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HomeMy WebLinkAbout8603_Surry_Elkin_MSWLF_CDLF_June20GW_20210106R.ENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD
NC DENR
Division of Waste Management - Solid Waste
loaded: Yes / No
Doc/Event #:
Environmental Monitoring
Reporting Form
Notice: This
form and
any
information attached
to it are "Public Records"
as defined in NC
General Statute 132-1. As such, these documents are
available for
inspection
and
examination by any
person upon request (NC
General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Municipal Engineering Services Co., PA
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Jonathan Pfohl Phone: (919)772-5393
E-mail: jpfohl@mesco.com
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Surry County Closed C&D and Landfill Road off Joe Mill Lane (SR 1121) 86-03 .1600 June 26, 2020
Closed MSW Landfill -Elkin Elkin, NC 28621
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑X Detection Monitoring QX Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data
Surface water monitoring data ❑
Notification attached?
Methane gas monitoring data
Corrective action data (specify)
Other(specity)
No. No groundwater or surface water standards were exceeded.
)( Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levelsand a preliminary analysis of the cause and significance of
, concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Benjamin Clawson, P.E.
Facility Represeny�t� Name (Print)
Signature
..
POBox 97, Garner, NC 27529
Facility Representative Address
C-0281
Date
Senior Project Manager
Title
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
(919) 772-5393
(Area Code) Telephone Number
Affix NC Licensed/ Professional Geologist Seal
CARO
SEAL
033710
i ;`�/ ��` • Oar
'ice • oG1N� .' �a
fl)i
Semi -Annual Water Quality Monitoring Report
Benjamin Clawson, P.E.
Senior Project Manager
bclawsonna,mesco.com
June 2020
Prepared for
Surry County Closed C&D and Closed Landfill
Elkin, North Carolina
Permit No. 86-03
Prepared by
Municipal Engineering Services Company, P.A.
P.O. BOX 97
Garner, North Carolina
MESCO Project Number: G20031.0
MUNICIPAL ENGINEERING
�� SERVICES COMPANY P.A.
y� 68 SHIPWASH DRIVE, GARNER, NC 27529 - PHONE: 91 9.772-5393
•,� P.O. Box 349, SOONE, NO ZB607 - PHONE: BZB-262-1767
LIr.FN.gF NINMRFP! C-=31
Jonathan Pfohl
Environmental Specialist
pfohing,mesco.com
TABLE OF CONTENTS
SECTION
Introduction....................................................................................................................................................................................................................................................................................................................................Page
1
Background......................................................................................................................................................................................................................................................................................................................................
Page 1
SamplingLocations............................................................................................................................................................................................................................................................................................................Page
1
SamplingProcedures........................................................................................................................................................................................................................................................................................................Page
2
FieldParameter Data......................................................................................................................................................................................................................................................................................................._Page
2
LaboratoryResults.............................................................................................................................................................................................................................................................................................................._Page
2
QualityControl Samples..........................................................................................................................................................................................................................................................................................Page
2
Groundwater Samples Detected Above Standards..........................................................................................................................................................................................................Page
3
Surface Water Samples Detected Above Standards......................................................................................................................................................................................................Page
3
Groundwater and Surface Water Characterization..........................................................................................................................................................................................................Page
3
Findings..................................................................................................................................................................................................................................................................................................................................................Page
3
Closing....................................................................................................................................................................................................................................................................................................................................................Page
3
SHEETS
TopographicMap with Site Location................................................................................................................................................................................................................................................Sheet 1
SingleEvent Potentiometric Map of Uppermost Aquifer...............................................................................................................................................................................Sheet 2
TABLES
Groundwater Monitoring Well Construction Table....................................................................................................................................................................................................Table
1
FieldObservations of Monitoring Locations.........................................................................................................................................................................................................................Table
2
FieldParameter Data Summary ................................................................................................................................................................................................................................................................_Table
3
Samplingand Analysis Summary ............................................................................................................................................................................................................................................................Table
4
Groundwaterand QC Sample Detections..................................................................................................................................................................................................................................Table
5
SurfaceWater Sample Detections............................................................................................................................................................................................................................................................Table
6
Hydrologic Properties at Monitoring Well Locations.............................................................................................................................................................................................Table
7
APPENDICIES
FieldSampling Parameter Data Sheet(s)....................................................................................................................................................................................................................._Appendix A
LaboratoryAnalysis Report and Chains of Custody..................................................................................................................................................................................Appendix B
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi -Annual Water Quality Monitoring Report for an event performed at the Surry County closed construction and
demolition (C&D) and closed unlined municipal solid waste landfill (MSWLF) located in Elkin NC (SWS Permit
No. 86-03) on June 25-26, 2020. The site is located at the end of Landfill Road off Joe Mill Lane (SR 1121),
Elkin, Surry County, North Carolina. The site location topographic map is depicted as Sheet 1.
NCDEQ Solid Waste Rule NCDEQ Solid Waste Rules 15ANCAC1313.1630 through .1637 require that Surry
County provide this monitoring report to the SWS on a semi-annual basis. In general accordance with 15A NCAC
13B.16320), the SWS Environmental Monitoring Report Form and SWS memorandums this report contains
sampling procedures, field and laboratory results, groundwater characterization and a brief discussion of the
findings. Detection tables, a potentiometric map, field parameters and the laboratory analytical reports with quality
assurance/quality control data and chains -of -custody (COC) are also included in this report.
Laboratory analytical results indicate that volatile organic compound(s) (VOC) were found above their reporting
limit and respective North Carolina Groundwater Standard in groundwater samples collected from MW-2. One or
two total recoverable metals were also detected above its respective groundwater Standard in samples collected
from MW-1, MW-2, MW-3A, MW-4, MW-6 and MW-8.
Background
Prior to operating as a C&D landfill the site operated as an unlined sanitary MSWLF that consisted of two units.
The first area was closed prior to October 1991 with a 24 inch final soil cover. The second area was closed with a
cohesive cap of 18 inches of soil with a minimum permeability of less than 1 x 10-5 cm/sec, and 18 inches of
erosive layer prior to December 31, 1998 in accordance with the Transition Plan. C&D was placed on top of the
cohesive capped MSW unit until 2008. The transfer station that operated at the landfill closed around June 2010
and the site has remained vacant since.
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available
since 1994. The landfill has been in assessment monitoring since 1997 in response to detections of VOCs. The
SWS approved a modification to the assessment monitoring program on October 15, 2014 (DIN:21983) which
entails a subset of wells to be sampled for Appendix I1 parameters once every three years which was performed
during the December 2017 event.
Sampling Locations
The groundwater monitoring network includes 12 locations; nine downgradient monitoring wells (MW-2, MW-3,
MW-3A, MW-4, MW-5, MW-6, MW-7S, MW-7D and MW-8), a background monitoring well (MW-1) and two
downstream surface water points (SW-1, SW-2). All locations were sampled during this event. Water monitoring
locations are depicted on Sheet 2. A summary detailing the construction of the water monitoring wells is
presented on Table 1.
Sampling Procedures
Sampling was conducted utilizing portable methodologies outlined in the NCDENR SWS guidance document Solid
Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008. The function
and integrity of all monitoring locations were visually evaluated as documented on Table 2. The depth to water in
each well was electronically gaged prior to purging to quantify the static water level elevation. Bailing or
submersible pumping was utilized to purge the wells a minimum of three times the volume of standing water in the
well or until dry. Surface water samples were dipped from the surface of Snow Creek at previously designated
locations. Stabilized field parameters were recorded during purging. Samples were then placed into laboratory -
prepared, pre -preserved containers. Samples were kept on ice and transported to a NC -certified laboratory under
proper chain of custody (C-O-C) protocol within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters recorded during purging included pH, specific conductance, temperature and turbidity.
A summary of the field parameter data is presented in Table 3 and field data sheets are in Appendix A. In general
field parameter results remain consistent with previously reported events.
Laboratory Results
Pace Analytical Laboratories (PACE) (NC Cert. #12 & 40) performed the laboratory analysis. Pace reported that
their procedures conformed to the most current, applicable TNI/NELAC standards and the their Quality Assurance
Manual, where applicable, unless otherwise noted in the body of the laboratory report.
Water samples were tested for constituents listed in 40 CFR 258 Appendix I and 1,4-dioxane. A sampling and
analysis table summarizing the locations, targeted constituents and methods is presented as Table 4. Laboratory
results and C-O-Cs are presented in Appendix B.
Water samples were analyzed to the laboratory -established Method Detection Limits (MDL) and any value between
the MDL and laboratory -established Reporting Limit (RL) is qualified by the laboratory as with a "J" which
indicates an estimated concentration. "J-qualified" concentrations are considered non -quantifiable and discretion
should be made prior to making decisions based on a value that the laboratory considers an estimate. Table 5
summarizes constituents detected in groundwater samples compared to Interim Maximum Allowable
Concentrations (IMAC) and North Carolina Groundwater Standards (2L) which are recognized by the NC SWS as
groundwater compliance Standards. Although not applicable for regulatory compliance purposes the detections are
also compared to the Maximum Contaminant Level (MCL) commonly referenced as the Federal Primary "Drinking
Water Standard". Table 6 lists the constituents detected in surface water samples compared to the North Carolina
Surface Water Standards (213), NC Protective Values, EPA Nationally Recommended Water Quality Criteria and
the MCL.
Quality Control Samples
Total cadmium was detected in the EB sample. Arsenic was detected in the laboratory quality control blanks
associated with samples MW-2, therefore they were flagged by the laboratory.
2
Groundwater Samples Above Standards
Metals
One or two total recoverable metals were detected above their respective NC 2L/IMAC value in samples collected
from six wells as summarized below.
Metals Detected Above Standards
Arsenic
Cadmium
Cobalt
2L/IMAC
10
2
1
MW-1
4.4
MW-2
14.2
MW-3A
4.1
22.1
MW-4
4.7
MW-6
3.5
MW-8
7.2
ug/L
VOCs
Benzene was detected in sample MW-2 at 2.3 ug/L which is above its RL (1 ug/L) and 2L Standard (1 ug/L).
Surface Water Samples Above Standards
No parameters were detected in either surface water sample in concentrations exceeding their 2B Standard.
Groundwater Characterization
A single -day potentiometric map constructed from groundwater levels collected during this event is presented as
Sheet 2. Groundwater flow rates and directions were calculated and are included in Table 7. Groundwater flows
generally southwest, towards the Snow Creek discharge feature. Groundwater average linear velocity rates
calculated from modified Darcy's equation indicate flow rates ranged from approximately 90 ft/yr (MW-3A) to 300
ft/yr (MW-4).
Findings
All constituents remain within their respective historically identified range. The reduction in VOC concentrations
over time and distance from the landfill and the prevalence of biodegradation byproducts indicate natural
attenuation is occurring and groundwater quality is expected to continue to improve.
Constituents above NC 2B Standards continue to be absent in the surface water samples (SW-1 and SW-2)
collected from the main Snow Creek discharge feature which also serves as the southern downgradient property
boundary.
Closing
Semi-annual water quality assessment monitoring was performed again in December 2020.
3
Sheets
Topographic Map with Site Location
Surry County Closed MSW/C&D Landfill - Elkin
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ROAD CLASSIFICATION
QUADRANGLE LEGEND Primary highway, Light -duty road, hard or
hard surface ..... _.............. improved surface........ --
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= 2�00� hard surface Unimproved road --_-- 1
Interstate Route C3 U. S. Route 0 State Route
Landfill Road (Off Joe Mill Ln SR 1121)
Elkin, NC 28621
Lat:36-17-49.4007
Long:-80-46-20.6499
Northing:931704.33
Easting:1477683.95
SHEET 1
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PIN: 497300733807 1 \ \ \ \ I \ \ \�O / / /// \ \ \ \ \ / 1 1 \ \ \\\\\\ \\\ \ \\\ \\ \950_
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NOTES:
I. TOPOGRAPHIC CONTOURS FROM NC ONEMAP (11-2013)
2. WELL LOCATIONS PLOTTED WITH ELEVATIONS EXTRAPOLATED
FROM AERIAL PHOTOGPAHY INSPECTION
3. PARCEL BOUNDARY FROM NC ONEMAP (10/2018)
W
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— APPROXIMATE WASTE BOUNDARY
• GROUNDWATER MONITORING WELL
SURFACE WATER MONITORING POINT
UPPERMOST GROUNDWATER FLOW DIRECTION (INFERRED)
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SCALE:
AS SHOWN
DATE:
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DRWN. BY:
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( IN FEET)
CHKD. BY:
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PROJECT
NUMBER
G20031.0
SHEET 2
DRAWING NO
SHEET NO.
Tables
Table 1
Groundwater Monitoring Well Construction Table
June 25-26, 2020
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length
Geology of Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
Latitude
Longitude
(inches)
(ft bgs)
(ft bgs)
(ft)
(ft amsl)
(ft amsl)
(ft amsl)
(ft btoc)
MW-1
11/28/89
4
80
70
10
Soil
1042
1041
984
52.65
36.29711
-80.77236
MW-2
11/08/89
4
79
69
10
Soil
948
947
890
55.91
36.29572
-80.77620
MW-3
11/28/89
4
63
53
10
Soil
932
931
881
48.79
36.29362
-80.77646
MW-3A
09/16/94
2
40
24
16
Fractured Rock
927
924
894
30.68
36.29457
-80.77675
MW-4
09/15/94
2
29
13
16
Fractured Rock
933
929
920
10.90
36.29379
-80.77528
MW-5
09/15/94
2
31
16
15
Fractured Rock
949
845
936
10.63
36.29450
-80.77456
MW-6
09/15/94
2
66
51
15
Fractured Rock
1005
1002
955
46.00
36.29780
-80.77270
MW-7S
06/05/01
2
24
9
15
Fractured Rock
901
889
890
10.57
36.29407
-80.77730
MW-7D
06/05/01
2
90
80
10
Fractured Rock
901
889
895
2.75
36.29407
-80.77730
MW-8
06/04/01
1 2
1 67
52
15
Fractured Rock
1015
1013
971
38.52
36.29739
1 -80.77246
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Slurry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 2
Field Observations of Monitoring Locations
June 25-26, 2020
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears to
be Effective
Comments
MW-1
Yes
Yes
Yes
Yes
Yes
Yes
4" Diameter. Orange purge water
MW-2
Yes
Yes
Yes
Yes
Yes
Yes
4" Diameter. Slow Recharge. Strong odor
MW-3
Yes
Yes
Yes
Yes
Yes
Yes
4" Diameter. Slow Recharge. Purge water odor
MW-3A
Yes
Yes
Yes
Yes
Yes
Unknown
Concrete pad covered with soi. Purge water odor
MW-4
Yes
Yes
Yes
Yes
Yes
Yes
MW-5
Yes
Yes
Yes
Yes
Yes
Unknown
Concrete pad covered with soil.
