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HomeMy WebLinkAbout5002_JacksonCounty_MSWLF_Oct20GW_FID1525972_20210119Data - Email CD (data loaded: Yes / No ) Doc/Event #:
INC DENR I i Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form_
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for Inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each Individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM. Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Anchor QEA of North Carolina, PLLC
Contact for questions about data formatting. Include data preparees name, telephone number and E-mail address:
Name: Alec Macbeth Phone: 828-281-3350
E-mail: amacbeth@anchorgea.com
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Jackson County Municipal Solid US Highway 441 5"2 .1600 October 12, 13, and 14, 2020
Waste Landfill Dillsboro, North Carolina 28725
Environmental Status: (Check all that apply)
Initial/Background Monitoring F1 Detection Monitoring © Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
Leachate monitoring data ❑
Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify) Natural Attenuation Parameters
Other(specify)
Notification attached?
® No. No groundwater or surface water standards were exceeded.
Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment
Alec Macbeth, PG Senior Scientist 828-281,3350
Facility Representative Na e(Print) Title (Area Code) Telephone
January 16, 2021 Affix NC L
Signature Date
231 Haywood Street, Asheville, North Carolina 28801
Facility Representative Address
P-1649
i
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R FP �yti.,
Seal
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
ti9
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•may
January 2021 ANCHOR
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 QEA `'`'"
Fall 2020
Semiannual Water Quality Monitoring Report
Prepared for Jackson County Solid Waste Department
January 2021
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Fall 2020
Semiannual Water Quality Monitoring Report
Prepared for
Jackson County Solid Waste Department
401 Grindstaff Cove Road
Sylva, North Carolina 28779
Alec Macbeth, PG
Project Geologist
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Number: C01480-01.02
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TABLE OF CONTENTS
1 Introduction............................................................................................................................1
2 Semiannual Monitoring.......................................................................................................2
2.1 Groundwater, Surface Water, Domestic Well, and Leachate Sampling............................................2
2.1.1 Monitoring Well Purging and Sampling Methods.....................................................................2
2.1.2 Surface Water Sampling Methods......................................................................................................3
2.1.3 Leachate Sampling Methods.................................................................................................................4
2.1.4 Domestic Well Sampling Methods.....................................................................................................4
2.2 Sample Handling, Documentation, and Analysis.........................................................................................4
3 Findings.................................................................................................................................. 7
3.1 Groundwater...................................................................................................................................................................7
3.1.1 Field Parameters...........................................................................................................................................8
3.1.2 Appendix II Metals (Total).......................................................................................................................8
3.1.3 Appendix II Metals (Dissolved).............................................................................................................9
3.1.4 Appendix II VOCs and 1,4-Dioxane....................................................................................................9
3.1.5 Appendix II SVOCs...................................................................................................................................10
3.1.6 Appendix II Pesticides.............................................................................................................................10
3.1.7 Appendix II Herbicides...........................................................................................................................10
3.1.8 Appendix II PCBs.......................................................................................................................................10
3.1.9 Natural Attenuation Parameters.......................................................................................................10
3.2 Surface Water..............................................................................................................................................................11
3.2.1 Field Parameters........................................................................................................................................11
3.2.2 Appendix II Metals...................................................................................................................................11
3.2.3 Appendix II VOCs and 1,4-Dioxane.................................................................................................12
3.2.4 Appendix II SVOCs, Pesticides, Herbicides, and PCBs............................................................12
3.3 Leachate.........................................................................................................................................................................12
3.4 Domestic Well.............................................................................................................................................................12
3.4.1 Field Parameters........................................................................................................................................13
3.4.2 VOCs................................................................................................................................................................13
3.5 Groundwater Flow Directions..............................................................................................................................13
4 Summary...............................................................................................................................14
4.1 Groundwater Quality...............................................................................................................................................14
4.1.1 Appendix II Metals...................................................................................................................................14
Fall 2020 Semiannual
Water Quality Monitoring Report i January 2021
4.1.2 Appendix II Volatile Organic Compounds and 1,4-Dioxane...............................................14
4.1.3 Field Parameters and Other Constituents....................................................................................14
4.2 Surface Water Quality.............................................................................................................................................15
4.3 Leachate Quality.........................................................................................................................................................15
4.4 Domestic Well Water Quality..............................................................................................................................15
5 Future Activities...................................................................................................................16
6 References.............................................................................................................................17
TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Well Construction Details and Corresponding Elevations
Table 3 Analytical Summary
Table 4 Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in
the Leachate Sample (LT-01)
FIGURES
Figure 1
Site Location Map
Figure 2
Site Layout Map
Figure 3
Generalized Groundwater Flow Direction
Figure 4
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-01)
Figure 5
Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-01)
Figure 6
Hydrograph and Vinyl Chloride Concentration vs. Time (Monitoring Well MW-01)
Figure 7
Hydrograph and 1,4-Dioxane Concentration vs. Time (Monitoring Well MW-04)
Figure 8
Hydrograph and 1,4-Dioxane Concentration vs. Time (Monitoring Well MW-05R)
Figure 9
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-07)
Figure 10
Hydrograph and 1,4-Dioxane Concentration vs. Time (Monitoring Well MW-07)
Figure 11
Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-07)
APPENDICES
Appendix A Well Sampling Logs, and Equipment Documentation and Instrument Calibration
Data Sheets
Appendix B Reports of Laboratory Analysis, Chain -of -Custody Documentation,
and Certificates of Analysis
Fall 2020 Semiannual
Water Quality Monitoring Report ii January 2021
ABBREVIATIONS
pg/L micrograms per liter
PS/cm microsiemens per centimeter
AM Analytical Method
bgs below ground surface
BOD biochemical oxygen demand
CAER Corrective Action Evaluation Report
CAP Corrective Action Plan
CFR Code of Federal Regulations
COD chemical oxygen demand
DENR North Carolina Department of Environment and Natural Resources
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
DWM Division of Waste Management
EPA U.S. Environmental Protection Agency
IMAC interim maximum allowable concentration
MDL method detection limit
mg/L milligrams per liter
MNA monitored natural attenuation
MSWLF Municipal Solid Waste Landfill
mV millivolts
NCAC North Carolina Administrative Code
NTU nephelometric turbidity unit
ORP oxidation reduction potential
PCBs polychlorinated biphenyls
PWR partially weathered rock
SC specific conductivity
Site Closed Municipal Solid Waste Landfill, approximately 0.75 mile west of Dillsboro,
North Carolina, on the northeast side of Old Dillsboro Road (Old U.S. Highway 74)
SM Standard Method
SU standard unit
SVOCs semivolatile organic compounds
SWS Solid Waste Section
TOC total organic carbon
TWSA Tuckasegee Water & Sewer Authority
VOC volatile organic compound
Waypoint Waypoint Analytical Laboratories
Fall 2020 Semiannual
Water Quality Monitoring Report iii January 2021
Introduction
The Jackson County Solid Waste Department maintains a closed Municipal Solid Waste Landfill (the
Site) approximately 0.75 mile west of Dillsboro, North Carolina, on the northeast side of
Old Dillsboro Road (Old U.S. Highway 74; Figure 1). Water quality monitoring at the landfill is
governed by the North Carolina Department of Environmental Quality (DEQ), Division of Waste
Management (DWM), Solid Waste Section (SWS), under Permit No. 50-02 issued to Jackson County.
The landfill permit requires semiannual monitoring of groundwater and surface water quality.
Since October 2007, when Anchor QEA of North Carolina, PLLC, began performing water quality
monitoring events at the Site, groundwater quality monitoring has indicated persistent low-level
concentrations of constituents that exceed groundwater quality standards. In response to the
continued exceedances of the analyzed constituents, an Assessment of Corrective Measures was
submitted to the North Carolina Department of Environment and Natural Resources (DENR; now the
DEQ) on September 7, 2010 (Altamont 2010). A Corrective Action Plan (CAP; Altamont 2011) was
implemented upon approval by the DENR, as recorded in the September 1, 2011 letter regarding
"Approval of the County's Corrective Action Plan" (DENR 2011). The implemented remedy includes the
extraction of leachate through dedicated submersible pumps installed within landfill gas extraction
wells and disposal of the leachate into the Tuckasegee Water & Sewer Authority (TWSA) collection
system. In addition to the leachate extraction, groundwater natural attenuation parameters are
monitored, and natural attenuation processes are evaluated. As discussed in the CAP, a corrective
action evaluation report is prepared every 5 years. The evaluation report analyzes the progress of the
approved corrective action remedy based on semiannual water quality monitoring data. The remedy
was implemented in a phased approach, with full implementation occurring on September 6, 2013. The
first Five -Year Corrective Action Evaluation Report (CAER), submitted by Altamont on October 31, 2016
(Altamont 2016), concluded that the current conditions of the monitored natural attenuation (MNA)
parameters and Site geochemical parameters allow for the slow degradation of the select contaminants
identified in the CAER. The second CAER is scheduled to be submitted in fall 2021.
This report serves as the second semiannual water quality monitoring report for 2020. The report
provides an evaluation of groundwater and surface water quality. The water quality monitoring
network is presented in Figure 2. The generalized groundwater flow direction in the upper parts of
the underlying aquifer system is provided in Figure 3. In addition to groundwater and surface water
monitoring, this report includes analysis of the extracted leachate and one domestic water well. The
water samples collected from selected monitoring points during the fall sampling event were
analyzed for a range of parameters, as presented in Section 2.2 and Table 1. The fall 2020 sampling
event was performed on October 12, 13, and 14, 2020, and is being reported in accordance with
requirements stipulated in the DEQ Solid Waste Management Rules codified under Title 15A,
Subchapter 13B of the North Carolina Administrative Code (NCAC).
Fall 2020 Semiannual
Water Quality Monitoring Report 1 January 2021
2 Semiannual Monitoring
2.1 Groundwater, Surface Water, Domestic Well, and Leachate
Sampling
The Site monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06, and MW-07), surface
water sample locations (SW-01 and SW-02), leachate sample location (LT-01), and domestic well
(DW-01) were sampled on October 12, 13, and 14, 2020, by Anchor QEA. Static groundwater level
measurements and field parameter data are included on the sampling logs presented in Appendix A.
Field equipment calibration logs for the YSI Professional Plus Multiparameter Water Quality Meter
and the Hach 2100Q Turbidimeter are also provided in Appendix A. The full suite of groundwater
and surface water laboratory analytical results is presented in the laboratory analysis reports in
Appendix B.
Monitoring wells MW-01 and MW-06 are considered to be the Site's upgradient monitoring wells;
MW-03 and MW-05R are located in the midgradient portion of the Site; and MW-02, MW-04, and
MW-07 monitor downgradient portions of the Site. As summarized in Table 2, the total depths of the
monitoring wells range from 40 to 110 feet below ground surface (bgs). The geology of the screened
intervals of the monitoring wells is as follows:
• Saprolite': MW-04 and MW-05R
• Partially Weathered Rock (PWR)Z: MW-03
• Bedrock3: MW-01, MW-02, MW-06, and MW-07
The locations of the monitoring wells, surface water samples, leachate, and domestic well sample
locations are shown in Figure 2.
2.7.7 Monitoring Well Purging and Sampling Methods
Before the monitoring wells were sampled, the static water level was gauged in each well, and an
initial round of field parameters was measured (consisting of pH, specific conductivity [SC], dissolved
oxygen [DO], turbidity, temperature, and oxidation reduction potential [ORP]). Due to a field
equipment malfunction, field pH measurements collected on October 13, 2020, were not considered
representative of groundwater quality and samples were submitted to the laboratory for pH analysis.
Therefore, the pH values discussed in the text of this report for monitoring wells MW-01, MW-03,
and MW-06 are based on laboratory results.
Saprolite is the result of in -place weathering that produces soil -like material that retains relict features of the parent rock.
z PWR is generally found above the bedrock and is softer than bedrock, but not as soft as saprolite.
3 Bedrock is solid competent rock that underlies saprolite and partially weathered rock.
Fall 2020 Semiannual
Water Quality Monitoring Report 2 January 2021
Anchor QEA personnel used either low -flow techniques or disposable bailers to purge the
monitoring wells and collect groundwater samples. The total depth, condition of the casing, and
groundwater recharge rate determined the purging and sample collection method employed at each
monitoring well.
Four of the monitoring wells (MW-03, MW-04, MW-06, and MW-07) were purged using low -flow
techniques in accordance with the procedures described by the U.S. Environmental Protection
Agency (EPA) in Low -Flow (Minimal Drawdown) Ground -Water Sampling Procedures (EPA 1996).
During purging, the field parameters (pH, SC, DO, ORP, turbidity, and temperature) were measured
and recorded approximately every 3 minutes. Well purging continued until these parameters had
generally stabilized for three consecutive readings. The required stabilization criteria are determined
by the EPA Region 4 Science and Ecosystem Support Division in Operating Procedure: Groundwater
Sampling (EPA 2017) and are summarized as follows:
• pH values within ±0.1 standard unit (SU)
• SC values within ±5%
• Temperature, DO, and turbidity values within ±10%
• ORP values within ±10 millivolts (mV)
Once the parameters had stabilized, a groundwater sample was collected by field personnel wearing
a new pair of nitrile gloves, using laboratory -supplied sample containers.
Because of their slow recharge rates, monitoring wells MW-01, MW-02, and MW-05R were purged
and sampled using disposable bailers. The wells were purged of three successive well volumes or
purged dry, whichever occurred first. Monitoring well MW-02 was purged dry on October 12 and
sampled on October 13, 2020, after the well had sufficient time to recharge. Monitoring well MW-
05R was purged dry in the morning on October 12 and sampled later that day after the well had
sufficient time to recharge. Monitoring well MW-01 was purged and sampled on October 14, 2020. A
round of field parameters was measured and recorded at the start of purging and after each
consecutive well volume had been purged.
Field parameter data are shown in the well sampling logs included in Appendix A.
2.7.2 Surface Water Sampling Methods
Surface water samples SW-01 and SW-02 were collected on October 14, 2020, at designated
locations from the Tuckasegee River, which is adjacent to and southwest of the landfill (Figure 2).
Sampling location SW-01 is assumed to represent surface water quality upstream of the landfill, and
sampling location SW-02 is assumed to represent surface water quality downstream of the landfill.
One round of field parameters was measured and recorded at each surface water sampling location
Fall 2020 Semiannual
Water Quality Monitoring Report 3 January 2021
immediately prior to collecting the sample (Appendix A). The surface water samples were collected in
laboratory -provided sample containers by a technician wearing a new pair of nitrile gloves.
2. 7.3 Leachate Sampling Methods
Dedicated bottom -loading air -powered pumps, air pressure lines, and a leachate force main
collection system are installed at the landfill. Pumps are installed in landfill gas extraction wells
EW-1 R, EW-2R, EW-3R, EW-4, EW-5, EW-6, EW-7, EW-8, EW-9, and EW-10. The gas extraction well
locations are presented in Figure 2. The leachate is pumped from the wells into a flow equalization
tank, which is connected to the TWSA wastewater collection system.
The flow equalization tank is east of the landfill, adjacent to the existing landfill gas flare. A grab
sample of leachate (LT-01) was acquired on October 14, 2020, by collecting a sample as the leachate
entered the flow equalization tank. One round of field parameters was measured and recorded after
the sample was collected (Appendix A).
2.1.4 Domestic Well Sampling Methods
The domestic well water sample (DW-01, owned by Mr. Frank Wilkie) was collected on October 14,
2020, from an outside spigot at the residence located at 318 Joe Wilkey Road, bordering the
northern boundary of the landfill (Figure 2). The well was purged of 30 gallons prior to sample
collection. One round of field parameters was measured and recorded after the 30 gallons had been
purged. The domestic well water sample was collected in laboratory -provided sample containers by
field personnel wearing a new pair of nitrile gloves.
Attempts to sample the second domestic water well (DW-2, owned by Mr. Joshua Bulla at
138 Joe Wilkey Road) were unsuccessful because the owner could not be contacted.
2.2 Sample Handling, Documentation, and Analysis
It should be noted that during most semiannual sampling events at the Jackson County Landfill,
water quality samples are submitted for Appendix I parameters only. A larger suite of Appendix II
parameters as noted below are analyzed for during the fall sampling event only on a biannual basis.
Field parameters and additional observations pertaining to the Site sampling locations are provided
in the sampling logs (Appendix A). Following sample collection, each groundwater, surface water,
leachate, and domestic well water sample was immediately placed on ice in a sample cooler for
transport to Waypoint Analytical Laboratories (Waypoint), a North Carolina -certified laboratory in
Charlotte, North Carolina. The groundwater samples collected from the monitoring wells were
analyzed for the following parameters (Table 1):
• Appendix II metals, including mercury, using EPA Methods 6020B and 7470A
• Appendix II volatile organic compounds (VOCs), using EPA Method 8260D
Fall 2020 Semiannual
Water Quality Monitoring Report 4 January 2021
• 1,4-Dioxane, using EPA Method 8260DSIM
• Appendix II semivolatile organic compounds (SVOCs), using EPA Method 8270D
• Appendix II herbicides, using EPA Method 8151A
• Appendix II pesticides, using EPA Methods 8081 B and 8141 B
• Appendix II polychlorinated biphenyls (PCBs), using EPA method 8082A
• MNA parameters:
— Alkalinity, using Standard Method (SM) 2320B
— Biochemical oxygen demand (BOD; 5-day), using SM 5210B
— Volatile fatty acids, carbon dioxide, ethane, ethene, and methane, using Analytical
Method (AM) 20GAX
— Hydrogen (only in MW-03, MW-04, MW-06, and MW-07), using AM20GAX
— Chemical oxygen demand (COD), using SM 5220D
— Chloride, nitrate, and sulfate, using EPA Method 9056A
— Ferrous iron, using SM 3500-Fe D
— Sulfide, using SM 4500-5 F
— Cyanide, using SM 4500-CN-E
— Total organic carbon (TOC), using SM 9060A
— Nitrate as N, chloride, and sulfate, using EPA Methods 9056A
The surface water samples were analyzed for the following parameters:
• Appendix II metals, including mercury, using EPA Methods 6020B and 7470A
• Appendix II VOCs, using EPA Method 8260D
• 1,4-Dioxane, using EPA Method 8260DSIM
• Hardness, using SM2340C
• Appendix II SVOCs, using EPA Method 8270D
• Appendix II herbicides, using EPA Method 8151A
• Appendix II pesticides, using EPA Methods 8081 B and 8141 B
• Appendix II PCBs, using EPA method 8082A
The leachate sample was analyzed for the following parameters:
• Appendix II VOCs, using EPA Method 8260D
• 1,4-Dioxane, using EPA Method 8260DSIM
• Appendix II metals, using EPA Method 6020B
The domestic well sample was analyzed for the following parameters:
• VOCs, using EPA Method 524.2
Fall 2020 Semiannual
Water Quality Monitoring Report 5 January 2021
Proper chain -of -custody documentation procedures were followed during collection and
transportation of each sample (Appendix B). Two trip blank samples for quality control/quality
assurance purposes were included in the sample coolers and analyzed for Appendix I VOCs when
applicable. The reports of the laboratory analyses are provided in Appendix B. Laboratory analyses
performed on the samples are summarized in Table 1.
Fall 2020 Semiannual
Water Quality Monitoring Report 6 January 2021
3 Findings
The field parameter data and laboratory analytical results for the groundwater samples (from
monitoring wells MW-01 through MW-07), surface water samples (SW-01 and SW-02), leachate
sample (LT-01), and domestic well sample (DW-01) collected at the landfill are included in
Appendices A and B. The results are also submitted separately to the DEQ DWM SWS in the
Electronic Data Deliverable format (DEQ 2020).
The laboratory analytical results were reported and appropriately qualified as follows:
• Non -Detections: Non -detections are values reported by the laboratory as less than the method
detection limits (MDLs). They are tabulated in Table 3 and flagged with a "U" qualifier. The MDL is
the minimum concentration of a substance that can be measured and reported by a laboratory
with 99% confidence that the constituent concentration is greater than zero.
• Estimated or " Y' Qualified: A "J" qualifier is used by the laboratory for parameters that are
detected at estimated concentrations greater than the MDL but less than the laboratory's
method reporting limit. The method reporting limit is the minimum concentration of a target
analyte that can be accurately determined by the referenced method.
• Groundwater Quality Standard: Detected concentrations of constituents in groundwater
samples were compared to applicable North Carolina groundwater quality standards. For
most constituents, this standard is the 2L standard, defined in 15A NCAC 2L .0202. Detected
concentrations of analytes in groundwater with no established 2L standard were compared to
the interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]). For the purposes of this report, groundwater
standards were taken from the October 15, 2018 list published by the North Carolina SWS
(DEQ 2018b).
2B Standard: Detections of analytes in surface water samples were compared to the
surface -water quality standards 2B standards, defined in 15A NCAC 2B. Hardness -dependent
2B surface water standards were calculated using the average analyzed hardness value
(calculated from the upstream and downstream surface water sampling location results) via
the most stringent hardness -dependent metal calculation.
Table 3 summarizes detected concentrations of analytes that exceeded their respective 2L standard,
IMAC, or 2B standard.
3.1 Groundwater
Measured field parameters and analytical results for groundwater samples collected from the
monitoring wells during the fall 2020 sampling event are discussed in the following sections and
summarized in Table 3.
Fall 2020 Semiannual
Water Quality Monitoring Report 7 January 2021
3.7.7 Field Parameters
Field parameter measurements were obtained from all site monitoring wells (MW-01, MW-02, MW-
03, MW-04, MW-05R, MW-06, and MW-07). The pH readings ranged from 5.70 SU in MW-01 to 7.1
SU in MW-06. Of these monitoring wells, the pH values for MW-01, MW-04, and MW-07 were less
than the 2L Standard pH range of 6.5 to 8.5 SU.
Turbidity ranged from 3.94 nephelometric turbidity units (NTU) in MW-04 to more than 1,000 NTU in
MW-02. Generally, the higher values were measured at the monitoring wells (MW-01, MW-02, and
MW-05R) that were purged and sampled using the bailer method (Section 2.1.1). The bailers were
lowered gently to minimize water column disturbance when the samples were collected.
Dissolved oxygen (DO) concentrations at the Site ranged from 1.43 milligram per liter (mg/L) in
monitoring well MW-05R to 5.08 mg/L in monitoring well MW-02. SC concentrations at the Site
ranged from 52.8 microsiemens per centimeter (pS/cm) in monitoring well MW-06 to 758 pS/cm in
monitoring well MW-07.ORP concentrations at the Site ranged from -139.9 mV in monitoring well
MW-06 to 302.8 mV in monitoring well MW-04. (As noted on the groundwater sampling logs
[Appendix A], the ORP values reported for monitoring wells MW-02 and MW-06 may not be
representative of groundwater quality because of equipment malfunction.) Groundwater standards
are not established for DO, SC, or ORP.
3.7.2 Appendix 11 Metals (Total)
Fourteen metals were detected in one or more of the monitoring well samples. Six of these metals,
chromium, cobalt, mercury, selenium, thallium, and vanadium, were detected at concentrations
above their respective NC21- and/or IMAC water quality standards in one or more of the groundwater
samples. Cobalt was detected at a concentration that exceeded its IMAC (1 microgram per liter
[pg/L]) in groundwater samples collected from MW-01, MW-02, MW-04, MW-05R, MW-06, and
MW-07. Cobalt concentrations in these samples ranged from an estimated 1 A pg/L (MW-07) to
160 pg/L (MW-01). As noted in Section 2.1, the latter monitoring well is considered to represent
upgradient conditions. The second upgradient well (MW-06) also showed an exceedance of cobalt (9
pg/L). Historically, cobalt has been present at concentrations that exceed its applicable water quality
standard in groundwater samples from each of the seven monitoring wells.
Mercury was detected at a concentration exceeding its 2L standard (1 pg/L) in groundwater samples
collected from MW-01 (1.1 pg/L), MW-03 (1.1 pg/L), and MW-06 (1.3 pg/L).
Additionally, chromium (61 pg/L), selenium (42 pg/L), thallium (estimated 0.96 pg/L), and vanadium
(71 pg/L) were detected at concentrations exceeding their respective NC 2L and/or IMAC standards
(10 pg/L, 20 pg/L, 0.2 pg/L, and 0.3 pg/L, respectively) in groundwater sample collected from MW-02.
These metals have historically been present at concentrations exceeding their water quality standard
Fall 2020 Semiannual
Water Quality Monitoring Report 8 January 2021
in samples collected from multiple groundwater monitoring wells at the Site. However, the elevated
turbidity value measured in the MW-02 sample may have affected the metal concentrations reported
here. During the spring 2020 sampling event, MW-02 showed a turbidity of 15.5 NTU with
consistently lower concentrations of these metals.
3.7.3 Appendix 11 Metals (Dissolved)
Laboratory -filtered analysis of Appendix II metals were performed for monitoring well samples
MW-02 and MW-05R because of their elevated turbidity readings (>1,000 NTU and 53.7 NTU,
respectively) during sample collection. The reported concentrations for the dissolved metals were
consistently lower than the total unfiltered metals analytical results in MW-02, with no exceedances
of the groundwater water protection standards. The dissolved metals results for MW-05 were
comparable to the associated total unfiltered metal analysis (Table 3).
3.7.4 Appendix 11 VOCs and 7,4-Dioxane
Nineteen VOCs were detected in one or more of the monitoring wells (Table 3). Four of these VOCs
(1,4-dichlorobenzene; 1,4-dioxane; benzene; and vinyl chloride) were detected at concentrations that
exceeded their respective 2L standards in the groundwater samples collected from one or more
monitoring wells. Concentration -versus -time graphs (trend plots) were created for the monitoring wells
that have historically exhibited VOC concentrations that exceed the associated 2L standards (Figures 4
through 11).
The detected concentration of 1,4-dichlorobenzene exceeded its 2L standard (6 pg/L) in monitoring
wells MW-01 (9.8 pg/L) and MW-05R (6.8 pg/L). The historical 1,4-dichlorobenzene concentration
trend in MW-01 remains relatively stable (Figure 4).
The detected concentrations of 1,4-dioxane equaled or exceeded its 2L standard (3 pg/L) in MW-04
(3.4 pg/L), MW-05R (3.5 pg/L), and MW-07 (17 pg/L). 1,4-Dioxane was not detected in monitoring
wells MW-01, MW-03 or MW-06. Trend plots for 1,4-dioxane concentrations in MW-04, MW-05R,
and MW-07 show stable concentrations (Figures 7, 8, and 10).
Benzene was detected at concentrations that slightly exceed its 2L standard of 1 pg/L in MW-01
(1.5 pg/L) and MW-07 (1.4 pg/L). Overall, historical benzene concentration trends in monitoring wells
MW-01 and MW-07 have been stable and slightly exceed the 2L standard (Figures 5 and 11).
The concentration of vinyl chloride in the sample collected from one monitoring well, MW-01,
(estimated 0.31 pg/L) slightly exceeded the compound's 2L standard (0.03 pg/L). A trend plot for
vinyl chloride concentrations in MW-01 shows consistently low concentrations of the constituent
(Figure 6).
Fall 2020 Semiannual
Water Quality Monitoring Report 9 January 2021
A review of historical groundwater data indicates that the VOCs (1,4-dichlorobenzene; 1,4-dioxane,
benzene; and vinyl chloride) exhibiting concentrations that exceed the 2L standards during the fall
2020 sampling event have been detected at relatively consistent concentrations for the past several
years. As described in Section 3.2.3, historical surface water samples from the Tuckasegee River,
which may receive discharge from the saprolite groundwater -bearing zone, have consistently shown
no detections of these compounds, or other VOCs.
3. 7.5 Appendix 11 SVOCs
Five SVOCs (1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene, dibenzofuran, and
diethyl phthalate) were detected in one or more of the monitoring wells on Site during the fall 2020
water quality monitoring event (Table 3). None of these detections exceeded their respective 2L or
IMAC standards. The analytical results of 1,4-dichlorobenzene reported under the VOC analysis are
discussed in Section 3.1.3.
3. 7.6 Appendix 11 Pesticides
Two pesticides (beta-BHC and gamma-BHC) were detected at concentrations above their respective
water quality standards (Table 3) in the groundwater samples collected from two of the monitoring
wells during the fall 2020 water quality monitoring event. These exceedances represent the second
time these compounds have been detected during a monitoring event. These compounds were last
sampled for in fall 2018. Beta-BHC was detected at an estimated concentration above the IMAC
(0.02 pg/L) in monitoring well MW-06 (0.14 pg/L). This compound was not detected in other
monitoring wells. Gamma-BHC exceeded the 2L standard (0.03 pg/L) in monitoring well MW-01
(0.051 pg/L). This parameter was detected but did not exceed its 2L standard in MW-05R.
3. 7.7 Appendix 11 Herbicides
Two pesticides (silvex and 2,4-dichlorophenoxyacetic acid) were detected in one or more of the
monitoring wells during the fall 2020 water quality monitoring event (Table 3). Neither of these
detections exceeded their respective 2L standards.
3. 7.8 Appendix 11 PCBs
No PCBs were detected in any of the groundwater samples collected during the fall 2020 water
quality monitoring event.
3.1.9 Natural Attenuation Parameters
During this sampling event, the groundwater samples were analyzed for MNA parameters as
described in Section 2.2 (Table 1). The results of these analyses are summarized in Table 3. These
parameters were detected in one or more groundwater samples collected from the monitoring wells.
Many of these parameters do not have established groundwater standards. Of the parameters that
Fall 2020 Semiannual
Water Quality Monitoring Report 10 January 2021
do have established groundwater standards, chloride, cyanide, and sulfate, there were no
exceedances (or detections in the case of cyanide). An in-depth analysis of the MNA parameters that
apply to the Site's select contaminants was presented in the first Five -Year CAER (Altamont 2016).
The CAER concluded that the MNA data provide evidence that reductive degradation and aerobic
degradation are occurring in different portions of the Site. The dataset of the MNA parameters
collected from spring 2017 to spring 2021 will be used in the second Five -Year CAER (scheduled for
fall 2021) to evaluate the degradation processes at the Site.
3.2 Surface Water
The following sections summarize the measured field parameters and analytical results associated
with the two surface water samples collected during the fall 2020 sampling event.
3.2. 7 Field Parameters
The pH readings for the upstream (SW-01) and downstream (SW-02) surface water samples collected
during the fall 2020 sampling event were 6.36 and 6.60 SU, respectively. The pH readings for both
surface water samples were within the 2B standard range of 6.0 to 9.0 SU.
The turbidity values measured in SW-01 (36.9 NTU) and SW-02 (29.0 NTU) were less than the
2B standard, which is established at less than or equal to 50 NTU for the receiving water in streams
not designated as trout waters.
DO was measured at a concentration of 10.35 mg/L in SW-01 and 10.67 mg/L in SW-02. The
2B standard is established as greater than or equal to 6 mg/L; thus, each sample is within the
acceptable DO range.
SC concentrations in surface water samples SW-01 and SW-02 were recorded at 36.7 and
26.7 pS/cm, respectively. ORP values for SW-01 and SW-02 were 127.9 and 153.6 mV, respectively.
These concentrations of SC and ORP are consistent with historical data for both surface water
samples. 2B standards do not exist for these parameters.
3.2.2 Appendix 11 Metals
Six metals were detected in both surface water sampling locations. Of these metals, only one (lead)
was detected at a concentration that slightly exceeded its 2B standard of 0.2 pg/L. Lead was detected
in upstream location SW-1 at an estimated 0.3 pg/L and downstream location SW-2 at an estimated
0.38 pg/L.
Fall 2020 Semiannual
Water Quality Monitoring Report 11 January 2021
3.2.3 Appendix 11 VOCs and 7,4-Dioxane
One VOC, naphthalene, was detected but did not exceed its 2B standard in the surface water
sampling location, SW-01. There were no other VOC detections or exceedances in either of the
surface water sampling locations.
3.2.4 Appendix 11 SVOCs, Pesticides, Herbicides, and PCBs
No SVOCs, pesticides, herbicides, or PCBs were detected in any of the surface water samples
collected during the fall 2020 water quality monitoring event.
3.3 Leachate
Eight metals (arsenic [2.9 pg/L], barium [500 pg/L], chromium [2.5 pg/L], cobalt [3.8 pg/L], mercury
[0.23 pg/L], nickel [20 pg/L], selenium [estimated 0.79 pg/L], and vanadium [estimated 2.4 pg/L])
were detected in the leachate sample (LT-01).
Seventeen VOCs (cis-1,2-dichloroethene [estimated 0.29 pg/L]; 1,3-dichlorobenzene [estimated
0.27 pg/L]; 1,4-dichlorobenzene [4.8 pg/L]; 1,4-dioxane [58 pg/L]; acetone [11 pg/L]; acetonitrile
[estimated 4.7 J pg/L]; benzene [2A pg/L]; chlorobenzene [4.4 pg/L]; chloroethane [estimated
0.47 pg/L]; ethylbenzene [1.8 pg/L]; m,p-xylene [1.7 pg/L]; naphthalene [13 pg/L]; o-xylene [2.0 pg/L];
tetrahydrofuran [94 pg/L]; toluene [0.79 pg/L]; and vinyl chloride [estimated 0.22 pg/L]) were
detected in the leachate sample (LT-01).
On September 1, 2012, leachate extraction was initiated following installation of leachate extraction
pumps in the 10 landfill gas extraction wells at the Site (Figure 2). Due to a temporary malfunction
with the leachate flow meter between October 2017 and March 2018, there is a gap in the mass
removal calculations represented in Table 4. Therefore, the total volume of leachate removed since
September 2012 is not known. However, based on readings taken from the leachate totalizer during
the October 2020 monitoring events, approximately 98,790 gallons of leachate were discharged
through a permanent connection to the TWSA between March 19 and October 14, 2020 (Table 4).
In fall 2013, the active portion of the approved corrective action remedy was initiated. Based on the
leachate analytical results for the sample collected on October 14, 2020, Anchor QEA estimates that
approximately 0.17 pounds of VOCs was removed with the extracted leachate between the March
and October 2020 sampling events. Mass removal calculations are included in Table 4.
3.4 Domestic Well
The following sections summarize measured field parameters and analytical results associated with
the domestic well water sample collected during the fall 2020 sampling event.
Fall 2020 Semiannual
Water Quality Monitoring Report 12 January 2021
3.4.7 Field Parameters
The pH reading for the domestic well sample (DW-01) was 6.46 SU, which isjust outside of the 2L
standard range of 6.5 to 8.5 SU.
Turbidity measured in DW-01 was 4.3 NTU. DO was measured at a concentration of 7.74 mg/L in
DW-01. SC and ORP values in DW-01 were recorded at 70.5 pS/cm and 186.7 mV, respectively. These
parameters do not have established water quality standards.
3.4.2 VOCs
No VOCs were detected at concentrations that exceeded their respective MDLs in the domestic well
water samples.
3.5 Groundwater Flow Directions
Groundwater levels in the saprolite, PWR, and bedrock are monitored at the Site. Three of the
bedrock monitoring wells (MW-01, MW-02, and MW-06) are located in the northern and
northwestern portions of the Site (Figure 3; Table 2). The fourth bedrock monitoring well (MW-07) is
located southwest of the landfill (Figure 3). The fall 2020 water level data collected from these four
bedrock wells were used to determine the generalized bedrock groundwater flow direction, which is
to the southwest (Figure 3).
PWR monitoring well MW-03 and saprolite monitoring wells MW-04 and MW-05R (Figure 3) are
located in the south-central and southern parts of the landfill, respectively. The fall 2020 water level
data collected from monitoring wells MW-03, MW-04, and MW-05R (Table 2) indicate that
groundwater flow direction in the combined saprolite and PWR zones is generally to the south-
southwest, toward the Tuckasegee River (Figure 3).
Fall 2020 Semiannual
Water Quality Monitoring Report 13 January 2021
4 Summary
The second semiannual water quality monitoring event of 2020 for the Site was performed on
October 12, 13, and 14, 2020. Appendices A and B and Table 3 provide detailed analytical results and
field data summarizing the groundwater, surface water, and leachate quality at the landfill.
4.1 Groundwater Quality
4. 7. 7 Appendix 11 Metals
Six metals (chromium, cobalt, mercury, selenium, thallium, and vanadium) were detected at
concentrations that exceeded their associated groundwater quality standards in one or more of the
monitoring wells (Table 3). Cobalt concentrations exceeded its 2L standard in all of the collected
groundwater samples excluding MW-03 but including the upgradient monitoring wells, MW-01 and
MW-06. These results are consistent with historical data.
The results for the two groundwater samples (MW-02 and MW-05R) submitted for dissolved filtered
metals showed significantly lower or comparable metals concentrations than the total unfiltered
samples.
4. 7.2 Appendix 11 Volatile Organic Compounds and 1,4-Dioxane
Four VOCs (1,4-dichlorobe nzene; benzene; vinyl chloride; and 1,4-dioxane) were detected at
concentrations that exceeded their respective 2L standards (Table 3) in one or more monitoring
wells, including 1,4-dichlorobenzene, benzene, and vinyl chloride in the upgradient monitoring well
MW-01. Trend plots for samples from monitoring wells that had VOC concentrations that exceeded
their 2L standards (Figures 4 through 11) show relatively stable concentrations with time.
4. 7.3 Field Parameters and Other Constituents
Three of the seven of the samples collected from the monitoring wells had pH readings outside of
the 2L standard range (6.5 to 8.5 SU). These results are consistent with historical data and are
characteristic of the natural groundwater quality of the region. Turbidity readings ranged from
3.94 NTU (MW-04) to more than 1,000 NTU (MW-02).
Natural attenuation parameters (alkalinity, BOD, COD, chloride, cyanide, nitrate as N, sulfate, sulfide,
TOC, ferrous iron, hydrogen, methane, acetic acid, formic acid, lactic acid, propionic acid, and carbon
dioxide) were detected at various concentrations in groundwater samples collected from one or
more of the monitoring wells. Natural attenuation parameters are being monitored to fulfill CAP
requirements; further evaluation of these parameters will be performed in the second Five -Year CAER
(scheduled for fall 2021).
Fall 2020 Semiannual
Water Quality Monitoring Report 14 January 2021
Five Appendix II SVOCs (1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene,
dibenzofuran, and diethyl phthalate) were detected in one or more of the monitoring wells but
exceeded their respective 2L or IMAC standards.
Two Appendix II Pesticides (beta-BHC in MW-06 and gamma-BHC in MW-01) were detected at
concentrations above their respective water quality standards in the groundwater samples collected
from two of the monitoring wells during the fall 2020 water quality monitoring event. This represents
the second time these compounds have been detected during a monitoring event.
Two Appendix II Pesticides (Silvex and 2,4-dichlorophenoxyacetic acid) were detected in one or more
of the monitoring wells but did not exceed their respective 2L standards.
No Appendix II PCBs were detected in the groundwater samples collected during the fall 2020 water
quality monitoring event.
4.2 Surface Water Quality
One metal, lead, was detected at a concentration that exceeded its applicable 2B standard for surface
water during this monitoring event. Concentrations in the upstream sample exceeded concentrations
in the downstream sample for all metals that were detected. No VOCs were detected at
concentrations that exceeded the applicable surface water standards. Field parameters measured in
both surface water samples, including pH, turbidity, and DO, were within the 2B standards
established for these parameters. Based on these data, the groundwater migrating from the landfill
toward the Tuckasegee River does not appear to be impacting surface water quality with regard to
metals and VOCs.
4.3 Leachate Quality
The leachate sample (LT-01) was collected from the flow equalization tank and analyzed for
Appendix I VOCs and 1,4-dioxane. Seventeen VOCs were detected in the leachate sample (Table 3).
There are no established water quality standards for leachate. 1,4-Dioxane was detected at 58 pg/L,
which is higher than the detected concentrations of the compound in the monitoring well
groundwater samples. This is the first sampling event where 1,4 dioxane was analyzed for in the
leachate.
4.4 Domestic Well Water Quality
No VOCs were detected at concentrations that exceeded their respective MDLs in the domestic well
water samples.
Fall 2020 Semiannual
Water Quality Monitoring Report 15 January 2021
5 Future Activities
Anchor QEA will continue to monitor the water quality on a semiannual basis at the Site. During
spring 2021, domestic well owners will be contacted, and groundwater samples will be collected
from domestic wells if permitted by the well owner, and if possible, based on well pump operability.
Domestic well samples will be analyzed for VOCs only. Samples will be collected from the monitoring
wells, surface water monitoring points, and leachate flow equalization tank during spring 2021 and
fall 2021. In addition to the MNA parameters that were added to the monitoring requirements as
part of the CAP, the analytical suites associated with the current and future sampling events are
outlined in the 2011 CAP (Altamont 2011) and the first Five -Year CAER (Altamont 2016). The
upcoming sampling event parameters are as follows:
Sampling Event
Analytical Suite
(not inclusive of natural attenuation parameters)
Appendix I VOCs (including 1,4-dioxane)
Spring 2021
Appendix I Metals
Sulfide
Appendix 11 VOCs (including 1,4-dioxane)
Fall 2021
Appendix 11 Metals
Sulfide
The second Five -Year CAER is scheduled for fall 2021. This evaluation will include a detailed analysis
of the contaminant and MNA parameter trends to assess effectiveness of the MNA program. This
report will also include an evaluation of MW-01 and MW-06 as representative background wells at
the Site.
Fall 2020 Semiannual
Water Quality Monitoring Report 16 January 2021
6 References
Altamont (Altamont Environmental, Inc.), 2010.Assessment of Corrective Measures. Prepared for the
North Carolina Department of Environment and Natural Resources. September 7, 2010.
Altamont, 2011. Corrective Action Plan. Prepared fort he North Carolina Department of Environment
and Natural Resources. June 30, 2011.
Altamont, 2016. Five -Year Corrective Action Evaluation Report. Prepared for the North Carolina
Department of Environmental Quality. October 31, 2016.
DENR (North Carolina Department of Environmental and Natural Resources), 2011. Letter to:
Altamont Environmental, Inc. Regarding: Approval of the County's Corrective Action Plan.
September 1, 2011.
DEQ (North Carolina Department of Environmental Quality), 2018a. Memorandum to: Solid Waste
Directors, Landfill Owners/Operators, and North Carolina Certified Laboratories. Regarding:
1,4-Dioxane Analysis, Solid Waste Section Limits, and Laboratory Analytical Methods.
May 29, 2018.
DEQ, 2018b. "Groundwater Protection Compliance Standards — Constituents List". Last modified
October 15, 2018. Available at:
https://edocs.deq.nc.gov/WasteManagement/0/edoc/1257181/SWS EnviroMonitoring Const
ituents List.pdf?searchid=13f8efbl-eel 1-485a-b03f-718f2287b271
DEQ, 2020. Memorandum Re: New Electronic Data Deliverable (EDD) Format. July 20, 2020.
EPA (U.S. Environmental Protection Agency), 1996. Low -Flow (Minimal Drawdown) Ground -Water
Sampling Procedures. OSWER, EPA/540/5-95/504.
EPA, 2017. Science and Ecosystem Support Division. Operating Procedure: Groundwater Sampling.
April 26, 2017.
Fall 2020 Semiannual
Water Quality Monitoring Report 17 January 2021
Tables
Table 1
Summary of Laboratory Analyses Performed on Samples
Groundwater Samples
Location ID
Date
Collected
Sample ID
Appendix II
VOCs
1,4-Dioxane
Appendix II
Metals
Mercury
Appendix II
SVOCs
Apendix II
Herbicides
Appendix II
Pesticides
Appendix II
PCBs
EPA 8260D
EPA 8260D
SIM
EPA 6020B
EPA 7470A
EPA 8270D
EPA 8151A
EPA 8081 B
and 8141 B
EPA 8082A
MW-01
10/14/2020
MW-01-20201014
X
X
X
X
X
X
X
X
MW-02
10/13/2020
MW-02-20201013
X
X
X
X
X
X
X
X
MW-03
10/13/2020
MW-03-20201013
X
X
X
X
X
X
X
X
MW-04
10/12/2020
MW-04-20201012
X
X
X
X
X
X
X
X
MW-05R
10/12/2020
MW-05R-20201012
X
X
X
X
X
X
X
X
MW-06
10/13/2020
MW-06-20201013
X
X
X
X
X
X
X
X
MW-07
10/12/2020
MW-07-20201012
X
X
X
X
X
X
X
X
Surface Water, Leachate, Domestic Well, and Quality Control Samples
Location ID
Date
Collected
Sample ID
Appendix II
VOCs
1,4-Dioxane
Appendix II
Metals
Mercury
Calcium,
Magnesium,
Hardness
Appendix II
SVOCs
Apendix II
Herbicides
Appendix II
Pesticides
Appendix II
PCBs
VOCs
EPA 8260D
EPA 8260D
SIM
EPA 6020B
EPA 7470A
EPA 200.7
EPA 8270D
EPA 8151A
EPA 8081 B
and 8141 B
EPA 8082A
EPA 524.2
DW-01
10/14/2020
DW-01-20201014
X
LT-01
10/14/2020
LT-01-20201014
X
X
X
SW-01
10/14/2020
SW-01-20201014
X
X
X
X
X
X
X
X
X
SW-02
10/14/2020
SW-02-20201014
X
X
X
X
X
X
X
X
X
TB-01
10/12/2020
TB-202010120000
X
TB-02
10/13/2020
TB-202010130000
X
TB-03
10/14/2020
TB-202010130000
X
Groundwater and Surface Water Samples: Monitored Natural Attenuation Parameters
Location ID
Date
Collected
Sample ID
COD
BOD
Ferrous Iron
Total
Alkalinity
to pH 4.5
Nitrate
as N
Chloride
Sulfate
TOC
Sulfide
Cyanide
Volatile Fatty
Acids
Carbon
Dioxide
Ethane,
Ethene,
Methane
Dissolved
Hydrogen
SM 5220D
SM 5210B
SM 3500-Fe D
SM 2320B
EPA 9056A
SM 9060A
SM4500-S F
SM 4500-CN-E
AM20GAX
MW-01
10/14/2020
MW-01-20201014
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-02
10/13/2020
MW-02-20201013
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-03
10/13/2020
MW-03-20201013
X
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-04
10/12/2020
MW-04-20201012
X
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-05R
10/12/2020
MW-05R-20201012
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-06
10/13/2020
MW-06-20201013
X
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-07
10/12/2020
MW-07-20201012
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Notes:
Appendix II constituents were analyzed per Title 40 Code of Federal Regulations, Part 258.
Blank cell: Analysis was not performed on that sample.
AM: Analytical Method
BOD: biochemical oxygen demand
COD: chemical oxygen demand
EPA: U.S. Environmental Protection Agency (method)
PCBs: Polychlorinated biphenyls
SIM: Selective Ion Monitoring
SM: Standard Method
SVOCs: Semi -volatile organic compounds
TB: Trip Blank
TOC: total organic carbon
VOC: volatile organic compound
Fall 2020 Semiannual Water Quality Monitoring Report Page 1 of 1
Jackson County Closed Municipal Solid Waste Landfill January 2021
Table 2
Well Construction Details and Corresponding Elevations
Stick Up
Depth to
Depth to
Elevation of
Ground
(feet
Depth To
Approximate
Approximate
Top of
Bottom of
Top Elevation
Bottom of
Surface
TOC
above
Total Well
Water
Depth to
Top of Bedrock
Screened
Screened
of Screened
Screened
Geology of
Source of Well
Elevation
Elevation
ground
Depth
(feet below
Groundwater
Bedrock
Elevation
Interval
Interval
Interval
Interval
Screened
Construction
Facility Permit
Well ID
Date Drilled
(feet)
(feet)
surface)
(feet bgs)
TOC)
Elevation (feet)
(feet bgs)
(feet)
(feet bgs)
(feet bgs)
(feet)
(feet)
Interval
Information
MW-01
04/23/1992
2,169.40
2,171.42
2.0
110.5
92.91
2,078.51
83.0
2,086.40
95.0
110.0
2,074.40
2,059.40
Bedrock
MW-02
04/22/1992
2,013.15
2,015.38
2.3
60.7
39.50
1,975.88
13.0
2,000.15
45.0
60.0
1,968.15
1,953.15
Bedrock
Partially
S&ME, Inc.
MW-03
04/21/1992
2,044.16
2,045.53
1.3
65.5
43.76
2,001.77
57.0
1,987.16
48.5
63.5
1,995.66
1,980.66
Weathered Rock
50-02
MW-04
04/21/1992
1,978.68
1,980.77
2.0
43.0
27.28
1,953.49
NA
NA
25.0
40.0
1,953.68
1,938.68
Saprolite
MW-05R
01/26/2012
2,027.98
2,030.95
2.8
54.0
43.58
1,987.37
NA
NA
44.0
54.0
1,983.98
1,973.98
Saprolite
MW-06
03/23/2004
2,136.58
2,139.57
3.0
94.0
76.04
2,063.53
47.6
2,088.98
84.6
94.6
2,051.98
2,041.98
Bedrock
Altamont
Environmental, Inc.
MW-07
07/30/2010
1,978.71
1,981.29
2.6
95.0
30.73
1,950.56
44.0
1,935.00
70.0
95.0
1,908.71
1,883.71
Bedrock
Notes:
Elevations associated with wells MW-01, MW-02, MW-03, MW-04, and MW-06 are measured relative to mean sea level and are based on surveying completed by Davenport & Associates, Inc.
Elevations associated with wells MW-05R and MW-07 are measured relative to horizontal North American Datum 83 and are based on surveying completed by Wes Cole Land Surveying, PA.
Depth to water was measured on October 12, 13, and 14, 2020 (Appendix A).
Depth to bedrock and screened interval for MW-01 through MW-04 was taken from S&ME, Inc., boring logs completed April 21 through 23, 1992.
Depth to bedrock and screened interval for MW-06 was taken from an Altamont Environmental, Inc., boring log completed March 23, 2004.
Depth to bedrock and screened interval for MW-07 was taken from an Altamont Environmental, Inc., boring log completed July 30, 2010.
Depth to bedrock and screened interval for MW-05R was taken from an Altamont Environmental, Inc., boring log completed January 26, 2012.
Monitoring well MW-05 was abandoned on January 26, 2012, by NYEG Drilling, LLC. Monitoring well MW-05R was installed by NYEG Drilling, LLC, on January 26, 2012, as a replacement to MW-05.
Monitoring well MW-05R was surveyed by Wes Cole Land Surveying, PA, on September 28, 2012.
bgs: below ground surface
NA: not applicable
TOC: top of casing
Fall 2020 Semiannual Water Quality Monitoring Report Page 1 of 1
Jackson County Closed Municipal Solid Waste Landfill January 2021
Table 3
Analytical Summary
Domestic Well
Sample
Leachate
Sample
Monitoring Well Samples
Surface Water Samples
QC Samples
Location ID
DW-01
LT-01
MW-01
MW-02
MW-03
MW-04
MW-05R
MW-06
MW-07
SW-01
SW-02
FieldQC
FieIdQC
FieIdQC
Sample ID
DW-01-
20201014
LT-01-
20201014
MW-01-
20201014
MW-02-
20201013
MW-03-
20201013
MW-04-
20201012
MW-0511-
20201012
MW-06-
20201013
MW-07-
20201012
SW-01-
20201014
SW-02-
20201014
TB-
202010120000
TB-
202010130000
TB -
202010140000
Sample Date
10/14/2020
10/14/2020
10/14/2020
10/13/2020
10/13/2020
10/12/2020
10/12/2020
10/13/2020
10/12/2020
10/14/2020
10/14/2020
10/12/2020
10/13/2020
10/14/2020
Sample Type
N
N
N
N
N
N
N
N
N
N
N
TB
TB
TB
Matrix
WG
WG
WG
WG
WG
WG
WG
WG
WG
WS
WS
WQ
WQ
WQ
X
730117.7
730041.8
729526.4
728841.4
729285.1
729406
729649.3
729170.4
729395.8
729383.4
728409
Y
618143.8
617628.1
618129.2
617869.4
617628.9
617105.4
617259.7
618177.5
617118.8
616840.8
618322.7
Method
NC2L
NC2L
IMAC
NC213
Conventional Parameters
Water Level Depth (ft)
Field Measure
--
--
92.91
39.5
43.76
27.28
43.58
76.04
30.73
--
--
-
-
Temperature (field) (°C)
Field Measure
16.1
20.2
15.8
18
17.9
17
26.3
16.5
16.8
15.7
16.1
-
-
pH (field) (SU)
Field Measure/SM4500
6.5-8.5
6.0-9.0
6.46
6.88
5.7
7.1 #
8.11
S.7S
6.82
7.11
6.07
6.36
6.6
--
-
Turbidity (field) (NTU)
Field Measure
:550
7.74
8.2
10
>1,000
5.19
3.94
53.7
5.99
7.06
36.9
29
--
-
Dissolved oxygen (field)
Field Measure
>_6
4.86
1.67
1.47
5.08
3.28
2.11
1.43
1.55
1.79
10.35
10.67
--
-
Specific Conductivity (field) (µS/cm)
Field Measure
70.5
3384
210.3
218.4
324
424.1
668
52.8
758
36.7
26.7
--
--
ORP (mV)
Field Measure
186.7
-85.1
30.5
-57.3
-112.4
302.8
-130
-139.9
138.4
127.9
153.6
--
--
Hardness as CaCO3 (mg/L)
SM2340C
--
--
--
--
Monitored Natural Attenuation Results
Alkalinity, Total (µg/L)
SM2320B
20000
100000
55000
140000
64000
240000
24000
250000
Biochemical oxygen demand (mg/L)
SM5210B
--
--
3.1
2.3
2 J
0.38 J
5.2
0.28 J
0.92 J
--
--
--
--
Chemical oxygen demand (mg/L)
SM5220C
--
--
24 J
37 J
35 J
13 J
42 J
11 U
18 J
--
--
--
--
Chloride (mg/L)
SW9056A
250
230
--
--
1.2
25
8.5
24
55
1.1
79
--
--
--
--
Cyanide (mg/L)
9014
70
0.014 U
0.014 U
0.014 U
0.014 U
0.014 U
0.014 U
0.014 U
Nitrate as nitrogen (mg/L)
SW9056A
--
--
0.045 U
0.17 J
8.3
6.5
0.075 J
0.096 J
0.092 J
--
--
--
--
Sulfate (mg/L)
SW9056
250
--
--
0.56 U
20
4
91
0.56 U
0.83 J
25
--
--
--
--
Sulfide (mg/L)
SM4500S2F
--
--
0.83 U
0.83 U
0.83 U
0.83 U
5
0.83 U
0.83 U
--
--
--
--
Total organic carbon (mg/L)
SM5310B
--
--
1.78
2.26
4.68
2.05
7.05
1.04
3.22
--
--
--
--
Ferrous iron (µg/L)
SM3500FEB
1000
--
--
39000
46 U
46 U
46 U
12000
46 U
360
--
--
--
--
-
Hydrogen (nM)
EPA RSK-175
--
--
43
10
--
4.1
10
Methane (µg/L)
AM20GAX
--
--
4000
5
3.5
390
3700
140
640
--
--
--
--
--
Acetic acid (mg/L)
AM23G
5000
--
--
0.45 J
0.76
0.95
0.54
4.2 J
0.58
0.45 J
--
--
--
--
--
Formic acid (mg/L)
AM23G
--
--
5.4
5.1
4.8
4.8
50
5
4.8
--
--
--
--
--
Lactic Acid (mg/L)
AM23G
0.053 U
0.053 U
0.072 J
0.053 U
0.53 U
0.053 U
0.53 U
Propionic Acid (mg/L)
AM23G
0.053 U
0.053 J
0.056 J
0.053 U
0.53 U
0.054 J
0.53 U
Carbon dioxide (µg/L)
AM20GAX
--
--
128000
37100
14700
99300
45300
159000
178000
--
--
--
--
--
Appendix II Metals, Total (Ng/L)
Arsenic
SW6020
10
10
--
2.9
0.17 U
7.5
0.31 J
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
--
--
--
Barium
SW6020
700
21000
--
500
100
250
110
81
110
47
390
16
16
--
--
-
Beryllium
SW6020
4
--
0.19 U
0.19 U
1.6
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
--
--
--
Cadmium
SW6020
2
*0.21
--
0.16 U
0.17 J
0.16 U
0.16 U
0.24 J
0.16 U
0.16 U
0.16 U
0.16 U
0.16 U
--
--
--
Chromium
SW6020
10
*6.63
--
2.S
0.99 J
61
0.86 J
0.79 U
0.79 U
0.79 U
0.9 J
0.86 J
0.94 J
--
--
--
Cobalt
SW6020
1
--
3.8
160
60
0.59 J
1.7 J
8.3
9
1.4 J
0.52 U
0.52 U
--
--
--
Copper
SW6020
1000
*0.72
--
3.8 U
3.8 U
61
3.8 J
3.8 U
5.5 J
3.8 U
3.8 U
3.8 U
3.8 U
--
--
-
Lead
SW6020
15
*0.09
--
0.26 U
0.26 U
14
0.26 U
0.26 U
0.26 U
0.26 U
0.26 U
0.3 J
0.38 J
--
--
--
Mercury
SW7470
1
--
0.23
1.1
0.87
1.1
1
0.73
1.3
0.53
1.1
0.95
--
--
--
Nickel
SW6020
100
*4.30
--
20
16
44
0.96 J
1 J
2.7 J
3.4
7.1
1.5 J
1.5 J
--
--
-
Selenium
SW6020
20
5
--
0.79 J
1 J
42
0.74 U
2.3 J
0.85 J
0.74 U
0.74 U
0.74 U
0.85 J
--
--
-
Thallium
SW6020
0.2
0.38 U
0.38 U
0.96 J
0.38 U
0.38 U
0.38 U
0.38 U
0.38 U
0.38 U
0.38 U
Vanadium
SW6020
0.3
2.4 J
7.3 U
71
7.3 U
7.3 U
7.3 U
7.3 U
7.3 U
1.3 U
1.3 U
Zinc
SW6020
1000
*9.72
--
6.9 U
11 J
140
6.9 U
6.9 U
18 J
20 J
6.9 U
6.9 U
6.9 U
--
--
--
Fall 2020 Semiannual Water Quality Monitoring Report Page 1 of 3
Jackson County Closed Municipal Solid Waste Landfill January 2021
Table 3
Analytical Summary
Domestic Well
Sample
Leachate
Sample
Monitoring Well Samples
Surface Water Samples
QC Samples
Location ID
DW-01
LT-01
MW-01
MW-02
MW-03
MW-04
MW-05R
MW-06
MW-07
SW-01
SW-02
FieldQC
FieIdQC
FieIdQC
Sample ID
DW-01-
20201014
LT-01-
20201014
MW-01-
20201014
MW-02-
20201013
MW-03-
20201013
MW-04-
20201012
MW-0511-
20201012
MW-06-
20201013
MW-07-
20201012
SW-01-
20201014
SW-02-
20201014
TB-
202010120000
TB-
202010130000
TB -
202010140000
Sample Date
10/14/2020
10/14/2020
10/14/2020
10/13/2020
10/13/2020
10/12/2020
10/12/2020
10/13/2020
10/12/2020
10/14/2020
10/14/2020
10/12/2020
10/13/2020
10/14/2020
Sample Type
N
N
N
N
N
N
N
N
N
N
N
TB
TB
TB
Matrix
WG
WG
WG
WG
WG
WG
WG
WG
WG
WS
WS
WQ
WQ
WQ
X
730117.7
730041.8
729526.4
728841.4
729285.1
729406
729649.3
729170.4
729395.8
729383.4
728409
Y
618143.8
617628.1
618129.2
617869.4
617628.9
617105.4
617259.7
618177.5
617118.8
616840.8
618322.7
Method
NC2L
NC2L
IMAC
NC213
Appendix II Metals, Dissolved (Ng/L)
Antimony SW6020
1
--
-
--
0.49 U
--
-
0.49 U
-
--
0.49 U
0.54 J
--
-
Arsenic SW6020
10
10
--
--
--
0.17 U
--
-
0.17 U
-
--
0.17 U
0.17 U
--
-
-
Barium SW6020
700
21000
--
--
--
24
--
-
60
-
--
12
10
--
--
-
Cobalt SW6020
1
--
--
--
0.52 U
--
--
8.3
-
--
0.52 U
0.52 U
--
--
-
Nickel SW6020
100
-4.30
--
--
--
0.81 J
--
--
1.4 J
--
--
0.51 U
0.51 U
--
--
-
Selenium SW6020
20
5
--
--
--
1.3 J
--
--
0.74 U
--
--
0.74 U
0.74 U
--
--
--
Zinc SW6020
1000
-9.72
--
--
--
6.9 U
--
--
181
--
--
6.9 U
6.9 U
--
--
--
Appendix II Volatile Organic Compounds (VOCs) and 1,4-Dioxane (Ng/L)
1,1-Dichloroethane
SW8260
6
100
0.00050 U
0.083 U
2.8
0.29 J
0.083 U
0.083 U
0.083 U
1.4
0.083 U
0.083 U
0.083 U
0.083 U
0.083 U
0.083 U
1,2,4-Trichlorobenzene
SW8260
70
0.076
0.00050 U
0.13 U
0.13 U
0.13 U
0.13 U
0.13 U
0.13 U
0.13 U
0.23 J
0.73 U
0.73 U
0.13 U
0.13 U
0.13 U
1,2-Dichlorobenzene
SW8260
20
400
0.00050 U
0.076 U
0.22 J
0.076 U
0.076 U
0.076 U
0.076 U
0.076 U
0.5
0.076 U
0.076 U
0.076 U
0.076 U
0.076 U
1,2-Dichloroethene, cis-
SW8260
70
720
0.00050 U
0.29 J
4.5
0.38 J
0.056 U
0.46 J
0.41 J
1.4
2.6
0.056 U
0.056 U
0.056 U
0.056 U
0.056 U
1,3-Dichlorobenzene
SW8260
200
--
0.27 J
0.054 U
0.054 U
0.054 U
0.054 U
0.054 U
0.054 U
0.054 U
0.054 U
0.054 U
0.054 U
0.054 U
0.054 U
1,4-Dichlorobenzene
SW8260
6
56
0.00050 U
4.8
9.8
0.05 U
0.05 U
0.85
0.89
2.6
6.8
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
1,4-Dioxane
SW8260
3
--
58
0.14 U
2.8
0.14 U
3.4
3.5
0.14 U
17
0.14 U
0.14 U
--
--
--
Acetone
SW8260
6000
2000
--
11
5.7
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
0.31 U
3.2 J
3 J
3 J
Acetonitrile (Ethanenitrile)
SW8260
--
4.7 J
3 U
3 U
3 U
3 U
3 U
3 U
3 U
3 U
3 U
3 U
3 U
3 U
Benzene
SW8260
1
51
0.00050 U
2.4
1.5
0.048 U
0.048 U
0.048 U
0.048 U
0.26 J
1.4
0.048 U
0.048 U
0.048 U
0.048 U
0.048 U
Chlorobenzene
SW8260
50
140
0.00050 U
4.4
1.9
0.062 U
0.062 U
0.69
0.67
0.41 J
6.1
0.062 U
0.062 U
0.062 U
0.062 U
0.062 U
Chloroethane
SW8260
3000
--
0.47 J
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
Dichlorodifluoromethane
SW8260
1000
--
0.11 U
0.11 U
0.11 U
0.11 U
0.23 J
0.3 J
0.11 U
0.11 U
0.11 U
0.11 U
0.11 U
0.11 U
0.11 U
Ethylbenzene
SW8260
600
97
0.00050 U
1.8
0.33 J
0.061 U
0.061 U
0.061 U
0.061 U
0.061 U
0.061 U
0.061 U
0.061 U
0.061 U
0.061 U
0.061 U
m,p-Xylene
SW8260
500
500
--
1.7
0.83 J
0.21 J
0.37 J
0.31 J
0.27 J
0.37 J
0.42 J
0.12 U
0.12 U
0.12 U
0.12 U
0.12 U
Naphthalene
SW8260
6
--
13
0.3 U
0.3 U
0.3 U
0.3 J
0.3 U
0.3 U
0.3 U
0.87 J
0.3 U
0.3 U
0.3 U
0.3 U
o-Xylene
SW8260
500
400
--
2
0.26 J
0.044 U
0.044 U
0.044 U
0.044 U
0.29 J
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
Tetrachloroethene (PCE)
SW8260
0.7
3.3
0.00050 U
0.098 U
0.48 J
0.098 U
0.098 U
0.098 U
0.098 U
0.25 J
0.098 U
0.098 U
0.098 U
0.098 U
0.098 U
0.098 U
Tetrahydrofuran
SW8260
--
94
1.1 U
1.1 U
1.1 U
1.1 U
1.1 U
1.1 U
1.6 J
1.1 U
1.1 U
1.1 U
1.1 U
1.1 U
Toluene
SW8260
600
0.36
0.00050 U
0.79
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
0.044 U
Total Xylene
SW8260
0.0010 U
3.7
1.11
0.21 J
0.37 J
0.31 J
0.27 J
0.66 J
0.42 J
0.15 U
0.15 U
0.15 U
0.15 U
0.15 U
Trichloroethene (TCE)
SW8260
3
30
0.00050 U
0.078 U
0.57
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
0.078 U
Vinyl chloride
SW8260
0.03
2.4
0.00050 U
0.22 J
0.31 J
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
0.097 U
Appendix II Semivolatile Organic Compounds (SVOCs) (Ng/L)
1,2-Dichlorobenzene
SW8270
20
470
--
--
0.661 U
0.647 U
0.843
0.629 U
0.629 U
0.699 U
0.629 U
0.839 U
0.647 U
--
--
--
1,3-Dichlorobenzene
SW8270
200
--
--
0.516 U
0.505 U
0.791
0.491 U
0.491 U
0.545 U
0.491 U
0.654 U
0.505 U
--
--
--
1,4-Dichlorobenzene
SW8270
6
56
--
--
4.94
0.597 U
0.746
0.58 U
3.41
0.779
2.66
0.773 U
0.597 U
--
--
--
Dibenzofuran
SW8270
28
--
--
0.444 U
0.435 U
0.427 U
0.423 U
0.518
0.47 U
0.423 U
0.564 U
0.435 U
--
--
--
Diethyl phthalate
SW8270
6000
--
--
1.16
4.65
0.59 U
0.585 U
2.28
0.709
0.585 U
0.78 U
0.602 U
--
--
--
Appendix II Pesticides (Ng/L)
Hexachlorocyclohexane (BHC), beta-
SW8081
0.02
--
--
0.011 U
0.011 U
0.011 U
0.011 U
0.011 U
0.14
0.011 U
0.011 U
0.011 U
--
--
--
Hexachlorocyclohexane (BHC), gamma- (Lindane)
SW8081
0.03
--
--
0.051
0.0063 U
0.0062 U
0.0062 U
0.01 J
0.0062 U
0.0061 U
0.0061 U
0.0062 U
--
--
--
Appendix II Herbicides (pg/L)
2,4,5-TP (Silvex)
SW8151
50
--
--
0.01634 U
0.01634 U
0.01634 U
0.01634 U
0.08098
0.01634 U
0.01634 U
0.01634 U
0.01634 U
--
--
--
2,4-D (2,4-Dichlorophenoxyacetic acid)
SW8151
70
--
--
0.3728
0.2078 U
0.2078 U
0.2078 U
0.2078 U
0.2078 U
0.2078 U
0.2078 U
0.2078 U
--
--
--
Fall 2020 Semiannual Water Quality Monitoring Report Page 2 of 3
Jackson County Closed Municipal Solid Waste Landfill January 2021
Table 3
Analytical Summary
Notes:
'Detected concentration is greater than NC2L or NC2L IMAC standard
Detected concentration is greater than NC213 standard
Bold: Detected result
Italicized: Non -detected concentration is above one or more identified NC2L standard
*: 2B surface water standard calculated using average analyzed hardness value (calculated from the upstream and downstream sampling location results) via the most stringent hardness -dependent metal calculation, per North Carolina Administrative Code, Title 15A: Department of Environmental Quality,
Subchapter 2B - Surface Water and Wetland Standards (last amended September 2017).
NC26: surface water standard per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 213 — Surface Water and Wetland Standards (last amended in September 2017), or the standard obtained from the EPA Nationally Recommended Water Quality Criteria for
Aquatic Life and Human Health.
NC2L: Subchapter 2L — Groundwater Classifications and Standards, Department of Environmental Quality (Amended April 1, 2013). Groundwater standard from North Carolina Administrative Code, Title 15A.
All nondetect results are reported at the method detection limit.
Appendix II: per 40 Code of Federal Regulations Part 258
Horizontal coordinate datum is NAD 1983 State Plane North Carolina FIPS 3200 (US Survey Feet).
--: not sampled
°C: degrees Celsius
Ng/L: micrograms per liter
ft:feet
IMAC: Interim Maximum Allowable Concentration. IMAC concentrations are listed in Appendix #1 of the 2L.
N: The laboratory does not hold NELAP/TNI accreditation for thi method or analyte
J: Estimated value
mg/L: milligrams per liter
mv: millivolts
N: normal environmental sample
NTU: nephelometric turbidity unit
ORP: oxidation-reduction potential
SU: standard unit
SW: surface water
TB: Trip Blank
U: Compound analyzed for, but not detected above minimum detection limit
WG: groundwater sample
WQ: water quality
I = sample analyzed in laboratory using EPA Method SM4500, because of field equipment malfunction
Fall 2020 Semiannual Water Quality Monitoring Report Page 3 of 3
Jackson County Closed Municipal Solid Waste Landfill January 2021
Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the Leachate Sample (LT-01)
Sample Dates
Detected Volatile Organic
Compounds
Concentration
in LT-01
(mg/L)
Cumulative
Flow at Gauge
(gallons)
Differential
Flow
(gallons)
Mass
Removed
(pounds)
Estimated Cumulative
Mass Removed
(pounds)
Beginning
Ending
09/01/2012
10/25/2012
1,4-Dichlorobenzene
0.0034
11,500
11,500
0.00033
4-Meth I-2- entanone (MIBK)
0.0021
J
0.00020
Acetone
0.0292
0.00280
Benzene
0.0021
0.00020
Chlorobenzene
0.0029
0.00028
cis- 1,2-Dichloroethene
0.00063
J
0.00006
Dichlorodifluoro-methane
0.00093
J
0.00009
Eth (benzene
0.0102
0.00098
Naphthalene
0.0069
0.00066
Styrene
0.00033
J
0.00003
Toluene
0.003
0.00029
X lene (Total)
10.0094
0.00090
Total
0.00682
0.00682
10/26/2012
04/11/2013
1,4-Dichlorobenzene
0.006
65,500
54,000
0.00270
Acetone
0.012
J
0.00540
Benzene
0.0011
0.00049
Carbon disulfide
0.0067
J
0.00301
Chlorobenzene
0.0024
J
0.00108
cis- 1,2-Dichloroethene
0.00058
J
0.00026
Eth (benzene
0.0083
0.00373
Toluene
0.00059
J
0.00027
X lene (Total)
0.0078
0.00351
Total
0.02045
0.02727
04/12/2013
10/08/2013
1,4-Dichlorobenzene
0.0055
114,737
49,237
0.00226
4-Meth I-2- entanone (MIBK)
0.0012
J
0.00049
Benzene
0.0020
0.00082
Chlorobenzene
0.0039
0.00160
cis- 1,2-Dichloroethene
0.00080
J
0.00033
Eth (benzene
0.0151
0.00619
Naphthalene
0.0184
0.00754
Toluene
0.0012
0.00049
X lene (Total)
0.0090
0.00369
Total
0.02341
0.05068
10/09/2013
04/08/2014
1,4-Dichlorobenzene
0.0056
168,821
54,084
0.00252
Benzene
0.0018
0.00081
Chlorobenzene
0.0051
0.00230
cis- 1,2-Dichloroethene
0.00049
J
0.00022
Eth (benzene
0.0047
0.00212
Toluene
10.00041
1 J
0.00018
X lene (Total)
10.0021
1 J
0.00095
Total
0.00910
0.05978
04/08/2014
10/23/2014
1,4-Dichlorobenzene
0.0053
179,652
10,831
0.00048
Benzene
0.0014
0.00013
Chlorobenzene
0.003
0.00027
cis- 1,2-Dichloroethene
0.00049
J
0.00004
Eth (benzene
10.0027
0.00024
Toluene
10.00051
1 J
0.00005
X lene (Total)
10.0014
1 J
0.00013
Total
0.00133
0.06111
10/23/2014
04/21/2015
1,2,3-Trimethyl benzene
0.00062
219,965
40,313
1,2,4-Trimethyl benzene
0.00076
0.00026
2-Chlorotoluene
0.00067
0.00022
1,4-Dichlorobenzene
0.0059
0.00198
Acetone
0.00790
0.00265
Benzene
0.0022
0.00074
Chlorobenzene
0.003
0.00101
Eth (benzene
0.0056
0.00188
Isopropyl benzene
0.0013
0.00044
Methy Tert-but I -Ether
0.0013
0.00044
Na thalene
0.024
0.00806
n-Propylbenzene
0.00088
0.00030
Tetrah drofuran
0.089
0.02988
Toluene
0.00054
J
0.00018
Vin I Chloride
0.00038
J
0.00013
X lene (Total)
10.0030
J
0.00101
Total
0.04937
0.11048
04/21/2015
10/13/2015
1,4-Dichlorobenzene
0.00600
256,685
36,720
0.00183
2-Butanone
0.00960
J
0.00294
Benzene
0.00210
0.00064
Chlorobenzene
0.0040
0.00122
Ethylbenzene
0.00710
0.00217
m, -X lenes
0.0014
0.00043
Naphthalene
0.021
0.00642
o-X lene
0.0017
0.00052
Tetrah drofuran
0.062
0.01896
Toluene
0.00058
J
0.00018
Total X lenes
0.0031
J
0.00095
Total
0.03626
0.14674
10/13/2015
04/05/2016
1,4-Dichlorobenzene
0.00590
315,663
1
58,978
0.00290
Benzene
0.00170
0.00083
Chlorobenzene
0.0038
0.00187
Eth (benzene
0.00500
0.00246
m, -X lenes
0.0010
0.00049
o-X lene
10.0015
1
0.00074
Toluene
10.00063
1 J
0.00031
Total X lenes
10.0025
1 J
0.00123
Total
0.01082
0.15756
04/05/2016 10/11/20161 No detected compounds. 331,010 1 15,347
0.00000
Total
0.00000
0.15756
Fall 2020 Semiannual Water Quality Monitoring Report Page 1 of 2
Jackson County Closed Municipal Solid Waste Landfill January 2021
Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the Leachate Sample (LT-01)
Sample Dates
Detected Volatile Organic
Compounds
Concentration
in LT-01
(mg/L)
Cumulative
Flow at Gauge
(gallons)
Differential
Flow
(gallons)
Mass
Removed
(pounds)
Estimated Cumulative
Mass Removed
(pounds)
Beginning
Ending
10/11/2016
03/21/2017
1,4-Dichlorobenzene
0.0046
334,212
3,202
0.00012
Acetone
0.0094
J
0.00025
Benzene
0.0015
0.00004
Chlorobenzene
0.0043
0.00011
Eth (benzene
0.0014
0.00004
m, -X lenes
0.0006
J
0.00002
o-X lene
0.00092
0.00002
Tetrah drofuran
10.066
1
0.00176
Total X lenes
10.0015
1 J
0.00004
Total
0.00241
0.15997
03/21/2017
10/11/2017
1,4-Dichlorobenzene
0.0041
364,76054
0. 4
Acetone
0.0067
J
0.00170
Acetonitrile
0.008
J
Benzene
0.00061
Chlorobenzene
0.0012
0.00031
Eth (benzene
10.00087
0.00022
Naphthalene
10.0012
0.00031
Tetrahydrofuran
10.12
0.03053
Total
0.03630
0.19627
Issue with totalizer
between October 2017 and March 2018
03/21/2018
10/18/2018
1,4-Dichlorobenzene
0.0028
1,784,710 159,341
0.00372
Acetone
0.017
0.02256
Benzene
0.0012
0.00159
Chlorobenzene
0.0024
0.00318
Eth (benzene
0.0018
0.00239
m, -X lenes
0.00038
J
0.00050
Methylene Chloride
0.00034
J
0.00045
o-X lene
0.00060
0.00080
X lenes, Total
0.00098
J
0.00130
Total
0.04
0.23
10/18/2018
10/22/2019
1,4-Dichlorobenzene
0.0037
2,045,960 261,250
0.00805
Acetone
0.006
1
0.01305
Benzene
0.0017
0.00370
Chlorobenzene
0.0038
0.00827
Eth (benzene
0.0016
0.00348
o-X lene
10.00110
1
0.00239
Toluene
10.00039
1 J
0.00085
X lenes, Total
10.0017
1 J
0.00370
Total
0.04
0.28
10/22/2019
03/18/2020
1,4-Dichlorobenzene
0.0056
2,139,992 94,032
0.00438
1,4-Dioxane
0.06
0.04697
Acetone
0.0064
0.00501
Benzene
0.0013
0.00102
Chlorobenzene
0.0032
0.00250
Eth (benzene
0.0027
0.00211
m, -X lenes
0.00089
J
0.00070
Methyl isobut I ketone
0.00079
J
0.00062
o-X lene
0.00120
0.00094
Toluene
0.00070
0.00055
Total
0.06
0.34
03/18/2020
10/14/2020
1,2-Dichloroethene, cis-
0.00029
J
2,238,782 98,790
0.00024
1,3-Dichlorobenzene
0.00027
J
0.00022
1,4-Dichlorobenzene
0.0048
0.00395
1,4-Dioxane
0.058
0.04770
Acetone
0.011
0.00905
Acetonitri e (Et anenrtn e)
0.0047
J
0.00387
Benzene
0.0024
0.00197
Chlorobenzene
0.0044
0.00362
Chloroethane
0.00047
J
0.00039
Eth (benzene
0.0018
0.00148
m, -X lene
0.0017
0.00140
Naphthalene
0.013
0.01069
o-X lene
0.002
0.00164
Tetrah drofuran
0.094
0.07731
Toluene
0.00079
0.00065
Total X lene
0.0037
0.00304
Vinyl chloride
0.00022
J
0.00018
Total
0.17
0.51
N otes:
1. No VOCs were detected in the leachate sample collected during the October 2016 sampling event.
Only detected volatile organic compounds (VOCs) in leachate sample LT-01 are included in the mass removal calculation.
Leachate extraction at the landfill was initiated on September 1, 2012.
Extraction volume measurements were recorded and provided by Jackson County staff.
Anchor QEA bases mass removal calculations on the assumption that the VOCs concentration in one sampling event is representative of leachate quality until the next sampling event occurs,
and that the leachate removal system has a 100% removal and treatment efficiency.
Due to a malfunction with the leachate totalizer, there is a gap in total volume calcuations between October 11, 2017 and March 21, 2018.
Represents the total flow between the LT-01 sample dates.
Estimated cumulative mass removed and treated is estimated based upon a conversion of milligrams to pounds and liters to gallons and the multiplication of the concentration by the
differential flow for the specified period.
mg/L: milligrams per liter
J: Indicates laboratory estimated concentration is above the adjusted method detection limit and below the adjusted reporting limit.
Fall 2020 Semiannual Water Quality Monitoring Report Page 2 of 2
Jackson County Closed Municipal Solid Waste Landfill January 2021
Figures
LI
UA
�� 1(� _'� � _., „� • `� +lf# III. ---• ��
� � r„ `L•i �:L.` �y��� f � i ///�/ it 2
\1 �JP\ f l
LEGEND: SOURCES:
1. BaUSGS Topographic Maps Greens
® Site Parcel Boundary Creekk and Whittier 7.5-minute Quadrangles
2. Parcel: Jackson County GIS
0 2,000
Feet
Publish Date: 2020/11/23, 8:10 AM I User: alesueur
Filepath:\\orcas\gisVobs\)acksonCounty_NC_1480\Maps\2020\FallWQ\AQ_Fig01_JacksonCounty_SpringWQ2020_SiteLocationMap.mxd
)P, ANCHOR Figure 1
Q E A Site Location Map
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
-02
le MW-03 LT-01
VkV9 1 n
MW-05R G11 ,
I
MW-07 MW-04 s
• 5W-01
O G
u
4 LF
LEGEND: NOTE:
41- Sample locations are approximate.
Monitoring Well — Road
Landfill Gas Extraction Well Elevation Contour (-Foot SOURCES:
Ct20Ft Interval) � Aerial Imagery: Esri Online Services
® Domestic Well Sample Location 0 Property Boundary Contours, Roads, and Parcels: Jackson County GIS
Leachate Sample Location and
Flow Equalization Tank
0 Surface Water Sample Location
Publish Date: 2020/11/23, 8:12 AM I User: alesueur
Filepath:\\orcas\gisVobs\JacksonCounty_NC_1480\Maps\2020\FaIIWQ\AQ_Fig02_JacksonCounty_SpringWQ2020_SampleLocationMap.mxd
n
0 500
Feet
11
kZANCHOR Figure 2
QEA-- Site Layout Map
Anchor QEA of North Carolina, PLLC
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
LEGEND:
® Saprolite Monitoring Well — Stream
® PWR Monitoring Well — Road
® Bedrock Monitoring Well Elevation Contour (20-Foot Interval)
Property Boundary (2,001.77) Groundwater Elevation
(October 12, 13, and 14, 2020)
immAi-nti
\ 2100
CONN
27g0
2120 aGS"C'
O
ta\`��eGtOG�
t
Ge � feat
Q� dot
•MW-03 0
(2,001.77) N
2�AO 60
Z c
3
Cqt o Q
w°
MW-07 \
,950.56)
MW-04
(1,953.49)
WILKEY
218
•MW-05R
i
2020
0987.37)
NOTES:
1. Monitoring well locations are approximate.
2. Groundwater elevations and flow direction are updated on a semiannual basis following sample collection events
in March and October.
3. Groundwater flow direction is based on groundwater elevations from all Site monitoring wells. Direction is
calculated based on depth to water measured on October 12, 13, and 14, 2020.
4. Last names of property owners are shown in parcels that border the landfill property.
5. PWR: partially weathered rock
6. Groundwater elevation in feet (North American Vertical Datum 1988)
Publish Date: 2020/11/23, 8:22 AM I User: alesueur
Filepath:\\orcas\gis\lobs\JacksonCounty_NC_1480\Maps\2020\FallWQ\AQ_Fig03_JacksonCounty_SpringWQ2020_GroundwaterElevationMap.mxd
WILKEY
WILKEY
0
N
/ Y
SOURCES:
1. Elevation contours, roads, and parcels: Jackson County GIS
2. Groundwater elevations: calculated from surveys
performed by Davenport & Associates, Inc. (MW-01, MW-02,
MW-03, MW-04, and MW-06) and Wes Cole Land Surveying,
PA (MW-05R and MW-07)
WILKEY
2100
0
0 200
Feet
N
0
Z}�
ANCHOR Figure 3
QEA—`-�" Generalized Groundwater Flow Direction
Anchor QEA of North Carolina, PLLC
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill
Figure 4
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-01)
20
in
16
J
a1
14
0
r 12
a
V
_
0 10
a,
a,
= 8
a,
0
6
s0
V
G
4
2
X
r` r` co Co M M O O — N
O O O O O
N
M m
� � v2
u2
R R
r: w 02 rn rn
o 0
N N
O O OO O O O O O CD O O
N N N N N N N N N N N
O
N
O CD
N N
CD
N N N
O
N
O E.
