MO-6872_27741_CA_MRP_20200512_Monitoring Report

SOUTHEASTERN GEOLOGICAL SERVICES
PO Box 441
Shelby, NC 28151
704 481 8558
TRANSMITTAL LETTER
LITTLE BUCK I1
The following report is issued on the accompanying CD in pdf format:
-) Little Buck II
-) Incident #: 27741
-) Monitoring Report
-) 5-12-20
-) Facility ID: 0-029778
Richard Kelly
Geologist

Monitoring Reports
Appendix A
Report Formats
8. Monitoring Reports
A. Site information
1. Site Identification
—late of Report: 5 -1 2 - 2 0
'Facility I.D.: 0-029778
-Site Risk: Inter Site Rank: _
c-7'SiteName: Little
UST Incident Number (if known): 27741
Land Use Categoryr-ommercial
Buck II
'Site Street Address: 20 Warren C Coleman Boulevard
City/Town: Concord Zip Code:28027 County. Cabarrus
Description of Geographical Data Point (e.g., diesel fill port):co nve n i e nce store - UST
'Location Method (GPS, topographical snap, other): GTS_ _
Latitude (decimal degrees): 35 23 47 Longitude (decimal degrees): -80 36 25
1 Information about Contacts Associated with the Leaking UST System (Addresses must include street, city,
state, zip code and mailing address, if different)
`'USTOwner: United Oil Company of the Carolinas
Address: POBox _8 Gastonia NC 28053 Tel_ 704 824 3561
BUST Operator. _ aka
Address: __ Tel:
� Property Owner: BP i qac- xr hur LLC
Address: 7111Indiana.Ave Ste300RiversideCa 92504 Tel:
QProperty Occupant: kite Aid --
Address: Tel:
-Consultant/Contractor: Southeastern Geological
Address: POBox441 Shelby NC 28151 Tei:704 481 8558
Analytical Laboratory: PACE Analytical State Certification No. 12
Address: 9800KlnceyAveSuite'i 00 Huntersville NC Tel: [phone]
3. Information about Release 28078
-Bate Discovered: March 2004
-Estimated Quantity of Release: unknown
-Cause of Release: UST
Source of Release (Dispenser/Piping/UST): UST basin & gasoline piping
-Sizes and contents of UST systein(s) from which the release occurred): One 4K gas, two 6K gas, one 2K D
—Criteria Used to Classify Risk , WSWs (not in use) within 1000' one one
1K550 IBC
4. Informmation about the Monitoring Report
""Date(s) of Groundwater Monitoring/Soil Sampling Event(s): 4 -1 4 - 2 0
�' Period of Time Reported: _ last report: 1 0 - 2 01 5
'Type of Monitoring Report (PreCAP, Active Remnediation, or Natural Attenuation): PreCap
S. Certification (77ie title page must display the seal and signature of the certBeing P.E. or L.G and the name and
certification number of the company or corporation ISee 15A NC`AC 2L .0103(e).1)
1, RiCliard Kelly , a Professional Engine'erff.i used Geologist (circle one) for (firm or company of
employment), do certify that the information' contained in this regort;is. correct and accurate to the best of my knowledge.
(Plea.4e Afla' Seal and Signature) `.,
SGS (Name of company nor corrporatian
both) in North Carolina. The certificatiori"imustmiier of the
Change 1
one or
333

B. EXECUTIVE SUMMARY
The site has been inactive due to its rank; the last sampling event was in September 2015.
Updated groundwater sampling was required. The site was sampled April 14, 2020; a summary
follows: (1) MW-1 (source well): benzene (44 ppb) was the only compound detected above its
standard, and (2) MWs 2-3-4-5, and VMW-1: all non -detect. Two noteworthy water supply
wells from the 2015 well survey were checked: WSWs 3 & 6. WSW-3 was not in use but had
the potential for use as an irrigation well, there has been no change in the status of this well.
WSW-6 was a potable well 1,015 feet down gradient of the source area. The residence serviced
by this well is now serviced by municipal water.
C. TABLE of CONTENTS
Section D
Site History 1
Section E
Site Assessment 2
Section F
Free Product 3
Section G
Soil Remediation 3
Section H
Groundwater Remediation 3
Section I
Conclusions 3
Section J
Figures 3
Section K
Tables 3
Section L
Appendices 3
D. SITE HISTORY and CHARACTERIZAION
A release was discovered from the petroleum facilities during a property assessment performed
in February and March 2004; the assessment was performed due to the potential sale of the
property. The petroleum facilities were removed in June 2004, they consisted of the following
USTs: (1) one 4000 gallon - gasoline, (2) two 6,000 gallon - gasoline, (3) one 2000 gallon -
diesel, (4) one 1000 gallon -kerosene, and (5) one 550 gallon heating oil. A Closure report was
submitted on July 16, 2004, soil contamination >10 ppm of TPH was discovered at all of the
USTs and along a gasoline product line.
A phase 2 LSA was performed in November and December 2004. Multiple compounds were
detected above their groundwater standards at the former UST basin, and EDB was detected
above its gross contaminant level. There were ten water supply wells within 1,500 feet of the
source area, but none of the wells within 1,000 feet were potable. The site was given an
intermediate rank and further work was suspended.
The site was activated in 2010 with scheduled groundwater monitoring. Monitor well 5 was
installed 70 feet down gradient of MW-1 in October 2015. Based on the September/October
2015 sampling results, and an updated water supply well survey, DENR determined that the site
could be closed with a notice of residual petroleum. A notice was not filed as the property
owner's consent was not obtained. No further action was taken until this sampling event.

E. SITE ASSESSMENT INFORMATION
1.0 WATER SUPPLY WELL SAMPLING
No water supply wells were sampled.
No potable water supply wells were found within 1,000 feet of the source area by the 2015 water
supply well survey. One potable well was identified within 1,500 feet; it was the Moose
residence well (WSW-6), at 1,015 feet. The survey found five wells within 1,000 feet of the
source area: four had been replaced by municipal water and the fifth (WSW-3 / Dover well) was
not in use. The Dover well was located on a vacant lot; it had no power and the piping had been
cut. Mr. Dover did not want to abandon his well as he was considering using the property for
"urban farming" and thought the well could be used for irrigation.
The Moose and Dover wells were checked for this report, the results follow.
1. Moose Residence / WSW-6
The City of Concord Utilities Department was contacted and the department now provides
municipal water to the Moose residence.
2. Dover Well / WSW-3
The Dover well was inspected during this sampling event and there has been no change since
2015. The property remains vacant; there is no evidence of farming.
2.0 MONITOR WELL SAMPLING
2.1 Sampling Protocol
Monitor wells 1, 2, 3, 4, 5, and VMW-1 were sampled April 14, 2020 with new, individual,
disposable bailers after first gauging the wells and then purging three well casing volumes. The
samples were placed in laboratory provided vials, fixed with a chain of custody, and placed on
ice for immediate delivery to PACE Analytical.
2.2 Sampling Results
The samples were analyzed by EPA method 6200B. The results are posted in Table B-4 and a
historical sampling results table is attached. A summary follows:
MW-1: benzene (44 ppb) > standard / < GCL,
MW-2: non -detect,
MW-3: non -detect,
MW-4: non -detect,
MW-5: non -detect, and
VMW-1: non -detect.

A comparison with the 2015 sampling event follows:
MW-1: BTEX/MTBE decrease,
MW-2: remain non -detect,
MW-3: remain non -detect,
MW-4: remain non -detect,
MW-5: MTBE (only 2015 detection) decrease to <1, and
VMW-1: remain non -detect.
F. FREE PRODUCT — none
G. SOIL REMEDIATION -- not applicable
H. GROUNDWATER REMEDIATION
Natural attenuation is effective at the site as all detected compounds decreased in MW-1 and
MTBE has dropped to non -detect in MW-5.
I. CONCLUSIONS
Groundwater contaminants are present in MW-1; benzene is the only compound detected above
its standard, but it is well below its gross contaminant level. Contaminant levels decreased from
the 2015 sampling event. The Moose residence is serviced by municipal water; their well was
the only potable well from the 2015 survey. The Dover well status has not changed; it is not in
use and the property is not developed.
J. FIGURES
USGS Topographic Map
Water Supply Well Map
Site Map
Groundwater Flow Map
Benzene Iso-Concentration Map
K. TABLES
Table B-4
Summary of Groundwater Sampling
Table 1
Historical Groundwater Sampling
Table B-5
Water Supply Well Information
Table B-7
Well Construction Information
L. APPENDICES: Laboratory Analysis / Chain of Custody — on CD
W

Buck iT
20 Wwan C Coleman Boulevard
Concord, North Camlima
A&W Pmjea No 041 MX
a RBI
conco.re-, Nc 7 Y2 Nrmm Qaa&angje
USM Topopmplav, map
Scd&- !"=2,GW