MW-6
Yes
Yes
Yes
Yes
Yes
Yes
MW-7S
Yes
Yes
Yes
Yes
Yes
Yes
MW-71)
Yes
Yes
Yes
Yes
Yes
Yes
pH elevated likely grout intrusion
MW-8
Yes
Yes
Yes
Yes
Yes
Yes
Purge water odor
SW-1
Yes
-
-
-
-
Moderate gage & high flow
SW-2
Yes
-
-
-
-
Moderate gage & high flow
Any unusual field conditions, observations, or events:
Facility no longer in operation or occupied since transfer station closed in - June 2010.
Vehicle access improved by County since last event.
Slurry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 3
Field Parameter Data Summary
June 25-26, 2020
Depth to
Water
Water
Elevation*
TOC
Elevation*
Temp.
pH
Specific
Conductance
Hardness
Turbidity of
Metals Sample
Parameter
ft (btoc)
ft (amsl)
ft (amsl)
C
SU
umhos/cm
mg/L
NTU
MW-1
52.65
989
1042.00
15.5
6.38
82
--
2.34
MW-2
55.91
892
948.00
15.3
6.85
1452
--
40.6
MW-3
48.79
883
932.00
15.3
6.53
265
--
0.75
MW-3A
30.68
896
926.50
14.8
6.48
776
--
1.93
MW-4
10.90
922
932.50
13.8
6.57
90
--
1.03
MW-5
10.63
938
948.50
13.0
6.39
65
--
1.59
MW-6
46.00
959
1004.50
14.8
6.38
332
--
33.6
MW-7S
10.57
890
901.01
13.6
6.39
380
--
0.45
MW-7D
2.75
898
900.95
13.7
7.93
204
--
1.82
MW-8
38.52
976
1014.87
14.7
6.40
144
--
1.79
Minimum
2.75
883
900.95
13
6.38
65
--
0.45
Average
30.74
924
955.08
14.5
6.6
379
--
8.59
Maximum
55.91
989
1042.00
15.5
7.93
1452
--
40.60
SW-1
-
-
-
18.1
7.15
110
40
6.23
SW-2
-
-
-
18.0
7.23
101
20
6.39
Minimum
-
-
-
18.0
7.15
101
20
6.23
Average
-
-
-
-
18.1
7.19
106
30
6
Maximum
-
-
18.1
7.23
110
40
6.39
NOTES:
= Elevation extrapolated from photo inspected LIDAR released in 2007 by NCDOT (Not Surveyed).
btoc = below top of casing
amsl = above mean sea level
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 4
Sampling and Analysis Summary
June 25-26, 2020
App.
I
Other
Field
Parameters
co
IZ
X
M
cn
>
U
Z,
U
0
�
a)
O>
v
H
2
U
a
H
0
0
0
0
0
0CD(°
C)
co
L
L
L
0
00
a)
a)
m
as
W
a
Y
w
w
J
co
J
N
J
N
LL
_N
LL
N
LL
N
LL
LL
MW-1
x
x
x
x
x
x
x
MW-2
x
x
x
x
x
x
x
MW-3
x
x
x
x
x
x
x
MW-3A
x
x
x
x
x
x
x
MW-4
x
x
x
x
x
x
x
MW-5
x
x
x
x
x
x
x
MW-6
x
x
x
x
x
x
x
MW-7S
x
x
x
x
x
x
x
MW-7D
x
x
x
x
x
x
x
MW-8
x
x
x
x
x
x
x
SW-1
x
x
x
x
x
x
x
x
SW-2
x
x
x
x
x
x
x
x
App I = List from current 40 GFR 258
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 5
Groundwater Sample Detections
June 26, 2020
Parameter Name
MDL
RL
2L Standard
MCL
MW-1
MW-2
MW-3
MW-3A
MW-4
5
MW-6
7D
MW-7S
MW-8
EB
FB
IMAC Value*
BG
s
s
s
S
s
s
s
s
s
QC
QC
Metals Tar eted 40CFR 258 Appendix I
Arsenic, total
4.7
10
10
10
14.2 B
Barium, total
3.5
5
700
2000
31.6
314
70.3
412
23.8
20.2
89.4
11.3
80.5
43.4
Cadmium, total
0.4
1
2
5
4.4 (N)
1.6
4.1 (N)
4.7 (N)
1.7
3.5 (N)
0.82 J
0.71 J
7.2 (N)
0.47 J
Cobalt, total
3.6
5
1`
NE
22.1 (N)
24.4 (N)
Nickel, total
3.5
5
100
NE
31.9
33.7
8.7
Zinc, total
9.5
10
1000
NE
12.1
VOCs (Tarcoeted
40CFR 258
Appendix
I & 1 4-Dioxane
1,1-Dichloroethane
0.27
1
6
NE
0.51 J
0.46J
1,2-Dichlorobenzene
0.29
1
20
NE
5.7
2.1
1.4
0.37 J
1,2-Dichloroethane
0.34
1
0.4
5
0.58 J
1,2-Dichloropropane
0.19
1
0.6
5
0.68 J
2-Butanone (MEK)
3.3
1
4000
NE
3.3 J
Benzene
0.15
1
1
5
2.3 (L)
0.86 J
0.46 J
0.34 J
Toluene
0.24
1
600
1000
0.71 J
Vinyl chloride
0.24
1
0.03
2
0.51 J
cis-1 2-Dichloroethene
1 0.29
1 1
1 70
1 70
1
1 0.36 J
1 5.4
1 5.3
1
1
1 2.2
10.33 J
1 1.4
1 2.4
Notes:
Units ug/L unless shown otherwise, Blank cells means not detected above MDL, NE means not established.
BG= Background Well Sample, QC = Quality Control Sample, S = Sentinel Well Sample
Bold Above RL and Established 2L/IMAC
Above Established Federal MCL Drinking Water Std. (NOT a regulatory compliance Standard)
U= Well Upgradient, D = Well Downgradient
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
RL = Reporting Limit defined by Pace laboratory as "The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix."
2L Standard and MAC Values recognized by the NC SWS as regulatory groundater Standards.
2L = NC 2L Groundater Standard 15A NCAC 02L .0202
MAC = Interim Maximum Allowable Concentration
MCL = Maximum Contaminant Level for drinking water established by the USEPA.
J = "J-qualified". Defined by the lab as "estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
BC = The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the laboratory reporting limit. May indicate a false positive.
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
(L) Prelilminary source is believed to be anthropogenic with Landfill Gas Wor leachate as suspected transport mechanism.
A definitive source of the detections was not determined as part of this report.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 6
Surface Water Sample Detections
June 26, 2020
Name
MDL
RL
NC �Parameter
STDB
NRWQC2
iSTV3
MCC
Downstream
Downstream
Targeted 40CFR 258 Appendix I & 1 4-Dioxane
Barium, total 0.03 1 1 1 NE
NE
200,000 1 2000 17.8
16.7
Hardness
Hardness 120,0001 NE I NE
NE
I NE I NE 40,000
20 000
Notes:
Units ug/L unless indicated otherwise, Blank cells means Not Detected, NE means Not Established
J = "J-qualified" by lab and defined as estimated concentration above the adusted method detection limit and below the adusted reporting limit.
Bold Above Applicable Established 2B Std.
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
analyte
in a specific matrix."
Receiving surface water is Snow Creek (12-62-15) Class C
' NC 2B STD = North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters. Presumed NC SWS adopted the numerical Standard for regulatory compliance purposes.
'EPA NRWQC = EPA Nationally Recommended Water Quality Criteria for Aquatic Life & Human Health.
Nationally Recommended Water Quality Criteria for which NC does not have a Water Quality Standard for one or more uses.
s NC ISTV= North Carolina In -Stream Target Value. Established per language in 15A NCAC 02B .0202 & .0208. Contact DWR staff for further information.
NC PV for barium from fresh and salt water All waters (Class C & SC) for fish consumption.
4 MCL= Maximum Contaminant Level. Federal 'Primary Drinking Water Standard". Shown for comparison purposes only. Not applicable for regulatory compliance purposes.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 7
Hydrologic Properties at Monitoring Locations
June 25-26, 2020
Monitoring
Well
Hydraulic
Conductivity
(cm/second)
Effective
Porosity
N
Hydraulic
Gradient
(feet/feet)
Groundwater
Average Linear
Velocity Rate
(feet/year)
Flow
Direction
Depth to
Groundwater
(ft btoc)
Groundwater
Potentiometric
Elevation*
(ft amsl)
Screened Interval
Lithology
MW-1
9.90E-05
5
0.250
512
N38W
52.75
989
Clay
MW-2
2.00E-05
5
na
na
na
57.28
892**
Clay
MW-3
5.00E-05
5
na
na
na
50.42
883**
Clay
Minimum
2.00E-05
5
0.250
512
-
50.42
880
-
Average
5.63E-05
5
0.250
512
-
53.48
917
-
Maximum
9.90E-05
5
0.250
512
-
57.28
983
-
MW-3A
2.50E-05
5
0.174
90
S62W
31.83
896
Fractured Rock
MW-4
4.20E-04
5
0.034
300
S68W
11.91
922
Fractured Rock
MW-5
2.70E-04
5
0.032
177
N77W
11.62
938
Fractured Rock
MW-6
1.20E-04
5
0.067
166
N11W
46.92
959
Fractured Rock
MW-7S
2.30E-04
5
0.045
216
S81W
11.18
890
Fractured Rock
MW-7D
na
na
na
na
na
3.07
898**
Fractured Rock
MW-8
2.40E-05
5
0.321
160
N26W
40.21
976
Fractured Rock
Minimum
2.40E-05
5
0.032
90
-
3.07
889
-
Average
1.82E-04
5
0.112
185
-
22.39
922
-
Maximum
4.20E-04
1 5
1 0.321
300
1-
46.92
1 970
1-
NOTE: Effective porosity data obtained from GAI Consultants' January 1995 Groundwater Sampling Report.
Hydraulic conductivity values from MW-7S and MW-8 derived from slug tests performed by Joyce Engineering on July 25, 2001.
Values for MW-1 through MW-6 obtained from GAI consultants' January 1995 Groundwater Sampling Report.
Hydrologic gradient calculated from groundwater elevations recorded June 25-26, 2020.
Wells screened in both the upper bedrock & unconfined aquifer utilized for flow directions/gradients.
= Datum used to determine elevation extrapolated from photo inspected LIDAR released 2007 by NCDOT (Not Surveyed).
* = Denotes wells with depressed potentiometric head. Therefore, flow directions and rates not calculable.
Average Linear Velocity Rate (Q) is defined by modified Darcy's equation:
where _ K A
Q ne dl
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Appendix A
Field Sampling Parameter Data Sheet(s)
C.sn�e¢ae, c.ur�n.." f �i� iu
Project:
Surry Co
Closed
MSWLF
&Closed
C&D LF,
Elkin
Samplers:
Page_1_of
1
1,-
� F^ � � s,
R
Sampling
Parameters
Water
Quality Parameters
Depth to
Lab
oes
Total
Specific
��
�'� �'�`
�'
Hard -
Monitoring
Purge
Purge
�,
sample
Sample
VVater
Parameters
Volume
Sampl
Dry
Depth
Total
CO2
DO
Temp.
�
Point
Date
Time
Date
Time
to be
Purged
Type
Durin
Measured
Depth
(mg/I)
(mg/L)
ORP pH
©
Cond.
(mg/L)
Hess
(B"fOP)
(Gal)
e
9
as
Expected
(us/cm
�
(mg/L)
Static
analyzed
for
ex ected
MW-1
�
�/,�,;
�`. -
�-�
I(7)
��..G�
-
�
80
�.��
_�
�y,; ..�
f-�,�dr.
�� ��P
._.�__
„%
,°!�
�
a�
,r�
I(5)
���'�
��
79
S7 s:
� ,
� �
'a-��?,
���
MW-2
� �'
%
MW-3
I
� l_�,
l - -�
r``sr
I(1)
''
�
`�"
80
�
��s;�s
�
�'
P - �
I(2)
�
/V
40
� o =���,
�_:
MW-3A
r;q
�
�
MW-6
�
��
I(3)
'�-�'J
/v
46�
�-t,
�-
�%, �
t f,
—
��F
� —
— k ��
�
I(6)
�% ,,�
���
24
�� � i
;��
�
T
MW-7S
MW-7D
�
�.
t
�
�
o ,.
_ ,
- ___
� � �
-
I(p)
—
_
_
,�, - ,
, � I �
pp
I
N
�
� ,
SW-1
..