N N
CD O CD E. CD CDO
N N N N N N
O
N N
0- U 0- U 0- U 0- U 0- U 0-
Q 0 Q 0 < 0 Q 0 Q 0 Q
U
0
0- U
Q 0
0- U 0-
< 0 Q
U
0
0- U
< 0
M U M U M U
2 0 g 0 2 0
M U
2 0
Notes:
1. NCH (2013) Standard = 6 micrograms per liter (µg/L)
g Samp lin Date
O 1,4-Dichlorobenzene
2. "J" indicates result is estimated by laboratory.
NC2L (2013) Standard
3. "<" indicates result is less than method detection limit.
4. Oct 2017 result reported in semivolatile organic compound list.
t Groundwater Elevation
2080
2078
INIYL
a
2074 o
a
a
W
2072
r
3
2070 3
0
1.2
2066
2064
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 January 2021
Figure 5
Hydrograph and Benzene Concentration vs. Time
(Monitoring Well MW-01)
12
10
2
X
r` r` e0 00 M rn o o N N m m t � 2 �2 R R w ao rn rn o 0
O O O O O O N N
O O O O O O O O CD CD O O CD CD CD E. CD O CD E. CD CDO O
N N N N N N N N N N N N N N N N N N N N N N N N N N N N
Q U Q UQ U Q U U Q U Q U Q U 0-U Q U M U M U U M U
�(< �(
Q 0 Q 0 0 Q 0 Q 0 Q 0 Q 0 0 Q 0 0 2 0 g 0 0 2 0
Notes:
1. NC21- (2013) Standard = 1 microgram per liter (µg/L) Sampling Date O Benzene
2. "J' indicates result is estimated by laboratory. NC2L (2013) Standard
3. "U" indicates result is less than method detection limit. *Groundwater Elevation
2080.00
2078.00
2076.00
2074.00
2072.000
2070.00`i
W
3
2068.00=
0
L
W
2066.00
2064.00
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 January 2021
Figure 6
Hydrograph and Vinyl Chloride Concentration vs. Time
(Monitoring Well MW-01)
1•
1
_ 0.7
0 0.6 - <0.58
L
r
C
0.5
C
O
V
0.4
L
0
s
0.3
0.1
0
ISI
2078
g1XIII
d
a
2074 0
a
W
2072
3
0.31 1 2070 c
n
1` r` 00 a0 M M O O
N N
M M
'IT
Iq u>
Ln
lfl
lfl
r- r` 00 a0 M M
O O
O O O O O O O O O O
N N N N N N N N N N
O O
N N
O O
N N
O
N
O O
N N
O
N
O
N
O
.
O O O O O O
N N N N N N
O O
N N
Q U V V V Q V
a o a o a o a o a o
V
Q o
Q V
a o
a
V
o a
V
o
Q
a
U
o
ro V ro V co V
2 o 2 o 2 o
fu V
2 o
Notes:
1. NC2L (2013) Standard = 0.03 micrograms per liter (µg/L)
Sampling
p g
Date
Vinyl chloride
2. "J" indicates result is estimated by laboratory.
NC21- (2013) Standard
3. " < " indicates result is less than method detection limit
0 Groundwater Elevation
1.E
2066
2064
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 January 2021
Figure 7
Hydrograph and 1,4-Dioxane Concentration vs. Time
(Monitoring Well MW-04)
12
WE
2
X
ao _rn a,
O O O
N N N
U U L (O
0
Notes:
1. NC21- (2018) Standard 2L Standard = 3 micrograms per liter (µg/L) Sampling Date
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
O O
N N
O O
N N
i U
fp V
> 0
O 1,4-Dioxane
NC2L (2018) Standard
*Groundwater Elevation (feet)
1960
1955
1950
1945 W
L
_
1940 0
L
to
1935
1930
January 2021
Figure 8
Hydrograph and 1,4-Dioxane Concentration vs. Time
(Monitoring Well MW-0511)
10.0
.E
:e
O
, 5.0
d
= 4.0
O
V
3.0
M
x
O
p 2.0
1.0
M
00 _rn _rn O
N
O O O O
N N N N
O g O g
Notes:
1. NCH (2018) Standard = 3 micrograms per liter (µg/L) Sampling Date
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
O
N
O
N
v
O
O 1,4-Dioxane
NC2L (2018) Standard
*Groundwater Elevation
1988
1986
a,
1984
a
O
.a
1982 „—°',
a�
�a
1980 C=
0
0
iGy%111111111111111
1976
January 2021
Figure 9
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-07)
8.0
6.0
c 4.0
u
2.0
C
11
N N n2 M It � L2 l2 lR lR
O O O O O O O O O O O (D
N N N N N N N N N N N N
Q V Q V Q V Q V Q V Q V
a o a o a o a o a o a o
Notes: Sampling Date
1. NC21- (2013) Standard = 6 micrograms per liter (µg/L)
2. "J" indicates result is estimated by laboratory
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
r` r` W 00 Ol 61 O O
N N
O O O O O O O O
N N N N N N N N
M V (6 V (p V (6 V
o o o o
1,4-Dichlorobenzene
NC2L (2013) Standard
0 Groundwater Elevation
1951
1951
1950
1950
0
1949
a,
W
L
1949
3
_
1948 0
ID
1948
1947
1947
January 2021
Figure 10
Hydrograph and 1,4-Dioxane Concentration vs. Time
(Monitoring Well MW-07)
30
25
20
I
02 rn rn CD 0
0 0 0 0 0
N N N N N
V 6 U c0 U
0 g O g 0
Notes:
1. NC21- (2018) Standard = 3 micrograms per liter (µg/L)
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Sampling Date 1,4-Dioxane
NC2L (2018) Standard
4 Groundwater Elevation
1951
1951
1950
1950
1949
1949
1948
1948
January 2021
Figure 11
Hydrograph and Benzene Concentration vs. Time
(Monitoring Well MW-07)
2
flu
1.6
J
1.4
0
1.2
L
_
GJ
1
0
v
a
0.8
N
_
GJ
ca
1A
0.2
A
N N m_ m2
v
L2 �2 �2 �2
o
0
O O
O O O O
O
O
O O O O
O O
lV
O O O O O
fV
O
N N
N N N N
N
N
N N N N
rQ N
N N N N N
N
Q V
Q O
Q U Q V
Q O Q O
Q
Q
U
O
Q U Q V
Q O Q O
(6 V
g O
c6 V (6 U c6
O g O
U U
O
Sampling Date
Benzene
Notes:
1. NC2L (2013) Standard
= 1 microgram per liter (µg/L)
NC2L (2013) Standard
2. "<" indicates result is less
than method detection limit.
--*—Groundwater Elevation
1951
1951
1950
0
1950 „°—,'
a,
_
1949 c
0
1949
1948
Fall 2020 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 January 2021
Appendix A
Well Sampling Logs, and Equipment
Documentation and Instrument
Calibration Data Sheets
I
ANCHOR
C,2EA
Nell Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill
Date:
y `�
Project Number:
- Q�
Weather.
o.
Sampling Personnel: �.
_
Sample Time:
Well ID: MW-01
Well Depth in Feet (WD):
110.5 ft TOC
Well Diameter. 2 inches
Water Level in Feet (WL):
q1.9 I
feet
Type of Casing: pVC
_
Length of Water Column:
ITS S
feet
Measuring Point: TOC
(WD) - (WL) = (LWC)
Flush Mount /Stick-U
One Casing Volume:
DI
gallons
Comments:
r ,V.
(LWC) x (WCV)
Three Casing Volumes:.
gallons
v�
Actual Volume Purged:
e -
gallons
Tagged bottom at:
6 ft
Time: Measuring Point:-b C/
Well Casing Volumes (WCV)
1" = 0.04 Gal/Ft 2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method:
Bailer-Disp.
Bailer -Teflon Dedicated Pump Whale Pump Grundfos
Other.
Sample Method:
Bailer-Disp.
Bailer -Teflon Dedicated Pump Whale Pump Grundfos
Other.
Lisserim
bpecuric
PM tbu4
uxt"ation
7
Gallons
Oxygen
Cond.
report to 0.1
Reduction
Turbidity
Reading
Time
Purged
Temp ('C)
(mg/L)
(PS/cm)
S.U.
Potential
(NTU)
Comments
.3 -33
1 etc;
2
QL2—
3.�
5 �•
c'
6
3
1
5:
1
4e
�.f
e
4
V
1 ;.
�
5
6
7
8
9
10
Sampling Container
Number of Containers Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
Other
Protective Casing: Pad: .-Lock: A�✓—'Vegetation:
Access:
Sampling Personnel Signature:
Date: �I
c� �1" 4-1-Notes:
Well Casing Volumes defined in Table 2 of t gion 4 Environmental Protection Agency (EPA) Science and Ecosystem Support Division (SESD) document titled Operating Procedure -
Groundwater Sampling last revised April 26, 2017.
Samples are analyzed immediately upon collection.
Minimum volume purged: 3 well volumes. Sample time determined by parameter stabilization.
°C: degrees Celsius
uS/cm: micro-Siemen per centimeter
ag/L: milligrams per liter
Method Reference:
Temperature: SM 2550 B-2010
DO: SM 4500 O G-2011
mV: millivolt
NTU: nephelometric turbidity units
S.U.: Standard Units
Specific conductivity: EPA Method 120.1, Rev. 1982
pH: SM 4500-H' B-2011
Page 1 of 1
ANCHOR
Well Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill Date: to l , G
Project Number: I Mep ,U0 _ Weather: �UGTr✓-if- H�G —
Sampling Personnel: _ Sample Time: : Ic
Well ID: MW-02 Well Depth in Feet (WD): 60.70 ft TOC
Well Diameter. 2 inches _ Water Level in Feet (WL):3C( 5-0 feet
Type of Casing: pVC _ Length of Water Column: '7—i. feet
Measuring Point: TOC (WD) - (WL) = (LWC)
Flush Moun / Stick -Up One Casing Volume: 3.51 gallons
Comments: (LWC) x (WCV)
Three Casing Volumes: to gallons
L Actual Volume Purged: gallons
Tagged bottom at: CU. qh ft Time: 100Z Measuring Point- —i 1!
Well Casing Volumes (WCV)
1" = 0.04 Gal/Ft 2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1A7 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method:
Bailer-Disp.
Bailer -Teflon
Dedicated Pump Whale Pump Grundfos
Other.
Sample Method:
Bailer-Disp.
Bailer -Teflon
Dedicated Pump Whale Pump Grund€os
Other.
LASSOrvftil Pe
Gallons
Oxygen Cond. report to 0. T
Reduction
Turbidity
Reading Time
Purged
Temp (°C)
(mg/L) (PS/cm) S.U.
Potential
(NTU) Comments
3
I6bC/
^i.Z
1, "It
4
0��
—
5
,�
`p0I
b�s©
--t+ 0V
�1
6
'
7
8
9
10
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
Other
Protective Casing:
Pad: 1_ Lock: Vegetation: Access:
Sampling Personnel Signature:
�~
Date:
Notes:
Well Casing Volumes defined in Table of a Region 4 Environmental Protection Agency (EPA) Science and Ecosystem Support Division (SESD) document titled Operating Procedu -
GroundwaterSomp(inq last revised Apr, 6, 2017.
Samples are analyzed immediately upon collection.
Minimum volume purged: 3 well volumes. Sample time determined by parameter stabilization.
'C: degrees Celsius mV: millivolt
uS/cm: micro-Siemen per centimeter NTU: nephelometric turbidity units �,p j
ng/L: milligrams per liter S.U.: Standard Units T t 6�,1/� 1� L
Method Reference: Specific conductivity: EPA Method 120.1, Rev. 1982
Temperature: SM 2550 B-2010 pH: SM 4500-H' B-2011
DO: SM 4500 O G-2011
Page 1 of 1
VL �� la,0
10;
ANCHOR
ow -Flow Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill
Project Number:
_
Location: Imo; l
Date:
Sampling Personnel: ` _
Weather:
Well ID: MW-03
Arrive at Well:
Screen Interval: 48.5-63.5 ft bgs
Start Time:
Depth to Water: `�� _ft
Sample Time:
Measuring Point: TOC Finish
Sample Time:
Depth of Pump Intake: 50 ft
Leave Well:
Drawdown Set: qLt ft
Pump Used (circle): Peristaltic Bladder Other (describe):
Well Diameter:
2 in
Comments: 1AAC*"V1rr"
Pure Rate:
wt1A
VW(A(D ,'<�� I a 1
Total Purge Volume:
Tagged bottom at: L' 0, ft Time: 2v
Pumpspeed:AjS 13s fill,3q S
pH (S.U.)
Time
DTW (feet)
Temp ("C)
DO (mg/L)
Specific Cond. (pS)
report O.T S.U.
ORP (mV)
Turbidity (NTU)
p
ptoo
I i I .
-
ice.
_•
6Y
'
--■ A
lei
Sampling Personnel Signature:
Date:
Notes:
Q-1-1, LI-11 V
Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity,- +/- 3% Conductivity; +/- 0.1 pH unit; +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
Samples are analyzed immediately upon collection,
pS: micro-Siemen
mv: millivolt
°C: degrees Celsius
f
7/� ♦ NTU: nephelometric turbidity units
bgs: below ground surface
F
'�
t1 `� lnr ORP: oxidation reduction potential
DO: dissolved oxygenFh*eAr
; ^ a� S.U: standard units
mg/L: milligrams per liter
C,
" v ��r v p toc: top of casing
Method Reference:
C1.
+ VL `a LVIJ►✓ `
emperature: SM 2550 B-2010
Specific conductivity: EPA Method 1201, Rev. 1982
+
JO: SM 4500 O G-2011(�
\ `� t pH: SM 4500-H* B-2011
Page 1 of 1
ANCHOR
QEA.'
%ow -Flow Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill
Location: U MS6&_61 No
Sampling Personnel: kvi AL,
Well ID: MW-04
Screen Interval: 25-40 ft bgs
Depth to Water: G . ft
Measuring Point: TQC
Depth of Pump Intake: 35 ft
Drawdown Set: ? � 1 -3 ft
Pump Used (circle): Peristaltic Bladder Other (describe):
Comments: 3 iq� L340
�+� �f F
<�Vp "UTK 6ttio _
Tagged bottom at: 4 d ft Time:�0�
Project Number: CO (LtM )� • 0 v
�o Date: 10 C4 qu
Weather. /VLOAA�S
Arrive at Well: �Z
Start Time:
Sample Time: l '%jC6
Finish Sample Time: 0
Leave Well: (if 10
Well Diameter: 2 in
Purge Rate: m— wt,iy�
Total volume Purged: '1_ ,77S
Pumpspeed: As 10 �Stt ?-5
Time
DTW (feet)
Temp (°C)
DO (mg/L)
Specific Cond. (pS)
PH (S.U.)
reportS0 0.1 S U.
ORP (mV)
Turbidity (NTU)
3
1?7
.50
(-1i
5
g,
bq
t q
fig- b
.-3I
f�. a
--= _
05:
�21
S.1S
5, 3
�5 0. a
-o
±U5 - -
3-
to
.55
ay 19
a.
6(1101
P-5
Tp-30
an 0
��
3
5.
5, Ile
,45
5
35
C
3
5 _q
0
q.
i
qaq.
5
1 3 a.
Sampling Personnel Signature:
Date: 1 �/ v—/
Notes:
LI C" L/
Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity, +/- 3% Conductivity, +/- 0.1 pH unit; +/- 70 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
Samples are analyzed immediately upon collection.
pS: micro-Siemen
°C: degrees Celsius
bgs: below ground surface
DO: dissolved oxygen
mg/L: milligrams per liter
Method Reference:
-emperature: SM 2550 B-2010
60: SM 4500 0 G-2011
mv: millivolt
NTU: nephelometric turbidity units
ORP: oxidation reduction potential _$
S.U.: standard units
toc: top of casing
Specific conductivity: EPA Method 120.1, Rev. 1982
PH: SM 4500-H' B-2011
Page 1 of 1
61i
ANCHOR
QEA
Well Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill Date:
0
Project Number:_���(�`'�t•Q�
Weather.
�1dU1S
Sampling Personnel: t
Sample Time:
Well ID: MW-05R
Well Depth in Feet (WD):
54.0 feet TOC
Well,Diameter: 2 inch
Water Level in Feet (WL):
k
feet
Type of Casing: PVC
Length of Water Column:
10 s `Ia
feet
Measuring Point: TOC
(WD) - (WL) = (LWC)
Flush Mount Stick Up
One Casing Volume:
1,677
gallons
Comments:
(LWC) x (WCV)
Three Casing Volumes:
C
gallons
Actual Volume Purged:
gallons
Tagged bottom at:, f, ffTOC
ft Time: a5 Measuring Point: T
Well Casing Volumes (WCV)
1" = 0.04 Gal/Ft 2" = 0.16 Gal/Ft 3" = 0.37
Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method: Bailer-Disp. I
Bailer -Teflon
Dedicated Pump Whale Pump Grundfos
Other:
Sample Method: Bailer-Dis .
Bailer -Teflon
Dedicated Pump Whale Pump Grundfos
Other.
LIMORRM mmic-ITIC PH [".1
x d son
Gallons
Oxygen Cond. report to 0.1
Reduction Turbidity
Reading Time Purged
Temp (°C)
(mg/L) (PS/cm) S.U.
Potential (NTU)
Comments
1
, f', I
0. -
'? ,A-/
b •-1
1.13
- (la ,
U
T
Lj L
JLLY
J3 Y
4
we it
dry a
-a vi
yt
5
^'
1. q
6
7
8
9
10
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
LA 1
i a
YL
125 mL Plastic
40 mL Glass
1 L Glass
F
S
Other
Protective Casing: Pad: Lock: Vegetatio Access:
VV-c) f (jN
I
Sampling Personnel Signature: r
Date: iv
L.
Notes:
Well Casing Volumes defined in Table 2 of the Region 4 Environmental Protection Agency (EPA) Science and Ecosystem Support Division (SESD) document titled Operating Procedure -
Groundwater 5ampiing last revised April 26, 2017.
Samples are analyzed immediately upon collection.
Minimum volume purged: 3 well volumes. Sample time determined by parameter stabilization.
°C: degrees Celsius
uS/cm: micro-Siemen per centimeter
ng/L: milligrams per liter
Method Reference:
Temperature: SM 2550 B-2010
DO: SM 4500 0 G-2011
mV: millivolt
NTU: nephelometric turbidity units
S.U.: Standard Units
Specific conductivity: EPA Method 120.1, Rev. 1982
PH: SM 4500-H' B-2011
Page 1 of 1
ANCHOR
It
..v QEA
Low -Flow Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill
Location: l�i��5fj t �t-/
Sampling Personnel:
Well ID: Mw-06
Screen Interval: 84-94 ft bgs
Depth to Water: _4(f, 0 L ft
Measuring Point: TQC
Depth of Pump Intake: 93 ft ft
Drawdown Set: ft
Pump Used (circle): Peristaltic Bladder Other (describe):
Comments: �'�
Project Number:
Date:
Weather: L i
Arrive at Well: !�?J
Start Time:
Sample Time:
Finish Sample Time: N `0
Leave Well:N4V
Well Diameter. 2 _ in
$�C
Stv�OZ/YO " 11{
Tagged bottom at ft
Time:1
urgeValww
heed:
Time
DTW (feet)
Temp (°C)
DO (mg/L)
Specific Cond. (NS)
PH (S.U.)
reportto O.l S.U. ORP (mV)
Turbidity (NTU)
` 34
19, Y
`tr 6L
G
-
LZ' 5-T�
3 00
_�,,52�,_�
1
�t3
S, 4
i1154
`.Ii3r$
r
6
1301
!G .T1``
o
'0 r
-1 0
©
3���"
t
3
, 'L
t
ti<
%
G
Z
i
t,5-+
S3,1
10,z
- 3 1
d
,Z7.
116,
".-s
sz, Fr
l
Sampling Personnel Signature:
Date: I
v ..
Notes:
J
Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity; +/- 3% Conductivity, +/- 0.1 pH unit +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
Samples are analyzed immediately upon collection. �( 0'V1 i
pS: micro-Siemen mv: millivolt f
l V
°C: degrees Celsius NTU: nephelometric turbidity units J A � ,...., , , ; ,jam
bgs: below ground surface ORP: oxidation reduction potential ` �J ��/V C�, R
DO: dissolved oxygen S.U.: standard units
mg/L: milligrams per liter toc: top of casing
Method Reference:
Temperature: SM 2560 6-2010 Specific conductivity: EPA Method 120.1, Rev, 1982
DO: SM 4600 0 G-2011 pH: SM 4500-H' B-2011
L
Page 1 of 1
ANCHOR
� QEA
Low -Flow Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: ,Jackson County Dlllsboro Landfill
Location: P! o5 AO" 6X/
Sampling Personnel: M(: AL
Well ID: MW-07
Screen Interval: 70-95 ft bgs
Depth to Water. )0,1 3 ft
Measuring Point: TQC
Depth of Pump Intake: 85 ft
Drawdown Set: _'3t.qq^ ft
Pump Used (circle): Peristaltic Bladder Other (describe):
Comments:_ 6('Ri
stfw WUS'C" IV
Project Number: Co tLf go c(, 0 a -
Date: 100 Z (2G
Weather..0 ?1 rC',sf -70 vfr
r
Arrive at Well: L03
Start Time: W
Sample Time:
Finish Sample Time: fi7
Leave Well: ("a 70
Well Diameter: 2 in
Pure Rate: 250 +nL eVA •.
Total Purge Volume:
Tagged bottom at: t Time: E S��
Pump speed: 14 di5
70 jaj,
Time
DTWjj(feet)
Temp (°C)
DO (mg/L)
Specific Cond. (pS)
PH (S.U.)
report to 0.1 S.U.
ORP (m1)
Turbidity (NTU)
a Y
j
l . I
144
10.3
s
30
���
-° i
!�-��-
�• —
t oC
(3� ��
Wtg
1 3131
to
�—
lo
?_
AS
g,
-0i0
Sampling Personnel Signature:
Date: (7 0—/
Notes: s '
Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity,, +/- 3% Conductivity, +/- 0.1 pH unit,' +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
Samples are analyzed immediately upon collection.
pS: micro-Siemen
°C: degrees Celsius
bgs: below ground surface
DO: dissolved oxygen
mg/L: milligrams per liter
Method Reference:
Temperature: SM 2550 B-2010
D0: SM 4500 0 G-2011
mv: millivolt
NTU: nephelometric turbidity units
ORP: oxidation reduction potential
S.U.: standard units
toc: top of casing
Specific conductivity: EPA Method 120.1, Rev. 1982
PH: SM 4500-H' B-2011
Page 1 of 1
ANCHOR
surface Water Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill
Project Number.. f �1l"lI]s� �� %1
Sampling Personnel:Q
Sample Name: SW_01
Comments: Upstream of landfill
Date:
Weather:
�vrr
Sample Method: Grab Syringe
Pump
Bailer-Disp.
Other
Dissolved
Time Temp (°C) Oxygen (mg/L)
Specific Cond.
(PS/cm)
pH (S.U.)
report to 0. J S.U.
Oxidation
Reduction
Potential (mV)
Turbidity
(NTU)
Comments
11�
IA
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
1
�iFrys
250 mL Plastic
ZeA ei
t
125 mL Plastic
40 mL Glass
co
VC
o ^
1 L Glassy
Other
Vegetation:
Sampling Personnel Signature:
Notes:
Samples are analyzed immediately upon collection.
°C: degrees Celsius
PS/cm: micro-Siemen per cubic centimeter
mg/L: milligrams per liter
mv: millivolt
NTU• nephelometric turbidity units
Access: k
Date:
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
pH: SM 4500-H' B-2011
S.U.: standard units f Se
ri
Page 1 of 1
A Z /A��NCHOR
1v[i: A C_06-16.i
aurface Water Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill
Project Number. a. Lqn .■ � .,�J _
Sampling Personnel: _ �y— I'S �Y v
Sample Name: SW-02
comments: Downstream of landfill
Date:
Weather: AA Iu
Sample Method:
Grab
Syringe Pump
Bailer-Disp. Other.
Time
Temp (°C)
Dissolved
Oxygen (mg/L)
Specific Cond.
(PS/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (mV)
Turbidity
(NTU) Comments
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
1 01
125 mL Plastic
40mLGlass
A
Mao ®� ao S`�-
1 L Glass
Other
Vegetation:
Access:
Sampling Personnel Signature: �� Date: �� ( tq V
Notes: (r
Samples are analyzed immediately upon collection.
°C: degrees Celsius
PS/cm: micro-Siemen per cubic centimeter
mg/L: milligrams per liter
mV: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
pH: SM 4500-H ` B-2011
r-
Page 1 of 1
,�z
ANCHOR
tiQEA
Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill Date:
Project Number. GQ 14 �Ib C)t- 02 Weather o-t.
Sampling Personnel: llla k
Sample Name: DW-01
Comments: Purged 30 gallons prior to sampling. Wilkey residence.
Sample Method(Grab
Syringe Pump
Bailer-Disp. Other.
Temp
rimeVC)
Specific Cond.
(PS)
Dissolved
Oxygen pH (S.U.)
(mg/L) report to 0.7 S.U.
Oxidation
i Reduction
Potential (m1)
Turbidity
(NTU)
Comments
pryry
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
V V
40 mL Glass
1 L Glass
Other
Vegetation:
Access:
Sampling Personnel Signature: Date: ( V 1 1 K I
Notes: A / Method Reference:
NS: micro-Siemen per cubic centimlerF/ Temperature: SM 2550 B-2010
"C: degrees Celsius Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter DO: SM 4500 O G-2011
mv: millivolt pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units
S.U.: standard units
Page 1 of 1
ANCHOR
`Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: Jackson County Dillsboro Landfill
Project Number:
Sampling Personnel:
Sample Name: LT-01
Date:
Weather:
C/Iyzt/
Comments:
collected from leachate tank
_ ✓e.
S/
r' vuh.,
6.1)
Sample Meth
Grab
Syringe Pump
Bailer-Disp.
Other:
Time
Temp
VC)
Specific Cond.
(PS)
Dissolved
Oxygen pH (S.U.)
(mg/L) report to 0.1 S.U.
Oxidation
Reduction
Potential (m%o
Turbidity
(NTU)
Comments
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plasticij
125 mL Plastic
40 mL Glass
(� "
1 L Glass
Other
Vegetation: V Access:
Sampling Personnel Signature: Date:
Notes:
NS: micro-Siemen per cubic centimeter
°C: degrees Celsius
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Page 1 of 1
ANCHOR
kpvLv QEA
Equipment Documentation and Instrument Calibration Data Sheet
CALIBRATION DOCUMENTATION
Project Name: Jackson County Dillsboro Landfill Person Conducting Calibration:
Project Number: (0Ig4;'1[)sD(.02--' Date of Calibration:
Project Location: a RC kodYO j� Date of Field Measurements:16
EQUIPMENT DOCUMENTATION
Rental sample analysis equipment or meters used to take measurements:
Equipment Type Brand Serial Number Date of Use Rental Company
Select Turbidimeter: Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Instrument Reading
Instrument Reading
(Hach 2100Q)
(HF Scientific MicroTPW)
10 NTU
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Calibration Expiration
t
�i
Date:
Cal: .�
Cal: i
Cal: -
Cal:
Cal:
Cal:
Time:
i
Time:
ii -
Time:
Time:
Time:
Time:
Calibration
*Pre -Analysis
Meas:
Time:
*Pre -Analysis
m
Time:
Verification:
Check (10 NTU):
�� s `�'
f'
Check (10 NTU):
*Post -Analysis
Meas:
Time:
st-Analysis
Meas:
Time:
Check (10 NTU):
�
Q
Fc*ck (10 NTU):
YSI Professional Plus Multiparameter Meter (s/n 118131101802)
Instrument Readings
Calibration Lot No.
& Expiration Date
Initial:
Cal:
mmHg:
Temperature (°C):
Time:
Dissolved Oxygen
l . � o
� q` r
tit
� � � y q / �
IV
G
D
pH 7 S.U.
initial-
pHmVx
Cal: �7
3, f
pHmV:
"—
Time:
� �
06 •�]
report to 0.1 S.U.
;�
1
pH 4 S.U.
initial
"[ 0 1
pHmV: pHmV:
"
Cal:
pHmV:
'
Time:
®
/� �{
report to 0.7 S.U.
•
V
pH 10 S.U.
Initial:
I C
pHmV:
Cal: L1.11
pHmV:
Time:
�
��y I
( I
report to 0.7 S. U.
(�
1
QC* PH 7 S.U. report
AM Time:
Mea
Mid Day Time:
Check:
PM Time:
Check
dS
to 0.1 S.U.
� 1,—T
Spec. Cond.
Initial:
Cal:
Time:
Time:
1 y�
31
0 V
1W o
1
Slcm
QC*:
AM Time:
Meas/::
Mid Day Time:
Check:
PM Time:
Check:
�h
D ��r
PS/cm
% Recovery=
,}�.�h
ORPmV
�
Initial:
Cal:
t emperature (°C):
-rime:
a .
JD.'
Signature: /'-� Date: j V
Notes:tl
Revision 3, 04/30/20, MHF
1. Electronic equipment calibrated according to the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
5. * QC check must be performed prior to sampling and following completion of sampling, at a minimum.
6. % Recovery = (Value Obtained, pS/cm _ True Value, pS/cm) x 100
Method Reference: Temp: SM 2550 B-2010 I Conductivity: EPA Method 720.1 1 DO: SM 4500 O G-2017 I pH: SM 4500-H+B-2017 I Turbidity: SM 2730 B-2077
I
Page 1 of 1
ANCHOR
C QEA �
Equipment Documentation and Instrument Calibration Data Sheet
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
CALIBRATION DOCUMENTATION
Project Name: Jackson County Dillsboro Landfill Person Conducting Calibration:
Project Number. Date of Calibration: �-?7
Project Location: N1.16`60v, f4c, Date of Field Measurements: a?'
EQUIPMENT DOCUMENTATION
Rental sample analysis equipment or meters used to take measurements:
Equipment Type Brand Serial Number Date of Use Rental �ompan
Select Turbidimeter: Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
rand. Doe7.vle�e, vwiil'c l� �n
o N c�ead%� s CQ r✓i �,Ye 6 w-lu.
IWU
1vK'Ol,�ia' b W�
Of
('R.Inirt �
Instrument Reading
Instrument Reading
(Hach 2100Q)
(HF Scientific MicroTPW)
10 NTU
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 N
Calibration Expiration
l�
it
Date:
Cal: q q
Cal: An 0
Cal: 91 cp
Cal:
Cal:
Time:
Time: r.`
IJ
Time:. ��
Time:
Time:
Time:
Calibration
*Pre -Analysis
Meas:
t L. ®
Time:
��
*Pre -Analysis
as:
Time:
Verification.-
Check (10 NTU):
Check (10 N
*Post -Analysis
Meas:
Time: y
P�-1
*Post -Analysis
Meas:
Time:
Check 00 NTU):
, a-
Check (10 NTU):
YSI Professional Plus Multiparameter Meter (s/n 18B701802)
Instrument Readings
Calibration Lot No.
& Expiration Date
Dissolved Oxygen
Initial:
K:6 It
Cal:
jw c �
mmHg:
3,u
u �
Temperature,(°C):
Time:
jT tib
'1��
PH 7 S.U.
Initial`: pQ(
pHmV:
Cal:
pHmV:
Time:
report to 0.1 S. U.
pH 4 S.U.
Initial: T
pHmV:
✓
Cal: L
0 V
✓
pHmV: -
�
Time: _ I _
-
report to 0.1 S.U.
E
I
l/°J,�_71•'f�
prt 10 S.U.
Initial-
u
pHmV.Cal:
1 v ®1
pHmV: /
Time: V
f
report to 0.1 S.U.
'I
.
1
V
QC* pH 7 S.U. report
AM Time:
Meas:
Mid Day Time:
Check:
PM Time:
Check:
to 0.1 S.U.
Spec.ffC��ond.
o V
Initial:(
0
Cal: j
Time:
V Ns/cm
D
QC*:
AM Time:
Meas:
Mid Day Time:
Check:
PM Time:
Check:
��rr�� n
Woo
uS/cm
V"l,0
% Recovery=
yh,
ORP V mV
Initial(: Mop
�-4Vr�
Cal:
�°�
Temperature (°C):
,
Time:
}
V
Signature: 11J A Date:
Notes: Ll
99 ,,y�
Revision 3, 04/3D/20, l :J l�/13�N `,�� af� 4 -
--)
1. Electronic equip nt calibrated according to the manufacturer's operation manual. j�
2. Specific Conductivity should be calibrated according to values representative of historic range. + �v V a �+
3.Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
5. * QC check must be performed prior to sampling and following completion of sampling, at a minimum.
6. % Recovery = (Value Obtained, pS/cm + True Value, pS/cm) x 100
Method Reference: Temp: SM 2550 B-2070 l Conductivity. EPA Method 720.7 l DO: SM 4500 O G-207 7 1 pH: SM 4500-H+B-2011 I Turbidity: SM 2730 B-2011
Page 1 of 1
ANCHOR
QEA
Equipment Documentation and Instrument Calibration Data Sheet
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
CALIBRATION DOCUMENTATION -�/ _
Project Name: Jackson County DillSboro Landfill Person Conducting Calibration: 12 Yin Y' LJ 1-
Project Number: 00i L4,R a-C(.(2 Z Date of Calibration: 110
Project Location: })}�(/ Date of Field Measurements:
EQUIPMENT DOCUMENTATION
Rental sample analysis equipment or meters used to take measurements:
Equipment Type
Brand
Serial Number
Date of Use
Rental Company
�
1
L
ect Turbidimeter. Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
Instrument Reading
Instrument Reading
(Hach 21000)
(HF Scientific MicroTPW)
10 NTU
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Calibration Expiration
Mal
11141
AU)
Date:
Cal: 11D1
C
Cal: r1
(!
Cal:
Cal:
Cal:
Cal: -
J
Time: Y,1S
Time: ,
Time: �71;�.'
C-�
Time:
Time: �.
Time:
Calibration
Verification:
*Pre -Analysis
Check (10 NTU):
Meas:
( A0
Time:
*Pre -Analysis
Check (10 NTU):
Meas. ''
Time:
*Post -Analysis
Check (10 NTU):
Meas• I
�'
Time• 77
�Jo
*Post -Anal s
Check NTU):
Meas:
Time:
YSI Professional Plus Multiparameter Meter (s/n 1813101802)
Instrument Readings
Calibration Lot No.
& Expiration Date
Dissolved Oxygen
InIal: 6
�1
Cal:
+ O 41
mmHg:
1 � ©
Temperature °C):
/
Ti
PH 7 S.U.
report to 0.1 S.U.
Initial r
�J ,,
pHmV:
Cal: 1�
7. G V
pHmV:
Timef,
PH 4 S.U.
report to 0.1 S.U.
Initi9k.
-) 1
pHmV:
Cal:4 (� U
pHmV:
Time; _ ��
7
r/ -7
a r,'
PH 10 S.U.
report to 0.1 S.U.
Initia;V :(
pHmV:
Cal: f 1l
pHmV:
Time Z
V Z,
QC* pH 7 S.U. report
to 0.1 S.U.
A ime:
Mea,,;, ,.
Mid Day Time:
Check:
PM Time:
Check:
�� L
Spec. Cond.
ao U S/crn
Initiel:�
1illVV��
Cal'1®, 0
iV{
Tim 73
O !z (
/
QC*: t l! /p�� pp�'�
l 6 V S/cm
AM Time:e::
'%
MQas
V 1i
Mid Day Time:
Check:
PM Time:
Check:
y
03/L
% Recovery=
ORP �� mV
it
Inrti
Calj�)%l
L `� V
Temperature °C):
1� i
Time:
-�
r/ 7-1
Signature: Date: ZQ l
Notes: L__!_
Revision 3, 04/30/20, MHF
1. Electronic equipment calibrated according to the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10%of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
5. " QC check must be performed prior to sampling and following completion of sampling, at a minimum.
6. % Recovery = (Value Obtained, pS/cm + True Value, pS/cm) x 100
Method Reference: Temp: SM 2550 B-2010 I Conductivity. EPA Method 720.7 I DO: SM 4500 0 G-2071 l pH: SM 4500-H+B-2077 I Turbidity: SM 2130 B-2071
0!4�
Page 1 of 1
Appendix B
Reports of Laboratory Analysis,
Chain -of -Custody Documentation,
and Certificates of Analysis
Way poi nt
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Jackson Cty Landfill 2020 Fall
Project No.: 50-02
Lab Submittal Date: 10/13/2020
Work Order: 0100161
Case Narrative
11 /30/20 10:34
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Dissolved hydrogen, Carbon dioxide, dissolved gasses and volatile fatty acids analyses were
subcontracted to Pace/GCAL. Laboratory report is attached.
Waypoint Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a,j
Angela D. Overcash
Senior Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 84
Data Qualifiers Key Reference:
A ECCV failed low. Samples were re -analyzed with confirming results. Initial data reported.
BRL BRL
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
DC The RPD between the primary and confirmation column concentrations is greater than 40. The result is reported
from the primary column.
HT Sample received and analyzed outside of the hold time.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
LCD2 LCS/LCSD RPD Value outside of the control limits. LCS and LCSD Values within the control limits.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
MI Matrix spike outside of the control limits. Matrix interference suspected.
SE Surrogate recovery outside of the QC limits due to emulsion.
SR Surrogate recovery outside of the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 84
1 Q
Waypoint..
ANALYTICAL
Sample Receipt Summary
11 /30/2020
Work Order: 0100161
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
MW-04-20201012
0100161-01
Water
MW-05R-20201012
0100161-02
Water
MW-07-20201012
0100161-03
Water
TB-202010120000
0100161-04
Water
Samples were received in good condition at 2.1 degrees C unless otherwise noted
10/12/20 13:00
10/12/20 14:34
10/12/20 10:57
10/12/20 0:00
10/13/20 8:25
10/13/20 8:25
10/13/20 8:25
10/13/20 8:25
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 3 of 84
Way poi nt
ANALYTICAL
Summary of Detections
11/30/202C
Work Order: 0100161
Prism ID
Client ID
Parameter
Method
Result
Units
0100161-01
MW-04-20201012
Chloride
9056A
24000
ug/L
0100161-01
MW-04-20201012
Nitrate as N
9056A
6500
ug/L
0100161-01
MW-04-20201012
Sulfate
9056A
91000
ug/L
0100161-01
MW-04-20201012
Biochemical Oxygen Demand
SM5210 B
380
J
ug/L
0100161-01
MW-04-20201012
Chemical Oxygen Demand
SM5220 D
13000
J
ug/L
0100161-01
MW-04-20201012
Total Alkalinity to pH 4.5
SM2320 B
64000
ug/L
0100161-01
MW-04-20201012
Mercury
7470A
1.0
ug/L
0100161-01
MW-04-20201012
Barium
6020B
81
ug/L
0100161-01
MW-04-20201012
Cadmium
6020B
0.24
J
ug/L
0100161-01
MW-04-20201012
Cobalt
6020B
1.7
J
ug/L
0100161-01
MW-04-20201012
Nickel
6020B
1.0
J
ug/L
0100161-01
MW-04-20201012
Selenium
6020B
2.3
J
ug/L
0100161-01
MW-04-20201012
TOC
531OC-2011
2.05
mg/L
0100161-01
MW-04-20201012
1,4-Dichlorobenzene
8260D
0.85
ug/L
0100161-01
MW-04-20201012
Chlorobenzene
8260D
0.69
ug/L
0100161-01
MW-04-20201012
cis-1,2-Dichloroethylene
8260D
0.46
J
ug/L
0100161-01
MW-04-20201012
Dichlorodifluoromethane
8260D
0.23
J
ug/L
0100161-01
MW-04-20201012
Hexachlorobutadiene
8260D
0.20
J
ug/L
0100161-01
MW-04-20201012
m,p-Xylenes
8260D
0.31
J
ug/L
0100161-01
MW-04-20201012
Naphthalene
8260D
0.30
J
ug/L
0100161-01
MW-04-20201012
Xylenes, total
8260D
0.31
J
ug/L
0100161-01
MW-04-20201012
1,4-Dioxane
8260D SIM
3.4
ug/L
0100161-02
MW-05R-20201012
Chloride
9056A
55000
ug/L
0100161-02
MW-05R-20201012
Nitrate as N
9056A
75
J
ug/L
0100161-02
MW-05R-20201012
Barium
6020B
60
ug/L
0100161-02
MW-05R-20201012
Cobalt
6020B
8.3
ug/L
0100161-02
MW-05R-20201012
Nickel
6020B
1.4
J
ug/L
0100161-02
MW-05R-20201012
Zinc
6020B
18
J
ug/L
0100161-02
MW-05R-20201012
Biochemical Oxygen Demand
SM5210 B
5200
ug/L
0100161-02
MW-05R-20201012
Chemical Oxygen Demand
SM5220 D
42000
J
ug/L
0100161-02
MW-05R-20201012
Ferrous Iron
SM3500-Fe B
12000
HT
ug/L
0100161-02
MW-05R-20201012
Sulfide
SM4500-S F
5000
ug/L
0100161-02
MW-05R-20201012
Total Alkalinity to pH 4.5
SM2320 B
240000
ug/L
0100161-02
MW-05R-20201012
gamma-BHC
8081B
0.010
DC, J
ug/L
0100161-02
MW-05R-20201012
2,4,5-TP (Silvex)
8151A
0.08098
J
pg/L
0100161-02
MW-05R-20201012
1,4-Dichlorobenzene
8270D
3.41
J
pg/L
0100161-02
MW-05R-20201012
Dibenzofuran
8270D
0.518
J
pg/L
0100161-02
MW-05R-20201012
Diethyl phthalate
8270D
2.28
J
pg/L
0100161-02
MW-05R-20201012
Mercury
7470A
0.73
ug/L
0100161-02
MW-05R-20201012
Barium
6020B
110
ug/L
0100161-02
MW-05R-20201012
Cobalt
6020B
8.3
ug/L
0100161-02
MW-05R-20201012
Copper
6020B
5.5
J
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 84
Waypoint.
ANALYTICAL
Summary of Detections
11/30/202C
Work Order: 0100161
Prism ID
Client ID
Parameter
Method
Result
Units
0100161-02
MW-05R-20201012
Nickel
6020B
2.7
J
ug/L
0100161-02
MW-05R-20201012
Selenium
6020B
0.85
J
ug/L
0100161-02
MW-05R-20201012
Zinc
6020B
18
J
ug/L
0100161-02
MW-05R-20201012
TOC
531OC-2011
7.05
mg/L
0100161-02
MW-05R-20201012
1,4-Dichlorobenzene
8260D
0.89
ug/L
0100161-02
MW-05R-20201012
Chlorobenzene
8260D
0.67
ug/L
0100161-02
MW-05R-20201012
cis-1,2-Dichloroethylene
8260D
0.41
J
ug/L
0100161-02
MW-05R-20201012
Dichlorodifluoromethane
8260D
0.30
J
ug/L
0100161-02
MW-05R-20201012
m,p-Xylenes
8260D
0.27
J
ug/L
0100161-02
MW-05R-20201012
Xylenes, total
8260D
0.27
.1
ug/L
0100161-02
MW-05R-20201012
1,4-Dioxane
8260D SIM
3.5
ug/L
0100161-03
MW-07-20201012
Chloride
9056A
79000
ug/L
0100161-03
MW-07-20201012
Nitrate as N
9056A
92
J
ug/L
0100161-03
MW-07-20201012
Sulfate
9056A
25000
ug/L
0100161-03
MW-07-20201012
Biochemical Oxygen Demand
SM5210 B
920
J
ug/L
0100161-03
MW-07-20201012
Chemical Oxygen Demand
SM5220 D
18000
J
ug/L
0100161-03
MW-07-20201012
Ferrous Iron
SM3500-Fe B
360
HT
ug/L
0100161-03
MW-07-20201012
Total Alkalinity to pH 4.5
SM2320 B
250000
ug/L
0100161-03
MW-07-20201012
1,4-Dichlorobenzene
8270D
2.66
J
pg/L
0100161-03
MW-07-20201012
Mercury
7470A
0.53
ug/L
0100161-03
MW-07-20201012
Barium
6020B
390
ug/L
0100161-03
MW-07-20201012
Chromium
6020B
0.90
J
ug/L
0100161-03
MW-07-20201012
Cobalt
6020B
1.4
J
ug/L
0100161-03
MW-07-20201012
Nickel
6020B
7.1
ug/L
0100161-03
MW-07-20201012
TOC
531OC-2011
3.22
mg/L
0100161-03
MW-07-20201012
1,2,4-Trichoorobenzene
8260D
0.23
J
ug/L
0100161-03
MW-07-20201012
1,2-Dichlorobenzene
8260D
0.50
ug/L
0100161-03
MW-07-20201012
1,4-Dichlorobenzene
8260D
6.8
ug/L
0100161-03
MW-07-20201012
Benzene
8260D
1.4
ug/L
0100161-03
MW-07-20201012
Chlorobenzene
8260D
6.1
ug/L
0100161-03
MW-07-20201012
cis-1,2-Dichloroethylene
8260D
2.6
ug/L
0100161-03
MW-07-20201012
m,p-Xylenes
8260D
0.42
J
ug/L
0100161-03
MW-07-20201012
Tetrahydrofuran
8260D
1.6
J
ug/L
0100161-03
MW-07-20201012
Xylenes, total
8260D
0.42
.1
ug/L
0100161-03
MW-07-20201012
1,4-Dioxane
8260D SIM
17
ug/L
0100161-04
TB-202010120000
Acetone
8260D
3.2
J
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 84
Laboratory Report
IL A i • . 0 11 /30/2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-04-20201012
Attn: Alec Macbeth Sample ID: 0100161-01
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 13:00
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Anions by Ion Chromatography
Chloride
24000
ug/L
NE
1000
350
1
9056A
10/13/20 19:25BMS
POJ0221
Nitrate as N
6500
ug/L
10000
200
45
1
9056A
10/13/20 19:25BMS
POJ0221
Sulfate
91000
ug/L
250000
2000
560
1
9056A
10/13/20 19:25BMS
POJ0221
General Chemistry Parameters
Biochemical Oxygen Demand
380 J
ug/L
NE
2000
210
1
SM5210 B
10/14/20 9:18 ENM
POJ0276
Chemical Oxygen Demand
13000 J
ug/L
NE
50000
11000
1
SM5220 D
10/16/20 11:18SLS
POJ0304
Cyanide
<14
ug/L
10
25
14
5
9014
10/20/20 12:30BMS
POJ0357
Ferrous Iron
<46 HT
ug/L
NE
200
46
1
SM3500-Fe B
10/13/20 11:14ENM
POJ0199
Sulfide
<830
ug/L
1000
2000
830
1
SM4500-S F
10/19/20 11:02ENM
POJ0337
Total Alkalinity to pH 4.5
64000
ug/L
NE
5000
770
1
SM2320 B
10/19/20 11:40 CLB
POJ0341
Organochlorine Pesticides by GC/ECD
A
4,4'-DDD
<0.027
ug/L
0.1
0.10
0.027
1
8081 B
10/14/20 20:31NMB
POJ0214
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081 B
10/14/20 20:31NMB
POJ0214
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081 B
10/14/20 20:31NMB
POJ0214
Aldrin
<0.015
ug/L
0.05
0.051
0.015
1
8081 B
10/14/20 20:31NMB
POJ0214
alpha-BHC
<0.0064
ug/L
0.05
0.051
0.0064
1
8081 B
10/14/20 20:31NMB
POJ0214
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/14/20 20:31NMB
POJ0214
beta-BHC
<0.011
ug/L
0.05
0.051
0.011
1
8081 B
10/14/20 20:31NMB
POJ0214
Chlordane
<0.18
ug/L
0.5
0.51
0.18
1
8081 B
10/14/20 20:31NMB
POJ0214
delta-BHC
<0.0083
ug/L
0.05
0.051
0.0083
1
8081 B
10/14/20 20:31NMB
POJ0214
Dieldrin
<0.014
ug/L
0.002
0.051
0.014
1
8081 B
10/14/20 20:31NMB
POJ0214
Endosulfan 1
<0.016
ug/L
0.1
0.051
0.016
1
8081 B
10/14/20 20:31NMB
POJ0214
Endosulfan 11
<0.012
ug/L
0.1
0.051
0.012
1
8081 B
10/14/20 20:31NMB
POJ0214
Endosulfan Sulfate
<0.017
ug/L
0.1
0.051
0.017
1
8081 B
10/14/20 20:31NMB
POJ0214
Endrin
<0.014
ug/L
0.1
0.051
0.014
1
8081 B
10/14/20 20:31NMB
POJ0214
Endrin Aldehyde
<0.016
ug/L
0.1
0.051
0.016
1
8081 B
10/14/20 20:31NMB
POJ0214
Endrin Ketone
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/14/20 20:31NMB
POJ0214
gamma-BHC
<0.0062
ug/L
0.05
0.051
0.0062
1
8081 B
10/14/20 20:31NMB
POJ0214
trans -Chlordane
<0.023
ug/L
NE
0.10
0.023
1
8081 B
10/14/20 20:31NMB
POJ0214
Heptachlor
<0.013
ug/L
0.05
0.051
0.013
1
8081 B
10/14/20 20:31NMB
POJ0214
Heptachlor Epoxide
<0.023
ug/L
0.075
0.10
0.023
1
8081 B
10/14/20 20:31NMB
POJ0214
Methoxychlor
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/14/20 20:31NMB
POJ0214
Toxaphene
<0.35
ug/L
1.5
1.0
0.35
1
8081 B
10/14/20 20:31NMB
POJ0214
Surrogate
Recovery Control Limits
Decachlorobiphenyl
17 %
13-186
Tetrachloro-m-xylene
41 %
40-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 84
Laboratory Report
• � 11 /30/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-04-20201012
Attn: Alec Macbeth Sample ID: 0100161-01
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 13:00
Time Submitted: 10/13/20 08:25
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Polychlorinated Biphenyls (PCBs) by GC/ECD
A
Aroclor 1016
<0.21
ug/L
NE
0.51
0.21
1
8082A
10/14/20 20:31NMB
POJ0214
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1
8082A
10/14/20 20:31NMB
POJ0214
Aroclor 1232
<0.16
ug/L
NE
0.51
0.16
1
8082A
10/14/20 20:31NMB
POJ0214
Aroclor 1242
<0.14
ug/L
NE
0.51
0.14
1
8082A
10/14/20 20:31NMB
POJ0214
Aroclor 1248
<0.14
ug/L
NE
0.51
0.14
1
8082A
10/14/20 20:31NMB
POJ0214
Aroclor 1254
<0.16
ug/L
NE
0.51
0.16
1
8082A
10/14/20 20:31NMB
POJ0214
Aroclor 1260
<0.50
ug/L
NE
1.0
0.50
1
8082A
10/14/20 20:31NMB
POJ0214
Surrogate
Recovery Control Limits
Tetrachloro-m-xylene 40 % 30-161
Decachlorobiphenyl 18 % 32-178
Total Metals
SE
Mercury
1.0
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 15:02EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/23/20 15:48JAB
POJ0239
Arsenic
<0.17
ug/L
10
1.0
0.17
1
6020B
10/23/20 15:48JAB
POJ0239
Barium
81
ug/L
100
2.0
0.81
1
6020B
10/23/20 15:48JAB
POJ0239
Beryllium
<0.19
CCV
ug/L
1
1.0
0.19
1
6020B
10/23/20 15:48JAB
POJ0239
Cadmium
0.24
J
ug/L
1
1.0
0.16
1
6020B
10/23/20 15:48JAB
POJ0239
Chromium
<0.79
ug/L
10
2.0
0.79
1
6020B
10/23/20 15:48JAB
POJ0239
Cobalt
1.7
J
ug/L
10
2.0
0.52
1
6020B
10/23/20 15:48JAB
POJ0239
Copper
<3.8
ug/L
10
10
3.8
1
6020B
10/23/20 15:48JAB
POJ0239
Lead
<0.26
ug/L
10
1.0
0.26
1
6020B
10/23/20 15:48JAB
POJ0239
Nickel
1.0
J
ug/L
50
3.0
0.51
1
6020B
10/23/20 15:48JAB
POJ0239
Selenium
2.3
J
ug/L
10
5.0
0.74
1
6020B
10/23/20 15:48JAB
POJ0239
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 18:33JAB
POJ0490
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/23/20 15:48JAB
POJ0239
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/23/20 15:48JAB
POJ0239
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/23/20 15:48JAB
POJ0239
Zinc
<6.9
ug/L
10
20
6.9
1
6020B
10/23/20 15:48JAB
POJ0239
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 17:27JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 17:27JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 17:27JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 17:27JLB
POJ0321
1, 1 -Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 17:27JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 17:27JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 17:27JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 84
Laboratory Report
A i • .0 11 /30/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-04-20201012
Attn: Alec Macbeth Sample ID: 0100161-01
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 13:00
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 17:27JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 17:27JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 17:27JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 17:27JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 17:27JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 17:27JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 17:27JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 17:27JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 17:27JLB
POJ0321
1,4-Dichlorobenzene
0.85
ug/L
1
0.50
0.050
1
8260D
10/21/20 17:27JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 17:27JLB
POJ0321
Acetone
<0.31
ug/L
100
5.0
0.31
1
8260D
10/21/20 17:27JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 17:27JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 17:27JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 17:27JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 17:27JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 17:27JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 17:27JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 17:27JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 17:27JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 17:27JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 17:27JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 17:27JLB
POJ0321
Chlorobenzene
0.69
ug/L
3
0.50
0.062
1
8260D
10/21/20 17:27JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 17:27JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 17:27JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 17:27JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 17:27JLB
POJ0321
cis-1,2-Dichloroethylene
0.46 J
ug/L
2
0.50
0.056
1
8260D
10/21/20 17:27JLB
POJ0321
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 17:27JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 17:27JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 17:27JLB
POJ0321
Dichlorodifluoromethane
0.23 J
ug/L
5
5.0
0.11
1
8260D
10/21/20 17:27JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 17:27JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 17:27JLB
POJ0321
Hexachlorobutadiene
0.20 J
ug/L
10
2.0
0.16
1
8260D
10/21/20 17:27JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 17:27JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 84
.
Laboratory Report
• �
Waynt..
11 /30/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID:
MW-04-20201012
Attn: Alec Macbeth
Sample ID: 0100161-01
231 Haywood Street
Project No.:
50-02
Work
Order: 0100161
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/12/20 13:00
Time
Submitted: 10/13/20
08:25
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
m,p-Xylenes
0.31
J ug/L
NE
1.0
0.12
1
8260D
10/21/20 17:27JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 17:27JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 17:27JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 17:27JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 17:27JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 17:27JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 17:27JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 17:27JLB
POJ0321
Naphthalene
0.30
J ug/L
10
1.0
0.30
1
8260D
10/21/20 17:27JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 17:27JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 17:27JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 17:27JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 17:27JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 17:27JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 17:27JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 17:27JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 17:27JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 17:27JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 17:27JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 17:27JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 17:27JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 17:27JLB
POJ0321
Xylenes, total
0.31
J ug/L
5
1.5
0.15
1
8260D
10/21/20 17:27JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
104 % 80-124
Dibromofluoromethane
109 % 75-129
Toluene-d8
100 % 77-123
Volatile Organic Compounds by GC/MS
SIM
1,4-Dioxane
3.4
ug/L
10
2.0
0.14
1
8260D SIM
10/16/20 20:23ANG
POJ0316
8270 Extended List
1,3,5-Trinitrobenzene
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
1,4-Naphthoquinone
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
1-Naphthylamine
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
2-Acetylaminofluorene
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
2-Naphthylamine
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
3-Methylcholanthrene
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
4-Aminobiphenyl
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
5-Nitro-o-toluidine
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 84
Laboratory Report
A i • .0 11 /30/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-04-20201012
Attn: Alec Macbeth Sample ID: 0100161-01
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 13:00
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
7,12-D1methyl benz(a)anthrace ne
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
Diallate
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
Hexachloropropene
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
Isosafrole
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
Kepone
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
Methapyrilene
<10
Ng/L
20
10
1
8270D
10/20/20 17:23BGV
L517325
N-Nitrosomethylethyl amine
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
N-Nitrosopiperidine
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
N-Nitrosopyrrolidine
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
o-Toluidine
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
p-Dimethylaminoazobenzene
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
p-Phenylenediamine
<10 L
pg/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
Pronamide
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
Safrole
<10
Ng/L
10
10
1
8270D
10/20/20 17:23BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
<0.01002
Ng/L
0.03
0.01002
1
8151A
10/21/20 1:33 VIC
L517362
2,4,5-TP (Silvex)
<0.01634
Ng/L
0.1
0.01634
1
8151A
10/21/20 1:33 VIC
L517362
2,4-D
<0.2078
Ng/L
0.25
0.2078
1
8151A
10/21/20 1:33 VIC
L517362
2,4-DB
<0.1364
Ng/L
0.1
0.1364
1
8151A
10/21/20 1:33 VIC
L517362
Dalapon
<0.5149
Ng/L
0.55
0.5149
1
8151A
10/21/20 1:33 VIC
L517362
Dicamba
<0.057
Ng/L
0.1
0.057
1
8151A
10/21/20 1:33 VIC
L517362
Dichlorprop
<0.07959
Ng/L
0.1
0.07959
1
8151A
10/21/20 1:33 VIC
L517362
Dinoseb
<0.02698
Ng/L
0.1
0.02698
1
8151A
10/21/20 1:33 VIC
L517362
MCPA
<18.98
Ng/L
50
18.98
1
8151A
10/21/20 1:33 VIC
L517362
MCPP
<11.75
Ng/L
50
11.75
1
8151A
10/21/20 1:33 VIC
L517362
Picloram
<0.04528
Ng/L
0.1
0.04528
1
8151A
10/21/20 1:33 VIC
L517362
Surrogate
Recovery Control Limits
DCAA
55.8 % 20-150
Semivolatile Organic Compounds - GC/MS
1,2,4,5-Tetrachlorobenzene
<0.317
Ng/L
5
0.317
1
8270D
10/19/20 18:53CCB
L517230
1,2,4-Trichlorobenzene
<0.482
Ng/L
5
0.482
1
8270D
10/19/20 18:53CCB
L517230
1,2-Dichlorobenzene
<0.629
Ng/L
5
0.629
1
8270D
10/19/20 18:53CCB
L517230
1,3-Dichlorobenzene
<0.491
Ng/L
5
0.491
1
8270D
10/19/20 18:53CCB
L517230
1,4-Dichlorobenzene
<0.58
Ng/L
5
0.58
1
8270D
10/19/20 18:53CCB
L517230
2,3,4,6-Tetrachlorophenol
<0.355
Ng/L
5
0.355
1
8270D
10/19/20 18:53CCB
L517230
2,4,5-Trichlorophenol
<0.35
Ng/L
5
0.35
1
8270D
10/19/20 18:53CCB
L517230
2,4,6-Trichlorophenol
<0.344
Ng/L
5
0.344
1
8270D
10/19/20 18:53CCB
L517230
2,4-Dichlorophenol
<1.52
Ng/L
5
1.52
1
8270D
10/19/20 18:53CCB
L517230
2,4-Dimethylphenol
<0.674
Ng/L
5
0.674
1
8270D
10/19/20 18:53CCB
L517230
2,4-Dinitrophenol
<4.85
pg/L
10
4.85
1
8270D
10/19/20 18:53CCB
L517230
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 84
® Laboratory Report
IL AL i • . 11 /30/2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-04-20201012
Attn: Alec Macbeth Sample ID: 0100161-01
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 13:00
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
2,4-Dinitrotoluene
<0.403
pg/L
5
0.403
1
8270D
10/19/20 18:53CCB
L517230
2,6-Dichlorophenol
<0.703
pg/L
5
0.703
1
8270D
10/19/20 18:53CCB
L517230
2,6-Dinitrotoluene
<0.413
pg/L
5
0.413
1
8270D
10/19/20 18:53CCB
L517230
2-Chloronaphthalene
<0.476
pg/L
5
0.476
1
8270D
10/19/20 18:53CCB
L517230
2-Chlorophenol
<0.736
pg/L
5
0.736
1
8270D
10/19/20 18:53CCB
L517230
2-Methyl naphthalene
<0.485
pg/L
2
0.485
1
8270D
10/19/20 18:53CCB
L517230
2-Methylphenol
<0.721
pg/L
5
0.721
1
8270D
10/19/20 18:53CCB
L517230
2-Nitroaniline
<0.574
pg/L
5
0.574
1
8270D
10/19/20 18:53CCB
L517230
2-Nitrophenol
<0.606
pg/L
5
0.606
1
8270D
10/19/20 18:53CCB
L517230
3&4 Methylphenol
<0.691
pg/L
5
0.691
1
8270D
10/19/20 18:53CCB
L517230
3,3' Dimethylbenzidine
<1.88
pg/L
10
1.88
1
8270D
10/19/20 18:53CCB
L517230
3,3'-Dichlorobenzidine
<3.74
pg/L
10
3.74
1
8270D
10/19/20 18:53CCB
L517230
3-Nitroaniline
<1.53
pg/L
10
1.53
1
8270D
10/19/20 18:53CCB
L517230
4,6-Dinitro-2-methylphenol
<3.47
pg/L
10
3.47
1
8270D
10/19/20 18:53CCB
L517230
4-Bromophenyl phenyl ether
<0.5
pg/L
5
0.5
1
8270D
10/19/20 18:53CCB
L517230
4-Chloro-3-methylphenol
<0.503
pg/L
5
0.503
1
8270D
10/19/20 18:53CCB
L517230
4-Chloroaniline
<0.526
pg/L
5
0.526
1
8270D
10/19/20 18:53CCB
L517230
4-Chlorophenyl phenyl ether
<0.479
pg/L
5
0.479
1
8270D
10/19/20 18:53CCB
L517230
4-Nitroaniline
<0.74
pg/L
5
0.74
1
8270D
10/19/20 18:53CCB
L517230
4-Nitrophenol
<1.39
pg/L
10
1.39
1
8270D
10/19/20 18:53CCB
L517230
Acenaphthene
<0.422
pg/L
2
0.422
1
8270D
10/19/20 18:53CCB
L517230
Acenaphthylene
<0.429
pg/L
2
0.429
1
8270D
10/19/20 18:53CCB
L517230
Acetophenone
<0.686
pg/L
5
0.686
1
8270D
10/19/20 18:53CCB
L517230
Aniline
<0.316
pg/L
5
0.316
1
8270D
10/19/20 18:53CCB
L517230
Anthracene
<0.467
pg/L
2
0.467
1
8270D
10/19/20 18:53CCB
L517230
Benzidine
<0.689
pg/L
20
0.689
1
8270D
10/19/20 18:53CCB
L517230
Benzo(a)anthracene
<0.427
pg/L
2
0.427
1
8270D
10/19/20 18:53CCB
L517230
Benzo(a)pyrene
<1
pg/L
2
1
1
8270D
10/19/20 18:53CCB
L517230
Benzo(b)fluoranthene
<0.941
pg/L
2
0.941
1
8270D
10/19/20 18:53CCB
L517230
Benzo(q,h,i)perylene
<1.36
pg/L
2
1.36
1
8270D
10/19/20 18:53CCB
L517230
Benzo(k)fluoranthene
<0.752
pg/L
2
0.752
1
8270D
10/19/20 18:53CCB
L517230
Benzoic Acid
<5
pg/L
10
5
1
8270D
10/19/20 18:53CCB
L517230
Benzyl alcohol
<3.01
pg/L
10
3.01
1
8270D
10/19/20 18:53CCB
L517230
Bis(2-Chloroethoxy)methane
<0.433
pg/L
5
0.433
1
8270D
10/19/20 18:53CCB
L517230
Bis(2-Chloroethyl)ether
<0.447
pg/L
5
0.447
1
8270D
10/19/20 18:53CCB
L517230
Bis(2-Chloroisopropyl)ether
<0.546
pg/L
5
0.546
1
8270D
10/19/20 18:53CCB
L517230
Bis(2-ethylhexyl)phthalate
<3.66
pg/L
5
3.66
1
8270D
10/19/20 18:53CCB
L517230
Butyl benzyl phthalate
<4.59
pg/L
5
4.59
1
8270D
10/19/20 18:53CCB
L517230
Carbazole
<0.476
pg/L
5
0.476
1
8270D
10/19/20 18:53CCB
L517230
Chrysene
<0.731
pg/L
2
0.731
1
8270D
10/19/20 18:53CCB
L517230
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 84
.
Laboratory Report
• �
Waynt.�
11 /30/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID: MW-04-20201012
Attn: Alec Macbeth
Sample ID: 0100161-01
231 Haywood Street
Project No.: 50-02
Work
Order: 0100161
Asheville, NC 28801
Sample Matrix: Water
Time
Collected:
10/12/20 13:00
Time
Submitted:
10/13/20 08:25
Parameter
Result
Units SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
D1benz(a,h)anthrace ne
<0.252
Ng/L
2
0.252
1
8270D
10/19/20 18:53CCB
L517230
Dibenzofuran
<0.423
Ng/L
5
0.423
1
8270D
10/19/20 18:53CCB
L517230
Diethyl phthalate
<0.585
Ng/L
5
0.585
1
8270D
10/19/20 18:53CCB
L517230
Dimethyl phthalate
<0.51
Ng/L
5
0.51
1
8270D
10/19/20 18:53CCB
L517230
Di-n-butyl phthalate
<1.58
Ng/L
5
1.58
1
8270D
10/19/20 18:53CCB
L517230
Di-n-Octyl Phthalate
<1.72
Ng/L
5
1.72
1
8270D
10/19/20 18:53CCB
L517230
Fluoranthene
<0.406
Ng/L
2
0.406
1
8270D
10/19/20 18:53CCB
L517230
Fluorene
<0.444
Ng/L
2
0.444
1
8270D
10/19/20 18:53CCB
L517230
Hexachlorobenzene
<2.57
Ng/L
5
2.57
1
8270D
10/19/20 18:53CCB
L517230
Hexachlorobutadiene
<0.405
Ng/L
5
0.405
1
8270D
10/19/20 18:53CCB
L517230
Hexachlorocyclopentadiene
<2.34
Ng/L
5
2.34
1
8270D
10/19/20 18:53CCB
L517230
Hexachloroethane
<0.277
pg/L
5
0.277
1
8270D
10/19/20 18:53CCB
L517230
Indeno(1,2,3-cd)pyrene
<1.01
Ng/L
2
1.01
1
8270D
10/19/20 18:53CCB
L517230
Isophorone
<0.36
Ng/L
5
0.36
1
8270D
10/19/20 18:53CCB
L517230
Naphthalene
<0.484
Ng/L
2
0.484
1
8270D
10/19/20 18:53CCB
L517230
Nitrobenzene
<0.531
Ng/L
5
0.531
1
8270D
10/19/20 18:53CCB
L517230
N-Nitrosodiethylamine
<0.4
Ng/L
5
0.4
1
8270D
10/19/20 18:53CCB
L517230
N-Nitrosodimethylamine
<0.249
Ng/L
5
0.249
1
8270D
10/19/20 18:53CCB
L517230
N-Nitroso-di-n-butylamine
<0.752
Ng/L
5
0.752
1
8270D
10/19/20 18:53CCB
L517230
N-Nitroso-di-n-propylamine
<0.334
pg/L
5
0.334
1
8270D
10/19/20 18:53CCB
L517230
N-Nitrosodiphenylamine
<0.783
pg/L
10
0.783
1
8270D
10/19/20 18:53CCB
L517230
Pentachlorophenol
<2.45
Ng/L
10
2.45
1
8270D
10/19/20 18:53CCB
L517230
Phenanthrene
<0.464
Ng/L
2
0.464
1
8270D
10/19/20 18:53CCB
L517230
Phenol
<0.389
Ng/L
5
0.389
1
8270D
10/19/20 18:53CCB
L517230
Pyrene
<1.04
pg/L
2
1.04
1
8270D
10/19/20 18:53CCB
L517230
Pyridine
<0.678
pg/L
10
0.678
1
8270D
10/19/20 18:53CCB
L517230
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
27.3 % 39-110
SR
2-Fluorobiphenyl
42.7 % 24-93
2-Fluorophenol
19 % 10-44
4-Terphenyl-d14
112 % 35-126
Nitrobenzene-d5
43.5 % 20-91
Phenol-d6
13.4 % 7-32
Total Organic Carbon
TOC
2.05
mg/L
1
0.498
1
531OC-2011 10/24/20 13:09DDB
L518399
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 84
.
Laboratory Report
• �
Waynt.�
11 /30/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID:
MW-05R-20201012
Attn: Alec Macbeth
Sample ID: 0100161-02
231 Haywood Street
Project No.:
50-02
Work Order: 0100161
Asheville, NC 28801
Sample Matrix:
Water
Time Collected: 10/12/20 14:34
Time Submitted:
10/13/20 08:25
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Anions by Ion Chromatography
Chloride
55000
ug/L
NE
1000
350
1
9056A
10/13/20 22:03BMS
POJ0221
Nitrate as N
75
J ug/L
10000
200
45
1
9056A
10/13/20 22:03BMS
POJ0221
Sulfate
<560
ug/L
250000
2000
560
1
9056A
10/13/20 22:03BMS
POJ0221
Dissolved Metals
Mercury
<0.034
ug/L
0.20
0.034
1
7470A
10/15/20 17:08EDV
POJ0259
Antimony
<0.49
ug/L
2.0
0.49
1
6020B
10/23/20 14:12JAB
POJ0218
Arsenic
<0.17
ug/L
1.0
0.17
1
6020B
10/23/20 14:12JAB
POJ0218
Barium
60
ug/L
100
10
0.81
1
6020B
10/23/20 14:12JAB
POJ0218
Beryllium
<0.19
ug/L
1.0
0.19
1
6020B
10/23/20 14:12JAB
POJ0218
Cadmium
<0.16
ug/L
1.0
0.16
1
6020B
10/23/20 14:12JAB
POJ0218
Chromium
<0.79
ug/L
2.0
0.79
1
6020B
10/23/20 14:12JAB
POJ0218
Cobalt
8.3
ug/L
2.0
0.52
1
6020B
10/23/20 14:12JAB
POJ0218
Copper
<3.8
ug/L
10
3.8
1
6020B
10/23/20 14:12JAB
POJ0218
Lead
<0.26
ug/L
1.0
0.26
1
6020B
10/23/20 14:12JAB
POJ0218
Nickel
1.4
J ug/L
50
3.0
0.51
1
6020B
10/23/20 14:12JAB
POJ0218
Selenium
<0.74
ug/L
10
5.0
0.74
1
6020B
10/23/20 14:12JAB
POJ0218
Silver
<0.11
ug/L
1.0
0.11
1
6020B
10/23/20 14:12JAB
POJ0218
Thallium
<0.57
ug/L
2.0
0.57
1
6020B
10/23/20 14:12JAB
POJ0218
Tin
<1.8
ug/L
5.0
1.8
1
6020B
10/23/20 14:12JAB
POJ0218
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/23/20 14:12JAB
POJ0218
Zinc
18
J ug/L
20
6.9
1
6020B
10/23/20 14:12JAB
POJ0218
General Chemistry Parameters
Biochemical Oxygen Demand
5200
ug/L
NE
2000
210
1
SM5210 B
10/14/20 9:18 ENM
POJ0276
Chemical Oxygen Demand
42000 J
ug/L
NE
50000
11000
1
SM5220 D
10/16/20 11:18SLS
POJ0304
Cyanide
<14
ug/L
10
25
14
5
9014
10/20/20 12:30BMS
POJ0357
Ferrous Iron
12000 HT
ug/L
NE
1000
230
5
SM3500-Fe B
10/13/20 11:14 ENM
POJ0199
Sulfide
5000
ug/L
1000
2000
830
1
SM4500-S F
10/19/20 11:02 ENM
POJ0337
Total Alkalinity to pH 4.5
240000
ug/L
NE
5000
770
1
SM2320 B
10/19/20 11:40 CLB
POJ0341
Organochlorine Pesticides by GC/ECD
A
4,4'-DDD
<0.026
ug/L
0.1
0.10
0.026
1
8081 B
10/16/20 8:28 NMB
POJ0214
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081 B
10/16/20 8:28 NMB
POJ0214
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081 B
10/16/20 8:28 NMB
POJ0214
Aldrin
<0.015
ug/L
0.05
0.050
0.015
1
8081 B
10/16/20 8:28 NMB
POJ0214
alpha-BHC
<0.0063
ug/L
0.05
0.050
0.0063
1
8081 B
10/16/20 8:28 NMB
POJ0214
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/16/20 8:28 NMB
POJ0214
beta-BHC
<0.011
ug/L
0.05
0.050
0.011
1
8081 B
10/16/20 8:28 NMB
POJ0214
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 84
Laboratory Report
A i • .0 11 /30/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-05R-20201012
Attn: Alec Macbeth Sample ID: 0100161-02
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 14:34
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Chlordane
<0.18
ug/L
0.5
0.50
0.18
1
8081 B
10/16/20
8:28 NMB
POJ0214
delta-BHC
<0.0082
ug/L
0.05
0.050
0.0082
1
8081 B
10/16/20
8:28 NMB
POJ0214
Dieldrin
<0.014
ug/L
0.002
0.050
0.014
1
8081 B
10/16/20
8:28 NMB
POJ0214
Endosulfan I
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/16/20
8:28 NMB
POJ0214
Endosulfan 11
<0.012
ug/L
0.1
0.050
0.012
1
8081 B
10/16/20
8:28 NMB
POJ0214
Endosulfan Sulfate
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/16/20
8:28 NMB
POJ0214
Endrin
<0.014
ug/L
0.1
0.050
0.014
1
8081 B
10/16/20
8:28 NMB
POJ0214
Endrin Aldehyde
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/16/20
8:28 NMB
POJ0214
Endrin Ketone
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/16/20
8:28 NMB
POJ0214
gamma-BHC
0.010 DC,
ug/L
0.05
0.050
0.0061
1
8081B
10/16/20
8:28 NMB
POJ0214
J
trans -Chlordane
<0.023
ug/L
NE
0.10 0.023 1
8081 B
10/16/20
8:28 NMB
POJ0214
Heptachlor
<0.013
ug/L
0.05
0.050 0.013 1
8081 B
10/16/20
8:28 NMB
POJ0214
Heptachlor Epoxide
<0.022
ug/L
0.075
0.10 0.022 1
8081 B
10/16/20
8:28 NMB
POJ0214
Methoxychlor
<0.018
ug/L
NE
0.10 0.018 1
8081 B
10/16/20
8:28 NMB
POJ0214
Toxaphene
<0.35
ug/L
1.5
1.0 0.35 1
8081 B
10/16/20
8:28 NMB
POJ0214
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
38 %
13-186
Tetrachloro-m-xylene
77 %
40-134
Polychlorinated Biphenyls (PCBs) by GC/ECD
A
Aroclor 1016
<0.21
ug/L
NE
0.50
0.21
1
8082A
10/16/20 8:28 NMB
POJ0214
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1
8082A
10/16/20 8:28 NMB
POJ0214
Aroclor 1232
<0.16
ug/L
NE
0.50
0.16
1
8082A
10/16/20 8:28 NMB
POJ0214
Aroclor 1242
<0.14
ug/L
NE
0.50
0.14
1
8082A
10/16/20 8:28 NMB
POJ0214
Aroclor 1248
<0.14
ug/L
NE
0.50
0.14
1
8082A
10/16/20 8:28 NMB
POJ0214
Aroclor 1254
<0.16
ug/L
NE
0.50
0.16
1
8082A
10/16/20 8:28 NMB
POJ0214
Aroclor 1260
<0.50
ug/L
NE
1.0
0.50
1
8082A
10/16/20 8:28 NMB
POJ0214
Surrogate
Recovery Control Limits
Tetrachloro-m-xylene
76 % 30-161
Decachlorobiphenyl
41 % 32-178
Total Metals
Mercury
0.73
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 14:51 EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/23/20 16:08JAB
POJ0239
Arsenic
<0.17
ug/L
10
1.0
0.17
1
6020B
10/23/20 14:12JAB
POJ0239
Barium
110
ug/L
100
2.0
0.81
1
6020B
10/23/20 16:08JAB
POJ0239
Beryllium
<0.19 CCV
ug/L
1
1.0
0.19
1
6020B
10/23/20 14:12JAB
POJ0239
Cadmium
<0.16
ug/L
1
1.0
0.16
1
6020B
10/23/20 14:12JAB
POJ0239
Chromium
<0.79
ug/L
10
2.0
0.79
1
6020B
10/23/20 14:12JAB
POJ0239
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 84
.
Laboratory Report
• �
Waynt.�
11 /30/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID:
MW-05R-20201012
Attn: Alec Macbeth
Sample ID: 0100161-02
231 Haywood Street
Project No.:
50-02
Work Order: 0100161
Asheville, NC 28801
Sample Matrix:
Water
Time Collected: 10/12/20 14:34
Time Submitted:
10/13/20 08:25
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Cobalt
8.3
ug/L
10
2.0
0.52
1
6020B
10/23/20 14:12JAB
POJ0239
Copper
5.5
J ug/L
10
10
3.8
1
6020B
10/23/20 16:08JAB
POJ0239
Lead
<0.26
ug/L
10
1.0
0.26
1
6020B
10/23/20 14:12JAB
POJ0239
Nickel
2.7
J ug/L
50
3.0
0.51
1
6020B
10/23/20 16:08JAB
POJ0239
Selenium
0.85
J ug/L
10
5.0
0.74
1
6020B
10/23/20 16:08JAB
POJ0239
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 18:26JAB
POJ0490
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/23/20 16:08JAB
POJ0239
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/23/20 14:12JAB
POJ0239
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/23/20 14:12JAB
POJ0239
Zinc
18
J ug/L
10
20
6.9
1
6020B
10/23/20 14:12JAB
POJ0239
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 18:01JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 18:01JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 18:01JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 18:01JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 18:01JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 18:01JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 18:01JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 18:01JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 18:01JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 18:01JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 18:01JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 18:01JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 18:01JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 18:01JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 18:01JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 18:01JLB
POJ0321
1,4-Dichlorobenzene
0.89
ug/L
1
0.50
0.050
1
8260D
10/21/20 18:01JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 18:01JLB
POJ0321
Acetone
<0.31
ug/L
100
5.0
0.31
1
8260D
10/21/20 18:01JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 18:01JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 18:01JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 18:01JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 18:01JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 18:01JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 18:01JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 18:01JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 84
Laboratory Report
A i • .0 11 /30/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-05R-20201012
Attn: Alec Macbeth Sample ID: 0100161-02
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 14:34
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 18:01JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 18:01JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 18:01JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 18:01JLB
POJ0321
Chlorobenzene
0.67
ug/L
3
0.50
0.062
1
8260D
10/21/20 18:01JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 18:01JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 18:01JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 18:01JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 18:01JLB
POJ0321
cis-1,2-Dichloroethylene
0.41 J
ug/L
2
0.50
0.056
1
8260D
10/21/20 18:01JLB
POJ0321
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 18:01JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 18:01JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 18:01JLB
POJ0321
Dichlorodifluoromethane
0.30 J
ug/L
5
5.0
0.11
1
8260D
10/21/20 18:01JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 18:01JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 18:01JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 18:01JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 18:01JLB
POJ0321
m,p-Xylenes
0.27 J
ug/L
NE
1.0
0.12
1
8260D
10/21/20 18:01JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 18:01JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 18:01JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 18:01JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 18:01JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 18:01JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 18:01JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 18:01JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 18:01JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 18:01JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 18:01JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 18:01JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 18:01JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 18:01JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 18:01JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 18:01JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 18:01JLB
POJ0321
trans- 1,4-Dich loro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 18:01JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 18:01JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 84
.
Laboratory Report
• �
Waynt.�
11 /30/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID:
MW-05R-20201012
Attn: Alec Macbeth
Sample ID: 0100161-02
231 Haywood Street
Project No.:
50-02
Work
Order: 0100161
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/12/20 14:34
Time
Submitted: 10/13/20
08:25
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 18:01JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 18:01JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 18:01JLB
POJ0321
Xylenes, total
0.27
J ug/L
5
1.5
0.15
1
8260D
10/21/20 18:01JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
100 % 80-124
Dibromofluoromethane
109 % 75-129
Toluene-d8
101
% 77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
3.5
ug/L
10
2.0
0.14
1
8260D SIM
10/16/20 20:48ANG
POJ0316
8270 Extended List
1,3,5-Trinitrobenzene
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
1,4-Naphthoqu!none
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
1-Naphthylamine
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
2-Acetylaminofluorene
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
2-Naphthylamine
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
3-Methylcholanthrene
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
4-Aminobiphenyl
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
5-Nitro-o-toluidine
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
7,12-Dimethyl benz(a)anthrace ne
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
Diallate
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
Hexachloropropene
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
Isosafrole
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
Kepone
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
Methapyrilene
<10
Ng/L
20
10
1
8270D
10/20/20 17:45BGV
L517325
N-Nitrosomethylethylamine
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
N-Nitrosopiperidine
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
N-Nitrosopyrrolidine
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
o-Toluidine
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
p-Dimethylaminoazobenzene
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
p-Phenylenediamine
<10
L Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
Pronamide
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
Safrole
<10
Ng/L
10
10
1
8270D
10/20/20 17:45BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
<0.01002
Ng/L
0.03
0.01002
1
8151A
10/21/20 0:16 VIC
L517362
2,4,5-TP (Silvex)
0.08098
J Ng/L
0.1
0.01634
1
8151A
10/21/20 0:16 VIC
L517362
2,4-D
<0.2078
Ng/L
0.25
0.2078
1
8151A
10/21/20 0:16 VIC
L517362
2,4-DB
<0.1364
Ng/L
0.1
0.1364
1
8151A
10/21/20 0:16 VIC
L517362
Dalapon
<0.5149
Ng/L
0.55
0.5149
1
8151A
10/21/20 0:16 VIC
L517362
Dicamba
<0.057
Ng/L
0.1
0.057
1
8151A
10/21/20 0:16 VIC
L517362
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 84
.