IVATERS--MYWdL-POTAW--ORUMM��NiZE
VU;v V. Q-1 MM� vmkm m
SLUEm: =a?"CpArx FM=
mam
Kiij -g � -, r, 9 1
DATE: M-111104
SCIU,-P : AS SHM
BY: DE

i
q Monitor Well
(0 Monitor Well; vertical extent
11 former UST basin
N SITE MAP
LITTLE BUCK 2
CABARRUS COUNTY
1" = 75`

small local.
hzcth
74.65
7.38 2
4
AXT� -Fr l I /1G7C e-lTi-
GROUNDWATER FLOW
LITTLE BUCK 2
CABARRUS COUNTY
75'
4-14-20

N
Benzene
STD; 1 ppb
GCL_ 5000 ppb
BENZENE CONCENTRATION MAP
LITTLE BUCK 2
CABARRUS COUNTY
1" - 75'
4-14-20

Appendix F
Guidance Pertaining to Releases from Contaminant Sources other than USTs
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 5-12-20 Incident Number and Name: 27741 Little Busk II Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)4
6200B
6200B
6200B'
6200B
6200B
6200B
6200B
6200B
6200B
504.1
Contaminant of Concern/ Field Measurement4
„
N
y
N
N
i
�
cC
W
Well or
Date
Sample
Incident
SW ID
Collected
ID
Phase
MW-1
4-14-20
MW-1
monitor
44
39
53
176
6
<1
5
<I
<1
MW-2
MW-2
C4<1
<1
<1
<2
<1
<1
<2
<1
<1
MW-3
MW-3
64<1
<1
<1
<2
<1
<1
<2
<1
<1
MW-4
MW-4
64<I
<I
<1
<2
<I
<1
<2
<I
<I
MW-5
MW-5
<1
<1
<1
<2
<1
<1
<2
<I
<1
VMW-1
VMW-1
<1
<1
<I
<2
<1
<1
<2
<I
<1
Minimum Reporting Limit (ug/1)
2L Standard (ug/1)
1
600
600
500
20
70
6
0.4
0.02
0.02
GCL (ug/1)
5000
260000
84500
85500
20000
70000
6000
400
50
50
NC 2B Standard or EPA National Criteria
(ug/1)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level
Results rounded to whole numbers

Appendix F
Guidance Pertaining to Releases from Contaminant Sources other than USTs
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 5-12-20 Incident Number and Name: 27741 Little Buck II Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)4
6200B
6200B
6200B
6200B'
6200B'
6200B
6200B
6200B
3030C
Contaminant of Concern/ Field Measurement4
U
U
N
N
It N
L
Cd
H
C
Well or
Date
Sample
Incident
SW ID
Collected
ID
Phase
MW-1
4-14-20
MW-I
monitor
<1
<1
<1
3
<1
<1
36
14
MW-2
64MW-2
66<1
<1
<1
<2
<1
<1
<2
<1
MW-3
MW-3
46<1
<1
<1
<2
<1
<1
<2
<1
MW-4
MW-4
64<1
<1
<1
<2
<1
<1
<2
<1
MW-5
MW-5
64<1
<1
<1
<2
<1
<1
<2
<1
VMW-1
VMW-1
<1
<1
<I
<2
<1
<I
<2
<1
Minimum Reporting Limit (ug/1)
2L Standard (ug/1)
70
70
70
70
70
70
400
400
15
GCL (ug/1)
6900
8500
15000
25000
30000
70000
28500
25000
15000
NC 2B Standard or EPA National Criteria
(ug/1)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level
Results rounded to whole numbers

TABLE 1
HISTORICAL GROUNDWATER SAMPLING
Benzene
Toluene
Ethylben.
Xylenes
MTBE
Naphtha
EDB
NC 2L Standard
1
600
600
500
20
6
0.02
Gross Cont. Level
5000
260000
84500
85500
20000
6000
50
TW-2 7-27-04
1900
4300
1300
6900
1400
87
940
MW-1 10-21-10
474
586
162
605
475
7
0.067
2-02-11
566
913
172
918
430
10
<1
8-30-11
528
911
192
1105
369
14
<1
3-21-12
550
882
155
769
403
<10
<3
10-19-12
379
638
126
637
403
<10
<3
4-18-13
428
710
143
654
396
<10
<3
11-16-13
86
9
19
324
<1
13
1
6-19-14
272
369
140
581
344
21
<1
2-10-15
401
601
162
683
319
7
<1
9-17-15
259
442
124
571
184
<10
<3
4-14-20
44
39
53
176
6
5
<1
MW-2 11-18-04
ND
ND
1
1
ND
ND
ND
10-21-10
<1
<1
<1
<2
<1
<2
<.019
8-30-11
<1
<1
1
2
<1
<2
<1
3-21-12
<1
<1
<1
<2
<1
<2
<1
10-19-12
<1
<1
<1
<2
<1
<2
<1
4-18-13
<1
<1
<1
<2
<1
<2
<1
11-16-13
<1
<1
<1
<2
<1
<2
<1
6-19-14
<1
<1
<1
<2
<1
<2
<1
2-10-15
<1
<1
<1
<2
<1
<2
<1
9-17-15
<1
<1
<1
<2
<1
<2
<1
4-14-20
<1
<1
<1
<2
<1
<2
<1

TABLE 1
HISTORICAL GROUNDWATER SAMPLING
Benzene
Toluene
Ethylben.
Xylenes
MTBE
Naphtha
EDB
NC 2L Standard
1
600
600
500
20
6
0.02
Gross Cont. Level
5000
260000
84500
85500
20000
6000
50
MW-3 11-18-04
ND
ND
ND
ND
3
ND
ND
10-21-10
<1
<1
<1
<2
<l
<2
<.020
8-30-11
<1
1
<1
2
<l
<2
<1
3-21-12
<1
<1
<1
<2
<l
<2
<1
10-19-12
<1
<1
<1
<2
<l
<2
<1
4-18-13
<1
<1
<1
<2
<1
<2
<1
11-16-13
<1
<1
<1
<2
<1
<2
<1
6-19-14
<1
<1
<1
<2
<l
<2
<1
2-10-15
<1
<1
<1
<2
<l
<2
<1
9-17-15
<1
<1
<1
<2
<l
<2
<1
4-14-20
<1
<1
<1
<2
<1
<2
<1
MW-4 12-06-04
ND
ND
ND
ND
ND
ND
ND
10-21-10
<1
<1
<1
<2
<1
<2
<.019
8-30-11
<1
<1
<1
<2
<1
<2
<1
3-21-12
<1
<1
<1
<2
<1
<2
<1
10-19-12
<1
<1
<1
<2
<1
<2
<1
4-18-13
<1
<1
<1
<2
<1
<2
<1
11-16-13
<1
<1
<1
<2
<1
<2
<1
6-19-14
<1
<1
<1
<2
<1
<2
<1
2-10-15
<1
<1
<1
<2
<1
<2
<1
9-17-15
<1
<1
<1
<2
<1
<2
<1
4-14-20
<1
<1
<1
<2
<1
<2
<1

TABLE 1
HISTORICAL GROUNDWATER SAMPLING
Benzene
Toluene
Ethylben.
Xylenes
MTBE
Naphtha
EDB
NC 2L Standard
1
600
600
500
20
6
0.02
Gross Cont. Level
5000
260000
84500
85500
20000
6000
50
MW-5 10-06-15
<1
<1
<1
<2
14
<2
<1
4-14-20
<1
<1
<1
<2
<1
<2
<1
VE-1 11-19-04
10
ND
7
41
3
ND
0.12
10-21-10
12
50
9
42
1
6
<.020
8-30-11
1
4
1
4
1
<2
<1
3-21-12
1
2
1
2
1
<2
<1
10-19-12
<1
<1
<1
<2
<1
<2
<1
4-18-13
<1
<1
<1
<2
<l
<2
<1
11-16-13
<1
<1
<1
<2
<l
<2
<1
6-19-14
<1
<1
<1
<2
<1
<2
<1
2-10-15
<1
<1
<1
<2
<1
<2
<1
9-17-15
<1
<1
<1
<2
<1
<2
<1
4-14-20
<1
<1
<1
<2
<1
<2
<1