�
t o ��
� i
-
--
-
-
-
�
� ,3
SW-2
� �
\
SS B=Stainless
Steel Baler,
D B=Disposable Baler, P=Low flow
Pump, PD=Purged
Dry
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear
NR=No Reading Attempted, NS=No Sample Obtained _
Appendix B
Laboratory Analysis Reports
Chains of Custody
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
July 07, 2020
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 30, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Steven R. Gandy, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
r
e
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 47
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 47
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE SUMMARY
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92484100001
MW-1
Water
06/26/20 16:33
06/30/20 09:00
92484100002
MW-2
Water
06/26/20 15:44
06/30/20 09:00
92484100003
MW-3
Water
06/26/20 15:57
06/30/20 09:00
92484100004
MW-3A
Water
06/26/20 15:41
06/30/20 09:00
92484100005
MW-4
Water
06/26/20 16:11
06/30/20 09:00
92484100006
MW-5
Water
06/26/20 16:15
06/30/20 09:00
92484100007
MW-6
Water
06/26/20 14:46
06/30/20 09:00
92484100008
MW-7D
Water
06/26/20 15:36
06/30/20 09:00
92484100009
MW-7S
Water
06/26/20 15:34
06/30/20 09:00
92484100010
MW-8
Water
06/26/20 14:49
06/30/20 09:00
92484100011
SW-1
Water
06/26/20 15:27
06/30/20 09:00
92484100012
SW-2
Water
06/26/20 15:18
06/30/20 09:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 47
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Surry Cloed LF-Elkin
92484100
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92484100001
MW-1
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100002
MW-2
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100003
MW-3
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100004
MW-3A
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100005
MW-4
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100006
MW-5
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100007
MW-6
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100008
MW-7D
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100009
MW-7S
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100010
MW-8
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100011
SW-1
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
92484100012
SW-2
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
LMB
49
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 47
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 47
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MWA Lab ID: 92484100001 Collected: 06/26/20 16:33 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 01:28
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:28
7440-38-2 BC
Barium
31.6
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:28
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 01:28
7440-41-7
Cadmium
4.4
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 01:28
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 01:28
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 01:28
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 01:28
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 01:28
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:28
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:28
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 01:28
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 01:28
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 01:28
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 17:39
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 07:24
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 07:24
107-13-1
ND
ug/L
1.0
0.15
1
07/02/20 07:24
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 07:24
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 07:24
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 07:24
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 07:24
74-83-9 IH,IK,v1
ND
ug/L
5.0
3.3
1
07/02/20 07:24
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 07:24
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 07:24
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 07:24
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 07:24
75-00-3 IK
ND
ug/L
5.0
2.3
1
07/02/20 07:24
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 07:24
74-87-3 v2
ND
ug/L
1.0
0.41
1
07/02/20 07:24
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 07:24
74-95-3
ND
ug/L
1.0
0.29
1
07/02/20 07:24
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 07:24
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 07:24
110-57-6
ND
ug/L
1.0
0.27
1
07/02/20 07:24
75-34-3
ND
ug/L
1.0
0.34
1
07/02/20 07:24
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 07:24
75-35-4
ND
ug/L
1.0
0.29
1
07/02/20 07:24
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 07:24
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-1 Lab ID: 92484100001 Collected: 06/26/20 16:33 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/20 07:24
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 07:24
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 07:24
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 07:24
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 07:24
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 07:24
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 07:24
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 07:24
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 07:24
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 07:24
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 07:24
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 07:24
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 07:24
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 07:24
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 07:24
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 07:24
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 07:24
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 07:24
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 07:24
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 07:24
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 07:24
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 07:24
1330-20-7
97
%
70-130
1
07/02/20 07:24
460-00-4
100
%
70-130
1
07/02/20 07:24
17060-07-0
97
%
70-130
1
07/02/20 07:24
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-2 Lab ID: 92484100002 Collected: 06/26/20 15:44 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 01:31
7440-36-0
Arsenic
14.2
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:31
7440-38-2 B
Barium
314
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:31
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 01:31
7440-41-7
Cadmium
1.6
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 01:31
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 01:31
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 01:31
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 01:31
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 01:31
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:31
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:31
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 01:31
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 01:31
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 01:31
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 18:25
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 07:43
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 07:43
107-13-1
2.3
ug/L
1.0
0.15
1
07/02/20 07:43
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 07:43
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 07:43
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 07:43
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 07:43
74-83-9 IH,IK,v1
ND
ug/L
5.0
3.3
1
07/02/20 07:43
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 07:43
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 07:43
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 07:43
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 07:43
75-00-3 IK
ND
ug/L
5.0
2.3
1
07/02/20 07:43
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 07:43
74-87-3 v2
ND
ug/L
1.0
0.41
1
07/02/20 07:43
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 07:43
74-95-3
5.7
ug/L
1.0
0.29
1
07/02/20 07:43
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 07:43
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 07:43
110-57-6
0.51J
ug/L
1.0
0.27
1
07/02/20 07:43
75-34-3
0.58J
ug/L
1.0
0.34
1
07/02/20 07:43
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 07:43
75-35-4
0.36J
ug/L
1.0
0.29
1
07/02/20 07:43
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 07:43
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-2 Lab ID: 92484100002 Collected: 06/26/20 15:44 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
0.68J
ug/L
1.0
0.19
1
07/02/20 07:43
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 07:43
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 07:43
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 07:43
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 07:43
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 07:43
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 07:43
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 07:43
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 07:43
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 07:43
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 07:43
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 07:43
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 07:43
127-18-4
0.71J
ug/L
1.0
0.24
1
07/02/20 07:43
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 07:43
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 07:43
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 07:43
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 07:43
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 07:43
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 07:43
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 07:43
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 07:43
1330-20-7
99
%
70-130
1
07/02/20 07:43
460-00-4
99
%
70-130
1
07/02/20 07:43
17060-07-0
99
%
70-130
1
07/02/20 07:43
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-3 Lab ID: 92484100003 Collected: 06/26/20 15:57 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 01:34
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:34
7440-38-2 BC
Barium
70.3
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:34
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 01:34
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 01:34
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 01:34
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 01:34
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 01:34
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 01:34
7439-92-1
Nickel
31.9
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:34
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:34
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 01:34
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 01:34
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 01:34
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
ND
ug/L
0.10
0.050
1 07/01/20 01:20
07/01/20 18:32
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 08:01
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 08:01
107-13-1
0.86J
ug/L
1.0
0.15
1
07/02/20 08:01
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 08:01
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 08:01
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 08:01
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 08:01
74-83-9
3.3J
ug/L
5.0
3.3
1
07/02/20 08:01
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 08:01
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 08:01
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 08:01
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 08:01
75-00-3
ND
ug/L
5.0
2.3
1
07/02/20 08:01
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 08:01
74-87-3
ND
ug/L
1.0
0.41
1
07/02/20 08:01
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 08:01
74-95-3
ND
ug/L
1.0
0.29
1
07/02/20 08:01
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 08:01
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 08:01
110-57-6
ND
ug/L
1.0
0.27
1
07/02/20 08:01
75-34-3
ND
ug/L
1.0
0.34
1
07/02/20 08:01
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 08:01
75-35-4
5.4
ug/L
1.0
0.29
1
07/02/20 08:01
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 08:01
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 10 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-3 Lab ID: 92484100003 Collected: 06/26/20 15:57 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/20 08:01
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 08:01
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 08:01
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 08:01
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 08:01
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 08:01
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 08:01
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 08:01
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 08:01
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 08:01
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 08:01
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 08:01
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 08:01
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 08:01
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 08:01
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 08:01
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 08:01
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 08:01
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 08:01
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 08:01
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 08:01
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 08:01
1330-20-7
98
%
70-130
1
07/02/20 08:01
460-00-4
100
%
70-130
1
07/02/20 08:01
17060-07-0
98
%
70-130
1
07/02/20 08:01
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-3A Lab ID: 92484100004 Collected: 06/26/20 15:41 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 01:37
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:37
7440-38-2 BC
Barium
412
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:37
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 01:37
7440-41-7
Cadmium
4.1
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 01:37
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 01:37
7440-47-3
Cobalt
22.1
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 01:37
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 01:37
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 01:37
7439-92-1
Nickel
33.7
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:37
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:37
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 01:37
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 01:37
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 01:37
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 18:40
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 08:20
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 08:20
107-13-1
ND
ug/L
1.0
0.15
1
07/02/20 08:20
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 08:20
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 08:20
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 08:20
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 08:20
74-83-9
ND
ug/L
5.0
3.3
1
07/02/20 08:20
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 08:20
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 08:20
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 08:20
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 08:20
75-00-3
ND
ug/L
5.0
2.3
1
07/02/20 08:20
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 08:20
74-87-3
ND
ug/L
1.0
0.41
1
07/02/20 08:20
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 08:20
74-95-3
2.1
ug/L
1.0
0.29
1
07/02/20 08:20
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 08:20
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 08:20
110-57-6
0.46J
ug/L
1.0
0.27
1
07/02/20 08:20
75-34-3
ND
ug/L
1.0
0.34
1
07/02/20 08:20
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 08:20
75-35-4
5.3
ug/L
1.0
0.29
1
07/02/20 08:20
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 08:20
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 12 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-3A Lab ID: 92484100004 Collected: 06/26/20 15:41 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/20 08:20
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 08:20
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 08:20
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 08:20
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 08:20
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 08:20
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 08:20
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 08:20
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 08:20
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 08:20
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 08:20
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 08:20
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 08:20
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 08:20
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 08:20
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 08:20
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 08:20
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 08:20
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 08:20
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 08:20
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 08:20
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 08:20
1330-20-7
97
%
70-130
1
07/02/20 08:20
460-00-4
101
%
70-130
1
07/02/20 08:20
17060-07-0
99
%
70-130
1
07/02/20 08:20
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-4 Lab ID: 92484100005 Collected: 06/26/20 16:11 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 01:54
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:54
7440-38-2 BC
Barium
23.8
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:54
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 01:54
7440-41-7
Cadmium
4.7
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 01:54
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 01:54
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 01:54
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 01:54
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 01:54
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:54
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:54
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 01:54
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 01:54
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 01:54
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 18:55
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 08:38
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 08:38
107-13-1
ND
ug/L
1.0
0.15
1
07/02/20 08:38
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 08:38
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 08:38
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 08:38
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 08:38
74-83-9
ND
ug/L
5.0
3.3
1
07/02/20 08:38
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 08:38
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 08:38