Laboratory Report
• �
Waynt.�
11 /30/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID: MW-05R-20201012
Attn: Alec Macbeth
Sample ID: 0100161-02
231 Haywood Street
Project No.: 50-02
Work Order: 0100161
Asheville, NC 28801
Sample Matrix: Water
Time Collected: 10/12/20 14:34
Time Submitted: 10/13/20 08:25
Parameter Result
Units SWSL
Report
MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Dichlorprop <0.07959
Ng/L
0.1
0.07959
1 8151A 10/21/20 0:16 VIC L517362
Dinoseb <0.02698
Ng/L
0.1
0.02698
1 8151A 10/21/20 0:16 VIC L517362
MCPA <18.98
Ng/L
50
18.98
1 8151A 10/21/20 0:16 VIC L517362
MCPP <11.75
Ng/L
50
11.75
1 8151A 10/21/20 0:16 VIC L517362
Picloram <0.04528
Ng/L
0.1
0.04528
1 8151A 10/21/20 0:16 VIC L517362
Surrogate
Recovery Control Limits
DCAA
73.3 % 20-150
Semivolatile Organic Compounds - GC/MS
1,2,4,5-Tetrachlorobenzene
<0.317
Ng/L
5
0.317
1
8270D
10/19/20 19:11 CCB
L517230
1,2,4-Trichlorobenzene
<0.482
Ng/L
5
0.482
1
8270D
10/19/20 19:11 CCB
L517230
1,2-Dichlorobenzene
<0.629
Ng/L
5
0.629
1
8270D
10/19/20 19:11 CCB
L517230
1,3-Dichlorobenzene
<0.491
pg/L
5
0.491
1
8270D
10/19/20 19:11 CCB
L517230
1,4-Dichlorobenzene
3.41 j
Ng/L
5
0.58
1
8270D
10/19/20 19:11 CCB
L517230
2,3,4,6-Tetrachlorophenol
<0.355
Ng/L
5
0.355
1
8270D
10/19/20 19:11 CCB
L517230
2,4,5-Trichlorophenol
<0.35
Ng/L
5
0.35
1
8270D
10/19/20 19:11 CCB
L517230
2,4,6-Trichlorophenol
<0.344
Ng/L
5
0.344
1
8270D
10/19/20 19:11 CCB
L517230
2,4-Dichlorophenol
<1.52
Ng/L
5
1.52
1
8270D
10/19/20 19:11 CCB
L517230
2,4-Dimethylphenol
<0.674
Ng/L
5
0.674
1
8270D
10/19/20 19:11 CCB
L517230
2,4-Dinitrophenol
<4.85
Ng/L
10
4.85
1
8270D
10/19/20 19:11 CCB
L517230
2,4-Dinitrotoluene
<0.403
Ng/L
5
0.403
1
8270D
10/19/20 19:11 CCB
L517230
2,6-Dichlorophenol
<0.703
Ng/L
5
0.703
1
8270D
10/19/20 19:11 CCB
L517230
2,6-Dinitrotoluene
<0.413
Ng/L
5
0.413
1
8270D
10/19/20 19:11 CCB
L517230
2-Chloronaphthalene
<0.476
pg/L
5
0.476
1
8270D
10/19/20 19:11 CCB
L517230
2-Chlorophenol
<0.736
Ng/L
5
0.736
1
8270D
10/19/20 19:11 CCB
L517230
2-Methyl naphthalene
<0.485
Ng/L
2
0.485
1
8270D
10/19/20 19:11 CCB
L517230
2-Methylphenol
<0.721
Ng/L
5
0.721
1
8270D
10/19/20 19:11 CCB
L517230
2-Nitroaniline
<0.574
Ng/L
5
0.574
1
8270D
10/19/20 19:11 CCB
L517230
2-Nitrophenol
<0.606
Ng/L
5
0.606
1
8270D
10/19/20 19:11 CCB
L517230
3&4 Methylphenol
<0.691
Ng/L
5
0.691
1
8270D
10/19/20 19:11 CCB
L517230
3,3' Dimethylbenzidine
<1.88
Ng/L
10
1.88
1
8270D
10/19/20 19:11 CCB
L517230
3,3'-Dichlorobenzidine
<3.74
pg/L
10
3.74
1
8270D
10/19/20 19:11 CCB
L517230
3-Nitroaniline
<1.53
pg/L
10
1.53
1
8270D
10/19/20 19:11 CCB
L517230
4,6-Dinitro-2-methylphenol
<3.47
Ng/L
10
3.47
1
8270D
10/19/20 19:11 CCB
L517230
4-Bromophenyl phenyl ether
<0.5
Ng/L
5
0.5
1
8270D
10/19/20 19:11 CCB
L517230
4-Chloro-3-methylphenol
<0.503
Ng/L
5
0.503
1
8270D
10/19/20 19:11 CCB
L517230
4-Chloroaniline
<0.526
pg/L
5
0.526
1
8270D
10/19/20 19:11 CCB
L517230
4-Chlorophenyl phenyl ether
<0.479
Ng/L
5
0.479
1
8270D
10/19/20 19:11 CCB
L517230
4-Nitroaniline
<0.74
Ng/L
5
0.74
1
8270D
10/19/20 19:11 CCB
L517230
4-Nitrophenol
<1.39
Ng/L
10
1.39
1
8270D
10/19/20 19:11 CCB
L517230
Acenaphthene
<0.422
Ng/L
2
0.422
1
8270D
10/19/20 19:11 CCB
L517230
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 84
® Laboratory Report
IL AL i • . 11 /30/2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-05R-20201012
Attn: Alec Macbeth Sample ID: 0100161-02
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 14:34
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Acenaphthylene
<0.429
pg/L
2
0.429
1
8270D
10/19/20 19:11 CCB
L517230
Acetophenone
<0.686
pg/L
5
0.686
1
8270D
10/19/20 19:11 CCB
L517230
Aniline
<0.316
pg/L
5
0.316
1
8270D
10/19/20 19:11 CCB
L517230
Anthracene
<0.467
pg/L
2
0.467
1
8270D
10/19/20 19:11 CCB
L517230
Benzidine
<0.689
pg/L
20
0.689
1
8270D
10/19/20 19:11 CCB
L517230
Benzo(a)anthracene
<0.427
pg/L
2
0.427
1
8270D
10/19/20 19:11 CCB
L517230
Benzo(a)pyrene
<1
pg/L
2
1
1
8270D
10/19/20 19:11 CCB
L517230
Benzo(b)fluoranthene
<0.941
pg/L
2
0.941
1
8270D
10/19/20 19:11 CCB
L517230
Benzo(g,hJ)perylene
<1.36
pg/L
2
1.36
1
8270D
10/19/20 19:11 CCB
L517230
Benzo(k)fluoranthene
<0.752
pg/L
2
0.752
1
8270D
10/19/20 19:11 CCB
L517230
Benzoic Acid
<5
pg/L
10
5
1
8270D
10/19/20 19:11 CCB
L517230
Benzyl alcohol
<3.01
pg/L
10
3.01
1
8270D
10/19/20 19:11 CCB
L517230
Bis(2-Chloroethoxy)methane
<0.433
pg/L
5
0.433
1
8270D
10/19/20 19:11 CCB
L517230
Bis(2-Chloroethyl)ether
<0.447
pg/L
5
0.447
1
8270D
10/19/20 19:11 CCB
L517230
Bis(2-Chloroisopropyl)ether
<0.546
pg/L
5
0.546
1
8270D
10/19/20 19:11 CCB
L517230
Bis(2-ethylhexyl)phthalate
<3.66
pg/L
5
3.66
1
8270D
10/19/20 19:11 CCB
L517230
Butyl benzyl phthalate
<4.59
pg/L
5
4.59
1
8270D
10/19/20 19:11 CCB
L517230
Carbazole
<0.476
pg/L
5
0.476
1
8270D
10/19/20 19:11 CCB
L517230
Chrysene
<0.731
pg/L
2
0.731
1
8270D
10/19/20 19:11 CCB
L517230
Dibenz(a,h)anthracene
<0.252
pg/L
2
0.252
1
8270D
10/19/20 19:11 CCB
L517230
Dibenzofuran
0.518 j
pg/L
5
0.423
1
8270D
10/19/20 19:11 CCB
L517230
Diethyl phthalate
2.28 j
pg/L
5
0.585
1
8270D
10/19/20 19:11 CCB
L517230
Dimethyl phthalate
<0.51
pg/L
5
0.51
1
8270D
10/19/20 19:11 CCB
L517230
Di-n-butyl phthalate
<1.58
pg/L
5
1.58
1
8270D
10/19/20 19:11 CCB
L517230
Di-n-Octyl Phthalate
<1.72
pg/L
5
1.72
1
8270D
10/19/20 19:11 CCB
L517230
Fluoranthene
<0.406
pg/L
2
0.406
1
8270D
10/19/20 19:11 CCB
L517230
Fluorene
<0.444
pg/L
2
0.444
1
8270D
10/19/20 19:11 CCB
L517230
Hexachlorobenzene
<2.57
pg/L
5
2.57
1
8270D
10/19/20 19:11 CCB
L517230
Hexachlorobutadiene
<0.405
pg/L
5
0.405
1
8270D
10/19/20 19:11 CCB
L517230
Hexachlorocyclopentadiene
<2.34
pg/L
5
2.34
1
8270D
10/19/20 19:11 CCB
L517230
Hexachloroethane
<0.277
pg/L
5
0.277
1
8270D
10/19/20 19:11 CCB
L517230
Indeno(1,2,3-cd)pyrene
<1.01
pg/L
2
1.01
1
8270D
10/19/20 19:11 CCB
L517230
Isophorone
<0.36
pg/L
5
0.36
1
8270D
10/19/20 19:11 CCB
L517230
Naphthalene
<0.484
pg/L
2
0.484
1
8270D
10/19/20 19:11 CCB
L517230
Nitrobenzene
<0.531
pg/L
5
0.531
1
8270D
10/19/20 19:11 CCB
L517230
N-Nitrosodiethylamine
<0.4
pg/L
5
0.4
1
8270D
10/19/20 19:11 CCB
L517230
N-Nitrosodimethylamine
<0.249
pg/L
5
0.249
1
8270D
10/19/20 19:11 CCB
L517230
N-Nitroso-di-n-butylamine
<0.752
pg/L
5
0.752
1
8270D
10/19/20 19:11 CCB
L517230
N-Nitroso-di-n-propylamine
<0.334
pg/L
5
0.334
1
8270D
10/19/20 19:11 CCB
L517230
N-Nitrosodiphenylamine
<0.783
pg/L
10
0.783
1
8270D
10/19/20 19:11 CCB
L517230
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 84
Laboratory Report
• � 11 /30/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-05R-20201012
Attn: Alec Macbeth Sample ID: 0100161-02
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 14:34
Time Submitted: 10/13/20 08:25
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pentachlorophenol <2.45 Ng/L
Phenanthrene <0.464 Ng/L
Phenol <0.389 Ng/L
Pyrene <1.04 Ng/L
Pyridine <0.678 ua/L
Total Organic Carbon
TOC 7.05 mg/L
10
2.45
1
8270D
10/19/20 19:11 CCB
L517230
2
0.464
1
8270D
10/19/20 19:11 CCB
L517230
5
0.389
1
8270D
10/19/20 19:11 CCB
L517230
2
1.04
1
8270D
10/19/20 19:11 CCB
L517230
10
0.678
1
8270D
10/19/20 19:11 CCB
L517230
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
49 %
39-110
2-Fluorobiphenyl
43.5 %
24-93
2-Fluorophenol
23.7 %
10-44
4-Terphenyl-d14
104 %
35-126
Nitrobenzene-d5
47.2 %
20-91
Phenol-d6
15.7 %
7-32
1 0.498 1 531 OC-2011 10/24/20 13:47 DDB L518399
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 84
Laboratory Report
• � 11 /30/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-07-20201012
Attn: Alec Macbeth Sample ID: 0100161-03
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 10:57
Time Submitted: 10/13/20 08:25
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Anions by Ion Chromatography
Chloride 79000 ug/L NE 1000 350 1 9056A 10/13/20 19:41 BMS POJ0221
Nitrate as N 92 J ug/L 10000 200 45 1 9056A 10/13/20 19:41 BMS POJ0221
Sulfate 25000 ug/L 250000 2000 560 1 9056A 10/13/20 19:41 BMS POJ0221
General Chemistry Parameters
Biochemical Oxygen Demand
920 J
ug/L
NE
2000
210
1
SM5210 B
10/14/20
9:18 ENM
POJ0276
Chemical Oxygen Demand
18000 J
ug/L
NE
50000
11000
1
SM5220 D
10/19/20
11:56SLS
POJ0361
Cyanide
<14
ug/L
10
25
14
5
9014
10/20/20
12:30BMS
POJ0357
Ferrous Iron
360 HT
ug/L
NE
200
46
1
SM3500-Fe B
10/13/20
11:14 ENM
POJ0199
Sulfide
<830
ug/L
1000
2000
830
1
SM4500-S F
10/19/20
11:02ENM
POJ0337
Total Alkalinity to pH 4.5
250000
ug/L
NE
5000
770
1
SM2320 B
10/19/20
11:40 CLB
POJ0341
Organochlorine Pesticides by GC/ECD
A
4,4'-DDD
<0.026
ug/L
0.1
0.10
0.026
1
8081 B
10/16/20
8:41 NMB
POJ0214
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081 B
10/16/20
8:41 NMB
POJ0214
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081 B
10/16/20
8:41 NMB
POJ0214
Aldrin
<0.015
ug/L
0.05
0.050
0.015
1
8081 B
10/16/20
8:41 NMB
POJ0214
alpha-BHC
<0.0063
ug/L
0.05
0.050
0.0063
1
8081 B
10/16/20
8:41 NMB
POJ0214
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/16/20
8:41 NMB
POJ0214
beta-BHC
<0.011
ug/L
0.05
0.050
0.011
1
8081 B
10/16/20
8:41 NMB
POJ0214
Chlordane
<0.18
ug/L
0.5
0.50
0.18
1
8081 B
10/16/20
8:41 NMB
POJ0214
delta-BHC
<0.0082
ug/L
0.05
0.050
0.0082
1
8081 B
10/16/20
8:41 NMB
POJ0214
Dieldrin
<0.014
ug/L
0.002
0.050
0.014
1
8081 B
10/16/20
8:41 NMB
POJ0214
Endosulfan 1
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/16/20
8:41 NMB
POJ0214
Endosulfan 11
<0.012
ug/L
0.1
0.050
0.012
1
8081 B
10/16/20
8:41 NMB
POJ0214
Endosulfan Sulfate
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/16/20
8:41 NMB
POJ0214
Endrin
<0.014
ug/L
0.1
0.050
0.014
1
8081 B
10/16/20
8:41 NMB
POJ0214
Endrin Aldehyde
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/16/20
8:41 NMB
POJ0214
Endrin Ketone
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/16/20
8:41 NMB
POJ0214
gamma-BHC
<0.0061
ug/L
0.05
0.050
0.0061
1
8081 B
10/16/20
8:41 NMB
POJ0214
trans -Chlordane
<0.023
ug/L
NE
0.10
0.023
1
8081 B
10/16/20
8:41 NMB
POJ0214
Heptachlor
<0.013
ug/L
0.05
0.050
0.013
1
8081 B
10/16/20
8:41 NMB
POJ0214
Heptachlor Epoxide
<0.022
ug/L
0.075
0.10
0.022
1
8081 B
10/16/20
8:41 NMB
POJ0214
Methoxychlor
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/16/20
8:41 NMB
POJ0214
Toxaphene
<0.35
ug/L
1.5
1.0
0.35
1
8081 B
10/16/20
8:41 NMB
POJ0214
Surrogate
Recovery Control Limits
Decachlorobiphenyl 34 % 13-186
Tetrachloro-m-xylene 72 % 40-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 84
Laboratory Report
• � 11 /30/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-07-20201012
Attn: Alec Macbeth Sample ID: 0100161-03
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 10:57
Time Submitted: 10/13/20 08:25
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Polychlorinated Biphenyls (PCBs) by GC/ECD
A
Aroclor 1016
<0.21
ug/L
NE
0.50
0.21
1
8082A
10/16/20
8:41 NMB
POJ0214
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1
8082A
10/16/20
8:41 NMB
POJ0214
Aroclor 1232
<0.16
ug/L
NE
0.50
0.16
1
8082A
10/16/20
8:41 NMB
POJ0214
Aroclor 1242
<0.14
ug/L
NE
0.50
0.14
1
8082A
10/16/20
8:41 NMB
POJ0214
Aroclor 1248
<0.14
ug/L
NE
0.50
0.14
1
8082A
10/16/20
8:41 NMB
POJ0214
Aroclor 1254
<0.16
ug/L
NE
0.50
0.16
1
8082A
10/16/20
8:41 NMB
POJ0214
Aroclor 1260
<0.50
ug/L
NE
1.0
0.50
1
8082A
10/16/20
8:41 NMB
POJ0214
Surrogate
Recovery Control Limits
Tetrachloro-m-xylene 72 % 30-161
Decachlorobiphenyl 35 % 32-178
Total Metals
Mercury
0.53
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 15:06EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/23/20 16:15JAB
POJ0239
Arsenic
<0.17
ug/L
10
1.0
0.17
1
6020B
10/23/20 16:15JAB
POJ0239
Barium
390
ug/L
100
2.0
0.81
1
6020B
10/23/20 16:15JAB
POJ0239
Beryllium
<0.19 CCV
ug/L
1
1.0
0.19
1
6020B
10/23/20 16:15JAB
POJ0239
Cadmium
<0.16
ug/L
1
1.0
0.16
1
6020B
10/23/20 16:15JAB
POJ0239
Chromium
0.90 J
ug/L
10
2.0
0.79
1
6020B
10/23/20 16:15JAB
POJ0239
Cobalt
1.4 J
ug/L
10
2.0
0.52
1
6020B
10/23/20 16:15JAB
POJ0239
Copper
<3.8
ug/L
10
10
3.8
1
6020B
10/23/20 16:15JAB
POJ0239
Lead
<0.26
ug/L
10
1.0
0.26
1
6020B
10/23/20 16:15JAB
POJ0239
Nickel
7.1
ug/L
50
3.0
0.51
1
6020B
10/23/20 16:15JAB
POJ0239
Selenium
<0.74
ug/L
10
5.0
0.74
1
6020B
10/23/20 16:15JAB
POJ0239
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 18:06JAB
POJ0490
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/23/20 16:15JAB
POJ0239
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/23/20 16:15JAB
POJ0239
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/23/20 16:15JAB
POJ0239
Zinc
<6.9
ug/L
10
20
6.9
1
6020B
10/23/20 16:15JAB
POJ0239
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 18:35JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 18:35JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 18:35JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 18:35JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 18:35JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 18:35JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 18:35JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 84
Laboratory Report
A i • .0 11 /30/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-07-20201012
Attn: Alec Macbeth Sample ID: 0100161-03
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 10:57
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 18:35JLB
POJ0321
1,2,4-Trichlorobenzene
0.23 J
ug/L
10
1.0
0.13
1
8260D
10/21/20 18:35JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 18:35JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 18:35JLB
POJ0321
1,2-Dichlorobenzene
0.50
ug/L
5
0.50
0.076
1
8260D
10/21/20 18:35JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 18:35JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 18:35JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 18:35JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 18:35JLB
POJ0321
1,4-Dichlorobenzene
6.8
ug/L
1
0.50
0.050
1
8260D
10/21/20 18:35JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 18:35JLB
POJ0321
Acetone
<0.31
ug/L
100
5.0
0.31
1
8260D
10/21/20 18:35JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 18:35JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 18:35JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 18:35JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 18:35JLB
POJ0321
Benzene
1.4
ug/L
1
0.50
0.048
1
8260D
10/21/20 18:35JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 18:35JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 18:35JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 18:35JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 18:35JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 18:35JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 18:35JLB
POJ0321
Chlorobenzene
6.1
ug/L
3
0.50
0.062
1
8260D
10/21/20 18:35JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 18:35JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 18:35JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 18:35JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 18:35JLB
POJ0321
cis-1,2-Dichloroethylene
2.6
ug/L
2
0.50
0.056
1
8260D
10/21/20 18:35JLB
POJ0321
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 18:35JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 18:35JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 18:35JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 18:35JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 18:35JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 18:35JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 18:35JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 18:35JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 84
.
Laboratory Report
• �
Waynt..
11 /30/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID:
MW-07-20201012
Attn: Alec Macbeth
Sample ID: 0100161-03
231 Haywood Street
Project No.:
50-02
Work
Order: 0100161
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/12/20 10:57
Time
Submitted: 10/13/20
08:25
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
m,p-Xylenes
0.42
J ug/L
NE
1.0
0.12
1
8260D
10/21/20 18:35JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 18:35JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 18:35JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 18:35JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 18:35JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 18:35JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 18:35JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 18:35JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 18:35JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 18:35JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 18:35JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 18:35JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 18:35JLB
POJ0321
Tetrahydrofuran
1.6
J ug/L
NE
10
1.1
1
8260D
10/21/20 18:35JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 18:35JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 18:35JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 18:35JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 18:35JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 18:35JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 18:35JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 18:35JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 18:35JLB
POJ0321
Xylenes, total
0.42
J ug/L
5
1.5
0.15
1
8260D
10/21/20 18:35JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
102 % 80-124
Dibromofluoromethane
105 % 75-129
Toluene-d8
99 % 77-123
Volatile Organic Compounds by GC/MS
SIM
1,4-Dioxane
17
ug/L
10
2.0
0.14
1
8260D SIM
10/16/20 21:13ANG
POJ0316
8270 Extended List
1,3,5-Trinitrobenzene
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
1,4-Naphthoquinone
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
1-Naphthylamine
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
2-Acetylaminofluorene
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
2-Naphthylamine
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
3-Methylcholanthrene
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
4-Aminobiphenyl
<10
Ng/L
10
10
1
8270D
10/20/20 18:07 BGV
L517325
5-Nitro-o-toluidine
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 84
Laboratory Report
A i • .0 11 /30/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-07-20201012
Attn: Alec Macbeth Sample ID: 0100161-03
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 10:57
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
7,12-D1methyl benz(a)anthrace ne
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
Diallate
<10
Ng/L
10
10
1
8270D
10/20/20 18:07 BGV
L517325
Hexachloropropene
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
Isosafrole
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
Kepone
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
Methapyrilene
<10
Ng/L
20
10
1
8270D
10/20/20 18:07BGV
L517325
N-Nitrosomethylethyl amine
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
N-Nitrosopiperidine
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
N-Nitrosopyrrolidine
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
o-Toluidine
<10
Ng/L
10
10
1
8270D
10/20/20 18:07 BGV
L517325
p-Dimethylaminoazobenzene
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
p-Phenylenediamine
<10 L
pg/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
Pronamide
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
Safrole
<10
Ng/L
10
10
1
8270D
10/20/20 18:07BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
<0.01002
Ng/L
0.03
0.01002
1
8151A
10/20/20 23:25VIC
L517362
2,4,5-TP (Silvex)
<0.01634
Ng/L
0.1
0.01634
1
8151A
10/20/20 23:25VIC
L517362
2,4-D
<0.2078
Ng/L
0.25
0.2078
1
8151A
10/20/20 23:25VIC
L517362
2,4-DB
<0.1364
Ng/L
0.1
0.1364
1
8151A
10/20/20 23:25VIC
L517362
Dalapon
<0.5149
Ng/L
0.55
0.5149
1
8151A
10/20/20 23:25VIC
L517362
Dicamba
<0.057
Ng/L
0.1
0.057
1
8151A
10/20/20 23:25VIC
L517362
Dichlorprop
<0.07959
Ng/L
0.1
0.07959
1
8151A
10/20/20 23:25VIC
L517362
Dinoseb
<0.02698
Ng/L
0.1
0.02698
1
8151A
10/20/20 23:25VIC
L517362
MCPA
<18.98
Ng/L
50
18.98
1
8151A
10/20/20 23:25VIC
L517362
MCPP
<11.75
Ng/L
50
11.75
1
8151A
10/20/20 23:25VIC
L517362
Picloram
<0.04528
Ng/L
0.1
0.04528
1
8151A
10/20/20 23:25VIC
L517362
Surrogate
Recovery Control Limits
DCAA
51.2 % 20-150
Semivolatile Organic Compounds - GUMS
1,2,4,5-Tetrachlorobenzene
<0.317
Ng/L
5
0.317
1
8270D
10/19/20 19:30CCB
L517230
1,2,4-Trichlorobenzene
<0.482
Ng/L
5
0.482
1
8270D
10/19/20 19:30CCB
L517230
1,2-Dichlorobenzene
<0.629
Ng/L
5
0.629
1
8270D
10/19/20 19:30CCB
L517230
1,3-Dichlorobenzene
<0.491
Ng/L
5
0.491
1
8270D
10/19/20 19:30CCB
L517230
1,4-Dichlorobenzene
2.66 j
Ng/L
5
0.58
1
8270D
10/19/20 19:30CCB
L517230
2,3,4,6-Tetrachlorophenol
<0.355
Ng/L
5
0.355
1
8270D
10/19/20 19:30CCB
L517230
2,4,5-Trichlorophenol
<0.35
Ng/L
5
0.35
1
8270D
10/19/20 19:30CCB
L517230
2,4,6-Trichlorophenol
<0.344
Ng/L
5
0.344
1
8270D
10/19/20 19:30CCB
L517230
2,4-Dichlorophenol
<1.52
Ng/L
5
1.52
1
8270D
10/19/20 19:30CCB
L517230
2,4-Dimethylphenol
<0.674
Ng/L
5
0.674
1
8270D
10/19/20 19:30CCB
L517230
2,4-Dinitrophenol
<4.85
Ng/L
10
4.85
1
8270D
10/19/20 19:30CCB
L517230
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 84
® Laboratory Report
IL AL i • . 11 /30/2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-07-20201012
Attn: Alec Macbeth Sample ID: 0100161-03
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 10:57
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
2,4-Dinitrotoluene
<0.403
pg/L
5
0.403
1
8270D
10/19/20 19:30CCB
L517230
2,6-Dichlorophenol
<0.703
pg/L
5
0.703
1
8270D
10/19/20 19:30CCB
L517230
2,6-Dinitrotoluene
<0.413
pg/L
5
0.413
1
8270D
10/19/20 19:30CCB
L517230
2-Chloronaphthalene
<0.476
pg/L
5
0.476
1
8270D
10/19/20 19:30CCB
L517230
2-Chlorophenol
<0.736
pg/L
5
0.736
1
8270D
10/19/20 19:30CCB
L517230
2-Methyl naphthalene
<0.485
pg/L
2
0.485
1
8270D
10/19/20 19:30CCB
L517230
2-Methylphenol
<0.721
pg/L
5
0.721
1
8270D
10/19/20 19:30CCB
L517230
2-Nitroaniline
<0.574
pg/L
5
0.574
1
8270D
10/19/20 19:30CCB
L517230
2-Nitrophenol
<0.606
pg/L
5
0.606
1
8270D
10/19/20 19:30CCB
L517230
3&4 Methylphenol
<0.691
pg/L
5
0.691
1
8270D
10/19/20 19:30CCB
L517230
3,3' Dimethylbenzidine
<1.88
pg/L
10
1.88
1
8270D
10/19/20 19:30CCB
L517230
3,3'-Dichlorobenzidine
<3.74
pg/L
10
3.74
1
8270D
10/19/20 19:30CCB
L517230
3-Nitroaniline
<1.53
pg/L
10
1.53
1
8270D
10/19/20 19:30CCB
L517230
4,6-Dinitro-2-methylphenol
<3.47
pg/L
10
3.47
1
8270D
10/19/20 19:30CCB
L517230
4-Bromophenyl phenyl ether
<0.5
pg/L
5
0.5
1
8270D
10/19/20 19:30CCB
L517230
4-Chloro-3-methylphenol
<0.503
pg/L
5
0.503
1
8270D
10/19/20 19:30CCB
L517230
4-Chloroaniline
<0.526
pg/L
5
0.526
1
8270D
10/19/20 19:30CCB
L517230
4-Chlorophenyl phenyl ether
<0.479
pg/L
5
0.479
1
8270D
10/19/20 19:30CCB
L517230
4-Nitroaniline
<0.74
pg/L
5
0.74
1
8270D
10/19/20 19:30CCB
L517230
4-Nitrophenol
<1.39
pg/L
10
1.39
1
8270D
10/19/20 19:30CCB
L517230
Acenaphthene
<0.422
pg/L
2
0.422
1
8270D
10/19/20 19:30CCB
L517230
Acenaphthylene
<0.429
pg/L
2
0.429
1
8270D
10/19/20 19:30CCB
L517230
Acetophenone
<0.686
pg/L
5
0.686
1
8270D
10/19/20 19:30CCB
L517230
Aniline
<0.316
pg/L
5
0.316
1
8270D
10/19/20 19:30CCB
L517230
Anthracene
<0.467
pg/L
2
0.467
1
8270D
10/19/20 19:30CCB
L517230
Benzidine
<0.689
pg/L
20
0.689
1
8270D
10/19/20 19:30CCB
L517230
Benzo(a)anthracene
<0.427
pg/L
2
0.427
1
8270D
10/19/20 19:30CCB
L517230
Benzo(a)pyrene
<1
pg/L
2
1
1
8270D
10/19/20 19:30CCB
L517230
Benzo(b)fluoranthene
<0.941
pg/L
2
0.941
1
8270D
10/19/20 19:30CCB
L517230
Benzo(q,h,i)perylene
<1.36
pg/L
2
1.36
1
8270D
10/19/20 19:30CCB
L517230
Benzo(k)fluoranthene
<0.752
pg/L
2
0.752
1
8270D
10/19/20 19:30CCB
L517230
Benzoic Acid
<5
pg/L
10
5
1
8270D
10/19/20 19:30CCB
L517230
Benzyl alcohol
<3.01
pg/L
10
3.01
1
8270D
10/19/20 19:30CCB
L517230
Bis(2-Chloroethoxy)methane
<0.433
pg/L
5
0.433
1
8270D
10/19/20 19:30CCB
L517230
Bis(2-Chloroethyl)ether
<0.447
pg/L
5
0.447
1
8270D
10/19/20 19:30CCB
L517230
Bis(2-Chloroisopropyl)ether
<0.546
pg/L
5
0.546
1
8270D
10/19/20 19:30CCB
L517230
Bis(2-ethylhexyl)phthalate
<3.66
pg/L
5
3.66
1
8270D
10/19/20 19:30CCB
L517230
Butyl benzyl phthalate
<4.59
pg/L
5
4.59
1
8270D
10/19/20 19:30CCB
L517230
Carbazole
<0.476
pg/L
5
0.476
1
8270D
10/19/20 19:30CCB
L517230
Chrysene
<0.731
pg/L
2
0.731
1
8270D
10/19/20 19:30CCB
L517230
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 84
.
Laboratory Report
• �
Waynt.�
11 /30/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID: MW-07-20201012
Attn: Alec Macbeth
Sample ID: 0100161-03
231 Haywood Street
Project No.: 50-02
Work
Order: 0100161
Asheville, NC 28801
Sample Matrix: Water
Time
Collected: 10/12/20 10:57
Time
Submitted: 10/13/20 08:25
Parameter
Result
Units SWSL
Report
MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
D1benz(a,h)anthrace ne
<0.252
Ng/L
2
0.252
1
8270D 10/19/20 19:30CCB
L517230
Dibenzofuran
<0.423
Ng/L
5
0.423
1
8270D 10/19/20 19:30CCB
L517230
Diethyl phthalate
<0.585
Ng/L
5
0.585
1
8270D 10/19/20 19:30CCB
L517230
Dimethyl phthalate
<0.51
Ng/L
5
0.51
1
8270D 10/19/20 19:30CCB
L517230
Di-n-butyl phthalate
<1.58
Ng/L
5
1.58
1
8270D 10/19/20 19:30CCB
L517230
Di-n-Octyl Phthalate
<1.72
Ng/L
5
1.72
1
8270D 10/19/20 19:30CCB
L517230
Fluoranthene
<0.406
Ng/L
2
0.406
1
8270D 10/19/20 19:30CCB
L517230
Fluorene
<0.444
Ng/L
2
0.444
1
8270D 10/19/20 19:30CCB
L517230
Hexachlorobenzene
<2.57
Ng/L
5
2.57
1
8270D 10/19/20 19:30CCB
L517230
Hexachlorobutadiene
<0.405
Ng/L
5
0.405
1
8270D 10/19/20 19:30CCB
L517230
Hexachlorocyclopentadiene
<2.34
Ng/L
5
2.34
1
8270D 10/19/20 19:30CCB
L517230
Hexachloroethane
<0.277
pg/L
5
0.277
1
8270D 10/19/20 19:30CCB
L517230
Indeno(1,2,3-cd)pyrene
<1.01
Ng/L
2
1.01
1
8270D 10/19/20 19:30CCB
L517230
Isophorone
<0.36
Ng/L
5
0.36
1
8270D 10/19/20 19:30CCB
L517230
Naphthalene
<0.484
Ng/L
2
0.484
1
8270D 10/19/20 19:30CCB
L517230
Nitrobenzene
<0.531
Ng/L
5
0.531
1
8270D 10/19/20 19:30CCB
L517230
N-Nitrosodiethylamine
<0.4
Ng/L
5
0.4
1
8270D 10/19/20 19:30CCB
L517230
N-Nitrosodimethylamine
<0.249
Ng/L
5
0.249
1
8270D 10/19/20 19:30CCB
L517230
N-Nitroso-di-n-butylamine
<0.752
Ng/L
5
0.752
1
8270D 10/19/20 19:30CCB
L517230
N-Nitroso-di-n-propylamine
<0.334
pg/L
5
0.334
1
8270D 10/19/20 19:30CCB
L517230
N-Nitrosodiphenylamine
<0.783
pg/L
10
0.783
1
8270D 10/19/20 19:30CCB
L517230
Pentachlorophenol
<2.45
Ng/L
10
2.45
1
8270D 10/19/20 19:30CCB
L517230
Phenanthrene
<0.464
Ng/L
2
0.464
1
8270D 10/19/20 19:30CCB
L517230
Phenol
<0.389
Ng/L
5
0.389
1
8270D 10/19/20 19:30CCB
L517230
Pyrene
<1.04
pg/L
2
1.04
1
8270D 10/19/20 19:30CCB
L517230
Pyridine
<0.678
pg/L
10
0.678
1
8270D 10/19/20 19:30CCB
L517230
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
47.4 % 39-110
2-Fluorobiphenyl
43.4 % 24-93
2-Fluorophenol
25.1 % 10-44
4-Terphenyl-d14
103 % 35-126
Nitrobenzene-d5
46.6 % 20-91
Phenol-d6
17.6 % 7-32
Total Organic Carbon
TOC
3.22
mg/L
1
0.498
1
531OC-2011 10/24/20 14:24DDB
L518399
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 84
Laboratory Report
• � 11 /30/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: TB-202010120000
Attn: Alec Macbeth Sample ID: 0100161-04
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 00:00
Time Submitted: 10/13/20 08:25
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 15:45JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 15:45JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 15:45JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 15:45JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 15:45JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 15:45JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 15:45JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 15:45JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 15:45JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 15:45JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 15:45JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 15:45JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 15:45JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 15:45JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 15:45JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 15:45JLB
POJ0321
1,4-Dichlorobenzene
<0.050
ug/L
1
0.50
0.050
1
8260D
10/21/20 15:45JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 15:45JLB
POJ0321
Acetone
3.2 J
ug/L
100
5.0
0.31
1
8260D
10/21/20 15:45JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 15:45JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 15:45JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 15:45JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 15:45JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 15:45JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 15:45JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 15:45JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 15:45JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 15:45JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 15:45JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 15:45JLB
POJ0321
Chlorobenzene
<0.062
ug/L
3
0.50
0.062
1
8260D
10/21/20 15:45JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 15:45JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 15:45JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 15:45JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 15:45JLB
POJ0321
cis- 1,2-Dichloroethylene
<0.056
ug/L
2
0.50
0.056
1
8260D
10/21/20 15:45JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 84
Laboratory Report
A i • .0 11 /30/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: TB-202010120000
Attn: Alec Macbeth Sample ID: 0100161-04
231 Haywood Street Project No.: 50-02 Work Order: 0100161
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/12/20 00:00
Time Submitted: 10/13/20 08:25
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 15:45JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 15:45JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 15:45JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 15:45JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 15:45JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 15:45JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 15:45JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 15:45JLB
POJ0321
m,p-Xylenes
<0.12
ug/L
NE
1.0
0.12
1
8260D
10/21/20 15:45JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 15:45JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 15:45JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 15:45JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 15:45JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 15:45JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 15:45JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 15:45JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 15:45JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 15:45JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 15:45JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 15:45JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 15:45JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 15:45JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 15:45JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 15:45JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 15:45JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 15:45JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 15:45JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 15:45JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 15:45JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 15:45JLB
POJ0321
Xylenes, total
<0.15
ug/L
5
1.5
0.15
1
8260D
10/21/20 15:45JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
101 % 80-124
Dibromofluoromethane
107 % 75-129
Toluene-d8
101 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 84
(2)
Way po Int
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
Blank (POJ0321-BLK1)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,1-Dichloropropylene
BRL
0.50
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
0.290
1.0
ug/L J
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,3-Dichlorobenzene
BRL
0.50
ug/L
1,3-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
Acetone
BRL
5.0
ug/L
Acetonitrile
BRL
10
ug/L
Acrolein
BRL
20
ug/L
Acrylonitrile
BRL
20
ug/L
Allyl Chloride (3-Chloropropylene)
BRL
10
ug/L
Benzene
BRL
0.50
ug/L
Bromochloromethane
BRL
0.50
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
0.50
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
Chloroprene
BRL
10
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
0.50
ug/L
Dichlorodifluoromethane
BRL
5.0
ug/L
Ethyl Methacrylate
BRL
10
ug/L
Ethylbenzene
BRL
0.50
ug/L
Hexachlorobutadiene
0.220
2.0
ug/L J
Isobutyl alcohol
BRL
50
ug/L
m,p-Xylenes
0.250
1.0
ug/L J
Methacrylonitrile
BRL
10
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 30 of 84
Waypoint '
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
Blank (POJ0321-BLK1)
Prepared & Analyzed: 10/21/20
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methyl Methacrylate
BRL
10
ug/L
Methylene Chloride
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
o-Xylene
BRL
0.50
ug/L
Propionitrile (Ethyl Cyanide)
BRL
10
ug/L
Styrene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrahydrofuran
BRL
10
ug/L
Toluene
BRL
0.50
ug/L
trans- 1,2-Dichloroethylene
BRL
0.50
ug/L
trans- 1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
Trichloroethylene
BRL
0.50
ug/L
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
0.250
1.5
ug/L
J
Surrogate:4-Bromofluorobenzene
50.3
ug/L
50.00
101
80-124
Surrogate: Dibromofluoromethane
53.8
ug/L
50.00
108
75-129
Surrogate: Toluene-d8
49.6
ug/L
50.00
99
77-123
LCS (POJ0321-BS1)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
21.5
0.50
ug/L
20.00
108
79-134
1,1,1-Trichloroethane
21.3
0.50
ug/L
20.00
106
75-136
1,1,2,2-Tetrachloroethane
21.0
0.50
ug/L
20.00
105
62-127
1,1,2-Trichloroethane
21.6
0.50
ug/L
20.00
108
70-140
1,1-Dichloroethane
21.6
0.50
ug/L
20.00
108
78-130
1,1-Dichloroethylene
21.2
0.50
ug/L
20.00
106
70-154
1, 1 -Dichloropropylene
22.0
0.50
ug/L
20.00
110
71-136
1,2,3-Trichloropropane
21.2
1.0
ug/L
20.00
106
71-127
1,2,4-Trichlorobenzene
20.4
1.0
ug/L
20.00
102
66-139
1,2-Dibromo-3-chloropropane
22.9
2.0
ug/L
20.00
114
63-134
1,2-Dibromoethane
21.3
0.50
ug/L
20.00
107
77-135
1,2-Dichlorobenzene
21.3
0.50
ug/L
20.00
106
78-128
1,2-Dichloroethane
21.6
0.50
ug/L
20.00
108
68-131
1,2-Dichloropropane
21.9
0.50
ug/L
20.00
110
77-130
1,3-Dichlorobenzene
21.5
0.50
ug/L
20.00
107
77-125
1,3-Dichloropropane
22.0
0.50
ug/L
20.00
110
76-132
1,4-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
75-126
2,2-Dichloropropane
23.8
2.0
ug/L
20.00
119
29-149
Acetone
39.6
5.0
ug/L
40.00
99
40-166
Acetonitrile
19.4
10
ug/L
20.00
97
70-130
Acrolein
45.9
20
ug/L
40.00
115
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 84
Waypoint '
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS (POJ0321-BSI)
Prepared &Analyzed: 10/21/20
Acrylonitrile
42.3
20
ug/L
40.00
106
81-127
Allyl Chloride (3-Chloropropylene)
19.4
10
ug/L
20.00
97
70-130
Benzene
22.7
0.50
ug/L
20.00
114
77-128
Bromochloromethane
22.1
0.50
ug/L
20.00
110
78-135
Bromodichloromethane
21.7
0.50
ug/L
20.00
108
76-138
Bromoform
22.4
1.0
ug/L
20.00
112
71-135
Bromomethane
21.0
1.0
ug/L
20.00
105
41-168
Carbon disulfide
21.1
5.0
ug/L
20.00
106
59-135
Carbon Tetrachloride
21.7
0.50
ug/L
20.00
109
72-142
Chlorobenzene
22.0
0.50
ug/L
20.00
110
78-119
Chloroethane
21.5
0.50
ug/L
20.00
107
57-142
Chloroform
21.0
0.50
ug/L
20.00
105
77-130
Chloromethane
20.5
0.50
ug/L
20.00
102
47-145
Chloroprene
19.7
10
ug/L
20.00
98
70-130
cis-1,2-Dichloroethylene
22.5
0.50
ug/L
20.00
113
76-141
cis-1,3-Dichloropropylene
22.4
0.50
ug/L
20.00
112
65-140
Dibromochloromethane
21.2
0.50
ug/L
20.00
106
75-134
Dibromomethane
21.8
0.50
ug/L
20.00
109
76-138
Dichlorodifluoromethane
25.2
5.0
ug/L
20.00
126
28-163
Ethyl Methacrylate
19.7
10
ug/L
20.00
99
70-130
Ethylbenzene
22.7
0.50
ug/L
20.00
114
80-127
Hexachlorobutadiene
20.1
2.0
ug/L
20.00
100
61-134
Isobutyl alcohol
24.0
50
ug/L
20.00
120
70-130 J
m,p-Xylenes
48.4
1.0
ug/L
40.00
121
77-133
Methacrylonitrile
19.5
10
ug/L
20.00
98
70-130
Methyl Butyl Ketone (2-Hexanone)
22.7
5.0
ug/L
20.00
114
64-137
Methyl Ethyl Ketone (2-Butanone)
20.2
5.0
ug/L
20.00
101
71-134
Methyl Iodide
23.5
5.0
ug/L
20.00
118
70-130
Methyl Isobutyl Ketone
23.8
5.0
ug/L
20.00
119
69-134
Methyl Methacrylate
20.3
10
ug/L
20.00
102
70-130
Methylene Chloride
20.7
1.0
ug/L
20.00
103
73-131
Naphthalene
21.0
1.0
ug/L
20.00
105
64-136
o-Xylene
22.8
0.50
ug/L
20.00
114
78-128
Propionitrile (Ethyl Cyanide)
22.1
10
ug/L
20.00
110
70-130
Styrene
23.3
0.50
ug/L
20.00
116
78-129
Tetrachloroethylene
21.2
0.50
ug/L
20.00
106
80-129
Tetrahydrofuran
22.3
10
ug/L
20.00
112
70-130
Toluene
22.5
0.50
ug/L
20.00
113
76-131
trans- 1,2-Dichloroethylene
21.6
0.50
ug/L
20.00
108
76-135
trans- 1,3-Dichloropropylene
23.1
0.50
ug/L
20.00
116
67-140
trans-1,4-Dichloro-2-butene
21.1
10
ug/L
20.00
105
70-130
Trichloroethylene
21.3
0.50
ug/L
20.00
107
77-133
Trichlorofluoromethane
22.6
0.50
ug/L
20.00
113
62-148
Vinyl acetate
26.3
2.0
ug/L
20.00
131
34-167
Vinyl chloride
22.4
0.50
ug/L
20.00
112
57-141
Xylenes, total
71.2
1.5
ug/L
60.00
119
77-133
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 32 of 84
Waypoint '
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS (POJ0321-BSI)
Prepared &Analyzed: 10/21/20
Surrogate:4-Bromofluorobenzene
48.4
ug/L
50.00
97
80-124
Surrogate: Dibromofluoromethane
49.3
ug/L
50.00
99
75-129
Surrogate: Toluene-d8
50.0
ug/L
50.00
100
77-123
LCS Dup (POJ0321-BSDI)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
21.4
0.50
ug/L
20.00
107
79-134
0.6
20
1,1,1-Trichloroethane
20.5
0.50
ug/L
20.00
102
75-136
4
20
1,1,2,2-Tetrachloroethane
20.7
0.50
ug/L
20.00
103
62-127
2
20
1,1,2-Trichloroethane
21.4
0.50
ug/L
20.00
107
70-140
1
20
1,1-Dichloroethane
20.4
0.50
ug/L
20.00
102
78-130
5
20
1,1-Dichloroethylene
20.2
0.50
ug/L
20.00
101
70-154
5
20
1, 1 -Dichloropropylene
21.0
0.50
ug/L
20.00
105
71-136
5
20
1,2,3-Trichloropropane
21.1
1.0
ug/L
20.00
106
71-127
0.6
20
1,2,4-Trichlorobenzene
20.7
1.0
ug/L
20.00
103
66-139
1
20
1,2-Dibromo-3-chloropropane
21.7
2.0
ug/L
20.00
108
63-134
5
20
1,2-Dibromoethane
20.9
0.50
ug/L
20.00
104
77-135
2
20
1,2-Dichlorobenzene
20.5
0.50
ug/L
20.00
103
78-128
4
20
1,2-Dichloroethane
21.1
0.50
ug/L
20.00
106
68-131
2
20
1,2-Dichloropropane
21.3
0.50
ug/L
20.00
107
77-130
3
20
1,3-Dichlorobenzene
21.1
0.50
ug/L
20.00
105
77-125
2
20
1,3-Dichloropropane
21.3
0.50
ug/L
20.00
106
76-132
3
20
1,4-Dichlorobenzene
20.4
0.50
ug/L
20.00
102
75-126
2
20
2,2-Dichloropropane
21.4
2.0
ug/L
20.00
107
29-149
11
20
Acetone
39.2
5.0
ug/L
40.00
98
40-166
1
20
Acetonitrile
21.5
10
ug/L
20.00
107
70-130
10
20
Acrolein
46.1
20
ug/L
40.00
115
70-130
0.5
20
Acrylonitrile
42.2
20
ug/L
40.00
105
81-127
0.4
20
Allyl Chloride (3-Chloropropylene)
18.8
10
ug/L
20.00
94
70-130
3
20
Benzene
21.8
0.50
ug/L
20.00
109
77-128
4
20
Bromochloromethane
20.5
0.50
ug/L
20.00
103
78-135
7
20
Bromodichloromethane
20.8
0.50
ug/L
20.00
104
76-138
4
20
Bromoform
21.5
1.0
ug/L
20.00
107
71-135
4
20
Bromomethane
19.7
1.0
ug/L
20.00
99
41-168
6
20
Carbon disulfide
20.5
5.0
ug/L
20.00
102
59-135
3
20
Carbon Tetrachloride
20.9
0.50
ug/L
20.00
105
72-142
4
20
Chlorobenzene
21.2
0.50
ug/L
20.00
106
78-119
4
20
Chloroethane
20.2
0.50
ug/L
20.00
101
57-142
6
20
Chloroform
20.6
0.50
ug/L
20.00
103
77-130
2
20
Chloromethane
20.0
0.50
ug/L
20.00
100
47-145
2
20
Chloroprene
18.8
10
ug/L
20.00
94
70-130
5
20
cis-1,2-Dichloroethylene
20.4
0.50
ug/L
20.00
102
76-141
10
20
cis-1,3-Dichloropropylene
21.9
0.50
ug/L
20.00
110
65-140
2
20
Dibromochloromethane
21.2
0.50
ug/L
20.00
106
75-134
0.1
20
Dibromomethane
21.3
0.50
ug/L
20.00
107
76-138
2
20
Dichlorodifluoromethane
24.2
5.0
ug/L
20.00
121
28-163
4
20
Ethyl Methacrylate
19.4
10
ug/L
20.00
97
70-130
1
20
Ethylbenzene
22.0
0.50
ug/L
20.00
110
80-127
3
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 84
• 0
Waypoint
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS Dup (POJ0321-BSD1)
Prepared &Analyzed: 10/21/20
Hexachlorobutadiene
19.9
2.0
ug/L
20.00
99
61-134
1
20
Isobutyl alcohol
21.3
50
ug/L
20.00
106
70-130
12
20 1
m,p-Xylenes
47.1
1.0
ug/L
40.00
118
77-133
3
20
Methacrylonitrile
19.2
10
ug/L
20.00
96
70-130
2
20
Methyl Butyl Ketone (2-Hexanone)
22.7
5.0
ug/L
20.00
113
64-137
0.3
20
Methyl Ethyl Ketone (2-Butanone)
19.7
5.0
ug/L
20.00
98
71-134
3
20
Methyl Iodide
22.6
5.0
ug/L
20.00
113
70-130
4
20
Methyl Isobutyl Ketone
22.7
5.0
ug/L
20.00
113
69-134
5
20
Methyl Methacrylate
19.7
10
ug/L
20.00
99
70-130
3
20
Methylene Chloride
19.8
1.0
ug/L
20.00
99
73-131
5
20
Naphthalene
21.4
1.0
ug/L
20.00
107
64-136
2
20
o-Xylene
22.3
0.50
ug/L
20.00
112
78-128
2
20
Propionitrile (Ethyl Cyanide)
19.9
10
ug/L
20.00
100
70-130
10
20
Styrene
22.7
0.50
ug/L
20.00
113
78-129
3
20
Tetrachloroethylene
20.4
0.50
ug/L
20.00
102
80-129
4
20
Tetrahydrofuran
22.0
10
ug/L
20.00
110
70-130
2
20
Toluene
21.6
0.50
ug/L
20.00
108
76-131
4
20
trans-1,2-Dichloroethylene
20.6
0.50
ug/L
20.00
103
76-135
5
20
trans-1,3-Dichloropropylene
22.2
0.50
ug/L
20.00
ill
67-140
4
20
trans-1,4-Dichloro-2-butene
19.6
10
ug/L
20.00
98
70-130
7
20
Trichloroethylene
21.2
0.50
ug/L
20.00
106
77-133
0.7
20
Trichlorofluoromethane
21.4
0.50
ug/L
20.00
107
62-148
6
20
Vinyl acetate
25.7
2.0
ug/L
20.00
129
34-167
2
20
Vinyl chloride
21.2
0.50
ug/L
20.00
106
57-141
5
20
Xylenes, total
69.4
1.5
ug/L
60.00
116
77-133
2
20
Surrogate:4-Bromofluorobenzene
48.3
ug/L
50.00
97
80-124
Surrogate: Dibromofluoromethane
49.5
ug/L
50.00
99
75-129
Surrogate: Toluene-d8
50.3
ug/L
50.00
101
77-123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Asheville, NC 28801
Volatile Organic Compounds by GC/MS SIM - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0316 - 5030B
Blank (POJ0316-BLK1) Prepared & Analyzed: 10/16/20
1,4-Dioxane BRL 2.0 ug/L
LCS (POJ0316-BS1) Prepared &Analyzed: 10/16/20
1,4-Dioxane 47.5 2.0 ug/L 50.00 95 55-145
LCS Dup (POJ0316-BSD1) Prepared &Analyzed: 10/16/20
1,4-Dioxane 47.1 2.0 ug/L 50.00 94 55-145 0.7 30
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 35 of 84
• 0
Waypoint
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0214 - 3510C GC
Blank (POJ0214-BLK1)
Prepared & Analyzed: 10/14/20
4,4'-DDD
BRL
0.10
ug/L
4,4'-DDE
BRL
0.10
ug/L
4,4'-DDT
BRL
0.10
ug/L
Aldrin
BRL
0.050
ug/L
alpha-BHC
BRL
0.050
ug/L
cis -Chlordane
BRL
0.10
ug/L
beta-BHC
BRL
0.050
ug/L
Chlordane
BRL
0.50
ug/L
delta-BHC
0.0100
0.050
ug/L
J
Dieldrin
BRL
0.050
ug/L
Endosulfan I
BRL
0.050
ug/L
Endosulfan II
BRL
0.050
ug/L
Endosulfan Sulfate
BRL
0.050
ug/L
Endrin
BRL
0.050
ug/L
Endrin Aldehyde
BRL
0.050
ug/L
Endrin Ketone
BRL
0.10
ug/L
gamma-BHC
BRL
0.050
ug/L
trans -Chlordane
BRL
0.10
ug/L
Heptachlor
BRL
0.050
ug/L
Heptachlor Epoxide
BRL
0.10
ug/L
Methoxychlor
BRL
0.10
ug/L
Toxaphene
BRL
1.0
ug/L
Surrogate: Decachlorobiphenyl
0.760
ug/L
1.000
76
13-186
Surrogate: Tetrachloro-m-xylene
0.530
ug/L
1.000
53
40-134
LCS (POJ0214-BS1)
Prepared &Analyzed:
10/14/20
4,4'-DDD
0.730
0.10
ug/L
1.000
73
56-143
4,4'-DDE
0.710
0.10
ug/L
1.000
71
57-135
4,4'-DDT
0.770
0.10
ug/L
1.000
77
51-143
Aldrin
0.630
0.050
ug/L
1.000
63
45-134
alpha-BHC
0.710
0.050
ug/L
1.000
71
54-138
cis -Chlordane
0.690
0.10
ug/L
1.000
69
60-129
beta-BHC
0.670
0.050
ug/L
1.000
67
56-136
delta-BHC
0.700
0.050
ug/L
1.000
70
52-142
Dieldrin
0.720
0.050
ug/L
1.000
72
60-136
Endosulfan 1
0.700
0.050
ug/L
1.000
70
62-126
Endosulfan II
0.730
0.050
ug/L
1.000
73
52-135
Endosulfan Sulfate
0.680
0.050
ug/L
1.000
68
62-133
Endrin
0.800
0.050
ug/L
1.000
80
60-138
Endrin Aldehyde
0.670
0.050
ug/L
1.000
67
51-132
Endrin Ketone
0.710
0.10
ug/L
1.000
71
58-134
gamma-BHC
0.690
0.050
ug/L
1.000
69
59-134
trans -Chlordane
0.650
0.10
ug/L
1.000
65
56-136
Heptachlor
0.670
0.050
ug/L
1.000
67
54-130
Heptachlor Epoxide
0.700
0.10
ug/L
1.000
70
61-133
Methoxychlor
0.760
0.10
ug/L
1.000
76
54-145
Surrogate: Decachlorobiphenyl
0.630
ug/L
1.000
63
13-186
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 of 84
• 0
Waypoint
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0214 - 3510C GC
LCS (POJ0214-BS1)
Prepared &Analyzed: 10/14/20
Surrogate: Tetrachloro-m-xylene
0.770
ug/L
1.000 77
40-134
LCS (POJ0214-BS2)
Prepared & Analyzed: 10/14/20
Chlordane
8.90
0.50 ug/L
10.00 89
62-140
Surrogate: Decachlorobiphenyl
0.690
ug/L
1.000 69
13-186
Surrogate: Tetrachloro-m-xylene
0.730
ug/L
1.000 73
40-134
LCS (POJ0214-BS3)
Prepared & Analyzed: 10/14/20
Toxaphene
7.66
1.0 ug/L
10.00 77
33-134
Surrogate: Decachlorobiphenyl
0.500
ug/L
1.000 50
13-186
Surrogate: Tetrachloro-m-xylene
0.610
ug/L
1.000 61
40-134
LCS Dup (POJ0214-BSD1)
Prepared &Analyzed: 10/14/20
4,4'-DDD
0.730
0.10
ug/L
1.000
73
56-143
0 30
4,4'-DDE
0.710
0.10
ug/L
1.000
71
57-135
0 30
4,4'-DDT
0.770
0.10
ug/L
1.000
77
51-143
0 30
Aldrin
0.630
0.050
ug/L
1.000
63
45-134
0 30
alpha-BHC
0.700
0.050
ug/L
1.000
70
54-138
1 30
cis -Chlordane
0.680
0.10
ug/L
1.000
68
60-129
1 30
beta-BHC
0.650
0.050
ug/L
1.000
65
56-136
3 30
delta-BHC
0.690
0.050
ug/L
1.000
69
52-142
1 30
Dieldrin
0.720
0.050
ug/L
1.000
72
60-136
0 30
Endosulfan 1
0.700
0.050
ug/L
1.000
70
62-126
0 30
Endosulfan 11
0.730
0.050
ug/L
1.000
73
52-135
0 30
Endosulfan Sulfate
0.680
0.050
ug/L
1.000
68
62-133
0 30
Endrin
0.800
0.050
ug/L
1.000
80
60-138
0 30
Endrin Aldehyde
0.670
0.050
ug/L
1.000
67
51-132
0 30
Endrin Ketone
0.720
0.10
ug/L
1.000
72
58-134
1 30
gamma-BHC
0.690
0.050
ug/L
1.000
69
59-134
0 30
trans -Chlordane
0.650
0.10
ug/L
1.000
65
56-136
0 30
Heptachlor
0.670
0.050
ug/L
1.000
67
54-130
0 30
Heptachlor Epoxide
0.690
0.10
ug/L
1.000
69
61-133
1 30
Methoxychlor
0.760
0.10
ug/L
1.000
76
54-145
0 30
Surrogate: Decachlorobiphenyl
0.650
ug/L
1.000
65
13-186
Surrogate: Tetrachloro-m-xylene
0.730
ug/L
1.000
73
40-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 of 84
• 0
Waypoint
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0214 - 3510C GC
Matrix Spike (POJ0214-MS1)
Source: 0100161-01
Prepared & Analyzed: 10/14/20
4,4'-DDD
BRL
0.20
ug/L
BRL
56-143
4,4'-DDE
BRL
0.20
ug/L
BRL
57-135
4,4'-DDT
BRL
0.20
ug/L
BRL
51-143
Aldrin
BRL
0.10
ug/L
BRL
45-134
alpha-BHC
BRL
0.10
ug/L
BRL
54-138
cis -Chlordane
BRL
0.20
ug/L
BRL
60-129
beta-BHC
BRL
0.10
ug/L
BRL
56-136
Chlordane
BRL
1.0
ug/L
BRL
62-140
delta-BHC
BRL
0.10
ug/L
BRL
52-142
Dieldrin
BRL
0.10
ug/L
BRL
60-136
Endosulfan I
BRL
0.10
ug/L
BRL
62-126
Endosulfan II
BRL
0.10
ug/L
BRL
52-135
Endosulfan Sulfate
BRL
0.10
ug/L
BRL
62-133
Endrin
BRL
0.10
ug/L
BRL
60-138
Endrin Aldehyde
BRL
0.10
ug/L
BRL
51-132
Endrin Ketone
BRL
0.20
ug/L
BRL
58-134
gamma-BHC
BRL
0.10
ug/L
BRL
59-134
trans -Chlordane
BRL
0.20
ug/L
BRL
56-136
Heptachlor
BRL
0.10
ug/L
BRL
54-130
Heptachlor Epoxide
BRL
0.20
ug/L
BRL
61-133
Methoxychlor
BRL
0.20
ug/L
BRL
54-145
Toxaphene
BRL
2.0
ug/L
BRL
33-134
Surrogate: Decachlorobiphenyl
1.52
ug/L
2.000 76
13-186
Surrogate: Tetrachloro-m-xylene
1.32
ug/L
2.000 66
40-134
Matrix Spike Dup (POJ0214-MSD1)
Source: 0100161-01
Prepared & Analyzed: 10/14/20
4,4'-DDD
BRL
0.24
ug/L
BRL
56-143
30
4,4'-DDE
BRL
0.24
ug/L
BRL
57-135
30
4,4'-DDT
BRL
0.24
ug/L
BRL
51-143
30
Aldrin
BRL
0.12
ug/L
BRL
45-134
30
alpha-BHC
BRL
0.12
ug/L
BRL
54-138
30
cis -Chlordane
BRL
0.24
ug/L
BRL
60-129
30
beta-BHC
BRL
0.12
ug/L
BRL
56-136
30
Chlordane
BRL
1.2
ug/L
BRL
62-140
30
delta-BHC
BRL
0.12
ug/L
BRL
52-142
30
Dieldrin
BRL
0.12
ug/L
BRL
60-136
30
Endosulfan I
BRL
0.12
ug/L
BRL
62-126
30
Endosulfan II
BRL
0.12
ug/L
BRL
52-135
30
Endosulfan Sulfate
BRL
0.12
ug/L
BRL
62-133
30
Endrin
BRL
0.12
ug/L
BRL
60-138
30
Endrin Aldehyde
BRL
0.12
ug/L
BRL
51-132
30
Endrin Ketone
BRL
0.24
ug/L
BRL
58-134
30
gamma-BHC
BRL
0.12
ug/L
BRL
59-134
30
trans -Chlordane
BRL
0.24
ug/L
BRL
56-136
30
Heptachlor
BRL
0.12
ug/L
BRL
54-130
30
Heptachlor Epoxide
BRL
0.24
ug/L
BRL
61-133
30
Methoxychlor
BRL
0.24
ug/L
BRL
54-145
30
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0214 - 3510C GC
Matrix Spike Dup (POJ0214-MSD1) Source: 0100161-01 Prepared & Analyzed: 10/14/20
Toxaphene BRL 2.4 ug/L BRL 33-134 30
Surrogate: Decachlorobiphenyl 1.69 ug/L 2.381 71 13-186
Surrogate: Tetrachloro-m-xylene 1.55 ug/L 2.381 65 40-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 39 of 84
• 0
Waypoint
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0214 - 3510C GC
Blank (POJ0214-BLK1)
Prepared & Analyzed: 10/14/20
Aroclor 1016
BRL
0.50
ug/L
Aroclor 1221
BRL
1.0
ug/L
Aroclor 1232
BRL
0.50
ug/L
Aroclor 1242
BRL
0.50
ug/L
Aroclor 1248
BRL
0.50
ug/L
Aroclor 1254
BRL
0.50
ug/L
Aroclor 1260
BRL
1.0
ug/L
Surrogate: Tetrachloro-m-xylene
0.510
ug/L
1.000
51
30-161
Surrogate: Decachlorobiphenyl
0.790
ug/L
1.000
79
32-178
LCS (POJ0214-BS4)
Prepared & Analyzed: 10/14/20
Aroclor 1016
6.83
0.50
ug/L
10.00
68
50-114
Aroclor 1221
BRL
1.0
ug/L
15-178
Aroclor 1232
BRL
0.50
ug/L
10-215
Aroclor 1242
BRL
0.50
ug/L
39-150
Aroclor 1248
BRL
0.50
ug/L
38-158
Aroclor 1254
BRL
0.50
ug/L
29-131
Aroclor 1260
7.90
1.0
ug/L
10.00
79
10-127
Surrogate: Tetrachloro-m-xylene
0.510
ug/L
1.000
51
30-161
Surrogate: Decachlorobiphenyl
0.800
ug/L
1.000
80
32-178
Matrix Spike (POJ0214-MS1)
Source: 0100161-01
Prepared & Analyzed: 10/14/20
Aroclor 1016
12.7
1.0
ug/L
20.00 BRL
63
50-114
Aroclor 1221
BRL
2.0
ug/L
BRL
15-178
Aroclor 1232
BRL
1.0
ug/L
BRL
10-215
Aroclor 1242
BRL
1.0
ug/L
BRL
39-150
Aroclor 1248
BRL
1.0
ug/L
BRL
38-158
Aroclor 1254
BRL
1.0
ug/L
BRL
29-131
Aroclor 1260
14.3
2.0
ug/L
20.00 BRL
72
10-127
Surrogate: Tetrachloro-m-xylene
1.32
ug/L
2.000
66
30-161
Surrogate: Decachlorobiphenyl
1.52
ug/L
2.000
76
32-178
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Asheville, NC 28801
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0214 - 3510C GC
Matrix Spike Dup (POJ0214-MSD1)
Source: 0100161-01
Prepared & Analyzed: 10/14/20
Aroclor 1016
16.0
1.2
ug/L
23.81
BRL
67
50-114 23
50
Aroclor 1221
BRL
2.4
ug/L
BRL
15-178
50
Aroclor 1232
BRL
1.2
ug/L
BRL
10-215
50
Aroclor 1242
BRL
1.2
ug/L
BRL
39-150
50
Aroclor 1248
BRL
1.2
ug/L
BRL
38-158
50
Aroclor 1254
BRL
1.2
ug/L
BRL
29-131
50
Aroclor 1260
17.7
2.4
ug/L
23.81
BRL
74
10-127 21
50
Surrogate: Tetrachloro-m-xylene
1.55
ug/L
2.381
65
30-161
Surrogate: Decachlorobiphenyl
1.69
ug/L
2.381
71
32-178
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 41 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0239 - 3005A
Blank (POJ0239-BLK1)
Prepared: 10/15/20 Analyzed: 10/23/20
Antimony
BRL
2.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
2.0
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
2.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
BRL
3.0
ug/L
Selenium
BRL
5.0
ug/L
Thallium
BRL
2.0
ug/L
Tin
BRL
5.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
LCS (POJ0239-BS1)
Prepared: 10/15/20 Analyzed: 10/23/20
Antimony
103
2.0
ug/L
100.0
103
80-120
Arsenic
96.8
1.0
ug/L
100.0
97
80-120
Barium
99.1
2.0
ug/L
100.0
99
80-120
Beryllium
93.3
1.0
ug/L
100.0
93
80-120
Cadmium
98.1
1.0
ug/L
100.0
98
80-120
Chromium
96.2
2.0
ug/L
100.0
96
80-120
Cobalt
100
2.0
ug/L
100.0
100
80-120
Copper
97.5
10
ug/L
100.0
97
80-120
Lead
98.4
1.0
ug/L
100.0
98
80-120
Nickel
98.4
3.0
ug/L
100.0
98
80-120
Selenium
93.8
5.0
ug/L
100.0
94
80-120
Thallium
96.8
2.0
ug/L
100.0
97
80-120
Tin
102
5.0
ug/L
100.0
102
80-120
Vanadium
96.5
5.0
ug/L
100.0
97
80-120
Zinc
94.1
20
ug/L
100.0
94
80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 42 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Batch POJ0239 - 3005A
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike (POJ0239-MS1)
Source: 0100161-01
Prepared: 10/15/20 Analyzed: 10/23/20
Antimony
107
2.0
ug/L
100.0
BRL
107
75-125
Arsenic
96.7
1.0
ug/L
100.0
BRL
97
75-125
Barium
174
2.0
ug/L
100.0
80.6
93
75-125
Beryllium
97.7
1.0
ug/L
100.0
BRL
98
75-125
Cadmium
99.1
1.0
ug/L
100.0
0.236
99
75-125
Chromium
96.7
2.0
ug/L
100.0
BRL
97
75-125
Cobalt
98.1
2.0
ug/L
100.0
1.68
96
75-125
Copper
96.2
10
ug/L
100.0
BRL
96
75-125
Lead
100
1.0
ug/L
100.0
BRL
100
75-125
Nickel
95.4
3.0
ug/L
100.0
1.00
94
75-125
Selenium
96.0
5.0
ug/L
100.0
2.30
94
75-125
Thallium
98.5
2.0
ug/L
100.0
BRL
99
75-125
Tin
104
5.0
ug/L
100.0
BRL
104
75-125
Vanadium
98.5
5.0
ug/L
100.0
BRL
98
75-125
Zinc
94.8
20
ug/L
100.0
BRL
95
75-125
Matrix Spike Dup (POJ0239-MSD1)
Source: 0100161-01
Prepared:
10/15/20 Analyzed: 10/23/20
Antimony
109
2.0
ug/L
100.0
BRL
109
75-125
1
20
Arsenic
96.5
1.0
ug/L
100.0
BRL
97
75-125
0.2
20
Barium
178
2.0
ug/L
100.0
80.6
97
75-125
2
20
Beryllium
103
1.0
ug/L
100.0
BRL
103
75-125
5
20
Cadmium
101
1.0
ug/L
100.0
0.236
101
75-125
2
20
Chromium
97.6
2.0
ug/L
100.0
BRL
98
75-125
0.9
20
Cobalt
98.3
2.0
ug/L
100.0
1.68
97
75-125
0.2
20
Copper
97.2
10
ug/L
100.0
BRL
97
75-125
1
20
Lead
101
1.0
ug/L
100.0
BRL
101
75-125
0.7
20
Nickel
96.9
3.0
ug/L
100.0
1.00
96
75-125
2
20
Selenium
92.8
5.0
ug/L
100.0
2.30
90
75-125
3
20
Thallium
99.1
2.0
ug/L
100.0
BRL
99
75-125
0.6
20
Tin
106
5.0
ug/L
100.0
BRL
106
75-125
3
20
Vanadium
99.7
5.0
ug/L
100.0
BRL
100
75-125
1
20
Zinc
95.6
20
ug/L
100.0
BRL
96
75-125
0.8
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 43 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0239 - 3005A
Post Spike (POJ0239-PS1)
Source: 0100161-01
Prepared:
10/15/20 Analyzed: 10/23/20
Antimony
102
ug/L
100.0
0.0480
102
80-120
Arsenic
96.7
ug/L
100.0
0.0980
97
80-120
Barium
173
ug/L
100.0
80.6
92
80-120
Beryllium
92.0
ug/L
100.0
0.0340
92
80-120
Cadmium
101
ug/L
100.0
0.236
101
80-120
Chromium
98.5
ug/L
100.0
0.0970
98
80-120
Cobalt
99.0
ug/L
100.0
1.68
97
80-120
Copper
97.7
ug/L
100.0
0.532
97
80-120
Lead
101
ug/L
100.0
0.0310
101
80-120
Nickel
96.7
ug/L
100.0
1.00
96
80-120
Selenium
96.8
ug/L
100.0
2.30
95
80-120
Thallium
99.3
ug/L
100.0
0.139
99
80-120
Tin
104
ug/L
100.0
0.0990
104
80-120
Vanadium
100
ug/L
100.0
-0.444
100
80-120
Zinc
97.4
ug/L
100.0
3.87
93
80-120
Batch POJ0374 - 7470A
Blank (POJ0374-BLK1) Prepared & Analyzed: 10/20/20
Mercury BRL 0.20 ug/L
LCS (POJ0374-BS1) Prepared &Analyzed: 10/20/20
Mercury 8.17 0.20 ug/L 9.375 87 80-120
Matrix Spike (POJ0374-MS1) Source: 0100161-02 Prepared & Analyzed: 10/20/20
Mercury 5.75 0.20 ug/L 9.375 0.727 54 80-120 MI
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 44 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Analyte
Reporting
Result Limit Units
Spike Source
Level Result %REC
%REC RPD
Limits RPD Limit Notes
Batch POJ0374 - 7470A
Matrix Spike Dup (POJ0374-MSD1)
Source: 0100161-02
Prepared & Analyzed: 10/20/20
Mercury
Post Spike (POJ0374-PS1)
5.67 0.20 ug/L
Source: 0100161-02
9.375 0.727 53
Prepared & Analyzed: 10/20/20
80-120 1 20 MI
Mercury
Batch POJ0490 - 3005A
3.41 ug/L
5.000 0.679 55
85-115 MI
Blank (POJ0490-BLK1)
Prepared & Analyzed: 10/27/20
Silver
BRL 1.0 ug/L
LCS (POJ0490-BS1)
Prepared &Analyzed: 10/27/20
Silver
97.6 1.0 ug/L
100.0 98
80-120
Matrix Spike (POJ0490-MS1)
Source: 0100161-03
Prepared & Analyzed: 10/27/20
Silver
99.2 1.0 ug/L
100.0 BRL 99
75-125
Matrix Spike Dup (POJ0490-MSD1)
Source: 0100161-03
Prepared & Analyzed: 10/27/20
Silver
99.5 1.0 ug/L
100.0 BRL 99
75-125 0.2 20
Post Spike (POJ0490-PS1)
Source: 0100161-03
Prepared: 10/27/20 Analyzed: 10/28/20
Silver
99.3 ug/L
100.0 0.00300 99
80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 45 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Dissolved Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0218 - 3005A
Blank (POJ0218-BLK1)
Prepared: 10/14/20 Analyzed: 10/23/20
Antimony
BRL
2.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
10
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
2.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
BRL
3.0
ug/L
Selenium
BRL
5.0
ug/L
Silver
BRL
1.0
ug/L
Thallium
BRL
2.0
ug/L
Tin
BRL
5.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
LCS (POJ0218-BS1)
Prepared: 10/14/20 Analyzed: 10/23/20
Antimony
94.6
2.0
ug/L
100.0 95 80-120
Arsenic
91.5
1.0
ug/L
100.0 92 80-120
Barium
91.9
10
ug/L
100.0 92 80-120
Beryllium
89.1
1.0
ug/L
100.0 89 80-120
Cadmium
97.3
1.0
ug/L
100.0 97 80-120
Chromium
93.6
2.0
ug/L
100.0 94 80-120
Cobalt
92.7
2.0
ug/L
100.0 93 80-120
Copper
91.1
10
ug/L
100.0 91 80-120
Lead
95.8
1.0
ug/L
100.0 96 80-120
Nickel
92.1
3.0
ug/L
100.0 92 80-120
Selenium
96.5
5.0
ug/L
100.0 96 80-120
Silver
45.6
1.0
ug/L
100.0 46 80-120 L
Thallium
95.0
2.0
ug/L
100.0 95 80-120
Tin
97.9
5.0
ug/L
100.0 98 80-120
Vanadium
92.4
5.0
ug/L
100.0 92 80-120
Zinc
89.2
20
ug/L
100.0 89 80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 46 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Dissolved Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0259 - 7470A
Blank (POJ0259-BLK1) Prepared & Analyzed: 10/15/20
Mercury BRL 0.20 ug/L
LCS (POJ0259-BS1) Prepared &Analyzed: 10/15/20
Mercury 9.44 0.20 ug/L 9.375 101 80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 47 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Anions by Ion Chromatography - Quality Control
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0221 - NO PREP
Blank (POJ0221-BLK1)
Prepared & Analyzed: 10/13/20
Chloride
BRL
1000
ug/L
Nitrate as N
BRL
200
ug/L
Sulfate
BRL
2000
ug/L
LCS (POJ0221-BS1)
Prepared &Analyzed: 10/13/20
Chloride
40900
1000
ug/L
40000 102
80-120
Nitrate as N
3970
210
ug/L
4000 99
80-120
Sulfate
41100
2100
ug/L
40000 103
80-120
Matrix Spike (POJ0221-MS1)
Source: 0100161-03
Prepared & Analyzed: 10/13/20
Chloride
119000
1000
ug/L
40000 78800 102
80-120
Nitrate as N
3950
210
ug/L
4000 92.4 97
80-120
Sulfate
65700
2100
ug/L
40000 25200 101
80-120
Matrix Spike Dup (POJ0221-MSD1)
Source: 0100161-03
Prepared & Analyzed: 10/13/20
Chloride
119000
1000
ug/L
40000 78800 101
80-120 0.3 15
Nitrate as N
3930
210
ug/L
4000 92.4 96
80-120 0.5 15
Sulfate
65700
2100
ug/L
40000 25200 101
80-120 0.008 15
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 48 of 84
Level II QC Report
0int 11/30/20
Waypo
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0199 - NO PREP
Blank (POJ0199-BLK1) Prepared & Analyzed: 10/13/20
Ferrous Iron BRL 200 ug/L
LCS (POJ0199-BS1) Prepared &Analyzed: 10/13/20
Ferrous Iron 1840 200 ug/L 2000 92 90-110
Matrix Spike (POJ0199-MS1) Source: 0100161-03 Prepared & Analyzed: 10/13/20
Ferrous Iron 2220 200 ug/L 2000 355 93 80-120 HT
Matrix Spike Dup (POJ0199-MSD1) Source: 0100161-03 Prepared & Analyzed: 10/13/20
Ferrous Iron 2180 200 ug/L 2000 355 91 80-120 2 20 HT
Batch POJ0276 - NO PREP
Blank (POJ0276-BLK1) Prepared & Analyzed: 10/14/20
Biochemical Oxygen Demand BRL 2000 ug/L
LCS (POJ0276-BS1) Prepared &Analyzed: 10/14/20
Biochemical Oxygen Demand 189000 2000 ug/L 198000 95 84.6-115.4
Batch POJ0304 - NO PREP
Blank (POJ0304-BLK1) Prepared & Analyzed: 10/16/20
Chemical Oxygen Demand BRL 50000 ug/L
LCS (POJ0304-BS1) Prepared &Analyzed: 10/16/20
Chemical Oxygen Demand 501000 50000 ug/L 500000 100 90-110
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 49 of 84
• 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Batch POJ0304 - NO PREP
Level II QC Report
11 /30/20
Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Project No: 50-02
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike (POJ0304-MS1) Source: 0100161-02 Prepared & Analyzed: 10/16/20
Chemical Oxygen Demand 532000 50000 ug/L 500000 42300 98 80-120
Matrix Spike Dup (POJ0304-MSD1) Source: 0100161-02 Prepared & Analyzed: 10/16/20
Chemical Oxygen Demand 521000 50000 ug/L 500000 42300 96 80-120 2 20
Batch POJ0337 - SM4500-S C
Blank (POJ0337-BLK1) Prepared & Analyzed: 10/19/20
Sulfide BRL 2000 ug/L
LCS (POJ0337-BS1) Prepared &Analyzed: 10/19/20
Sulfide 7900 2000 ug/L 10000 79 70-122
Matrix Spike (POJ0337-MS1) Source: 0100161-01 Prepared & Analyzed: 10/19/20
Sulfide 8300 2000 ug/L 10000 BRL 83 70-130
Matrix Spike Dup (POJ0337-MSD1) Source: 0100161-01 Prepared & Analyzed: 10/19/20
Sulfide 8600 2000 ug/L 10000 BRL 86 70-130 4 20
Batch POJ0341 - NO PREP
Blank (POJ0341-BLK1) Prepared & Analyzed: 10/19/20
Total Alkalinity to pH 4.5 BRL 5000 ug/L
LCS (POJ0341-BS1) Prepared &Analyzed: 10/19/20
Total Alkalinity to pH 4.5 249000 5000 ug/L 90-110
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 50 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0357 - 9010C
Blank (POJ0357-BLK1) Prepared & Analyzed: 10/20/20
Cyanide BRL 25 ug/L
LCS (POJ0357-BS1) Prepared &Analyzed: 10/20/20
Cyanide 96.5 25 ug/L 100.0 96 85-115
Batch POJ0361 - NO PREP
Blank (POJ0361-BLK1) Prepared & Analyzed: 10/19/20
Chemical Oxygen Demand BRL 50000 ug/L
LCS (POJ0361-BSI) Prepared &Analyzed: 10/19/20
Chemical Oxygen Demand 498000 50000 ug/L 90-110
Matrix Spike (POJ0361-MS1) Source: 0100161-03 Prepared & Analyzed: 10/19/20
Chemical Oxygen Demand 475000 50000 ug/L 18000 80-120
Matrix Spike Dup (POJ0361-MSD1) Source: 0100161-03 Prepared & Analyzed: 10/19/20
Chemical Oxygen Demand 487000 50000 ug/L 18000 80-120 2 20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 51 of 84
• 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
8270 Extended List - Quality Control
Analyte
Batch L517325 - 3510C
Level II QC Report
11 /30/20
Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Project No: 50-02
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
BSD (0100161 LCSD-L517325)
Source: 0100161 LCS-L517Prepared: 10/19/20 Analyzed: 10/21/20
5-Nitro-o-toluidine
48.6
10.0
pg/L
50
45.1
97.2
20-120
7.4
20
Kepone
60
10.0
pg/L
50
53.4
120
20-120
11.6
20
Isosafrole
43.9
10.0
pg/L
50
41.9
87.8
20-120
4.6
20
Hexachloropropene
22.6
10.0
pg/L
50
18.9
45.2
20-120
17.8
20
Methapyrilene
49.8
10.0
pg/L
50
35.1
99.6
20-120
34.6
20
LCD2
7,12-Dimethylbenz(a)anthracene
58.1
10.0
pg/L
50
48.7
116
20-120
17.6
20
p-Dimethylaminoazobenzene
61.3
10.0
pg/L
50
51.1
123
20-120
18.1
20
L2
Diallate
48.4
10.0
pg/L
50
48.3
96.8
20-120
0.2
20
N-Nitrosomethylethylamine
27.4
10.0
pg/L
50
26.2
54.8
20-120
4.4
20
N-Nitrosopiperidine
34.1
10.0
pg/L
50
33.6
68.2
20-120
1.4
20
o-Toluidine
29.9
10.0
pg/L
50
29.4
59.8
20-120
1.6
20
p-Phenylenediamine
0
10.0
pg/L
50
0
0
20-120
0
20
L
Safrole
39.9
10.0
pg/L
50
39.7
79.8
20-120
0.5
20
Pronamide
56.1
10.0
pg/L
50
51
112
20-120
9.5
20
4-Aminobiphenyl
38.8
10.0
pg/L
50
37
77.6
20-120
4.7
20
N-Nitrosopyrrolidine
34.3
10.0
pg/L
50
34.4
68.6
20-120
0.2
20
3-Methylcholanthrene
57.1
10.0
pg/L
50
53
114
20-120
7.4
20
2-Acetylaminofluorene
49.1
10.0
pg/L
50
53.1
98.2
20-120
7.8
20
2-Naphthylamine
20.3
10.0
pg/L
50
22.7
40.6
20-120
11.1
20
1-Naphthylamine
28.8
10.0
pg/L
50
28.9
57.6
20-120
0.3
20
1,3,5-Trinitrobenzene
65.8
10.0
pg/L
50
60.4
132
20-120
8.5
20
LH
1,4-Naphthoquinone
44.6
10.0
pg/L
50
41.7
89.2
20-120
6.7
20
BS (0100161 LCS-L517325)
Prepared:
10/19/20
Analyzed:
10/21/20
N-Nitrosomethylethylamine
26.2
10.0
pg/L
50
52.4
20-120
o-Toluidine
29.4
10.0
pg/L
50
58.8
20-120
Isosafrole
41.9
10.0
pg/L
50
83.8
20-120
Kepone
53.4
10.0
pg/L
50
107
20-120
p-Dimethylaminoazobenzene
51.1
10.0
pg/L
50
102
20-120
Methapyrilene
35.1
10.0
pg/L
50
70.2
20-120
p-Phenylenediamine
0
10.0
pg/L
50
0
20-120
L
1-Naphthylamine
28.9
10.0
pg/L
50
57.8
20-120
N-Nitrosopiperidine
33.6
10.0
pg/L
50
67.2
20-120
N-Nitrosopyrrolidine
34.4
10.0
pg/L
50
68.8
20-120
1,4-Naphthoquinone
41.7
10.0
pg/L
50
83.4
20-120
2-Naphthylamine
22.7
10.0
pg/L
50
45.4
20-120
4-Aminobiphenyl
37
10.0
pg/L
50
74
20-120
3-Methylcholanthrene
53
10.0
pg/L
50
106
20-120
Safrole
39.7
10.0
pg/L
50
79.4
20-120
5-Nitro-o-toluidine
45.1
10.0
pg/L
50
90.2
20-120
7,12-Dimethylbenz(a)anthracene
48.7
10.0
pg/L
50
97.4
20-120
2-Acetylaminofluorene
53.1
10.0
pg/L
50
106
20-120
Pronamide
51
10.0
pg/L
50
102
20-120
Diallate
48.3
10.0
pg/L
50
96.6
20-120
1,3,5-Trinitrobenzene
60.4
10.0
pg/L
50
121