Appendix B
Reporting Tables
Table B S Public and. Private Water Su�p� plWell and Other Receptor Information
Revision Date: 201 5 Incident Number and Name: Litt e uek II Facility 1D4:
(Include the following information. The well number (can use tax number). well owner and user names, addresses and telephone numbers, use of the well
(potable, agricultural, etc.), well depth, type of ',vell (Le., drilled or bored). well casing depth, well screen interval and distance of well from the source area of the
release)
Public and Private Water Sunoly Wells
Distance
Well
Well
Well
from
v
Well 9
Well Owner/ User
Address
Phone
Well
Depth
Type
°
Casing
Sereen
interval
source
area of
o
C.
(indicate which)
Number
Use
(ft
Well
Depth (t,
(Y'tov
release
Owner
Concord NC 28027
704
>��s}
acs}
ft. 1305)
(a.)
3
WSW-1
Beamon, Paul
705 Cab-arrus Ave
7860913
aban.
140
drill
?
?
525
dcown
WSW-2
Spears, Carol
703 Cabarrus Ave
786 2244
NU
?
?
?
?
475
down
WSW-3
Dover, Aubry
557 Cabarrus .Ave
786 7044
NU
100+
drill
?
?
600
down
WSW-4
Carpenter, Jeffel7y745
Cabarrus Ave
786 723
NLU
?
?
?
?
62..5
up
WSW-5
CFCU
see below
NU
?
?
?
?
950
up
W&R-6
Moose, C E
6 Second St
782 250
potab
e 144
drill
?
?
1015
down
Ft BGS w feet below ground surface
Other Receptors 2020 update: Moose residence serviced by municipal water
(other public water supplies, reservoirs. water supply Ilnes, surface water bodies, we]lhead protectloi1 areas, recharge areas for deep aquifers, subsurface
StructuregI
Receptor
ID
Description
Location
Contact
Phone
Number
Usage
Up or
down-
gradient
Distance from
source area of
release ft.)
NU = not in use
CFCU: Call Federal Credit Union, 4605 Commerce Rd, Richmond VA 23234
1 800 796 2328 ext 41270 / Karen Salmons
75

Appendix 13
Reporting, Tables
Table B -- 5 :Public and Private Water Supply Well and Other Receptor Information
Revision Dale: 2 015 Incident Nuinber and Nanie: Little Buck 11 Facility IDN:
(Inc ILI de the I'laIIowing inrorination. The we I I nuinber (can use tax nwnber)• weII owner and user names, addresses and telephone numbers, use of' the well
(potable, agricultural, etc.), wel! depth. type of well (i.e., drilled or bored). well casing depth. well screen interval and distance of well from the source area orthe
release)
Public and Private Water Surmlv Wells
Distance
Wei]
Well
Well
front
Well N
Well Owner/ User
Address
Phone
Well
Depth
Type
Of
Casinged
Screen
Ltterval
source
area of
o
CIO
(indicate which)
Number
Use
(ft
Well
Depth (f .
(Yto V
release
a
Owner
Concord, NC 28027
704
13GS)
BG5)
fl. SGS)
(11.)
�
WSW-7
Cook, Richard
8 Second St
7862509
IW
?
drill
?
?
1030
down.
WSW-8
First Assembly
150 W C Coleman
7934740
IR
?
?
?
?
1000.1-
down
WSW-9
Blvd
"
1R
?
?
?
?
1000+
down.
WSW-10
Wolfe, James
553 Irish Potato
7886441
NU
?
?
?
?
750
down
Rd 28025
Ft € OS = feet below ground surl'ace
Other Receptors
tother public water supplies. reservoirs, water supply lines, surface water bodies. titi•ellliead protection areas. recharge areas for deep aquifers, subsurl:ace
clrisr.niresl
Receptor
1D
Description
Location
Contact
Phone
Number
Usage
Up or
down-
gradient
Distance front
source area of
release ft.)
1R = irrigation
First Assembly not respond, irrigation is from 2004 survey
City of. Concord confirm public water to First Assembly
75

Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 5-12-20 Incident Number and Name: Little Buck 2 Facility ID#:
Date
Date
Well
Well
Screened
Depth
Top of
Depth to
Free
Groundwater
Latitude/
Well ID
Installed
Water
Casing
Casing
Interval
of Well
Casing
Water
Product
Elevation*
Longitude
(m/dd/yy)
Level
Diameter
Depth
(x to y
(ft.
Elevation*
from Top
Thickness
(ft.)
(decimal
Measured
(in.)
(ft.
ft. BGS)
BGS)
(ft.)
of Casing
** (ft.)
degrees)***
m/dd/
BGS
ft.
MW-1
11-18-04
4-14-20
2
25
25-40
40
100.00
28.99
0.00
71.01
35.3966
80.6067
MW-2
11-18-04
2
25
25-40
40
96.17
21.52
74.65
35.3970
80.6065
MW-3
11-18-04
2
25
40
40
96.16
23.78
`°
72.38
35.3968
80.6064
MW-4
12-02-04
2
25
25-40
40
103.13
25.07
78.06
35.3961
80.6072
MW-5
10-04-15
2
22
22-32
32
95.45
25.30
70.15
35.3966
80.6065
35.3966
VMW-1
11-19-04
2
65
65-70
70
100.01
26.93
73.08
80.6067
Ft BGS = feet below ground surface
* Reference Point for Elevation MeasurementsMW-1, Assumed Elevation: 100.00 ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation -Depth to Water] + [free product thickness x 0.8581]
*** The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 28, 2020
Mr. Richard Kelly
SE Geologic
301 Windsor Dr.
Shelby, NC 28150
RE: Project: Little Buck 2
Pace Project No.: 92473680
Dear Mr. Kelly:
Enclosed are the analytical results for sample(s) received by the laboratory on April 14, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: Little Buck 2
Pace Project No.: 92473680
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Little Buck 2
Pace Project No.: 92473680
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92473680001 MW-1
SM 6200B
SAS
63
PASI-C
92473680002 MW-2
SM 6200B
SAS
63
PASI-C
92473680003 MW-3
SM 6200B
SAS
63
PASI-C
92473680004 MW-4
SM 6200B
SAS
63
PASI-C
92473680005 MW-5
SM 6200B
SAS
63
PASI-C
92473680006 VMW-1
SM 6200B
SAS
63
PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-1 Lab ID: 92473680001 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
44.3
ug/L
0.50
1
04/27/20 22:39
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/27/20 22:39
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
04/27/20 22:39
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/27/20 22:39
75-27-4
Bromoform
ND
ug/L
0.50
1
04/27/20 22:39
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/27/20 22:39
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
04/27/20 22:39
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/27/20 22:39
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
04/27/20 22:39
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/27/20 22:39
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/27/20 22:39
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/27/20 22:39
75-00-3
Chloroform
ND
ug/L
0.50
1
04/27/20 22:39
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/27/20 22:39
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/27/20 22:39
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/27/20 22:39
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/27/20 22:39
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/27/20 22:39
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/27/20 22:39
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/27/20 22:39
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/27/20 22:39
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/27/20 22:39
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/27/20 22:39
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/27/20 22:39
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/27/20 22:39
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/27/20 22:39
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/27/20 22:39
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/27/20 22:39
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/27/20 22:39
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/27/20 22:39
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/27/20 22:39
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/27/20 22:39
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/27/20 22:39
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/27/20 22:39
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
04/27/20 22:39
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
04/27/20 22:39
108-20-3
Ethylbenzene
53.4
ug/L
0.50
1
04/27/20 22:39
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/27/20 22:39
87-68-3
Isopropylbenzene (Cumene)
2.5
ug/L
0.50
1
04/27/20 22:39
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/27/20 22:39
75-09-2
Methyl-tert-butyl ether
5.8
ug/L
0.50
1
04/27/20 22:39
1634-04-4
Naphthalene
5.0
ug/L
2.0
1
04/27/20 22:39
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/27/20 22:39
103-65-1
Styrene
ND
ug/L
0.50
1
04/27/20 22:39
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/27/20 22:39
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/27/20 22:39
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-1 Lab ID: 92473680001 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
04/27/20 22:39
127-18-4
Toluene
39.0
ug/L
0.50
1
04/27/20 22:39
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/27/20 22:39
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/27/20 22:39
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/27/20 22:39
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/27/20 22:39
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/27/20 22:39
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/27/20 22:39
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/27/20 22:39
96-18-4
1,2,4-Trimethylbenzene
36.1
ug/L
0.50
1
04/27/20 22:39
95-63-6
1,3,5-Trimethylbenzene
14.3
ug/L
0.50
1
04/27/20 22:39
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/27/20 22:39
75-01-4
m&p-Xylene
140
ug/L
1.0
1
04/27/20 22:39
179601-23-1
o-Xylene
36.3
ug/L
0.50
1
04/27/20 22:39
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
92
%
70-130
1
04/27/20 22:39
17060-07-0
4-Bromofluorobenzene (S)
97
%
70-130
1
04/27/20 22:39
460-00-4
Toluene-d8(S)
103
%
70-130
1
04/27/20 22:39
2037-26-5
Date: 04/28/2020 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-2 Lab ID: 92473680002 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
04/25/20 19:09
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/25/20 19:09
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
04/25/20 19:09
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/25/20 19:09
75-27-4
Bromoform
ND
ug/L
0.50
1
04/25/20 19:09
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/25/20 19:09
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
04/25/20 19:09
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/25/20 19:09
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
04/25/20 19:09
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/25/20 19:09
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/25/20 19:09
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/25/20 19:09
75-00-3
Chloroform
ND
ug/L
0.50
1
04/25/20 19:09
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/25/20 19:09
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 19:09
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 19:09
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/25/20 19:09
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/25/20 19:09
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/25/20 19:09
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/25/20 19:09
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 19:09
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 19:09
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 19:09
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/25/20 19:09
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/25/20 19:09
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/25/20 19:09
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/25/20 19:09
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 19:09
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 19:09
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 19:09
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/25/20 19:09
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 19:09
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/25/20 19:09
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 19:09
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 19:09
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
04/25/20 19:09
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
04/25/20 19:09
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/25/20 19:09
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
04/25/20 19:09
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/25/20 19:09
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/25/20 19:09
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/25/20 19:09
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/25/20 19:09
103-65-1
Styrene
ND
ug/L
0.50
1
04/25/20 19:09
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 19:09
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 19:09
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-2 Lab ID: 92473680002 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
04/25/20 19:09
127-18-4
Toluene
ND
ug/L
0.50
1
04/25/20 19:09
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 19:09
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 19:09
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/25/20 19:09
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/25/20 19:09
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/25/20 19:09
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/25/20 19:09
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/25/20 19:09
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 19:09
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 19:09
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/25/20 19:09
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
04/25/20 19:09
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/25/20 19:09
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
04/25/20 19:09
17060-07-0
4-Bromofluorobenzene (S)
97
%
70-130
1
04/25/20 19:09
460-00-4
Toluene-d8(S)
104
%
70-130
1
04/25/20 19:09
2037-26-5
Date: 04/28/2020 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-3 Lab ID: 92473680003 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
04/25/20 20:03
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/25/20 20:03
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
04/25/20 20:03
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/25/20 20:03
75-27-4
Bromoform
ND
ug/L
0.50
1
04/25/20 20:03
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/25/20 20:03
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
04/25/20 20:03
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/25/20 20:03
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
04/25/20 20:03
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/25/20 20:03
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/25/20 20:03
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/25/20 20:03
75-00-3
Chloroform
ND
ug/L
0.50
1
04/25/20 20:03
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/25/20 20:03
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 20:03
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 20:03
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/25/20 20:03
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/25/20 20:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/25/20 20:03
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/25/20 20:03
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:03
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:03
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:03
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/25/20 20:03
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/25/20 20:03
