1302_Cabarrus_CDLF_Sept20GW_FID1521976_20201229

Cabarrus County C&D Landfill
Semi -Annual Sampling Report
Facility Permit # 1302-CDLF-2006
(September 2020 Sampling Event)
Prepared December 2020

I!5iF10
INS �rvrs Environmental Monitoring
Division of Waste Management- Solid Waste Reigortina Form
Notice: This farm and any information aeached to it are "Public Recurde as defined in NO General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare om farm for each individually monifered unit.
Please type or print legibly.
• Attach a notification table with values that attain or exceed NO 2L groundwater standards or NO 28 surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site soume, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface watervatues that equal or exceed the reporting limits.
Attach a nci ificadon bible of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 138.1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-OWM, Solid Waste
Section, 1646 Mail Service Genter, Raleigh, NO 27699-1646.
Solid Waste Monitorina Data Submittal Information
Name of entity submitting date (laboratory, consultant, facility owner)
Consultant - CDM Smith Inc.
Contact for questions about data famishing. Include data preparer's name, telephone number and E-mail address:
GF^'A
E-mail: colonendoodmsmith.cam
Phonic (919) 3253500
NO Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit# (.0500 or.1600) October 2044, 2006)
Cabamis County CAD Landfill
nW�dhN
r��23, and 25,
C rol�ina 28025
2W6-CDLF1-7117
Emimmeental Status: (Check all that apply)
❑ InitiallBackground Monitoring ❑x Detection Monitoring ❑ Assessment Monitoring Corrective Action
T of data submitted: (Check all that apply)
X Groundwater monitoring data from monitoring wells
❑
Methane gas monitoring data
Groundwater monitoring data from private water supply wells
Corrective action data (specify)
Leachate monitoring data
Surface water monitoring data
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
H. Yes. a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analyfical values, NO 2L groundwater standard, NO 28 surface water standard or NO Said Waste GWPS and
preliminary analysis of the muse and significance of any concentration.
❑ Yes. a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information imported and statements made on this data submittal and attachments are bass and coned
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
(Prim)
Affix NO Licensed/
5400 Glenwood Avenue Suite 400 Raleioh North Carolina 27612
Facility Representative Address
NO PE Firm License Number (dapplica0le effective May 1,
Revised 62009

Smith
5400 Glenwood Avenue, Suite 400
Raleigh, North Carolina 27612
tel: [phone]
fax: [phone]
December 29, 2020
Ms. Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
2090 U.S. 70 Highway
Swannanoa, North Carolina 28778
Subject: September 2020 Semi -Annual Sampling Report
Cabarrus County C&D Landfill
Facility Permit No. 1302-CDLF-2006
Dear Ms. Drummond:
CDM Smith Inc., on behalf of Cabarrus County, is submitting an electronic copy of the September 2020
semi-annual sampling event report for the Cabarrus County C&D Landfill. This letter report presents the
results of the recently completed sampling at the C&D Landfill and constitutes the second semi-annual
sampling event for 2020.
The approved monitoring well network for the C&D Landfill consists of background wells CD -Is and -1d;
compliance wells CD-2, -4 Rep, -7, and -9; and surface water sample location SW-3. CD-4 Rep was
installed in January 2009 as part of the proposed Phase 1 C&D Landfill expansion. Monitoring well CD-7,
formerly piezometer B-7, was added to the monitoring program in July 2014 as part of the Phase 2 C&D
Landfill expansion. Monitoring well CD-9 was installed on March 19, 2017, as part of the Phase 3 C&D
Landfill expansion. Field activities and sampling results for the groundwater and surface water samples
are discussed below.
Field Activities
Groundwater and surface water samples from the Cabarrus County C&D Landfill were collected on
September 22, 23, and 25, 2020. Groundwater samples were collected from the monitoring wells by use
of disposable, laboratory decontaminated bailers. Monitoring well locations and the surface water
location for the C&D Landfill are provided on Figure 1.
Groundwater elevations were measured at each well prior to sampling and are presented in Table 1.
Well construction details for each monitoring well are also provided in Table 1. These groundwater
elevations were used to construct potentiometric contours for this sampling event and are presented on
Figure 1. After depth to groundwater was measured, each well was purged prior to sampling to provide
fresh formation water within the well water column. Each purge volume was measured for pH,
Of
WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES

Smith
Ms. Jaclynne Drummond
December 29, 2020
Page 2
conductivity, turbidity, temperature, dissolved oxygen, and oxidation-reduction potential using a YSI-556
multi -parameter water quality meter and a HANNA HI 98703 turbidity meter. The water quality
parameters at the time of sampling are presented in Table 2.
Sampling Results
Pace Analytical Services, LLC, located in West Columbia, South Carolina, analyzed the groundwater and
surface water samples for North Carolina Appendix I volatile organic compounds (VOCs) plus
tetrahydrofuran, North Carolina Appendix I metals plus iron, mercury, and manganese, alkalinity, total
dissolved solids (TDS), chloride, and sulfate with the exception of CD-4 Rep. Samples collected from CD-4
Rep were analyzed for North Carolina Appendix I VOCs and metals.
In a letter dated May 28, 2019, the Solid Waste Section requested that all groundwater and surface
water samples collected from landfills be analyzed for 1,4-dioxane after July 1, 2018. On July 1, 2019,
the Solid Waste Section approved the removal of 1,4-dioxane from the sampling program due to two
consecutive non -detect events (January and May 2019), except for SW-3. 1,4-Dioxane sample results for
SW-3 are provided below.
The analytical results were reported to the laboratory specific method detection limit (MDL) and are
quantifiable at or below the method reporting limit (MRL). All monitoring wells for the C&D Landfill had
detections of analytes above the MDL but below the MRL. These detections were qualified as estimated
or "J" flags. The following list indicates the analytes detected above the MRL at each sampling location.
No "J" flag detections are provided. Underlined analytes exceeded the 15A NCAC 02L .0202 (NC 2L)
Groundwater Standard, Interim Maximum Allowable Concentration (IMAC) Standard, or 15A NCAC 02B
.0211 (NC 2B) or North Carolina In -Stream Target Value Surface Water Quality Standards for Class C
Waters.
CD-1s (Background)
General Chemistry:
Metals:
Volatile Organic Compounds:
CD-1d (Background)
General Chemistry:
Metals:
Volatile Organic Compounds:
Alkalinity, Chloride, Sulfate, TDS
Barium, Iron, Manganese
None Detected
Alkalinity, Chloride, Sulfate, TDS
Barium, Copper, Iron, Manganese, Vanadium, Zinc
None Detected
CD-2
General Chemistry: Alkalinity, Chloride, Sulfate, TDS
Metals: Barium, Copper, Iron, Lead, Manganese, Nickel, Vanadium, Zinc
Volatile Organic Compounds: Benzene, Chloroethane, 1,1-Dichloroethane, cis-1,2-Dichloroethene
0

Smith
Ms. Jaclynne Drummond
December 29, 2020
Page 3
CD-4 Rep
Metals:
Volatile Organic Compounds:
CD-7
General Chemistry:
Metals:
Volatile Organic Compounds:
CD-9
General Chemistry:
Metals:
Volatile Organic Compounds:
SW-3
General Chemistry:
Metals:
Volatile Organic Compounds:
Barium, Beryllium, Lead, Nickel, Vanadium
1,1-Dichloroethane
Alkalinity, Chloride, Sulfate, TDS
Barium, Cobalt, Copper, Iron, Lead, Manganese, Nickel, Vanadium
Benzene, Chloroethane, 1,1-Dichloroethane, cis-1,2-Dichloroethene,
Methylene Chloride, Tetra chloroethene, Tetrahydrofuran,
Trichlorofluoromethane, Vinyl Chloride
Alkalinity, Chloride, Sulfate, TDS
Barium, Copper, Iron, Manganese, Nickel, Vanadium
1,4-DichIorobenzene, 1,1-Dichloroethane, cis-1,2-Dichloroethene,
Trichlorofluoromethane
None Detected
Barium, Copper, Iron, Manganese, Vanadium
None Detected
"J" flags were not included in the previous list, but several locations had "J" flag detections that
exceeded the standards. These constituents along with their location are listed below.
Cobalt: CD-2, -4 Rep, and -9
Lead: SW-3
Thallium: CD-7
Vanadium: CD-1s
Equipment and trip blanks were analyzed for quality control. A duplicate sample was also analyzed for
quality control. Methylene chloride was detected in the trip blank as an estimated concentration below
its NC 2L Groundwater Standard. Acetone was detected as an estimated concentration in the equipment
blank below its NC 2L Groundwater Standard. The duplicate sample, identified as CD DUP, was collected
from CD-9. The duplicate sample had similar concentrations as those detected in CD-9, except for an
estimated detection of beryllium below its IMAC and a detection of lead below its NC 2L Groundwater
Standard.
Metals detected above the standards are likely naturally occurring based on concentrations in the
background monitoring wells or are from elevated turbidity at the time of sample collection. Benzene,
tetra chloroethene, and vinyl chloride have recently been detected above the NC 2L Groundwater
0

Smith
Ms. Jaclynne Drummond
December 29, 2020
Page 4
Standards in samples collected from CD-7. In September 2020, only vinyl chloride was detected above
the NC 2L Standards.
A complete summary of all detected constituents from the September 2020 sampling event is presented
in Table 3. The laboratory analytical reports are provided in Appendix A. The next semi-annual sampling
event will be completed in the spring of 2021.
If you have any questions or require further explanation, do not hesitate to call me at [phone] or
by email at [e-mail].
Very truly yours,
Mathew F. Colone, P.G.
CDM Smith Inc.
cc: Kevin Grant, Cabarrus County
0

Table 1
Monitoring Well Construction Summary and Groundwater Elevations
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
Depth..Measured
• ,,
Facility Permit
MonitoringMonitoring
ology of
Total Depth
Well
Latitude
Longitude
Number
Code
Date
Screened Interval
(feet BTOC)
Screen
Filter
Seal
(inches)
TOC
Groundwater
Groundwater
Interval
Interval
Interval
Elevation
:.
Elevation
CD-1s
1302-CDLF-2006
8/7/2006
35.47788
80.52334
Saprolite
29.53
18.0-28.0
16.0-28.0
14.0-16.0
2.0
755.00
21.25
733.75
(background well)
CD-1d
1302-CDLF-2006
7/21/2004
35.47788
80.52340
PWR
52.15
40.0-50.0
38.0-50.0
36.0-38.0
2.0
757.40
23.92
733.48
(background well)
1302-CDLF-2006
CD-2
9/12/2006
35.47698
80.52494
Saprolite
25.69
9.0-24.0
7.0-24.0
5.0-7.0
2.0
733.00
10.57
722.43
1302-CDLF-2006
CD-4 Rep
1/15/2009
35.47656
80.52210
Saprolite
19.41
6.0-16.0
4.0-16.0
2.0-4.0
2.0
739.15
8.63
730.52
1302-CDLF-2006
CD-7
11/25/2002
35.47567
80.52551
Bedrock
46.31
34.0-44.0
32.0-44.0
30.0-32.0
2.0
744.81
38.05
706.76
1302-CDLF-2006
CD-9
3/9/2017
35.47488
80.52564
PWR
51.00
36.0-51.0
34.0-51.0
32.0-36.0
2.0
748.13
41.98
706.15
Notes:
1. BTOC - Below Top of Casing
2. bgs - Below Ground Surface
3. PWR - Partially Weathered Rock
4. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in November 2010.
5. CD-7 (formerly piezometer B-7) was added to the monitoring program in July 2014 as part of the Phase 2 C&D Landfill expansion.
6. CD-9 was installed as part of the Phase 3 C&D Landfill expansion in March 2017.
CDM
Smith Page 1 of 1 December 2020

Table 2
Water Quality Measurements
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
Water Quality Measurements
Monitoring Well Code Dissolved
PH Conductivity Temperature ORP Turbidity
(S.U.) (Vs/cm) (degrees Celsius) Oxygen (mg/L) (mvs) (NTUs)
® ®®�
(background well)
(background well)
Surface Water Sample Location
Notes:
1. Water quality measurements were collected on September 21-23 and 25, 2020.
2. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in November 2010.
3. CD-7 (formerly piezometer B-7) was added to the monitoring program in July 2014 as part of the Phase 2 C&D
Landfill expansion.
4. CD-9 was installed as part of the Phase 3 C&D Landfill expansion in March 2017.
5. µ5/cm - Microsiemens per centimeter
6. mg/L - Milligrams per liter
7. ORP - Oxidation -Reduction Potential
8. NTUs - Nephelometric Turbidity Units
9. mvs - Millivolts
10. S.U. - Standard Unit
CDNI Page 1 of 1 December 2020
Smith

Table 3a
Detected Groundwater Constituents - General Chemistry and Metals
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
CII 3-May-11
47,000
3,600
1,200J
146,000
81.4J 0.19J
5.45JB 4.231
16.0 7,770
2.32J
190
5.93J
0.14J
20.61 26.5
CII 8-Nov-11
40,000
4,000
1,1001
65,000
59.7J 0.25JB
4.461 2.67J
12.4 5,350
1.91
127
4.41J
0.081
11.2J 18.2
CII 7-May-12
46,000
3,900
158,000
45.5J
3.30J 1.191
8.75J 3,120
1.12J
63.4
3.01J
12.71 12.613
CII 28-Nov-12
39,000
4,100
110,000
63.8J 0.111
5.651 3.051
11.6 5,210
1.431
4.66J
17.1J 16.9
CII 7-May-13
42,000
4,000
120,000
0.94J
2.4JB
35.6J
0.88J 0.671
4.04J 1,340
0.39J
37.7
1.78J
0. 13J
6.061 5.08J
CII 5-Nov-13
30,000
3,800
80,500
46.8J 0.121
3.591 S.63J
10.2 4,200
1.351
3.50J
18.4JB 15.413
=
CII 6-May-14
42,000
3,800
111,000
28.8J
4.14JB
1.48J 347E
0.11J
10.18
1.03J
0.311
3.401 2.98JB
CII 4-Nov-14
41,000
3,900
102,000
28.7J
0.13J
1.311 118
0.061
6.6J
1.04J
0.111
2.57JB 1.58J
CII 5-May-15
38,000
3,800
<5,000
113,000
1.63J
29.5JB
1.33J 371
0.15J
13.8
0.303JB
1.17J
2.401 2.75JB
1302-CDLF-2006
CII 27-Oct-15
CII 17-May-16
43,000
43,000
3,800
3,700
1,000J
110,000
130,000
28.4J
23.9J
0.801 0.391
0.941
0.751 234
0.991 446
0.121
0.12J
35.9
17.OJ
1.21J
1.01J
4.19CN,J 0.15J
4.101 3.3613-01)
4.701 1.93J
CII 1-Nov-16
46,000
4,200
<5,000
71,000
30.5J
1.23J 1.32J
1.361 647
0.281
1.35J
4.30J
=
24.4
CII 9-May-17
49,000
3,600
1,300J
120,000
34.3J
1.171
1.26J 522
0.20J
0.97J
6.691 1.82J
CII 31-Oct-17
50,000
4,200
1,000J
161,000
0.52J
36.3J
1.81J 0.54J
2.871 1,270
0.37J
31.2J
1.41J
6.911 4.00J
CII 11-Jun-18
49,000
3,890
904J
(1)
28.9J
214J
8.1J
0.0511
4.3J 4.41
CII 17-Dec-18
46,000
3,720
9911
119,000
26.7J
0.60J
3.61 498
16.6
15.01
7.OJ 9.5J
CII 7-May-19
43,000
2,930
12,600
158,000
29.8
638
17.6
1.3J
7.OJ 5.11
CII 5-Nov-19
43,000
3,750
2,160J
129,OOO111
31.9
1.01
1.81E 153
0.070J
7.OJ
0.73J
5.01 7.3JB
CII 18-May-20
49,100
4,570
4,280
141,OOO111
0.46J
34.5
2.2J
0.92J 437
0.231
11.3
1.4J
6.4J 6.91
CII 23-Sep-20
51,000
5,500
2,500
140,000
34
1.31
1.51 630
21
4.9J 4.2J
CII 3-May-11
57,000
2,600
3,000J
206,000
2.44J
231
2.03
16.7 18.6
112 49,400
14.0
22.3J
0.11J
101 103
CI 8-Nov-11
30,000
2,900
3,000J
98,000
74.5J
0.51J
4.081 4.27J
27 9,190
2.841
144
5.68J
24.6J 26.3
CII 7-May-12
50,000
2,800
150,000
72.4J
0.58J
3.91J 4.671
25 9,380
2.81J
170
5.58J
26 27.913
CI 28-Nov-12
46,000
3,000
128,000
0.33J
37.7J
0.07J 2.38J 0.94J
12.6 1,900
1.14J
41.4
2.50J
8.901 13
CII 7-May-13
52,000
3,000
125,000
0.88J
1.02JB
31.2J
0.07J 0.78J
4.5J 1,080
0.491
25.5
1.92J
6.18J 13.1
CI 5-Nov-13
42,000
3,000
104,000
35.OJ
0.861 4.341
1.13J 812
1.90J
46.2
17.1JB 10.813
CII 6-May-14
46,000
2,900
119,000
1.14J
37.81
0.07J
0.051 3.22JB 1.161
7.34J 1,610E
0.811
49.6E
2.741
0. 12J
6.16J 9.41JB
CI 4-Nov-14
43,000
3,100
101,000
43.1J
0.16J
0.11J 2.25J
9.091 3,400
0.87J
2.88J
10.2JB 10.7
32.5
CII 5-May-15
44,000
2,900
<5000
115,000
34.SJB
0.841
3.63J 1,320
0.391
1.42J
5.181 3.68JB
1302-CDLF-2006
CI 27-Oct-15
CII 17-May-16
46,000
96,000
2,900
18,000
14,000J
120,000
202,000
0.42J
42.3J
81.31
0.13J
0.46J
1.871 2.15J
4.86J 7.42J
8.181 3,170
26.0 12,000
0.97J
3.131
2.49J
7.11J 2.111
4.37CN,J 0.06J
0.07J
10.9J 14.013-01
29.3 29.7
CI 1-Nov-16
52,000
3,400
<5,000
99,000
32.6J
1.191 0.77J
2.82J 1,200
0.33J
31.3J
1.24J
7.96J 4.29J
CII 9-May-17
53,000
2,800
3,700J
167,000
33.91
1.271 0.52J
1.811 720
6.921
25.8J
1.091
6.95J 3.12J
CI 31-Oct-17
52,000
3,300
3,300J
154,000
29.5J
0.68J
0.61J 226J
0.111
11.81
0.64J
5.38J 1.24J
CII 12-Jun-18
51,000
3,200
3,330J
117,000
32.41
2.51 432
13.2J
1.01
6.91 3.21
CI 17-Dec-18
53,000
3,110
3,360J
121,000
31.9J
9.3J
2.3J 591
0.41J
18.1
3.OJ
6.8J 4.1J
CII 7-May-19
52,000
2,840
3,140J
134,000
30.7
1.4J 517
9.7J
7.41 2.91
CI 5-Nov-19
48,000
3,140
3,070J
137,OOO111
0.48J
30.1
1.91
1.1JB 197
0.13J
8.9J
1.81
4.7J 8.2JB
CII 18-May-20
54,300
2,450
2,630
121,OOO111
29.1
0.64J
27.2J
2.OJ
0.331
5.6J 2.01
CII 22-Sep-20
53,000
3,100
2,000
130,000
0.671
38
1.91
8.6
0.991
1 47
4.21
8.8 36
i -th Page 1 of 9 December 2020