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 08:38
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 08:38
75-00-3
ND
ug/L
5.0
2.3
1
07/02/20 08:38
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 08:38
74-87-3
ND
ug/L
1.0
0.41
1
07/02/20 08:38
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 08:38
74-95-3
ND
ug/L
1.0
0.29
1
07/02/20 08:38
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 08:38
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 08:38
110-57-6
ND
ug/L
1.0
0.27
1
07/02/20 08:38
75-34-3
ND
ug/L
1.0
0.34
1
07/02/20 08:38
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 08:38
75-35-4
ND
ug/L
1.0
0.29
1
07/02/20 08:38
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 08:38
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 14 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-4 Lab ID: 92484100005 Collected: 06/26/20 16:11 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/20 08:38
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 08:38
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 08:38
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 08:38
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 08:38
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 08:38
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 08:38
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 08:38
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 08:38
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 08:38
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 08:38
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 08:38
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 08:38
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 08:38
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 08:38
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 08:38
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 08:38
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 08:38
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 08:38
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 08:38
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 08:38
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 08:38
1330-20-7
99
%
70-130
1
07/02/20 08:38
460-00-4
101
%
70-130
1
07/02/20 08:38
17060-07-0
100
%
70-130
1
07/02/20 08:38
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-5 Lab ID: 92484100006 Collected: 06/26/20 16:15 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 01:57
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:57
7440-38-2 BC
Barium
20.2
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:57
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 01:57
7440-41-7
Cadmium
1.7
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 01:57
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 01:57
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 01:57
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 01:57
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 01:57
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 01:57
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 01:57
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 01:57
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 01:57
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 01:57
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 19:03
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 08:57
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 08:57
107-13-1
ND
ug/L
1.0
0.15
1
07/02/20 08:57
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 08:57
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 08:57
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 08:57
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 08:57
74-83-9
ND
ug/L
5.0
3.3
1
07/02/20 08:57
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 08:57
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 08:57
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 08:57
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 08:57
75-00-3
ND
ug/L
5.0
2.3
1
07/02/20 08:57
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 08:57
74-87-3
ND
ug/L
1.0
0.41
1
07/02/20 08:57
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 08:57
74-95-3
ND
ug/L
1.0
0.29
1
07/02/20 08:57
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 08:57
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 08:57
110-57-6
ND
ug/L
1.0
0.27
1
07/02/20 08:57
75-34-3
ND
ug/L
1.0
0.34
1
07/02/20 08:57
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 08:57
75-35-4
ND
ug/L
1.0
0.29
1
07/02/20 08:57
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 08:57
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 16 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-5 Lab ID: 92484100006 Collected: 06/26/20 16:15 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/20 08:57
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 08:57
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 08:57
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 08:57
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 08:57
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 08:57
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 08:57
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 08:57
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 08:57
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 08:57
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 08:57
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 08:57
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 08:57
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 08:57
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 08:57
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 08:57
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 08:57
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 08:57
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 08:57
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 08:57
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 08:57
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 08:57
1330-20-7
98
%
70-130
1
07/02/20 08:57
460-00-4
101
%
70-130
1
07/02/20 08:57
17060-07-0
100
%
70-130
1
07/02/20 08:57
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-6 Lab ID: 92484100007 Collected: 06/26/20 14:46 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 02:00
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:00
7440-38-2 BC
Barium
89.4
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:00
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 02:00
7440-41-7
Cadmium
3.5
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 02:00
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 02:00
7440-47-3
Cobalt
24.4
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 02:00
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 02:00
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 02:00
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:00
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:00
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 02:00
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 02:00
7440-62-2
Zinc
12.1
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 02:00
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 19:10
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 09:15
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 09:15
107-13-1
0.46J
ug/L
1.0
0.15
1
07/02/20 09:15
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 09:15
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 09:15
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 09:15
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 09:15
74-83-9
ND
ug/L
5.0
3.3
1
07/02/20 09:15
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 09:15
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 09:15
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 09:15
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 09:15
75-00-3
ND
ug/L
5.0
2.3
1
07/02/20 09:15
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 09:15
74-87-3
ND
ug/L
1.0
0.41
1
07/02/20 09:15
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 09:15
74-95-3
1.4
ug/L
1.0
0.29
1
07/02/20 09:15
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 09:15
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 09:15
110-57-6
ND
ug/L
1.0
0.27
1
07/02/20 09:15
75-34-3
ND
ug/L
1.0
0.34
1
07/02/20 09:15
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 09:15
75-35-4
2.2
ug/L
1.0
0.29
1
07/02/20 09:15
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 09:15
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 18 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-6 Lab ID: 92484100007 Collected: 06/26/20 14:46 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/20 09:15
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 09:15
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 09:15
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 09:15
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 09:15
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 09:15
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 09:15
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 09:15
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 09:15
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 09:15
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 09:15
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 09:15
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 09:15
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 09:15
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 09:15
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 09:15
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 09:15
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 09:15
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 09:15
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 09:15
108-05-4
0.511
ug/L
1.0
0.24
1
07/02/20 09:15
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 09:15
1330-20-7
97
%
70-130
1
07/02/20 09:15
460-00-4
101
%
70-130
1
07/02/20 09:15
17060-07-0
97
%
70-130
1
07/02/20 09:15
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-7D Lab ID: 92484100008 Collected: 06/26/20 15:36 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 02:03
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:03
7440-38-2 BC
Barium
11.3
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:03
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 02:03
7440-41-7
Cadmium
0.82J
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 02:03
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 02:03
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 02:03
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 02:03
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 02:03
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:03
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:03
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 02:03
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 02:03
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 02:03
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 19:18
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 09:34
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 09:34
107-13-1
ND
ug/L
1.0
0.15
1
07/02/20 09:34
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 09:34
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 09:34
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 09:34
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 09:34
74-83-9
ND
ug/L
5.0
3.3
1
07/02/20 09:34
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 09:34
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 09:34
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 09:34
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 09:34
75-00-3
ND
ug/L
5.0
2.3
1
07/02/20 09:34
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 09:34
74-87-3
ND
ug/L
1.0
0.41
1
07/02/20 09:34
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 09:34
74-95-3
ND
ug/L
1.0
0.29
1
07/02/20 09:34
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 09:34
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 09:34
110-57-6
ND
ug/L
1.0
0.27
1
07/02/20 09:34
75-34-3
ND
ug/L
1.0
0.34
1
07/02/20 09:34
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 09:34
75-35-4
0.33J
ug/L
1.0
0.29
1
07/02/20 09:34
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 09:34
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 20 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-7D Lab ID: 92484100008 Collected: 06/26/20 15:36 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/20 09:34
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 09:34
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 09:34
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 09:34
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 09:34
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 09:34
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 09:34
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 09:34
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 09:34
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 09:34
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 09:34
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 09:34
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 09:34
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 09:34
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 09:34
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 09:34
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 09:34
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 09:34
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 09:34
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 09:34
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 09:34
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 09:34
1330-20-7
100
%
70-130
1
07/02/20 09:34
460-00-4
99
%
70-130
1
07/02/20 09:34
17060-07-0
98
%
70-130
1
07/02/20 09:34
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-7S Lab ID: 92484100009 Collected: 06/26/20 15:34 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 02:06
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:06
7440-38-2 BC
Barium
80.5
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:06
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 02:06
7440-41-7
Cadmium
0.71J
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 02:06
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 02:06
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 02:06
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 02:06
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 02:06
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:06
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:06
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 02:06
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 02:06
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 02:06
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 19:25
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/20 09:52
67-64-1
ND
ug/L
10.0
0.90
1
07/02/20 09:52
107-13-1
ND
ug/L
1.0
0.15
1
07/02/20 09:52
71-43-2
ND
ug/L
1.0
0.34
1
07/02/20 09:52
74-97-5
ND
ug/L
1.0
0.26
1
07/02/20 09:52
75-27-4
ND
ug/L
1.0
0.62
1
07/02/20 09:52
75-25-2
ND
ug/L
2.0
0.62
1
07/02/20 09:52
74-83-9
ND
ug/L
5.0
3.3
1
07/02/20 09:52
78-93-3
ND
ug/L
2.0
0.40
1
07/02/20 09:52
75-15-0
ND
ug/L
1.0
0.22
1
07/02/20 09:52
56-23-5
ND
ug/L
1.0
0.23
1
07/02/20 09:52
108-90-7
ND
ug/L
1.0
0.49
1
07/02/20 09:52
75-00-3
ND
ug/L
5.0
2.3
1
07/02/20 09:52
67-66-3
ND
ug/L
1.0
0.39
1
07/02/20 09:52
74-87-3
ND
ug/L
1.0
0.41
1
07/02/20 09:52
124-48-1
ND
ug/L
1.0
0.46
1
07/02/20 09:52
74-95-3
ND
ug/L
1.0
0.29
1
07/02/20 09:52
95-50-1
ND
ug/L
1.0
0.26
1
07/02/20 09:52
106-46-7
ND
ug/L
1.0
0.54
1
07/02/20 09:52
110-57-6
ND
ug/L
1.0
0.27
1
07/02/20 09:52
75-34-3
ND
ug/L
1.0
0.34
1
07/02/20 09:52
107-06-2
ND
ug/L
1.0
0.24
1
07/02/20 09:52
75-35-4
1.4
ug/L
1.0
0.29
1
07/02/20 09:52
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 09:52
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 22 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-7S Lab ID: 92484100009 Collected: 06/26/20 15:34 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/20 09:52
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 09:52
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 09:52
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 09:52
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 09:52
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 09:52
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 09:52
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 09:52
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 09:52
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 09:52
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 09:52
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 09:52
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 09:52
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 09:52
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 09:52
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 09:52
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 09:52
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 09:52
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 09:52
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 09:52
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 09:52
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 09:52
1330-20-7
95
%
70-130
1
07/02/20 09:52
460-00-4
99
%
70-130
1
07/02/20 09:52
17060-07-0
99
%
70-130
1
07/02/20 09:52
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-8 Lab ID: 92484100010 Collected: 06/26/20 14:49 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 02:10
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:10
7440-38-2 BC
Barium
43.4
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:10
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 02:10
7440-41-7
Cadmium
7.2
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 02:10
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 02:10
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 02:10
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 02:10
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 02:10
7439-92-1
Nickel
8.7
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:10
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:10
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 02:10
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 02:10
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 02:10
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 19:40
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/2010:11
67-64-1
ND
ug/L
10.0
0.90
1
07/02/2010:11
107-13-1
0.34J
ug/L
1.0
0.15
1
07/02/2010:11
71-43-2
ND
ug/L
1.0
0.34
1
07/02/2010:11
74-97-5
ND
ug/L
1.0
0.26
1
07/02/2010:11
75-27-4
ND
ug/L
1.0
0.62
1
07/02/2010:11
75-25-2
ND
ug/L
2.0
0.62
1
07/02/2010:11
74-83-9
ND
ug/L
5.0
3.3
1
07/02/2010:11
78-93-3
ND
ug/L
2.0
0.40
1
07/02/2010:11
75-15-0
ND
ug/L
1.0
0.22
1
07/02/2010:11
56-23-5
ND
ug/L
1.0
0.23
1
07/02/2010:11
108-90-7
ND
ug/L
1.0
0.49
1
07/02/2010:11
75-00-3
ND
ug/L
5.0
2.3
1
07/02/2010:11
67-66-3
ND
ug/L
1.0
0.39
1
07/02/2010:11
74-87-3
ND
ug/L
1.0
0.41
1
07/02/2010:11
124-48-1
ND
ug/L
1.0
0.46
1
07/02/2010:11
74-95-3
0.37J
ug/L
1.0
0.29
1
07/02/2010:11
95-50-1
ND
ug/L
1.0
0.26
1
07/02/2010:11
106-46-7
ND
ug/L
1.0
0.54
1
07/02/2010:11
110-57-6
ND
ug/L
1.0
0.27
1
07/02/2010:11
75-34-3
ND
ug/L
1.0
0.34
1
07/02/2010:11
107-06-2
ND
ug/L
1.0
0.24
1
07/02/2010:11
75-35-4
2.4
ug/L
1.0
0.29
1
07/02/2010:11
156-59-2
ND