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/25/20 20:03
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:03
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:03
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:03
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:03
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:03
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:03
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:03
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
04/25/20 20:03
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
04/25/20 20:03
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/25/20 20:03
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
04/25/20 20:03
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/25/20 20:03
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/25/20 20:03
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/25/20 20:03
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/25/20 20:03
103-65-1
Styrene
ND
ug/L
0.50
1
04/25/20 20:03
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 20:03
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 20:03
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-3 Lab ID: 92473680003 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
04/25/20 20:03
127-18-4
Toluene
ND
ug/L
0.50
1
04/25/20 20:03
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 20:03
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 20:03
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/25/20 20:03
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/25/20 20:03
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/25/20 20:03
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/25/20 20:03
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/25/20 20:03
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 20:03
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 20:03
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/25/20 20:03
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
04/25/20 20:03
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/25/20 20:03
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
04/25/20 20:03
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
1
04/25/20 20:03
460-00-4
Toluene-d8(S)
104
%
70-130
1
04/25/20 20:03
2037-26-5
Date: 04/28/2020 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-4 Lab ID: 92473680004 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
04/25/20 20:21
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/25/20 20:21
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
04/25/20 20:21
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/25/20 20:21
75-27-4
Bromoform
ND
ug/L
0.50
1
04/25/20 20:21
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/25/20 20:21
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
04/25/20 20:21
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/25/20 20:21
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
04/25/20 20:21
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/25/20 20:21
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/25/20 20:21
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/25/20 20:21
75-00-3
Chloroform
ND
ug/L
0.50
1
04/25/20 20:21
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/25/20 20:21
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 20:21
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 20:21
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/25/20 20:21
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/25/20 20:21
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/25/20 20:21
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/25/20 20:21
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:21
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:21
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:21
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/25/20 20:21
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/25/20 20:21
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/25/20 20:21
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:21
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:21
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:21
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:21
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:21
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:21
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:21
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:21
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
04/25/20 20:21
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
04/25/20 20:21
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/25/20 20:21
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
04/25/20 20:21
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/25/20 20:21
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/25/20 20:21
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/25/20 20:21
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/25/20 20:21
103-65-1
Styrene
ND
ug/L
0.50
1
04/25/20 20:21
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 20:21
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 20:21
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-4 Lab ID: 92473680004 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
04/25/20 20:21
127-18-4
Toluene
ND
ug/L
0.50
1
04/25/20 20:21
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 20:21
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 20:21
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/25/20 20:21
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/25/20 20:21
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/25/20 20:21
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/25/20 20:21
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/25/20 20:21
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 20:21
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 20:21
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/25/20 20:21
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
04/25/20 20:21
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/25/20 20:21
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
04/25/20 20:21
17060-07-0
4-Bromofluorobenzene (S)
99
%
70-130
1
04/25/20 20:21
460-00-4
Toluene-d8(S)
105
%
70-130
1
04/25/20 20:21
2037-26-5
Date: 04/28/2020 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-5 Lab ID: 92473680005 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
04/25/20 20:38
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/25/20 20:38
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
04/25/20 20:38
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/25/20 20:38
75-27-4
Bromoform
ND
ug/L
0.50
1
04/25/20 20:38
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/25/20 20:38
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
04/25/20 20:38
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/25/20 20:38
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
04/25/20 20:38
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/25/20 20:38
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/25/20 20:38
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/25/20 20:38
75-00-3
Chloroform
ND
ug/L
0.50
1
04/25/20 20:38
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/25/20 20:38
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 20:38
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 20:38
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/25/20 20:38
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/25/20 20:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/25/20 20:38
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/25/20 20:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:38
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:38
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:38
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/25/20 20:38
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/25/20 20:38
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/25/20 20:38
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:38
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:38
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:38
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:38
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:38
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:38
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
04/25/20 20:38
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
04/25/20 20:38
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/25/20 20:38
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
04/25/20 20:38
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/25/20 20:38
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/25/20 20:38
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/25/20 20:38
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/25/20 20:38
103-65-1
Styrene
ND
ug/L
0.50
1
04/25/20 20:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 20:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 20:38
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: MW-5 Lab ID: 92473680005 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
04/25/20 20:38
127-18-4
Toluene
ND
ug/L
0.50
1
04/25/20 20:38
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 20:38
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 20:38
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/25/20 20:38
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/25/20 20:38
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/25/20 20:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/25/20 20:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/25/20 20:38
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 20:38
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 20:38
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/25/20 20:38
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
04/25/20 20:38
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/25/20 20:38
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
04/25/20 20:38
17060-07-0
4-Bromofluorobenzene (S)
97
%
70-130
1
04/25/20 20:38
460-00-4
Toluene-d8(S)
105
%
70-130
1
04/25/20 20:38
2037-26-5
Date: 04/28/2020 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: VMW-1 Lab ID: 92473680006 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
04/25/20 20:56
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/25/20 20:56
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
04/25/20 20:56
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/25/20 20:56
75-27-4
Bromoform
ND
ug/L
0.50
1
04/25/20 20:56
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/25/20 20:56
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
04/25/20 20:56
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/25/20 20:56
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
04/25/20 20:56
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/25/20 20:56
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/25/20 20:56
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/25/20 20:56
75-00-3
Chloroform
ND
ug/L
0.50
1
04/25/20 20:56
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/25/20 20:56
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 20:56
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/25/20 20:56
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/25/20 20:56
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/25/20 20:56
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/25/20 20:56
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/25/20 20:56
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:56
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:56
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/25/20 20:56
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/25/20 20:56