Table 3a
Detected Groundwater Constituents - General Chemistry and Metals
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
CD-2 3-May-11
2,850
6,800
1,30OJ
209,000
1.78J 55.9J 0.23J
3.04JB
3.621
7.91J
5,560
2.75J
92.21
O.O31J
3.60J
22.21 12B
CD-2 8-Nov-11
9,000
7,500
1,4001
41,500
22.1J 0.21JB
1.411
2.15J
3.531
1,660
1.071
47.4
1.91
4.99J
CD-2 7-May-12
21,000
7,200
104,000
36.4J 0.19J
2.71J
3.381
5.03J
2,760
1.94J
74.11
2.95J
9.81 16.56
CD-2 28-Nov-12
25,000
6,700
(1)
39.5J 0.131
2.891
2.95J
4.401
2,720
1.421
67.2
2.72J
10.11 7.92J
CD-2 7-May-13
20,000
7,200
80,000
O.34J
1.25JB 39.4J 0.23J
1.32J
2.8J
4.44J
2,450
1.34J
57.8
2.59J
0.08J
9.021 8.79J
CD-2 5-Nov-13
28,000
6,600
55,000
45.1J 0.201
0.641
3.31J
4.011
1,600
1.601
68.8
0.0871
2.38J
14J 7.77JB
CD-2 7-May-14
16,000
8,200
135,000
37.5J 0.1OJ
1.98JB
2.481
2.26J
1,130E
0.78JB
49.3
0.305J
2.00J
5.001
CD-2 5-Nov-14
25,000
7,500
330,000
O.O7J
46.0J
2.21JB
2.69J
3.591
2,00013
1.101
59.6
(1)
2.47J
7.23J 6.92JB
CD-2 6-May-15
16,000
8,100
136,000
52.0JB 0.18J
2.30JB
2.901
5.91J
2240
1.37J
57.6
0.158JB
3.74J
6.971 8.02JB
CD-2 27-Oct-15
7,750
7,300
5,9001
178,000
0.831 60.0J 0.421
3.94B-01,J
3.71J
8.711
5,150
2.671
83.8
0.0731
5.50J
4.05CN,1
0.081
16.3J 13.3
1302-CDLF-2006
CD-2 18-May-16
20,000
7,900
<5,000
147,000
49.8J 0.22J
2.32J
3.411
3.56J
2,350
1.20J
71.7
0.189J
2.68J
8.34J 7.62J
850,000 -02
CD-2 1-Nov-16
20,000
8,100
<5,000
64.5J 0.26J
3.101
4.15J
5.481
4,010
2.551
99.5
0.O56J
3.11J
15.3J 13.9
CD-2 9-May-17
12,500
9,100
2,500J
125,000
54.5J 0.28J
2.4OJ
3.491
3.71J
2,5506-01
1.71J
68.1
0.115J
2.80J
0.05J
8.631 7.26J
CD-2 1-Nov-17
15,000
7,900
2,9001
635,000
54.0J 0.16J
1.791
3.1OJ
2.781
1,630
1.021
62.3
O.O79J
2.58J
7.101 7.22J
CD-2 (dup) 1-Nov-17
16,000
7,400
1,600J
885,000
57.6J 0.17J
2.05J
3.001
4.01J
1,840
1.08J
64.1
O.O7OJ
2.776J
8.O4J 8.19J
CD-2 12-Jun-18
29,000
7,250
4,82OJ
88,000
58.5J 0.17J
2.21
2.8J
2.61
1,280
0.631
51.6
0.12J
3.1J
6.61 8.7J
CD-2(dup) 12-Jun-18
27,000
7,460
4,62OJ
91,000
56.3J 0.17J
1.91
2.61
2.6J
1,200
0.63J
48.3
O.11J
2.8J
9.01 8.8J
CD-2 18-Jan-19
40,000
10,500
18,700
107,000
27.2J 0.081J
1.41
300
0.311
30.6
0.15J
1.2J
4.2J
CD-2 7-May-19
40,000
8,400
10,500
161,000
0.42J 41.7 0.081J
0.981
1.91
1.3J
782
0.44J
49.7
2.2J
4.7J 5.4J
CD-2 6-Nov-19
64,000
6,220
7,370
151,000
1.2J 68.6 0.11J
1.21
2.3J
2.31E
896
0.60JB
75.0
3.0J
8.11 9.0JB
CD-2 20-May-20
77,700
7,630
5,200
112,000
0.61J 78.5
0.72J
2.0J
1.2J
309
0.28J
79.7
2.9J
4.5J 8.5J
CD-2 25-Sep-20
79,000
9,400
2,900
230,000
110 0.26J
4.6J
2.9J
7.8
3,900
2.8
110
5.0
12 13
CD-3 3-May-11
105,000
4,300
3,20OJ
404,000
48.9J 0.11J
2.361
7.57J
3,580
1.30J
93.6
2.48J
12.2J 8.64JB
CD-3 8-Nov-11
85,000
5,400
3,90OJ
144,000
25.5J
0.651
1.011
178
24.9
1.48J
5.16J
CD-3 7-May-12
75,000
4,500
177,000
41.7J
0.84J
1.271
3.84J
1,170
0.54J
32.6
3.37J
6.18J 6.81J,B
CD-3 28-Nov-12
104,000
5,100
(1)
46.7J
1.411
1.9OJ
4.351
1,740
0.821
68.9
1.86J
9.52J 6.93J
CD-3 7-May-13
122,000
4,800
181,000
33.8J
1.2OJ
2.351
880
0.42J
56.3
1.41J
5.86J 2.89J
1302-CDLF-2006
CD-3 5-Nov-13
CD-3 7-May-14
59,000
61,600
4,500
4,200
121,000
127,000
64J 0.21J
28.7J
0.741
1.66JB
3.47J
10.6
0.721
5,170
83.28
2.061
139
4.4J
3.25J
1.14J
21.2J 12.213
2.42J
CD-3 5-Nov-14
82,000
13,000
13,OOOJ
425,000
162 0.14J
1.85JB
3.00J
6.221
3,77013
1.211
1,030
(1)
8.65J
12.9J 9.94JB
CD-3 6-May-15
89,000
13,000
22,OOOJ
280,000
1.38J 159 0.11J
1.26J
2.841
1,230E
0.42J
1,090
0.302JB
7.25J
5.29J 5.93J
CD-3 27-Oct-15
95,000
13,000
23,OOOJ
255,000
155 0.1OJ
1.02B-01,1
1.82J
3.911
2,010
0.681
936
7.72J
2.6OCN,J
6.03J 6.81J
CD-3 18-May-16
100,000
14,000
26,OOOJ
311,000
194 0.12J
1.6OJ
1.351
607
0.24J
1,010
7.88J
1.191
4.02J 3.73J
CD-3 1-Nov-16
95,000
14,000
27,OOOJ
162,000
158 0.13J
2.071
2.77J
1,400
0.491
6.811
6.82J
rh Page 2 of 9 December 2020

Table 3a
Detected Groundwater Constituents - General Chemistry and Metals
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
CII Rep 3-May-11
124,000
9,700
--
--
206
0.9JB 17.6
0.621
--
--
--
8.39J
2.72JB
CII Rep (dup) 3-May-11
--
--
--
--
0.21J
206
17.9
0.681
--
--
--
8.98J
0. 17J
2.85J
CII Rep 8-Nov-11
--
--
--
--
0.14J
191
0.93J 18.2
1.001
--
--
--
8.86J
9.44J
CII Rep 9-May-12
-
-
-
--
184
1.691 18.1
1.701
--
0.171
--
--
11.3J
3.031 16.113
CII Rep 29-Nov-12
--
--
--
--
172
13.7
0.621
--
--
--
7.03J
2.84J 2.14JB
CII Rep 10-May-13
-
-
-
--
75.5J 0.51
2.711 7.87)
1.941
--
0.881
--
--
11.2J
11.11 10.3
CII Rep 7-Nov-13
--
--
--
--
1.36J
60.4J 0.35J 0.07J
0.77J 5.31J
1.831
--
0.571
--
--
SAD
0.131
32 4.40JB
CII Rep 7-May-14
-
-
-
--
62.4J 0.311 0.05J
3.25JB 5.02J
1.701
--
0.321
--
--
6.52J
22.21 2.97JB
CII Rep 5-Nov-14
--
--
--
--
70.OJ 0.31J
2.59J
1.461
--
0.721
--
--
4.29J
14.8JB 6.85J
CII Rep 6-May-15
--
--
--
--
58.4J 0.39J
1.13J 5.94J
1.901
--
--
--
4.72J
14.OJ 2.99J
1302-CDLF-2006
CII Rep 27-Oct-15
-
-
-
--
0.791
57.9J 0.321
2.181 5.86)
8.951
--
1.26J
--
--
10.7J
4.14CN,1
13.91 8.3413-01)
CII Rep 18-May-16
-
-
-
--
1.09J
56.2J 0.46J
1.24J 7.31J
1.021
--
0.661
-
-
5.43J
18.01 3.70J
CII Rep 2-Nov-16
-
-
-
--
46.3J 0.27J
1.351 1.59)
1.181
--
0.901
--
--
4.18J
1.11J
18.11 8.811
CII Rep 9-May-17
-
-
-
--
53.8J 0.46J
0.95J 5.91J
1.721
--
0.521
-
-
4.38J
10.51 3.73J
CII Rep 31-Oct-17
-
-
-
--
45.OJ 0.18J
0.971 0.821
0.581
--
0.45J
--
--
2.75J
1.88J
7.681 2.76J
CII Rep 6-Jun-18
-
-
-
--
52.9J 0.41J
3.41
--
0.741
--
-
3.3J
13.31 4.01
CII Rep 19-Dec-18
-
-
-
--
1.1J
50.9J 0.96J
4.61 5.51
2.61
--
2.9J
--
--
7.OJ
1.41
15.51 11.6
CII Rep 7-May-19
-
-
-
--
45.9 0.38J
2.1 7.0
1.41
--
1.1
--
-
5.8
6.2J 13.7
CII Rep 7-Nov-19
--
-
-
--
1.4J
31.5 0.40J
1.81 1.31
1.4JB
--
0.83J
--
--
3.8J
21.0 9.5JB
CII Rep 18-May-20
--
--
--
--
1.1
70.9 0.48J
0.981 6.6
0.771
--
0.571
--
-
5.1
11.6 12.5
CII Rep 23-Sep-20
--
--
--
--
56 0.52
2.21 3.11
1.5J
--
1.4
--
--
5.6
11 7.31
CII 1-Jul-14
66,000
7,600
15,000J
420,000
53.1J 0.131J
669
8.74J
4.111 4.061
CII 5-Nov-14
77,000
8,500
18,000J
1,170,000
1.32J
118 3.74
15.16 3.71J
40.0
21,100E
13.6
IM
(1)
8.91J
0.241
75.8 19.46
CII 6-May-15
86,000
9,800
25,0001
660,000
1.71J
66.8J 0.28J
0.451
4.361
1,630B
0.861
43.4
3.36J
4.14J 3.33J
CII 27-Oct-15
81,000
11,000
28,000J
291,000
87.2J 1.12
5.33E-03,1 L.52J
16.6
6,560
4.69J
145
0.138J
6.61J
3.81CN,1
23.4J 11.3
CII 18-May-16
90,000
10,000
29,000J
282,000
74.8J 0.43J
2.18J 0.36J
4.74J
2,160
1.20J
59.4
0.164J
4.90J
10.2J 4.03J
CII 1-Nov-16
100,000
13,000
34,000
413,000
82.61 0.28J
1.211
3.45J
1,200
1.06J
170
5.581
4.98J
CII 9-May-17
120,000
14,000
35,000
667,000
86.8J 0.34J
1.851
4.64J
1,8808-01
1.70J
123
5.501
8.70J 4.13J
1302-CDLF-2006
CII 31-Oct-17
114,000
15,000
39,000
1,100,000
94.51 0.27J
1.301 0.44J
3.85J
1,300
1.13J
219
6.261
8.571 4.18J
CII 12-Jun-18
112,000
16,900
44,300J
350,000
1.OJ
97.9J 0.13J
3.11
231J
215
7.6J
6.31 6.3J
CII 18-Jan-19
126,000
17,600
50,400
280,000
152 0.24J
2.OJ 12.5
7.81
178
3,930
17.51
5.11
CII 7-May-19
130,000
19,400
47,400
359,000
141 0.32J 0.12J
0.41J 5.0
6.3
64.9
2,570
13.7
1.91 7.21
CII (dup) 7-May-19
129,000
19,100
48,000
391,000
147 0.36J
0.881 5.4
9.9
847
0.311
4,860
13.5
4.7J 8.81
CII 7-Nov-19
148,000
21,800
47,800
332,000
152 0.29J
0.931 5.2
6.96
1,240
0.60JB
2,860
10.9
0.0731
3.9J 10.913
CII 19-May-20
153,000
21,100
70,700
358,000
0.73J
142 0.34J
0.691 7.9
6.3
318
0.27J
2,800
12.5
2.61 10.3
CII 22-Sep-20
170,000
23,000
56,000
370,000
180 0.39J 0.25J
1.5J 8.4
25
1,100
1.3
14
0.25J
5.4 7.9J
rh Page 3 of 9 December 2020