20-120
LH
Hexachloropropene
18.9
10.0
pg/L
50
37.8
20-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 52 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
8270 Extended List - Quality Control
Analyte
Batch L517325 - 3510C
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
BILK (0100161 LRB-L517325)
Prepared: 10/19/20 Analyzed: 10/20/20
p-Phenylenediamine
BRL
10.0
pg/L -
1,3,5-Trinitrobenzene
BRL
10.0
pg/L
o-Toluidine
BRL
10.0
pg/L
Pronamide
BRL
10.0
pg/L
Safrole
BRL
10.0
pg/L
p-Dimethylaminoazobenzene
BRL
10.0
pg/L
2-Acetylaminofluorene
BRL
10.0
pg/L
N-Nitrosopyrrolidine
BRL
10.0
pg/L
1,4-Naphthoquinone
BRL
10.0
pg/L
4-Aminobiphenyl
BRL
10.0
pg/L
5-Nitro-o-toluidine
BRL
10.0
pg/L
7,12-Dimethylbenz(a)anthracene
BRL
10.0
pg/L
Diallate
BRL
10.0
pg/L
3-Methylcholanthrene
BRL
10.0
pg/L
Hexachloropropene
BRL
10.0
pg/L
Isosafrole
BRL
10.0
pg/L
Kepone
BRL
10.0
pg/L
1-Naphthylamine
BRL
10.0
pg/L
Methapyrilene
BRL
20.0
pg/L
N-Nitrosomethylethylamine
BRL
10.0
pg/L
N-Nitrosopiperidine
BRL
10.0
pg/L
2-Naphthylamine
BRL
10.0
pg/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 53 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Phenoxy Acid Herbicides - GC/ECD - Quality Control
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517362 - 8151A
BSD (0100161 LCSD-L517362)
Source: 0100161 LCS-L517Prepared: 10/19/20 Analyzed: 10/20/20
MCPA
250.8
18.98
pg/L
500
200.4
50.1
20-120
22.3
20
LCD2
Dichlorprop
2.547
0.07959
pg/L
5
2.019
50.9
20-120
23.1
20
LCD2
Dalapon
3.626
0.5149
pg/L
12.5
4.011
29
20-120
10
20
Dicamba
0.255
0.05700
pg/L
0.5
0.2384
51
20-120
6.7
20
Dinoseb
1.507
0.02698
pg/L
2.5
1.16
60.2
20-120
26
20
LCD2
2,4-DB
2.624
0.1364
pg/L
5
2.123
52.4
20-120
21.1
20
LCD2
2,4-D
2.493
0.2078
pg/L
5
1.997
49.8
20-120
22
20
LCD2
MCPP
301.9
11.75
pg/L
500
258.1
60.3
20-120
15.6
20
Picloram
0.6016
0.04528
pg/L
1.25
0.4532
48.1
20-120
28.1
20
LCD2
2,4,5-TP (Silvex)
0.2371
0.01634
pg/L
0.5
0.187
47.4
20-120
23.6
20
LCD2
2,4,5-T
0.2697
0.01002
pg/L
0.5
0.2279
53.9
20-120
16.8
20
Surrogate: DCAA
1.393
ug/L
2.5
1.156
55.7
20-150
BS (0100161 LCS-L517362)
Prepared:
10/19/20 Analyzed:
10/20/20
MCPP
258.1
11.75
pg/L
500
51.6
20-120
MCPA
200.4
18.98
pg/L
500
40
20-120
Dinoseb
1.16
0.02698
pg/L
2.5
46.4
20-120
Dichlorprop
2.019
0.07959
pg/L
5
40.3
20-120
Dicamba
0.2384
0.05700
pg/L
0.5
47.6
20-120
Picloram
0.4532
0.04528
pg/L
1.25
36.2
20-120
2,4,5-TP (Silvex)
0.187
0.01634
pg/L
0.5
37.4
20-120
2,4,5-T
0.2279
0.01002
pg/L
0.5
45.5
20-120
Dalapon
4.011
0.5149
pg/L
12.5
32
20-120
2,4-D
1.997
0.2078
pg/L
5
39.9
20-120
2,4-DB
2.123
0.1364
pg/L
5
42.4
20-120
Surrogate: DCAA
1.156
ug/L
2.5
46.2
20-150
BLK (0100161 LRB-L517362)
Prepared:
10/19/20 Analyzed:
10/20/20
Dicamba
BRL
0.1000
pg/L
-
2,4,5-T
BRL
0.03000
pg/L
2,4,5-TP (Silvex)
BRL
0.1000
pg/L
MCPP
BRL
50.00
pg/L
2,4-D
BRL
0.2500
pg/L
2,4-DB
BRL
0.1000
pg/L
Dinoseb
BRL
0.1000
pg/L
Dalapon
BRL
0.5500
pg/L
Dichlorprop
BRL
0.1000
pg/L
MCPA
BRL
50.00
pg/L
Picloram
BRL
0.1000
pg/L
-
Surrogate: DCAA
1.286
ug/L
2.5
51.4
20-150
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 54 of 84
• 0
Waypoint
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517230 - 3510C
BSD (0100161 LCSD-L517230)
Source: 0100161
LCS-L517Prepared
& Analyzed:
10/19/20
4,6-Dinitro-2-methylphenol
35.7
3.47
pg/L
50
47.1
71.4
27-128
27.5
20
LCD2
Dimethyl phthalate
36.4
0.510
pg/L
50
33
72.8
34-123
9.7
20
3,3' Dimethylbenzidine
76.3
1.88
pg/L
200
55.8
38.1
6-192
31
20
LCD2
Diethyl phthalate
36.5
0.585
pg/L
50
33.6
73
36-130
8.2
20
3,3'-Dichlorobenzidine
112
3.74
pg/L
150
95.9
74.6
6-192
15.4
20
Chrysene
36
0.731
pg/L
50
32.3
72
30-124
10.8
20
3-Nitroaniline
36.9
1.53
pg/L
50
32.3
73.8
28-142
13.2
20
Dibenz(a,h)anthrace ne
34.2
0.252
pg/L
50
29.9
68.4
27-124
13.4
20
3&4 Methylphenol
26.8
0.691
pg/L
50
23.7
53.6
21-96
12.2
20
Dibenzofuran
36.3
0.423
pg/L
50
33.2
72.6
40-108
8.9
20
Di-n-butyl phthalate
37
1.58
pg/L
50
34.5
74
19-158
6.9
20
2-Nitrophenol
32.4
0.606
pg/L
50
28.6
64.8
25-114
12.4
20
Di-n-Octyl Phthalate
44.9
1.72
pg/L
50
36.4
89.8
29-136
20.9
20
LCD2
2-Nitroaniline
38.4
0.574
pg/L
50
35
76.8
32-127
9.2
20
Fluoranthene
39
0.406
pg/L
50
36
78
28-127
8
20
2-Methylphenol
25
0.721
pg/L
50
22
50
22-97
12.7
20
Fluorene
34.1
0.444
pg/L
50
31.4
68.2
41-116
8.2
20
4-Bromophenyl phenyl ether
36.7
0.500
pg/L
50
33.4
73.4
31-124
9.4
20
Hexachlorobenzene
36.2
2.57
pg/L
50
33.6
72.4
18-136
7.4
20
Bis(2-Chloroisopropyl)ether
22.2
0.546
pg/L
50
19.4
44.4
28-108
13.4
20
Hexachlorobutadiene
25.5
0.405
pg/L
50
22.5
51
22-109
12.5
20
Hexachlorocyclopentadiene
12.1
2.34
pg/L
50
13.9
24.2
10-102
13.8
20
2-Methyl naphthalene
32.1
0.485
pg/L
50
29.7
64.2
34-108
7.7
20
Hexachloroethane
21.7
0.277
pg/L
50
19
43.4
16-107
13.2
20
Anthracene
36.1
0.467
pg/L
50
33.8
72.2
34-128
6.5
20
Benzo(b)fluoranthene
41.4
0.941
pg/L
50
38.4
82.8
36-131
7.5
20
Aniline
22.1
0.316
pg/L
50
18.1
44.2
16-133
19.9
20
Benzo(g,h,i)perylene
33.7
1.36
pg/L
50
30.6
67.4
26-123
9.6
20
Acetophenone
31.3
0.686
pg/L
50
27.2
62.6
25-108
14
20
Benzo(k)fluoranthene
43.7
0.752
pg/L
50
34.5
87.4
32-132
23.5
20
LCD2
Acenaphthylene
32.8
0.429
pg/L
50
29.7
65.6
37-114
9.9
20
Benzoic Acid
18.9
5.00
pg/L
150
30.6
12.6
11-68
47.2
20
LCD2
Acenaphthene
31.1
0.422
pg/L
50
27.4
62.2
38-117
12.6
20
Bis(2-ethylhexyl)phthalate
37.9
3.66
pg/L
50
37.4
75.8
21-162
1.3
20
Bis(2-Chloroethoxy)methane
30.7
0.433
pg/L
50
27.3
61.4
20-126
11.7
20
Benzo(a)pyrene
35.5
1.00
pg/L
50
30.9
71
34-131
13.8
20
4-Nitrophenol
11.3
1.39
pg/L
50
10.6
22.6
1-76
6.3
20
Bis(2-Chloroethyl)ether
28.8
0.447
pg/L
50
25.1
57.6
16-122
13.7
20
4-Nitroaniline
53.9
0.740
pg/L
50
52.8
108
23-139
2
20
N-Nitrosodiphenylamine
31
0.783
pg/L
50
27.7
62
45-135
11.2
20
4-Chlorophenyl phenyl ether
34.8
0.479
pg/L
50
32.5
69.6
39-110
6.8
20
4-Chloroaniline
28.7
0.526
pg/L
50
24.4
57.4
24-127
16.1
20
Benzidine
49.1
0.689
pg/L
150
37.5
32.7
2-176
26.7
20
LCD2
Butyl benzyl phthalate
38.1
4.59
pg/L
50
39.7
76.2
33-142
4.1
20
Carbazole
42.2
0.476
pg/L
50
39.1
84.4
20-147
7.6
20
4-Chloro-3-methylphenol
36.3
0.503
pg/L
50
32.5
72.6
35-117
11
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 55 of 84
• 0
Waypoint
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517230 - 3510C
BSD (0100161 LCSD-L517230)
Source: 0100161 LCS-L517Prepared & Analyzed: 10/19/20
Benzyl alcohol
23.8
3.01
pg/L
50
20.5
47.6
20-109
14.8
20
1,3-Dichlorobenzene
24.2
0.491
pg/L
50
20.6
48.4
21-102
16
20
2,4-Dinitrophenol
77.8
4.85
pg/L
150
103
51.8
10-132
27.8
20 LCD2
Pentachlorophenol
48.7
2.45
pg/L
50
49.5
97.4
17-142
1.6
20
N-Nitrosodiethylamine
32.6
0.400
pg/L
50
28.1
65.2
25-107
14.8
20
2,4-Dimethylphenol
33.7
0.674
pg/L
50
30.2
67.4
34-105
10.9
20
N-Nitrosodimethylamine
15.1
0.249
pg/L
50
12.8
30.2
14-84
16.4
20
2,4-Dinitrotoluene
35.3
0.403
pg/L
50
33.4
70.6
24-147
5.5
20
2,4-Dichlorophenol
25.7
1.52
pg/L
50
23.3
51.4
32-110
9.7
20
Phenanthrene
36.1
0.464
pg/L
50
33.2
72.2
40-120
8.3
20
2-Chorophenol
28.4
0.736
pg/L
50
25
56.8
27-102
12.7
20
1,4-Dichlorobenzene
24.8
0.580
pg/L
50
21.3
49.6
24-99
15.1
20
N-Nitroso-di-n-butylamine
30
0.752
pg/L
50
26.5
60
25-126
12.3
20
N-Nitroso-di-n-propylamine
28.9
0.334
pg/L
50
25.3
57.8
29-114
13.2
20
2,4,5-Trichlorophenol
39.4
0.350
pg/L
50
35.1
78.8
26-118
11.5
20
2,3,4,6-Tetrachlorophenol
38.5
0.355
pg/L
50
35.7
77
28-118
7.5
20
Phenol
11.9
0.389
pg/L
50
10.5
23.8
11-55
12.5
20
Pyrene
33
1.04
pg/L
50
40.7
66
20-154
20.8
20 LCD2
Pyridine
15.7
0.678
pg/L
50
12.9
31.4
10-71
19.5
20
2,6-Dinitrotoluene
36.8
0.413
pg/L
50
33.5
73.6
36-125
9.3
20
1,2-Dichlorobenzene
25.5
0.629
pg/L
50
22.5
51
26-100
12.5
20
2-Chloronaphthalene
29.5
0.476
pg/L
50
26
59
29-137
12.6
20
Benzo(a)anthracene
35.3
0.427
pg/L
50
32.5
70.6
36-127
8.2
20
Indeno(1,2,3-cd)pyrene
40.4
1.01
pg/L
50
33.1
80.8
22-126
19.8
20
1,2,4,5-Tetrachlorobenzene
30.2
0.317
pg/L
50
26.8
60.4
28-110
11.9
20
Isophorone
26.6
0.360
pg/L
50
23.3
53.2
31-116
13.2
20
2,6-Dichlorophenol
35.5
0.703
pg/L
50
31.1
71
25-112
13.2
20
Naphthalene
28
0.484
pg/L
50
24.7
56
33-108
12.5
20
2,4,6-Trichlorophenol
38.5
0.344
pg/L
50
34.3
77
26-115
11.5
20
1,2,4-Trichlorobenzene
27.3
0.482
pg/L
50
24.3
54.6
23-106
11.6
20
Nitrobenzene
30
0.531
pg/L
50
26.3
60
27-117
13.1
20
Surrogate:2-Fluorophenol
23.5
pg/L
100
20.2
23.5
10-44
Surrogate:2-Fluorobiphenyl
45
pg/L
100
43.6
45
24-93
Surrogate:4-Terphenyl-d14
55.2
pg/L
100
74.7
55.2
35-126
Surrogate: 2,4,6-Tribromophenol
67.8
pg/L
100
63.3
67.8
39-110
Surrogate: Phenol-d6
16.4
pg/L
100
14.8
16.4
7-32
Surrogate: Nitrobenzene-d5
49.7
pg/L
100
47.4
49.7
20-91
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 56 of 84
• 0
Waypoint
ANALYTICAL
Level II QC Report
11 /30/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100161
Attn: Alec Macbeth Time Submitted: 10/13/2020 8:25:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517230 - 3510C
BS (0100161 LCS-L517230)
Prepared & Analyzed: 10/19/20
Benzo(g,h,i)perylene
30.6
1.36
pg/L
50
61.2
26-123
Benzo(a)pyrene
30.9
1.00
pg/L
50
61.8
34-131
Bis(2-Chloroisopropyl)ether
19.4
0.546
pg/L
50
38.8
28-108
Bis(2-Chloroethyl)ether
25.1
0.447
pg/L
50
50.2
16-122
Phenanthrene
33.2
0.464
pg/L
50
66.4
40-120
Bis(2-Chloroethoxy)methane
27.3
0.433
pg/L
50
54.6
20-126
Phenol
10.5
0.389
pg/L
50
21
11-55
Benzyl alcohol
20.5
3.01
pg/L
50
41
20-109
Pyrene
40.7
1.04
pg/L
50
81.4
20-154
Benzo(k)fluoranthene
34.5
0.752
pg/L
50
69
32-132
Benzoic Acid
30.6
5.00
pg/L
150
20.4
11-68
Benzo(b)fluoranthene
38.4
0.941
pg/L
50
76.8
36-131
Dimethyl phthalate
33
0.510
pg/L
50
66
34-123
Hexachloroethane
19
0.277
pg/L
50
38
16-107
Hexachlorocyclopentadiene
13.9
2.34
pg/L
50
27.8
10-102
Hexachlorobutadiene
22.5
0.405
pg/L
50
45
22-109
Indeno(1,2,3-cd)pyrene
33.1
1.01
pg/L
50
66.2
22-126
Hexachlorobenzene
33.6
2.57
pg/L
50
67.2
18-136
Isophorone
23.3
0.360
pg/L
50
46.6
31-116
Fluorene
31.4
0.444
pg/L
50
62.8
41-116
Naphthalene
24.7
0.484
pg/L
50
49.4
33-108
Fluoranthene
36
0.406
pg/L
50
72
28-127
Di-n-Octyl Phthalate
36.4
1.72
pg/L
50
72.8
29-136
Nitrobenzene
26.3
0.531
pg/L
50
52.6
27-117
Carbazole
39.1
0.476
pg/L
50
78.2
20-147
Pentachlorophenol
49.5
2.45
pg/L
50
99
17-142
N-Nitrosodiethylamine
28.1
0.400
pg/L
50
56.2
25-107
Diethyl phthalate
33.6
0.585
pg/L
50
67.2
36-130
Dibenzofuran
33.2
0.423
pg/L
50
66.4
40-108
Dibenz(a,h)anthrace ne
29.9
0.252
pg/L
50
59.8
27-124
N-Nitrosodimethylamine
12.8
0.249
pg/L
50
25.6
14-84
Pyridine
12.9
0.678
pg/L
50
25.8
10-71
N-Nitroso-di-n-butylamine
26.5
0.752
pg/L
50
53
25-126
Chrysene
32.3
0.731
pg/L
50
64.6
30-124
N-Nitroso-di-n-propylamine
25.3
0.334
pg/L
50
50.6
29-114
Butyl benzyl phthalate
39.7
4.59
pg/L
50
79.4
33-142
Bis(2-ethylhexyl)phthalate
37.4
3.66
pg/L
50
74.8
21-162
N-Nitrosodiphenylamine
27.7
0.783
pg/L
50
55.4
45-135
Di-n-butyl phthalate
34.5
1.58
pg/L
50
69
19-158
2-Nitrophenol
28.6
0.606
pg/L
50
57.2
25-114
4-Bromophenyl phenyl ether
33.4
0.500
pg/L
50
66.8
31-124
2-Methylphenol
22
0.721
pg/L
50
44
22-97
2,4-Dinitrophenol
103
4.85
pg/L
150
68.6
10-132
4-Nitroaniline
52.8
0.740
pg/L
50
106
23-139
4-Chlorophenyl phenyl ether
32.5
0.479
pg/L
50
65
39-110
2,4,5-Trichlorophenol
35.1
0.350
pg/L
50
70.2
26-118
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 57 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517230 - 3510C
BS (0100161 LCS-L517230)
Prepared & Analyzed: 10/19/20
2,6-Dichlorophenol
31.1
0.703
pg/L
50
62.2
25-112
2-Nitroaniline
35
0.574
pg/L
50
70
32-127
2,3,4,6-Tetrachlorophenol
35.7
0.355
pg/L
50
71.4
28-118
4-Chloro-3-methyl phenol
32.5
0.503
pg/L
50
65
35-117
4-Nitrophenol
10.6
1.39
pg/L
50
21.2
1-76
2-Chorophenol
25
0.736
pg/L
50
50
27-102
2,4,6-Trichlorophenol
34.3
0.344
pg/L
50
68.6
26-115
2,4-Dinitrotoluene
33.4
0.403
pg/L
50
66.8
24-147
4,6-Dinitro-2-methylphenol
47.1
3.47
pg/L
50
94.2
27-128
2,4-Dichlorophenol
23.3
1.52
pg/L
50
46.6
32-110
3-Nitroaniline
32.3
1.53
pg/L
50
64.6
28-142
3&4 Methylphenol
23.7
0.691
pg/L
50
47.4
21-96
3,3'-Dichlorobenzidine
95.9
3.74
pg/L
150
63.9
6-192
2,4-Dimethylphenol
30.2
0.674
pg/L
50
60.4
34-105
3,3' Dimethylbenzidine
55.8
1.88
pg/L
200
27.9
6-192
4-Chloroaniline
24.4
0.526
pg/L
50
48.8
24-127
Aniline
18.1
0.316
pg/L
50
36.2
16-133
Benzidine
37.5
0.689
pg/L
150
25
2-176
1,2,4,5-Tetrachlorobenzene
26.8
0.317
pg/L
50
53.6
28-110
Anthracene
33.8
0.467
pg/L
50
67.6
34-128
1,2,4-Trichlorobenzene
24.3
0.482
pg/L
50
48.6
23-106
1,2-Dichlorobenzene
22.5
0.629
pg/L
50
45
26-100
1,4-Dichlorobenzene
21.3
0.580
pg/L
50
42.6
24-99
Acetophenone
27.2
0.686
pg/L
50
54.4
25-108
Acenaphthylene
29.7
0.429
pg/L
50
59.4
37-114
1,3-Dichlorobenzene
20.6
0.491
pg/L
50
41.2
21-102
2-Methyl naphthalene
29.7
0.485
pg/L
50
59.4
34-108
Acenaphthene
27.4
0.422
pg/L
50
54.8
38-117
Benzo(a)anthracene
32.5
0.427
pg/L
50
65
36-127
2,6-Dinitrotoluene
33.5
0.413
pg/L
50
67
36-125
2-Chloronaphthalene
26
0.476
pg/L
50
52
29-137
Surrogate: Phenol-d6
14.8
Ng/L
100
14.8
7-32
Surrogate: Nitrobenzene-d5
47.4
pg/L
100
47.4
20-91
Surrogate: 2,4,6-Tribromophenol
63.3
Ng/L
100
63.3
39-110
Surrogate:2-Fluorobiphenyl
43.6
Ng/L
100
43.6
24-93
Surrogate:2-Fluorophenol
20.2
Ng/L
100
20.2
10-44
Surrogate:4-Terphenyl-d14
74.7
Ng/L
100
74.7
35-126
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 58 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517230 - 3510C
BILK (0100161 LRB-11-517230)
Prepared & Analyzed: 10/19/20
Indeno(1,2,3-cd)pyrene
BRL
2.00
pg/L
2,4-Dinitrophenol
BRL
10.0
pg/L
2-Chlorophenol
BRL
5.00
pg/L
2,4-Dinitrotoluene
BRL
5.00
pg/L
2,6-Dichlorophenol
BRL
5.00
pg/L
Isophorone
BRL
5.00
pg/L
Nitrobenzene
BRL
5.00
pg/L
2,6-Dinitrotoluene
BRL
5.00
pg/L
Naphthalene
BRL
2.00
pg/L
2-Chloronaphthalene
BRL
5.00
pg/L
2,3,4,6-Tetrachlorophenol
BRL
5.00
pg/L
Pyridine
BRL
10.0
pg/L
1,2,4,5-Tetrachlorobenzene
BRL
5.00
pg/L
Pyrene
BRL
2.00
pg/L
1,2,4-Trichlorobenzene
BRL
5.00
pg/L
1,2-Dichlorobenzene
BRL
5.00
pg/L
Phenol
BRL
5.00
pg/L
1,3-Dichlorobenzene
BRL
5.00
pg/L
1,4-Dichlorobenzene
BRL
5.00
pg/L
Pentachlorophenol
BRL
10.0
pg/L
N-Nitrosodiphenylamine
BRL
10.0
pg/L
N-Nitroso-di-n-propylamine
BRL
5.00
pg/L
2,4,5-Trichlorophenol
BRL
5.00
pg/L
2-Methylphenol
BRL
5.00
pg/L
N-Nitroso-di-n-butylamine
BRL
5.00
pg/L
N-Nitrosodimethylamine
BRL
5.00
pg/L
2,4-Dichlorophenol
BRL
5.00
pg/L
2,4-Dimethylphenol
BRL
5.00
pg/L
N-Nitrosodiethylamine
BRL
5.00
pg/L
Phenanthrene
BRL
2.00
pg/L
Acenaphthylene
BRL
2.00
pg/L
Hexachloroethane
BRL
5.00
pg/L
Butyl benzyl phthalate
BRL
5.00
pg/L
2-Methyl naphthalene
BRL
2.00
pg/L
4-Chlorophenyl phenyl ether
BRL
5.00
pg/L
Bis(2-Chloroisopropyl)ether
BRL
5.00
pg/L
4-Nitroaniline
BRL
5.00
pg/L
Bis(2-Chloroethyl)ether
BRL
5.00
pg/L
4-Nitrophenol
BRL
10.0
pg/L
Bis(2-Chloroethoxy)methane
BRL
5.00
pg/L
4-Chloro-3-methylphenol
BRL
5.00
pg/L
Acenaphthene
BRL
2.00
pg/L
4-Chloroaniline
BRL
5.00
pg/L
Benzoic Acid
BRL
10.0
pg/L
Benzo(k)fluoranthene
BRL
2.00
pg/L
Acetophenone
BRL
5.00
pg/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 59 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517230 - 3510C
BILK (0100161 LRB-11-517230)
Prepared & Analyzed: 10/19/20
Benzo(g,h,i)perylene
BRL
2.00
pg/L
Aniline
BRL
5.00
pg/L
Anthracene
BRL
2.00
pg/L
Benzo(b)fluoranthene
BRL
2.00
pg/L
Benzo(a)pyrene
BRL
2.00
pg/L
Benzidine
BRL
20.0
pg/L
Benzo(a)anthracene
BRL
2.00
pg/L
Benzyl alcohol
BRL
10.0
pg/L
2-Nitrophenol
BRL
5.00
pg/L
Hexachlorocyclopentadiene
BRL
5.00
pg/L
Hexachlorobutadiene
BRL
5.00
pg/L
Hexachlorobenzene
BRL
5.00
pg/L
2,4,6-Trichlorophenol
BRL
5.00
pg/L
Fluorene
BRL
2.00
pg/L
Fluoranthene
BRL
2.00
pg/L
Bis(2-ethylhexyl)phthalate
BRL
5.00
pg/L
Di-n-Octyl Phthalate
BRL
5.00
pg/L
Carbazole
BRL
5.00
pg/L
Dibenzofuran
BRL
5.00
pg/L
Chrysene
BRL
2.00
pg/L
4-Bromophenyl phenyl ether
BRL
5.00
pg/L
2-Nitroaniline
BRL
5.00
pg/L
Dibenz(a,h)anthrace ne
BRL
2.00
pg/L
Di-n-butyl phthalate
BRL
5.00
pg/L
3-Nitroaniline
BRL
10.0
pg/L
3,3'-Dichlorobenzidine
BRL
10.0
pg/L
Diethyl phthalate
BRL
5.00
pg/L
Dimethyl phthalate
BRL
5.00
pg/L
3,3' Dimethylbenzidine
BRL
10.0
pg/L
3&4 Methylphenol
BRL
5.00
pg/L
4,6-Dinitro-2-methylphenol
BRL
10.0
pg/L
-
Surrogate: Phenol-d6
16.3
Ng/L
100
16.3
7-32
Surrogate: 2,4,6-Tribromophenol
68.5
ug/L
100
68.5
39-110
Surrogate: Nitrobenzene-d5
54.3
Ng/L
100
54.3
20-91
Surrogate:4-Terphenyl-d14
71.7
Ng/L
100
71.7
35-126
Surrogate:2-Fluorobiphenyl
47.9
Ng/L
100
47.9
24-93
Surrogate:2-Fluorophenol
24.2
Ng/L
100
24.2
10-44
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 60 of 84
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Organic Carbon - Quality Control
Analyte
Batch L518399 - 531 OC-2011
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
11 /30/20
Work Order: 0100161
Time Submitted: 10/13/2020 8:25:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
MSD (0100161 L 90962-MSD-L518399)
Source: 0100161 L 90962-hPrepared: 10/23/20 Analyzed: 10/24/20
TOC
8.77 0.522 mg/L
5.26 8.56 105 70-130 2.4
MS (0100161 L 90962-MS-L518399)
Source: 0100161-03
Prepared: 10/23/20 Analyzed: 10/24/20
TOC
8.56 0.522 mg/L
5.26 3.22 101 70-130
BS (0100161 LCS-L518399)
Prepared: 10/23/20 Analyzed: 10/24/20
TOC
5.23 0.498 mg/L
5 105 85-115
BILK (0100161 LRB-L518399)
Prepared: 10/23/20 Analyzed: 10/24/20
TOC
BRL 1.00 mg/L
-
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 61 of 84
Sample Extraction Data
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
0100161-02
POJ0218
50
mL
50 mL
10/14/20 10:20
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
0100161-02
POJ0259
20
mL
30 mL
10/15/20 11:56
Prep Method: 9010C
Lab Number
Batch
Initial
Final
Date/Time
0100161-01
POJ0357
50
mL
50 mL
10/20/20 8:10
0100161-02
POJ0357
50
mL
50 mL
10/20/20 8:10
0100161-03
POJ0357
50
mL
50 mL
10/20/20 8:10
Prep Method: SM4500-S C
Lab Number
Batch
Initial
Final
Date/Time
0100161-01
POJ0337
200
mL
200 mL
10/19/20 11:02
0100161-02
POJ0337
200
mL
200 mL
10/19/20 11:02
0100161-03
POJ0337
200
mL
200 mL
10/19/20 11:02
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
0100161-01
POJ0214
990
mL
10 mL
10/14/20 11:30
0100161-02
POJ0214
1000
mL
10 mL
10/14/20 11:30
0100161-03
POJ0214
1000
mL
10 mL
10/14/20 11:30
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
0100161-01
POJ0214
990
mL
10 mL
10/14/20 11:30
0100161-02
POJ0214
1000
mL
10 mL
10/14/20 11:30
0100161-03
POJ0214
1000
mL
10 mL
10/14/20 11:30
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
0100161-01
POJ0239
50
mL
50 mL
10/15/20 7:44
0100161-01
POJ0490
50
mL
50 mL
10/27/20 7:00
0100161-02
POJ0239
50
mL
50 mL
10/15/20 7:44
0100161-02
POJ0490
50
mL
50 mL
10/27/20 7:00
0100161-02
POJ0239
50
mL
50 mL
10/15/20 7:44
0100161-03
POJ0239
50
mL
50 mL
10/15/20 7:44
0100161-03
POJ0490
50
mL
50 mL
10/27/20 7:00
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
0100161-01
POJ0374
20
mL
30 mL
10/20/20 11:55
0100161-02
POJ0374
20
mL
30 mL
10/20/20 11:55
0100161-03
POJ0374
20
mL
30 mL
10/20/20 11:55
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
0100161-01
POJ0321
10
mL
10 mL
10/21/20 10:00
0100161-02
POJ0321
10
mL
10 mL
10/21/20 10:00
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 62 of 84
Sample Extraction Data
Prep Method: 5030E
Lab Number Batch Initial Final Date/Time
0100161-03 POJ0321 10 mL 10 mL 10/21/20 10:00
0100161-04 POJ0321 10 mL 10 mL 10/21/20 10:00
Prep Method: 5030E
Lab Number Batch Initial Final Date/Time
0100161-01
POJ0316
5 mL
5 mL 10/16/20 10:00
0100161-02
POJ0316
5 mL
5 mL 10/16/20 10:00
0100161-03
POJ0316
5 mL
5 mL 10/16/20 10:00
Sample Extraction Data
Prep Method: 3510C
Lab Number
Batch
Initial
Final Date/Time
0100161-01
L517325
10/19/20 15:45
0100161-02
L517325
10/19/20 15:45
0100161-03
L517325
10/19/20 15:45
Prep Method: 8151A
Lab Number
Batch
Initial
Final Date/Time
0100161-01 L517362 10/19/20 17:11
0100161-02 L517362 10/19/20 17:11
0100161-03 L517362 10/19/20 17:11
Prep Method: 3510C
Lab Number Batch Initial Final Date/Time
0100161-01 L517230 10/19/20 11:30
0100161-02 L517230 10/19/20 11:30
0100161-03 L517230 10/19/20 11:30
Prep Method: 5310C-2011
Lab Number Batch Initial Final Date/Time
0100161-01 L518399 10/23/20 14:11
0100161-02 L518399 10/23/20 14:11
0100161-03 L518399 10/23/20 14:11
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 63 of 84
Subcontracted Analyses
The following analyses were subcontracted to Pace Analytical Gulf Coast
Lab Number
Analysis
0100161-01
Carbon Dioxide AM20GAX
0100161-01
Hydrogen AM20GAX
0100161-01
Methane, Ethane, Ethene (AM20GAX)
0100161-01
Volatile Fatty Acids (Sub)
0100161-02
Carbon Dioxide AM20GAX
0100161-02
Hydrogen AM20GAX
0100161-02
Methane, Ethane, Ethene (AM20GAX)
0100161-02
Volatile Fatty Acids (Sub)
0100161-03
Carbon Dioxide AM20GAX
0100161-03
Hydrogen AM20GAX
0100161-03
Methane, Ethane, Ethene (AM20GAX)
0100161-03
Volatile Fatty Acids (Sub)
The following analyses were subcontracted to Waypoint Analytical
Lab Number
Analysis
O100161-01
8270 (App. II)
0100161-01
Herbicides (Sub)
0100161-01
TOC (Sub)
0100161-02
8270 (App. I1)
0100161-02
Herbicides (Sub)
O100161-02
TOC (Sub)
0100161-03
8270 (App. I1)
0100161-03
Herbicides (Sub)
0100161-03
TOC (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 64 of 84
CHAIN OF CUSTODY RECORD
LAB USE ONLY
Waypoint
PAGE A 1 PROPER BILLING:
YES NO N/A
— OF QUOTE # TO ENSURE
Samples INTACT upon arrival? �
ANALYTICAL
fit-
Project Name: �'�JTl ��
Received IN ICE?
449 Sprone 7 brook41529 Road • Charlotte, NC 28217
Phone 704/529-6364 Fax: 704/525-0409
Short Hold Anal sis Yes No T Project: Yes No
y (Yes) ) J ( ( )
PROPER PRESERVATIVES indicated?
*Please ATTACH any p ct specific reporting (QC LEVEL 1 II III I
Received WITHIN HOLDING TIMES? 1�
Client Company Name:
provisions and/or QC Requirements
CUSTODY SEALS INTACT?
Report To/Contact Name:i.C. MCAT
Invoice To -
VOLATILES rec'd W/OUT HEADSPACE?
��qy
Reporting Address: ' QQ / woo(A�
Address:
(
PROPER CONTAINERS use ? f
TEMP: Therm ID:_��ii Observed 4 �C/Corr. Z'� �C
Phone: R}�?��� 50 Fax (Yes)(No):
Purchase Order No./Billing -6 a ®
PERSONNEL
Reference
TO BE FILLEDIN BY CJ�IENT/SAMPLING
Email Address:
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'5
Certification: NC SC
EDD Type: PDF Excel Other
"Working Days" ❑ 6-9 Days Crd'Standard 10 days ❑ Rush Work Must Be
Pre Approved
Other N/A�
Site Location Name: 3LlGLt-SOA C/>1. ��..{��
Samples received after 15:00 will be processed next business da y.
Site Location Physical Address: DI tl ob",
WC/ Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT)
SarrTles Iced Upon Collection: - YES_NO
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ALY Ij �ED `
J
"TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER, OR
TIVESiV
A
�v
ID NO.
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
Q� O
RkK-6+40,Na1a'
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1 • •
Sampler's Signature
ampled By (Print Name) 1 1 Affiliation LAB USE ONLY
Upon relinquishing, s Chain of Custody is your authorization
for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be Site Arrival Time:
submitted in writing tot Wa o' t Analytical Project
Manager. There will be charges for any changes after analyses have been initialized.
Relinquished By: (Signatur
Received B ' ignature) Da Military/Hours Additional Comments: Site Departure Time:
RBlinquished y: (Sig ture)
Received By: (Signatu ) Date
gg Field Tech Fee:
l
Relin ' hed By: i at�
ceived For Waypoint Analytical By: Date Mileage:
Metho of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTA ION THE LABO ORY. COCK3roUp No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEI ED qT THE LABORATOR . a -
❑ Fed Ex ❑ UPS ❑ Hand -delivered ❑ Waypoint Analytical Field Service ❑ Other —19A • 1 •
NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA:.. BRW LD LANDFILL _OTHER:
❑ NC ❑ sc ❑ NC ❑ sc NC LA ❑ NC ❑ SC �C ❑ SC ❑ NC ❑ SC ❑ NC ❑ Sc C :1SC ❑ NC ❑ SC Page 65 of 84
❑ ❑ ❑ ❑ ❑— �0— ❑
*rnkMAurvo T Mc rnnoc. Tr _ Tnflnn-I inn.4 r-.,_• v^A 17-- u., A Q---- I
CHAIN -OF -CUSTODY Analytical Request Document
�aceAnalytieal`
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
LAB USE ONLY -Affix Workorder/Login Label Here or List Pace Workorder Number or
MTJL Log -in Number Here
ALL SHADED AREAS are for LAB USE ONLY
Company:
� NG
Billing Information:
U wv " `'�
Address: �+ �@ d
(
Container Preservative Type **
Lab Project Manager:
Report To:
Email To:
** Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
�J
Copy To: t CJ
Site Collection Info/Address:
Analyses
Lab Profile/Line:
Customer Project Name/Number: I �
-SO-C"C I l l✓W/ V L
State: County/City: Time Zone Collected:
NI 16LCY W [ ] PT [ ] MT [ ] CT ET
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y
N
4
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Lab Sample Receipt checklist:
Custody Seals Present/Intact Y N NA
Custody Signatures Present Y N NA
Collector Signature Present Y N NA
Bottles Intact Y N NA
correct Bottles Y N NA
Sufficient Volume Y N NA
Samples Received on Ice Y N NA
VOA - Headspace Acceptable Y N NA
USDA Regulated Soils Y N NA
Samples in Holding Time Y N NA
Residual Chlorine Present Y N NA
Cl Strips:
Sample pH Acceptable Y N NA
pH Strips:
Sulfide Present Y N NA
Lead Acetate Strips:
LAB USE ONLY:
Lab Sample # /Comments:
Phone:
Email:
Site/Facility ID #:
Compliance Monitoring?
14 Yes [ ] No
Collected By (print):
Purchase Order #:
Quote #: —Dt s�L
DW PWS ID #:
DW Location Code:
C011ecte y na e):
Turnaround Date Required:
Immediately Packed on Ice:
a. [ ]No
Sampl Disposal:
[ ispose as appropriate [ ] Return
[ ] Archive:
[ ] Hold:
Rush:
[ ] Same Day [ ] Next Day
[ ] 2 Day [ ] 3 Day [ ] 4 Day [ ] 5 Day
(Expedite Charges Apply)
Field Filtered (if applicable):
[ ] Yes [ -4l 0
Analysis:
* Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid [SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Customer Sample ID
Matrix *
Comp /
Grab
Collected (or
Composite Start)
Composite End
Res
Cl
# of
Ctns
Date
Time
Date
Time
NL-U�'-�av►ol�
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to
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Customer Remarks / Special Conditions / Possible Hazards:
Type of Ice Used: We Blue Dry None
SHORT HOLDS PRESENT (<72 hours): Y N N/A
Lab Sample Temperature Info:
Temp Blank Received: Y N NA
ThermID#:
Cooler 1 Temp Upon Receipt: oC
Cooler 1 Therm Corr. Factor: oC
Cooler 1 Corrected Temp: oC
Comments:
Packing Material Use
Lab Tracking #:
2594653
Radchem sample(s) screened (<500 cpm): Y N NA
Samples received via:
FEDEX UPS Client Courier Pace Courier
Relinquished /Co an : (Signature)
Date/Time:
Received%�/CCoom�pany: (Signature)
Date/Time:)
MTJL LAB USE ONLY
Table #:
Acctnum:
Template:
Prel gin:
11610'rquisg—ed bb company: (Signature)
1
Date/Time:
I y ' / u c��
Received by/Company: TS n—atture)
AQ " �
Date/Time:
V'3
Trip Blank Received: Y N NA
HCL McOH TSP Other
Relinquished by/Company: (Signature)
Date/Time:
hJ
0
Received by/Compa . ( gna re)
t� ;
Date/Time:
0
li •��"�l� l: �L
PM:
Non Conformance{
YES / NO
Page 66 of 84
aceAna lytical
D eliver To
LELAP CERTIFICATE 116JM ER: 01955
D DO -ELAP ACCREDITNTIO MUM ER: 74960
ANALYTICAL RESULTS
A ngie Overcash
W aypoint Analytical
4 49 Springbrook Road
PO Box 240543
C harlotte, NC 28224
7 04 529 6364
PERFCIRM D BY
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
(225) 769-4900
Report Date 10/26/2020
Report # 220101613
Project 0100161
dditional Recipients
ONE
V
ISO
PJLA '� 7426
Wst ny
DOD ELAF f
Pace G If Coast Report#: 220101613 1 Page 67 of 84
ac6Anaoical Report#: 20101613
11!®
r Project ID: @00161
eport Date: @/26/2020
Laboratory Endersem nt
Saar le analysis was perfoon d in accordance with approveden thodologies provided by the Envirorun ntal Protection Agency or other recognized
agencies. The sW les and their corresponding extracts will bean intained for a period of 30 days unless otherwise arranged. Following this
retention period the sgan les will be disposed in accordance with Pace G If Coast's Standar¢ O erating Procedures.
Corn on Abbreviations that m y be Utilized in this Report
ND ndicates the result was Not Detected at the specified reporting lim t
NO Indicates the saran le did not ignite when prelim nary test perfoon d for EPPeM thod 1030
DO ndicates the result was Dialed O t
IM ndicates the result was subject tcbM trix Interference
TNTC ndicateslthe result was Too Nam rous To Count
SUBC ndicates the analysis was Sub -Contracted
FLD ndicates the analysib was perfoen d in the Field
DL etection Liim t D
no im t of Detection L
@O im t of Q antitation
RE e-analysis R
CF PLC cEG Confien tion H
00:01 eported ER a *n equivalent to 12:00 AM
Reporting Flags that m y be Utilized in this Report
J or I ndicates the result is between the[M L andQO
J DO flag on analyte in the parent saran le fo0VDW D outside acceptance criteria
U ndicates the cgan ound was analyzed for bdt not detected
B or V ndicatesl the analyte was detected in the associatedBM thod Blank
Q Indicates a non-cqun liarf£Q Result (See Q Flag Application Report)
ndicates a non-cqun liant or not applicablCQ rebovery or RPD — see narrative
E rganics - The result is estbn ted because it @xceeded the instruen nt calibration range
E etals - % diference for the serial dilution is M0%
L eporting Lim is adjusted toen et risk -based I5h t.
P PD between priffn ry and confian tion resulfds greater than 40
DL iluted analysis — when appended[Bo Client Saran le ID
Saar le receipt at Pace G If Coast is docum nted through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written perm ssion of Pace G If Coast. The results contained within this report relate only to the s;frn les
reported. The docuen nted results are presented within this report.
This report pertains only to the sawn les listed in the Report Sawn le Scam ary and should be retained as a peon nent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the infoon tion contained in this report is prohibited.
I certify that this data package is in cgan Hance with The NELAC Institute (TNI) Standard 2009 and teen and conditions of the contract and
Statem nt of ft rk both technically and for cgan leteness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the cgnn uter readable data subm tted has been authorized by the Q ality Assuranceam nager or his/her designee,
as verified by the following signature.
Estbn ted uncertainty ofen asureEn nt is available upon request. This report is in cgzn liance with the DO SQ M as specified in the contract if
applicable.
Authorized Signature
Pace G If Coast Report 220101613
Pace G If Coast Report#: 220101613 1 Page 68 of 84
ac6Anaoical Report#: 20101613
11!®
r Project ID: @00161
Certifications
eport Date: @/26/2020
Certification
ertification Nuhi er
[DO ELAP
4960
Alabam
1955
Arkansas
8-0655
Colorado
1955
Delaware
1955
Florida
87854
G orgia
1955
Hawaii
1955
Idaho
1955
Illinois
00048
Indiana
1955
Kansas
-10354
Kentucky
5
Louisiana
1955
M r land
1955
M ssachusetts
1955
M chi an
1955
M ssissippi
1955
M ssouri
1955
M ntana
/A
Nebraska
1955
NeveM xico
1955
North Carolina
18
North Dakota
-195
O lahem
403
South Carolina
3006001
South Dakota
1955
Tennessee
1955
Texas
104704178
Veom nt
1955
Virginia
60215
M shin ton
929
USDA Soil Perm t
330-16-00234
Pace G If Coast Report#: 220101613 1 Page 69 of 84
ac6Anaoical Report#: 20101613
11!®
r Project ID: @00161
Case Narrative
Client: Waypoint Analytical Report: 220101613
eport Date: @/26/2020
Pace Analytical G If Coast received and analyzed the spm le(s) listed
on the Report Spm le Smn ary page of this report. Receipt of the spm le(s) is docem nted
by the attached chain of custody. This applies only to the spm le(s) listed in this report.
No spm le integrity or quality control exceptions were identified unless noted below.
LYO ATILEA G S CHVRO ATO RAPHY
In the AMPOG X analysis for analytical batch 695200p M thane was detected at an estim ted concentration in theem thod blank.
This is probable laboratory contem nation.
Pace G If Coast Report#: 220101613 1 Page 70 of 84
aceAnaly�ical®
r
Report#: 20101613
Project ID: @00161
eport Date: m/26/2020
pSa rya lens u m ry
LAB ID Client ID atrix ollect Date/Tien
22010161301
W-04-20201012
22010161302
W-04-20201012 (1-12)
22010161303
W-05R-20201012
22010161304
W-07-20201012
22010161305
W-07-20201012 (1-12)
Alb
0/12/202013:00
ubdble Strip
0/12/2020 13:00
Mbr
0/12/202014:34
Nbr
0/12/202010:57
ubdble Strip
0/12/2020 10:57
eceive Date/Time
0/ 14/2020 15:05
0/14/202015:05 B
0/ 14/2020 15:05
0/14/2020 15:05
0/14/202015:05 B
Pace G If Coast Report#: 220101613 1 Page 71 of 84
ac6Anaoical Report#: 20101613
11!®
r Project ID: @00161 eport Date: @/26/2020
a nSum ry ofpCom ounds Detected
Collect Date 10/12/2020 13:00 LAB ID 22010161301
I M-04-20201012
Receive Date 10/14/2020 15:05 M trix VVd ter
EPA RSK-175
CAS#
aram ter
Result
DL
@O P
Units
124-38-9
arbon Dioxide
9300
29340
18000
ug/L
AM 3G
CAS#
aram ter
esult
L
@O P
Units
64-19-7
cetic Acid
.54
.12
A 0.50
ig /L
64-18-6
orin c Acid
.8
.055
F 0.50
ig /L
2A% OG X
CAS#
aram ter
esult
L
@O P
Units
74-82-8
ethane
90
.5
M 5.0
ug/L
Collect Date 10/12/2020 13:00 LAB ID 22010161302
I M-04-20201012 (H2)
Receive Date 10/14/2020 15:05 M trix Bubble Strip
2A% OG X
CAS# aram ter Result DL @O P Units
1333-74-0 ydrogen 0 H 0.49 1.9 nM
Collect Date 10/12/2020 14:34 LAB ID 22010161303
I M-05R-20201012
Receive Date 10/14/2020 15:05 M trix V\5 ter
EPA RSK-175
CAS#
aram ter
124-38-9
arbon Dioxide
AM 3G
CAS#
aram ter
64-19-7
cetic Acid
Result
DL
@O P
Units
5300
2590
18000
ug/L
esult
L
QO P
Units
.2J
.2
A 5.0
Kj /L
Pace G If Coast Report#: 220101613 1 Page 72 of 84
Report#: 20101613
aceAnalytica!
Project ID: 000161 eport Date: m/26/2020
a nSum ry ofpCom ounds Detected
Collect Date 10/12/2020 14:34 LAB ID 22010161303
I M-05R-20201012
Receive Date 10/14/2020 15:05 M trix VVa ter
2AM 3G (Continued)
CAS# aram ter
Result
DL
@O P
Units
64-18-6 ortn c Acid
0
0.55
F 5.0
ig /L
2A% OG X
CAS# aram ter
esult
L
GO P
Units
74-82-8 ethane
700
.5
M 5.0
ug/L
Collect Date 10/12/2020 10:57 LAB ID 22010161304
I M-07-20201012
Receive Date 10/14/2020 15:05 M trix VVa ter
EPA RSK-175
CAS#
aram ter
Result
124-38-9
arbon Dioxide
78000
2AM 3G
CAS#
aram ter
esult
64-19-7
cetic Acid
.45J
64-18-6
orin c Acid
.8
2A% OG X
CAS#
aram ter
esult
74-82-8
ethane
40
DL @O P Units
2530 18000 ug/L
L QO P Units
.12 A 0.50 ig /L
055 F 0.50 ig /L
L QO P Units
.5 M 5.0 ug/L
Pace G If Coast Report#: 220101613 1 Page 73 of 84
aceAnaly�ical®
r
Report#: 20101613
Project ID: @00161
eport Date: m/26/2020
a nSum ry ofpCom ounds Detected
Collect Date 10/12/2020 10:57 LAB ID 22010161305
I M-07-20201012 (H2)
Receive Date 10/14/2020 15:05 M trix Bubble Strip
2AM OG X
CAS# aram ter
1333-74-0 ydrogen
Result DL
0 H 0.49
QO P Units
1.9 nM
Pace G If Coast Report#: 220101613 1 Page 74 of 84
aceAnaly�ical®
r
Report#: 20101613
Project ID: (000161
pSam le Results
eport Date: m/26/2020
Collect Date 10/12/2020 13:00 LAB ID 22010161301
I M-04-20201012
Receive Date 10/14/2020 15:05 M trix VVd ter
'A RSK-175
Prep Date rep Batch repEM thod P ilution nagrsis Date A y D nalytical Batch
NA NA A 0 0/22/202011:13 Rvl 95300 6
CAS# aram ter
124-38-9 arbon Dioxide
2AM 3G
Result
DL
GO P
Units
9300
2940
18000
ug/L
Prep Date rep Batch repdM thod P ilution naPysis Date A y D nalytical Batch
NA NA A 0/22/202010:32 S 95177 6 N
CAS#
aram ter
64-19-7
cetic Acid
107-92-6
utyric Acid
64-18-6
orin c Acid
142-62-1
exanoic Acid
646-07-1
-Hexanoic Acid
503-74-2
-Pentanoic Acid
50-21-5
actic Acid
109-52-4
entanoic Acid
79-09-4
ropionic Acid
127-17-3
yruvic Acid
2A% OG X
1
esult
L
410 P
Units
.54
.12
A
0.50
ig /L
058U
.058
0.50
gn /L
.8
.055
F
0.50
ig /L
058U
.098
0.50
gn /L
056U
.056
0.50
gn /L
061 U
.061
0.50
gn /L
053U
.053
L
0.50
gn /L
056U
.086
0.50
gn /L
053U
.053
P
0.50
gn /L
060U
.060
0.50
gn /L
Prep Date rep Batch repdVl thod P ilution niitysis Date A y D nalytical Batch
NA NA A 0/21/202017:52 CK2 95200 6 N
CAS#
aram ter
74-84-0
thane
74-85-1
thene
74-82-8
ethane
A
1
esult
L
00 P
Units
075U
.075
E 1.0
ug/L
.121-1
.12
E 1.0
ug/L
90
.5
M 5.0
ug/L
Pace G If Coast Report#: 220101613 1 Page 75 of 84
ac6Anaoical Report#: 20101613
11!®
r Project ID: @00161 eport Date: @/26/2020
pSam le Results
Collect Date 10/12/2020 13:00 LAB ID 22010161302
I M-04-20201012 (H2)
Receive Date 10/14/2020 15:05 M trix Bubble Strip
2AP
i X
Prep Date rep Batch repeM thod P ilution naPysis Date A y D nalytical Batch
NA NA A 0/22/202018:03 VE 95308 6 N
CAS# aram ter
1333-74-0 ydrogen
1
Result
DL
GO P
Units
0 H
0.49
1.9
nM
Collect Date 10/12/2020 14:34 LAB ID 22010161303
M-05R-20201012
Receive Date 10/14/2020 15:05 M trix VUa ter
PA RSK-175
Prep Date rep Batch repdVl thod P ilution nail rsis Date A y D nalytical Batch Ja
NA NA A 0 0/22/202011:18 Rvl 95300 6
CAS#
124-38-9
2AM 3G
aram ter
arbon Dioxide
Result
DL
GO P
Units
5300
29340
18000
ug/L
Prep Date rep Batch repeM thod P ilution naPysis Date A y D nalytical Batch
NA NA A 0 0/22/202011:25 S 95177 6 N
CAS#
aram ter
64-19-7
cetic Acid
107-92-6
utyric Acid
64-18-6
orin c Acid
142-62-1
exanoic Acid
646-07-1
-Hexanoic Acid
503-74-2
-Pentanoic Acid
50-21-5
actic Acid
109-52-4
entanoic Acid
79-09-4
ropionic Acid
127-17-3
yruvic Acid
2A% OG X
Result
DL
QO P
Units
.2J
1.2
A 5.0
aq /L
.58U
OE38
5.0
gn /L
0
0.55
F 5.0
ig /L
.58U
OM
5.0
gn /L
.561-1
Oi56
5.0
gn /L
.61 U
Oi61
5.0
gn /L
.53U
0.53
L 5.0
gn /L
.561-1
0P56
5.0
gn /L
.53U
0.53
P 5.0
gn /L
.60U
Of80
5.0
gn /L
Prep Date rep Batch repdVl thod P ilution nfflysis Date A y D nalytical Batch
NA NA A 0/21/202018:04 CK2 95200 6 N
CAS# aram ter
74-84-0 thane
A
1
esult L 00 P Units
075U .075 E 1.0 ug/L
Pace G If Coast Report#: 220101613 1 Page 76 of 84
acmnalytical
Report#: 20101613
Project ID: 000161
pSam le Results
eport Date: m/26/2020
Collect Date 10/12/2020 14:34 LAB ID 22010161303
M 05R-20201012
Receive Date 10/14/2020 15:05 M trix VVa ter
2Ar
X (Continued)
Prep Date rep Batch repEM thod P ilution nfflysis Date A y D nalytical Batch
NA NA A 0/21/202018:04 CK2 95200 6 N
CAS#
arass ter
74-85-1
thene
74-82-8
thane
Result DL QO P
.12U 0.12 E 1.0
700 2.5 M 5.0
Collect Date 10/12/2020 10:57 LAB ID 22010161304
M 07-20201012
Receive Date 10/14/2020 15:05 M trix VVa ter
RSK-175
Prep Date rep Batch repdV1 thod P ilution naFjsis Date A y D nalytical Batch
NA NA A 0 0/22/202011:29 Rvl 95300 6
CAS# aram ter
124-38-9 arbon Dioxide
2AM 3G
Result
DL
@O P
Units
78000
2930
18000
ug/L
Prep Date rep Batch repeM thod P ilution naFysis Date A y D nalytical Batch
NA NA A 0/22/202012:18 OS 95177 6 N
CAS#
arms+ ter
64-19-7
cetic Acid
107-92-6
utyric Acid
64-18-6
orin c Acid
142-62-1
exanoic Acid
646-07-1
-Hexanoic Acid
503-74-2
-Pentanoic Acid
50-21-5
actic Acid
109-52-4
entanoic Acid
79-09-4
ropionic Acid
127-17-3
yruvic Acid
1
esult
L
CIO P
Units
.45J
.12
A
0.50
g /L
058U
.058
0.50
gn /L
.8
.055
F
0.50
g /L
058U
.0198
0.50
gn /L
056U
.056
0.50
gn /L
061 U
.061
0.50
gn /L
053U
.053
L
0.50
gn /L
056U
.0136
0.50
gn /L
053U
.053
P
0.50
gn /L
060U
090
0.50
gn /L
Pace G If Coast Report#: 220101613 1 Page 77 of 84
aceAnaly�ical®
r
Report#: 20101613
Project ID: @00161
pSam le Results
eport Date: m/26/2020
Collect Date 10/12/2020 10:57 LAB ID 22010161304
M 07-20201012
Receive Date 10/14/2020 15:05 M trix VVa ter
2Ar
X
Prep Date rep Batch repdN thod P ilution ndTysis Date A y D nalytical Batch
NA NA A 0/21/202018:16 CK2 95200 6 N
CAS#
aram ter
74-84-0
thane
74-85-1
thene
74-82-8
thane
A
1
esult L @O P Units
075U .075 E 1.0 ug/L
.12U .12 E 1.0 ug/L
40 .5 M 5.0 ug/L
Collect Date 10/12/2020 10:57 LAB ID 22010161305
M 07-20201012 (H2)
Receive Date 10/14/2020 15:05 dJl trix Bubble Strip
2Ar
X
Prep Date rep Batch repeM thod P ilution naPysis Date A y D nalytical Batch
NA NA A 0/22/202018:15 VE 95308 6 N
CAS# aram ter
1333-74-0 ydrogen
1
Result DL QO P Units
0 H 0.49 1.9 nM
Pace G If Coast Report#: 220101613 1 Page 78 of 84
ac6Anaoical Report#: 20101613
11!®
r Project ID: @00161
C G Voldtiles Q nSum ry
eport Date: @/26/2020
Analytical Batch Client ID
MB695300
LCS695300
LCSD695300
695300 LAB ID
2099792
2099793
2099794
Senn le Type
W
LCS
LCSD
Prep Date
Analysis Date
10/22/20 09:47
10/22/20 09:56
10/22/20 10:01
aM trix
Wa ter
Wa ter
Wa ter
EPA RSK-175
Units
ug/L
I
Spike
Result
,n
Control
Spike
Result
'R
RPD
RPD
Result
DLI
Added
Lim ts'R
1 Added
Lim t
Carbon Dioxide 24-38-9
27UI
1271
87001
9070
11041
38 - 147
1 7001
9570
1-001
5
1 0
Pace G If Coast Report#: 220101613 1 Page 79 of 84
ac6Anaoical Report#: 20101613
11!®
Project ID: @00161
G neral CherEstryO rfbum ry
eport Date: @/26/2020
Analytical Batch Client ID
MB695177
LCS695177
LCSD695177
695177 LAB ID
2099261
2099262
2099263
Selnn le Type
W
LCS
LCSD
Prep Date
Analysis Date
10/22/20 09:38
10/22/20 08:45
10/22/20 20:46
aM trix
VVa ter
VVa ter
VVa ter
ARM 3G
Units
gn /L
Spike
Result
IR
Control
Spike
Result
1R
RPD
RPD
Result
DL
Added
Lim tS(R
Added
Lim t
Acetic Acid
4-19-7
.12U
0.12
2.0
2.0
99
A - 130
.0
C2.0
101
3
0
Butyric Acid
07-92-6
.058U
0.058
2.0
2.0
102
70 - 130 C
.0
2.1
103
1
0
Form c Acid
4-18-6
.055U
0.055
2.0
2.0
100
70-130
0 .0
2.0
101
1
0
Hexanoic Acid
42-62-1
.058U
0.058
2.0
1.9
97
A - 130 C
.0
2.0
100
3
0
i-Hexanoic Acid
46-07-1
.056U
0.056
2.0
2.0
99
A - 130 C
.0
2.0
101
2
0
i-Pentanoic Acid
03-74-2
.061 U
0.061
2.0
2.0
102
70 - 130 C
.0
2.1
103
1
0
Lactic Acid
0-21-5
.053U
0.053
2.0
1.9
96
A - 130
0 .0
1.9
97
1
0
Pentanoic Acid
09-52-4
.056U
0.056
2.0
2.0
98
A - 130 C
.0
2.0
99
1
0
Propionic Acid
9-09-4
.053U
0.053
2.0
2.0
100
70-130
0 .0
2.0
102
2
0
Pyruvic Acid
27-17-3
.060U
0.060
2.0
1.7
87
A - 130 C
.0
1.8
89
2
0
Pace G If Coast Report#: 220101613 1 Page 80 of 84
ac6Anaoical Report#: 20101613
11!®
Project ID: @00161
G neral Unrom togrOphyQ nSum ry
eport Date: @/26/2020
Analytical Batch Client ID
MB695308
LCS695308
LCSD695308
695308 LAB ID
2099843
2099844
2099845
Senn le Type
LCS
LCSD
Prep Date
Analysis Date
10/22/20 16:01
10/22/20 16:13
10/22/20 16:25
aM trix
ARM AG X
Units
nM
Spike
I Result
Control
Spike
Result
`R
I
RPD
I
RPD
I
Result
DLI
Added
Lim tsR
I Added
Lim t
Hydrogen 333-74-0
.49U
1 0.491
121
12
199
1 70 - 130
1 210
1211021
0
Analytical Batch
Client ID
MB695200
LCS695200
LCSD695200
695200
LAB ID
2099339
2099340
2099341
Senn le Type
W
LCS
LCSD
Prep Date
Analysis Date
10/21/20 15:05
10/21/20 13:42
10/21/20 13:54
aM trix
Wa ter
V\1a ter
VUa ter
ARM AOG X
Units
ug/L
Spike
I Result
IR
Control
Spike
Result
IR
RPD
RPD
Result
DL
Added
Lim is R
Added
Lim t
Ethane
74-84-0
.075U
0.075
100
99
98
A - 130
0 00
110
109
11
1 0
Ethene
74-85-1
.12U
0.12
140
140
95
A - 130
40
050
106
11
1 0
thane
74-82-8
.2J
2.5
490
460
94
70-130
90
510
104
9 3
4 0
Pace G If Coast Report#: 220101613 1 Page 81 of 84
O Q � ❑
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Pace G If Coast Report#: 220101613 Page 16 of 18
0
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Pace G If Coast Report#: 220101613
n
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Page 17 of 18
a
�.paiyres p SFM LE RECEIVING CHECKLIST IINNYIIIIIIVI
SAMPLE DELIVERY GROUP
220101613
CHECKLIST
ES
O
Client PM RWe
ransport Method
T
Samples received with proper thermal preservation?
0
❑
PrisniabNC- Waypoint
F®E X
Analytical
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
0
Q
Profileftm er
Received By
284507
N/bane, Dodie Ni
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
0
0
Line(Item s)
Receive Date(s)
2 - Hydrogen
10/14/20
6 - VFA, IVY. CC2
Preservative added to any containers?
0
If received, was headspace for VOC water containers < 6mm?
0
Samples collected in containers provided by Pace Gulf Coast?
0
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Tberei
m ter ID: E26
pTem °C
None
None
771788277750
1.0
NOTES
Revision 1.6
Page 1 of 1
Pace G If Coast Report#: 220101613
Page 18 of 18
Way poi nt
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Jackson Cty Landfill 2020 Fall
Project No.: 50-02
Lab Submittal Date: 10/14/2020
Work Order: 0100174
Case Narrative
12/31/20 13:17
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a,-1
Angela D. Overcash
Senior Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 62
Data Qualifiers Key Reference:
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
DC The RPD between the primary and confirmation column concentrations is greater than 40. The result is reported
from the primary column.
DID Difference between sample dilutions is greater than 30%.
HA Sample analyzed outside of hold time.
HT Sample received and analyzed outside of the hold time.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
LCD2 LCS/LCSD RPD Value outside of the control limits. LCS and LCSD Values within the control limits.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
MI Matrix spike outside of the control limits. Matrix interference suspected.
SR Surrogate recovery outside of the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 62
1 Q
Waypoint..
ANALYTICAL
Sample Receipt Summary
12/31 /2020
Work Order: 0100174
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
MW-02-20201013
0100174-01
Water
MW-03-20201013
0100174-02
Water
MW-06-20201013
0100174-03
Water
TB-202010130000
0100174-04
Water
Samples were received in good condition at 2.0 degrees C unless otherwise noted
10/13/20 14:50
10/13/20 10:29
10/13/20 13:15
10/13/20 0:00
10/14/20 9:10
10/14/20 9:10
10/14/20 9:10
10/14/20 9:10
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 3 of 62
Way poi nt
ANALYTICAL
Summary of Detections
12/31/202C
Work Order: 0100174
Prism ID
Client ID
Parameter
Method
Result
Units
0100174-01
MW-02-20201013
Chloride
9056A
25000
ug/L
0100174-01
MW-02-20201013
Nitrate as N
9056A
170
J
ug/L
0100174-01
MW-02-20201013
Sulfate
9056A
20000
ug/L
0100174-01
MW-02-20201013
Barium
6020B
24
ug/L
0100174-01
MW-02-20201013
Beryllium
6020B
0.20
J
ug/L
0100174-01
MW-02-20201013
Nickel
6020B
0.81
J
ug/L
0100174-01
MW-02-20201013
Selenium
6020B
1.3
J
ug/L
0100174-01
MW-02-20201013
Biochemical Oxygen Demand
SM5210 B
2300
ug/L
0100174-01
MW-02-20201013
Chemical Oxygen Demand
SM5220 D
37000
J
ug/L
0100174-01
MW-02-20201013
pH
SM4500-H B
7.1
HT
pH Units
0100174-01
MW-02-20201013
Temperature
SM2550 B
20.5
HT
°C
0100174-01
MW-02-20201013
Total Alkalinity to pH 4.5
SM2320 B
55000
ug/L
0100174-01
MW-02-20201013
Diethyl phthalate
8270D
4.65
J
pg/L
0100174-01
MW-02-20201013
Mercury
7470A
0.87
ug/L
0100174-01
MW-02-20201013
Arsenic
6020B
7.5
ug/L
0100174-01
MW-02-20201013
Barium
6020B
250
ug/L
0100174-01
MW-02-20201013
Beryllium
6020B
1.6
ug/L
0100174-01
MW-02-20201013
Chromium
6020B
61
ug/L
0100174-01
MW-02-20201013
Cobalt
6020B
60
ug/L
0100174-01
MW-02-20201013
Copper
6020B
61
ug/L
0100174-01
MW-02-20201013
Lead
6020B
14
ug/L
0100174-01
MW-02-20201013
Nickel
6020B
44
ug/L
0100174-01
MW-02-20201013
Selenium
6020B
42
ug/L
0100174-01
MW-02-20201013
Silver
6020B
0.11
J
ug/L
0100174-01
MW-02-20201013
Thallium
6020B
0.96
.1
ug/L
0100174-01
MW-02-20201013
Vanadium
6020B
71
ug/L
0100174-01
MW-02-20201013
Zinc
6020B
140
ug/L
0100174-01
MW-02-20201013
TOC
531OC-2011
2.26
mg/L
0100174-01
MW-02-20201013
1,1-Dichloroethane
8260D
0.29
J
ug/L
0100174-01
MW-02-20201013
cis-1,2-Dichloroethylene
8260D
0.38
J
ug/L
0100174-01
MW-02-20201013
m,p-Xylenes
8260D
0.21
J
ug/L
0100174-01
MW-02-20201013
Xylenes, total
8260D
0.21
J
ug/L
0100174-01
MW-02-20201013
1,4-Dioxane
8260D SIM
2.8
ug/L
0100174-02
MW-03-20201013
Chloride
9056A
8500
ug/L
0100174-02
MW-03-20201013
Nitrate as N
9056A
8300
ug/L
0100174-02
MW-03-20201013
Sulfate
9056A
4000
ug/L
0100174-02
MW-03-20201013
Biochemical Oxygen Demand
SM5210 B
2000
DID
ug/L
0100174-02
MW-03-20201013
Chemical Oxygen Demand
SM5220 D
35000
J
ug/L
0100174-02
MW-03-20201013
pH
SM4500-H B
8.1
HT
pH Units
0100174-02
MW-03-20201013
Temperature
SM2550 B
20.3
HT
°C
0100174-02
MW-03-20201013
Total Alkalinity to pH 4.5
SM2320 B
140000
ug/L
0100174-02
MW-03-20201013
1,2-Dichlorobenzene
8270D
0.843
J
pg/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 62
Waypoint.
ANALYTICAL
Summary of Detections
12/31/202C
Work Order: 0100174
Prism ID
Client ID
Parameter
Method
Result
Units
0100174-02
MW-03-20201013
1,3-Dichlorobenzene
8270D
0.791
J
pg/L
0100174-02
MW-03-20201013
1,4-Dichlorobenzene
8270D
0.746
J
pg/L
0100174-02
MW-03-20201013
Mercury
7470A
1.1
ug/L
0100174-02
MW-03-20201013
Arsenic
6020B
0.31
J
ug/L
0100174-02
MW-03-20201013
Barium
6020B
110
ug/L
0100174-02
MW-03-20201013
Chromium
6020B
0.86
J
ug/L
0100174-02
MW-03-20201013
Cobalt
6020B
0.59
J
ug/L
0100174-02
MW-03-20201013
Copper
6020B
3.8
J
ug/L
0100174-02
MW-03-20201013
Nickel
6020B
0.96
J
ug/L
0100174-02
MW-03-20201013
TOC
531OC-2011
4.68
mg/L
0100174-02
MW-03-20201013
m,p-Xylenes
8260D
0.37
J
ug/L
0100174-02
MW-03-20201013
Xylenes, total
8260D
0.37
J
ug/L
0100174-03
MW-06-20201013
Chloride
9056A
1100
ug/L
0100174-03
MW-06-20201013
Nitrate as N
9056A
96
J
ug/L
0100174-03
MW-06-20201013
Sulfate
9056A
830
J
ug/L
0100174-03
MW-06-20201013
Biochemical Oxygen Demand
SM5210 B
280
J
ug/L
0100174-03
MW-06-20201013
pH
SM4500-H B
7.1
HT
pH Units
0100174-03
MW-06-20201013
Temperature
SM2550 B
20.0
HT
°C
0100174-03
MW-06-20201013
Total Alkalinity to pH 4.5
SM2320 B
24000
ug/L
0100174-03
MW-06-20201013
beta-BHC
8081B
0.14
DC
ug/L
0100174-03
MW-06-20201013
1,4-Dichlorobenzene
8270D
0.779
.1
pg/L
0100174-03
MW-06-20201013
Diethyl phthalate
8270D
0.709
J
pg/L
0100174-03
MW-06-20201013
Mercury
7470A
1.3
ug/L
0100174-03
MW-06-20201013
Barium
6020B
47
ug/L
0100174-03
MW-06-20201013
Cobalt
6020B
9.0
ug/L
0100174-03
MW-06-20201013
Nickel
6020B
3.4
ug/L
0100174-03
MW-06-20201013
Zinc
6020B
20
ug/L
0100174-03
MW-06-20201013
TOC
531OC-2011
1.04
mg/L
0100174-03
MW-06-20201013
1,1-Dichloroethane
8260D
1.4
ug/L
0100174-03
MW-06-20201013
1,4-Dichlorobenzene
8260D
2.6
ug/L
0100174-03
MW-06-20201013
Benzene
8260D
0.26
J
ug/L
0100174-03
MW-06-20201013
Chlorobenzene
8260D
0.41
J
ug/L
0100174-03
MW-06-20201013
cis-1,2-Dichloroethylene
8260D
1.4
ug/L
0100174-03
MW-06-20201013
m,p-Xylenes
8260D
0.37
.1
ug/L
0100174-03
MW-06-20201013
o-Xylene
8260D
0.29
J
ug/L
0100174-03
MW-06-20201013
Tetrachloroethylene
8260D
0.25
J
ug/L
0100174-03
MW-06-20201013
Xylenes, total
8260D
0.66
J
ug/L
0100174-04
TB-202010130000
Acetone
8260D
3.0
J
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 62
Laboratory Report
IL A i • . 0 12/31/2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-02-20201013
Attn: Alec Macbeth Sample ID: 0100174-01
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 14:50
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Anions by Ion Chromatography
Chloride
25000
ug/L
NE
1000
350
1
9056A
10/14/20 18:39BMS
POJ0250
Nitrate as N
170
J
ug/L
10000
200
45
1
9056A
10/14/20 18:39BMS
POJ0250
Sulfate
20000
ug/L
250000
2000
560
1
9056A
10/14/20 18:39BMS
POJ0250
Dissolved Metals
Mercury
<0.034
HA
ug/L
0.20
0.034
1
7470A
12/28/20 16:31MMR
POL0504
Antimony
<0.49
ug/L
2.0
0.49
1
6020B
12/30/20 22:3WAB
POL0558
Arsenic
<0.17
ug/L
1.0
0.17
1
6020B
12/30/20 22:30JAB
POL0558
Barium
24
ug/L
100
10
0.81
1
6020B
12/30/20 22:30JAB
POL0558
Beryllium
0.20
J
ug/L
1.0
0.19
1
6020B
12/30/20 22:30JAB
POL0558
Cadmium
<0.16
ug/L
1.0
0.16
1
6020B
12/30/20 22:30JAB
POL0558
Chromium
<0.79
ug/L
2.0
0.79
1
6020B
12/30/20 22:30JAB
POL0558
Cobalt
<0.52
ug/L
2.0
0.52
1
6020B
12/30/20 22:30JAB
POL0558
Copper
<3.8
ug/L
10
3.8
1
6020B
12/30/20 22:30JAB
POL0558
Lead
<0.26
ug/L
1.0
0.26
1
6020B
12/30/20 22:30JAB
POL0558
Nickel
0.81
J
ug/L
50
3.0
0.51
1
6020B
12/30/20 22:30JAB
POL0558
Selenium
1.3
J
ug/L
10
5.0
0.74
1
6020B
12/30/20 22:30JAB
POL0558
Silver
<0.11
ug/L
1.0
0.11
1
6020B
12/30/20 22:30JAB
POL0558
Thallium
<0.57
ug/L
2.0
0.57
1
6020B
12/30/20 22:30JAB
POL0558
Tin
<1.8
ug/L
5.0
1.8
1
6020B
12/30/20 22:30JAB
POL0558
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
12/30/20 22:30JAB
POL0558
Zinc
<6.9
ug/L
20
6.9
1
6020B
12/30/20 22:30JAB
POL0558
General Chemistry Parameters
Biochemical Oxygen Demand
2300
ug/L
NE
2000
210
1
SM5210 B
10/14/20 17:01 ENM
POJ0276
Chemical Oxygen Demand
37000
J
ug/L
NE
50000
11000
1
SM5220 D
10/19/20 11:56SLS
POJ0361
Cyanide
<0.014
mg/L
10
0.025
0.014
5
9014
10/20/20 12:30BMS
POJ0357
Ferrous Iron
<46
HT
ug/L
NE
200
46
1
SM3500-Fe B
10/15/20 9:51 ENM
POJ0282
pH
7.1
HT
pH Units
NE
1
SM4500-H B
12/18/20 11:30CLB
POL0392
Sulfide
<830
ug/L
1000
2000
830
1
SM4500-S F
10/19/20 11:02ENM
POJ0337
Temperature
20.5
HT
°C
1
SM2550 B
12/18/20 11:30CLB
POL0392
Total Alkalinity to pH 4.5
55000
ug/L
NE
5000
770
1
SM2320 B
10/19/20 11:40 CLB
POJ0341
Organochlorine Pesticides by GC/ECD
4,4'-DDD
<0.027
ug/L
0.1
0.10
0.027
1
8081 B
10/19/20 11:57NMB
POJ0286
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081 B
10/19/20 11:57NMB
POJ0286
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081 B
10/19/20 11:57NMB
POJ0286
Aldrin
<0.016
ug/L
0.05
0.052
0.016
1
8081 B
10/19/20 11:57NMB
POJ0286
alpha-BHC
<0.0065
ug/L
0.05
0.052
0.0065
1
8081 B
10/19/20 11:57NMB
POJ0286
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 62
Laboratory Report
A i • .0 12/31/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-02-20201013
Attn: Alec Macbeth Sample ID: 0100174-01
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 14:50
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/19/20 11:57NMB
POJ0286
beta-BHC
<0.011
ug/L
0.05
0.052
0.011
1
8081 B
10/19/20 11:57NMB
POJ0286
Chlordane
<0.19
ug/L
0.5
0.52
0.19
1
8081 B
10/19/20 11:57NMB
POJ0286
delta-BHC
<0.0085
ug/L
0.05
0.052
0.0085
1
8081 B
10/19/20 11:57NMB
POJ0286
Dieldrin
<0.014
ug/L
0.002
0.052
0.014
1
8081 B
10/19/20 11:57NMB
POJ0286
Endosulfan I
<0.016
ug/L
0.1
0.052
0.016
1
8081 B
10/19/20 11:57NMB
POJ0286
Endosulfan 11
<0.012
ug/L
0.1
0.052
0.012
1
8081 B
10/19/20 11:57NMB
POJ0286
Endosulfan Sulfate
<0.017
ug/L
0.1
0.052
0.017
1
8081 B
10/19/20 11:57NMB
POJ0286
Endrin
<0.014
ug/L
0.1
0.052
0.014
1
8081 B
10/19/20 11:57NMB
POJ0286
Endrin Aldehyde
<0.016
ug/L
0.1
0.052
0.016
1
8081 B
10/19/20 11:57NMB
POJ0286
Endrin Ketone
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/19/20 11:57NMB
POJ0286
gamma-BHC
<0.0063
ug/L
0.05
0.052
0.0063
1
8081 B
10/19/20 11:57NMB
POJ0286
trans -Chlordane
<0.024
ug/L
NE
0.10
0.024
1
8081 B
10/19/20 11:57NMB
POJ0286
Heptachlor
<0.013
ug/L
0.05
0.052
0.013
1
8081 B
10/19/20 11:57NMB
POJ0286
Heptachlor Epoxide
<0.023
ug/L
0.075
0.10
0.023
1
8081 B
10/19/20 11:57NMB
POJ0286
Methoxychlor
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/19/20 11:57NMB
POJ0286
Toxaphene
<0.36
ug/L
1.5
1.0
0.36
1
8081 B
10/19/20 11:57NMB
POJ0286
Surrogate
Recovery Control Limits
Decachlorobiphenyl
51 % 13-186
Tetrachloro-m-xylene
70 % 40-134
Polychlorinated Biphenyls (PCBs) by GC/ECD
Aroclor 1016
<0.22
ug/L
NE
0.52
0.22
1
8082A
10/19/20 11:57NMB
POJ0286
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1
8082A
10/19/20 11:57NMB
POJ0286
Aroclor 1232
<0.16
ug/L
NE
0.52
0.16
1
8082A
10/19/20 11:57NMB
POJ0286
Aroclor 1242
<0.14
ug/L
NE
0.52
0.14
1
8082A
10/19/20 11:57NMB
POJ0286
Aroclor 1248
<0.14
ug/L
NE
0.52
0.14
1
8082A
10/19/20 11:57NMB
POJ0286
Aroclor 1254
<0.16
ug/L
NE
0.52
0.16
1
8082A
10/19/20 11:57NMB
POJ0286
Aroclor 1260
<0.51
ug/L
NE
1.0
0.51
1
8082A
10/19/20 11:57NMB
POJ0286
Surrogate
Recovery Control Limits
Tetrachloro-m-xylene
68 % 30-161
Decachlorobiphenyl
53 % 32-178
Total Metals
Mercury
0.87
ug/L
0.2
0.20 0.034
1
7470A
10/20/20 15:26EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0 0.49
1
6020B
10/23/20 16:35JAB
POJ0239
Arsenic
7.5
ug/L
10
1.0 0.17
1
6020B
10/23/20 16:35JAB
POJ0239
Barium
250
ug/L
100
2.0 0.81
1
6020B
10/23/20 16:35JAB
POJ0239
Beryllium
1.6
ug/L
1
1.0 0.19
1
6020B
10/27/20 11:44JAB
POJ0239
Cadmium
<0.16
ug/L
1
1.0 0.16
1
6020B
10/23/20 16:35JAB
POJ0239
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 62
.
Laboratory Report
• �
Waynt.�
12/31/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID:
MW-02-20201013
Attn: Alec Macbeth
Sample ID: 0100174-01
231 Haywood Street
Project No.:
50-02
Work Order: 0100174
Asheville, NC 28801
Sample Matrix:
Water
Time Collected: 10/13/20 14:50
Time Submitted:
10/14/20 09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chromium
61
ug/L
10
2.0
0.79
1
6020B
10/23/20 16:35JAB
POJ0239
Cobalt
60
ug/L
10
2.0
0.52
1
6020B
10/23/20 16:35JAB
POJ0239
Copper
61
ug/L
10
10
3.8
1
6020B
10/23/20 16:35JAB
POJ0239
Lead
14
ug/L
10
1.0
0.26
1
6020B
10/23/20 16:35JAB
POJ0239
Nickel
44
ug/L
50
3.0
0.51
1
6020B
10/23/20 16:35JAB
POJ0239
Selenium
42
ug/L
10
5.0
0.74
1
6020B
10/23/20 16:35JAB
POJ0239
Silver
0.11
J ug/L
10
1.0
0.11
1
6020B
10/27/20 18:40JAB
POJ0490
Thallium
0.96
J ug/L
5.5
2.0
0.38
1
6020B
10/23/20 16:35JAB
POJ0239
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/23/20 16:35JAB
POJ0239
Vanadium
71
ug/L
25
5.0
1.3
1
6020B
10/23/20 16:35JAB
POJ0239
Zinc
140
ug/L
10
20
6.9
1
6020B
10/23/20 16:35JAB
POJ0239
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 19:09JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 19:09JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 19:09JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 19:09JLB
POJ0321
1,1-Dichloroethane
0.29
J ug/L
5
0.50
0.083
1
8260D
10/21/20 19:09JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 19:09JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 19:09JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 19:09JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 19:09JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 19:09JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 19:09JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 19:09JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 19:09JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 19:09JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 19:09JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 19:09JLB
POJ0321
1,4-Dichlorobenzene
<0.050
ug/L
1
0.50
0.050
1
8260D
10/21/20 19:09JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 19:09JLB
POJ0321
Acetone
<0.31
ug/L
100
5.0
0.31
1
8260D
10/21/20 19:09JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 19:09JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 19:09JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 19:09JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 19:09JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 19:09JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 19:09JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 19:09JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 62
Laboratory Report
A i • .0 12/31/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-02-20201013
Attn: Alec Macbeth Sample ID: 0100174-01
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 14:50
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 19:09JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 19:09JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 19:09JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 19:09JLB
POJ0321
Chlorobenzene
<0.062
ug/L
3
0.50
0.062
1
8260D
10/21/20 19:09JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 19:09JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 19:09JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 19:09JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 19:09JLB
POJ0321
cis-1,2-Dichloroethylene
0.38 J
ug/L
2
0.50
0.056
1
8260D
10/21/20 19:09JLB
POJ0321
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 19:09JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 19:09JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 19:09JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 19:09JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 19:09JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 19:09JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 19:09JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 19:09JLB
POJ0321
m,p-Xylenes
0.21 J
ug/L
NE
1.0
0.12
1
8260D
10/21/20 19:09JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 19:09JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 19:09JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 19:09JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 19:09JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 19:09JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 19:09JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 19:09JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 19:09JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 19:09JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 19:09JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 19:09JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 19:09JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 19:09JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 19:09JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 19:09JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 19:09JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 19:09JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 19:09JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 62
.
Laboratory Report
• �
Waynt.�
12/31/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID:
MW-02-20201013
Attn: Alec Macbeth
Sample ID: 0100174-01
231 Haywood Street
Project No.:
50-02
Work
Order: 0100174
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/13/20 14:50
Time
Submitted: 10/14/20
09:10
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 19:09JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 19:09JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 19:09JLB
POJ0321
Xylenes, total
0.21
J ug/L
5
1.5
0.15
1
8260D
10/21/20 19:09JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
101
% 80-124
Dibromofluoromethane
107
% 75-129
Toluene-d8
99 % 77-123
Volatile Organic Compounds by GUMS
SIM
1,4-Dioxane
2.8
ug/L
10
2.0
0.14
1
8260D SIM
10/16/20 21:38ANG
POJ0316
8270 Extended List
1,3,5-Trinitrobenzene
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29
L517325
1,4-Naphthoqu!none
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
1-Naphthylamine
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
2-Acetylaminofluorene
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29 BGV
L517325
2-Naphthylamine
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29 BGV
L517325
3-Methylcholanthrene
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29 BGV
L517325
4-Aminobiphenyl
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
5-Nitro-o-toluidine
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
7,12-Dimethyl benz(a)anthrace ne
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
Diallate
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
Hexachloropropene
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
Isosafrole
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
Kepone
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29 BGV
L517325
Methapyrilene
U
Ng/L
20.6
10.3
1
8270D
10/20/20 18:29BGV
L517325
N-Nitrosomethylethylamine
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
N-Nitrosopiperidine
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
N-Nitrosopyrrolidine
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
o-Toluidine
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29 BGV
L517325
p-Dimethylaminoazobenzene
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
p-Phenylenediamine
U
L Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
Pronamide
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29BGV
L517325
Safrole
U
Ng/L
10.3
10.3
1
8270D
10/20/20 18:29 BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
U
Ng/L
0.03
0.01002
1
8151A
10/21/20 0:42 VIC
L517362
2,4,5-TP (Silvex)
U
Ng/L
0.1
0.01634
1
8151A
10/21/20 0:42 VIC
L517362
2,4-D
U
Ng/L
0.25
0.2078
1
8151A
10/21/20 0:42 VIC
L517362
2,4-DB
U
Ng/L
0.1
0.1364
1
8151A
10/21/20 0:42 VIC
L517362
Dalapon
U
Ng/L
0.55
0.5149
1
8151A
10/21/20 0:42 VIC
L517362
Dicamba
U
Ng/L
0.1
0.057
1
8151A
10/21/20 0:42 VIC
L517362
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 62
.