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/25/20 20:56
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/25/20 20:56
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:56
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:56
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/25/20 20:56
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:56
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:56
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/25/20 20:56
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:56
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:56
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
04/25/20 20:56
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
04/25/20 20:56
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
04/25/20 20:56
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/25/20 20:56
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
04/25/20 20:56
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/25/20 20:56
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/25/20 20:56
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/25/20 20:56
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/25/20 20:56
103-65-1
Styrene
ND
ug/L
0.50
1
04/25/20 20:56
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 20:56
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/25/20 20:56
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Little Buck 2
Pace Project No.: 92473680
Sample: VMW-1 Lab ID: 92473680006 Collected: 04/14/20 12:00 Received: 04/14/20 16:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
04/25/20 20:56
127-18-4
Toluene
ND
ug/L
0.50
1
04/25/20 20:56
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 20:56
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/25/20 20:56
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/25/20 20:56
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/25/20 20:56
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/25/20 20:56
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/25/20 20:56
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/25/20 20:56
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 20:56
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
04/25/20 20:56
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/25/20 20:56
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
04/25/20 20:56
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/25/20 20:56
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
04/25/20 20:56
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
1
04/25/20 20:56
460-00-4
Toluene-d8(S)
105
%
70-130
1
04/25/20 20:56
2037-26-5
Date: 04/28/2020 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
QC Batch: 537925 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92473680002, 92473680003, 92473680004, 92473680005, 92473680006
METHOD BLANK: 2868580 Matrix: Water
Associated Lab Samples: 92473680002, 92473680003, 92473680004, 92473680005, 92473680006
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
04/25/20 18:51
1,1,1-Trichloroethane
ug/L
ND
0.50
04/25/20 18:51
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
04/25/20 18:51
1,1,2-Trichloroethane
ug/L
ND
0.50
04/25/20 18:51
1,1-Dichloroethane
ug/L
ND
0.50
04/25/20 18:51
1,1-Dichloroethene
ug/L
ND
0.50
04/25/20 18:51
1,1-Dichloropropene
ug/L
ND
0.50
04/25/20 18:51
1,2,3-Trichlorobenzene
ug/L
ND
2.0
04/25/20 18:51
1,2,3-Trichloropropane
ug/L
ND
0.50
04/25/20 18:51
1,2,4-Trichlorobenzene
ug/L
ND
2.0
04/25/20 18:51
1,2,4-Trimethylbenzene
ug/L
ND
0.50
04/25/20 18:51
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
04/25/20 18:51
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
04/25/20 18:51
1,2-Dichlorobenzene
ug/L
ND
0.50
04/25/20 18:51
1,2-Dichloroethane
ug/L
ND
0.50
04/25/20 18:51
1,2-Dichloropropane
ug/L
ND
0.50
04/25/20 18:51
1,3,5-Trimethylbenzene
ug/L
ND
0.50
04/25/20 18:51
1,3-Dichlorobenzene
ug/L
ND
0.50
04/25/20 18:51
1,3-Dichloropropane
ug/L
ND
0.50
04/25/20 18:51
1,4-Dichlorobenzene
ug/L
ND
0.50
04/25/20 18:51
2,2-Dichloropropane
ug/L
ND
0.50
04/25/20 18:51
2-Chlorotoluene
ug/L
ND
0.50
04/25/20 18:51
4-Chlorotoluene
ug/L
ND
0.50
04/25/20 18:51
Benzene
ug/L
ND
0.50
04/25/20 18:51
Bromobenzene
ug/L
ND
0.50
04/25/20 18:51
Bromochloromethane
ug/L
ND
0.50
04/25/20 18:51
Bromodichloromethane
ug/L
ND
0.50
04/25/20 18:51
Bromoform
ug/L
ND
0.50
04/25/20 18:51
Bromomethane
ug/L
ND
5.0
04/25/20 18:51
Carbon tetrachloride
ug/L
ND
0.50
04/25/20 18:51
Chlorobenzene
ug/L
ND
0.50
04/25/20 18:51
Chloroethane
ug/L
ND
1.0
04/25/20 18:51
Chloroform
ug/L
ND
0.50
04/25/20 18:51
Chloromethane
ug/L
ND
1.0
04/25/20 18:51
cis-1,2-Dichloroethene
ug/L
ND
0.50
04/25/20 18:51
cis-1,3-Dichloropropene
ug/L
ND
0.50
04/25/20 18:51
Dibromochloromethane
ug/L
ND
0.50
04/25/20 18:51
Dibromomethane
ug/L
ND
0.50
04/25/20 18:51
Dichlorodifluoromethane
ug/L
ND
0.50
04/25/20 18:51
Diisopropyl ether
ug/L
ND
0.50
04/25/20 18:51
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
METHOD BLANK: 2868580 Matrix: Water
Associated Lab Samples: 92473680002, 92473680003, 92473680004, 92473680005, 92473680006
Blank Reporting
Parameter Units Result Limit Analyzed
Ethylbenzene
ug/L
ND
0.50
04/25/20 18:51
Hexachloro-1,3-butadiene
ug/L
ND
2.0
04/25/20 18:51
Isopropylbenzene (Cumene)
ug/L
ND
0.50
04/25/20 18:51
m&p-Xylene
ug/L
ND
1.0
04/25/20 18:51
Methyl-tert-butyl ether
ug/L
ND
0.50
04/25/20 18:51
Methylene Chloride
ug/L
ND
2.0
04/25/20 18:51
n-Butylbenzene
ug/L
ND
0.50
04/25/20 18:51
n-Propylbenzene
ug/L
ND
0.50
04/25/20 18:51
Naphthalene
ug/L
ND
2.0
04/25/20 18:51
o-Xylene
ug/L
ND
0.50
04/25/20 18:51
sec-Butylbenzene
ug/L
ND
0.50
04/25/20 18:51
Styrene
ug/L
ND
0.50
04/25/20 18:51
tert-Butyl benzene
ug/L
ND
0.50
04/25/20 18:51
Tetrachloroethene
ug/L
ND
0.50
04/25/20 18:51
Toluene
ug/L
ND
0.50
04/25/20 18:51
trans-1,2-Dichloroethene
ug/L
ND
0.50
04/25/20 18:51
trans- 1,3-Dichloropropene
ug/L
ND
0.50
04/25/20 18:51
Trichloroethene
ug/L
ND
0.50
04/25/20 18:51
Trichlorofluoromethane
ug/L
ND
1.0
04/25/20 18:51
Vinyl chloride
ug/L
ND
1.0
04/25/20 18:51
1,2-Dichloroethane-d4 (S)
%
97
70-130
04/25/20 18:51
4-Bromofluorobenzene (S)
%
96
70-130
04/25/20 18:51
Toluene-d8 (S)
%
104
70-130
04/25/20 18:51
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2868581
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
52.6
105
60-140
1,1,1-Trichloroethane
ug/L
50
50.6
101
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
49.5
99
60-140
1,1,2-Trichloroethane
ug/L
50
48.9
98
60-140
1,1-Dichloroethane
ug/L
50
49.0
98
60-140
1,1-Dichloroethene
ug/L
50
50.2
100
60-140
1,1-Dichloropropene
ug/L
50
53.9
108
60-140
1,2,3-Trichlorobenzene
ug/L
50
54.5
109
60-140
1,2,3-Trichloropropane
ug/L
50
48.2
96
60-140
1,2,4-Trichlorobenzene
ug/L
50
52.9
106
60-140
1,2,4-Trimethylbenzene
ug/L
50
49.3
99
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
51.5
103
60-140
1,2-Dibromoethane (EDB)
ug/L
50
53.1
106
60-140
1,2-Dichlorobenzene
ug/L
50
50.4
101
60-140
1,2-Dichloroethane
ug/L
50
45.7
91
60-140
1,2-Dichloropropane
ug/L
50
50.0
100
60-140
1,3,5-Trimethylbenzene
ug/L
50
50.2
100
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
LABORATORY CONTROL SAMPLE:
Parameter
2868581
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
50.1
100
60-140
1,3-Dichloropropane
ug/L
50
50.3
101
60-140
1,4-Dichlorobenzene
ug/L
50
49.4
99
60-140
2,2-Dichloropropane
ug/L
50
50.8
102
60-140
2-Chlorotoluene
ug/L
50
50.6
101
60-140
4-Chlorotoluene
ug/L
50
50.9
102
60-140
Benzene
ug/L
50
51.1
102
60-140
Bromobenzene
ug/L
50
47.7
95
60-140
Bromochloromethane
ug/L
50
50.6
101
60-140
Bromodichloromethane
ug/L
50
54.5
109
60-140
Bromoform
ug/L
50
52.9
106
60-140
Bromomethane
ug/L
50
56.8
114
60-140
Carbon tetrachloride
ug/L
50
55.0
110
60-140
Chlorobenzene
ug/L
50
50.6
101
60-140
Chloroethane
ug/L
50
45.2
90
60-140
Chloroform
ug/L
50
49.8
100
60-140
Chloromethane
ug/L
50
44.8
90
60-140
cis-1,2-Dichloroethene
ug/L
50
49.5
99
60-140
cis-1,3-Dichloropropene
ug/L
50
54.3
109
60-140
Dibromochloromethane
ug/L
50
52.2
104
60-140
Dibromomethane
ug/L
50
49.6
99
60-140
Dichlorodifluoromethane
ug/L
50
49.8
100
60-140
Diisopropyl ether
ug/L
50
51.4
103
60-140
Ethylbenzene
ug/L
50
48.3
97
60-140
Hexachloro-1,3-butadiene
ug/L
50
53.8
108
60-140
Isopropylbenzene (Cumene)
ug/L
50
51.2
102
60-140
m&p-Xylene
ug/L
100
99.4
99
60-140
Methyl-tert-butyl ether
ug/L
50
53.2
106
60-140
Methylene Chloride
ug/L
50
47.5
95
60-140
n-Butylbenzene
ug/L
50
50.8
102
60-140
n-Propylbenzene
ug/L
50
48.2
96
60-140
Naphthalene
ug/L
50
55.8
112
60-140
o-Xylene
ug/L
50
49.7
99
60-140
sec-Butylbenzene
ug/L
50
49.5
99
60-140
Styrene
ug/L
50
54.0
108
60-140
tert-Butyl benzene
ug/L
50
42.3
85
60-140
Tetrachloroethene
ug/L
50
51.9
104
60-140
Toluene
ug/L
50
47.2
94
60-140
trans-1,2-Dichloroethene
ug/L
50
51.0
102
60-140
trans- 1,3-Dichloropropene
ug/L
50
54.8
110
60-140
Trichloroethene
ug/L
50
51.9
104
60-140
Trichlorofluoromethane
ug/L
50
43.9
88
60-140
Vinyl chloride
ug/L
50
47.9
96
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2870468
2870469
MS
MSD
92474518006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
1000
1000
1100
1070
110
107
60-140
3
1,1,1-Trichloroethane
ug/L
ND
1000
1000
1140
1140
114
114
60-140
0
1,1,2,2-Tetrachloroethane
ug/L
ND
1000
1000
1080
1020
108
102
60-140
5
1,1,2-Trichloroethane
ug/L
ND
1000
1000
991
975
99
97
60-140
2
1,1-Dichloroethane
ug/L
ND
1000
1000
1090
1090
109
109
60-140
0
1,1-Dichloroethene
ug/L
ND
1000
1000
1170
1160
117
116
60-140
1
1,1-Dichloropropene
ug/L
ND
1000
1000
1220
1190
122
119
60-140
3
1,2,3-Trichlorobenzene
ug/L
ND
1000
1000
1050
1010
105
101
60-140
3
1,2,3-Trichloropropane
ug/L
ND
1000
1000
1050
962
105
96
60-140
9
1,2,4-Trichlorobenzene
ug/L
ND
1000
1000
1060
1070
106
107
60-140
1
1,2,4-Trimethylbenzene
ug/L
1070
1000
1000
2240
2180
117
111
60-140
2
1,2-Dibromo-3-chloropropane
ug/L
ND
1000
1000
1130
1130
113
113
60-140
0
1,2-Dibromoethane (EDB)
ug/L
ND
1000
1000
1090
1080
109
108
60-140
1
1,2-Dichlorobenzene
ug/L
ND
1000
1000
1050
1010
105
101
60-140
4
1,2-Dichloroethane
ug/L
132
1000
1000
1090
1090
96
95
60-140
0
1,2-Dichloropropane
ug/L
ND
1000
1000
1080
1050
108
105
60-140
3
1,3,5-Trimethylbenzene
ug/L
378
1000
1000
1510
1470
113
109
60-140
3
1,3-Dichlorobenzene
ug/L
ND
1000
1000
1030
1020
103
102
60-140
1
1,3-Dichloropropane
ug/L
ND
1000
1000
1050
1020
105
102
60-140
3
1,4-Dichlorobenzene
ug/L
ND
1000
1000
1060
1010
106
101
60-140
5
2,2-Dichloropropane
ug/L
ND
1000
1000
1180
1170
118
117
60-140
1
2-Chlorotoluene
ug/L
ND
1000
1000
1100
1070
110
107
60-140
3
4-Chlorotoluene
ug/L
ND
1000
1000
1070
1050
107
105
60-140
2
Benzene
ug/L
6550
1000
1000
6560
6650
1
10
60-140
1 M1
Bromobenzene
ug/L
ND
1000
1000
1000
1020
100
102
60-140
1
Bromochloromethane
ug/L
ND
1000
1000
1090
1100
109
110
60-140
1
Bromodichloromethane
ug/L
ND
1000
1000
1150
1100
115
110
60-140
4
Bromoform
ug/L
ND
1000
1000
1150
1110
115
111
60-140
4
Bromomethane
ug/L
ND
1000
1000
1400
1330
140
133
60-140
5
Carbon tetrachloride
ug/L
ND
1000
1000
1210
1190
121
119
60-140
2
Chlorobenzene
ug/L
ND
1000
1000
1070
1050
107
105
60-140
2
Chloroethane
ug/L
ND
1000
1000
1040
1150
104
115
60-140
10
Chloroform
ug/L
ND
1000
1000
1060
1030
106
103
60-140
3
Chloromethane
ug/L
ND
1000
1000
934
923
93
92
60-140
1
cis-1,2-Dichloroethene
ug/L
ND
1000
1000
1090
1070
109
107
60-140
2
cis-1,3-Dichloropropene
ug/L
ND
1000
1000
1170
1130
117
113
60-140
4
Dibromochloromethane
ug/L
ND
1000
1000
1100
1070
110
107
60-140
3
Dibromomethane
ug/L
ND
1000
1000
1030
982
103
98
60-140
5
Dichlorodifluoromethane
ug/L
ND
1000
1000
1160
1180
116
118
60-140
1
Diisopropyl ether
ug/L
104
1000
1000
1170
1170
106
106
60-140
0
Ethylbenzene
ug/L
1550
1000
1000
2480
2460
92
91
60-140
1
Hexachloro-1,3-butadiene
ug/L
ND
1000
1000
1140
1170
114
117
60-140
3
Isopropylbenzene(Cumene)
ug/L
108
1000
1000
1220
1190
111
108
60-140
3
m&p-Xylene
ug/L
4790
2000
2000
6660
6640
93
93
60-140
0
Methyl-tert-butyl ether
ug/L
227
1000
1000
1350
1340
113
111
60-140