Table 3a
Detected Groundwater Constituents - General Chemistry and Metals
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
rrrr
250,000
500,000
1.
1 10
700 1
V
2 1 10
,,,
300 1
15
so
I I
1 100
,,,
CD-8
1-Jul-14
75,000
3,900
3,70OJ
120,000
O.256J
421
0.191J
12.6
78
26,600
6.55J
1,360
13.8J
0.238J
93.3
79.6
CD-8
5-Nov-14
86,000
3,500
253,000
83.4J
1.641B
1.201
7.151
2,360B
0.591
131
(1)
3.34J
8.181
11.013
CD-8
6-May-15
57,000
3,300
<5000
138,000
O.36J
53.8.113
0.481
4.13.1
1,030
0.27.1
58.5
0.09518
2.43J
4.031
9.73JB
CD-8
27-Oct-15
72,000
3,600
1,1001
132,000
O.75J
1.791
162
0.321
O.21J 5.88B-01,J
1.901
38.6
2,960
2.291
95.2
9.53J
3.65CN,1
11.21
1,430
1302-CDLF-2006
CD-8 (dup)
27-Oct-15
70,000
3,500
130,000
O.40J
1.72.1
160
0.33.1
0.21J 5.54E-01,1
1.80J
36.3
2,630
2.12.1
82.4
8.69J
4.2OCN,J
10.61
1,310
CD-8
19-May-16
115,000
2,000
<5,000
205,000
O.49J
1.521
133
0.201
3.541
1.401
28.1
2,320
1.281
123
8.72J
13.21
1,250
CD-8 (dup)
19-May-16
110,000
2,000
<5,000
215,000
1.55.1
136
0.23.1
0.30J 4.41.1
1.63J
31.2
3,230
1.87.1
129
9.76J
14.81
1,600
CD-8
1-Nov-16
90,000
3,400
<5,000
517, -
94.6J
0.171
2.271
2.521
15.6
3,350
1.061
433
3.96J
18.11
244
CD-8 (du)
1-Nov-16
80,000
3,500
2,1001
428,0001-1-02
96.71
0.211
3.111
2.471
18.8
4,640
1.18J
412
4.O9J
22.21
247
CD-9
9-May-17
115,000
5,200
3,60OJ
85,000
155
7.281
8.73J
44.7
8,700E-01
1.03.1
374
8.76.1
0.11J
34.2
25.3
CD-9 (dup)
9-May-17
110,000
5,700
3,6001
124,000
92.4J
0.101
2.141
4.671
14.1
2,62013-01
0.491
236
5.56J
11.91
7.56J
CD-9
31-Oct-17
111,000
5,000
3,40OJ
380,000
0.59.1
307
0.56.1
M
20.9
126
23,300
2.88.1
680
13.8.1 2.391
O.22J
93.0
62.9
CD-9
12-Jun-18
115,000
5,130
3,8101
183,000
1.1J
131
0.16.1
6.21
4.01
30.4
5,380
0.981
139
5.01
26.8
15.2
CD-9
18-Jan-19
130,000
6,300
8,520
189,000
95.31
0.050.1
1.31
3.1J
374
158
6.8.1
3.91
3.01
CD-9 (dup)
18-Jan-19
132,000
6,220
8,500
182,000
99.91
1.21
2.61
149
157
6.5J
3.61
2.2.1
1302-CDLF-2006
CD-9
7-May-19
118,000
6,460
6,340
214,000
96.8
1.11
2.5J
162
188
6.6
4.11
2.91
CD-9
7-Nov-19
123,000
5,930
4,5601
222,000
0.861
104
1.41
1.51
6.26
963
0.161B
166
6.0
9.01
8.2JB
CD-9(dup)
7-Nov-19
132,000
5,850
4,49OJ
191,000
0.95.1
67.2
0.761
3.51
4.5JB
667
0.20JB
179
4.2.1
9.51
6.1JB
CD-9
20-May-20
136,000
5,190
3,840
218,000
0.821
147
0.36.1
10.6
7.0
53.3
9,790
1.7
334
9.6
0.0881
40.9
23.7
CD-9 (dup)
20-May-20
148,000
5,190
3,810
221,000
0.8OJ
155
0.34.1
13.3
7.3
53.1
10,100
1.7
337
10.3
0.0901
41.3
23.4
CD-9
22-Sep-20
130,000
4,900
1,800
210,000
99
1.61
1.41
8.9
1,300
160
5.5
7.3
5.01
CD-9 (dup)
22-Sep-20
130,000
4,900
1,800
200,000
170
0.281
8.0
6.3
51
9,200
1.3
300
9.0
34
22
Notes:
1. All units are in micrograms per liter (parts per billion).
2. "- Interim Maximum Allowable Concentration (IMAC)
3. NE -Standard Not Established; dup - Duplicate Sample
4. (--) - Not Analyzed
5. J - Indicates the analytical result is an estimated concentration between the method detection limit and the adjusted reporting limit.
6. B, B-01-The analyte concentration detected in the method blank was greater than the method detection limit.
7. CN - Detected silver concentrations were determined to be the result of contamination from the preservative acid used.
8. H-02, H1- Analysis was completed outside of hold time.
9. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in January 2009. Beginning November 2011 samples collected from CD-4 Rep are only analyzed for Appendix I metals.
10. Alkalinity, chloride, sulfate, and total dissolved solids were added to the sampling program in May 2010.
11. (1) - Not analyzed due to laboratory oversight.
12. CD-3 was relocated on July 1, 2014, as part of the Phase 2 C&D Landfill expansion.
13. CD-7 and -8 (formerly piezometers B-7 and -19) were added to the monitoring program in July 2014 as part of the Phase 2 C&D Landfill expansion.
14. CD-3 and -8 were abandoned on February 2, 2017, as part of the Phase 3 C&D Landfill Expansion.
15. CD-9 was installed on March 9, 2017, as part of the Phase 3 C&D Landfill Expansion.
Concentration exceeds the 15A NCAC 02L .0202 (North Carolina 2L) or IMAC Standard
- Indicates the result is below the detection limit.
rh Page 4 of 9 December 2020

Table 3b
Detected Groundwater Constituents - Volatile Organic Compounds
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
$m ath Page 5 of 9 December 2020

Table 3b
Detected Groundwater Constituents - Volatile Organic Compounds
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
$m ath Page 6 of 9 December 2020

Table 3b
Detected Groundwater Constituents - Volatile Organic Compounds
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
CD-7 (B-7)
22-Mar-12
CD-7 (B-7)
3-May-12
0.65J
0.671
CD-7
1-Jul-14
CD-7
4-Nov-14
CD-7
6-May-15
0.41
CD-7
27-Oct-15
0.41
0.5.1
CD-7
17-May-16
0.71
1.01
1.9
CD-7
1-Nov-16
1.21
13.1
5.8
1302-CDLF-2006
CD-7
9-May-17
1.01
1.41
3.5
CD-7
31-Oct-17
0.91
1.01
7.1
CD-7
12-Jun-18
1.3
7.1
0.901
CD-7
18-Jan-19
0.711
1.9
25.0
1.01
7.1
1.2
CD-7
7-May-19
0.911
1.2
0.561
1.8
1.1
27.3
5.7
1.9
CD-7 (dup)
7-May-19
0.92J
1.4
0.62.1
1.9
1.1
24.5
0.37J
6.0
2.0
CD-7
6-Nov-19
1.0
1.5
3.3
0.92J
27.8
0.371
5.7
M
CD-7
19-May-20
0.69J
1.2
0.561
0.36J
1.3
12.8
1.8
CD-7
22-Se -20
0.95
0.69
1.4
2.8
0.80
0.57
9.2
1.6
1.6
CD-8 (B-19)
22-Jan-09
1.21
0.22J
3.34.1
2.84.1
0.891
2.2
1.21
CD-8 (B-19)
22-Mar-12
1.13
2.24
1.03
CD-8 (B-19)
3-May-12
0.18J
0.80.1
1.51
0.901
CD-8
1-Jul-14
3.21
0.571
1.5
0.45J
CD-8
4-Nov-14
0.81
1302-CDLF-2006
CD-8
6-May-15
0.5J
CD-8
27-Oct-15
0.6.1
CD-8 (dup)
27-Oct-15
0.5.1
CD-8
18-May-16
CD-8 (dup)
18-May-16
CD-8
1-Nov-16
CD-8 (dup)
1-Nov-16
CD-9
9-May-17
3.21
14
1.0
CD-9 (dup)
9-May-17
3.21
14
1.0
CD-9
31-Oct-17
0.71
3.1.1
12
0.7J
CD-9
12-Jun-18
13.1
0.75J
CD-9
18-Jan-19
3.21
11.8
0.93J
9.11
1.4
3.0
CD-9 (dup)
18-Jan-19
3. 1.1
10.6
0.971
8.2.1
1.3
2.9
1302-CDLF-2006
CD-9
7-May-19
1.7
3.5
14.6
4.71
0.871
2.6
CD-9
6-Nov-19
1.4
2.7
12.0
0.51J
1.1
CD-9 (dup)
6-Nov-19
0.991
1.8
8.6
0.77J
CD-9
20-May-20
1.1
1.9
7.7
0.54J
0.511
CD-9 (dup)
20-May-20
1.7
7.0
0.59J
CD-9
22-Sep-20
1.1
1.9
6.9
0.42J
0.68
CD-9 (dup)
22-Seo-20
1.1
2.0
7.0
0.421
0.70
Notes:
1. All units are in micrograms per liter (parts per billion).
2. dup - Duplicate Sample
3. J - Indicates the analytical result is an estimated concentration between the method detection limit and the adjusted reporting limit.
4. B -The analyte concentration detected in the method blank was greater than the method detection limit.
5. NE - Standard Not Established
6. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in January 2009.
7. CD-3 was relocated on July 1, 2014, as part of the Phase 2 C&D Landfill expansion.
8. CD-7 and -8 (formerly piezometers B-7 and -19) were added to the monitoring program in July 2014 as part of the Phase 2 C&D Landfill expansion.
9. CD-3 and -8 were abandoned on February 2, 2017, as part of the Phase 3 C&D Landfill Expansion.
10. CD-9 was installed on March 9, 2017, as part of the Phase 3 C&D Landfill Expansion.
Concentration exceeds the 15A NCAC 02L .0202 (North Carolina 2L) Standard.
Indicates the result is below the detection limit.
$m ath Page 7 of 9 December 2020

Table 3c
Detected Surface Water Constituents - Metals and General Chemistry
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
Value Freshwater
Aquatic Life
SW-3
Standard
9-Nov-11
DRY
DRY
SW-3
9-May-12
DRY
DRY
SW-3
29-Nov-12
DRY
DRY
SW-3
10-May-13
0.27.11
1 152
1 1
12.23J I 3.07J 4.30J
996 1 0.49J
I 887E I
I 4.68J I
1 10.10J13.01JI33.4
60
1 20
240J
482
SW-3
5-Nov-13
DRY
DRY
SW-3
6-May-14
17.70JI
301
1 2.41 0.22.130.16 158.3
1 39.9
1 67,600E 121.4131
9,250 1
129.4.113.71J
1 10.2111011
354
530
1 71
1 440
1 1,430
SW-3
4-Nov-14
DRY
DRY
SW-3
5-May-15
DRY
DRY
SW-3
27-Oct-15
DRY
DRY
1302-CDLF-2006
SW-3
19-May-16
111.11
200
15.951
1 38.1117.11
22.4
1 59,700 1 48.11
576 1
115.51118.0
1 1 0.31J 1 180
1 85.3
25
1 3.2
1 471
I 908H-02
SW-3
3-Nov-16
DRY
DRY
SW-3
10-May-17
2.071 14.37.11
166
10.68.11 0.08.11
11.2 117.8
1 14.0
19,93013-0113.16.11
2,770 1
1 8.85J I 2.78J
I T0,06JTl6.7JF
442
60
1 16
1 1901
1 451
SW-3
31-Oct-17
DRY
DRY
SW-3
12-Jun-18
DRY
DRY
SW-3
18-Jan-19
10.1
1 2711
164
10.28.11
1 112 9.1J
8.9J
1 3,440 1 2.2.1
1 3,130 1
1 12.8J I 2.4J
1 1 47.61
23.8
1,100
1 100
1 389
2,220
SW-3
7-May-19
DRY
DRY
SW-3
7-Nov-19
DRY
DRY
SW-3
SW-3
20-May-20
25-Sep-20
0.33.1
1 2.6.1
1.9.1
72.2
34
1 0.31J
0.18J
10.2
2.5J
2.5J
11.5
6.2
6,190
1,800
5.2
0.99J
185
42
3.1J
2.1J
24.0
6.5
36.8
5.8.1
40.3
2.87
31.3
164
Notes:
1. Metal concentrations are in micrograms per liter (parts per billion).
2. General chemistry concentrations are in milligrams per liter (parts per million).
3. Standards obtained from section 15A NCAC 02B .0211 (North Carolina 26) or In -Stream Target Value Surface Water Standards for Class C Waters (June 2019).
4. (4) - A Standard for total chromium has not been established. The value provided is for chromium (III).
5. * - North Carolina In -Stream Target Value
6. NS - No Standard
7. J - Indicates the analytical result is an estimated concentration between the method detection limit and the adjusted reporting limit.
8. B, B-01 - The analyte concentration detected in the method blank was greater than the method detection limit.
9. H-02 - Total dissolved solids analysis was analyzed outside of hold time for SW-3.
Concentration exceeds the North Carolina 2B or In -Stream Target Value Freshwater Aquatic Life Standard for Class C Waters
Indicates the result is below the detection limit.
DM Page 8 of 9 December 2020

Table 3d
Detected Surface Water Constituents - Volatile Organic Compounds
September 2020 Semi -Annual Sampling Event
Cabarrus County C&D Landfill
Facility Permit Number 1302-CDLF-2006
Facility Permit
Number
Surface
Water Code
2B or In -Stream
Aquatic Life
Sample
Date
Target
Standard
GJ
C
c a c ^
}+ N (6 0
°; 3 c
N L
U
2,000* NS 26,000* 100*
v
C c
v i0 L
C C 7
W
X c CL
N R
o x ^' s
v o
r-I' W N 41 ++
N H
NS 97* NS 26,000* 110,000* 11
North Carolina
Value Freshwater
Notes:
1. Volatile organic compound concentrations are in micrograms per liter (parts per billion).
2. Standards obtained from section 15A NCAC 02B .0211 (North Carolina 2B) or In -Stream Target Value Surface Water
Standards for Class C Waters (June 2019).
3. * - North Carolina In -Stream Target Value
4. NS - No Standard
5. J - Indicates the analytical result is an estimated concentration between the method detection limit and the
adjusted reporting limit.
- Concentration exceeds the North Carolina 2B or In -Stream Target Value Freshwater Aquatic Life
Standard for Class C Waters
- Indicates the result is below the detection limit.
DM Page 9 of 9 December 2020

N
W+E
TVs
MGW-15
MGW-1
-i# CD-1s
o\ 733.75 CD-1tl MGW-14
SW-3
733.48
1 9°
°'O ` CD-4 Rep 4 -
CD-2\ C&D` ` 730.52 M
722.43 Landfill
> ,1ti0
CD-7-\
706.76
CD-9
706.15�
Unit 2
-
----I
o MGW-17
I
_
-----_
Unit'
—`—�710
700.83
MGW-2
689.38
MW-10
MW-8A '
/
693.14
710.17"
MGW-16
695.49
MW
/MW-G
707.06
I 685.86
680.980.96
MW-11
690
MW-X
�
/U
_
� '
678.32
�
t 3 � MW-6
MGW-13
p MGW-12
7
700.62 I nl
- 1 679.18 6a ,. Borrow Area
MGW-3� 'MW-E Rep
0
y
>. I 686.55 i SW-1
690 MW-DM67627deep,
MW-F
/
MW� 696.64 :.;,I 1 672.87
.1 / - - '
685.43 `
/ ,
-670
MGW-8
MW-K 1 -i
682.20-;t1r:.., / MW-1
MGW-4� AMW-1d1-*i 665.85 - -
- 660
580 67Z33.\
'SW-2
- AMW-1s
MW-H Mw5 l
MGW-7
676.70� �-
MW-H deep AMW-2s /MW-3 yy°
676.22 fi74.43 65749/
670
AMW-2tl °� / MW69
677.59 649.69
6y 658.18 6y°
MW-3 deep MGW-6
MW-L deep 659.66
659.90
MGW-5
Scale in Feet
0 Soo 1000
Map Data Source: 2015 Aerial Photograph, Cabarrus County, North Carolina OneMap.
MGW-11
MGW-10
MGW-9
Is
AXH:11Iww,
Groundwater Monitoring Well
Surface Water Sample Location
♦ Landfill Gas Well Location
Potentiometric Contour
680 — (dashed where inferred(
Contour Interval = 10 Feet

Appendix A

aceAnalytical
Report of Analysis
CDM Smith
5400 Glenwood Avenue
Suite 400
Raleigh, NC 27612
Attention: Mathew Colone
Project Name: Cabarrus County LF Background Wells
Lot Number:V124026
Date Completed:10/18/2020
10/18/2020 12:34 PM
Approved and released by:
Project Manager 11: Cathy S. Dover
=w�4 aecRFo���A16
TNI /
AM Amflvue Acm^rmm Fvu rj
('
4eOfFAi�
ACC R E OI TEO
TESTINGL aORlTOAY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 50

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
CDM Smith
Lot Number: V124026
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
BOD
The seed correction factor was above the method range of 0.6 to 1.0 for V124026-001 (CD-1 s).
SCF=1.44.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 50

PACE ANALYTICAL SERVICES, LLC
Sample Summary
CDM Smith
Lot Number: V124026
Project Name: Cabarrus County LF Background Wells
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 CD-1s Aqueous 09/23/2020 0830 09/24/2020
002 CD-1d Aqueous 09/22/20201700 09/24/2020
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 50

PACE ANALYTICAL SERVICES, LLC
Detection Summary
CDM Smith
Lot Number: V124026
Project Name: Cabarrus County LF Background Wells
Project Number:
Sample Sample ID
Matrix
Parameter
Method Result
Q
Units
Page
001
CD-1s
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
51
mg
5
001
CD-1s
Aqueous
Chloride
9056A
5.5
mg/L
5
001
CD-1s
Aqueous
CO2 (calculation)
SM 4500-CO2
96
mg/L
5
001
CD-1s
Aqueous
Nitrate - N
9056A
0.21
mg/L
5
001
CD-1s
Aqueous
Sulfate
9056A
2.5
mg/L
5
001
CD-1s
Aqueous
TDS
SM 2540C-
140
mg/L
5
001
CD-1s
Aqueous
Methane
RSK - 175
5.9
J
ug/L
8
001
CD-1s
Aqueous
Barium
6020B
34
ug/L
10
001
CD-1s
Aqueous
Chromium
6020B
1.3
J
ug/L
10
001
CD-1s
Aqueous
Copper
6020B
1.5
J
ug/L
10
001
CD-1s
Aqueous
Iron
6020B
630
ug/L
10
001
CD-1s
Aqueous
Manganese
6020B
21
ug/L
10
001
CD-1s
Aqueous
Vanadium
6020B
4.9
J
ug/L
10
001
CD-1s
Aqueous
Zinc
6020B
4.2
J
ug/L
10
002
CD-1d
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
53
mg
11
002
CD-1d
Aqueous
Chloride
9056A
3.1
mg/L
11
002
CD-1d
Aqueous
Sulfate
9056A
2.0
mg/L
11
002
CD-1d
Aqueous
TDS
SM 2540C-
130
mg/L
11
002
CD-1d
Aqueous
Antimony
6020B
0.67
J
ug/L
15
002
CD-1d
Aqueous
Barium
6020B
38
ug/L
15
002
CD-1d
Aqueous
Chromium
6020B
1.9
J
ug/L
15
002
CD-1d
Aqueous
Copper
6020B
8.6
ug/L
15
002
CD-1d
Aqueous
Iron
6020B
2300
ug/L
15
002
CD-1d
Aqueous
Lead
6020B
0.99
J
ug/L
15
002
CD-1d
Aqueous
Manganese
6020B
47
ug/L
15
002
CD-1d
Aqueous
Nickel
6020B
4.2
J
ug/L
15
002
CD-1d
Aqueous
Vanadium
6020B
8.8
ug/L
15
002
CD-1d
Aqueous
Zinc
6020B
36
ug/L
15
(28 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 50