ug/L
1.0
0.25
1
07/02/2010:11
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 24 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: MW-8 Lab ID: 92484100010 Collected: 06/26/20 14:49 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/2010:11
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 10:11
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/2010:11
10061-02-6
ND
ug/L
150
56.2
1
07/02/2010:11
123-91-1
ND
ug/L
1.0
0.26
1
07/02/2010:11
100-41-4
ND
ug/L
5.0
0.57
1
07/02/2010:11
591-78-6
ND
ug/L
20.0
12.5
1
07/02/2010:11
74-88-4
ND
ug/L
5.0
3.7
1
07/02/2010:11
75-09-2
ND
ug/L
5.0
4.5
1
07/02/2010:11
108-10-1
ND
ug/L
1.0
0.27
1
07/02/2010:11
100-42-5
ND
ug/L
1.0
0.34
1
07/02/2010:11
630-20-6
ND
ug/L
1.0
0.22
1
07/02/2010:11
79-34-5
ND
ug/L
1.0
0.16
1
07/02/2010:11
127-18-4
ND
ug/L
1.0
0.24
1
07/02/2010:11
108-88-3
ND
ug/L
1.0
0.18
1
07/02/2010:11
71-55-6
ND
ug/L
1.0
0.24
1
07/02/2010:11
79-00-5
ND
ug/L
1.0
0.22
1
07/02/2010:11
79-01-6
ND
ug/L
1.0
0.31
1
07/02/2010:11
75-69-4
ND
ug/L
1.0
0.35
1
07/02/2010:11
96-18-4
ND
ug/L
2.0
1.4
1
07/02/2010:11
108-05-4
ND
ug/L
1.0
0.24
1
07/02/2010:11
75-01-4
ND
ug/L
1.0
0.63
1
07/02/2010:11
1330-20-7
99
%
70-130
1
07/02/2010:11
460-00-4
103
%
70-130
1
07/02/2010:11
17060-07-0
99
%
70-130
1
07/02/2010:11
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: SW-1 Lab ID: 92484100011 Collected: 06/26/20 15:27 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 02:13
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:13
7440-38-2 BC
Barium
17.8
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:13
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 02:13
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 02:13
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 02:13
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 02:13
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 02:13
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 02:13
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:13
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:13
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 02:13
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 02:13
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 02:13
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 19:48
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/2010:29
67-64-1
ND
ug/L
10.0
0.90
1
07/02/2010:29
107-13-1
ND
ug/L
1.0
0.15
1
07/02/2010:29
71-43-2
ND
ug/L
1.0
0.34
1
07/02/2010:29
74-97-5
ND
ug/L
1.0
0.26
1
07/02/2010:29
75-27-4
ND
ug/L
1.0
0.62
1
07/02/2010:29
75-25-2
ND
ug/L
2.0
0.62
1
07/02/2010:29
74-83-9
ND
ug/L
5.0
3.3
1
07/02/2010:29
78-93-3
ND
ug/L
2.0
0.40
1
07/02/2010:29
75-15-0
ND
ug/L
1.0
0.22
1
07/02/2010:29
56-23-5
ND
ug/L
1.0
0.23
1
07/02/2010:29
108-90-7
ND
ug/L
1.0
0.49
1
07/02/2010:29
75-00-3
ND
ug/L
5.0
2.3
1
07/02/2010:29
67-66-3
ND
ug/L
1.0
0.39
1
07/02/2010:29
74-87-3
ND
ug/L
1.0
0.41
1
07/02/2010:29
124-48-1
ND
ug/L
1.0
0.46
1
07/02/2010:29
74-95-3
ND
ug/L
1.0
0.29
1
07/02/2010:29
95-50-1
ND
ug/L
1.0
0.26
1
07/02/2010:29
106-46-7
ND
ug/L
1.0
0.54
1
07/02/2010:29
110-57-6
ND
ug/L
1.0
0.27
1
07/02/2010:29
75-34-3
ND
ug/L
1.0
0.34
1
07/02/2010:29
107-06-2
ND
ug/L
1.0
0.24
1
07/02/2010:29
75-35-4
ND
ug/L
1.0
0.29
1
07/02/2010:29
156-59-2
ND
ug/L
1.0
0.25
1
07/02/2010:29
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 26 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: SW-1 Lab ID: 92484100011 Collected: 06/26/20 15:27 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/2010:29
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 10:29
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/2010:29
10061-02-6
ND
ug/L
150
56.2
1
07/02/2010:29
123-91-1
ND
ug/L
1.0
0.26
1
07/02/2010:29
100-41-4
ND
ug/L
5.0
0.57
1
07/02/2010:29
591-78-6
ND
ug/L
20.0
12.5
1
07/02/2010:29
74-88-4
ND
ug/L
5.0
3.7
1
07/02/2010:29
75-09-2
ND
ug/L
5.0
4.5
1
07/02/2010:29
108-10-1
ND
ug/L
1.0
0.27
1
07/02/2010:29
100-42-5
ND
ug/L
1.0
0.34
1
07/02/2010:29
630-20-6
ND
ug/L
1.0
0.22
1
07/02/2010:29
79-34-5
ND
ug/L
1.0
0.16
1
07/02/2010:29
127-18-4
ND
ug/L
1.0
0.24
1
07/02/2010:29
108-88-3
ND
ug/L
1.0
0.18
1
07/02/2010:29
71-55-6
ND
ug/L
1.0
0.24
1
07/02/2010:29
79-00-5
ND
ug/L
1.0
0.22
1
07/02/2010:29
79-01-6
ND
ug/L
1.0
0.31
1
07/02/2010:29
75-69-4
ND
ug/L
1.0
0.35
1
07/02/2010:29
96-18-4
ND
ug/L
2.0
1.4
1
07/02/2010:29
108-05-4
ND
ug/L
1.0
0.24
1
07/02/2010:29
75-01-4
ND
ug/L
1.0
0.63
1
07/02/2010:29
1330-20-7
99
%
70-130
1
07/02/2010:29
460-00-4
101
%
70-130
1
07/02/2010:29
17060-07-0
99
%
70-130
1
07/02/2010:29
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: SW-2 Lab ID: 92484100012 Collected: 06/26/20 15:18 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/01/20 01:47
07/02/20 02:16
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:16
7440-38-2 BC
Barium
16.7
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:16
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/01/20 01:47
07/02/20 02:16
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/01/20 01:47
07/02/20 02:16
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/01/20 01:47
07/02/20 02:16
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/01/20 01:47
07/02/20 02:16
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/01/20 01:47
07/02/20 02:16
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/01/20 01:47
07/02/20 02:16
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/01/20 01:47
07/02/20 02:16
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/01/20 01:47
07/02/20 02:16
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/01/20 01:47
07/02/20 02:16
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/01/20 01:47
07/02/20 02:16
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/01/20 01:47
07/02/20 02:16
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
0.050
1
07/01/20 01:20 07/01/20 19:56
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
6.2
1
07/02/2010:48
67-64-1
ND
ug/L
10.0
0.90
1
07/02/2010:48
107-13-1
ND
ug/L
1.0
0.15
1
07/02/2010:48
71-43-2
ND
ug/L
1.0
0.34
1
07/02/2010:48
74-97-5
ND
ug/L
1.0
0.26
1
07/02/2010:48
75-27-4
ND
ug/L
1.0
0.62
1
07/02/2010:48
75-25-2
ND
ug/L
2.0
0.62
1
07/02/2010:48
74-83-9
ND
ug/L
5.0
3.3
1
07/02/2010:48
78-93-3
ND
ug/L
2.0
0.40
1
07/02/2010:48
75-15-0
ND
ug/L
1.0
0.22
1
07/02/2010:48
56-23-5
ND
ug/L
1.0
0.23
1
07/02/2010:48
108-90-7
ND
ug/L
1.0
0.49
1
07/02/2010:48
75-00-3
ND
ug/L
5.0
2.3
1
07/02/2010:48
67-66-3
ND
ug/L
1.0
0.39
1
07/02/2010:48
74-87-3
ND
ug/L
1.0
0.41
1
07/02/2010:48
124-48-1
ND
ug/L
1.0
0.46
1
07/02/2010:48
74-95-3
ND
ug/L
1.0
0.29
1
07/02/2010:48
95-50-1
ND
ug/L
1.0
0.26
1
07/02/2010:48
106-46-7
ND
ug/L
1.0
0.54
1
07/02/2010:48
110-57-6
ND
ug/L
1.0
0.27
1
07/02/2010:48
75-34-3
ND
ug/L
1.0
0.34
1
07/02/2010:48
107-06-2
ND
ug/L
1.0
0.24
1
07/02/2010:48
75-35-4
ND
ug/L
1.0
0.29
1
07/02/2010:48
156-59-2
ND
ug/L
1.0
0.25
1
07/02/2010:48
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH,IK,v1
IK
v2
Page 28 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Sample: SW-2 Lab ID: 92484100012 Collected: 06/26/20 15:18 Received: 06/30/20 09:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/07/2020 01:52 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.19
1
07/02/2010:48
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 10:48
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/2010:48
10061-02-6
ND
ug/L
150
56.2
1
07/02/2010:48
123-91-1
ND
ug/L
1.0
0.26
1
07/02/2010:48
100-41-4
ND
ug/L
5.0
0.57
1
07/02/2010:48
591-78-6
ND
ug/L
20.0
12.5
1
07/02/2010:48
74-88-4
ND
ug/L
5.0
3.7
1
07/02/2010:48
75-09-2
ND
ug/L
5.0
4.5
1
07/02/2010:48
108-10-1
ND
ug/L
1.0
0.27
1
07/02/2010:48
100-42-5
ND
ug/L
1.0
0.34
1
07/02/2010:48
630-20-6
ND
ug/L
1.0
0.22
1
07/02/2010:48
79-34-5
ND
ug/L
1.0
0.16
1
07/02/2010:48
127-18-4
ND
ug/L
1.0
0.24
1
07/02/2010:48
108-88-3
ND
ug/L
1.0
0.18
1
07/02/2010:48
71-55-6
ND
ug/L
1.0
0.24
1
07/02/2010:48
79-00-5
ND
ug/L
1.0
0.22
1
07/02/2010:48
79-01-6
ND
ug/L
1.0
0.31
1
07/02/2010:48
75-69-4
ND
ug/L
1.0
0.35
1
07/02/2010:48
96-18-4
ND
ug/L
2.0
1.4
1
07/02/2010:48
108-05-4
ND
ug/L
1.0
0.24
1
07/02/2010:48
75-01-4
ND
ug/L
1.0
0.63
1
07/02/2010:48
1330-20-7
97
%
70-130
1
07/02/2010:48
460-00-4
100
%
70-130
1
07/02/2010:48
17060-07-0
100
%
70-130
1
07/02/2010:48
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 29 of 47
lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
QC Batch: 550618 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92484100001, 92484100002, 92484100003, 92484100004, 92484100005, 92484100006, 92484100007,
92484100008,92484100009,92484100010,92484100011,92484100012
METHOD BLANK: 2927226 Matrix: Water
Associated Lab Samples: 92484100001, 92484100002, 92484100003, 92484100004, 92484100005, 92484100006, 92484100007,
92484100008,92484100009,92484100010,92484100011,92484100012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony
ug/L
ND
5.0
3.0
07/02/20 00:55
Arsenic
ug/L
4.8J
10.0
4.7
07/02/20 00:55 BC
Barium
ug/L
ND
5.0
3.5
07/02/20 00:55
Beryllium
ug/L
ND
1.0
0.70
07/02/20 00:55
Cadmium
ug/L
ND
1.0
0.40
07/02/20 00:55
Chromium
ug/L
ND
5.0
3.7
07/02/20 00:55
Cobalt
ug/L
ND
5.0
3.6
07/02/20 00:55
Copper
ug/L
ND
5.0
4.3
07/02/20 00:55
Lead
ug/L
ND
5.0
4.5
07/02/20 00:55
Nickel
ug/L
ND
5.0
3.5
07/02/20 00:55
Selenium
ug/L
ND
10.0
4.7
07/02/20 00:55
Silver
ug/L
ND
5.0
2.5
07/02/20 00:55
Vanadium
ug/L
ND
5.0
3.9
07/02/20 00:55
Zinc
ug/L
ND
10.0
9.5
07/02/20 00:55
LABORATORY CONTROL SAMPLE: 2927227
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Antimony
ug/L
500
483
97
80-120
Arsenic
ug/L
500
476
95
80-120 BC
Barium
ug/L
500
491
98
80-120
Beryllium
ug/L
500
488
98
80-120
Cadmium
ug/L
500
492
98
80-120
Chromium
ug/L
500
504
101
80-120
Cobalt
ug/L
500
485
97
80-120
Copper
ug/L
500
509
102
80-120
Lead
ug/L
500
489
98
80-120
Nickel
ug/L
500
496
99
80-120
Selenium
ug/L
500
471
94
80-120
Silver
ug/L
250
240
96
80-120
Vanadium
ug/L
500
494
99
80-120
Zinc
ug/L
500
456
91
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry Cloed LF-Elkin
92484100
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2927228
2927229
MS
MSD
92483975001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
513
512
103
102
75-125
0
20
Arsenic
ug/L
ND
500
500
509
510
102
102
75-125
0
20 BC
Barium
ug/L
9.2
500
500
524
529
103
104
75-125
1
20
Beryllium
ug/L
ND
500
500
512
518
102
104
75-125
1
20
Cadmium
ug/L
ND
500
500
528
529
106
106
75-125
0
20
Chromium
ug/L
ND
500
500
533
543
107
109
75-125
2
20
Cobalt
ug/L
ND
500
500
509
509
102
102
75-125
0
20
Copper
ug/L
ND
500
500
535
543
107
109
75-125
2
20
Lead
ug/L
ND
500
500
516
516
103
103
75-125
0
20
Nickel
ug/L
ND
500
500
520
520
104
104
75-125
0
20
Selenium
ug/L
ND
500
500
526
532
105
106
75-125
1
20
Silver
ug/L
ND
250
250
257
261
103
105
75-125
2
20
Vanadium
ug/L
ND
500
500
524
532
105
106
75-125
1
20
Zinc
ug/L
ND
500
500
489
489
98
98
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
QC Batch: 550619 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92484100001, 92484100002, 92484100003, 92484100004, 92484100005, 92484100006, 92484100007,
92484100008,92484100009,92484100010,92484100011,92484100012
METHOD BLANK: 2927230 Matrix: Water
Associated Lab Samples: 92484100001, 92484100002, 92484100003, 92484100004, 92484100005, 92484100006, 92484100007,
92484100008,92484100009,92484100010,92484100011,92484100012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.10 0.050 07/01/2017:05
LABORATORY CONTROL SAMPLE: 2927231
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.9 109 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2927232 2927233
MS MSD
92484100001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 10.7 10.7 107 107 75-125 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
QC Batch: 550892 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92484100001, 92484100002, 92484100003, 92484100004, 92484100005
METHOD BLANK: 2928458 Matrix: Water
Associated Lab Samples: 92484100001, 92484100002, 92484100003, 92484100004, 92484100005
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
07/02/20 02:10
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
07/02/20 02:10
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
07/02/20 02:10
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
07/02/20 02:10
1,1-Dichloroethane
ug/L
ND
1.0
0.27
07/02/20 02:10
1,1-Dichloroethene
ug/L
ND
1.0
0.24
07/02/20 02:10
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
07/02/20 02:10
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
07/02/20 02:10
1,2-Dichloroethane
ug/L
ND
1.0
0.34
07/02/20 02:10
1,2-Dichloropropene
ug/L
ND
1.0
0.19
07/02/20 02:10
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
07/02/20 02:10
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
07/02/20 02:10
2-Butanone (MEK)
ug/L
ND
5.0
3.3
07/02/20 02:10
2-Hexanone
ug/L
ND
5.0
0.57
07/02/20 02:10
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
07/02/20 02:10
Acetone
ug/L
ND
25.0
6.2
07/02/20 02:10
Acrylonitrile
ug/L
ND
10.0
0.90
07/02/20 02:10
Benzene
ug/L
ND
1.0
0.15
07/02/20 02:10
Bromochloromethane
ug/L
ND
1.0
0.34
07/02/20 02:10
Bromodichloromethane
ug/L
ND
1.0
0.26
07/02/20 02:10
Bromoform
ug/L
ND
1.0
0.62
07/02/20 02:10
Bromomethane
ug/L
ND
2.0
0.62
07/02/20 02:10
Carbon disulfide
ug/L
ND
2.0
0.40
07/02/20 02:10
Carbon tetrachloride
ug/L
ND
1.0
0.22
07/02/20 02:10
Chlorobenzene
ug/L
ND
1.0
0.23
07/02/20 02:10
Chloroethane
ug/L
ND
1.0
0.49
07/02/20 02:10
Chloroform
ug/L
ND
5.0
2.3
07/02/20 02:10
Chloromethane
ug/L
ND
1.0
0.39
07/02/20 02:10
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
07/02/20 02:10
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
07/02/20 02:10
Dibromochloromethane
ug/L
ND
1.0
0.41
07/02/20 02:10
Dibromomethane
ug/L
ND
1.0
0.46
07/02/20 02:10
Ethylbenzene
ug/L
ND
1.0
0.26
07/02/20 02:10
lodomethane
ug/L
ND
20.0
12.5
07/02/20 02:10
Methylene Chloride
ug/L
ND
5.0
3.7
07/02/20 02:10
Styrene
ug/L
ND
1.0
0.27
07/02/20 02:10
Tetrachloroethene
ug/L
ND
1.0
0.16
07/02/20 02:10
Toluene
ug/L
ND
1.0
0.24
07/02/20 02:10
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
07/02/20 02:10
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
07/02/20 02:10
Qualifiers
IH,IK,v1
IK
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
METHOD BLANK: 2928458
Matrix:
Water
Associated Lab Samples:
92484100001, 92484100002, 92484100003, 92484100004, 92484100005
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
07/02/20 02:10
Trichloroethene
ug/L
ND
1.0
0.22
07/02/20 02:10
Trichlorofluoromethane
ug/L
ND
1.0
0.31
07/02/20 02:10
Vinyl acetate
ug/L
ND
2.0
1.4
07/02/20 02:10
Vinyl chloride
ug/L
ND
1.0
0.24
07/02/20 02:10
Xylene (Total)
ug/L
ND
1.0
0.63
07/02/20 02:10
1,2-Dichloroethane-d4 (S)
%
100
70-130
07/02/20 02:10
4-Bromofluorobenzene (S)
%
97
70-130
07/02/20 02:10
Toluene-d8 (S)
%
97
70-130
07/02/20 02:10
LABORATORY CONTROL SAMPLE: 2928459
Parameter
Qualifiers
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
51.5
103
70-130
1,1,1-Trichloroethane
ug/L
50
56.1
112
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.9
102
70-130
1,1,2-Trichloroethane
ug/L
50
51.6
103
70-130
1,1-Dichloroethane
ug/L
50
52.8
106
70-130
1,1-Dichloroethene
ug/L
50
57.1
114
70-130
1,2,3-Trichloropropane
ug/L
50
51.7
103
70-130
1,2-Dichlorobenzene
ug/L
50
52.8
106
70-130
1,2-Dichloroethane
ug/L
50
50.6
101
70-130
1,2-Dichloropropane
ug/L
50
53.0
106
70-130
1,4-Dichlorobenzene
ug/L
50
51.6
103
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1040
104
59-169
2-Butanone (MEK)
ug/L
100
88.3
88
64-135
2-Hexanone
ug/L
100
91.3
91
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
94.7
95
70-130
Acetone
ug/L
100
101
101
61-157
Acrylonitrile
ug/L
250
232
93
61-143
Benzene
ug/L
50
53.7
107
70-130
Bromochloromethane
ug/L
50
55.4
111
70-130
Bromodichloromethane
ug/L
50
47.7
95
70-130
Bromoform
ug/L
50
51.0
102
70-130
Bromomethane
ug/L
50
61.4
123
38-1301H,IK,v1
Carbon disulfide
ug/L
50
53.7
107
68-130
Carbon tetrachloride
ug/L
50
55.9
112
70-130
Chlorobenzene
ug/L
50
51.7
103
70-130
Chloroethane
ug/L
50
43.6
87
37-142 IK
Chloroform
ug/L
50
51.1
102
70-130
Chloromethane
ug/L
50
39.5
79
48-130 v3
cis-1,2-Dichloroethene
ug/L
50
52.0
104
70-130
cis-1,3-Dichloropropene
ug/L
50
55.3
111
70-130
Dibromochloromethane
ug/L
50
52.3
105
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
LABORATORY CONTROL SAMPLE:
2928459
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Dibromomethane
ug/L
50
54.4
109
70-130
Ethylbenzene
ug/L
50
51.9
104
70-130
lodomethane
ug/L
100
101
101
40-130
Methylene Chloride
ug/L
50
47.8
96
67-132
Styrene
ug/L
50
53.9
108
70-130
Tetrachloroethene
ug/L
50
53.5
107
69-130
Toluene
ug/L
50
53.4
107
70-130
trans-1,2-Dichloroethene
ug/L
50
55.5
111
70-130
trans- 1,3-Dichloropropene
ug/L
50
53.1
106
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
46.6
93
35-189
Trichloroethene
ug/L
50
54.3
109
70-130
Trichlorofluoromethane
ug/L
50
51.7
103
63-130
Vinyl acetate
ug/L
100
97.6
98
55-143
Vinyl chloride
ug/L
50
46.8
94
70-131
Xylene (Total)
ug/L
150
158
105
70-130
1,2-Dichloroethane-d4 (S)
%
92
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE SAMPLE:
2928460
92484100004
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.0
100
73-134
1,1,1-Trichloroethane
ug/L
ND
20
17.7
88
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.7
98
70-136
1,1,2-Trichloroethane
ug/L
ND
20
17.7
89
70-135
1,1-Dichloroethane
ug/L
0.46J
20
18.1
88
70-139
1,1-Dichloroethene
ug/L
ND
20
18.7
94
70-154
1,2,3-Trichloropropane
ug/L
ND
20
20.4
102
71-137
1,2-Dichlorobenzene
ug/L
2.1
20
20.5
92
70-133
1,2-Dichloroethane
ug/L
ND
20
15.5
78
70-137
1,2-Dichloropropane
ug/L
ND
20
17.9
89
70-140
1,4-Dichlorobenzene
ug/L
ND
20
21.6
108
70-133
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
386
97
53-168
2-Butanone (MEK)
ug/L
ND
40
36.2
90
60-139
2-Hexanone
ug/L
ND
40
43.7
109
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
34.9
87
65-135
Acetone
ug/L
ND
40
40.8
102
60-148
Acrylonitrile
ug/L
ND
100
89.1
89
64-147
Benzene
ug/L
ND
20
19.1
95
70-151
Bromochloromethane
ug/L
ND
20
18.5
92
70-141
Bromodichloromethane
ug/L
ND
20
16.3
81
70-138
Bromoform
ug/L
ND
20
17.5
87
63-130 v1
Bromomethane
ug/L
ND
20
22.4
112
15-152 IH
Carbon disulfide
ug/L
ND
20
18.6
93
69-149
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
MATRIX SPIKE SAMPLE:
Parameter
2928460
Units
92484100004
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Carbon tetrachloride
ug/L
ND
20
19.0
95
70-143
Chlorobenzene
ug/L
ND
20
21.6
108
70-138
Chloroethane
ug/L
ND
20
17.0
85
52-163
Chloroform
ug/L
ND
20
17.2
86
70-139
Chloromethane
ug/L
ND
20
13.9
70
41-139 v3
cis-1,2-Dichloroethene
ug/L
5.3
20
21.5
81
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
19.4
97
70-137
Dibromochloromethane
ug/L
ND
20
19.3
97
70-134
Dibromomethane
ug/L
ND
20
20.5
103
70-138
Ethylbenzene
ug/L
ND
20
20.1
100
66-153
lodomethane
ug/L
ND
40
30.2
75
20-138 v3
Methylene Chloride
ug/L
ND
20
17.0
85
42-159
Styrene
ug/L
ND
20
19.1
96
70-135
Tetrachloroethene
ug/L
ND
20
20.9
104
59-143
Toluene
ug/L
ND
20
17.9
90
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
17.7
89
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
18.6
93
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
16.2
81
47-1351K
Trichloroethene
ug/L
ND
20
19.0
95
70-147
Trichlorofluoromethane
ug/L
ND
20
15.1
75
70-148
Vinyl acetate
ug/L
ND
40
34.4
86
49-151
Vinyl chloride
ug/L
ND
20
16.0
80
70-156
Xylene (Total)
ug/L
ND
60
61.0
102
63-158
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 2928461
Parameter
Units
92484100005
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
SAMPLE DUPLICATE: 2928461
Parameter
Units
92484100005
Result
Dup
Result
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
101
107
4-Bromofluorobenzene (S)
%
99
100
Toluene-d8(S)
%
100
98
Max
RPD RPD
Qualifiers
30
30
30
30
30
30 v1
30
30
30
30
30
30
30 I H, v2
30
30
30
30
30
30 v2
30
30
30
30
30
30
30 I K
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC.