Laboratory Report
• �
Waynt.�
12/31/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID: MW-02-20201013
Attn: Alec Macbeth
Sample ID: 0100174-01
231 Haywood Street
Project No.: 50-02
Work Order: 0100174
Asheville, NC 28801
Sample Matrix: Water
Time Collected: 10/13/20 14:50
Time Submitted: 10/14/20 09:10
Parameter
Result Units SWSL
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
Dichlorprop
U
Ng/L
0.1
0.07959
1 8151A 10/21/20 0:42 VIC
L517362
Dinoseb
U
Ng/L
0.1
0.02698
1 8151A 10/21/20 0:42 VIC
L517362
MCPA
U
Ng/L
50
18.98
1 8151A 10/21/20 0:42 VIC
L517362
MCPP
U
Ng/L
50
11.75
1 8151A 10/21/20 0:42 VIC
L517362
Picloram
U
Ng/L
0.1
0.04528
1 8151A 10/21/20 0:42 VIC
L517362
Surrogate
Recovery Control Limits
DCAA
66.2 % 20-150
Semivolatile Organic Compounds - GC/MS
1,2,4,5-Tetrachlorobenzene
U
Ng/L
5.15
0.326
1
8270D
10/20/20 18:29BGV
L517328
1,2,4-Trichlorobenzene
U
Ng/L
5.15
0.496
1
8270D
10/20/20 18:29BGV
L517328
1,2-Dichlorobenzene
U
Ng/L
5.15
0.647
1
8270D
10/20/20 18:29BGV
L517328
1,3-Dichlorobenzene
U
pg/L
5.15
0.505
1
8270D
10/20/20 18:29BGV
L517328
1,4-Dichlorobenzene
U
Ng/L
5.15
0.597
1
8270D
10/20/20 18:29BGV
L517328
2,3,4,6-Tetrachlorophenol
U
Ng/L
5.15
0.365
1
8270D
10/20/20 18:29 BGV
L517328
2,4,5-Trichlorophenol
U
Ng/L
5.15
0.36
1
8270D
10/20/20 18:29 BGV
L517328
2,4,6-Trichlorophenol
U
Ng/L
5.15
0.354
1
8270D
10/20/20 18:29 BGV
L517328
2,4-Dichlorophenol
U
Ng/L
5.15
1.57
1
8270D
10/20/20 18:29BGV
L517328
2,4-Dimethylphenol
U
Ng/L
5.15
0.694
1
8270D
10/20/20 18:29BGV
L517328
2,4-Dinitrophenol
U
Ng/L
10.3
5
1
8270D
10/20/20 18:29BGV
L517328
2,4-Dinitrotoluene
U
Ng/L
5.15
0.415
1
8270D
10/20/20 18:29BGV
L517328
2,6-Dichlorophenol
U
Ng/L
5.15
0.724
1
8270D
10/20/20 18:29BGV
L517328
2,6-Dinitrotoluene
U
Ng/L
5.15
0.425
1
8270D
10/20/20 18:29BGV
L517328
2-Chloronaphthalene
U
Ng/L
5.15
0.49
1
8270D
10/20/20 18:29BGV
L517328
2-Chlorophenol
U
Ng/L
5.15
0.758
1
8270D
10/20/20 18:29BGV
L517328
2-Methyl naphthalene
U
Ng/L
2.06
0.499
1
8270D
10/20/20 18:29BGV
L517328
2-Methylphenol
U
Ng/L
5.15
0.742
1
8270D
10/20/20 18:29BGV
L517328
2-Nitroaniline
U
Ng/L
5.15
0.591
1
8270D
10/20/20 18:29BGV
L517328
2-Nitrophenol
U
Ng/L
5.15
0.624
1
8270D
10/20/20 18:29 BGV
L517328
3&4 Methylphenol
U
Ng/L
5.15
0.711
1
8270D
10/20/20 18:29BGV
L517328
3,3' Dimethylbenzidine
U
Ng/L
10.3
1.94
1
8270D
10/20/20 18:29 BGV
L517328
3,3'-Dichlorobenzidine
U
Ng/L
10.3
3.85
1
8270D
10/20/20 18:29BGV
L517328
3-Nitroaniline
U
Ng/L
10.3
1.58
1
8270D
10/20/20 18:29BGV
L517328
4,6-Dinitro-2-methylphenol
U
Ng/L
10.3
3.57
1
8270D
10/20/20 18:29BGV
L517328
4-Bromophenyl phenyl ether
U
Ng/L
5.15
0.515
1
8270D
10/20/20 18:29BGV
L517328
4-Chloro-3-methylphenol
U
Ng/L
5.15
0.518
1
8270D
10/20/20 18:29BGV
L517328
4-Chloroaniline
U
Ng/L
5.15
0.541
1
8270D
10/20/20 18:29BGV
L517328
4-Chlorophenyl phenyl ether
U
Ng/L
5.15
0.493
1
8270D
10/20/20 18:29 BGV
L517328
4-Nitroaniline
U
Ng/L
5.15
0.762
1
8270D
10/20/20 18:29BGV
L517328
4-Nitrophenol
U
Ng/L
10.3
1.43
1
8270D
10/20/20 18:29 BGV
L517328
Acenaphthene
U
Ng/L
2.06
0.434
1
8270D
10/20/20 18:29 BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 62
® Laboratory Report
IL AL i • . 12/31 /2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-02-20201013
Attn: Alec Macbeth Sample ID: 0100174-01
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 14:50
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Acenaphthylene
U
pg/L
2.06
0.441
1
8270D
10/20/20 18:29BGV
L517328
Acetophenone
U
pg/L
5.15
0.706
1
8270D
10/20/20 18:29BGV
L517328
Aniline
U
pg/L
5.15
0.325
1
8270D
10/20/20 18:29BGV
L517328
Anthracene
U
pg/L
2.06
0.481
1
8270D
10/20/20 18:29BGV
L517328
Benzidine
U
pg/L
20.6
0.709
1
8270D
10/20/20 18:29BGV
L517328
Benzo(a)anthracene
U
pg/L
2.06
0.439
1
8270D
10/20/20 18:29BGV
L517328
Benzo(a)pyrene
U
pg/L
2.06
1.03
1
8270D
10/20/20 18:29BGV
L517328
Benzo(b)fluoranthene
U
pg/L
2.06
0.969
1
8270D
10/20/20 18:29BGV
L517328
Benzo(g,hJ)perylene
U
pg/L
2.06
1.4
1
8270D
10/20/20 18:29BGV
L517328
Benzo(k)fluoranthene
U
pg/L
2.06
0.774
1
8270D
10/20/20 18:29BGV
L517328
Benzoic Acid
U
pg/L
10.3
5.15
1
8270D
10/20/20 18:29 BGV
L517328
Benzyl alcohol
U
pg/L
10.3
3.1
1
8270D
10/20/20 18:29BGV
L517328
Bis(2-Chloroethoxy)methane
U
pg/L
5.15
0.445
1
8270D
10/20/20 18:29BGV
L517328
Bis(2-Chloroethyl)ether
U
pg/L
5.15
0.46
1
8270D
10/20/20 18:29BGV
L517328
Bis(2-Chloroisopropyl)ether
U
pg/L
5.15
0.562
1
8270D
10/20/20 18:29BGV
L517328
Bis(2-ethylhexyl)phthalate
U
pg/L
5.15
3.77
1
8270D
10/20/20 18:29BGV
L517328
Butyl benzyl phthalate
U
pg/L
5.15
4.73
1
8270D
10/20/20 18:29BGV
L517328
Carbazole
U
pg/L
5.15
0.49
1
8270D
10/20/20 18:29BGV
L517328
Chrysene
U
pg/L
2.06
0.752
1
8270D
10/20/20 18:29BGV
L517328
Dibenz(a,h)anthracene
U
pg/L
2.06
0.259
1
8270D
10/20/20 18:29BGV
L517328
Dibenzofuran
U
pg/L
5.15
0.435
1
8270D
10/20/20 18:29BGV
L517328
Diethyl phthalate
4.65 j
pg/L
5.15
0.602
1
8270D
10/20/20 18:29BGV
L517328
Dimethyl phthalate
U
pg/L
5.15
0.525
1
8270D
10/20/20 18:29BGV
L517328
Di-n-butyl phthalate
U
pg/L
5.15
1.62
1
8270D
10/20/20 18:29BGV
L517328
Di-n-Octyl Phthalate
U
pg/L
5.15
1.77
1
8270D
10/20/20 18:29BGV
L517328
Fluoranthene
U
pg/L
2.06
0.418
1
8270D
10/20/20 18:29BGV
L517328
Fluorene
U
pg/L
2.06
0.457
1
8270D
10/20/20 18:29BGV
L517328
Hexachlorobenzene
U
pg/L
5.15
2.65
1
8270D
10/20/20 18:29BGV
L517328
Hexachlorobutadiene
U
pg/L
5.15
0.417
1
8270D
10/20/20 18:29BGV
L517328
Hexachlorocyclopentadiene
U
pg/L
5.15
2.41
1
8270D
10/20/20 18:29BGV
L517328
Hexachloroethane
U
pg/L
5.15
0.285
1
8270D
10/20/20 18:29BGV
L517328
Indeno(1,2,3-cd)pyrene
U
pg/L
2.06
1.04
1
8270D
10/20/20 18:29BGV
L517328
Isophorone
U
pg/L
5.15
0.37
1
8270D
10/20/20 18:29BGV
L517328
Naphthalene
U
pg/L
2.06
0.498
1
8270D
10/20/20 18:29BGV
L517328
Nitrobenzene
U
pg/L
5.15
0.546
1
8270D
10/20/20 18:29BGV
L517328
N-Nitrosodiethylamine
U
pg/L
5.15
0.412
1
8270D
10/20/20 18:29BGV
L517328
N-Nitrosodimethylamine
U
pg/L
5.15
0.256
1
8270D
10/20/20 18:29BGV
L517328
N-Nitroso-di-n-butylamine
U
pg/L
5.15
0.774
1
8270D
10/20/20 18:29BGV
L517328
N-Nitroso-di-n-propylamine
U
pg/L
5.15
0.344
1
8270D
10/20/20 18:29BGV
L517328
N-Nitrosodiphenylamine
U
pg/L
10.3
0.806
1
8270D
10/20/20 18:29BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 62
Laboratory Report
• � 12/31/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-02-20201013
Attn: Alec Macbeth Sample ID: 0100174-01
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 14:50
Time Submitted: 10/14/20 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pentachlorophenol U Ng/L
Phenanthrene U Ng/L
Phenol U Ng/L
Pyrene U Ng/L
Pyridine U ua/L
Total Organic Carbon
TOC 2.26 mg/L
10.3
2.52
1
8270D
10/20/20 18:29BGV
L517328
2.06
0.477
1
8270D
10/20/20 18:29BGV
L517328
5.15
0.4
1
8270D
10/20/20 18:29BGV
L517328
2.06
1.07
1
8270D
10/20/20 18:29BGV
L517328
10.3
0.698
1
8270D
10/20/20 18:29BGV
L517328
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
21.5 %
39-110 SR
2-Fluorobiphenyl
42.3 %
24-93
2-Fluorophenol
8.3 %
10-44 SR
4-Terphenyl-d14
13.3 %
35-126 SR
Nitrobenzene-d5
45.4 %
20-91
Phenol-d6
8.3 %
7-32
1 0.498 1 531OC-2011 10/22/20 2:13 DDB L517921
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 62
Laboratory Report
• � 12/31/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-03-20201013
Attn: Alec Macbeth Sample ID: 0100174-02
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 10:29
Time Submitted: 10/14/20 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Anions by Ion Chromatography
Chloride 8500
ug/L NE 1000 350 1 9056A 10/14/20 18:23BMS POJ0250
Nitrate as N 8300
ug/L 10000 200 45 1 9056A 10/14/20 18:23BMS POJ0250
Sulfate 4000
ug/L 250000 2000 560 1 9056A 10/14/20 18:23BMS POJ0250
General Chemistry Parameters
Biochemical Oxygen Demand 2000
Chemical Oxygen Demand 35000
Cyanide <0.014
Ferrous Iron <46
pH 8.1
Sulfide <830
Temperature 20.3
Total Alkalinity to pH 4.5 140000
Organochlorine Pesticides by GC/ECD
DD
J
HT
HT
HT
ug/L
ug/L
mg/L
ug/L
pH Units
ug/L
°C
ug/L
NE
NE
10
NE
NE
1000
NE
2000
50000
0.025
200
2000
5000
210
11000
0.014
46
830
770
1
1
5
1
1
1
1
1
SM5210 B
SM5220 D
9014
SM3500-Fe B
SM4500-H B
SM4500-S F
SM2550 B
SM2320 B
10/14/20 17:01 ENM
10/19/20 11:56SLS
10/20/20 12:30BMS
10/15/20 9:51 ENM
12/18/20 11:30CL13
10/19/20 11:02ENM
12/18/20 11:30CL13
10/19/20 11:40 CLB
POJ0276
POJ0361
POJ0357
POJ0282
POL0392
POJ0337
POL0392
POJ0341
4,4'-DDD
<0.027
ug/L
0.1
0.10
0.027
1
8081 B
10/19/20 12:10NMB
POJ0286
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081 B
10/19/20 12:10NMB
POJ0286
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081 B
10/19/20 12:10NMB
POJ0286
Aldrin
<0.015
ug/L
0.05
0.051
0.015
1
8081 B
10/19/20 12:10NMB
POJ0286
alpha-BHC
<0.0064
ug/L
0.05
0.051
0.0064
1
8081 B
10/19/20 12:10NMB
POJ0286
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/19/20 12:10NMB
POJ0286
beta-BHC
<0.011
ug/L
0.05
0.051
0.011
1
8081 B
10/19/20 12:10NMB
POJ0286
Chlordane
<0.18
ug/L
0.5
0.51
0.18
1
8081 B
10/19/20 12:10NMB
POJ0286
delta-BHC
<0.0083
ug/L
0.05
0.051
0.0083
1
8081 B
10/19/20 12:10NMB
POJ0286
Dieldrin
<0.014
ug/L
0.002
0.051
0.014
1
8081 B
10/19/20 12:10NMB
POJ0286
Endosulfan 1
<0.016
ug/L
0.1
0.051
0.016
1
8081 B
10/19/20 12:10NMB
POJ0286
Endosulfan 11
<0.012
ug/L
0.1
0.051
0.012
1
8081 B
10/19/20 12:10NMB
POJ0286
Endosulfan Sulfate
<0.017
ug/L
0.1
0.051
0.017
1
8081 B
10/19/20 12:10NMB
POJ0286
Endrin
<0.014
ug/L
0.1
0.051
0.014
1
8081 B
10/19/20 12:10NMB
POJ0286
Endrin Aldehyde
<0.016
ug/L
0.1
0.051
0.016
1
8081 B
10/19/20 12:10NMB
POJ0286
Endrin Ketone
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/19/20 12:10NMB
POJ0286
gamma-BHC
<0.0062
ug/L
0.05
0.051
0.0062
1
8081 B
10/19/20 12:10NMB
POJ0286
trans -Chlordane
<0.023
ug/L
NE
0.10
0.023
1
8081 B
10/19/20 12:10NMB
POJ0286
Heptachlor
<0.013
ug/L
0.05
0.051
0.013
1
8081 B
10/19/20 12:10NMB
POJ0286
Heptachlor Epoxide
<0.023
ug/L
0.075
0.10
0.023
1
8081 B
10/19/20 12:10NMB
POJ0286
Methoxychlor
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/19/20 12:10NMB
POJ0286
Toxaphene
<0.35
ug/L
1.5
1.0
0.35
1
8081 B
10/19/20 12:10NMB
POJ0286
Surrogate
Recovery Control Limits
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 62
Laboratory Report
• � 12/31/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-03-20201013
Attn: Alec Macbeth Sample ID: 0100174-02
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 10:29
Time Submitted: 10/14/20 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Decachlorobiphenyl 58 % 13-186
Tetrachloro-m-xylene 67 % 40-134
Polychlorinated Biphenyls (PCBs) by GC/ECD
Aroclor 1016
<0.21
ug/L
NE
0.51
0.21
1
8082A
10/19/20 12:10NMB
POJ0286
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1
8082A
10/19/20 12:10NMB
POJ0286
Aroclor 1232
<0.16
ug/L
NE
0.51
0.16
1
8082A
10/19/20 12:10NMB
POJ0286
Aroclor 1242
<0.14
ug/L
NE
0.51
0.14
1
8082A
10/19/20 12:10NMB
POJ0286
Aroclor 1248
<0.14
ug/L
NE
0.51
0.14
1
8082A
10/19/20 12:10NMB
POJ0286
Aroclor 1254
<0.16
ug/L
NE
0.51
0.16
1
8082A
10/19/20 12:10NMB
POJ0286
Aroclor 1260
<0.50
ug/L
NE
1.0
0.50
1
8082A
10/19/20 12:10NMB
POJ0286
Total Metals
Surrogate
Recovery Control Limits
Tetrachloro-m-xylene 65 % 30-161
Decachlorobiphenyl 60 % 32-178
Mercury
1.1
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 15:30EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/23/20 16:42JAB
POJ0239
Arsenic
0.31
J
ug/L
10
1.0
0.17
1
6020B
10/23/20 16:42JAB
POJ0239
Barium
110
ug/L
100
2.0
0.81
1
6020B
10/23/20 16:42JAB
POJ0239
Beryllium
<0.19
CCV
ug/L
1
1.0
0.19
1
6020B
10/23/20 17:37JAB
POJ0239
Cadmium
<0.16
ug/L
1
1.0
0.16
1
6020B
10/23/20 16:42JAB
POJ0239
Chromium
0.86
J
ug/L
10
2.0
0.79
1
6020B
10/23/20 16:42JAB
POJ0239
Cobalt
0.59
J
ug/L
10
2.0
0.52
1
6020B
10/23/20 16:42JAB
POJ0239
Copper
3.8
J
ug/L
10
10
3.8
1
6020B
10/23/20 16:42JAB
POJ0239
Lead
<0.26
ug/L
10
1.0
0.26
1
6020B
10/23/20 16:42JAB
POJ0239
Nickel
0.96
J
ug/L
50
3.0
0.51
1
6020B
10/23/20 16:42JAB
POJ0239
Selenium
<0.74
ug/L
10
5.0
0.74
1
6020B
10/23/20 16:42JAB
POJ0239
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 18:46JAB
POJ0490
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/23/20 16:42JAB
POJ0239
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/23/20 16:42JAB
POJ0239
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/23/20 16:42JAB
POJ0239
Zinc
<6.9
ug/L
10
20
6.9
1
6020B
10/23/20 16:42JAB
POJ0239
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 19:43JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 19:43JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 19:43JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 19:43JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 19:43JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 19:43JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 62
Laboratory Report
A i • .0 12/31/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-03-20201013
Attn: Alec Macbeth Sample ID: 0100174-02
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 10:29
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 19:43JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 19:43JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 19:43JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 19:43JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 19:43JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 19:43JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 19:43JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 19:43JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 19:43JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 19:43JLB
POJ0321
1,4-Dichlorobenzene
<0.050
ug/L
1
0.50
0.050
1
8260D
10/21/20 19:43JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 19:43JLB
POJ0321
Acetone
<0.31
ug/L
100
5.0
0.31
1
8260D
10/21/20 19:43JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 19:43JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 19:43JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 19:43JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 19:43JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 19:43JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 19:43JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 19:43JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 19:43JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 19:43JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 19:43JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 19:43JLB
POJ0321
Chlorobenzene
<0.062
ug/L
3
0.50
0.062
1
8260D
10/21/20 19:43JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 19:43JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 19:43JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 19:43JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 19:43JLB
POJ0321
cis- 1,2-Dichloroethylene
<0.056
ug/L
2
0.50
0.056
1
8260D
10/21/20 19:43JLB
POJ0321
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 19:43JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 19:43JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 19:43JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 19:43JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 19:43JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 19:43JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 19:43JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 62
Laboratory Report
A i • .0 12/31/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-03-20201013
Attn: Alec Macbeth Sample ID: 0100174-02
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 10:29
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 19:43JLB
POJ0321
m,p-Xylenes
0.37 J
ug/L
NE
1.0
0.12
1
8260D
10/21/20 19:43JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 19:43JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 19:43JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 19:43JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 19:43JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 19:43JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 19:43JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 19:43JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 19:43JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 19:43JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 19:43JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 19:43JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 19:43JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 19:43JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 19:43JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 19:43JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 19:43JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 19:43JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 19:43JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 19:43JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 19:43JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 19:43JLB
POJ0321
Xylenes, total
0.37 J
ug/L
5
1.5
0.15
1
8260D
10/21/20 19:43JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
101 % 80-124
Dibromofluoromethane
110 % 75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/16/20 22:03ANG
POJ0316
8270 Extended List
1,3,5-Trinitrobenzene
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
1,4-Naphthoquinone
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
1-Naphthylamine
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
2-Acetylaminofluorene
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
2-Naphthylamine
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
3-Methylcholanthrene
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
4-Aminobiphenyl
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 62
Laboratory Report
A i • .0 12/31/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-03-20201013
Attn: Alec Macbeth Sample ID: 0100174-02
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 10:29
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
5-Nitro-o-toluidine
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
7,12-D1methyl benz(a)anthrace ne
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
Diallate
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
Hexachloropropene
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
Isosafrole
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
Kepone
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
Methapyrilene
U
Ng/L
20.2
10.1
1
8270D
10/20/20 18:51 BGV
L517325
N-Nitrosomethylethylamine
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
N-Nitrosopiperidine
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
N-Nitrosopyrrolidine
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
o-Toluidine
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
p-Dimethylaminoazobenzene
U
pg/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
p-Phenylenediamine
U L
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
Pronamide
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
Safrole
U
Ng/L
10.1
10.1
1
8270D
10/20/20 18:51 BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
U
Ng/L
0.03
0.01002
1
8151A
10/20/20 23:51 VIC
L517362
2,4,5-TP (Silvex)
U
Ng/L
0.1
0.01634
1
8151A
10/20/20 23:51 VIC
L517362
2,4-D
U
Ng/L
0.25
0.2078
1
8151A
10/20/20 23:51 VIC
L517362
2,4-DB
U
Ng/L
0.1
0.1364
1
8151A
10/20/20 23:51 VIC
L517362
Dalapon
U
Ng/L
0.55
0.5149
1
8151A
10/20/20 23:51 VIC
L517362
Dicamba
U
Ng/L
0.1
0.057
1
8151A
10/20/20 23:51 VIC
L517362
Dichlorprop
U
Ng/L
0.1
0.07959
1
8151A
10/20/20 23:51 VIC
L517362
Dinoseb
U
Ng/L
0.1
0.02698
1
8151A
10/20/20 23:51 VIC
L517362
MCPA
U
Ng/L
50
18.98
1
8151A
10/20/20 23:51 VIC
L517362
MCPP
U
Ng/L
50
11.75
1
8151A
10/20/20 23:51 VIC
L517362
Picloram
U
Ng/L
0.1
0.04528
1
8151A
10/20/20 23:51 VIC
L517362
Surrogate
Recovery Control Limits
DCAA
57.5 % 20-150
Semivolatile Organic Compounds - GC/MS
1,2,4,5-Tetrachlorobenzene
U
Ng/L
5.05
0.32
1
8270D
10/20/20 18:51 BGV
L517328
1,2,4-Trichlorobenzene
U
Ng/L
5.05
0.486
1
8270D
10/20/20 18:51 BGV
L517328
1,2-Dichlorobenzene
0.843 j
Ng/L
5.05
0.635
1
8270D
10/20/20 18:51 BGV
L517328
1,3-Dichlorobenzene
0.791 j
Ng/L
5.05
0.495
1
8270D
10/20/20 18:51 BGV
L517328
1,4-Dichlorobenzene
0.746 j
Ng/L
5.05
0.585
1
8270D
10/20/20 18:51 BGV
L517328
2,3,4,6-Tetrachlorophenol
U
Ng/L
5.05
0.358
1
8270D
10/20/20 18:51 BGV
L517328
2,4,5-Trichlorophenol
U
Ng/L
5.05
0.353
1
8270D
10/20/20 18:51 BGV
L517328
2,4,6-Trichlorophenol
U
Ng/L
5.05
0.347
1
8270D
10/20/20 18:51 BGV
L517328
2,4-Dichlorophenol
U
Ng/L
5.05
1.54
1
8270D
10/20/20 18:51 BGV
L517328
2,4-Dimethylphenol
U
Ng/L
5.05
0.68
1
8270D
10/20/20 18:51 BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 62
® Laboratory Report
IL AL i • . 12/31 /2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-03-20201013
Attn: Alec Macbeth Sample ID: 0100174-02
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 10:29
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
2,4-Dinitrophenol
U
pg/L
10.1
4.9
1
8270D
10/20/20 18:51 BGV
L517328
2,4-Dinitrotoluene
U
pg/L
5.05
0.407
1
8270D
10/20/20 18:51 BGV
L517328
2,6-Dichlorophenol
U
pg/L
5.05
0.71
1
8270D
10/20/20 18:51 BGV
L517328
2,6-Dinitrotoluene
U
pg/L
5.05
0.417
1
8270D
10/20/20 18:51 BGV
L517328
2-Chloronaphthalene
U
pg/L
5.05
0.48
1
8270D
10/20/20 18:51 BGV
L517328
2-Chlorophenol
U
pg/L
5.05
0.743
1
8270D
10/20/20 18:51 BGV
L517328
2-Methyl naphthalene
U
pg/L
2.02
0.489
1
8270D
10/20/20 18:51 BGV
L517328
2-Methylphenol
U
pg/L
5.05
0.728
1
8270D
10/20/20 18:51 BGV
L517328
2-Nitroaniline
U
pg/L
5.05
0.579
1
8270D
10/20/20 18:51 BGV
L517328
2-Nitrophenol
U
pg/L
5.05
0.612
1
8270D
10/20/20 18:51 BGV
L517328
3&4 Methylphenol
U
pg/L
5.05
0.697
1
8270D
10/20/20 18:51 BGV
L517328
3,3' Dimethylbenzidine
U
pg/L
10.1
1.9
1
8270D
10/20/20 18:51 BGV
L517328
3,3'-Dichlorobenzidine
U
pg/L
10.1
3.78
1
8270D
10/20/20 18:51 BGV
L517328
3-Nitroaniline
U
pg/L
10.1
1.55
1
8270D
10/20/20 18:51 BGV
L517328
4,6-Dinitro-2-methylphenol
U
pg/L
10.1
3.5
1
8270D
10/20/20 18:51 BGV
L517328
4-Bromophenyl phenyl ether
U
pg/L
5.05
0.505
1
8270D
10/20/20 18:51 BGV
L517328
4-Chloro-3-methylphenol
U
pg/L
5.05
0.508
1
8270D
10/20/20 18:51 BGV
L517328
4-Chloroaniline
U
pg/L
5.05
0.531
1
8270D
10/20/20 18:51 BGV
L517328
4-Chlorophenyl phenyl ether
U
pg/L
5.05
0.483
1
8270D
10/20/20 18:51 BGV
L517328
4-Nitroaniline
U
pg/L
5.05
0.747
1
8270D
10/20/20 18:51 BGV
L517328
4-Nitrophenol
U
pg/L
10.1
1.4
1
8270D
10/20/20 18:51 BGV
L517328
Acenaphthene
U
pg/L
2.02
0.426
1
8270D
10/20/20 18:51 BGV
L517328
Acenaphthylene
U
pg/L
2.02
0.433
1
8270D
10/20/20 18:51 BGV
L517328
Acetophenone
U
pg/L
5.05
0.692
1
8270D
10/20/20 18:51 BGV
L517328
Aniline
U
pg/L
5.05
0.319
1
8270D
10/20/20 18:51 BGV
L517328
Anthracene
U
pg/L
2.02
0.471
1
8270D
10/20/20 18:51 BGV
L517328
Benzidine
U
pg/L
20.2
0.695
1
8270D
10/20/20 18:51 BGV
L517328
Benzo(a)anthracene
U
pg/L
2.02
0.431
1
8270D
10/20/20 18:51 BGV
L517328
Benzo(a)pyrene
U
pg/L
2.02
1.01
1
8270D
10/20/20 18:51 BGV
L517328
Benzo(b)fluoranthene
U
pg/L
2.02
0.95
1
8270D
10/20/20 18:51 BGV
L517328
Benzo(q,hJ)perylene
U
pg/L
2.02
1.37
1
8270D
10/20/20 18:51 BGV
L517328
Benzo(k)fluoranthene
U
pg/L
2.02
0.759
1
8270D
10/20/20 18:51 BGV
L517328
Benzoic Acid
U
pg/L
10.1
5.05
1
8270D
10/20/20 18:51 BGV
L517328
Benzyl alcohol
U
pg/L
10.1
3.04
1
8270D
10/20/20 18:51 BGV
L517328
Bis(2-Chloroethoxy)methane
U
pg/L
5.05
0.437
1
8270D
10/20/20 18:51 BGV
L517328
Bis(2-Chloroethyl)ether
U
pg/L
5.05
0.451
1
8270D
10/20/20 18:51 BGV
L517328
Bis(2-Chloroisopropyl)ether
U
pg/L
5.05
0.551
1
8270D
10/20/20 18:51 BGV
L517328
Bis(2-ethylhexyl)phthalate
U
pg/L
5.05
3.7
1
8270D
10/20/20 18:51 BGV
L517328
Butyl benzyl phthalate
U
pg/L
5.05
4.64
1
8270D
10/20/20 18:51 BGV
L517328
Carbazole
U
pg/L
5.05
0.48
1
8270D
10/20/20 18:51 BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 62
.
Laboratory Report
• �
Waynt.�
12/31/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID: MW-03-20201013
Attn: Alec Macbeth
Sample ID: 0100174-02
231 Haywood Street
Project No.: 50-02
Work
Order: 0100174
Asheville, NC 28801
Sample Matrix: Water
Time
Collected: 10/13/20 10:29
Time
Submitted: 10/14/20 09:10
Parameter
Result
Units SWSL
Report
MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chrysene
U
Ng/L
2.02
0.738
1
8270D 10/20/20 18:51 BGV
L517328
D1benz(a,h)anthrace ne
U
Ng/L
2.02
0.254
1
8270D 10/20/20 18:51 BGV
L517328
Dibenzofuran
U
Ng/L
5.05
0.427
1
8270D 10/20/20 18:51 BGV
L517328
Diethyl phthalate
U
Ng/L
5.05
0.59
1
8270D 10/20/20 18:51 BGV
L517328
Dimethyl phthalate
U
Ng/L
5.05
0.515
1
8270D 10/20/20 18:51 BGV
L517328
Di-n-butyl phthalate
U
Ng/L
5.05
1.59
1
8270D 10/20/20 18:51 BGV
L517328
Di-n-Octyl Phthalate
U
Ng/L
5.05
1.74
1
8270D 10/20/20 18:51 BGV
L517328
Fluoranthene
U
Ng/L
2.02
0.41
1
8270D 10/20/20 18:51 BGV
L517328
Fluorene
U
Ng/L
2.02
0.448
1
8270D 10/20/20 18:51 BGV
L517328
Hexachlorobenzene
U
Ng/L
5.05
2.6
1
8270D 10/20/20 18:51 BGV
L517328
Hexachlorobutadiene
U
Ng/L
5.05
0.409
1
8270D 10/20/20 18:51 BGV
L517328
Hexachlorocyclopentadiene
U
pg/L
5.05
2.36
1
8270D 10/20/20 18:51 BGV
L517328
Hexachloroethane
U
Ng/L
5.05
0.279
1
8270D 10/20/20 18:51 BGV
L517328
Indeno(1,2,3-cd)pyrene
U
Ng/L
2.02
1.02
1
8270D 10/20/20 18:51 BGV
L517328
Isophorone
U
Ng/L
5.05
0.363
1
8270D 10/20/20 18:51 BGV
L517328
Naphthalene
U
Ng/L
2.02
0.488
1
8270D 10/20/20 18:51 BGV
L517328
Nitrobenzene
U
Ng/L
5.05
0.536
1
8270D 10/20/20 18:51 BGV
L517328
N-Nitrosodiethylamine
U
Ng/L
5.05
0.404
1
8270D 10/20/20 18:51 BGV
L517328
N-Nitrosodimethylamine
U
Ng/L
5.05
0.251
1
8270D 10/20/20 18:51 BGV
L517328
N-Nitroso-di-n-butylamine
U
pg/L
5.05
0.759
1
8270D 10/20/20 18:51 BGV
L517328
N-Nitroso-di-n-propylamine
U
pg/L
5.05
0.337
1
8270D 10/20/20 18:51 BGV
L517328
N-Nitrosodiphenylamine
U
Ng/L
10.1
0.79
1
8270D 10/20/20 18:51 BGV
L517328
Pentachlorophenol
U
Ng/L
10.1
2.47
1
8270D 10/20/20 18:51 BGV
L517328
Phenanthrene
U
Ng/L
2.02
0.468
1
8270D 10/20/20 18:51 BGV
L517328
Phenol
U
pg/L
5.05
0.392
1
8270D 10/20/20 18:51 BGV
L517328
Pyrene
U
Ng/L
2.02
1.05
1
8270D 10/20/20 18:51 BGV
L517328
Pyridine
U
Ng/L
10.1
0.684
1
8270D 10/20/20 18:51 BGV
L517328
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
22.7 % 39-110
SR
2-Fluorobiphenyl
39.6 % 24-93
2-Fluorophenol
9.7 % 10-44
SR
4-Terphenyl-d14
16.4 % 35-126
SR
Nitrobenzene-d5
44.2 % 20-91
Phenol-d6
8.1 % 7-32
Total Organic Carbon
TOC
4.68
mg/L
1
0.498
1
531OC-2011 10/22/20 2:51 DDB
L517921
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 62
Laboratory Report
• � 12/31/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-06-20201013
Attn: Alec Macbeth Sample ID: 0100174-03
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 13:15
Time Submitted: 10/14/20 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Anions by Ion Chromatography
Chloride
1100
ug/L
NE
1000
350
1
9056A
10/14/20 17:36BMS
POJ0250
Nitrate as N
96
J
ug/L
10000
200
45
1
9056A
10/14/20 17:36BMS
POJ0250
Sulfate
830
J
ug/L
250000
2000
560
1
9056A
10/14/20 17:36BMS
POJ0250
General Chemistry Parameters
Biochemical Oxygen Demand
280
J
ug/L
NE
2000
210
1
SM5210 B
10/14/20 17:01 ENM
POJ0276
Chemical Oxygen Demand
<11000
ug/L
NE
50000
11000
1
SM5220 D
10/19/20 11:56SLS
POJ0361
Cyanide
<0.014
mg/L
10
0.025
0.014
5
9014
10/20/20 12:30BMS
POJ0357
Ferrous Iron
<46
HT
ug/L
NE
200
46
1
SM3500-Fe B
10/15/20 9:51 ENM
POJ0282
pH
7.1
HT
pH Units
NE
1
SM4500-H B
12/18/20 11:30CLB
POL0392
Sulfide
<830
ug/L
1000
2000
830
1
SM4500-S F
10/19/20 11:02ENM
POJ0337
Temperature
20.0
HT
°C
1
SM2550 B
12/18/20 11:30CLB
POL0392
Total Alkalinity to pH 4.5
24000
ug/L
NE
5000
770
1
SM2320 B
10/19/20 11:40 CLB
POJ0341
Organochlorine Pesticides by GC/ECD
4,4'-DDD
<0.027
ug/L
0.1
0.10
0.027
1
8081 B
10/19/20 12:22NMB
POJ0286
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081 B
10/19/20 12:22NMB
POJ0286
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081 B
10/19/20 12:22NMB
POJ0286
Aldrin
<0.015
ug/L
0.05
0.051
0.015
1
8081 B
10/19/20 12:22NMB
POJ0286
alpha-BHC
<0.0064
ug/L
0.05
0.051
0.0064
1
8081 B
10/19/20 12:22NMB
POJ0286
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/19/20 12:22NMB
POJ0286
beta-BHC
0.14
DC
ug/L
0.05
0.051
0.011
1
8081 B
10/19/20 12:22NMB
POJ0286
Chlordane
<0.18
ug/L
0.5
0.51
0.18
1
8081 B
10/19/20 12:22NMB
POJ0286
delta-BHC
<0.0083
ug/L
0.05
0.051
0.0083
1
8081 B
10/19/20 12:22NMB
POJ0286
Dieldrin
<0.014
ug/L
0.002
0.051
0.014
1
8081 B
10/19/20 12:22NMB
POJ0286
Endosulfan 1
<0.016
ug/L
0.1
0.051
0.016
1
8081 B
10/19/20 12:22NMB
POJ0286
Endosulfan 11
<0.012
ug/L
0.1
0.051
0.012
1
8081 B
10/19/20 12:22NMB
POJ0286
Endosulfan Sulfate
<0.017
ug/L
0.1
0.051
0.017
1
8081 B
10/19/20 12:22NMB
POJ0286
Endrin
<0.014
ug/L
0.1
0.051
0.014
1
8081 B
10/19/20 12:22NMB
POJ0286
Endrin Aldehyde
<0.016
ug/L
0.1
0.051
0.016
1
8081 B
10/19/20 12:22NMB
POJ0286
Endrin Ketone
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/19/20 12:22NMB
POJ0286
gamma-BHC
<0.0062
ug/L
0.05
0.051
0.0062
1
8081 B
10/19/20 12:22NMB
POJ0286
trans -Chlordane
<0.023
ug/L
NE
0.10
0.023
1
8081 B
10/19/20 12:22NMB
POJ0286
Heptachlor
<0.013
ug/L
0.05
0.051
0.013
1
8081 B
10/19/20 12:22NMB
POJ0286
Heptachlor Epoxide
<0.023
ug/L
0.075
0.10
0.023
1
8081 B
10/19/20 12:22NMB
POJ0286
Methoxychlor
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/19/20 12:22NMB
POJ0286
Toxaphene
<0.35
ug/L
1.5
1.0
0.35
1
8081 B
10/19/20 12:22NMB
POJ0286
Surrogate Recovery Control Limits
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 62
Laboratory Report
• � 12/31/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-06-20201013
Attn: Alec Macbeth Sample ID: 0100174-03
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 13:15
Time Submitted: 10/14/20 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Decachlorobiphenyl 55 % 13-186
Tetrachloro-m-xylene 67 % 40-134
Polychlorinated Biphenyls (PCBs) by GC/ECD
Aroclor 1016
<0.21
ug/L
NE
0.51
0.21
1
8082A
10/19/20 12:22NMB
POJ0286
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1
8082A
10/19/20 12:22NMB
POJ0286
Aroclor 1232
<0.16
ug/L
NE
0.51
0.16
1
8082A
10/19/20 12:22NMB
POJ0286
Aroclor 1242
<0.14
ug/L
NE
0.51
0.14
1
8082A
10/19/20 12:22NMB
POJ0286
Aroclor 1248
<0.14
ug/L
NE
0.51
0.14
1
8082A
10/19/20 12:22NMB
POJ0286
Aroclor 1254
<0.16
ug/L
NE
0.51
0.16
1
8082A
10/19/20 12:22NMB
POJ0286
Aroclor 1260
<0.50
ug/L
NE
1.0
0.50
1
8082A
10/19/20 12:22NMB
POJ0286
Total Metals
Surrogate
Recovery Control Limits
Tetrachloro-m-xylene 68 % 30-161
Decachlorobiphenyl 58 % 32-178
Mercury
1.3
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 15:34EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/23/20 16:49JAB
POJ0239
Arsenic
<0.17
ug/L
10
1.0
0.17
1
6020B
10/23/20 16:49JAB
POJ0239
Barium
47
ug/L
100
2.0
0.81
1
6020B
10/23/20 16:49JAB
POJ0239
Beryllium
<0.19 CCV
ug/L
1
1.0
0.19
1
6020B
10/23/20 16:49JAB
POJ0239
Cadmium
<0.16
ug/L
1
1.0
0.16
1
6020B
10/23/20 16:49JAB
POJ0239
Chromium
<0.79
ug/L
10
2.0
0.79
1
6020B
10/23/20 16:49JAB
POJ0239
Cobalt
9.0
ug/L
10
2.0
0.52
1
6020B
10/23/20 16:49JAB
POJ0239
Copper
<3.8
ug/L
10
10
3.8
1
6020B
10/23/20 16:49JAB
POJ0239
Lead
<0.26
ug/L
10
1.0
0.26
1
6020B
10/23/20 16:49JAB
POJ0239
Nickel
3.4
ug/L
50
3.0
0.51
1
6020B
10/23/20 16:49JAB
POJ0239
Selenium
<0.74
ug/L
10
5.0
0.74
1
6020B
10/23/20 16:49JAB
POJ0239
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 19:07JAB
POJ0490
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/23/20 16:49JAB
POJ0239
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/23/20 16:49JAB
POJ0239
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/23/20 16:49JAB
POJ0239
Zinc
20
ug/L
10
20
6.9
1
6020B
10/23/20 16:49JAB
POJ0239
Volatile Organic Compounds by GUMS
1,1,1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 20:17JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 20:17JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 20:17JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 20:17JLB
POJ0321
1,1-Dichloroethane
1.4
ug/L
5
0.50
0.083
1
8260D
10/21/20 20:17JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 20:17JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 62
Laboratory Report
A i • .0 12/31/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-06-20201013
Attn: Alec Macbeth Sample ID: 0100174-03
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 13:15
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 20:17JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 20:17JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 20:17JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 20:17JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 20:17JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 20:17JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 20:17JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 20:17JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 20:17JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 20:17JLB
POJ0321
1,4-Dichlorobenzene
2.6
ug/L
1
0.50
0.050
1
8260D
10/21/20 20:17JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 20:17JLB
POJ0321
Acetone
<0.31
ug/L
100
5.0
0.31
1
8260D
10/21/20 20:17JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 20:17JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 20:17JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 20:17JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 20:17JLB
POJ0321
Benzene
0.26 J
ug/L
1
0.50
0.048
1
8260D
10/21/20 20:17JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 20:17JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 20:17JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 20:17JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 20:17JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 20:17JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 20:17JLB
POJ0321
Chlorobenzene
0.41 J
ug/L
3
0.50
0.062
1
8260D
10/21/20 20:17JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 20:17JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 20:17JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 20:17JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 20:17JLB
POJ0321
cis-1,2-Dichloroethylene
1.4
ug/L
2
0.50
0.056
1
8260D
10/21/20 20:17JLB
POJ0321
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 20:17JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 20:17JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 20:17JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 20:17JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 20:17JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 20:17JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 20:17JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 62
.
Laboratory Report
• �
Waynt..
12/31/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID:
MW-06-20201013
Attn: Alec Macbeth
Sample ID: 0100174-03
231 Haywood Street
Project No.:
50-02
Work
Order: 0100174
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/13/20 13:15
Time
Submitted: 10/14/20
09:10
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 20:17JLB
POJ0321
m,p-Xylenes
0.37
J ug/L
NE
1.0
0.12
1
8260D
10/21/20 20:17JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 20:17JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 20:17JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 20:17JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 20:17JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 20:17JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 20:17JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 20:17JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 20:17JLB
POJ0321
o-Xylene
0.29
J ug/L
NE
0.50
0.044
1
8260D
10/21/20 20:17JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 20:17JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 20:17JLB
POJ0321
Tetrachloroethylene
0.25
J ug/L
1
0.50
0.098
1
8260D
10/21/20 20:17JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 20:17JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 20:17JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 20:17JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 20:17JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 20:17JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 20:17JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 20:17JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 20:17JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 20:17JLB
POJ0321
Xylenes, total
0.66
J ug/L
5
1.5
0.15
1
8260D
10/21/20 20:17JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
103 % 80-124
Dibromofluoromethane
108 % 75-129
Toluene-d8
99 % 77-123
Volatile Organic Compounds by GUMS
SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/16/20 22:29ANG
POJ0316
8270 Extended List
1,3,5-Trinitrobenzene
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
1,4-Naphthoquinone
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
1-Naphthylamine
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
2-Acetylaminofluorene
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
2-Naphthylamine
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
3-Methylcholanthrene
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
4-Aminobiphenyl
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 62
Laboratory Report
A i • .0 12/31/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-06-20201013
Attn: Alec Macbeth Sample ID: 0100174-03
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 13:15
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
5-Nitro-o-toluidine
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
7,12-D1methyl benz(a)anthrace ne
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
Diallate
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
Hexachloropropene
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
Isosafrole
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
Kepone
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
Methapyrilene
U
Ng/L
22.2
11.1
1
8270D
10/20/20 19:13BGV
L517325
N-Nitrosomethylethyl amine
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
N-Nitrosopiperidine
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
N-Nitrosopyrrolidine
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
o-Toluidine
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
p-Dimethylaminoazobenzene
U
pg/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
p-Phenylenediamine
U L
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
Pronamide
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
Safrole
U
Ng/L
11.1
11.1
1
8270D
10/20/20 19:13BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
U
Ng/L
0.03
0.01002
1
8151A
10/21/20
1:07 VIC
L517362
2,4,5-TP (Silvex)
U
Ng/L
0.1
0.01634
1
8151A
10/21/20
1:07 VIC
L517362
2,4-D
U
Ng/L
0.25
0.2078
1
8151A
10/21/20
1:07 VIC
L517362
2,4-DB
U
Ng/L
0.1
0.1364
1
8151A
10/21/20
1:07 VIC
L517362
Dalapon
U
Ng/L
0.55
0.5149
1
8151A
10/21/20
1:07 VIC
L517362
Dicamba
U
Ng/L
0.1
0.057
1
8151A
10/21/20
1:07 VIC
L517362
Dichlorprop
U
Ng/L
0.1
0.07959
1
8151A
10/21/20
1:07 VIC
L517362
Dinoseb
U
Ng/L
0.1
0.02698
1
8151A
10/21/20
1:07 VIC
L517362
MCPA
U
Ng/L
50
18.98
1
8151A
10/21/20
1:07 VIC
L517362
MCPP
U
Ng/L
50
11.75
1
8151A
10/21/20
1:07 VIC
L517362
Picloram
U
Ng/L
0.1
0.04528
1
8151A
10/21/20
1:07 VIC
L517362
Surrogate
Recovery
Control Limits
DCAA
62.6 %
20-150
Semivolatile Organic Compounds - GC/MS
1,2,4,5-Tetrachlorobenzene
U
Ng/L
5.56
0.352
1
8270D
10/20/20 19:13BGV
L517328
1,2,4-Trichlorobenzene
U
Ng/L
5.56
0.535
1
8270D
10/20/20 19:13BGV
L517328
1,2-Dichlorobenzene
U
Ng/L
5.56
0.699
1
8270D
10/20/20 19:13BGV
L517328
1,3-Dichlorobenzene
U
Ng/L
5.56
0.545
1
8270D
10/20/20 19:13BGV
L517328
1,4-Dichlorobenzene
0.779 j
Ng/L
5.56
0.644
1
8270D
10/20/20 19:13BGV
L517328
2,3,4,6-Tetrachlorophenol
U
Ng/L
5.56
0.394
1
8270D
10/20/20 19:13BGV
L517328
2,4,5-Trichlorophenol
U
Ng/L
5.56
0.389
1
8270D
10/20/20 19:13BGV
L517328
2,4,6-Trichlorophenol
U
Ng/L
5.56
0.382
1
8270D
10/20/20 19:13BGV
L517328
2,4-Dichlorophenol
U
Ng/L
5.56
1.69
1
8270D
10/20/20 19:13BGV
L517328
2,4-Dimethylphenol
U
Ng/L
5.56
0.749
1
8270D
10/20/20 19:13BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 62
® Laboratory Report
IL AL i • . 12/31 /2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-06-20201013
Attn: Alec Macbeth Sample ID: 0100174-03
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 13:15
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
2,4-Dinitrophenol
U
pg/L
11.1
5.38
1
8270D
10/20/20 19:13BGV
L517328
2,4-Dinitrotoluene
U
pg/L
5.56
0.448
1
8270D
10/20/20 19:13BGV
L517328
2,6-Dichlorophenol
U
pg/L
5.56
0.781
1
8270D
10/20/20 19:13BGV
L517328
2,6-Dinitrotoluene
U
pg/L
5.56
0.459
1
8270D
10/20/20 19:13BGV
L517328
2-Chloronaphthalene
U
pg/L
5.56
0.529
1
8270D
10/20/20 19:13BGV
L517328
2-Chlorophenol
U
pg/L
5.56
0.818
1
8270D
10/20/20 19:13BGV
L517328
2-Methyl naphthalene
U
pg/L
2.22
0.538
1
8270D
10/20/20 19:13BGV
L517328
2-Methylphenol
U
pg/L
5.56
0.801
1
8270D
10/20/20 19:13BGV
L517328
2-Nitroaniline
U
pg/L
5.56
0.638
1
8270D
10/20/20 19:13BGV
L517328
2-Nitrophenol
U
pg/L
5.56
0.673
1
8270D
10/20/20 19:13BGV
L517328
3&4 Methylphenol
U
pg/L
5.56
0.768
1
8270D
10/20/20 19:13BGV
L517328
3,3' Dimethylbenzidine
U
pg/L
11.1
2.09
1
8270D
10/20/20 19:13BGV
L517328
3,3'-Dichlorobenzidine
U
pg/L
11.1
4.15
1
8270D
10/20/20 19:13BGV
L517328
3-Nitroaniline
U
pg/L
11.1
1.7
1
8270D
10/20/20 19:13BGV
L517328
4,6-Dinitro-2-methylphenol
U
pg/L
11.1
3.85
1
8270D
10/20/20 19:13BGV
L517328
4-Bromophenyl phenyl ether
U
pg/L
5.56
0.556
1
8270D
10/20/20 19:13BGV
L517328
4-Chloro-3-methylphenol
U
pg/L
5.56
0.559
1
8270D
10/20/20 19:13BGV
L517328
4-Chloroaniline
U
pg/L
5.56
0.584
1
8270D
10/20/20 19:13BGV
L517328
4-Chlorophenyl phenyl ether
U
pg/L
5.56
0.532
1
8270D
10/20/20 19:13BGV
L517328
4-Nitroaniline
U
pg/L
5.56
0.822
1
8270D
10/20/20 19:13BGV
L517328
4-Nitrophenol
U
pg/L
11.1
1.54
1
8270D
10/20/20 19:13BGV
L517328
Acenaphthene
U
pg/L
2.22
0.468
1
8270D
10/20/20 19:13BGV
L517328
Acenaphthylene
U
pg/L
2.22
0.476
1
8270D
10/20/20 19:13BGV
L517328
Acetophenone
U
pg/L
5.56
0.762
1
8270D
10/20/20 19:13BGV
L517328
Aniline
U
pg/L
5.56
0.351
1
8270D
10/20/20 19:13BGV
L517328
Anthracene
U
pg/L
2.22
0.518
1
8270D
10/20/20 19:13BGV
L517328
Benzidine
U
pg/L
22.2
0.764
1
8270D
10/20/20 19:13BGV
L517328
Benzo(a)anthracene
U
pg/L
2.22
0.473
1
8270D
10/20/20 19:13BGV
L517328
Benzo(a)pyrene
U
pg/L
2.22
1.11
1
8270D
10/20/20 19:13BGV
L517328
Benzo(b)fluoranthene
U
pg/L
2.22
1.04
1
8270D
10/20/20 19:13BGV
L517328
Benzo(q,hJ)perylene
U
pg/L
2.22
1.51
1
8270D
10/20/20 19:13BGV
L517328
Benzo(k)fluoranthene
U
pg/L
2.22
0.834
1
8270D
10/20/20 19:13BGV
L517328
Benzoic Acid
U
pg/L
11.1
5.55
1
8270D
10/20/20 19:13 BGV
L517328
Benzyl alcohol
U
pg/L
11.1
3.34
1
8270D
10/20/20 19:13BGV
L517328
Bis(2-Chloroethoxy)methane
U
pg/L
5.56
0.481
1
8270D
10/20/20 19:13BGV
L517328
Bis(2-Chloroethyl)ether
U
pg/L
5.56
0.497
1
8270D
10/20/20 19:13BGV
L517328
Bis(2-Chloroisopropyl)ether
U
pg/L
5.56
0.607
1
8270D
10/20/20 19:13BGV
L517328
Bis(2-ethylhexyl)phthalate
U
pg/L
5.56
4.07
1
8270D
10/20/20 19:13BGV
L517328
Butyl benzyl phthalate
U
pg/L
5.56
5.11
1
8270D
10/20/20 19:13BGV
L517328
Carbazole
U
pg/L
5.56
0.529
1
8270D
10/20/20 19:13BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 62
.
Laboratory Report
• �
Waynt.�
12/31/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID: MW-06-20201013
Attn: Alec Macbeth
Sample ID: 0100174-03
231 Haywood Street
Project No.: 50-02
Work
Order: 0100174
Asheville, NC 28801
Sample Matrix: Water
Time
Collected: 10/13/20 13:15
Time
Submitted: 10/14/20 09:10
Parameter
Result Units SWSL
Report
MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chrysene
U
Ng/L
2.22
0.811
1
8270D 10/20/20 19:13BGV
L517328
D1benz(a,h)anthrace ne
U
Ng/L
2.22
0.279
1
8270D 10/20/20 19:13BGV
L517328
Dibenzofuran
U
Ng/L
5.56
0.47
1
8270D 10/20/20 19:13BGV
L517328
Diethyl phthalate 0.709
j Ng/L
5.56
0.65
1
8270D 10/20/20 19:13BGV
L517328
Dimethyl phthalate
U
Ng/L
5.56
0.567
1
8270D 10/20/20 19:13BGV
L517328
Di-n-butyl phthalate
U
Ng/L
5.56
1.75
1
8270D 10/20/20 19:13BGV
L517328
Di-n-Octyl Phthalate
U
Ng/L
5.56
1.91
1
8270D 10/20/20 19:13BGV
L517328
Fluoranthene
U
Ng/L
2.22
0.45
1
8270D 10/20/20 19:13BGV
L517328
Fluorene
U
Ng/L
2.22
0.492
1
8270D 10/20/20 19:13BGV
L517328
Hexachlorobenzene
U
Ng/L
5.56
2.86
1
8270D 10/20/20 19:13BGV
L517328
Hexachlorobutadiene
U
Ng/L
5.56
0.45
1
8270D 10/20/20 19:13BGV
L517328
Hexachlorocyclopentadiene
U
Ng/L
5.56
2.6
1
8270D 10/20/20 19:13BGV
L517328
Hexachloroethane
U
Ng/L
5.56
0.308
1
8270D 10/20/20 19:13BGV
L517328
Indeno(1,2,3-cd)pyrene
U
Ng/L
2.22
1.12
1
8270D 10/20/20 19:13BGV
L517328
Isophorone
U
Ng/L
5.56
0.4
1
8270D 10/20/20 19:13BGV
L517328
Naphthalene
U
Ng/L
2.22
0.537
1
8270D 10/20/20 19:13BGV
L517328
Nitrobenzene
U
Ng/L
5.56
0.59
1
8270D 10/20/20 19:13BGV
L517328
N-Nitrosodiethylamine
U
pg/L
5.56
0.444
1
8270D 10/20/20 19:13BGV
L517328
N-Nitrosodimethylamine
U
Ng/L
5.56
0.276
1
8270D 10/20/20 19:13BGV
L517328
N-Nitroso-di-n-butylamine
U
Ng/L
5.56
0.836
1
8270D 10/20/20 19:13BGV
L517328
N-Nitroso-di-n-propylamine
U
Ng/L
5.56
0.371
1
8270D 10/20/20 19:13BGV
L517328
N-Nitrosodiphenylamine
U
Ng/L
11.1
0.869
1
8270D 10/20/20 19:13BGV
L517328
Pentachlorophenol
U
Ng/L
11.1
2.72
1
8270D 10/20/20 19:13BGV
L517328
Phenanthrene
U
Ng/L
2.22
0.515
1
8270D 10/20/20 19:13BGV
L517328
Phenol
U
Ng/L
5.56
0.432
1
8270D 10/20/20 19:13BGV
L517328
Pyrene
U
Ng/L
2.22
1.15
1
8270D 10/20/20 19:13BGV
L517328
Pyridine
U
Ng/L
11.1
0.752
1
8270D 10/20/20 19:13BGV
L517328
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
26.2 % 39-110
SR
2-Fluorobiphenyl
46.2 % 24-93
2-Fluorophenol
12.7 % 10-44
4-Terphenyl-d14
21.9 % 35-126
SR
Nitrobenzene-d5
50 % 20-91
Phenol-d6
10.3 % 7-32
Total Organic Carbon
TOC
1.04
mg/L
1
0.498
1
531OC-2011 10/22/20 3:29 DDB
L517921
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 62
Laboratory Report
• � 12/31/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: TB-202010130000
Attn: Alec Macbeth Sample ID: 0100174-04
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 00:00
Time Submitted: 10/14/20 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 16:19JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 16:19JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 16:19JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 16:19JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 16:19JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 16:19JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 16:19JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 16:19JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 16:19JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 16:19JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 16:19JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 16:19JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 16:19JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 16:19JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 16:19JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 16:19JLB
POJ0321
1,4-Dichlorobenzene
<0.050
ug/L
1
0.50
0.050
1
8260D
10/21/20 16:19JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 16:19JLB
POJ0321
Acetone
3.0 J
ug/L
100
5.0
0.31
1
8260D
10/21/20 16:19JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 16:19JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 16:19JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 16:19JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 16:19JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 16:19JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 16:19JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 16:19JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 16:19JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 16:19JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 16:19JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 16:19JLB
POJ0321
Chlorobenzene
<0.062
ug/L
3
0.50
0.062
1
8260D
10/21/20 16:19JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 16:19JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 16:19JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 16:19JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 16:19JLB
POJ0321
cis- 1,2-Dichloroethylene
<0.056
ug/L
2
0.50
0.056
1
8260D
10/21/20 16:19JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 62
Laboratory Report
A i • .0 12/31/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: TB-202010130000
Attn: Alec Macbeth Sample ID: 0100174-04
231 Haywood Street Project No.: 50-02 Work Order: 0100174
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/13/20 00:00
Time Submitted: 10/14/20 09:10
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 16:19JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 16:19JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 16:19JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 16:19JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 16:19JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 16:19JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 16:19JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 16:19JLB
POJ0321
m,p-Xylenes
<0.12
ug/L
NE
1.0
0.12
1
8260D
10/21/20 16:19JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 16:19JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 16:19JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 16:19JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 16:19JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 16:19JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 16:19JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 16:19JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 16:19JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 16:19JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 16:19JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 16:19JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 16:19JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 16:19JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 16:19JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 16:19JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 16:19JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 16:19JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 16:19JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 16:19JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 16:19JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 16:19JLB
POJ0321
Xylenes, total
<0.15
ug/L
5
1.5
0.15
1
8260D
10/21/20 16:19JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
104 % 80-124
Dibromofluoromethane
106 % 75-129
Toluene-d8
101 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 62
(2)
Way po Int
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
Blank (POJ0321-BLK1)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,1-Dichloropropylene
BRL
0.50
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
0.290
1.0
ug/L J
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,3-Dichlorobenzene
BRL
0.50
ug/L
1,3-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
Acetone
BRL
5.0
ug/L
Acetonitrile
BRL
10
ug/L
Acrolein
BRL
20
ug/L
Acrylonitrile
BRL
20
ug/L
Allyl Chloride (3-Chloropropylene)
BRL
10
ug/L
Benzene
BRL
0.50
ug/L
Bromochloromethane
BRL
0.50
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
0.50
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
Chloroprene
BRL
10
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
0.50
ug/L
Dichlorodifluoromethane
BRL
5.0
ug/L
Ethyl Methacrylate
BRL
10
ug/L
Ethylbenzene
BRL
0.50
ug/L
Hexachlorobutadiene
0.220
2.0
ug/L J
Isobutyl alcohol
BRL
50
ug/L
m,p-Xylenes
0.250
1.0
ug/L J
Methacrylonitrile
BRL
10
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 30 of 62
Waypoint '
ANALYTICAL
Level II QC Report
12/31/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
Blank (POJ0321-BLK1)
Prepared & Analyzed: 10/21/20
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methyl Methacrylate
BRL
10
ug/L
Methylene Chloride
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
o-Xylene
BRL
0.50
ug/L
Propionitrile (Ethyl Cyanide)
BRL
10
ug/L
Styrene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrahydrofuran
BRL
10
ug/L
Toluene
BRL
0.50
ug/L
trans- 1,2-Dichloroethylene
BRL
0.50
ug/L
trans- 1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
Trichloroethylene
BRL
0.50
ug/L
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
0.250
1.5
ug/L
J
Surrogate:4-Bromofluorobenzene
50.3
ug/L
50.00
101
80-124
Surrogate: Dibromofluoromethane
53.8
ug/L
50.00
108
75-129
Surrogate: Toluene-d8
49.6
ug/L
50.00
99
77-123
LCS (POJ0321-BS1)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
21.5
0.50
ug/L
20.00
108
79-134
1,1,1-Trichloroethane
21.3
0.50
ug/L
20.00
106
75-136
1,1,2,2-Tetrachloroethane
21.0
0.50
ug/L
20.00
105
62-127
1,1,2-Trichloroethane
21.6
0.50
ug/L
20.00
108
70-140
1,1-Dichloroethane
21.6
0.50
ug/L
20.00
108
78-130
1,1-Dichloroethylene
21.2
0.50
ug/L
20.00
106
70-154
1, 1 -Dichloropropylene
22.0
0.50
ug/L
20.00
110
71-136
1,2,3-Trichloropropane
21.2
1.0
ug/L
20.00
106
71-127
1,2,4-Trichlorobenzene
20.4
1.0
ug/L
20.00
102
66-139
1,2-Dibromo-3-chloropropane
22.9
2.0
ug/L
20.00
114
63-134
1,2-Dibromoethane
21.3
0.50
ug/L
20.00
107
77-135
1,2-Dichlorobenzene
21.3
0.50
ug/L
20.00
106
78-128
1,2-Dichloroethane
21.6
0.50
ug/L
20.00
108
68-131
1,2-Dichloropropane
21.9
0.50
ug/L
20.00
110
77-130
1,3-Dichlorobenzene
21.5
0.50
ug/L
20.00
107
77-125
1,3-Dichloropropane
22.0
0.50
ug/L
20.00
110
76-132
1,4-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
75-126
2,2-Dichloropropane
23.8
2.0
ug/L
20.00
119
29-149
Acetone
39.6
5.0
ug/L
40.00
99
40-166
Acetonitrile
19.4
10
ug/L
20.00
97
70-130
Acrolein
45.9
20
ug/L
40.00
115
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 62
Waypoint '
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
12/31/20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS (POJ0321-BSI)
Prepared &Analyzed: 10/21/20
Acrylonitrile
42.3
20
ug/L
40.00
106
81-127
Allyl Chloride (3-Chloropropylene)
19.4
10
ug/L
20.00
97
70-130
Benzene
22.7
0.50
ug/L
20.00
114
77-128
Bromochloromethane
22.1
0.50
ug/L
20.00
110
78-135
Bromodichloromethane
21.7
0.50
ug/L
20.00
108
76-138
Bromoform
22.4
1.0
ug/L
20.00
112
71-135
Bromomethane
21.0
1.0
ug/L
20.00
105
41-168
Carbon disulfide
21.1
5.0
ug/L
20.00
106
59-135
Carbon Tetrachloride
21.7
0.50
ug/L
20.00
109
72-142
Chlorobenzene
22.0
0.50
ug/L
20.00
110
78-119
Chloroethane
21.5
0.50
ug/L
20.00
107
57-142
Chloroform
21.0
0.50
ug/L
20.00
105
77-130
Chloromethane
20.5
0.50
ug/L
20.00
102
47-145
Chloroprene
19.7
10
ug/L
20.00
98
70-130
cis-1,2-Dichloroethylene
22.5
0.50
ug/L
20.00
113
76-141
cis-1,3-Dichloropropylene
22.4
0.50
ug/L
20.00
112
65-140
Dibromochloromethane
21.2
0.50
ug/L
20.00
106
75-134
Dibromomethane
21.8
0.50
ug/L
20.00
109
76-138
Dichlorodifluoromethane
25.2
5.0
ug/L
20.00
126
28-163
Ethyl Methacrylate
19.7
10
ug/L
20.00
99
70-130
Ethylbenzene
22.7
0.50
ug/L
20.00
114
80-127
Hexachlorobutadiene
20.1
2.0
ug/L
20.00
100
61-134
Isobutyl alcohol
24.0
50
ug/L
20.00
120
70-130 J
m,p-Xylenes
48.4
1.0
ug/L
40.00
121
77-133
Methacrylonitrile
19.5
10
ug/L
20.00
98
70-130
Methyl Butyl Ketone (2-Hexanone)
22.7
5.0
ug/L
20.00
114
64-137
Methyl Ethyl Ketone (2-Butanone)
20.2
5.0
ug/L
20.00
101
71-134
Methyl Iodide
23.5
5.0
ug/L
20.00
118
70-130
Methyl Isobutyl Ketone
23.8
5.0
ug/L
20.00
119
69-134
Methyl Methacrylate
20.3
10
ug/L
20.00
102
70-130
Methylene Chloride
20.7
1.0
ug/L
20.00
103
73-131
Naphthalene
21.0
1.0
ug/L
20.00
105
64-136
o-Xylene
22.8
0.50
ug/L
20.00
114
78-128
Propionitrile (Ethyl Cyanide)
22.1
10
ug/L
20.00
110
70-130
Styrene
23.3
0.50
ug/L
20.00
116
78-129
Tetrachloroethylene
21.2
0.50
ug/L
20.00
106
80-129
Tetrahydrofuran
22.3
10
ug/L
20.00
112
70-130
Toluene
22.5
0.50
ug/L
20.00
113
76-131
trans- 1,2-Dichloroethylene
21.6
0.50
ug/L
20.00
108
76-135
trans- 1,3-Dichloropropylene
23.1
0.50
ug/L
20.00
116
67-140
trans-1,4-Dichloro-2-butene
21.1
10
ug/L
20.00
105
70-130
Trichloroethylene
21.3
0.50
ug/L
20.00
107
77-133
Trichlorofluoromethane
22.6
0.50
ug/L
20.00
113
62-148
Vinyl acetate
26.3
2.0
ug/L
20.00
131
34-167
Vinyl chloride
22.4
0.50
ug/L
20.00
112
57-141
Xylenes, total
71.2
1.5
ug/L
60.00
119
77-133
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 32 of 62
Waypoint '
ANALYTICAL
Level II QC Report
12/31/20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS (POJ0321-BSI)
Prepared &Analyzed: 10/21/20
Surrogate:4-Bromofluorobenzene
48.4
ug/L
50.00
97
80-124
Surrogate: Dibromofluoromethane
49.3
ug/L
50.00
99
75-129
Surrogate: Toluene-d8
50.0
ug/L
50.00
100
77-123
LCS Dup (POJ0321-BSDI)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
21.4
0.50
ug/L
20.00
107
79-134
0.6
20
1,1,1-Trichloroethane
20.5
0.50
ug/L
20.00
102
75-136
4
20
1,1,2,2-Tetrachloroethane
20.7
0.50
ug/L
20.00
103
62-127
2
20
1,1,2-Trichloroethane
21.4
0.50
ug/L
20.00
107
70-140
1
20
1,1-Dichloroethane
20.4
0.50
ug/L
20.00
102
78-130
5
20
1,1-Dichloroethylene
20.2
0.50
ug/L
20.00
101
70-154
5
20
1, 1 -Dichloropropylene
21.0
0.50
ug/L
20.00
105
71-136
5
20
1,2,3-Trichloropropane
21.1
1.0
ug/L
20.00
106
71-127
0.6
20
1,2,4-Trichlorobenzene
20.7
1.0
ug/L
20.00
103
66-139
1
20
1,2-Dibromo-3-chloropropane
21.7
2.0
ug/L
20.00
108
63-134
5
20
1,2-Dibromoethane
20.9
0.50
ug/L
20.00
104
77-135
2
20
1,2-Dichlorobenzene
20.5
0.50
ug/L
20.00
103
78-128
4
20
1,2-Dichloroethane
21.1
0.50
ug/L
20.00
106
68-131
2
20
1,2-Dichloropropane
21.3
0.50
ug/L
20.00
107
77-130
3
20
1,3-Dichlorobenzene
21.1
0.50
ug/L
20.00
105
77-125
2
20
1,3-Dichloropropane
21.3
0.50
ug/L
20.00
106
76-132
3
20
1,4-Dichlorobenzene
20.4
0.50
ug/L
20.00
102
75-126
2
20
2,2-Dichloropropane
21.4
2.0
ug/L
20.00
107
29-149
11
20
Acetone
39.2
5.0
ug/L
40.00
98
40-166
1
20
Acetonitrile
21.5
10
ug/L
20.00
107
70-130
10
20
Acrolein
46.1
20
ug/L
40.00
115
70-130
0.5
20
Acrylonitrile
42.2
20
ug/L
40.00
105
81-127
0.4
20
Allyl Chloride (3-Chloropropylene)
18.8
10
ug/L
20.00
94
70-130
3
20
Benzene
21.8
0.50
ug/L
20.00
109
77-128
4
20
Bromochloromethane
20.5
0.50
ug/L
20.00
103
78-135
7
20
Bromodichloromethane
20.8
0.50
ug/L
20.00
104
76-138
4
20
Bromoform
21.5
1.0
ug/L
20.00
107
71-135
4
20
Bromomethane
19.7
1.0
ug/L
20.00
99
41-168
6
20
Carbon disulfide
20.5
5.0
ug/L
20.00
102
59-135
3
20
Carbon Tetrachloride
20.9
0.50
ug/L
20.00
105
72-142
4
20
Chlorobenzene
21.2
0.50
ug/L
20.00
106
78-119
4
20
Chloroethane
20.2
0.50
ug/L
20.00
101
57-142
6
20
Chloroform
20.6
0.50
ug/L
20.00
103
77-130
2
20
Chloromethane
20.0
0.50
ug/L
20.00
100
47-145
2
20
Chloroprene
18.8
10
ug/L
20.00
94
70-130
5
20
cis-1,2-Dichloroethylene
20.4
0.50
ug/L
20.00
102
76-141
10
20
cis-1,3-Dichloropropylene
21.9
0.50
ug/L
20.00
110
65-140
2
20
Dibromochloromethane
21.2
0.50
ug/L
20.00
106
75-134
0.1
20
Dibromomethane
21.3
0.50
ug/L
20.00
107
76-138
2
20
Dichlorodifluoromethane
24.2
5.0
ug/L
20.00
121
28-163
4
20
Ethyl Methacrylate
19.4
10
ug/L
20.00
97
70-130
1
20
Ethylbenzene
22.0
0.50
ug/L
20.00
110
80-127
3
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 62
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/31 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS Dup (POJ0321-BSD1)
Prepared &Analyzed: 10/21/20
Hexachlorobutadiene
19.9
2.0
ug/L
20.00
99
61-134
1
20
Isobutyl alcohol
21.3
50
ug/L
20.00
106
70-130
12
20 1
m,p-Xylenes
47.1
1.0
ug/L
40.00
118
77-133
3
20
Methacrylonitrile
19.2
10
ug/L
20.00
96
70-130
2
20
Methyl Butyl Ketone (2-Hexanone)
22.7
5.0
ug/L
20.00
113
64-137
0.3
20
Methyl Ethyl Ketone (2-Butanone)
19.7
5.0
ug/L
20.00
98
71-134
3
20
Methyl Iodide
22.6
5.0
ug/L
20.00
113
70-130
4
20
Methyl Isobutyl Ketone
22.7
5.0
ug/L
20.00
113
69-134
5
20
Methyl Methacrylate
19.7
10
ug/L
20.00
99
70-130
3
20
Methylene Chloride
19.8
1.0
ug/L
20.00
99
73-131
5
20
Naphthalene
21.4
1.0
ug/L
20.00
107
64-136
2
20
o-Xylene
22.3
0.50
ug/L
20.00
112
78-128
2
20
Propionitrile (Ethyl Cyanide)
19.9
10
ug/L
20.00
100
70-130
10
20
Styrene
22.7
0.50
ug/L
20.00
113
78-129
3
20
Tetrachloroethylene
20.4
0.50
ug/L
20.00
102
80-129
4
20
Tetrahydrofuran
22.0
10
ug/L
20.00
110
70-130
2
20
Toluene
21.6
0.50
ug/L
20.00
108
76-131
4
20
trans-1,2-Dichloroethylene
20.6
0.50
ug/L
20.00
103
76-135
5
20
trans-1,3-Dichloropropylene
22.2
0.50
ug/L
20.00
ill
67-140
4
20
trans-1,4-Dichloro-2-butene
19.6
10
ug/L
20.00
98
70-130
7
20
Trichloroethylene
21.2
0.50
ug/L
20.00
106
77-133
0.7
20
Trichlorofluoromethane
21.4
0.50
ug/L
20.00
107
62-148
6
20
Vinyl acetate
25.7
2.0
ug/L
20.00
129
34-167
2
20
Vinyl chloride
21.2
0.50
ug/L
20.00
106
57-141
5
20
Xylenes, total
69.4
1.5
ug/L
60.00
116
77-133
2
20
Surrogate:4-Bromofluorobenzene
48.3
ug/L
50.00
97
80-124
Surrogate: Dibromofluoromethane
49.5
ug/L
50.00
99
75-129
Surrogate: Toluene-d8
50.3
ug/L
50.00
101
77-123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Asheville, NC 28801
Volatile Organic Compounds by GC/MS SIM - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0316 - 5030B
Blank (POJ0316-BLK1) Prepared & Analyzed: 10/16/20
1,4-Dioxane BRL 2.0 ug/L
LCS (POJ0316-BS1) Prepared &Analyzed: 10/16/20
1,4-Dioxane 47.5 2.0 ug/L 50.00 95 55-145
LCS Dup (POJ0316-BSD1) Prepared &Analyzed: 10/16/20
1,4-Dioxane 47.1 2.0 ug/L 50.00 94 55-145 0.7 30
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 35 of 62
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/31 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
Blank (POJ0286-BLK1)
Prepared: 10/16/20 Analyzed: 10/19/20
4,4'-DDD
BRL
0.10
ug/L
4,4'-DDE
BRL
0.10
ug/L
4,4'-DDT
BRL
0.10
ug/L
Aldrin
BRL
0.050
ug/L
alpha-BHC
BRL
0.050
ug/L
cis -Chlordane
BRL
0.10
ug/L
beta-BHC
BRL
0.050
ug/L
Chlordane
BRL
0.50
ug/L
delta-BHC
BRL
0.050
ug/L
Dieldrin
BRL
0.050
ug/L
Endosulfan I
BRL
0.050
ug/L
Endosulfan II
BRL
0.050
ug/L
Endosulfan Sulfate
BRL
0.050
ug/L
Endrin
BRL
0.050
ug/L
Endrin Aldehyde
BRL
0.050
ug/L
Endrin Ketone
BRL
0.10
ug/L
gamma-BHC
BRL
0.050
ug/L
trans -Chlordane
BRL
0.10
ug/L
Heptachlor
BRL
0.050
ug/L
Heptachlor Epoxide
BRL
0.10
ug/L
Methoxychlor
BRL
0.10
ug/L
Toxaphene
BRL
1.0
ug/L
Surrogate: Decachlorobiphenyl
0.560
ug/L
1.000
56
13-186
Surrogate: Tetrachloro-m-xylene
0.630
ug/L
1.000
63
40-134
LCS (POJ0286-BS1)
Prepared: 10/16/20 Analyzed: 10/19/20
4,4'-DDD
0.690
0.10
ug/L
1.000
69
56-143
4,4'-DDE
0.700
0.10
ug/L
1.000
70
57-135
4,4'-DDT
0.740
0.10
ug/L
1.000
74
51-143
Aldrin
0.640
0.050
ug/L
1.000
64
45-134
alpha-BHC
0.680
0.050
ug/L
1.000
68
54-138
cis -Chlordane
0.680
0.10
ug/L
1.000
68
60-129
beta-BHC
0.640
0.050
ug/L
1.000
64
56-136
delta-BHC
0.680
0.050
ug/L
1.000
68
52-142
Dieldrin
0.710
0.050
ug/L
1.000
71
60-136
Endosulfan 1
0.690
0.050
ug/L
1.000
69
62-126
Endosulfan II
0.710
0.050
ug/L
1.000
71
52-135
Endosulfan Sulfate
0.670
0.050
ug/L
1.000
67
62-133
Endrin
0.790
0.050
ug/L
1.000
79
60-138
Endrin Aldehyde
0.630
0.050
ug/L
1.000
63
51-132
Endrin Ketone
0.670
0.10
ug/L
1.000
67
58-134
gamma-BHC
0.670
0.050
ug/L
1.000
67
59-134
trans -Chlordane
