLOW
CONCRETE PAD:
FORMER WASTE
STORAGE AND
SOLIFICATION AREA
722 7
2
4
7
2
6
728 726724718716714712720
85
(84.90)
(84.90)
(87.03)
(85.50)
(83.68)
TMW-2/BG-1
TMW-4/BG-2
TMW-1
TMW-3
8587858587858383S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Figures\Site and Surround Map.dwg, FIG.5, 4/2/2020 11:58:45 AM, sperry

Appendix A

Brownfields Receptor Survey
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site: Blythe Isenhour
Address: 4920 Old Pineville Road
City: Charlotte
County: Mecklenburg
Brownfields Project Number: 23067-19-060
Property and Building Characteristics
a. Provide occupancy and use information.
1960s and were utlizied by a general contractor business from the early 1960s until the 1990s. The Site buildings were occupied by Four Seasons
Environmental from the late 1990s until the Early 2000s, when Heartwood operations began.
The Site office building is constructed as a one-story wood-frame office with brick exteriors and multiple windows.
The warehouse building was constructed with exterior metal siding and one roll-up bay door.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
The foundation construction of the offie building and warehouse building on the Site consist of concrete slab-on-grade.
An HVAC system is currently located on the roof of the on-Site office buidling.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No subslab ventilation systems are currently in place. It is unknown is a moisture barrier is currently in-place
beneath the Site building.
% of property that is wooded/brush
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If
numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed.
b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay
doors), and height (number of stories).
% of property that is covered by buildings
1.67
0
~85
~5
The existing office and warehouse buildings are currently occupied by Heartwood Tree Service. The Site buildings were constructed in the early
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information requested
below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield’s Project Manager
(PM).
Current Usage Proposed UsageSurface Conditions
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design
considerations (e.g. positive pressure?).
0
~10
The Brownfields property will be
developed with residential townhomes,
asphalt-paved parking areas, and
landscaped features.
% of property that is grassed areas (unpaved)
% of property that is agricultural crops
% of property that is paved
Size of Property (acres)
Rev. 09/2015 Page 1 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
N----
N----
N----
Utilities
Is there a septic system on-site? (Y or N) NO
Please provide the utility providers for the subject property
a. Natural Gas: Piedmont Natural Gas (underground)
b. Sewer: Charlotte Water (underground)
c. Electricity: Duke Energy (above and below ground)
d. Other: Communication (underground)
For surrounding properties, please complete the following table with available information.
Y<5 E
Y<5 E
N-- --
Y10 E
Y<5 E
Y<5 E
N-- --
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Is there a basement within 1,000 ft of the Property
Distance
(ft)Address
--
Zoning/Land Use
--
--
Proposed Usage Current Use/Occupant
Is a school or daycare center within 1,000 ft of the Property?
DirectionUtility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property.
NA
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If
specific receptors are present, please provide addresses of the facilities.
NA
NA
NA
Mixed Commercial / Self Storage Facility (TOD-CC)
Vacant Land (TOD-CC)
Multi-tenant Commercial Shopping Center (B-1SCD)
Mixed Commercial / Joyner & Benefield (TOD-CC)
For the subject property, please provide a map of known buried utilites. If available, include depth to top, construction material, and
diameter of the utilities. In addition, please provide the following information on utilty providers. If additional assessment is required,
the public utility locators should be contacted. This information can then be added to a site map.
Y/N *
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Distance
(ft)
Is a sanitary sewer within 100 ft of the Property boundary?
Is there a residence within 1,000 ft of the Property?
Rev. 09/2015 Page 2 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public X Private ______
Charlotte Water
N -- -- --
Y 650 /
1,100 SW / NW 517 Round Tree Road /
333 Springbrook Road
Y 1,200 SW 415 Round Tree Road
Surface Water & Wetlands
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield
survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be present.
Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the windshield survey. If
multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please attach a separate
table to list all wells. Please note, the PM may opt for a more extensive water supply well survey if needed.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
Address
Provide Information regarding Surface Water and Wetlands
No
Are there surface water features on the property? (If yes,
please complete a. to d.)
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water
providers name.
Distance
(ft)Direction
a. Is the water body naturally developed or man-made?
--
--
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the
Property.
b. List the uses of the water body.
Rev. 09/2015 Page 3 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
--
--
Unnamed tributary of Kings Branch (~400 ft west)
No
c. What is the source of the water for the water body?
d. What is the nature of the bottom of the water body
(e.g., rocky or concrete bottom, drainage ways or
impoundments)
If no on-site surface water features, what is the nearest
surface water body?
Are there any wetlands present on the property? If no
wetlands on-site, are wetlands suspected on adjoining
properties?
Rev. 09/2015 Page 4 of 4

Appendix B

Boring Logs & Well Construction Records
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-1A
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 3.00 (0') Silty SAND (SM); loose, moist, brown
(1.5') Sandy SILT (ML); medium stiff, moist, dull red
(3') Boring terminated
1.2
1.0
0.7 SB-1A(2-3)
0
1
2
3
4
5
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-1B
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 3.00 (0') Sandy SILT (ML); medium stiff, moist, dull red
(3') Boring terminated
1.4
1.0
0.3
0
1
2
3
4
5
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-1C
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 3.00 (0') Sandy SILT (ML); medium stiff, moist, dull red
(3') Boring terminated
2.4
1.3
0.7
0
1
2
3
4
5
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-1D
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 3.00 (0') Sandy SILT (ML); medium stiff, moist, dull red, (Fill)
(3') Boring terminated
1.2
1.4
1.0
0
1
2
3
4
5
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-2A
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 3.00 (0') Silty SAND with gravel (SM); little coarse gravel, loose, moist, brown
(1') Sandy SILT (ML); medium stiff, moist, dull red
(3') Boring terminated
1.1
0.8
0.8 SB2-2A
0
1
2
3
4
5
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-2B
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 3.00 (0') Silty GRAVEL (GM); loose
(0.5') Sandy SILT (ML); medium stiff, moist, dull red
(3') Boring terminated
2.0
1.7
1.7
0
1
2
3
4
5
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-2C
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 3.00 (0') Silty GRAVEL (GM); loose
(0.5') Sandy SILT (ML); medium stiff, moist, dull red
(3') Boring terminated
1.8
1.6
1.6
0
1
2
3
4
5
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Well No.
Page:
SGP-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
5.0
2.25
Grab
Vapor Pin Depth (ft):
Vapor Pin Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
0.010
Teflon Tubing
Stainless Steel
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELVAPOR PIN COMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR 5.00 (0') Well-graded GRAVEL (GW)
(0.5') Sandy SILT (ML); stiff, moist, dull reddish orange
(5') Boring terminated
2.9
2.0
1.9
0
5
10
5.0
John Allen
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Well No.
Page:
SGP-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
5.0
2.25
Grab
Vapor Pin Depth (ft):
Vapor Pin Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
0.010
Teflon Tubing
Stainless Steel
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELVAPOR PIN COMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR 5.00 (0') Well-graded GRAVEL (GW)
(0.5') Sandy SILT (ML); stiff, moist, dull red
(5') Boring terminated
3.4
2.9
2.8
0
5
10
5.0
John Allen
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Well No.
Page:
SGP-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Direct Push
AMS Power Probe
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
10.0
2.25
Vapor Pin Depth (ft):
Vapor Pin Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
0.010
Teflon Tubing
Stainless Steel
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELVAPOR PIN COMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
GR
DP
5.00
5.00
(0') Sandy SILT (ML); stiff, moist, dull red
(2') Sandy SILT (ML); medium stiff, moist, orange, black, and tan
(10') Boring terminated
2.5
2.3
2.4
4.6
2.2
0
5
10
15
10.0
Terry White
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Well No.
Page:
SGP-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Other
Hand Auger
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
5.0
2.25
Grab
Vapor Pin Depth (ft):
Vapor Pin Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
0.010
Teflon Tubing
Stainless Steel
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELVAPOR PIN COMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR 5.00 (0') Well-graded GRAVEL (GW)
(0.5') Sandy SILT (ML); stiff, moist, dull reddish orange
(5') Boring terminated
0.8
1.3
0.8
0
5
10
5.0
John Allen
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Well No.
Page:
SGP-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Direct Push
AMS Power Probe
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
8.0
2.25
DP, GR
Vapor Pin Depth (ft):
Vapor Pin Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
0.010
Teflon Tubing
Stainless Steel
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELVAPOR PINCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR
DP
5.00
3.00
(0') Sandy SILT (ML); stiff, moist, dull red
(2') Sandy SILT (ML); medium stiff, moist, dull red and brown, odor
(6') Sandy SILT (ML); medium stiff, moist, orange
(8') Boring terminated
84.5
757.0
489.0
16.0
SGP-5 (2-4)
0
5
10
8.0
Terry White
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Well No.
Page:
SGP-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Direct Push
AMS Power Probe
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
12.0
2.25
DP, GR
Vapor Pin Depth (ft):
Vapor Pin Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
0.010
Teflon Tubing
Stainless Steel
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELVAPOR PINCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
GR
DP
5.00
7.00
(0') Asphalt and loose gravel
(0.5') Sandy SILT (ML); stiff, moist, dull red, (Fill)
(6') SILT (ML); some clay, medium stiff, moist, dull red and tan, trace mica
(12') Boring terminated
3.0
2.4
2.5
3.7
3.6
3.5
0
5
10
15
12.0
Terry White
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
BORING LOG
Well No.
Page:
SGP-7
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/4/2020
3/4/2020
IET
Direct Push
AMS Power Probe
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
12.0
2.25
DP, GR
Vapor Pin Depth (ft):
Vapor Pin Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
0.25
0.010
Teflon Tubing
Stainless Steel
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELVAPOR PIN COMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
GR
DP
5.00
7.00
(0') Sandy SILT (ML); stiff, moist, dull red
(4') SILT (ML); some clay, medium stiff, moist, dull red, tan, and orange
(12') Boring terminated
1.9
1.2
1.3
2.1
1.8
2.8
0
5
10
15
12.0
Terry White
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/3/2020
3/3/2020
IET
Direct Push
AMS Power Probe
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
20.0
2.25
Well Depth:
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
16.5 ft bgs
1.0
0.010
Sch 40 PVC
PVC Prepack
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
(0') Well-graded GRAVEL (GW); some wood debris
(0.5') Silty SAND (SM); loose, dry, brown and tan
(2') Sandy SILT (ML); medium stiff, dull red
(8') SILT (ML); some clay, medium stiff, moist, orange, tan, and black
(15') SILT (ML); some clay, soft, wet, orange, tan, and black
(20') As Above: saturated
(20') Boring terminated
1.7
2.1
1.8
2.6
2.9
3.3
2.9
1.9
0
5
10
15
20
25
Terry White
7.70 ft bTOC
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-2/BG-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/3/2020
3/3/2020
IET
Direct Push
AMS Power Probe
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25.0
2.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
1.0
0.010
Sch 40 PVC
PVC Prepack
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
(0') Sandy SILT (ML); medium stiff, moist, orange and dull red
(5') SILT (ML); some clay, soft, moist, orange tan and black
(15') SILT (ML); some clay, soft, wet, orange tan and black
(20') As Above: saturated
(25') Boring terminated
1.4
2.3
1.7
1.8
2.0
2.1
2.4
2.1
2.3
2.5
2.5
BG-1
0
5
10
15
20
25
30
Terry White
15.10 ft bTOC
24.0 ft bgs
NOTES: Hole precleared using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
IET
Direct Push
AMS Power Probe
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25.0
2.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
24.0 ft bgs
1.0
0.010
Sch 40 PVC
PVC Prepack
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
(0') Asphalt
(0.25') Sandy SILT (ML); stiff, moist, orange and dull red
(4') As Above: trace gravel
(5') SILT (ML); some clay, medium stiff, moist, orange and tan
(14') SILT (ML); some clay, soft, wet, orange tan and black
(20') As Above: saturated
(25') Boring terminated
2.6
2.1
2.1
2.4
2.6
2.8
2.7
2.4
0
5
10
15
20
25
30
3/3/2020
3/3/2020
Terry White
15.10 ft bTOC
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Boulevard Real Estate Advisors
BOU-014
4920 Old Pineville Road,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-4/BG-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/3/2020
3/3/2020
IET
Direct Push
AMS Power Probe
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
15.0
2.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
1.0
0.010
Sch 40 PVC
PVC Prepack
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Sandy SILT (ML); medium stiff, moist, dull red
(5') SILT (ML); some clay, medium stiff, wet, reddish-orange and tan
(10') As Above: saturated
(15') Boring terminated
2.5
2.0
3.3
2.0
1.4
0.7
0
5
10
15
20
BG-2
Terry White
5.61 ft bTOC
13.0 ft bgs
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
SIP Permit # 70002730
one
3/4/2020 TMW-1
Heartwood Tree Service
4920 Old Pineville Rd., Charlotte, 28217
Mecklenburg
35 10 23 80 52 45
16.5
7.7
2
Direct Push
3/6/2020
7.7 16.5 Brown soil
0 1.5 1 sch40 pvc
1.5 16.5 1 0.010 sch40 pvc
0
1
1
16.5
Bentonite
#2 Sand Poured
Poured/5LB
See Consultant Log
Prepack Screens were used.
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
SIP Permit # 70002730
one
3/4/2020 TMW-2
Heartwood Tree Service
4920 Old Pineville Rd., Charlotte, 28217
Mecklenburg
35 10 23 80 52 45
24
15.10
2
Direct Push
3/6/2020
15.10 24 Brown soil
0 9 1 sch40 pvc
9 24 1 0.010 sch40 pvc
0
7
7
24
Bentonite
#2 Sand Poured
Poured/15LB
See Consultant Log
Prepack Screens were used.
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
SIP Permit # 70002730
one
3/4/2020 TMW-3
Heartwood Tree Service
4920 Old Pineville Rd., Charlotte, 28217
Mecklenburg
35 10 23 80 52 45
24
15.10
2
Direct Push
3/6/2020
15.10 24 Brown soil
0 9 1 sch40 pvc
9 24 1 0.010 sch40 pvc
0
7
7
24
Bentonite
#2 Sand Poured
Poured/15LB
See Consultant Log
Prepack Screens were used.
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
SIP Permit # 70002730
one
3/4/2020 TMW-4
Heartwood Tree Service
4920 Old Pineville Rd., Charlotte, 28217
Mecklenburg
35 10 23 80 52 45
13
5.61
2
Direct Push
3/6/2020
5.61 13 Brown soil
0 3 1 sch40 pvc
3 13 1 0.010 sch40 pvc
0
2
2
13
Bentonite
#2 Sand Poured
Poured/2.5LB
See Consultant Log
Prepack Screens were used.

Appendix C

Laboratory Analytical Reports
#=CL#
March 12, 2020
LIMS USE: FR - RALPH MCGEE
LIMS OBJECT ID: 92468257
92468257
Project:
Pace Project No.:
RE:
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
BOU-014
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on March 05, 2020. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
cc:Haley Martin, Hart & Hickman
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 52
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92468257
BOU-014
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 52
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92468257
BOU-014
Lab ID Sample ID Matrix Date Collected Date Received
92468257001 BG-1 Solid 03/03/20 09:15 03/05/20 07:00
92468257002 BG-2 Solid 03/03/20 13:10 03/05/20 07:00
92468257003 COMP-1 Solid 03/04/20 09:30 03/05/20 07:00
92468257004 COMP-2 Solid 03/04/20 09:55 03/05/20 07:00
92468257005 SB-1A (2-3)Solid 03/04/20 09:30 03/05/20 07:00
92468257006 SB-2A (2-3)Solid 03/04/20 09:55 03/05/20 07:00
92468257007 SGP-5 (2-4)Solid 03/04/20 12:10 03/05/20 07:00
92468257008 SB-DUP Solid 03/04/20 00:00 03/05/20 07:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 52
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92468257
BOU-014
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92468257001 BG-1 EPA 6020B 7 PANLAT
EPA 7471B 1 PANTCT
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92468257002 BG-2 EPA 6020B 7 PANLAT
EPA 7471B 1 PANTCT
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92468257003 COMP-1 EPA 6020B 7 PANLAT
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92468257004 COMP-2 EPA 6020B 7 PANLAT
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92468257005 SB-1A (2-3)EPA 8082A 8 PASI-CSEM
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92468257006 SB-2A (2-3)EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92468257007 SGP-5 (2-4)EPA 6020B 7 PANLAT
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92468257008 SB-DUP EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:BG-1 Lab ID:92468257001 Collected:03/03/20 09:15 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 3.67 mg/kg 03/09/20 11:55 7440-38-203/08/20 07:190.653 0.163 5
Barium 48.6 mg/kg 03/09/20 11:55 7440-39-303/08/20 07:191.31 0.209 5
Cadmium ND mg/kg 03/09/20 11:55 7440-43-903/08/20 07:190.653 0.104 5
Chromium 47.4 mg/kg 03/09/20 11:55 7440-47-303/08/20 07:191.31 0.353 5
Lead 15.1 mg/kg 03/09/20 11:55 7439-92-103/08/20 07:190.653 0.157 5
Selenium 0.988 mg/kg 03/09/20 11:55 7782-49-203/08/20 07:190.653 0.248 5
Silver ND mg/kg 03/09/20 11:55 7440-22-403/08/20 07:190.653 0.202 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0842 mg/kg 03/09/20 20:40 7439-97-603/09/20 11:070.0392 0.00366 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 76.6 %03/10/20 09:3603/10/20 09:251
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.415J mg/kg 03/11/20 11:42 18540-29-9 J03/10/20 12:481.31 0.333 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:BG-2 Lab ID:92468257002 Collected:03/03/20 13:10 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 6.47 mg/kg 03/09/20 11:58 7440-38-203/08/20 07:190.644 0.161 5
Barium 16.8 mg/kg 03/09/20 11:58 7440-39-303/08/20 07:191.29 0.206 5
Cadmium ND mg/kg 03/09/20 11:58 7440-43-903/08/20 07:190.644 0.103 5
Chromium 122 mg/kg 03/09/20 12:49 7440-47-303/08/20 07:192.58 0.696 10
Lead 6.44 mg/kg 03/09/20 11:58 7439-92-103/08/20 07:190.644 0.155 5
Selenium 0.673 mg/kg 03/09/20 11:58 7782-49-203/08/20 07:190.644 0.245 5
Silver ND mg/kg 03/09/20 11:58 7440-22-403/08/20 07:190.644 0.200 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.139 mg/kg 03/09/20 20:48 7439-97-603/09/20 11:070.0387 0.00361 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 77.6 %03/10/20 09:3603/10/20 09:251
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.584J mg/kg 03/11/20 11:47 18540-29-9 J03/10/20 12:481.29 0.329 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:COMP-1 Lab ID:92468257003 Collected:03/04/20 09:30 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 2.46 mg/kg 03/09/20 12:02 7440-38-203/08/20 07:190.685 0.171 5
Barium 116 mg/kg 03/09/20 12:02 7440-39-303/08/20 07:191.37 0.219 5
Cadmium ND mg/kg 03/09/20 12:02 7440-43-903/08/20 07:190.685 0.110 5
Chromium 32.1 mg/kg 03/09/20 12:02 7440-47-303/08/20 07:191.37 0.370 5
Lead 7.93 mg/kg 03/09/20 12:02 7439-92-103/08/20 07:190.685 0.164 5
Selenium 0.818 mg/kg 03/09/20 12:02 7782-49-203/08/20 07:190.685 0.260 5
Silver ND mg/kg 03/09/20 12:02 7440-22-403/08/20 07:190.685 0.212 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0585 mg/kg 03/09/20 20:50 7439-97-603/09/20 11:070.0411 0.00384 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 03/06/20 16:48 83-32-903/06/20 13:504121061
Acenaphthylene ND ug/kg 03/06/20 16:48 208-96-803/06/20 13:5041297.5 1
Aniline ND ug/kg 03/06/20 16:48 62-53-303/06/20 13:5041292.5 1
Anthracene ND ug/kg 03/06/20 16:48 120-12-703/06/20 13:504121071
Benzo(a)anthracene ND ug/kg 03/06/20 16:48 56-55-303/06/20 13:504121311
Benzo(a)pyrene ND ug/kg 03/06/20 16:48 50-32-803/06/20 13:504121791
Benzo(b)fluoranthene ND ug/kg 03/06/20 16:48 205-99-203/06/20 13:504121661
Benzo(g,h,i)perylene ND ug/kg 03/06/20 16:48 191-24-203/06/20 13:504121611
Benzo(k)fluoranthene ND ug/kg 03/06/20 16:48 207-08-903/06/20 13:504121741
Benzoic Acid ND ug/kg 03/06/20 16:48 65-85-003/06/20 13:5020604451
Benzyl alcohol ND ug/kg 03/06/20 16:48 100-51-603/06/20 13:508242191
4-Bromophenylphenyl ether ND ug/kg 03/06/20 16:48 101-55-303/06/20 13:504121081
Butylbenzylphthalate ND ug/kg 03/06/20 16:48 85-68-703/06/20 13:504121101
4-Chloro-3-methylphenol ND ug/kg 03/06/20 16:48 59-50-703/06/20 13:508242511
4-Chloroaniline ND ug/kg 03/06/20 16:48 106-47-803/06/20 13:508242521
bis(2-Chloroethoxy)methane ND ug/kg 03/06/20 16:48 111-91-103/06/20 13:504121101
bis(2-Chloroethyl) ether ND ug/kg 03/06/20 16:48 111-44-403/06/20 13:5041287.5 1
2-Chloronaphthalene ND ug/kg 03/06/20 16:48 91-58-703/06/20 13:5041291.8 1
2-Chlorophenol ND ug/kg 03/06/20 16:48 95-57-803/06/20 13:5041295.9 1
4-Chlorophenylphenyl ether ND ug/kg 03/06/20 16:48 7005-72-303/06/20 13:504121071
Chrysene ND ug/kg 03/06/20 16:48 218-01-903/06/20 13:504121201
Dibenz(a,h)anthracene ND ug/kg 03/06/20 16:48 53-70-303/06/20 13:504121651
Dibenzofuran ND ug/kg 03/06/20 16:48 132-64-903/06/20 13:504121031
1,2-Dichlorobenzene ND ug/kg 03/06/20 16:48 95-50-103/06/20 13:5041289.2 1
1,3-Dichlorobenzene ND ug/kg 03/06/20 16:48 541-73-103/06/20 13:5041292.8 1
1,4-Dichlorobenzene ND ug/kg 03/06/20 16:48 106-46-703/06/20 13:5041290.6 1
3,3'-Dichlorobenzidine ND ug/kg 03/06/20 16:48 91-94-103/06/20 13:508242871
2,4-Dichlorophenol ND ug/kg 03/06/20 16:48 120-83-203/06/20 13:504121361
Diethylphthalate ND ug/kg 03/06/20 16:48 84-66-203/06/20 13:5041289.4 1
2,4-Dimethylphenol ND ug/kg 03/06/20 16:48 105-67-903/06/20 13:504121031
Dimethylphthalate ND ug/kg 03/06/20 16:48 131-11-303/06/20 13:5041293.1 1
Di-n-butylphthalate ND ug/kg 03/06/20 16:48 84-74-203/06/20 13:504121021
4,6-Dinitro-2-methylphenol ND ug/kg 03/06/20 16:48 534-52-103/06/20 13:508246641
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:COMP-1 Lab ID:92468257003 Collected:03/04/20 09:30 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 03/06/20 16:48 51-28-503/06/20 13:50206013201
2,4-Dinitrotoluene ND ug/kg 03/06/20 16:48 121-14-203/06/20 13:504121091
2,6-Dinitrotoluene ND ug/kg 03/06/20 16:48 606-20-203/06/20 13:504121081
Di-n-octylphthalate ND ug/kg 03/06/20 16:48 117-84-0 v103/06/20 13:504122351
bis(2-Ethylhexyl)phthalate ND ug/kg 03/06/20 16:48 117-81-703/06/20 13:504121351
Fluoranthene ND ug/kg 03/06/20 16:48 206-44-003/06/20 13:504121241
Fluorene ND ug/kg 03/06/20 16:48 86-73-703/06/20 13:504121101
Hexachloro-1,3-butadiene ND ug/kg 03/06/20 16:48 87-68-3 v203/06/20 13:504121001
Hexachlorobenzene ND ug/kg 03/06/20 16:48 118-74-103/06/20 13:504121051
Hexachlorocyclopentadiene ND ug/kg 03/06/20 16:48 77-47-403/06/20 13:504121651
Hexachloroethane ND ug/kg 03/06/20 16:48 67-72-103/06/20 13:5041293.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/06/20 16:48 193-39-503/06/20 13:504121891
Isophorone ND ug/kg 03/06/20 16:48 78-59-103/06/20 13:5041289.5 1
1-Methylnaphthalene ND ug/kg 03/06/20 16:48 90-12-003/06/20 13:504121101
2-Methylnaphthalene ND ug/kg 03/06/20 16:48 91-57-603/06/20 13:504121051
2-Methylphenol(o-Cresol)ND ug/kg 03/06/20 16:48 95-48-703/06/20 13:5041291.3 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/06/20 16:48 15831-10-403/06/20 13:504121041
Naphthalene ND ug/kg 03/06/20 16:48 91-20-303/06/20 13:5041298.6 1
2-Nitroaniline ND ug/kg 03/06/20 16:48 88-74-403/06/20 13:5020602071
3-Nitroaniline ND ug/kg 03/06/20 16:48 99-09-203/06/20 13:5020602191
4-Nitroaniline ND ug/kg 03/06/20 16:48 100-01-603/06/20 13:508242041
Nitrobenzene ND ug/kg 03/06/20 16:48 98-95-303/06/20 13:5041298.4 1
2-Nitrophenol ND ug/kg 03/06/20 16:48 88-75-503/06/20 13:504121271
4-Nitrophenol ND ug/kg 03/06/20 16:48 100-02-703/06/20 13:5020606571
N-Nitrosodimethylamine ND ug/kg 03/06/20 16:48 62-75-903/06/20 13:504121161
N-Nitroso-di-n-propylamine ND ug/kg 03/06/20 16:48 621-64-703/06/20 13:504121151
N-Nitrosodiphenylamine ND ug/kg 03/06/20 16:48 86-30-603/06/20 13:504121051
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/06/20 16:48 108-60-103/06/20 13:504121141
Pentachlorophenol ND ug/kg 03/06/20 16:48 87-86-503/06/20 13:508241891
Phenanthrene ND ug/kg 03/06/20 16:48 85-01-803/06/20 13:504121041
Phenol ND ug/kg 03/06/20 16:48 108-95-203/06/20 13:5041298.4 1
Pyrene ND ug/kg 03/06/20 16:48 129-00-003/06/20 13:504121131
Pyridine ND ug/kg 03/06/20 16:48 110-86-103/06/20 13:504121041
1,2,4-Trichlorobenzene ND ug/kg 03/06/20 16:48 120-82-103/06/20 13:5041294.4 1
2,4,5-Trichlorophenol ND ug/kg 03/06/20 16:48 95-95-403/06/20 13:504121071
2,4,6-Trichlorophenol ND ug/kg 03/06/20 16:48 88-06-203/06/20 13:504121041
Surrogates
Nitrobenzene-d5 (S)57 %03/06/20 16:48 4165-60-003/06/20 13:5023-110 1
2-Fluorobiphenyl (S)42 %03/06/20 16:48 321-60-803/06/20 13:5030-110 1
Terphenyl-d14 (S)61 %03/06/20 16:48 1718-51-003/06/20 13:5028-110 1
Phenol-d6 (S)49 %03/06/20 16:48 13127-88-303/06/20 13:5022-110 1
2-Fluorophenol (S)50 %03/06/20 16:48 367-12-403/06/20 13:5013-110 1
2,4,6-Tribromophenol (S)38 %03/06/20 16:48 118-79-603/06/20 13:5027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:COMP-1 Lab ID:92468257003 Collected:03/04/20 09:30 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.9 %03/05/20 17:480.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 73.0 %03/10/20 09:3603/10/20 09:251
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 03/11/20 11:52 18540-29-903/10/20 12:481.37 0.349 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:COMP-2 Lab ID:92468257004 Collected:03/04/20 09:55 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 3.19 mg/kg 03/09/20 12:05 7440-38-203/08/20 07:190.630 0.158 5
Barium 30.6 mg/kg 03/09/20 12:05 7440-39-303/08/20 07:191.26 0.202 5
Cadmium ND mg/kg 03/09/20 12:05 7440-43-903/08/20 07:190.630 0.101 5
Chromium 31.4 mg/kg 03/09/20 12:05 7440-47-303/08/20 07:191.26 0.340 5
Lead 11.0 mg/kg 03/09/20 12:05 7439-92-103/08/20 07:190.630 0.151 5
Selenium 0.523J mg/kg 03/09/20 12:05 7782-49-2 J03/08/20 07:190.630 0.239 5
Silver ND mg/kg 03/09/20 12:05 7440-22-403/08/20 07:190.630 0.195 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0675 mg/kg 03/09/20 20:53 7439-97-603/09/20 11:070.0378 0.00353 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 03/06/20 17:15 83-32-903/06/20 13:504151071
Acenaphthylene ND ug/kg 03/06/20 17:15 208-96-803/06/20 13:5041598.1 1
Aniline ND ug/kg 03/06/20 17:15 62-53-303/06/20 13:5041593.1 1
Anthracene ND ug/kg 03/06/20 17:15 120-12-703/06/20 13:504151081
Benzo(a)anthracene ND ug/kg 03/06/20 17:15 56-55-303/06/20 13:504151321
Benzo(a)pyrene ND ug/kg 03/06/20 17:15 50-32-803/06/20 13:504151801
Benzo(b)fluoranthene ND ug/kg 03/06/20 17:15 205-99-203/06/20 13:504151671
Benzo(g,h,i)perylene ND ug/kg 03/06/20 17:15 191-24-203/06/20 13:504151621
Benzo(k)fluoranthene ND ug/kg 03/06/20 17:15 207-08-903/06/20 13:504151751
Benzoic Acid ND ug/kg 03/06/20 17:15 65-85-003/06/20 13:5020704471
Benzyl alcohol ND ug/kg 03/06/20 17:15 100-51-603/06/20 13:508292201
4-Bromophenylphenyl ether ND ug/kg 03/06/20 17:15 101-55-303/06/20 13:504151091
Butylbenzylphthalate ND ug/kg 03/06/20 17:15 85-68-703/06/20 13:504151101
4-Chloro-3-methylphenol ND ug/kg 03/06/20 17:15 59-50-703/06/20 13:508292531
4-Chloroaniline ND ug/kg 03/06/20 17:15 106-47-803/06/20 13:508292541
bis(2-Chloroethoxy)methane ND ug/kg 03/06/20 17:15 111-91-103/06/20 13:504151111
bis(2-Chloroethyl) ether ND ug/kg 03/06/20 17:15 111-44-403/06/20 13:5041588.1 1
2-Chloronaphthalene ND ug/kg 03/06/20 17:15 91-58-703/06/20 13:5041592.3 1
2-Chlorophenol ND ug/kg 03/06/20 17:15 95-57-803/06/20 13:5041596.5 1
4-Chlorophenylphenyl ether ND ug/kg 03/06/20 17:15 7005-72-303/06/20 13:504151081
Chrysene ND ug/kg 03/06/20 17:15 218-01-903/06/20 13:504151201
Dibenz(a,h)anthracene ND ug/kg 03/06/20 17:15 53-70-303/06/20 13:504151661
Dibenzofuran ND ug/kg 03/06/20 17:15 132-64-903/06/20 13:504151041
1,2-Dichlorobenzene ND ug/kg 03/06/20 17:15 95-50-103/06/20 13:5041589.7 1
1,3-Dichlorobenzene ND ug/kg 03/06/20 17:15 541-73-103/06/20 13:5041593.3 1
1,4-Dichlorobenzene ND ug/kg 03/06/20 17:15 106-46-703/06/20 13:5041591.2 1
3,3'-Dichlorobenzidine ND ug/kg 03/06/20 17:15 91-94-103/06/20 13:508292891
2,4-Dichlorophenol ND ug/kg 03/06/20 17:15 120-83-203/06/20 13:504151371
Diethylphthalate ND ug/kg 03/06/20 17:15 84-66-203/06/20 13:5041589.9 1
2,4-Dimethylphenol ND ug/kg 03/06/20 17:15 105-67-903/06/20 13:504151031
Dimethylphthalate ND ug/kg 03/06/20 17:15 131-11-303/06/20 13:5041593.7 1
Di-n-butylphthalate ND ug/kg 03/06/20 17:15 84-74-203/06/20 13:504151021
4,6-Dinitro-2-methylphenol ND ug/kg 03/06/20 17:15 534-52-103/06/20 13:508296681
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:COMP-2 Lab ID:92468257004 Collected:03/04/20 09:55 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 03/06/20 17:15 51-28-503/06/20 13:50207013201
2,4-Dinitrotoluene ND ug/kg 03/06/20 17:15 121-14-203/06/20 13:504151101
2,6-Dinitrotoluene ND ug/kg 03/06/20 17:15 606-20-203/06/20 13:504151081
Di-n-octylphthalate ND ug/kg 03/06/20 17:15 117-84-0 v103/06/20 13:504152361
bis(2-Ethylhexyl)phthalate ND ug/kg 03/06/20 17:15 117-81-703/06/20 13:504151361
Fluoranthene ND ug/kg 03/06/20 17:15 206-44-003/06/20 13:504151251
Fluorene ND ug/kg 03/06/20 17:15 86-73-703/06/20 13:504151111
Hexachloro-1,3-butadiene ND ug/kg 03/06/20 17:15 87-68-3 v203/06/20 13:504151011
Hexachlorobenzene ND ug/kg 03/06/20 17:15 118-74-103/06/20 13:504151051
Hexachlorocyclopentadiene ND ug/kg 03/06/20 17:15 77-47-403/06/20 13:504151661
Hexachloroethane ND ug/kg 03/06/20 17:15 67-72-103/06/20 13:5041594.5 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/06/20 17:15 193-39-503/06/20 13:504151901
Isophorone ND ug/kg 03/06/20 17:15 78-59-103/06/20 13:5041590.1 1
1-Methylnaphthalene ND ug/kg 03/06/20 17:15 90-12-003/06/20 13:504151101
2-Methylnaphthalene ND ug/kg 03/06/20 17:15 91-57-603/06/20 13:504151061
2-Methylphenol(o-Cresol)ND ug/kg 03/06/20 17:15 95-48-703/06/20 13:5041591.8 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/06/20 17:15 15831-10-403/06/20 13:504151041
Naphthalene ND ug/kg 03/06/20 17:15 91-20-303/06/20 13:5041599.2 1
2-Nitroaniline ND ug/kg 03/06/20 17:15 88-74-403/06/20 13:5020702091
3-Nitroaniline ND ug/kg 03/06/20 17:15 99-09-203/06/20 13:5020702201