Page 37 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
QC Batch: 550893 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92484100006,92484100007,92484100008,92484100009,92484100010,92484100011,92484100012
METHOD BLANK: 2928462 Matrix: Water
Associated Lab Samples: 92484100006,92484100007,92484100008,92484100009,92484100010,92484100011,92484100012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
07/02/20 02:28
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
07/02/20 02:28
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
07/02/20 02:28
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
07/02/20 02:28
1,1-Dichloroethane
ug/L
ND
1.0
0.27
07/02/20 02:28
1,1-Dichloroethene
ug/L
ND
1.0
0.24
07/02/20 02:28
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
07/02/20 02:28
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
07/02/20 02:28
1,2-Dichloroethane
ug/L
ND
1.0
0.34
07/02/20 02:28
1,2-Dichloropropene
ug/L
ND
1.0
0.19
07/02/20 02:28
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
07/02/20 02:28
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
07/02/20 02:28
2-Butanone (MEK)
ug/L
ND
5.0
3.3
07/02/20 02:28
2-Hexanone
ug/L
ND
5.0
0.57
07/02/20 02:28
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
07/02/20 02:28
Acetone
ug/L
ND
25.0
6.2
07/02/20 02:28
Acrylonitrile
ug/L
ND
10.0
0.90
07/02/20 02:28
Benzene
ug/L
ND
1.0
0.15
07/02/20 02:28
Bromochloromethane
ug/L
ND
1.0
0.34
07/02/20 02:28
Bromodichloromethane
ug/L
ND
1.0
0.26
07/02/20 02:28
Bromoform
ug/L
ND
1.0
0.62
07/02/20 02:28
Bromomethane
ug/L
ND
2.0
0.62
07/02/20 02:28
Carbon disulfide
ug/L
ND
2.0
0.40
07/02/20 02:28
Carbon tetrachloride
ug/L
ND
1.0
0.22
07/02/20 02:28
Chlorobenzene
ug/L
ND
1.0
0.23
07/02/20 02:28
Chloroethane
ug/L
ND
1.0
0.49
07/02/20 02:28
Chloroform
ug/L
ND
5.0
2.3
07/02/20 02:28
Chloromethane
ug/L
ND
1.0
0.39
07/02/20 02:28
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
07/02/20 02:28
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
07/02/20 02:28
Dibromochloromethane
ug/L
ND
1.0
0.41
07/02/20 02:28
Dibromomethane
ug/L
ND
1.0
0.46
07/02/20 02:28
Ethylbenzene
ug/L
ND
1.0
0.26
07/02/20 02:28
lodomethane
ug/L
ND
20.0
12.5
07/02/20 02:28
Methylene Chloride
ug/L
ND
5.0
3.7
07/02/20 02:28
Styrene
ug/L
ND
1.0
0.27
07/02/20 02:28
Tetrachloroethene
ug/L
ND
1.0
0.16
07/02/20 02:28
Toluene
ug/L
ND
1.0
0.24
07/02/20 02:28
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
07/02/20 02:28
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
07/02/20 02:28
IH,IK,v1
IK
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
METHOD BLANK: 2928462 Matrix: Water
Associated Lab Samples: 92484100006,92484100007,92484100008,92484100009,92484100010,92484100011,92484100012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
07/02/20 02:28
Trichloroethene
ug/L
ND
1.0
0.22
07/02/20 02:28
Trichlorofluoromethane
ug/L
ND
1.0
0.31
07/02/20 02:28
Vinyl acetate
ug/L
ND
2.0
1.4
07/02/20 02:28
Vinyl chloride
ug/L
ND
1.0
0.24
07/02/20 02:28
Xylene (Total)
ug/L
ND
1.0
0.63
07/02/20 02:28
1,2-Dichloroethane-d4 (S)
%
100
70-130
07/02/20 02:28
4-Bromofluorobenzene (S)
%
99
70-130
07/02/20 02:28
Toluene-d8 (S)
%
97
70-130
07/02/20 02:28
LABORATORY CONTROL SAMPLE: 2928463
Parameter
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.6
101
70-130
1,1,1-Trichloroethane
ug/L
50
53.8
108
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.2
102
70-130
1,1,2-Trichloroethane
ug/L
50
52.2
104
70-130
1,1-Dichloroethane
ug/L
50
50.2
100
70-130
1,1-Dichloroethene
ug/L
50
55.3
111
70-130
1,2,3-Trichloropropane
ug/L
50
50.2
100
70-130
1,2-Dichlorobenzene
ug/L
50
52.4
105
70-130
1,2-Dichloroethane
ug/L
50
48.8
98
70-130
1,2-Dichloropropane
ug/L
50
51.8
104
70-130
1,4-Dichlorobenzene
ug/L
50
51.7
103
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1080
108
59-169
2-Butanone (MEK)
ug/L
100
89.0
89
64-135
2-Hexanone
ug/L
100
93.9
94
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
96.5
96
70-130
Acetone
ug/L
100
102
102
61-157
Acrylonitrile
ug/L
250
229
91
61-143
Benzene
ug/L
50
52.3
105
70-130
Bromochloromethane
ug/L
50
55.1
110
70-130
Bromodichloromethane
ug/L
50
48.5
97
70-130
Bromoform
ug/L
50
51.5
103
70-130
Bromomethane
ug/L
50
62.7
125
38-1301H,IK,v1
Carbon disulfide
ug/L
50
51.0
102
68-130
Carbon tetrachloride
ug/L
50
54.2
108
70-130
Chlorobenzene
ug/L
50
50.2
100
70-130
Chloroethane
ug/L
50
41.4
83
37-142 IK
Chloroform
ug/L
50
51.3
103
70-130
Chloromethane
ug/L
50
38.4
77
48-130 v3
cis-1,2-Dichloroethene
ug/L
50
50.5
101
70-130
cis-1,3-Dichloropropene
ug/L
50
55.1
110
70-130
Dibromochloromethane
ug/L
50
51.4
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
LABORATORY CONTROL SAMPLE:
2928463
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Dibromomethane
ug/L
50
55.5
111
70-130
Ethylbenzene
ug/L
50
50.8
102
70-130
lodomethane
ug/L
100
96.6
97
40-130
Methylene Chloride
ug/L
50
46.2
92
67-132
Styrene
ug/L
50
52.8
106
70-130
Tetrachloroethene
ug/L
50
51.6
103
69-130
Toluene
ug/L
50
52.4
105
70-130
trans-1,2-Dichloroethene
ug/L
50
53.1
106
70-130
trans- 1,3-Dichloropropene
ug/L
50
53.5
107
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
46.6
93
35-189
Trichloroethene
ug/L
50
53.4
107
70-130
Trichlorofluoromethane
ug/L
50
49.7
99
63-130
Vinyl acetate
ug/L
100
94.9
95
55-143
Vinyl chloride
ug/L
50
46.1
92
70-131
Xylene (Total)
ug/L
150
155
104
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE SAMPLE:
2928464
92484340003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
15.2
76
73-134
1,1,1-Trichloroethane
ug/L
ND
20
14.8
74
82-143 M1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
16.0
80
70-136
1,1,2-Trichloroethane
ug/L
ND
20
14.7
74
70-135
1,1-Dichloroethane
ug/L
ND
20
15.0
75
70-139
1,1-Dichloroethene
ug/L
ND
20
15.9
79
70-154
1,2,3-Trichloropropane
ug/L
ND
20
17.2
86
71-137
1,2-Dichlorobenzene
ug/L
ND
20
15.4
77
70-133
1,2-Dichloroethane
ug/L
ND
20
12.7
63
70-137 M1
1,2-Dichloropropane
ug/L
ND
20
14.4
72
70-140
1,4-Dichlorobenzene
ug/L
ND
20
14.8
74
70-133
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
379
95
53-168
2-Butanone (MEK)
ug/L
ND
40
31.7
79
60-139
2-Hexanone
ug/L
ND
40
40.1
100
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
31.0
77
65-135
Acetone
ug/L
ND
40
35.0
88
60-148
Acrylonitrile
ug/L
ND
100
80.3
80
64-147
Benzene
ug/L
ND
20
15.5
78
70-151
Bromochloromethane
ug/L
ND
20
15.8
79
70-141
Bromodichloromethane
ug/L
ND
20
12.9
64
70-138 M1
Bromoform
ug/L
ND
20
17.8
89
63-130 v1
Bromomethane
ug/L
ND
20
20.7
104
15-152 IH
Carbon disulfide
ug/L
ND
20
14.4
72
69-149
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
MATRIX SPIKE SAMPLE:
Parameter
2928464
Units
92484340003
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Carbon tetrachloride
ug/L
ND
20
15.1
76
70-143
Chlorobenzene
ug/L
ND
20
15.6
78
70-138
Chloroethane
ug/L
ND
20
13.1
66
52-163
Chloroform
ug/L
ND
20
13.5
68
70-139 M1
Chloromethane
ug/L
ND
20
11.4
57
41-139 v3
cis-1,2-Dichloroethene
ug/L
ND
20
14.3
71
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
15.7
79
70-137
Dibromochloromethane
ug/L
ND
20
16.1
80
70-134
Dibromomethane
ug/L
ND
20
16.5
82
70-138
Ethylbenzene
ug/L
ND
20
15.1
75
66-153
lodomethane
ug/L
ND
40
26.4
66
20-138 v3
Methylene Chloride
ug/L
ND
20
13.8
69
42-159
Styrene
ug/L
ND
20
14.6
73
70-135
Tetrachloroethene
ug/L
ND
20
16.9
85
59-143
Toluene
ug/L
ND
20
14.1
70
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
14.8
74
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
14.9
75
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
13.3
66
47-1351K
Trichloroethene
ug/L
ND
20
14.9
74
70-147
Trichlorofluoromethane
ug/L
ND
20
11.9
59
70-148 M1
Vinyl acetate
ug/L
ND
40
28.6
71
49-151
Vinyl chloride
ug/L
ND
20
12.5
62
70-156 M1
Xylene (Total)
ug/L
ND
60
46.4
77
63-158
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
93
70-130
SAMPLE DUPLICATE: 2928465
Parameter
Units
92484340007
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 47
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
SAMPLE DUPLICATE: 2928465
Parameter
Units
92484340007
Result
Dup
Result
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
102
108
4-Bromofluorobenzene (S)
%
97
97
Toluene-d8(S)
%
98
102
Max
RPD RPD Qualifiers
30
30
30
30
30
30 v1
30 I H
30
30
30
30
30
30 v2
30
30
30
30
30
30 v2
30
30
30
30
30
30
30 I K
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC.
Page 42 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALIFIERS
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 47
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Surry Cloed LF-Elkin
Pace Project No.: 92484100
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92484100001
MW-1
EPA 3010A
550618
EPA 6010D
550620
92484100002
MW-2
EPA 3010A
550618
EPA 6010D
550620
92484100003
MW-3
EPA 3010A
550618
EPA 6010D
550620
92484100004
MW-3A
EPA 3010A
550618
EPA 6010D
550620
92484100005
MW-4
EPA 3010A
550618
EPA 6010D
550620
92484100006
MW-5
EPA 3010A
550618
EPA 6010D
550620
92484100007
MW-6
EPA 3010A
550618
EPA 6010D
550620
92484100008
MW-7D
EPA 3010A
550618
EPA 6010D
550620
92484100009
MW-7S
EPA 3010A
550618
EPA 6010D
550620
92484100010
MW-8
EPA 3010A
550618
EPA 6010D
550620
92484100011
SW-1
EPA 3010A
550618
EPA 6010D
550620
92484100012
SW-2
EPA 3010A
550618
EPA 6010D
550620
92484100001
MW-1
EPA 3010A
550619
EPA 6020B
550623
92484100002
MW-2
EPA 3010A
550619
EPA 6020B
550623
92484100003
MW-3
EPA 3010A
550619
EPA 6020B
550623
92484100004
MW-3A
EPA 3010A
550619
EPA 6020B
550623
92484100005
MW-4
EPA 3010A
550619
EPA 6020B
550623
92484100006
MW-5
EPA 3010A
550619
EPA 6020B
550623
92484100007
MW-6
EPA 3010A
550619
EPA 6020B
550623
92484100008
MW-7D
EPA 3010A
550619
EPA 6020B
550623
92484100009
MW-7S
EPA 3010A
550619
EPA 6020B
550623
92484100010
MW-8
EPA 3010A
550619
EPA 6020B
550623
92484100011
SW-1
EPA 3010A
550619
EPA 6020B
550623
92484100012
SW-2
EPA 3010A
550619
EPA 6020B
550623
92484100001
MW-1
EPA 8260D
550892
92484100002
MW-2
EPA 8260D
550892
92484100003
MW-3
EPA 8260D
550892
92484100004
MW-3A
EPA 8260D
550892
92484100005
MW-4
EPA 8260D
550892
92484100006
MW-5
EPA 8260D
550893
92484100007
MW-6
EPA 8260D
550893
92484100008
MW-7D
EPA 8260D
550893
92484100009
MW-7S
EPA 8260D
550893
92484100010
MW-8
EPA 8260D
550893
92484100011
SW-1
EPA 8260D
550893
92484100012
SW-2
EPA 8260D
550893
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/07/2020 01:52 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 47
Document Name:
Document Revised: February 7, 2018
9
93ce
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
Analytical
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Htantersvill Raleigh[] Mechanicsville[]
Sample.Client Name:
,r A Project #: WO# : 92484100
Courier,, []Fed Ex ❑UPS ❑USPS OClient 111111
❑ Commercial Y❑Pace ❑Other:
924841O0
Custody Seal Present? ❑Yes ❑No Seals Intact? ❑Yes pNo
DatellniValsPersanExaminingfontents: r�
Packing Material: ❑aubble Wrap fTftbbie Sags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes [:]No�/A
_&Ft Gun ID: 92�TO61 Type of Ice: wet ❑Slue ❑None
Cooler Temp ('C): l Correction Factor: Add/Subtract ('C) +0.l
c� Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): ] ❑samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil (P�J- N/A, water sample)
Did samples originate in a quarantine zone %vithin the United States: CA, HY, nr SC (check maps)? Did sarnoesorigsnate from a foreign source (internationally,
r-r., cr:
[]Yes kjNo
fncrumngnewdu aiiu rUtI w n ., u — s "-
Corn men ts/DIscre ancy:
Chain of Custody Present? ,❑Yes ❑Na ❑N/A
1.