0.670
0.10
ug/L
1.000
67
56-136
Heptachlor
0.670
0.050
ug/L
1.000
67
54-130
Heptachlor Epoxide
0.690
0.10
ug/L
1.000
69
61-133
Methoxychlor
0.710
0.10
ug/L
1.000
71
54-145
Surrogate: Decachlorobiphenyl
0.500
ug/L
1.000
50
13-186
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 of 62
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/31 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
LCS (POJ0286-BS1)
Prepared: 10/16/20 Analyzed: 10/19/20
Surrogate: Tetrachloro-m-xylene
0.730
ug/L
1.000
73
40-134
LCS (POJ0286-BS2)
Prepared: 10/16/20 Analyzed: 10/19/20
Chlordane
7.87
0.50
ug/L
10.00
79
62-140
Surrogate: Decachlorobiphenyl
0.580
ug/L
1.000
58
13-186
Surrogate: Tetrachloro-m-xylene
0.630
ug/L
1.000
63
40-134
LCS (POJ0286-BS3)
Prepared: 10/16/20 Analyzed: 10/19/20
Toxaphene
9.00
1.0
ug/L
10.00
90
33-134
Surrogate: Decachlorobiphenyl
0.510
ug/L
1.000
51
13-186
Surrogate: Tetrachloro-m-xylene
0.690
ug/L
1.000
69
40-134
LCS Dup (POJ0286-BSD1)
Prepared: 10/16/20 Analyzed: 10/19/20
4,4'-DDD
0.660
0.10
ug/L
1.000
66
56-143
4
30
4,4'-DDE
0.670
0.10
ug/L
1.000
67
57-135
4
30
4,4'-DDT
0.710
0.10
ug/L
1.000
71
51-143
4
30
Aldrin
0.610
0.050
ug/L
1.000
61
45-134
5
30
alpha-BHC
0.660
0.050
ug/L
1.000
66
54-138
3
30
cis -Chlordane
0.650
0.10
ug/L
1.000
65
60-129
5
30
beta-BHC
0.570
0.050
ug/L
1.000
57
56-136
12
30
delta-BHC
0.620
0.050
ug/L
1.000
62
52-142
9
30
Dieldrin
0.680
0.050
ug/L
1.000
68
60-136
4
30
Endosulfan 1
0.670
0.050
ug/L
1.000
67
62-126
3
30
Endosulfan 11
0.690
0.050
ug/L
1.000
69
52-135
3
30
Endosulfan Sulfate
0.630
0.050
ug/L
1.000
63
62-133
6
30
Endrin
0.750
0.050
ug/L
1.000
75
60-138
5
30
Endrin Aldehyde
0.600
0.050
ug/L
1.000
60
51-132
5
30
Endrin Ketone
0.650
0.10
ug/L
1.000
65
58-134
3
30
gamma-BHC
0.640
0.050
ug/L
1.000
64
59-134
5
30
trans -Chlordane
0.640
0.10
ug/L
1.000
64
56-136
5
30
Heptachlor
0.640
0.050
ug/L
1.000
64
54-130
5
30
Heptachlor Epoxide
0.670
0.10
ug/L
1.000
67
61-133
3
30
Methoxychlor
0.680
0.10
ug/L
1.000
68
54-145
4
30
Surrogate: Decachlorobiphenyl
0.560
ug/L
1.000
56
13-186
Surrogate: Tetrachloro-m-xylene
0.680
ug/L
1.000
68
40-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 of 62
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/31 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
Matrix Spike (POJ0286-MS1)
Source: 0100174-01
Prepared: 10/16/20 Analyzed: 10/19/20
4,4'-DDD
BRL
0.22
ug/L
BRL
56-143
4,4'-DDE
BRL
0.22
ug/L
BRL
57-135
4,4'-DDT
BRL
0.22
ug/L
BRL
51-143
Aldrin
BRL
0.11
ug/L
BRL
45-134
alpha-BHC
BRL
0.11
ug/L
BRL
54-138
cis -Chlordane
BRL
0.22
ug/L
BRL
60-129
beta-BHC
BRL
0.11
ug/L
BRL
56-136
Chlordane
BRL
1.1
ug/L
BRL
62-140
delta-BHC
BRL
0.11
ug/L
BRL
52-142
Dieldrin
BRL
0.11
ug/L
BRL
60-136
Endosulfan I
BRL
0.11
ug/L
BRL
62-126
Endosulfan II
BRL
0.11
ug/L
BRL
52-135
Endosulfan Sulfate
BRL
0.11
ug/L
BRL
62-133
Endrin
BRL
0.11
ug/L
BRL
60-138
Endrin Aldehyde
BRL
0.11
ug/L
BRL
51-132
Endrin Ketone
BRL
0.22
ug/L
BRL
58-134
gamma-BHC
BRL
0.11
ug/L
BRL
59-134
trans -Chlordane
BRL
0.22
ug/L
BRL
56-136
Heptachlor
BRL
0.11
ug/L
BRL
54-130
Heptachlor Epoxide
BRL
0.22
ug/L
BRL
61-133
Methoxychlor
BRL
0.22
ug/L
BRL
54-145
Toxaphene
BRL
2.2
ug/L
BRL
33-134
Surrogate: Decachlorobiphenyl
1.00
ug/L
2.222
45 13-186
Surrogate: Tetrachloro-m-xylene
1.58
ug/L
2.222
71 40-134
Matrix Spike Dup (POJ0286-MSD1)
Source: 0100174-01
Prepared: 10/16/20
Analyzed: 10/19/20
4,4'-DDD
BRL
0.22
ug/L
BRL
56-143
30
4,4'-DDE
BRL
0.22
ug/L
BRL
57-135
30
4,4'-DDT
BRL
0.22
ug/L
BRL
51-143
30
Aldrin
BRL
0.11
ug/L
BRL
45-134
30
alpha-BHC
BRL
0.11
ug/L
BRL
54-138
30
cis -Chlordane
BRL
0.22
ug/L
BRL
60-129
30
beta-BHC
BRL
0.11
ug/L
BRL
56-136
30
Chlordane
BRL
1.1
ug/L
BRL
62-140
30
delta-BHC
BRL
0.11
ug/L
BRL
52-142
30
Dieldrin
BRL
0.11
ug/L
BRL
60-136
30
Endosulfan I
BRL
0.11
ug/L
BRL
62-126
30
Endosulfan II
BRL
0.11
ug/L
BRL
52-135
30
Endosulfan Sulfate
BRL
0.11
ug/L
BRL
62-133
30
Endrin
BRL
0.11
ug/L
BRL
60-138
30
Endrin Aldehyde
BRL
0.11
ug/L
BRL
51-132
30
Endrin Ketone
BRL
0.22
ug/L
BRL
58-134
30
gamma-BHC
BRL
0.11
ug/L
BRL
59-134
30
trans -Chlordane
BRL
0.22
ug/L
BRL
56-136
30
Heptachlor
BRL
0.11
ug/L
BRL
54-130
30
Heptachlor Epoxide
BRL
0.22
ug/L
BRL
61-133
30
Methoxychlor
BRL
0.22
ug/L
BRL
54-145
30
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
Matrix Spike Dup (POJ0286-MSD1) Source: 0100174-01 Prepared: 10/16/20 Analyzed: 10/19/20
Toxaphene BRL 2.2 ug/L BRL 33-134 30
Surrogate: Decachlorobiphenyl 1.31 ug/L 2.222 59 13-186
Surrogate: Tetrachloro-m-xylene 1.47 ug/L 2.222 66 40-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 39 of 62
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/31 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
Blank (POJ0286-BLK1)
Prepared: 10/16/20 Analyzed: 10/19/20
Aroclor 1016
BRL
0.50
ug/L
Aroclor 1221
BRL
1.0
ug/L
Aroclor 1232
BRL
0.50
ug/L
Aroclor 1242
BRL
0.50
ug/L
Aroclor 1248
BRL
0.50
ug/L
Aroclor 1254
BRL
0.50
ug/L
Aroclor 1260
BRL
1.0
ug/L
Surrogate: Tetrachloro-m-xylene
0.610
ug/L
1.000
61
30-161
Surrogate: Decachlorobiphenyl
0.580
ug/L
1.000
58
32-178
LCS (POJ0286-BS4)
Prepared: 10/16/20
Analyzed: 10/19/20
Aroclor 1016
6.63
0.50
ug/L
10.00
66
50-114
Aroclor 1221
BRL
1.0
ug/L
15-178
Aroclor 1232
BRL
0.50
ug/L
10-215
Aroclor 1242
BRL
0.50
ug/L
39-150
Aroclor 1248
BRL
0.50
ug/L
38-158
Aroclor 1254
BRL
0.50
ug/L
29-131
Aroclor 1260
7.65
1.0
ug/L
10.00
76
10-127
Surrogate: Tetrachloro-m-xylene
0.620
ug/L
1.000
62
30-161
Surrogate: Decachlorobiphenyl
0.690
ug/L
1.000
69
32-178
Matrix Spike (POJ0286-MS1)
Source: 0100174-01
Prepared: 10/16/20
Analyzed: 10/19/20
Aroclor 1016
15.2
1.1
ug/L
22.22 BRL
68
50-114
Aroclor 1221
BRL
2.2
ug/L
BRL
15-178
Aroclor 1232
BRL
1.1
ug/L
BRL
10-215
Aroclor 1242
BRL
1.1
ug/L
BRL
39-150
Aroclor 1248
BRL
1.1
ug/L
BRL
38-158
Aroclor 1254
BRL
1.1
ug/L
BRL
29-131
Aroclor 1260
15.0
2.2
ug/L
22.22 BRL
68
10-127
Surrogate: Tetrachloro-m-xylene
1.58
ug/L
2.222
71
30-161
Surrogate: Decachlorobiphenyl
1.00
ug/L
2.222
45
32-178
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Asheville, NC 28801
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
Matrix Spike Dup (POJ0286-MSD1)
Source: 0100174-01
Prepared:
10/16/20
Analyzed: 10/19/20
Aroclor 1016
14.4
1.1
ug/L
22.22
BRL
65
50-114 6
50
Aroclor 1221
BRL
2.2
ug/L
BRL
15-178
50
Aroclor 1232
BRL
1.1
ug/L
BRL
10-215
50
Aroclor 1242
BRL
1.1
ug/L
BRL
39-150
50
Aroclor 1248
BRL
1.1
ug/L
BRL
38-158
50
Aroclor 1254
BRL
1.1
ug/L
BRL
29-131
50
Aroclor 1260
15.7
2.2
ug/L
22.22
BRL
71
10-127 5
50
Surrogate: Tetrachloro-m-xylene
1.47
ug/L
2.222
66
30-161
Surrogate: Decachlorobiphenyl
1.31
ug/L
2.222
59
32-178
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 41 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0239 - 3005A
Blank (POJ0239-BLK1)
Prepared: 10/15/20 Analyzed: 10/23/20
Antimony
BRL
2.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
2.0
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
2.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
BRL
3.0
ug/L
Selenium
BRL
5.0
ug/L
Thallium
BRL
2.0
ug/L
Tin
BRL
5.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
LCS (POJ0239-BS1)
Prepared: 10/15/20 Analyzed: 10/23/20
Antimony
103
2.0
ug/L
100.0
103
80-120
Arsenic
96.8
1.0
ug/L
100.0
97
80-120
Barium
99.1
2.0
ug/L
100.0
99
80-120
Beryllium
93.3
1.0
ug/L
100.0
93
80-120
Cadmium
98.1
1.0
ug/L
100.0
98
80-120
Chromium
96.2
2.0
ug/L
100.0
96
80-120
Cobalt
100
2.0
ug/L
100.0
100
80-120
Copper
97.5
10
ug/L
100.0
97
80-120
Lead
98.4
1.0
ug/L
100.0
98
80-120
Nickel
98.4
3.0
ug/L
100.0
98
80-120
Selenium
93.8
5.0
ug/L
100.0
94
80-120
Thallium
96.8
2.0
ug/L
100.0
97
80-120
Tin
102
5.0
ug/L
100.0
102
80-120
Vanadium
96.5
5.0
ug/L
100.0
97
80-120
Zinc
94.1
20
ug/L
100.0
94
80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 42 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0374 - 7470A
Blank (POJ0374-BLK1) Prepared & Analyzed: 10/20/20
Mercury BRL 0.20 ug/L
LCS (POJ0374-BS1) Prepared &Analyzed: 10/20/20
Mercury 8.17 0.20 ug/L 9.375 87 80-120
Batch POJ0490 - 3005A
Blank (POJ0490-BLK1) Prepared & Analyzed: 10/27/20
Silver BRL 1.0 ug/L
LCS (POJ0490-BS1) Prepared &Analyzed: 10/27/20
Silver 97.6 1.0 ug/L 100.0 98 80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 43 of 62
Level II QC Report
0int 12/31/20
Waypo
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Dissolved Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POL0504 - 7470A
Blank (POL0504-BLK1)
Prepared & Analyzed: 12/28/20
Mercury
BRL 0.20 ug/L
LCS (POL0504-BS1)
Prepared &Analyzed: 12/28/20
Mercury
9.67 0.20 ug/L
9.375 103
80-120
Matrix Spike (POL0504-MS1)
Source: 0100174-01
Prepared & Analyzed: 12/28/20
Mercury
6.23 0.20 ug/L
9.375 BRL 66
80-120 MI
Matrix Spike Dup (POL0504-MSD1)
Source: 0100174-01
Prepared & Analyzed: 12/28/20
Mercury
6.17 0.20 ug/L
9.375 BRL 66
80-120 0.9 20 MI
Post Spike (POL0504-PS1)
Source: 0100174-01
Prepared & Analyzed: 12/28/20
Mercury
2.73 ug/L
3.750-0.00536 73
85-115 MI
Batch POL0558 - 3005A
Blank (POL0558-BLK1)
Prepared & Analyzed: 12/30/20
Antimony
BRL
2.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
10
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
2.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
BRL
3.0
ug/L
Selenium
1.22
5.0
ug/L J
Silver
BRL
1.0
ug/L
Thallium
BRL
2.0
ug/L
Tin
BRL
5.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 44 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Dissolved Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POL0558 - 3005A
LCS (POL0558-BS1)
Prepared &Analyzed: 12/30/20
Antimony
86.6
2.0
ug/L
100.0
87
80-120
Arsenic
97.2
1.0
ug/L
100.0
97
80-120
Barium
98.0
10
ug/L
100.0
98
80-120
Beryllium
95.8
1.0
ug/L
100.0
96
80-120
Cadmium
99.0
1.0
ug/L
100.0
99
80-120
Chromium
101
2.0
ug/L
100.0
101
80-120
Cobalt
100
2.0
ug/L
100.0
100
80-120
Copper
97.1
10
ug/L
100.0
97
80-120
Lead
97.6
1.0
ug/L
100.0
98
80-120
Nickel
99.0
3.0
ug/L
100.0
99
80-120
Selenium
105
5.0
ug/L
100.0
105
80-120
Silver
97.8
1.0
ug/L
100.0
98
80-120
Thallium
96.9
2.0
ug/L
100.0
97
80-120
Tin
96.2
5.0
ug/L
100.0
96
80-120
Vanadium
97.8
5.0
ug/L
100.0
98
80-120
Zinc
93.2
20
ug/L
100.0
93
80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 45 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Anions by Ion Chromatography - Quality Control
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0250 - NO PREP
Blank (POJ0250-BLK1)
Prepared & Analyzed: 10/14/20
Chloride
BRL
1000
ug/L
Nitrate as N
BRL
200
ug/L
Sulfate
BRL
2000
ug/L
LCS (POJ0250-BS1)
Prepared &Analyzed: 10/14/20
Chloride
41200
1000
ug/L
40000 103
80-120
Nitrate as N
4010
210
ug/L
4000 100
80-120
Sulfate
41400
2100
ug/L
40000 104
80-120
Matrix Spike (POJ0250-MS1)
Source: 0100174-03
Prepared & Analyzed: 10/14/20
Chloride
42600
1000
ug/L
40000 1100 104
80-120
Nitrate as N
4110
210
ug/L
4000 96.3 100
80-120
Sulfate
43700
2100
ug/L
40000 828 107
80-120
Matrix Spike Dup (POJ0250-MSD1)
Source: 0100174-03
Prepared & Analyzed: 10/14/20
Chloride
42200
1000
ug/L
40000 1100 103
80-120 0.9 15
Nitrate as N
4050
210
ug/L
4000 96.3 99
80-120 1 15
Sulfate
43000
2100
ug/L
40000 828 105
80-120 2 15
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 46 of 62
• 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Batch POJ0276 - NO PREP
Level II QC Report
12/31 /20
Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Project No: 50-02
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (POJ0276-BLK1) Prepared & Analyzed: 10/14/20
Biochemical Oxygen Demand BRL 2000 ug/L
LCS (POJ0276-BS1) Prepared &Analyzed: 10/14/20
Biochemical Oxygen Demand 189000 2000 ug/L 198000 95 84.6-115.4
Batch POJ0282 - NO PREP
Blank (POJ0282-BLK1) Prepared & Analyzed: 10/15/20
Ferrous Iron BRL 200 ug/L
LCS (POJ0282-BSI) Prepared &Analyzed: 10/15/20
Ferrous Iron 1930 200 ug/L 2000 96 90-110
Matrix Spike (POJ0282-MS1) Source: 0100174-03 Prepared & Analyzed: 10/15/20
Ferrous Iron 1880 200 ug/L 2000 BRL 94 80-120 HT
Matrix Spike Dup (POJ0282-MSD1) Source: 0100174-03 Prepared & Analyzed: 10/15/20
Ferrous Iron 1860 200 ug/L 2000 BRL 93 80-120 0.6 20 HT
Batch POJ0337 - SM4500-S C
Blank (POJ0337-BLK1) Prepared & Analyzed: 10/19/20
Sulfide BRL 2000 ug/L
LCS (POJ0337-BS1) Prepared &Analyzed: 10/19/20
Sulfide 7900 2000 ug/L 10000 79 70-122
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
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Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 47 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0341 - NO PREP
Blank (POJ0341-BLK1) Prepared & Analyzed: 10/19/20
Total Alkalinity to pH 4.5 BRL 5000 ug/L
LCS (POJ0341-BS1) Prepared &Analyzed: 10/19/20
Total Alkalinity to pH 4.5 249000 5000 ug/L 90-110
Batch POJ0357 - 901OC
Blank (POJ0357-BLK1) Prepared & Analyzed: 10/20/20
Cyanide BRL 0.025 mg/L
LCS (POJ0357-BS1) Prepared &Analyzed: 10/20/20
Cyanide 0.0965 0.025 mg/L 0.1000 96 85-115
Batch POJ0361 - NO PREP
Blank (POJ0361-BLK1) Prepared & Analyzed: 10/19/20
Chemical Oxygen Demand BRL 50000 ug/L
LCS (POJ0361-BS1) Prepared &Analyzed: 10/19/20
Chemical Oxygen Demand 498000 50000 ug/L 90-110
Batch POL0392 - NO PREP
LCS (POL0392-BS1) Prepared &Analyzed: 12/18/20
pH 6.87 pH Units 6.870 100 98.5-101.5
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Page 48 of 62
• 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POL0392 - NO PREP
Duplicate (POL0392-DUP1) Source: 0100174-03 Prepared &Analyzed: 12/18/20
pH 7.10 pH Units 7.12 0.281 10 HT
Temperature 20.0 °C 20.0 0.00 20 HT
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 49 of 62
0int-
Level II QC Report
Waypo
12/31/20
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill
2020 Fall
Work Order: 0100174
Attn: Alec Macbeth
Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street
Project No: 50-02
Asheville, NC 28801
8270 Extended List - Quality Control
Reporting
Spike
Source
%REC
RPD
Analyte
Result
Limit
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Batch L517325 - 3510C
BSD (0100174 LCSD-L517325)
Source: 0100174 LCS-L517Prepared:
10/19/20
Analyzed:
10/21/20
5-Nitro-o-toluidine
48.6
10.0
pg/L
50
45.1
97.2
20-120
7.4
20
o-Toluidine
29.9
10.0
pg/L
50
29.4
59.8
20-120
1.6
20
3-Methylcholanthrene
57.1
10.0
pg/L
50
53
114
20-120
7.4
20
4-Aminobiphenyl
38.8
10.0
pg/L
50
37
77.6
20-120
4.7
20
N-Nitrosopyrrolidine
34.3
10.0
pg/L
50
34.4
68.6
20-120
0.2
20
N-Nitrosopiperidine
34.1
10.0
pg/L
50
33.6
68.2
20-120
1.4
20
N-Nitrosomethylethylamine
27.4
10.0
pg/L
50
26.2
54.8
20-120
4.4
20
7,12-Dimethylbenz(a)anthracene
58.1
10.0
pg/L
50
48.7
116
20-120
17.6
20
Methapyrilene
49.8
10.0
pg/L
50
35.1
99.6
20-120
34.6
20 LCD2
2-Naphthylamine
20.3
10.0
pg/L
50
22.7
40.6
20-120
11.1
20
Hexachloropropene
22.6
10.0
pg/L
50
18.9
45.2
20-120
17.8
20
p-Phenylenediamine
0
10.0
pg/L
50
0
0
20-120
0
20 L
Diallate
48.4
10.0
pg/L
50
48.3
96.8
20-120
0.2
20
Pronamide
56.1
10.0
pg/L
50
51
112
20-120
9.5
20
p-Dimethylaminoazobenzene
61.3
10.0
pg/L
50
51.1
123
20-120
18.1
20 LH
Safrole
39.9
10.0
pg/L
50
39.7
79.8
20-120
0.5
20
Kepone
60
10.0
pg/L
50
53.4
120
20-120
11.6
20
2-Acetylaminofluorene
49.1
10.0
pg/L
50
53.1
98.2
20-120
7.8
20
1-Naphthylamine
28.8
10.0
pg/L
50
28.9
57.6
20-120
0.3
20
1,3,5-Trinitrobenzene
65.8
10.0
pg/L
50
60.4
132
20-120
8.5
20 LH
Isosafrole
43.9
10.0
pg/L
50
41.9
87.8
20-120
4.6
20
1,4-Naphthoquinone
44.6
10.0
pg/L
50
41.7
89.2
20-120
6.7
20
BS (0100174 LCS-L517325)
Prepared:
10/19/20
Analyzed:
10/21/20
Isosafrole
41.9
10.0
pg/L
50
83.8
20-120
Kepone
53.4
10.0
pg/L
50
107
20-120
Safrole
39.7
10.0
pg/L
50
79.4
20-120
Methapyrilene
35.1
10.0
pg/L
50
70.2
20-120
p-Dimethylaminoazobenzene
51.1
10.0
pg/L
50
102
20-120
Pronamide
51
10.0
pg/L
50
102
20-120
N-Nitrosopiperidine
33.6
10.0
pg/L
50
67.2
20-120
p-Phenylenediamine
0
10.0
pg/L
50
0
20-120
L
N-Nitrosopyrrolidine
34.4
10.0
pg/L
50
68.8
20-120
o-Toluidine
29.4
10.0
pg/L
50
58.8
20-120
N-Nitrosomethylethylamine
26.2
10.0
pg/L
50
52.4
20-120
5-Nitro-o-toluidine
45.1
10.0
pg/L
50
90.2
20-120
2-Naphthylamine
22.7
10.0
pg/L
50
45.4
20-120
3-Methylcholanthrene
53
10.0
pg/L
50
106
20-120
4-Aminobiphenyl
37
10.0
pg/L
50
74
20-120
1-Naphthylamine
28.9
10.0
pg/L
50
57.8
20-120
2-Acetylaminofluorene
53.1
10.0
pg/L
50
106
20-120
1,4-Naphthoquinone
41.7
10.0
pg/L
50
83.4
20-120
7,12-Dimethylbenz(a)anthracene
48.7
10.0
pg/L
50
97.4
20-120
Diallate
48.3
10.0
pg/L
50
96.6
20-120
Hexachloropropene
18.9
10.0
pg/L
50
37.8
20-120
1,3,5-Trinitrobenzene
60.4
10.0
pg/L
50
121
20-120
LH
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 50 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
8270 Extended List - Quality Control
Analyte
Batch L517325 - 3510C
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
BILK (0100174 LRB-L517325)
Prepared: 10/19/20 Analyzed: 10/20/20
Safrole
U
10.0
pg/L -
1,4-Naphthoquinone
U
10.0
pg/L
2-Naphthylamine
U
10.0
pg/L
Kepone
U
10.0
pg/L
p-Phenylenediamine
U
10.0
pg/L
Hexachloropropene
U
10.0
pg/L
p-Dimethylaminoazobenzene
U
10.0
pg/L
1,3,5-Trinitrobenzene
U
10.0
pg/L
2-Acetylaminofluorene
U
10.0
pg/L
Pronamide
U
10.0
pg/L
Methapyrilene
U
20.0
pg/L
1-Naphthylamine
U
10.0
pg/L
o-Toluidine
U
10.0
pg/L
Isosafrole
U
10.0
pg/L
Diallate
U
10.0
pg/L
7,12-Dimethylbenz(a)anthracene
U
10.0
pg/L
N-Nitrosomethylethylamine
U
10.0
pg/L
5-Nitro-o-toluidine
U
10.0
pg/L
4-Aminobiphenyl
U
10.0
pg/L
N-Nitrosopiperidine
U
10.0
pg/L
N-Nitrosopyrrolidine
U
10.0
pg/L
3-Methylcholanthrene
U
10.0
pg/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 51 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Phenoxy Acid Herbicides - GC/ECD - Quality Control
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517362 - 8151A
BSD (0100174 LCSD-L517362)
Source: 0100174 LCS-L517Prepared: 10/19/20 Analyzed: 10/20/20
2,4,5-T
0.2697
0.01002
pg/L
0.5
0.2279
53.9
20-120
16.8
20
2,4-D
2.493
0.2078
pg/L
5
1.997
49.8
20-120
22
20
LCD2
Dalapon
3.626
0.5149
pg/L
12.5
4.011
29
20-120
10
20
Dichlorprop
2.547
0.07959
pg/L
5
2.019
50.9
20-120
23.1
20
LCD2
2,4-DB
2.624
0.1364
pg/L
5
2.123
52.4
20-120
21.1
20
LCD2
Dinoseb
1.507
0.02698
pg/L
2.5
1.16
60.2
20-120
26
20
LCD2
Dicamba
0.255
0.05700
pg/L
0.5
0.2384
51
20-120
6.7
20
MCPA
250.8
18.98
pg/L
500
200.4
50.1
20-120
22.3
20
LCD2
MCPP
301.9
11.75
pg/L
500
258.1
60.3
20-120
15.6
20
Picloram
0.6016
0.04528
pg/L
1.25
0.4532
48.1
20-120
28.1
20
LCD2
2,4,5-TP (Silvex)
0.2371
0.01634
pg/L
0.5
0.187
47.4
20-120
23.6
20
LCD2
Surrogate: DCAA
1.393
ug/L
2.5
1.156
55.7
20-150
BS (0100174 LCS-L517362)
Prepared:
10/19/20 Analyzed:
10/20/20
MCPA
200.4
18.98
pg/L
500
40
20-120
Dinoseb
1.16
0.02698
pg/L
2.5
46.4
20-120
MCPP
258.1
11.75
pg/L
500
51.6
20-120
Dichlorprop
2.019
0.07959
pg/L
5
40.3
20-120
Dicamba
0.2384
0.05700
pg/L
0.5
47.6
20-120
Picloram
0.4532
0.04528
pg/L
1.25
36.2
20-120
2,4-D
1.997
0.2078
pg/L
5
39.9
20-120
Dalapon
4.011
0.5149
pg/L
12.5
32
20-120
2,4,5-T
0.2279
0.01002
pg/L
0.5
45.5
20-120
2,4-DB
2.123
0.1364
pg/L
5
42.4
20-120
2,4,5-TP (Silvex)
0.187
0.01634
pg/L
0.5
37.4
20-120
Surrogate: DCAA
1.156
ug/L
2.5
46.2
20-150
BLK (0100174 LRB-L517362)
Prepared:
10/19/20 Analyzed:
10/20/20
2,4,5-TP (Silvex)
U
0.1000
pg/L
-
Picloram
U
0.1000
pg/L
2,4,5-T
U
0.03000
pg/L
Dicamba
U
0.1000
pg/L
MCPP
U
50.00
pg/L
MCPA
U
50.00
pg/L
2,4-DB
U
0.1000
pg/L
Dinoseb
U
0.1000
pg/L
Dichlorprop
U
0.1000
pg/L
Dalapon
U
0.5500
pg/L
2,4-D
U
0.2500
pg/L
-
Surrogate: DCAA
1.286
ug/L
2.5
51.4
20-150
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 52 of 62
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/31 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BSD (0100174 LCSD-L517328)
Source: 0100174
LCS-L517Prepared
& Analyzed:
10/19/20
3,3'-Dichlorobenzidine
112
3.74
pg/L
150
95.9
74.6
6-192
15.4
20
Dimethyl phthalate
36.4
0.510
pg/L
50
33
72.8
34-123
9.7
20
3,3' Dimethylbenzidine
76.3
1.88
pg/L
200
55.8
38.1
6-192
31
20
LCD2
Diethyl phthalate
36.5
0.585
pg/L
50
33.6
73
36-130
8.2
20
Dibenzofuran
36.3
0.423
pg/L
50
33.2
72.6
40-108
8.9
20
3-Nitroaniline
36.9
1.53
pg/L
50
32.3
73.8
28-142
13.2
20
Benzidine
49.1
0.689
pg/L
150
37.5
32.7
2-176
26.7
20
LCD2
Dibenz(a,h)anthrace ne
34.2
0.252
pg/L
50
29.9
68.4
27-124
13.4
20
Hexachlorobenzene
36.2
2.57
pg/L
50
33.6
72.4
18-136
7.4
20
4,6-Dinitro-2-methylphenol
35.7
3.47
pg/L
50
47.1
71.4
27-128
27.5
20
LCD2
Di-n-butyl phthalate
37
1.58
pg/L
50
34.5
74
19-158
6.9
20
2-Nitrophenol
32.4
0.606
pg/L
50
28.6
64.8
25-114
12.4
20
Di-n-Octyl Phthalate
44.9
1.72
pg/L
50
36.4
89.8
29-136
20.9
20
LCD2
2-Nitroaniline
38.4
0.574
pg/L
50
35
76.8
32-127
9.2
20
2-Methylphenol
25
0.721
pg/L
50
22
50
22-97
12.7
20
Fluoranthene
39
0.406
pg/L
50
36
78
28-127
8
20
4-Bromophenyl phenyl ether
36.7
0.500
pg/L
50
33.4
73.4
31-124
9.4
20
2-Methyl naphthalene
32.1
0.485
pg/L
50
29.7
64.2
34-108
7.7
20
4-Nitrophenol
11.3
1.39
pg/L
50
10.6
22.6
1-76
6.3
20
Hexachlorobutadiene
25.5
0.405
pg/L
50
22.5
51
22-109
12.5
20
Hexachlorocyclopentadiene
12.1
2.34
pg/L
50
13.9
24.2
10-102
13.8
20
Fluorene
34.1
0.444
pg/L
50
31.4
68.2
41-116
8.2
20
Benzyl alcohol
23.8
3.01
pg/L
50
20.5
47.6
20-109
14.8
20
2-Chlorophenol
28.4
0.736
pg/L
50
25
56.8
27-102
12.7
20
Benzo(a)pyrene
35.5
1.00
pg/L
50
30.9
71
34-131
13.8
20
Benzo(b)fluoranthene
41.4
0.941
pg/L
50
38.4
82.8
36-131
7.5
20
Anthracene
36.1
0.467
pg/L
50
33.8
72.2
34-128
6.5
20
Benzo(g,h,i)perylene
33.7
1.36
pg/L
50
30.6
67.4
26-123
9.6
20
Aniline
22.1
0.316
pg/L
50
18.1
44.2
16-133
19.9
20
Acetophenone
31.3
0.686
pg/L
50
27.2
62.6
25-108
14
20
Benzo(k)fluoranthene
43.7
0.752
pg/L
50
34.5
87.4
32-132
23.5
20
LCD2
Acenaphthylene
32.8
0.429
pg/L
50
29.7
65.6
37-114
9.9
20
Bis(2-Chloroisopropyl)ether
22.2
0.546
pg/L
50
19.4
44.4
28-108
13.4
20
Acenaphthene
31.1
0.422
pg/L
50
27.4
62.2
38-117
12.6
20
Chrysene
36
0.731
pg/L
50
32.3
72
30-124
10.8
20
Bis(2-Chloroethoxy)methane
30.7
0.433
pg/L
50
27.3
61.4
20-126
11.7
20
Bis(2-Chloroethyl)ether
28.8
0.447
pg/L
50
25.1
57.6
16-122
13.7
20
4-Nitroaniline
53.9
0.740
pg/L
50
52.8
108
23-139
2
20
4-Chlorophenyl phenyl ether
34.8
0.479
pg/L
50
32.5
69.6
39-110
6.8
20
Bis(2-ethylhexyl)phthalate
37.9
3.66
pg/L
50
37.4
75.8
21-162
1.3
20
Butyl benzyl phthalate
38.1
4.59
pg/L
50
39.7
76.2
33-142
4.1
20
4-Chloroaniline
28.7
0.526
pg/L
50
24.4
57.4
24-127
16.1
20
Carbazole
42.2
0.476
pg/L
50
39.1
84.4
20-147
7.6
20
4-Chloro-3-methylphenol
36.3
0.503
pg/L
50
32.5
72.6
35-117
11
20
Benzoic Acid
18.9
5.00
pg/L
150
30.6
12.6
11-68
47.2
20
LCD2
Phenanthrene
36.1
0.464
pg/L
50
33.2
72.2
40-120
8.3
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 53 of 62
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/31 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BSD (0100174 LCSD-L517328)
Source: 0100174 LCS-L517Prepared & Analyzed: 10/19/20
2,4-Dichlorophenol
25.7
1.52
pg/L
50
23.3
51.4
32-110
9.7
20
N-Nitrosodiethylamine
32.6
0.400
pg/L
50
28.1
65.2
25-107
14.8
20
N-Nitrosodimethylamine
15.1
0.249
pg/L
50
12.8
30.2
14-84
16.4
20
N-Nitroso-di-n-butylamine
30
0.752
pg/L
50
26.5
60
25-126
12.3
20
N-Nitroso-di-n-propylamine
28.9
0.334
pg/L
50
25.3
57.8
29-114
13.2
20
2,4,5-Trichlorophenol
39.4
0.350
pg/L
50
35.1
78.8
26-118
11.5
20
N-Nitrosodiphenylamine
31
0.783
pg/L
50
27.7
62
45-135
11.2
20
2,3,4,6-Tetrachlorophenol
38.5
0.355
pg/L
50
35.7
77
28-118
7.5
20
2,4-Dimethylphenol
33.7
0.674
pg/L
50
30.2
67.4
34-105
10.9
20
1,4-Dichlorobenzene
24.8
0.580
pg/L
50
21.3
49.6
24-99
15.1
20
2,4,6-Trichlorophenol
38.5
0.344
pg/L
50
34.3
77
26-115
11.5
20
1,3-Dichlorobenzene
24.2
0.491
pg/L
50
20.6
48.4
21-102
16
20
Phenol
11.9
0.389
pg/L
50
10.5
23.8
11-55
12.5
20
Benzo(a)anthracene
35.3
0.427
pg/L
50
32.5
70.6
36-127
8.2
20
1,2-Dichlorobenzene
25.5
0.629
pg/L
50
22.5
51
26-100
12.5
20
3&4 Methylphenol
26.8
0.691
pg/L
50
23.7
53.6
21-96
12.2
20
Pyrene
33
1.04
pg/L
50
40.7
66
20-154
20.8
20 L
1,2,4-Trichlorobenzene
27.3
0.482
pg/L
50
24.3
54.6
23-106
11.6
20
1,2,4,5-Tetrachlorobenzene
30.2
0.317
pg/L
50
26.8
60.4
28-110
11.9
20
Pyridine
15.7
0.678
pg/L
50
12.9
31.4
10-71
19.5
20
Pentachlorophenol
48.7
2.45
pg/L
50
49.5
97.4
17-142
1.6
20
Naphthalene
28
0.484
pg/L
50
24.7
56
33-108
12.5
20
2,6-Dichlorophenol
35.5
0.703
pg/L
50
31.1
71
25-112
13.2
20
Isophorone
26.6
0.360
pg/L
50
23.3
53.2
31-116
13.2
20
2,6-Dinitrotoluene
36.8
0.413
pg/L
50
33.5
73.6
36-125
9.3
20
Nitrobenzene
30
0.531
pg/L
50
26.3
60
27-117
13.1
20
2-Chloronaphthalene
29.5
0.476
pg/L
50
26
59
29-137
12.6
20
2,4-Dinitrotoluene
35.3
0.403
pg/L
50
33.4
70.6
24-147
5.5
20
2,4-Dinitrophenol
77.8
4.85
pg/L
150
103
51.8
10-132
27.8
20 LCD2
Hexachloroethane
21.7
0.277
pg/L
50
19
43.4
16-107
13.2
20
Indeno(1,2,3-cd)pyrene
40.4
1.01
pg/L
50
33.1
80.8
22-126
19.8
20
Surrogate:2-Fluorophenol
23.5
pg/L
100
20.2
23.5
10-44
Surrogate:2-Fluorobiphenyl
45
pg/L
100
43.6
45
24-93
Surrogate: Phenol-d6
16.4
pg/L
100
14.8
16.4
7-32
Surrogate:4-Terphenyl-d14
55.2
pg/L
100
74.7
55.2
35-126
Surrogate: 2,4,6-Tribromophenol
67.8
pg/L
100
63.3
67.8
39-110
Surrogate: Nitrobenzene-d5
49.7
pg/L
100
47.4
49.7
20-91
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 54 of 62
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/31 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100174
Attn: Alec Macbeth Time Submitted: 10/14/2020 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BS (0100174 LCS-L517328)
Prepared & Analyzed: 10/19/20
Isophorone
23.3
0.360
pg/L
50
46.6
31-116
Phenol
10.5
0.389
pg/L
50
21
11-55
Fluorene
31.4
0.444
pg/L
50
62.8
41-116
Phenanthrene
33.2
0.464
pg/L
50
66.4
40-120
Benzyl alcohol
20.5
3.01
pg/L
50
41
20-109
Bis(2-Chloroethoxy)methane
27.3
0.433
pg/L
50
54.6
20-126
Hexachlorobenzene
33.6
2.57
pg/L
50
67.2
18-136
Benzoic Acid
30.6
5.00
pg/L
150
20.4
11-68
Indeno(1,2,3-cd)pyrene
33.1
1.01
pg/L
50
66.2
22-126
Benzo(k)fluoranthene
34.5
0.752
pg/L
50
69
32-132
Benzo(g,h,i)perylene
30.6
1.36
pg/L
50
61.2
26-123
Pyrene
40.7
1.04
pg/L
50
81.4
20-154
Pyridine
12.9
0.678
pg/L
50
25.8
10-71
Benzo(b)fluoranthene
38.4
0.941
pg/L
50
76.8
36-131
Hexachloroethane
19
0.277
pg/L
50
38
16-107
Benzo(a)pyrene
30.9
1.00
pg/L
50
61.8
34-131
Hexachlorobutadiene
22.5
0.405
pg/L
50
45
22-109
Dimethyl phthalate
33
0.510
pg/L
50
66
34-123
N-Nitrosodiethylamine
28.1
0.400
pg/L
50
56.2
25-107
Diethyl phthalate
33.6
0.585
pg/L
50
67.2
36-130
Di-n-butyl phthalate
34.5
1.58
pg/L
50
69
19-158
N-Nitrosodimethylamine
12.8
0.249
pg/L
50
25.6
14-84
Dibenzofuran
33.2
0.423
pg/L
50
66.4
40-108
Dibenz(a,h)anthrace ne
29.9
0.252
pg/L
50
59.8
27-124
Di-n-Octyl Phthalate
36.4
1.72
pg/L
50
72.8
29-136
Pentachlorophenol
49.5
2.45
pg/L
50
99
17-142
Hexachlorocyclopentadiene
13.9
2.34
pg/L
50
27.8
10-102
Bis(2-Chloroethyl)ether
25.1
0.447
pg/L
50
50.2
16-122
Carbazole
39.1
0.476
pg/L
50
78.2
20-147
Nitrobenzene
26.3
0.531
pg/L
50
52.6
27-117
N-Nitroso-di-n-propylamine
25.3
0.334
pg/L
50
50.6
29-114
Butyl benzyl phthalate
39.7
4.59
pg/L
50
79.4
33-142
Naphthalene
24.7
0.484
pg/L
50
49.4
33-108
Fluoranthene
36
0.406
pg/L
50
72
28-127
Bis(2-ethylhexyl)phthalate
37.4
3.66
pg/L
50
74.8
21-162
Bis(2-Chloroisopropyl)ether
19.4
0.546
pg/L
50
38.8
28-108
N-Nitrosodiphenylamine
27.7
0.783
pg/L
50
55.4
45-135
N-Nitroso-di-n-butylamine
26.5
0.752
pg/L
50
53
25-126
Chrysene
32.3
0.731
pg/L
50
64.6
30-124
2,4-Dinitrophenol
103
4.85
pg/L
150
68.6
10-132
2,4,5-Trichlorophenol
35.1
0.350
pg/L
50
70.2
26-118
4-Chlorophenyl phenyl ether
32.5
0.479
pg/L
50
65
39-110
4-Chloroaniline
24.4
0.526
pg/L
50
48.8
24-127
2,4,6-Trichlorophenol
34.3
0.344
pg/L
50
68.6
26-115
4-Bromophenyl phenyl ether
33.4
0.500
pg/L
50
66.8
31-124
2,4-Dichlorophenol
23.3
1.52
pg/L
50
46.6
32-110
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 55 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BS (0100174 LCS-L517328)
Prepared & Analyzed: 10/19/20
4,6-Dinitro-2-methylphenol
47.1
3.47
pg/L
50
94.2
27-128
2,4-Dimethylphenol
30.2
0.674
pg/L
50
60.4
34-105
3-Nitroaniline
32.3
1.53
pg/L
50
64.6
28-142
3,3'-Dichlorobenzidine
95.9
3.74
pg/L
150
63.9
6-192
4-Nitroaniline
52.8
0.740
pg/L
50
106
23-139
3&4 Methylphenol
23.7
0.691
pg/L
50
47.4
21-96
4-Chloro-3-methylphenol
32.5
0.503
pg/L
50
65
35-117
2-Nitrophenol
28.6
0.606
pg/L
50
57.2
25-114
2-Nitroaniline
35
0.574
pg/L
50
70
32-127
2,4-Dinitrotoluene
33.4
0.403
pg/L
50
66.8
24-147
2-Methylphenol
22
0.721
pg/L
50
44
22-97
Benzo(a)anthracene
32.5
0.427
pg/L
50
65
36-127
2,6-Dichlorophenol
31.1
0.703
pg/L
50
62.2
25-112
2,6-Dinitrotoluene
33.5
0.413
pg/L
50
67
36-125
2-Methyl naphthalene
29.7
0.485
pg/L
50
59.4
34-108
2-Chloronaphthalene
26
0.476
pg/L
50
52
29-137
2-Chorophenol
25
0.736
pg/L
50
50
27-102
3,3' Dimethylbenzidine
55.8
1.88
pg/L
200
27.9
6-192
1,4-Dichlorobenzene
21.3
0.580
pg/L
50
42.6
24-99
1,2-Dichlorobenzene
22.5
0.629
pg/L
50
45
26-100
Acetophenone
27.2
0.686
pg/L
50
54.4
25-108
Aniline
18.1
0.316
pg/L
50
36.2
16-133
Acenaphthene
27.4
0.422
pg/L
50
54.8
38-117
1,3-Dichlorobenzene
20.6
0.491
pg/L
50
41.2
21-102
Acenaphthylene
29.7
0.429
pg/L
50
59.4
37-114
1,2,4-Trichlorobenzene
24.3
0.482
pg/L
50
48.6
23-106
Anthracene
33.8
0.467
pg/L
50
67.6
34-128
Benzidine
37.5
0.689
pg/L
150
25
2-176
2,3,4,6-Tetrachlorophenol
35.7
0.355
pg/L
50
71.4
28-118
1,2,4,5-Tetrachlorobenzene
26.8
0.317
pg/L
50
53.6
28-110
4-Nitrophenol
10.6
1.39
pg/L
50
21.2
1-76
Surrogate: Phenol-d6
14.8
Ng/L
100
14.8
7-32
Surrogate: Nitrobenzene-d5
47.4
pg/L
100
47.4
20-91
Surrogate: 2,4,6-Tribromophenol
63.3
Ng/L
100
63.3
39-110
Surrogate:2-Fluorophenol
20.2
Ng/L
100
20.2
10-44
Surrogate:2-Fluorobiphenyl
43.6
Ng/L
100
43.6
24-93
Surrogate:4-Terphenyl-d14
74.7
Ng/L
100
74.7
35-126
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 56 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BILK (0100174 LRB-11-517328)
Prepared & Analyzed: 10/19/20
Indeno(1,2,3-cd)pyrene
U
2.00
pg/L
1,2,4-Trichlorobenzene
U
5.00
pg/L
2,6-Dichlorophenol
U
5.00
pg/L
2,6-Dinitrotoluene
U
5.00
pg/L
Phenol
U
5.00
pg/L
Pyrene
U
2.00
pg/L
Naphthalene
U
2.00
pg/L
1,2-Dichlorobenzene
U
5.00
pg/L
Isophorone
U
5.00
pg/L
2,4-Dinitrotoluene
U
5.00
pg/L
Pyridine
U
10.0
pg/L
1,2,4,5-Tetrachlorobenzene
U
5.00
pg/L
Phenanthrene
U
2.00
pg/L
N-Nitrosodiphenylamine
U
10.0
pg/L
N-Nitroso-di-n-propylamine
U
5.00
pg/L
2,4,5-Trichlorophenol
U
5.00
pg/L
Pentachlorophenol
U
10.0
pg/L
N-Nitroso-di-n-butylamine
U
5.00
pg/L
2-Methyl naphthalene
U
2.00
pg/L
Hexachloroethane
U
5.00
pg/L
N-Nitrosodimethylamine
U
5.00
pg/L
Nitrobenzene
U
5.00
pg/L
1,4-Dichlorobenzene
U
5.00
pg/L
2,4-Dichlorophenol
U
5.00
pg/L
1,3-Dichlorobenzene
U
5.00
pg/L
N-Nitrosodiethylamine
U
5.00
pg/L
2,4-Dimethylphenol
U
5.00
pg/L
2,3,4,6-Tetrachlorophenol
U
5.00
pg/L
2,4-Dinitrophenol
U
10.0
pg/L
2,4,6-Trichlorophenol
U
5.00
pg/L
Acenaphthylene
U
2.00
pg/L
2-Chloronaphthalene
U
5.00
pg/L
Butyl benzyl phthalate
U
5.00
pg/L
Hexachlorobenzene
U
5.00
pg/L
4-Chlorophenyl phenyl ether
U
5.00
pg/L
4-Nitroaniline
U
5.00
pg/L
Bis(2-Chloroisopropyl)ether
U
5.00
pg/L
Bis(2-Chloroethyl)ether
U
5.00
pg/L
4-Nitrophenol
U
10.0
pg/L
Bis(2-Chloroethoxy)methane
U
5.00
pg/L
4-Chloro-3-methylphenol
U
5.00
pg/L
Acenaphthene
U
2.00
pg/L
4-Chloroaniline
U
5.00
pg/L
Benzoic Acid
U
10.0
pg/L
Acetophenone
U
5.00
pg/L
Benzo(k)fluoranthene
U
2.00
pg/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 57 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BILK (0100174 LRB-11-517328)
Prepared & Analyzed: 10/19/20
Benzo(g,h,i)perylene
U
2.00
pg/L
Aniline
U
5.00
pg/L
Anthracene
U
2.00
pg/L
Benzo(b)fluoranthene
U
2.00
pg/L
Benzidine
U
20.0
pg/L
Benzo(a)pyrene
U
2.00
pg/L
Benzo(a)anthracene
U
2.00
pg/L
Benzyl alcohol
U
10.0
pg/L
Di-n-Octyl Phthalate
U
5.00
pg/L
2-Chorophenol
U
5.00
pg/L
Hexachlorocyclopentadiene
U
5.00
pg/L
Hexachlorobutadiene
U
5.00
pg/L
3&4 Methylphenol
U
5.00
pg/L
Fluorene
U
2.00
pg/L
2-Methylphenol
U
5.00
pg/L
Bis(2-ethylhexyl)phthalate
U
5.00
pg/L
Fluoranthene
U
2.00
pg/L
Carbazole
U
5.00
pg/L
Dibenzofuran
U
5.00
pg/L
4-Bromophenyl phenyl ether
U
5.00
pg/L
Chrysene
U
2.00
pg/L
2-Nitroaniline
U
5.00
pg/L
4,6-Dinitro-2-methylphenol
U
10.0
pg/L
2-Nitrophenol
U
5.00
pg/L
3-Nitroaniline
U
10.0
pg/L
3,3'-Dichlorobenzidine
U
10.0
pg/L
Diethyl phthalate
U
5.00
pg/L
3,3' Dimethylbenzidine
U
10.0
pg/L
Dimethyl phthalate
U
5.00
pg/L
Di-n-butyl phthalate
U
5.00
pg/L
Dibenz(a,h)anthrace ne
U
2.00
pg/L
-
Surrogate: Phenol-d6
16.3
Ng/L
100
16.3
7-32
Surrogate: Nitrobenzene-d5
54.3
pg/L
100
54.3
20-91
Surrogate: 2,4,6-Tribromophenol
68.5
Ng/L
100
68.5
39-110
Surrogate:4-Terphenyl-d14
71.7
Ng/L
100
71.7
35-126
Surrogate:2-Fluorobiphenyl
47.9
Ng/L
100
47.9
24-93
Surrogate:2-Fluorophenol
24.2
Ng/L
100
24.2
10-44
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Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 58 of 62
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Organic Carbon - Quality Control
Analyte
Batch L517921 - 531 OC-2011
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/31 /20
Work Order: 0100174
Time Submitted: 10/14/2020 9:10:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
MSD (0100174 L 91642-MSD-L517921) Source: 0100174 L 91642-hPrepared: 10/21/20 Analyzed: 10/22/20
TOC 7.6 0.522 mg/L 5.26 7.34 103 70-130 3.4 20
MS (0100174 L 91642-MS-L517921) Prepared: 10/21/20 Analyzed: 10/22/20
TOC 7.34 0.522 mg/L 5.26 98 70-130
BS (0100174 LCS-L517921) Prepared &Analyzed: 10/21/20
TOC 5.24 0.498 mg/L 5 105 85-115
BILK (0100174 LRB-L517921) Prepared & Analyzed: 10/21/20
TOC U 1.00 mg/L -
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
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Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 59 of 62
Sample Extraction Data
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
0100174-01
POL0558
50
mL
50 mL
12/30/20 14:30
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
0100174-01
POL0504
20
mL
30 mL
12/28/20 10:50
Prep Method: 9010C
Lab Number
Batch
Initial
Final
Date/Time
0100174-01
POJ0357
50
mL
50 mL
10/20/20 8:10
0100174-02
POJ0357
50
mL
50 mL
10/20/20 8:10
0100174-03
POJ0357
50
mL
50 mL
10/20/20 8:10
Prep Method: SM4500-S C
Lab Number
Batch
Initial
Final
Date/Time
0100174-01
POJ0337
200
mL
200 mL
10/19/20 11:02
0100174-02
POJ0337
200
mL
200 mL
10/19/20 11:02
0100174-03
POJ0337
200
mL
200 mL
10/19/20 11:02
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
0100174-01
POJ0286
970
mL
10 mL
10/16/20 10:15
0100174-02
POJ0286
990
mL
10 mL
10/16/20 10:15
0100174-03
POJ0286
990
mL
10 mL
10/16/20 10:15
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
0100174-01
POJ0286
970
mL
10 mL
10/16/20 10:15
0100174-02
POJ0286
990
mL
10 mL
10/16/20 10:15
0100174-03
POJ0286
990
mL
10 mL
10/16/20 10:15
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
0100174-01
POJ0239
50
mL
50 mL
10/15/20 7:44
0100174-01
POJ0490
50
mL
50 mL
10/27/20 7:00
0100174-01
POJ0239
50
mL
50 mL
10/15/20 7:44
0100174-02
POJ0239
50
mL
50 mL
10/15/20 7:44
0100174-02
POJ0239
50
mL
50 mL
10/15/20 7:44
0100174-02
POJ0239
50
mL
50 mL
10/15/20 7:44
0100174-02
POJ0490
50
mL
50 mL
10/27/20 7:00
0100174-03
POJ0239
50
mL
50 mL
10/15/20 7:44
0100174-03
POJ0490
50
mL
50 mL
10/27/20 7:00
Prep Method: 7470A
Lab Number
Batch
Initial
Final
DatelTime
0100174-01
POJ0374
20
mL
30 mL
10/20/20 11:55
0100174-02
POJ0374
20
mL
30 mL
10/20/20 11:55
0100174-03
POJ0374
20
mL
30 mL
10/20/20 11:55
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
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Sample Extraction Data
Prep Method: 5030E
Lab Number Batch Initial Final Date/Time
0100174-01
POJ0321
10
mL
10 mL
10/21/20 10:00
0100174-02
POJ0321
10
mL
10 mL
10/21/20 10:00
0100174-03
POJ0321
10
mL
10 mL
10/21/20 10:00
0100174-04
POJ0321
10
mL
10 mL
10/21/20 10:00
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
0100174-01
POJ0316
5 mL
5 mL 10/16/20 10:00
0100174-02
POJ0316
5 mL
5 mL 10/16/20 10:00
0100174-03
POJ0316
5 mL
5 mL 10/16/20 10:00
Sample Extraction Data
Prep Method:3510C
Lab Number
Batch
Initial
Final Date/Time
0100174-01
L517325
10/19/20 15:45
0100174-02
L517325
10/19/20 15:45
0100174-03
L517325
10/19/20 15:45
Prep Method: 8151A
Lab Number
Batch Initial
Final Date/Time
0100174-01
L517362
10/19/20 17:11
0100174-02
L517362
10/19/20 17:11
0100174-03
L517362
10/19/20 17:11
Prep Method: 3510C
Lab Number
Batch Initial
Final Date/Time
0100174-01
L517328
10/19/20 15:45
0100174-02
L517328
10/19/20 15:45
0100174-03
L517328
10/19/20 15:45
Prep Method: 5310C-2011
Lab Number
Batch Initial Final
Date/Time
0100174-01
L517921
10/21/20 14:36
0100174-02
L517921
10/21/20 14:36
0100174-03
L517921
10/21/20 14:36
Subcontracted Analyses
The following analyses were subcontracted to Waypoint Analytical, LLC
Lab Number
Analysis
0100174-01
8270 (App. II)
0100174-01
Herbicides (Sub)
0100174-01
TOC (Sub)
0100174-02
8270 (App. 11)
0100174-02
Herbicides (Sub)
0100174-02
TOC (Sub)
0100174-03
8270 (App. II)
0100174-03
Herbicides (Sub)
0100174-03
TOC (Sub)
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Waypoint
ANALYTICAL
449 Springbrook Road • Charlotte, NC 28217
Phone 704/529-6364 Fax: 704/525-0409
Client Company Name: Vckor QeA 61F WC -
Report To/Contact Name' W fir_ Lu'.Qr:+e°
Reporting Address: hE!(,gy-dJA &A,
r
CHAIN OF CUSTODY RECORD
PAGE t` OF I --QUOTE # TO ENSURE PROPER BILLING:
Project Name: 1ALX-- An
Short Hold Analysis (Yes) No) UST Project: (Yes)
*Please ATTACH any pr specific reporting (QC LEVEL I II III IV)
Provisions and/or QC Requirements
Invoice To: n__
Address:
YES NO N/A
Samples INTACT upon arrival?
f
Received IN ICE?
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec'd W/OUT HEADSPACE?
✓
PROPER CONTAINERS used?
TEMP: Therm ID:_ I �j IS Observed?- • 0 *C /Corr. Z - Z) *C
Phone: 1?5 el)-", V Fax (Yes)(No):
Purchase Order No./Billing ReferenceLnl 6(90 —M .0Z
TO BE FILLED IN BY C� IENT/SAMPLING PERSONNEL
Email Address: AVlA t.C� ►&''<1,� Ar.'I
EDD Type: PDF Excel Other
Pcc.('r.4M Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
"Working Days" ❑ 6-9 Days )"ndard 10 days ❑ h Work Must Be
Certification' NC
-
Z SC
--��
Site Location Name: r)(k/_.rGS21VM �, ��
pre
Samples received after 15:00 will be processed next business day.
y.
Turnaround
Other N/A
Site Location Physical Address: QS 1 ( C 4,p
baG time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING ERVIPJ=S
Samples Iced Upon Collection: YES,
RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT)
CLIENT
DATE
TIME
COLLECTED
MATRIX
SAMPLE CONTAINER
\�y�V
ISgEQ S jD
SAMPLE DESCRIPTION
COLLECTED
MILITARY
(SOIL,
WATER, OR
PRESERVA-
TIMES
�i��+ -Uy �� .^v ate
Q� y a ` (
ID NO.
*TYPE
NO.
SIZE
HOURS
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SEE BELOW
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Sampler's Signature
Sampled By (Print Name) MdawioAffiliation dTKaw
GAG"
LAB USE ONLY
Upon relinquishin , his Chain of Custody is your authorization
for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be
submitted in writin the W point Analytical Project
Manager. There will be charges for any changes after analyses have been initialized.
Site Arrival Time:
Relinquished By: (Sign re)
Received By: (' ) Date
/
Military/Hours Additional Comments: Site Departure Time:
\
ReIinqui y: (SiWe
Rec . ed By: (S' nature) Date
Field Tech Fee:
Relinqu' d By: (Si alure
Received For Wayp int Analytical By: D/a
V
Mileage:
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATI O HE LABO RY. CO Grou o.
RY
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL R VE AT THE LABORATOSEE
❑ Fed Ex ❑ UPS O ?
o�
REVERSE FOR
❑ Hand -delivered ❑ Waypoint Analytical Field Service El Other
TERMS & CONDITIONS
NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: BRWNFLD —LANDFILL
❑ NC ❑ SC ElNC ❑ SC �Ic ❑ SC ❑ NC ❑ SC Nc ❑ SC ❑ NC C]sc ❑ NC El SC C ❑ Sc
OTHER:
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Page 62 of 6211
CI
Is.
D'
dl
*CONTAINER TYPE Rr?nI=-Q- A - Amh— r = rl—r r_- r_i -.- o - olefin• TI = T.fl—1 inwrl r`.- vnn A.. I--;� 17^— Ll— �____•
Way poi nt
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Jackson Cty Landfill 2020 Fall
Project No.: 50-02
Lab Submittal Date: 10/15/2020
Work Order: 0100203
Case Narrative
12/1/20 8:48
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Dissolved hydrogen, Carbon dioxide, dissolved gasses and volatile fatty acids analyses were
subcontracted to Pace/GCAL. Laboratory report is attached.
524 analysis was subcontracted to Pace Huntersville. Laboratory report is attached.
Waypoint Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a -,--,I
Angela D. Overcash
Senior Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
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Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 96
Data Qualifiers Key Reference:
BRL BRL
HT Sample received and analyzed outside of the hold time.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
LCD2 LCS/LCSD RPD Value outside of the control limits. LCS and LCSD Values within the control limits.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
SR Surrogate recovery outside of the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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0
Waypo i nt ..
ANALYTICAL
Sample Receipt Summary
12/01 /2020
Work Order: 0100203
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
MW-01-20201014
0100203-01
Water
10/14/20
12:00
10/15/20
8:45
LT-01-20201014
0100203-02
Water
10/14/20
12:25
10/15/20
8:45
SW-01-20201014
0100203-03
Water
10/14/20
13:00
10/15/20
8:45
SW-02-20201014
0100203-04
Water
10/14/20
13:30
10/15/20
8:45
DW-01-20201014
0100203-05
Drinking Water
10/14/20
14:00
10/15/20
8:45
TB-202010140000
0100203-06
Water
10/14/20
0:00
10/15/20
8:45
MW-02-20201013
0100203-07
Water
10/13/20
14:50
10/15/20
8:45
MW-03-20201013
0100203-08
Water
10/13/20
10:29
10/15/20
8:45
MW-06-20201013
0100203-09
Water
10/13/20
13:15
10/15/20
8:45
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 3 of 96
Way poi nt
ANALYTICAL
Summary of Detections
12/01/202C
Work Order: 0100203
Prism ID
Client ID
Parameter
Method
Result
Units
0100203-01
MW-01-20201014
Chloride
9056A
1200
ug/L
0100203-01
MW-01-20201014
Biochemical Oxygen Demand
SM5210 B
3100
ug/L
0100203-01
MW-01-20201014
Chemical Oxygen Demand
SM5220 D
24000
J
ug/L
0100203-01
MW-01-20201014
Ferrous Iron
SM3500-Fe B
39000
HT
ug/L
0100203-01
MW-01-20201014
Total Alkalinity to pH 4.5
SM2320 B
100000
ug/L
0100203-01
MW-01-20201014
gamma-BHC
8081B
0.051
ug/L
0100203-01
MW-01-20201014
2,4-D
8151A
0.3728
pg/L
0100203-01
MW-01-20201014
1,4-Dichlorobenzene
8270D
4.94
J
pg/L
0100203-01
MW-01-20201014
Diethyl phthalate
8270D
1.16
J
pg/L
0100203-01
MW-01-20201014
Mercury
7470A
1.1
ug/L
0100203-01
MW-01-20201014
Barium
6020B
100
ug/L
0100203-01
MW-01-20201014
Cadmium
6020B
0.17
J
ug/L
0100203-01
MW-01-20201014
Chromium
6020B
0.99
J
ug/L
0100203-01
MW-01-20201014
Cobalt
6020B
160
ug/L
0100203-01
MW-01-20201014
Nickel
6020B
16
ug/L
0100203-01
MW-01-20201014
Selenium
6020B
1.0
J
ug/L
0100203-01
MW-01-20201014
Zinc
6020B
11
J
ug/L
0100203-01
MW-01-20201014
TOC
531OC-2011
1.78
mg/L
0100203-01
MW-01-20201014
1,1-Dichloroethane
8260D
2.8
ug/L
0100203-01
MW-01-20201014
1,2-Dichlorobenzene
8260D
0.22
J
ug/L
0100203-01
MW-01-20201014
1,4-Dichlorobenzene
8260D
9.8
ug/L
0100203-01
MW-01-20201014
Acetone
8260D
5.7
ug/L
0100203-01
MW-01-20201014
Benzene
8260D
1.5
ug/L
0100203-01
MW-01-20201014
Chlorobenzene
8260D
1.9
ug/L
0100203-01
MW-01-20201014
cis-1,2-Dichloroethylene
8260D
4.5
ug/L
0100203-01
MW-01-20201014
Ethylbenzene
8260D
0.33
J
ug/L
0100203-01
MW-01-20201014
m,p-Xylenes
8260D
0.83
J
ug/L
0100203-01
MW-01-20201014
o-Xylene
8260D
0.26
J
ug/L
0100203-01
MW-01-20201014
Tetrachloroethylene
8260D
0.48
.1
ug/L
0100203-01
MW-01-20201014
Trichloroethylene
8260D
0.57
ug/L
0100203-01
MW-01-20201014
Vinyl chloride
8260D
0.31
J
ug/L
0100203-01
MW-01-20201014
Xylenes, total
8260D
1.1
J
ug/L
0100203-02
LT-01-20201014
Mercury
7470A
0.23
ug/L
0100203-02
LT-01-20201014
Arsenic
6020B
2.9
ug/L
0100203-02
LT-01-20201014
Barium
6020B
500
ug/L
0100203-02
LT-01-20201014
Chromium
6020B
2.5
ug/L
0100203-02
LT-01-20201014
Cobalt
6020B
3.8
ug/L
0100203-02
LT-01-20201014
Nickel
6020B
20
ug/L
0100203-02
LT-01-20201014
Selenium
6020B
0.79
J
ug/L
0100203-02
LT-01-20201014
Vanadium
6020B
2.4
J
ug/L
0100203-02
LT-01-20201014
1,3-Dichlorobenzene
8260D
0.27
J
ug/L
0100203-02
LT-01-20201014
1,4-Dichlorobenzene
8260D
4.8
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Waypoint.
ANALYTICAL
Summary of Detections
12/01/202C
Work Order: 0100203
Prism ID
Client ID
Parameter
Method
Result
Units
0100203-02
LT-01-20201014
Acetone
8260D
11
ug/L
0100203-02
LT-01-20201014
Acetonitrile
8260D
4.7
J
ug/L
0100203-02
LT-01-20201014
Benzene
8260D
2.4
ug/L
0100203-02
LT-01-20201014
Chlorobenzene
8260D
4.4
ug/L
0100203-02
LT-01-20201014
Chloroethane
8260D
0.47
J
ug/L
0100203-02
LT-01-20201014
cis-1,2-Dichloroethylene
8260D
0.29
J
ug/L
0100203-02
LT-01-20201014
Ethylbenzene
8260D
1.8
ug/L
0100203-02
LT-01-20201014
m,p-Xylenes
8260D
1.7
ug/L
0100203-02
LT-01-20201014
Naphthalene
8260D
13
ug/L
0100203-02
LT-01-20201014
o-Xylene
8260D
2.0
ug/L
0100203-02
LT-01-20201014
Tetrahydrofuran
8260D
94
ug/L
0100203-02
LT-01-20201014
Toluene
8260D
0.79
ug/L
0100203-02
LT-01-20201014
Vinyl chloride
8260D
0.22
J
ug/L
0100203-02
LT-01-20201014
Xylenes, total
8260D
3.7
ug/L
0100203-02
LT-01-20201014
1,4-Dioxane
8260D SIM
58
ug/L
0100203-03
SW-01-20201014
Barium
6020B
12
ug/L
0100203-03
SW-01-20201014
Hardness
SM2340 C
5000
ug/L
0100203-03
SW-01-20201014
Mercury
7470A
1.1
ug/L
0100203-03
SW-01-20201014
Barium
6020B
16
ug/L
0100203-03
SW-01-20201014
Chromium
6020B
0.86
J
ug/L
0100203-03
SW-01-20201014
Lead
6020B
0.30
J
ug/L
0100203-03
SW-01-20201014
Nickel
6020B
1.5
J
ug/L
0100203-03
SW-01-20201014
Naphthalene
8260D
0.87
J
ug/L
0100203-04
SW-02-20201014
Antimony
6020B
0.54
J
ug/L
0100203-04
SW-02-20201014
Barium
6020B
10
ug/L
0100203-04
SW-02-20201014
Hardness
SM2340 C
5500
ug/L
0100203-04
SW-02-20201014
Mercury
7470A
0.95
ug/L
0100203-04
SW-02-20201014
Barium
6020B
16
ug/L
0100203-04
SW-02-20201014
Chromium
6020B
0.94
J
ug/L
0100203-04
SW-02-20201014
Lead
6020B
0.38
J
ug/L
0100203-04
SW-02-20201014
Nickel
6020B
1.5
J
ug/L
0100203-04
SW-02-20201014
Selenium
6020B
0.85
J
ug/L
0100203-06
TB-202010140000
Acetone
8260D
3.0
J
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 96
Laboratory Report
IL A i • . 0 12/01/2020
ANALYTICAL
Anchor QEAof North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-01
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 12:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Anions by Ion Chromatography
Chloride
1200
ug/L
NE
1000
350
1
9056A
10/15/20 11:50BMS
POJ0299
Nitrate as N
<45
ug/L
10000
200
45
1
9056A
10/15/20 11:50BMS
POJ0299
Sulfate
<560
ug/L
250000
2000
560
1
9056A
10/15/20 11:50BMS
POJ0299
General Chemistry Parameters
Biochemical Oxygen Demand
3100
ug/L
NE
2000
210
1
SM5210 B
10/15/20 15:55ENM
POJ0340
Chemical Oxygen Demand
24000 J
ug/L
NE
50000
11000
1
SM5220 D
10/19/20 11:56SLS
POJ0361
Cyanide
<14
ug/L
10
25
14
5
9014
10/20/20 12:30BMS
POJ0357
Ferrous Iron
39000 HT
ug/L
NE
5000
1200
25
SM3500-Fe B
10/15/20 9:51 ENM
POJ0282
Sulfide
<830
ug/L
1000
2000
830
1
SM4500-S F
10/19/20 11:02ENM
POJ0337
Total Alkalinity to pH 4.5
100000
ug/L
NE
5000
770
1
SM2320 B
10/19/20 11:40 CLB
POJ0341
Organochlorine Pesticides by GC/ECD
4,4'-DDD
<0.027
ug/L
0.1
0.10
0.027
1
8081B
10/19/20 12:35NMB
POJ0286
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081B
10/19/20 12:35NMB
POJ0286
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081B
10/19/20 12:35NMB
POJ0286
Aldrin
<0.016
ug/L
0.05
0.051
0.016
1
8081B
10/19/20 12:35NMB
POJ0286
alpha-BHC
<0.0064
ug/L
0.05
0.051
0.0064
1
8081B
10/19/20 12:35NMB
POJ0286
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081B
10/19/20 12:35NMB
POJ0286
beta-BHC
<0.011
ug/L
0.05
0.051
0.011
1
8081B
10/19/20 12:35NMB
POJ0286
Chlordane
<0.18
ug/L
0.5
0.51
0.18
1
8081B
10/19/20 12:35NMB
POJ0286
delta-BHC
<0.0084
ug/L
0.05
0.051
0.0084
1
8081B
10/19/20 12:35NMB
POJ0286
Dieldrin
<0.014
ug/L
0.002
0.051
0.014
1
8081B
10/19/20 12:35NMB
POJ0286
Endosulfan 1
<0.016
ug/L
0.1
0.051
0.016
1
8081B
10/19/20 12:35NMB
POJ0286
Endosulfan 11
<0.012
ug/L
0.1
0.051
0.012
1
8081B
10/19/20 12:35NMB
POJ0286
Endosulfan Sulfate
<0.017
ug/L
0.1
0.051
0.017
1
8081B
10/19/20 12:35NMB
POJ0286
Endrin
<0.014
ug/L
0.1
0.051
0.014
1
8081B
10/19/20 12:35NMB
POJ0286
Endrin Aldehyde
<0.016
ug/L
0.1
0.051
0.016
1
8081B
10/19/20 12:35NMB
POJ0286
Endrin Ketone
<0.018
ug/L
NE
0.10
0.018
1
8081B
10/19/20 12:35NMB
POJ0286
gamma-BHC
0.051
ug/L
0.05
0.051
0.0062
1
8081B
10/19/20 12:35NMB
POJ0286
trans -Chlordane
<0.024
ug/L
NE
0.10
0.024
1
8081B
10/19/20 12:35NMB
POJ0286
Heptachlor
<0.013
ug/L
0.05
0.051
0.013
1
8081B
10/19/20 12:35NMB
POJ0286
Heptachlor Epoxide
<0.023
ug/L
0.075
0.10
0.023
1
8081B
10/19/20 12:35NMB
POJ0286
Methoxychlor
<0.018
ug/L
NE
0.10
0.018
1
8081B
10/19/20 12:35NMB
POJ0286
Toxaphene
<0.36
ug/L
1.5
1.0
0.36
1
8081B
10/19/20 12:35NMB
POJ0286
Surrogate
Recovery Control Limits
Decachlorobiphenyl
44 %
13-186
Tetrachloro-m-xylene
77 %
40-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 96
Laboratory Report
• � 12/01/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-01
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 12:00
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Polychlorinated Biphenyls (PCBs) by GC/ECD
Aroclor 1016
<0.21
ug/L
NE
0.51
0.21
1
8082A
10/19/20 12:35NMB
POJ0286
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1
8082A
10/19/20 12:35NMB
POJ0286
Aroclor 1232
<0.16
ug/L
NE
0.51
0.16
1
8082A
10/19/20 12:35NMB
POJ0286
Aroclor 1242
<0.14
ug/L
NE
0.51
0.14
1
8082A
10/19/20 12:35NMB
POJ0286
Aroclor 1248
<0.14
ug/L
NE
0.51
0.14
1
8082A
10/19/20 12:35NMB
POJ0286
Aroclor 1254
<0.16
ug/L
NE
0.51
0.16
1
8082A
10/19/20 12:35NMB
POJ0286
Aroclor 1260
<0.51
ug/L
NE
1.0
0.51
1
8082A
10/19/20 12:35NMB
POJ0286
Total Metals
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
Recovery Control Limits
77 % 30-161
46 % 32-178
Mercury
1.1
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 15:37EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/24/20 7:49 JAB
POJ0312
Arsenic
<0.17
ug/L
10
1.0
0.17
1
6020B
10/24/20 7:49 JAB
POJ0312
Barium
100
ug/L
100
2.0
0.81
1
6020B
10/24/20 7:49 JAB
POJ0312
Beryllium
<0.19
ug/L
1
1.0
0.19
1
6020B
10/27/20 15:09JAB
POJ0312
Cadmium
0.17
J
ug/L
1
1.0
0.16
1
6020B
10/24/20 7:49 JAB
POJ0312
Chromium
0.99
J
ug/L
10
2.0
0.79
1
6020B
10/27/20 22:04JAB
POJ0491
Cobalt
160
ug/L
10
2.0
0.52
1
6020B
10/24/20 7:49 JAB
POJ0312
Copper
<3.8
ug/L
10
10
3.8
1
6020B
10/24/20 7:49 JAB
POJ0312
Lead
<0.26
ug/L
10
1.0
0.26
1
6020B
10/24/20 7:49 JAB
POJ0312
Nickel
16
ug/L
50
3.0
0.51
1
6020B
10/24/20 7:49 JAB
POJ0312
Selenium
1.0
J
ug/L
10
5.0
0.74
1
6020B
10/24/20 7:49 JAB
POJ0312
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 22:04JAB
POJ0491
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/24/20 7:49 JAB
POJ0312
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/27/20 22:04JAB
POJ0491
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/24/20 7:49 JAB
POJ0312
Zinc
11
J
ug/L
10
20
6.9
1
6020B
10/24/20 7:49 JAB
POJ0312
Volatile Organic Compounds
by GUMS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 20:51JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 20:51JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 20:51JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 20:51JLB
POJ0321
1,1-Dichloroethane
2.8
ug/L
5
0.50
0.083
1
8260D
10/21/20 20:51JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 20:51JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 20:51JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 20:51JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 96
Laboratory Report
A i • .0 12/01/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-01
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 12:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 20:51JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 20:51JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 20:51JLB
POJ0321
1,2-Dichlorobenzene
0.22 J
ug/L
5
0.50
0.076
1
8260D
10/21/20 20:51JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 20:51JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 20:51JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 20:51JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 20:51JLB
POJ0321
1,4-Dichlorobenzene
9.8
ug/L
1
0.50
0.050
1
8260D
10/21/20 20:51JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 20:51JLB
POJ0321
Acetone
5.7
ug/L
100
5.0
0.31
1
8260D
10/21/20 20:51JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 20:51JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 20:51JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 20:51JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 20:51JLB
POJ0321
Benzene
1.5
ug/L
1
0.50
0.048
1
8260D
10/21/20 20:51JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 20:51JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 20:51JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 20:51JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 20:51JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 20:51JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 20:51JLB
POJ0321
Chlorobenzene
1.9
ug/L
3
0.50
0.062
1
8260D
10/21/20 20:51JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 20:51JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 20:51JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 20:51JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 20:51JLB
POJ0321
cis-1,2-Dichloroethylene
4.5
ug/L
2
0.50
0.056
1
8260D
10/21/20 20:51JLB
POJ0321
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 20:51JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 20:51JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 20:51JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 20:51JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 20:51JLB
POJ0321
Ethylbenzene
0.33 J
ug/L
1
0.50
0.061
1
8260D
10/21/20 20:51JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 20:51JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 20:51JLB
POJ0321
m,p-Xylenes
0.83 J
ug/L
NE
1.0
0.12
1
8260D
10/21/20 20:51JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 96
.
Laboratory Report
• �
Waynt..
12/01/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID:
MW-01-20201014
Attn: Alec Macbeth
Sample ID: 0100203-01
231 Haywood Street
Project No.:
50-02
Work
Order: 0100203
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/14/20 12:00
Time
Submitted: 10/15/20
08:45
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 20:51JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 20:51JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 20:51JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 20:51JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 20:51JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 20:51JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 20:51JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 20:51JLB
POJ0321
o-Xylene
0.26
J ug/L
NE
0.50
0.044
1
8260D
10/21/20 20:51JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 20:51JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 20:51JLB
POJ0321
Tetrachloroethylene
0.48
J ug/L
1
0.50
0.098
1
8260D
10/21/20 20:51JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 20:51JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 20:51JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 20:51JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 20:51JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 20:51JLB
POJ0321
Trichloroethylene
0.57
ug/L
1
0.50
0.078
1
8260D
10/21/20 20:51JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 20:51JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 20:51JLB
POJ0321
Vinyl chloride
0.31
J ug/L
1
0.50
0.097
1
8260D
10/21/20 20:51JLB
POJ0321
Xylenes, total
1.1
J ug/L
5
1.5
0.15
1
8260D
10/21/20 20:51JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
101
% 80-124
Dibromofluoromethane
108 % 75-129
Toluene-d8
98 % 77-123
Volatile Organic Compounds by GC/MS
SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/16/20 22:54ANG
POJ0316
8270 Extended List
1,3,5-Trinitrobenzene
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
1,4-Naphthoquinone
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
1-Naphthylamine
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
2-Acetylaminofluorene
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
2-Naphthylamine
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
3-Methylcholanthrene
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
4-Aminobiphenyl
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
5-Nitro-o-toluidine
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
7,12-Dimethyl benz(a)anthrace ne
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 96
Laboratory Report
A i • .0 12/01/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-01
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 12:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Diallate
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
Hexachloropropene
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
Isosafrole
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
Kepone
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
Methapyrilene
<10.6
Ng/L
21.1
10.6
1
8270D
10/20/20 19:35BGV
L517325
WIN itrosomethylethyl amine
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
N-Nitrosopiperidine
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
N-Nitrosopyrrolidine
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
o-Toluidine
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
p-Dimethylaminoazobenzene
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
p-Phenylenediamine
<10.5 L
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
Pronamide
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
Safrole
<10.5
Ng/L
10.5
10.5
1
8270D
10/20/20 19:35BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
<0.01002
Ng/L
0.03
0.01002
1
8151A
10/22/20 17:19VIC
L517923
2,4,5-TP (Silvex)
<0.01634
Ng/L
0.1
0.01634
1
8151A
10/22/20 17:19VIC
L517923
2,4-D
0.3728
Ng/L
0.25
0.2078
1
8151A
10/22/20 17:19VIC
L517923
2,4-DB
<0.1364
Ng/L
0.1
0.1364
1
8151A
10/22/20 17:19VIC
L517923
Dalapon
<0.5149
Ng/L
0.55
0.5149
1
8151A
10/22/20 17:19VIC
L517923
Dicamba
<0.057
Ng/L
0.25
0.057
1
8151A
10/22/20 17:19VIC
L517923
Dichlorprop
<0.07959
Ng/L
0.1
0.07959
1
8151A
10/22/20 17:19VIC
L517923
Dinoseb
<0.02698
Ng/L
0.1
0.02698
1
8151A
10/22/20 17:19VIC
L517923
MCPA
<18.98
Ng/L
50
18.98
1
8151A
10/22/20 17:19VIC
L517923
MCPP
<11.75
Ng/L
50
11.75
1
8151A
10/22/20 17:19VIC
L517923
Picloram
<0.04528
Ng/L
0.1
0.04528
1
8151A
10/22/20 17:19VIC
L517923
Surrogate
Recovery Control Limits
DCAA
51.2 % 20-150
Semivolatile Organic Compounds - GC/MS
1,2,4,5-Tetrachlorobenzene
<0.333
Ng/L
5.26
0.333
1
8270D
10/20/20 19:35BGV
L517328
1,2,4-Trichlorobenzene
<0.507
Ng/L
5.26
0.507
1
8270D
10/20/20 19:35BGV
L517328
1,2-Dichlorobenzene
<0.661
Ng/L
5.26
0.661
1
8270D
10/20/20 19:35BGV
L517328
1,3-Dichlorobenzene
<0.516
Ng/L
5.26
0.516
1
8270D
10/20/20 19:35BGV
L517328
1,4-Dichlorobenzene
4.94 j
Ng/L
5.26
0.61
1
8270D
10/20/20 19:35BGV
L517328
2,3,4,6-Tetrachlorophenol
<0.373
Ng/L
5.26
0.373
1
8270D
10/20/20 19:35BGV
L517328
2,4,5-Trichlorophenol
<0.368
Ng/L
5.26
0.368
1
8270D
10/20/20 19:35BGV
L517328
2,4,6-Trichlorophenol
<0.361
Ng/L
5.26
0.361
1
8270D
10/20/20 19:35BGV
L517328
2,4-Dichlorophenol
<1.6
Ng/L
5.26
1.6
1
8270D
10/20/20 19:35BGV
L517328
2,4-Dimethylphenol
<0.709
Ng/L
5.26
0.709
1
8270D
10/20/20 19:35BGV
L517328
2,4-Dinitrophenol
<5.09
Ng/L
10.5
5.09
1
8270D
10/20/20 19:35BGV
L517328
2,4-Dinitrotoluene
<0.423
Ng/L
5.26
0.423
1
8270D
10/20/20 19:35BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 96
® Laboratory Report
IL AL i • . 12/01 /2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: MW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-01
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 12:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
2,6-Dichlorophenol
<0.739
pg/L
5.26
0.739
1
8270D
10/20/20 19:35BGV
L517328
2,6-Dinitrotoluene
<0.434
pg/L
5.26
0.434
1
8270D
10/20/20 19:35BGV
L517328
2-Chloronaphthalene
<0.5
pg/L
5.26
0.5
1
8270D
10/20/20 19:35BGV
L517328
2-Chlorophenol
<0.774
pg/L
5.26
0.774
1
8270D
10/20/20 19:35BGV
L517328
2-Methyl naphthalene
<0.511
pg/L
2.11
0.511
1
8270D
10/20/20 19:35BGV
L517328
2-Methylphenol
<0.758
pg/L
5.26
0.758
1
8270D
10/20/20 19:35BGV
L517328
2-Nitroaniline
<0.603
pg/L
5.26
0.603
1
8270D
10/20/20 19:35BGV
L517328
2-Nitrophenol
<0.637
pg/L
5.26
0.637
1
8270D
10/20/20 19:35BGV
L517328
3&4 Methylphenol
<0.726
pg/L
5.26
0.726
1
8270D
10/20/20 19:35BGV
L517328
3,3' Dimethylbenzidine
<1.97
pg/L
10.5
1.97
1
8270D
10/20/20 19:35BGV
L517328
3,3'-Dichlorobenzidine
<3.93
pg/L
10.5
3.93
1
8270D
10/20/20 19:35BGV
L517328
3-Nitroaniline
<1.61
pg/L
10.5
1.61
1
8270D
10/20/20 19:35BGV
L517328
4,6-Dinitro-2-methylphenol
<3.64
pg/L
10.5
3.64
1
8270D
10/20/20 19:35BGV
L517328
4-Bromophenyl phenyl ether
<0.526
pg/L
5.26
0.526
1
8270D
10/20/20 19:35BGV
L517328
4-Chloro-3-methylphenol
<0.529
pg/L
5.26
0.529
1
8270D
10/20/20 19:35BGV
L517328
4-Chloroaniline
<0.553
pg/L
5.26
0.553
1
8270D
10/20/20 19:35BGV
L517328
4-Chlorophenyl phenyl ether
<0.503
pg/L
5.26
0.503
1
8270D
10/20/20 19:35BGV
L517328
4-Nitroaniline
<0.778
pg/L
5.26
0.778
1
8270D
10/20/20 19:35BGV
L517328
4-Nitrophenol
<1.46
pg/L
10.5
1.46
1
8270D
10/20/20 19:35BGV
L517328
Acenaphthene
<0.445
pg/L
2.11
0.445
1
8270D
10/20/20 19:35BGV
L517328
Acenaphthylene
<0.452
pg/L
2.11
0.452
1
8270D
10/20/20 19:35BGV
L517328
Acetophenone
<0.721
pg/L
5.26
0.721
1
8270D
10/20/20 19:35BGV
L517328
Aniline
<0.332
pg/L
5.26
0.332
1
8270D
10/20/20 19:35BGV
L517328
Anthracene
<0.492
pg/L
2.11
0.492
1
8270D
10/20/20 19:35BGV
L517328
Benzidine
<0.726
pg/L
21.1
0.726
1
8270D
10/20/20 19:35BGV
L517328
Benzo(a)anthracene
<0.45
pg/L
2.11
0.45
1
8270D
10/20/20 19:35BGV
L517328
Benzo(a)pyrene
<1.06
pg/L
2.11
1.06
1
8270D
10/20/20 19:35BGV
L517328
Benzo(b)fluoranthene
<0.992
pg/L
2.11
0.992
1
8270D
10/20/20 19:35BGV
L517328
Benzo(q,hJ)perylene
<1.43
pg/L
2.11
1.43
1
8270D
10/20/20 19:35BGV
L517328
Benzo(k)fluoranthene
<0.793
pg/L
2.11
0.793
1
8270D
10/20/20 19:35BGV
L517328
Benzoic Acid
<5.25
pg/L
10.5
5.25
1
8270D
10/20/20 19:35BGV
L517328
Benzyl alcohol
<3.16
pg/L
10.5
3.16
1
8270D
10/20/20 19:35BGV
L517328
Bis(2-Chloroethoxy)methane
<0.455
pg/L
5.26
0.455
1
8270D
10/20/20 19:35BGV
L517328
Bis(2-Chloroethyl)ether
<0.47
pg/L
5.26
0.47
1
8270D
10/20/20 19:35BGV
L517328
Bis(2-Chloroisopropyl)ether
<0.574
pg/L
5.26
0.574
1
8270D
10/20/20 19:35BGV
L517328
Bis(2-ethylhexyl)phthalate
<3.85
pg/L
5.26
3.85
1
8270D
10/20/20 19:35BGV
L517328
Butyl benzyl phthalate
<4.83
pg/L
5.26
4.83
1
8270D
10/20/20 19:35BGV
L517328
Carbazole
<0.5
pg/L
5.26
0.5
1
8270D
10/20/20 19:35BGV
L517328
Chrysene
<0.771
pg/L
2.11
0.771
1
8270D
10/20/20 19:35BGV
L517328
Dibenz(a,h)anthracene
<0.265
pg/L
2.11
0.265
1
8270D
10/20/20 19:35BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 96
.