4-Nitroaniline ND ug/kg 03/06/20 17:15 100-01-603/06/20 13:508292051
Nitrobenzene ND ug/kg 03/06/20 17:15 98-95-303/06/20 13:5041599.0 1
2-Nitrophenol ND ug/kg 03/06/20 17:15 88-75-503/06/20 13:504151281
4-Nitrophenol ND ug/kg 03/06/20 17:15 100-02-703/06/20 13:5020706611
N-Nitrosodimethylamine ND ug/kg 03/06/20 17:15 62-75-903/06/20 13:504151171
N-Nitroso-di-n-propylamine ND ug/kg 03/06/20 17:15 621-64-703/06/20 13:504151161
N-Nitrosodiphenylamine ND ug/kg 03/06/20 17:15 86-30-603/06/20 13:504151061
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/06/20 17:15 108-60-103/06/20 13:504151151
Pentachlorophenol ND ug/kg 03/06/20 17:15 87-86-503/06/20 13:508291901
Phenanthrene ND ug/kg 03/06/20 17:15 85-01-803/06/20 13:504151041
Phenol ND ug/kg 03/06/20 17:15 108-95-203/06/20 13:5041599.0 1
Pyrene ND ug/kg 03/06/20 17:15 129-00-003/06/20 13:504151141
Pyridine ND ug/kg 03/06/20 17:15 110-86-103/06/20 13:504151051
1,2,4-Trichlorobenzene ND ug/kg 03/06/20 17:15 120-82-103/06/20 13:5041595.0 1
2,4,5-Trichlorophenol ND ug/kg 03/06/20 17:15 95-95-403/06/20 13:504151081
2,4,6-Trichlorophenol ND ug/kg 03/06/20 17:15 88-06-203/06/20 13:504151041
Surrogates
Nitrobenzene-d5 (S)67 %03/06/20 17:15 4165-60-003/06/20 13:5023-110 1
2-Fluorobiphenyl (S)61 %03/06/20 17:15 321-60-803/06/20 13:5030-110 1
Terphenyl-d14 (S)60 %03/06/20 17:15 1718-51-003/06/20 13:5028-110 1
Phenol-d6 (S)62 %03/06/20 17:15 13127-88-303/06/20 13:5022-110 1
2-Fluorophenol (S)63 %03/06/20 17:15 367-12-403/06/20 13:5013-110 1
2,4,6-Tribromophenol (S)68 %03/06/20 17:15 118-79-603/06/20 13:5027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:COMP-2 Lab ID:92468257004 Collected:03/04/20 09:55 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.3 %03/05/20 17:480.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 79.3 %03/10/20 09:3603/10/20 09:251
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 03/11/20 11:57 18540-29-903/10/20 12:481.26 0.321 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SB-1A (2-3)Lab ID:92468257005 Collected:03/04/20 09:30 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 03/06/20 20:07 12674-11-203/06/20 10:3939.4 10.6 1
PCB-1221 (Aroclor 1221)ND ug/kg 03/06/20 20:07 11104-28-203/06/20 10:3939.4 14.0 1
PCB-1232 (Aroclor 1232)ND ug/kg 03/06/20 20:07 11141-16-503/06/20 10:3939.4 9.9 1
PCB-1242 (Aroclor 1242)ND ug/kg 03/06/20 20:07 53469-21-903/06/20 10:3939.4 2.6 1
PCB-1248 (Aroclor 1248)ND ug/kg 03/06/20 20:07 12672-29-603/06/20 10:3939.4 6.9 1
PCB-1254 (Aroclor 1254)ND ug/kg 03/06/20 20:07 11097-69-103/06/20 10:3939.4 7.4 1
PCB-1260 (Aroclor 1260)ND ug/kg 03/06/20 20:07 11096-82-503/06/20 10:3939.4 9.1 1
Surrogates
Decachlorobiphenyl (S)35 %03/06/20 20:07 2051-24-303/06/20 10:3910-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 16.6J ug/kg 03/06/20 16:11 67-64-103/06/20 10:1796.6 9.1 1
Benzene ND ug/kg 03/06/20 16:11 71-43-203/06/20 10:174.8 0.87 1
Bromobenzene ND ug/kg 03/06/20 16:11 108-86-103/06/20 10:174.8 1.3 1
Bromochloromethane ND ug/kg 03/06/20 16:11 74-97-503/06/20 10:174.8 1.2 1
Bromodichloromethane ND ug/kg 03/06/20 16:11 75-27-403/06/20 10:174.8 0.94 1
Bromoform ND ug/kg 03/06/20 16:11 75-25-203/06/20 10:174.8 2.4 1
Bromomethane ND ug/kg 03/06/20 16:11 74-83-903/06/20 10:179.7 2.3 1
2-Butanone (MEK)ND ug/kg 03/06/20 16:11 78-93-303/06/20 10:1796.6 11.5 1
n-Butylbenzene ND ug/kg 03/06/20 16:11 104-51-803/06/20 10:174.8 2.7 1
sec-Butylbenzene ND ug/kg 03/06/20 16:11 135-98-803/06/20 10:174.8 2.0 1
tert-Butylbenzene ND ug/kg 03/06/20 16:11 98-06-603/06/20 10:174.8 1.6 1
Carbon tetrachloride ND ug/kg 03/06/20 16:11 56-23-503/06/20 10:174.8 0.93 1
Chlorobenzene ND ug/kg 03/06/20 16:11 108-90-703/06/20 10:174.8 0.93 1
Chloroethane ND ug/kg 03/06/20 16:11 75-00-303/06/20 10:179.7 2.0 1
Chloroform ND ug/kg 03/06/20 16:11 67-66-303/06/20 10:174.8 1.0 1
Chloromethane ND ug/kg 03/06/20 16:11 74-87-3 v203/06/20 10:179.7 3.2 1
2-Chlorotoluene ND ug/kg 03/06/20 16:11 95-49-803/06/20 10:174.8 1.5 1
4-Chlorotoluene ND ug/kg 03/06/20 16:11 106-43-403/06/20 10:174.8 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/06/20 16:11 96-12-803/06/20 10:174.8 2.5 1
Dibromochloromethane ND ug/kg 03/06/20 16:11 124-48-103/06/20 10:174.8 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 03/06/20 16:11 106-93-403/06/20 10:174.8 1.1 1
Dibromomethane ND ug/kg 03/06/20 16:11 74-95-303/06/20 10:174.8 1.4 1
1,2-Dichlorobenzene ND ug/kg 03/06/20 16:11 95-50-103/06/20 10:174.8 1.7 1
1,3-Dichlorobenzene ND ug/kg 03/06/20 16:11 541-73-103/06/20 10:174.8 1.7 1
1,4-Dichlorobenzene ND ug/kg 03/06/20 16:11 106-46-703/06/20 10:174.8 1.7 1
Dichlorodifluoromethane ND ug/kg 03/06/20 16:11 75-71-803/06/20 10:179.7 4.0 1
1,1-Dichloroethane ND ug/kg 03/06/20 16:11 75-34-303/06/20 10:174.8 0.71 1
1,2-Dichloroethane ND ug/kg 03/06/20 16:11 107-06-203/06/20 10:174.8 0.97 1
1,1-Dichloroethene ND ug/kg 03/06/20 16:11 75-35-403/06/20 10:174.8 1.1 1
cis-1,2-Dichloroethene ND ug/kg 03/06/20 16:11 156-59-203/06/20 10:174.8 0.84 1
trans-1,2-Dichloroethene ND ug/kg 03/06/20 16:11 156-60-503/06/20 10:174.8 0.95 1
1,2-Dichloropropane ND ug/kg 03/06/20 16:11 78-87-503/06/20 10:174.8 1.8 1
1,3-Dichloropropane ND ug/kg 03/06/20 16:11 142-28-903/06/20 10:174.8 1.8 1
2,2-Dichloropropane ND ug/kg 03/06/20 16:11 594-20-703/06/20 10:174.8 0.48 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SB-1A (2-3)Lab ID:92468257005 Collected:03/04/20 09:30 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
1,1-Dichloropropene ND ug/kg 03/06/20 16:11 563-58-603/06/20 10:174.8 2.0 1
cis-1,3-Dichloropropene ND ug/kg 03/06/20 16:11 10061-01-503/06/20 10:174.8 2.2 1
trans-1,3-Dichloropropene ND ug/kg 03/06/20 16:11 10061-02-603/06/20 10:174.8 0.84 1
Diisopropyl ether ND ug/kg 03/06/20 16:11 108-20-303/06/20 10:174.8 2.8 1
Ethylbenzene ND ug/kg 03/06/20 16:11 100-41-403/06/20 10:174.8 1.0 1
Hexachloro-1,3-butadiene ND ug/kg 03/06/20 16:11 87-68-303/06/20 10:174.8 2.4 1
2-Hexanone ND ug/kg 03/06/20 16:11 591-78-603/06/20 10:1748.3 5.0 1
Isopropylbenzene (Cumene)ND ug/kg 03/06/20 16:11 98-82-803/06/20 10:174.8 1.4 1
p-Isopropyltoluene ND ug/kg 03/06/20 16:11 99-87-603/06/20 10:174.8 2.3 1
Methylene Chloride ND ug/kg 03/06/20 16:11 75-09-203/06/20 10:1719.3 5.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/06/20 16:11 108-10-103/06/20 10:1748.3 3.6 1
Methyl-tert-butyl ether ND ug/kg 03/06/20 16:11 1634-04-403/06/20 10:174.8 2.8 1
Naphthalene ND ug/kg 03/06/20 16:11 91-20-303/06/20 10:174.8 4.1 1
n-Propylbenzene ND ug/kg 03/06/20 16:11 103-65-103/06/20 10:174.8 1.6 1
Styrene ND ug/kg 03/06/20 16:11 100-42-503/06/20 10:174.8 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/06/20 16:11 630-20-603/06/20 10:174.8 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/06/20 16:11 79-34-503/06/20 10:174.8 1.7 1
Tetrachloroethene ND ug/kg 03/06/20 16:11 127-18-403/06/20 10:174.8 1.5 1
Toluene ND ug/kg 03/06/20 16:11 108-88-303/06/20 10:174.8 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 03/06/20 16:11 87-61-603/06/20 10:174.8 3.4 1
1,2,4-Trichlorobenzene ND ug/kg 03/06/20 16:11 120-82-103/06/20 10:174.8 2.6 1
1,1,1-Trichloroethane ND ug/kg 03/06/20 16:11 71-55-603/06/20 10:174.8 0.84 1
1,1,2-Trichloroethane ND ug/kg 03/06/20 16:11 79-00-503/06/20 10:174.8 1.1 1
Trichloroethene ND ug/kg 03/06/20 16:11 79-01-603/06/20 10:174.8 1.3 1
Trichlorofluoromethane ND ug/kg 03/06/20 16:11 75-69-403/06/20 10:174.8 1.1 1
1,2,3-Trichloropropane ND ug/kg 03/06/20 16:11 96-18-403/06/20 10:174.8 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 03/06/20 16:11 95-63-603/06/20 10:174.8 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 03/06/20 16:11 108-67-803/06/20 10:174.8 1.6 1
Vinyl acetate ND ug/kg 03/06/20 16:11 108-05-403/06/20 10:1748.3 15.7 1
Vinyl chloride ND ug/kg 03/06/20 16:11 75-01-403/06/20 10:179.7 1.8 1
Xylene (Total)ND ug/kg 03/06/20 16:11 1330-20-703/06/20 10:179.7 3.4 1
m&p-Xylene ND ug/kg 03/06/20 16:11 179601-23-103/06/20 10:179.7 2.3 1
o-Xylene ND ug/kg 03/06/20 16:11 95-47-603/06/20 10:174.8 1.1 1
Surrogates
Toluene-d8 (S)101 %03/06/20 16:11 2037-26-503/06/20 10:1770-130 1
4-Bromofluorobenzene (S)101 %03/06/20 16:11 460-00-403/06/20 10:1770-130 1
1,2-Dichloroethane-d4 (S)93 %03/06/20 16:11 17060-07-003/06/20 10:1770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.7 %03/05/20 17:480.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SB-2A (2-3)Lab ID:92468257006 Collected:03/04/20 09:55 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 78.2J ug/kg 03/09/20 11:52 67-64-103/09/20 10:581029.6 1
Benzene ND ug/kg 03/09/20 11:52 71-43-203/09/20 10:585.1 0.92 1
Bromobenzene ND ug/kg 03/09/20 11:52 108-86-103/09/20 10:585.1 1.4 1
Bromochloromethane ND ug/kg 03/09/20 11:52 74-97-503/09/20 10:585.1 1.3 1
Bromodichloromethane ND ug/kg 03/09/20 11:52 75-27-403/09/20 10:585.1 1.0 1
Bromoform ND ug/kg 03/09/20 11:52 75-25-203/09/20 10:585.1 2.5 1
Bromomethane ND ug/kg 03/09/20 11:52 74-83-903/09/20 10:5810.2 2.4 1
2-Butanone (MEK)ND ug/kg 03/09/20 11:52 78-93-303/09/20 10:5810212.2 1
n-Butylbenzene ND ug/kg 03/09/20 11:52 104-51-803/09/20 10:585.1 2.9 1
sec-Butylbenzene ND ug/kg 03/09/20 11:52 135-98-803/09/20 10:585.1 2.2 1
tert-Butylbenzene ND ug/kg 03/09/20 11:52 98-06-603/09/20 10:585.1 1.7 1
Carbon tetrachloride ND ug/kg 03/09/20 11:52 56-23-503/09/20 10:585.1 0.98 1
Chlorobenzene ND ug/kg 03/09/20 11:52 108-90-703/09/20 10:585.1 0.99 1
Chloroethane ND ug/kg 03/09/20 11:52 75-00-303/09/20 10:5810.2 2.1 1
Chloroform ND ug/kg 03/09/20 11:52 67-66-303/09/20 10:585.1 1.1 1
Chloromethane ND ug/kg 03/09/20 11:52 74-87-3 v203/09/20 10:5810.2 3.3 1
2-Chlorotoluene ND ug/kg 03/09/20 11:52 95-49-803/09/20 10:585.1 1.6 1
4-Chlorotoluene ND ug/kg 03/09/20 11:52 106-43-403/09/20 10:585.1 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/09/20 11:52 96-12-803/09/20 10:585.1 2.6 1
Dibromochloromethane ND ug/kg 03/09/20 11:52 124-48-103/09/20 10:585.1 2.6 1
1,2-Dibromoethane (EDB)ND ug/kg 03/09/20 11:52 106-93-403/09/20 10:585.1 1.1 1
Dibromomethane ND ug/kg 03/09/20 11:52 74-95-303/09/20 10:585.1 1.5 1
1,2-Dichlorobenzene ND ug/kg 03/09/20 11:52 95-50-103/09/20 10:585.1 1.8 1
1,3-Dichlorobenzene ND ug/kg 03/09/20 11:52 541-73-103/09/20 10:585.1 1.8 1
1,4-Dichlorobenzene ND ug/kg 03/09/20 11:52 106-46-703/09/20 10:585.1 1.8 1
Dichlorodifluoromethane ND ug/kg 03/09/20 11:52 75-71-803/09/20 10:5810.2 4.2 1
1,1-Dichloroethane ND ug/kg 03/09/20 11:52 75-34-303/09/20 10:585.1 0.75 1
1,2-Dichloroethane ND ug/kg 03/09/20 11:52 107-06-203/09/20 10:585.1 1.0 1
1,1-Dichloroethene ND ug/kg 03/09/20 11:52 75-35-403/09/20 10:585.1 1.2 1
cis-1,2-Dichloroethene ND ug/kg 03/09/20 11:52 156-59-203/09/20 10:585.1 0.89 1
trans-1,2-Dichloroethene ND ug/kg 03/09/20 11:52 156-60-503/09/20 10:585.1 1.0 1
1,2-Dichloropropane ND ug/kg 03/09/20 11:52 78-87-503/09/20 10:585.1 1.9 1
1,3-Dichloropropane ND ug/kg 03/09/20 11:52 142-28-903/09/20 10:585.1 1.9 1
2,2-Dichloropropane ND ug/kg 03/09/20 11:52 594-20-703/09/20 10:585.1 0.50 1
1,1-Dichloropropene ND ug/kg 03/09/20 11:52 563-58-603/09/20 10:585.1 2.2 1
cis-1,3-Dichloropropene ND ug/kg 03/09/20 11:52 10061-01-503/09/20 10:585.1 2.3 1
trans-1,3-Dichloropropene ND ug/kg 03/09/20 11:52 10061-02-603/09/20 10:585.1 0.89 1
Diisopropyl ether ND ug/kg 03/09/20 11:52 108-20-303/09/20 10:585.1 2.9 1
Ethylbenzene ND ug/kg 03/09/20 11:52 100-41-403/09/20 10:585.1 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 03/09/20 11:52 87-68-303/09/20 10:585.1 2.5 1
2-Hexanone ND ug/kg 03/09/20 11:52 591-78-603/09/20 10:5851.1 5.3 1
Isopropylbenzene (Cumene)ND ug/kg 03/09/20 11:52 98-82-803/09/20 10:585.1 1.5 1
p-Isopropyltoluene ND ug/kg 03/09/20 11:52 99-87-603/09/20 10:585.1 2.5 1
Methylene Chloride ND ug/kg 03/09/20 11:52 75-09-203/09/20 10:5820.4 6.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/09/20 11:52 108-10-103/09/20 10:5851.1 3.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SB-2A (2-3)Lab ID:92468257006 Collected:03/04/20 09:55 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 03/09/20 11:52 1634-04-403/09/20 10:585.1 2.9 1
Naphthalene ND ug/kg 03/09/20 11:52 91-20-303/09/20 10:585.1 4.3 1
n-Propylbenzene ND ug/kg 03/09/20 11:52 103-65-103/09/20 10:585.1 1.7 1
Styrene ND ug/kg 03/09/20 11:52 100-42-503/09/20 10:585.1 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/09/20 11:52 630-20-603/09/20 10:585.1 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/09/20 11:52 79-34-503/09/20 10:585.1 1.8 1
Tetrachloroethene ND ug/kg 03/09/20 11:52 127-18-403/09/20 10:585.1 1.6 1
Toluene ND ug/kg 03/09/20 11:52 108-88-303/09/20 10:585.1 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/09/20 11:52 87-61-603/09/20 10:585.1 3.6 1
1,2,4-Trichlorobenzene ND ug/kg 03/09/20 11:52 120-82-103/09/20 10:585.1 2.7 1
1,1,1-Trichloroethane ND ug/kg 03/09/20 11:52 71-55-603/09/20 10:585.1 0.89 1
1,1,2-Trichloroethane ND ug/kg 03/09/20 11:52 79-00-503/09/20 10:585.1 1.2 1
Trichloroethene ND ug/kg 03/09/20 11:52 79-01-603/09/20 10:585.1 1.3 1
Trichlorofluoromethane ND ug/kg 03/09/20 11:52 75-69-403/09/20 10:585.1 1.2 1
1,2,3-Trichloropropane ND ug/kg 03/09/20 11:52 96-18-403/09/20 10:585.1 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/09/20 11:52 95-63-603/09/20 10:585.1 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 03/09/20 11:52 108-67-803/09/20 10:585.1 1.7 1
Vinyl acetate ND ug/kg 03/09/20 11:52 108-05-4 v103/09/20 10:5851.1 16.6 1
Vinyl chloride ND ug/kg 03/09/20 11:52 75-01-403/09/20 10:5810.2 1.9 1
Xylene (Total)ND ug/kg 03/09/20 11:52 1330-20-703/09/20 10:5810.2 3.6 1
m&p-Xylene ND ug/kg 03/09/20 11:52 179601-23-103/09/20 10:5810.2 2.4 1
o-Xylene ND ug/kg 03/09/20 11:52 95-47-603/09/20 10:585.1 1.2 1
Surrogates
Toluene-d8 (S)101 %03/09/20 11:52 2037-26-503/09/20 10:5870-130 1
4-Bromofluorobenzene (S)103 %03/09/20 11:52 460-00-403/09/20 10:5870-130 1
1,2-Dichloroethane-d4 (S)97 %03/09/20 11:52 17060-07-003/09/20 10:5870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.3 %03/05/20 17:480.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SGP-5 (2-4)Lab ID:92468257007 Collected:03/04/20 12:10 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 1.73 mg/kg 03/09/20 12:08 7440-38-203/08/20 07:190.682 0.170 5
Barium 7.81 mg/kg 03/09/20 12:08 7440-39-303/08/20 07:191.36 0.218 5
Cadmium ND mg/kg 03/09/20 12:08 7440-43-903/08/20 07:190.682 0.109 5
Chromium 25.1 mg/kg 03/09/20 12:08 7440-47-303/08/20 07:191.36 0.368 5
Lead 7.34 mg/kg 03/09/20 12:08 7439-92-103/08/20 07:190.682 0.164 5
Selenium 0.581J mg/kg 03/09/20 12:08 7782-49-2 J03/08/20 07:190.682 0.259 5
Silver ND mg/kg 03/09/20 12:08 7440-22-403/08/20 07:190.682 0.211 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0478 mg/kg 03/09/20 20:55 7439-97-603/09/20 11:070.0409 0.00382 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 03/06/20 17:43 83-32-903/06/20 13:504181081
Acenaphthylene ND ug/kg 03/06/20 17:43 208-96-803/06/20 13:5041899.0 1
Aniline ND ug/kg 03/06/20 17:43 62-53-303/06/20 13:5041893.9 1
Anthracene ND ug/kg 03/06/20 17:43 120-12-703/06/20 13:504181091
Benzo(a)anthracene ND ug/kg 03/06/20 17:43 56-55-303/06/20 13:504181331
Benzo(a)pyrene ND ug/kg 03/06/20 17:43 50-32-803/06/20 13:504181811
Benzo(b)fluoranthene ND ug/kg 03/06/20 17:43 205-99-203/06/20 13:504181691
Benzo(g,h,i)perylene ND ug/kg 03/06/20 17:43 191-24-203/06/20 13:504181641
Benzo(k)fluoranthene ND ug/kg 03/06/20 17:43 207-08-903/06/20 13:504181761
Benzoic Acid ND ug/kg 03/06/20 17:43 65-85-003/06/20 13:5020904511
Benzyl alcohol ND ug/kg 03/06/20 17:43 100-51-603/06/20 13:508372221
4-Bromophenylphenyl ether ND ug/kg 03/06/20 17:43 101-55-303/06/20 13:504181101
Butylbenzylphthalate ND ug/kg 03/06/20 17:43 85-68-703/06/20 13:504181111
4-Chloro-3-methylphenol ND ug/kg 03/06/20 17:43 59-50-703/06/20 13:508372551
4-Chloroaniline ND ug/kg 03/06/20 17:43 106-47-803/06/20 13:508372561
bis(2-Chloroethoxy)methane ND ug/kg 03/06/20 17:43 111-91-103/06/20 13:504181121
bis(2-Chloroethyl) ether ND ug/kg 03/06/20 17:43 111-44-403/06/20 13:5041888.9 1
2-Chloronaphthalene ND ug/kg 03/06/20 17:43 91-58-703/06/20 13:5041893.2 1
2-Chlorophenol ND ug/kg 03/06/20 17:43 95-57-803/06/20 13:5041897.4 1
4-Chlorophenylphenyl ether ND ug/kg 03/06/20 17:43 7005-72-303/06/20 13:504181091
Chrysene ND ug/kg 03/06/20 17:43 218-01-903/06/20 13:504181211
Dibenz(a,h)anthracene ND ug/kg 03/06/20 17:43 53-70-303/06/20 13:504181671
Dibenzofuran ND ug/kg 03/06/20 17:43 132-64-903/06/20 13:504181051
1,2-Dichlorobenzene ND ug/kg 03/06/20 17:43 95-50-103/06/20 13:5041890.5 1
1,3-Dichlorobenzene ND ug/kg 03/06/20 17:43 541-73-103/06/20 13:5041894.2 1
1,4-Dichlorobenzene ND ug/kg 03/06/20 17:43 106-46-703/06/20 13:5041892.0 1
3,3'-Dichlorobenzidine ND ug/kg 03/06/20 17:43 91-94-103/06/20 13:508372921
2,4-Dichlorophenol ND ug/kg 03/06/20 17:43 120-83-203/06/20 13:504181381
Diethylphthalate ND ug/kg 03/06/20 17:43 84-66-203/06/20 13:5041890.8 1
2,4-Dimethylphenol ND ug/kg 03/06/20 17:43 105-67-903/06/20 13:504181041
Dimethylphthalate ND ug/kg 03/06/20 17:43 131-11-303/06/20 13:5041894.6 1
Di-n-butylphthalate ND ug/kg 03/06/20 17:43 84-74-203/06/20 13:504181031
4,6-Dinitro-2-methylphenol ND ug/kg 03/06/20 17:43 534-52-103/06/20 13:508376741
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SGP-5 (2-4)Lab ID:92468257007 Collected:03/04/20 12:10 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 03/06/20 17:43 51-28-503/06/20 13:50209013401
2,4-Dinitrotoluene ND ug/kg 03/06/20 17:43 121-14-203/06/20 13:504181111
2,6-Dinitrotoluene ND ug/kg 03/06/20 17:43 606-20-203/06/20 13:504181091
Di-n-octylphthalate ND ug/kg 03/06/20 17:43 117-84-0 v103/06/20 13:504182381
bis(2-Ethylhexyl)phthalate ND ug/kg 03/06/20 17:43 117-81-703/06/20 13:504181371
Fluoranthene ND ug/kg 03/06/20 17:43 206-44-003/06/20 13:504181261
Fluorene ND ug/kg 03/06/20 17:43 86-73-703/06/20 13:504181121
Hexachloro-1,3-butadiene ND ug/kg 03/06/20 17:43 87-68-3 v203/06/20 13:504181021
Hexachlorobenzene ND ug/kg 03/06/20 17:43 118-74-103/06/20 13:504181061
Hexachlorocyclopentadiene ND ug/kg 03/06/20 17:43 77-47-403/06/20 13:504181671
Hexachloroethane ND ug/kg 03/06/20 17:43 67-72-103/06/20 13:5041895.3 1
Indeno(1,2,3-cd)pyrene ND ug/kg 03/06/20 17:43 193-39-503/06/20 13:504181911
Isophorone ND ug/kg 03/06/20 17:43 78-59-103/06/20 13:5041890.9 1
1-Methylnaphthalene ND ug/kg 03/06/20 17:43 90-12-003/06/20 13:504181111
2-Methylnaphthalene ND ug/kg 03/06/20 17:43 91-57-603/06/20 13:504181061
2-Methylphenol(o-Cresol)ND ug/kg 03/06/20 17:43 95-48-703/06/20 13:5041892.7 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/06/20 17:43 15831-10-403/06/20 13:504181051
Naphthalene 110J ug/kg 03/06/20 17:43 91-20-303/06/20 13:504181001
2-Nitroaniline ND ug/kg 03/06/20 17:43 88-74-403/06/20 13:5020902101
3-Nitroaniline ND ug/kg 03/06/20 17:43 99-09-203/06/20 13:5020902221
4-Nitroaniline ND ug/kg 03/06/20 17:43 100-01-603/06/20 13:508372071
Nitrobenzene ND ug/kg 03/06/20 17:43 98-95-303/06/20 13:5041899.9 1
2-Nitrophenol ND ug/kg 03/06/20 17:43 88-75-503/06/20 13:504181291
4-Nitrophenol ND ug/kg 03/06/20 17:43 100-02-703/06/20 13:5020906671
N-Nitrosodimethylamine ND ug/kg 03/06/20 17:43 62-75-903/06/20 13:504181181
N-Nitroso-di-n-propylamine ND ug/kg 03/06/20 17:43 621-64-703/06/20 13:504181171
N-Nitrosodiphenylamine ND ug/kg 03/06/20 17:43 86-30-603/06/20 13:504181071
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/06/20 17:43 108-60-103/06/20 13:504181161
Pentachlorophenol ND ug/kg 03/06/20 17:43 87-86-503/06/20 13:508371911
Phenanthrene ND ug/kg 03/06/20 17:43 85-01-803/06/20 13:504181051
Phenol ND ug/kg 03/06/20 17:43 108-95-203/06/20 13:5041899.9 1
Pyrene ND ug/kg 03/06/20 17:43 129-00-003/06/20 13:504181151
Pyridine ND ug/kg 03/06/20 17:43 110-86-103/06/20 13:504181061
1,2,4-Trichlorobenzene ND ug/kg 03/06/20 17:43 120-82-103/06/20 13:5041895.8 1
2,4,5-Trichlorophenol ND ug/kg 03/06/20 17:43 95-95-403/06/20 13:504181091
2,4,6-Trichlorophenol ND ug/kg 03/06/20 17:43 88-06-203/06/20 13:504181051
Surrogates
Nitrobenzene-d5 (S)68 %03/06/20 17:43 4165-60-003/06/20 13:5023-110 1
2-Fluorobiphenyl (S)61 %03/06/20 17:43 321-60-803/06/20 13:5030-110 1
Terphenyl-d14 (S)62 %03/06/20 17:43 1718-51-003/06/20 13:5028-110 1
Phenol-d6 (S)50 %03/06/20 17:43 13127-88-303/06/20 13:5022-110 1
2-Fluorophenol (S)62 %03/06/20 17:43 367-12-403/06/20 13:5013-110 1
2,4,6-Tribromophenol (S)78 %03/06/20 17:43 118-79-603/06/20 13:5027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SGP-5 (2-4)Lab ID:92468257007 Collected:03/04/20 12:10 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 59.2J ug/kg 03/06/20 17:26 67-64-103/06/20 10:1711010.4 1
Benzene ND ug/kg 03/06/20 17:26 71-43-203/06/20 10:175.5 0.99 1
Bromobenzene ND ug/kg 03/06/20 17:26 108-86-103/06/20 10:175.5 1.5 1
Bromochloromethane ND ug/kg 03/06/20 17:26 74-97-503/06/20 10:175.5 1.4 1
Bromodichloromethane ND ug/kg 03/06/20 17:26 75-27-403/06/20 10:175.5 1.1 1
Bromoform ND ug/kg 03/06/20 17:26 75-25-203/06/20 10:175.5 2.7 1
Bromomethane ND ug/kg 03/06/20 17:26 74-83-903/06/20 10:1711.0 2.6 1
2-Butanone (MEK)ND ug/kg 03/06/20 17:26 78-93-303/06/20 10:1711013.1 1
n-Butylbenzene 48.8 ug/kg 03/06/20 17:26 104-51-803/06/20 10:175.5 3.1 1
sec-Butylbenzene 73.9 ug/kg 03/06/20 17:26 135-98-803/06/20 10:175.5 2.3 1
tert-Butylbenzene ND ug/kg 03/06/20 17:26 98-06-603/06/20 10:175.5 1.9 1
Carbon tetrachloride ND ug/kg 03/06/20 17:26 56-23-503/06/20 10:175.5 1.1 1
Chlorobenzene ND ug/kg 03/06/20 17:26 108-90-703/06/20 10:175.5 1.1 1
Chloroethane ND ug/kg 03/06/20 17:26 75-00-303/06/20 10:1711.0 2.3 1
Chloroform ND ug/kg 03/06/20 17:26 67-66-303/06/20 10:175.5 1.2 1
Chloromethane ND ug/kg 03/06/20 17:26 74-87-3 v203/06/20 10:1711.0 3.6 1
2-Chlorotoluene ND ug/kg 03/06/20 17:26 95-49-803/06/20 10:175.5 1.7 1
4-Chlorotoluene ND ug/kg 03/06/20 17:26 106-43-403/06/20 10:175.5 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/06/20 17:26 96-12-803/06/20 10:175.5 2.8 1
Dibromochloromethane ND ug/kg 03/06/20 17:26 124-48-103/06/20 10:175.5 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 03/06/20 17:26 106-93-403/06/20 10:175.5 1.2 1
Dibromomethane ND ug/kg 03/06/20 17:26 74-95-303/06/20 10:175.5 1.6 1
1,2-Dichlorobenzene ND ug/kg 03/06/20 17:26 95-50-103/06/20 10:175.5 1.9 1
1,3-Dichlorobenzene ND ug/kg 03/06/20 17:26 541-73-103/06/20 10:175.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 03/06/20 17:26 106-46-703/06/20 10:175.5 1.9 1
Dichlorodifluoromethane ND ug/kg 03/06/20 17:26 75-71-803/06/20 10:1711.0 4.5 1
1,1-Dichloroethane ND ug/kg 03/06/20 17:26 75-34-303/06/20 10:175.5 0.81 1
1,2-Dichloroethane ND ug/kg 03/06/20 17:26 107-06-203/06/20 10:175.5 1.1 1
1,1-Dichloroethene ND ug/kg 03/06/20 17:26 75-35-403/06/20 10:175.5 1.3 1
cis-1,2-Dichloroethene ND ug/kg 03/06/20 17:26 156-59-203/06/20 10:175.5 0.96 1
trans-1,2-Dichloroethene ND ug/kg 03/06/20 17:26 156-60-503/06/20 10:175.5 1.1 1
1,2-Dichloropropane ND ug/kg 03/06/20 17:26 78-87-503/06/20 10:175.5 2.1 1
1,3-Dichloropropane ND ug/kg 03/06/20 17:26 142-28-903/06/20 10:175.5 2.1 1
2,2-Dichloropropane ND ug/kg 03/06/20 17:26 594-20-703/06/20 10:175.5 0.54 1
1,1-Dichloropropene ND ug/kg 03/06/20 17:26 563-58-603/06/20 10:175.5 2.3 1
cis-1,3-Dichloropropene ND ug/kg 03/06/20 17:26 10061-01-503/06/20 10:175.5 2.5 1
trans-1,3-Dichloropropene ND ug/kg 03/06/20 17:26 10061-02-603/06/20 10:175.5 0.96 1
Diisopropyl ether ND ug/kg 03/06/20 17:26 108-20-303/06/20 10:175.5 3.1 1
Ethylbenzene 1.5J ug/kg 03/06/20 17:26 100-41-403/06/20 10:175.5 1.2 1
Hexachloro-1,3-butadiene ND ug/kg 03/06/20 17:26 87-68-303/06/20 10:175.5 2.7 1
2-Hexanone ND ug/kg 03/06/20 17:26 591-78-603/06/20 10:1755.0 5.7 1
Isopropylbenzene (Cumene)67.4 ug/kg 03/06/20 17:26 98-82-803/06/20 10:175.5 1.6 1
p-Isopropyltoluene 143 ug/kg 03/06/20 17:26 99-87-603/06/20 10:175.5 2.7 1
Methylene Chloride ND ug/kg 03/06/20 17:26 75-09-203/06/20 10:1722.0 6.5 1
4-Methyl-2-pentanone (MIBK)156 ug/kg 03/06/20 17:26 108-10-103/06/20 10:1755.0 4.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SGP-5 (2-4)Lab ID:92468257007 Collected:03/04/20 12:10 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 03/06/20 17:26 1634-04-403/06/20 10:175.5 3.1 1
Naphthalene 13.1 ug/kg 03/06/20 17:26 91-20-303/06/20 10:175.5 4.7 1
n-Propylbenzene 163 ug/kg 03/06/20 17:26 103-65-103/06/20 10:175.5 1.8 1
Styrene ND ug/kg 03/06/20 17:26 100-42-503/06/20 10:175.5 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/06/20 17:26 630-20-603/06/20 10:175.5 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/06/20 17:26 79-34-503/06/20 10:175.5 1.9 1
Tetrachloroethene ND ug/kg 03/06/20 17:26 127-18-403/06/20 10:175.5 1.7 1
Toluene ND ug/kg 03/06/20 17:26 108-88-303/06/20 10:175.5 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 03/06/20 17:26 87-61-603/06/20 10:175.5 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 03/06/20 17:26 120-82-103/06/20 10:175.5 2.9 1
1,1,1-Trichloroethane ND ug/kg 03/06/20 17:26 71-55-603/06/20 10:175.5 0.96 1
1,1,2-Trichloroethane ND ug/kg 03/06/20 17:26 79-00-503/06/20 10:175.5 1.2 1
Trichloroethene ND ug/kg 03/06/20 17:26 79-01-603/06/20 10:175.5 1.4 1
Trichlorofluoromethane ND ug/kg 03/06/20 17:26 75-69-403/06/20 10:175.5 1.3 1
1,2,3-Trichloropropane ND ug/kg 03/06/20 17:26 96-18-403/06/20 10:175.5 1.9 1
1,2,4-Trimethylbenzene 18300 ug/kg 03/10/20 15:52 95-63-603/09/20 13:48509198100
1,3,5-Trimethylbenzene 7000 ug/kg 03/10/20 15:52 108-67-803/09/20 13:48509170100
Vinyl acetate ND ug/kg 03/06/20 17:26 108-05-403/06/20 10:1755.0 17.9 1
Vinyl chloride ND ug/kg 03/06/20 17:26 75-01-403/06/20 10:1711.0 2.1 1
Xylene (Total)ND ug/kg 03/06/20 17:26 1330-20-703/06/20 10:1711.0 3.9 1
m&p-Xylene ND ug/kg 03/06/20 17:26 179601-23-103/06/20 10:1711.0 2.6 1
o-Xylene ND ug/kg 03/06/20 17:26 95-47-603/06/20 10:175.5 1.3 1
Surrogates
Toluene-d8 (S)94 %03/06/20 17:26 2037-26-503/06/20 10:1770-130 1
4-Bromofluorobenzene (S)156 %03/06/20 17:26 460-00-4 S503/06/20 10:1770-130 1
1,2-Dichloroethane-d4 (S)92 %03/06/20 17:26 17060-07-003/06/20 10:1770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.3 %03/05/20 17:480.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 73.4 %03/10/20 09:2303/10/20 09:131
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 03/11/20 12:02 18540-29-903/10/20 12:481.36 0.348 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SB-DUP Lab ID:92468257008 Collected:03/04/20 00:00 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 14.4J ug/kg 03/06/20 17:01 67-64-103/06/20 10:1797.7 9.2 1
Benzene ND ug/kg 03/06/20 17:01 71-43-203/06/20 10:174.9 0.88 1
Bromobenzene ND ug/kg 03/06/20 17:01 108-86-103/06/20 10:174.9 1.3 1
Bromochloromethane ND ug/kg 03/06/20 17:01 74-97-503/06/20 10:174.9 1.2 1
Bromodichloromethane ND ug/kg 03/06/20 17:01 75-27-403/06/20 10:174.9 0.96 1
Bromoform ND ug/kg 03/06/20 17:01 75-25-203/06/20 10:174.9 2.4 1
Bromomethane ND ug/kg 03/06/20 17:01 74-83-903/06/20 10:179.8 2.3 1
2-Butanone (MEK)ND ug/kg 03/06/20 17:01 78-93-303/06/20 10:1797.7 11.6 1
n-Butylbenzene ND ug/kg 03/06/20 17:01 104-51-803/06/20 10:174.9 2.8 1
sec-Butylbenzene ND ug/kg 03/06/20 17:01 135-98-803/06/20 10:174.9 2.1 1
tert-Butylbenzene ND ug/kg 03/06/20 17:01 98-06-603/06/20 10:174.9 1.7 1
Carbon tetrachloride ND ug/kg 03/06/20 17:01 56-23-503/06/20 10:174.9 0.94 1
Chlorobenzene ND ug/kg 03/06/20 17:01 108-90-703/06/20 10:174.9 0.95 1
Chloroethane ND ug/kg 03/06/20 17:01 75-00-303/06/20 10:179.8 2.0 1
Chloroform ND ug/kg 03/06/20 17:01 67-66-303/06/20 10:174.9 1.0 1
Chloromethane ND ug/kg 03/06/20 17:01 74-87-3 v203/06/20 10:179.8 3.2 1
2-Chlorotoluene ND ug/kg 03/06/20 17:01 95-49-803/06/20 10:174.9 1.5 1
4-Chlorotoluene ND ug/kg 03/06/20 17:01 106-43-403/06/20 10:174.9 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/06/20 17:01 96-12-803/06/20 10:174.9 2.5 1
Dibromochloromethane ND ug/kg 03/06/20 17:01 124-48-103/06/20 10:174.9 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 03/06/20 17:01 106-93-403/06/20 10:174.9 1.1 1
Dibromomethane ND ug/kg 03/06/20 17:01 74-95-303/06/20 10:174.9 1.5 1
1,2-Dichlorobenzene ND ug/kg 03/06/20 17:01 95-50-103/06/20 10:174.9 1.7 1
1,3-Dichlorobenzene ND ug/kg 03/06/20 17:01 541-73-103/06/20 10:174.9 1.7 1
1,4-Dichlorobenzene ND ug/kg 03/06/20 17:01 106-46-703/06/20 10:174.9 1.7 1
Dichlorodifluoromethane ND ug/kg 03/06/20 17:01 75-71-803/06/20 10:179.8 4.0 1
1,1-Dichloroethane ND ug/kg 03/06/20 17:01 75-34-303/06/20 10:174.9 0.72 1
1,2-Dichloroethane ND ug/kg 03/06/20 17:01 107-06-203/06/20 10:174.9 0.98 1
1,1-Dichloroethene ND ug/kg 03/06/20 17:01 75-35-403/06/20 10:174.9 1.1 1
cis-1,2-Dichloroethene ND ug/kg 03/06/20 17:01 156-59-203/06/20 10:174.9 0.85 1
trans-1,2-Dichloroethene ND ug/kg 03/06/20 17:01 156-60-503/06/20 10:174.9 0.96 1
1,2-Dichloropropane ND ug/kg 03/06/20 17:01 78-87-503/06/20 10:174.9 1.8 1
1,3-Dichloropropane ND ug/kg 03/06/20 17:01 142-28-903/06/20 10:174.9 1.8 1
2,2-Dichloropropane ND ug/kg 03/06/20 17:01 594-20-703/06/20 10:174.9 0.48 1
1,1-Dichloropropene ND ug/kg 03/06/20 17:01 563-58-603/06/20 10:174.9 2.1 1
cis-1,3-Dichloropropene ND ug/kg 03/06/20 17:01 10061-01-503/06/20 10:174.9 2.2 1
trans-1,3-Dichloropropene ND ug/kg 03/06/20 17:01 10061-02-603/06/20 10:174.9 0.85 1
Diisopropyl ether ND ug/kg 03/06/20 17:01 108-20-303/06/20 10:174.9 2.8 1
Ethylbenzene ND ug/kg 03/06/20 17:01 100-41-403/06/20 10:174.9 1.0 1
Hexachloro-1,3-butadiene ND ug/kg 03/06/20 17:01 87-68-303/06/20 10:174.9 2.4 1
2-Hexanone ND ug/kg 03/06/20 17:01 591-78-603/06/20 10:1748.8 5.1 1
Isopropylbenzene (Cumene)ND ug/kg 03/06/20 17:01 98-82-803/06/20 10:174.9 1.4 1
p-Isopropyltoluene ND ug/kg 03/06/20 17:01 99-87-603/06/20 10:174.9 2.4 1
Methylene Chloride ND ug/kg 03/06/20 17:01 75-09-203/06/20 10:1719.5 5.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/06/20 17:01 108-10-103/06/20 10:1748.8 3.6 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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Page 21 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468257
BOU-014
Sample:SB-DUP Lab ID:92468257008 Collected:03/04/20 00:00 Received:03/05/20 07:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 03/06/20 17:01 1634-04-403/06/20 10:174.9 2.8 1
Naphthalene ND ug/kg 03/06/20 17:01 91-20-303/06/20 10:174.9 4.2 1
n-Propylbenzene ND ug/kg 03/06/20 17:01 103-65-103/06/20 10:174.9 1.6 1
Styrene ND ug/kg 03/06/20 17:01 100-42-503/06/20 10:174.9 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/06/20 17:01 630-20-603/06/20 10:174.9 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/06/20 17:01 79-34-503/06/20 10:174.9 1.7 1
Tetrachloroethene ND ug/kg 03/06/20 17:01 127-18-403/06/20 10:174.9 1.5 1
Toluene ND ug/kg 03/06/20 17:01 108-88-303/06/20 10:174.9 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 03/06/20 17:01 87-61-603/06/20 10:174.9 3.5 1
1,2,4-Trichlorobenzene ND ug/kg 03/06/20 17:01 120-82-103/06/20 10:174.9 2.6 1
1,1,1-Trichloroethane ND ug/kg 03/06/20 17:01 71-55-603/06/20 10:174.9 0.85 1
1,1,2-Trichloroethane ND ug/kg 03/06/20 17:01 79-00-503/06/20 10:174.9 1.1 1
Trichloroethene ND ug/kg 03/06/20 17:01 79-01-603/06/20 10:174.9 1.3 1
Trichlorofluoromethane ND ug/kg 03/06/20 17:01 75-69-403/06/20 10:174.9 1.2 1
1,2,3-Trichloropropane ND ug/kg 03/06/20 17:01 96-18-403/06/20 10:174.9 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/06/20 17:01 95-63-603/06/20 10:174.9 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 03/06/20 17:01 108-67-803/06/20 10:174.9 1.6 1
Vinyl acetate ND ug/kg 03/06/20 17:01 108-05-403/06/20 10:1748.8 15.9 1
Vinyl chloride ND ug/kg 03/06/20 17:01 75-01-403/06/20 10:179.8 1.9 1
Xylene (Total)ND ug/kg 03/06/20 17:01 1330-20-703/06/20 10:179.8 3.4 1
m&p-Xylene ND ug/kg 03/06/20 17:01 179601-23-103/06/20 10:179.8 2.3 1
o-Xylene ND ug/kg 03/06/20 17:01 95-47-603/06/20 10:174.9 1.1 1
Surrogates
Toluene-d8 (S)101 %03/06/20 17:01 2037-26-503/06/20 10:1770-130 1
4-Bromofluorobenzene (S)101 %03/06/20 17:01 460-00-403/06/20 10:1770-130 1