Samples Arrived within Hold Time? QYeS QNO ❑N/A
2.
Short Hold Tlme Analysis (<72 hr.)? ❑Yes E%o []N/A
3.
Rush Turn Around Time Requested? ❑Yes �96 ❑N/A
4.
Sufficient Volume? Dyes ❑No ❑NIA
5.
Correct Containers Used? 'O,yes ❑No []N/A
6.
-Pace Containers Used? res ❑No ❑N/A
T
Containers Intact? 'LIT_ ONO ❑NIA
7.
Dissolved analysis: Samples Field Filtered? []yes ❑No $N/A
8-
C Yes 171110 N A
9.
Includes DatelTime/ID/Analysls Matrk
Heads ace in VOA Vials (>S-6mm)? ❑Yes o ❑N/A
10.
Trip Blank Present? []yes E]go— []N/A
11.
Trip Blank Custody Seals Present? []Yes ❑No _EJ91A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of spit containers:
CLIENT NOTIFICATION/RE50LUTION
Field Data Required? ❑Ye5 []No
Person contacted: Datefiime:
Project Manager SCURF Review,, i r l YJ Date:
Project Manager SRF Review: hate:
Page 45 of 47
GBAnafy1fc3i
Document Name:
Sample Condition Upon Retef t(SCJA)
Ncurnent Revised: February 7, 2018
Page 1 of 2
Document Na.:
F-CAR-CS-033-Rev.06
lSSUing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Conform, TOC, oil and Grease, ORO/8015 {water} DOC, ILHg
**Bottom half of box is to list number of bottle
Project # W0# ; 92484100
PH: RMB Due CLIENT: 82-Municipal
paDafe: 07/16/20
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pH Adjustment Log for Preserved Samples
Sample ID I Type of Preservative pH upon receipt Date preservation adjusted Time preservallan Amount of Preservative Lot k
adjusted d led I
Note: Whenever there Is a dlscrepanry affecting North Carolina compilance samples, a copy of this form will be sent to the North Carolina DEHNA Certification Office (i.e.
out of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 46 of 47
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lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
July 02, 2020
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry Blanks
Pace Project No.: 92483826
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 26, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Steven R. Gandy, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
r
e
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without the written consent of Pace Analytical Services, LLC.
Page 1 of 20
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Surry Blanks
Pace Project No.: 92483826
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE SUMMARY
Project: Surry Blanks
Pace Project No.: 92483826
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92483826001
92483826002
EB
FIB
Water
Water
06/25/2015:50
06/25/2015:52
06/26/20 14:41
06/26/20 14:41
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project: Surry Blanks
Pace Project No.: 92483826
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92483826001 EB
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
CL
51
PASI-C
92483826002 FIB
EPA 6010D
SH1
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
CL
51
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92483826
Sample: EB
Lab ID:
92483826001
Collected:
06/25/20
15:50
Received: 06/26/20 14:41 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 6010D
Preparation Method: EPA 3010A
Pace Analytical
Services
-Asheville
Antimony
ND
ug/L
5.0
3.0
1
06/30/20 00:35
07/01/20 01:02
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/30/20 00:35
07/01/20 01:02
7440-38-2
Barium
ND
ug/L
5.0
3.5
1
06/30/20 00:35
07/01/20 01:02
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
06/30/20 00:35
07/01/20 01:02
7440-41-7
Cadmium
0.47J
ug/L
1.0
0.40
1
06/30/20 00:35
07/01/20 01:02
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
06/30/20 00:35
07/01/20 01:02
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
06/30/20 00:35
07/01/20 01:02
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
06/30/20 00:35
07/01/20 01:02
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
06/30/20 00:35
07/01/20 01:02
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
06/30/20 00:35
07/01/20 01:02
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/30/20 00:35
07/01/20 01:02
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/30/20 00:35
07/01/20 01:02
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
06/30/20 00:35
07/01/20 01:02
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
06/30/20 00:35
07/01/20 01:02
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method: EPA 3010A
Pace Analytical
Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
06/30/20 00:13
06/30/20 14:38
7440-28-0
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Acetone
ND
ug/L
25.0
6.2
1
07/02/20 04:11
67-64-1
Acrylonitrile
ND
ug/L
10.0
0.90
1
07/02/20 04:11
107-13-1
Benzene
ND
ug/L
1.0
0.15
1
07/02/20 04:11
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.34
1
07/02/20 04:11
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.26
1
07/02/20 04:11
75-27-4
Bromoform
ND
ug/L
1.0
0.62
1
07/02/20 04:11
75-25-2
Bromomethane
ND
ug/L
2.0
0.62
1
07/02/20 04:11
74-83-9 IK
2-Butanone (MEK)
ND
ug/L
5.0
3.3
1
07/02/20 04:11
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.40
1
07/02/20 04:11
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.22
1
07/02/20 04:11
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.23
1
07/02/20 04:11
108-90-7
Chloroethane
ND
ug/L
1.0
0.49
1
07/02/20 04:11
75-00-3
Chloroform
ND
ug/L
5.0
2.3
1
07/02/20 04:11
67-66-3
Chloromethane
ND
ug/L
1.0
0.39
1
07/02/20 04:11
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
0.26
1
07/02/20 04:11
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.41
1
07/02/20 04:11
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.26
1
07/02/20 04:11
106-93-4
Dibromomethane
ND
ug/L
1.0
0.46
1
07/02/20 04:11
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.29
1
07/02/20 04:11
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.26
1
07/02/20 04:11
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.54
1
07/02/20 04:11
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.27
1
07/02/20 04:11
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.34
1
07/02/20 04:11
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.24
1
07/02/20 04:11
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20
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ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92483826
Sample: EB Lab ID: 92483826001 Collected: 06/25/20 15:50 Received: 06/26/20 14:41 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/02/2020 04:47 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.29
1
07/02/20 04:11
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 04:11
156-60-5
ND
ug/L
1.0
0.19
1
07/02/20 04:11
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 04:11
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 04:11
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 04:11
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 04:11
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 04:11
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 04:11
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 04:11
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 04:11
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 04:11
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 04:11
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 04:11
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 04:11
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 04:11
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 04:11
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 04:11
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 04:11
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 04:11
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 04:11
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 04:11
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 04:11
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 04:11
1330-20-7
93
%
70-130
1
07/02/20 04:11
460-00-4
90
%
70-130
1
07/02/20 04:11
17060-07-0
99
%
70-130
1
07/02/20 04:11
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92483826
Sample: FIB
Lab ID:
92483826002
Collected:
06/25/20
15:52
Received: 06/26/20 14:41 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 6010D
Preparation Method: EPA 3010A
Pace Analytical
Services
-Asheville
Antimony
ND
ug/L
5.0
3.0
1
06/30/20 00:35
07/01/20 01:05
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/30/20 00:35
07/01/20 01:05
7440-38-2
Barium
ND
ug/L
5.0
3.5
1
06/30/20 00:35
07/01/20 01:05
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
06/30/20 00:35
07/01/20 01:05
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/30/20 00:35
07/01/20 01:05
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
06/30/20 00:35
07/01/20 01:05
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
06/30/20 00:35
07/01/20 01:05
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
06/30/20 00:35
07/01/20 01:05
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
06/30/20 00:35
07/01/20 01:05
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
06/30/20 00:35
07/01/20 01:05
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/30/20 00:35
07/01/20 01:05
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/30/20 00:35
07/01/20 01:05
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
06/30/20 00:35
07/01/20 01:05
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
06/30/20 00:35
07/01/20 01:05
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method: EPA 3010A
Pace Analytical
Services
-Asheville
Thallium
ND
ug/L
0.10
0.050
1
06/30/20 00:13
06/30/20 14:42
7440-28-0
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Acetone
ND
ug/L
25.0
6.2
1
07/02/20 04:29
67-64-1
Acrylonitrile
ND
ug/L
10.0
0.90
1
07/02/20 04:29
107-13-1
Benzene
ND
ug/L
1.0
0.15
1
07/02/20 04:29
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.34
1
07/02/20 04:29
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.26
1
07/02/20 04:29
75-27-4
Bromoform
ND
ug/L
1.0
0.62
1
07/02/20 04:29
75-25-2
Bromomethane
ND
ug/L
2.0
0.62
1
07/02/20 04:29
74-83-9 IK
2-Butanone (MEK)
ND
ug/L
5.0
3.3
1
07/02/20 04:29
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.40
1
07/02/20 04:29
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.22
1
07/02/20 04:29
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.23
1
07/02/20 04:29
108-90-7
Chloroethane
ND
ug/L
1.0
0.49
1
07/02/20 04:29
75-00-3
Chloroform
ND
ug/L
5.0
2.3
1
07/02/20 04:29
67-66-3
Chloromethane
ND
ug/L
1.0
0.39
1
07/02/20 04:29
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
0.26
1
07/02/20 04:29
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.41
1
07/02/20 04:29
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.26
1
07/02/20 04:29
106-93-4
Dibromomethane
ND
ug/L
1.0
0.46
1
07/02/20 04:29
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.29
1
07/02/20 04:29
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.26
1
07/02/20 04:29
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.54
1
07/02/20 04:29
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.27
1
07/02/20 04:29
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.34
1
07/02/20 04:29
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.24
1
07/02/20 04:29
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 20
lceAnalyircal
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Blanks
Pace Project No.: 92483826
Sample: FIB Lab ID: 92483826002 Collected: 06/25/20 15:52 Received: 06/26/20 14:41 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/02/2020 04:47 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.29
1
07/02/20 04:29
156-59-2
ND
ug/L
1.0
0.25
1
07/02/20 04:29
156-60-5
ND
ug/L
1.0
0.19
1
07/02/20 04:29
78-87-5
ND
ug/L
1.0
0.30
1
07/02/20 04:29
10061-01-5
ND
ug/L
1.0
0.31
1
07/02/20 04:29
10061-02-6
ND
ug/L
150
56.2
1
07/02/20 04:29
123-91-1
ND
ug/L
1.0
0.26
1
07/02/20 04:29
100-41-4
ND
ug/L
5.0
0.57
1
07/02/20 04:29
591-78-6
ND
ug/L
20.0
12.5
1
07/02/20 04:29
74-88-4
ND
ug/L
5.0
3.7
1
07/02/20 04:29
75-09-2
ND
ug/L
5.0
4.5
1
07/02/20 04:29
108-10-1
ND
ug/L
1.0
0.27
1
07/02/20 04:29
100-42-5
ND
ug/L
1.0
0.34
1
07/02/20 04:29
630-20-6
ND
ug/L
1.0
0.22
1
07/02/20 04:29
79-34-5
ND
ug/L
1.0
0.16
1
07/02/20 04:29
127-18-4
ND
ug/L
1.0
0.24
1
07/02/20 04:29
108-88-3
ND
ug/L
1.0
0.18
1
07/02/20 04:29
71-55-6
ND
ug/L
1.0
0.24
1
07/02/20 04:29
79-00-5
ND
ug/L
1.0
0.22
1
07/02/20 04:29
79-01-6
ND
ug/L
1.0
0.31
1
07/02/20 04:29
75-69-4
ND
ug/L
1.0
0.35
1
07/02/20 04:29
96-18-4
ND
ug/L
2.0
1.4
1
07/02/20 04:29
108-05-4
ND
ug/L
1.0
0.24
1
07/02/20 04:29
75-01-4
ND
ug/L
1.0
0.63
1
07/02/20 04:29
1330-20-7
95
%
70-130
1
07/02/20 04:29
460-00-4
89
%
70-130
1
07/02/20 04:29
17060-07-0
100
%
70-130
1
07/02/20 04:29
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 20
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92483826
QC Batch: 550337 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92483826001, 92483826002
METHOD BLANK: 2926131
Associated Lab Samples: 92483826001, 92483826002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
06/30/20 23:57
Arsenic
ug/L
ND
10.0
4.7
06/30/20 23:57
Barium
ug/L
ND
5.0
3.5
06/30/20 23:57
Beryllium
ug/L
ND
1.0
0.70
06/30/20 23:57
Cadmium
ug/L
ND
1.0
0.40
06/30/20 23:57
Chromium
ug/L
ND
5.0
3.7
07/01/2018:57
Cobalt
ug/L
ND
5.0
3.6
06/30/20 23:57
Copper
ug/L
ND
5.0
4.3
06/30/20 23:57
Lead
ug/L
ND
5.0
4.5
06/30/20 23:57
Nickel
ug/L
ND
5.0
3.5
06/30/20 23:57
Selenium
ug/L
ND
10.0
4.7
06/30/20 23:57
Silver
ug/L
ND
5.0
2.5
06/30/20 23:57
Vanadium
ug/L
ND
5.0
3.9
07/01/2018:57
Zinc
ug/L
ND
10.0
9.5
06/30/20 23:57
LABORATORY CONTROL SAMPLE:
Parameter
2926132
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
489
98
80-120
Arsenic
ug/L
500
492
98
80-120
Barium
ug/L
500
484
97
80-120
Beryllium
ug/L
500
470
94
80-120
Cadmium
ug/L
500
472
94
80-120
Chromium
ug/L
500
495
99
80-120
Cobalt
ug/L
500
473
95
80-120
Copper
ug/L
500
491
98
80-120
Lead
ug/L
500
478
96
80-120
Nickel
ug/L
500
472
94
80-120