Laboratory Report
• �
Waynt.�
12/01/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020
Fall
Client Sample ID: MW-01-20201014
Attn: Alec Macbeth
Sample ID: 0100203-01
231 Haywood Street
Project No.: 50-02
Work
Order: 0100203
Asheville, NC 28801
Sample Matrix: Water
Time
Collected: 10/14/20 12:00
Time
Submitted: 10/15/20 08:45
Parameter
Result Units SWSL
Report
MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Dibenzofuran
<0.444
Ng/L
5.26
0.444
1
8270D 10/20/20 19:35BGV
L517328
Diethyl phthalate
1.16
j Ng/L
5.26
0.615
1
8270D 10/20/20 19:35BGV
L517328
Dimethyl phthalate
<0.536
pg/L
5.26
0.536
1
8270D 10/20/20 19:35BGV
L517328
Di-n-butyl phthalate
<1.66
Ng/L
5.26
1.66
1
8270D 10/20/20 19:35BGV
L517328
Di-n-Octyl Phthalate
<1.81
Ng/L
5.26
1.81
1
8270D 10/20/20 19:35BGV
L517328
Fluoranthene
<0.428
Ng/L
2.11
0.428
1
8270D 10/20/20 19:35BGV
L517328
Fluorene
<0.468
Ng/L
2.11
0.468
1
8270D 10/20/20 19:35BGV
L517328
Hexachlorobenzene
<2.7
Ng/L
5.26
2.7
1
8270D 10/20/20 19:35BGV
L517328
Hexachlorobutadiene
<0.426
Ng/L
5.26
0.426
1
8270D 10/20/20 19:35BGV
L517328
Hexachlorocyclopentadiene
<2.46
Ng/L
5.26
2.46
1
8270D 10/20/20 19:35BGV
L517328
Hexachloroethane
<0.291
Ng/L
5.26
0.291
1
8270D 10/20/20 19:35BGV
L517328
Indeno(1,2,3-cd)pyrene
<1.07
Ng/L
2.11
1.07
1
8270D 10/20/20 19:35BGV
L517328
Isophorone
<0.378
Ng/L
5.26
0.378
1
8270D 10/20/20 19:35BGV
L517328
Naphthalene
<0.51
Ng/L
2.11
0.51
1
8270D 10/20/20 19:35BGV
L517328
Nitrobenzene
<0.558
Ng/L
5.26
0.558
1
8270D 10/20/20 19:35BGV
L517328
N-Nitrosodiethylamine
<0.42
Ng/L
5.26
0.42
1
8270D 10/20/20 19:35BGV
L517328
N-Nitrosodimethylamine
<0.261
Ng/L
5.26
0.261
1
8270D 10/20/20 19:35BGV
L517328
N-Nitroso-di-n-butylamine
<0.791
pg/L
5.26
0.791
1
8270D 10/20/20 19:35BGV
L517328
N-Nitroso-di-n-propylamine
<0.351
Ng/L
5.26
0.351
1
8270D 10/20/20 19:35BGV
L517328
N-Nitrosodiphenylamine
<0.822
Ng/L
10.5
0.822
1
8270D 10/20/20 19:35BGV
L517328
Pentachlorophenol
<2.57
Ng/L
10.5
2.57
1
8270D 10/20/20 19:35BGV
L517328
Phenanthrene
<0.489
Ng/L
2.11
0.489
1
8270D 10/20/20 19:35BGV
L517328
Phenol
<0.409
Ng/L
5.26
0.409
1
8270D 10/20/20 19:35BGV
L517328
Pyrene
<1.1
Ng/L
2.11
1.1
1
8270D 10/20/20 19:35BGV
L517328
Pyridine
<0.711
pg/L
10.5
0.711
1
8270D 10/20/20 19:35BGV
L517328
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
21.7 % 39-110
SR
2-Fluorobiphenyl
45.3 % 24-93
2-Fluorophenol
10.1 % 10-44
4-Terphenyl-d14
20 % 35-126
SR
Nitrobenzene-d5
49.7 % 20-91
Phenol-d6
9.3 % 7-32
Total Organic Carbon
TOC
1.78
mg/L
1
0.498
1
531OC-2011 10/24/20 17:34DDB
L518400
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 96
Laboratory Report
• � 12/01/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: LT-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-02
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 12:25
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Total Metals
Mercury
0.23
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 15:41 EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/24/20 7:55 JAB
POJ0312
Arsenic
2.9
ug/L
10
1.0
0.17
1
6020B
10/24/20 7:55 JAB
POJ0312
Barium
500
ug/L
100
2.0
0.81
1
6020B
10/24/20 7:55 JAB
POJ0312
Beryllium
<0.19
ug/L
1
1.0
0.19
1
6020B
10/27/20 15:15JAB
POJ0312
Cadmium
<0.16
ug/L
1
1.0
0.16
1
6020B
10/24/20 7:55 JAB
POJ0312
Chromium
2.5
ug/L
10
2.0
0.79
1
6020B
10/27/20 22:10JAB
POJ0491
Cobalt
3.8
ug/L
10
2.0
0.52
1
6020B
10/24/20 7:55 JAB
POJ0312
Copper
<3.8
ug/L
10
10
3.8
1
6020B
10/24/20 7:55 JAB
POJ0312
Lead
<0.26
ug/L
10
1.0
0.26
1
6020B
10/24/20 7:55 JAB
POJ0312
Nickel
20
ug/L
50
3.0
0.51
1
6020B
10/24/20 7:55 JAB
POJ0312
Selenium
0.79 J
ug/L
10
5.0
0.74
1
6020B
10/24/20 7:55 JAB
POJ0312
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 22:1OJAB
POJ0491
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/24/20 7:55 JAB
POJ0312
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/27/20 22:1OJAB
POJ0491
Vanadium
2.4 J
ug/L
25
5.0
1.3
1
6020B
10/24/20 7:55 JAB
POJ0312
Zinc
<6.9
ug/L
10
20
6.9
1
6020B
10/24/20 7:55 JAB
POJ0312
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 21:24JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 21:24JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 21:24JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 21:24JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 21:24JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 21:24JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 21:24JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 21:24JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 21:24JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 21:24JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 21:24JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 21:24JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 21:24JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 21:24JLB
POJ0321
1,3-Dichlorobenzene
0.27 J
ug/L
5
0.50
0.054
1
8260D
10/21/20 21:24JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 21:24JLB
POJ0321
1,4-Dichlorobenzene
4.8
ug/L
1
0.50
0.050
1
8260D
10/21/20 21:24JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 21:24JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 96
Laboratory Report
A i • .0 12/01/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: LT-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-02
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 12:25
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Acetone
11
ug/L
100
5.0
0.31
1
8260D
10/21/20 21:24JLB
POJ0321
Acetonitrile
4.7 J
ug/L
55
10
3.0
1
8260D
10/21/20 21:24JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 21:24JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 21:24JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 21:24JLB
POJ0321
Benzene
2.4
ug/L
1
0.50
0.048
1
8260D
10/21/20 21:24JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 21:24JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 21:24JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 21:24JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 21:24JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 21:24JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 21:24JLB
POJ0321
Chlorobenzene
4.4
ug/L
3
0.50
0.062
1
8260D
10/21/20 21:24JLB
POJ0321
Chloroethane
0.47 J
ug/L
10
0.50
0.22
1
8260D
10/21/20 21:24JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 21:24JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 21:24JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 21:24JLB
POJ0321
cis-1,2-Dichloroethylene
0.29 J
ug/L
2
0.50
0.056
1
8260D
10/21/20 21:24JLB
POJ0321
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 21:24JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 21:24JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 21:24JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 21:24JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 21:24JLB
POJ0321
Ethylbenzene
1.8
ug/L
1
0.50
0.061
1
8260D
10/21/20 21:24JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 21:24JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 21:24JLB
POJ0321
m,p-Xylenes
1.7
ug/L
NE
1.0
0.12
1
8260D
10/21/20 21:24JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 21:24JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 21:24JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 21:24JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 21:24JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 21:24JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 21:24JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 21:24JLB
POJ0321
Naphthalene
13
ug/L
10
1.0
0.30
1
8260D
10/21/20 21:24JLB
POJ0321
o-Xylene
2.0
ug/L
NE
0.50
0.044
1
8260D
10/21/20 21:24JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 21:24JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 21:24JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 96
.
Laboratory Report
• �
Waynt.�
12/01/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID: LT-01-20201014
Attn: Alec Macbeth
Sample ID: 0100203-02
231 Haywood Street
Project No.:
50-02
Work Order: 0100203
Asheville, NC 28801
Sample Matrix:
Water
Time Collected: 10/14/20 12:25
Time Submitted: 10/15/20 08:45
Parameter
Result Units
SWSL
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1 8260D 10/21/20 21:24JLB
POJ0321
Tetrahydrofuran
94
ug/L
NE
10
1.1
1 8260D 10/21/20 21:24JLB
POJ0321
Toluene
0.79
ug/L
1
0.50
0.044
1 8260D 10/21/20 21:24JLB
POJ0321
trans-1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1 8260D 10/21/20 21:24JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1 8260D 10/21/20 21:24JLB
POJ0321
trans-1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1 8260D 10/21/20 21:24JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1 8260D 10/21/20 21:24JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1 8260D 10/21/20 21:24JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1 8260D 10/21/20 21:24JLB
POJ0321
Vinyl chloride
0.22
J ug/L
1
0.50
0.097
1 8260D 10/21/20 21:24JLB
POJ0321
Xylenes, total
3.7
ug/L
5
1.5
0.15
1 8260D 10/21/20 21:24JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
102 % 80-124
Dibromofluoromethane
106 % 75-129
Toluene-d8
100 % 77-123
Volatile Organic Compounds by GUMS
SIM
1,4-Dioxane
58
ug/L
10
2.0
0.14
1 8260D SIM 10/16/20 23:19ANG
POJ0316
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 15 of 96
Laboratory Report
A i • .0 12/01/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-03
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Dissolved Metals
Mercury
<0.034
ug/L
0.20
0.034
1
7470A
10/21/20 15:59EDV
POJ0394
Antimony
<0.49
ug/L
2.0
0.49
1
6020B
10/28/20 12:25JAB
POJ0496
Arsenic
<0.17
ug/L
1.0
0.17
1
6020B
10/28/20 12:25JAB
POJ0496
Barium
12
ug/L
100
10
0.81
1
6020B
10/28/20 12:25JAB
POJ0496
Beryllium
<0.19
ug/L
1.0
0.19
1
6020B
10/28/20 12:25JAB
POJ0496
Cadmium
<0.16
ug/L
1.0
0.16
1
6020B
10/28/20 12:25JAB
POJ0496
Chromium
<0.79
ug/L
2.0
0.79
1
6020B
10/28/20 12:25JAB
POJ0496
Cobalt
<0.52
ug/L
2.0
0.52
1
6020B
10/28/20 12:25JAB
POJ0496
Copper
<3.8
ug/L
10
3.8
1
6020B
10/28/20 12:25JAB
POJ0496
Lead
<0.26
ug/L
1.0
0.26
1
6020B
10/28/20 12:25JAB
POJ0496
Nickel
<0.51
ug/L
50
3.0
0.51
1
6020B
10/28/20 12:25JAB
POJ0496
Selenium
<0.74
ug/L
10
5.0
0.74
1
6020B
10/28/20 12:25JAB
POJ0496
Silver
<0.11
ug/L
1.0
0.11
1
6020B
10/28/20 12:25JAB
POJ0496
Thallium
<0.57
ug/L
2.0
0.57
1
6020B
10/28/20 12:25JAB
POJ0496
Tin
<1.8
ug/L
5.0
1.8
1
6020B
10/28/20 12:25JAB
POJ0496
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/28/20 12:25JAB
POJ0496
Zinc
<6.9
ug/L
20
6.9
1
6020B
10/28/20 12:25JAB
POJ0496
General Chemistry Parameters
Hardness
5000
ug/L
5000
570
1
SM2340 C
10/15/20 15:43BMS
POJ0269
Organochlorine Pesticides by GC/ECD
4,4'-DDD
<0.026
ug/L
0.1
0.10
0.026
1
8081 B
10/19/20 12:48NMB
POJ0286
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081 B
10/19/20 12:48NMB
POJ0286
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081 B
10/19/20 12:48NMB
POJ0286
Aldrin
<0.015
ug/L
0.05
0.050
0.015
1
8081 B
10/19/20 12:48NMB
POJ0286
alpha-BHC
<0.0063
ug/L
0.05
0.050
0.0063
1
8081 B
10/19/20 12:48NMB
POJ0286
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/19/20 12:48NMB
POJ0286
beta-BHC
<0.011
ug/L
0.05
0.050
0.011
1
8081 B
10/19/20 12:48NMB
POJ0286
Chlordane
<0.18
ug/L
0.5
0.50
0.18
1
8081 B
10/19/20 12:48NMB
POJ0286
delta-BHC
<0.0082
ug/L
0.05
0.050
0.0082
1
8081 B
10/19/20 12:48NMB
POJ0286
Dieldrin
<0.014
ug/L
0.002
0.050
0.014
1
8081 B
10/19/20 12:48NMB
POJ0286
Endosulfan 1
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/19/20 12:48NMB
POJ0286
Endosulfan 11
<0.012
ug/L
0.1
0.050
0.012
1
8081 B
10/19/20 12:48NMB
POJ0286
Endosulfan Sulfate
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/19/20 12:48NMB
POJ0286
Endrin
<0.014
ug/L
0.1
0.050
0.014
1
8081 B
10/19/20 12:48NMB
POJ0286
Endrin Aldehyde
<0.016
ug/L
0.1
0.050
0.016
1
8081 B
10/19/20 12:48NMB
POJ0286
Endrin Ketone
<0.018
ug/L
NE
0.10
0.018
1
8081B
10/19/20 12:48NMB
POJ0286
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 96
Laboratory Report
A i • .0 12/01/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-03
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
gamma-BHC
<0.0061
ug/L
0.05
0.050
0.0061
1
8081 B
10/19/20 12:48NMB
POJ0286
trans -Chlordane
<0.023
ug/L
NE
0.10
0.023
1
8081B
10/19/20 12:48NMB
POJ0286
Heptachlor
<0.013
ug/L
0.05
0.050
0.013
1
8081B
10/19/20 12:48NMB
POJ0286
Heptachlor Epoxide
<0.022
ug/L
0.075
0.10
0.022
1
8081B
10/19/20 12:48NMB
POJ0286
Methoxychlor
<0.018
ug/L
NE
0.10
0.018
1
8081B
10/19/20 12:48NMB
POJ0286
Toxaphene
<0.35
ug/L
1.5
1.0
0.35
1
8081B
10/19/20 12:48NMB
POJ0286
Surrogate
Recovery Control Limits
Decachlorobiphenyl
62 % 13-186
Tetrachloro-m-xylene
56 % 40-134
Polychlorinated Biphenyls
(PCBs) by GC/ECD
Aroclor 1016
<0.21
ug/L
NE
0.50
0.21
1
8082A
10/19/20 12:48NMB
POJ0286
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1
8082A
10/19/20 12:48NMB
POJ0286
Aroclor 1232
<0.16
ug/L
NE
0.50
0.16
1
8082A
10/19/20 12:48NMB
POJ0286
Aroclor 1242
<0.14
ug/L
NE
0.50
0.14
1
8082A
10/19/20 12:48NMB
POJ0286
Aroclor 1248
<0.14
ug/L
NE
0.50
0.14
1
8082A
10/19/20 12:48NMB
POJ0286
Aroclor 1254
<0.16
ug/L
NE
0.50
0.16
1
8082A
10/19/20 12:48NMB
POJ0286
Aroclor 1260
<0.50
ug/L
NE
1.0
0.50
1
8082A
10/19/20 12:48NMB
POJ0286
Surrogate
Recovery Control Limits
Tetrachloro-m-xylene
56 % 30-161
Decachlorobiphenyl
64 % 32-178
Total Metals
Mercury
1.1
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 15:45EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/24/20 8:02 JAB
POJ0312
Arsenic
<0.17
ug/L
10
1.0
0.17
1
6020B
10/24/20 8:02 JAB
POJ0312
Barium
16
ug/L
100
2.0
0.81
1
6020B
10/24/20 8:02 JAB
POJ0312
Beryllium
<0.19
ug/L
1
1.0
0.19
1
6020B
10/27/20 15:22JAB
POJ0312
Cadmium
<0.16
ug/L
1
1.0
0.16
1
6020B
10/24/20 8:02 JAB
POJ0312
Chromium
0.86 J
ug/L
10
2.0
0.79
1
6020B
10/27/20 22:17JAB
POJ0491
Cobalt
<0.52
ug/L
10
2.0
0.52
1
6020B
10/24/20 8:02 JAB
POJ0312
Copper
<3.8
ug/L
10
10
3.8
1
6020B
10/24/20 8:02 JAB
POJ0312
Lead
0.30 J
ug/L
10
1.0
0.26
1
6020B
10/24/20 8:02 JAB
POJ0312
Nickel
1.5 J
ug/L
50
3.0
0.51
1
6020B
10/24/20 8:02 JAB
POJ0312
Selenium
<0.74
ug/L
10
5.0
0.74
1
6020B
10/24/20 8:02 JAB
POJ0312
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 22:17JAB
POJ0491
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/24/20 8:02 JAB
POJ0312
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/27/20 22:17JAB
POJ0491
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/24/20 8:02 JAB
POJ0312
Zinc
<6.9
ug/L
10
20
6.9
1
6020B
10/24/20 8:02 JAB
POJ0312
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 96
Laboratory Report
• � 12/01/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-03
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:00
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 21:58JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 21:58JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 21:58JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 21:58JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 21:58JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 21:58JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 21:58JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 21:58JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 21:58JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 21:58JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 21:58JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 21:58JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 21:58JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 21:58JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 21:58JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 21:58JLB
POJ0321
1,4-Dichlorobenzene
<0.050
ug/L
1
0.50
0.050
1
8260D
10/21/20 21:58JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 21:58JLB
POJ0321
Acetone
<0.31
ug/L
100
5.0
0.31
1
8260D
10/21/20 21:58JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 21:58JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 21:58JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 21:58JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 21:58JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 21:58JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 21:58JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 21:58JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 21:58JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 21:58JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 21:58JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 21:58JLB
POJ0321
Chlorobenzene
<0.062
ug/L
3
0.50
0.062
1
8260D
10/21/20 21:58JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 21:58JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 21:58JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 21:58JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 21:58JLB
POJ0321
cis- 1,2-Dichloroethylene
<0.056
ug/L
2
0.50
0.056
1
8260D
10/21/20 21:58JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 96
.
Laboratory Report
• �
Waynt..
12/01/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID:
SW-01-20201014
Attn: Alec Macbeth
Sample ID: 0100203-03
231 Haywood Street
Project No.:
50-02
Work
Order: 0100203
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/14/20 13:00
Time
Submitted: 10/15/20
08:45
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 21:58JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 21:58JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 21:58JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 21:58JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 21:58JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 21:58JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 21:58JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 21:58JLB
POJ0321
m,p-Xylenes
<0.12
ug/L
NE
1.0
0.12
1
8260D
10/21/20 21:58JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 21:58JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 21:58JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 21:58JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 21:58JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 21:58JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 21:58JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 21:58JLB
POJ0321
Naphthalene
0.87
J ug/L
10
1.0
0.30
1
8260D
10/21/20 21:58JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 21:58JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 21:58JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 21:58JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 21:58JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 21:58JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 21:58JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 21:58JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 21:58JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 21:58JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 21:58JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 21:58JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 21:58JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 21:58JLB
POJ0321
Xylenes, total
<0.15
ug/L
5
1.5
0.15
1
8260D
10/21/20 21:58JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
100 % 80-124
Dibromofluoromethane
110 % 75-129
Toluene-d8
100 % 77-123
Volatile Organic Compounds by GC/MS
SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/16/20 23:44ANG
POJ0316
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 96
Laboratory Report
• � 12/01/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-03
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:00
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
8270 Extended List
1,3,5-Tri n itrobenzene
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
1,4-Naphthoquinone
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
1-Naphthylamine
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
2-Acetylaminofluorene
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
2-Naphthylamine
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
3-Methylcholanthrene
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
4-Aminobiphenyl
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
5-Nitro-o-toluidine
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
7,12-D1methyl benz(a)anthrace ne
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
Diallate
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
Hexachloropropene
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
Isosafrole
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
Kepone
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
Methapyrilene
<13.4
Ng/L
26.7
13.4
1
8270D
10/20/20 19:57BGV
L517325
N-Nitrosomethylethyl amine
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
N-Nitrosopiperidine
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
N-Nitrosopyrrolidine
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
o-Toluidine
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
p-Dimethylaminoazobenzene
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
p-Phenylenediamine
<13.3 L
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57 BGV
L517325
Pronamide
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
Safrole
<13.3
Ng/L
13.3
13.3
1
8270D
10/20/20 19:57BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
<0.01002
Ng/L
0.03
0.01002
1
8151A
10/22/20 17:45VIC
L517923
2,4,5-TP (Silvex)
<0.01634
Ng/L
0.1
0.01634
1
8151A
10/22/20 17:45VIC
L517923
2,4-D
<0.2078
Ng/L
0.25
0.2078
1
8151A
10/22/20 17:45VIC
L517923
2,4-DB
<0.1364
Ng/L
0.1
0.1364
1
8151A
10/22/20 17:45VIC
L517923
Dalapon
<0.5149
Ng/L
0.55
0.5149
1
8151A
10/22/20 17:45VIC
L517923
Dicamba
<0.057
Ng/L
0.25
0.057
1
8151A
10/22/20 17:45VIC
L517923
Dichlorprop
<0.07959
Ng/L
0.1
0.07959
1
8151A
10/22/20 17:45VIC
L517923
Dinoseb
<0.02698
Ng/L
0.1
0.02698
1
8151A
10/22/20 17:45VIC
L517923
MCPA
<18.98
Ng/L
50
18.98
1
8151A
10/22/20 17:45VIC
L517923
MCPP
<11.75
Ng/L
50
11.75
1
8151A
10/22/20 17:45VIC
L517923
Picloram
<0.04528
Ng/L
0.1
0.04528
1
8151A
10/22/20 17:45VIC
L517923
Surrogate
Recovery Control Limits
DCAA 48.1 % 20-150
Semivolatile Organic Compounds - GC/MS
1,2,4,5-Tetrachlorobenzene <0.422 Ng/L 6.67 0.422 1 8270D 10/20/20 19:57BGV L517328
1,2,4-Trichlorobenzene <0.642 Ng/L 6.67 0.642 1 8270D 10/20/20 19:57BGV L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 96
® Laboratory Report
IL AL i • . 12/01 /2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-03
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
1,2-Dichlorobenzene
<0.839
pg/L
6.67
0.839
1
8270D
10/20/20 19:57BGV
L517328
1,3-Dichlorobenzene
<0.654
pg/L
6.67
0.654
1
8270D
10/20/20 19:57BGV
L517328
1,4-Dichlorobenzene
<0.773
pg/L
6.67
0.773
1
8270D
10/20/20 19:57BGV
L517328
2,3,4,6-Tetrachlorophenol
<0.473
pg/L
6.67
0.473
1
8270D
10/20/20 19:57BGV
L517328
2,4,5-Trichlorophenol
<0.466
pg/L
6.67
0.466
1
8270D
10/20/20 19:57BGV
L517328
2,4,6-Trichlorophenol
<0.458
pg/L
6.67
0.458
1
8270D
10/20/20 19:57BGV
L517328
2,4-Dichlorophenol
<2.03
pg/L
6.67
2.03
1
8270D
10/20/20 19:57BGV
L517328
2,4-Dimethylphenol
<0.899
pg/L
6.67
0.899
1
8270D
10/20/20 19:57BGV
L517328
2,4-Dinitrophenol
<6.45
pg/L
13.3
6.45
1
8270D
10/20/20 19:57BGV
L517328
2,4-Dinitrotoluene
<0.537
pg/L
6.67
0.537
1
8270D
10/20/20 19:57BGV
L517328
2,6-Dichlorophenol
<0.937
pg/L
6.67
0.937
1
8270D
10/20/20 19:57BGV
L517328
2,6-Dinitrotoluene
<0.55
pg/L
6.67
0.55
1
8270D
10/20/20 19:57BGV
L517328
2-Chloronaphthalene
<0.634
pg/L
6.67
0.634
1
8270D
10/20/20 19:57BGV
L517328
2-Chlorophenol
<0.981
pg/L
6.67
0.981
1
8270D
10/20/20 19:57BGV
L517328
2-Methyl naphthalene
<0.647
pg/L
2.67
0.647
1
8270D
10/20/20 19:57BGV
L517328
2-Methylphenol
<0.961
pg/L
6.67
0.961
1
8270D
10/20/20 19:57BGV
L517328
2-Nitroaniline
<0.765
pg/L
6.67
0.765
1
8270D
10/20/20 19:57BGV
L517328
2-Nitrophenol
<0.808
pg/L
6.67
0.808
1
8270D
10/20/20 19:57BGV
L517328
3&4 Methylphenol
<0.921
pg/L
6.67
0.921
1
8270D
10/20/20 19:57BGV
L517328
3,3' Dimethylbenzidine
<2.5
pg/L
13.3
2.5
1
8270D
10/20/20 19:57BGV
L517328
3,3'-Dichlorobenzidine
<4.97
pg/L
13.3
4.97
1
8270D
10/20/20 19:57BGV
L517328
3-Nitroaniline
<2.03
pg/L
13.3
2.03
1
8270D
10/20/20 19:57BGV
L517328
4,6-Dinitro-2-methylphenol
<4.62
pg/L
13.3
4.62
1
8270D
10/20/20 19:57BGV
L517328
4-Bromophenyl phenyl ether
<0.667
pg/L
6.67
0.667
1
8270D
10/20/20 19:57BGV
L517328
4-Chloro-3-methylphenol
<0.671
pg/L
6.67
0.671
1
8270D
10/20/20 19:57BGV
L517328
4-Chloroaniline
<0.701
pg/L
6.67
0.701
1
8270D
10/20/20 19:57BGV
L517328
4-Chlorophenyl phenyl ether
<0.638
pg/L
6.67
0.638
1
8270D
10/20/20 19:57BGV
L517328
4-Nitroaniline
<0.987
pg/L
6.67
0.987
1
8270D
10/20/20 19:57BGV
L517328
4-Nitrophenol
<1.85
pg/L
13.3
1.85
1
8270D
10/20/20 19:57BGV
L517328
Acenaphthene
<0.563
pg/L
2.67
0.563
1
8270D
10/20/20 19:57BGV
L517328
Acenaphthylene
<0.572
pg/L
2.67
0.572
1
8270D
10/20/20 19:57BGV
L517328
Acetophenone
<0.915
pg/L
6.67
0.915
1
8270D
10/20/20 19:57BGV
L517328
Aniline
<0.421
pg/L
6.67
0.421
1
8270D
10/20/20 19:57BGV
L517328
Anthracene
<0.623
pg/L
2.67
0.623
1
8270D
10/20/20 19:57BGV
L517328
Benzidine
<0.919
pg/L
26.7
0.919
1
8270D
10/20/20 19:57BGV
L517328
Benzo(a)anthracene
<0.57
pg/L
2.67
0.57
1
8270D
10/20/20 19:57BGV
L517328
Benzo(a)pyrene
<1.34
pg/L
2.67
1.34
1
8270D
10/20/20 19:57BGV
L517328
Benzo(b)fluoranthene
<1.26
pg/L
2.67
1.26
1
8270D
10/20/20 19:57BGV
L517328
Benzo(g,hJ)perylene
<1.81
pg/L
2.67
1.81
1
8270D
10/20/20 19:57BGV
L517328
Benzo(k)fluoranthene
<1
pg/L
2.67
1
1
8270D
10/20/20 19:57BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 96
® Laboratory Report
IL AL i • . 12/01 /2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-01-20201014
Attn: Alec Macbeth Sample ID: 0100203-03
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Benzoic Acid
<6.65
pg/L
13.3
6.65
1
8270D
10/20/20 19:57 BGV
L517328
Benzyl alcohol
<4
pg/L
13.3
4
1
8270D
10/20/20 19:57BGV
L517328
Bis(2-Chloroethoxy)methane
<0.577
pg/L
6.67
0.577
1
8270D
10/20/20 19:57BGV
L517328
Bis(2-Chloroethyl)ether
<0.596
pg/L
6.67
0.596
1
8270D
10/20/20 19:57BGV
L517328
Bis(2-Chloroisopropyl)ether
<0.728
pg/L
6.67
0.728
1
8270D
10/20/20 19:57BGV
L517328
Bis(2-ethylhexyl)phthalate
<4.88
pg/L
6.67
4.88
1
8270D
10/20/20 19:57BGV
L517328
Butyl benzyl phthalate
<6.13
pg/L
6.67
6.13
1
8270D
10/20/20 19:57BGV
L517328
Carbazole
<0.634
pg/L
6.67
0.634
1
8270D
10/20/20 19:57BGV
L517328
Chrysene
<0.975
pg/L
2.67
0.975
1
8270D
10/20/20 19:57BGV
L517328
Dibenz(a,h)anthracene
<0.336
pg/L
2.67
0.336
1
8270D
10/20/20 19:57BGV
L517328
Dibenzofuran
<0.564
pg/L
6.67
0.564
1
8270D
10/20/20 19:57BGV
L517328
Diethyl phthalate
<0.78
pg/L
6.67
0.78
1
8270D
10/20/20 19:57BGV
L517328
Dimethyl phthalate
<0.68
pg/L
6.67
0.68
1
8270D
10/20/20 19:57BGV
L517328
Di-n-butyl phthalate
<2.1
pg/L
6.67
2.1
1
8270D
10/20/20 19:57BGV
L517328
Di-n-Octyl Phthalate
<2.3
pg/L
6.67
2.3
1
8270D
10/20/20 19:57BGV
L517328
Fluoranthene
<0.542
pg/L
2.67
0.542
1
8270D
10/20/20 19:57BGV
L517328
Fluorene
<0.592
pg/L
2.67
0.592
1
8270D
10/20/20 19:57BGV
L517328
Hexachlorobenzene
<3.43
pg/L
6.67
3.43
1
8270D
10/20/20 19:57BGV
L517328
Hexachlorobutadiene
<0.54
pg/L
6.67
0.54
1
8270D
10/20/20 19:57BGV
L517328
Hexachlorocyclopentadiene
<3.12
pg/L
6.67
3.12
1
8270D
10/20/20 19:57BGV
L517328
Hexachloroethane
<0.369
pg/L
6.67
0.369
1
8270D
10/20/20 19:57BGV
L517328
Indeno(1,2,3-cd)pyrene
<1.35
pg/L
2.67
1.35
1
8270D
10/20/20 19:57BGV
L517328
Isophorone
<0.48
pg/L
6.67
0.48
1
8270D
10/20/20 19:57BGV
L517328
Naphthalene
<0.646
pg/L
2.67
0.646
1
8270D
10/20/20 19:57BGV
L517328
Nitrobenzene
<0.708
pg/L
6.67
0.708
1
8270D
10/20/20 19:57BGV
L517328
N-Nitrosodiethylamine
<0.533
pg/L
6.67
0.533
1
8270D
10/20/20 19:57BGV
L517328
N-Nitrosodimethylamine
<0.332
pg/L
6.67
0.332
1
8270D
10/20/20 19:57BGV
L517328
N-Nitroso-di-n-butylamine
<1
pg/L
6.67
1
1
8270D
10/20/20 19:57BGV
L517328
N-Nitroso-di-n-propylamine
<0.445
pg/L
6.67
0.445
1
8270D
10/20/20 19:57BGV
L517328
N-Nitrosodiphenylamine
<1.04
pg/L
13.3
1.04
1
8270D
10/20/20 19:57BGV
L517328
Pentachlorophenol
<3.26
pg/L
13.3
3.26
1
8270D
10/20/20 19:57BGV
L517328
Phenanthrene
<0.619
pg/L
2.67
0.619
1
8270D
10/20/20 19:57BGV
L517328
Phenol
<0.518
pg/L
6.67
0.518
1
8270D
10/20/20 19:57BGV
L517328
Pyrene
<1.39
pg/L
2.67
1.39
1
8270D
10/20/20 19:57BGV
L517328
Pyridine
<0.901
pg/L
13.3
0.901
1
8270D
10/20/20 19:57BGV
L517328
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
27.5 % 39-110
SR
2-Fluorobiphenyl
41.6 % 24-93
2-Fluorophenol
11.8 % 10-44
4-Terphenyl-d14
41.8 % 35-126
Nitrobenzene-d5
44.6 % 20-91
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 96
0
Way poi nt.
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2020 Fall
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
12/01/2020
Client Sample ID: SW-01-20201014
Sample ID: 0100203-03
Work Order: 0100203
Time Collected: 10/14/20 13:00
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Phenol-d6
10.3 % 7-32
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 23 of 96
Laboratory Report
A i • .0 12/01/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-02-20201014
Attn: Alec Macbeth Sample ID: 0100203-04
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:30
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Dissolved Metals
Mercury
<0.034
ug/L
0.20
0.034
1
7470A
10/21/20 16:18EDV
POJ0394
Antimony
0.54 J
ug/L
2.0
0.49
1
6020B
10/28/20 12:45JAB
POJ0496
Arsenic
<0.17
ug/L
1.0
0.17
1
6020B
10/28/20 12:45JAB
POJ0496
Barium
10
ug/L
100
10
0.81
1
6020B
10/28/20 12:45JAB
POJ0496
Beryllium
<0.19
ug/L
1.0
0.19
1
6020B
10/28/20 12:45JAB
POJ0496
Cadmium
<0.16
ug/L
1.0
0.16
1
6020B
10/28/20 12:45JAB
POJ0496
Chromium
<0.79
ug/L
2.0
0.79
1
6020B
10/28/20 12:45JAB
POJ0496
Cobalt
<0.52
ug/L
2.0
0.52
1
6020B
10/28/20 12:45JAB
POJ0496
Copper
<3.8
ug/L
10
3.8
1
6020B
10/28/20 12:45JAB
POJ0496
Lead
<0.26
ug/L
1.0
0.26
1
6020B
10/28/20 12:45JAB
POJ0496
Nickel
<0.51
ug/L
50
3.0
0.51
1
6020B
10/28/20 12:45JAB
POJ0496
Selenium
<0.74
ug/L
10
5.0
0.74
1
6020B
10/28/20 12:45JAB
POJ0496
Silver
<0.11
ug/L
1.0
0.11
1
6020B
10/28/20 12:45JAB
POJ0496
Thallium
<0.57
ug/L
2.0
0.57
1
6020B
10/28/20 12:45JAB
POJ0496
Tin
<1.8
ug/L
5.0
1.8
1
6020B
10/28/20 12:45JAB
POJ0496
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/28/20 12:45JAB
POJ0496
Zinc
<6.9
ug/L
20
6.9
1
6020B
10/28/20 12:45JAB
POJ0496
General Chemistry Parameters
Hardness
5500
ug/L
5000
570
1
SM2340 C
10/15/20 15:43BMS
POJ0269
Organochlorine Pesticides by GC/ECD
4,4'-DDD
<0.027
ug/L
0.1
0.10
0.027
1
8081 B
10/19/20 13:01NMB
POJ0286
4,4'-DDE
<0.022
ug/L
0.1
0.10
0.022
1
8081 B
10/19/20 13:01NMB
POJ0286
4,4'-DDT
<0.018
ug/L
0.1
0.10
0.018
1
8081 B
10/19/20 13:01NMB
POJ0286
Aldrin
<0.015
ug/L
0.05
0.051
0.015
1
8081 B
10/19/20 13:01NMB
POJ0286
alpha-BHC
<0.0064
ug/L
0.05
0.051
0.0064
1
8081 B
10/19/20 13:01NMB
POJ0286
cis -Chlordane
<0.019
ug/L
NE
0.10
0.019
1
8081 B
10/19/20 13:01NMB
POJ0286
beta-BHC
<0.011
ug/L
0.05
0.051
0.011
1
8081 B
10/19/20 13:01NMB
POJ0286
Chlordane
<0.18
ug/L
0.5
0.51
0.18
1
8081 B
10/19/20 13:01NMB
POJ0286
delta-BHC
<0.0083
ug/L
0.05
0.051
0.0083
1
8081 B
10/19/20 13:01NMB
POJ0286
Dieldrin
<0.014
ug/L
0.002
0.051
0.014
1
8081 B
10/19/20 13:01NMB
POJ0286
Endosulfan 1
<0.016
ug/L
0.1
0.051
0.016
1
8081 B
10/19/20 13:01NMB
POJ0286
Endosulfan 11
<0.012
ug/L
0.1
0.051
0.012
1
8081 B
10/19/20 13:01NMB
POJ0286
Endosulfan Sulfate
<0.017
ug/L
0.1
0.051
0.017
1
8081 B
10/19/20 13:01NMB
POJ0286
Endrin
<0.014
ug/L
0.1
0.051
0.014
1
8081 B
10/19/20 13:01NMB
POJ0286
Endrin Aldehyde
<0.016
ug/L
0.1
0.051
0.016
1
8081 B
10/19/20 13:01NMB
POJ0286
Endrin Ketone
<0.018
ug/L
NE
0.10
0.018
1
8081 B
10/19/20 13:01NMB
POJ0286
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 96
.
Laboratory Report
•
Waynt.�
�
12/01/2020
poi
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2020 Fall
Client Sample ID: SW-02-20201014
Attn: Alec Macbeth
Sample ID: 0100203-04
231 Haywood Street
Project No.:
50-02
Work Order: 0100203
Asheville, NC 28801
Sample Matrix:
Water
Time Collected:
10/14/20 13:30
Time Submitted:
10/15/20 08:45
Parameter
Result
Units
SWSL
Report
MDL
Dilution Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
gamma-BHC
<0.0062
ug/L
0.05
0.051
0.0062
1 8081 B
10/19/20 13:01NMB
POJ0286
trans -Chlordane
<0.023
ug/L
NE
0.10
0.023
1 8081 B
10/19/20 13:01NMB
POJ0286
Heptachlor
<0.013
ug/L
0.05
0.051
0.013
1 8081 B
10/19/20 13:01NMB
POJ0286
Heptachlor Epoxide
<0.023
ug/L
0.075
0.10
0.023
1 8081 B
10/19/20 13:01NMB
POJ0286
Methoxychlor
<0.018
ug/L
NE
0.10
0.018
1 8081 B
10/19/20 13:01NMB
POJ0286
Toxaphene
<0.35
ug/L
1.5
1.0
0.35
1 8081 B
10/19/20 13:01NMB
POJ0286
Surrogate
Recovery Control Limits
Decachlorobiphenyl
73 % 13-186
Tetrachloro-m-xylene
73 % 40-134
Polychlorinated Biphenyls (PCBs) by GC/ECD
Aroclor 1016
<0.21
ug/L
NE
0.51
0.21
1 8082A
10/19/20 13:01NMB
POJ0286
Aroclor 1221
<0.11
ug/L
NE
1.0
0.11
1 8082A
10/19/20 13:01NMB
POJ0286
Aroclor 1232
<0.16
ug/L
NE
0.51
0.16
1 8082A
10/19/20 13:01NMB
POJ0286
Aroclor 1242
<0.14
ug/L
NE
0.51
0.14
1 8082A
10/19/20 13:01NMB
POJ0286
Aroclor 1248
<0.14
ug/L
NE
0.51
0.14
1 8082A
10/19/20 13:01NMB
POJ0286
Aroclor 1254
<0.16
ug/L
NE
0.51
0.16
1 8082A
10/19/20 13:01NMB
POJ0286
Aroclor 1260
<0.50
ug/L
NE
1.0
0.50
1 8082A
10/19/20 13:01NMB
POJ0286
Surrogate
Recovery Control Limits
Tetrachloro-m-xylene
71 % 30-161
Decachlorobiphenyl
76 % 32-178
Total Metals
Mercury
0.95
ug/L
0.2
0.20
0.034
1
7470A
10/20/20 15:49EDV
POJ0374
Antimony
<0.49
ug/L
6
2.0
0.49
1
6020B
10/24/20 8:09 JAB
POJ0312
Arsenic
<0.17
ug/L
10
1.0
0.17
1
6020B
10/24/20 8:09 JAB
POJ0312
Barium
16
ug/L
100
2.0
0.81
1
6020B
10/24/20 8:09 JAB
POJ0312
Beryllium
<0.19
ug/L
1
1.0
0.19
1
6020B
10/27/20 15:29JAB
POJ0312
Cadmium
<0.16
ug/L
1
1.0
0.16
1
6020B
10/24/20 8:09 JAB
POJ0312
Chromium
0.94
J
ug/L
10
2.0
0.79
1
6020B
10/27/20 22:24JAB
POJ0491
Cobalt
<0.52
ug/L
10
2.0
0.52
1
6020B
10/24/20 8:09 JAB
POJ0312
Copper
<3.8
ug/L
10
10
3.8
1
6020B
10/24/20 8:09 JAB
POJ0312
Lead
0.38
J
ug/L
10
1.0
0.26
1
6020B
10/24/20 8:09 JAB
POJ0312
Nickel
1.5
J
ug/L
50
3.0
0.51
1
6020B
10/24/20 8:09 JAB
POJ0312
Selenium
0.85
J
ug/L
10
5.0
0.74
1
6020B
10/24/20 8:09 JAB
POJ0312
Silver
<0.11
ug/L
10
1.0
0.11
1
6020B
10/27/20 22:24JAB
POJ0491
Thallium
<0.38
ug/L
5.5
2.0
0.38
1
6020B
10/24/20 8:09 JAB
POJ0312
Tin
<1.8
ug/L
100
5.0
1.8
1
6020B
10/27/20 22:24JAB
POJ0491
Vanadium
<1.3
ug/L
25
5.0
1.3
1
6020B
10/24/20 8:09 JAB
POJ0312
Zinc
<6.9
ug/L
10
20
6.9
1
6020B
10/24/20 8:09 JAB
POJ0312
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 25 of 96
Laboratory Report
• � 12/01/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-02-20201014
Attn: Alec Macbeth Sample ID: 0100203-04
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:30
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 22:32JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 22:32JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 22:32JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 22:32JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 22:32JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 22:32JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 22:32JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 22:32JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 22:32JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 22:32JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 22:32JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 22:32JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 22:32JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 22:32JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 22:32JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 22:32JLB
POJ0321
1,4-Dichlorobenzene
<0.050
ug/L
1
0.50
0.050
1
8260D
10/21/20 22:32JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 22:32JLB
POJ0321
Acetone
<0.31
ug/L
100
5.0
0.31
1
8260D
10/21/20 22:32JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 22:32JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 22:32JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 22:32JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 22:32JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 22:32JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 22:32JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 22:32JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 22:32JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 22:32JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 22:32JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 22:32JLB
POJ0321
Chlorobenzene
<0.062
ug/L
3
0.50
0.062
1
8260D
10/21/20 22:32JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 22:32JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 22:32JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 22:32JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 22:32JLB
POJ0321
cis- 1,2-Dichloroethylene
<0.056
ug/L
2
0.50
0.056
1
8260D
10/21/20 22:32JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 96
Laboratory Report
A i • .0 12/01/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-02-20201014
Attn: Alec Macbeth Sample ID: 0100203-04
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:30
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 22:32JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 22:32JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 22:32JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 22:32JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 22:32JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 22:32JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 22:32JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 22:32JLB
POJ0321
m,p-Xylenes
<0.12
ug/L
NE
1.0
0.12
1
8260D
10/21/20 22:32JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 22:32JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 22:32JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 22:32JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 22:32JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 22:32JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 22:32JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 22:32JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 22:32JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 22:32JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 22:32JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 22:32JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 22:32JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 22:32JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 22:32JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 22:32JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 22:32JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 22:32JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 22:32JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 22:32JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 22:32JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 22:32JLB
POJ0321
Xylenes, total
<0.15
ug/L
5
1.5
0.15
1
8260D
10/21/20 22:32JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
102 % 80-124
Dibromofluoromethane
111 % 75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GC/MS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/17/20 0:09ANG
POJ0316
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 96
Laboratory Report
• � 12/01/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-02-20201014
Attn: Alec Macbeth Sample ID: 0100203-04
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:30
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
8270 Extended List
1,3,5-Tri n itrobenzene
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
1,4-Naphthoquinone
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
1-Naphthylamine
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
2-Acetylaminofluorene
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
2-Naphthylamine
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
3-Methylcholanthrene
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
4-Aminobiphenyl
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
5-Nitro-o-toluidine
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
7,12-D1methyl benz(a)anthrace ne
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
Diallate
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
Hexachloropropene
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
Isosafrole
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
Kepone
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19 BGV
L517325
Methapyrilene
<10.3
Ng/L
20.6
10.3
1
8270D
10/20/20 20:19BGV
L517325
N-Nitrosomethylethyl amine
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
N-Nitrosopiperidine
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
N-Nitrosopyrrolidine
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
o-Toluidine
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
p-Dimethylaminoazobenzene
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
p-Phenylenediamine
<10.3 L
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19 BGV
L517325
Pronamide
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
Safrole
<10.3
Ng/L
10.3
10.3
1
8270D
10/20/20 20:19BGV
L517325
Phenoxy Acid Herbicides - GC/ECD
2,4,5-T
<0.01002
Ng/L
0.03
0.01002
1
8151A
10/22/20 18:10VIC
L517923
2,4,5-TP (Silvex)
<0.01634
Ng/L
0.1
0.01634
1
8151A
10/22/20 18:10VIC
L517923
2,4-D
<0.2078
Ng/L
0.25
0.2078
1
8151A
10/22/20 18:10VIC
L517923
2,4-DB
<0.1364
Ng/L
0.1
0.1364
1
8151A
10/22/20 18:10VIC
L517923
Dalapon
<0.5149
Ng/L
0.55
0.5149
1
8151A
10/22/20 18:10VIC
L517923
Dicamba
<0.057
Ng/L
0.25
0.057
1
8151A
10/22/20 18:10VIC
L517923
Dichlorprop
<0.07959
Ng/L
0.1
0.07959
1
8151A
10/22/20 18:10VIC
L517923
Dinoseb
<0.02698
Ng/L
0.1
0.02698
1
8151A
10/22/20 18:10VIC
L517923
MCPA
<18.98
Ng/L
50
18.98
1
8151A
10/22/20 18:10VIC
L517923
MCPP
<11.75
Ng/L
50
11.75
1
8151A
10/22/20 18:10VIC
L517923
Picloram
<0.04528
Ng/L
0.1
0.04528
1
8151A
10/22/20 18:10VIC
L517923
Surrogate
Recovery Control Limits
DCAA 55.7 % 20-150
Semivolatile Organic Compounds - GC/MS
1,2,4,5-Tetrachlorobenzene <0.326 Ng/L 5.15 0.326 1 8270D 10/20/20 20:19BGV L517328
1,2,4-Trichlorobenzene <0.496 Ng/L 5.15 0.496 1 8270D 10/20/20 20:19BGV L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 96
® Laboratory Report
IL AL i • . 12/01 /2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-02-20201014
Attn: Alec Macbeth Sample ID: 0100203-04
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:30
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
1,2-Dichlorobenzene
<0.647
pg/L
5.15
0.647
1
8270D
10/20/20 20:19BGV
L517328
1,3-Dichlorobenzene
<0.505
pg/L
5.15
0.505
1
8270D
10/20/20 20:19BGV
L517328
1,4-Dichlorobenzene
<0.597
pg/L
5.15
0.597
1
8270D
10/20/20 20:19BGV
L517328
2,3,4,6-Tetrachlorophenol
<0.365
pg/L
5.15
0.365
1
8270D
10/20/20 20:19BGV
L517328
2,4,5-Trichlorophenol
<0.36
pg/L
5.15
0.36
1
8270D
10/20/20 20:19BGV
L517328
2,4,6-Trichlorophenol
<0.354
pg/L
5.15
0.354
1
8270D
10/20/20 20:19BGV
L517328
2,4-Dichlorophenol
<1.57
pg/L
5.15
1.57
1
8270D
10/20/20 20:19BGV
L517328
2,4-Dimethylphenol
<0.694
pg/L
5.15
0.694
1
8270D
10/20/20 20:19BGV
L517328
2,4-Dinitrophenol
<5
pg/L
10.3
5
1
8270D
10/20/20 20:19BGV
L517328
2,4-Dinitrotoluene
<0.415
pg/L
5.15
0.415
1
8270D
10/20/20 20:19BGV
L517328
2,6-Dichlorophenol
<0.724
pg/L
5.15
0.724
1
8270D
10/20/20 20:19BGV
L517328
2,6-Dinitrotoluene
<0.425
pg/L
5.15
0.425
1
8270D
10/20/20 20:19BGV
L517328
2-Chloronaphthalene
<0.49
pg/L
5.15
0.49
1
8270D
10/20/20 20:19BGV
L517328
2-Chlorophenol
<0.758
pg/L
5.15
0.758
1
8270D
10/20/20 20:19BGV
L517328
2-Methyl naphthalene
<0.499
pg/L
2.06
0.499
1
8270D
10/20/20 20:19BGV
L517328
2-Methylphenol
<0.742
pg/L
5.15
0.742
1
8270D
10/20/20 20:19BGV
L517328
2-Nitroaniline
<0.591
pg/L
5.15
0.591
1
8270D
10/20/20 20:19BGV
L517328
2-Nitrophenol
<0.624
pg/L
5.15
0.624
1
8270D
10/20/20 20:19BGV
L517328
3&4 Methylphenol
<0.711
pg/L
5.15
0.711
1
8270D
10/20/20 20:19BGV
L517328
3,3' Dimethylbenzidine
<1.94
pg/L
10.3
1.94
1
8270D
10/20/20 20:19BGV
L517328
3,3'-Dichlorobenzidine
<3.85
pg/L
10.3
3.85
1
8270D
10/20/20 20:19BGV
L517328
3-Nitroaniline
<1.58
pg/L
10.3
1.58
1
8270D
10/20/20 20:19BGV
L517328
4,6-Dinitro-2-methylphenol
<3.57
pg/L
10.3
3.57
1
8270D
10/20/20 20:19BGV
L517328
4-Bromophenyl phenyl ether
<0.515
pg/L
5.15
0.515
1
8270D
10/20/20 20:19BGV
L517328
4-Chloro-3-methylphenol
<0.518
pg/L
5.15
0.518
1
8270D
10/20/20 20:19BGV
L517328
4-Chloroaniline
<0.541
pg/L
5.15
0.541
1
8270D
10/20/20 20:19BGV
L517328
4-Chlorophenyl phenyl ether
<0.493
pg/L
5.15
0.493
1
8270D
10/20/20 20:19BGV
L517328
4-Nitroaniline
<0.762
pg/L
5.15
0.762
1
8270D
10/20/20 20:19BGV
L517328
4-Nitrophenol
<1.43
pg/L
10.3
1.43
1
8270D
10/20/20 20:19BGV
L517328
Acenaphthene
<0.434
pg/L
2.06
0.434
1
8270D
10/20/20 20:19BGV
L517328
Acenaphthylene
<0.441
pg/L
2.06
0.441
1
8270D
10/20/20 20:19BGV
L517328
Acetophenone
<0.706
pg/L
5.15
0.706
1
8270D
10/20/20 20:19BGV
L517328
Aniline
<0.325
pg/L
5.15
0.325
1
8270D
10/20/20 20:19BGV
L517328
Anthracene
<0.481
pg/L
2.06
0.481
1
8270D
10/20/20 20:19BGV
L517328
Benzidine
<0.709
pg/L
20.6
0.709
1
8270D
10/20/20 20:19BGV
L517328
Benzo(a)anthracene
<0.439
pg/L
2.06
0.439
1
8270D
10/20/20 20:19BGV
L517328
Benzo(a)pyrene
<1.03
pg/L
2.06
1.03
1
8270D
10/20/20 20:19BGV
L517328
Benzo(b)fluoranthene
<0.969
pg/L
2.06
0.969
1
8270D
10/20/20 20:19BGV
L517328
Benzo(g,hJ)perylene
<1.4
pg/L
2.06
1.4
1
8270D
10/20/20 20:19BGV
L517328
Benzo(k)fluoranthene
<0.774
pg/L
2.06
0.774
1
8270D
10/20/20 20:19BGV
L517328
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 96
® Laboratory Report
IL AL i • . 12/01 /2020
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: SW-02-20201014
Attn: Alec Macbeth Sample ID: 0100203-04
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 13:30
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Benzoic Acid
<5.15
pg/L
10.3
5.15
1
8270D
10/20/20 20:19 BGV
L517328
Benzyl alcohol
<3.1
pg/L
10.3
3.1
1
8270D
10/20/20 20:19BGV
L517328
Bis(2-Chloroethoxy)methane
<0.445
pg/L
5.15
0.445
1
8270D
10/20/20 20:19BGV
L517328
Bis(2-Chloroethyl)ether
<0.46
pg/L
5.15
0.46
1
8270D
10/20/20 20:19BGV
L517328
Bis(2-Chloroisopropyl)ether
<0.562
pg/L
5.15
0.562
1
8270D
10/20/20 20:19BGV
L517328
Bis(2-ethylhexyl)phthalate
<3.77
pg/L
5.15
3.77
1
8270D
10/20/20 20:19BGV
L517328
Butyl benzyl phthalate
<4.73
pg/L
5.15
4.73
1
8270D
10/20/20 20:19BGV
L517328
Carbazole
<0.49
pg/L
5.15
0.49
1
8270D
10/20/20 20:19BGV
L517328
Chrysene
<0.752
pg/L
2.06
0.752
1
8270D
10/20/20 20:19BGV
L517328
Dibenz(a,h)anthracene
<0.259
pg/L
2.06
0.259
1
8270D
10/20/20 20:19BGV
L517328
Dibenzofuran
<0.435
pg/L
5.15
0.435
1
8270D
10/20/20 20:19BGV
L517328
Diethyl phthalate
<0.602
pg/L
5.15
0.602
1
8270D
10/20/20 20:19BGV
L517328
Dimethyl phthalate
<0.525
pg/L
5.15
0.525
1
8270D
10/20/20 20:19BGV
L517328
Di-n-butyl phthalate
<1.62
pg/L
5.15
1.62
1
8270D
10/20/20 20:19BGV
L517328
Di-n-Octyl Phthalate
<1.77
pg/L
5.15
1.77
1
8270D
10/20/20 20:19BGV
L517328
Fluoranthene
<0.418
pg/L
2.06
0.418
1
8270D
10/20/20 20:19BGV
L517328
Fluorene
<0.457
pg/L
2.06
0.457
1
8270D
10/20/20 20:19BGV
L517328
Hexachlorobenzene
<2.65
pg/L
5.15
2.65
1
8270D
10/20/20 20:19BGV
L517328
Hexachlorobutadiene
<0.417
pg/L
5.15
0.417
1
8270D
10/20/20 20:19BGV
L517328
Hexachlorocyclopentadiene
<2.41
pg/L
5.15
2.41
1
8270D
10/20/20 20:19BGV
L517328
Hexachloroethane
<0.285
pg/L
5.15
0.285
1
8270D
10/20/20 20:19BGV
L517328
Indeno(1,2,3-cd)pyrene
<1.04
pg/L
2.06
1.04
1
8270D
10/20/20 20:19BGV
L517328
Isophorone
<0.37
pg/L
5.15
0.37
1
8270D
10/20/20 20:19BGV
L517328
Naphthalene
<0.498
pg/L
2.06
0.498
1
8270D
10/20/20 20:19BGV
L517328
Nitrobenzene
<0.546
pg/L
5.15
0.546
1
8270D
10/20/20 20:19BGV
L517328
N-Nitrosodiethylamine
<0.412
pg/L
5.15
0.412
1
8270D
10/20/20 20:19BGV
L517328
N-Nitrosodimethylamine
<0.256
pg/L
5.15
0.256
1
8270D
10/20/20 20:19BGV
L517328
N-Nitroso-di-n-butylamine
<0.774
pg/L
5.15
0.774
1
8270D
10/20/20 20:19BGV
L517328
N-Nitroso-di-n-propylamine
<0.344
pg/L
5.15
0.344
1
8270D
10/20/20 20:19BGV
L517328
N-Nitrosodiphenylamine
<0.806
pg/L
10.3
0.806
1
8270D
10/20/20 20:19BGV
L517328
Pentachlorophenol
<2.52
pg/L
10.3
2.52
1
8270D
10/20/20 20:19BGV
L517328
Phenanthrene
<0.477
pg/L
2.06
0.477
1
8270D
10/20/20 20:19BGV
L517328
Phenol
<0.4
pg/L
5.15
0.4
1
8270D
10/20/20 20:19BGV
L517328
Pyrene
<1.07
pg/L
2.06
1.07
1
8270D
10/20/20 20:19BGV
L517328
Pyridine
<0.698
pg/L
10.3
0.698
1
8270D
10/20/20 20:19BGV
L517328
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
45.3 % 39-110
2-Fluorobiphenyl
40.6 % 24-93
2-Fluorophenol
15.6 % 10-44
4-Terphenyl-d14
35 % 35-126
Nitrobenzene-d5
44 % 20-91
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 of 96
0
Way poi nt.
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2020 Fall
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
12/01/2020
Client Sample ID: SW-02-20201014
Sample ID: 0100203-04
Work Order: 0100203
Time Collected: 10/14/20 13:30
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Phenol-d6
11.9 % 7-32
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 31 of 96
Laboratory Report
• � 12/01/2020
PA Waynt.�
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: TB-202010140000
Attn: Alec Macbeth Sample ID: 0100203-06
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 00:00
Time Submitted: 10/15/20 08:45
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.11
ug/L
5
0.50
0.11
1
8260D
10/21/20 16:53JLB
POJ0321
1, 1, 1 -Trichloroethane
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 16:53JLB
POJ0321
1,1,2,2-Tetrachloroethane
<0.036
ug/L
3
0.50
0.036
1
8260D
10/21/20 16:53JLB
POJ0321
1,1,2-Trichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 16:53JLB
POJ0321
1,1-Dichloroethane
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 16:53JLB
POJ0321
1,1-Dichloroethylene
<0.083
ug/L
5
0.50
0.083
1
8260D
10/21/20 16:53JLB
POJ0321
1, 1 -Dichloropropylene
<0.051
ug/L
5
0.50
0.051
1
8260D
10/21/20 16:53JLB
POJ0321
1,2,3-Trichloropropane
<0.14
ug/L
1
1.0
0.14
1
8260D
10/21/20 16:53JLB
POJ0321
1,2,4-Trichlorobenzene
<0.13
ug/L
10
1.0
0.13
1
8260D
10/21/20 16:53JLB
POJ0321
1,2-Dibromo-3-chloropropane
<0.17
ug/L
13
2.0
0.17
1
8260D
10/21/20 16:53JLB
POJ0321
1,2-Dibromoethane
<0.051
ug/L
1
0.50
0.051
1
8260D
10/21/20 16:53JLB
POJ0321
1,2-Dichlorobenzene
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 16:53JLB
POJ0321
1,2-Dichloroethane
<0.066
ug/L
1
0.50
0.066
1
8260D
10/21/20 16:53JLB
POJ0321
1,2-Dichloropropane
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 16:53JLB
POJ0321
1,3-Dichlorobenzene
<0.054
ug/L
5
0.50
0.054
1
8260D
10/21/20 16:53JLB
POJ0321
1,3-Dichloropropane
<0.043
ug/L
1
0.50
0.043
1
8260D
10/21/20 16:53JLB
POJ0321
1,4-Dichlorobenzene
<0.050
ug/L
1
0.50
0.050
1
8260D
10/21/20 16:53JLB
POJ0321
2,2-Dichloropropane
<0.11
ug/L
15
2.0
0.11
1
8260D
10/21/20 16:53JLB
POJ0321
Acetone
3.0 J
ug/L
100
5.0
0.31
1
8260D
10/21/20 16:53JLB
POJ0321
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
10/21/20 16:53JLB
POJ0321
Acrolein
<0.20
ug/L
53
20
0.20
1
8260D
10/21/20 16:53JLB
POJ0321
Acrylonitrile
<0.20
ug/L
200
20
0.20
1
8260D
10/21/20 16:53JLB
POJ0321
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
10/21/20 16:53JLB
POJ0321
Benzene
<0.048
ug/L
1
0.50
0.048
1
8260D
10/21/20 16:53JLB
POJ0321
Bromochloromethane
<0.14
ug/L
3
0.50
0.14
1
8260D
10/21/20 16:53JLB
POJ0321
Bromodichloromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 16:53JLB
POJ0321
Bromoform
<0.040
ug/L
3
1.0
0.040
1
8260D
10/21/20 16:53JLB
POJ0321
Bromomethane
<0.18
ug/L
10
1.0
0.18
1
8260D
10/21/20 16:53JLB
POJ0321
Carbon disulfide
<0.075
ug/L
100
5.0
0.075
1
8260D
10/21/20 16:53JLB
POJ0321
Carbon Tetrachloride
<0.11
ug/L
1
0.50
0.11
1
8260D
10/21/20 16:53JLB
POJ0321
Chlorobenzene
<0.062
ug/L
3
0.50
0.062
1
8260D
10/21/20 16:53JLB
POJ0321
Chloroethane
<0.22
ug/L
10
0.50
0.22
1
8260D
10/21/20 16:53JLB
POJ0321
Chloroform
<0.076
ug/L
5
0.50
0.076
1
8260D
10/21/20 16:53JLB
POJ0321
Chloromethane
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 16:53JLB
POJ0321
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
10/21/20 16:53JLB
POJ0321
cis- 1,2-Dichloroethylene
<0.056
ug/L
2
0.50
0.056
1
8260D
10/21/20 16:53JLB
POJ0321
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 96
Laboratory Report
A i • .0 12/01/2020
- -ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Client Sample ID: TB-202010140000
Attn: Alec Macbeth Sample ID: 0100203-06
231 Haywood Street Project No.: 50-02 Work Order: 0100203
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/14/20 00:00
Time Submitted: 10/15/20 08:45
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
cis- 1,3-Dichloropropylene
<0.079
ug/L
1
0.50
0.079
1
8260D
10/21/20 16:53JLB
POJ0321
Dibromochloromethane
<0.081
ug/L
3
0.50
0.081
1
8260D
10/21/20 16:53JLB
POJ0321
Dibromomethane
<0.065
ug/L
10
0.50
0.065
1
8260D
10/21/20 16:53JLB
POJ0321
Dichlorodifluoromethane
<0.11
ug/L
5
5.0
0.11
1
8260D
10/21/20 16:53JLB
POJ0321
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
10/21/20 16:53JLB
POJ0321
Ethylbenzene
<0.061
ug/L
1
0.50
0.061
1
8260D
10/21/20 16:53JLB
POJ0321
Hexachlorobutadiene
<0.16
ug/L
10
2.0
0.16
1
8260D
10/21/20 16:53JLB
POJ0321
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
10/21/20 16:53JLB
POJ0321
m,p-Xylenes
<0.12
ug/L
NE
1.0
0.12
1
8260D
10/21/20 16:53JLB
POJ0321
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
10/21/20 16:53JLB
POJ0321
Methyl Butyl Ketone (2-Hexanone)
<0.065
ug/L
50
5.0
0.065
1
8260D
10/21/20 16:53JLB
POJ0321
Methyl Ethyl Ketone (2-Butanone)
<0.24
ug/L
100
5.0
0.24
1
8260D
10/21/20 16:53JLB
POJ0321
Methyl Iodide
<0.33
ug/L
10
5.0
0.33
1
8260D
10/21/20 16:53JLB
POJ0321
Methyl Isobutyl Ketone
<1.0
ug/L
100
5.0
1.0
1
8260D
10/21/20 16:53JLB
POJ0321
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
10/21/20 16:53JLB
POJ0321
Methylene Chloride
<0.083
ug/L
1
1.0
0.083
1
8260D
10/21/20 16:53JLB
POJ0321
Naphthalene
<0.30
ug/L
10
1.0
0.30
1
8260D
10/21/20 16:53JLB
POJ0321
o-Xylene
<0.044
ug/L
NE
0.50
0.044
1
8260D
10/21/20 16:53JLB
POJ0321
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
10/21/20 16:53JLB
POJ0321
Styrene
<0.047
ug/L
1
0.50
0.047
1
8260D
10/21/20 16:53JLB
POJ0321
Tetrachloroethylene
<0.098
ug/L
1
0.50
0.098
1
8260D
10/21/20 16:53JLB
POJ0321
Tetrahydrofuran
<1.1
ug/L
NE
10
1.1
1
8260D
10/21/20 16:53JLB
POJ0321
Toluene
<0.044
ug/L
1
0.50
0.044
1
8260D
10/21/20 16:53JLB
POJ0321
trans- 1,2-Dichloroethylene
<0.094
ug/L
5
0.50
0.094
1
8260D
10/21/20 16:53JLB
POJ0321
trans- 1,3-Dichloropropylene
<0.070
ug/L
1
0.50
0.070
1
8260D
10/21/20 16:53JLB
POJ0321
trans- 1,4-Dichloro-2-butene
<0.12
ug/L
100
10
0.12
1
8260D
10/21/20 16:53JLB
POJ0321
Trichloroethylene
<0.078
ug/L
1
0.50
0.078
1
8260D
10/21/20 16:53JLB
POJ0321
Trichlorofluoromethane
<0.062
ug/L
1
0.50
0.062
1
8260D
10/21/20 16:53JLB
POJ0321
Vinyl acetate
<0.060
ug/L
50
2.0
0.060
1
8260D
10/21/20 16:53JLB
POJ0321
Vinyl chloride
<0.097
ug/L
1
0.50
0.097
1
8260D
10/21/20 16:53JLB
POJ0321
Xylenes, total
<0.15
ug/L
5
1.5
0.15
1
8260D
10/21/20 16:53JLB
POJ0321
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
102 % 80-124
Dibromofluoromethane
112 % 75-129
Toluene-d8
100 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 96
(2)
Way po Int
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
1211120
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
Blank (POJ0321-BLK1)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,1-Dichloropropylene
BRL
0.50
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
0.290
1.0
ug/L J
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,3-Dichlorobenzene
BRL
0.50
ug/L
1,3-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
Acetone
BRL
5.0
ug/L
Acetonitrile
BRL
10
ug/L
Acrolein
BRL
20
ug/L
Acrylonitrile
BRL
20
ug/L
Allyl Chloride (3-Chloropropylene)
BRL
10
ug/L
Benzene
BRL
0.50
ug/L
Bromochloromethane
BRL
0.50
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
0.50
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
Chloroprene
BRL
10
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
0.50
ug/L
Dichlorodifluoromethane
BRL
5.0
ug/L
Ethyl Methacrylate
BRL
10
ug/L
Ethylbenzene
BRL
0.50
ug/L
Hexachlorobutadiene
0.220
2.0
ug/L J
Isobutyl alcohol
BRL
50
ug/L
m,p-Xylenes
0.250
1.0
ug/L J
Methacrylonitrile
BRL
10
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 34 of 96
Waypoint '
ANALYTICAL
Level II QC Report
12/1 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
Blank (POJ0321-BLK1)
Prepared & Analyzed: 10/21/20
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methyl Methacrylate
BRL
10
ug/L
Methylene Chloride
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
o-Xylene
BRL
0.50
ug/L
Propionitrile (Ethyl Cyanide)
BRL
10
ug/L
Styrene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrahydrofuran
BRL
10
ug/L
Toluene
BRL
0.50
ug/L
trans- 1,2-Dichloroethylene
BRL
0.50
ug/L
trans- 1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
Trichloroethylene
BRL
0.50
ug/L
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
0.250
1.5
ug/L
J
Surrogate:4-Bromofluorobenzene
50.3
ug/L
50.00
101
80-124
Surrogate: Dibromofluoromethane
53.8
ug/L
50.00
108
75-129
Surrogate: Toluene-d8
49.6
ug/L
50.00
99
77-123
LCS (POJ0321-BS1)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
21.5
0.50
ug/L
20.00
108
79-134
1,1,1-Trichloroethane
21.3
0.50
ug/L
20.00
106
75-136
1,1,2,2-Tetrachloroethane
21.0
0.50
ug/L
20.00
105
62-127
1,1,2-Trichloroethane
21.6
0.50
ug/L
20.00
108
70-140
1,1-Dichloroethane
21.6
0.50
ug/L
20.00
108
78-130
1,1-Dichloroethylene
21.2
0.50
ug/L
20.00
106
70-154
1, 1 -Dichloropropylene
22.0
0.50
ug/L
20.00
110
71-136
1,2,3-Trichloropropane
21.2
1.0
ug/L
20.00
106
71-127
1,2,4-Trichlorobenzene
20.4
1.0
ug/L
20.00
102
66-139
1,2-Dibromo-3-chloropropane
22.9
2.0
ug/L
20.00
114
63-134
1,2-Dibromoethane
21.3
0.50
ug/L
20.00
107
77-135
1,2-Dichlorobenzene
21.3
0.50
ug/L
20.00
106
78-128
1,2-Dichloroethane
21.6
0.50
ug/L
20.00
108
68-131
1,2-Dichloropropane
21.9
0.50
ug/L
20.00
110
77-130
1,3-Dichlorobenzene
21.5
0.50
ug/L
20.00
107
77-125
1,3-Dichloropropane
22.0
0.50
ug/L
20.00
110
76-132
1,4-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
75-126
2,2-Dichloropropane
23.8
2.0
ug/L
20.00
119
29-149
Acetone
39.6
5.0
ug/L
40.00
99
40-166
Acetonitrile
19.4
10
ug/L
20.00
97
70-130
Acrolein
45.9
20
ug/L
40.00
115
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 of 96
Waypoint '
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS (POJ0321-BSI)
Prepared &Analyzed: 10/21/20
Acrylonitrile
42.3
20
ug/L
40.00
106
81-127
Allyl Chloride (3-Chloropropylene)
19.4
10
ug/L
20.00
97
70-130
Benzene
22.7
0.50
ug/L
20.00
114
77-128
Bromochloromethane
22.1
0.50
ug/L
20.00
110
78-135
Bromodichloromethane
21.7
0.50
ug/L
20.00
108
76-138
Bromoform
22.4
1.0
ug/L
20.00
112
71-135
Bromomethane
21.0
1.0
ug/L
20.00
105
41-168
Carbon disulfide
21.1
5.0
ug/L
20.00
106
59-135
Carbon Tetrachloride
21.7
0.50
ug/L
20.00
109
72-142
Chlorobenzene
22.0
0.50
ug/L
20.00
110
78-119
Chloroethane
21.5
0.50
ug/L
20.00
107
57-142
Chloroform
21.0
0.50
ug/L
20.00
105
77-130
Chloromethane
20.5
0.50
ug/L
20.00
102
47-145
Chloroprene
19.7
10
ug/L
20.00
98
70-130
cis-1,2-Dichloroethylene
22.5
0.50
ug/L
20.00
113
76-141
cis-1,3-Dichloropropylene
22.4
0.50
ug/L
20.00
112
65-140
Dibromochloromethane
21.2
0.50
ug/L
20.00
106
75-134
Dibromomethane
21.8
0.50
ug/L
20.00
109
76-138
Dichlorodifluoromethane
25.2
5.0
ug/L
20.00
126
28-163
Ethyl Methacrylate
19.7
10
ug/L
20.00
99
70-130
Ethylbenzene
22.7
0.50
ug/L
20.00
114
80-127
Hexachlorobutadiene
20.1
2.0
ug/L
20.00
100
61-134
Isobutyl alcohol
24.0
50
ug/L
20.00
120
70-130 J
m,p-Xylenes
48.4
1.0
ug/L
40.00
121
77-133
Methacrylonitrile
19.5
10
ug/L
20.00
98
70-130
Methyl Butyl Ketone (2-Hexanone)
22.7
5.0
ug/L
20.00
114
64-137
Methyl Ethyl Ketone (2-Butanone)
20.2
5.0
ug/L
20.00
101
71-134
Methyl Iodide
23.5
5.0
ug/L
20.00
118
70-130
Methyl Isobutyl Ketone
23.8
5.0
ug/L
20.00
119
69-134
Methyl Methacrylate
20.3
10
ug/L
20.00
102
70-130
Methylene Chloride
20.7
1.0
ug/L
20.00
103
73-131
Naphthalene
21.0
1.0
ug/L
20.00
105
64-136
o-Xylene
22.8
0.50
ug/L
20.00
114
78-128
Propionitrile (Ethyl Cyanide)
22.1
10
ug/L
20.00
110
70-130
Styrene
23.3
0.50
ug/L
20.00
116
78-129
Tetrachloroethylene
21.2
0.50
ug/L
20.00
106
80-129
Tetrahydrofuran
22.3
10
ug/L
20.00
112
70-130
Toluene
22.5
0.50
ug/L
20.00
113
76-131
trans- 1,2-Dichloroethylene
21.6
0.50
ug/L
20.00
108
76-135
trans- 1,3-Dichloropropylene
23.1
0.50
ug/L
20.00
116
67-140
trans-1,4-Dichloro-2-butene
21.1
10
ug/L
20.00
105
70-130
Trichloroethylene
21.3
0.50
ug/L
20.00
107
77-133
Trichlorofluoromethane
22.6
0.50
ug/L
20.00
113
62-148
Vinyl acetate
26.3
2.0
ug/L
20.00
131
34-167
Vinyl chloride
22.4
0.50
ug/L
20.00
112
57-141
Xylenes, total
71.2
1.5
ug/L
60.00
119
77-133
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 36 of 96
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/1 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS (POJ0321-BSI)
Prepared &Analyzed: 10/21/20
Surrogate:4-Bromofluorobenzene
48.4
ug/L
50.00
97
80-124
Surrogate: Dibromofluoromethane
49.3
ug/L
50.00
99
75-129
Surrogate: Toluene-d8
50.0
ug/L
50.00
100
77-123
LCS Dup (POJ0321-BSD1)
Prepared &Analyzed: 10/21/20
1,1,1,2-Tetrachloroethane
21.4
0.50
ug/L
20.00
107
79-134
0.6
20
1,1,1-Trichloroethane
20.5
0.50
ug/L
20.00
102
75-136
4
20
1,1,2,2-Tetrachloroethane
20.7
0.50
ug/L
20.00
103
62-127
2
20
1,1,2-Trichloroethane
21.4
0.50
ug/L
20.00
107
70-140
1
20
1,1-Dichloroethane
20.4
0.50
ug/L
20.00
102
78-130
5
20
1,1-Dichloroethylene
20.2
0.50
ug/L
20.00
101
70-154
5
20
1,1-Dichloropropylene
21.0
0.50
ug/L
20.00
105
71-136
5
20
1,2,3-Trichloropropane
21.1
1.0
ug/L
20.00
106
71-127
0.6
20
1,2,4-Trichlorobenzene
20.7
1.0
ug/L
20.00
103
66-139
1
20
1,2-Dibromo-3-chloropropane
21.7
2.0
ug/L
20.00
108
63-134
5
20
1,2-Dibromoethane
20.9
0.50
ug/L
20.00
104
77-135
2
20
1,2-Dichlorobenzene
20.5
0.50
ug/L
20.00
103
78-128
4
20
1,2-Dichloroethane
21.1
0.50
ug/L
20.00
106
68-131
2
20
1,2-Dichloropropane
21.3
0.50
ug/L
20.00
107
77-130
3
20
1,3-Dichlorobenzene
21.1
0.50
ug/L
20.00
105
77-125
2
20
1,3-Dichloropropane
21.3
0.50
ug/L
20.00
106
76-132
3
20
1,4-Dichlorobenzene
20.4
0.50
ug/L
20.00
102
75-126
2
20
2,2-Dichloropropane
21.4
2.0
ug/L
20.00
107
29-149
11
20
Acetone
39.2
5.0
ug/L
40.00
98
40-166
1
20
Acetonitrile
21.5
10
ug/L
20.00
107
70-130
10
20
Acrolein
46.1
20
ug/L
40.00
115
70-130
0.5
20
Acrylonitrile
42.2
20
ug/L
40.00
105
81-127
0.4
20
Allyl Chloride (3-Chloropropylene)
18.8
10
ug/L
20.00
94
70-130
3
20
Benzene
21.8
0.50
ug/L
20.00
109
77-128
4
20
Bromochloromethane
20.5
0.50
ug/L
20.00
103
78-135
7
20
Bromodichloromethane
20.8
0.50
ug/L
20.00
104
76-138
4
20
Bromoform
21.5
1.0
ug/L
20.00
107
71-135
4
20
Bromomethane
19.7
1.0
ug/L
20.00
99
41-168
6
20
Carbon disulfide
20.5
5.0
ug/L
20.00
102
59-135
3
20
Carbon Tetrachloride
20.9
0.50
ug/L
20.00
105
72-142
4
20
Chlorobenzene
21.2
0.50
ug/L
20.00
106
78-119
4
20
Chloroethane
20.2
0.50
ug/L
20.00
101
57-142
6
20
Chloroform
20.6
0.50
ug/L
20.00
103
77-130
2
20
Chloromethane
20.0
0.50
ug/L
20.00
100
47-145
2
20
Chloroprene
18.8
10
ug/L
20.00
94
70-130
5
20
cis-1,2-Dichloroethylene
20.4
0.50
ug/L
20.00
102
76-141
10
20
cis-1,3-Dichloropropylene
21.9
0.50
ug/L
20.00
110
65-140
2
20
Dibromochloromethane
21.2
0.50
ug/L
20.00
106
75-134
0.1
20
Dibromomethane
21.3
0.50
ug/L
20.00
107
76-138
2
20
Dichlorodifluoromethane
24.2
5.0
ug/L
20.00
121
28-163
4
20
Ethyl Methacrylate
19.4
10
ug/L
20.00
97
70-130
1
20
Ethylbenzene
22.0
0.50
ug/L
20.00
110
80-127
3
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 of 96
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/1 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0321 - 5030B
LCS Dup (POJ0321-BSD1)
Prepared &Analyzed: 10/21/20
Hexachlorobutadiene
19.9
2.0
ug/L
20.00
99
61-134
1
20
Isobutyl alcohol
21.3
50
ug/L
20.00
106
70-130
12
20 1
m,p-Xylenes
47.1
1.0
ug/L
40.00
118
77-133
3
20
Methacrylonitrile
19.2
10
ug/L
20.00
96
70-130
2
20
Methyl Butyl Ketone (2-Hexanone)
22.7
5.0
ug/L
20.00
113
64-137
0.3
20
Methyl Ethyl Ketone (2-Butanone)
19.7
5.0
ug/L
20.00
98
71-134
3
20
Methyl Iodide
22.6
5.0
ug/L
20.00
113
70-130
4
20
Methyl Isobutyl Ketone
22.7
5.0
ug/L
20.00
113
69-134
5
20
Methyl Methacrylate
19.7
10
ug/L
20.00
99
70-130
3
20
Methylene Chloride
19.8
1.0
ug/L
20.00
99
73-131
5
20
Naphthalene
21.4
1.0
ug/L
20.00
107
64-136
2
20
o-Xylene
22.3
0.50
ug/L
20.00
112
78-128
2
20
Propionitrile (Ethyl Cyanide)
19.9
10
ug/L
20.00
100
70-130
10
20
Styrene
22.7
0.50
ug/L
20.00
113
78-129
3
20
Tetrachloroethylene
20.4
0.50
ug/L
20.00
102
80-129
4
20
Tetrahydrofuran
22.0
10
ug/L
20.00
110
70-130
2
20
Toluene
21.6
0.50
ug/L
20.00
108
76-131
4
20
trans-1,2-Dichloroethylene
20.6
0.50
ug/L
20.00
103
76-135
5
20
trans-1,3-Dichloropropylene
22.2
0.50
ug/L
20.00
ill
67-140
4
20
trans-1,4-Dichloro-2-butene
19.6
10
ug/L
20.00
98
70-130
7
20
Trichloroethylene
21.2
0.50
ug/L
20.00
106
77-133
0.7
20
Trichlorofluoromethane
21.4
0.50
ug/L
20.00
107
62-148
6
20
Vinyl acetate
25.7
2.0
ug/L
20.00
129
34-167
2
20
Vinyl chloride
21.2
0.50
ug/L
20.00
106
57-141
5
20
Xylenes, total
69.4
1.5
ug/L
60.00
116
77-133
2
20
Surrogate:4-Bromofluorobenzene
48.3
ug/L
50.00
97
80-124
Surrogate: Dibromofluoromethane