1,2-Dichloroethane-d4 (S)98 %03/06/20 17:01 17060-07-003/06/20 10:1770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.9 %03/05/20 17:490.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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Page 22 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1440109
3050B
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples:92468257001, 92468257002, 92468257003, 92468257004, 92468257007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3506765-1
Associated Lab Samples:92468257001, 92468257002, 92468257003, 92468257004, 92468257007
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.500 03/09/20 10:100.125
Barium mg/kg ND 1.00 03/09/20 10:100.160
Cadmium mg/kg ND 0.500 03/09/20 10:100.0800
Chromium mg/kg ND 1.00 03/09/20 10:100.270
Lead mg/kg ND 0.500 03/09/20 10:100.120
Selenium mg/kg ND 0.500 03/09/20 10:100.190
Silver mg/kg ND 0.500 03/09/20 10:100.155
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3506765-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 98.6100 98.6 80.0-120
Barium mg/kg 99.2100 99.2 80.0-120
Cadmium mg/kg 106100 106 80.0-120
Chromium mg/kg 102100 102 80.0-120
Lead mg/kg 103100 103 80.0-120
Selenium mg/kg 104100 104 80.0-120
Silver mg/kg 21.820.0 109 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3506765-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1196302-01
R3506765-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 23.0 93.0 75.0-12586.7 6.62 2023.05.42 112 105
Barium mg/kg 23.0 108 75.0-12588.2 10.7 2023.097.1 221 198
Cadmium mg/kg 23.0 102 75.0-12595.9 6.37 2023.00.532 118 111
Chromium mg/kg MH,R123.0 100 75.0-125184 52.3 2023.020.5 136 232
Lead mg/kg P623.0 0.00 75.0-1250.00 0.127 2023.02720 183 183
Selenium mg/kg 23.0 102 75.0-12594.6 7.65 2023.00.357 118 109
Silver mg/kg 4.59 104 75.0-12594.9 9.25 204.59ND 23.9 21.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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Huntersville, NC 28078
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Page 23 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1440077
7471A
EPA 7471B
Mercury 7471B
Associated Lab Samples:92468257001, 92468257002, 92468257003, 92468257004, 92468257007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3506899-1
Associated Lab Samples:92468257001, 92468257002, 92468257003, 92468257004, 92468257007
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0300 03/09/20 19:480.00280
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3506899-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.4800.500 96.0 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3506899-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1196511-02
R3506899-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.500 87.1 75.0-12595.7 9.45 200.500ND 0.435 0.479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
528971
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92468257005, 92468257007, 92468257008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2825134
Associated Lab Samples:92468257005, 92468257007, 92468257008
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/06/20 11:101.2
1,1,1-Trichloroethane ug/kg ND 5.0 03/06/20 11:100.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/06/20 11:101.7
1,1,2-Trichloroethane ug/kg ND 5.0 03/06/20 11:101.1
1,1-Dichloroethane ug/kg ND 5.0 03/06/20 11:100.74
1,1-Dichloroethene ug/kg ND 5.0 03/06/20 11:101.2
1,1-Dichloropropene ug/kg ND 5.0 03/06/20 11:102.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/06/20 11:103.6
1,2,3-Trichloropropane ug/kg ND 5.0 03/06/20 11:101.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/06/20 11:102.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/06/20 11:102.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/06/20 11:102.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/06/20 11:101.1
1,2-Dichlorobenzene ug/kg ND 5.0 03/06/20 11:101.8
1,2-Dichloroethane ug/kg ND 5.0 03/06/20 11:101.0
1,2-Dichloropropane ug/kg ND 5.0 03/06/20 11:101.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/06/20 11:101.7
1,3-Dichlorobenzene ug/kg ND 5.0 03/06/20 11:101.8
1,3-Dichloropropane ug/kg ND 5.0 03/06/20 11:101.9
1,4-Dichlorobenzene ug/kg ND 5.0 03/06/20 11:101.7
2,2-Dichloropropane ug/kg ND 5.0 03/06/20 11:100.49
2-Butanone (MEK)ug/kg ND 100 03/06/20 11:1011.9
2-Chlorotoluene ug/kg ND 5.0 03/06/20 11:101.5
2-Hexanone ug/kg ND 50.0 03/06/20 11:105.2
4-Chlorotoluene ug/kg ND 5.0 03/06/20 11:101.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 03/06/20 11:103.7
Acetone ug/kg ND 100 03/06/20 11:109.4
Benzene ug/kg ND 5.0 03/06/20 11:100.90
Bromobenzene ug/kg ND 5.0 03/06/20 11:101.4
Bromochloromethane ug/kg ND 5.0 03/06/20 11:101.2
Bromodichloromethane ug/kg ND 5.0 03/06/20 11:100.98
Bromoform ug/kg ND 5.0 03/06/20 11:102.4
Bromomethane ug/kg ND 10.0 03/06/20 11:102.4
Carbon tetrachloride ug/kg ND 5.0 03/06/20 11:100.96
Chlorobenzene ug/kg ND 5.0 03/06/20 11:100.97
Chloroethane ug/kg ND 10.0 03/06/20 11:102.1
Chloroform ug/kg ND 5.0 03/06/20 11:101.1
Chloromethane ug/kg ND 10.0 v203/06/20 11:103.3
cis-1,2-Dichloroethene ug/kg ND 5.0 03/06/20 11:100.87
cis-1,3-Dichloropropene ug/kg ND 5.0 03/06/20 11:102.3
Dibromochloromethane ug/kg ND 5.0 03/06/20 11:102.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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[phone]
Page 25 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2825134
Associated Lab Samples:92468257005, 92468257007, 92468257008
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.0 03/06/20 11:101.5
Dichlorodifluoromethane ug/kg ND 10.0 03/06/20 11:104.1
Diisopropyl ether ug/kg ND 5.0 03/06/20 11:102.9
Ethylbenzene ug/kg ND 5.0 03/06/20 11:101.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 03/06/20 11:102.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/06/20 11:101.4
m&p-Xylene ug/kg ND 10.0 03/06/20 11:102.4
Methyl-tert-butyl ether ug/kg ND 5.0 03/06/20 11:102.9
Methylene Chloride ug/kg ND 20.0 03/06/20 11:105.9
n-Butylbenzene ug/kg ND 5.0 03/06/20 11:102.8
n-Propylbenzene ug/kg ND 5.0 03/06/20 11:101.7
Naphthalene ug/kg ND 5.0 03/06/20 11:104.2
o-Xylene ug/kg ND 5.0 03/06/20 11:101.2
p-Isopropyltoluene ug/kg ND 5.0 03/06/20 11:102.4
sec-Butylbenzene ug/kg ND 5.0 03/06/20 11:102.1
Styrene ug/kg ND 5.0 03/06/20 11:101.5
tert-Butylbenzene ug/kg ND 5.0 03/06/20 11:101.7
Tetrachloroethene ug/kg ND 5.0 03/06/20 11:101.6
Toluene ug/kg ND 5.0 03/06/20 11:101.6
trans-1,2-Dichloroethene ug/kg ND 5.0 03/06/20 11:100.98
trans-1,3-Dichloropropene ug/kg ND 5.0 03/06/20 11:100.88
Trichloroethene ug/kg ND 5.0 03/06/20 11:101.3
Trichlorofluoromethane ug/kg ND 5.0 03/06/20 11:101.2
Vinyl acetate ug/kg ND 50.0 03/06/20 11:1016.3
Vinyl chloride ug/kg ND 10.0 03/06/20 11:101.9
Xylene (Total)ug/kg ND 10.0 03/06/20 11:103.5
1,2-Dichloroethane-d4 (S)%91 70-132 03/06/20 11:10
4-Bromofluorobenzene (S)%102 70-130 03/06/20 11:10
Toluene-d8 (S)%101 70-130 03/06/20 11:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2825135LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2825136
1,1,1,2-Tetrachloroethane ug/kg 53.250 106 70-13010753.4 0 30
1,1,1-Trichloroethane ug/kg 44.450 89 70-1308944.5 0 30
1,1,2,2-Tetrachloroethane ug/kg 49.050 98 55-13010049.9 2 30
1,1,2-Trichloroethane ug/kg 51.050 102 70-13010451.8 2 30
1,1-Dichloroethane ug/kg 42.750 85 68-1308642.9 1 30
1,1-Dichloroethene ug/kg 45.150 90 70-1309045.1 0 30
1,1-Dichloropropene ug/kg 47.350 95 70-1309647.9 1 30
1,2,3-Trichlorobenzene ug/kg 54.450 109 70-13010753.5 2 30
1,2,3-Trichloropropane ug/kg 47.750 95 70-1309849.0 3 30
1,2,4-Trichlorobenzene ug/kg 56.050 112 70-13010854.0 4 30
1,2,4-Trimethylbenzene ug/kg 54.750 109 69-13010854.1 1 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 26 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2825135LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2825136
1,2-Dibromo-3-chloropropane ug/kg 52.850 106 57-14110552.5 0 30
1,2-Dibromoethane (EDB)ug/kg 49.850 100 70-13010049.9 0 30
1,2-Dichlorobenzene ug/kg 52.750 105 70-13010653.1 1 30
1,2-Dichloroethane ug/kg 43.950 88 70-1308844.1 0 30
1,2-Dichloropropane ug/kg 48.650 97 70-1309849.0 1 30
1,3,5-Trimethylbenzene ug/kg 55.350 111 70-13011055.1 0 30
1,3-Dichlorobenzene ug/kg 53.750 107 70-13010753.3 1 30
1,3-Dichloropropane ug/kg 48.350 97 70-1309949.3 2 30
1,4-Dichlorobenzene ug/kg 54.350 109 70-13010954.7 1 30
2,2-Dichloropropane ug/kg 45.050 90 70-1308944.5 1 30
2-Butanone (MEK)ug/kg 89.1J100 89 60-1309292.2J 30
2-Chlorotoluene ug/kg 55.450 111 70-13010954.5 2 30
2-Hexanone ug/kg 97.9100 98 70-132101101 3 30
4-Chlorotoluene ug/kg 56.050 112 70-13010954.3 3 30
4-Methyl-2-pentanone (MIBK)ug/kg 97.2100 97 69-130100100 3 30
Acetone ug/kg 82.6J100 83 49-1488382.8J 30
Benzene ug/kg 47.450 95 70-1309647.9 1 30
Bromobenzene ug/kg 54.350 109 70-13010954.7 1 30
Bromochloromethane ug/kg 44.050 88 70-1309045.2 3 30
Bromodichloromethane ug/kg 51.550 103 70-13010351.5 0 30
Bromoform ug/kg 52.350 105 68-13610552.7 1 30
Bromomethane ug/kg 55.750 111 60-14011356.3 1 30
Carbon tetrachloride ug/kg 50.850 102 70-13010050.2 1 30
Chlorobenzene ug/kg 52.150 104 70-13010351.5 1 30
Chloroethane ug/kg 44.550 89 51-1479547.7 7 30
Chloroform ug/kg 43.650 87 70-1309346.7 7 30
Chloromethane ug/kg 33.6 v3506748-1306733.3 1 30
cis-1,2-Dichloroethene ug/kg 43.050 86 70-1308642.9 0 30
cis-1,3-Dichloropropene ug/kg 50.550 101 70-13010050.2 1 30
Dibromochloromethane ug/kg 52.550 105 70-13010451.8 1 30
Dibromomethane ug/kg 48.250 96 70-1309648.2 0 30
Dichlorodifluoromethane ug/kg 44.050 88 49-1308844.1 0 30
Diisopropyl ether ug/kg 45.650 91 66-1309246.0 1 30
Ethylbenzene ug/kg 50.050 100 70-1309949.3 1 30
Hexachloro-1,3-butadiene ug/kg 59.850 120 70-13011557.6 4 30
Isopropylbenzene (Cumene)ug/kg 52.850 106 70-13010452.1 1 30
m&p-Xylene ug/kg 103100 103 70-130101101 1 30
Methyl-tert-butyl ether ug/kg 45.550 91 70-1309346.4 2 30
Methylene Chloride ug/kg 41.050 82 50-1378341.6 2 30
n-Butylbenzene ug/kg 55.850 112 70-13010854.2 3 30
n-Propylbenzene ug/kg 54.750 109 70-13010753.6 2 30
Naphthalene ug/kg 50.550 101 70-13110451.8 3 30
o-Xylene ug/kg 51.350 103 70-13010250.8 1 30
p-Isopropyltoluene ug/kg 56.650 113 70-13011155.4 2 30
sec-Butylbenzene ug/kg 54.650 109 70-13010653.2 3 30
Styrene ug/kg 53.350 107 70-13010552.7 1 30
tert-Butylbenzene ug/kg 48.750 97 69-1309647.8 2 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
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Page 27 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2825135LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2825136
Tetrachloroethene ug/kg 51.650 103 56-13010150.7 2 30
Toluene ug/kg 48.950 98 70-1309748.7 0 30
trans-1,2-Dichloroethene ug/kg 43.250 86 70-1308542.7 1 30
trans-1,3-Dichloropropene ug/kg 51.450 103 70-13010552.5 2 30
Trichloroethene ug/kg 51.750 103 70-14110150.4 3 30
Trichlorofluoromethane ug/kg 46.250 92 67-1309145.7 1 30
Vinyl acetate ug/kg 118100 118 10-136113113 4 30
Vinyl chloride ug/kg 47.750 95 67-1309547.6 0 30
Xylene (Total)ug/kg 154150 103 70-130101152 1 30
1,2-Dichloroethane-d4 (S)%88 70-13286
4-Bromofluorobenzene (S)%98 70-13097
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
529261
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92468257006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2826678
Associated Lab Samples:92468257006
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/09/20 11:271.2
1,1,1-Trichloroethane ug/kg ND 5.0 03/09/20 11:270.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/09/20 11:271.7
1,1,2-Trichloroethane ug/kg ND 5.0 03/09/20 11:271.1
1,1-Dichloroethane ug/kg ND 5.0 03/09/20 11:270.74
1,1-Dichloroethene ug/kg ND 5.0 03/09/20 11:271.2
1,1-Dichloropropene ug/kg ND 5.0 03/09/20 11:272.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/09/20 11:273.6
1,2,3-Trichloropropane ug/kg ND 5.0 03/09/20 11:271.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/09/20 11:272.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/09/20 11:272.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/09/20 11:272.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/09/20 11:271.1
1,2-Dichlorobenzene ug/kg ND 5.0 03/09/20 11:271.8
1,2-Dichloroethane ug/kg ND 5.0 03/09/20 11:271.0
1,2-Dichloropropane ug/kg ND 5.0 03/09/20 11:271.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/09/20 11:271.7
1,3-Dichlorobenzene ug/kg ND 5.0 03/09/20 11:271.8
1,3-Dichloropropane ug/kg ND 5.0 03/09/20 11:271.9
1,4-Dichlorobenzene ug/kg ND 5.0 03/09/20 11:271.7
2,2-Dichloropropane ug/kg ND 5.0 03/09/20 11:270.49
2-Butanone (MEK)ug/kg ND 100 03/09/20 11:2711.9
2-Chlorotoluene ug/kg ND 5.0 03/09/20 11:271.5
2-Hexanone ug/kg ND 50.0 03/09/20 11:275.2
4-Chlorotoluene ug/kg ND 5.0 03/09/20 11:271.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 03/09/20 11:273.7
Acetone ug/kg ND 100 03/09/20 11:279.4
Benzene ug/kg ND 5.0 03/09/20 11:270.90
Bromobenzene ug/kg ND 5.0 03/09/20 11:271.4
Bromochloromethane ug/kg ND 5.0 03/09/20 11:271.2
Bromodichloromethane ug/kg ND 5.0 03/09/20 11:270.98
Bromoform ug/kg ND 5.0 03/09/20 11:272.4
Bromomethane ug/kg ND 10.0 03/09/20 11:272.4
Carbon tetrachloride ug/kg ND 5.0 03/09/20 11:270.96
Chlorobenzene ug/kg ND 5.0 03/09/20 11:270.97
Chloroethane ug/kg ND 10.0 03/09/20 11:272.1
Chloroform ug/kg ND 5.0 03/09/20 11:271.1
Chloromethane ug/kg ND 10.0 v203/09/20 11:273.3
cis-1,2-Dichloroethene ug/kg ND 5.0 03/09/20 11:270.87
cis-1,3-Dichloropropene ug/kg ND 5.0 03/09/20 11:272.3
Dibromochloromethane ug/kg ND 5.0 03/09/20 11:272.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2826678
Associated Lab Samples:92468257006
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.0 03/09/20 11:271.5
Dichlorodifluoromethane ug/kg ND 10.0 03/09/20 11:274.1
Diisopropyl ether ug/kg ND 5.0 03/09/20 11:272.9
Ethylbenzene ug/kg ND 5.0 03/09/20 11:271.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 03/09/20 11:272.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/09/20 11:271.4
m&p-Xylene ug/kg ND 10.0 03/09/20 11:272.4
Methyl-tert-butyl ether ug/kg ND 5.0 03/09/20 11:272.9
Methylene Chloride ug/kg ND 20.0 03/09/20 11:275.9
n-Butylbenzene ug/kg ND 5.0 03/09/20 11:272.8
n-Propylbenzene ug/kg ND 5.0 03/09/20 11:271.7
Naphthalene ug/kg ND 5.0 03/09/20 11:274.2
o-Xylene ug/kg ND 5.0 03/09/20 11:271.2
p-Isopropyltoluene ug/kg ND 5.0 03/09/20 11:272.4
sec-Butylbenzene ug/kg ND 5.0 03/09/20 11:272.1
Styrene ug/kg ND 5.0 03/09/20 11:271.5
tert-Butylbenzene ug/kg ND 5.0 03/09/20 11:271.7
Tetrachloroethene ug/kg ND 5.0 03/09/20 11:271.6
Toluene ug/kg ND 5.0 03/09/20 11:271.6
trans-1,2-Dichloroethene ug/kg ND 5.0 03/09/20 11:270.98
trans-1,3-Dichloropropene ug/kg ND 5.0 03/09/20 11:270.88
Trichloroethene ug/kg ND 5.0 03/09/20 11:271.3
Trichlorofluoromethane ug/kg ND 5.0 03/09/20 11:271.2
Vinyl acetate ug/kg ND 50.0 v103/09/20 11:2716.3
Vinyl chloride ug/kg ND 10.0 03/09/20 11:271.9
Xylene (Total)ug/kg ND 10.0 03/09/20 11:273.5
1,2-Dichloroethane-d4 (S)%98 70-132 03/09/20 11:27
4-Bromofluorobenzene (S)%102 70-130 03/09/20 11:27
Toluene-d8 (S)%102 70-130 03/09/20 11:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2826679LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 52.950 106 70-130
1,1,1-Trichloroethane ug/kg 46.350 93 70-130
1,1,2,2-Tetrachloroethane ug/kg 48.850 98 55-130
1,1,2-Trichloroethane ug/kg 51.250 102 70-130
1,1-Dichloroethane ug/kg 43.550 87 68-130
1,1-Dichloroethene ug/kg 46.350 93 70-130
1,1-Dichloropropene ug/kg 48.050 96 70-130
1,2,3-Trichlorobenzene ug/kg 52.250 104 70-130
1,2,3-Trichloropropane ug/kg 47.850 96 70-130
1,2,4-Trichlorobenzene ug/kg 55.250 110 70-130
1,2,4-Trimethylbenzene ug/kg 53.450 107 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2826679LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 50.750 101 57-141
1,2-Dibromoethane (EDB)ug/kg 49.550 99 70-130
1,2-Dichlorobenzene ug/kg 51.450 103 70-130
1,2-Dichloroethane ug/kg 45.350 91 70-130
1,2-Dichloropropane ug/kg 48.550 97 70-130
1,3,5-Trimethylbenzene ug/kg 52.850 106 70-130
1,3-Dichlorobenzene ug/kg 52.750 105 70-130
1,3-Dichloropropane ug/kg 48.550 97 70-130
1,4-Dichlorobenzene ug/kg 52.750 105 70-130
2,2-Dichloropropane ug/kg 47.350 95 70-130
2-Butanone (MEK)ug/kg 96.2J100 96 60-130
2-Chlorotoluene ug/kg 53.450 107 70-130
2-Hexanone ug/kg 99.3100 99 70-132
4-Chlorotoluene ug/kg 53.350 107 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 98.9100 99 69-130
Acetone ug/kg 84.9J100 85 49-148
Benzene ug/kg 48.350 97 70-130
Bromobenzene ug/kg 52.150 104 70-130
Bromochloromethane ug/kg 46.750 93 70-130
Bromodichloromethane ug/kg 51.750 103 70-130
Bromoform ug/kg 54.050 108 68-136
Bromomethane ug/kg 54.650 109 60-140
Carbon tetrachloride ug/kg 51.950 104 70-130
Chlorobenzene ug/kg 50.250 100 70-130
Chloroethane ug/kg 45.650 91 51-147
Chloroform ug/kg 45.950 92 70-130
Chloromethane ug/kg 34.4 v3506948-130
cis-1,2-Dichloroethene ug/kg 43.650 87 70-130
cis-1,3-Dichloropropene ug/kg 50.350 101 70-130
Dibromochloromethane ug/kg 51.550 103 70-130
Dibromomethane ug/kg 47.950 96 70-130
Dichlorodifluoromethane ug/kg 46.350 93 49-130
Diisopropyl ether ug/kg 46.950 94 66-130
Ethylbenzene ug/kg 48.450 97 70-130
Hexachloro-1,3-butadiene ug/kg 58.650 117 70-130
Isopropylbenzene (Cumene)ug/kg 52.250 104 70-130
m&p-Xylene ug/kg 99.6100 100 70-130
Methyl-tert-butyl ether ug/kg 49.250 98 70-130
Methylene Chloride ug/kg 41.750 83 50-137
n-Butylbenzene ug/kg 52.750 105 70-130
n-Propylbenzene ug/kg 51.350 103 70-130
Naphthalene ug/kg 49.950 100 70-131
o-Xylene ug/kg 50.150 100 70-130
p-Isopropyltoluene ug/kg 53.350 107 70-130
sec-Butylbenzene ug/kg 51.750 103 70-130
Styrene ug/kg 52.850 106 70-130
tert-Butylbenzene ug/kg 46.250 92 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2826679LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 51.750 103 56-130
Toluene ug/kg 49.050 98 70-130
trans-1,2-Dichloroethene ug/kg 42.950 86 70-130
trans-1,3-Dichloropropene ug/kg 50.850 102 70-130
Trichloroethene ug/kg 52.450 105 70-141
Trichlorofluoromethane ug/kg 48.050 96 67-130
Vinyl acetate ug/kg 126 v110012610-136
Vinyl chloride ug/kg 49.250 98 67-130
Xylene (Total)ug/kg 150150 100 70-130
1,2-Dichloroethane-d4 (S)%88 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2827182MATRIX SPIKE SAMPLE:
MSSpike
Result
92468413002
1,1,1,2-Tetrachloroethane ug/kg 30.637.3 82 52-133ND
1,1,1-Trichloroethane ug/kg 23.437.3 63 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 30.637.3 82 39-150ND
1,1,2-Trichloroethane ug/kg 29.437.3 79 48-140ND
1,1-Dichloroethane ug/kg 22.237.3 59 46-135ND
1,1-Dichloroethene ug/kg 11.8 M137.3 32 38-149ND
1,1-Dichloropropene ug/kg 23.537.3 63 41-140ND
1,2,3-Trichlorobenzene ug/kg 9.937.3 26 10-158ND
1,2,3-Trichloropropane ug/kg 25.837.3 69 33-157ND
1,2,4-Trichlorobenzene ug/kg 13.037.3 35 10-155ND
1,2,4-Trimethylbenzene ug/kg 49.137.3 132 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 23.937.3 64 33-158ND
1,2-Dibromoethane (EDB)ug/kg 33.237.3 89 40-136ND
1,2-Dichlorobenzene ug/kg 20.637.3 55 27-146ND
1,2-Dichloroethane ug/kg 26.337.3 70 49-140ND
1,2-Dichloropropane ug/kg 29.437.3 79 44-143ND
1,3,5-Trimethylbenzene ug/kg 33.137.3 89 40-144ND
1,3-Dichlorobenzene ug/kg 24.137.3 64 33-140ND
1,3-Dichloropropane ug/kg 33.037.3 88 47-147ND
1,4-Dichlorobenzene ug/kg 23.437.3 63 35-139ND
2,2-Dichloropropane ug/kg 22.837.3 61 41-140ND
2-Butanone (MEK)ug/kg 147J M174.7 188 10-181ND
2-Chlorotoluene ug/kg 31.937.3 85 38-147ND
2-Hexanone ug/kg 200 M174.7 267 18-169ND
4-Chlorotoluene ug/kg 29.737.3 79 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 168 M174.7 226 16-175ND
Acetone ug/kg 344 M174.7 252 10-200ND
Benzene ug/kg 25.437.3 68 46-136ND
Bromobenzene ug/kg 29.037.3 78 38-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2827182MATRIX SPIKE SAMPLE:
MSSpike
Result
92468413002
Bromochloromethane ug/kg 25.537.3 68 44-142ND
Bromodichloromethane ug/kg 31.937.3 85 41-140ND
Bromoform ug/kg 23.537.3 63 34-145ND
Bromomethane ug/kg 6.6J37.3 18 14-162ND
Carbon tetrachloride ug/kg 25.137.3 67 44-141ND
Chlorobenzene ug/kg 28.437.3 76 39-141ND
Chloroethane ug/kg 7.8J37.3 21 10-182ND
Chloroform ug/kg 28.237.3 76 45-140ND
Chloromethane ug/kg ND M1,v337.3 3 19-149ND
cis-1,2-Dichloroethene ug/kg 22.937.3 61 38-150ND
cis-1,3-Dichloropropene ug/kg 28.237.3 75 30-144ND
Dibromochloromethane ug/kg 30.837.3 83 36-145ND
Dibromomethane ug/kg 27.237.3 73 41-145ND
Dichlorodifluoromethane ug/kg ND M137.3 0 16-146ND
Diisopropyl ether ug/kg 26.237.3 70 41-143ND
Ethylbenzene ug/kg 46.737.3 125 35-144ND
Hexachloro-1,3-butadiene ug/kg 19.237.3 51 10-160ND
Isopropylbenzene (Cumene)ug/kg 37.637.3 101 30-152ND
m&p-Xylene ug/kg 58.174.7 78 33-145ND
Methyl-tert-butyl ether ug/kg 25.937.3 69 49-140ND
Methylene Chloride ug/kg 25.7J37.3 59 10-174ND
n-Butylbenzene ug/kg 33.837.3 91 10-160ND
n-Propylbenzene ug/kg 59.7 M137.3 160 24-159ND
Naphthalene ug/kg 32.337.3 87 10-171ND
o-Xylene ug/kg 28.137.3 75 31-150ND
p-Isopropyltoluene ug/kg 37.137.3 87 21-154ND
sec-Butylbenzene ug/kg 39.337.3 105 19-159ND
Styrene ug/kg 19.037.3 51 15-152ND
tert-Butylbenzene ug/kg 31.637.3 85 31-141ND
Tetrachloroethene ug/kg 29.237.3 78 19-141ND
Toluene ug/kg 28.037.3 75 31-146ND
trans-1,2-Dichloroethene ug/kg 17.737.3 47 28-157ND
trans-1,3-Dichloropropene ug/kg 28.237.3 76 25-146ND
Trichloroethene ug/kg 28.337.3 76 34-149ND
Trichlorofluoromethane ug/kg 8.6J37.3 23 10-167ND
Vinyl acetate ug/kg 43.4J v174.7 58 10-200ND
Vinyl chloride ug/kg ND M137.3 3 36-155ND
Xylene (Total)ug/kg 86.2112 77 29-148ND
1,2-Dichloroethane-d4 (S)%88 70-132
4-Bromofluorobenzene (S)%90 70-130
Toluene-d8 (S)%94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92468413001
2827181SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg 47.6J 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 431 D63330600
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND v230ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92468413001
2827181SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND v130ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%97104
4-Bromofluorobenzene (S)%100100
Toluene-d8 (S)%100100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
528947
EPA 3546
EPA 8082A
8082 GCS PCB
Associated Lab Samples:92468257005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2825068
Associated Lab Samples:92468257005
Matrix:Solid
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/kg ND 33.4 03/06/20 21:189.0
PCB-1221 (Aroclor 1221)ug/kg ND 33.4 03/06/20 21:1811.9
PCB-1232 (Aroclor 1232)ug/kg ND 33.4 03/06/20 21:188.4
PCB-1242 (Aroclor 1242)ug/kg ND 33.4 03/06/20 21:182.2
PCB-1248 (Aroclor 1248)ug/kg ND 33.4 03/06/20 21:185.9
PCB-1254 (Aroclor 1254)ug/kg ND 33.4 03/06/20 21:186.3
PCB-1260 (Aroclor 1260)ug/kg ND 33.4 03/06/20 21:187.7
Decachlorobiphenyl (S)%78 10-130 03/06/20 21:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2825069LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/kg 128168 76 35-130
PCB-1260 (Aroclor 1260)ug/kg 119168 71 46-130
Decachlorobiphenyl (S)%79 10-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2825070MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92468257005
2825071
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
PCB-1016 (Aroclor 1016)ug/kg 201 48 10-13059 21 30203ND96.7 119
PCB-1260 (Aroclor 1260)ug/kg 201 40 10-13053 28 30203ND81.1 108
Decachlorobiphenyl (S)%52 10-13053
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
528950
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92468257003, 92468257004, 92468257007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2825072
Associated Lab Samples:92468257003, 92468257004, 92468257007
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 336 03/06/20 15:5576.9
1,2-Dichlorobenzene ug/kg ND 336 03/06/20 15:5572.6
1,3-Dichlorobenzene ug/kg ND 336 03/06/20 15:5575.6
1,4-Dichlorobenzene ug/kg ND 336 03/06/20 15:5573.8
1-Methylnaphthalene ug/kg ND 336 03/06/20 15:5589.4
2,2'-Oxybis(1-chloropropane)ug/kg ND 336 03/06/20 15:5593.3
2,4,5-Trichlorophenol ug/kg ND 336 03/06/20 15:5587.2
2,4,6-Trichlorophenol ug/kg ND 336 03/06/20 15:5584.3
2,4-Dichlorophenol ug/kg ND 336 03/06/20 15:55111
2,4-Dimethylphenol ug/kg ND 336 03/06/20 15:5583.6
2,4-Dinitrophenol ug/kg ND 1680 03/06/20 15:551070
2,4-Dinitrotoluene ug/kg ND 336 03/06/20 15:5588.9
2,6-Dinitrotoluene ug/kg ND 336 03/06/20 15:5587.8
2-Chloronaphthalene ug/kg ND 336 03/06/20 15:5574.7
2-Chlorophenol ug/kg ND 336 03/06/20 15:5578.1
2-Methylnaphthalene ug/kg ND 336 03/06/20 15:5585.4
2-Methylphenol(o-Cresol)ug/kg ND 336 03/06/20 15:5574.3
2-Nitroaniline ug/kg ND 1680 03/06/20 15:55169
2-Nitrophenol ug/kg ND 336 03/06/20 15:55104
3&4-Methylphenol(m&p Cresol)ug/kg ND 336 03/06/20 15:5584.4
3,3'-Dichlorobenzidine ug/kg ND 671 03/06/20 15:55234
3-Nitroaniline ug/kg ND 1680 03/06/20 15:55178
4,6-Dinitro-2-methylphenol ug/kg ND 671 03/06/20 15:55541
4-Bromophenylphenyl ether ug/kg ND 336 03/06/20 15:5588.1
4-Chloro-3-methylphenol ug/kg ND 671 03/06/20 15:55204
4-Chloroaniline ug/kg ND 671 03/06/20 15:55205
4-Chlorophenylphenyl ether ug/kg ND 336 03/06/20 15:5587.2
4-Nitroaniline ug/kg ND 671 03/06/20 15:55166
4-Nitrophenol ug/kg ND 1680 03/06/20 15:55535
Acenaphthene ug/kg ND 336 03/06/20 15:5586.3
Acenaphthylene ug/kg ND 336 03/06/20 15:5579.4
Aniline ug/kg ND 336 03/06/20 15:5575.4
Anthracene ug/kg ND 336 03/06/20 15:5587.1
Benzo(a)anthracene ug/kg ND 336 03/06/20 15:55107
Benzo(a)pyrene ug/kg ND 336 03/06/20 15:55145
Benzo(b)fluoranthene ug/kg ND 336 03/06/20 15:55135
Benzo(g,h,i)perylene ug/kg ND 336 03/06/20 15:55131
Benzo(k)fluoranthene ug/kg ND 336 03/06/20 15:55141
Benzoic Acid ug/kg ND 1680 03/06/20 15:55362
Benzyl alcohol ug/kg ND 671 03/06/20 15:55178
bis(2-Chloroethoxy)methane ug/kg ND 336 03/06/20 15:5589.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2825072
Associated Lab Samples:92468257003, 92468257004, 92468257007
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 336 03/06/20 15:5571.3
bis(2-Ethylhexyl)phthalate ug/kg ND 336 03/06/20 15:55110
Butylbenzylphthalate ug/kg ND 336 03/06/20 15:5589.4
Chrysene ug/kg ND 336 03/06/20 15:5597.4
Di-n-butylphthalate ug/kg ND 336 03/06/20 15:5582.8
Di-n-octylphthalate ug/kg ND 336 03/06/20 15:55191
Dibenz(a,h)anthracene ug/kg ND 336 03/06/20 15:55134
Dibenzofuran ug/kg ND 336 03/06/20 15:5583.9
Diethylphthalate ug/kg ND 336 03/06/20 15:5572.8
Dimethylphthalate ug/kg ND 336 03/06/20 15:5575.9
Fluoranthene ug/kg ND 336 03/06/20 15:55101
Fluorene ug/kg ND 336 03/06/20 15:5589.8
Hexachloro-1,3-butadiene ug/kg ND 336 03/06/20 15:5581.6
Hexachlorobenzene ug/kg ND 336 03/06/20 15:5585.2
Hexachlorocyclopentadiene ug/kg ND 336 03/06/20 15:55134
Hexachloroethane ug/kg ND 336 03/06/20 15:5576.5
Indeno(1,2,3-cd)pyrene ug/kg ND 336 03/06/20 15:55154
Isophorone ug/kg ND 336 03/06/20 15:5572.9
N-Nitroso-di-n-propylamine ug/kg ND 336 03/06/20 15:5594.0
N-Nitrosodimethylamine ug/kg ND 336 03/06/20 15:5594.4
N-Nitrosodiphenylamine ug/kg ND 336 03/06/20 15:5585.6
Naphthalene ug/kg ND 336 03/06/20 15:5580.3
Nitrobenzene ug/kg ND 336 03/06/20 15:5580.1
Pentachlorophenol ug/kg ND 671 03/06/20 15:55154
Phenanthrene ug/kg ND 336 03/06/20 15:5584.5
Phenol ug/kg ND 336 03/06/20 15:5580.1
Pyrene ug/kg ND 336 03/06/20 15:5592.3
Pyridine ug/kg ND 336 03/06/20 15:5584.9
2,4,6-Tribromophenol (S)%57 27-110 03/06/20 15:55
2-Fluorobiphenyl (S)%55 30-110 03/06/20 15:55
2-Fluorophenol (S)%58 13-110 03/06/20 15:55
Nitrobenzene-d5 (S)%53 23-110 03/06/20 15:55
Phenol-d6 (S)%53 22-110 03/06/20 15:55
Terphenyl-d14 (S)%57 28-110 03/06/20 15:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2825073LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10401690 62 52-130
1,2-Dichlorobenzene ug/kg 9681690 57 51-130
1,3-Dichlorobenzene ug/kg 9731690 57 50-130
1,4-Dichlorobenzene ug/kg 9601690 57 49-130
1-Methylnaphthalene ug/kg 10501690 62 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 9531690 56 30-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2825073LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/kg 10201690 60 55-130
2,4,6-Trichlorophenol ug/kg 10201690 60 57-130
2,4-Dichlorophenol ug/kg 9901690 58 56-130
2,4-Dimethylphenol ug/kg 11301690 67 51-130
2,4-Dinitrophenol ug/kg 51408470 61 27-133
2,4-Dinitrotoluene ug/kg 12701690 75 61-130
2,6-Dinitrotoluene ug/kg 12301690 72 60-130
2-Chloronaphthalene ug/kg 10201690 60 52-130
2-Chlorophenol ug/kg 10101690 60 54-130
2-Methylnaphthalene ug/kg 10301690 61 54-130
2-Methylphenol(o-Cresol)ug/kg 9531690 56 51-130
2-Nitroaniline ug/kg 19603390 58 51-130
2-Nitrophenol ug/kg 10401690 61 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 9551690 56 11-163
3,3'-Dichlorobenzidine ug/kg 20503390 61 10-132
3-Nitroaniline ug/kg 20803390 61 55-130
4,6-Dinitro-2-methylphenol ug/kg 24103390 71 47-142
4-Bromophenylphenyl ether ug/kg 11301690 66 59-130
4-Chloro-3-methylphenol ug/kg 21703390 64 55-130
4-Chloroaniline ug/kg 19703390 58 54-130
4-Chlorophenylphenyl ether ug/kg 10801690 63 58-130
4-Nitroaniline ug/kg 22103390 65 54-130
4-Nitrophenol ug/kg 58208470 69 48-130
Acenaphthene ug/kg 10301690 61 60-130
Acenaphthylene ug/kg 11701690 69 60-130
Aniline ug/kg 8801690 52 43-130
Anthracene ug/kg 12101690 71 63-130
Benzo(a)anthracene ug/kg 13701690 81 59-130
Benzo(a)pyrene ug/kg 13201690 78 57-130
Benzo(b)fluoranthene ug/kg 12601690 74 54-130
Benzo(g,h,i)perylene ug/kg 13101690 77 59-130
Benzo(k)fluoranthene ug/kg 12101690 71 54-130
Benzoic Acid ug/kg 38108470 45 19-130
Benzyl alcohol ug/kg 20703390 61 50-130
bis(2-Chloroethoxy)methane ug/kg 9651690 57 54-130
bis(2-Chloroethyl) ether ug/kg 9631690 57 48-130
bis(2-Ethylhexyl)phthalate ug/kg 12601690 75 45-134
Butylbenzylphthalate ug/kg 12801690 75 46-138
Chrysene ug/kg 13201690 78 58-130
Di-n-butylphthalate ug/kg 12101690 71 60-130
Di-n-octylphthalate ug/kg 14601690 86 53-130
Dibenz(a,h)anthracene ug/kg 12401690 73 59-130
Dibenzofuran ug/kg 10801690 64 60-130
Diethylphthalate ug/kg 11801690 70 60-130
Dimethylphthalate ug/kg 11501690 68 60-130
Fluoranthene ug/kg 12901690 76 65-130
Fluorene ug/kg 11501690 68 63-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2825073LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/kg 10201690 60 46-130
Hexachlorobenzene ug/kg 10801690 64 58-130
Hexachlorocyclopentadiene ug/kg 9691690 57 23-130
Hexachloroethane ug/kg 10001690 59 47-130
Indeno(1,2,3-cd)pyrene ug/kg 13401690 79 60-130
Isophorone ug/kg 10201690 60 49-130
N-Nitroso-di-n-propylamine ug/kg 9221690 54 47-130
N-Nitrosodimethylamine ug/kg 9481690 56 45-130
N-Nitrosodiphenylamine ug/kg 10901690 64 59-130
Naphthalene ug/kg 10601690 62 55-130
Nitrobenzene ug/kg 10001690 59 49-130
Pentachlorophenol ug/kg 21903390 64 10-132
Phenanthrene ug/kg 11901690 70 62-130
Phenol ug/kg 10101690 60 46-130
Pyrene ug/kg 12801690 76 53-130
Pyridine ug/kg 7811690 46 37-130
2,4,6-Tribromophenol (S)%73 27-110
2-Fluorobiphenyl (S)%58 30-110
2-Fluorophenol (S)%63 13-110
Nitrobenzene-d5 (S)%58 23-110
Phenol-d6 (S)%58 22-110
Terphenyl-d14 (S)%61 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92467796013
2825075SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92467796013
2825075SAMPLE DUPLICATE:
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND v130ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND v130ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND v230ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92467796013
2825075SAMPLE DUPLICATE:
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%0 S20
2-Fluorobiphenyl (S)%0 S20
2-Fluorophenol (S)%0 S20
Nitrobenzene-d5 (S)%0 D3,P3,S20
Phenol-d6 (S)%0 S20
Terphenyl-d14 (S)%0 S20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
528847
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92468257003, 92468257004, 92468257005, 92468257006, 92468257007, 92468257008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92468257003
2824793SAMPLE DUPLICATE:
Percent Moisture %19.2 3 2519.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1440575
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92468257001, 92468257002, 92468257003, 92468257004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3507452-1