Inorganic non-metals
Client:CDM Smith Laboratory ID:VI24026-001
Description: CD-1s Matrix: Aqueous
Date Sampled:09/23/2020 0830 Project Name: Cabarrus County LF
Date Received: 09/24/2020 Project Number:
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(Alkalinity @) SM 2320B-2011
1
09/28/2020 1221 AAB
68132
1
(BOD, 5 day) SM 521OB-2011
1
09/29/2020 1456 MOM
09/24/2020 1859 13595
1
(Chloride) 9056A
1
09/24/2020 2234 AMR
67957
1
(CO2 (calcula) SM 4500-CO2 D
1
09/28/2020 1221 AAB
1
(COD) SM 5220D-2011
1
10/03/2020 2053 SRB
68746
1
(Nitrate - N) 9056A
1
09/24/2020 2234 AMR
67959
1
(Sulfate) 9056A
1
09/24/2020 2234 AMR
67954
1
(TDS) SM 2540C-2011
1
09/27/2020 1820 MOM
68070
1
(TOC) SM 531OC-2011
1
10/01/2020 1842 DMA
68547
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
51
20
20
mg CaCO3/L
1
BOD, 5 day
SM 521 OB-2011
2.0
U7
2.0
0.18
mg/L
1
Chloride
9056A
5.5
1.0
0.20
mg/L
1
CO2 (calculation)
124-38-9 SM 4500-CC2 D
96
27
27
mg/L
1
COD
SM 5220D-2011
20
U
20
20
mg/L
1
Nitrate - N
9056A
0.21
0.020
0.0050
mg/L
1
Sulfate
9056A
2.5
1.0
0.20
mg/L
1
TDS
SM 2540C-2011
140
25
25
mg/L
1
TOC
SM 531OC-2011
1.0
U
1.0
1.0
mg/L
1
Footnote(s): 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 50

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24026-001
Description: CD-1s Matrix: Aqueous
Date Sampled:09/23/2020 0830 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/28/20201839 TML
68113
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.50
U
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
5.0
U
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.50
U
0.50
0.40
ug/L
1
Footnote(s): 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 50

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24026-001
Description: CD-1s Matrix: Aqueous
Date Sampled:09/23/2020 0830 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/28/20201839 TML 68113
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
0.50
U
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
105 70-130
1,2-Dichloroethane-d4
112 70-130
Toluene-d8
98 70-130
Footnote(s): 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 50

Dissolved Gases
Client:CDM Smith Laboratory ID:VI24026-001
Description: CD-1s Matrix: Aqueous
Date Sampled:09/23/2020 0830 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 10/01/2020 1348 TML 68503
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1
Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1
Methane 74-82-8 RSK - 175 5.9 J 10 2.5 ug/L 1
Footnote(s): 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 50

CVAA
Client:CDM Smith Laboratory ID:VI24026-001
Description: CD-1s Matrix: Aqueous
Date Sampled:09/23/2020 0830 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 09/25/2020 1509 JA132 09/25/2020 1000 67859
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1
Footnote(s): 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 50

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24026-001
Description: CD-1s Matrix: Aqueous
Date Sampled:09/23/2020 0830 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method
1 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/06/2020 0218 BPK
Prep Date Batch
10/03/2020 1555 68279
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
2.0
U
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
2.0
U
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
34
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.40
U
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.50
U
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
1.3
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
5.0
U
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
1.5
J
5.0
1.3
ug/L
1
Iron
7439-89-6
6020B
630
50
13
ug/L
1
Lead
7439-92-1
6020B
1.0
U
1.0
0.25
ug/L
1
Manganese
7439-96-5
6020B
21
5.0
1.3
ug/L
1
Nickel
7440-02-0
6020B
5.0
U
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.50
U
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
4.9
J
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
4.2
J
10
2.5
ug/L
1
Footnote(s): 7-SCF Out of range
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 50

Inorganic non-metals
Client:CDM Smith Laboratory ID:VI24026-002
Description: CD-1d Matrix: Aqueous
Date Sampled:09/22/2020 1700 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1
09/28/2020 1227 AAB
68132
1
(Chloride) 9056A
1
10/01/2020 2333 AMR
68633
1
(Sulfate) 9056A
1
10/01/2020 2333 AMR
68625
1
(TDS) SM 2540C-2011
1
09/27/2020 1820 MOM
68070
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Alkalinity @ pH 4.5 su
Chloride
Sulfate
TDS
SM 2320B-2011
53
20
20
mg CaCO3/L 1
9056A
3.1
1.0
0.20
mg/L 1
9056A
2.0
1.0
0.20
mg/L 1
SM 254OC-2011
130
25
25
mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 50

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24026-002
Description: CD-1d Matrix: Aqueous
Date Sampled:09/22/2020 1700 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/28/20201901 TML
68113
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.50
U
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
5.0
U
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.50
U
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 50

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24026-002
Description: CD-1d Matrix: Aqueous
Date Sampled:09/22/2020 1700 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/28/20201901 TML 68113
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
0.50
U
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
100 70-130
1,2-Dichloroethane-d4
110 70-130
Toluene-d8
103 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 50

CVAA
Client:CDM Smith Laboratory ID:VI24026-002
Description: CD-1d Matrix: Aqueous
Date Sampled:09/22/2020 1700 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 09/25/2020 1511 JA132 09/25/2020 1000 67859
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 50

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24026-002
Description: CD-1d Matrix: Aqueous
Date Sampled:09/22/2020 1700 Project Name: Cabarrus County LF
Date Received:09/24/2020 Project Number:
Run Prep Method
1 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/06/2020 0225 BPK
Prep Date Batch
10/03/2020 1555 68279
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
0.67
J
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
2.0
U
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
38
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.40
U
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.50
U
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
1.9
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
5.0
U
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
8.6
5.0
1.3
ug/L
1
Iron
7439-89-6
6020B
2300
50
13
ug/L
1
Lead
7439-92-1
6020B
0.99
J
1.0
0.25
ug/L
1
Manganese
7439-96-5
6020B
47
5.0
1.3
ug/L
1
Nickel
7440-02-0
6020B
4.2
J
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.50
U
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
8.8
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
36
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 50

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 50

Inorganic non-metals - MB
Sample ID: VQ67954-001 Matrix: Aqueous
Batch: 67954
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate 1.0 U 1 1.0 0.20 mg/L 09/24/2020 2138
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ67954-002 Matrix: Aqueous
Batch: 67954
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 20 1 101 80-120 09/24/2020 2215
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MB
Sample ID: VQ67957-001 Matrix: Aqueous
Batch: 67957
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride 1.0 U 1 1.0 0.20 mg/L 09/24/2020 2138
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ67957-002 Matrix: Aqueous
Batch: 67957
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 21 1 103 80-120 09/24/2020 2215
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MB
Sample ID: VQ67959-001 Matrix: Aqueous
Batch: 67959
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Nitrate - N 0.020 U 1 0.020 0.0050 mg/L 09/24/2020 2138
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ67959-002 Matrix: Aqueous
Batch: 67959
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.80 0.82 1 102 80-120 09/24/2020 2215
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MB
Sample ID: VQ68070-001 Matrix: Aqueous
Batch:68070
Analytical Method: SM 2540C-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
TDS 25 U 1 25 25 mg/L 09/27/20201820
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ68070-002 Matrix: Aqueous
Batch:68070
Analytical Method: SM 2540C-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TDS 1500 1500 1 101 90-110 09/27/20201820
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ68132-002 Matrix: Aqueous
Batch: 68132
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg CaCO3/L) (mg CaCO3/LP Dil % Rec Limit Analysis Date
Alkalinity @ pH 4.5 su 100 100 1 103 90-110 09/28/2020 1210
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MB
Sample ID: VQ68547-001 Matrix: Aqueous
Batch: 68547
Analytical Method: SM 531 OC-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
TOC 1.0 U 1 1.0 1.0 mg/L 10101120201749
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ68547-002 Matrix: Aqueous
Batch: 68547
Analytical Method: SM 531 OC-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TOC 20 20 1 100 90-110 10101120201802
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MS
Sample ID: V124026-001MS Matrix: Aqueous
Batch: 68547
Analytical Method: SM 531 OC-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TOC 0.0 50 49 1 98 70-130 10101120201855
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MSD
Sample ID: V124026-001MD Matrix: Aqueous
Batch: 68547
Analytical Method: SM 531 OC-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
TOC 0.0 50 48 1 96 2.3 70-130 20 10101120201908
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MB
Sample ID: VQ68625-001 Matrix: Aqueous
Batch: 68625
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate 1.0 U 1 1.0 0.20 mg/L 10101120201830
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ68625-002 Matrix: Aqueous
Batch: 68625
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 18 1 90 80-120 10101120201908
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MB
Sample ID: VQ68633-001 Matrix: Aqueous
Batch:68633
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride 1.0 U 1 1.0 0.20 mg/L 10101120201830
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ68633-002 Matrix: Aqueous
Batch:68633
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 19 1 96 80-120 10101120201908
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - MB
Sample ID: VQ68746-001 Matrix: Aqueous
Batch:68746
Analytical Method: SM 5220D-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
COD 20 U 1 20 20 mg/L 10/03/2020 2051
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 50
QC Data for Lot Number: V124026

Inorganic non-metals - LCS
Sample ID: VQ68746-002 Matrix: Aqueous
Batch:68746
Analytical Method: SM 5220D-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
COD 40 40 1 101 95-105 10/03/2020 2052
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 50
QC Data for Lot Number: V124026

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ68113-001 Matrix: Aqueous
Batch: 68113 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
10
U
1
10
4.0
ug/L
09/28/2020 1235
Acrylonitrile
5.0
U
1
5.0
0.80
ug/L
09/28/2020 1235
Benzene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Bromochloromethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Bromodichloromethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Bromoform
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Bromomethane (Methyl bromide)
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
2-Butanone (MEK)
10
U
1
10
2.0
ug/L
09/28/2020 1235
Carbon disulfide
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Carbon tetrachloride
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Chlorobenzene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Chloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Chloroform
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Chloromethane (Methyl chloride)
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
1,2-Dibromo-3-chloropropane (DBCP)
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Dibromochloromethane
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1235
1,2-Dibromoethane (EDB)
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1235
Dibromomethane (Methylene bromide)
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1235
trans- 1,4-Dichloro-2-butene
2.0
u
1
2.0
0.40
ug/L
09/28/2020 1235
1,2-Dichlorobenzene
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1235
1,4-Dichlorobenzene
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1235
1,1-Dichloroethane
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1235
1,2-Dichloroethane
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1235
1,1-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
cis- 1,2-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
trans- 1,2-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
1,2-Dichloropropane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
cis- 1,3-Dichloropropene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
trans- 1,3-Dichloropropene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Ethylbenzene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
2-Hexanone
10
U
1
10
2.0
ug/L
09/28/2020 1235
Methacrylonitrile
5.0
U
1
5.0
2.0
ug/L
09/28/2020 1235
Methyl iodide (lodomethane)
5.0
U
1
5.0
0.40
ug/L
09/28/2020 1235
4-Methyl-2-pentanone
10
U
1
10
2.0
ug/L
09/28/2020 1235
Methylene chloride
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Styrene
0.50
U
1
0.50
0.41
ug/L
09/28/2020 1235
1,1,1,2-Tetrachloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
1,1,2,2-Tetrachloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Tetrachloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Tetrahydrofuran
5.0
U
1
5.0
1.0
ug/L
09/28/2020 1235
Toluene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
1,1,1-Trichloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
1,1,2-Trichloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Trichloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 36 of 50
QC Data for Lot Number: V124026

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ68113-001 Matrix: Aqueous
Batch: 68113 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Trichlorofluoromethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
1,2,3-Trichloropropane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Vinyl acetate
5.0
U
1
5.0
1.2
ug/L
09/28/2020 1235
Vinyl chloride
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1235
Xylenes (total)
1.0
U
1
1.0
0.40
ug/L
09/28/2020 1235
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 95 70-130
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 37 of 50

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ68113-002
Matrix: Aqueous
Batch: 68113
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
90
1
90
60-140
09/28/2020 1014
Acrylonitrile
100
97
1
97
70-130
09/28/2020 1014
Benzene
50
50
1
99
70-130
09/28/2020 1014
Bromochloromethane
50
52
1
103
70-130
09/28/2020 1014
Bromodichloromethane
50
49
1
98
70-130
09/28/2020 1014
Bromoform
50
49
1
98
70-130
09/28/2020 1014
Bromomethane (Methyl bromide)
50
47
1
94
70-130
09/28/2020 1014
2-Butanone (MEK)
100
93
1
93
70-130
09/28/2020 1014
Carbon disulfide
50
51
1
102
70-130
09/28/2020 1014
Carbon tetrachloride
50
46
1
92
70-130
09/28/2020 1014
Chlorobenzene
50
50
1
100
70-130
09/28/2020 1014
Chloroethane
50
48
1
96
70-130
09/28/2020 1014
Chloroform
50
47
1
94
70-130
09/28/2020 1014
Chloromethane (Methyl chloride)
50
46
1
92
60-140
09/28/2020 1014
1,2-Dibromo-3-chloropropane (DBCP)
50
48
1
96
70-130
09/28/2020 1014
Dibromochloromethane
50
49
1
98
70-130
09/28/2020 1014
1,2-Dibromoethane (EDB)
50
50
1
99
70-130
09/28/2020 1014
Dibromomethane (Methylene bromide)
50
46
1
92
70-130
09/28/2020 1014
trans- 1,4-Dichloro-2-butene
50
49
1
97
70-130
09/28/2020 1014
1,2-Dichlorobenzene
50
49
1
98
70-130
09/28/2020 1014
1,4-Dichlorobenzene
50
51
1
102
70-130
09/28/2020 1014
1,1-Dichloroethane
50
49
1
97
70-130
09/28/2020 1014
1,2-Dichloroethane
50
47
1
93
70-130
09/28/2020 1014
1,1-Dichloroethene
50
50
1
99
70-130
09/28/2020 1014
cis- 1,2-Dichloroethene
50
50
1
100
70-130
09/28/2020 1014
trans- 1,2-Dichloroethene
50
49
1
98
70-130
09/28/2020 1014
1,2-Dichloropropane
50
48
1
96
70-130
09/28/2020 1014
cis- 1,3-Dichloropropene
50
49
1
98
70-130
09/28/2020 1014
trans- 1,3-Dichloropropene
50
50
1
101
70-130
09/28/2020 1014
Ethylbenzene
50
50
1
100
70-130
09/28/2020 1014
2-Hexanone
100
83
1
83
70-130
09/28/2020 1014
Methacrylonitrile
250
240
1
96
70-130
09/28/2020 1014
Methyl iodide (lodomethane)
50
49
1
98
70-130
09/28/2020 1014
4-Methyl-2-pentanone
100
87
1
87
70-130
09/28/2020 1014
Methylene chloride
50
48
1
95
70-130
09/28/2020 1014
Styrene
50
50
1
100
70-130
09/28/2020 1014
1,1,1,2-Tetrachloroethane
50
46
1
93
70-130
09/28/2020 1014
1,1,2,2-Tetrachloroethane
50
48
1
95
70-130
09/28/2020 1014
Tetrachloroethene
50
49
1
99
70-130
09/28/2020 1014
Tetrahydrofuran
50
45
1
90
70-130
09/28/2020 1014
Toluene
50
52
1
104
70-130
09/28/2020 1014
1,1,1-Trichloroethane
50
51
1
102
70-130
09/28/2020 1014
1,1,2-Trichloroethane
50
48
1
96
70-130
09/28/2020 1014
Trichloroethene
50
51
1
102
70-130
09/28/2020 1014
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 38 of 50
QC Data for Lot Number: V124026

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ68113-002
Matrix: Aqueous
Batch: 68113
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Trichlorofluoromethane
50
46
1 92
70-130
09/28/2020 1014
1,2,3-Trichloropropane
50
46
1 91
70-130
09/28/2020 1014
Vinyl acetate
50
52
1 105
60-140
09/28/2020 1014
Vinyl chloride
50
46
1 93
70-130
09/28/2020 1014
Xylenes (total)
100
100
1 101
70-130
09/28/2020 1014
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 98 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 50

Dissolved Gases - MB
Sample ID: VQ68503-001 Matrix: Aqueous
Batch: 68503
Analytical Method: RSK - 175
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Ethane
10
U
1
10
2.5
ug/L
10/01/20201112
Ethene
10
U
1
10
2.5
ug/L
10/01/20201112
Methane
10
U
1
10
2.5
ug/L
10/01/20201112
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 50
QC Data for Lot Number: V124026