1
Methylene Chloride
ug/L
ND
1000
1000
1070
1060
101
100
60-140
1
Results presented on
this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2870468
2870469
MS
MSD
92474518006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
1000
1000
1140
1120
114
112
60-140
2
n-Propylbenzene
ug/L
ND
1000
1000
1160
1150
116
115
60-140
1
Naphthalene
ug/L
722
1000
1000
1850
1870
112
114
60-140
1
o-Xylene
ug/L
1980
1000
1000
2940
2920
96
94
60-140
1
sec-Butylbenzene
ug/L
ND
1000
1000
1120
1090
112
109
60-140
3
Styrene
ug/L
30.5
1000
1000
1140
1110
111
108
60-140
2
tert-Butyl benzene
ug/L
ND
1000
1000
924
924
92
92
60-140
0
Tetrachloroethene
ug/L
ND
1000
1000
1150
1080
115
108
60-140
6
Toluene
ug/L
4520
1000
1000
5020
5000
50
49
60-140
0 M1
trans-1,2-Dichloroethene
ug/L
ND
1000
1000
1150
1120
115
112
60-140
2
trans- 1,3-Dichloropropene
ug/L
ND
1000
1000
1160
1100
116
110
60-140
5
Trichloroethene
ug/L
ND
1000
1000
1110
1050
111
105
60-140
6
Trichlorofluoromethane
ug/L
ND
1000
1000
1040
1060
104
106
60-140
2
Vinyl chloride
ug/L
ND
1000
1000
1150
1120
115
112
60-140
3
1,2-Dichloroethane-d4 (S)
%
102
102
70-130
4-Bromofluorobenzene (S)
%
100
99
70-130
Toluene-d8(S)
%
100
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
QC Batch: 538344 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92473680001
METHOD BLANK: 2870565
Associated Lab Samples: 92473680001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
04/27/20 16:58
1,1,1-Trichloroethane
ug/L
ND
0.50
04/27/20 16:58
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
04/27/20 16:58
1,1,2-Trichloroethane
ug/L
ND
0.50
04/27/20 16:58
1,1-Dichloroethane
ug/L
ND
0.50
04/27/20 16:58
1,1-Dichloroethene
ug/L
ND
0.50
04/27/20 16:58
1,1-Dichloropropene
ug/L
ND
0.50
04/27/20 16:58
1,2,3-Trichlorobenzene
ug/L
ND
2.0
04/27/20 16:58
1,2,3-Trichloropropane
ug/L
ND
0.50
04/27/20 16:58
1,2,4-Trichlorobenzene
ug/L
ND
2.0
04/27/20 16:58
1,2,4-Trimethylbenzene
ug/L
ND
0.50
04/27/20 16:58
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
04/27/20 16:58
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
04/27/20 16:58
1,2-Dichlorobenzene
ug/L
ND
0.50
04/27/20 16:58
1,2-Dichloroethane
ug/L
ND
0.50
04/27/20 16:58
1,2-Dichloropropane
ug/L
ND
0.50
04/27/20 16:58
1,3,5-Trimethylbenzene
ug/L
ND
0.50
04/27/20 16:58
1,3-Dichlorobenzene
ug/L
ND
0.50
04/27/20 16:58
1,3-Dichloropropane
ug/L
ND
0.50
04/27/20 16:58
1,4-Dichlorobenzene
ug/L
ND
0.50
04/27/20 16:58
2,2-Dichloropropane
ug/L
ND
0.50
04/27/20 16:58
2-Chlorotoluene
ug/L
ND
0.50
04/27/20 16:58
4-Chlorotoluene
ug/L
ND
0.50
04/27/20 16:58
Benzene
ug/L
ND
0.50
04/27/20 16:58
Bromobenzene
ug/L
ND
0.50
04/27/20 16:58
Bromochloromethane
ug/L
ND
0.50
04/27/20 16:58
Bromodichloromethane
ug/L
ND
0.50
04/27/20 16:58
Bromoform
ug/L
ND
0.50
04/27/20 16:58
Bromomethane
ug/L
ND
5.0
04/27/20 16:58
Carbon tetrachloride
ug/L
ND
0.50
04/27/20 16:58
Chlorobenzene
ug/L
ND
0.50
04/27/20 16:58
Chloroethane
ug/L
ND
1.0
04/27/20 16:58
Chloroform
ug/L
ND
0.50
04/27/20 16:58
Chloromethane
ug/L
ND
1.0
04/27/20 16:58
cis-1,2-Dichloroethene
ug/L
ND
0.50
04/27/20 16:58
cis-1,3-Dichloropropene
ug/L
ND
0.50
04/27/20 16:58
Dibromochloromethane
ug/L
ND
0.50
04/27/20 16:58
Dibromomethane
ug/L
ND
0.50
04/27/20 16:58
Dichlorodifluoromethane
ug/L
ND
0.50
04/27/20 16:58
Diisopropyl ether
ug/L
ND
0.50
04/27/20 16:58
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
METHOD BLANK: 2870565
Associated Lab Samples: 92473680001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
04/27/20 16:58
Hexachloro-1,3-butadiene
ug/L
ND
2.0
04/27/20 16:58
Isopropylbenzene (Cumene)
ug/L
ND
0.50
04/27/20 16:58
m&p-Xylene
ug/L
ND
1.0
04/27/20 16:58
Methyl-tert-butyl ether
ug/L
ND
0.50
04/27/20 16:58
Methylene Chloride
ug/L
ND
2.0
04/27/20 16:58
n-Butylbenzene
ug/L
ND
0.50
04/27/20 16:58
n-Propylbenzene
ug/L
ND
0.50
04/27/20 16:58
Naphthalene
ug/L
ND
2.0
04/27/20 16:58
o-Xylene
ug/L
ND
0.50
04/27/20 16:58
sec-Butylbenzene
ug/L
ND
0.50
04/27/20 16:58
Styrene
ug/L
ND
0.50
04/27/20 16:58
tert-Butyl benzene
ug/L
ND
0.50
04/27/20 16:58
Tetrachloroethene
ug/L
ND
0.50
04/27/20 16:58
Toluene
ug/L
ND
0.50
04/27/20 16:58
trans-1,2-Dichloroethene
ug/L
ND
0.50
04/27/20 16:58
trans- 1,3-Dichloropropene
ug/L
ND
0.50
04/27/20 16:58
Trichloroethene
ug/L
ND
0.50
04/27/20 16:58
Trichlorofluoromethane
ug/L
ND
1.0
04/27/20 16:58
Vinyl chloride
ug/L
ND
1.0
04/27/20 16:58
1,2-Dichloroethane-d4 (S)
%
100
70-130
04/27/20 16:58
4-Bromofluorobenzene (S)
%
97
70-130
04/27/20 16:58
Toluene-d8 (S)
%
104
70-130
04/27/20 16:58
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2870566
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
54.9
110
60-140
1,1,1-Trichloroethane
ug/L
50
54.8
110
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
51.9
104
60-140
1,1,2-Trichloroethane
ug/L
50
52.4
105
60-140
1,1-Dichloroethane
ug/L
50
53.3
107
60-140
1,1-Dichloroethene
ug/L
50
55.7
111
60-140
1,1-Dichloropropene
ug/L
50
58.8
118
60-140
1,2,3-Trichlorobenzene
ug/L
50
56.9
114
60-140
1,2,3-Trichloropropane
ug/L
50
50.3
101
60-140
1,2,4-Trichlorobenzene
ug/L
50
56.2
112
60-140
1,2,4-Trimethylbenzene
ug/L
50
52.4
105
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
59.3
119
60-140
1,2-Dibromoethane (EDB)
ug/L
50
56.3
113
60-140
1,2-Dichlorobenzene
ug/L
50
54.0
108
60-140
1,2-Dichloroethane
ug/L
50
49.0
98
60-140
1,2-Dichloropropane
ug/L
50
53.1
106
60-140
1,3,5-Trimethylbenzene
ug/L
50
54.2
108
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
LABORATORY CONTROL SAMPLE:
Parameter
2870566
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
54.0
108
60-140
1,3-Dichloropropane
ug/L
50
53.1
106
60-140
1,4-Dichlorobenzene
ug/L
50
52.7
105
60-140
2,2-Dichloropropane
ug/L
50
57.7
115
60-140
2-Chlorotoluene
ug/L
50
54.0
108
60-140
4-Chlorotoluene
ug/L
50
54.1
108
60-140
Benzene
ug/L
50
54.9
110
60-140
Bromobenzene
ug/L
50
50.1
100
60-140
Bromochloromethane
ug/L
50
55.1
110
60-140
Bromodichloromethane
ug/L
50
56.9
114
60-140
Bromoform
ug/L
50
59.8
120
60-140
Bromomethane
ug/L
50
60.0
120
60-140
Carbon tetrachloride
ug/L
50
58.9
118
60-140
Chlorobenzene
ug/L
50
53.5
107
60-140
Chloroethane
ug/L
50
51.4
103
60-140
Chloroform
ug/L
50
53.8
108
60-140
Chloromethane
ug/L
50
45.6
91
60-140
cis-1,2-Dichloroethene
ug/L
50
53.7
107
60-140
cis-1,3-Dichloropropene
ug/L
50
59.6
119
60-140
Dibromochloromethane
ug/L
50
57.6
115
60-140
Dibromomethane
ug/L
50
53.9
108
60-140
Dichlorodifluoromethane
ug/L
50
57.1
114
60-140
Diisopropyl ether
ug/L
50
54.5
109
60-140
Ethylbenzene
ug/L
50
51.1
102
60-140
Hexachloro-1,3-butadiene
ug/L
50
57.1
114
60-140
Isopropylbenzene (Cumene)
ug/L
50
53.2
106
60-140
m&p-Xylene
ug/L
100
105
105
60-140
Methyl-tert-butyl ether
ug/L
50
57.9
116
60-140
Methylene Chloride
ug/L
50
50.7
101
60-140
n-Butylbenzene
ug/L
50
54.0
108
60-140
n-Propylbenzene
ug/L
50
51.5
103
60-140
Naphthalene
ug/L
50
59.0
118
60-140
o-Xylene
ug/L
50
53.4
107
60-140
sec-Butylbenzene
ug/L
50
52.8
106
60-140
Styrene
ug/L
50
56.3
113
60-140
tert-Butyl benzene
ug/L
50
44.7
89
60-140
Tetrachloroethene
ug/L
50
55.6
111
60-140
Toluene
ug/L
50
50.3
101
60-140
trans-1,2-Dichloroethene
ug/L
50
54.9
110
60-140
trans- 1,3-Dichloropropene
ug/L
50
59.4
119
60-140
Trichloroethene
ug/L
50
55.2
110
60-140
Trichlorofluoromethane
ug/L
50
46.9
94
60-140
Vinyl chloride
ug/L
50
54.6
109
60-140
1,2-Dichloroethane-d4 (S)
%
104
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
99
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2870567
2870568
MS
MSD
92474518001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
500
500
524
532
105
106
60-140
2
1,1,1-Trichloroethane
ug/L
ND
500
500
518
505
104
101
60-140
3
1,1,2,2-Tetrachloroethane
ug/L
ND
500
500
497
518
99
104
60-140
4
1,1,2-Trichloroethane
ug/L
ND
500
500
489
490
98
98
60-140
0
1,1-Dichloroethane
ug/L
ND
500
500
498
499
100
100
60-140
0
1,1-Dichloroethene
ug/L
ND
500
500
540
538
108
108
60-140
0
1,1-Dichloropropene
ug/L
ND
500
500
561
557
112
111
60-140
1
1,2,3-Trichlorobenzene
ug/L
ND
500
500
550
459
110
92
60-140
18
1,2,3-Trichloropropane
ug/L
ND
500
500
510
481
102
96
60-140
6
1,2,4-Trichlorobenzene
ug/L
ND
500
500
528
479
106
96
60-140
10
1,2,4-Trimethylbenzene
ug/L
1010
500
500
1460
1400
91
79
60-140
4
1,2-Dibromo-3-chloropropane
ug/L
ND
500
500
510
512
102
102
60-140
0
1,2-Dibromoethane (EDB)
ug/L
128
500
500
678
675
110
109
60-140
0
1,2-Dichlorobenzene
ug/L
ND
500
500
509
495
102
99
60-140
3
1,2-Dichloroethane
ug/L
35.7
500
500
472
472
87
87
60-140
0
1,2-Dichloropropane
ug/L
ND
500
500
521
527
104
105
60-140
1
1,3,5-Trimethylbenzene
ug/L
376
500
500
878
857
100
96
60-140
2
1,3-Dichlorobenzene
ug/L
ND
500
500
505
509
101
102
60-140
1
1,3-Dichloropropane
ug/L
ND
500
500
518
511
104
102
60-140
1
1,4-Dichlorobenzene
ug/L
ND
500
500
509
496
102
99
60-140
2
2,2-Dichloropropane
ug/L
ND
500
500
403
397
81
79
60-140
2
2-Chlorotoluene
ug/L
ND
500
500
532
520
106
104
60-140
2
4-Chlorotoluene
ug/L
ND
500
500
512
502
102
100
60-140
2
Benzene
ug/L
1930
500
500
2460
2420
106
98
60-140
2
Bromobenzene
ug/L
ND
500
500
495
481
99
96
60-140
3
Bromochloromethane
ug/L
ND
500
500
524
512
105
102
60-140
2
Bromodichloromethane
ug/L
ND
500
500
546
522
109
104
60-140
4
Bromoform
ug/L
ND
500
500
525
506
105
101
60-140
4
Bromomethane
ug/L
ND
500
500
682
701
136
140
60-140
3
Carbon tetrachloride
ug/L
ND
500
500
553
556
111
111
60-140
0
Chlorobenzene
ug/L
ND
500
500
533
522
107
104
60-140
2
Chloroethane
ug/L
ND
500
500
503
531
101
106
60-140
6
Chloroform
ug/L
ND
500
500
500
514
100
103
60-140
3
Chloromethane
ug/L
ND
500
500
426
430
85
86
60-140
1
cis-1,2-Dichloroethene
ug/L
ND
500
500
509
505
102
101
60-140
1
cis-1,3-Dichloropropene
ug/L
ND
500
500
530
517
106
103
60-140
3
Dibromochloromethane
ug/L
ND
500
500
536
523
107
105
60-140
2
Dibromomethane
ug/L
ND
500
500
498
493
100
99
60-140
1
Dichlorodifluoromethane
ug/L
ND
500
500
509
506
102
101
60-140
1
Diisopropyl ether
ug/L
31.4
500
500
525
523
99
98
60-140
0
Ethylbenzene
ug/L
966
500
500
1440
1420
94
91
60-140
1
Hexachloro-1,3-butadiene
ug/L
ND
500
500
563
504
113
101
60-140
11
Isopropylbenzene(Cumene)
ug/L
97.8
500
500
622
625
105
105
60-140
0
m&p-Xylene
ug/L
3420
1000
1000
4350
4290
93
87
60-140
1
Methyl-tert-butyl ether
ug/L
36.9
500
500
546
539
102
100
60-140
1
Methylene Chloride
ug/L
ND
500
500
481
487
96
97
60-140
1
Results presented on
this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Little Buck 2
Pace Project No.: 92473680
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2870567
2870568
MS
MSD
92474518001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
500
500
547
543
109
109
60-140
1
n-Propylbenzene
ug/L
ND
500
500
605
590
121
118
60-140
2
Naphthalene
ug/L
627
500
500
1110
946
96
64
60-140
15
o-Xylene
ug/L
1690
500
500
2150
2170
92
97
60-140
1
sec-Butylbenzene
ug/L
ND
500
500
537
521
107
104
60-140
3
Styrene
ug/L
ND
500
500
561
557
112
111
60-140
1
tert-Butyl benzene
ug/L
ND
500
500
442
446
88
89
60-140
1
Tetrachloroethene
ug/L
ND
500
500
521
524
104
105
60-140
1
Toluene
ug/L
3320
500
500
3700
3630
77
62
60-140
2
trans-1,2-Dichloroethene
ug/L
ND
500
500
530
517
106
103
60-140
2
trans- 1,3-Dichloropropene
ug/L
ND
500
500
515
518
103
104
60-140
1
Trichloroethene
ug/L
ND
500
500
532
536
106
107
60-140
1
Trichlorofluoromethane
ug/L
ND
500
500
477
466
95
93
60-140
2
Vinyl chloride
ug/L
ND
500
500
547
533
109
107
60-140
3
1,2-Dichloroethane-d4 (S)
%
99
98
70-130
4-Bromofluorobenzene (S)
%
98
99
70-130
Toluene-d8(S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Little Buck 2
Pace Project No.: 92473680
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/28/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Little Buck 2
Pace Project No.: 92473680
Lab ID
Sample ID
QC
Batch Method
QC Batch
92473680001
MW-1
SM
6200B
538344
92473680002
MW-2
SM
6200B
537925
92473680003
MW-3
SM
6200B
537925
92473680004
MW-4
SM
6200B
537925
92473680005
MW-5
SM
6200B
537925
92473680006
VMW-1
SM
6200E
537925
Date: 04/28/2020 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 27 of 29