Associated Lab Samples:92468257001, 92468257002, 92468257003, 92468257004
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 03/10/20 09:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3507452-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92468257001
R3507452-3SAMPLE DUPLICATE:
Total Solids %76.2 0.472 1076.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1440576
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92468257007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3507451-1
Associated Lab Samples:92468257007
Matrix:Solid
AnalyzedMDL
Total Solids %ND 03/10/20 09:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3507451-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1196290-01
R3507451-3SAMPLE DUPLICATE:
Total Solids %86.9 0.0459 1086.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468257
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1440286
3060A
EPA 7199
Wet Chemistry 7199
Associated Lab Samples:92468257001, 92468257002, 92468257003, 92468257004, 92468257007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3507545-1
Associated Lab Samples:92468257001, 92468257002, 92468257003, 92468257004, 92468257007
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 03/11/20 10:120.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3507545-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.6610.0 96.6 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3507545-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1196212-01
R3507545-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg R123.8 79.9 75.0-125103 23.1 2023.81.81 20.8 26.3
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3507545-5MATRIX SPIKE SAMPLE:
MSSpike
Result
L1196212-01
Chromium, Hexavalent mg/kg 10101060 94.7 75.0-1251.81
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1196212-02
R3507545-7SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND D8200200.388
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92468257007
R3507545-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92468257
BOU-014
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The sample and duplicate results for this parameter are less than 5 times the reporting limit, the RPD may not be
statistically valid.D8
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.P3
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.P6
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 52
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92468257
BOU-014
ANALYTE QUALIFIERS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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9800 Kincey Ave. Suite 100
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Page 48 of 52
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92468257
BOU-014
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92468257005 528947 529233SB-1A (2-3)EPA 3546 EPA 8082A
92468257001 1440109 1440109BG-1 3050B EPA 6020B
92468257002 1440109 1440109BG-2 3050B EPA 6020B
92468257003 1440109 1440109COMP-1 3050B EPA 6020B
92468257004 1440109 1440109COMP-2 3050B EPA 6020B
92468257007 1440109 1440109SGP-5 (2-4)3050B EPA 6020B
92468257001 1440077 1440077BG-1 7471A EPA 7471B
92468257002 1440077 1440077BG-2 7471A EPA 7471B
92468257003 1440077 1440077COMP-1 7471A EPA 7471B
92468257004 1440077 1440077COMP-2 7471A EPA 7471B
92468257007 1440077 1440077SGP-5 (2-4)7471A EPA 7471B
92468257003 528950 529221COMP-1 EPA 3546 EPA 8270E
92468257004 528950 529221COMP-2 EPA 3546 EPA 8270E
92468257007 528950 529221SGP-5 (2-4)EPA 3546 EPA 8270E
92468257005 528971 528976SB-1A (2-3)EPA 5035A EPA 8260D
92468257006 529261 529296SB-2A (2-3)EPA 5035A EPA 8260D
92468257007 528971 528976SGP-5 (2-4)EPA 5035A EPA 8260D
92468257008 528971 528976SB-DUP EPA 5035A EPA 8260D
92468257003 528847COMP-1 ASTM D2974-87
92468257004 528847COMP-2 ASTM D2974-87
92468257005 528847SB-1A (2-3)ASTM D2974-87
92468257006 528847SB-2A (2-3)ASTM D2974-87
92468257007 528847SGP-5 (2-4)ASTM D2974-87
92468257008 528847SB-DUP ASTM D2974-87
92468257001 1440575 1440575BG-1 SM 2540 G SM 2540G
92468257002 1440575 1440575BG-2 SM 2540 G SM 2540G
92468257003 1440575 1440575COMP-1 SM 2540 G SM 2540G
92468257004 1440575 1440575COMP-2 SM 2540 G SM 2540G
92468257007 1440576 1440576SGP-5 (2-4)SM 2540 G SM 2540G
92468257001 1440286 1440286BG-1 3060A EPA 7199
92468257002 1440286 1440286BG-2 3060A EPA 7199
92468257003 1440286 1440286COMP-1 3060A EPA 7199
92468257004 1440286 1440286COMP-2 3060A EPA 7199
92468257007 1440286 1440286SGP-5 (2-4)3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:26 PM
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Page 49 of 52
Page 50 of 52
Page 51 of 52
Page 52 of 52
#=CL#
March 12, 2020
LIMS USE: FR - RALPH MCGEE
LIMS OBJECT ID: 92468428
92468428
Project:
Pace Project No.:
RE:
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
BOU-014
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on March 05, 2020. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 49
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92468428
BOU-014
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
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DOD Certification: #1461.01
EPA# TN00003
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New Mexico DW Certification
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North Carolina Aquatic Toxicity Certification #: 41
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South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
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USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
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Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
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South Carolina Certification #: 99006001
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Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 49
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92468428
BOU-014
Lab ID Sample ID Matrix Date Collected Date Received
92468428001 TMW-1 Water 03/04/20 18:00 03/05/20 13:55
92468428002 TMW-2 Water 03/04/20 11:25 03/05/20 13:55
92468428003 TMW-3 Water 03/04/20 14:30 03/05/20 13:55
92468428004 TMW-4 Water 03/04/20 17:05 03/05/20 13:55
92468428005 TMW-DUP Water 03/04/20 00:00 03/05/20 13:55
92468428006 TB Water 03/04/20 00:00 03/05/20 13:55
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92468428
BOU-014
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92468428001 TMW-1 EPA 6020B 7 PANLD
EPA 7470A 1 PANSD
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CDLK
92468428002 TMW-2 EPA 6020B 7 PANLD
EPA 7470A 1 PANSD
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CDLK
92468428003 TMW-3 EPA 6020B 7 PANLD
EPA 7470A 1 PANSD
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CDLK
92468428004 TMW-4 EPA 6020B 7 PANLD
EPA 7470A 1 PANSD
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CDLK
92468428005 TMW-DUP EPA 6020B 7 PANLD
EPA 7470A 1 PANSD
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CDLK
92468428006 TB EPA 8260D 63 PASI-CDLK
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-1 Lab ID:92468428001 Collected:03/04/20 18:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic 0.646J ug/L 03/08/20 21:08 7440-38-2 J03/08/20 13:462.00 0.250 1
Barium 52.8 ug/L 03/08/20 21:08 7440-39-303/08/20 13:465.00 0.360 1
Cadmium ND ug/L 03/08/20 21:08 7440-43-903/08/20 13:461.00 0.160 1
Chromium 1.12J ug/L 03/08/20 21:08 7440-47-3 B,J03/08/20 13:462.00 0.540 1
Lead ND ug/L 03/08/20 21:08 7439-92-103/08/20 13:462.00 0.240 1
Selenium 0.410J ug/L 03/08/20 21:08 7782-49-2 J03/08/20 13:462.00 0.380 1
Silver ND ug/L 03/08/20 21:08 7440-22-403/08/20 13:462.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 03/09/20 13:26 7439-97-603/08/20 20:160.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 03/10/20 13:47 83-32-9 R103/09/20 17:0810.0 1.4 1
Acenaphthylene ND ug/L 03/10/20 13:47 208-96-8 R103/09/20 17:0810.0 1.5 1
Aniline ND ug/L 03/10/20 13:47 62-53-3 R103/09/20 17:0810.0 1.6 1
Anthracene ND ug/L 03/10/20 13:47 120-12-7 R103/09/20 17:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 03/10/20 13:47 56-55-303/09/20 17:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 03/10/20 13:47 50-32-803/09/20 17:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 03/10/20 13:47 205-99-203/09/20 17:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 03/10/20 13:47 191-24-203/09/20 17:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 03/10/20 13:47 207-08-903/09/20 17:0810.0 1.5 1
Benzoic Acid ND ug/L 03/10/20 13:47 65-85-003/09/20 17:0850.0 19.5 1
Benzyl alcohol ND ug/L 03/10/20 13:47 100-51-6 R103/09/20 17:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 03/10/20 13:47 101-55-3 R103/09/20 17:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 03/10/20 13:47 85-68-703/09/20 17:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 03/10/20 13:47 59-50-7 R103/09/20 17:0810.0 2.8 1
4-Chloroaniline ND ug/L 03/10/20 13:47 106-47-8 R103/09/20 17:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/20 13:47 111-91-1 M1,R103/09/20 17:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 03/10/20 13:47 111-44-4 R103/09/20 17:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 03/10/20 13:47 91-58-7 M1,R103/09/20 17:0810.0 1.4 1
2-Chlorophenol ND ug/L 03/10/20 13:47 95-57-8 R103/09/20 17:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 03/10/20 13:47 7005-72-3 R103/09/20 17:0810.0 1.5 1
Chrysene ND ug/L 03/10/20 13:47 218-01-903/09/20 17:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 03/10/20 13:47 53-70-303/09/20 17:0810.0 1.6 1
Dibenzofuran ND ug/L 03/10/20 13:47 132-64-9 M1,R103/09/20 17:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 03/10/20 13:47 95-50-1 R103/09/20 17:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 03/10/20 13:47 541-73-1 R103/09/20 17:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 03/10/20 13:47 106-46-7 R103/09/20 17:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 03/10/20 13:47 91-94-103/09/20 17:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 03/10/20 13:47 120-83-2 M1,R103/09/20 17:0810.0 1.5 1
Diethylphthalate ND ug/L 03/10/20 13:47 84-66-2 R103/09/20 17:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 03/10/20 13:47 105-67-9 M1,R103/09/20 17:0810.0 1.5 1
Dimethylphthalate ND ug/L 03/10/20 13:47 131-11-3 M1,R103/09/20 17:0810.0 1.4 1
Di-n-butylphthalate ND ug/L 03/10/20 13:47 84-74-203/09/20 17:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/20 13:47 534-52-103/09/20 17:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 03/10/20 13:47 51-28-5 R103/09/20 17:0850.0 7.3 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-1 Lab ID:92468428001 Collected:03/04/20 18:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 03/10/20 13:47 121-14-2 R103/09/20 17:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 03/10/20 13:47 606-20-2 M1,R103/09/20 17:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/20 13:47 117-84-003/09/20 17:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/20 13:47 117-81-703/09/20 17:086.0 2.0 1
Fluoranthene ND ug/L 03/10/20 13:47 206-44-003/09/20 17:0810.0 1.6 1
Fluorene ND ug/L 03/10/20 13:47 86-73-7 R103/09/20 17:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 03/10/20 13:47 87-68-3 R103/09/20 17:0810.0 1.6 1
Hexachlorobenzene ND ug/L 03/10/20 13:47 118-74-1 R103/09/20 17:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 03/10/20 13:47 77-47-4 R103/09/20 17:0810.0 2.4 1
Hexachloroethane ND ug/L 03/10/20 13:47 67-72-1 R103/09/20 17:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/20 13:47 193-39-503/09/20 17:0810.0 1.7 1
Isophorone ND ug/L 03/10/20 13:47 78-59-1 M1,R103/09/20 17:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 03/10/20 13:47 90-12-0 M1,R103/09/20 17:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 03/10/20 13:47 91-57-6 M1,R103/09/20 17:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/20 13:47 95-48-7 M1,R103/09/20 17:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/20 13:47 15831-10-4 R103/09/20 17:0810.0 1.2 1
Naphthalene ND ug/L 03/10/20 13:47 91-20-3 R103/09/20 17:0810.0 1.6 1
2-Nitroaniline ND ug/L 03/10/20 13:47 88-74-4 M1,R103/09/20 17:0820.0 3.0 1
3-Nitroaniline ND ug/L 03/10/20 13:47 99-09-2 R103/09/20 17:0820.0 2.8 1
4-Nitroaniline ND ug/L 03/10/20 13:47 100-01-603/09/20 17:0820.0 3.1 1
Nitrobenzene ND ug/L 03/10/20 13:47 98-95-3 R103/09/20 17:0810.0 1.5 1
2-Nitrophenol ND ug/L 03/10/20 13:47 88-75-5 R103/09/20 17:0810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/20 13:47 100-02-703/09/20 17:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 03/10/20 13:47 62-75-9 R103/09/20 17:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/20 13:47 621-64-7 M1,R103/09/20 17:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/10/20 13:47 86-30-6 R103/09/20 17:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/20 13:47 108-60-1 R103/09/20 17:0810.0 1.3 1
Pentachlorophenol ND ug/L 03/10/20 13:47 87-86-503/09/20 17:0820.0 2.8 1
Phenanthrene ND ug/L 03/10/20 13:47 85-01-8 R103/09/20 17:0810.0 1.4 1
Phenol ND ug/L 03/10/20 13:47 108-95-2 R103/09/20 17:0810.0 1.5 1
Pyrene ND ug/L 03/10/20 13:47 129-00-003/09/20 17:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 03/10/20 13:47 120-82-1 M1,R103/09/20 17:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 03/10/20 13:47 95-95-4 M1,R103/09/20 17:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 03/10/20 13:47 88-06-2 M1,R103/09/20 17:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)46 %03/10/20 13:47 4165-60-003/09/20 17:0813-130 1
2-Fluorobiphenyl (S)42 %03/10/20 13:47 321-60-803/09/20 17:0813-130 1
Terphenyl-d14 (S)76 %03/10/20 13:47 1718-51-003/09/20 17:0825-130 1
Phenol-d6 (S)28 %03/10/20 13:47 13127-88-303/09/20 17:0810-130 1
2-Fluorophenol (S)38 %03/10/20 13:47 367-12-403/09/20 17:0810-130 1
2,4,6-Tribromophenol (S)51 %03/10/20 13:47 118-79-603/09/20 17:0810-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 03/09/20 16:48 67-64-1 v125.0 6.2 1
Benzene ND ug/L 03/09/20 16:48 71-43-21.0 0.15 1
Bromobenzene ND ug/L 03/09/20 16:48 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 6 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-1 Lab ID:92468428001 Collected:03/04/20 18:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 03/09/20 16:48 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 03/09/20 16:48 75-27-41.0 0.26 1
Bromoform ND ug/L 03/09/20 16:48 75-25-21.0 0.62 1
Bromomethane ND ug/L 03/09/20 16:48 74-83-9 IH,IK2.0 0.62 1
2-Butanone (MEK)ND ug/L 03/09/20 16:48 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 03/09/20 16:48 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 03/09/20 16:48 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/09/20 16:48 75-00-3 IK1.0 0.49 1
Chloroform ND ug/L 03/09/20 16:48 67-66-35.0 2.3 1
Chloromethane ND ug/L 03/09/20 16:48 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 03/09/20 16:48 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 03/09/20 16:48 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 03/09/20 16:48 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 03/09/20 16:48 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 03/09/20 16:48 106-93-41.0 0.26 1
Dibromomethane ND ug/L 03/09/20 16:48 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 03/09/20 16:48 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 03/09/20 16:48 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 03/09/20 16:48 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 03/09/20 16:48 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 03/09/20 16:48 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 03/09/20 16:48 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 03/09/20 16:48 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 03/09/20 16:48 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 03/09/20 16:48 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 03/09/20 16:48 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 03/09/20 16:48 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 03/09/20 16:48 594-20-7 IK,L1,v11.0 0.27 1
1,1-Dichloropropene ND ug/L 03/09/20 16:48 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 03/09/20 16:48 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 03/09/20 16:48 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 03/09/20 16:48 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 03/09/20 16:48 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 03/09/20 16:48 87-68-31.0 0.44 1
2-Hexanone ND ug/L 03/09/20 16:48 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 03/09/20 16:48 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 03/09/20 16:48 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/20 16:48 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 03/09/20 16:48 1634-04-41.0 0.28 1
Naphthalene ND ug/L 03/09/20 16:48 91-20-31.0 0.35 1
Styrene ND ug/L 03/09/20 16:48 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 03/09/20 16:48 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 03/09/20 16:48 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 03/09/20 16:48 127-18-41.0 0.16 1
Toluene ND ug/L 03/09/20 16:48 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/09/20 16:48 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-1 Lab ID:92468428001 Collected:03/04/20 18:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 03/09/20 16:48 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 03/09/20 16:48 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 03/09/20 16:48 79-00-51.0 0.24 1
Trichloroethene ND ug/L 03/09/20 16:48 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 03/09/20 16:48 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 03/09/20 16:48 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 03/09/20 16:48 108-05-4 v12.0 1.4 1
Vinyl chloride ND ug/L 03/09/20 16:48 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 03/09/20 16:48 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 03/09/20 16:48 179601-23-12.0 0.41 1
o-Xylene ND ug/L 03/09/20 16:48 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)97 %03/09/20 16:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %03/09/20 16:48 17060-07-070-130 1
Toluene-d8 (S)105 %03/09/20 16:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-2 Lab ID:92468428002 Collected:03/04/20 11:25 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic ND ug/L 03/08/20 21:18 7440-38-203/08/20 13:462.00 0.250 1
Barium 94.0 ug/L 03/08/20 21:18 7440-39-303/08/20 13:465.00 0.360 1
Cadmium 0.173J ug/L 03/08/20 21:18 7440-43-9 J03/08/20 13:461.00 0.160 1
Chromium 0.861J ug/L 03/08/20 21:18 7440-47-3 B,J03/08/20 13:462.00 0.540 1
Lead ND ug/L 03/08/20 21:18 7439-92-103/08/20 13:462.00 0.240 1
Selenium 0.393J ug/L 03/08/20 21:18 7782-49-2 J03/08/20 13:462.00 0.380 1
Silver ND ug/L 03/08/20 21:18 7440-22-403/08/20 13:462.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 03/09/20 13:28 7439-97-603/08/20 20:160.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 03/10/20 15:04 83-32-903/09/20 17:0810.0 1.4 1
Acenaphthylene ND ug/L 03/10/20 15:04 208-96-803/09/20 17:0810.0 1.5 1
Aniline ND ug/L 03/10/20 15:04 62-53-303/09/20 17:0810.0 1.6 1
Anthracene ND ug/L 03/10/20 15:04 120-12-703/09/20 17:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 03/10/20 15:04 56-55-303/09/20 17:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 03/10/20 15:04 50-32-803/09/20 17:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 03/10/20 15:04 205-99-203/09/20 17:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 03/10/20 15:04 191-24-203/09/20 17:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 03/10/20 15:04 207-08-903/09/20 17:0810.0 1.5 1
Benzoic Acid ND ug/L 03/10/20 15:04 65-85-003/09/20 17:0850.0 19.5 1
Benzyl alcohol ND ug/L 03/10/20 15:04 100-51-603/09/20 17:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 03/10/20 15:04 101-55-303/09/20 17:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 03/10/20 15:04 85-68-703/09/20 17:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 03/10/20 15:04 59-50-703/09/20 17:0810.0 2.8 1
4-Chloroaniline ND ug/L 03/10/20 15:04 106-47-803/09/20 17:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/20 15:04 111-91-103/09/20 17:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 03/10/20 15:04 111-44-403/09/20 17:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 03/10/20 15:04 91-58-703/09/20 17:0810.0 1.4 1
2-Chlorophenol ND ug/L 03/10/20 15:04 95-57-803/09/20 17:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 03/10/20 15:04 7005-72-303/09/20 17:0810.0 1.5 1
Chrysene ND ug/L 03/10/20 15:04 218-01-903/09/20 17:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 03/10/20 15:04 53-70-303/09/20 17:0810.0 1.6 1
Dibenzofuran ND ug/L 03/10/20 15:04 132-64-903/09/20 17:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 03/10/20 15:04 95-50-103/09/20 17:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 03/10/20 15:04 541-73-103/09/20 17:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 03/10/20 15:04 106-46-703/09/20 17:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 03/10/20 15:04 91-94-103/09/20 17:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 03/10/20 15:04 120-83-203/09/20 17:0810.0 1.5 1
Diethylphthalate ND ug/L 03/10/20 15:04 84-66-203/09/20 17:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 03/10/20 15:04 105-67-903/09/20 17:0810.0 1.5 1
Dimethylphthalate ND ug/L 03/10/20 15:04 131-11-303/09/20 17:0810.0 1.4 1
Di-n-butylphthalate ND ug/L 03/10/20 15:04 84-74-203/09/20 17:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/20 15:04 534-52-103/09/20 17:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 03/10/20 15:04 51-28-503/09/20 17:0850.0 7.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-2 Lab ID:92468428002 Collected:03/04/20 11:25 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 03/10/20 15:04 121-14-203/09/20 17:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 03/10/20 15:04 606-20-203/09/20 17:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/20 15:04 117-84-003/09/20 17:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/20 15:04 117-81-703/09/20 17:086.0 2.0 1
Fluoranthene ND ug/L 03/10/20 15:04 206-44-003/09/20 17:0810.0 1.6 1
Fluorene ND ug/L 03/10/20 15:04 86-73-703/09/20 17:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 03/10/20 15:04 87-68-303/09/20 17:0810.0 1.6 1
Hexachlorobenzene ND ug/L 03/10/20 15:04 118-74-103/09/20 17:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 03/10/20 15:04 77-47-403/09/20 17:0810.0 2.4 1
Hexachloroethane ND ug/L 03/10/20 15:04 67-72-103/09/20 17:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/20 15:04 193-39-503/09/20 17:0810.0 1.7 1
Isophorone ND ug/L 03/10/20 15:04 78-59-103/09/20 17:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 03/10/20 15:04 90-12-003/09/20 17:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 03/10/20 15:04 91-57-603/09/20 17:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/20 15:04 95-48-703/09/20 17:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/20 15:04 15831-10-403/09/20 17:0810.0 1.2 1
Naphthalene ND ug/L 03/10/20 15:04 91-20-303/09/20 17:0810.0 1.6 1
2-Nitroaniline ND ug/L 03/10/20 15:04 88-74-403/09/20 17:0820.0 3.0 1
3-Nitroaniline ND ug/L 03/10/20 15:04 99-09-203/09/20 17:0820.0 2.8 1
4-Nitroaniline ND ug/L 03/10/20 15:04 100-01-603/09/20 17:0820.0 3.1 1
Nitrobenzene ND ug/L 03/10/20 15:04 98-95-303/09/20 17:0810.0 1.5 1
2-Nitrophenol ND ug/L 03/10/20 15:04 88-75-503/09/20 17:0810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/20 15:04 100-02-703/09/20 17:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 03/10/20 15:04 62-75-903/09/20 17:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/20 15:04 621-64-703/09/20 17:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/10/20 15:04 86-30-603/09/20 17:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/20 15:04 108-60-103/09/20 17:0810.0 1.3 1
Pentachlorophenol ND ug/L 03/10/20 15:04 87-86-503/09/20 17:0820.0 2.8 1
Phenanthrene ND ug/L 03/10/20 15:04 85-01-803/09/20 17:0810.0 1.4 1
Phenol ND ug/L 03/10/20 15:04 108-95-203/09/20 17:0810.0 1.5 1
Pyrene ND ug/L 03/10/20 15:04 129-00-003/09/20 17:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 03/10/20 15:04 120-82-103/09/20 17:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 03/10/20 15:04 95-95-403/09/20 17:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 03/10/20 15:04 88-06-203/09/20 17:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)54 %03/10/20 15:04 4165-60-003/09/20 17:0813-130 1
2-Fluorobiphenyl (S)48 %03/10/20 15:04 321-60-803/09/20 17:0813-130 1
Terphenyl-d14 (S)79 %03/10/20 15:04 1718-51-003/09/20 17:0825-130 1
Phenol-d6 (S)28 %03/10/20 15:04 13127-88-303/09/20 17:0810-130 1
2-Fluorophenol (S)39 %03/10/20 15:04 367-12-403/09/20 17:0810-130 1
2,4,6-Tribromophenol (S)64 %03/10/20 15:04 118-79-603/09/20 17:0810-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 03/09/20 17:07 67-64-1 v125.0 6.2 1
Benzene ND ug/L 03/09/20 17:07 71-43-21.0 0.15 1
Bromobenzene ND ug/L 03/09/20 17:07 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-2 Lab ID:92468428002 Collected:03/04/20 11:25 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 03/09/20 17:07 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 03/09/20 17:07 75-27-41.0 0.26 1
Bromoform ND ug/L 03/09/20 17:07 75-25-21.0 0.62 1
Bromomethane ND ug/L 03/09/20 17:07 74-83-9 IH,IK2.0 0.62 1
2-Butanone (MEK)ND ug/L 03/09/20 17:07 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 03/09/20 17:07 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 03/09/20 17:07 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/09/20 17:07 75-00-3 IK1.0 0.49 1
Chloroform ND ug/L 03/09/20 17:07 67-66-35.0 2.3 1
Chloromethane ND ug/L 03/09/20 17:07 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 03/09/20 17:07 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 03/09/20 17:07 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 03/09/20 17:07 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 03/09/20 17:07 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 03/09/20 17:07 106-93-41.0 0.26 1
Dibromomethane ND ug/L 03/09/20 17:07 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 03/09/20 17:07 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 03/09/20 17:07 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 03/09/20 17:07 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 03/09/20 17:07 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 03/09/20 17:07 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 03/09/20 17:07 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 03/09/20 17:07 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 03/09/20 17:07 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 03/09/20 17:07 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 03/09/20 17:07 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 03/09/20 17:07 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 03/09/20 17:07 594-20-7 IK,L1,v11.0 0.27 1
1,1-Dichloropropene ND ug/L 03/09/20 17:07 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 03/09/20 17:07 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 03/09/20 17:07 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 03/09/20 17:07 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 03/09/20 17:07 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 03/09/20 17:07 87-68-31.0 0.44 1
2-Hexanone ND ug/L 03/09/20 17:07 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 03/09/20 17:07 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 03/09/20 17:07 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/20 17:07 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 03/09/20 17:07 1634-04-41.0 0.28 1
Naphthalene ND ug/L 03/09/20 17:07 91-20-31.0 0.35 1
Styrene ND ug/L 03/09/20 17:07 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 03/09/20 17:07 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 03/09/20 17:07 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 03/09/20 17:07 127-18-41.0 0.16 1
Toluene 0.28J ug/L 03/09/20 17:07 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/09/20 17:07 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-2 Lab ID:92468428002 Collected:03/04/20 11:25 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 03/09/20 17:07 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 03/09/20 17:07 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 03/09/20 17:07 79-00-51.0 0.24 1
Trichloroethene ND ug/L 03/09/20 17:07 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 03/09/20 17:07 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 03/09/20 17:07 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 03/09/20 17:07 108-05-4 v12.0 1.4 1
Vinyl chloride ND ug/L 03/09/20 17:07 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 03/09/20 17:07 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 03/09/20 17:07 179601-23-12.0 0.41 1
o-Xylene ND ug/L 03/09/20 17:07 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %03/09/20 17:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %03/09/20 17:07 17060-07-070-130 1
Toluene-d8 (S)102 %03/09/20 17:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
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Page 12 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-3 Lab ID:92468428003 Collected:03/04/20 14:30 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic 0.317J ug/L 03/08/20 21:22 7440-38-2 J03/08/20 13:462.00 0.250 1
Barium 29.1 ug/L 03/08/20 21:22 7440-39-303/08/20 13:465.00 0.360 1
Cadmium ND ug/L 03/08/20 21:22 7440-43-903/08/20 13:461.00 0.160 1
Chromium 2.32 ug/L 03/08/20 21:22 7440-47-3 B03/08/20 13:462.00 0.540 1
Lead ND ug/L 03/08/20 21:22 7439-92-103/08/20 13:462.00 0.240 1
Selenium ND ug/L 03/08/20 21:22 7782-49-203/08/20 13:462.00 0.380 1
Silver ND ug/L 03/08/20 21:22 7440-22-403/08/20 13:462.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 03/09/20 13:30 7439-97-603/08/20 20:160.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 03/10/20 15:30 83-32-903/09/20 17:0810.0 1.4 1
Acenaphthylene ND ug/L 03/10/20 15:30 208-96-803/09/20 17:0810.0 1.5 1
Aniline ND ug/L 03/10/20 15:30 62-53-303/09/20 17:0810.0 1.6 1
Anthracene ND ug/L 03/10/20 15:30 120-12-703/09/20 17:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 03/10/20 15:30 56-55-303/09/20 17:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 03/10/20 15:30 50-32-803/09/20 17:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 03/10/20 15:30 205-99-203/09/20 17:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 03/10/20 15:30 191-24-203/09/20 17:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 03/10/20 15:30 207-08-903/09/20 17:0810.0 1.5 1
Benzoic Acid ND ug/L 03/10/20 15:30 65-85-003/09/20 17:0850.0 19.5 1
Benzyl alcohol ND ug/L 03/10/20 15:30 100-51-603/09/20 17:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 03/10/20 15:30 101-55-303/09/20 17:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 03/10/20 15:30 85-68-703/09/20 17:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 03/10/20 15:30 59-50-703/09/20 17:0810.0 2.8 1
4-Chloroaniline ND ug/L 03/10/20 15:30 106-47-803/09/20 17:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/20 15:30 111-91-103/09/20 17:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 03/10/20 15:30 111-44-403/09/20 17:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 03/10/20 15:30 91-58-703/09/20 17:0810.0 1.4 1
2-Chlorophenol ND ug/L 03/10/20 15:30 95-57-803/09/20 17:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 03/10/20 15:30 7005-72-303/09/20 17:0810.0 1.5 1
Chrysene ND ug/L 03/10/20 15:30 218-01-903/09/20 17:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 03/10/20 15:30 53-70-303/09/20 17:0810.0 1.6 1