Dissolved Gases - LCS
Sample ID: VQ68503-002 Matrix: Aqueous
Batch: 68503
Analytical Method: RSK - 175
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec
Limit
Analysis Date
Ethane
550
630 1
114
70-130
10/01/20201022
Ethene
520
570 1
ill
70-130
10/01/2020 1022
Methane
300
330 1
113
70-130
10/01/20201022
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 50
QC Data for Lot Number: V124026

ICP-MS Metals - MB
Sample ID: VQ68279-001 Matrix: Aqueous
Batch: 68279 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 10/03/2020 1555
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
2.0
U
1
2.0
0.50
ug/L
10/06/2020 0118
Arsenic
2.0
U
1
2.0
1.3
ug/L
10/06/2020 0118
Barium
5.0
U
1
5.0
1.3
ug/L
10/06/2020 0118
Beryllium
0.40
U
1
0.40
0.15
ug/L
10/06/2020 0118
Cadmium
0.50
U
1
0.50
0.13
ug/L
10/06/2020 0118
Chromium
5.0
U
1
5.0
1.3
ug/L
10/06/2020 0118
Cobalt
5.0
U
1
5.0
1.3
ug/L
10/06/2020 0118
Copper
5.0
U
1
5.0
1.3
ug/L
10/06/2020 0118
Iron
50
U
1
50
13
ug/L
10/06/2020 0118
Lead
1.0
U
1
1.0
0.25
ug/L
10/06/2020 0118
Manganese
5.0
U
1
5.0
1.3
ug/L
10/06/2020 0118
Nickel
5.0
U
1
5.0
1.3
ug/L
10/06/2020 0118
Selenium
5.0
U
1
5.0
1.3
ug/L
10/06/2020 0118
Silver
1.0
U
1
1.0
0.25
ug/L
10/06/2020 0118
Thallium
0.50
U
1
0.50
0.15
ug/L
10/06/2020 0118
Vanadium
5.0
U
1
5.0
2.5
ug/L
10/06/2020 0118
Zinc
10
U
1
10
2.5
ug/L
10/06/2020 0118
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 42 of 50
QC Data for Lot Number: V124026

ICP-MS Metals - LCS
Sample ID: VQ68279-002
Matrix: Aqueous
Batch: 68279
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 10/03/2020 1555
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
Antimony
100
93
1 93
80-120
10/06/2020 0125
Arsenic
100
98
1 98
80-120
10/06/2020 0125
Barium
100
95
1 95
80-120
10/06/2020 0125
Beryllium
100
90
1 90
80-120
10/06/2020 0125
Cadmium
100
95
1 95
80-120
10/06/2020 0125
Chromium
100
98
1 98
80-120
10/06/2020 0125
Cobalt
100
110
1 107
80-120
10/06/2020 0125
Copper
100
110
1 109
80-120
10/06/2020 0125
Iron
1000
960
1 96
80-120
10/06/2020 0125
Lead
100
97
1 97
80-120
10/06/2020 0125
Manganese
100
100
1 100
80-120
10/06/2020 0125
Nickel
100
110
1 108
80-120
10/06/2020 0125
Selenium
100
85
1 85
80-120
10/06/2020 0125
Silver
100
100
1 103
80-120
10/06/2020 0125
Thallium
100
96
1 96
80-120
10/06/2020 0125
Vanadium
100
94
1 94
80-120
10/06/2020 0125
Zinc
100
92
1 92
80-120
10/06/2020 0125
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 50
QC Data for Lot Number: V124026

CVAA -MB
Sample ID: VQ67859-001 Matrix: Aqueous
Batch: 67859 Prep Method:
Analytical Method: 7470A Prep Date: 09/25/2020 1000
Parameter Result Q Dil LOQ DL Units Analysis Date
Mercury 0.00020 U 1 0.00020 0.000091 mg/L 09/25/20201504
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 44 of 50
QC Data for Lot Number: V124026

CVAA - LCS
Sample ID: VQ67859-002 Matrix: Aqueous
Batch: 67859 Prep Method:
Analytical Method: 7470A Prep Date: 09/25/2020 1000
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury 0.0020 0.0018 1 92 80-120 09/25/20201506
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 50
QC Data for Lot Number: V124026

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 46 of 50

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 47 of 50

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 48 of 50

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 49 of 50

PACE ANALYTICAL SERVICES, LLC
Sbpmly Prvircmrrn[il Seninm, Iro. Pap 1 M".
1;cgwmcnt n urn": MUP 1 Br_-1 a 1:1fidiv a VOW. it -F3U 16
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PM $trip JD; Nd !LodneStrip JD; NA- 'ICrXl.EJhy:NA
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❑ Yes
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formation (ID, date, time) Pgma with thy, COC?
0 Yes
❑ ML5
11. Were msrs to be perfatlm
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(unhmken, tier, ion, Mtn.)?
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the proper containers for each D5t arlr:/ci' i1L gOOLL cnndiliOr,
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Yes
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Yes
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Yes
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c0c into tht- comment section bi I..1 h1S?
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4, iJND3, 14C1, NaOH using SR # NA
Servod-m is nodded, please note it the cgrnmcnts below,
5arrlple{s) NA --
w4ro reseiv ed with laul�trl rx r-%0 rr m in c;iameter_
Samples(s) .NA _ _
were received with TR C; > CI.5 mg,'L (If fl t 9 is true) w id wore
!adjusted accnrrlinCly in ssln•1plo mcpNing widi sodiu:11 l LinwLdfa#e (i ataS3 s) whit Shealy ID: NA
'SR baroode labels o;aplicd by: JSI I Date, 09,�2C+2020
Conunent�.AMWSANIPLF51.,4BCL.GD.4;Slhf%1ltON a3N1'TATNERS_
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 50 of 50

aceAnalytical
Report of Analysis
CDM Smith
5400 Glenwood Avenue
Suite 400
Raleigh, NC 27612
Attention: Mathew Colone
Project Name: Cabarrus Co. C&D LF
Lot Number:V124036
Date Completed:10/12/2020
10/21/2020 10:43 PM
Approved and released by:
Project Manager 11: Cathy S. Dover
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TNI /
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ACC R E OI TEO
TESTINGL aORlTOAY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
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Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 81

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
CDM Smith
Lot Number: V124036
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
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Page 2 of 81

PACE ANALYTICAL SERVICES, LLC
Sample Summary
CDM Smith
Lot Number: V124036
Project Name: Cabarrus Co. C&D LF
Project Number:
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
CD-7
Aqueous
09/22/20201745
09/24/2020
002
CD-9
Aqueous
09/22/20201745
09/24/2020
003
CD DUP
Aqueous
09/22/2020 1730
09/24/2020
004
Trip Blank
Aqueous
09/22/2020
09/24/2020
005
CD-2
Aqueous
09/25/2020 0915
09/26/2020
006
SW-3
Aqueous
09/25/2020 0925
09/26/2020
007
EQ BLANK
Aqueous
09/25/2020 1455
09/26/2020
(7 samples)
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Page 3 of 81

PACE ANALYTICAL SERVICES, LLC
Detection Summary
CDM Smith
Lot Number: V124036
Project Name: Cabarrus Co. C&D LF
Project Number:
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
CD-7
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
170
mg
7
001
CD-7
Aqueous
Chloride
9056A
23
mg/L
7
001
CD-7
Aqueous
Sulfate
9056A
56
mg/L
7
001
CD-7
Aqueous
TDS
SM 2540C-
370
mg/L
7
001
CD-7
Aqueous
Benzene
8260D
0.95
ug/L
8
001
CD-7
Aqueous
Chloroethane
8260D
0.69
ug/L
8
001
CD-7
Aqueous
1,1-Dichloroethane
8260D
1.4
ug/L
8
001
CD-7
Aqueous
cis- 1,2-Dichloroethene
8260D
2.8
ug/L
8
001
CD-7
Aqueous
Methylene chloride
8260D
0.80
ug/L
8
001
CD-7
Aqueous
Tetrachloroethene
8260D
0.57
ug/L
8
001
CD-7
Aqueous
Tetrahydrofuran
8260D
9.2
ug/L
8
001
CD-7
Aqueous
Trichlorofluoromethane
8260D
1.6
ug/L
9
001
CD-7
Aqueous
Vinyl chloride
8260D
1.6
ug/L
9
001
CD-7
Aqueous
Barium
6020B
180
ug/L
11
001
CD-7
Aqueous
Beryllium
6020B
0.39
J
ug/L
11
001
CD-7
Aqueous
Cadmium
6020B
0.25
J
ug/L
11
001
CD-7
Aqueous
Chromium
6020B
1.5
J
ug/L
11
001
CD-7
Aqueous
Cobalt
6020B
8.4
ug/L
11
001
CD-7
Aqueous
Copper
6020B
25
ug/L
11
001
CD-7
Aqueous
Iron
6020B
1100
ug/L
11
001
CD-7
Aqueous
Lead
6020B
1.3
ug/L
11
001
CD-7
Aqueous
Manganese
6020B
3100
ug/L
11
001
CD-7
Aqueous
Nickel
6020B
14
ug/L
11
001
CD-7
Aqueous
Thallium
6020B
0.25
J
ug/L
11
001
CD-7
Aqueous
Vanadium
6020B
5.4
ug/L
11
001
CD-7
Aqueous
Zinc
6020B
7.9
J
ug/L
11
002
CD-9
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
130
mg
12
002
CD-9
Aqueous
Chloride
9056A
4.9
mg/L
12
002
CD-9
Aqueous
Sulfate
9056A
1.8
mg/L
12
002
CD-9
Aqueous
TDS
SM 2540C-
210
mg/L
12
002
CD-9
Aqueous
1,4-Dichlorobenzene
8260D
1.1
ug/L
13
002
CD-9
Aqueous
1,1-Dichloroethane
8260D
1.9
ug/L
13
002
CD-9
Aqueous
cis- 1,2-Dichloroethene
8260D
6.9
ug/L
13
002
CD-9
Aqueous
Trichloroethene
8260D
0.42
J
ug/L
13
002
CD-9
Aqueous
Trichlorofluoromethane
8260D
0.68
ug/L
14
002
CD-9
Aqueous
Barium
6020B
99
ug/L
16
002
CD-9
Aqueous
Chromium
6020B
1.6
J
ug/L
16
002
CD-9
Aqueous
Cobalt
6020B
1.4
J
ug/L
16
002
CD-9
Aqueous
Copper
6020B
8.9
ug/L
16
002
CD-9
Aqueous
Iron
6020B
1300
ug/L
16
002
CD-9
Aqueous
Manganese
6020B
160
ug/L
16
002
CD-9
Aqueous
Nickel
6020B
5.5
ug/L
16
002
CD-9
Aqueous
Vanadium
6020B
7.3
ug/L
16
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 81

Detection Summary (Continued)
Lot Number: V124036
Sample Sample ID Matrix Parameter Method Result Q Units Page
002
CD-9
Aqueous
Zinc
6020B
5.0
J
ug/L
003
CD DUP
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
130
mg
003
CD DUP
Aqueous
Chloride
9056A
4.9
mg/L
003
CD DUP
Aqueous
Sulfate
9056A
1.8
mg/L
003
CD DUP
Aqueous
TDS
SM 2540C-
200
mg/L
003
CD DUP
Aqueous
1,4-Dichlorobenzene
8260D
1.1
ug/L
003
CD DUP
Aqueous
1,1-Dichloroethane
8260D
2.0
ug/L
003
CD DUP
Aqueous
cis- 1,2-Dichloroethene
8260D
7.0
ug/L
003
CD DUP
Aqueous
Trichloroethene
8260D
0.42
J
ug/L
003
CD DUP
Aqueous
Trichlorofluoromethane
8260D
0.70
ug/L
003
CD DUP
Aqueous
Barium
6020B
170
ug/L
003
CD DUP
Aqueous
Beryllium
6020B
0.28
J
ug/L
003
CD DUP
Aqueous
Chromium
6020B
8.0
ug/L
003
CD DUP
Aqueous
Cobalt
6020B
6.3
ug/L
003
CD DUP
Aqueous
Copper
6020B
51
ug/L
003
CD DUP
Aqueous
Iron
6020B
9200
ug/L
003
CD DUP
Aqueous
Lead
6020B
1.3
ug/L
003
CD DUP
Aqueous
Manganese
6020B
300
ug/L
003
CD DUP
Aqueous
Nickel
6020B
9.0
ug/L
003
CD DUP
Aqueous
Vanadium
6020B
34
ug/L
003
CD DUP
Aqueous
Zinc
6020B
22
ug/L
004
Trip Blank
Aqueous
Methylene chloride
8260D
0.42
J
ug/L
005
CD-2
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
79
mg
005
CD-2
Aqueous
Chloride
9056A
9.4
mg/L
005
CD-2
Aqueous
Sulfate
9056A
2.9
mg/L
005
CD-2
Aqueous
TDS
SM 2540C-
230
mg/L
005
CD-2
Aqueous
Benzene
8260D
0.53
ug/L
005
CD-2
Aqueous
Chloroethane
8260D
0.59
ug/L
005
CD-2
Aqueous
1,1-Dichloroethane
8260D
6.7
ug/L
005
CD-2
Aqueous
cis-1,2-Dichloroethene
8260D
0.66
ug/L
005
CD-2
Aqueous
Barium
6020B
110
ug/L
005
CD-2
Aqueous
Beryllium
6020B
0.26
J
ug/L
005
CD-2
Aqueous
Chromium
6020B
4.6
J
ug/L
005
CD-2
Aqueous
Cobalt
6020B
2.9
J
ug/L
005
CD-2
Aqueous
Copper
6020B
7.8
ug/L
005
CD-2
Aqueous
Iron
6020B
3900
ug/L
005
CD-2
Aqueous
Lead
6020B
2.8
ug/L
005
CD-2
Aqueous
Manganese
6020B
110
ug/L
005
CD-2
Aqueous
Nickel
6020B
5.0
ug/L
005
CD-2
Aqueous
Vanadium
6020B
12
ug/L
005
CD-2
Aqueous
Zinc
6020B
13
ug/L
006
SW-3
Aqueous
Arsenic
6020B
1.9
J
ug/L
006
SW-3
Aqueous
Barium
6020B
34
ug/L
006
SW-3
Aqueous
Beryllium
6020B
0.18
J
ug/L
006
SW-3
Aqueous
Chromium
6020B
2.5
J
ug/L
006
SW-3
Aqueous
Copper
6020B
6.2
ug/L
006
SW-3
Aqueous
Iron
6020B
1800
ug/L
006
SW-3
Aqueous
Lead
6020B
0.99
J
ug/L
16
17
17
17
17
18
18
18
18
19
21
21
21
21
21
21
21
21
21
21
21
22
24
24
24
24
25
25
25
25
28
28
28
28
28
28
28
28
28
28
28
32
32
32
32
32
32
32
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 81

Detection Summary (Continued)
Lot Number: V124036
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
006 SW-3
Aqueous
Manganese
6020B
42
ug/L
32
006 SW-3
Aqueous
Nickel
6020B
2.1
J
ug/L
32
006 SW-3
Aqueous
Vanadium
6020B
6.5
ug/L
32
006 SW-3
Aqueous
Zinc
6020B
5.8
J
ug/L
32
007 EQ BLANK
Aqueous
Acetone
8260D
4.0
J
ug/L
34
(96 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 81

Inorganic non-metals
Client:CDM Smith Laboratory ID:VI24036-001
Description: CD-7 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1
09/28/2020 1355 AAB
68132
1
(Chloride) 9056A
1
10/01/2020 2352 AMR
68633
1
(Sulfate) 9056A
1
10/01/2020 2352 AMR
68625
1
(TDS) SM 2540C-2011
1
09/27/2020 1820 MOM
68070
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Alkalinity @ pH 4.5 su
Chloride
Sulfate
TDS
SM 2320B-2011
170
20
20
mg CaCO3/L 1
9056A
23
1.0
0.20
mg/L 1
9056A
56
1.0
0.20
mg/L 1
SM 254OC-2011
370
25
25
mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-001
Description: CD-7 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/28/20201753 TML
68138
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.95
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.69
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
1.4
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1, 1 -Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260D
2.8
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.80
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.57
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
9.2
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.50
U
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-001
Description: CD-7 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/28/20201753 TML 68138
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
1.6
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50 U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0 U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
1.6
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0 U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
94 70-130
Toluene-d8
92 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 81

CVAA
Client:CDM Smith Laboratory ID:VI24036-001
Description: CD-7 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 09/25/2020 1514 JA132 09/25/2020 1000 67859
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 81

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24036-001
Description: CD-7 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method
1 3005A
2 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/02/2020 2015 BPK
6020B 100 10/05/2020 1750 BPK
Prep Date Batch
10/01/2020 1546 68305
10/01/2020 1546 68305
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
2.0
U
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
2.0
U
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
180
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.39
J
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.25
J
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
1.5
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
8.4
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
25
5.0
1.3
ug/L
1
Iron
7439-89-6
6020B
1100
50
13
ug/L
1
Lead
7439-92-1
6020B
1.3
1.0
0.25
ug/L
1
Manganese
7439-96-5
6020B
3100
500
130
ug/L
2
Nickel
7440-02-0
6020B
14
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.25
J
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
5.4
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
7.9
J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 81