Selenium
ug/L
500
481
96
80-120
Silver
ug/L
250
225
90
80-120
Vanadium
ug/L
500
499
100
80-120
Zinc
ug/L
500
442
88
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 20
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry Blanks
92483826
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926133
2926134
MS
MSD
92483926003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
512
507
102
101
75-125
1
20
Arsenic
ug/L
ND
500
500
524
517
105
103
75-125
1
20
Barium
ug/L
60.9
500
500
560
550
100
98
75-125
2
20
Beryllium
ug/L
ND
500
500
493
476
99
95
75-125
4
20
Cadmium
ug/L
ND
500
500
504
495
101
99
75-125
2
20
Chromium
ug/L
ND
500
500
515
ND
103
0
75-125
20 M1
Cobalt
ug/L
ND
500
500
495
483
99
97
75-125
2
20
Copper
ug/L
ND
500
500
500
496
100
99
75-125
1
20
Lead
ug/L
ND
500
500
494
488
99
98
75-125
1
20
Nickel
ug/L
ND
500
500
494
482
98
96
75-125
2
20
Selenium
ug/L
ND
500
500
533
530
107
106
75-125
1
20
Silver
ug/L
ND
250
250
237
232
95
93
75-125
2
20
Vanadium
ug/L
ND
500
500
513
ND
103
0
75-125
20 M1
Zinc
ug/L
ND
500
500
490
469
97
93
75-125
4
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 20
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92483826
QC Batch: 550340 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92483826001, 92483826002
METHOD BLANK: 2926143 Matrix: Water
Associated Lab Samples: 92483826001, 92483826002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.10 0.050 06/30/2013:04
LABORATORY CONTROL SAMPLE: 2926144
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.1 101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926145 2926146
MS MSD
92483822002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 10.1 10.3 100 102 75-125 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 20
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92483826
QC Batch: 550875 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92483826001, 92483826002
METHOD BLANK: 2928332
Associated Lab Samples: 92483826001, 92483826002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
07/02/20 00:15
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
07/02/20 00:15
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
07/02/20 00:15
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
07/02/20 00:15
1,1-Dichloroethane
ug/L
ND
1.0
0.27
07/02/20 00:15
1,1-Dichloroethene
ug/L
ND
1.0
0.24
07/02/20 00:15
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
07/02/20 00:15
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
0.26
07/02/20 00:15
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.26
07/02/20 00:15
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
07/02/20 00:15
1,2-Dichloroethane
ug/L
ND
1.0
0.34
07/02/20 00:15
1,2-Dichloropropane
ug/L
ND
1.0
0.19
07/02/20 00:15
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
07/02/20 00:15
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
07/02/20 00:15
2-Butanone (MEK)
ug/L
ND
5.0
3.3
07/02/20 00:15
2-Hexanone
ug/L
ND
5.0
0.57
07/02/20 00:15
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
07/02/20 00:15
Acetone
ug/L
ND
25.0
6.2
07/02/20 00:15
Acrylonitrile
ug/L
ND
10.0
0.90
07/02/20 00:15
Benzene
ug/L
ND
1.0
0.15
07/02/20 00:15
Bromochloromethane
ug/L
ND
1.0
0.34
07/02/20 00:15
Bromodichloromethane
ug/L
ND
1.0
0.26
07/02/20 00:15
Bromoform
ug/L
ND
1.0
0.62
07/02/20 00:15
Bromomethane
ug/L
ND
2.0
0.62
07/02/20 00:15 IK
Carbon disulfide
ug/L
ND
2.0
0.40
07/02/20 00:15
Carbon tetrachloride
ug/L
ND
1.0
0.22
07/02/20 00:15
Chlorobenzene
ug/L
ND
1.0
0.23
07/02/20 00:15
Chloroethane
ug/L
ND
1.0
0.49
07/02/20 00:15
Chloroform
ug/L
ND
5.0
2.3
07/02/20 00:15
Chloromethane
ug/L
ND
1.0
0.39
07/02/20 00:15 v2
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
07/02/20 00:15
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
07/02/20 00:15
Dibromochloromethane
ug/L
ND
1.0
0.41
07/02/20 00:15
Dibromomethane
ug/L
ND
1.0
0.46
07/02/20 00:15
Ethylbenzene
ug/L
ND
1.0
0.26
07/02/20 00:15
lodomethane
ug/L
ND
20.0
12.5
07/02/20 00:15
Methylene Chloride
ug/L
ND
5.0
3.7
07/02/20 00:15
Styrene
ug/L
ND
1.0
0.27
07/02/20 00:15
Tetrachloroethene
ug/L
ND
1.0
0.16
07/02/20 00:15
Toluene
ug/L
ND
1.0
0.24
07/02/20 00:15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 20
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92483826
METHOD BLANK: 2928332
Associated Lab Samples: 92483826001, 92483826002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
07/02/20 00:15
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
07/02/20 00:15
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
07/02/20 00:15
Trichloroethene
ug/L
ND
1.0
0.22
07/02/20 00:15
Trichlorofluoromethane
ug/L
ND
1.0
0.31
07/02/20 00:15
Vinyl acetate
ug/L
ND
2.0
1.4
07/02/20 00:15
Vinyl chloride
ug/L
ND
1.0
0.24
07/02/20 00:15
Xylene (Total)
ug/L
ND
1.0
0.63
07/02/20 00:15
1,2-Dichloroethane-d4 (S)
%
90
70-130
07/02/20 00:15
4-Bromofluorobenzene (S)
%
95
70-130
07/02/20 00:15
Toluene-d8 (S)
%
99
70-130
07/02/20 00:15
LABORATORY CONTROL SAMPLE:
Parameter
2928333
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.7
107
70-130
1,1,1-Trichloroethane
ug/L
50
47.5
95
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
53.5
107
70-130
1,1,2-Trichloroethane
ug/L
50
50.2
100
70-130
1,1-Dichloroethane
ug/L
50
46.3
93
70-130
1,1-Dichloroethene
ug/L
50
49.5
99
70-130
1,2,3-Trichloropropane
ug/L
50
52.9
106
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.0
102
70-130
1,2-Dibromoethane (EDB)
ug/L
50
52.3
105
70-130
1,2-Dichlorobenzene
ug/L
50
52.2
104
70-130
1,2-Dichloroethane
ug/L
50
48.2
96
70-130
1,2-Dichloropropane
ug/L
50
50.0
100
70-130
1,4-Dichlorobenzene
ug/L
50
51.9
104
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1060
106
59-169
2-Butanone (MEK)
ug/L
100
88.8
89
64-135
2-Hexanone
ug/L
100
103
103
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
96.9
97
70-130
Acetone
ug/L
100
86.1
86
61-157
Acrylonitrile
ug/L
250
223
89
61-143
Benzene
ug/L
50
49.4
99
70-130
Bromochloromethane
ug/L
50
47.3
95
70-130
Bromodichloromethane
ug/L
50
46.4
93
70-130
Bromoform
ug/L
50
54.0
108
70-130
Bromomethane
ug/L
50
43.4
87
38-130lK
Carbon disulfide
ug/L
50
43.2
86
68-130
Carbon tetrachloride
ug/L
50
50.4
101
70-130
Chlorobenzene
ug/L
50
51.3
103
70-130
Chloroethane
ug/L
50
51.5
103
37-142
Chloroform
ug/L
50
47.1
94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92483826
LABORATORY CONTROL SAMPLE:
Parameter
2928333
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
33.5
cis-1,2-Dichloroethene
ug/L
50
47.0
cis-1,3-Dichloropropene
ug/L
50
51.7
Dibromochloromethane
ug/L
50
53.5
Dibromomethane
ug/L
50
51.2
Ethylbenzene
ug/L
50
51.3
lodomethane
ug/L
100
77.6
Methylene Chloride
ug/L
50
46.5
Styrene
ug/L
50
54.7
Tetrachloroethene
ug/L
50
50.4
Toluene
ug/L
50
48.4
trans-1,2-Dichloroethene
ug/L
50
47.7
trans- 1,3-Dichloropropene
ug/L
50
50.8
trans-1,4-Dichloro-2-butene
ug/L
50
50.2
Trichloroethene
ug/L
50
51.9
Trichlorofluoromethane
ug/L
50
45.5
Vinyl acetate
ug/L
100
94.3
Vinyl chloride
ug/L
50
40.7
Xylene (Total)
ug/L
150
156
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
67
48-130 v3
94
70-130
103
70-130
107
70-130
102
70-130
103
70-130
78
40-130
93
67-132
109
70-130
101
69-130
97
70-130
95
70-130
102
70-130
100
35-189
104
70-130
91
63-130
94
55-143
81
70-131
104
70-130
92
70-130
104
70-130
96
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928334
MS
92483822003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2928335
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.2
20.9
106
105
73-134
1
30
1,1,1-Trichloroethane
ug/L
ND
20
20
24.0
23.9
120
119
82-143
1
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
23.4
23.3
117
116
70-136
1
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.9
21.7
109
108
70-135
1
30
1,1-Dichloroethane
ug/L
ND
20
20
25.8
25.6
129
128
70-139
1
30
1,1-Dichloroethene
ug/L
ND
20
20
26.5
26.4
132
132
70-154
0
30
1,2,3-Trichloropropane
ug/L
ND
20
20
22.5
22.9
112
115
71-137
2
30
1,2-Dibromo-3-
ug/L
ND
20
20
20.6
20.4
103
102
65-134
1
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.6
22.6
113
113
70-137
0
30
1,2-Dichlorobenzene
ug/L
ND
20
20
23.0
23.0
115
115
70-133
0
30
1,2-Dichloroethane
ug/L
ND
20
20
24.4
24.4
122
122
70-137
0
30
1,2-Dichloropropane
ug/L
ND
20
20
24.1
24.1
121
121
70-140
0
30
1,4-Dichlorobenzene
ug/L
ND
20
20
22.5
22.4
112
112
70-133
0
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
479
485
120
121
53-168
1
30
2-Butanone (MEK)
ug/L
ND
40
40
53.2
51.9
133
130
60-139
2
30
2-Hexanone
ug/L
ND
40
40
48.1
47.5
120
119
65-138
1
30
4-Methyl-2-pentanone
ug/L
ND
40
40
46.4
45.8
116
114
65-135
1
30
(MIBK)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 20
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Blanks
Pace Project No.: 92483826
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928334
2928335
MS
MSD
92483822003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/L
ND
40
40
56.4
54.7
141
137
60-148
3
30 v1
Acrylonitrile
ug/L
ND
100
100
123
126
123
126
64-147
2
30
Benzene
ug/L
ND
20
20
23.3
23.4
117
117
70-151
0
30
Bromochloromethane
ug/L
ND
20
20
23.7
23.8
118
119
70-141
0
30
Bromodichloromethane
ug/L
ND
20
20
19.3
19.6
97
98
70-138
2
30
Bromoform
ug/L
ND
20
20
18.2
18.2
91
91
63-130
0
30
Bromomethane
ug/L
ND
20
20
28.5
28.8
142
144
15-152
1
30
Carbon disulfide
ug/L
ND
20
20
25.9
25.8
129
129
69-149
1
30
Carbon tetrachloride
ug/L
ND
20
20
20.9
21.3
104
106
70-143
2
30
Chlorobenzene
ug/L
ND
20
20
22.5
22.7
112
113
70-138
1
30
Chloroethane
ug/L
ND
20
20
38.1
37.4
190
187
52-163
2
30 IK,IL,
M1,v1
Chloroform
ug/L
ND
20
20
23.8
23.6
119
118
70-139
1
30
Chloromethane
ug/L
ND
20
20
24.4
24.6
122
123
41-139
1
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
25.0
25.0
125
125
70-141
0
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.6
22.6
113
113
70-137
0
30
Dibromochloromethane
ug/L
ND
20
20
20.4
20.3
102
101
70-134
1
30
Dibromomethane
ug/L
ND
20
20
20.5
20.4
103
102
70-138
1
30
Ethylbenzene
ug/L
ND
20
20
22.8
22.9
114
115
66-153
0
30
lodomethane
ug/L
ND
40
40
28.6
28.0
71
70
20-138
2
30 v3
Methylene Chloride
ug/L
ND
20
20
25.3
25.5
126
127
42-159
1
30
Styrene
ug/L
ND
20
20
22.8
22.5
114
113
70-135
1
30
Tetrachloroethene
ug/L
ND
20
20
20.7
21.2
103
106
59-143
3
30
Toluene
ug/L
ND
20
20
22.4
22.5
112
112
59-148
0
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
26.2
26.4
131
132
70-146
1
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.7
21.8
108
109
70-135
0
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
17.7
17.8
88
89
47-135
1
30
Trichloroethene
ug/L
ND
20
20
22.1
22.3
110
111
70-147
1
30
Trichlorofluoromethane
ug/L
ND
20
20
25.0
25.1
125
125
70-148
0
30
Vinyl acetate
ug/L
ND
40
40
50.8
49.8
127
125
49-151
2
30
Vinyl chloride
ug/L
ND
20
20
23.4
23.0
117
115
70-156
2
30
Xylene (Total)
ug/L
ND
60
60
68.8
69.3
115
115
63-158
1
30
1,2-Dichloroethane-d4 (S)
%
115
116
70-130
4-Bromofluorobenzene (S)
%
101
101
70-130
Toluene-d8 (S)
%
102
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 20
Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: Surry Blanks
Pace Project No.: 92483826
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Surry Blanks
Pace Project No.: 92483826
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92483826001
EB
EPA 3010A
550337
EPA 6010D
550349
92483826002
FB
EPA 3010A
550337
EPA 6010D
550349
92483826001
EB
EPA 3010A
550340
EPA 6020B
550353
92483826002
FB
EPA 3010A
550340
EPA 6020B
550353
92483826001
EB
EPA 8260D
550875
92483826002
FB
EPA 8260D
550875
Date: 07/02/2020 04:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 20
Document Name: Document Revised: February 7, 2018
Sample Condition Upon Recelpt(SCUR) Page 1 of 2
�C@A0001 Document No.: Issuing Authority:
r
F-CAR-CS•033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ �iuntersville Raleigh[:] iVlechanitsdille❑
ConditionSample Client Name: PrQJeet #: WO# :92483826
Upon Receipt n 16, nS-eyvc-_' l! I
Courier, ❑F c � []UPS CI
USPS other: ❑Client
❑ Commercial a e ❑ 92463826 I 111I 1
Custody Seal Present? Des C i Seats Intact? Des o Zq I (�J T
E Enln Contents _ J
Pacidng Material: []Bubble Wrap ubble Sags []None ❑ Other
Thermometer: 92TQ61 Type of Ice: W-t ❑ewe
❑IR Gun ID:
Cooler Temp (°C): I - q %Correction Factor: Add/Subtract CQ +�
Cooler Temp Corrected ("C): `�
USDA Regulated Soil ( /A, water sample)
Did samples originate in a quarantine sane within the United States: CA, NY, or SC )check maps)?
Chain of Custady Present?
samples Arrived within Hold Time?
Short Hold Time Analysis j<72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Heads ace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTSISAMPLE DISCREPANCY
]No ❑N/A I 1•
N
[]N/A
2,
3.
go❑N/ON/A
g4.
A
[]No
❑NIA
5.
[:]No
❑N/A
6.
[]No
❑N/A
I1Nn
l`INGd1
7.
DateHnitlalsPerson Nam g
Biological Tissue F zen?
[]yes []No /A
[]None
Temp should be above freezing to VC
❑5arnples out of temptnteria. Samples an Ice, tooling process
has begun
Did samptes ariginate from a foreign source {internationally,
includingNavra" and Puerto Rico!? Oyes []No
Lot It) of spit containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted_
Project Manager SCURF Review:
Project Manager SRF Review:
Dateffime:
Date:
date:.
Field Oata Required? []Yes ❑No
Page 18 of 20
Document Name:
Document Revised: February 7, 2018
aceAnalytical
Sample Condition Upon Retelpt(5CUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLH8
**Bottom half of box is to list number of bottle
Project It W4# a 92483826
PM: AMB Due Date: 07/13/20
CLIENT: 92-Municipal
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pH Adjustment tog for Preserved Samples
Sample In
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 0
Nate: Whenever there is a discrepancy affec[Irg North Carolina compilance samples, a copy of this form will be Sent to the North Carolina DFHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect contalners.
Page 19 of 20
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