Dibenzofuran ND ug/L 03/10/20 15:30 132-64-903/09/20 17:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 03/10/20 15:30 95-50-103/09/20 17:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 03/10/20 15:30 541-73-103/09/20 17:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 03/10/20 15:30 106-46-703/09/20 17:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 03/10/20 15:30 91-94-103/09/20 17:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 03/10/20 15:30 120-83-203/09/20 17:0810.0 1.5 1
Diethylphthalate ND ug/L 03/10/20 15:30 84-66-203/09/20 17:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 03/10/20 15:30 105-67-903/09/20 17:0810.0 1.5 1
Dimethylphthalate ND ug/L 03/10/20 15:30 131-11-303/09/20 17:0810.0 1.4 1
Di-n-butylphthalate ND ug/L 03/10/20 15:30 84-74-203/09/20 17:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/20 15:30 534-52-103/09/20 17:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 03/10/20 15:30 51-28-503/09/20 17:0850.0 7.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-3 Lab ID:92468428003 Collected:03/04/20 14:30 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 03/10/20 15:30 121-14-203/09/20 17:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 03/10/20 15:30 606-20-203/09/20 17:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/20 15:30 117-84-003/09/20 17:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/20 15:30 117-81-703/09/20 17:086.0 2.0 1
Fluoranthene ND ug/L 03/10/20 15:30 206-44-003/09/20 17:0810.0 1.6 1
Fluorene ND ug/L 03/10/20 15:30 86-73-703/09/20 17:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 03/10/20 15:30 87-68-303/09/20 17:0810.0 1.6 1
Hexachlorobenzene ND ug/L 03/10/20 15:30 118-74-103/09/20 17:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 03/10/20 15:30 77-47-403/09/20 17:0810.0 2.4 1
Hexachloroethane ND ug/L 03/10/20 15:30 67-72-103/09/20 17:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/20 15:30 193-39-503/09/20 17:0810.0 1.7 1
Isophorone ND ug/L 03/10/20 15:30 78-59-103/09/20 17:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 03/10/20 15:30 90-12-003/09/20 17:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 03/10/20 15:30 91-57-603/09/20 17:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/20 15:30 95-48-703/09/20 17:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/20 15:30 15831-10-403/09/20 17:0810.0 1.2 1
Naphthalene ND ug/L 03/10/20 15:30 91-20-303/09/20 17:0810.0 1.6 1
2-Nitroaniline ND ug/L 03/10/20 15:30 88-74-403/09/20 17:0820.0 3.0 1
3-Nitroaniline ND ug/L 03/10/20 15:30 99-09-203/09/20 17:0820.0 2.8 1
4-Nitroaniline ND ug/L 03/10/20 15:30 100-01-603/09/20 17:0820.0 3.1 1
Nitrobenzene ND ug/L 03/10/20 15:30 98-95-303/09/20 17:0810.0 1.5 1
2-Nitrophenol ND ug/L 03/10/20 15:30 88-75-503/09/20 17:0810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/20 15:30 100-02-703/09/20 17:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 03/10/20 15:30 62-75-903/09/20 17:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/20 15:30 621-64-703/09/20 17:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/10/20 15:30 86-30-603/09/20 17:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/20 15:30 108-60-103/09/20 17:0810.0 1.3 1
Pentachlorophenol ND ug/L 03/10/20 15:30 87-86-503/09/20 17:0820.0 2.8 1
Phenanthrene ND ug/L 03/10/20 15:30 85-01-803/09/20 17:0810.0 1.4 1
Phenol ND ug/L 03/10/20 15:30 108-95-203/09/20 17:0810.0 1.5 1
Pyrene ND ug/L 03/10/20 15:30 129-00-003/09/20 17:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 03/10/20 15:30 120-82-103/09/20 17:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 03/10/20 15:30 95-95-403/09/20 17:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 03/10/20 15:30 88-06-203/09/20 17:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)49 %03/10/20 15:30 4165-60-003/09/20 17:0813-130 1
2-Fluorobiphenyl (S)45 %03/10/20 15:30 321-60-803/09/20 17:0813-130 1
Terphenyl-d14 (S)72 %03/10/20 15:30 1718-51-003/09/20 17:0825-130 1
Phenol-d6 (S)27 %03/10/20 15:30 13127-88-303/09/20 17:0810-130 1
2-Fluorophenol (S)38 %03/10/20 15:30 367-12-403/09/20 17:0810-130 1
2,4,6-Tribromophenol (S)63 %03/10/20 15:30 118-79-603/09/20 17:0810-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 03/09/20 17:25 67-64-1 v125.0 6.2 1
Benzene ND ug/L 03/09/20 17:25 71-43-21.0 0.15 1
Bromobenzene ND ug/L 03/09/20 17:25 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-3 Lab ID:92468428003 Collected:03/04/20 14:30 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 03/09/20 17:25 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 03/09/20 17:25 75-27-41.0 0.26 1
Bromoform ND ug/L 03/09/20 17:25 75-25-21.0 0.62 1
Bromomethane ND ug/L 03/09/20 17:25 74-83-9 IH,IK2.0 0.62 1
2-Butanone (MEK)ND ug/L 03/09/20 17:25 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 03/09/20 17:25 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 03/09/20 17:25 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/09/20 17:25 75-00-3 IK1.0 0.49 1
Chloroform ND ug/L 03/09/20 17:25 67-66-35.0 2.3 1
Chloromethane ND ug/L 03/09/20 17:25 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 03/09/20 17:25 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 03/09/20 17:25 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 03/09/20 17:25 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 03/09/20 17:25 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 03/09/20 17:25 106-93-41.0 0.26 1
Dibromomethane ND ug/L 03/09/20 17:25 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 03/09/20 17:25 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 03/09/20 17:25 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 03/09/20 17:25 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 03/09/20 17:25 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 03/09/20 17:25 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 03/09/20 17:25 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 03/09/20 17:25 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 03/09/20 17:25 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 03/09/20 17:25 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 03/09/20 17:25 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 03/09/20 17:25 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 03/09/20 17:25 594-20-7 IK,L1,v11.0 0.27 1
1,1-Dichloropropene ND ug/L 03/09/20 17:25 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 03/09/20 17:25 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 03/09/20 17:25 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 03/09/20 17:25 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 03/09/20 17:25 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 03/09/20 17:25 87-68-31.0 0.44 1
2-Hexanone ND ug/L 03/09/20 17:25 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 03/09/20 17:25 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 03/09/20 17:25 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/20 17:25 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 03/09/20 17:25 1634-04-41.0 0.28 1
Naphthalene ND ug/L 03/09/20 17:25 91-20-31.0 0.35 1
Styrene ND ug/L 03/09/20 17:25 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 03/09/20 17:25 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 03/09/20 17:25 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 03/09/20 17:25 127-18-41.0 0.16 1
Toluene 1.7 ug/L 03/09/20 17:25 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/09/20 17:25 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-3 Lab ID:92468428003 Collected:03/04/20 14:30 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 03/09/20 17:25 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 03/09/20 17:25 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 03/09/20 17:25 79-00-51.0 0.24 1
Trichloroethene ND ug/L 03/09/20 17:25 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 03/09/20 17:25 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 03/09/20 17:25 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 03/09/20 17:25 108-05-4 v12.0 1.4 1
Vinyl chloride ND ug/L 03/09/20 17:25 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 03/09/20 17:25 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 03/09/20 17:25 179601-23-12.0 0.41 1
o-Xylene ND ug/L 03/09/20 17:25 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %03/09/20 17:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %03/09/20 17:25 17060-07-070-130 1
Toluene-d8 (S)106 %03/09/20 17:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-4 Lab ID:92468428004 Collected:03/04/20 17:05 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic ND ug/L 03/08/20 21:25 7440-38-203/08/20 13:462.00 0.250 1
Barium 11.5 ug/L 03/08/20 21:25 7440-39-303/08/20 13:465.00 0.360 1
Cadmium ND ug/L 03/08/20 21:25 7440-43-903/08/20 13:461.00 0.160 1
Chromium 0.635J ug/L 03/08/20 21:25 7440-47-3 B,J03/08/20 13:462.00 0.540 1
Lead ND ug/L 03/08/20 21:25 7439-92-103/08/20 13:462.00 0.240 1
Selenium ND ug/L 03/08/20 21:25 7782-49-203/08/20 13:462.00 0.380 1
Silver ND ug/L 03/08/20 21:25 7440-22-403/08/20 13:462.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 03/09/20 13:32 7439-97-603/08/20 20:160.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 03/10/20 15:55 83-32-903/09/20 17:0810.0 1.4 1
Acenaphthylene ND ug/L 03/10/20 15:55 208-96-803/09/20 17:0810.0 1.5 1
Aniline ND ug/L 03/10/20 15:55 62-53-303/09/20 17:0810.0 1.6 1
Anthracene ND ug/L 03/10/20 15:55 120-12-703/09/20 17:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 03/10/20 15:55 56-55-303/09/20 17:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 03/10/20 15:55 50-32-803/09/20 17:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 03/10/20 15:55 205-99-203/09/20 17:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 03/10/20 15:55 191-24-203/09/20 17:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 03/10/20 15:55 207-08-903/09/20 17:0810.0 1.5 1
Benzoic Acid ND ug/L 03/10/20 15:55 65-85-003/09/20 17:0850.0 19.5 1
Benzyl alcohol ND ug/L 03/10/20 15:55 100-51-603/09/20 17:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 03/10/20 15:55 101-55-303/09/20 17:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 03/10/20 15:55 85-68-703/09/20 17:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 03/10/20 15:55 59-50-703/09/20 17:0810.0 2.8 1
4-Chloroaniline ND ug/L 03/10/20 15:55 106-47-803/09/20 17:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/20 15:55 111-91-103/09/20 17:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 03/10/20 15:55 111-44-403/09/20 17:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 03/10/20 15:55 91-58-703/09/20 17:0810.0 1.4 1
2-Chlorophenol ND ug/L 03/10/20 15:55 95-57-803/09/20 17:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 03/10/20 15:55 7005-72-303/09/20 17:0810.0 1.5 1
Chrysene ND ug/L 03/10/20 15:55 218-01-903/09/20 17:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 03/10/20 15:55 53-70-303/09/20 17:0810.0 1.6 1
Dibenzofuran ND ug/L 03/10/20 15:55 132-64-903/09/20 17:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 03/10/20 15:55 95-50-103/09/20 17:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 03/10/20 15:55 541-73-103/09/20 17:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 03/10/20 15:55 106-46-703/09/20 17:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 03/10/20 15:55 91-94-103/09/20 17:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 03/10/20 15:55 120-83-203/09/20 17:0810.0 1.5 1
Diethylphthalate ND ug/L 03/10/20 15:55 84-66-203/09/20 17:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 03/10/20 15:55 105-67-903/09/20 17:0810.0 1.5 1
Dimethylphthalate ND ug/L 03/10/20 15:55 131-11-303/09/20 17:0810.0 1.4 1
Di-n-butylphthalate ND ug/L 03/10/20 15:55 84-74-203/09/20 17:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/20 15:55 534-52-103/09/20 17:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 03/10/20 15:55 51-28-503/09/20 17:0850.0 7.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
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Page 17 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-4 Lab ID:92468428004 Collected:03/04/20 17:05 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 03/10/20 15:55 121-14-203/09/20 17:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 03/10/20 15:55 606-20-203/09/20 17:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/20 15:55 117-84-003/09/20 17:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/20 15:55 117-81-703/09/20 17:086.0 2.0 1
Fluoranthene ND ug/L 03/10/20 15:55 206-44-003/09/20 17:0810.0 1.6 1
Fluorene ND ug/L 03/10/20 15:55 86-73-703/09/20 17:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 03/10/20 15:55 87-68-303/09/20 17:0810.0 1.6 1
Hexachlorobenzene ND ug/L 03/10/20 15:55 118-74-103/09/20 17:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 03/10/20 15:55 77-47-403/09/20 17:0810.0 2.4 1
Hexachloroethane ND ug/L 03/10/20 15:55 67-72-103/09/20 17:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/20 15:55 193-39-503/09/20 17:0810.0 1.7 1
Isophorone ND ug/L 03/10/20 15:55 78-59-103/09/20 17:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 03/10/20 15:55 90-12-003/09/20 17:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 03/10/20 15:55 91-57-603/09/20 17:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/20 15:55 95-48-703/09/20 17:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/20 15:55 15831-10-403/09/20 17:0810.0 1.2 1
Naphthalene ND ug/L 03/10/20 15:55 91-20-303/09/20 17:0810.0 1.6 1
2-Nitroaniline ND ug/L 03/10/20 15:55 88-74-403/09/20 17:0820.0 3.0 1
3-Nitroaniline ND ug/L 03/10/20 15:55 99-09-203/09/20 17:0820.0 2.8 1
4-Nitroaniline ND ug/L 03/10/20 15:55 100-01-603/09/20 17:0820.0 3.1 1
Nitrobenzene ND ug/L 03/10/20 15:55 98-95-303/09/20 17:0810.0 1.5 1
2-Nitrophenol ND ug/L 03/10/20 15:55 88-75-503/09/20 17:0810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/20 15:55 100-02-703/09/20 17:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 03/10/20 15:55 62-75-903/09/20 17:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/20 15:55 621-64-703/09/20 17:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/10/20 15:55 86-30-603/09/20 17:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/20 15:55 108-60-103/09/20 17:0810.0 1.3 1
Pentachlorophenol ND ug/L 03/10/20 15:55 87-86-503/09/20 17:0820.0 2.8 1
Phenanthrene ND ug/L 03/10/20 15:55 85-01-803/09/20 17:0810.0 1.4 1
Phenol ND ug/L 03/10/20 15:55 108-95-203/09/20 17:0810.0 1.5 1
Pyrene ND ug/L 03/10/20 15:55 129-00-003/09/20 17:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 03/10/20 15:55 120-82-103/09/20 17:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 03/10/20 15:55 95-95-403/09/20 17:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 03/10/20 15:55 88-06-203/09/20 17:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)47 %03/10/20 15:55 4165-60-003/09/20 17:0813-130 1
2-Fluorobiphenyl (S)42 %03/10/20 15:55 321-60-803/09/20 17:0813-130 1
Terphenyl-d14 (S)69 %03/10/20 15:55 1718-51-003/09/20 17:0825-130 1
Phenol-d6 (S)27 %03/10/20 15:55 13127-88-303/09/20 17:0810-130 1
2-Fluorophenol (S)37 %03/10/20 15:55 367-12-403/09/20 17:0810-130 1
2,4,6-Tribromophenol (S)50 %03/10/20 15:55 118-79-603/09/20 17:0810-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 03/12/20 14:07 67-64-125.0 6.2 1
Benzene ND ug/L 03/12/20 14:07 71-43-21.0 0.15 1
Bromobenzene ND ug/L 03/12/20 14:07 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
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Huntersville, NC 28078
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Page 18 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-4 Lab ID:92468428004 Collected:03/04/20 17:05 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 03/12/20 14:07 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 03/12/20 14:07 75-27-41.0 0.26 1
Bromoform ND ug/L 03/12/20 14:07 75-25-21.0 0.62 1
Bromomethane ND ug/L 03/12/20 14:07 74-83-9 IH,L12.0 0.62 1
2-Butanone (MEK)ND ug/L 03/12/20 14:07 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 03/12/20 14:07 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 03/12/20 14:07 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/12/20 14:07 75-00-3 v11.0 0.49 1
Chloroform ND ug/L 03/12/20 14:07 67-66-35.0 2.3 1
Chloromethane ND ug/L 03/12/20 14:07 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 03/12/20 14:07 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 03/12/20 14:07 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 03/12/20 14:07 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 03/12/20 14:07 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 03/12/20 14:07 106-93-41.0 0.26 1
Dibromomethane ND ug/L 03/12/20 14:07 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 03/12/20 14:07 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 03/12/20 14:07 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 03/12/20 14:07 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 03/12/20 14:07 75-71-8 IH,v11.0 0.23 1
1,1-Dichloroethane ND ug/L 03/12/20 14:07 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 03/12/20 14:07 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 03/12/20 14:07 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 03/12/20 14:07 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 03/12/20 14:07 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 03/12/20 14:07 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 03/12/20 14:07 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 03/12/20 14:07 594-20-7 L1,v11.0 0.27 1
1,1-Dichloropropene ND ug/L 03/12/20 14:07 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 03/12/20 14:07 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 03/12/20 14:07 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 03/12/20 14:07 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 03/12/20 14:07 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 03/12/20 14:07 87-68-31.0 0.44 1
2-Hexanone ND ug/L 03/12/20 14:07 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 03/12/20 14:07 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 03/12/20 14:07 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/12/20 14:07 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 03/12/20 14:07 1634-04-41.0 0.28 1
Naphthalene ND ug/L 03/12/20 14:07 91-20-31.0 0.35 1
Styrene ND ug/L 03/12/20 14:07 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 03/12/20 14:07 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 03/12/20 14:07 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 03/12/20 14:07 127-18-41.0 0.16 1
Toluene ND ug/L 03/12/20 14:07 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/12/20 14:07 87-61-6 L11.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-4 Lab ID:92468428004 Collected:03/04/20 17:05 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 03/12/20 14:07 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 03/12/20 14:07 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 03/12/20 14:07 79-00-51.0 0.24 1
Trichloroethene ND ug/L 03/12/20 14:07 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 03/12/20 14:07 75-69-4 v11.0 0.31 1
1,2,3-Trichloropropane ND ug/L 03/12/20 14:07 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 03/12/20 14:07 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 03/12/20 14:07 75-01-4 IH,v11.0 0.24 1
Xylene (Total)ND ug/L 03/12/20 14:07 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 03/12/20 14:07 179601-23-12.0 0.41 1
o-Xylene ND ug/L 03/12/20 14:07 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)95 %03/12/20 14:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %03/12/20 14:07 17060-07-070-130 1
Toluene-d8 (S)102 %03/12/20 14:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 20 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-DUP Lab ID:92468428005 Collected:03/04/20 00:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic ND ug/L 03/08/20 21:28 7440-38-203/08/20 13:462.00 0.250 1
Barium 53.4 ug/L 03/08/20 21:28 7440-39-303/08/20 13:465.00 0.360 1
Cadmium ND ug/L 03/08/20 21:28 7440-43-903/08/20 13:461.00 0.160 1
Chromium 1.12J ug/L 03/08/20 21:28 7440-47-3 B,J03/08/20 13:462.00 0.540 1
Lead ND ug/L 03/08/20 21:28 7439-92-103/08/20 13:462.00 0.240 1
Selenium ND ug/L 03/08/20 21:28 7782-49-203/08/20 13:462.00 0.380 1
Silver ND ug/L 03/08/20 21:28 7440-22-403/08/20 13:462.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 03/09/20 13:34 7439-97-603/08/20 20:160.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 03/10/20 16:21 83-32-903/09/20 17:0810.0 1.4 1
Acenaphthylene ND ug/L 03/10/20 16:21 208-96-803/09/20 17:0810.0 1.5 1
Aniline ND ug/L 03/10/20 16:21 62-53-303/09/20 17:0810.0 1.6 1
Anthracene ND ug/L 03/10/20 16:21 120-12-703/09/20 17:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 03/10/20 16:21 56-55-303/09/20 17:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 03/10/20 16:21 50-32-803/09/20 17:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 03/10/20 16:21 205-99-203/09/20 17:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 03/10/20 16:21 191-24-203/09/20 17:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 03/10/20 16:21 207-08-903/09/20 17:0810.0 1.5 1
Benzoic Acid ND ug/L 03/10/20 16:21 65-85-003/09/20 17:0850.0 19.5 1
Benzyl alcohol ND ug/L 03/10/20 16:21 100-51-603/09/20 17:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 03/10/20 16:21 101-55-303/09/20 17:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 03/10/20 16:21 85-68-703/09/20 17:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 03/10/20 16:21 59-50-703/09/20 17:0810.0 2.8 1
4-Chloroaniline ND ug/L 03/10/20 16:21 106-47-803/09/20 17:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 03/10/20 16:21 111-91-103/09/20 17:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 03/10/20 16:21 111-44-403/09/20 17:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 03/10/20 16:21 91-58-703/09/20 17:0810.0 1.4 1
2-Chlorophenol ND ug/L 03/10/20 16:21 95-57-803/09/20 17:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 03/10/20 16:21 7005-72-303/09/20 17:0810.0 1.5 1
Chrysene ND ug/L 03/10/20 16:21 218-01-903/09/20 17:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 03/10/20 16:21 53-70-303/09/20 17:0810.0 1.6 1
Dibenzofuran ND ug/L 03/10/20 16:21 132-64-903/09/20 17:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 03/10/20 16:21 95-50-103/09/20 17:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 03/10/20 16:21 541-73-103/09/20 17:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 03/10/20 16:21 106-46-703/09/20 17:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 03/10/20 16:21 91-94-103/09/20 17:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 03/10/20 16:21 120-83-203/09/20 17:0810.0 1.5 1
Diethylphthalate ND ug/L 03/10/20 16:21 84-66-203/09/20 17:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 03/10/20 16:21 105-67-903/09/20 17:0810.0 1.5 1
Dimethylphthalate ND ug/L 03/10/20 16:21 131-11-303/09/20 17:0810.0 1.4 1
Di-n-butylphthalate ND ug/L 03/10/20 16:21 84-74-203/09/20 17:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 03/10/20 16:21 534-52-103/09/20 17:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 03/10/20 16:21 51-28-503/09/20 17:0850.0 7.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-DUP Lab ID:92468428005 Collected:03/04/20 00:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 03/10/20 16:21 121-14-203/09/20 17:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 03/10/20 16:21 606-20-203/09/20 17:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 03/10/20 16:21 117-84-003/09/20 17:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/10/20 16:21 117-81-703/09/20 17:086.0 2.0 1
Fluoranthene ND ug/L 03/10/20 16:21 206-44-003/09/20 17:0810.0 1.6 1
Fluorene ND ug/L 03/10/20 16:21 86-73-703/09/20 17:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 03/10/20 16:21 87-68-303/09/20 17:0810.0 1.6 1
Hexachlorobenzene ND ug/L 03/10/20 16:21 118-74-103/09/20 17:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 03/10/20 16:21 77-47-403/09/20 17:0810.0 2.4 1
Hexachloroethane ND ug/L 03/10/20 16:21 67-72-103/09/20 17:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/10/20 16:21 193-39-503/09/20 17:0810.0 1.7 1
Isophorone ND ug/L 03/10/20 16:21 78-59-103/09/20 17:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 03/10/20 16:21 90-12-003/09/20 17:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 03/10/20 16:21 91-57-603/09/20 17:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 03/10/20 16:21 95-48-703/09/20 17:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/10/20 16:21 15831-10-403/09/20 17:0810.0 1.2 1
Naphthalene ND ug/L 03/10/20 16:21 91-20-303/09/20 17:0810.0 1.6 1
2-Nitroaniline ND ug/L 03/10/20 16:21 88-74-403/09/20 17:0820.0 3.0 1
3-Nitroaniline ND ug/L 03/10/20 16:21 99-09-203/09/20 17:0820.0 2.8 1
4-Nitroaniline ND ug/L 03/10/20 16:21 100-01-603/09/20 17:0820.0 3.1 1
Nitrobenzene ND ug/L 03/10/20 16:21 98-95-303/09/20 17:0810.0 1.5 1
2-Nitrophenol ND ug/L 03/10/20 16:21 88-75-503/09/20 17:0810.0 1.7 1
4-Nitrophenol ND ug/L 03/10/20 16:21 100-02-703/09/20 17:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 03/10/20 16:21 62-75-903/09/20 17:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 03/10/20 16:21 621-64-703/09/20 17:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/10/20 16:21 86-30-603/09/20 17:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/10/20 16:21 108-60-103/09/20 17:0810.0 1.3 1
Pentachlorophenol ND ug/L 03/10/20 16:21 87-86-503/09/20 17:0820.0 2.8 1
Phenanthrene ND ug/L 03/10/20 16:21 85-01-803/09/20 17:0810.0 1.4 1
Phenol ND ug/L 03/10/20 16:21 108-95-203/09/20 17:0810.0 1.5 1
Pyrene ND ug/L 03/10/20 16:21 129-00-003/09/20 17:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 03/10/20 16:21 120-82-103/09/20 17:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 03/10/20 16:21 95-95-403/09/20 17:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 03/10/20 16:21 88-06-203/09/20 17:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)50 %03/10/20 16:21 4165-60-003/09/20 17:0813-130 1
2-Fluorobiphenyl (S)47 %03/10/20 16:21 321-60-803/09/20 17:0813-130 1
Terphenyl-d14 (S)78 %03/10/20 16:21 1718-51-003/09/20 17:0825-130 1
Phenol-d6 (S)25 %03/10/20 16:21 13127-88-303/09/20 17:0810-130 1
2-Fluorophenol (S)36 %03/10/20 16:21 367-12-403/09/20 17:0810-130 1
2,4,6-Tribromophenol (S)66 %03/10/20 16:21 118-79-603/09/20 17:0810-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 03/09/20 17:43 67-64-1 v125.0 6.2 1
Benzene ND ug/L 03/09/20 17:43 71-43-21.0 0.15 1
Bromobenzene ND ug/L 03/09/20 17:43 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
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9800 Kincey Ave. Suite 100
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Page 22 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-DUP Lab ID:92468428005 Collected:03/04/20 00:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 03/09/20 17:43 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 03/09/20 17:43 75-27-41.0 0.26 1
Bromoform ND ug/L 03/09/20 17:43 75-25-21.0 0.62 1
Bromomethane ND ug/L 03/09/20 17:43 74-83-9 IH,IK2.0 0.62 1
2-Butanone (MEK)ND ug/L 03/09/20 17:43 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 03/09/20 17:43 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 03/09/20 17:43 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/09/20 17:43 75-00-3 IK1.0 0.49 1
Chloroform ND ug/L 03/09/20 17:43 67-66-35.0 2.3 1
Chloromethane ND ug/L 03/09/20 17:43 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 03/09/20 17:43 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 03/09/20 17:43 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 03/09/20 17:43 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 03/09/20 17:43 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 03/09/20 17:43 106-93-41.0 0.26 1
Dibromomethane ND ug/L 03/09/20 17:43 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 03/09/20 17:43 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 03/09/20 17:43 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 03/09/20 17:43 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 03/09/20 17:43 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 03/09/20 17:43 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 03/09/20 17:43 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 03/09/20 17:43 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 03/09/20 17:43 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 03/09/20 17:43 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 03/09/20 17:43 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 03/09/20 17:43 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 03/09/20 17:43 594-20-7 IK,L1,v11.0 0.27 1
1,1-Dichloropropene ND ug/L 03/09/20 17:43 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 03/09/20 17:43 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 03/09/20 17:43 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 03/09/20 17:43 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 03/09/20 17:43 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 03/09/20 17:43 87-68-31.0 0.44 1
2-Hexanone ND ug/L 03/09/20 17:43 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 03/09/20 17:43 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 03/09/20 17:43 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/20 17:43 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 03/09/20 17:43 1634-04-41.0 0.28 1
Naphthalene ND ug/L 03/09/20 17:43 91-20-31.0 0.35 1
Styrene ND ug/L 03/09/20 17:43 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 03/09/20 17:43 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 03/09/20 17:43 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 03/09/20 17:43 127-18-41.0 0.16 1
Toluene ND ug/L 03/09/20 17:43 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/09/20 17:43 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
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Page 23 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TMW-DUP Lab ID:92468428005 Collected:03/04/20 00:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 03/09/20 17:43 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 03/09/20 17:43 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 03/09/20 17:43 79-00-51.0 0.24 1
Trichloroethene ND ug/L 03/09/20 17:43 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 03/09/20 17:43 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 03/09/20 17:43 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 03/09/20 17:43 108-05-4 v12.0 1.4 1
Vinyl chloride ND ug/L 03/09/20 17:43 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 03/09/20 17:43 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 03/09/20 17:43 179601-23-12.0 0.41 1
o-Xylene ND ug/L 03/09/20 17:43 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)97 %03/09/20 17:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %03/09/20 17:43 17060-07-070-130 1
Toluene-d8 (S)100 %03/09/20 17:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 24 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TB Lab ID:92468428006 Collected:03/04/20 00:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 03/09/20 14:40 67-64-1 v125.0 6.2 1
Benzene ND ug/L 03/09/20 14:40 71-43-21.0 0.15 1
Bromobenzene ND ug/L 03/09/20 14:40 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 03/09/20 14:40 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 03/09/20 14:40 75-27-41.0 0.26 1
Bromoform ND ug/L 03/09/20 14:40 75-25-21.0 0.62 1
Bromomethane ND ug/L 03/09/20 14:40 74-83-9 IH,IK2.0 0.62 1
2-Butanone (MEK)ND ug/L 03/09/20 14:40 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 03/09/20 14:40 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 03/09/20 14:40 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/09/20 14:40 75-00-3 IK1.0 0.49 1