Inorganic non-metals
Client:CDM Smith Laboratory ID:VI24036-002
Description: CD-9 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1
09/28/2020 1402 AAB
68132
1
(Chloride) 9056A
1
10/02/2020 0011 AMR
68633
1
(Sulfate) 9056A
1
10/02/2020 0011 AMR
68625
1
(TDS) SM 2540C-2011
1
09/27/2020 1820 MOM
68070
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Alkalinity @ pH 4.5 su
Chloride
Sulfate
TDS
SM 2320B-2011
130
20
20
mg CaCO3/L 1
9056A
4.9
1.0
0.20
mg/L 1
9056A
1.8
1.0
0.20
mg/L 1
SM 254OC-2011
210
25
25
mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-002
Description: CD-9 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/28/20201817 TML
68138
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
1.1
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
1.9
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1, 1 -Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260D
6.9
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.50
U
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
5.0
U
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.42
J
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-002
Description: CD-9 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/28/20201817 TML 68138
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
0.68
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
94 70-130
Toluene-d8
94 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 81

CVAA
Client:CDM Smith Laboratory ID:VI24036-002
Description: CD-9 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 09/25/2020 1521 JA132 09/25/2020 1000 67859
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 81

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24036-002
Description: CD-9 Matrix: Aqueous
Date Sampled:09/22/2020 1745 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method
1 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/02/2020 2023 BPK
Prep Date Batch
10/01/2020 1546 68305
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
2.0
U
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
2.0
U
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
99
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.40
U
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.50
U
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
1.6
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
1.4
J
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
8.9
5.0
1.3
ug/L
1
Iron
7439-89-6
6020B
1300
50
13
ug/L
1
Lead
7439-92-1
6020B
1.0
U
1.0
0.25
ug/L
1
Manganese
7439-96-5
6020B
160
5.0
1.3
ug/L
1
Nickel
7440-02-0
6020B
5.5
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.50
U
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
7.3
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
5.0
J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 81

Inorganic non-metals
Client:CDM Smith Laboratory ID:VI24036-003
Description: CD DUP Matrix: Aqueous
Date Sampled:09/22/2020 1730 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1
09/28/2020 1409 AAB
68132
1
(Chloride) 9056A
1
10/02/2020 0030 AMR
68633
1
(Sulfate) 9056A
1
10/02/2020 0030 AMR
68625
1
(TDS) SM 2540C-2011
1
09/27/2020 1820 MOM
68070
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Alkalinity @ pH 4.5 su
Chloride
Sulfate
TDS
SM 2320B-2011
130
20
20
mg CaCO3/L 1
9056A
4.9
1.0
0.20
mg/L 1
9056A
1.8
1.0
0.20
mg/L 1
SM 254OC-2011
200
25
25
mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-003
Description: CD DUP Matrix: Aqueous
Date Sampled:09/22/2020 1730 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/28/20201841 TML
68138
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
1.1
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
2.0
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1, 1 -Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260D
7.0
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.50
U
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
5.0
U
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.42
J
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-003
Description: CD DUP Matrix: Aqueous
Date Sampled:09/22/2020 1730 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/28/20201841 TML 68138
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
0.70
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
95 70-130
Toluene-d8
95 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 81

CVAA
Client:CDM Smith Laboratory ID:VI24036-003
Description: CD DUP Matrix: Aqueous
Date Sampled:09/22/2020 1730 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 09/25/2020 1524 JA132 09/25/2020 1000 67859
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 81

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24036-003
Description: CD DUP Matrix: Aqueous
Date Sampled:09/22/2020 1730 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method
1 3005A
2 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/02/2020 2030 BPK
6020B 10 10/05/2020 1735 BPK
Prep Date Batch
10/01/2020 1546 68305
10/01/2020 1546 68305
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
2.0
U
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
2.0
U
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
170
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.28
J
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.50
U
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
8.0
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
6.3
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
51
5.0
1.3
ug/L
1
Iron
7439-89-6
6020B
9200
50
13
ug/L
1
Lead
7439-92-1
6020B
1.3
1.0
0.25
ug/L
1
Manganese
7439-96-5
6020B
300
50
13
ug/L
2
Nickel
7440-02-0
6020B
9.0
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.50
U
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
34
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
22
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-004
Description: Trip Blank Matrix: Aqueous
Date Sampled:09/22/2020 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/28/20201555 TML
68138
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.42
J
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
5.0
U
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.50
U
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-004
Description: Trip Blank Matrix: Aqueous
Date Sampled:09/22/2020 Project Name: Cabarrus Co. C&D LF
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/28/20201555 TML 68138
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
0.50
U
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
96 70-130
1,2-Dichloroethane-d4
95 70-130
Toluene-d8
94 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 81

Inorganic non-metals
Client:CDM Smith Laboratory ID:VI24036-005
Description: CD-2 Matrix: Aqueous
Date Sampled:09/25/2020 0915 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1
09/29/2020 1306 AAB
68349
1
(Chloride) 9056A
1
10/02/2020 0126 AMR
68633
1
(Sulfate) 9056A
1
10/02/2020 0126 AMR
68625
1
(TDS) SM 2540C-2011
1
09/30/2020 2353 MOM
68445
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Alkalinity @ pH 4.5 su
Chloride
Sulfate
TDS
SM 2320B-2011
79
20
20
mg CaCO3/L 1
9056A
9.4
1.0
0.20
mg/L 1
9056A
2.9
1.0
0.20
mg/L 1
SM 254OC-2011
230
25
25
mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-005
Description: CD-2 Matrix: Aqueous
Date Sampled:09/25/2020 0915 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/30/20201242 TML
68353
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.53
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.59
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
6.7
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1, 1 -Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260D
0.66
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.50
U
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
5.0
U
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.50
U
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-005
Description: CD-2 Matrix: Aqueous
Date Sampled:09/25/2020 0915 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/30/20201242 TML 68353
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
0.50
U
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
100 70-130
Toluene-d8
99 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 81

CVAA
Client:CDM Smith Laboratory ID:VI24036-005
Description: CD-2 Matrix: Aqueous
Date Sampled:09/25/2020 0915 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 09/29/2020 1803 JA132 09/29/2020 0933 68176
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 81

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24036-005
Description: CD-2 Matrix: Aqueous
Date Sampled:09/25/2020 0915 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method
1 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/01/2020 2337 BPK
Prep Date Batch
10/01/2020 0855 68268
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
2.0
U
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
2.0
U
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
110
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.26
J
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.50
U
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
4.6
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
2.9
J
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
7.8
5.0
1.3
ug/L
1
Iron
7439-89-6
6020B
3900
50
13
ug/L
1
Lead
7439-92-1
6020B
2.8
1.0
0.25
ug/L
1
Manganese
7439-96-5
6020B
110
5.0
1.3
ug/L
1
Nickel
7440-02-0
6020B
5.0
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.50
U
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
12
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
13
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-006
Description: SW-3 Matrix: Aqueous
Date Sampled:09/25/2020 0925 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/30/20201305 TML
68353
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.50
U
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
5.0
U
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.50
U
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-006
Description: SW-3 Matrix: Aqueous
Date Sampled:09/25/2020 0925 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/30/20201305 TML 68353
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
0.50
U
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
96 70-130
1,2-Dichloroethane-d4
99 70-130
Toluene-d8
98 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 81

Volatile Organic Compounds by GC/MS (SIM)
Client:CDM Smith Laboratory ID:VI24036-006
Description: SW-3 Matrix: Aqueous
Date Sampled:09/25/2020 0925 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D (SIM) 1 10/01/2020 1716 BWS 68512
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,4-Dioxane 123-91-1 8260D (SIM) 3.0 U 3.0 1.0 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4
109 40-170
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 81

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24036-006
Description: SW-3 Matrix: Aqueous
Date Sampled:09/25/2020 0925 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method
1 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/01/2020 2101 BPK
Prep Date Batch
10/01/2020 0855 68268
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
2.0
U
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
1.9
J
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
34
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.18
J
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.50
U
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
2.5
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
5.0
U
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
6.2
5.0
1.3
ug/L
1
Iron
7439-89-6
6020B
1800
50
13
ug/L
1
Lead
7439-92-1
6020B
0.99
J
1.0
0.25
ug/L
1
Manganese
7439-96-5
6020B
42
5.0
1.3
ug/L
1
Nickel
7440-02-0
6020B
2.1
J
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.50
U
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
6.5
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
5.8
J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 81

Inorganic non-metals
Client:CDM Smith Laboratory ID:VI24036-007
Description: EQ BLANK Matrix: Aqueous
Date Sampled:09/25/2020 1455 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1
09/29/2020 1311 AAB
68349
1
(Chloride) 9056A
1
10/02/2020 0223 AMR
68633
1
(Sulfate) 9056A
1
10/01/2020 2223 AMR
68625
1
(TDS) SM 2540C-2011
1
09/30/2020 2353 MOM
68445
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Alkalinity @ pH 4.5 su
Chloride
Sulfate
TDS
SM 2320B-2011
20
U
20
20
mg CaCO3/L 1
9056A
1.0
U
1.0
0.20
mg/L 1
9056A
1.0
U
1.0
0.20
mg/L 1
SM 2540C-2011
25
U
25
25
mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-007
Description: EQ BLANK Matrix: Aqueous
Date Sampled:09/25/2020 1455 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/30/2020 0956 TML
68353
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
4.0
J
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.50
U
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
5.0
U
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.50
U
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24036-007
Description: EQ BLANK Matrix: Aqueous
Date Sampled:09/25/2020 1455 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/30/2020 0956 TML 68353
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichlorofluoromethane
75-69-4
8260D
0.50
U
0.50
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
97 70-130
Toluene-d8
95 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 81

CVAA
Client:CDM Smith Laboratory ID:VI24036-007
Description: EQ BLANK Matrix: Aqueous
Date Sampled:09/25/2020 1455 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 1 09/29/2020 1811 JA132 09/29/2020 0933 68176
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 36 of 81

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24036-007
Description: EQ BLANK Matrix: Aqueous
Date Sampled:09/25/2020 1455 Project Name: Cabarrus Co. C&D LF
Date Received:09/26/2020 Project Number:
Run Prep Method
1 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/01/2020 2046 BPK
Prep Date Batch
10/01/2020 0855 68268
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
2.0
U
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
2.0
U
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
5.0
U
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.40
U
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.50
U
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
5.0
U
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
5.0
U
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
5.0
U
5.0
1.3
ug/L
1
Iron
7439-89-6
6020B
50
U
50
13
ug/L
1
Lead
7439-92-1
6020B
1.0
U
1.0
0.25
ug/L
1
Manganese
7439-96-5
6020B
5.0
U
5.0
1.3
ug/L
1
Nickel
7440-02-0
6020B
5.0
U
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.50
U
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
5.0
U
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
10
U
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 37 of 81

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24027-013
Description: CD-4 Rep Matrix: Aqueous
Date Sampled:09/23/2020 1730 Project Name: Cabarrus County LF Unit 2
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 09/28/20201730 TML
68138
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
10
U
10
4.0
ug/L
1
Acrylonitrile
107-13-1
8260D
5.0
U
5.0
0.80
ug/L
1
Benzene
71-43-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
0.50
U
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
0.50
U
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
0.50
U
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
0.50
U
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
10
U
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
0.50
U
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
0.50
U
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
0.50
U
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
0.50
U
0.50
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
2.0
U
2.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
0.50
U
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
0.66
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
0.50
U
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
0.50
U
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
0.50
U
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
0.50
U
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
0.50
U
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
0.50
U
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
10
U
10
2.0
ug/L
1
Methacrylonitrile
126-98-7
8260D
5.0
U
5.0
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
5.0
U
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
10
U
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
0.50
U
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
0.50
U
0.50
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
0.50
U
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
0.50
U
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
0.50
U
0.50
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
0.50
U
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
0.50
U
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 70 of 198

Volatile Organic Compounds by GC/MS
Client:CDM Smith Laboratory ID:VI24027-013
Description: CD-4 Rep Matrix: Aqueous
Date Sampled:09/23/2020 1730 Project Name: Cabarrus County LF Unit 2
Date Received:09/24/2020 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 09/28/20201730 TML 68138
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2,3-Trichloropropane
96-18-4
8260D
0.50
U
0.50
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
5.0
U
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
0.50
U
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
1.0
U
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
96 70-130
93 70-130
92 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 71 of 198

ICP-MS Metals
Client:CDM Smith Laboratory ID:VI24027-013
Description: CD-4 Rep Matrix: Aqueous
Date Sampled:09/23/2020 1730 Project Name: Cabarrus County LF Unit 2
Date Received:09/24/2020 Project Number:
Run Prep Method
1 3005A
Analytical Method Dilution Analysis Date Analyst
6020B 1 10/06/2020 0447 BPK
Prep Date Batch
10/03/2020 1555 68279
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0
6020B
2.0
U
2.0
0.50
ug/L
1
Arsenic
7440-38-2
6020B
2.0
U
2.0
1.3
ug/L
1
Barium
7440-39-3
6020B
56
5.0
1.3
ug/L
1
Beryllium
7440-41-7
6020B
0.52
0.40
0.15
ug/L
1
Cadmium
7440-43-9
6020B
0.50
U
0.50
0.13
ug/L
1
Chromium
7440-47-3
6020B
2.2
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4
6020B
3.1
J
5.0
1.3
ug/L
1
Copper
7440-50-8
6020B
1.5
J
5.0
1.3
ug/L
1
Lead
7439-92-1
6020B
1.4
1.0
0.25
ug/L
1
Nickel
7440-02-0
6020B
5.6
5.0
1.3
ug/L
1
Selenium
7782-49-2
6020B
5.0
U
5.0
1.3
ug/L
1
Silver
7440-22-4
6020B
1.0
U
1.0
0.25
ug/L
1
Thallium
7440-28-0
6020B
0.50
U
0.50
0.15
ug/L
1
Vanadium
7440-62-2
6020B
11
5.0
2.5
ug/L
1
Zinc
7440-66-6
6020B
7.3
J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
U = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 72 of 198

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124036
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 38 of 81

Inorganic non-metals - MB
Sample ID: VQ68070-001 Matrix: Aqueous
Batch:68070
Analytical Method: SM 2540C-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
TDS 25 U 1 25 25 mg/L 09/27/20201820
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - LCS
Sample ID: VQ68070-002 Matrix: Aqueous
Batch:68070
Analytical Method: SM 2540C-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TDS 1500 1500 1 101 90-110 09/27/20201820
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - LCS
Sample ID: VQ68132-002 Matrix: Aqueous
Batch: 68132
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg CaCO3/L) (mg CaCO3/LP Dil % Rec Limit Analysis Date
Alkalinity @ pH 4.5 su 100 100 1 103 90-110 09/28/2020 1210
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - LCS
Sample ID: VQ68349-002 Matrix: Aqueous
Batch: 68349
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg CaCO3/L) (mg CaCO3/LP Dil % Rec Limit Analysis Date
Alkalinity @ pH 4.5 su 100 110 1 108 90-110 09/29/2020 1300
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 42 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - MB
Sample ID: VQ68445-001 Matrix: Aqueous
Batch: 68445
Analytical Method: SM 2540C-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
TDS 25 U 1 25 25 mg/L 09/30/2020 2353
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - LCS
Sample ID: VQ68445-002 Matrix: Aqueous
Batch: 68445
Analytical Method: SM 2540C-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TDS 1500 1500 1 100 90-110 09/30/2020 2353
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 44 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - MB
Sample ID: VQ68625-001 Matrix: Aqueous
Batch: 68625
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate 1.0 U 1 1.0 0.20 mg/L 10101120201830
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - LCS
Sample ID: VQ68625-002 Matrix: Aqueous
Batch: 68625
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 18 1 90 80-120 10101120201908
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 46 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - MS
Sample ID: V124036-003MS Matrix: Aqueous
Batch: 68625
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 1.8 10 10 1 85 80-120 10/02/2020 0049
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 47 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - MSD
Sample ID: V124036-003MD Matrix: Aqueous
Batch: 68625
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 1.8 10 10 1 84 0.98 80-120 20 10/02/2020 0107
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 48 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - MB
Sample ID: VQ68633-001 Matrix: Aqueous
Batch:68633
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride 1.0 U 1 1.0 0.20 mg/L 10101120201830
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 49 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - LCS
Sample ID: VQ68633-002 Matrix: Aqueous
Batch:68633
Analytical Method: 9056A
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 19 1 96 80-120 10101120201908
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 50 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - MS
Sample ID: V124036-003MS Matrix: Aqueous
Batch:68633
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 4.9 10 15 1 105 80-120 10/02/2020 0049
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 51 of 81
QC Data for Lot Number: V124036

Inorganic non-metals - MSD
Sample ID: V124036-003MD Matrix: Aqueous
Batch:68633
Analytical Method: 9056A
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Chloride 4.9 10 15 1 104 0.65 80-120 20 10/02/2020 0107
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 52 of 81
QC Data for Lot Number: V124036