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age 28 of 29

ACeAaalydcal
Document No.:
f-CAR-CS-033-Rev.06
Page 1 of 2
Issuing Authority:
Pace Carolinas Qualltv Office
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Enceptlons: VOA, Calif'orm, TOC, Oil and Grease, #SRO/9015 (waterf DOC, UHg
"Sottom half of box is to list number of bottle
projeed ..
WO#:92473680
PM: MWB Due Date: 04/28/20
CLIENT: 92-SE CEO
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pH Adjustment Log for preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date Preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot k
ivuce: vvnenever were Is a mscrepancy an'ecting Mftn Carolina Compliance samples, a copy or tors rorm Will be Sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect contalner3.
Page 29 of 29

Beverly, Trudy
From: Beverly, Trudy
Sent: Wednesday, July 29, 2020 8:44 AM
To: Gunny Kelly
Subject: RE: [External] Little Buck 2
For me, you can just email the report, no cd or uploading to Filezilla needed. I will email you back stating that I
received the report. I would suggest you check with any other UST project managers to see if email only
submission is acceptable to them.
Received.
Have a great day,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
^�' 1-1' '� '-' � k:UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenr. -gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-manaaement/ust
Branch's Above Ground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hLtps://deg.nc.gov/about/divisions/waste-manaaement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.eov/nedeci/Waste%2OManaeement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Gunny Kelly [mailto:[e-mail]]
Sent: Tuesday, July 28, 2020 6:02 PM
To: Beverly, Trudy <[e-mail]>
Subject: Re: [External] Little Buck 2
off • External email. Do not click links or open attachments unless you verify. Send all s 91W ent to
[e-mail]
Thanks, I missed this.
The report is attached, a CD should have been included with the paper report.
It looks as if DENR doesn't really want the report by email; I assume you're helping me out on this
one.
Few questions:
-) DENR prefer the report be submitted on the FTP site?

-) if so, how access the site - need to get access from Ron?
-) reads as if I may not get access, mentions still sending CDs; if so then mail CD only, no paper
copy?
Sorry to bother you with this - please send name if someone is designated to help with this.
Richard Kelly
On Monday, July 27, 2020, 6:58:05 AM EDT, Beverly, Trudy <trudy.beverly(@ncdenr.gov> wrote:
Good Morning Richard,
The UST Section transitioned to electronic report submittals at the end of March. See the "What's New"
section of the UST website for details. You can email me a pdf copy of the report.
Thanks,
Trudy
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Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenr. og_v
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: htips:Hdeg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
htWs:Hdeq.nc.,gov/about/divisions/waste-management/waste-management-rules-data/waste-mana eg ment ig s=maps
File Review Procedures:
hfps:Hdeq.nc. gov/about/divisions/waste-managementlustlfile-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https:Hdeq.nc. gov/about/divisions/waste-manaaement/laserfiche

Document Submittal & UST File Names for Laserfiche Policies:
https://files.ne.2oy/ncdeq/Waste%20Manallement/D W MIUSTIW hatsNew/Fin al-Electronic-Document-Submittal-Poliev.pdf
https:llfiles.nc.�,ovincdeq/Waste%20ManagementIDWM[USTICorrective%2OAction[UST%2Ofile%20names%20for%2OLaserfiche.doex
From: Gunny Kelly [mailto:sgsrykCcD-yahoo.com]
Sent: Saturday, July 25, 2020 12:02 AM
To: Beverly, Trudy <trudy.beverlyCa)ncdenr.gov>
Subject: [External] Little Buck 2
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to report.spam(@nc.gov
Little Buck 2
27741
Ms. Beverly:
Checking on the monitoring report issued 5-12-20. 1 have not found an approval date for the report, and it is required for
trust fund reimbursement. The report was mailed the 12th but you may not have received, if not I'll send another. I know
the virus work schedule has disrupted report review. Appreciate any information.
Thanks, hope all is well.
Richard Kelly