Chloroform ND ug/L 03/09/20 14:40 67-66-35.0 2.3 1
Chloromethane ND ug/L 03/09/20 14:40 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 03/09/20 14:40 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 03/09/20 14:40 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 03/09/20 14:40 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 03/09/20 14:40 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 03/09/20 14:40 106-93-41.0 0.26 1
Dibromomethane ND ug/L 03/09/20 14:40 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 03/09/20 14:40 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 03/09/20 14:40 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 03/09/20 14:40 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 03/09/20 14:40 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 03/09/20 14:40 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 03/09/20 14:40 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 03/09/20 14:40 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 03/09/20 14:40 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 03/09/20 14:40 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 03/09/20 14:40 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 03/09/20 14:40 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 03/09/20 14:40 594-20-7 IK,L1,v11.0 0.27 1
1,1-Dichloropropene ND ug/L 03/09/20 14:40 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 03/09/20 14:40 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 03/09/20 14:40 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 03/09/20 14:40 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 03/09/20 14:40 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 03/09/20 14:40 87-68-31.0 0.44 1
2-Hexanone ND ug/L 03/09/20 14:40 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 03/09/20 14:40 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 03/09/20 14:40 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/09/20 14:40 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 03/09/20 14:40 1634-04-41.0 0.28 1
Naphthalene ND ug/L 03/09/20 14:40 91-20-31.0 0.35 1
Styrene ND ug/L 03/09/20 14:40 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 03/09/20 14:40 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 03/09/20 14:40 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468428
BOU-014
Sample:TB Lab ID:92468428006 Collected:03/04/20 00:00 Received:03/05/20 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 03/09/20 14:40 127-18-41.0 0.16 1
Toluene ND ug/L 03/09/20 14:40 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/09/20 14:40 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 03/09/20 14:40 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 03/09/20 14:40 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 03/09/20 14:40 79-00-51.0 0.24 1
Trichloroethene ND ug/L 03/09/20 14:40 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 03/09/20 14:40 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 03/09/20 14:40 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 03/09/20 14:40 108-05-4 v12.0 1.4 1
Vinyl chloride ND ug/L 03/09/20 14:40 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 03/09/20 14:40 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 03/09/20 14:40 179601-23-12.0 0.41 1
o-Xylene ND ug/L 03/09/20 14:40 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %03/09/20 14:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %03/09/20 14:40 17060-07-070-130 1
Toluene-d8 (S)104 %03/09/20 14:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1440142
3015
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428004, 92468428005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3506556-1
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428004, 92468428005
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 2.00 03/08/20 20:380.250
Barium ug/L ND 5.00 03/08/20 20:380.360
Cadmium ug/L ND 1.00 03/08/20 20:380.160
Chromium ug/L 0.573J 2.00 J03/08/20 20:380.540
Lead ug/L ND 2.00 03/08/20 20:380.240
Selenium ug/L ND 2.00 03/08/20 20:380.380
Silver ug/L ND 2.00 03/08/20 20:380.310
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3506556-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 47.150.0 94.1 80.0-120
Barium ug/L 45.850.0 91.5 80.0-120
Cadmium ug/L 49.950.0 99.7 80.0-120
Chromium ug/L 48.850.0 97.7 80.0-120
Lead ug/L 47.750.0 95.3 80.0-120
Selenium ug/L 49.250.0 98.4 80.0-120
Silver ug/L 48.050.0 96.0 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3506556-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1196694-01
R3506556-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 50.0 93.9 75.0-12592.9 1.10 2050.00.349 47.3 46.8
Barium ug/L 50.0 76.8 75.0-12578.1 0.658 2050.053.8 92.2 92.8
Cadmium ug/L 50.0 96.7 75.0-12595.0 1.44 2050.09.74 58.1 57.2
Chromium ug/L 50.0 96.4 75.0-12596.6 0.142 2050.00.879 49.1 49.2
Lead ug/L 50.0 96.2 75.0-12596.4 0.236 2050.0ND 48.1 48.2
Selenium ug/L 50.0 99.3 75.0-12598.7 0.589 2050.0ND 49.7 49.4
Silver ug/L 50.0 95.7 75.0-12594.3 1.49 2050.0ND 47.9 47.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1440072
7470A
EPA 7470A
Mercury 7470A
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428004, 92468428005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3506738-1
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428004, 92468428005
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 03/09/20 12:410.0490
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3506738-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.943.00 98.1 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3506738-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1195894-11
R3506738-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 101 75.0-12598.6 2.69 203.00ND 3.04 2.96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
529282
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428005, 92468428006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2826952
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428005, 92468428006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/09/20 13:450.34
1,1,1-Trichloroethane ug/L ND 1.0 03/09/20 13:450.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/09/20 13:450.22
1,1,2-Trichloroethane ug/L ND 1.0 03/09/20 13:450.24
1,1-Dichloroethane ug/L ND 1.0 03/09/20 13:450.27
1,1-Dichloroethene ug/L ND 1.0 03/09/20 13:450.24
1,1-Dichloropropene ug/L ND 1.0 03/09/20 13:450.21
1,2,3-Trichlorobenzene ug/L ND 1.0 03/09/20 13:450.34
1,2,3-Trichloropropane ug/L ND 1.0 03/09/20 13:450.35
1,2,4-Trichlorobenzene ug/L ND 1.0 03/09/20 13:450.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 03/09/20 13:450.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/09/20 13:450.26
1,2-Dichlorobenzene ug/L ND 1.0 03/09/20 13:450.29
1,2-Dichloroethane ug/L ND 1.0 03/09/20 13:450.34
1,2-Dichloropropane ug/L ND 1.0 03/09/20 13:450.19
1,3-Dichlorobenzene ug/L ND 1.0 03/09/20 13:450.22
1,3-Dichloropropane ug/L ND 1.0 03/09/20 13:450.16
1,4-Dichlorobenzene ug/L ND 1.0 03/09/20 13:450.26
2,2-Dichloropropane ug/L ND 1.0 IK,v103/09/20 13:450.27
2-Butanone (MEK)ug/L ND 5.0 03/09/20 13:453.3
2-Chlorotoluene ug/L ND 1.0 03/09/20 13:450.20
2-Hexanone ug/L ND 5.0 03/09/20 13:450.57
4-Chlorotoluene ug/L ND 1.0 03/09/20 13:450.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/09/20 13:454.5
Acetone ug/L ND 25.0 v103/09/20 13:456.2
Benzene ug/L ND 1.0 03/09/20 13:450.15
Bromobenzene ug/L ND 1.0 03/09/20 13:450.22
Bromochloromethane ug/L ND 1.0 03/09/20 13:450.34
Bromodichloromethane ug/L ND 1.0 03/09/20 13:450.26
Bromoform ug/L ND 1.0 03/09/20 13:450.62
Bromomethane ug/L ND 2.0 IH,IK03/09/20 13:450.62
Carbon tetrachloride ug/L ND 1.0 03/09/20 13:450.22
Chlorobenzene ug/L ND 1.0 03/09/20 13:450.23
Chloroethane ug/L ND 1.0 IK03/09/20 13:450.49
Chloroform ug/L ND 5.0 03/09/20 13:452.3
Chloromethane ug/L ND 1.0 03/09/20 13:450.39
cis-1,2-Dichloroethene ug/L ND 1.0 03/09/20 13:450.29
cis-1,3-Dichloropropene ug/L ND 1.0 03/09/20 13:450.30
Dibromochloromethane ug/L ND 1.0 03/09/20 13:450.41
Dibromomethane ug/L ND 1.0 03/09/20 13:450.46
Dichlorodifluoromethane ug/L ND 1.0 03/09/20 13:450.23
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2826952
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428005, 92468428006
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/09/20 13:450.22
Ethylbenzene ug/L ND 1.0 03/09/20 13:450.26
Hexachloro-1,3-butadiene ug/L ND 1.0 03/09/20 13:450.44
m&p-Xylene ug/L ND 2.0 03/09/20 13:450.41
Methyl-tert-butyl ether ug/L ND 1.0 03/09/20 13:450.28
Methylene Chloride ug/L ND 5.0 03/09/20 13:453.7
Naphthalene ug/L ND 1.0 03/09/20 13:450.35
o-Xylene ug/L ND 1.0 03/09/20 13:450.22
p-Isopropyltoluene ug/L ND 1.0 03/09/20 13:450.21
Styrene ug/L ND 1.0 03/09/20 13:450.27
Tetrachloroethene ug/L ND 1.0 03/09/20 13:450.16
Toluene ug/L ND 1.0 03/09/20 13:450.24
trans-1,2-Dichloroethene ug/L ND 1.0 03/09/20 13:450.25
trans-1,3-Dichloropropene ug/L ND 1.0 03/09/20 13:450.31
Trichloroethene ug/L ND 1.0 03/09/20 13:450.22
Trichlorofluoromethane ug/L ND 1.0 03/09/20 13:450.31
Vinyl acetate ug/L ND 2.0 v103/09/20 13:451.4
Vinyl chloride ug/L ND 1.0 03/09/20 13:450.24
Xylene (Total)ug/L ND 1.0 03/09/20 13:450.63
1,2-Dichloroethane-d4 (S)%103 70-130 03/09/20 13:45
4-Bromofluorobenzene (S)%99 70-130 03/09/20 13:45
Toluene-d8 (S)%103 70-130 03/09/20 13:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2826953LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.850 114 70-130
1,1,1-Trichloroethane ug/L 56.550 113 70-130
1,1,2,2-Tetrachloroethane ug/L 54.150 108 70-130
1,1,2-Trichloroethane ug/L 54.750 109 70-130
1,1-Dichloroethane ug/L 56.650 113 70-130
1,1-Dichloroethene ug/L 60.450 121 70-130
1,1-Dichloropropene ug/L 58.050 116 70-130
1,2,3-Trichlorobenzene ug/L 59.050 118 70-130
1,2,3-Trichloropropane ug/L 58.450 117 70-130
1,2,4-Trichlorobenzene ug/L 59.150 118 70-130
1,2-Dibromo-3-chloropropane ug/L 53.650 107 70-130
1,2-Dibromoethane (EDB)ug/L 57.450 115 70-130
1,2-Dichlorobenzene ug/L 57.850 116 70-130
1,2-Dichloroethane ug/L 53.950 108 70-130
1,2-Dichloropropane ug/L 54.850 110 70-130
1,3-Dichlorobenzene ug/L 57.950 116 70-130
1,3-Dichloropropane ug/L 55.550 111 70-131
1,4-Dichlorobenzene ug/L 57.650 115 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 30 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2826953LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 69.3 IK,L1,v15013969-130
2-Butanone (MEK)ug/L 110100 110 64-135
2-Chlorotoluene ug/L 58.250 116 70-130
2-Hexanone ug/L 112100 112 66-135
4-Chlorotoluene ug/L 58.550 117 70-130
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 70-130
Acetone ug/L 129 v110012961-157
Benzene ug/L 55.150 110 70-130
Bromobenzene ug/L 56.750 113 70-130
Bromochloromethane ug/L 59.950 120 70-130
Bromodichloromethane ug/L 57.250 114 70-130
Bromoform ug/L 57.050 114 70-130
Bromomethane ug/L 61.0 IH,IK5012238-130
Carbon tetrachloride ug/L 59.050 118 70-130
Chlorobenzene ug/L 55.250 110 70-130
Chloroethane ug/L 44.0 IK508837-142
Chloroform ug/L 54.650 109 70-130
Chloromethane ug/L 41.650 83 48-130
cis-1,2-Dichloroethene ug/L 55.250 110 70-130
cis-1,3-Dichloropropene ug/L 57.350 115 70-130
Dibromochloromethane ug/L 57.250 114 70-130
Dibromomethane ug/L 55.250 110 70-130
Dichlorodifluoromethane ug/L 48.450 97 53-134
Diisopropyl ether ug/L 57.050 114 70-135
Ethylbenzene ug/L 52.350 105 70-130
Hexachloro-1,3-butadiene ug/L 60.950 122 68-132
m&p-Xylene ug/L 108100 108 70-130
Methyl-tert-butyl ether ug/L 57.450 115 70-130
Methylene Chloride ug/L 54.550 109 67-132
Naphthalene ug/L 60.850 122 70-130
o-Xylene ug/L 55.150 110 70-131
p-Isopropyltoluene ug/L 60.750 121 70-130
Styrene ug/L 58.650 117 70-130
Tetrachloroethene ug/L 55.650 111 69-130
Toluene ug/L 52.550 105 70-130
trans-1,2-Dichloroethene ug/L 58.150 116 70-130
trans-1,3-Dichloropropene ug/L 58.650 117 70-130
Trichloroethene ug/L 53.350 107 70-130
Trichlorofluoromethane ug/L 51.050 102 63-130
Vinyl acetate ug/L 127 v110012755-143
Vinyl chloride ug/L 57.050 114 70-131
Xylene (Total)ug/L 164150 109 70-130
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2826954MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92467909001
2826955
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 125 73-134128 3 30200ND249256
1,1,1-Trichloroethane ug/L 200 106 82-143112 5 30200ND212224
1,1,2,2-Tetrachloroethane ug/L 200 122 70-136126 4 30200ND244253
1,1,2-Trichloroethane ug/L 200 122 70-135125 2 30200ND244249
1,1-Dichloroethane ug/L 200 95 70-139100 6 30200ND190201
1,1-Dichloroethene ug/L M12006370-15464 3 30200ND125129
1,1-Dichloropropene ug/L 200 105 70-149110 4 30200ND210220
1,2,3-Trichlorobenzene ug/L 200 123 70-135130 5 30200ND247260
1,2,3-Trichloropropane ug/L 200 97 71-137101 4 30200ND194202
1,2,4-Trichlorobenzene ug/L 200 125 73-140130 4 30200ND251261
1,2-Dibromo-3-
chloropropane ug/L 200 122 65-134122 0 30200ND245244
1,2-Dibromoethane (EDB)ug/L 200 123 70-137129 5 30200ND245259
1,2-Dichlorobenzene ug/L 200 128 70-133132 3 30200ND257263
1,2-Dichloroethane ug/L 200 107 70-137113 5 30200ND222233
1,2-Dichloropropane ug/L 200 112 70-140118 5 30200ND225236
1,3-Dichlorobenzene ug/L 200 130 70-135132 2 30200ND260264
1,3-Dichloropropane ug/L 200 120 70-143127 5 30200ND240254
1,4-Dichlorobenzene ug/L 200 131 70-133133 2 30200ND261266
2,2-Dichloropropane ug/L IK,v120011761-148131 11 30200ND235262
2-Butanone (MEK)ug/L 400 113 60-139115 1 30400392844851
2-Chlorotoluene ug/L M120015270-144153 1 30200ND303306
2-Hexanone ug/L M140014265-138144 1 30400ND568576
4-Chlorotoluene ug/L 200 133 70-137137 3 30200ND266273
4-Methyl-2-pentanone
(MIBK)ug/L 400 124 65-135122 1 3040060.6 558 550
Acetone ug/L v14009960-148106 3 3040068410801110
Benzene ug/L 200 115 70-151111 0 30200138016101600
Bromobenzene ug/L 200 126 70-136130 3 30200ND253260
Bromochloromethane ug/L 200 114 70-141119 5 30200ND227239
Bromodichloromethane ug/L 200 122 70-138127 4 30200ND244255
Bromoform ug/L 200 122 63-130127 4 30200ND244253
Bromomethane ug/L IH,IK2006815-15261 10 30200ND135122
Carbon tetrachloride ug/L 200 107 70-143111 4 30200ND214222
Chlorobenzene ug/L 200 124 70-138129 4 30200ND247257
Chloroethane ug/L IK,M12003052-16331 6 30200ND59.1 62.8
Chloroform ug/L 200 112 70-139116 4 30200ND223232
Chloromethane ug/L M12003841-13935 7 30200ND75.1 70.1
cis-1,2-Dichloroethene ug/L 200 102 70-141107 4 30200ND205214
cis-1,3-Dichloropropene ug/L 200 116 70-137121 4 30200ND232241
Dibromochloromethane ug/L 200 121 70-134129 6 30200ND242257
Dibromomethane ug/L 200 115 70-138118 2 30200ND231235
Dichlorodifluoromethane ug/L M1200047-1550 30200NDNDND
Diisopropyl ether ug/L 200 108 63-144111 3 3020033.3 249 255
Ethylbenzene ug/L 200 119 66-153128 3 30200357596614
Hexachloro-1,3-butadiene ug/L 200 136 65-149139 2 30200ND273278
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2826954MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92467909001
2826955
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 400 124 69-152135 3 30400101015101550
Methyl-tert-butyl ether ug/L 200 98 54-156102 4 30200ND196204
Methylene Chloride ug/L 200 97 42-159103 6 30200ND194206
Naphthalene ug/L 200 129 61-148137 4 30200149407422
o-Xylene ug/L 200 127 70-148137 3 30200483737757
p-Isopropyltoluene ug/L 200 138 70-146140 1 3020011.4 288 292
Styrene ug/L M120013970-135145 4 30200ND277290
Tetrachloroethene ug/L 200 120 59-143124 3 30200ND241247
Toluene ug/L 200 115 59-148113 1 30200409639634
trans-1,2-Dichloroethene ug/L 200 87 70-14692 6 30200ND174184
trans-1,3-Dichloropropene ug/L 200 118 70-135125 6 30200ND236251
Trichloroethene ug/L 200 109 70-147113 4 30200ND218227
Trichlorofluoromethane ug/L M12003770-14839 5 30200ND73.8 77.7
Vinyl acetate ug/L v140011449-151122 6 30400ND457487
Vinyl chloride ug/L M1200870-1568 4 30200ND15.2 15.9
Xylene (Total)ug/L 600 125 63-158136 3 30600150022502310
1,2-Dichloroethane-d4 (S)%104 70-130105
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
529831
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples:92468428004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2829734
Associated Lab Samples:92468428004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/12/20 13:130.34
1,1,1-Trichloroethane ug/L ND 1.0 03/12/20 13:130.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/12/20 13:130.22
1,1,2-Trichloroethane ug/L ND 1.0 03/12/20 13:130.24
1,1-Dichloroethane ug/L ND 1.0 03/12/20 13:130.27
1,1-Dichloroethene ug/L ND 1.0 03/12/20 13:130.24
1,1-Dichloropropene ug/L ND 1.0 03/12/20 13:130.21
1,2,3-Trichlorobenzene ug/L ND 1.0 03/12/20 13:130.34
1,2,3-Trichloropropane ug/L ND 1.0 03/12/20 13:130.35
1,2,4-Trichlorobenzene ug/L ND 1.0 03/12/20 13:130.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 03/12/20 13:130.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/12/20 13:130.26
1,2-Dichlorobenzene ug/L ND 1.0 03/12/20 13:130.29
1,2-Dichloroethane ug/L ND 1.0 03/12/20 13:130.34
1,2-Dichloropropane ug/L ND 1.0 03/12/20 13:130.19
1,3-Dichlorobenzene ug/L ND 1.0 03/12/20 13:130.22
1,3-Dichloropropane ug/L ND 1.0 03/12/20 13:130.16
1,4-Dichlorobenzene ug/L ND 1.0 03/12/20 13:130.26
2,2-Dichloropropane ug/L ND 1.0 v103/12/20 13:130.27
2-Butanone (MEK)ug/L ND 5.0 03/12/20 13:133.3
2-Chlorotoluene ug/L ND 1.0 03/12/20 13:130.20
2-Hexanone ug/L ND 5.0 03/12/20 13:130.57
4-Chlorotoluene ug/L ND 1.0 03/12/20 13:130.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/12/20 13:134.5
Acetone ug/L ND 25.0 03/12/20 13:136.2
Benzene ug/L ND 1.0 03/12/20 13:130.15
Bromobenzene ug/L ND 1.0 03/12/20 13:130.22
Bromochloromethane ug/L ND 1.0 03/12/20 13:130.34
Bromodichloromethane ug/L ND 1.0 03/12/20 13:130.26
Bromoform ug/L ND 1.0 03/12/20 13:130.62
Bromomethane ug/L ND 2.0 IH03/12/20 13:130.62
Carbon tetrachloride ug/L ND 1.0 03/12/20 13:130.22
Chlorobenzene ug/L ND 1.0 03/12/20 13:130.23
Chloroethane ug/L ND 1.0 v103/12/20 13:130.49
Chloroform ug/L ND 5.0 03/12/20 13:132.3
Chloromethane ug/L ND 1.0 03/12/20 13:130.39
cis-1,2-Dichloroethene ug/L ND 1.0 03/12/20 13:130.29
cis-1,3-Dichloropropene ug/L ND 1.0 03/12/20 13:130.30
Dibromochloromethane ug/L ND 1.0 03/12/20 13:130.41
Dibromomethane ug/L ND 1.0 03/12/20 13:130.46
Dichlorodifluoromethane ug/L ND 1.0 IH,v103/12/20 13:130.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 34 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2829734
Associated Lab Samples:92468428004
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/12/20 13:130.22
Ethylbenzene ug/L ND 1.0 03/12/20 13:130.26
Hexachloro-1,3-butadiene ug/L ND 1.0 03/12/20 13:130.44
m&p-Xylene ug/L ND 2.0 03/12/20 13:130.41
Methyl-tert-butyl ether ug/L ND 1.0 03/12/20 13:130.28
Methylene Chloride ug/L ND 5.0 03/12/20 13:133.7
Naphthalene ug/L ND 1.0 03/12/20 13:130.35
o-Xylene ug/L ND 1.0 03/12/20 13:130.22
p-Isopropyltoluene ug/L ND 1.0 03/12/20 13:130.21
Styrene ug/L ND 1.0 03/12/20 13:130.27
Tetrachloroethene ug/L ND 1.0 03/12/20 13:130.16
Toluene ug/L ND 1.0 03/12/20 13:130.24
trans-1,2-Dichloroethene ug/L ND 1.0 03/12/20 13:130.25
trans-1,3-Dichloropropene ug/L ND 1.0 03/12/20 13:130.31
Trichloroethene ug/L ND 1.0 03/12/20 13:130.22
Trichlorofluoromethane ug/L ND 1.0 v103/12/20 13:130.31
Vinyl acetate ug/L ND 2.0 03/12/20 13:131.4
Vinyl chloride ug/L ND 1.0 IH,v103/12/20 13:130.24
Xylene (Total)ug/L ND 1.0 03/12/20 13:130.63
1,2-Dichloroethane-d4 (S)%100 70-130 03/12/20 13:13
4-Bromofluorobenzene (S)%98 70-130 03/12/20 13:13
Toluene-d8 (S)%102 70-130 03/12/20 13:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2829735LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.450 111 70-130
1,1,1-Trichloroethane ug/L 56.450 113 70-130
1,1,2,2-Tetrachloroethane ug/L 54.150 108 70-130
1,1,2-Trichloroethane ug/L 54.150 108 70-130
1,1-Dichloroethane ug/L 56.350 113 70-130
1,1-Dichloroethene ug/L 60.450 121 70-130
1,1-Dichloropropene ug/L 59.150 118 70-130
1,2,3-Trichlorobenzene ug/L 65.6 L15013170-130
1,2,3-Trichloropropane ug/L 54.150 108 70-130
1,2,4-Trichlorobenzene ug/L 62.750 125 70-130
1,2-Dibromo-3-chloropropane ug/L 54.150 108 70-130
1,2-Dibromoethane (EDB)ug/L 58.050 116 70-130
1,2-Dichlorobenzene ug/L 57.550 115 70-130
1,2-Dichloroethane ug/L 52.450 105 70-130
1,2-Dichloropropane ug/L 55.850 112 70-130
1,3-Dichlorobenzene ug/L 57.150 114 70-130
1,3-Dichloropropane ug/L 57.050 114 70-131
1,4-Dichlorobenzene ug/L 57.950 116 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2829735LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 67.6 L1,v15013569-130
2-Butanone (MEK)ug/L 121100 121 64-135
2-Chlorotoluene ug/L 54.650 109 70-130
2-Hexanone ug/L 113100 113 66-135
4-Chlorotoluene ug/L 56.750 113 70-130
4-Methyl-2-pentanone (MIBK)ug/L 106100 106 70-130
Acetone ug/L 130100 130 61-157
Benzene ug/L 56.550 113 70-130
Bromobenzene ug/L 55.450 111 70-130
Bromochloromethane ug/L 58.050 116 70-130
Bromodichloromethane ug/L 58.350 117 70-130
Bromoform ug/L 50.450 101 70-130
Bromomethane ug/L 78.5 IH,L15015738-130
Carbon tetrachloride ug/L 59.650 119 70-130
Chlorobenzene ug/L 56.150 112 70-130
Chloroethane ug/L 50.3 v15010137-142
Chloroform ug/L 54.350 109 70-130
Chloromethane ug/L 54.750 109 48-130
cis-1,2-Dichloroethene ug/L 55.450 111 70-130
cis-1,3-Dichloropropene ug/L 58.250 116 70-130
Dibromochloromethane ug/L 58.450 117 70-130
Dibromomethane ug/L 53.250 106 70-130
Dichlorodifluoromethane ug/L 59.4 IH,v15011953-134
Diisopropyl ether ug/L 57.750 115 70-135
Ethylbenzene ug/L 53.050 106 70-130
Hexachloro-1,3-butadiene ug/L 64.050 128 68-132
m&p-Xylene ug/L 108100 108 70-130
Methyl-tert-butyl ether ug/L 56.750 113 70-130
Methylene Chloride ug/L 55.050 110 67-132
Naphthalene ug/L 64.650 129 70-130
o-Xylene ug/L 54.550 109 70-131
p-Isopropyltoluene ug/L 59.950 120 70-130
Styrene ug/L 58.850 118 70-130
Tetrachloroethene ug/L 56.350 113 69-130
Toluene ug/L 51.750 103 70-130
trans-1,2-Dichloroethene ug/L 59.250 118 70-130
trans-1,3-Dichloropropene ug/L 59.750 119 70-130
Trichloroethene ug/L 56.850 114 70-130
Trichlorofluoromethane ug/L 51.2 v15010263-130
Vinyl acetate ug/L 123100 123 55-143
Vinyl chloride ug/L 64.3 IH,v15012970-131
Xylene (Total)ug/L 162150 108 70-130
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2830494MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
2629830001
2830495
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 800 109 73-134107 1 3080040.0 U 869 859
1,1,1-Trichloroethane ug/L 800 115 82-143115 1 3080040.0 U 923 918
1,1,2,2-Tetrachloroethane ug/L 800 107 70-136105 2 3080040.0 U 855 840
1,1,2-Trichloroethane ug/L 800 109 70-135108 1 3080040.0 U 869 862
1,1-Dichloroethane ug/L 800 116 70-139110 6 3080040.0 U 930 878
1,1-Dichloroethene ug/L 800 130 70-154120 8 3080040.0 U 1040 962
1,1-Dichloropropene ug/L 800 122 70-149117 4 3080040.0 U 976 935
1,2,3-Trichlorobenzene ug/L 800 113 70-135113 0 3080040.0 U 900 905
1,2,3-Trichloropropane ug/L 800 109 71-137104 5 3080040.0 U 875 829
1,2,4-Trichlorobenzene ug/L 800 110 73-140109 0 3080040.0 U 877 875
1,2-Dibromo-3-
chloropropane ug/L 800 102 65-134102 0 30800200 U 815 814
1,2-Dibromoethane (EDB)ug/L 800 115 70-137106 7 3080040.0 U 918 852
1,2-Dichlorobenzene ug/L 800 105 70-133104 1 3080040.0 U 842 833
1,2-Dichloroethane ug/L 800 103 70-137101 2 3080040.0 U 822 805
1,2-Dichloropropane ug/L 800 112 70-140104 8 3080040.0 U 897 831
1,3-Dichlorobenzene ug/L 800 106 70-135104 1 3080040.0 U 844 832
1,3-Dichloropropane ug/L 800 112 70-143109 3 3080040.0 U 896 872
1,4-Dichlorobenzene ug/L 800 103 70-133103 0 3080040.0 U 827 827
2,2-Dichloropropane ug/L v180013961-148130 7 3080040.0 U 1120 1040
2-Butanone (MEK)ug/L 1600 107 60-139106 1 301600200 U 1710 1690
2-Chlorotoluene ug/L 800 108 70-144105 3 3080040.0 U 863 837
2-Hexanone ug/L 1600 109 65-138107 2 301600200 U 1740 1710
4-Chlorotoluene ug/L 800 106 70-137106 0 3080040.0 U 848 851
4-Methyl-2-pentanone
(MIBK)ug/L 1600 108 65-135103 5 301600200 U 1740 1650
Acetone ug/L 1600 107 60-14897 10 3016001000 U 1710 1550
Benzene ug/L 800 115 70-151113 2 3080040.0 U 923 908
Bromobenzene ug/L 800 105 70-136105 0 3080040.0 U 843 840
Bromochloromethane ug/L 800 117 70-141109 7 3080040.0 U 938 871
Bromodichloromethane ug/L 800 116 70-138107 8 3080040.0 U 928 860
Bromoform ug/L 800 95 63-13091 4 3080040.0 U 761 727
Bromomethane ug/L IH,M080018615-152185 0 3080080.0 U 1490 1480
Carbon tetrachloride ug/L 800 125 70-143122 3 3080040.0 U 1000 973
Chlorobenzene ug/L 800 111 70-138107 3 3080040.0 U 886 858
Chloroethane ug/L v180012552-163117 7 3080040.0 U 1000 938
Chloroform ug/L 800 108 70-139110 2 30800200 U 868 881
Chloromethane ug/L 800 123 41-139113 8 3080040.0 U 982 908
cis-1,2-Dichloroethene ug/L 800 116 70-141106 6 3080048014101330
cis-1,3-Dichloropropene ug/L 800 118 70-137110 6 3080040.0 U 942 883
Dibromochloromethane ug/L 800 112 70-134106 5 3080040.0 U 897 850
Dibromomethane ug/L 800 110 70-138109 1 3080040.0 U 878 869
Dichlorodifluoromethane ug/L IH,v180013647-155121 12 3080040.0 U 1090 968
Diisopropyl ether ug/L 800 110 63-144106 3 3080040.0 U 879 849
Ethylbenzene ug/L 800 107 66-153103 4 3080040.0 U 858 828
Hexachloro-1,3-butadiene ug/L 800 126 65-149123 2 3080040.0 U 1000 983
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2830494MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
2629830001
2830495
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 1600 109 69-152105 4 30160080.0 U 1750 1680
Methyl-tert-butyl ether ug/L 800 109 54-156104 5 3080040.0 U 872 830
Methylene Chloride ug/L 800 116 42-159109 7 30800200 U 930 870
Naphthalene ug/L 800 108 61-148108 0 3080018.0J 881 881
o-Xylene ug/L 800 106 70-148104 2 3080040.0 U 850 831
p-Isopropyltoluene ug/L 800 116 70-146112 4 3080040.0 U 931 897
Styrene ug/L 800 111 70-135108 3 3080040.0 U 890 861
Tetrachloroethene ug/L M180014459-143128 3 30800385050004880
Toluene ug/L 800 109 59-148103 5 3080040.0 U 871 826
trans-1,2-Dichloroethene ug/L 800 125 70-146114 9 3080040.0 U 999 913
trans-1,3-Dichloropropene ug/L 800 119 70-135112 6 3080040.0 U 949 898
Trichloroethene ug/L 800 118 70-147111 6 3080067.1 1010 954
Trichlorofluoromethane ug/L v180011970-148114 4 3080040.0 U 953 913
Vinyl acetate ug/L 1600 118 49-151113 5 30160080.0 U 1890 1810
Vinyl chloride ug/L IH,v180014470-156134 7 3080040.0 U 1150 1070
Xylene (Total)ug/L 2400 108 63-158105 3 30240040.0 U 2600 2510
1,2-Dichloroethane-d4 (S)%100 70-130101
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
529318
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428004, 92468428005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2827200
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428004, 92468428005
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 03/10/20 12:561.6
1,2-Dichlorobenzene ug/L ND 10.0 03/10/20 12:561.4
1,3-Dichlorobenzene ug/L ND 10.0 03/10/20 12:561.4
1,4-Dichlorobenzene ug/L ND 10.0 03/10/20 12:561.5
1-Methylnaphthalene ug/L ND 10.0 03/10/20 12:561.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 03/10/20 12:561.3
2,4,5-Trichlorophenol ug/L ND 10.0 03/10/20 12:561.5
2,4,6-Trichlorophenol ug/L ND 10.0 03/10/20 12:561.4
2,4-Dichlorophenol ug/L ND 10.0 03/10/20 12:561.5
2,4-Dimethylphenol ug/L ND 10.0 03/10/20 12:561.5
2,4-Dinitrophenol ug/L ND 50.0 03/10/20 12:567.3
2,4-Dinitrotoluene ug/L ND 10.0 03/10/20 12:561.7
2,6-Dinitrotoluene ug/L ND 10.0 03/10/20 12:561.7
2-Chloronaphthalene ug/L ND 10.0 03/10/20 12:561.4
2-Chlorophenol ug/L ND 10.0 03/10/20 12:561.4
2-Methylnaphthalene ug/L ND 10.0 03/10/20 12:561.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/10/20 12:561.2
2-Nitroaniline ug/L ND 20.0 03/10/20 12:563.0
2-Nitrophenol ug/L ND 10.0 03/10/20 12:561.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/10/20 12:561.2
3,3'-Dichlorobenzidine ug/L ND 20.0 03/10/20 12:562.7
3-Nitroaniline ug/L ND 20.0 03/10/20 12:562.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/10/20 12:564.5
4-Bromophenylphenyl ether ug/L ND 10.0 03/10/20 12:561.2
4-Chloro-3-methylphenol ug/L ND 10.0 03/10/20 12:562.8
4-Chloroaniline ug/L ND 20.0 03/10/20 12:562.8
4-Chlorophenylphenyl ether ug/L ND 10.0 03/10/20 12:561.5
4-Nitroaniline ug/L ND 20.0 03/10/20 12:563.1
4-Nitrophenol ug/L ND 50.0 03/10/20 12:569.4
Acenaphthene ug/L ND 10.0 03/10/20 12:561.4
Acenaphthylene ug/L ND 10.0 03/10/20 12:561.5
Aniline ug/L ND 10.0 03/10/20 12:561.6
Anthracene ug/L ND 10.0 03/10/20 12:561.6
Benzo(a)anthracene ug/L ND 10.0 03/10/20 12:561.5
Benzo(a)pyrene ug/L ND 10.0 03/10/20 12:561.8
Benzo(b)fluoranthene ug/L ND 10.0 03/10/20 12:561.7
Benzo(g,h,i)perylene ug/L ND 10.0 03/10/20 12:561.6
Benzo(k)fluoranthene ug/L ND 10.0 03/10/20 12:561.5
Benzoic Acid ug/L ND 50.0 03/10/20 12:5619.5
Benzyl alcohol ug/L ND 20.0 03/10/20 12:562.6
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/10/20 12:561.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2827200
Associated Lab Samples:92468428001, 92468428002, 92468428003, 92468428004, 92468428005
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 03/10/20 12:561.7
bis(2-Ethylhexyl)phthalate ug/L 2.2J 6.0 03/10/20 12:562.0
Butylbenzylphthalate ug/L ND 10.0 03/10/20 12:561.9
Chrysene ug/L ND 10.0 03/10/20 12:561.4
Di-n-butylphthalate ug/L ND 10.0 03/10/20 12:561.6
Di-n-octylphthalate ug/L ND 10.0 03/10/20 12:562.2
Dibenz(a,h)anthracene ug/L ND 10.0 03/10/20 12:561.6
Dibenzofuran ug/L ND 10.0 03/10/20 12:561.3
Diethylphthalate ug/L ND 10.0 03/10/20 12:561.6
Dimethylphthalate ug/L ND 10.0 03/10/20 12:561.4
Fluoranthene ug/L ND 10.0 03/10/20 12:561.6
Fluorene ug/L ND 10.0 03/10/20 12:561.4
Hexachloro-1,3-butadiene ug/L ND 10.0 03/10/20 12:561.6
Hexachlorobenzene ug/L ND 10.0 03/10/20 12:561.3
Hexachlorocyclopentadiene ug/L ND 10.0 03/10/20 12:562.4
Hexachloroethane ug/L ND 10.0 03/10/20 12:561.3
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/10/20 12:561.7
Isophorone ug/L ND 10.0 03/10/20 12:561.3
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/10/20 12:561.3
N-Nitrosodimethylamine ug/L ND 10.0 03/10/20 12:561.8
N-Nitrosodiphenylamine ug/L ND 10.0 03/10/20 12:561.4
Naphthalene ug/L ND 10.0 03/10/20 12:561.6
Nitrobenzene ug/L ND 10.0 03/10/20 12:561.5
Pentachlorophenol ug/L ND 20.0 03/10/20 12:562.8
Phenanthrene ug/L ND 10.0 03/10/20 12:561.4
Phenol ug/L ND 10.0 03/10/20 12:561.5
Pyrene ug/L ND 10.0 03/10/20 12:561.5
2,4,6-Tribromophenol (S)%46 10-137 03/10/20 12:56
2-Fluorobiphenyl (S)%42 13-130 03/10/20 12:56
2-Fluorophenol (S)%34 10-130 03/10/20 12:56
Nitrobenzene-d5 (S)%46 13-130 03/10/20 12:56
Phenol-d6 (S)%24 10-130 03/10/20 12:56
Terphenyl-d14 (S)%65 25-130 03/10/20 12:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2827201LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 26.650 53 30-130
1,2-Dichlorobenzene ug/L 29.450 59 30-130
1,3-Dichlorobenzene ug/L 29.050 58 20-130
1,4-Dichlorobenzene ug/L 30.450 61 30-130
1-Methylnaphthalene ug/L 29.750 59 30-130
2,2'-Oxybis(1-chloropropane)ug/L 35.750 71 20-130
2,4,5-Trichlorophenol ug/L 30.850 62 40-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2827201LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 29.850 60 40-130
2,4-Dichlorophenol ug/L 29.250 58 31-130
2,4-Dimethylphenol ug/L 27.250 54 30-130
2,4-Dinitrophenol ug/L 168250 67 30-130
2,4-Dinitrotoluene ug/L 37.950 76 49-130
2,6-Dinitrotoluene ug/L 35.050 70 50-130
2-Chloronaphthalene ug/L 29.650 59 30-130
2-Chlorophenol ug/L 30.050 60 30-130
2-Methylnaphthalene ug/L 29.850 60 30-130
2-Methylphenol(o-Cresol)ug/L 28.050 56 30-130
2-Nitroaniline ug/L 62.7100 63 40-130
2-Nitrophenol ug/L 32.850 66 20-130
3&4-Methylphenol(m&p Cresol)ug/L 26.050 52 20-130
3,3'-Dichlorobenzidine ug/L 72.5100 73 10-150
3-Nitroaniline ug/L 73.2100 73 40-130
4,6-Dinitro-2-methylphenol ug/L 79.2100 79 40-130
4-Bromophenylphenyl ether ug/L 32.750 65 30-130
4-Chloro-3-methylphenol ug/L 60.5100 61 30-130
4-Chloroaniline ug/L 56.2100 56 20-130
4-Chlorophenylphenyl ether ug/L 29.050 58 20-130
4-Nitroaniline ug/L 80.6100 81 40-130
4-Nitrophenol ug/L 111250 45 10-130
Acenaphthene ug/L 30.850 62 30-130
Acenaphthylene ug/L 31.550 63 30-130
Aniline ug/L 24.550 49 20-130