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ68138-001 Matrix: Aqueous
Batch: 68138 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
10
U
1
10
4.0
ug/L
09/28/2020 1408
Acrylonitrile
5.0
U
1
5.0
0.80
ug/L
09/28/2020 1408
Benzene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Bromochloromethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Bromodichloromethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Bromoform
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Bromomethane (Methyl bromide)
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
2-Butanone (MEK)
10
U
1
10
2.0
ug/L
09/28/2020 1408
Carbon disulfide
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Carbon tetrachloride
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Chlorobenzene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Chloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Chloroform
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Chloromethane (Methyl chloride)
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
1,2-Dibromo-3-chloropropane (DBCP)
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Dibromochloromethane
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1408
1,2-Dibromoethane (EDB)
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1408
Dibromomethane (Methylene bromide)
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1408
trans- 1,4-Dichloro-2-butene
2.0
u
1
2.0
0.40
ug/L
09/28/2020 1408
1,2-Dichlorobenzene
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1408
1,4-Dichlorobenzene
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1408
1,1-Dichloroethane
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1408
1,2-Dichloroethane
0.50
u
1
0.50
0.40
ug/L
09/28/2020 1408
1,1-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
cis- 1,2-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
trans- 1,2-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
1,2-Dichloropropane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
cis- 1,3-Dichloropropene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
trans- 1,3-Dichloropropene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Ethylbenzene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
2-Hexanone
10
U
1
10
2.0
ug/L
09/28/2020 1408
Methacrylonitrile
5.0
U
1
5.0
2.0
ug/L
09/28/2020 1408
Methyl iodide (lodomethane)
5.0
U
1
5.0
0.40
ug/L
09/28/2020 1408
4-Methyl-2-pentanone
10
U
1
10
2.0
ug/L
09/28/2020 1408
Methylene chloride
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Styrene
0.50
U
1
0.50
0.41
ug/L
09/28/2020 1408
1,1,1,2-Tetrachloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
1,1,2,2-Tetrachloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Tetrachloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Tetrahydrofuran
5.0
U
1
5.0
1.0
ug/L
09/28/2020 1408
Toluene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
1,1,1-Trichloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
1,1,2-Trichloroethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Trichloroethene
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 53 of 81
QC Data for Lot Number: V124036

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ68138-001 Matrix: Aqueous
Batch: 68138 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Trichlorofluoromethane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
1,2,3-Trichloropropane
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Vinyl acetate
5.0
U
1
5.0
1.2
ug/L
09/28/2020 1408
Vinyl chloride
0.50
U
1
0.50
0.40
ug/L
09/28/2020 1408
Xylenes (total)
1.0
U
1
1.0
0.40
ug/L
09/28/2020 1408
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 91 70-130
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124036
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 54 of 81

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ68138-002
Matrix: Aqueous
Batch: 68138
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
110
1
110
60-140
09/28/2020 1320
Acrylonitrile
100
110
1
105
70-130
09/28/2020 1320
Benzene
50
54
1
108
70-130
09/28/2020 1320
Bromochloromethane
50
53
1
107
70-130
09/28/2020 1320
Bromodichloromethane
50
52
1
105
70-130
09/28/2020 1320
Bromoform
50
53
1
106
70-130
09/28/2020 1320
Bromomethane (Methyl bromide)
50
47
1
95
70-130
09/28/2020 1320
2-Butanone (MEK)
100
110
1
110
70-130
09/28/2020 1320
Carbon disulfide
50
57
1
114
70-130
09/28/2020 1320
Carbon tetrachloride
50
57
1
115
70-130
09/28/2020 1320
Chlorobenzene
50
52
1
103
70-130
09/28/2020 1320
Chloroethane
50
59
1
118
70-130
09/28/2020 1320
Chloroform
50
52
1
105
70-130
09/28/2020 1320
Chloromethane (Methyl chloride)
50
43
1
87
60-140
09/28/2020 1320
1,2-Dibromo-3-chloropropane (DBCP)
50
49
1
99
70-130
09/28/2020 1320
Dibromochloromethane
50
51
1
103
70-130
09/28/2020 1320
1,2-Dibromoethane (EDB)
50
52
1
104
70-130
09/28/2020 1320
Dibromomethane (Methylene bromide)
50
53
1
107
70-130
09/28/2020 1320
trans- 1,4-Dichloro-2-butene
50
52
1
105
70-130
09/28/2020 1320
1,2-Dichlorobenzene
50
50
1
100
70-130
09/28/2020 1320
1,4-Dichlorobenzene
50
50
1
100
70-130
09/28/2020 1320
1,1-Dichloroethane
50
56
1
112
70-130
09/28/2020 1320
1,2-Dichloroethane
50
50
1
101
70-130
09/28/2020 1320
1,1-Dichloroethene
50
60
1
120
70-130
09/28/2020 1320
cis- 1,2-Dichloroethene
50
53
1
106
70-130
09/28/2020 1320
trans- 1,2-Dichloroethene
50
55
1
111
70-130
09/28/2020 1320
1,2-Dichloropropane
50
52
1
104
70-130
09/28/2020 1320
cis- 1,3-Dichloropropene
50
54
1
108
70-130
09/28/2020 1320
trans- 1,3-Dichloropropene
50
53
1
105
70-130
09/28/2020 1320
Ethylbenzene
50
55
1
109
70-130
09/28/2020 1320
2-Hexanone
100
100
1
102
70-130
09/28/2020 1320
Methacrylonitrile
250
270
1
108
70-130
09/28/2020 1320
Methyl iodide (lodomethane)
50
57
1
114
70-130
09/28/2020 1320
4-Methyl-2-pentanone
100
100
1
103
70-130
09/28/2020 1320
Methylene chloride
50
52
1
105
70-130
09/28/2020 1320
Styrene
50
54
1
108
70-130
09/28/2020 1320
1,1,1,2-Tetrachloroethane
50
55
1
110
70-130
09/28/2020 1320
1,1,2,2-Tetrachloroethane
50
51
1
101
70-130
09/28/2020 1320
Tetrachloroethene
50
56
1
111
70-130
09/28/2020 1320
Tetrahydrofuran
50
55
1
110
70-130
09/28/2020 1320
Toluene
50
53
1
107
70-130
09/28/2020 1320
1,1,1-Trichloroethane
50
56
1
112
70-130
09/28/2020 1320
1,1,2-Trichloroethane
50
51
1
102
70-130
09/28/2020 1320
Trichloroethene
50
53
1
106
70-130
09/28/2020 1320
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 55 of 81
QC Data for Lot Number: V124036

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ68138-002
Matrix: Aqueous
Batch: 68138
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Trichlorofluoromethane
50
53
1 107
70-130
09/28/2020 1320
1,2,3-Trichloropropane
50
50
1 101
70-130
09/28/2020 1320
Vinyl acetate
50
64
1 129
60-140
09/28/2020 1320
Vinyl chloride
50
56
1 113
70-130
09/28/2020 1320
Xylenes (total)
100
110
1 110
70-130
09/28/2020 1320
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 93 70-130
1,2-Dichloroethane-d4 91 70-130
Toluene-d8 91 70-130
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124036
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 56 of 81

Volatile Organic Compounds by GC/MS - LCSD
Sample ID: VQ68138-003
Matrix: Aqueous
Batch: 68138
Prep
Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
% RPD
Limit
Limit
Analysis Date
Acetone
100
94
1
94
15
60-140
20
09/28/2020 1508
Acrylonitrile
100
100
1
101
4.6
70-130
40
09/28/2020 1508
Benzene
50
52
1
104
3.1
70-130
20
09/28/2020 1508
Bromochloromethane
50
52
1
103
3.0
70-130
20
09/28/2020 1508
Bromodichloromethane
50
53
1
105
0.46
70-130
20
09/28/2020 1508
Bromoform
50
52
1
105
1.1
70-130
20
09/28/2020 1508
Bromomethane (Methyl bromide)
50
51
1
101
6.3
70-130
20
09/28/2020 1508
2-Butanone (MEK)
100
110
1
107
3.4
70-130
20
09/28/2020 1508
Carbon disulfide
50
54
1
108
5.1
70-130
20
09/28/2020 1508
Carbon tetrachloride
50
54
1
108
6.2
70-130
20
09/28/2020 1508
Chlorobenzene
50
51
1
103
0.50
70-130
20
09/28/2020 1508
Chloroethane
50
54
1
108
8.8
70-130
20
09/28/2020 1508
Chloroform
50
52
1
103
1.6
70-130
20
09/28/2020 1508
Chloromethane (Methyl chloride)
50
51
1
101
15
60-140
20
09/28/2020 1508
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
94
4.4
70-130
20
09/28/2020 1508
Dibromochloromethane
50
51
1
103
0.15
70-130
20
09/28/2020 1508
1,2-Dibromoethane (EDB)
50
51
1
102
2.4
70-130
20
09/28/2020 1508
Dibromomethane (Methylene bromide)
50
51
1
102
4.0
70-130
20
09/28/2020 1508
trans- 1,4-Dichloro-2-butene
50
51
1
101
3.0
70-130
20
09/28/2020 1508
1,2-Dichlorobenzene
50
50
1
101
0.38
70-130
20
09/28/2020 1508
1,4-Dichlorobenzene
50
50
1
100
0.060
70-130
20
09/28/2020 1508
1,1-Dichloroethane
50
54
1
107
4.6
70-130
20
09/28/2020 1508
1,2-Dichloroethane
50
51
1
103
2.3
70-130
20
09/28/2020 1508
1,1-Dichloroethene
50
56
1
111
7.5
70-130
20
09/28/2020 1508
cis- 1,2-Dichloroethene
50
52
1
104
1.9
70-130
20
09/28/2020 1508
trans- 1,2-Dichloroethene
50
53
1
106
4.9
70-130
20
09/28/2020 1508
1,2-Dichloropropane
50
52
1
105
0.55
70-130
20
09/28/2020 1508
cis- 1,3-Dichloropropene
50
53
1
106
2.5
70-130
20
09/28/2020 1508
trans- 1,3-Dichloropropene
50
50
1
101
4.4
70-130
20
09/28/2020 1508
Ethylbenzene
50
53
1
106
3.7
70-130
20
09/28/2020 1508
2-Hexanone
100
110
1
106
3.2
70-130
20
09/28/2020 1508
Methacrylonitrile
250
260
1
105
2.3
70-130
20
09/28/2020 1508
Methyl iodide (lodomethane)
50
54
1
107
6.5
70-130
20
09/28/2020 1508
4-Methyl-2-pentanone
100
110
1
106
3.0
70-130
20
09/28/2020 1508
Methylene chloride
50
50
1
101
4.2
70-130
20
09/28/2020 1508
Styrene
50
53
1
106
1.8
70-130
20
09/28/2020 1508
1,1,1,2-Tetrachloroethane
50
53
1
106
3.6
70-130
20
09/28/2020 1508
1,1,2,2-Tetrachloroethane
50
50
1
99
1.6
70-130
20
09/28/2020 1508
Tetrachloroethene
50
52
1
104
6.9
70-130
20
09/28/2020 1508
Tetrahydrofuran
50
53
1
107
3.4
70-130
20
09/28/2020 1508
Toluene
50
51
1
102
4.8
70-130
20
09/28/2020 1508
1,1,1-Trichloroethane
50
53
1
107
4.3
70-130
20
09/28/2020 1508
1,1,2-Trichloroethane
50
50
1
100
1.3
70-130
20
09/28/2020 1508
Trichloroethene
50
53
1
106
0.28
70-130
20
09/28/2020 1508
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 57 of 81
QC Data for Lot Number: V124036

Volatile Organic Compounds by GC/MS - LCSD
Sample ID: VQ68138-003
Matrix: Aqueous
Batch: 68138
Prep
Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec % RPD
Limit
Limit
Analysis Date
Trichlorofluoromethane
50
52
1
104 2.6
70-130
20
09/28/2020 1508
1,2,3-Trichloropropane
50
52
1
104 3.0
70-130
20
09/28/2020 1508
Vinyl acetate
50
47 +
1
94 31
60-140
20
09/28/2020 1508
Vinyl chloride
50
55
1
110 2.9
70-130
20
09/28/2020 1508
Xylenes (total)
100
100
1
104 5.9
70-130
20
09/28/2020 1508
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 96 70-130
Toluene-d8 94 70-130
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124036
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 58 of 81

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ68353-001 Matrix: Aqueous
Batch: 68353 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
10
U
1
10
4.0
ug/L
09/30/2020 0920
Acrylonitrile
5.0
U
1
5.0
0.80
ug/L
09/30/2020 0920
Benzene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Bromochloromethane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Bromodichloromethane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Bromoform
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Bromomethane (Methyl bromide)
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
2-Butanone (MEK)
10
U
1
10
2.0
ug/L
09/30/2020 0920
Carbon disulfide
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Carbon tetrachloride
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Chlorobenzene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Chloroethane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Chloroform
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Chloromethane (Methyl chloride)
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
1,2-Dibromo-3-chloropropane (DBCP)
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Dibromochloromethane
0.50
u
1
0.50
0.40
ug/L
09/30/2020 0920
1,2-Dibromoethane (EDB)
0.50
u
1
0.50
0.40
ug/L
09/30/2020 0920
Dibromomethane (Methylene bromide)
0.50
u
1
0.50
0.40
ug/L
09/30/2020 0920
trans- 1,4-Dichloro-2-butene
2.0
u
1
2.0
0.40
ug/L
09/30/2020 0920
1,2-Dichlorobenzene
0.50
u
1
0.50
0.40
ug/L
09/30/2020 0920
1,4-Dichlorobenzene
0.50
u
1
0.50
0.40
ug/L
09/30/2020 0920
1,1-Dichloroethane
0.50
u
1
0.50
0.40
ug/L
09/30/2020 0920
1,2-Dichloroethane
0.50
u
1
0.50
0.40
ug/L
09/30/2020 0920
1,1-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
cis- 1,2-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
trans- 1,2-Dichloroethene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
1,2-Dichloropropane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
cis- 1,3-Dichloropropene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
trans- 1,3-Dichloropropene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Ethylbenzene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
2-Hexanone
10
U
1
10
2.0
ug/L
09/30/2020 0920
Methacrylonitrile
5.0
U
1
5.0
2.0
ug/L
09/30/2020 0920
Methyl iodide (lodomethane)
5.0
U
1
5.0
0.40
ug/L
09/30/2020 0920
4-Methyl-2-pentanone
10
U
1
10
2.0
ug/L
09/30/2020 0920
Methylene chloride
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Styrene
0.50
U
1
0.50
0.41
ug/L
09/30/2020 0920
1,1,1,2-Tetrachloroethane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
1,1,2,2-Tetrachloroethane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Tetrachloroethene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Tetrahydrofuran
5.0
U
1
5.0
1.0
ug/L
09/30/2020 0920
Toluene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
1,1,1-Trichloroethane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
1,1,2-Trichloroethane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Trichloroethene
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 59 of 81
QC Data for Lot Number: V124036

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ68353-001 Matrix: Aqueous
Batch: 68353 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Trichlorofluoromethane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
1,2,3-Trichloropropane
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Vinyl acetate
5.0
U
1
5.0
1.2
ug/L
09/30/2020 0920
Vinyl chloride
0.50
U
1
0.50
0.40
ug/L
09/30/2020 0920
Xylenes (total)
1.0
U
1
1.0
0.40
ug/L
09/30/2020 0920
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124036
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 60 of 81

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ68353-002
Matrix: Aqueous
Batch: 68353
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
91
1
91
60-140
09/30/2020 0816
Acrylonitrile
100
120
1
117
70-130
09/30/2020 0816
Benzene
50
53
1
106
70-130
09/30/2020 0816
Bromochloromethane
50
51
1
103
70-130
09/30/2020 0816
Bromodichloromethane
50
52
1
105
70-130
09/30/2020 0816
Bromoform
50
48
1
96
70-130
09/30/2020 0816
Bromomethane (Methyl bromide)
50
48
1
97
70-130
09/30/2020 0816
2-Butanone (MEK)
100
120
1
116
70-130
09/30/2020 0816
Carbon disulfide
50
53
1
107
70-130
09/30/2020 0816
Carbon tetrachloride
50
53
1
106
70-130
09/30/2020 0816
Chlorobenzene
50
51
1
102
70-130
09/30/2020 0816
Chloroethane
50
58
1
117
70-130
09/30/2020 0816
Chloroform
50
55
1
110
70-130
09/30/2020 0816
Chloromethane (Methyl chloride)
50
54
1
109
60-140
09/30/2020 0816
1,2-Dibromo-3-chloropropane (DBCP)
50
45
1
91
70-130
09/30/2020 0816
Dibromochloromethane
50
49
1
98
70-130
09/30/2020 0816
1,2-Dibromoethane (EDB)
50
51
1
102
70-130
09/30/2020 0816
Dibromomethane (Methylene bromide)
50
51
1
102
70-130
09/30/2020 0816
trans- 1,4-Dichloro-2-butene
50
51
1
103
70-130
09/30/2020 0816
1,2-Dichlorobenzene
50
49
1
99
70-130
09/30/2020 0816
1,4-Dichlorobenzene
50
49
1
99
70-130
09/30/2020 0816
1,1-Dichloroethane
50
58
1
115
70-130
09/30/2020 0816
1,2-Dichloroethane
50
51
1
102
70-130
09/30/2020 0816
1,1-Dichloroethene
50
55
1
110
70-130
09/30/2020 0816
cis- 1,2-Dichloroethene
50
55
1
109
70-130
09/30/2020 0816
trans- 1,2-Dichloroethene
50
56
1
112
70-130
09/30/2020 0816
1,2-Dichloropropane
50
55
1
109
70-130
09/30/2020 0816
cis- 1,3-Dichloropropene
50
53
1
107
70-130
09/30/2020 0816
trans- 1,3-Dichloropropene
50
50
1
100
70-130
09/30/2020 0816
Ethylbenzene
50
53
1
105
70-130
09/30/2020 0816
2-Hexanone
100
110
1
113
70-130
09/30/2020 0816
Methacrylonitrile
250
290
1
115
70-130
09/30/2020 0816
Methyl iodide (lodomethane)
50
50
1
101
70-130
09/30/2020 0816
4-Methyl-2-pentanone
100
110
1
109
70-130
09/30/2020 0816
Methylene chloride
50
52
1
105
70-130
09/30/2020 0816
Styrene
50
53
1
106
70-130
09/30/2020 0816
1,1,1,2-Tetrachloroethane
50
51
1
103
70-130
09/30/2020 0816
1,1,2,2-Tetrachloroethane
50
52
1
104
70-130
09/30/2020 0816
Tetrachloroethene
50
49
1
98
70-130
09/30/2020 0816
Tetrahydrofuran
50
58
1
117
70-130
09/30/2020 0816
Toluene
50
52
1
103
70-130
09/30/2020 0816
1,1,1-Trichloroethane
50
54
1
107
70-130
09/30/2020 0816
1,1,2-Trichloroethane
50
51
1
102
70-130
09/30/2020 0816
Trichloroethene
50
49
1
99
70-130
09/30/2020 0816
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 61 of 81
QC Data for Lot Number: V124036