49.5
ug/L
50.00
99
75-129
Surrogate: Toluene-d8
50.3
ug/L
50.00
101
77-123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Asheville, NC 28801
Volatile Organic Compounds by GC/MS SIM - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0316 - 5030B
Blank (POJ0316-BLK1) Prepared & Analyzed: 10/16/20
1,4-Dioxane BRL 2.0 ug/L
LCS (POJ0316-BS1) Prepared &Analyzed: 10/16/20
1,4-Dioxane 47.5 2.0 ug/L 50.00 95 55-145
LCS Dup (POJ0316-BSD1) Prepared &Analyzed: 10/16/20
1,4-Dioxane 47.1 2.0 ug/L 50.00 94 55-145 0.7 30
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 39 of 96
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/1 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
Blank (POJ0286-BLK1)
Prepared: 10/16/20 Analyzed: 10/19/20
4,4'-DDD
BRL
0.10
ug/L
4,4'-DDE
BRL
0.10
ug/L
4,4'-DDT
BRL
0.10
ug/L
Aldrin
BRL
0.050
ug/L
alpha-BHC
BRL
0.050
ug/L
cis -Chlordane
BRL
0.10
ug/L
beta-BHC
BRL
0.050
ug/L
Chlordane
BRL
0.50
ug/L
delta-BHC
BRL
0.050
ug/L
Dieldrin
BRL
0.050
ug/L
Endosulfan I
BRL
0.050
ug/L
Endosulfan II
BRL
0.050
ug/L
Endosulfan Sulfate
BRL
0.050
ug/L
Endrin
BRL
0.050
ug/L
Endrin Aldehyde
BRL
0.050
ug/L
Endrin Ketone
BRL
0.10
ug/L
gamma-BHC
BRL
0.050
ug/L
trans -Chlordane
BRL
0.10
ug/L
Heptachlor
BRL
0.050
ug/L
Heptachlor Epoxide
BRL
0.10
ug/L
Methoxychlor
BRL
0.10
ug/L
Toxaphene
BRL
1.0
ug/L
Surrogate: Decachlorobiphenyl
0.560
ug/L
1.000
56
13-186
Surrogate: Tetrachloro-m-xylene
0.630
ug/L
1.000
63
40-134
LCS (POJ0286-BS1)
Prepared: 10/16/20 Analyzed: 10/19/20
4,4'-DDD
0.690
0.10
ug/L
1.000
69
56-143
4,4'-DDE
0.700
0.10
ug/L
1.000
70
57-135
4,4'-DDT
0.740
0.10
ug/L
1.000
74
51-143
Aldrin
0.640
0.050
ug/L
1.000
64
45-134
alpha-BHC
0.680
0.050
ug/L
1.000
68
54-138
cis -Chlordane
0.680
0.10
ug/L
1.000
68
60-129
beta-BHC
0.640
0.050
ug/L
1.000
64
56-136
delta-BHC
0.680
0.050
ug/L
1.000
68
52-142
Dieldrin
0.710
0.050
ug/L
1.000
71
60-136
Endosulfan 1
0.690
0.050
ug/L
1.000
69
62-126
Endosulfan II
0.710
0.050
ug/L
1.000
71
52-135
Endosulfan Sulfate
0.670
0.050
ug/L
1.000
67
62-133
Endrin
0.790
0.050
ug/L
1.000
79
60-138
Endrin Aldehyde
0.630
0.050
ug/L
1.000
63
51-132
Endrin Ketone
0.670
0.10
ug/L
1.000
67
58-134
gamma-BHC
0.670
0.050
ug/L
1.000
67
59-134
trans -Chlordane
0.670
0.10
ug/L
1.000
67
56-136
Heptachlor
0.670
0.050
ug/L
1.000
67
54-130
Heptachlor Epoxide
0.690
0.10
ug/L
1.000
69
61-133
Methoxychlor
0.710
0.10
ug/L
1.000
71
54-145
Surrogate: Decachlorobiphenyl
0.500
ug/L
1.000
50
13-186
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 96
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/1 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
LCS (POJ0286-BS1)
Prepared: 10/16/20 Analyzed: 10/19/20
Surrogate: Tetrachloro-m-xylene
0.730
ug/L
1.000
73
40-134
LCS (POJ0286-BS2)
Prepared: 10/16/20 Analyzed: 10/19/20
Chlordane
7.87
0.50
ug/L
10.00
79
62-140
Surrogate: Decachlorobiphenyl
0.580
ug/L
1.000
58
13-186
Surrogate: Tetrachloro-m-xylene
0.630
ug/L
1.000
63
40-134
LCS (POJ0286-BS3)
Prepared: 10/16/20 Analyzed: 10/19/20
Toxaphene
9.00
1.0
ug/L
10.00
90
33-134
Surrogate: Decachlorobiphenyl
0.510
ug/L
1.000
51
13-186
Surrogate: Tetrachloro-m-xylene
0.690
ug/L
1.000
69
40-134
LCS Dup (POJ0286-BSD1)
Prepared: 10/16/20 Analyzed: 10/19/20
4,4'-DDD
0.660
0.10
ug/L
1.000
66
56-143
4
30
4,4'-DDE
0.670
0.10
ug/L
1.000
67
57-135
4
30
4,4'-DDT
0.710
0.10
ug/L
1.000
71
51-143
4
30
Aldrin
0.610
0.050
ug/L
1.000
61
45-134
5
30
alpha-BHC
0.660
0.050
ug/L
1.000
66
54-138
3
30
cis -Chlordane
0.650
0.10
ug/L
1.000
65
60-129
5
30
beta-BHC
0.570
0.050
ug/L
1.000
57
56-136
12
30
delta-BHC
0.620
0.050
ug/L
1.000
62
52-142
9
30
Dieldrin
0.680
0.050
ug/L
1.000
68
60-136
4
30
Endosulfan 1
0.670
0.050
ug/L
1.000
67
62-126
3
30
Endosulfan 11
0.690
0.050
ug/L
1.000
69
52-135
3
30
Endosulfan Sulfate
0.630
0.050
ug/L
1.000
63
62-133
6
30
Endrin
0.750
0.050
ug/L
1.000
75
60-138
5
30
Endrin Aldehyde
0.600
0.050
ug/L
1.000
60
51-132
5
30
Endrin Ketone
0.650
0.10
ug/L
1.000
65
58-134
3
30
gamma-BHC
0.640
0.050
ug/L
1.000
64
59-134
5
30
trans -Chlordane
0.640
0.10
ug/L
1.000
64
56-136
5
30
Heptachlor
0.640
0.050
ug/L
1.000
64
54-130
5
30
Heptachlor Epoxide
0.670
0.10
ug/L
1.000
67
61-133
3
30
Methoxychlor
0.680
0.10
ug/L
1.000
68
54-145
4
30
Surrogate: Decachlorobiphenyl
0.560
ug/L
1.000
56
13-186
Surrogate: Tetrachloro-m-xylene
0.680
ug/L
1.000
68
40-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 41 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0286 - 3510C GC
Blank (POJ0286-BLK1)
Prepared: 10/16/20 Analyzed: 10/19/20
Aroclor 1016
BRL
0.50
ug/L
Aroclor 1221
BRL
1.0
ug/L
Aroclor 1232
BRL
0.50
ug/L
Aroclor 1242
BRL
0.50
ug/L
Aroclor 1248
BRL
0.50
ug/L
Aroclor 1254
BRL
0.50
ug/L
Aroclor 1260
BRL
1.0
ug/L
Surrogate: Tetrachloro-m-xylene
0.610
ug/L
1.000
61
30-161
Surrogate: Decachlorobiphenyl
0.580
ug/L
1.000
58
32-178
LCS (POJ0286-BS4)
Prepared: 10/16/20 Analyzed: 10/19/20
Aroclor 1016
6.63
0.50
ug/L
10.00
66
50-114
Aroclor 1221
BRL
1.0
ug/L
15-178
Aroclor 1232
BRL
0.50
ug/L
10-215
Aroclor 1242
BRL
0.50
ug/L
39-150
Aroclor 1248
BRL
0.50
ug/L
38-158
Aroclor 1254
BRL
0.50
ug/L
29-131
Aroclor 1260
7.65
1.0
ug/L
10.00
76
10-127
Surrogate: Tetrachloro-m-xylene
0.620
ug/L
1.000
62
30-161
Surrogate: Decachlorobiphenyl
0.690
ug/L
1.000
69
32-178
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 42 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0312 - 3005A
Blank (POJ0312-BLK1)
Prepared: 10/16/20 Analyzed: 10/24/20
Antimony
BRL
2.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
2.0
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
0.697
3.0
ug/L
J
Selenium
BRL
5.0
ug/L
Thallium
BRL
2.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
LCS (POJ0312-BS1)
Prepared: 10/16/20 Analyzed: 10/24/20
Antimony
113
2.0
ug/L
100.0 113 80-120
Arsenic
97.2
1.0
ug/L
100.0 97 80-120
Barium
93.2
2.0
ug/L
100.0 93 80-120
Beryllium
104
1.0
ug/L
100.0 104 80-120
Cadmium
101
1.0
ug/L
100.0 101 80-120
Cobalt
99.6
2.0
ug/L
100.0 100 80-120
Copper
98.6
10
ug/L
100.0 99 80-120
Lead
101
1.0
ug/L
100.0 101 80-120
Nickel
99.0
3.0
ug/L
100.0 99 80-120
Selenium
94.9
5.0
ug/L
100.0 95 80-120
Thallium
98.7
2.0
ug/L
100.0 99 80-120
Vanadium
99.9
5.0
ug/L
100.0 100 80-120
Zinc
95.2
20
ug/L
100.0 95 80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 43 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0374 - 7470A
Blank (POJ0374-BLK1) Prepared & Analyzed: 10/20/20
Mercury BRL 0.20 ug/L
LCS (POJ0374-BS1) Prepared &Analyzed: 10/20/20
Mercury 8.17 0.20 ug/L 9.375 87 80-120
Batch POJ0491 - 3005A
Blank (POJ0491-BLK1) Prepared & Analyzed: 10/27/20
Chromium BRL 2.0 ug/L
Silver BRL 1.0 ug/L
Tin BRL 5.0 ug/L
LCS (POJ0491-BS1)
Prepared &Analyzed: 10/27/20
Chromium
93.0 2.0 ug/L
100.0 93 80-120
Silver
97.8 1.0 ug/L
100.0 98 80-120
Tin
99.3 5.0 ug/L
100.0 99 80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 44 of 96
Level II QC Report
0int 12/1/20
Waypo
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Dissolved Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0394 - 7470A
Blank (POJ0394-BLK1)
Prepared &Analyzed: 10/21/20
Mercury
BRL 0.20 ug/L
LCS (POJ0394-BS1)
Prepared &Analyzed: 10/21/20
Mercury
8.50 0.20 ug/L
9.375 91 80-120
Matrix Spike (POJ0394-MS1)
Source: 0100203-03
Prepared & Analyzed: 10/21/20
Mercury
8.52 0.20 ug/L
9.375 BRL 91 80-120
Matrix Spike Dup (POJ0394-MSD1)
Source: 0100203-03
Prepared &Analyzed: 10/21/20
Mercury
8.50 0.20 ug/L
9.375 BRL 91 80-120 0.3 20
Post Spike (POJ0394-PS1)
Source: 0100203-03
Prepared &Analyzed: 10/21/20
Mercury
4.47 ug/L
5.000-0.000620 89 85-115
Batch POJ0496 - 3005A
Blank (POJ0496-BLK1)
Prepared: 10/27/20 Analyzed: 10/28/20
Antimony
BRL
2.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
10
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
2.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
BRL
3.0
ug/L
Selenium
BRL
5.0
ug/L
Silver
BRL
1.0
ug/L
Thallium
BRL
2.0
ug/L
Tin
BRL
5.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 45 of 96
Level II QC Report
0int 12/1/20
Waypo
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Dissolved Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0496 - 3005A
LCS (POJ0496-BS1)
Prepared: 10/27/20 Analyzed: 10/28/20
Antimony
88.3
2.0
ug/L
100.0
88
80-120
Arsenic
92.1
1.0
ug/L
100.0
92
80-120
Barium
97.5
10
ug/L
100.0
98
80-120
Beryllium
90.5
1.0
ug/L
100.0
91
80-120
Cadmium
97.2
1.0
ug/L
100.0
97
80-120
Chromium
93.1
2.0
ug/L
100.0
93
80-120
Cobalt
93.6
2.0
ug/L
100.0
94
80-120
Copper
90.8
10
ug/L
100.0
91
80-120
Lead
93.6
1.0
ug/L
100.0
94
80-120
Nickel
92.1
3.0
ug/L
100.0
92
80-120
Selenium
96.4
5.0
ug/L
100.0
96
80-120
Silver
94.0
1.0
ug/L
100.0
94
80-120
Thallium
93.5
2.0
ug/L
100.0
93
80-120
Tin
94.9
5.0
ug/L
100.0
95
80-120
Vanadium
93.5
5.0
ug/L
100.0
94
80-120
Zinc
95.4
20
ug/L
100.0
95
80-120
Matrix Spike (POJ0496-MS1)
Source: 0100203-03
Prepared:
10/27/20
Analyzed: 10/28/20
Antimony
88.2
2.0
ug/L
100.0
BRL
88
75-125
Arsenic
92.9
1.0
ug/L
100.0
BRL
93
75-125
Barium
110
10
ug/L
100.0
11.6
98
75-125
Beryllium
98.7
1.0
ug/L
100.0
BRL
99
75-125
Cadmium
96.3
1.0
ug/L
100.0
BRL
96
75-125
Chromium
94.3
2.0
ug/L
100.0
BRL
94
75-125
Cobalt
95.1
2.0
ug/L
100.0
BRL
95
75-125
Copper
92.5
10
ug/L
100.0
BRL
93
75-125
Lead
96.3
1.0
ug/L
100.0
BRL
96
75-125
Nickel
93.1
3.0
ug/L
100.0
BRL
93
75-125
Selenium
98.9
5.0
ug/L
100.0
BRL
99
75-125
Silver
94.4
1.0
ug/L
100.0
BRL
94
75-125
Thallium
94.7
2.0
ug/L
100.0
BRL
95
75-125
Tin
94.4
5.0
ug/L
100.0
BRL
94
75-125
Vanadium
94.3
5.0
ug/L
100.0
BRL
94
75-125
Zinc
98.5
20
ug/L
100.0
BRL
99
75-125
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 46 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Dissolved Metals - Quality Control
Analyte
Batch POJ0496 - 3005A
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (POJ0496-MSD1)
Source: 0100203-03
Prepared: 10/27/20 Analyzed: 10/28/20
Antimony
89.9
2.0
ug/L
100.0
BRL
90
75-125
2
20
Arsenic
90.8
1.0
ug/L
100.0
BRL
91
75-125
2
20
Barium
109
10
ug/L
100.0
11.6
97
75-125
1
20
Beryllium
97.2
1.0
ug/L
100.0
BRL
97
75-125
2
20
Cadmium
98.0
1.0
ug/L
100.0
BRL
98
75-125
2
20
Chromium
92.8
2.0
ug/L
100.0
BRL
93
75-125
2
20
Cobalt
94.4
2.0
ug/L
100.0
BRL
94
75-125
0.7
20
Copper
91.9
10
ug/L
100.0
BRL
92
75-125
0.6
20
Lead
94.8
1.0
ug/L
100.0
BRL
95
75-125
1
20
Nickel
92.2
3.0
ug/L
100.0
BRL
92
75-125
0.9
20
Selenium
97.2
5.0
ug/L
100.0
BRL
97
75-125
2
20
Silver
93.6
1.0
ug/L
100.0
BRL
94
75-125
0.9
20
Thallium
94.2
2.0
ug/L
100.0
BRL
94
75-125
0.5
20
Tin
96.2
5.0
ug/L
100.0
BRL
96
75-125
2
20
Vanadium
93.1
5.0
ug/L
100.0
BRL
93
75-125
1
20
Zinc
98.5
20
ug/L
100.0
BRL
99
75-125
0.009
20
Post Spike (POJ0496-PS1)
Source: 0100203-03
Prepared:
10/27/20 Analyzed: 10/28/20
Antimony
92.0
ug/L
100.0
0.394
92
80-120
Arsenic
93.3
ug/L
100.0
0.114
93
80-120
Barium
115
ug/L
100.0
11.6
103
80-120
Beryllium
95.2
ug/L
100.0
0.101
95
80-120
Cadmium
100
ug/L
100.0
0.00500
100
80-120
Chromium
95.6
ug/L
100.0
0.00100
96
80-120
Cobalt
96.2
ug/L
100.0
0.0220
96
80-120
Copper
93.8
ug/L
100.0
0.268
94
80-120
Lead
97.5
ug/L
100.0
0.0680
97
80-120
Nickel
95.5
ug/L
100.0
0.180
95
80-120
Selenium
101
ug/L
100.0
0.247
101
80-120
Silver
96.6
ug/L
100.0
0.0100
97
80-120
Thallium
96.6
ug/L
100.0
0.0350
97
80-120
Tin
98.5
ug/L
100.0
0.153
98
80-120
Vanadium
94.1
ug/L
100.0
0.0710
94
80-120
Zinc
103
ug/L
100.0
3.18
100
80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 47 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Anions by Ion Chromatography - Quality Control
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0299 - NO PREP
Blank (POJ0299-BLK1)
Prepared & Analyzed: 10/15/20
Chloride
BRL
1000
ug/L
Nitrate as N
BRL
200
ug/L
Sulfate
BRL
2000
ug/L
LCS (POJ0299-BS1)
Prepared &Analyzed: 10/15/20
Chloride
41100
1000
ug/L
40000 103
80-120
Nitrate as N
4000
210
ug/L
4000 100
80-120
Sulfate
41500
2100
ug/L
40000 104
80-120
Matrix Spike (POJ0299-MS1)
Source: 0100203-01
Prepared & Analyzed: 10/15/20
Chloride
42300
1000
ug/L
40000 1170 103
80-120
Nitrate as N
4000
210
ug/L
4000 BRL 100
80-120
Sulfate
42200
2100
ug/L
40000 BRL 105
80-120
Matrix Spike Dup (POJ0299-MSD1)
Source: 0100203-01
Prepared & Analyzed: 10/15/20
Chloride
42100
1000
ug/L
40000 1170 102
80-120 0.5 15
Nitrate as N
3980
210
ug/L
4000 BRL 99
80-120 0.6 15
Sulfate
41900
2100
ug/L
40000 BRL 105
80-120 0.6 15
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 48 of 96
Level II QC Report
0int 12/1/20
Waypo
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0269 - NO PREP
Blank (POJ0269-BLK1) Prepared & Analyzed: 10/15/20
Hardness BRL 5000 ug/L
LCS (POJ0269-BS1) Prepared &Analyzed: 10/15/20
Hardness 50000 5000 ug/L 50000 100 90-110
Matrix Spike (POJ0269-MS1) Source: 0100203-04 Prepared & Analyzed: 10/15/20
Hardness 15500 5000 ug/L 10000 5500 100 80-120
Matrix Spike Dup (POJ0269-MSD1) Source: 0100203-04 Prepared & Analyzed: 10/15/20
Hardness 15000 5000 ug/L 10000 5500 95 80-120 3 20
Batch POJ0282 - NO PREP
Blank (POJ0282-BLK1) Prepared & Analyzed: 10/15/20
Ferrous Iron BRL 200 ug/L
LCS (POJ0282-BS1) Prepared &Analyzed: 10/15/20
Ferrous Iron 1930 200 ug/L 2000 96 90-110
Batch POJ0337 - SM4500-S C
Blank (POJ0337-BLK1) Prepared & Analyzed: 10/19/20
Sulfide BRL 2000 ug/L
LCS (POJ0337-BS1) Prepared &Analyzed: 10/19/20
Sulfide 7900 2000 ug/L 10000 79 70-122
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 49 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0340 - NO PREP
Blank (POJ0340-BLK1) Prepared & Analyzed: 10/15/20
Biochemical Oxygen Demand BRL 2000 ug/L
LCS (POJ0340-BS1) Prepared &Analyzed: 10/15/20
Biochemical Oxygen Demand 194000 2000 ug/L 198000 98 84.6-115.4
Batch POJ0341 - NO PREP
Blank (POJ0341-BLK1) Prepared & Analyzed: 10/19/20
Total Alkalinity to pH 4.5 BRL 5000 ug/L
LCS (POJ0341-BSI) Prepared &Analyzed: 10/19/20
Total Alkalinity to pH 4.5 249000 5000 ug/L 90-110
Batch POJ0357 - 9010C
Blank (POJ0357-BLK1) Prepared & Analyzed: 10/20/20
Cyanide BRL 25 ug/L
LCS (POJ0357-BS1) Prepared &Analyzed: 10/20/20
Cyanide 96.5 25 ug/L 100.0 96 85-115
Matrix Spike (POJ0357-MS1) Source: 0100203-01 Prepared & Analyzed: 10/20/20
Cyanide 95.0 25 ug/L 100.0 BRL 95 80-120
Matrix Spike Dup (POJ0357-MSD1) Source: 0100203-01 Prepared & Analyzed: 10/20/20
Cyanide 112 25 ug/L 100.0 BRL 112 80-120 16 20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 50 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POJ0361 - NO PREP
Blank (POJ0361-BLK1) Prepared & Analyzed: 10/19/20
Chemical Oxygen Demand BRL 50000 ug/L
LCS (POJ0361-BS1) Prepared &Analyzed: 10/19/20
Chemical Oxygen Demand 498000 50000 ug/L 90-110
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 51 of 96
0int-
Level II QC Report
Waypo
12/1/20
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill
2020 Fall
Work Order: 0100203
Attn: Alec Macbeth
Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street
Project No: 50-02
Asheville, NC 28801
8270 Extended List - Quality Control
Reporting
Spike
Source
%REC
RPD
Analyte
Result
Limit
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Batch L517325 - 3510C
BSD (0100203 LCSD-L517325)
Source: 0100203 LCS-L517Prepared:
10/19/20
Analyzed:
10/21/20
2-Acetylaminofluorene
49.1
10.0
pg/L
50
53.1
98.2
20-120
7.8
20
N-Nitrosomethylethylamine
27.4
10.0
pg/L
50
26.2
54.8
20-120
4.4
20
4-Aminobiphenyl
38.8
10.0
pg/L
50
37
77.6
20-120
4.7
20
7,12-Dimethylbenz(a)anthracene
58.1
10.0
pg/L
50
48.7
116
20-120
17.6
20
N-Nitrosopiperidine
34.1
10.0
pg/L
50
33.6
68.2
20-120
1.4
20
3-Methylcholanthrene
57.1
10.0
pg/L
50
53
114
20-120
7.4
20
Isosafrole
43.9
10.0
pg/L
50
41.9
87.8
20-120
4.6
20
Diallate
48.4
10.0
pg/L
50
48.3
96.8
20-120
0.2
20
Methapyrilene
49.8
10.0
pg/L
50
35.1
99.6
20-120
34.6
20 LCD2
o-Toluidine
29.9
10.0
pg/L
50
29.4
59.8
20-120
1.6
20
5-Nitro-o-toluidine
48.6
10.0
pg/L
50
45.1
97.2
20-120
7.4
20
p-Dimethylaminoazobenzene
61.3
10.0
pg/L
50
51.1
123
20-120
18.1
20 LH
N-Nitrosopyrrolidine
34.3
10.0
pg/L
50
34.4
68.6
20-120
0.2
20
Kepone
60
10.0
pg/L
50
53.4
120
20-120
11.6
20
p-Phenylenediamine
0
10.0
pg/L
50
0
0
20-120
0
20 L
1-Naphthylamine
28.8
10.0
pg/L
50
28.9
57.6
20-120
0.3
20
Pronamide
56.1
10.0
pg/L
50
51
112
20-120
9.5
20
1,4-Naphthoquinone
44.6
10.0
pg/L
50
41.7
89.2
20-120
6.7
20
Hexachloropropene
22.6
10.0
pg/L
50
18.9
45.2
20-120
17.8
20
1,3,5-Trinitrobenzene
65.8
10.0
pg/L
50
60.4
132
20-120
8.5
20 LH
Safrole
39.9
10.0
pg/L
50
39.7
79.8
20-120
0.5
20
2-Naphthylamine
20.3
10.0
pg/L
50
22.7
40.6
20-120
11.1
20
BS (0100203 LCS-L517325)
Prepared:
10/19/20
Analyzed:
10/21/20
Kepone
53.4
10.0
pg/L
50
107
20-120
Isosafrole
41.9
10.0
pg/L
50
83.8
20-120
Methapyrilene
35.1
10.0
pg/L
50
70.2
20-120
N-Nitrosomethylethylamine
26.2
10.0
pg/L
50
52.4
20-120
N-Nitrosopiperidine
33.6
10.0
pg/L
50
67.2
20-120
o-Toluidine
29.4
10.0
pg/L
50
58.8
20-120
p-Dimethylaminoazobenzene
51.1
10.0
pg/L
50
102
20-120
p-Phenylenediamine
0
10.0
pg/L
50
0
20-120
L
Pronamide
51
10.0
pg/L
50
102
20-120
Safrole
39.7
10.0
pg/L
50
79.4
20-120
N-Nitrosopyrrolidine
34.4
10.0
pg/L
50
68.8
20-120
7,12-Dimethylbenz(a)anthracene
48.7
10.0
pg/L
50
97.4
20-120
3-Methylcholanthrene
53
10.0
pg/L
50
106
20-120
2-Acetylaminofluorene
53.1
10.0
pg/L
50
106
20-120
4-Aminobiphenyl
37
10.0
pg/L
50
74
20-120
5-Nitro-o-toluidine
45.1
10.0
pg/L
50
90.2
20-120
2-Naphthylamine
22.7
10.0
pg/L
50
45.4
20-120
Hexachloropropene
18.9
10.0
pg/L
50
37.8
20-120
1-Naphthylamine
28.9
10.0
pg/L
50
57.8
20-120
Diallate
48.3
10.0
pg/L
50
96.6
20-120
1,4-Naphthoquinone
41.7
10.0
pg/L
50
83.4
20-120
1,3,5-Trinitrobenzene
60.4
10.0
pg/L
50
121
20-120
LH
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 52 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
8270 Extended List - Quality Control
Analyte
Batch L517325 - 3510C
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
BLK (0100203 LRB-L517325)
Prepared: 10/19/20 Analyzed: 10/20/20
N-Nitrosomethylethylamine
BRL
10.0
pg/L -
1,4-Naphthoquinone
BRL
10.0
pg/L
Pronamide
BRL
10.0
pg/L
p-Dimethylaminoazobenzene
BRL
10.0
pg/L
2-Acetylaminofluorene
BRL
10.0
pg/L
2-Naphthylamine
BRL
10.0
pg/L
Safrole
BRL
10.0
pg/L
p-Phenylenediamine
BRL
10.0
pg/L
Diallate
BRL
10.0
pg/L
1-Naphthylamine
BRL
10.0
pg/L
o-Toluidine
BRL
10.0
pg/L
Isosafrole
BRL
10.0
pg/L
Kepone
BRL
10.0
pg/L
Methapyrilene
BRL
20.0
pg/L
7,12-Dimethylbenz(a)anthracene
BRL
10.0
pg/L
1,3,5-Trinitrobenzene
BRL
10.0
pg/L
5-Nitro-o-toluidine
BRL
10.0
pg/L
N-Nitrosopiperidine
BRL
10.0
pg/L
4-Aminobiphenyl
BRL
10.0
pg/L
N-Nitrosopyrrolidine
BRL
10.0
pg/L
3-Methylcholanthrene
BRL
10.0
pg/L
Hexachloropropene
BRL
10.0
pg/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 53 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Phenoxy Acid Herbicides - GC/ECD - Quality Control
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517923 - 8151A
BSD (0100203 LCSD-L517923)
Source: 0100203 LCS-L517Prepared: 10/21/20 Analyzed: 10/22/20
2,4-D
3.125
0.2078
pg/L
5
2.515
62.5
20-120
21.6
20
LCD2
Dicamba
0.3084
0.05700
pg/L
0.5
0.2569
61.6
20-120
18.2
20
Dalapon
3.799
0.5149
pg/L
12.5
2.931
30.3
20-120
25.7
20
LCD2
Dichlorprop
3.184
0.07959
pg/L
5
2.557
63.6
20-120
21.8
20
LCD2
Dinoseb
1.749
0.02698
pg/L
2.5
1.391
69.9
20-120
22.8
20
LCD2
2,4-DB
4.446
0.1364
pg/L
5
3.118
88.9
20-120
35.1
20
LCD2
MCPA
310.5
18.98
pg/L
500
247.3
62.1
20-120
22.6
20
LCD2
MCPP
366.9
11.75
pg/L
500
304.1
73.3
20-120
18.7
20
2,4,5-T
0.3553
0.01002
pg/L
0.5
0.2808
71
20-120
23.4
20
LCD2
Picloram
0.7292
0.04528
pg/L
1.25
0.5291
58.3
20-120
31.8
20
LCD2
2,4,5-TP (Silvex)
0.2916
0.01634
pg/L
0.5
0.2363
58.3
20-120
20.9
20
LCD2
Surrogate: DCAA
1.588
ug/L
2.5
1.276
63.5
20-150
BS (0100203 LCS-L517923)
Prepared:
10/21/20 Analyzed:
10/22/20
MCPA
247.3
18.98
pg/L
500
49.4
20-120
Dinoseb
1.391
0.02698
pg/L
2.5
55.6
20-120
MCPP
304.1
11.75
pg/L
500
60.8
20-120
Dichlorprop
2.557
0.07959
pg/L
5
51.1
20-120
Picloram
0.5291
0.04528
pg/L
1.25
42.3
20-120
Dicamba
0.2569
0.05700
pg/L
0.5
51.3
20-120
2,4,5-TP (Silvex)
0.2363
0.01634
pg/L
0.5
47.2
20-120
2,4,5-T
0.2808
0.01002
pg/L
0.5
56.1
20-120
2,4-D
2.515
0.2078
pg/L
5
50.3
20-120
2,4-DB
3.118
0.1364
pg/L
5
62.3
20-120
Dalapon
2.931
0.5149
pg/L
12.5
23.4
20-120
Surrogate: DCAA
1.276
ug/L
2.5
51
20-150
BLK (0100203 LRB-L517923)
Prepared:
10/21/20 Analyzed:
10/22/20
MCPP
BRL
50.00
pg/L
-
Picloram
BRL
0.1000
pg/L
2,4,5-TP (Silvex)
BRL
0.1000
pg/L
Dalapon
BRL
0.5500
pg/L
Dicamba
BRL
0.2500
pg/L
2,4,5-T
BRL
0.03000
pg/L
MCPA
BRL
50.00
pg/L
2,4-D
BRL
0.2500
pg/L
2,4-DB
BRL
0.1000
pg/L
Dichlorprop
BRL
0.1000
pg/L
Dinoseb
BRL
0.1000
pg/L
-
Surrogate: DCAA
1.455
ug/L
2.5
58.2
20-150
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 54 of 96
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/1 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BSD (0100203 LCSD-L517328)
Source: 0100203 LCS-L517Prepared & Analyzed: 10/19/20
2-Methylphenol
25
0.721
pg/L
50
22
50
22-97
12.7 20
Fluoranthene
39
0.406
pg/L
50
36
78
28-127
8 20
2-Nitroaniline
38.4
0.574
pg/L
50
35
76.8
32-127
9.2 20
Benzyl alcohol
23.8
3.01
pg/L
50
20.5
47.6
20-109
14.8 20
Bis(2-Chloroethoxy)methane
30.7
0.433
pg/L
50
27.3
61.4
20-126
11.7 20
Di-n-Octyl Phthalate
44.9
1.72
pg/L
50
36.4
89.8
29-136
20.9 20
2-Nitrophenol
32.4
0.606
pg/L
50
28.6
64.8
25-114
12.4 20
Fluorene
34.1
0.444
pg/L
50
31.4
68.2
41-116
8.2 20
Hexachloroethane
21.7
0.277
pg/L
50
19
43.4
16-107
13.2 20
Hexachlorobenzene
36.2
2.57
pg/L
50
33.6
72.4
18-136
7.4 20
2-Methyl naphthalene
32.1
0.485
pg/L
50
29.7
64.2
34-108
7.7 20
Acenaphthene
31.1
0.422
pg/L
50
27.4
62.2
38-117
12.6 20
Benzo(a)anthracene
35.3
0.427
pg/L
50
32.5
70.6
36-127
8.2 20
Anthracene
36.1
0.467
pg/L
50
33.8
72.2
34-128
6.5 20
Hexachlorocyclopentadiene
12.1
2.34
pg/L
50
13.9
24.2
10-102
13.8 20
3,3'-Dichlorobenzidine
112
3.74
pg/L
150
95.9
74.6
6-192
15.4 20
2-Chloronaphthalene
29.5
0.476
pg/L
50
26
59
29-137
12.6 20
Acenaphthylene
32.8
0.429
pg/L
50
29.7
65.6
37-114
9.9 20
2-Chlorophenol
28.4
0.736
pg/L
50
25
56.8
27-102
12.7 20
4-Nitroaniline
53.9
0.740
pg/L
50
52.8
108
23-139
2 20
Bis(2-ethylhexyl)phthalate
37.9
3.66
pg/L
50
37.4
75.8
21-162
1.3 20
Butyl benzyl phthalate
38.1
4.59
pg/L
50
39.7
76.2
33-142
4.1 20
4-Chlorophenyl phenyl ether
34.8
0.479
pg/L
50
32.5
69.6
39-110
6.8 20
Carbazole
42.2
0.476
pg/L
50
39.1
84.4
20-147
7.6 20
4-Chloro-3-methyl phenol
36.3
0.503
pg/L
50
32.5
72.6
35-117
11 20
Bis(2-Chloroisopropyl)ether
22.2
0.546
pg/L
50
19.4
44.4
28-108
13.4 20
4-Bromophenyl phenyl ether
36.7
0.500
pg/L
50
33.4
73.4
31-124
9.4 20
Chrysene
36
0.731
pg/L
50
32.3
72
30-124
10.8 20
Diethyl phthalate
36.5
0.585
pg/L
50
33.6
73
36-130
8.2 20
Dibenz(a,h)anthrace ne
34.2
0.252
pg/L
50
29.9
68.4
27-124
13.4 20
4-Nitrophenol
11.3
1.39
pg/L
50
10.6
22.6
1-76
6.3 20
3-Nitroaniline
36.9
1.53
pg/L
50
32.3
73.8
28-142
13.2 20
Dibenzofuran
36.3
0.423
pg/L
50
33.2
72.6
40-108
8.9 20
2,4-Dinitrotoluene
35.3
0.403
pg/L
50
33.4
70.6
24-147
5.5 20
Bis(2-Chloroethyl)ether
28.8
0.447
pg/L
50
25.1
57.6
16-122
13.7 20
Indeno(1,2,3-cd)pyrene
40.4
1.01
pg/L
50
33.1
80.8
22-126
19.8 20
Dimethyl phthalate
36.4
0.510
pg/L
50
33
72.8
34-123
9.7 20
3,3' Dimethylbenzidine
76.3
1.88
pg/L
200
55.8
38.1
6-192
31 20
Di-n-butyl phthalate
37
1.58
pg/L
50
34.5
74
19-158
6.9 20
3&4 Methylphenol
26.8
0.691
pg/L
50
23.7
53.6
21-96
12.2 20
4,6-Dinitro-2-methylphenol
35.7
3.47
pg/L
50
47.1
71.4
27-128
27.5 20
1,3-Dichlorobenzene
24.2
0.491
pg/L
50
20.6
48.4
21-102
16 20
N-Nitroso-di-n-butylamine
30
0.752
pg/L
50
26.5
60
25-126
12.3 20
2,6-Dinitrotoluene
36.8
0.413
pg/L
50
33.5
73.6
36-125
9.3 20
N-Nitroso-di-n-propylamine
28.9
0.334
pg/L
50
25.3
57.8
29-114
13.2 20
2,4,5-Trichlorophenol
39.4
0.350
pg/L
50
35.1
78.8
26-118
11.5 20
LCD2
LCD2
LCD2
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 55 of 96
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/1 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BSD (0100203 LCSD-L517328)
Source: 0100203 LCS-L517Prepared & Analyzed: 10/19/20
2,3,4,6-Tetrachlorophenol
38.5
0.355
pg/L
50
35.7
77
28-118
7.5
20
Pentachlorophenol
48.7
2.45
pg/L
50
49.5
97.4
17-142
1.6
20
1,4-Dichlorobenzene
24.8
0.580
pg/L
50
21.3
49.6
24-99
15.1
20
Benzo(b)fluoranthene
41.4
0.941
pg/L
50
38.4
82.8
36-131
7.5
20
Aniline
22.1
0.316
pg/L
50
18.1
44.2
16-133
19.9
20
Benzo(a)pyrene
35.5
1.00
pg/L
50
30.9
71
34-131
13.8
20
Phenol
11.9
0.389
pg/L
50
10.5
23.8
11-55
12.5
20
Benzidine
49.1
0.689
pg/L
150
37.5
32.7
2-176
26.7
20
LCD2
1,2-Dichlorobenzene
25.5
0.629
pg/L
50
22.5
51
26-100
12.5
20
1,2,4-Trichlorobenzene
27.3
0.482
pg/L
50
24.3
54.6
23-106
11.6
20
Pyrene
33
1.04
pg/L
50
40.7
66
20-154
20.8
20
LCD2
1,2,4,5-Tetrachlorobenzene
30.2
0.317
pg/L
50
26.8
60.4
28-110
11.9
20
Pyridine
15.7
0.678
pg/L
50
12.9
31.4
10-71
19.5
20
Phenanthrene
36.1
0.464
pg/L
50
33.2
72.2
40-120
8.3
20
Nitrobenzene
30
0.531
pg/L
50
26.3
60
27-117
13.1
20
Isophorone
26.6
0.360
pg/L
50
23.3
53.2
31-116
13.2
20
2,6-Dichlorophenol
35.5
0.703
pg/L
50
31.1
71
25-112
13.2
20
Benzoic Acid
18.9
5.00
pg/L
150
30.6
12.6
11-68
47.2
20
LCD2
Naphthalene
28
0.484
pg/L
50
24.7
56
33-108
12.5
20
4-Chloroaniline
28.7
0.526
pg/L
50
24.4
57.4
24-127
16.1
20
Benzo(k)fluoranthene
43.7
0.752
pg/L
50
34.5
87.4
32-132
23.5
20
LCD2
N-Nitrosodiphenylamine
31
0.783
pg/L
50
27.7
62
45-135
11.2
20
Hexachlorobutadiene
25.5
0.405
pg/L
50
22.5
51
22-109
12.5
20
2,4,6-Trichlorophenol
38.5
0.344
pg/L
50
34.3
77
26-115
11.5
20
N-Nitrosodiethylamine
32.6
0.400
pg/L
50
28.1
65.2
25-107
14.8
20
N-Nitrosodimethylamine
15.1
0.249
pg/L
50
12.8
30.2
14-84
16.4
20
Acetophenone
31.3
0.686
pg/L
50
27.2
62.6
25-108
14
20
2,4-Dimethylphenol
33.7
0.674
pg/L
50
30.2
67.4
34-105
10.9
20
2,4-Dinitrophenol
77.8
4.85
pg/L
150
103
51.8
10-132
27.8
20
LCD2
Benzo(g,h,i)perylene
33.7
1.36
pg/L
50
30.6
67.4
26-123
9.6
20
2,4-Dichlorophenol
25.7
1.52
pg/L
50
23.3
51.4
32-110
9.7
20
Surrogate:4-Terphenyl-d14
55.2
pg/L
100
74.7
55.2
35-126
Surrogate:2-Fluorophenol
23.5
pg/L
100
20.2
23.5
10-44
Surrogate:2-Fluorobiphenyl
45
Ng/L
100
43.6
45
24-93
Surrogate: 2,4,6-Tribromophenol
67.8
pg/L
100
63.3
67.8
39-110
Surrogate: Phenol-d6
16.4
Ng/L
100
14.8
16.4
7-32
Surrogate: Nitrobenzene-d5
49.7
Ng/L
100
47.4
49.7
20-91
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 56 of 96
• 0
Waypoint
ANALYTICAL
Level II QC Report
12/1 /20
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall Work Order: 0100203
Attn: Alec Macbeth Time Submitted: 10/15/2020 8:45:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BS (0100203 LCS-L517328)
Prepared & Analyzed: 10/19/20
Benzo(a)anthrace ne
32.5
0.427
pg/L
50
65
36-127
Benzoic Acid
30.6
5.00
pg/L
150
20.4
11-68
Benzo(a)pyrene
30.9
1.00
pg/L
50
61.8
34-131
Benzyl alcohol
20.5
3.01
pg/L
50
41
20-109
Benzo(k)fluoranthene
34.5
0.752
pg/L
50
69
32-132
Bis(2-Chloroethoxy)methane
27.3
0.433
pg/L
50
54.6
20-126
Bis(2-Chloroethyl)ether
25.1
0.447
pg/L
50
50.2
16-122
Benzo(b)fluoranthene
38.4
0.941
pg/L
50
76.8
36-131
Benzo(g,h,i)perylene
30.6
1.36
pg/L
50
61.2
26-123
Bis(2-Chloroisopropyl)ether
19.4
0.546
pg/L
50
38.8
28-108
N-Nitrosodiphenylamine
27.7
0.783
pg/L
50
55.4
45-135
Hexachlorobutadiene
22.5
0.405
pg/L
50
45
22-109
Nitrobenzene
26.3
0.531
pg/L
50
52.6
27-117
N-Nitrosodiethylamine
28.1
0.400
pg/L
50
56.2
25-107
N-Nitrosodimethylamine
12.8
0.249
pg/L
50
25.6
14-84
Isophorone
23.3
0.360
pg/L
50
46.6
31-116
N-Nitroso-di-n-propylamine
25.3
0.334
pg/L
50
50.6
29-114
Indeno(1,2,3-cd)pyrene
33.1
1.01
pg/L
50
66.2
22-126
Pentachlorophenol
49.5
2.45
pg/L
50
99
17-142
Phenanthrene
33.2
0.464
pg/L
50
66.4
40-120
Phenol
10.5
0.389
pg/L
50
21
11-55
Pyrene
40.7
1.04
pg/L
50
81.4
20-154
Pyridine
12.9
0.678
pg/L
50
25.8
10-71
N-Nitroso-di-n-butylamine
26.5
0.752
pg/L
50
53
25-126
Di-n-butyl phthalate
34.5
1.58
pg/L
50
69
19-158
Butyl benzyl phthalate
39.7
4.59
pg/L
50
79.4
33-142
Carbazole
39.1
0.476
pg/L
50
78.2
20-147
Chrysene
32.3
0.731
pg/L
50
64.6
30-124
Dibenz(a,h)anthrace ne
29.9
0.252
pg/L
50
59.8
27-124
Dibenzofuran
33.2
0.423
pg/L
50
66.4
40-108
Naphthalene
24.7
0.484
pg/L
50
49.4
33-108
Dimethyl phthalate
33
0.510
pg/L
50
66
34-123
Bis(2-ethylhexyl)phthalate
37.4
3.66
pg/L
50
74.8
21-162
Di-n-Octyl Phthalate
36.4
1.72
pg/L
50
72.8
29-136
Fluoranthene
36
0.406
pg/L
50
72
28-127
Fluorene
31.4
0.444
pg/L
50
62.8
41-116
Hexachlorobenzene
33.6
2.57
pg/L
50
67.2
18-136
Hexachlorocyclopentadiene
13.9
2.34
pg/L
50
27.8
10-102
Hexachloroethane
19
0.277
pg/L
50
38
16-107
Diethyl phthalate
33.6
0.585
pg/L
50
67.2
36-130
2,4-Dimethylphenol
30.2
0.674
pg/L
50
60.4
34-105
4-Chloroaniline
24.4
0.526
pg/L
50
48.8
24-127
2,4,5-Trichlorophenol
35.1
0.350
pg/L
50
70.2
26-118
4-Chloro-3-methylphenol
32.5
0.503
pg/L
50
65
35-117
2-Methyl naphthalene
29.7
0.485
pg/L
50
59.4
34-108
4,6-Dinitro-2-methylphenol
47.1
3.47
pg/L
50
94.2
27-128
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 57 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BS (0100203 LCS-L517328)
Prepared & Analyzed: 10/19/20
2,4,6-Trichlorophenol
34.3
0.344
pg/L
50
68.6
26-115
3-Nitroaniline
32.3
1.53
pg/L
50
64.6
28-142
2,4-Dichlorophenol
23.3
1.52
pg/L
50
46.6
32-110
3,3'-Dichlorobenzidine
95.9
3.74
pg/L
150
63.9
6-192
2,3,4,6-Tetrachlorophenol
35.7
0.355
pg/L
50
71.4
28-118
3&4 Methylphenol
23.7
0.691
pg/L
50
47.4
21-96
4-Bromophenyl phenyl ether
33.4
0.500
pg/L
50
66.8
31-124
2-Nitrophenol
28.6
0.606
pg/L
50
57.2
25-114
2,4-Dinitrophenol
103
4.85
pg/L
150
68.6
10-132
2-Nitroaniline
35
0.574
pg/L
50
70
32-127
2-Methylphenol
22
0.721
pg/L
50
44
22-97
2,4-Dinitrotoluene
33.4
0.403
pg/L
50
66.8
24-147
2,6-Dichlorophenol
31.1
0.703
pg/L
50
62.2
25-112
2,6-Dinitrotoluene
33.5
0.413
pg/L
50
67
36-125
2-Chloronaphthalene
26
0.476
pg/L
50
52
29-137
2-Chorophenol
25
0.736
pg/L
50
50
27-102
3,3' Dimethylbenzidine
55.8
1.88
pg/L
200
27.9
6-192
1,2,4-Trichlorobenzene
24.3
0.482
pg/L
50
48.6
23-106
Acetophenone
27.2
0.686
pg/L
50
54.4
25-108
4-Chlorophenyl phenyl ether
32.5
0.479
pg/L
50
65
39-110
1,2-Dichlorobenzene
22.5
0.629
pg/L
50
45
26-100
Acenaphthene
27.4
0.422
pg/L
50
54.8
38-117
Aniline
18.1
0.316
pg/L
50
36.2
16-133
Anthracene
33.8
0.467
pg/L
50
67.6
34-128
Acenaphthylene
29.7
0.429
pg/L
50
59.4
37-114
1,3-Dichlorobenzene
20.6
0.491
pg/L
50
41.2
21-102
1,2,4,5-Tetrachlorobenzene
26.8
0.317
pg/L
50
53.6
28-110
4-Nitroaniline
52.8
0.740
pg/L
50
106
23-139
4-Nitrophenol
10.6
1.39
pg/L
50
21.2
1-76
Benzidine
37.5
0.689
pg/L
150
25
2-176
1,4-Dichlorobenzene
21.3
0.580
pg/L
50
42.6
24-99
Surrogate: Nitrobenzene-d5
47.4
Ng/L
100
47.4
20-91
Surrogate: Phenol-d6
14.8
pg/L
100
14.8
7-32
Surrogate: 2,4,6-Tribromophenol
63.3
Ng/L
100
63.3
39-110
Surrogate:2-Fluorophenol
20.2
Ng/L
100
20.2
10-44
Surrogate:2-Fluorobiphenyl
43.6
Ng/L
100
43.6
24-93
Surrogate:4-Terphenyl-d14
74.7
Ng/L
100
74.7
35-126
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 58 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BILK (0100203 LRB-L517328)
Prepared & Analyzed: 10/19/20
Nitrobenzene
BRL
5.00
pg/L
1,2,4-Trichlorobenzene
BRL
5.00
pg/L
Pyridine
BRL
10.0
pg/L
2,4-Dinitrotoluene
BRL
5.00
pg/L
Naphthalene
BRL
2.00
pg/L
2,6-Dichlorophenol
BRL
5.00
pg/L
Hexachloroethane
BRL
5.00
pg/L
1,2,4,5-Tetrachlorobenzene
BRL
5.00
pg/L
1,2-Dichlorobenzene
BRL
5.00
pg/L
Indeno(1,2,3-cd)pyrene
BRL
2.00
pg/L
Isophorone
BRL
5.00
pg/L
2,6-Dinitrotoluene
BRL
5.00
pg/L
Pyrene
BRL
2.00
pg/L
1,3-Dichlorobenzene
BRL
5.00
pg/L
2,3,4,6-Tetrachlorophenol
BRL
5.00
pg/L
N-Nitrosodiphenylamine
BRL
10.0
pg/L
Pentachlorophenol
BRL
10.0
pg/L
N-Nitroso-di-n-propylamine
BRL
5.00
pg/L
2,4,5-Trichlorophenol
BRL
5.00
pg/L
Phenanthrene
BRL
2.00
pg/L
1,4-Dichlorobenzene
BRL
5.00
pg/L
N-Nitroso-di-n-butylamine
BRL
5.00
pg/L
N-Nitrosodimethylamine
BRL
5.00
pg/L
2,4,6-Trichlorophenol
BRL
5.00
pg/L
2,4-Dichlorophenol
BRL
5.00
pg/L
N-Nitrosodiethylamine
BRL
5.00
pg/L
Phenol
BRL
5.00
pg/L
2,4-Dimethylphenol
BRL
5.00
pg/L
2,4-Dinitrophenol
BRL
10.0
pg/L
2-Chloronaphthalene
BRL
5.00
pg/L
Benzyl alcohol
BRL
10.0
pg/L
2-Chlorophenol
BRL
5.00
pg/L
4-Chloro-3-methyl phenol
BRL
5.00
pg/L
Hexachlorobenzene
BRL
5.00
pg/L
4-Chloroaniline
BRL
5.00
pg/L
Bis(2-ethylhexyl)phthalate
BRL
5.00
pg/L
4-Chlorophenyl phenyl ether
BRL
5.00
pg/L
Bis(2-Chloroisopropyl)ether
BRL
5.00
pg/L
Bis(2-Chloroethyl)ether
BRL
5.00
pg/L
4-Nitroaniline
BRL
5.00
pg/L
Bis(2-Chloroethoxy)methane
BRL
5.00
pg/L
4-Bromophenyl phenyl ether
BRL
5.00
pg/L
Carbazole
BRL
5.00
pg/L
Benzoic Acid
BRL
10.0
pg/L
Acenaphthene
BRL
2.00
pg/L
Acenaphthylene
BRL
2.00
pg/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 59 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2020 Fall
Attn: Alec Macbeth
231 Haywood Street Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Asheville, NC 28801
Semivolatile Organic Compounds - GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch L517328 - 3510C
BILK (0100203 LRB-11-517328)
Prepared & Analyzed: 10/19/20
Benzo(k)fluoranthene
BRL
2.00
pg/L
Acetophenone
BRL
5.00
pg/L
Benzo(g,h,i)perylene
BRL
2.00
pg/L
Benzo(b)fluoranthene
BRL
2.00
pg/L
Anthracene
BRL
2.00
pg/L
Benzidine
BRL
20.0
pg/L
Benzo(a)pyrene
BRL
2.00
pg/L
4-Nitrophenol
BRL
10.0
pg/L
2-Nitroaniline
BRL
5.00
pg/L
Hexachlorocyclopentadiene
BRL
5.00
pg/L
Hexachlorobutadiene
BRL
5.00
pg/L
Aniline
BRL
5.00
pg/L
2-Methyl naphthalene
BRL
2.00
pg/L
Benzo(a)anthracene
BRL
2.00
pg/L
Fluorene
BRL
2.00
pg/L
Butyl benzyl phthalate
BRL
5.00
pg/L
Fluoranthene
BRL
2.00
pg/L
Chrysene
BRL
2.00
pg/L
Diethyl phthalate
BRL
5.00
pg/L
4,6-Dinitro-2-methylphenol
BRL
10.0
pg/L
Dibenz(a,h)anthrace ne
BRL
2.00
pg/L
2-Methylphenol
BRL
5.00
pg/L
3-Nitroaniline
BRL
10.0
pg/L
Di-n-Octyl Phthalate
BRL
5.00
pg/L
3,3'-Dichlorobenzidine
BRL
10.0
pg/L
3,3' Dimethylbenzidine
BRL
10.0
pg/L
Dimethyl phthalate
BRL
5.00
pg/L
Di-n-butyl phthalate
BRL
5.00
pg/L
3&4 Methylphenol
BRL
5.00
pg/L
2-Nitrophenol
BRL
5.00
pg/L
Dibenzofuran
BRL
5.00
pg/L
-
Surrogate: Phenol-d6
16.3
Ng/L
100
16.3
7-32
Surrogate: Nitrobenzene-d5
54.3
pg/L
100
54.3
20-91
Surrogate: 2,4,6-Tribromophenol
68.5
Ng/L
100
68.5
39-110
Surrogate:4-Terphenyl-d14
71.7
Ng/L
100
71.7
35-126
Surrogate:2-Fluorobiphenyl
47.9
Ng/L
100
47.9
24-93
Surrogate:2-Fluorophenol
24.2
Ng/L
100
24.2
10-44
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 60 of 96
1 0
Waypoint
ANALYTICAL
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Organic Carbon - Quality Control
Analyte
Batch L518400 - 531 OC-2011
Project: Jackson Cty Landfill 2020 Fall
Project No: 50-02
Level II QC Report
12/1 /20
Work Order: 0100203
Time Submitted: 10/15/2020 8:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
MSD (0100203 G 84826-MSD-L518400)
Source: 0100203 G 84826-rPrepared: 10/23/20 Analyzed: 10/25/20
TOC
19.9 0.522 mg/L
5.26 20.2 91 70-130 1.4 20
MS (0100203 G 84826-MS-L518400)
Prepared: 10/23/20 Analyzed: 10/25/20
TOC
20.2 0.522 mg/L
5.26 97 70-130
BS (0100203 LCS-L518400)
Prepared: 10/23/20 Analyzed: 10/24/20
TOC
5.24 0.498 mg/L
5 105 85-115
BILK (0100203 LRB-L518400)
Prepared: 10/23/20 Analyzed: 10/24/20
TOC
BRL 1.00 mg/L
-
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Page 61 of 96
Sample Extraction Data
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
0100203-03
POJ0496
50
mL
50 mL
10/27/20 9:15
0100203-04
POJ0496
50
mL
50 mL
10/27/20 9:15
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
0100203-03
POJ0394
20
mL
30 mL
10/21/20 11:39
0100203-04
POJ0394
20
mL
30 mL
10/21/20 11:39
Prep Method: 9010C
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
POJ0357
50
mL
50 mL
10/20/20 8:10
Prep Method: SM4500-S C
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
POJ0337
200
mL
200 mL
10/19/20 11:02
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
POJ0286
980
mL
10 mL
10/16/20 10:15
0100203-03
POJ0286
1000
mL
10 mL
10/16/20 10:15
0100203-04
POJ0286
990
mL
10 mL
10/16/20 10:15
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
POJ0286
980
mL
10 mL
10/16/20 10:15
0100203-03
POJ0286
1000
mL
10 mL
10/16/20 10:15
0100203-04
POJ0286
990
mL
10 mL
10/16/20 10:15
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
POJ0312
50
mL
50 mL
10/16/20 8:32
0100203-01
POJ0312
50
mL
50 mL
10/16/20 8:32
0100203-01
POJ0491
50
mL
50 mL
10/27/20 7:00
0100203-02
POJ0312
50
mL
50 mL
10/16/20 8:32
0100203-02
POJ0312
50
mL
50 mL
10/16/20 8:32
0100203-02
POJ0491
50
mL
50 mL
10/27/20 7:00
0100203-03
POJ0312
50
mL
50 mL
10/16/20 8:32
0100203-03
POJ0312
50
mL
50 mL
10/16/20 8:32
0100203-03
POJ0491
50
mL
50 mL
10/27/20 7:00
0100203-04
POJ0491
50
mL
50 mL
10/27/20 7:00
0100203-04
POJ0312
50
mL
50 mL
10/16/20 8:32
0100203-04
POJ0312
50
mL
50 mL
10/16/20 8:32
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
POJ0374
20
mL
30 mL
10/20/20 11:55
0100203-02
POJ0374
20
mL
30 mL
10/20/20 11:55
0100203-03
POJ0374
20
mL
30 mL
10/20/20 11:55
0100203-04
POJ0374
20
mL
30 mL
10/20/20 11:55
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 62 of 96
Sample Extraction Data
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
POJ0321
10
mL
10 mL
10/21/20 10:00
0100203-02
POJ0321
10
mL
10 mL
10/21/20 10:00
0100203-03
POJ0321
10
mL
10 mL
10/21/20 10:00
0100203-04
POJ0321
10
mL
10 mL
10/21/20 10:00
0100203-06
POJ0321
10
mL
10 mL
10/21/20 10:00
Prep Method: 5030B
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
POJ0316
5
mL
5 mL
10/16/20 10:00
0100203-02
POJ0316
5
mL
5 mL
10/16/20 10:00
0100203-03
POJ0316
5
mL
5 mL
10/16/20 10:00
0100203-04
POJ0316
5
mL
5 mL
10/16/20 10:00
Sample Extraction
Data
Prep Method: 3510C
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
L517325
10/19/20 15:45
0100203-03
L517325
10/19/20 15:45
0100203-04
L517325
10/19/20 15:45
Prep Method: 8151A
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
L517923
10/21/20 16:30
0100203-03
L517923
10/21/20 16:30
0100203-04
L517923
10/21/20 16:30
Prep Method: 3510C
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
L517328
10/19/20 15:45
0100203-03
L517328
10/19/20 15:45
0100203-04
L517328
10/19/20 15:45
Prep Method: 5310C-2011
Lab Number
Batch
Initial
Final
Date/Time
0100203-01
L518400
10/23/20 14:11
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 63 of 96
Subcontracted Analyses
The following analyses were subcontracted to Pace Analytical Gulf Coast
Lab Number
Analysis
0100203-01
Carbon Dioxide AM20GAX
0100203-01
Methane, Ethane, Ethene (AM20GAX)
0100203-01
Volatile Fatty Acids (Sub)
0100203-07
Carbon Dioxide AM20GAX
0100203-07
Methane, Ethane, Ethene (AM20GAX)
0100203-07
Volatile Fatty Acids (Sub)
0100203-08
Carbon Dioxide AM20GAX
0100203-08
Hydrogen AM20GAX
0100203-08
Methane, Ethane, Ethene (AM20GAX)
0100203-08
Volatile Fatty Acids (Sub)
0100203-09
Carbon Dioxide AM20GAX
0100203-09
Hydrogen AM20GAX
0100203-09
Methane, Ethane, Ethene (AM20GAX)
0100203-09
Volatile Fatty Acids (Sub)
The following analyses were subcontracted to Pace Analytical, Inc
Lab Number
0100203-05
Analysis
524.2 (Sub)
The following analyses were subcontracted to Waypoint Analytical
Lab Number
Analysis
0100203-01
8270 (App. II)
0100203-01
Herbicides (Sub)
0100203-01
TOC (Sub)
0100203-03
8270 (App.11)
0100203-03
Herbicides (Sub)
0100203-04
8270 (App.11)
0100203-04
Herbicides (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 64 of 96
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aceAna lytical
LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
PERFORMED BY
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
(225) 769-4900
Report Date 10/29/2020
Report k 230101903
11111111111111111111
Project 0100203
Deliver To Additional Recipients
Angie Overcash NONE
Waypoint Analytical
449 Springbrook Road
PO Box 240543
Charlotte, NC 28224
704 529 6364
I25
At 1. 1 SO
PJ� �o
Testing
Doi} EIAP
Kcnto
$vTAA1
Pace Gulf Coast Report#: 220101903 1 Page 67 of 96
Report#: 220101903
ZeAnaly�ical®
Project ID: 0100203 Report Date: 10/29/2020
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
Pace Gulf Coast Report 220101903
Pace Gulf Coast Report#: 220101903 1 Page 68 of 96
Report#: 220101903
aceAnaly�ical®
r
Project ID: 0100203
Certifications
Report Date: 10/29/2020
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Pace Gulf Coast Report#: 220101903 1 Page 69 of 96
Report#: 220101903
ZeAnalytical®
Project ID: 0100203 Report Date: 10/29/2020
Case Narrative
Client: Waypoint Analytical Report: 220101903
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
VOLATILES GAS CHROMATOGRAPHY
In the AM20GAX analysis for analytical batch 695200, Methane was detected at an estimated concentration in the method blank.
This is probable laboratory contamination.
Pace Gulf Coast Report#: 220101903 1 Page 70 of 96
ZeAnalytical®
Report#:
Project ID:
220101903
0100203
Report Date:
10/29/2020
Sample Summary
LAB ID
Client ID
Matrix
Collect Date/Time
Receive Date/Time
22010190301
MW-01-20201014
Water
10/14/202012:00
10/16/2020 12:36
22010190302
MW-02-20201013
Water
10/13/202014:50
10/16/2020 12:36
22010190303
MW-03-20201013
Water
10/13/202010:29
10/16/2020 12:36
22010190304
MW-06-20201013
Water
10/13/202013:15
10/16/2020 12:36
22010190305
MW-03-20201013 (1-12)
Bubble Strip
10/13/2020 10:29
10/16/2020 12:36
22010190306
MW-06-20201013 (1-12)
Bubble Strip
10/13/2020 13:15
10/16/2020 12:36
Pace Gulf Coast Report#: 220101903 1 Page 71 of 96
Report#: 220101903
ZeAnaly�ical®
Project ID: 0100203 Report Date: 10/29/2020
Summary of Compounds Detected
Collect Date 10/14/2020 12:00 LAB ID 22010190301
MW-01-20201014
Receive Date 10/16/2020 12:36 Matrix Water
EPA RSK-175
CAS#
Parameter
Result
DL
LOQ
Units
124-38-9
Carbon Dioxide
128000
2540
18000
ug/L
AM23G
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.45J
0.12
0.50
mg/L
64-18-6
Formic Acid
5.4
0.055
0.50
mg/L
AM20GAX
CAS#
Parameter
Result
DL
LOQ
Units
74-82-8
Methane
4000
2.5
5.0
ug/L
Collect Date 10/13/2020 14:50 LAB ID 22010190302
MW-02-20201013
Receive Date 10/16/2020 12:36 Matrix Water
EPA RSK-175
CAS#
Parameter
124-38-9
Carbon Dioxide
AM23G
CAS#
Parameter
64-19-7
Acetic Acid
64-18-6
Formic Acid
79-09-4
Propionic Acid
AM20GAX
CAS#
Parameter
74-82-8
Methane
Result
DL
LOQ
Units
37100
2540
18000
ug/L
Result
DL
LOQ
Units
0.76
0.12
0.50
mg/L
5.1
0.055
0.50
mg/L
0.053.1
0.053
0.50
mg/L
Result
DL
LOQ
Units
5.0
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220101903 1 Page 72 of 96
Report#: 220101903
ZeAnaly�ical®
Project ID: 0100203 Report Date: 10/29/2020
Summary of Compounds Detected
Collect Date 10/13/2020 10:29 LAB ID 22010190303
MW-03-20201013
Receive Date 10/16/2020 12:36 Matrix Water
EPA RSK-175
CAS#
Parameter
Result
DL
LOQ
Units
124-38-9
Carbon Dioxide
14700
635
4500
ug/L
AM23G
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.95
0.12
0.50
mg/L
64-18-6
Formic Acid
4.8
0.055
0.50
mg/L
50-21-5
Lactic Acid
0.072J
0.053
0.50
mg/L
79-09-4
Propionic Acid
0.056J
0.053
0.50
mg/L
AM20GAX
CAS#
Parameter
Result
DL
LOQ
Units
74-82-8
Methane
3.5,1
2.5
5.0
ug/L
Collect Date 10/13/2020 13:15 LAB ID 22010190304
MW-06-20201013
Receive Date 10/16/2020 12:36 Matrix Water
EPA RSK-175
CAS#
Parameter
124-38-9
Carbon Dioxide
AM23G
CAS#
Parameter
64-19-7
Acetic Acid
64-18-6
Formic Acid
79-09-4
Propionic Acid
Result
DL
LOQ
Units
159000
2540
18000
ug/L
Result
DL
LOQ
Units
0.58
0.12
0.50
mg/L
5.0
0.055
0.50
mg/L
0.054J
0.053
0.50
mg/L
Pace Gulf Coast Report#: 220101903 1 Page 73 of 96
aceAnaly�ical®
r
Report#: 220101903
Project ID: 0100203
Report Date: 10/29/2020
Summary of Compounds Detected
Collect Date 10/13/2020 13:15 LAB ID 22010190304
MW-06-20201013
Receive Date 10/16/2020 12:36 Matrix Water
AM20GAX
CAS# Parameter Result DL LOQ Units
74-82-8 Methane 140 2.5 5.0 ug/L
Collect Date 10/13/2020 10:29 LAB ID 22010190305
MW-03-20201013 (H2)
Receive Date 10/16/2020 12:36 Matrix Bubble Strip
AM20GAX
CAS# Parameter Result DL LOQ Units
1333-74-0 Hydrogen 43 0.49 1.9 nM
Collect Date 10/13/2020 13:15 LAB ID 22010190306
MW-06-20201013 (H2)
Receive Date 10/16/2020 12:36 Matrix Bubble Strip
AM20GAX
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
4.1
0.49
1.9
nM
Pace Gulf Coast Report#: 220101903 1 Page 74 of 96
Report#: 220101903
(ac6AnalXical'
Project ID: 0100203 Report Date: 10/29/2020
Sample Results
Collect Date 10/14/2020 12:00 LAB ID 22010190301
MW-01-20201014
Receive Date 10/16/2020 12:36 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 10/27/202011:57 BMR 695686
CAS#
124-38-9
AM23G
Parameter Result DL LOQ Units
Carbon Dioxide 128000 2540 18000 ug/L
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/26/2020 06:51 MOS 695547
CAS#
Parameter
Result
DL
64-19-7
Acetic Acid
0.45J
0.12
107-92-6
Butyric Acid
0.058U
0.058
64-18-6
Formic Acid
5.4
0.055
142-62-1
Hexanoic Acid
0.058U
0.058
646-07-1
i-Hexanoic Acid
0.056U
0.056
503-74-2
i-Pentanoic Acid
0.061 U
0.061
50-21-5
Lactic Acid
0.053U
0.053
109-52-4
Pentanoic Acid
0.056U
0.056
79-09-4
Propionic Acid
0.053U
0.053
127-17-3
Pyruvic Acid
0.060LI
0.060
/_1 L 101IZa—i'VEVI
LOQ
Units
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/21/202018:28 JCK2 695200
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
74-82-8
Methane
4000
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220101903 1 Page 75 of 96
Report#: 220101903
ZeAnaly�ical®
Project ID: 0100203 Report Date: 10/29/2020
Sample Results
Collect Date 10/13/2020 14:50 LAB ID 22010190302
MW-02-20201013
Receive Date 10/16/2020 12:36 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 10/27/202012:02 BMR 695686
CAS#
124-38-9
AM23G
Parameter Result DL LOQ Units
Carbon Dioxide 37100 2540 18000 ug/L
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/26/2020 07:45 MOS 695547
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.76
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
5.1
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053J
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/21/202018:40 JCK2 695200
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
74-82-8
Methane
5.0
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220101903 1 Page 76 of 96
Report#: 220101903
ZeAnaly�ical®
Project ID: 0100203 Report Date: 10/29/2020
Sample Results
Collect Date 10/13/2020 10:29 LAB ID 22010190303
MW-03-20201013
Receive Date 10/16/2020 12:36 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 5 10/27/202012:17 BMR 695686
CAS#
124-38-9
AM23G
Parameter Result DL LOQ Units
Carbon Dioxide 14700 635 4500 ug/L
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/26/2020 08:38 MOS 695547
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.95
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
4.8
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.072J
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.056J
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/21/202018:52 JCK2 695200
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
74-82-8
Methane
3.5,1
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220101903 1 Page 77 of 96
Report#: 220101903
ZeAnaly�ical®
Project ID: 0100203 Report Date: 10/29/2020
Sample Results
Collect Date 10/13/2020 13:15 LAB ID 22010190304
MW-06-20201013
Receive Date 10/16/2020 12:36 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 20 10/27/202012:22 BMR 695686
CAS#
124-38-9
AM23G
Parameter Result DL LOQ Units
Carbon Dioxide 159000 2540 18000 ug/L
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/26/2020 09:32 MOS 695547
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.58
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
5.0
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.053U
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.054J
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/21/202019:04 JCK2 695200
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.075U
0.075
1.0
ug/L
74-85-1
Ethene
0.12U
0.12
1.0
ug/L
74-82-8
Methane
140
2.5
5.0
ug/L
Pace Gulf Coast Report#: 220101903 1 Page 78 of 96
aceAnaly�ical®
r
Report#: 220101903
Project ID: 0100203
Sample Results
Report Date: 10/29/2020
Collect Date 10/13/2020 10:29 LAB ID 22010190305
MW-03-20201013 (H2)
Receive Date 10/16/2020 12:36 Matrix Bubble Strip
At
%X
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/26/202012:27 AWE 695596
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ
43 0.49 1.9
Collect Date 10/13/2020 13:15 LAB ID 22010190306
MW-06-20201013 (H2)
Receive Date 10/16/2020 12:36 Matrix Bubble Strip
At
\X
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 10/26/202012:39 AWE 695596
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
4.1
0.49
1.9
nM
Pace Gulf Coast Report#: 220101903 1 Page 79 of 96
11!26Analytical
r
Report#: 220101903
Project ID: 0100203
GC Volatiles QC Summary
Report Date: 10/29/2020
Analytical Batch Client ID
MB695686
LCS695686
LCSD695686
695686 LAB ID
2102274
2102275
2102276
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
10/27/20 09:35
10/27/20 09:46
10/27/20 09:56
Matrix
Water
Water
Water
EPA RSK-175
Units
ug/L
Spike
Result
%R
I
Control
Spike
Result
I
%R
RPD
RPD
Result
DLI
Added
Limits%R
1 Added
Limit
Carbon Dioxide 124-38-9
127U
1 1271
87001
83401
96
1 38 - 147
1 87001
8250
95
1 1
1 40
Pace Gulf Coast Report#: 220101903 1 Page 80 of 96
11!26Analytical
Report#: 220101903
Project ID: 0100203
General Chemistry QC Summary
Report Date: 10/29/2020
Analytical Batch Client ID
MB695547
LCS695547
695547 LAB ID
2101734
2101735
Sample Type
MB
LCS
Prep Date
Analysis Date
10/25/20 18:24
10/25/20 17:30
Matrix
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Result
DL
Added
Limits%R
Acetic Acid
64-19-7
0.12U
0.12
2.0
1.9
97
70 - 130
Butyric Acid
107-92-6
0.058U
0.058
2.0
2.0
99
70 - 130
Formic Acid
64-18-6
0.055U
0.055
2.0
2.0
98
70 - 130
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
1.9
96
70 - 130
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
2.0
98
70 - 130
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
2.0
100
70 - 130
Lactic Acid
50-21-5
0.053U
0.053
2.0
1.9
94
70 - 130
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
1.9
95
70 - 130
Propionic Acid
79-09-4
0.053U
0.053
2.0
2.0
99
70 - 130
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
1.7
85
70 - 130
Pace Gulf Coast Report#: 220101903 1 Page 81 of 96
11!26Analytical
Report#: 220101903
Project ID: 0100203
General Chromatography QC Summary
Report Date: 10/29/2020
Analytical Batch Client ID
MB695596
LCS695596
LCSD695596
695596 LAB ID
2101937
2101938
2101939
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
10/26/20 11:01
10/26/20 11:14
10/26/20 11:26
Matrix
AM20GAX
Units
nM
Spike
Result
I
%R
I
Control
I
Spike
Result
%R
RPD
RPD
Result
DLI
Added
Limits%R
1 Added
Limit
Hydrogen 1333-74-0
0.49U
1 0.491
121
10186
1 70 - 130
1 121
9.9184
1 3
1 20
Analytical Batch
Client ID
MB695200
LCS695200
LCSD695200
695200
LAB ID
2099339
2099340
2099341
Sample Type
MB
LCS
LCSD
Prep Date
Analysis Date
10/21/20 15:05
10/21/20 13:42
10/21/20 13:54
Matrix
Water
Water
Water
AM20GAX
Units
ug/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
Result
DL
Added
Limits%R
Added
Ethane
74-84-0
0.075U
0.075
100
99
98
70 - 130
100
110
109
11
T20
Ethene
74-85-1
0.12U
0.12
140
140
95
70-130
140
150
106
11
Methane
74-82-8
3.2J
2.5
490
460
94
70-130
490
510
104
9
Pace Gulf Coast Report#: 220101903 1 Page 82 of 96
m
,-<<4- r�
Client 11): PrismLablSIC - Waypoint Analytical
0 SDG: 220101903 - -
Way pNoi nt PM: RWe
-72 1 1�/
) 3 V460
SUBCONTRACT ORDER
467
Certification: NELAC USAGE
Waypoint Analytical NC x
SC_ Other
0100203
SENDING LABORATORY:
RECEIVING LABORATORN':
Waypoint Analytical
Pace Analytical Guif Coast
P. C. Box 240543
10781 Coursey Blvd
Charlotte, NC 28224-0543
Baton Rouge, LA 70816
Phone: 800-529-6364
Phone :(225) 769-4900
Fax: 704-525-0409
Fax: (225) 767-5717
Project Manager: Angela D. Cvercash
Need 5 day TAT
Analysis Due
Expires Laboratory ID Comments
Sample la: 0100203-01 Water
S2mpled:10114/20 12:00 11LV-01-20201014
'l
Volatile Fatty Acids (Sub)
10/21/20 12:00
Methane. Ethane. Ethene (AM2
10/15/20 12:00
Carbon Dioxide AM20GAX
10/28/20 12:00
Containers Supplied:
-7), �oL4P,Iflo-S
Sample 10: 0100203-07 Water
Sampled:10113120 14:50 MW-02-20201013
Carbon Dioxide AM20GAX
10/27/20 14:50
Volatile Fatty Acids (Sub)
10/20/20 14:50
Methane. Ethane, Ethene (AM2
10/1400 14:50
Containers Supplied,
Sample ID: 0100203-09 Water
Sampied:10/13/20 10.29 MW-03-20201013
Volatile Fatty Acids {Sub}
10/20/20 10:29
Hydrogen AM20GAX
10/27/20 10:29
Carbon Dioxide AM20GAX
10/27/20 10:29
Methane. Ethane. Ethene (AM2
10/14/20 I0:29
Co tns - Supplied,
x Cav,�:-���u
{D �S-
Date Received By
Date
By 3 a Date
Released By Date Received By Date
Released By Date Received By Date
Page 1 of 2
0
rl-
Page 83 of 96 1
Analysis
0
w
SUBCONTRACT ORDER V3 — t U (Lr ]
Certification: NELAC USAGE
Waypoint Analytical NC SC Other
0100203
Due Expires Laboratory 1D Comments
Sample 117: 0100203-09 Water Sampled:10113120 13.15 MW-06-20201013
Volatile Fatty Acids (Sub) 10/20/20 13:15
Methane, Ethane, Ethene (AM2 10/14/20 13:15
Hydrogen AM20GAX 10/27/20 13:15
Carbon Dioxide AM200AX 10/27/20 13:15
Containers Supplied:
J CdL' �fk
'l"q
ny
Released
Client ID- PrismLabNC - Waypoint Analytical
SDG: 220101903 11 iiiiiiiiiiiiiiiiih i��PM: RWe IIII111111�1I1ill1li
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Released By Date Received By Date
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Page 2 of 2
Page 84 of 96 1
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Page 85 of 96 1
15C-ta.Analytical
WmV.paeelahs.eam
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
October 23, 2020
Robbi A. Jones
Prism Laboratories, Inc.
P.O. Box 240543
Charlotte, NC 28224
RE: Project: 0100203
Pace Project No.: 92500841
Dear Robbi Jones:
Enclosed are the analytical results for sample(s) received by the laboratory on October 16, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
matthew.brainard@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Angela Overcash, Prism
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 86 of 96
15C-ta.Analytical
WmV.paeelahs.eam
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
CERTIFICATIONS
Project: 0100203
Pace Project No.: 92500841
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Montana Certification #: Cert 0074
Alaska DEC- CS/UST/LUST
Nebraska Certification: NE-OS-28-14
Alabama Certification #: 41320
New Hampshire Certification M 2958
Arizona Certification# AZ0819
New Jersey Certification M FL022
Colorado Certification: FL NELAC Reciprocity
New York Certification #: 11608
Connecticut Certification #: PH-0216
North Carolina Environmental Certificate #: 667
Delaware Certification: FL NELAC Reciprocity
North Carolina Certification #: 12710
Florida Certification #: E83079
North Dakota Certification #: R-216
Georgia Certification #: 955
Ohio DEP 87780
Guam Certification: FL NELAC Reciprocity
Oklahoma Certification #: D9947
Hawaii Certification: FL NELAC Reciprocity
Pennsylvania Certification #: 68-00547
Illinois Certification #: 200068
Puerto Rico Certification M FL01264
Indiana Certification: FL NELAC Reciprocity
South Carolina Certification: #96042001
Kansas Certification #: E-10383
Tennessee Certification #: TN02974
Kentucky Certification #: 90050
Texas Certification: FL NELAC Reciprocity
Louisiana Certification #: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Louisiana Environmental Certificate M 05007
Virginia Environmental Certification #: 460165
Maryland Certification: #346
West Virginia Certification #: 9962C
Michigan Certification #: 9911
Wisconsin Certification #: 399079670
Mississippi Certification: FL NELAC Reciprocity
Wyoming (EPA Region 8): FL NELAC Reciprocity
Missouri Certification M 236
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 87 of 96
15C-ta.Analytical
WmV.paeelabs.eam
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project: 0100203
Pace Project No.: 92500841
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92500841001 0100203-05 EPA 524.2 JLR 24 PASI-O
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 88 of 96
15C-ta.Analytical
WmV.paeelabs.eam
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: 0100203
Pace Project No.: 92500841
Sample: 0100203-05 Lab ID: 92500841001 Collected: 10/14/20 14:00 Received: 10/16/20 10:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV
Analytical Method: EPA 524.2
Pace Analytical
Services - Ormond
Beach
Benzene
ND
mg/L
0.00050
1
10/20/20 13:06
71-43-2
Carbon tetrachloride
ND
mg/L
0.00050
1
10/20/20 13:06
56-23-5
Chlorobenzene
ND
mg/L
0.00050
1
10/20/20 13:06
108-90-7
1,2-Dichlorobenzene
ND
mg/L
0.00050
1
10/20/20 13:06
95-50-1
1,4-Dichlorobenzene
ND
mg/L
0.00050
1
10/20/20 13:06
106-46-7
1,2-Dichloroethane
ND
mg/L
0.00050
1
10/20/20 13:06
107-06-2
1,1-Dichloroethene
ND
mg/L
0.00050
1
10/20/20 13:06
75-35-4
cis-1,2-Dichloroethene
ND
mg/L
0.00050
1
10/20/20 13:06
156-59-2
trans-1,2-Dichloroethene
ND
mg/L
0.00050
1
10/20/20 13:06
156-60-5
1,2-Dichloropropane
ND
mg/L
0.00050
1
10/20/20 13:06
78-87-5
Ethylbenzene
ND
mg/L
0.00050
1
10/20/20 13:06
100-41-4
Methylene Chloride
ND
mg/L
0.0010
1
10/20/20 13:06
75-09-2
Styrene
ND
mg/L
0.00050
1
10/20/20 13:06
100-42-5
Tetrachloroethene
ND
mg/L
0.00050
1
10/20/20 13:06
127-18-4
Toluene
ND
mg/L
0.00050
1
10/20/20 13:06
108-88-3
1,2,4-Trichlorobenzene
ND
mg/L
0.00050
1
10/20/20 13:06
120-82-1
1,1,1-Trichloroethane
ND
mg/L
0.00050
1
10/20/20 13:06
71-55-6
1,1,2-Trichloroethane
ND
mg/L
0.00050
1
10/20/20 13:06
79-00-5
Trichloroethene
ND
mg/L
0.00050
1
10/20/20 13:06
79-01-6
Vinyl chloride
ND
mg/L
0.00050
1
10/20/20 13:06
75-01-4
Xylene (Total)
ND
mg/L
0.0010
1
10/20/20 13:06
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
10/20/20 13:06
460-00-4
Toluene-d8 (S)
96
%
70-130
1
10/20/20 13:06
2037-26-5
1,2-Dichlorobenzene-d4 (S)
100
%
70-130
1
10/20/20 13:06
2199-69-1
Date: 10/23/2020 05:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L1
Page 89 of 96
15C-ta.Analytical
www.pacelahs.l:am
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: 0100203
Pace Project No.: 92500841
QC Batch: 674985 Analysis Method: EPA 524.2
QC Batch Method: EPA 524.2 Analysis Description: 524.2 MSV
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92500841001
METHOD BLANK: 3671469
Associated Lab Samples: 92500841001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
mg/L
ND
0.00050
10/20/20 11:23
1,1,2-Trichloroethane
mg/L
ND
0.00050
10/20/20 11:23
1,1-Dichloroethene
mg/L
ND
0.00050
10/20/20 11:23
1,2,4-Trichlorobenzene
mg/L
ND
0.00050
10/20/20 11:23
1,2-Dichlorobenzene
mg/L
ND
0.00050
10/20/20 11:23
1,2-Dichloroethane
mg/L
ND
0.00050
10/20/20 11:23
1,2-Dichloropropane
mg/L
ND
0.00050
10/20/20 11:23
1,4-Dichlorobenzene
mg/L
ND
0.00050
10/20/20 11:23
Benzene
mg/L
ND
0.00050
10/20/20 11:23
Carbon tetrachloride
mg/L
ND
0.00050
10/20/20 11:23
Chlorobenzene
mg/L
ND
0.00050
10/20/20 11:23
cis-1,2-Dichloroethene
mg/L
ND
0.00050
10/20/20 11:23
Ethylbenzene
mg/L
ND
0.00050
10/20/20 11:23
Methylene Chloride
mg/L
ND
0.0010
10/20/20 11:23
Styrene
mg/L
ND
0.00050
10/20/20 11:23
Tetrachloroethene
mg/L
ND
0.00050
10/20/20 11:23
Toluene
mg/L
ND
0.00050
10/20/20 11:23
trans-1,2-Dichloroethene
mg/L
ND
0.00050
10/20/20 11:23
Trichloroethene
mg/L
ND
0.00050
10/20/20 11:23
Vinyl chloride
mg/L
ND
0.00050
10/20/20 11:23
Xylene (Total)
mg/L
ND
0.0010
10/20/20 11:23
1,2-Dichlorobenzene-d4 (S)
%
101
70-130
10/20/20 11:23
4-Bromofluorobenzene (S)
%
96
70-130
10/20/20 11:23
Toluene-d8 (S)
%
100
70-130
10/20/20 11:23
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
3671470
Units
Spike
Conc.
3671471
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,1,1-Trichloroethane
mg/L
0.04
0.035
0.038
86
95
70-130
9
20
1,1,2-Trichloroethane
mg/L
0.04
0.036
0.038
90
94
70-130
4
20
1,1-Dichloroethene
mg/L
0.04
0.035
0.039
87
98
70-130
12
20
1,2,4-Trichlorobenzene
mg/L
0.04
0.036
0.038
91
96
70-130
5
20
1,2-Dichlorobenzene
mg/L
0.04
0.035
0.037
88
91
70-130
3
20
1,2-Dichloroethane
mg/L
0.04
0.036
0.038
90
95
70-130
6
20
1,2-Dichloropropane
mg/L
0.04
0.036
0.037
90
93
70-130
4
20
1,4-Dichlorobenzene
mg/L
0.04
0.033
0.034
82
85
70-130
4
20
Benzene
mg/L
0.04
0.036
0.039
89
97
70-130
8
20
Carbon tetrachloride
mg/L
0.04
0.036
0.040
89
99
70-130
11
20
Chlorobenzene
mg/L
0.04
0.035
0.037
88
92
70-130
5
20
Results presented on this page are in the units indicated by the "Units"
column except where an alternate unit is
presented to the right of the
result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/23/2020 05:56 PM without the written consent of Pace Analytical Services, LLC.
Page 90 of 96
15C-ta.Analytical
www.pacelahs.l:am
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: 0100203
Pace Project No.: 92500841
LABORATORY CONTROL SAMPLE & LCSD:
3671470
3671471
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
cis-1,2-Dichloroethene
mg/L
0.04
0.034
0.038
86
96
70-130
11
20
Ethylbenzene
mg/L
0.04
0.036
0.038
90
94
70-130
5
20
Methylene Chloride
mg/L
0.04
0.034
0.038
86
96
70-130
11
20
Styrene
mg/L
0.04
0.036
0.038
91
95
70-130
4
20
Tetrachloroethene
mg/L
0.04
0.037
0.038
92
95
70-130
4
20
Toluene
mg/L
0.04
0.035
0.036
87
91
70-130
4
20
trans-1,2-Dichloroethene
mg/L
0.04
0.034
0.038
86
96
70-130
12
20
Trichloroethene
mg/L
0.04
0.035
0.037
89
93
70-130
5
20
Vinyl chloride
mg/L
0.04
0.056
0.063
140
158
70-130
12
20 L1
Xylene (Total)
mg/L
0.12
0.11
0.11
90
94
70-130
5
20
1,2-Dichlorobenzene-d4 (S)
%
101
99
70-130
4-Bromofluorobenzene (S)
%
103
102
70-130
Toluene-d8 (S)
%
99
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/23/2020 05:56 PM without the written consent of Pace Analytical Services, LLC. pari
Page 91 of 96
15C-ta.Analytical
WmV.paeelahs.eam
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALIFIERS
Project: 0100203
Pace Project No.: 92500841
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/23/2020 05:56 PM without the written consent of Pace Analytical Services, LLC.
Page 92 of 96
15C-ta.Analytical
WmV.paeelabs.eam
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: 0100203
Pace Project No.: 92500841
Lab ID
92500841001
Sample ID
0100203-05
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method
EPA 524.2
QC Batch Analytical Method
674985
REPORT OF LABORATORY ANALYSIS
Analytical
Batch
This report shall not be reproduced, except in full,
Date: 10/23/2020 05:56 PM without the written consent of Pace Analytical Services, LLC.
Page 93 of 96
Document Name:
Document Revised: February 7, 2013
8ceAnayical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
f
F•CAR-Cs-033-Rev,D6
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
Sample... Client Name:upon Receipt Project #WO# : 92500841
Courier: QFed Ex COPS ❑USPS Client
❑ Commerciai ❑Pace ❑Other: 92500841 f l I1111 1111 1 1
Custody Seal Present? MY s i 71No seats Intact? myes nNo
Date/hItlals Person Examining Contents: 1
't
Packing Material: Bubble Wrap QBubble Bags ❑None ❑ other
Thermometer: 92TO61 Tvpe of Ice: ❑Wet []Blue
❑IR Gun ID:
Cooler Temp (°C): ! ( Correction Factor: Add/Subtract (°C) 4.0
Cooler Temp Corrected (°C):
USDA Regulated Soil (Q`N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
Biological Time Frozen?
[]Yesf❑No ❑N/A
[-]None
Temp should be above freezing to VC
❑Samples outof temp criteria, samples on ice, cooling process
has begun
Did samples originate from a foreign source;IntemationallV,
Includln¢ Hawall and Puerto RICO]? FlYes 17No
Comments/Discrepancy:
Chain of Custody Present?
❑Yes
(:]No
[]NIA
1,
Samples Arrived within Nold Timed
DYes'
❑No
❑N/A
2,
Rush Turn Around Time Requested?
❑Yes
ONO
❑NIA
4.
Sufficient Volume?
❑Yes .
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
❑Ye.s
❑Yes
[]NO
[]No
❑N/A
❑NIA
6.
Containers Intact?
Ones
[]No ,
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
Orvo
❑N/A
8.
Sample Labels Match CDC?
❑Yes
❑No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
r
Headspace in VOA Vials (>S-Gmm)?
❑Yes
❑NO
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Des
QNo
ONo
[]N/A
❑N/A
11,
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATIONJRESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Lot ID of split containers:
Date:
Date:
Field Data Requ"d? Dyes []NO
Page 94 of 96
Document Name: Cocument iieviseci: February 7, 201a
Sample Condition ULwn Aecei tISCVFj Page 1 of 2
�acs
AnalyUcal Document No.: Issuing Authority:
*Check mavk top half of box If pH and/or dechtorination Is
verified and within the acceptance range for preservation
samples.
Esceptlorts: VOA, Collforrn, TOC, Oil and Grease, DRO/9015 (water) DOC, LLMS
"Bottom half of box Is to list number of bottle
Project A WO# : 925008 1
PM: MW8 Due Date: 10/23/20
CLIENT: 92-Prism
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PH Adjustment Log for Preserved Samples
Sample 10 Type Of Rratervative pH upon receipt Elate preservation adiusted Time preservation Amount of Preservative Lot k
adiwW added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wilt beient to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, inc orrect containers.
Page 95 of 96
IN
l� fE'f
Waypoint
ANALYTICAL
SUBCONTRACT ORDER � �1 � 1 71-1
Certification: NELAC_ USACE
Waypoint Analytical NC x SC_ Other
0100203
SENDING LABORXFORY: RECEIVING LABORATORY:
Waypoint Analytical
P. O. Box 240543
Charlotte, NC 28224-0543
Phone: 800-529-6364
Fax: 704-525-0409
Project Manager: Angela D. Overcash
Pace Analytical, Inc
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
Phone :(704) 875-9092
Fax: (704) 875-9091
Need 5 day TAT
Analysis Due Expires Laboratory ID Comments
Sample ID: 0100203-05 Water Sampled:10/14/20 14:00 DW-01-20201014
524.2 (Sub)
Containers Supplied
10/28/20 14:00
'}mod-(X
Released By L 'Date Rec " d By Date
Released By Date Received By Date
Released By Date Rccci; ed 13c Date
Released By Date Received By Date
Page 1 of 1
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