Anthracene ug/L 37.250 74 50-130
Benzo(a)anthracene ug/L 39.550 79 50-130
Benzo(a)pyrene ug/L 40.950 82 50-130
Benzo(b)fluoranthene ug/L 39.950 80 50-130
Benzo(g,h,i)perylene ug/L 42.350 85 50-130
Benzo(k)fluoranthene ug/L 41.150 82 50-130
Benzoic Acid ug/L 84.1250 34 10-130
Benzyl alcohol ug/L 57.0100 57 20-130
bis(2-Chloroethoxy)methane ug/L 29.650 59 30-130
bis(2-Chloroethyl) ether ug/L 30.750 61 30-130
bis(2-Ethylhexyl)phthalate ug/L 52.050 104 50-130
Butylbenzylphthalate ug/L 48.950 98 50-150
Chrysene ug/L 39.450 79 50-130
Di-n-butylphthalate ug/L 46.950 94 50-130
Di-n-octylphthalate ug/L 52.950 106 50-130
Dibenz(a,h)anthracene ug/L 42.950 86 40-130
Dibenzofuran ug/L 30.350 61 40-130
Diethylphthalate ug/L 38.250 76 40-130
Dimethylphthalate ug/L 33.950 68 40-130
Fluoranthene ug/L 38.950 78 30-130
Fluorene ug/L 31.850 64 20-130
Hexachloro-1,3-butadiene ug/L 25.550 51 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2827201LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 34.050 68 30-130
Hexachlorocyclopentadiene ug/L 25.650 51 10-150
Hexachloroethane ug/L 29.850 60 10-130
Indeno(1,2,3-cd)pyrene ug/L 42.350 85 40-130
Isophorone ug/L 30.550 61 30-130
N-Nitroso-di-n-propylamine ug/L 30.850 62 30-130
N-Nitrosodimethylamine ug/L 25.250 50 10-130
N-Nitrosodiphenylamine ug/L 36.050 72 30-130
Naphthalene ug/L 30.050 60 20-130
Nitrobenzene ug/L 30.050 60 20-130
Pentachlorophenol ug/L 82.9100 83 10-140
Phenanthrene ug/L 36.850 74 50-130
Phenol ug/L 19.450 39 10-130
Pyrene ug/L 38.750 77 50-130
2,4,6-Tribromophenol (S)%96 10-137
2-Fluorobiphenyl (S)%68 13-130
2-Fluorophenol (S)%53 10-130
Nitrobenzene-d5 (S)%72 13-130
Phenol-d6 (S)%39 10-130
Terphenyl-d14 (S)%83 25-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2827202MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92468428001
2827203
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M1,R1505130-13026 64 3050ND25.3 13.1
1,2-Dichlorobenzene ug/L R1505630-13030 62 3050ND28.0 14.8
1,3-Dichlorobenzene ug/L R1505520-13030 61 3050ND27.6 14.8
1,4-Dichlorobenzene ug/L R1505830-13031 61 3050ND29.0 15.5
1-Methylnaphthalene ug/L M1,R1505530-13028 66 3050ND27.7 14.0
2,2'-Oxybis(1-
chloropropane)ug/L R1507220-13035 70 3050ND36.0 17.4
2,4,5-Trichlorophenol ug/L M1,R1506140-13031 67 3050ND30.5 15.3
2,4,6-Trichlorophenol ug/L M1,R1506040-13030 69 3050ND30.2 14.8
2,4-Dichlorophenol ug/L M1,R1505731-13028 69 3050ND28.7 14.0
2,4-Dimethylphenol ug/L M1,R1505930-13028 70 3050ND29.3 14.2
2,4-Dinitrophenol ug/L R12506630-13044 39 30250ND164111
2,4-Dinitrotoluene ug/L R1507549-13050 40 3050ND37.5 25.1
2,6-Dinitrotoluene ug/L M1,R1507150-13039 59 3050ND35.6 19.4
2-Chloronaphthalene ug/L M1,R1505830-13029 65 3050ND28.9 14.7
2-Chlorophenol ug/L R1506030-13030 66 3050ND30.2 15.2
2-Methylnaphthalene ug/L M1,R1505730-13028 66 3050ND28.3 14.2
2-Methylphenol(o-Cresol)ug/L M1,R1505630-13028 68 3050ND28.2 13.9
2-Nitroaniline ug/L M1,R11006740-13035 62 30100ND66.5 35.2
2-Nitrophenol ug/L R1506620-13032 69 3050ND33.2 16.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2827202MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92468428001
2827203
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L R1505020-13026 65 3050ND25.1 12.8
3,3'-Dichlorobenzidine ug/L 100 67 10-15061 9 30100ND66.7 61.1
3-Nitroaniline ug/L R11007440-13040 60 30100ND73.9 39.9
4,6-Dinitro-2-methylphenol ug/L 100 75 40-13058 25 30100ND74.9 58.2
4-Bromophenylphenyl ether ug/L R1506330-13037 53 3050ND31.6 18.4
4-Chloro-3-methylphenol ug/L R11005930-13030 65 30100ND58.8 30.0
4-Chloroaniline ug/L R11005720-13030 62 30100ND57.3 30.1
4-Chlorophenylphenyl ether ug/L R1505720-13030 62 3050ND28.3 15.0
4-Nitroaniline ug/L 100 75 40-13061 21 30100ND74.7 60.6
4-Nitrophenol ug/L 250 40 10-13036 9 30250ND99.4 91.0
Acenaphthene ug/L R1506130-13031 65 3050ND30.6 15.5
Acenaphthylene ug/L R1506330-13031 66 3050ND31.3 15.7
Aniline ug/L R1505120-13026 66 3050ND25.3 12.8
Anthracene ug/L R1507150-13050 35 3050ND35.7 25.0
Benzo(a)anthracene ug/L 50 72 50-13071 2 3050ND36.1 35.4
Benzo(a)pyrene ug/L 50 75 50-13072 4 3050ND37.4 36.0
Benzo(b)fluoranthene ug/L 50 72 50-13069 3 3050ND35.8 34.7
Benzo(g,h,i)perylene ug/L 50 79 50-13075 6 3050ND39.5 37.3
Benzo(k)fluoranthene ug/L 50 75 50-13072 3 3050ND37.3 36.0
Benzoic Acid ug/L 250 34 10-13019 30250ND83.9 46.7J
Benzyl alcohol ug/L R11005720-13029 67 30100ND57.4 28.7
bis(2-
Chloroethoxy)methane ug/L M1,R1505830-13029 67 3050ND29.1 14.5
bis(2-Chloroethyl) ether ug/L R1506230-13031 68 3050ND31.2 15.3
bis(2-Ethylhexyl)phthalate ug/L 50 88 50-13086 3 3050ND44.2 42.9
Butylbenzylphthalate ug/L 50 86 50-15083 3 3050ND42.8 41.5
Chrysene ug/L 50 73 50-13072 2 3050ND36.5 35.8
Di-n-butylphthalate ug/L 50 81 50-13075 7 3050ND40.5 37.6
Di-n-octylphthalate ug/L 50 91 50-13087 5 3050ND45.3 43.3
Dibenz(a,h)anthracene ug/L 50 79 40-13075 6 3050ND39.6 37.4
Dibenzofuran ug/L M1,R1506140-13032 63 3050ND30.5 15.9
Diethylphthalate ug/L R1507340-13047 43 3050ND36.3 23.6
Dimethylphthalate ug/L M1,R1506840-13039 55 3050ND34.1 19.4
Fluoranthene ug/L 50 71 30-13067 7 3050ND35.7 33.3
Fluorene ug/L R1506320-13034 60 3050ND31.3 16.9
Hexachloro-1,3-butadiene ug/L R1504810-13024 66 3050ND23.8 12.0
Hexachlorobenzene ug/L R1506630-13042 43 3050ND32.8 21.2
Hexachlorocyclopentadiene ug/L R1504910-15023 71 3050ND24.5 11.6
Hexachloroethane ug/L R1505610-13028 66 3050ND27.8 14.0
Indeno(1,2,3-cd)pyrene ug/L 50 79 40-13075 5 3050ND39.4 37.4
Isophorone ug/L M1,R1506130-13029 70 3050ND30.4 14.6
N-Nitroso-di-n-propylamine ug/L M1,R1506130-13029 69 3050ND30.4 14.7
N-Nitrosodimethylamine ug/L R1505110-13028 60 3050ND25.6 13.9
N-Nitrosodiphenylamine ug/L R1507130-13044 47 3050ND35.6 22.1
Naphthalene ug/L R1505820-13030 63 3050ND29.1 15.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468428
BOU-014
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2827202MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92468428001
2827203
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrobenzene ug/L R1506220-13031 65 3050ND30.8 15.7
Pentachlorophenol ug/L 100 75 10-14063 18 30100ND75.3 63.1
Phenanthrene ug/L R1507150-13050 36 3050ND35.6 24.8
Phenol ug/L R1503710-13021 58 3050ND18.7 10.3
Pyrene ug/L 50 73 50-13070 4 3050ND36.4 34.9
2,4,6-Tribromophenol (S)%83 10-13754
2-Fluorobiphenyl (S)%62 13-13032
2-Fluorophenol (S)%49 10-13028
Nitrobenzene-d5 (S)%67 13-13036
Phenol-d6 (S)%35 10-13019
Terphenyl-d14 (S)%68 25-13068
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92468428
BOU-014
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 49
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92468428
BOU-014
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92468428001 1440142 1440142TMW-1 3015 EPA 6020B
92468428002 1440142 1440142TMW-2 3015 EPA 6020B
92468428003 1440142 1440142TMW-3 3015 EPA 6020B
92468428004 1440142 1440142TMW-4 3015 EPA 6020B
92468428005 1440142 1440142TMW-DUP 3015 EPA 6020B
92468428001 1440072 1440072TMW-1 7470A EPA 7470A
92468428002 1440072 1440072TMW-2 7470A EPA 7470A
92468428003 1440072 1440072TMW-3 7470A EPA 7470A
92468428004 1440072 1440072TMW-4 7470A EPA 7470A
92468428005 1440072 1440072TMW-DUP 7470A EPA 7470A
92468428001 529318 529529TMW-1 EPA 3510C EPA 8270E
92468428002 529318 529529TMW-2 EPA 3510C EPA 8270E
92468428003 529318 529529TMW-3 EPA 3510C EPA 8270E
92468428004 529318 529529TMW-4 EPA 3510C EPA 8270E
92468428005 529318 529529TMW-DUP EPA 3510C EPA 8270E
92468428001 529282TMW-1 EPA 8260D
92468428002 529282TMW-2 EPA 8260D
92468428003 529282TMW-3 EPA 8260D
92468428004 529831TMW-4 EPA 8260D
92468428005 529282TMW-DUP EPA 8260D
92468428006 529282TBEPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2020 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 49
Page 47 of 49
Page 48 of 49
Page 49 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 18, 2020
Ralph McGee
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
Project Location: Charlotte, NC
Client Job Number:
Project Number: BOU-014
Laboratory Work Order Number: 20C0604
Enclosed are results of analyses for samples received by the laboratory on March 10, 2020. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/18/2020Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
ATTN: Ralph McGee
BOU-014
20C0604
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
BOU-014
SGP-1 20C0604-01 Soil Gas -
EPA TO-15
SGP-2 20C0604-02 Soil Gas -
EPA TO-15
SGP-3 20C0604-03 Soil Gas -
EPA TO-15
SGP-4 20C0604-04 Soil Gas -
EPA TO-15
SGP-5 20C0604-05 Soil Gas -
EPA TO-15
SGP-6 20C0604-06 Soil Gas -
EPA TO-15
SGP-7 20C0604-07 Soil Gas -
EPA TO-15
SG-DUP 20C0604-08 Soil Gas -
EPA TO-15
Page 2 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
20C0604-05[SGP-5]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
1,2,4-Trichlorobenzene, Benzyl chloride, Hexachlorobutadiene, Naphthalene
20C0604-01[SGP-1], 20C0604-02[SGP-2], 20C0604-03[SGP-3], 20C0604-04[SGP-4], 20C0604-05[SGP-5], 20C0604-06[SGP-6], 20C0604-07[SGP-7],
20C0604-08[SG-DUP], B254524-BLK1, B254524-BS1, S046722-CCV1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 3 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-1
Sample ID: 20C0604-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -9.6
Sampled: 3/5/2020 10:01
Canister ID: 2248
Flow Controller ID: 4116
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 3/18/20 0:25 BRFND4192.8 6.6
Benzene 0.37 0.20 3/18/20 0:25 BRF1.2 40.640.082 0.26
Benzyl chloride ND 0.20 3/18/20 0:25 BRFV-05 ND 41.00.052 0.27
Bromodichloromethane ND 0.20 3/18/20 0:25 BRFND41.30.074 0.49
Bromoform ND 0.20 3/18/20 0:25 BRFND42.10.090 0.93
Bromomethane ND 0.40 3/18/20 0:25 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 3/18/20 0:25 BRFND40.440.15 0.32
2-Butanone (MEK)3.0 8.0 3/18/20 0:25 BRFJ8.7 4240.37 1.1
Carbon Disulfide ND 2.0 3/18/20 0:25 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/18/20 0:25 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/18/20 0:25 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/18/20 0:25 BRFND40.530.20 0.52
Chloroform 0.13 0.20 3/18/20 0:25 BRFJ0.64 40.980.074 0.36
Chloromethane ND 0.40 3/18/20 0:25 BRFND40.830.14 0.28
Cyclohexane 1.9 0.20 3/18/20 0:25 BRF6.5 40.690.14 0.49
Dibromochloromethane ND 0.20 3/18/20 0:25 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/18/20 0:25 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/18/20 0:25 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/18/20 0:25 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/18/20 0:25 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/18/20 0:25 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/18/20 0:25 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/18/20 0:25 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/18/20 0:25 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/18/20 0:25 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/18/20 0:25 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/18/20 0:25 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/18/20 0:25 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/18/20 0:25 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/18/20 0:25 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/18/20 0:25 BRFND47.21.3 4.6
Ethanol 95 8.0 3/18/20 0:25 BRF180 4153.6 6.7
Ethyl Acetate ND 0.20 3/18/20 0:25 BRFND40.720.15 0.54
Ethylbenzene 0.62 0.20 3/18/20 0:25 BRF2.7 40.870.12 0.50
4-Ethyltoluene 0.23 0.20 3/18/20 0:25 BRF1.1 40.980.12 0.60
Heptane 9.9 0.20 3/18/20 0:25 BRF41 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/18/20 0:25 BRFV-05 ND 42.10.092 0.98
Hexane 1.3 8.0 3/18/20 0:25 BRFJ4.7 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/18/20 0:25 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/18/20 0:25 BRFND4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/18/20 0:25 BRFND40.720.10 0.36
Methylene Chloride 1.1 2.0 3/18/20 0:25 BRFJ3.7 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/18/20 0:25 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/18/20 0:25 BRFV-05 ND 41.00.15 0.80
Propene ND 8.0 3/18/20 0:25 BRFND4140.37 0.64
Styrene ND 0.20 3/18/20 0:25 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/18/20 0:25 BRFND41.40.089 0.61
Page 4 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-1
Sample ID: 20C0604-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -9.6
Sampled: 3/5/2020 10:01
Canister ID: 2248
Flow Controller ID: 4116
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.26 0.20 3/18/20 0:25 BRF1.8 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/18/20 0:25 BRFND40.590.20 0.59
Toluene 4.2 0.20 3/18/20 0:25 BRF16 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/18/20 0:25 BRFV-05 ND 41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/18/20 0:25 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/18/20 0:25 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/18/20 0:25 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)ND 0.80 3/18/20 0:25 BRFND44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/18/20 0:25 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene 0.67 0.20 3/18/20 0:25 BRF3.3 40.980.13 0.63
1,3,5-Trimethylbenzene 0.21 0.20 3/18/20 0:25 BRF1.0 40.980.13 0.62
Vinyl Acetate ND 4.0 3/18/20 0:25 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 3/18/20 0:25 BRFND40.510.13 0.32
m&p-Xylene 2.2 0.40 3/18/20 0:25 BRF9.7 41.70.23 1.00
o-Xylene 0.70 0.20 3/18/20 0:25 BRF3.0 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)97.5 3/18/20 0:2570-130
Page 5 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-2
Sample ID: 20C0604-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.5
Sampled: 3/5/2020 11:08
Canister ID: 2321
Flow Controller ID: 4311
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 27 8.0 3/18/20 1:06 BRF63 4192.8 6.6
Benzene 0.98 0.20 3/18/20 1:06 BRF3.1 40.640.082 0.26
Benzyl chloride ND 0.20 3/18/20 1:06 BRFV-05 ND 41.00.052 0.27
Bromodichloromethane ND 0.20 3/18/20 1:06 BRFND41.30.074 0.49
Bromoform ND 0.20 3/18/20 1:06 BRFND42.10.090 0.93
Bromomethane ND 0.40 3/18/20 1:06 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 3/18/20 1:06 BRFND40.440.15 0.32
2-Butanone (MEK)2.1 8.0 3/18/20 1:06 BRFJ6.1 4240.37 1.1
Carbon Disulfide ND 2.0 3/18/20 1:06 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/18/20 1:06 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/18/20 1:06 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/18/20 1:06 BRFND40.530.20 0.52
Chloroform 0.21 0.20 3/18/20 1:06 BRF1.0 40.980.074 0.36
Chloromethane ND 0.40 3/18/20 1:06 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/18/20 1:06 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/18/20 1:06 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/18/20 1:06 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/18/20 1:06 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/18/20 1:06 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/18/20 1:06 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.36 0.20 3/18/20 1:06 BRF1.8 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/18/20 1:06 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/18/20 1:06 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/18/20 1:06 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/18/20 1:06 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/18/20 1:06 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/18/20 1:06 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/18/20 1:06 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/18/20 1:06 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/18/20 1:06 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/18/20 1:06 BRFND47.21.3 4.6
Ethanol 31 8.0 3/18/20 1:06 BRF59 4153.6 6.7
Ethyl Acetate ND 0.20 3/18/20 1:06 BRFND40.720.15 0.54
Ethylbenzene 1.6 0.20 3/18/20 1:06 BRF7.0 40.870.12 0.50
4-Ethyltoluene ND 0.20 3/18/20 1:06 BRFND40.980.12 0.60
Heptane 16 0.20 3/18/20 1:06 BRF67 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/18/20 1:06 BRFV-05 ND 42.10.092 0.98
Hexane ND 8.0 3/18/20 1:06 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/18/20 1:06 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/18/20 1:06 BRFND4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/18/20 1:06 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 3/18/20 1:06 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/18/20 1:06 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/18/20 1:06 BRFV-05 ND 41.00.15 0.80
Propene ND 8.0 3/18/20 1:06 BRFND4140.37 0.64
Styrene ND 0.20 3/18/20 1:06 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/18/20 1:06 BRFND41.40.089 0.61
Page 6 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-2
Sample ID: 20C0604-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.5
Sampled: 3/5/2020 11:08
Canister ID: 2321
Flow Controller ID: 4311
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.57 0.20 3/18/20 1:06 BRF3.9 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/18/20 1:06 BRFND40.590.20 0.59
Toluene 12 0.20 3/18/20 1:06 BRF47 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/18/20 1:06 BRFV-05 ND 41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/18/20 1:06 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/18/20 1:06 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/18/20 1:06 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.20 0.80 3/18/20 1:06 BRFJ1.1 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/18/20 1:06 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene 1.3 0.20 3/18/20 1:06 BRF6.6 40.980.13 0.63
1,3,5-Trimethylbenzene 0.38 0.20 3/18/20 1:06 BRF1.9 40.980.13 0.62
Vinyl Acetate ND 4.0 3/18/20 1:06 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 3/18/20 1:06 BRFND40.510.13 0.32
m&p-Xylene 6.0 0.40 3/18/20 1:06 BRF26 41.70.23 1.00
o-Xylene 1.9 0.20 3/18/20 1:06 BRF8.4 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)96.8 3/18/20 1:0670-130
Page 7 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-3
Sample ID: 20C0604-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -25
Final Vacuum(in Hg): -11.5
Receipt Vacuum(in Hg): -12.1
Sampled: 3/5/2020 14:20
Canister ID: 2325
Flow Controller ID: 4158
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 13 8.0 3/18/20 1:47 BRF31 4192.8 6.6
Benzene 0.83 0.20 3/18/20 1:47 BRF2.7 40.640.082 0.26
Benzyl chloride ND 0.20 3/18/20 1:47 BRFV-05 ND 41.00.052 0.27
Bromodichloromethane ND 0.20 3/18/20 1:47 BRFND41.30.074 0.49
Bromoform ND 0.20 3/18/20 1:47 BRFND42.10.090 0.93
Bromomethane ND 0.40 3/18/20 1:47 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 3/18/20 1:47 BRFND40.440.15 0.32
2-Butanone (MEK)1.8 8.0 3/18/20 1:47 BRFJ5.4 4240.37 1.1
Carbon Disulfide 2.3 2.0 3/18/20 1:47 BRF7.1 46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/18/20 1:47 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/18/20 1:47 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/18/20 1:47 BRFND40.530.20 0.52
Chloroform ND 0.20 3/18/20 1:47 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/18/20 1:47 BRFND40.830.14 0.28
Cyclohexane 1.7 0.20 3/18/20 1:47 BRF5.8 40.690.14 0.49
Dibromochloromethane ND 0.20 3/18/20 1:47 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/18/20 1:47 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/18/20 1:47 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/18/20 1:47 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/18/20 1:47 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.33 0.20 3/18/20 1:47 BRF1.6 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/18/20 1:47 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/18/20 1:47 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/18/20 1:47 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/18/20 1:47 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/18/20 1:47 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/18/20 1:47 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/18/20 1:47 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/18/20 1:47 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/18/20 1:47 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/18/20 1:47 BRFND47.21.3 4.6
Ethanol 30 8.0 3/18/20 1:47 BRF57 4153.6 6.7
Ethyl Acetate ND 0.20 3/18/20 1:47 BRFND40.720.15 0.54
Ethylbenzene 2.3 0.20 3/18/20 1:47 BRF9.9 40.870.12 0.50
4-Ethyltoluene 13 0.20 3/18/20 1:47 BRF63 40.980.12 0.60
Heptane 19 0.20 3/18/20 1:47 BRF79 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/18/20 1:47 BRFV-05 ND 42.10.092 0.98
Hexane ND 8.0 3/18/20 1:47 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/18/20 1:47 BRFND40.820.12 0.48
Isopropanol 3.2 8.0 3/18/20 1:47 BRFJ8.0 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/18/20 1:47 BRFND40.720.10 0.36
Methylene Chloride 1.1 2.0 3/18/20 1:47 BRFJ4.0 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/18/20 1:47 BRFND40.820.10 0.43
Naphthalene 43 0.20 3/18/20 1:47 BRFV-05 220 41.00.15 0.80
Propene 2.8 8.0 3/18/20 1:47 BRFJ4.8 4140.37 0.64
Styrene ND 0.20 3/18/20 1:47 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/18/20 1:47 BRFND41.40.089 0.61
Page 8 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-3
Sample ID: 20C0604-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -25
Final Vacuum(in Hg): -11.5
Receipt Vacuum(in Hg): -12.1
Sampled: 3/5/2020 14:20
Canister ID: 2325
Flow Controller ID: 4158
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.30 0.20 3/18/20 1:47 BRF2.0 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/18/20 1:47 BRFND40.590.20 0.59
Toluene 14 0.20 3/18/20 1:47 BRF52 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/18/20 1:47 BRFV-05 ND 41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/18/20 1:47 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/18/20 1:47 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/18/20 1:47 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.20 0.80 3/18/20 1:47 BRFJ1.1 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/18/20 1:47 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene 73 0.20 3/18/20 1:47 BRF360 40.980.13 0.63
1,3,5-Trimethylbenzene 30 0.20 3/18/20 1:47 BRF150 40.980.13 0.62
Vinyl Acetate ND 4.0 3/18/20 1:47 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 3/18/20 1:47 BRFND40.510.13 0.32
m&p-Xylene 6.8 0.40 3/18/20 1:47 BRF29 41.70.23 1.00
o-Xylene 3.0 0.20 3/18/20 1:47 BRF13 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)97.8 3/18/20 1:4770-130
Page 9 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-4
Sample ID: 20C0604-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.5
Sampled: 3/9/2020 15:36
Canister ID: 2333
Flow Controller ID: 4154
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 11 8.0 3/18/20 2:28 BRF25 4192.8 6.6
Benzene 0.12 0.20 3/18/20 2:28 BRFJ0.37 40.640.082 0.26
Benzyl chloride ND 0.20 3/18/20 2:28 BRFV-05 ND 41.00.052 0.27
Bromodichloromethane ND 0.20 3/18/20 2:28 BRFND41.30.074 0.49
Bromoform ND 0.20 3/18/20 2:28 BRFND42.10.090 0.93
Bromomethane ND 0.40 3/18/20 2:28 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 3/18/20 2:28 BRFND40.440.15 0.32
2-Butanone (MEK)2.7 8.0 3/18/20 2:28 BRFJ8.0 4240.37 1.1
Carbon Disulfide ND 2.0 3/18/20 2:28 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/18/20 2:28 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/18/20 2:28 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/18/20 2:28 BRFND40.530.20 0.52
Chloroform ND 0.20 3/18/20 2:28 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/18/20 2:28 BRFND40.830.14 0.28
Cyclohexane 3.3 0.20 3/18/20 2:28 BRF11 40.690.14 0.49
Dibromochloromethane ND 0.20 3/18/20 2:28 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/18/20 2:28 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/18/20 2:28 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/18/20 2:28 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/18/20 2:28 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/18/20 2:28 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/18/20 2:28 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/18/20 2:28 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/18/20 2:28 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/18/20 2:28 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/18/20 2:28 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/18/20 2:28 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/18/20 2:28 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/18/20 2:28 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/18/20 2:28 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/18/20 2:28 BRFND47.21.3 4.6
Ethanol 73 8.0 3/18/20 2:28 BRF140 4153.6 6.7
Ethyl Acetate 19 0.20 3/18/20 2:28 BRF69 40.720.15 0.54
Ethylbenzene 0.34 0.20 3/18/20 2:28 BRF1.5 40.870.12 0.50
4-Ethyltoluene 0.50 0.20 3/18/20 2:28 BRF2.4 40.980.12 0.60
Heptane ND 0.20 3/18/20 2:28 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/18/20 2:28 BRFV-05 ND 42.10.092 0.98
Hexane ND 8.0 3/18/20 2:28 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/18/20 2:28 BRFND40.820.12 0.48
Isopropanol 5.8 8.0 3/18/20 2:28 BRFJ14 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/18/20 2:28 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 3/18/20 2:28 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)0.65 0.20 3/18/20 2:28 BRF2.7 40.820.10 0.43
Naphthalene 0.96 0.20 3/18/20 2:28 BRFV-05 5.1 41.00.15 0.80
Propene ND 8.0 3/18/20 2:28 BRFND4140.37 0.64
Styrene ND 0.20 3/18/20 2:28 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/18/20 2:28 BRFND41.40.089 0.61
Page 10 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-4
Sample ID: 20C0604-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.5
Sampled: 3/9/2020 15:36
Canister ID: 2333
Flow Controller ID: 4154
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 3/18/20 2:28 BRFND41.40.11 0.75
Tetrahydrofuran ND 0.20 3/18/20 2:28 BRFND40.590.20 0.59
Toluene 0.69 0.20 3/18/20 2:28 BRF2.6 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/18/20 2:28 BRFV-05 ND 41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/18/20 2:28 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/18/20 2:28 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/18/20 2:28 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.26 0.80 3/18/20 2:28 BRFJ1.5 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.29 0.80 3/18/20 2:28 BRFJ2.2 46.10.15 1.2
1,2,4-Trimethylbenzene 1.5 0.20 3/18/20 2:28 BRF7.5 40.980.13 0.63
1,3,5-Trimethylbenzene 1.2 0.20 3/18/20 2:28 BRF5.9 40.980.13 0.62
Vinyl Acetate ND 4.0 3/18/20 2:28 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 3/18/20 2:28 BRFND40.510.13 0.32
m&p-Xylene 0.98 0.40 3/18/20 2:28 BRF4.3 41.70.23 1.00
o-Xylene 0.49 0.20 3/18/20 2:28 BRF2.1 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)95.7 3/18/20 2:2870-130
Page 11 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-5
Sample ID: 20C0604-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -7
Receipt Vacuum(in Hg): -8.1
Sampled: 3/9/2020 15:05
Canister ID: 2322
Flow Controller ID: 4320
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
Sample Flags: RL-11
MDL MDL
Acetone ND 80 3/18/20 6:30 BRFND401902866
Benzene 9.6 2.0 3/18/20 6:30 BRF31 406.40.82 2.6
Benzyl chloride ND 2.0 3/18/20 6:30 BRFV-05 ND 40100.52 2.7
Bromodichloromethane ND 2.0 3/18/20 6:30 BRFND40130.74 4.9
Bromoform ND 2.0 3/18/20 6:30 BRFND40210.90 9.3
Bromomethane ND 4.0 3/18/20 6:30 BRFND40161.4 5.3
1,3-Butadiene ND 2.0 3/18/20 6:30 BRFND404.41.5 3.2
2-Butanone (MEK)ND 80 3/18/20 6:30 BRFND402403.7 11
Carbon Disulfide ND 20 3/18/20 6:30 BRFND40621.4 4.3
Carbon Tetrachloride ND 2.0 3/18/20 6:30 BRFND40130.65 4.1
Chlorobenzene ND 2.0 3/18/20 6:30 BRFND409.20.98 4.5
Chloroethane ND 2.0 3/18/20 6:30 BRFND405.32.0 5.2
Chloroform ND 2.0 3/18/20 6:30 BRFND409.80.74 3.6
Chloromethane ND 4.0 3/18/20 6:30 BRFND408.31.4 2.8
Cyclohexane 23 2.0 3/18/20 6:30 BRF79 406.91.4 4.9
Dibromochloromethane ND 2.0 3/18/20 6:30 BRFND40170.66 5.7
1,2-Dibromoethane (EDB)ND 2.0 3/18/20 6:30 BRFND40150.78 6.0
1,2-Dichlorobenzene ND 2.0 3/18/20 6:30 BRFND40120.96 5.8
1,3-Dichlorobenzene ND 2.0 3/18/20 6:30 BRFND40121.0 6.2
1,4-Dichlorobenzene ND 2.0 3/18/20 6:30 BRFND40121.2 7.3
Dichlorodifluoromethane (Freon 12)ND 2.0 3/18/20 6:30 BRFND409.90.87 4.3
1,1-Dichloroethane ND 2.0 3/18/20 6:30 BRFND408.10.61 2.5
1,2-Dichloroethane ND 2.0 3/18/20 6:30 BRFND408.10.76 3.1
1,1-Dichloroethylene ND 2.0 3/18/20 6:30 BRFND407.91.1 4.3
cis-1,2-Dichloroethylene ND 2.0 3/18/20 6:30 BRFND407.90.82 3.2
trans-1,2-Dichloroethylene ND 2.0 3/18/20 6:30 BRFND407.90.81 3.2
1,2-Dichloropropane ND 2.0 3/18/20 6:30 BRFND409.20.71 3.3
cis-1,3-Dichloropropene ND 2.0 3/18/20 6:30 BRFND409.10.70 3.2
trans-1,3-Dichloropropene ND 2.0 3/18/20 6:30 BRFND409.10.73 3.3
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 2.0 3/18/20 6:30 BRFND40141.1 7.9
1,4-Dioxane ND 20 3/18/20 6:30 BRFND40721346
Ethanol ND 80 3/18/20 6:30 BRFND401503667
Ethyl Acetate ND 2.0 3/18/20 6:30 BRFND407.21.5 5.4
Ethylbenzene 86 2.0 3/18/20 6:30 BRF370 408.71.2 5.0
4-Ethyltoluene 300 2.0 3/18/20 6:30 BRF1500 409.81.2 6.0
Heptane 56 2.0 3/18/20 6:30 BRF230 408.21.2 4.8
Hexachlorobutadiene ND 2.0 3/18/20 6:30 BRFV-05 ND 40210.92 9.8
Hexane ND 80 3/18/20 6:30 BRFND402803.5 12
2-Hexanone (MBK)ND 2.0 3/18/20 6:30 BRFND408.21.2 4.8
Isopropanol ND 80 3/18/20 6:30 BRFND402003.7 9.0
Methyl tert-Butyl Ether (MTBE)ND 2.0 3/18/20 6:30 BRFND407.21.0 3.6
Methylene Chloride ND 20 3/18/20 6:30 BRFND40692.4 8.4
4-Methyl-2-pentanone (MIBK)ND 2.0 3/18/20 6:30 BRFND408.21.0 4.3
Naphthalene ND 2.0 3/18/20 6:30 BRFV-05 ND 40101.5 8.0
Propene ND 80 3/18/20 6:30 BRFND401403.7 6.4
Styrene ND 2.0 3/18/20 6:30 BRFND408.51.2 5.3
1,1,2,2-Tetrachloroethane ND 2.0 3/18/20 6:30 BRFND40140.89 6.1
Page 12 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-5
Sample ID: 20C0604-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -7
Receipt Vacuum(in Hg): -8.1
Sampled: 3/9/2020 15:05
Canister ID: 2322
Flow Controller ID: 4320
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
Sample Flags: RL-11
MDL MDL
Tetrachloroethylene ND 2.0 3/18/20 6:30 BRFND40141.1 7.5
Tetrahydrofuran ND 2.0 3/18/20 6:30 BRFND405.92.0 5.9
Toluene 15 2.0 3/18/20 6:30 BRF55 407.51.0 3.9
1,2,4-Trichlorobenzene ND 2.0 3/18/20 6:30 BRFV-05 ND 40151.4 10
1,1,1-Trichloroethane ND 2.0 3/18/20 6:30 BRFND40110.75 4.1
1,1,2-Trichloroethane ND 2.0 3/18/20 6:30 BRFND40110.82 4.5
Trichloroethylene ND 2.0 3/18/20 6:30 BRFND40110.81 4.3
Trichlorofluoromethane (Freon 11)ND 8.0 3/18/20 6:30 BRFND40451.5 8.5
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 8.0 3/18/20 6:30 BRFND40611.5 12
1,2,4-Trimethylbenzene 860 2.0 3/18/20 6:30 BRF4200 409.81.3 6.3
1,3,5-Trimethylbenzene 760 2.0 3/18/20 6:30 BRF3700 409.81.3 6.2
Vinyl Acetate ND 40 3/18/20 6:30 BRFND401401.2 4.4
Vinyl Chloride ND 2.0 3/18/20 6:30 BRFND405.11.3 3.2
m&p-Xylene 110 4.0 3/18/20 6:30 BRF470 40172.3 10.0
o-Xylene 84 2.0 3/18/20 6:30 BRF360 408.71.2 5.4
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)98.9 3/18/20 6:3070-130
Page 13 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-6
Sample ID: 20C0604-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.8
Sampled: 3/9/2020 14:10
Canister ID: 2344
Flow Controller ID: 4355
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 3/18/20 3:09 BRFND4192.8 6.6
Benzene 1.3 0.20 3/18/20 3:09 BRF4.0 40.640.082 0.26
Benzyl chloride ND 0.20 3/18/20 3:09 BRFV-05 ND 41.00.052 0.27
Bromodichloromethane ND 0.20 3/18/20 3:09 BRFND41.30.074 0.49
Bromoform ND 0.20 3/18/20 3:09 BRFND42.10.090 0.93
Bromomethane ND 0.40 3/18/20 3:09 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 3/18/20 3:09 BRFND40.440.15 0.32
2-Butanone (MEK)1.1 8.0 3/18/20 3:09 BRFJ3.1 4240.37 1.1
Carbon Disulfide 36 2.0 3/18/20 3:09 BRF110 46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/18/20 3:09 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/18/20 3:09 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/18/20 3:09 BRFND40.530.20 0.52