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ68353-002
Matrix: Aqueous
Batch: 68353
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Trichlorofluoromethane
50
52
1 104
70-130
09/30/2020 0816
1,2,3-Trichloropropane
50
50
1 101
70-130
09/30/2020 0816
Vinyl acetate
50
60
1 119
60-140
09/30/2020 0816
Vinyl chloride
50
65
1 129
70-130
09/30/2020 0816
Xylenes (total)
100
100
1 104
70-130
09/30/2020 0816
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 98 70-130
Toluene-d8 94 70-130
LOQ = Limit of Quantitation U = Not detected at or above the LOD N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: V124036
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 62 of 81

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: VQ68512-001 Matrix: Aqueous
Batch: 68512 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane 3.0 U 1 3.0 1.0 ug/L 10/01/2020 0924
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
107 40-170
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 63 of 81
QC Data for Lot Number: V124036

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: VQ68512-002 Matrix: Aqueous
Batch: 68512 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 47 1 94 70-130 10/01/2020 0824
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
107 40-170
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 64 of 81
QC Data for Lot Number: V124036

ICP-MS Metals - MB
Sample ID: VQ68268-001 Matrix: Aqueous
Batch:68268 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 10/01/2020 0855
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
2.0
U
1
2.0
0.50
ug/L
10/01/2020 2031
Arsenic
2.0
U
1
2.0
1.3
ug/L
10/01/2020 2031
Barium
5.0
U
1
5.0
1.3
ug/L
10/01/2020 2031
Beryllium
0.40
U
1
0.40
0.15
ug/L
10/01/2020 2031
Cadmium
0.50
U
1
0.50
0.13
ug/L
10/01/2020 2031
Chromium
5.0
U
1
5.0
1.3
ug/L
10/01/2020 2031
Cobalt
5.0
U
1
5.0
1.3
ug/L
10/01/2020 2031
Copper
5.0
U
1
5.0
1.3
ug/L
10/01/2020 2031
Iron
50
U
1
50
13
ug/L
10/01/2020 2031
Lead
1.0
U
1
1.0
0.25
ug/L
10/01/2020 2031
Manganese
5.0
U
1
5.0
1.3
ug/L
10/01/2020 2031
Nickel
5.0
U
1
5.0
1.3
ug/L
10/01/2020 2031
Selenium
5.0
U
1
5.0
1.3
ug/L
10/01/2020 2031
Silver
1.0
U
1
1.0
0.25
ug/L
10/01/2020 2031
Thallium
0.50
U
1
0.50
0.15
ug/L
10/01/2020 2031
Vanadium
5.0
U
1
5.0
2.5
ug/L
10/01/2020 2031
Zinc
10
U
1
10
2.5
ug/L
10/01/2020 2031
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 65 of 81
QC Data for Lot Number: V124036

ICP-MS Metals - LCS
Sample ID: VQ68268-002
Matrix: Aqueous
Batch:68268
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 10/01/2020 0855
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
Antimony
100
98
1 98
80-120
10/01/2020 2053
Arsenic
100
98
1 98
80-120
10/01/2020 2053
Barium
100
97
1 97
80-120
10/01/2020 2053
Beryllium
100
95
1 95
80-120
10/01/2020 2053
Cadmium
100
98
1 98
80-120
10/01/2020 2053
Chromium
100
99
1 99
80-120
10/01/2020 2053
Cobalt
100
110
1 105
80-120
10/01/2020 2053
Copper
100
110
1 110
80-120
10/01/2020 2053
Iron
1000
940
1 94
80-120
10/01/2020 2053
Lead
100
110
1 106
80-120
10/01/2020 2053
Manganese
100
100
1 104
80-120
10/01/2020 2053
Nickel
100
110
1 107
80-120
10/01/2020 2053
Selenium
100
89
1 89
80-120
10/01/2020 2053
Silver
100
100
1 103
80-120
10/01/2020 2053
Thallium
100
100
1 104
80-120
10/01/2020 2053
Vanadium
100
96
1 96
80-120
10/01/2020 2053
Zinc
100
94
1 94
80-120
10/01/2020 2053
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 66 of 81
QC Data for Lot Number: V124036

ICP-MS Metals - MS
Sample ID: V124036-006MS
Matrix: Aqueous
Batch:68268
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 10/01/2020 0855
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
0.0
100
94
1
94
70-130
10/01/2020 2108
Arsenic
1.9
100
99
1
97
70-130
10/01/2020 2108
Barium
34
100
130
1
99
70-130
10/01/2020 2108
Beryllium
0.18
100
99
1
99
70-130
10/01/2020 2108
Cadmium
0.0
100
96
1
96
70-130
10/01/2020 2108
Chromium
2.5
100
96
1
94
70-130
10/01/2020 2108
Cobalt
0.0
100
100
1
101
70-130
10/01/2020 2108
Copper
6.2
100
110
1
102
70-130
10/01/2020 2108
Iron
1800
1000
2600
1
87
70-130
10/01/2020 2108
Lead
0.99
100
100
1
99
70-130
10/01/2020 2108
Manganese
42
100
140
1
96
70-130
10/01/2020 2108
Nickel
2.1
100
100
1
100
70-130
10/01/2020 2108
Selenium
0.0
100
94
1
94
70-130
10/01/2020 2108
Silver
0.0
100
100
1
100
70-130
10/01/2020 2108
Thallium
0.0
100
99
1
99
70-130
10/01/2020 2108
Vanadium
6.5
100
98
1
92
70-130
10/01/2020 2108
Zinc
5.8
100
110
1
100
70-130
10/01/2020 2108
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 67 of 81
QC Data for Lot Number: V124036

ICP-MS Metals - MSD
Sample ID: V124036-006MD
Matrix: Aqueous
Batch:68268
Prep Method:
3005A
Analytical Method: 6020B
Prep Date: 10/01/2020 0855
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Antimony
0.0
100
92
1
92
1.4
70-130
20
10/01/2020 2116
Arsenic
1.9
100
100
1
98
0.96
70-130
20
10/01/2020 2116
Barium
34
100
130
1
98
0.71
70-130
20
10/01/2020 2116
Beryllium
0.18
100
100
1
103
3.8
70-130
20
10/01/2020 2116
Cadmium
0.0
100
96
1
96
0.23
70-130
20
10/01/2020 2116
Chromium
2.5
100
100
1
97
3.3
70-130
20
10/01/2020 2116
Cobalt
0.0
100
100
1
103
2.0
70-130
20
10/01/2020 2116
Copper
6.2
100
110
1
105
2.6
70-130
20
10/01/2020 2116
Iron
1800
1000
3000
1
122
12
70-130
20
10/01/2020 2116
Lead
0.99
100
99
1
98
0.41
70-130
20
10/01/2020 2116
Manganese
42
100
140
1
100
3.1
70-130
20
10/01/2020 2116
Nickel
2.1
100
100
1
103
2.5
70-130
20
10/01/2020 2116
Selenium
0.0
100
94
1
94
0.0059
70-130
20
10/01/2020 2116
Silver
0.0
100
100
1
100
0.15
70-130
20
10/01/2020 2116
Thallium
0.0
100
99
1
99
0.35
70-130
20
10/01/2020 2116
Vanadium
6.5
100
100
1
96
3.9
70-130
20
10/01/2020 2116
Zinc
5.8
100
110
1
101
0.71
70-130
20
10/01/2020 2116
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 68 of 81
QC Data for Lot Number: V124036

ICP-MS Metals - MB
Sample ID: VQ68305-001 Matrix: Aqueous
Batch: 68305 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 10/01/2020 1546
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
2.0
U
1
2.0
0.50
ug/L
10/02/2020 2000
Arsenic
2.0
U
1
2.0
1.3
ug/L
10/02/2020 2000
Barium
5.0
U
1
5.0
1.3
ug/L
10/02/2020 2000
Beryllium
0.40
U
1
0.40
0.15
ug/L
10/02/2020 2000
Cadmium
0.50
U
1
0.50
0.13
ug/L
10/02/2020 2000
Chromium
5.0
U
1
5.0
1.3
ug/L
10/02/2020 2000
Cobalt
5.0
U
1
5.0
1.3
ug/L
10/02/2020 2000
Copper
5.0
U
1
5.0
1.3
ug/L
10/02/2020 2000
Iron
50
U
1
50
13
ug/L
10/02/2020 2000
Lead
1.0
U
1
1.0
0.25
ug/L
10/02/2020 2000
Manganese
5.0
U
1
5.0
1.3
ug/L
10/02/2020 2000
Nickel
5.0
U
1
5.0
1.3
ug/L
10/02/2020 2000
Selenium
5.0
U
1
5.0
1.3
ug/L
10/02/2020 2000
Silver
1.0
U
1
1.0
0.25
ug/L
10/02/2020 2000
Thallium
0.50
U
1
0.50
0.15
ug/L
10/02/2020 2000
Vanadium
5.0
U
1
5.0
2.5
ug/L
10/02/2020 2000
Zinc
10
U
1
10
2.5
ug/L
10/02/2020 2000
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 69 of 81
QC Data for Lot Number: V124036

ICP-MS Metals - LCS
Sample ID: VQ68305-002
Matrix: Aqueous
Batch: 68305
Prep Method: 3005A
Analytical Method: 6020B
Prep Date: 10/01/2020 1546
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit
Analysis Date
Antimony
100
94
1 94
80-120
10/02/2020 2008
Arsenic
100
98
1 98
80-120
10/02/2020 2008
Barium
100
99
1 99
80-120
10/02/2020 2008
Beryllium
100
94
1 94
80-120
10/02/2020 2008
Cadmium
100
96
1 96
80-120
10/02/2020 2008
Chromium
100
100
1 101
80-120
10/02/2020 2008
Cobalt
100
110
1 106
80-120
10/02/2020 2008
Copper
100
110
1 109
80-120
10/02/2020 2008
Iron
1000
930
1 93
80-120
10/02/2020 2008
Lead
100
100
1 101
80-120
10/02/2020 2008
Manganese
100
100
1 103
80-120
10/02/2020 2008
Nickel
100
110
1 107
80-120
10/02/2020 2008
Selenium
100
91
1 91
80-120
10/02/2020 2008
Silver
100
100
1 103
80-120
10/02/2020 2008
Thallium
100
99
1 99
80-120
10/02/2020 2008
Vanadium
100
96
1 96
80-120
10/02/2020 2008
Zinc
100
88
1 88
80-120
10/02/2020 2008
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 70 of 81
QC Data for Lot Number: V124036

CVAA -MB
Sample ID: VQ67859-001 Matrix: Aqueous
Batch: 67859 Prep Method:
Analytical Method: 7470A Prep Date: 09/25/2020 1000
Parameter Result Q Dil LOQ DL Units Analysis Date
Mercury 0.00020 U 1 0.00020 0.000091 mg/L 09/25/20201504
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 71 of 81
QC Data for Lot Number: V124036

CVAA - LCS
Sample ID: VQ67859-002 Matrix: Aqueous
Batch: 67859 Prep Method:
Analytical Method: 7470A Prep Date: 09/25/2020 1000
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury 0.0020 0.0018 1 92 80-120 09/25/20201506
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 72 of 81
QC Data for Lot Number: V124036

CVAA -MB
Sample ID: VQ68176-001 Matrix: Aqueous
Batch: 68176 Prep Method:
Analytical Method: 7470A Prep Date: 09/29/2020 0933
Parameter Result Q Dil LOQ DL Units Analysis Date
Mercury 0.00020 U 1 0.00020 0.000091 mg/L 09/29/20201753
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 73 of 81
QC Data for Lot Number: V124036

CVAA - LCS
Sample ID: VQ68176-002 Matrix: Aqueous
Batch: 68176 Prep Method:
Analytical Method: 7470A Prep Date: 09/29/2020 0933
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury 0.0020 0.0017 1 87 80-120 09/29/20201801
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 74 of 81
QC Data for Lot Number: V124036

CVAA - MS
Sample ID: V124036-005MS Matrix: Aqueous
Batch: 68176 Prep Method:
Analytical Method: 7470A Prep Date: 09/29/2020 0933
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury 0.0 0.0020 0.0018 1 88 85-115 09/29/20201806
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 75 of 81
QC Data for Lot Number: V124036

CVAA - MSD
Sample ID: V124036-005MD Matrix: Aqueous
Batch: 68176 Prep Method:
Analytical Method: 7470A Prep Date: 09/29/2020 0933
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Mercury 0.0 0.0020 0.0017 1 86 2.1 85-115 20 09/29/20201808
LOQ = Limit of Quantitation
DL = Detection Limit
U = Not detected at or above the LOD
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 76 of 81
QC Data for Lot Number: V124036

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 77 of 81

PACE ANALYTICAL SERVICES. LLC
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Page 78 of 81

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 79 of 81

PACE ANALYTICAL SERVICES, LLC
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Page 80 of 81

PACE ANALYTICAL SERVICES, LLC
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aYes ❑ No ❑NA 4. Is the cominercial u,uricr': pmking,sJip attached in &is f6 m?
Yes ❑ Two 5, Were proper c.' Nludy Twu"dures (rclm uished,7eceived) followed?
F Yes El No 6, lh = sample Ms Bared im the
•,J C �'7
Yes ❑ N i, Wen- 5.wnple' IDs jisr d im all 4nlli1r. conmineJS? -
E+Ycs ❑ Na S. Was collcction date & tirne lihEed on #bo C OC?
❑ Ycs -9�No 9, '<'ras collection date & tirne lirwd on all saluple coritainerx?
El Ycs ❑ No 10. Did all conmintr label in(r mwicwl (11), date; nine) ko%= with the C oc?'
10 Yes ❑ No J 1- YVcrc tests to be perfojwltA liglyd an the CDC;?
Yes No J 2. Did all sampics arrhre in the proper cmltaincr5 for eadl trst and.lor in goad con ditior,
(tmbrekcn, lids on, etc.)?
EM-VCS ❑ No 1.;. Was a&Tiate sample' C&lurr,e �tvailnblc',
l'cs No 14. WeTs all satnnles iect iwea with' 'ry t"e holding, time or dA hnr�rs, WJlfC.7�}`er GrmcS �l�t'�
Yes li(, [ i. Rfere any win las e(mtairie . NW € f N]e one) samples Not listed an COC`(
1 G_ For VDA m d RSK-17: samp es, ,. , cs present r " pea-sJ•r_e" ('A"Lyr bmm in diamnl a-',
❑ Yes &N o 0 NA in any of the VOA vi al.R?
4E-Y- N15 U N.A. 17- IV= all DF.Uhnetals+nutrient 4anipk5 received at a pH of-, 2`?
NO N!i IS. Were A c+'an n3e Nrunplcs rccolved at a .I I > 12 and st.iftde sat}s ] es rCu iml at a pl 1 .:- 9?
^� 19. Wuc all app l a NT4,:'TK-R!c}anideepheeoll62(-: O,Sr +l j samples free of rest aal
❑ i 4 ❑ Vol lD N?l
chlorine"
0. +Nero client re.Ilarks.rrtquo 3 (i.o, requested dilulinas, Mlx.`1wISJD desirmaUuns, etc—)
Yes [] No'"� N.4 u4trr[:�tl}transcribed tiortt thn C't�[ ; inFo the couutr�� t `sc,ula�n in 1�1145 ,'
Cyyl l0 21. Was the quow nurnher listed on the C4iltainer lal .l'A 1f 'os. c%te r
llsample Presexrv$tion (MwiL be compk-tcd for any sample{h) inc-,mTe- ly presei-vexl or with hcadspace_1
q,-knnr.1r.(ti) _. were received inuvg4y preservedanJ w�,Tc attjusted amiTclhtggly
in sample receiving wcth A1111 ml. nf•c.irrlii Luc; H2 . €TNO3, HCL NdQH using SR 9 _
lime of preservation AZ IIf more than one pi'ascrw4ivti is uccded, plea.;e noin in the c01ii.M nts beluw,
5atlnplc(s} _ /4 wau rcccivcd vwlth hifbblas >-6 mm in diarl. uwm
Sanipkz(s) -- w&e rcooivod witli 7RC', =• 0. 4 mgiL (if i19 i€. na ) Hnd were
�adjusied acatrrdingly in stifltplc roccii&E W ith sMium thiosulfare (Nk,9�03) wish Shealy JD-.
SIZ ')2n_.nde labels tiprlicxl by: 1Datc: Zp
c
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 81 of 81
c
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 81 of 81