Chloroform ND 0.20 3/18/20 3:09 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/18/20 3:09 BRFND40.830.14 0.28
Cyclohexane 3.6 0.20 3/18/20 3:09 BRF12 40.690.14 0.49
Dibromochloromethane ND 0.20 3/18/20 3:09 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/18/20 3:09 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/18/20 3:09 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/18/20 3:09 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/18/20 3:09 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/18/20 3:09 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/18/20 3:09 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/18/20 3:09 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/18/20 3:09 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/18/20 3:09 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/18/20 3:09 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/18/20 3:09 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/18/20 3:09 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/18/20 3:09 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/18/20 3:09 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/18/20 3:09 BRFND47.21.3 4.6
Ethanol 19 8.0 3/18/20 3:09 BRF35 4153.6 6.7
Ethyl Acetate ND 0.20 3/18/20 3:09 BRFND40.720.15 0.54
Ethylbenzene 1.3 0.20 3/18/20 3:09 BRF5.7 40.870.12 0.50
4-Ethyltoluene ND 0.20 3/18/20 3:09 BRFND40.980.12 0.60
Heptane 110 0.20 3/18/20 3:09 BRF460 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/18/20 3:09 BRFV-05 ND 42.10.092 0.98
Hexane 7.8 8.0 3/18/20 3:09 BRFJ27 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/18/20 3:09 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/18/20 3:09 BRFND4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/18/20 3:09 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 3/18/20 3:09 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/18/20 3:09 BRFND40.820.10 0.43
Naphthalene 0.16 0.20 3/18/20 3:09 BRFV-05, J 0.84 41.00.15 0.80
Propene 58 8.0 3/18/20 3:09 BRF100 4140.37 0.64
Styrene ND 0.20 3/18/20 3:09 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/18/20 3:09 BRFND41.40.089 0.61
Page 14 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-6
Sample ID: 20C0604-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.8
Sampled: 3/9/2020 14:10
Canister ID: 2344
Flow Controller ID: 4355
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 20 0.20 3/18/20 3:09 BRF140 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/18/20 3:09 BRFND40.590.20 0.59
Toluene 14 0.20 3/18/20 3:09 BRF53 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/18/20 3:09 BRFV-05 ND 41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/18/20 3:09 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/18/20 3:09 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/18/20 3:09 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)8.1 0.80 3/18/20 3:09 BRF46 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.42 0.80 3/18/20 3:09 BRFJ3.2 46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/18/20 3:09 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/18/20 3:09 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/18/20 3:09 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 3/18/20 3:09 BRFND40.510.13 0.32
m&p-Xylene 3.8 0.40 3/18/20 3:09 BRF17 41.70.23 1.00
o-Xylene 0.96 0.20 3/18/20 3:09 BRF4.2 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)95.3 3/18/20 3:0970-130
Page 15 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-7
Sample ID: 20C0604-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.5
Sampled: 3/5/2020 13:34
Canister ID: 2338
Flow Controller ID: 4311
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 10 8.0 3/18/20 4:30 BRF24 4192.8 6.6
Benzene 1.0 0.20 3/18/20 4:30 BRF3.3 40.640.082 0.26
Benzyl chloride ND 0.20 3/18/20 4:30 BRFV-05 ND 41.00.052 0.27
Bromodichloromethane ND 0.20 3/18/20 4:30 BRFND41.30.074 0.49
Bromoform ND 0.20 3/18/20 4:30 BRFND42.10.090 0.93
Bromomethane ND 0.40 3/18/20 4:30 BRFND41.60.14 0.53
1,3-Butadiene 4.3 0.20 3/18/20 4:30 BRF9.4 40.440.15 0.32
2-Butanone (MEK)1.3 8.0 3/18/20 4:30 BRFJ3.9 4240.37 1.1
Carbon Disulfide 2.4 2.0 3/18/20 4:30 BRF7.5 46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/18/20 4:30 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/18/20 4:30 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/18/20 4:30 BRFND40.530.20 0.52
Chloroform ND 0.20 3/18/20 4:30 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/18/20 4:30 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/18/20 4:30 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/18/20 4:30 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/18/20 4:30 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/18/20 4:30 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/18/20 4:30 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/18/20 4:30 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.34 0.20 3/18/20 4:30 BRF1.7 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/18/20 4:30 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/18/20 4:30 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/18/20 4:30 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/18/20 4:30 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/18/20 4:30 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/18/20 4:30 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/18/20 4:30 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/18/20 4:30 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/18/20 4:30 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/18/20 4:30 BRFND47.21.3 4.6
Ethanol 16 8.0 3/18/20 4:30 BRF30 4153.6 6.7
Ethyl Acetate ND 0.20 3/18/20 4:30 BRFND40.720.15 0.54
Ethylbenzene 1.1 0.20 3/18/20 4:30 BRF4.7 40.870.12 0.50
4-Ethyltoluene 0.27 0.20 3/18/20 4:30 BRF1.3 40.980.12 0.60
Heptane 20 0.20 3/18/20 4:30 BRF84 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/18/20 4:30 BRFV-05 ND 42.10.092 0.98
Hexane ND 8.0 3/18/20 4:30 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/18/20 4:30 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/18/20 4:30 BRFND4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/18/20 4:30 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 3/18/20 4:30 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/18/20 4:30 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/18/20 4:30 BRFV-05 ND 41.00.15 0.80
Propene 67 8.0 3/18/20 4:30 BRF110 4140.37 0.64
Styrene ND 0.20 3/18/20 4:30 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/18/20 4:30 BRFND41.40.089 0.61
Page 16 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SGP-7
Sample ID: 20C0604-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.5
Sampled: 3/5/2020 13:34
Canister ID: 2338
Flow Controller ID: 4311
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.26 0.20 3/18/20 4:30 BRF1.8 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/18/20 4:30 BRFND40.590.20 0.59
Toluene 9.2 0.20 3/18/20 4:30 BRF35 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/18/20 4:30 BRFV-05 ND 41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/18/20 4:30 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/18/20 4:30 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/18/20 4:30 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.38 0.80 3/18/20 4:30 BRFJ2.2 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/18/20 4:30 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene 0.93 0.20 3/18/20 4:30 BRF4.6 40.980.13 0.63
1,3,5-Trimethylbenzene 0.26 0.20 3/18/20 4:30 BRF1.3 40.980.13 0.62
Vinyl Acetate ND 4.0 3/18/20 4:30 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 3/18/20 4:30 BRFND40.510.13 0.32
m&p-Xylene 3.9 0.40 3/18/20 4:30 BRF17 41.70.23 1.00
o-Xylene 1.3 0.20 3/18/20 4:30 BRF5.7 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)96.6 3/18/20 4:3070-130
Page 17 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SG-DUP
Sample ID: 20C0604-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.7
Sampled: 3/5/2020 00:00
Canister ID: 2347
Flow Controller ID: 4117
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 10 8.0 3/18/20 5:50 BRF24 4192.8 6.6
Benzene 1.0 0.20 3/18/20 5:50 BRF3.3 40.640.082 0.26
Benzyl chloride ND 0.20 3/18/20 5:50 BRFV-05 ND 41.00.052 0.27
Bromodichloromethane ND 0.20 3/18/20 5:50 BRFND41.30.074 0.49
Bromoform ND 0.20 3/18/20 5:50 BRFND42.10.090 0.93
Bromomethane ND 0.40 3/18/20 5:50 BRFND41.60.14 0.53
1,3-Butadiene 4.2 0.20 3/18/20 5:50 BRF9.4 40.440.15 0.32
2-Butanone (MEK)1.3 8.0 3/18/20 5:50 BRFJ4.0 4240.37 1.1
Carbon Disulfide 2.4 2.0 3/18/20 5:50 BRF7.4 46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/18/20 5:50 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/18/20 5:50 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/18/20 5:50 BRFND40.530.20 0.52
Chloroform ND 0.20 3/18/20 5:50 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/18/20 5:50 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/18/20 5:50 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/18/20 5:50 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/18/20 5:50 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/18/20 5:50 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/18/20 5:50 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/18/20 5:50 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.36 0.20 3/18/20 5:50 BRF1.8 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/18/20 5:50 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/18/20 5:50 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/18/20 5:50 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/18/20 5:50 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/18/20 5:50 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/18/20 5:50 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/18/20 5:50 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/18/20 5:50 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/18/20 5:50 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/18/20 5:50 BRFND47.21.3 4.6
Ethanol 14 8.0 3/18/20 5:50 BRF26 4153.6 6.7
Ethyl Acetate ND 0.20 3/18/20 5:50 BRFND40.720.15 0.54
Ethylbenzene 1.1 0.20 3/18/20 5:50 BRF4.6 40.870.12 0.50
4-Ethyltoluene 0.26 0.20 3/18/20 5:50 BRF1.3 40.980.12 0.60
Heptane 20 0.20 3/18/20 5:50 BRF84 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/18/20 5:50 BRFV-05 ND 42.10.092 0.98
Hexane 2.4 8.0 3/18/20 5:50 BRFJ8.5 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/18/20 5:50 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/18/20 5:50 BRFND4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/18/20 5:50 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 3/18/20 5:50 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/18/20 5:50 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/18/20 5:50 BRFV-05 ND 41.00.15 0.80
Propene 65 8.0 3/18/20 5:50 BRF110 4140.37 0.64
Styrene ND 0.20 3/18/20 5:50 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/18/20 5:50 BRFND41.40.089 0.61
Page 18 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/10/2020
Work Order: 20C0604Sample Description/Location:
Field Sample #: SG-DUP
Sample ID: 20C0604-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.7
Sampled: 3/5/2020 00:00
Canister ID: 2347
Flow Controller ID: 4117
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.60 0.20 3/18/20 5:50 BRF4.1 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/18/20 5:50 BRFND40.590.20 0.59
Toluene 9.5 0.20 3/18/20 5:50 BRF36 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/18/20 5:50 BRFV-05 ND 41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/18/20 5:50 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/18/20 5:50 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/18/20 5:50 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.41 0.80 3/18/20 5:50 BRFJ2.3 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/18/20 5:50 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/18/20 5:50 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene 0.25 0.20 3/18/20 5:50 BRF1.2 40.980.13 0.62
Vinyl Acetate ND 4.0 3/18/20 5:50 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 3/18/20 5:50 BRFND40.510.13 0.32
m&p-Xylene 3.8 0.40 3/18/20 5:50 BRF17 41.70.23 1.00
o-Xylene 1.2 0.20 3/18/20 5:50 BRF5.4 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)97.2 3/18/20 5:5070-130
Page 19 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
20C0604-01 [SGP-1]B254524 2 1 N/A 1000 400 200 03/17/20
20C0604-02 [SGP-2]B254524 1.5 1 N/A 1000 400 150 03/17/20
20C0604-03 [SGP-3]B254524 2 1 N/A 1000 400 200 03/17/20
20C0604-04 [SGP-4]B254524 1.5 1 N/A 1000 400 150 03/17/20
20C0604-05 [SGP-5]B254524 1.5 1 N/A 1000 400 15 03/17/20
20C0604-06 [SGP-6]B254524 1.5 1 N/A 1000 400 150 03/17/20
20C0604-07 [SGP-7]B254524 1.5 1 N/A 1000 400 150 03/17/20
20C0604-08 [SG-DUP]B254524 1.5 1 N/A 1000 400 150 03/17/20
Page 20 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B254524 - TO-15 Prep
Blank (B254524-BLK1)Prepared & Analyzed: 03/17/20
0.80NDAcetone
0.020NDBenzene
0.020 V-05NDBenzyl chloride
0.020NDBromodichloromethane
0.020NDBromoform
0.020NDBromomethane
0.020ND1,3-Butadiene
0.80ND2-Butanone (MEK)
0.20NDCarbon Disulfide
0.020NDCarbon Tetrachloride
0.020NDChlorobenzene
0.020NDChloroethane
0.020NDChloroform
0.040NDChloromethane
0.020NDCyclohexane
0.020NDDibromochloromethane
0.020ND1,2-Dibromoethane (EDB)
0.020ND1,2-Dichlorobenzene
0.020ND1,3-Dichlorobenzene
0.020ND1,4-Dichlorobenzene
0.020NDDichlorodifluoromethane (Freon 12)
0.020ND1,1-Dichloroethane
0.020ND1,2-Dichloroethane
0.020ND1,1-Dichloroethylene
0.020NDcis-1,2-Dichloroethylene
0.020NDtrans-1,2-Dichloroethylene
0.020ND1,2-Dichloropropane
0.020NDcis-1,3-Dichloropropene
0.020NDtrans-1,3-Dichloropropene
0.020ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.20ND1,4-Dioxane
0.80NDEthanol
0.020NDEthyl Acetate
0.020NDEthylbenzene
0.020ND4-Ethyltoluene
0.020NDHeptane
0.020 V-05NDHexachlorobutadiene
0.80NDHexane
0.020ND2-Hexanone (MBK)
0.80NDIsopropanol
0.020NDMethyl tert-Butyl Ether (MTBE)
0.20NDMethylene Chloride
0.020ND4-Methyl-2-pentanone (MIBK)
0.020 V-05NDNaphthalene
0.80NDPropene
0.020NDStyrene
Page 21 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B254524 - TO-15 Prep
Blank (B254524-BLK1)Prepared & Analyzed: 03/17/20
0.020ND1,1,2,2-Tetrachloroethane
0.020NDTetrachloroethylene
0.020NDTetrahydrofuran
0.020NDToluene
0.020 V-05ND1,2,4-Trichlorobenzene
0.020ND1,1,1-Trichloroethane
0.020ND1,1,2-Trichloroethane
0.020NDTrichloroethylene
0.080NDTrichlorofluoromethane (Freon 11)
0.080ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.020ND1,2,4-Trimethylbenzene
0.020ND1,3,5-Trimethylbenzene
0.40NDVinyl Acetate
0.020NDVinyl Chloride
0.040NDm&p-Xylene
0.020NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)95.77.66
LCS (B254524-BS1)Prepared & Analyzed: 03/17/20
5.00 70-1301206.00Acetone
5.00 70-13085.14.25Benzene
5.00 V-0570-13096.24.81Benzyl chloride
5.00 70-13083.24.16Bromodichloromethane
5.00 70-1301015.04Bromoform
5.00 70-1301035.16Bromomethane
5.00 70-13094.24.711,3-Butadiene
5.00 70-1301025.112-Butanone (MEK)
5.00 70-13097.54.87Carbon Disulfide
5.00 70-13082.94.14Carbon Tetrachloride
5.00 70-13090.64.53Chlorobenzene
5.00 70-13094.44.72Chloroethane
5.00 70-13092.74.64Chloroform
5.00 70-13091.54.58Chloromethane
5.00 70-13078.43.92Cyclohexane
5.00 70-13093.14.66Dibromochloromethane
5.00 70-13091.04.551,2-Dibromoethane (EDB)
5.00 70-13099.74.991,2-Dichlorobenzene
5.00 70-13099.04.951,3-Dichlorobenzene
5.00 70-13098.64.931,4-Dichlorobenzene
5.00 70-1301035.17Dichlorodifluoromethane (Freon 12)
5.00 70-13092.64.631,1-Dichloroethane
5.00 70-13086.44.321,2-Dichloroethane
5.00 70-13090.84.541,1-Dichloroethylene
5.00 70-13091.04.55cis-1,2-Dichloroethylene
5.00 70-13093.14.66trans-1,2-Dichloroethylene
5.00 70-13086.04.301,2-Dichloropropane
Page 22 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B254524 - TO-15 Prep
LCS (B254524-BS1)Prepared & Analyzed: 03/17/20
5.00 70-13080.14.00cis-1,3-Dichloropropene
5.00 70-13085.84.29trans-1,3-Dichloropropene
5.00 70-13096.14.811,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-1301025.121,4-Dioxane
5.00 70-1301296.45Ethanol
5.00 70-13088.94.44Ethyl Acetate
5.00 70-13089.44.47Ethylbenzene
5.00 70-13095.74.794-Ethyltoluene
5.00 70-13082.34.11Heptane
5.00 V-0570-13088.54.42Hexachlorobutadiene
5.00 70-1301075.35Hexane
5.00 70-13099.54.982-Hexanone (MBK)
5.00 70-13099.54.98Isopropanol
5.00 70-13089.74.48Methyl tert-Butyl Ether (MTBE)
5.00 70-13095.24.76Methylene Chloride
5.00 70-13090.54.534-Methyl-2-pentanone (MIBK)
5.00 V-0570-1301015.07Naphthalene
5.00 70-1301025.12Propene
5.00 70-13095.54.77Styrene
5.00 70-13091.14.561,1,2,2-Tetrachloroethane
5.00 70-13089.84.49Tetrachloroethylene
5.00 70-1301095.43Tetrahydrofuran
5.00 70-13090.64.53Toluene
5.00 V-0570-1301025.121,2,4-Trichlorobenzene
5.00 70-13076.33.821,1,1-Trichloroethane
5.00 70-13090.74.541,1,2-Trichloroethane
5.00 70-13086.14.30Trichloroethylene
5.00 70-1301055.23Trichlorofluoromethane (Freon 11)
5.00 70-13094.14.701,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-13095.34.761,2,4-Trimethylbenzene
5.00 70-13094.34.711,3,5-Trimethylbenzene
5.00 70-1301095.45Vinyl Acetate
5.00 70-13095.34.77Vinyl Chloride
10.0 70-13091.59.15m&p-Xylene
5.00 70-13092.14.60o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)98.27.85
Page 23 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Elevated reporting limit due to high concentration of target compounds.RL-11
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
ANALYST
Rebecca FaustRLF
PDF Management StationSTATION
Kerry K. McGeeKKM
Brittany R. FiskBRF
Page 24 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S041952-ICV1 )Lab File ID: G1930117.D Analyzed: 10/28/19 23:11
Bromochloromethane (1)392547 8.54 392415 8.54 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)984411 10.314 974698 10.32 60 - 140101 -0.0060 +/-0.50
Chlorobenzene-d5 (1)925298 14.691 911790 14.691 60 - 140101 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S046722-CCV1 )Lab File ID: G2007704.D Analyzed: 03/17/20 13:20
Bromochloromethane (1)287120 8.527 392415 8.54 60 - 14073 -0.0130 +/-0.50
1,4-Difluorobenzene (1)758595 10.308 974698 10.32 60 - 14078 -0.0120 +/-0.50
Chlorobenzene-d5 (1)682826 14.685 911790 14.691 60 - 14075 -0.0060 +/-0.50
LCS (B254524-BS1 )Lab File ID: G2007705.D Analyzed: 03/17/20 14:00
Bromochloromethane (1)285371 8.527 287120 8.527 60 - 14099 0.0000 +/-0.50
1,4-Difluorobenzene (1)756403 10.308 758595 10.308 60 - 140100 0.0000 +/-0.50
Chlorobenzene-d5 (1)684612 14.685 682826 14.685 60 - 140100 0.0000 +/-0.50
Blank (B254524-BLK1 )Lab File ID: G2007710.D Analyzed: 03/17/20 17:32
Bromochloromethane (1)280972 8.533 287120 8.527 60 - 14098 0.0060 +/-0.50
1,4-Difluorobenzene (1)724475 10.307 758595 10.308 60 - 14096 -0.0010 +/-0.50
Chlorobenzene-d5 (1)651372 14.685 682826 14.685 60 - 14095 0.0000 +/-0.50
SGP-1 (20C0604-01 )Lab File ID: G2007720.D Analyzed: 03/18/20 00:25
Bromochloromethane (1)290616 8.527 287120 8.527 60 - 140101 0.0000 +/-0.50
1,4-Difluorobenzene (1)741509 10.308 758595 10.308 60 - 14098 0.0000 +/-0.50
Chlorobenzene-d5 (1)678723 14.685 682826 14.685 60 - 14099 0.0000 +/-0.50
SGP-2 (20C0604-02 )Lab File ID: G2007721.D Analyzed: 03/18/20 01:06
Bromochloromethane (1)289479 8.528 287120 8.527 60 - 140101 0.0010 +/-0.50
1,4-Difluorobenzene (1)738236 10.308 758595 10.308 60 - 14097 0.0000 +/-0.50
Chlorobenzene-d5 (1)674782 14.685 682826 14.685 60 - 14099 0.0000 +/-0.50
SGP-3 (20C0604-03 )Lab File ID: G2007722.D Analyzed: 03/18/20 01:47
Bromochloromethane (1)287556 8.527 287120 8.527 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)737034 10.308 758595 10.308 60 - 14097 0.0000 +/-0.50
Chlorobenzene-d5 (1)677522 14.685 682826 14.685 60 - 14099 0.0000 +/-0.50
SGP-4 (20C0604-04 )Lab File ID: G2007723.D Analyzed: 03/18/20 02:28
Bromochloromethane (1)306452 8.527 287120 8.527 60 - 140107 0.0000 +/-0.50
1,4-Difluorobenzene (1)785558 10.308 758595 10.308 60 - 140104 0.0000 +/-0.50
Chlorobenzene-d5 (1)705921 14.685 682826 14.685 60 - 140103 0.0000 +/-0.50
Page 25 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SGP-6 (20C0604-06 )Lab File ID: G2007724.D Analyzed: 03/18/20 03:09
Bromochloromethane (1)294235 8.527 287120 8.527 60 - 140102 0.0000 +/-0.50
1,4-Difluorobenzene (1)764873 10.308 758595 10.308 60 - 140101 0.0000 +/-0.50
Chlorobenzene-d5 (1)703656 14.685 682826 14.685 60 - 140103 0.0000 +/-0.50
SGP-7 (20C0604-07 )Lab File ID: G2007726.D Analyzed: 03/18/20 04:30
Bromochloromethane (1)287257 8.527 287120 8.527 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)745115 10.307 758595 10.308 60 - 14098 -0.0010 +/-0.50
Chlorobenzene-d5 (1)678940 14.685 682826 14.685 60 - 14099 0.0000 +/-0.50
SG-DUP (20C0604-08 )Lab File ID: G2007728.D Analyzed: 03/18/20 05:50
Bromochloromethane (1)290929 8.527 287120 8.527 60 - 140101 0.0000 +/-0.50
1,4-Difluorobenzene (1)747409 10.307 758595 10.308 60 - 14099 -0.0010 +/-0.50
Chlorobenzene-d5 (1)685683 14.685 682826 14.685 60 - 140100 0.0000 +/-0.50
SGP-5 (20C0604-05 )Lab File ID: G2007729.D Analyzed: 03/18/20 06:30
Bromochloromethane (1)283864 8.533 287120 8.527 60 - 14099 0.0060 +/-0.50
1,4-Difluorobenzene (1)739231 10.307 758595 10.308 60 - 14097 -0.0010 +/-0.50
Chlorobenzene-d5 (1)695045 14.685 682826 14.685 60 - 140102 0.0000 +/-0.50
Page 26 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S046722-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.8873502A -1.8 304.91 0.90382385.00Acetone
0.7774014A -23.3 303.83 1.0140395.00Benzene
0.6755525A -38.5 *303.08 1.0980465.00Benzyl chloride
0.5405382A -25.4 303.73 0.72484135.00Bromodichloromethane
0.399092A -16.8 304.16 0.47983765.00Bromoform
0.5168069A -10.2 304.49 0.57547255.00Bromomethane
0.4453831A -14.8 304.26 0.52281445.001,3-Butadiene
1.289785A -12.0 304.40 1.46565.002-Butanone (MEK)
1.838061A -13.9 304.30 2.1356815.00Carbon Disulfide
0.4117043A -23.8 303.81 0.54013625.00Carbon Tetrachloride
0.6964093A -21.7 303.91 0.88954195.00Chlorobenzene
0.2930956A -14.7 304.26 0.34361455.00Chloroethane
1.321187A -17.1 304.15 1.5933635.00Chloroform
0.5645026A -13.7 304.32 0.65400955.00Chloromethane
0.3182853A -26.9 303.66 0.43525775.00Cyclohexane
0.4854297A -18.3 304.09 0.59391695.00Dibromochloromethane
0.4853477A -20.5 303.98 0.61055525.001,2-Dibromoethane (EDB)
0.4768864A -28.6 303.57 0.66778785.001,2-Dichlorobenzene
0.5390094A -25.0 303.75 0.71854575.001,3-Dichlorobenzene
0.5383134A -25.8 303.71 0.72554295.001,4-Dichlorobenzene
1.506102A -5.9 304.70 1.6007995.00Dichlorodifluoromethane (Freon 12)
1.159081A -18.6 304.07 1.4236055.001,1-Dichloroethane
0.785985A -23.6 303.82 1.0281225.001,2-Dichloroethane
1.012065A -16.3 304.18 1.2096035.001,1-Dichloroethylene
0.8524101A -18.1 304.09 1.041165.00cis-1,2-Dichloroethylene
0.8901755A -16.6 304.17 1.0672335.00trans-1,2-Dichloroethylene
0.2894657A -22.5 303.87 0.37358195.001,2-Dichloropropane
0.4390032A -26.7 303.66 0.5988965.00cis-1,3-Dichloropropene
0.3603694A -27.2 303.64 0.49517085.00trans-1,3-Dichloropropene
1.505857A -6.1 304.70 1.6034585.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.1474853A -17.5 304.13 0.17866815.001,4-Dioxane
0.1687378A 26.5 306.33 0.13334985.00Ethanol
0.2424909A -9.8 304.51 0.26886115.00Ethyl Acetate
1.219834A -21.4 303.93 1.5517955.00Ethylbenzene
1.185956A -21.1 303.94 1.5038535.004-Ethyltoluene
0.2422057A -23.7 303.82 0.31737615.00Heptane
0.2367947A -39.4 *303.03 0.39086215.00Hexachlorobutadiene
0.7449652L -2.2 304.89 0.91474595.00Hexane
Page 27 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S046722-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.6095374A -11.7 304.42 0.69035625.002-Hexanone (MBK)
1.018963A 3.3 305.17 0.98624535.00Isopropanol
1.675408A -16.5 304.18 2.0052845.00Methyl tert-Butyl Ether (MTBE)
0.7356701A -14.1 304.30 0.85608435.00Methylene Chloride
0.6005924A -18.2 304.09 0.73396925.004-Methyl-2-pentanone (MIBK)
0.6967257A -43.6 *302.82 1.2347615.00Naphthalene
0.5579716A -5.1 304.74 0.58820095.00Propene
0.6588501A -20.8 303.96 0.83144665.00Styrene
0.713585A -25.6 303.72 0.9588535.001,1,2,2-Tetrachloroethane
0.358482A -19.3 304.03 0.44433235.00Tetrachloroethylene
0.2656227A -10.7 304.46 0.29745935.00Tetrahydrofuran
0.9739453A -19.4 304.03 1.2079475.00Toluene
0.276034A -40.7 *302.96 0.46579535.001,2,4-Trichlorobenzene
0.4566632A -24.8 303.76 0.60760325.001,1,1-Trichloroethane
0.3301784A -20.3 303.99 0.41421065.001,1,2-Trichloroethane
0.317391A -23.0 303.85 0.41236235.00Trichloroethylene
1.240178A -5.0 304.75 1.3059775.00Trichlorofluoromethane (Freon 11)
1.237269A -12.6 304.37 1.4163125.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.925195A -22.7 303.87 1.1962765.001,2,4-Trimethylbenzene
0.9671829A -20.6 303.97 1.2174955.001,3,5-Trimethylbenzene
1.73956A -13.1 304.35 2.0014535.00Vinyl Acetate
0.6137977A -13.2 304.34 0.70697865.00Vinyl Chloride
0.9343112A -20.5 307.95 1.1750310.0m&p-Xylene
0.952969A -20.6 303.97 1.2006045.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 28 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 29 of 33
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2021
LAO00112Rhode Island Department of HealthRI 12/30/2020
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
Page 30 of 33
Page 31 of 33
Page 32 of 33
Page 33 of 33

Appendix D

Groundwater Sampling Forms
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSBOU-014Blythe Isenhour3/4/2016.50 7.70HHM SMSPoly/Silicone 14.00Overcast,60s Beganpurgingat 917:2517:3017:3517:4017:4517:5017:559.899.939.949.949.959.959.96500 mL1000 mL1500 mL2000 mL2500 mL3000 mL3500 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min5.214.414.384.404.404.384.3817.417.117.117.217.217.217.284.785.485.584.785.385.785.85.305.375.325.335.315.335.33176.6153.5150.3151.5152.9151.2150.715.2020.2017.2012.2015.7012.2010.40YSI Pro, Alexis Peristaltic Pump, Hach 2100Q Turbidimetercourier3-40 mL amber vial w/HCL, 2-100 mL amberglass unpreserved, 1-250 mLplastic w/HNO3PeristalticPVC1-inch18:00Pace AnalyticalTMW-1
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSBOU-014Blythe Isenhour3/4/2024.00 15.10HHM SMSPoly/Silicone 20.00Overcast,60s Beganpurgingat 9:5010:3510:4510:5511:0511:1511:2011:2515.8615.8715.8415.8115.8415.8615.86750 mL1500 mL1500 mL1500 mL1500 mL750 mL750 mL150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min5.825.705.885.875.845.935.9017.718.017.718.018.018.118.0104.7105.5104.6104.7104.7103.6104.14.794.734.724.674.614.584.54148.7155.1154.5156.7157.6158.4161.1174.0067.8064.5059.2014.8014.008.68YSI Pro, Alexis Peristaltic Pump, Hach 2100Q Turbidimetercourier3-40 mL amber vial w/HCL, 2-100 mL amberglass unpreserved, 1-250 mLplastic w/HNO3PeristalticPVC1-inch11:25Pace AnalyticalTMW-2
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSBOU-014Blythe Isenhour3/4/2024.00 15.10HHM SMSPoly/Silicone 20.00Overcast,60s Beganpurgingat12:0313:2513:3010:4013:4513:5514:0514:1514:2014:2515.9015.9015.9015.9115.9815.9816.0216.0116.02500 mL500 mL1000 mL500 mL1000 mL1000 mL1000 mL1000 mL1000 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min1.641.621.571.431.371.351.381.391.3816.316.316.416.416.516.416.516.416.456.458.859.056.959.857.058.758.558.24.464.534.584.554.654.564.574.574.5697.296.397.997.391.897.5103.4107.4102.718.3038.1032.5035.4052.4013.3018.2013.2010.20YSI Pro, Alexis Peristaltic Pump, Hach 2100Q Turbidimetercourier3-40 mL amber vial w/HCL, 2-100 mL amberglass unpreserved, 1-250 mLplastic w/HNO3PeristalticPVC1-inch14:30Pace AnalyticalTMW-3
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSBOU-014Blythe Isenhour3/4/2013.00 5.61HHM SMSPoly/Silicone 9.00Overcast,60s Beganpurgingat 14:5816:2516:3516:4016:4516:5016:5517:007.777.837.857.877.857.857.852000 mL1000 mL500 mL500 mL500 mL500 mL500 mL100mL/min100mL/min100mL/min100mL/min100mL/min100mL/min100mL/min1.722.021.781.721.751.741.7314.714.714.714.614.514.514.535.836.035.935.935.835.835.74.614.554.574.574.564.574.56168.2175.9177.0178.0176.7175.2175.750.1077.5065.5040.2025.1011.5010.50YSI Pro, Alexis Peristaltic Pump, Hach 2100Q Turbidimetercourier3-40 mL amber vial w/HCL, 2-100 mL amberglass unpreserved, 1-250 mLplastic w/HNO3PeristalticPVC1-inch17:05Pace AnalyticalTMW-4

Appendix E

DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Haley Martin, PG
Ralph McGee, PG
Site Wide Soil Gas - Hypothetical Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Blythe Isenhour
4920 Old Pineville Road, Charlotte, Mecklenburg County
Division of Waste Management - Brownfields Program
23067-19-060
December 2019
November 2019 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: 23067-19-060
Exposure Unit ID: Site Wide Soil Gas - Hypothetical Worst Case
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration to Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: 23067-19-060
Exposure Unit ID: Site Wide Soil Gas - Hypothetical Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: 23067-19-060
Exposure Unit ID: Site Wide Soil Gas - Hypothetical Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use* NC NC NC
Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 9.6E-05 6.5E+00 YES
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: December 2019Basis: November 2019 EPA RSL TableSite ID: 23067-19-060Exposure Unit ID: Site Wide Soil Gas - Hypothetical Worst CaseDescription of Exposure Point Concentration Selection:Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.Exposure Point Concentration (ug/m3)Notes: CAS Number ChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion63 67-64-1 Acetoneug/m331 71-43-2 Benzeneug/m39.4 106-99-0 Butadiene, 1,3-ug/m3110 75-15-0 Carbon Disulfideug/m31 67-66-3 Chloroformug/m379 110-82-7 Cyclohexaneug/m31.8 75-71-8 Dichlorodifluoromethaneug/m369 141-78-6 Ethyl Acetateug/m3370 100-41-4 Ethylbenzeneug/m3460 142-82-5 Heptane, N-ug/m327 110-54-3 Hexane, N-ug/m314 67-63-0 Isopropanolug/m38.7 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m32.7 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m34 75-09-2 Methylene Chlorideug/m3220 91-20-3 ~Naphthaleneug/m3140 127-18-4 Tetrachloroethyleneug/m355 108-88-3 Tolueneug/m33.2 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m34200 95-63-6 Trimethylbenzene, 1,2,4-ug/m33700 108-67-8 Trimethylbenzene, 1,3,5-ug/m3470 108-38-3 Xylene, m-ug/m3360 95-47-6 Xylene, o-ug/m3Input Form 2DSoil Gas Exposure Point Concentration TableNorth Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: 23067-19-060
Exposure Unit ID: Site Wide Soil Gas - Hypothetical Worst Case
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 63 1.89 - 6.5E+03 5.8E-05
71-43-2 Benzene 31 0.93 3.6E-01 6.3E+00 2.6E-06 3.0E-02
106-99-0 Butadiene, 1,3- 9.4 0.282 9.4E-02 4.2E-01 3.0E-06 1.4E-01
75-15-0 Carbon Disulfide 110 3.3 - 1.5E+02 4.5E-03
67-66-3 Chloroform 1 0.03 1.2E-01 2.0E+01 2.5E-07 2.9E-04
110-82-7 Cyclohexane 79 2.37 - 1.3E+03 3.8E-04
75-71-8 Dichlorodifluoromethane 1.8 0.054 - 2.1E+01 5.2E-04
141-78-6 Ethyl Acetate 69 2.07 - 1.5E+01 2.8E-02
100-41-4 Ethylbenzene 370 11.1 1.1E+00 2.1E+02 9.9E-06 1.1E-02
142-82-5 Heptane, N- 460 13.8 - 8.3E+01 3.3E-02
110-54-3 Hexane, N- 27 0.81 - 1.5E+02 1.1E-03
67-63-0 Isopropanol 14 0.42 - 4.2E+01 2.0E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone) 8.7 0.261 - 1.0E+03 5.0E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 2.7 0.081 - 6.3E+02 2.6E-05
75-09-2 Methylene Chloride 4 0.12 1.0E+02 1.3E+02 1.2E-09 1.9E-04
91-20-3 ~Naphthalene 220 6.6 8.3E-02 6.3E-01 8.0E-05 2.1E+00
127-18-4 Tetrachloroethylene 140 4.2 1.1E+01 8.3E+00 3.9E-07 1.0E-01
108-88-3 Toluene 55 1.65 - 1.0E+03 3.2E-04
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 3.2 0.096 - 1.0E+03 1.8E-05
95-63-6 Trimethylbenzene, 1,2,4- 4200 126 - 1.3E+01 2.0E+00
108-67-8 Trimethylbenzene, 1,3,5- 3700 111 - 1.3E+01 1.8E+00
108-38-3 Xylene, m- 470 14.1 - 2.1E+01 1.4E-01
95-47-6 Xylene, o- 360 10.8 - 2.1E+01 1.0E-01
Cumulative: 9.6E-05 6.5E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator