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HomeMy WebLinkAboutWheat Fields Development Brownfields Assessment Report 11.04.19WithersRavenel 4400 . Our People. Your Success. BROWN FI ELDS ASSESSMENT REPORT Wheat Fields Development BF Project No. 22051-18-092 Sassom, LLC ±5.32-Acre Site 1009 Forestville Road Wake Forest , Wake County, North Carolina WR Project No. 02180643.01 Prepared for: North Carolina Department of Environmental Quality Division of Waste Management Brownfields Section 1646 Mail Service Center Raleigh, NC 27699 Prepared by: WithersRavenel 115 MacKenan Drive Cary, North Carolina 27511 North Carolina Firm License No. C-0832 November 4, 2019 .. ,. Our People. Your Success. November 4, 2019 North Carolina Department of Environmental Quality Division of Waste Management - Brownfields Section 1646 Mail Service Center Raleigh, NC 27699 Attn: Mr. Kelly Johnson Brownfields Section Project Manager RE: Brownfields Assessment Report Wheat Fields Development: BF Project No. 22051-18-092 Sassom, LLC 1009 Forestville Road Wake Forest, Wake County, North Carolina WR Project No. 02180643.01 Mr. Johnson: On behalf of Sassom, LLC WithersRavenel, Inc. (WR) is pleased to submit this Brownfields Assessment Report, which describes the procedures used to determine the presence or absence of contaminants in surface soils, groundwater and soil vapor beneath the subject property. The report describes the collection of soil, groundwater, and soil vapor samples near onsite structures that are scheduled to be built in accordance with a proposed North Carolina Department of Environmental Quality (NCDEQ) Brownfields Agreement. Should you have any questions regarding the contents of the enclosed workplan, please do not hesitate to contact us. Sincerely, WithersRavenel Laura Robertson Elliott, P.G. Project Manager Brian J. Bellis, P.G. Senior Hydrogeologist 115 MacKenan Drive I Cary, NC 27511 t: 919.469.3340 1 f: 919.467.6008 1 www.withersravenel.com I License No. C-0832 Asheville I Cary I Greensboro I Pittsboro I Raleigh I Wilmington WithersRavenel 4400 . Our People. Your Success. Table of Contents 1. Background and Purpose................................................................................................ ...1 2. Soil Sampling and Analytical Results................................................................................2 3. Groundwater Sampling and Analytical Results.............................................................. 3 4. Soil Vapor Sampling and Analytical Results...................................................................4 5. Conclusions .............................................. _._............................ 5 Figure 1 General Location Map Figure 2 Site Map Figure 3 Commercial Plan with Sampling Locations Map Figure 4 Soil Analytical Results Map (January 2019) Figure 5 Groundwater Hydraulic Gradient Map (January 2019) Figure 6 Groundwater Analytical Results Map (January 2019) Figure 7 Soil Vapor Probe Analytical Results Map (October 2019) Table 1 Summary of Soil Analytical Results Table 2 Monitoring Well Construction Information Table 3 Summary of Groundwater Analytical Results Table 4 Summary of Soil Vapor Probe Analytical Results Appendix A Brownfields Receptor Survey Appendix B Boring Logs, Monitoring Well Construction Logs, and Soil Vapor Probe Construction Logs Appendix C Photo Log, Groundwater Sampling Forms, Vapor Probe Sampling Forms, Field Notes Appendix D Laboratory Reports and Chains of Custody Appendix E EPA Risk Calculator Input and Output Forms 40 ..Our People. Your Success. 1. BACKGROUND AND PURPOSE WithersRavenel (WR) performed a Receptor Survey for the ±5.32-acre site located at 1009 Forestville Road, Wake Forest, Wake County, North Carolina (Figure 1). According to Wake County GIS records, the subject property consists of the following parcel: 1749680479 1 Sassom, LLC 1 1009 Forestville Road 1 ±5.32 Historically, a farm operated at the property and made use of two unregistered commercial underground storage tanks (USTs), one containing diesel and one containing gasoline, that were removed in 2005. After removal of the USTs, soil samples revealed concentrations of petroleum -related contaminants in excess of NCDEQ action levels and groundwater samples revealed concentrations of petroleum -related contaminants exceeding the North Carolina 15A NCAC 2L .0202 Groundwater Quality Standards at monitoring wells MW- 1 and MW-2. The onsite water supply well was sampled in August 2015, and the results of the sampling event showed no volatile organic compounds (VOCs) at concentrations above laboratory reporting limits in water from the well on that date. One vacant, single-family, brick, ranch house is present on the property, which is 2,326 sq. feet in area and was built in 1957, according to Wake County iMAPS website. The former storage building to its southeast is no longer present. One of the monitoring wells installed in one of the former UST basins has been destroyed, and the water supply well is in the far southeast corner of the property. The water supply well is currently not in use, but is considered active. The property is surrounded by new commercial and residential developments, as well as Heritage High School. Sassom, LLC received a Letter of Eligibility to enter the Brownfields Program on August 21, 2018. After the meeting held on October 9, 2018 with the representatives of Sassom, WR and NCDEQ Brownfields Program, several issues that require additional investigation per the Program were identified. These issues involve areas where additional contamination may be present. Those areas are described below: 1) Groundwater upgradient and downgradient of the known groundwater contamination in the source area of the former USTs; 2) Soils surrounding or beneath the former two USTs which were not over -excavated at the time of UST removal; 3) Soil vapor in areas under proposed building footprints in the vicinity of the former USTs. Specific areas of the property which will be developed into parking areas or building (retail space and restaurants) and therefore will be investigated include the following: A 3,000-gallon diesel fuel underground storage tank (UST) was removed from the site in March 2005. No over -excavation was conducted. The final excavation measured approximately 15.5 feet x 22 feet x 12.5 feet deep, according to the UST Closure Report, dated July 8, 2005. Product lines and dispensers were located immediately above the UST and were removed during the excavation. The dimensions of the diesel UST were 8 feet x 14 feet. Upon removal, the UST was observed to be coated and in good condition. One monitoring well (MW-2) was installed on the north side of the tank pit in July 2007, as part of the Limited Site Assessment conducted per NCDEQ UST section requirements. Wheat Fields Development: BF Project No. 22051-18-092 WR No. 02180643.01 Brownfields Assessment Report November 2019 1 40 1. Our People. Your Success. A 2,000-gallon gasoline fuel UST was removed from the site in March 2005. No over -excavation was conducted. The final excavation measured approximately 11 feet x 23 feet x 10.5 feet deep, according to the UST Closure Report, dated July 8, 2005. The UST dimensions were 5 feet x 17 feet. Upon removal, minor holes were noted along the bottom of the UST and it displayed rusting and pitting. One monitoring well (MW-1) was installed within the tank pit in July 2007 as part of the Limited Site Assessment. In January 2019, WR conducted soil sampling in the locations of the two former USTs on site to delineate the extent of petroleum in the surrounding soils, and WR installed three new monitoring wells. Groundwater was collected from the existing monitoring well MW-1, along with samples from the three new onsite monitoring wells. The results of the soil and groundwater analyses have been submitted to the Brownfields Program. Monitoring well MW-2 had been destroyed, and was properly abandoned by a licensed driller. A receptor survey was conducted in January 2019, the results of which are included in Figure 2 and Appendix A. Figure 2 includes a site map of the subject property with nearby surface waters and three known water supply wells in the vicinity. In October 2019, WR conducted soil vapor sampling at nine locations that will be under proposed building footprints, according to the current site commercial plan. Figure 3 includes the commercial plan with all sampling locations mapped. WR has prepared this report to document the sample locations, sample acquisition details, and sample analysis results from the January 2019 soil and groundwater investigation as well as the October 2019 vapor intrusion investigation. This report includes soil, groundwater and soil vapor sampling data and laboratory analytical reports for the analyses described in the Brownfields Assessment Workplan dated January 7, 2019 for soil and groundwater sampling, and the Brownfields Assessment Workplan dated October 2, 2019 for soil vapor sampling (workplans). This report also discusses the comparisons of the analytical results to the appropriate NCDEQ standards, screening levels and preliminary soil remediation goals, and the potential implications with regard to the need for further action. 2. SOIL SAMPLING AND ANALYTICAL RES ULTS On January 9, 2019, WR mobilized to the subject property with Quantex, Inc. (sub -contractor driller) to advance soil borings around the former UST areas to determine the extent of petroleum -impacted soils at the locations illustrated on Figure 3. The known depth of grade at the site is not yet known for the development of the property. Therefore, WR screened and collected soil samples at approximately 5 feet below ground surface (bgs) from eight locations; four locations surrounding each tank pit. The samples were labeled as T1(UST Tank 1) SW1-SW4 (Sidewalls 1-4) and T2 (UST Tank 2) SW1-SW4 and their locations are shown on Figure 3. Off -set borings were installed to define the lateral extent of soil contamination; these included T1SW2-2, T1SW3-1 through T1SW3-5, and T1SW4-2. These locations are where previous investigation had not been conducted, as the tanks were removed but no over -excavation was conducted, and which may be disturbed by planned future redevelopment activities. Historical investigation groundwater results indicate that contaminants may be present at these locations. Boring logs are included in Appendix B. WR also collected soil samples at the locations where monitoring wells were installed. Soils were screened with a PID and collected at a depth of 5 feet bgs, to compare to results from the two tank pit areas, T1 and T2. The samples were collected using a new, dedicated macrocore liner in accordance with the procedures provided in the January 7, 2019 workplan. Wheat Fields Development: BF Project No. 22051-18-092 WR No. 02180643.01 Brownfields Assessment Report November 2019 2 40 1. Our People. Your Success. The samples were screened with a Photoionization Detector (PID) and collected using a new, dedicated macrocore liner and placed in laboratory prepared containers. The samples were submitted to a NC certified laboratory under standard Chain -of -Custody procedures for analysis of the following: • Volatile organic compounds (VOCs) by EPA Method 8260B • Semi-VOCs (SVOCs) by EPA Method 8270D, and • RCRA Metals by EPA Methods 6010 and 7470. Analytical results indicated that there were no detected petroleum -related compounds in the soil surrounding former Tank 2, but some petroleum -related compounds were detected in the soils surrounding former Tank 1. The horizontal extent of petroleum -contaminated soil is generally defined as extending to the east and south of the former Tank 1 location. Table 1 and Figure 4 show the analytical results of the soil sampling at the extent of the petroleum footprint. Samples were collected from the depth of each boring with the highest VOC reading on the PID during sampling activities. Field notes are included in Appendix C, and laboratory analytical reports are included in Appendix D. 3. GROUNDWATER SAMPLING AND ANALYTICAL RESULTS On January 8, 2019, WR installed three additional groundwater monitoring wells on the site (MW-3, MW- 4, and MW-5) in the locations indicated in Figure 3. The locations and relative elevations of the monitoring wells were surveyed in order to determine groundwater elevations and flow direction on site. The monitoring wells were installed at these locations to determine whether petroleum -contaminated groundwater on site is migrating to the south and east, which is the inferred direction of groundwater flow from the source area in the vicinity of monitoring well MW-1, based on topography and surficial drainage patterns at the site. Monitoring well MW-5 was intended to be indicative of background conditions. While onsite, WR discovered what appeared to be the destroyed remains of former monitoring well MW-2. On January 9, 2019, WR properly abandoned MW-2 according to 15A NCAC 02C rules. Each boring was logged in the field. Boring log information includes but is not limited to; detailed soil description and lithology at depths, depth of groundwater observed during drilling, notable reaction of drill rig during advancement, depth of competent rock encountered, detailed notes/remarks, and a well construction diagram. Boring log and monitoring well construction information is available in Appendix B. After the Brownfields Program approved the three proposed locations, the monitoring wells were installed by a NC Certified Well Contractor. A permanent 2-inch diameter groundwater monitoring well was installed in each boring. Hollow stem augers were utilized to advance the borings. Well installation was done in compliance with the most current 15A NCAC 2C well construction standards, and the wells are equipped with locking aboveground protective covers. WR determined the relative top of casing elevations for the one existing monitoring well and three newly - installed monitoring wells so that the direction of groundwater flow from the source area could be evaluated. Well construction details including installation date, top of casing elevations, ground surface elevations, total well depths, well screen intervals, depths to groundwater, and groundwater elevations are summarized in Table 2. WR used an electronic water level indicator to record static water level measurements in the wells to determine the static groundwater elevation in the well. Figure 5 shows groundwater elevation contours and flow directions as well as land surface topography, surface water features, and monitoring well locations. The groundwater elevation data collected in January 2019 imply that surficial groundwater flow is toward the northwest across the site; not to the southeast as was previously inferred from topography and drainage features shown on Figures 1 and 2. Wheat Fields Development: BF Project No. 22051-18-092 WR No. 02180643.01 Brownfields Assessment Report November 2019 3 40 1. Our People. Your Success. On January 10, 2019, WR collected groundwater samples from existing monitoring well MW-1 and the three newly installed monitoring wells (MW-3, MW-4 and MW-5). After the static water level was recorded, the wells were purged and water quality parameters including pH, temperature, specific conductance and turbidity were monitored until stabile in accordance with criteria described in the January 7, 2019 workplan. Groundwater samples were then obtained by the low flow method described in that workplan. Copies of the groundwater sampling forms that document the purging and sampling activities are included in Appendix C. The samples were submitted to a NC certified laboratory under standard Chain -of -Custody procedures for analysis of the following: VOCs by EPA Test Method 8260B; and SVOCs by EPA Test Method 8270D. Groundwater sample results were compared to the North Carolina Groundwater Quality Standards as listed in 15A NCAC 2L .0202 (2L Standards). Analytical results indicated that petroleum compounds are present in the groundwater at the former Tank 1 location, which includes monitoring well MW-1. Several petroleum -related compounds were identified in the groundwater sample from monitoring well MW-1 at concentrations exceeding their respective 2L Standards and above the Non -Residential VI GWSLs. Petroleum -related compounds were not detected in the groundwater samples from the remaining monitoring wells MW-3, MW-4, and MW-5. The analytical results are summarized in Table 3, and on Figure 6, and the full laboratory report is provided in Appendix D. 4. TICAL RESULTS On October 9, 2019 and under the direction of WR, SAEDACCO (sub -contractor driller) advanced nine soil borings on the Wheat Fields Development property for the purpose of constructing temporary soil vapor probes at locations SV-1 through SV-9 (see Figure 3). Each soil vapor probe boring was advanced to a depth of five feet below the ground surface. The borings were advanced using Direct Push Technology, and new Teflon tubing, fittings and sealants were used in the construction of each probe. The probes were installed in accordance with the procedures described in the October 2, 2019 workplan. Each soil gas probe was capped following installation, and allowed to equilibrate for at least 2 hours before sampling. Soil vapor probe construction records are provided in Appendix B. On October 10, 2019, the nine probes were leak tested using the helium shroud method for quality control purposes, and then sampled using one -liter summa canisters in accordance with the procedures provided in the October 2, 2019 workplan. One duplicate sample was collected. Photographs of each soil vapor probe are included in Appendix C. Helium concentration measurements at the start and end of each leak check, along with the helium concentration for each of the three purge volumes are recorded on the field log book pages for October 10, 2019 contained in Appendix C. The summa canisters were not be allowed to reach 0" Hg vacuum and they were closed when the remaining vacuum pressure within the canister was approximately 5" Hg. The field log pages containing the initial and final vacuums are included in Appendix C. The laboratory also recorded the remaining vacuum pressure within the summa canisters upon receipt (see laboratory reports in Appendix D). The soil vapor samples were submitted to a NC Certified Laboratory for analysis of VOCs by EPA Method TO-15. The purpose of collecting and testing the soil vapor samples was to determine if past leaking USTs have adversely affected soil vapor at locations beneath the proposed building foundations. Concentrations of individual VOCs that were detected within the soil vapor samples obtained from the site were compared to the most current version of the NCDEQ Division of Waste Management (DWM) �RMftields Development: BF Project No. 22051-18-092 WR No. 02180643.01 Brownfields Assessment Report November 2019 4 40 1. Our People. Your Success. Hazardous Sites Branch Vapor Intrusion Screening Levels. Detectable concentrations of petroleum -related compounds were identified in all of the soil vapor samples and the duplicate sample collected on October 10, 2019. However, none of the reported concentrations exceeded the February 2018 NCDEQ DWM Exterior Soil Gas Screening Levels (SGSLs) for residential or non-residential settings. Comparison of the VOC concentrations identified within the soil vapor samples to the SGSLs is provided in Table 4, and Figure 7 shows the analytical results for each soil vapor sampling location. 5. CONCLUSIONS WR prepared a risk calculation using the most recent NCDEQ risk calculator, and using the highest concentration for each detected compound among all samples of soil, groundwater, and soil vapor to generate a conservative risk value for the entire site. Appendix E includes the input data used and resulting risk calculations. These are summarized below as shown on Output Form 1A. For the Primary Calculators, the soil combined pathways did indicate an unacceptable risk to residents, however, the pathways did not indicate unacceptable risk to non-residential workers or construction workers. The carcinogenic risk and hazard indices for the groundwater combined pathways were exceeded for potential residents and non-residential workers. For the Vapor Intrusion Calculators, utilizing the highest concentrations of compounds detected within the soil, groundwater, and soil vapor samples collected, the carcinogenic risk and hazard indices determined for the groundwater -to -indoor -air pathway were exceeded for potential residents and non- residential workers. The calculated carcinogenic risk and hazard indices for the soil -gas -to -indoor -air pathway risk did not indicate unacceptable risk for potential residents or non-residential workers. The Contaminant Migration Calculators did determine that the source soil and source groundwater exceeded target POE concentrations for the Protection of Groundwater Use Pathway. Wheat Fields Development: BF Project No. 22051-18-092 WR No. 02180643.01 Brownfields Assessment Report November 2019 5 Figures OOF I/ *011d IrA - i � 0/ 00 ( S�BI-ECT SI r FOX 0 250 500 1000 ` y 1 inch = 500 ft. 1 / WHEAT FIELDS DEVELOPMENT DRAWN BY : SCALE: FIGURE NO.: 1009 FORESTVILLE ROAD BC 1"=500' bl i t h e rs Ra ve n e l 1 1 / WAKE FOREST, WAKE COUNTY, NC Engineers I Planners I Surveyors �]/� APPROVED BY: DATE: PROJECT NO.: 115 MaCKenao Drive I Cary, NC 275111 t: 919.469.33401 license #:C-0832I GENERAL LOCATION MAP LRE 10/21/19 02180643.01 K.\le�l.-e6�Mlee6�i01-Nrd ivies ewxeeerer\Eevi %CAD\rYrrer I'l— - - ----' IMIM119 e- WIG - F 011 rYM *- � . w do i t 4' l' r � � I 40 to r • r i � Lu i L Vie �v do + 4 4w ,0 �O ! r \ WS -2 WSW-3 ® ®SW-4 LEGEND GROUNDWATER MONITORING WELL \ ,410 ® WATER SUPPLY WELL NOTES. 1.) 2017 AERIAL OBTAINED FROM WAKE COUNTY GIS DEFT. GRAPHIC SCALE ` " + . 0 150 300 600 49 - k 1 inch = 300 ft. - o o z � v u 0 a O N R o� O Cl) p N 04 4 LLi II a o � S m m a U ° w 0 o a � LINKS Rpm _ a a uui in .am. d!� H Z Z :- W pow W op 1 W > w a-� o-� J OLL Lu rt W o 0 w i Y W � C o I > o lIrk i sQ)u, N u v ? i � v FOUNDATION DR PROPOSED IIa DEDICATION I I 14.50' WIDENING j o FT PAVEMENT I AND 30" CURB & GUTTER) I III I l I Y I I PROPOSED 5' SIW ALONG FORESTVILLE ROAD (BY OTHERS) I s j II I h � U I Z a I U � I I I a � h I m I i I � LEGEND I GROUNDWATER MONITORING WELL y Q SOIL BORING SOIL VAPOR PROBE ® WATER SUPPLY WELL NOTES: I 1.) 2017 AERIAL OBTAINED FROM WAKE COUNTY GIS DEPT. El 2.) Former UST pits are approximated on map. 3.) Proposed Site Plan by Red Line Engineering, Dated August 5, 2019. BEIP 65 PUBLIC S ROGERS B-5 / M W- 5 BRANCH EXT. 20'STREETSCAPE BUFFER ' PROPOSED ENTRYWAY AND MONUMENT SIGN I / (SIGNAGE TO BE APPROVED SEPARATELY) _ FLAGPOLE LOCATION - IPROPOSED ( I I R15.0' 75 ( .80' R9.5' R4.0' R15.0' I 26.00' 1 R6.0' R6.0' o ( R15.0' d' ( R15.0' _619ONC'.SID WALK I R6.0' PROPOSED ' I F'--' 26.0' OUTDOOR AMENITY SPACE ♦ I I I 14 O 9 O 9FORMER FUEL I TANK LOCATION � I PROFO w BUILDI 8,450 5.0 f Lu • �a 18.5' ♦~26.0'�1 18.5' ,4 ^ •• ,•r 1 26.0' 7. w N I 1 11 9.0' ER FUEL 1 I I T TANK LOCATIO � t I I w PROP OUT AM CE ' I R3.5' R4.0' I 'Sll A' I e ` I R15ff R14.5' C HC 1 - ` R5.0' EIP 224 4 A f I r 4027,,. / EIP 0' I CONTROL / 10'X70' SIGHT CORNER DISTANCE I N(y):798,697.97' TRANGLES (TYP) Q E(x):2,146,334.37' 52.0' ` SITE PLAN INFORMATION: 6 C ONC.SIDEWALK. 2.31' 1. NAME: i p♦, 2. STREETADDRESS: 27.0' B-BI`. R15.0' O R15.0' V 1 sv-1 • R6.0' L 3.0' 490,1_40kw U. R4.5' R4.5' lJ 1- 9.0' R4.5' R15.0' PROPOSED 2 BUILDING #1 25,200 SF (70'X360') I \ 3. P.I.N.: � 4. LAND USE (EXISTING/PROPOSED): to 5. TOTAL NUMBER OF LOTS: w 6. LANDAREAS r� AREA OF PARCEL A: AREA OF PARCEL B: R/W TO BE DEDICATED: RESIDUAL AREA OF PARCEL A: RESIDUAL AREA OF PARCEL B: � 7. DISTURBED AREA: \ B. CURRENTZONING: 9. EXISTING BUILDING AREAS: LL10. LL PROPOSED ADDITIONAL SQUARE FOOTAGE: al b N ` 11. PROPOSED BUILDING LOT COVERAGE: I ` � 12. MAXIMUM BUILDING HEIGHT: 13. PROPOSED BUILDING HEIGHT: N/F STROUD- WAKE FOREST LP 14. BUILDING SETBACKS: D.B. 16902, PAGE 1059 B.M. 1989, PAGE 690 CCPIN# 1749.02-67-9852 w 15. INSIDE CITY LIMITS: rn - 16. INSIDE FLOOD HAZARD BOUNDARY: 17. PARKING SUMMARY: GENERAL COMMERCIAL RESTAURANT MAXIMUM SPACES ALLOWED TOTAL SPACES PROVIDED 18. IMPERVIOUS SURFACE AREA: EXISTING: PROPOSED: TOTAL: 19. INSIDE PROTECTED WATERSHED AREA 20. DEDICATED STREET RIGHT OF WAY: 21. OWNER: •• ASV-4 Y Y OUTDOOR Q AMENITY SPACE PROPOSED Cam\ /� PROPOSED J NIP / I I BUILDING#3 J V BUILDING#2 5,250 SF (70'X75') I10,500 SF (70'X150') o BOV ( i / NIP •..... ..6,. to ALK ss } .N , A - - - - - - - - - GRAPHIC SCALE \I s9°5906" W NIP 0 30 60 I I 120 STORM ER NOTE: ALL SITE ❑ SHALL BE TREATED AND DISCH / O UNDERGROUND STORMWATER / (TO BE DETERMINED AT CONST 1 inch = 60 ft. DRIV 0 O 00- d Z LL CM M k ° `100 3 F 00 U Iq P o N R O a 0 O O M N G II LLi oS O a vl m y S Z (n 0 J < o 19 _ O 231 }1 104 41, U 196 a 98, i J 226Col �V = L ♦ (CE E EXI G M PR G V) PR 11 U 219 3S 25 Z FR( W SID C U D L Z RE a YE No W` O= 0 EF / u U W Y (1 0 F Q LU 811 N LU (IS = F 100 J LL LU MIN W 01 O LL 184 O LU 276 Y 187 W 1 14,2 28 143 A- ro 12. W RO O SA 101 i WA \ ) T/ � C rq �..� rq 1 L� v _ ao LLI G GE ,, 'ST CTI I I \ I II I I II BEIP it I P I II i w. � MH / I � 65' BLIC R/W /y / ' - I ROGERS SIB 5 M W= 5 FOUNDATION D R PU � BRANCH - - -.00 nalyfical Method EPA-8270D 8260E -Volatile Oraanic Compounds EPA-7471A Sample z z z j w w w Depth w z N z x z O w w Sample (Feet Below ate z w "70. w w z w J w z x x F- Ground ColDlected w w m N 9 a z � w I-u ruu � Surface) w t- Z w Z C W Z m > rj o o. o o K w a O K O Z $ w Z w 2 2 16 K F < o m u� . m K °J m aJo O a < F D_ O z w K K w a w I-u m Y J 2 9 x o u 5 °N a J N J` rc rc a W LL z a < o' m z o u w d z z 0 °� X m 0 w 86-73-7 91-203 85-01-8 67-64-1 71-43-2 10451$ 13538$ 96-12$ 10633d 100d1d 98-82$ 99$7E 78333 91-20J 10365-1 100d2S 108$8-3 95636 10867$ 1330-20-7 744039-3 744047-3 743M2-1 7439976 SB3 16-17 1/8/2019 <0.00772 <0.0101 <0.00598 <0.0155 <0.000453 <0.00435 <0.00286 <0.00577 <0.000594 <0.000600 <0.000977 <0.00264 <0.0142 <0.00353 <0.00134 <0.00309 <0.00142 <0.00131 <0.00122 <0.00541 191 266 10.6 <0.00317 S84 15-16 1/8/2019 <0.00775 <0.0101 <0.00600 <0.0156 <0.000454 <0.00436 <0.00287 <0.00579 <0.000597 <0.000602 <0.000981 <0.00265 <0.0142 <0.00354 <0.00134 <0.00310 <0.00142 <0.00132 <0.00123 <0.00543 76.4 6.36 11.9 0.0241 SB-5 16-17 1/8/2019 <0.00737 I <0.00960 <0.00570 0.0293 B <0.000467 <0.00448 <0.00295 <0.00595 <0.000612 <0.000618 <0.00101 <0.00272 <0.0146 <0.00364 <0.00137 <0.00319 <0.00146 <0.00135 <0.00126 <0.00557 76.8 13.9 4.43 <0.00302 T1SW1 2-3 1/9/2019 <0.00788 <0.0103 <0.00610 <0.0158 <0.000462 <0.00443 <0.00292 <0.00589 <0.000606 0.00515 <0.000997 <0.00269 <0.0144 0.0247 0.0107 <0.00315 <0.00144 0.103 0.0276 0.0479 78.4 9.14 4.36 0.128 TISW24 14-15 1/9/2019 0.0627 12.1 0.0711 <0.0158 <0.000462 10.2 1.49 <0.00589 <0.000606 4.9 1.75 1.15 0.228 144 6.97 <0.00315 0.434 58.2 15.5 37.9 167 9.97 17.1 <0.00323 TlSW34 20-21 1/9/2019 0.0722 6.11 0.0422 <0.0144 <0.000422 3.55 0.619 <0.00538 <0.000554 1.55 0.583 0.287 0.0449 4.76 217 <0.00288 0.011 24.4 6.62 10.4 104 274 14.8 <0.00295 TlSW44 8-9 1/9/2019 0.16 16.3 0.0714 <0.127 0.358 9.17 4.71 0.338 0.218 33.2 5.37 2.51 4.75 143 16.8 0.18 50.7 135 41 252 55.1 5.17 25.7 <0.00324 T2SW1 16-17 1/9/2019 <0.00747 <0.00974 <0.00578 <0.0150 <0.000438 <0.00421 <0.00277 <0.00559 <0.000575 <0.000581 <0.000946 <0.00255 <0.0137 <0.00342 <0.00129 <0.00299 <0.00137 <0.00127 <0.00118 <0.00524 85.5 1.7 2.68 <0.00307 T2SW2 12-13 1/9/2019 <0.00841 <0.0110 <0.00651 <0.0169 <0.000494 <0.00474 <0.00312 <0.00629 <0.000648 <0.000654 <0.00106 <0.00287 <0.0154 <0.00385 <0.00146 <0.00337 <0.00154 <0.00143 <0.00133 <0.00590 79.2 3.7 14.8 <0.00345 T2SW3 18-19 1/9/2019 <0.00729 <0.00951 <0.00565 <0.0152 <0.000445 <0.00427 <0.00281 <0.00567 <0.000584 <0.000589 <0.000960 <0.00259 <0.0139 <0.00346 <0.00132 <0.00304 <0.00139 <0.00129 <0.00120 <0.00531 72.5 1.58 6.59 <0.00299 T2SW4 16-17 1/9/2019 <0.00787 <0.0103 <0.00610 <0.0158 <0.000462 <0.00443 <0.00292 <0.00589 <0.000606 <0.000612 <0.000996 <0.00269 <0.0144 <0.00360 <0.00136 <0.00315 <0.00144 <0.00134 <0.00125 <0.00552 85 13.2 20.1 <0.00323 IHSB PSRGs -Residential Health Based 940 4.1 L 122200 1.2 780 1600 0.0056 0.038 6.1 NL NL 5,500 41 780 200 90 63 56 120 3100 0.31 NL 21.3 PSRGs- Protection of Groundwater 630 0.3IHSB NL 5 0.1 4.1 0.00035 0.00011 13 NL NL 170 1.5 8.3 12 1101 9.9 580 3.8 27 IHSB PSRGs- Industrial/Comm ercial Health Based 14000 5A 14.5 2000 23000 0.068 0.17 27 NL NL 400 00 7300 9700 370 320 i 530 1 47000 1 6.5 NI 9.7 Result = Result Exceeds Minimum Detection Limits Result = Result Exceeds IHSB Residential Health Based PSRG Result = Result Exceeds IHSB Protection of Groundwater PSRG Result = Result Exceeds IHSB Industrial/Commercial Health Based PSRG LEGEND GROUNDWATER MONITORING WELL Q SOIL BORING ® WATER SUPPLY WELL ---- FORMER TANK LOCATION GRAPHIC SCALE NOTES: 0 30 60 120 1.) 2017 AERIAL DETAINED FROM WAKE COUNTY GIS DEPT, 2.) Site Plan Overlay by Wm. G. Daniel & Assoc. dated September 7, 2018. 3.) Former UST pits are approximated on map. 1 inch = 60 ft. M I I I I R4.5' IR4.5 I PROPOSED 5' SAN ALONG FORESTVILLE ROAD OTHERS) w ti 18.6 l -- 26.0' (BY uj 85.00' EXIST. RAN I I 97.50' PROPOSED RAN ' I I I I I R3.5' I R4.0' A I I I I I I R15. 46 I; Ci Z ' R14 I jLU I In I N ' N I Q3 I Q N 0 g -wr _J f Ix Ix 1 I I i I I El d o I --1 18.5' 9.0' T- 0 IE BUFFER i "RYWAY AND MONUMENT SIGN _ EAPPROVED SEPARATELY) _ LE LOCATION .-. - R15.0' PROPOSED BUILDING #3 10,500 SF (70'X150') 26.00' 1 R6.0' OUTDOOR PROFOS BUILDI 8,450 SF ( 5' ) FORMER FUEL TANK LOCATIO $ ,PROP D/ 0'UTgq /\MENt CE !^ `r J SI / 8 iC A S`�[ R5.0' 9• 1 \ 26.0' W2 9FORMERFUEL TANK LOCATION 6- 10PA .40 ? " 0 / 10'X70' SIGHT I CI,DISTANCE I, 52.0'� TRANGLES (TYP) 0 '`' '•'r.. ECONC. IE AK>: :2.31' L 27.0' B-B _If ' .I- R15.0' V1 R6.0' 1 9.0' R4.5' k0 �6 18.5' 1- 9.0' T- PROPOSED BUILDING #2 5,250 SF (70'X75') R3.0' 'y^._.• z PROPOSED Z BUILDING #1 25,200 SF 4i W (70'X360') Z la 0o� J Q Z LU O: IF J LJJ J_ t. Vf w Q � F OLL w 1 0p OLL O LL Y B-4/MWI; 4i It L3 W i O w . V 2.06' W i \ ) � PROPOSED OUTDOOR m/ AMENITY SPACE NIP C f^ V / ro UV ro EL o BOV L NIP s= LU `` 89°59'O6" W NIP ,, FOUNDATION DR I6 LI GROUNDWATER MONITORING WELL ® WATER SUPPLY WELL NOTES: 1.) 2017 AERIAL OBTAINED FROM WAKE COUNTY GIS DEPT. 2.) Surficial groundwater elevations are based on a local site survey conducted by WR with relative elevations, using MW-1 top of casing as a benchmark of 100.00 feet. All measurements are in feet. Data collected in January 2019. GRAPHIC SCALE 0 40 80 160 1 inch = 80 ft. a ILJ i' i IF �l1A gal MW-5 (77.38) 18 1$ _19 r s 0 MW-42(F0R R' 'O S., "I O� �MW-1 (82.80) MW-(82.53) $3 84 MW-4 (84.07) erCIO 0 WSW ~ r 0 Ln 0 0 z V � _P O N R K O O M ai II N � O odi o `~ R a m m Ln Q LI 0 J 0 Q LU p N - Ip U p Z =i Z Oga Inc 2 � H W v a Z O�� W 0, w U W - �' Y Q > < NL� pLU� J OLL � WLL. O, oO W Y Q � W J- (ii ;2 C v 1 ^ C V 1 � L— ii W u L� Ul F Lj LU a = w w LU W N UU N LU UU z LU z �O Z LUUULU z Z w g z UU z w Sample Date UU z w LU^w c=i w a ID Collected m LUm N z LULU 4a O z y� LU z LU 03r rj w a Q S } w z ~ I-`,' w LU UU is LU f Uj W w m DO o D_ a O w N z W o: o: w z f z O m ti a O a a � v " LU a o 4 w m z w (n W (n a z Z Q) __ O F t.i 1`i os r X a z (V 7143-2 10451-8 135-98-8 100-414 98-82-8 91-20-3 103-65-1 100-42-5 630-20-6 108-88-3 95-63-6 526-73-8 108-67-8 1330-20-7 91-20-3 105-67-9 07/23/07 NA NA 500 NA 160 82 82 NA 1400 500 NA NA 2040 NA NA MW-1 08/28/15 1 1 18 12 66 300 150 150 16 6500 1200 NA 290 6600 NA NA 01/10/19 07/23/07 501 8.3 1 <18.0 NA <18.2 NA NA 89.8 NA 581 NA 232 NA <15.4 NA 1 <19.2 NA 6220 NA 1600 NA 429 NA 1 434 NA 1100 NA 273 NA 11.9 NA MW 2 01/10/19 ABANDONED 1-9-2019 MW-3 01/10/19 <0.331 <0.361 <0.365 <0.384 <0.326 <1.00 <0.349 <0.307 <0.385 1 <0.412 <0.373 <0.321 1 <0.387 1 <1.06 <0.372 <0.264 MW-4 01/10/19 <0.331 <0.361 <0.365 <0.384 <0.326 <1.00 <0.349 <0.307 <0.385 <0.412 <0.373 <0.321 <0.387 <1.06 <0.372 1 <0.264 MW-5 01/10/19 <0.331 <0.361 <0.365 <0.384 <0.326 <1.00 <0.349 <0.307 <0.36 NC 2L Standard 1 70 70 600 70 6 70 70 210 Residential VI GWSL 16 NE NE 35 NE 35 490 1900 37 Non -Residential VI GWSL 69 NE NE 150 NE 150 2000 7800 160 NA = Not Available in Historical Reports; Only compounds with detected concentrations greater than the 2L Standards were listed in the 2007 LSA Report. Result = Result Exceeds Laboratory Method Detection Limits Result .I = Result Exceeds 2L Standard = Result Exceeds Non -Residential VI GWSL ( - MIN liilll� �y FOUNDATION D ; LEGEND GROUNDWATER MONITORING WELL ® WATER SUPPLY WELL NOTES: 1.) 2017 AERIAL OBTAINED FROM WAKE COUNTY CIS DEPT. 2.) Analytical laboratory reports from the 2019 sampling event are available in the report Appendix D. GRAPHIC SCALE 0 40 80 160 1 inch = 80 ft. FH •�I S I PROPOSED 12.5tl f ' I DEDICACATION I42 14.50' WIDENING 1(12 FT PAVEMENT AND30-CUR8& I GUTTER) I /J ■ I I I PROPOSED 5'SNV ALONG FORESTVILLE ROAD (BY OTHERS) I I I � IU FII I I I I O I EI I <0.412 <0.373 <0.321 600 400 3800 50 70 16000 210 290 a 35 77 35 NE / 150 320 150 NE i 0 limp 65' ' PUBLIC RNJ - - - - '- ROGERS BRANCH C - _EX' �-- 20'STREETSCAPE BUFFER PROPOSED ENTRYWAY AND MONUMENT SIGN (SIGNAGETOBEAPPROVEDSEPARATELY) _ I / PROPOSED FLAGPOLE LOCATION / ( I 15 I R15.0' ( PA. R15.0' 28.W Re.tl 1 Re.tl I R15.0' ( R15.0' ' �6'CONC,.SIgEWALK. I RB.tl PROPOSED ( OUTDOOR I AMENITY SPACE I--26.0'--I I I 14 O 9FORMER FUEL I:• TANK LOCATION I I R4.5' PROPOSED BUILDING R4.5' ( u I R4.5' 8,450 BE(65'X1301 CI a 18.50' j� 28.0'�t�37.0 18.5' I--28.0'-{ iB5 1 h I � � 1 J- = FORMER FUEL 1 .• 1t T 11 . i TANK LOCATION I I O PROPOSED OUTDOOR l I AMENITY SPACE I R3.5' I R4.tl . 7 6 Cj1N0. SIDEWAIk .. R3.0' I 8O 18.5' o-FD ( I R15.tlNo C RR15.0' l R14.5' t R5.tl I9.tl 26.tl l Mel 27.0' B43 9.0' R 1 9.tl N H � J W D � N 2a W J z U O� � J 1 CONTROL VICINITY MAP III ��I�jj Q / 10'X]0'SIGHT CORNER V DISTANCE I N(y):798,69].9]' SCALE: 1"=500� Z TRANGLES(TYP) A E(z):2,146,334.37'SITE �111111�Id11��1�I(ii"'�"�1111��� IPROP ,c BED SITE EIP . 4pZ., / / EIP I.. C� 1. NAME: 2. STREETADDRESS: 3. P.LN: 4. LAND USE WHEAT FIELD SHOPPING CEN 1009 FORESTVILLE ROAD WAKE FOREST, NORTH CAROL 1749.68-0479 SINGLE FAMILY/COMMERCIAL g \ 5. TOTAL NUMBER OF LOTS: 2 I- 6. LANDAREAS (.� I. AREA OF PARCEL 231,735 SF / 6.32 ACRES W AREA OF PARCEL B: RMTO BE DEDICATED: 104,045 SF / 2.38 ACRES 41,406 BE 10.95 ACRES U J C RE SIDUALAREAOFPARCELA: RESIDUAL AREA OF PARCEL B: 196,203 BE/4.50 ACRES 98,171 SF/2.25 ACRES Z DISTURBED AREA: 226,175 BE 15.19 ACRES O 0 F CURRENTZONING: CONDITIONAL USE NEIGHBOR J Q Z }, IVIER) I. IVIC l J: \ (CU NB) 0 O S. EXISTING BUILDING AREAS: EXISTING DWELLING (TO BE RF > W U ADDITIONAL SQUARE FOOTAGE: PROPOSED BUILD No W J LLI PROPOSED BUILDING#2 '., rPROPOSED PROPOSED BUILDING#3 Q ; Q PROPOSED BUILDING#4 F \ TOTAL PROPOSED SQUARER W \ Q 11. PROPOSED BUILDING LOT COVERAGE: 21% 0 i 12. MAXIMUM BUILDING HEIGHT: 3 STORIES (50 FT) O LU Uj PROPOSED BUILDING #1 13. PROPOSED BUILDING HEIGHT: 2STORY(35 FT) p O 25,200 SF N/FLL O STROUD-WAKE (]0'X360') FOREST LP D.B. 16902, PAGE 1059 B.M. 1989, PAGE 690 14. BUILDING SETBACKS: FRONT-20 FT. SIDE LOT -15 FT. -200FFT. W ` 1/ r a J PIN#1]49.02-6]-9852 A�.'.� 15. INSIDE CITY LIMITS: YES Uj 5 _ 16. INSIDE FLOOD HAZARD BOUNDARY: NO (PER FEMA MAP #3]201749 2 EFFECTIVE DATE: MAY 2, 2006 17. PARKING SUMMARY: L'. GENERAL COMMERCIAL (1SPACE /350BE) °29D SF 811 SPACES REQUIRED F I RESTAURANT (1 SPACE 1200 SF) °20,000 SF 100 SPACESREQUIRED -+ /A'� � MINIMUM PARKING REQUIRED W i �L /� d IYI W I• T MAXIMUM SPACES ALLOWED TOTAL SPACES PROVIDED 184.1.5=276 SPACES 276 SPACES MAX ALLOWED 187 SPACES PROVIDED (179 R C T N a i �/ II I.'. 18. IMPERVIOUS SURFACE AREA: EXISTING: 14,371 BE 10.33 ACRES(7%) > Z) V) _- PROPOSED: 128,748 SF / 2.90 ACRES (66%) Y TOTAL: 143.119 /3.29 ACRES (73%) 8 \/ i I: 1S INSIDE NO 20. DEDICATED STREET RIGHT OFEWDAAY: 12.5 FT ALONG FORESTVILLE R ROGERS BRANCH EXT. ,� C V IVY III ro 2.08' 21. OWNER: SASSOM, LLC. _ CAPITAL 80ULEVAAR WAKE WAKE FOREST, NORTH CAROL W i PROPOSED 01 OUTDOOR Q) AMENITY SPACE NIP 5 W � •• LL � o� NIPAFAN 69°59'OB" W NIP ST.RMWATER NOTE: ALL SITE.T.RMWATER FOUNDATION D Soil Vapor Probe ID: SV-9 Duplicate (SV-9) Sample Date: 10/10/19 10/10/19 Acetone 780 1,300 Benzene 31 28 Carbon Disulfide 55 60 Carbon Tetrachloride 0.91 0.88 Ethanol 16 ND Ethylbenzene 6.0 5.5 4-Ethyltoluene 4.0 4.0 Heptane 110 87 4-Methyl-2-pentanone(MIBK) 3.2 2.3 Naphthalene 2.5 2.6 Propene 1,500 1,800 Tetrachloroethylene 6.0 6.3 Toluene 27 25 1,2,4-Trimethylbenzene 4.8 4.8 1,3,5-Trimethylbenzene 1.6 1.6 m&p-Xylene 11 10 o-Xylene 5.1 4.6 LEGEND SOIL VAPOR PROBE NOTES: 1.) 2017 Aerial Obtained from Wake County GIS Dept. 2.) Proposed Site Plan by Red Line Engineering, Dated August 5, 2019. 3.) Former UST pits are approximated on map. 4.) All Soil Vapor Concentrations are in ug/m3. 5.) Full Soil Vapor Analytical Results are Included in Appendix D of Report. I '- I I Soil Vapor Probe ID: SV-6 7j8.37 Sample Date: 10/10/19 Acetone 46 B Benzene 4.0 2-Butanone (MEK) 3.1 Carbon Disulfide 16 Ethylbenzene 1.5 4-Ethyltoluene 2.6 Heptane 1.9 _ Isopropanol 4.5 Tetrachloroethylene 1.0 Toluene 5.2 s _ _ _ _ _ _ PUBLICRAN - 1,1,1-Trichloroethane 0.5 ROGERS Trichlorofluoromethane 2.0 BRANCH EXT. 3 ;1,2,4-Trimethylbenzene 3.2 - - - - - - 1,3,5-Trimethylbenzene 1.3 m&p-Xylene 4.1 o-Xylene 2.2 (g s) 20' STREETSCAPE BUFFER PROPOSED ENTRYWAY AND MONUMENT SIGN f I - (SIGNAGE TO BE APPROVED SEPARATELY)FH ( PR OSED FLAGPOLE LOCATION o/ I I 15 It I I I I 11.80, • el R ° R9.5' d I -� I 28.00' 1 R6.0' R8.0' ' ( I R15.0' I � O 3 I I R6.0'..'�6'6 'SID WALK':. PROPOSED 12.5V ( I PROPOSED OUTDOOR - RAN AMENITYSPACE I DEDICATION ) 126.0' �{ rn I II 14.50' WIDENING (12 FT PAVEMENT AND 30" CURB & I I GUTTER) I.I I - G I I I R4.5' V PROPOSED yAS BUILDING1 I ( I I LL I R4.5' 0 8,450 S (65'X') PROPOSED 5' S/W w L 18,5' �-- 26.0' --I 18.5' ALONG FORESTVILLE '• ROAD (BY OTHERS) y Y -- Soil Vapor Probe ID: SV-8 o a 11 9.0' 8 FORMER FUEL Sample Date: 10/10/19 I I T o TANK LOCATION Acetone 25 Benzene 7.2 I 'p PROPOSED OUTDOOR 2-Butanone (ME K) 3.7 I I AMENITYSPACE Carbon Disulfide 49 I R3.5' Ethylbenzene 2.7 I R4.0' 6'CQNC'SIOEWALR�. 4 Ethyltoluene 2.9 Q�C 1ss Heptane 10 I I R15.0' Isopropanol 3.3 I R114.6 Naphthalene 2.2 9.0' 26.0' Tetrachloroethylene 1.3 I Toluene 9.7 Soil Vapor Probe ID: SV-5 c 9.0 1,2,4-Trimethylbenzene 3.5 I Sample Date: 30/10/19 18.5' 1,3,5-Trimethylbenzene 1.3 I Acetone 290 m&p Xylene 6.7 Benzene 7.5 sldE�v D-Xylene 2.9 2-Butanone (MEK) 9.8 I I Carbon Disulfide 52 o I Ethylbenzene 2.5 wl �.v 4-Ethyltoluene 3.9 S /- 5 V I Heptane 34 Naphthalene 2A I I Toluene 8.6 S� I 1,2,4-Trimethylbenzene 5.2 S � 1,3,5-Trimethylbenzene 1.5 $ ' m&p-Xylene 6.6 • 4 ° ` 7'• " ` - I o-Xylene 2.6 I EI R5.0' 18.50' weer-eenev+nvee D.B. 6895, PAGE 732 R R,1 -, DGr_e 1, Soil Vapor Probe ID: SV-7 Sample Date: 10/10/19 Acetone 120 Benzene 6.1 2-Butanone (MEK) 7.1 Carbon Disulfide 42 Carbon Tetrachloride 1.2 1,3-Dichlorobenzene 1.9 Ethanol Ethylbenzene 14 1.9 4-Ethyltoluene 4.1 Heptane 16 Isopropanol 13 4-Methyl-2-pentanone (MIBK) 1.6 Naphthalene 2.9 Tetrachloroethylene 1.3 Tetrahydrofuran 1.7 Toluene 6.4 1,1,1-Trichloroethane 0.55 1,2,4-Trimethylbenzene 5.1 1,3,5-Trimethylbenzene 1.9 m&p-Xylene 5.5 o-Xylene 2.7 R15.0' R15.0' R15.0' 990, R6.0' 99 ER FUEL R4.5'� LOCATION � I / / EIP CONTRO 4x70' SIGHT CORNER DISTANCE I N(y):798,1 TRANGLES (TYP) E(x):2,14f SV-1 - 2BUILDING#1 25,200 SF R4.5' R4.5' 10 U (70'X360') - 26.0' r}^ 37.0' 26.0' ---1 18.5' 0' T g.0' 11 11 R4.5' ] T SV-3 R15.0' R15.0' R3.0' R9 ASV-4 PROPOSED BUILDING #2 5,250 SF (70'X75') Soil Vapor Probe ID: SV-4 Sample Date: 10/10/19 Acetone 930 Benzene 1.4 2-Butanone (MEK) 14 Carbon Disulfide 2.0 Ethanol 25 Ethyl Acetate 2.8 Ethylbenzene 1.1 Heptane 0.97 Isopropanol 12 4-Methyl-2-pentanone(MIBK) 0.61 Naphthalene 1.5 Toluene 3.6 Trichlorofluoromethane 1.3 1,1,2-Trichloro-1,2,2-trifluoroethane 1.2 1,2,4-Trimethylbenzene 5.3 1,3,5-Trimethylbenzene 1.1 m&p-Xylene 4.4 o-Xylene 2.2 Soil Vapor Probe ID: SV-1 Sample Date: 10/10/19 Acetone 950 Benzene 5.8 2-Butanone (MEK) 27 Carbon Disulfide 13 Carbon Tetrachloride 0.53 Chloroform 2.2 Ethanol 61 Ethylbenzene 1.2 4-Ethyltoluene 0.9 Heptane 4.5 Hexane 39 Naphthalene 1.6 Propene 260 Toluene 5.3 Trichlorofluoromethane 1.4 1,2,4-Trimethylbenzene 4.7 1,3,5 -Trimethyl benzene 1.0 m&p-Xylene 4.3 o-Xylene 2.1 SITE PLAN INFORMATION: 1 1. NAME: 2. STREETADDRESS: W m J 3. P.I.N.: 4. LAND USE (EXISTING/PROPOSED): W \ C 5. TOTAL NUMBER OF LOTS: a � N 6. LANDAREAS O J W I AREA OF PARCEL A' Q Soil Vapor Probe ID: SV-2 Sample Date: 10/10/19 Acetone 1,700 Benzene 12 2-Butanone (MEK) 28 Carbon Disulfide 16 Ethanol 92 Ethylbenzene 2.1 4-Ethyltoluene 1.4 Heptane 30 Hexane 190 Naphthalene 2.4 Propene 1,100 Toluene 9.0 Trichlorofluoromethane 1.5 1,3,5-Trimethylbenzene 1.5 m&p-Xylene 7.1 o-Xylene 3.1 Soil Vapor Probe ID: SV-3 Sample Date: 10/10/19 Acetone 940 Benzene 2.5 2-Butanone (MEK) 20 Carbon Disulfide 16 Carbon Tetrachloride 0.43 Ethanol 26 Ethylbenzene 1.1 4-Ethyltoluene 1.3 Heptane 2.0 Hexane 53 Naphthalene 2.3 Styrene 0.75 Toluene 3.9 Trichlorofluoromethane 1.4 1,2,4-Trimethylbenzene 7.3 1,3,5-Trimethylbenzene 1.5 m&p-Xylene 5.2 o Xylene 2.6 AREA OF PARCEL B: IZ U m R/W TO BE DEDICATED: a O RESIDUAL AREA OF PARCEL A; RESIDUAL AREA OF PARCEL B. J J 7. DISTURBEDAREA: O 3. CURRENTZONING: O Z 1 3. EXISTING BUILDING AREAS: y 0. PROPOSED ADDITIONAL SQUARE 11. PROPOSED BUILDING LOT COS 12. MAXIMUM BUILDING HEIGHT: 13. PROPOSED BUILDING HEIGHT: 14. BUILDING SETBACKS: 15. INSIDE CITY LIMITS: 6. INSIDE FLOOD HAZARD BOUNC 7. PARKING SUMMARY: GENERAL COMMERCIAL RESTAURANT MAXIMUM SPACES ALLOWED TOTAL SPACES PROVIDED 8. IMPERVIOUS SURFACE AREA: EXISTING: PROPOSED: TOTAL: 9. INSIDE PROTECTED WATERSH 0. DEDICATED STREET RIGHT OF 1. OWNER: GRAPHIC SCALE v 30 60 120 IP 1 inch = 60 ft. d i W U a Z W 0O w U J J LU y�� Q 0 F mow W o O O LL O Y a � W 3 W I^_ C O ^, a W (Ij ) ro i c v) L o_ i v w `` ,, Tables TABLE 1 SUMMARY OF SOIL ANALYTICAL RESULTS WHEAT FIELDS DEVELOPMENT 1009 FORESTVILLE ROAD WAKE FOREST, WAKE COUNTY, NORTH CAROLINA WR Project # 02180643.01 Data Collected Notes: 1) All results provided in mg/kg (milligrams per kilogram) or parts per million. 2) Compounds are only listed in this table if detected above laboratory detection limits. See the laboratory report for a full list of constituents. 3) IHSB PSRGs= Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (February 2018) 4) Chemical Abstract Service (CAS) Registry Numbers shown for compounds detected. QuallBers: B: The analyte was found in the associated blank. NA = Not Analyzed by Method Shown Result = Result Exceeds Minimum Detection Limits Result = Result Exceeds IHSB Residential Health Based PSRG Resut = Result Exceeds IHSB Protection of Groundwater PSRG R= Result Exceeds IHSB Industrial/Commercial Health Based PSRG TABLE 2 MONITORING WELL CONSTRUCTION INFORMATION WHEAT FIELDS DEVELOPMENT BROWNFIELDS 1009 FORESTVILLE ROAD WAKE FOREST, WAKE COUNTY, NORTH CAROLINA WR Project # 02180643.01 Well Well Date Water Depth -to -Water Groundwater Well Coordinates Well ID Date Installed Casing Total Casing Screened Top -of -Casing Level from Elevation on Free Product (NC State Plane NAD 83 Feet) Diameter Depth Interval Elevation Thickness Depth Measured Top of Casing 01-10-19 (inches) Easting Northing MW-1 07/22/07 2 40 0-25 25-40 100.00 01/10/19 17.18 1 82.82 N/A 2146138.73 798437.20 MW-2 07/22/07 2 40 0-25 25-40 Well Abandoned 2146169.458 798551.8577 MW-3 01/08/19 2 29 0-14 14-29 101.01 01/10/19 17.67 83.34 N/A 2146130.35 798298.16 MW-4 01/08/19 2 22 0-7 7-22 95.99 01/10/19 10.20 85.79 N/A 2146287.54 798366.03 MW-5 01/08/19 2 29 0-14 14-29 101.65 01/10/19 23.24 78.41 N/A 2146026.93 798712.07 Notes: 1) All measurements shown in feet, unless otherwise indicated. 2) N/A denotes Not Applicable Page 1 of 1 TABLE 3 SUMMARY OF GROUNDWATER ANALYTICAL RESULTS WHEAT FIELDS DEVELOPMENT 1009 FORESTVILLE ROAD WAKE FOREST, WAKE COUNTY, NORTH CAROLINA WR Project # 02180643.01 Analytical Method EPA-8260B EPA-8270D Lu < = w w w w w w w w w W z z z O w w w z O J w m w m w m z w Sample Date w z w z w N U } } } < w ID Collected z m w m z w < O z } w m J } N J d W m W w �_ w �_ w �_ W = w Z } D w 0c O < = } 0-Z w w Z �/j w < S W w N H m J } �' ~ = w N w � Z w = mLU 0- 0 d r� � _ N N M CO Z (n w Z Z (n X Z N 71-43-2 104-51-8 135-98-8 100-41-4 98-82-8 91-20-3 103-65 1 100-42-5 630-20-6 108-88-3 95-63-6 526-73-8 108-67-8 1330-20-7 91-20-3 105-67-9 07/23/07 1800 NA NA 500 NA 160 82 82 NA 1400 500 NA NA 2040 NA NA MW-1 08/28/15 1500 18 12 1600 66 300 150 150 16 6500 1200 NA 290 6600 NA NA 01/10/19 501 <18.0 <18.2 2180 89.8 581 232 <15.4 <19.2 6220 1600 429 434 11000 273 11.9 MW-2 07/23/07 8.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 01/10/19 ABANDONED 1-9-2019 MW-3 01/10/19 <0.331 <0.361 <0.365 <0.384 <0.326 <1.00 <0.349 <0.307 <0.385 <0.412 <0.373 <0.321 <0.387 <1.06 <0.372 <0.264 MW-4 01/10/19 <0.331 <0.361 <0.365 <0.384 <0.326 <1.00 <0.349 <0.307 <0.385 <0.412 <0.373 <0.321 <0.387 <1.06 <0.372 <0.264 MW-5 01/10/19 <0.331 <0.361 <0.365 <0.384 <0.326 <1.00 <0.349 <0.307 <0.385 <0.412 <0.373 <0.321 <0.387 <1.06 <0.372 <0.264 NC 2L Standard 1 70 70 600 70 6 70 70 210 600 400 -- 400 500 6 100 Residential VI GWSL 16 NE NE 35 NE 35 490 1900 37 3800 50 70 35 77 35 NE Non -Residential VI GWSL 69 NE NE 150 NE 150 2000 7800 160 16000 210 290 150 320 150 NE NA = Not Available in Historical Reports; Only compounds with detected concentrations greater than the 2L Standards were listed in the 2007 LSA Report. Result = Result Exceeds Laboratory Method Detection Limits Result = Result Exceeds 2L Standard Result = Result Exceeds Non -Residential VI GWSL Page 1 of 1 TABLE 4 SUMMARY OF SOIL VAPOR PROBE ANALYTICAL RESULTS WHEAT FIELDS DEVELOPMENT 1009 FORESTVILLE ROAD WAKE FOREST, WAKE COUNTY, NC WR PROJECT NO.02180643.01 Soil Vapor Probe ID: SV-1 SV-2 SV-3 SV-4 SV-5 SV-6 SV-7 SV-8 SV-9 te Duplicate Residential SGSL (ug/m3) Non -Residential SGSL (ug/m3) Sample Date: 10/10/19 10/10/19 10/10/19 10/10/19 10/10/19 10/10/19 10/10/19 10/10/19 10/10/19 10/10/19 Acetone 950 1,700 940 930 290 46 120 25 780 1,300 220,000 2,700,000 Benzene 5.8 12 2.5 1.4 7.5 4.0 6.1 7.2 31 28 120 1,600 2-Butanone (MEK) 27 28 20 14 9.8 3.1 7.1 3.7 <1.1 <1.1 35,000 440,000 Carbon Disulfide 13 16 16 2.0 52 16 42 49 55 60 4,900 61,000 Carbon Tetrachloride 0.53 <0.41 0.43 <0.41 <0.41 <0.41 1.2 <0.41 0.91 0.88 160 2,000 Chloroform 2.2 <0.36 <0.36 <0.36 <0.36 <0.36 <0.36 <0.36 <0.36 <0.36 41 530 1,3-Dichlorobenzene <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 1.9 <0.62 <0.62 <0.62 NE NE Ethanol 61 1 92 26 25 <6.7 <6.7 14 <6.7 16 <6.7 NE NE Ethyl Acetate <0.54 <0.54 <0.54 2.8 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 490 6,100 Ethylbenzene 1.2 2.1 1.1 1.1 2.5 1.5 1.9 2.7 6.0 5.5 370 4,900 4-Ethyltoluene 0.9 1.4 1.3 <0.60 3.9 2.6 4.1 2.9 4.0 4.0 NE NE Heptane 4.5 30 2.0 0.97 34 1.9 16 10 110 87 2,800 35,000 Hexane 39 1 190 53 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 4,900 61,000 Isopropanol <0.90 <0.90 <0.90 12 <0.90 4.5 13 3.3 <0.90 <0.90 1,400 18,000 4-Methyl-2-pentanone (MIBK) <0.43 <0.43 <0.43 0.61 <0.43 <0.43 1.6 <0.43 3.2 2.3 21,000 260,000 Naphthalene 1.6 2.4 2.3 1.5 2.4 <0.80 2.9 2.2 2.5 2.6 21 260 Propene 260 1,100 <0.64 <0.64 <0.64 <0.64 <0.64 <0.64 1,500 1,800 21,000 260,000 Styrene <0.53 1 <0.53 0.75 0.61 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 7,000 88,000 Tetrachloroethylene <0.75 <0.75 <0.75 <0.75 <0.75 1.0 1.3 1.3 6.0 6.3 280 3,500 Tetrahydrofuran <0.59 <0.59 <0.59 <0.59 <0.59 <0.59 1.7 <0.59 <0.59 <0.59 NE NE Toluene 5.3 9.0 3.9 3.6 8.6 5.2 6.4 9.7 27 25 35,000 440,000 1,1,1-Trichloroethane <0.41 <0.41 <0.41 <0.41 <0.41 0.5 0.55 <0.41 <0.41 <0.41 35,000 440,000 TrichIorofIuoromet hane 1.4 1.5 1.4 1.3 <0.85 2.0 <0.85 <0.85 <0.85 <0.85 NE NE 1,1,2-TrichIoro-1,2,2-trifIuoroethane <1.2 <1.2 <1.2 1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 35,000 440,000 1,2,4-Trimethylbenzene 4.7 <0.63 7.3 5.3 5.2 3.2 5.1 3.5 4.8 4.8 420 5,300 1,3,5-Trimethylbenzene 1.0 1.5 1.5 1.1 1.5 1.3 1.9 1.3 1.6 1 1.6 420 5,300 m&p-Xylene 4.3 7.1 5.2 4.4 6.6 4.1 5.5 6.7 11 10 700 8,800 o-Xylene 1 2.1 3.1 2.6 2.2 1 2.6 2.2 1 2.7 1 2.9 5.1 4.6 700 8,800 Notes: All units in ug/m3 SGSL = Exterior Soil Gas Screening Levels from DWM Vapor Intrusion Screening Levels, February 2018. NE = Not Established Only analytes with sampling detections are listed in this table. For the full analytical report, see Appendix C of this report. Appendix A Brownfields Receptor Survey North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program BROWNFIELDS PROPERTY RECEPTOR SURVEY This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield's Project Manager (PM). Site: Wheat Fields Address: 1009 Forestville Road City: Wake Forest, NC County: Wake County Brownfields Project Number: 22051-18-092 Property and Building Characteristics Surface Conditions Current Usage Proposed Usage Size of Property (acres) 5.32 +/- 4.50 +/- % of property that is wooded/brush 3.38% 0.00% % of property that is grassed areas 93.04% 34.00% % of property that is agricultural crops 0.00% 0.00% % of property that is paved 2.26% 40.80% % of property that is covered by buildings 1.32% 25.20% Note: Rogers Branch Ext. will extend onto the northern portion of the property in the proposed site plan. If an existing building is on -site, please respond to the following. Information can be provided on additional sheets as needed. If numerous buildings are on -site, consult with your PM as only information on specific buildings may be needed. a. Provide occupancy and use information. Single Family Home b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay doors), and height (number of stories). One-story brick frame on cinder block foundation, shingle roof, crawl space beneath. Windows and doors are standard for a single -story single family home. Building to northeast of home has been razed - cement slab remains in place. c. Describe the foundation construction. Include details on type, floor construction, and depth below grade. Cinder block foundation, crawl space beneath. Cement slab at carport, driveway, and former storage building. d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design considerations (e.g. positive pressure?). One HVAC unit exists on north side of house, standard for a single family home. e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details. None known. Rev. 09/2016 Page 1 of 4 North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Surrounding Property Land Use Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If specific receptors are present, please provide addresses of the facilities. Zoning/Land Use Current Use/Occupant Proposed Usage North Empty lot, New Market Heritage Shopping Center, and Residential/Commercial McDonalds Restaurant Two single family homes (one for sale that is now zoned South commercial, and one occupied), and a large development of Residential/Commercial many single family homes. East A large development of single family homes. Residential West Heritage High School School 'Note - see attached zoning map printed from Wake County iMAPS* Specific Land Uses of Interest Y/N * Distance Direction Address Is a school or daycare center within 1,000 ft of the Y West 1150 Forestville Road Is there a residence within 1,000 ft of the Property? Y not yet East 6512,6516,6520,6524,6528,6532,6536 available Penfield Street (new construction) Is there a basement within 1,000 ft of the Property N * If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses. - Utilities For the subject property, please provide a map of known buried utilites. If available, include depth to top, construction material, and diameter of the utilities. In addition, please provide the following information on utilty providers. If additional assessment is required, the public utility locators should be contacted. This information can then be added to a site map. Is there a septic system on -site? (Y or N) Y Please provide the utility providers for the subject property a. Natural Gas _ PSNC b. Sewer _ City of Raleigh c. Electricity _ Wake County d. Other For surrounding properties, please complete the following table with available information. Utility/Potential Receptor Y/N * Dis(tatance Direction Is a storm water pipe within 100 ft of the Property boundary? Y 75 W/NW Is a sanitary sewer within 100 ft of the Property boundary? Y 30 SE Is a septic system leach field within 500 ft of the Property boundary? Y 110 E/NE Is a water line main within 100 ft of Property boundary? Y 90 W Is a natural gas line main within 100 ft of the Property boundary? Y 100 W Is a buried telephone/ cable main within 100 ft of the Property boundary? Y 90 W Is a buried electrical cable main within 100 ft of Property boundary? N * If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property. Information collected during site visit and from the Wake County GIS Website. Rev. 09/2016 Page 2 of 4 North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Water Supply The purpose of this section is to provide information on the water supply for the site and surrounding areas. What is the potable water supply for the property? Public Y Private If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water providers name. The onsite water supply well will be abandoned. Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be present. Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please attach a separate table to list all wells. Please note, the PM may opt for a more extensive water supply well survey if needed. Water Supply Wells Y/N Distance (ft) Direction Address Is a public water supply well within 1 mile of the Property N Is a private water supply well within 1,500 ft of the Property boundary? Y 730 ft 800 ft 930 ft SE E E 1129 Forestville Road; 3700 Rogers Branch Rd; 3716 Rogers Branch Rd Is an irrigation well within 1,500 ft of the Property boundary? N Surface Water & Wetlands The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the Property. Provide Information regarding Surface Water Response/Comments and Wetlands Are there surface water features on the property? (If yes, please complete a. to d.) No a. Is the water body naturally developed or man-made? N/A b. List the uses of the water body. N/A c. What is the source of the water for the water body? N/A d. What is the nature of the bottom of the water body (e.g., rocky or concrete bottom, N/A drainage ways or impoundments) If no on -site surface water features, what is the nearest surface water body? A stream and pond to the southeast and south of the property on the adjacent property to the south. Are there any wetlands present on the property? If no wetlands on -site, are wetlands No suspected on adjoining properties? Rev. 09/2016 Page 3 of 4 TABLE B-4 WATER SUPPLY WELL OWNER INFORMATION Wheat Fields Development Property 1009 Forestville Road Wake Forest, Wake County, North Carolina Approximate Well ID # Current Owner and Owner Well Casing Distance From property Address Property Type /Use Of Well (PIN Number) Address Depth (ft) Depth (ft) Release Source 1 Margaret Perry Marshall 1009 Forestville Road Commercial /Well is Not Used; (Parcel # 1749680479) 250 FT 537 Hidden Valley Road Wake Forest, NC 27587 Will be Abandoned Unknown Unknown Wilmington, NC 28409 2 Margaret P. Schepp 1129 Forestville Road (Parcel # 1749670589) 900 ft 1129 Forestville Road Wake Forest, NC 27587 Residential / Drinking Unknown Unknown Wake Forest, NC 27587 3 Edward Ralph Schwerin, Jr. 3700 Rogers Branch Road (Parcel # 1749781509) 1000 ft 3700 Rogers Branch Road Wake Forest, NC 27587 Residential / Drinking Unknown Unknown Wake Forest, NC 27587 4 Richard B. Fecteau Trust 3716 Rogers Branch Road (Parcel # 1749782560) 1150 ft 3716 Rogers Branch Road Wake Forest, NC 27587 Residential / Drinking Unknown Unknown Wake Forest, NC 27587 Note: Well ID #s are depicted on Figure 2. /,-j h�A�V) / Wake County and Wake Forest Zoning -from Wake County IMAPS Website IMM �r ia AD-1- AD-2 AEH AD-11 CURD-1I CAJ-Hi3 MH CLI-RR CAJ-1-1 CLI-1-2 CtNA i CU-O&J C"-10 CU-R-15 CIJ-R-20 CU-R-30 CU-R-[l H HC HO 1-1 MH 0&1 PD H-1 0 R-1 5 R-20 r R-30 R-4R R-WW ■ R-80 I1484YY RA H on Wake Forest Zoning PUD, Plan -nod Unit Development OS, Open Space FAD, Rural Holding DisllAct GRIO, Generai Residential 10 GR5, General Residential 5 GR3, General ResideatiaJ 3 UR, Urban Residential RWI , Residential Wxed- Ise NMX, Neighborhood MtKed-Use RA FiG, Renaissance Area Historic Gofe UW Wb n Mixed -Use NB, NoighboftGd Business NR, Highway Business IGD, InffituUmall Campus Oewloprnent Li, Light IMustiaa Hi, Heavy In-dusbial Appendix 6 Boring Logs, Monitoring Well Construction Logs, and Soil Vapor Probe Construction Logs ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-1 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798440.5569 Easting 2146133.1145 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 1.0 dark brown, organic rich, coarse grained silty sand --- --- 1.0 12.0 reddish brown, coarse grained sandy silt, moist, no odor 0' - 2' 5.1 2' - 4' 4.1 4' - 6' 3.8 6'-8' 3.2 8' - 10' 2.4 10' - 12' 2.3 12.0 18.0 pinkish gray, light brown, coarse grained sandy silt, dry, no odor, quartz fragments 12' - 14' 2.4 14' - 16' 2.2 16' - 18' 2.3 Refusal @ 18' Sample 2' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water El=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina z7511 to%919.469.334o fax.919.467 6008 www, withersravenel. com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-2-1 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798413.5976 Easting 2146113.3418 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 1.0 dark brown, organic rich, coarse grained silty sand --- --- 1.0 13.0 reddish brown, coarse grained sandy silt, moist 0' - 2' 5.1 2' - 4' 3.9 4' - 6' 3.0 6' - 8' 2.6 8' - 10' 34.3 10' - 12' 6.2 13.0 18.0 pinkish gray, light brown, coarse grained sandy silt, dry odor 12' - 14' 1248.0 14' - 16' 676.8 16' - 18' 61.9 Refusal @ 18' Sample 14' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o fax.919.467 6008 www, wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-2-2 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798413.5558 Easting 2146100.6435 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 0.5 organics, dark brown coarse grained silty sand --- --- 0.5 12.0 reddish brown, coarse grained sandy clayey silt, moist, no odor 0' - 2' 1.4 2' - 4' 1.6 4' - 6' 2.1 6'-8' 1.8 8'-10' 1.3 10' - 12' 1.7 12.0 14.0 light brown, coarse grained sandy silt, moist 12' - 14' 1.4 14.0 18.0 pinkish gray, coarse grained sandy silt, dry 14'-16' 1.6 16' - 18' 4.2 18.0 20.0 light brown, clayey silt, moist 18' - 20' 5.0 NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o Fax.919.467 6008 www, wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-3-1 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798390.8185 Easting 2146123.0307 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 2.0 dark gray, brown, organics, coarse grained silty sand 0' - 2' 3.9 2.0 11.0 reddish brown, coarse grained silty sand, moist, odor 2' - 4' 2.7 4' - 6' 2.6 6' - 8' 15 8' - 10' 762.1 10' - 12' 606.8 11.0 20.0 pinkish gray, light brown, coarse grained sandy silt, dry, odor 12' - 14' 23.9 14' - 16' 567.1 16' - 18' 99.9 18'-20' 1171.0 Sample 20' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water El=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o fax.919.467 6008 www, withersravenel. com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-3-2 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798386.6277 Easting 2146153.6235 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 0.5 organics, dark brown coarse grained silty sand --- --- 0.5 9.0 reddish brown, coarse grained sandy silt, moist, no odor 0' - 2' 1.0 2' - 4' 0.5 4' - 6' 0.6 6' - 8' 0.5 9.0 10.0 pinkish gray, coarse grained sandy silt with quartz, dry 8' - 10' 0.4 10.0 13.0 light brown, sandy clayey silt, moist 10' - 12' 0.7 12' - 14' 0.5 13.0 20.0 pinkish gray, coarse grained sandy silt with quartz, dry 14'-16' 1.2 16' - 18' 1.1 18'-20' 1.0 NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o fax.919.467 6008 www, wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-3-3 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798387.0985 Easting 2146138.2034 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 0.5 organics, dark brown coarse grained silty sand --- --- 0.5 11.0 reddish brown, clayey sand, moist, no odor 0' - 2' 1.6 2' - 4' 1.2 4' - 6' 1.6 6'-8' 1.2 8'-10' 1.2 11.0 14.0 light brown, sandy silt, moist 10' - 12' 0.9 12'-14' 1.2 14.0 17.0 light brown, coarse grained sandy silt to light and dark brown, sandy silt @ 15', dry 14' - 16' 1.2 16' - 18' 1.1 17.0 20.0 pinkish gray, light brown, coarse grained sandy silt, dry, no odor 18' - 20' 10.3 NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina z7511 to%919.469.334o Fax.919.467 6008 www, wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-3-4 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798378.9594 Easting 2146121.0685 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 1.0 dark brown, organic rich, coarse grained silty sand --- --- 1.0 12.0 reddish brown, coarse grained sandy silt, moist, no odor 0' - 2' 0.5 2' - 4' 0.8 4' - 6' 0.9 6'-8' 0.7 8' - 10' 1.0 10' - 12' 1.4 12.0 18.0 pinkish gray, light brown, coarse grained sandy silt, dry, no odor, quartz fragments 12' - 14' 1.2 14' - 16' 1.1 16' - 18' 1.0 Refusal @ 18' NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water El=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina z7511 to%919.469.334o fax.919.467 6008 www, withersravenel. com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-3-5 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798392.9585 Easting 2146108.4032 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 0.25 organics --- --- 0.25 9.0 light brown, sandy clayey silt, moist 0' - 2' 1.0 2' - 4' 1.1 4' - 6' 0.9 6'-8' 1.2 9.0 10.0 pinkish gray, light brown, coarse grained sandy silt, dry 8' - 10' 0.6 10.0 14.0 light brown, coarse grained sandy silt, moist 10' - 12' 1.3 12' - 14' 1.7 14.0 20.0 pinkish gray, light brown, coarse grained sandy silt, dry, odor 14'-16' 1.8 16' - 18' 2.1 18'-20' 219.9 NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o Fax.919.467 6008 www, wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-4-1 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798412.9236 Easting 2146142.5515 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 1.5 dark brown, organic rich, coarse grained silty sand 0' - 2' 1.3 1.5 12.0 reddish brown, coarse grained sandy silt, moist, strong odor from sleeves 2' - 4' 1.5 4' - 6' 400.2 6' - 8' 2104 8' - 10' 34.6 10' - 12' 938.4 12.0 15.0 pinkish gray, light brown, coarse grained sandy silt, dry, strong odor 12' - 14' --- 14' - 15' 27.7 Refusal @ 15' Sample 8' & 12' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina z7511 to%919.469.334o fax.919.467 6008 www. wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T1SW-4-2 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798410.6770 Easting 2146154.9094 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 0.5 gray, brown, organics, coarse grained silty sand --- --- 0.5 4.0 reddish brown, sandy clayey silt, moist 0' - 2' 0.1 2' - 4' 0.3 4.0 9.0 light brown, sandy silt, dry 4' - 6' 1.6 6' - 8' 1.6 8'-10' 1.3 9.0 15.0 pinkish gray, light brown, coarse grained sandy silt with quartz throughout, dry, no odor 10' - 12' 1.7 12' - 14' --- 14' - 15' 1.4 Refusal @ 15' Sample 8' & 12' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o Fax.919.467 6008 www. wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T2SW-1 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798558.1684 Easting 2146169.1225 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 0.5 organics, brown, sandy silty clay, moist --- --- 0.5 4.0 reddish brown, coarse grained sandy silt, dry 0' - 2' 0.5 2' - 4' 0.4 4.0 8.0 pinkish gray, light brown, coarse grained sandy silt, dry, some weather quartz/rock 4' - 6' 0.3 6'-8' 0.3 8.0 20.0 light gray, light brown, coarse grained sandy silt with quartz fragments, dry, no odor 8' - 10' 0.4 10' - 12' 0.3 12' - 14' 0.6 14' - 16' 0.8 16' - 18' 0.7 18'-20' 0.8 Sample 16' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water EI=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o fax.919.467 6008 www, withersravenel. com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T2SW-2 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798531.0778 Easting 2146154.7101 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 8.0 organics (0.25'), reddish brown, coarse grained sandy silt, moist 0' - 2' 1.1 2' - 4' 1.0 4' - 6' 0.6 6'-8' 1.2 8.0 18.0 pinkish -gray, light brown, coarse grained sandy silt, dry quartz fragments throughout 8' - 10' 0.7 10' - 12' 1.5 12' - 14' 0.9 14'-16' 1.3 16' - 18' 1.1 Refusal @ 18' Sample 12' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o fax.919.467 6008 www. wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T2SW-3 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Grid EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798510.3016 Easting 2146170.6472 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 2.5 organics (0.25'), reddish brown, coarse grained sandy silt, mottled, moist 0' - 2' 0.8 2.5 18.0 pinkish -gray, light brown, coarse grained sandy silt, dry, quartz fragments throughout 2' - 4' 1.2 4' - 6' 1.0 6'-8' 1.1 8' - 10' 1.0 10' - 12' 1.1 12' - 14' 0.9 14'-16' 1.2 16' - 18' 1.4 Refusal @ 18' Sample 18' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water E1=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o Fax.919.467 6008 www, wither5ravenel com ;!WithersRavenel Engineers I Planners I Surveyors SOIL BORING LOG Boring # T2SW-4 Job Name Wheat Fields Development Job # 2180643.01 Date 1/9/2019 Site Loc. Wake Forest, NC Gnd EL NA WR Rep LE Driller Quantex, Inc. GW EL NA Northing 798530.6512 Easting 2146184.2954 Depth in Feet From To Soil Description (Field USCS Classification) Total VOCs (in ppm) Sample Interval PID 0.0 3.0 organics (0.25'), reddish brown, coarse grained sandy silt, slightly moist 0' - 2' 0.9 2' - 4' 0.8 3.0 7.0 light brown, sandy clayey silt, dry 4' - 6' 1.2 6' - 8' 0.9 7.0 20.0 light gray, light brown, coarse grained sandy silt with quartz throughout, dry, no odor 8'-10' 1.2 10' - 12' 1.0 12' - 14' 1.0 14' - 16' 1.4 16' - 18' 1.1 18'-20' 0.9 Sample 16' bgs NR=No reading ppm=parts per million NA=Not Applicable GW=Ground Water BGS=Below ground surface USCS=Unified Soil Classification System TOC=Top of Casing GW=Ground Water El=Elevation Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 to%919.469.334o fax.919.467 6008 www, withersravenel. com QpWithersRavenel Our People. Your Success. WELL CONSTRUCTION LOG Well ID: MW-3 / SB-3 Job Name: Wheat Fields Development Job #: 2180643.01 Date: January 8, 2019 Site Loc.: Wake Forest, NC TOC EL: 99.99 WR Rep: LE Driller: Quantex, Inc. GW EL: 82.53 Depth in PID Soil Description Well Construction Feet m (Field USCS Classification) 0 Ground Surface 1 1.0 0-5 ft Grout 2 3 dark brown, organic rich clayey sand, From O'to 4 0.9 moist (0.5') to reddish brown, clayey silty sand, moist 7' 0-9 ft 2" Dia. PVC - 5 Casing 5-7 ft Bentonite 6 7 1.0 light brown, clayey silty sand, moist From Tto 9 10 1.0 12' 11 12 13 0.9 pinkish gray, light brown, sandy silt, dry From 12' to - 14 15 16 0.9 19, 7-29 ft Clean -Washed Torpedo SAND 9-29 ft 2" Dia. - 17 18 19 N/A 0.010-Slot PVC Well Screen 20 light brown, sandy silt, very moist to wet From 19' to 29' 21 22 23 - 24 25 26 27 2 29 30 Notes: 1.) Boring Terminated at 40' BLS, monitoring well built at 29' 2.) BLS - Below Land Surface = = Groundwater Level (Measured Beneath BLS) 3.) TOC - Top of Casing Page 1 of 1 ii5Mackenan Drive Cary, North Carolina 27511 tel-PIP.46p.334o fax:91.9.467.6008 wwwwithersravenelcom 410 WithersRavenel NOOur People. Your Success. WELL CONSTRUCTION LOG Well ID: MW-4 / SB-4 Job Name: Wheat Fields Development Job #: Date: January 8, 2019 Site Loc.: Wake Forest, NC TOC EL: WR Rep: LE Driller: Quantex, Inc. GW EL: 2180643.01 94.99 84.07 Depth in Feet (PID Soil Description (Field USCS Classification) Well Construction E: 0 Ground Surface 1 0.3 dark -medium brown, organic, coarse grained silty sand, moist (0'-l'), reddish brown, coarse grained silty sand, dry From to 8' 0-3 ft Grout 3-5 ft Bentonite 5-22 ft Clean -Washed Torpedo SAND 0-7 ft 2" Dia. PVC Casing 7-22 ft 2" Dia. 0.010-Slot PVC Well Screen - 2 3 4 0.6 - 5 6 7 0.6 - 8 9 light brown, coarse grained clayey silty sand, slightly moist From 8' to 12' 10 0.7 - 11 12 13 0.6 pinkish -gray, light brown, coarse grained sandy silt, dry From 12' to 22' - 14 15 16 1.7 17 18 19 20 1.4 21 22 23 24 25 26 27 28 29 30 Notes: 1.) Boring Terminated at 25' BLS, monitoring well built at 22' 2.) BLS - Below Land Surface = = Groundwater Level (Measured Beneath BLS) 3.) TOC - Top of Casing Page 1 of 1 115Macl(enan Drive Cary, North Carolina 27511 tel.-919-46p.334o fax.-PIR-467.6008 www.withersravenelcom WithersRavenel :i Our People. Your Success. WELL CONSTRUCTION LOG Well ID: MW-5 / SB-5 Job Name: Wheat Fields Development Job #: 2180643.01 Date: January 8, 2019 Site Loc.: Wake Forest, NC TOC EL: 100.64 WR Rep: LE Driller: Quantex, Inc. GW EL: 77.38 Depth in PID Soil Description Well Construction Feet m (Field USCS Classification) 0 Ground Surface dark brown, organic silty sand (05) to reddish brown, coarse grained clayey From 0'to g: ma 2 sand, moist 3' 3 0.4 4 reddish brown, coarse grained silty From 3' to 0-10 ft Grout 6 0.4 sand, dry 8' �® a 7 A® ®® PVC Casing 8o e 9 0.5 10 11 From 8' to 10-12 ft Bentonite15'"' �: ®® 12 light brown/gray, silty sand, dry ®® 13 0.4 12-29 ft Clean -Washed Torpedo SAND 14 15 14-29 ft 2" Dia. 0.010-Slot PVC Well Screen 16 pinkish gray to light brown, sandy silt, dry From 15' to 17' 17 1.0 18 N/A same as above From 17' to 29' 19 20 21 22 23 24 25 26 27 28 29 30 Notes: 1.) Boring Terminated at 29' BLS, monitoring well built at 29' 2.) BLS - Below Land Surface = = Groundwater Level (Measured Beneath BLS) 3.) TOC - Top of Casing Page 1 of 1 :i5MacKenanDrive Cary, NorthCarolina 27511 tet.•919.469.334o fax:919.467.6008 www.withersravenei.com 40 WithersRavenel NoOur People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-1 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146261.44 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 Grout to Surface 1.0 1.5 2.0 0-4.5' 1/4" Teflon 2.5 Tubing Bentonite (1'-4') 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' 3.5 4.0 4.5 5.0 Sand Pack (4'-5.5') ®®® ®®® 4.5'-5' 1/2" Stainless ® Steel Screen Point 5.5 ®®� Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o fax.919.467.6008 www.wither5ravenel.com ■� WithersRavenel . Our People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-2 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146261.12 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 Grout to Surface 1.0 1.5 2.0 Bentonite (0.5'-35) 0-4.5' 1/4" Teflon 2.5 Tubing 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' 3.5 4.0 ®® 4.5 Sand Pack (3.5'-55) ®®® 4.5'-5' 1/2" Stainless 5.0 ® Steel Screen Point 5.5®®� Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o faX.919.467.6008 www.wither5ravenel.com 40 WithersRavenel . Our People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-3 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146263.99 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 1.0 Grout to Surface 1.5 2.0 0-4.5' 1/4" Teflon 2.5 Tubing 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' Bentonite (0.5-35) 3.5 4.0 4.5 5.0 Sand Pack (4'-5.5') ®®® ®®® 4.5'-5' 1/2" Stainless ® Steel Screen Point 5.5 Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o fax.919.467.6008 www.wither5ravenel.com 40 WithersRavenel . Our People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-4 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146166.55 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 1.0 Grout to Surface 1.5 2.0 0-4.5' 1/4" Teflon 2.5 Tubing 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' Bentonite (0.5'-35) 3.5 4.0 4.5 5.0 Sand Pack (4'-5.5') ®®® ®®® 4.5'-5' 1/2" Stainless ® Steel Screen Point 5.5 Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o fax.919.467.6008 www.wither5ravenel.com 40 WithersRavenel . Our People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-5 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146077.27 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 1.0 Grout to Surface 1.5 2.0 0-4.5' 1/4" Teflon 2.5 Tubing 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' Bentonite (0.5'-35) 3.5 4.0 4.5 5.0 Sand Pack (4'-5.5') ®®® ®®® 4.5'-5' 1/2" Stainless ® Steel Screen Point 5.5 Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o fax.919.467.6008 www.wither5ravenel.com 40 WithersRavenel . Our People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-6 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146029.35 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 1.0 Grout to Surface 1.5 2.0 0-4.5' 1/4" Teflon 2.5 Tubing 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' Bentonite (0.5'-35) 3.5 4.0 4.5 5.0 Sand Pack (4'-5.5') ®®® ®®® 4.5'-5' 1/2" Stainless ® Steel Screen Point 5.5 Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o fax.919.467.6008 www.wither5ravenel.com 40 WithersRavenel . Our People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-7 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146088.68 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 1.0 Grout to Surface 1.5 2.0 0-4.5' 1/4" Teflon 2.5 Tubing 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' Bentonite (0.5'-35) 3.5 4.0 4.5 5.0 Sand Pack (4'-5.5') ®®® ®®® 4.5'-5' 1/2" Stainless ® Steel Screen Point 5.5 Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o fax.919.467.6008 www.wither5ravenel.com 40 WithersRavenel . Our People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-8 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146048.62 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 1.0 Grout to Surface 1.5 2.0 0-4.5' 1/4" Teflon 2.5 Tubing 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' Bentonite (0.5'-35) 3.5 4.0 4.5 5.0 Sand Pack (4'-5.5') ®®® ®®® 4.5'-5' 1/2" Stainless ® Steel Screen Point 5.5 Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o fax.919.467.6008 www.wither5ravenel.com 40 WithersRavenel . Our People. Your Success. SOIL VAPOR PROBE CONSTRUCTION LOG Well ID: SV-9 Job Name: Wheat Fields Development Job #: _ Date: October 9, 2019 Site Loc.: Wake Forest, NC TOC EL: _ WR Rep: Jackson Cates Driller: SAEDEACCO Drilling GW EL: _ NC NAD83 Easting: 2146088.15 NC NAD83 Northing: 02180643.01 Depth in Soil Description Well Construction Feet Field USCS Classification) 0 Ground Surface Ground Surface 0.5 Grout to Surface 1.0 1.5 2.0 0-4.5' 1/4" Teflon 2.5 Bentonite (1'-4') Tubing 3.0 DIRECT PUSH - NO CUTTINGS 0' to 5.5' 3.5 4.0 4.5 5.0 Sand Pack (4'-5.5') ®®®® ®® 4.5'-5' 1/2" Stainless ® Steel Screen Point 5.5 ®®� Notes: 1.) Boring Terminated at 5.5' BLS 2.) BLS - Below Land Surface 3.) TOC - Top of Casing 4.) NA - Not Applicable Page 1 of 1 115 MacKenan Drive Cary, North Carolina 27511 tei.919.469.334o fax.919.467.6008 www.wither5ravenel.com Appendix C Photo Log, Groundwater Sampling Forms, Soil Vapor Sampling Forms, and Field Notes ..Our People. Your Success. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 40 ..Our People. Your Success. M'k View facing 1. east 1 adjace nt to vacant house Apo A- carport Drill rig is at w •. • n . Octobe '2019. x View facing k north- west », • vacant house toward Forest- J. ville d, r Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 40 ..Our People. Your Success. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 ..Our People. Your Success. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 Frame No. 9 x�,,�•h"y�,�-ram � ��- OZ- 40 ..Our People. Your Success. s c_ Soil vapor .� probe mow _f SV-3 upon install- ation Octobe 2019. -:05 4.-- 1 Frame No. 10 Soil vapor probe SV-3 helium shroud setup before sampli ng on Octobe r 10, 2019. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 Frame No. 11 �GF,s f Frame No. 12 40 .im Our People. Your Success. r, G V� •'"�4 Soil vapor " probe SV-4 upon " °Nt! ' install- ation S Octobe 1 - r 9, B . 2019. Soil vapor probe SV-4 helium shroud setup before sampli ng on Octobe r 10, 2019. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 40 ..Our People. Your Success. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 40 ..Our People. Your Success. Frame No. 15 Soil vapor probe SV-6 upon install- ation y Octobe y 4 2019. a r , �•- La � "fir..:. ,� � �a ��' �s � M,� t `- � Frame No. 16 i Soil vapor t probe SV-6 helium shroud setup before AN ��.* - sampli r 1 ng on Octobe — f r 10, 2019. ar Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 ..Our People. Your Success. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 ..Our People. Your Success. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 40 ..Our People. Your Success. Frame No. 21 :A Xy Soil .�.� vapor probe SV-8 upon install- L ation Octobe .w$ - r9 2019. Frame No. 22 jit WIN 1 Msf ;" ri C't .il I vapor p robe SV-8 with '; Y{ poly Oren sheetin g and �,.. helium u ' shroud W._ before va �. ii seal on Octobe AM' 2019. 77 Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 40 ..Our People. Your Success. Frame No. 23 Soil vapor probe SV-8 with �,-AA 00"" sealed helium F shroud on Octobe a r 9, joy -J fit- _� " a,� V! 2019. Frame No. 24 3 �� s�`� uaa ie. �"• t �` -� 1ry� � V'� 4���`�•�'�iA„p�� 1 � fiCgdIX'. �F, - - F Sd n��l �t _ � e` 'r��a, Soil w ►� s� vapor �� :� probe R :: X SV-8 helium �. A ` ■... shroud setup before k� a tIS t.1.ngon sampli n,Ra Octobe r 10, a 2019. �+{ '¢� �k••��'.�`A`� fX�'.+�' Cr* :�i' � 'ffi_ \S '!n�i �y��� N�a& ( - F �'S,,. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 40 ..Our People. Your Success. Frame No. 25 R - . ;b View of x- " F soil .y; vapor r� 3: sampli -_ n g - from SV-8. Frame No. 26 Soil vapor probe SV-9 upon install- ation Octobe r 9, ' 2019. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 ..Our People. Your Success. Wheat Fields Development WR Project No. 02180643.01 Soil Vapor Probe Installation and Sampling Photographic Record November 2019 ;!WithersRavenel Engineers I Planners I Surveyors Page 1 of 4 Job Number 02180643.01 Groundwater Sampling Form State ID Well ID MW-1 Site Name Wheat Fields Development Date 1/10/2019 Well Depth 40 Depth to Water 17.18 Well Diameter 2 Casing Material PVC Screen Length 15 Well Water Volume 3.720 Sampling Crew JC Pump Type Peri Tubing Type poly Intake set at -- 30' Weather Conditions 30-407F, sunny, breezy Notes (eg. odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.) (from TOC) (Gals.) (ma/L) (°C) (uS/cm) (standard) (mv) (NTU) Other Parameters NA Sampled at Samples delivered to ESC 1505 Parameters taken with YSI Pro/Lutron Turbidity Meter by Fed Ex at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 250 ml glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3 None 125 ml plastic 48 Hours Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Cr VI 48 Hours Well Volume Calculation 1" well [well depth -depth to water] * 0.0408 gallons 2" well [well depth -depth to water] * 0.163 3.720 gallons 4" well [well depth -depth to water] * 0.653 gallons K:\18\18-0640\180643.01-Wheat Fields Development\Enviro\Reports and Del iverables\REPORTING\GW Samplinc Forms_January 2019 1OWithersRavenel Engineers I Planners I Surveyors Page 2 of 4 Job Number 02180643.01 Groundwater Sampling Form State ID Well ID MW-3 Site Name Wheat Fields Development Date 1/10/2019 Well Depth 29 Depth to Water 17.67 Well Diameter 2 Casing Material PVC Screen Length 15 Well Water Volume 1.847 Sampling Crew JC Pump Type Peri Tubing Type poly Intake set at -- 20' Weather Conditions 30-407F, sunny, breezy Notes (eg. odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.) (from TOC) (Gals.) (ma/L) PC) (uS/cm) (standard) (mv) (NTU) 1400 --- --- 7.69 13.61 0.148 5.81 49.5 350 1405 --- --- 4.41 13.63 0.152 5.76 25.5 311 1410 --- --- 4.19 12.16 0.148 5.75 28.8 283 1415 --- --- 3.55 12.18 0.147 5.59 24.2 275 1420 --- --- 3.59 12.12 0.146 5.62 19.5 222 1423 --- --- 3.52 12.12 0.147 5.63 16.7 199 1426 --- --- 3.45 12.14 0.146 5.65 13.3 183 1429 --- --- 3.46 12.15 0.15 5.65 12.9 175 Other Parameters NA Sampled at Samples delivered to ESC 1430 Parameters taken with YSI Pro/Lutron Turbidity Meter by Fed Ex at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 250 ml glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3 None 125 ml plastic 48 Hours Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Cr VI 48 Hours Well Volume Calculation 1" well [well depth -depth to water] * 0.0408 gallons 2" well [well depth -depth to water] * 0.163 1.847 gallons 4" well [well depth -depth to water] * 0.653 gallons K:\18\18-0640\180643.01-Wheat Fields Development\Enviro\Reports and Del iverables\REPORTING\GW Samplinc Forms_January 2019 1OWithersRavenel Engineers I Planners I Surveyors Page 3 of 4 Job Number 02180643.01 Groundwater Sampling Form State ID Well ID MW-4 Site Name Wheat Fields Development Date 1/10/2019 Well Depth 22 Depth to Water 10.20 Well Diameter 2 Casing Material PVC Screen Length 15 Well Water Volume 1.923 Sampling Crew JC Pump Type Peri Tubing Type poly Intake set at -- 13' Weather Conditions 30-407F, sunny, breezy Notes (eg. odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.) (from TOC) (Gals.) (ma/L) PC) (uS/cm) (standard) (mv) (NTU) 1200 --- --- --- --- 1225 --- --- 10.00 12.36 0.095 6.34 21.6 646 1230 --- --- 5.07 12.35 0.092 5.88 12.9 645 1235 --- --- 5.43 11.51 0.091 5.74 17.2 575 1240 --- --- 5.20 11.17 0.091 5.66 17.2 505 1245 --- --- 5.15 11.00 0.091 5.73 22.3 344 1250 --- --- 5.22 10.45 0.089 5.63 23.6 206 1300 --- --- 5.26 11.17 0.09 5.70 28.1 96 1303 --- --- 5.53 11.21 0.091 5.68 30.4 67 1306 --- --- 5.45 11.23 0.092 5.68 30.6 55 1309 --- --- 5.43 11.24 0.092 5.68 30.5 55 Other Parameters NA Sampled at Samples delivered to ESC 1310 Parameters taken with YSI Pro/Lutron Turbidity Meter by Fed Ex at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 250 ml glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3 None 125 ml plastic 48 Hours Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Cr VI 48 Hours Well Volume Calculation 1" well [well depth -depth to water] * 0.0408 gallons 2" well [well depth -depth to water] * 0.163 1.923 gallons 4" well [well depth -depth to water] * 0.653 gallons K:\18\18-0640\180643.01-Wheat Fields Development\Enviro\Reports and Del iverables\REPORTING\GW Samplinc Forms_January 2019 ;!WithersRavenel Engineers I Planners I Surveyors Page 4 of 4 Job Number 02180643.01 Groundwater Sampling Form State ID Well ID MW-5 Site Name Wheat Fields Development Date 1/10/2019 Well Depth 29 Depth to Water 23.24 Well Diameter 2 Casing Material PVC Screen Length 15 Well Water Volume 0.939 Sampling Crew JC Pump Type Peri Tubing Type poly Intake set at -- 20' Weather Conditions 30-407F, sunny, breezy Notes (eg. odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.) (from TOC) (Gals.) (MOIL) PC) (uS/cm) (standard) (mv) (NTU) Other Parameters NA Sampled at Samples delivered to ESC 1135 Parameters taken with YSI Pro/Lutron Turbidity Meter by Fed Ex at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 250 ml glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3 None 125 ml plastic 48 Hours Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Cr VI 48 Hours Well Volume Calculation 1" well [well depth -depth to water] * 0.0408 gallons 2" well [well depth -depth to water] * 0.163 0.939 gallons 4" well [well depth -depth to water] * 0.653 gallons K:\18\18-0640\180643.01-Wheat Fields Development\Enviro\Reports and Del iverables\REPORTING\GW Samplinc Forms_January 2019 WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-1 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 1 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 730 F cloudy Barometric Pressure 30.12 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING: Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) 2.1 LF Gas Meter Readings: Methane (in %) NA Oxygen (in %) NA Carbon Dioxide (in %) NA Carbon Monoxide (CO in PPM) NA Hydrogen Sulfide (H2S in PPM) NA SAMPLING MEDIA: Canister ID # 2305 Canister Volume (in Liters) Regulator ID # 4328 Duration and/or Setting Vacuum Pre -Test: Pass or Fail (Circle One) Starting Vacuum 29.5 Starting Time 1640 Ending Vacuum 5 Ending Time 1650 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-2 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 2 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 730 F cloudy Barometric Pressure 30.14 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) LF Gas Meter Readings: Methane (in %) Oxygen (in %) Carbon Dioxide (in %) Carbon Monoxide (CO in PPM) Hydrogen Sulfide (H2S in PPM) SAMPLING MEDIA: 2.3 NA NA NA NA NA Canister ID # 2299 Canister Volume (in Liters) Regulator ID # 4340 Duration and/or Setting Vacuum Pre -Test: Pass or Fail (Circle One) Starting Vacuum 30 Starting Time 1545 Ending Vacuum 5 Ending Time 1555 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-3 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 3 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 730 F cloudy Barometric Pressure 30.15 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) LF Gas Meter Readings: Methane (in %) Oxygen (in %) Carbon Dioxide (in %) Carbon Monoxide (CO in PPM) Hydrogen Sulfide (H2S in PPM) SAMPLING MEDIA: Canister ID # Regulator ID # Vacuum Pre -Test: Starting Vacuum Ending Vacuum 0.0 NA NA NA NA NA 2244 Canister Volume (in Liters) 4138 Duration and/or Setting Pass or Fail (Circle One) 28 Starting Time 1445 5 Ending Time 1455 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-4 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 4 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 710 F cloudy Barometric Pressure 30.17 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) LF Gas Meter Readings: Methane (in %) Oxygen (in %) Carbon Dioxide (in %) Carbon Monoxide (CO in PPM) Hydrogen Sulfide (H2S in PPM) SAMPLING MEDIA: Canister ID # Regulator ID # Vacuum Pre -Test: Starting Vacuum Ending Vacuum 2241 4139 0.2 NA NA NA NA NA Canister Volume (in Liters) Duration and/or Setting Pass or Fail (Circle One) 27 Starting Time 1350 5 Ending Time 1400 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-5 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 5 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 690 F cloudy Barometric Pressure 30.18 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) LF Gas Meter Readings: Methane (in %) Oxygen (in %) Carbon Dioxide (in %) Carbon Monoxide (CO in PPM) Hydrogen Sulfide (H2S in PPM) SAMPLING MEDIA: Canister ID # Regulator ID # Vacuum Pre -Test: Starting Vacuum Ending Vacuum 2236 4229 2.3 NA NA NA NA NA Canister Volume (in Liters) Duration and/or Setting Pass or Fail (Circle One) 27 Starting Time 1256 5 Ending Time 1306 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-6 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 6 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 590 F cloudy Barometric Pressure 30.21 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) LF Gas Meter Readings: Methane (in %) Oxygen (in %) Carbon Dioxide (in %) Carbon Monoxide (CO in PPM) Hydrogen Sulfide (H2S in PPM) SAMPLING MEDIA: 2.1 NA NA NA NA NA Canister ID # 2257 Canister Volume (in Liters) Regulator ID # 4321 Duration and/or Setting Vacuum Pre -Test: Pass or Fail (Circle One) Starting Vacuum 30 Starting Time 1118 Ending Vacuum 5 Ending Time 1128 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-7 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 7 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 630 F cloudy Barometric Pressure 30.2 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) LF Gas Meter Readings: Methane (in %) Oxygen (in %) Carbon Dioxide (in %) Carbon Monoxide (CO in PPM) Hydrogen Sulfide (H2S in PPM) SAMPLING MEDIA: Canister ID # Regulator ID # Vacuum Pre -Test: Starting Vacuum Ending Vacuum 2338 4262 1.3 NA NA NA NA NA Canister Volume (in Liters) Duration and/or Setting Pass or Fail (Circle One) 29 Starting Time 1201 5 Ending Time 1210 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-8 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 8 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 570 F cloudy Barometric Pressure 30.22 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) LF Gas Meter Readings: Methane (in %) Oxygen (in %) Carbon Dioxide (in %) Carbon Monoxide (CO in PPM) Hydrogen Sulfide (H2S in PPM) SAMPLING MEDIA: Canister ID # Regulator ID # Vacuum Pre -Test: Starting Vacuum Ending Vacuum 2319 4337 3.3 NA NA NA NA NA Canister Volume (in Liters) Duration and/or Setting Pass or Fail (Circle One) 28.5 Starting Time 1023 5 Ending Time 1032 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log WO WithersRavenel Engineers I Planners I Surveyors PROBE NO: TOTAL DEPTH LOCATION: SV-9 5.5 feet (TD) Wake Forest, NC VAPOR PROBE SAMPLING LOG PAGE 9 OF 9 PROJECT: Wheat Fields Development PROJECT NO: 02180643.01 DATE: 10/10/2019 SAMPLER: JC LABORATORY: Con -Test WEATHER CONDITIONS: Air Temperature 720 F cloudy Barometric Pressure 30.11 Stable, Rising, or Falling (Circle One) Moisture Description Sampling Zone (Dry, Moist, Saturated, or Flooded) dry to slightly moist PURGING Calculated Purge Volume (in CCs) 52.8 Headspace Reading VOCs by PID (in PPM) 9.3 LF Gas Meter Readings: Methane (in %) NA Oxygen (in %) NA Carbon Dioxide (in %) NA Carbon Monoxide (CO in PPM) NA Hydrogen Sulfide (H2S in PPM) NA SAMPLING MEDIA: Duplicate Canister ID # 2300 2302 Canister Volume (in Liters) Regulator ID # 4310 4310 Duration and/or Setting Vacuum Pre -Test: Pass or Fail (Circle One) Starting Vacuum 29 Starting Time 1740 Ending Vacuum 5 Ending Time 1750 COMMENTS: Sampling Event Successful Yes or No (Circle One) Other Notes: 1L 10 min 100 CC Vapor Probe Sampling Log I f; ee 18O&Y3 a �3v cues ►a s J tire, �- LlG a . 44v/ �o (2z, (d CA Y rt�¢CA) JSC It 0 \, Page of EnaSnPlanners � �iirev, Job Number 0z'I go (eq3, Groundwater Sampling Form State ID Well ID r( - I Site Name t GlL( �P'"�� Date /lo liq Well Depth (YU Depth to Water 1?,I g Well Diameter 2- Casing Material PVC Screen Length Well Water Volume Sampling Crew _3 L Pump Type Cc,,, Tubing Type ec,f ; Intake set at Weather Conditions 3�=q,-,`s �i� 6r-e ea.Notes (eg. odor or color) ,-, i 6-, I44 3 5 Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.) (from TOC) (Gals ) (mo1L) (°C) (uSlcm) (standard) fmV) (NTU) ■tea ��� . ��� Utner Parameters NA Sampled at / u Parameters taken with YSI Pro/Lutron Turbidity Meter Samples delivered to ESC by Fed Ex at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 250 ml glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3 None 125 ml plastic 48 Hours Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Cr VI 48 Hours vveii volume uaicuiauon 1" well [well depth -depth to water] " 0.0408 gallons 2" well [well depth -depth to water] ' 0.163 gallons 4" well [well depth -depth to water] ' 0.653 gallons C:\Users\jcates\Desktop\GW Sampling Form 2018 14 2- Page 2 of q Job Number o 2-1$ 0(e<<3. Z) r Groundwater Sampling Form State ID Site Name LJ�., } 5 �dJ_ Well ID 1'v - 3 Date ! v Well Depth 'SO Depth to Water (7.�? Well Diameter 2 Casing Material PVC Screen Length Well Water Volume Sampling Crew _. L Pump Type mi Tubing Type_?_(r Intake set at Weather Conditions kU 5 In r-4 Win; Notes (eg. odor or color) r 3 Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.) (from TOC) (Gals.) (malt] (°C) (uS/cm) (standard) (mV) (NTU) ■tea � .�.:1 ��■�� umer varameiers Sampled at Samples delivered to Parameters taken with YSI Pro/Lutron Turbidity Meter by Fed Ex at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 250 ml glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3 None 125 ml plastic 48 Hours Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Cr VI 48 Hours U,r ckFv 1 well volume calculation 1" well [well depth -depth to water] * 0.0408 gallons 2" well [well depth -depth to water] * 0.163 gallons 4" well [well depth -depth to water] * 0.653 gallons T-e­p= 1 Z. !g C:\Users\jcates\Desktop\GW Sampling Form 2018 (2�, :: T Page of Job Number GZL�°O�`f3.o Groundwater Sampling Form State ID r� Well ID c• Site Name [,�� icA#1�Q��`� [raw Date 1710 Well Depth Depth to Water Well Diameter Casing Material PVC Screen Length Well Water Volume Sampling Crew L_ Pump Type Tubing Type -oI.Y Intake set at Weather Conditions` 5 y NN t�❑dor or color) G Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.) (from TOC) (Gals.) (mclL) (°C) fuS/cm) (stanriarrll (mV) (NTl1) 00 �so�oe viner rarameiers NH Sampled at Samples delivered to Parameters taken with YSI Pro/Lutron Turbidity Meter by Fed Ex at Analysis Preservative Bottle ware Number of Battles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 250 ml glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3 None 125 ml plastic 48 Hours Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Cr VI 48 Hours vveii voiume t.aiculaifon 1" well [well depth -depth to water] * 0.0408 gallons 2" well [well depth -depth to water] * 0.163 gallons 4" well [well depth -depth to water] * 0.653 gallons C:\Users\jcates\Desktop\GW Sampling Form 2018 WithersRavenel wooEngineer s 1 Planners 1 surrieyors Groundwater Sampling Form Page of Job Number State I D W 11 111 � � � 9 � e Site Name ���.( � Date Well Depth Z Depth to Waterer Well Diameter Z Casing Material PVC Screen Length Well Water Volume Sampling Crew_ f> Pump Type pe I`, Tubing Type cbin Intake set at Weather Conditions t ,�'� hr �c 5,, ..z� Notes (eg. odor or color) b3 a Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.) (from TOC) (Gals.) (mglL) (°C) (µS/cm) standard mV NTU �e �a�eaeo Other Parameters Sampled at Samples delivered to Parameters taken with YSI Pro/Lutron Turbidity Meter by Fed Ex at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 250 ml glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3 None 125 ml plastic 48 Hours Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Cr VI 48 Hours Well Volume Calculation 1" well [well depth -depth to water] * 0.0408 gallons 2" well [well depth -depth to water] * 0.163 gallons 4" well [well depth -depth to water] * 0.653 gallons C:\Users\jcates\Desktop\GW Sampling Form 2018 2l V cR, Y- w 69c I I i C1 �(o 6 c 4 --I P II- 1sc ` oz �-b 12�52/ � i 1• Ji J V—)V's Z Sc 7 — `/ 33 -7 28 5 s ;� 1a 5 s i • O _ 9 rh le.�� ilo dl z — Wo �� �1•3 — Ill Q�� 1 AA- .-1 C :1 _ Jsc _4 . f / 441 ��ts� 63oCE I ErD �0, o 1 / 3 5 .5 6—)5', /Ito L.J. -C-1 w �� Vw � ' 521f�o6,,:, '? Li % (n%/o /; Z it 0Am r �II _2 zqq [. 5 - Ll 75 0. o vo1 � 2 ' A-7 2, �iGco A-0 Y oo liv-ci ot (0) t p per., 1te40 2��5 -G p t � c.FF JSC Appendix D Laboratory Analytical Reports and Chains of Custody O �FaceAnalXical o National Center for Testing & Innovation r Ad ANALYTICAL REPORT January 15, 2019 Withers & Ravenel Eng. - Standard Sample Delivery Group: L1060257 Samples Received: 01/11/2019 Project Number: 02180643.01 Description: Wheat Fields Development Report To: Laura Elliott 115 MacKenan Drive Cary, NC 27511 Entire Report Reviewed By: 4�41 Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. V F# 4 + � k dk_ U I & 4b TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1 Fn Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 6 Sr: Sample Results 7 FS SB-5 16-17' L1060257-01 7 [Cn] SB-4 15-16' L1060257-02 10 SB-3 16-17' L1060257-03 13 FSr T2SW1 16' L1060257-04 16 T2SW4 16' L1060257-05 19 RC T2SW3 18' L1060257-06 22 �GI T2SW2 12' L1060257-07 25 T1SW4-1 8' L1060257-08 28 rAl T1SW2-1 14' L1060257-09 31 T1SW3-1 20' L1060257-10 34 FSC T1SW1 2' L1060257-11 37 Qc: Quality Control Summary 40 Total Solids by Method 2540 G-2011 40 Mercury by Method 7471B 43 Metals (ICP) by Method 6010D 44 Volatile Organic Compounds (GC/MS) by Method 8260B 45 Semi Volatile Organic Compounds (GC/MS) by Method 8270D 50 GI: Glossary of Terms 54 Al: Accreditations & Locations 55 Sc: Sample Chain of Custody 56 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 2 of 57 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time S13-5 16-17' L1060257-01 Solid Laura Elliott 01/08/1909:00 01/11/1908:45 FP1 Method Batch Dilution Preparation Analysis Analyst date/time date/time FTC Total Solids by Method 2540 G-2011 WG1222495 1 01/14/19 08:06 01/14/19 08:19 KDW Mercury by Method 7471B WG1223174 1 01/14/1913:01 01/14/1916:21 TCT Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1911:23 TRB Volatile Organic Compounds (GC/MS) by Method 8260B WG1222924 1.08 01/11/19 23:11 01/13/1915:44 DWR Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 06:47 AO [Cn] Collected by Collected date/time Received date/time FSr SB-4 15-16 L1060257-02 SolidLaura Elliott 01/08/19 09:50 01/11/19 08:45 Method Batch Dilution Preparation Analysis Analyst RCdate/time date/time Total Solids by Method 2540 G-2011 WG1222495 1 01/14/19 08:06 01/14/19 08:19 KDW Mercury by Method 7471E WG1223174 1 01/14/1913:01 01/14/1916:23 TCT GI Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1911:48 TRB Volatile Organic Compounds (GC/MS) by Method 8260E WG1222924 1 01/11/19 23:11 01/13/1916:04 DWR FAI Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 07:09 AO FSC Collected by Collected date/time Received date/time S13-3 16-17' L1060257-03 Solid Laura Elliott 01/08/1911:15 01/11/1908:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1222495 1 01/14/19 08:06 01/14/19 08:19 KDW Mercury by Method 7471B WG1223174 1 01/14/1913:01 01/14/1916:26 TCT Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1911:51 TRB Volatile Organic Compounds (GC/MS) by Method 8260B WG1222924 1 01/11/19 23:11 01/13/1916:24 DWR Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 03:43 AO Collected by Collected date/time Received date/time T2SW1 16' L1060257-04 Solid Laura Elliott 01/09/1910:00 01/11/1908:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1222495 1 01/14/19 08:06 01/14/19 08:19 KDW Mercury by Method 7471E WG1223174 1 01/14/1913:01 01/14/1916:28 TCT Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1911:53 TRB Volatile Organic Compounds (GC/MS) by Method 8260E WG1222924 1 01/11/19 23:11 01/13/1916:43 DWR Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 04:06 AO Collected by Collected date/time Received date/time T2SW4 16' L1060257-05 Solid Laura Elliott 01/09/1910:10 01/11/1908:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1223031 1 01/14/19 07:39 01/14/19 07:52 JD Mercury by Method 7471B WG1223174 1 01/14/1913:01 01/14/1916:31 TCT Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1911:56 TRB Volatile Organic Compounds (GC/MS) by Method 8260B WG1222924 1 01/11/19 23:11 01/13/1917:03 DWR Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 04:29 AO ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 3 of 57 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time T2SW3 18' L1060257-06 Solid Laura Elliott 01/09/1910:15 01/11/1908:45 FP1 Method Batch Dilution Preparation Analysis Analyst date/time date/time FTC Total Solids by Method 2540 G-2011 WG1223031 1 01/14/19 07:39 01/14/19 07:52 JD Mercury by Method 7471B WG1223174 1 01/14/1913:01 01/14/1916:33 TCT Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1911:59 TRB Volatile Organic Compounds (GC/MS) by Method 8260B WG1222924 1.04 01/11/19 23:11 01/13/1917:23 DWR Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 04:52 AO [Cn] Collected by Collected date/time Received date/time FSr T2SW2 12 L1060257-07 SolidLaura Elliott 01/09/1910:25 01/11/19 08:45 Method Batch Dilution Preparation Analysis Analyst RCdate/time date/time Total Solids by Method 2540 G-2011 WG1223031 1 01/14/19 07:39 01/14/19 07:52 JD Mercury by Method 7471E WG1223174 1 01/14/1913:01 01/14/1916:36 TCT GI Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1912:02 TRB Volatile Organic Compounds (GC/MS) by Method 8260E WG1222924 1 01/11/19 23:11 01/13/1917:42 DWR FAI Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 05:15 AO FSC Collected by Collected date/time Received date/time T1SW4-1 8' L1060257-08 Solid Laura Elliott 01/09/1915:35 01/11/1908:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1223031 1 01/14/19 07:39 01/14/19 07:52 JD Mercury by Method 7471B WG1223174 1 01/14/1913:01 01/14/1916:38 TCT Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1912:04 TRB Volatile Organic Compounds (GC/MS) by Method 8260B WG1222924 8 01/11/19 23:11 01/13/19 20:20 JHH Volatile Organic Compounds (GC/MS) by Method 8260B WG1223188 200 01/11/19 23:11 01/15/19 00:10 JHH Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 07:32 AO Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 20 01/13/19 22:19 01/14/1911:46 AO Collected by Collected date/time Received date/time T1SW2-1 14' L1060257-09 Solid Laura Elliott 01/09/1915:45 01/11/1908:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1223031 1 01/14/19 07:39 01/14/19 07:52 JD Mercury by Method 7471E WG1223174 1 01/14/1913:01 01/14/1916:41 TCT Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1912:07 TRB Volatile Organic Compounds (GC/MS) by Method 8260E WG1222924 1 01/11/19 23:11 01/13/1918:01 DWR Volatile Organic Compounds (GC/MS) by Method 8260E WG1223188 40 01/11/19 23:11 01/15/19 00:31 JHH Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 05:38 AO Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 20 01/13/19 22:19 01/14/1911:00 AO Collected by Collected date/time Received date/time T1SW3-1 20' L1060257-10 Solid Laura Elliott 01/09/1915:50 01/11/1908:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1223031 1 01/14/19 07:39 01/14/19 07:52 JD Mercury by Method 7471E WG1223174 1 01/14/1913:01 01/14/1916:44 TCT Metals (ICP) by Method 6010D WG1222487 1 01/12/19 09:00 01/12/1912:10 TRB Volatile Organic Compounds (GC/MS) by Method 8260B WG1222924 1 01/11/19 23:11 01/13/1918:21 DWR Volatile Organic Compounds (GC/MS) by Method 8260B WG1223188 20 01/11/19 23:11 01/15/19 00:51 JHH Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 1 01/13/19 22:19 01/14/19 06:01 AO Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222614 10 01/13/19 22:19 01/14/1911:23 AO ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 4 of 57 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time T1SW1 2' L1060257-11 Solid Laura Elliott 01/09/1916:00 01/11/1908:45 C P Method Total Solids by Method 2540 G-2011 Mercury by Method 7471B Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260B Volatile Organic Compounds (GC/MS) by Method 8260B Semi Volatile Organic Compounds (GC/MS) by Method 8270D Batch WG1223079 WG1223174 WG1222487 WG1222924 WG1223188 WG1222614 Dilution Preparation date/time 1 01/14/19 09:51 1 01/14/1913:01 1 01/12/19 09:00 1 01/11/19 23:11 1 01/11/19 23:11 1 01/13/19 22:19 Analysis Analyst date/time 01/14/1910:02 01/14/1916:51 01/12/1912:13 01/13/1918:41 01/14/19 23:09 01/14/19 06:24 KDW TCT TRB DWR JHH AO FTC M [Cn] FSr RC F, FAI FSC ACCOUNT: PROJECT: SDG: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 DATE/TIME: 01/15/19 14:54 PAGE: 5 of 57 CASE NARRATIVE ONE LAB. NATIONWIDE. FP1 All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. FSr FC-1 4�j �GI Heather J Wagner FAI Project Manager FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 6 of 57 SB-5 16-17' SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 01/08/19 09:00 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 92.6 1 01/14/2019 08:19 WG1222495 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time [Cn] Mercury ND 0.0216 1 01/14/201916:21 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.16 1 01/12/201911:23 WG1222487 Barium 76.8 0.540 1 01/12/201911:23 WG1222487 7G1 Cadmium ND 0.540 1 01/12/201911:23 WG1222487 Chromium 13.9 1.08 1 01/12/201911:23 WG1222487 Lead 4.43 0.540 1 01/12/201911:23 WG1222487 FAI Selenium ND 2.16 1 01/12/201911:23 WG1222487 Silver ND 1.08 1 01/12/201911:23 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone 0.0293 B 0.0292 1.08 01/13/201915:44 WG1222924 Acrylonitrile ND 0.0146 1.08 01/13/201915:44 WG1222924 Benzene ND 0.00117 1.08 01/13/201915:44 WG1222924 Bromobenzene ND 0.0146 1.08 01/13/201915:44 WG1222924 Bromodichloromethane ND 0.00292 1.08 01/13/201915:44 WG1222924 Bromoform ND J4 0.0292 1.08 01/13/201915:44 WG1222924 Bromomethane ND 0.0146 1.08 01/13/201915:44 WG1222924 n-Butylbenzene ND 0.0146 1.08 01/13/201915:44 WG1222924 sec -Butyl benzene ND 0.0146 1.08 01/13/201915:44 WG1222924 ter[-Butylbenzene ND 0.00583 1.08 01/13/201915:44 WG1222924 Carbon tetrachloride ND 0.00583 1.08 01/13/201915:44 WG1222924 Chlorobenzene ND 0.00292 1.08 01/13/201915:44 WG1222924 Chlorodibromomethane ND 0.00292 1.08 01/13/201915:44 WG1222924 Chloroethane ND 0.00583 1.08 01/13/201915:44 WG1222924 Chloroform ND 0.00292 1.08 01/13/201915:44 WG1222924 Chloromethane ND 0.0146 1.08 01/13/201915:44 WG1222924 2-Chlorotoluene ND 0.00292 1.08 01/13/201915:44 WG1222924 4-Chlorotoluene ND 0.00583 1.08 01/13/201915:44 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0292 1.08 01/13/201915:44 WG1222924 1,2-Dibromoethane ND 0.00292 1.08 01/13/201915:44 WG1222924 Dibromomethane ND 0.00583 1.08 01/13/201915:44 WG1222924 1,2-Dichlorobenzene ND 0.00583 1.08 01/13/201915:44 WG1222924 1,3-Dichlorobenzene ND 0.00583 1.08 01/13/201915:44 WG1222924 1,4-Dichlorobenzene ND 0.00583 1.08 01/13/201915:44 WG1222924 Dichlorodifluoromethane ND 0.00292 1.08 01/13/201915:44 WG1222924 1,1-Dichloroethane ND 0.00292 1.08 01/13/201915:44 WG1222924 1,2-Dichloroethane ND 0.00292 1.08 01/13/201915:44 WG1222924 1,1-Dichloroethene ND 0.00292 1.08 01/13/201915:44 WG1222924 cis-1,2-Dichloroethene ND 0.00292 1.08 01/13/201915:44 WG1222924 trans-1,2-Dichloroethene ND 0.00583 1.08 01/13/201915:44 WG1222924 1,2-Dichloropropane ND 0.00583 1.08 01/13/201915:44 WG1222924 1,1-Dichloropropene ND 0.00292 1.08 01/13/201915:44 WG1222924 1,3-Dichloropropane ND 0.00583 1.08 01/13/201915:44 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 7 of 57 SB-5 16-17' SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 01/08/19 09:00 L1060257 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch FP1 Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00292 1.08 01/13/201915:44 WG1222924 FTc trans-1,3-Dichloropropene ND 0.00583 1.08 01/13/201915:44 WG1222924 2,2-Dichloropropane ND 0.00292 1.08 01/13/201915:44 WG1222924 Di -isopropyl ether ND 0.00117 1.08 01/13/201915:44 WG1222924 FSS Ethylbenzene ND 0.00292 1.08 01/13/201915:44 WG1222924 Hexachloro-1,3-butadiene ND 0.0292 1.08 01/13/201915:44 WG1222924 rCn Isopropylbenzene ND 0.00292 1.08 01/13/201915:44 WG1222924 p-Isopropyltoluene ND 0.00583 1.08 01/13/201915:44 WG1222924 2-Butanone (MEK) ND 0.0292 1.08 01/13/201915:44 WG1222924 Methylene Chloride ND 0.0292 1.08 01/13/201915:44 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0292 1.08 01/13/201915:44 WG1222924 Fc Methyl tert-butyl ether ND 0.00117 1.08 01/13/201915:44 WG1222924 Naphthalene ND 0.0146 1.08 01/13/201915:44 WG1222924 n-Propylbenzene ND 0.00583 1.08 01/13/201915:44 WG1222924 GI Styrene ND 0.0146 1.08 01/13/201915:44 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00292 1.08 01/13/201915:44 WG1222924 FAI 1,1,2,2-Tetrachloroethane ND 0.00292 1.08 01/13/201915:44 WG1222924 Tetrachloroethene ND 0.00292 1.08 01/13/201915:44 WG1222924 Toluene ND 0.00583 1.08 01/13/201915:44 WG1222924 FSC 1,2,3-Trichlorobenzene ND 0.00292 1.08 01/13/201915:44 WG1222924 1,2,4-Trichlorobenzene ND 0.0146 1.08 01/13/201915:44 WG1222924 1,1,1-Trichloroethane ND 0.00292 1.08 01/13/201915:44 WG1222924 1,1,2-Trichloroethane ND 0.00292 1.08 01/13/201915:44 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00292 1.08 01/13/201915:44 WG1222924 Trichloroethene ND 0.00117 1.08 01/13/201915:44 WG1222924 Trichlorofluoromethane ND 0.00292 1.08 01/13/201915:44 WG1222924 1,2,3-Trichloropropane ND 0.0146 1.08 01/13/201915:44 WG1222924 1,2,4-Trimethylbenzene ND 0.00583 1.08 01/13/201915:44 WG1222924 1,3,5-Trimethyl benzene ND 0.00583 1.08 01/13/201915:44 WG1222924 Vinyl chloride ND 0.00292 1.08 01/13/201915:44 WG1222924 Xylenes, Total ND 0.00758 1.08 01/13/201915:44 WG1222924 (S Toluene-d8 109 75.0-131 011131201915.44 WG1222924 (S Dibromofluoromethane 91.6 65.0-129 011131201915.44 WG1222924 (S 4-Bromof/uorobenzene 99.0 67.0-138 011131201915.44 WG1222924 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0360 1 01/14/2019 06:47 WG1222614 Acenaphthylene ND 0.0360 1 01/14/2019 06:47 WG1222614 Anthracene ND 0.0360 1 01/14/2019 06:47 WG1222614 Benzidine ND J4 0.360 1 01/14/2019 06:47 WG1222614 Benzo(a)anth race ne ND 0.0360 1 01/14/2019 06:47 WG1222614 Benzo(b)fluoranthene ND 0.0360 1 01/14/2019 06:47 WG1222614 Benzo(k)fluoranthene ND 0.0360 1 01/14/2019 06:47 WG1222614 Benzo(g,h,i)perylene ND 0.0360 1 01/14/2019 06:47 WG1222614 Benzo(a)pyrene ND 0.0360 1 01/14/2019 06:47 WG1222614 Bis(2-chlorethoxy)methane ND 0.360 1 01/14/2019 06:47 WG1222614 Bis(2-chloroethyl)ether ND 0.360 1 01/14/2019 06:47 WG1222614 Bis(2-chloroisopropyl)ether ND 0.360 1 01/14/2019 06:47 WG1222614 4-Bromophenyl-phenylether ND 0.360 1 01/14/2019 06:47 WG1222614 2-Chloronaphthalene ND 0.0360 1 01/14/2019 06:47 WG1222614 4-Chlorophenyl-phenylether ND 0.360 1 01/14/2019 06:47 WG1222614 Chrysene ND 0.0360 1 01/14/2019 06:47 WG1222614 Dibenz(a,h)anthracene ND 0.0360 1 01/14/2019 06:47 WG1222614 3,3-Dichlorobenzidine ND 0.360 1 01/14/2019 06:47 WG1222614 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 8 of 57 ONE LAB. NATIONWIDE. SB-5 16-17' SAMPLE RESULTS - 01 Collected date/time: 01/08/19 09:00 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Analyte 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene HexachIoro-1,3-butadiene HexachIorocyclopentadiene Hexachloroethane Ind eno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-N itros o d i-n-p ro pyl a mine Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result (dry) mg/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 63.7 58.1 45.5 51.3 56.2 56.7 Qualifier RDL (dry) Dilution Analysis Batch mg/kg date / time 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.0360 1 01/14/2019 06:47 WG1222614 0.0360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 J0 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.0360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.0360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.0360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.0360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 0.360 1 01/14/2019 06:47 WG1222614 12.0-120 0111412019 06.47 WG1222614 10.0-120 0111412019 06.47 WG1222614 10.0-122 0111412019 06.47 WG1222614 15.0-120 0111412019 06.47 WG1222614 10.0-127 0111412019 06.47 WG1222614 10.0-120 0111412019 06.47 WG1222614 FP FTc FS Fn FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 9 of 57 SB-4 15-16' SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 01/08/19 09:50 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 88.0 1 01/14/2019 08:19 WG1222495 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 4 CCl Mercury 0.0241 B 0.0227 1 01/14/201916:23 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.27 1 01/12/201911:48 WG1222487 Barium 76.4 0.568 1 01/12/201911:48 WG1222487 7G1 Cadmium ND 0.568 1 01/12/201911:48 WG1222487 Chromium 6.36 1.14 1 01/12/201911:48 WG1222487 Lead 11.9 0.568 1 01/12/201911:48 WG1222487 FAI Selenium ND 2.27 1 01/12/201911:48 WG1222487 Silver ND 1.14 1 01/12/201911:48 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0284 1 01/13/201916:04 WG1222924 Acrylonitrile ND 0.0142 1 01/13/201916:04 WG1222924 Benzene ND 0.00114 1 01/13/201916:04 WG1222924 Bromobenzene ND 0.0142 1 01/13/201916:04 WG1222924 Bromodichloromethane ND 0.00284 1 01/13/201916:04 WG1222924 Bromoform ND J4 0.0284 1 01/13/201916:04 WG1222924 Bromomethane ND 0.0142 1 01/13/201916:04 WG1222924 n-Butylbenzene ND 0.0142 1 01/13/201916:04 WG1222924 sec -Butyl benzene ND 0.0142 1 01/13/201916:04 WG1222924 ter[-Butylbenzene ND 0.00568 1 01/13/201916:04 WG1222924 Carbon tetrachloride ND 0.00568 1 01/13/201916:04 WG1222924 Chlorobenzene ND 0.00284 1 01/13/201916:04 WG1222924 Chlorodibromomethane ND 0.00284 1 01/13/201916:04 WG1222924 Chloroethane ND 0.00568 1 01/13/201916:04 WG1222924 Chloroform ND 0.00284 1 01/13/201916:04 WG1222924 Chloromethane ND 0.0142 1 01/13/201916:04 WG1222924 2-Chlorotoluene ND 0.00284 1 01/13/201916:04 WG1222924 4-Chlorotoluene ND 0.00568 1 01/13/201916:04 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0284 1 01/13/201916:04 WG1222924 1,2-Dibromoethane ND 0.00284 1 01/13/201916:04 WG1222924 Dibromomethane ND 0.00568 1 01/13/201916:04 WG1222924 1,2-Dichlorobenzene ND 0.00568 1 01/13/201916:04 WG1222924 1,3-Dichlorobenzene ND 0.00568 1 01/13/201916:04 WG1222924 1,4-Dichlorobenzene ND 0.00568 1 01/13/201916:04 WG1222924 Dichlorodifluoromethane ND 0.00284 1 01/13/201916:04 WG1222924 1,1-Dichloroethane ND 0.00284 1 01/13/201916:04 WG1222924 1,2-Dichloroethane ND 0.00284 1 01/13/201916:04 WG1222924 1,1-Dichloroethene ND 0.00284 1 01/13/201916:04 WG1222924 cis-1,2-Dichloroethene ND 0.00284 1 01/13/201916:04 WG1222924 trans-1,2-Dichloroethene ND 0.00568 1 01/13/201916:04 WG1222924 1,2-Dichloropropane ND 0.00568 1 01/13/201916:04 WG1222924 1,1-Dichloropropene ND 0.00284 1 01/13/201916:04 WG1222924 1,3-Dichloropropane ND 0.00568 1 01/13/201916:04 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 10 of 57 SB-4 15-16' SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 01/08/19 09:50 L1060257 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch FP1 Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00284 1 01/13/201916:04 WG1222924 FTc trans-1,3-Dichloropropene ND 0.00568 1 01/13/201916:04 WG1222924 2,2-Dichloropropane ND 0.00284 1 01/13/201916:04 WG1222924 Di -isopropyl ether ND 0.00114 1 01/13/201916:04 WG1222924 FSS Ethylbenzene ND 0.00284 1 01/13/201916:04 WG1222924 Hexachloro-1,3-butadiene ND 0.0284 1 01/13/201916:04 WG1222924 rCn Isopropylbenzene ND 0.00284 1 01/13/201916:04 WG1222924 p-Isopropyltoluene ND 0.00568 1 01/13/201916:04 WG1222924 2-Butanone (MEK) ND 0.0284 1 01/13/201916:04 WG1222924 Methylene Chloride ND 0.0284 1 01/13/201916:04 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0284 1 01/13/201916:04 WG1222924 Fc Methyl tert-butyl ether ND 0.00114 1 01/13/201916:04 WG1222924 Naphthalene ND 0.0142 1 01/13/201916:04 WG1222924 n-Propylbenzene ND 0.00568 1 01/13/201916:04 WG1222924 GI Styrene ND 0.0142 1 01/13/201916:04 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00284 1 01/13/201916:04 WG1222924 FAI 1,1,2,2-Tetrachloroethane ND 0.00284 1 01/13/201916:04 WG1222924 Tetrachloroethene ND 0.00284 1 01/13/201916:04 WG1222924 Toluene ND 0.00568 1 01/13/201916:04 WG1222924 FSC 1,2,3-Trichlorobenzene ND 0.00284 1 01/13/201916:04 WG1222924 1,2,4-Trichlorobenzene ND 0.0142 1 01/13/201916:04 WG1222924 1,1,1-Trichloroethane ND 0.00284 1 01/13/201916:04 WG1222924 1,1,2-Trichloroethane ND 0.00284 1 01/13/201916:04 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00284 1 01/13/201916:04 WG1222924 Trichloroethene ND 0.00114 1 01/13/201916:04 WG1222924 Trichlorofluoromethane ND 0.00284 1 01/13/201916:04 WG1222924 1,2,3-Trichloropropane ND 0.0142 1 01/13/201916:04 WG1222924 1,2,4-Trimethylbenzene ND 0.00568 1 01/13/201916:04 WG1222924 1,3,5-Trimethyl benzene ND 0.00568 1 01/13/201916:04 WG1222924 Vinyl chloride ND 0.00284 1 01/13/201916:04 WG1222924 Xylenes, Total ND 0.00739 1 01/13/201916:04 WG1222924 (S Toluene-d8 109 75.0-131 011131201916:04 WG1222924 (S) Dibromofluoromethane 92.5 65.0-129 011131201916:04 WG1222924 (S 4-Bromof/uorobenzene 98.5 67.0-138 011131201916:04 WG1222924 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0378 1 01/14/2019 07:09 WG1222614 Acenaphthylene ND 0.0378 1 01/14/2019 07:09 WG1222614 Anthracene ND 0.0378 1 01/14/2019 07:09 WG1222614 Benzidine ND J4 0.378 1 01/14/2019 07:09 WG1222614 Benzo(a)anth race ne ND 0.0378 1 01/14/2019 07:09 WG1222614 Benzo(b)fluoranthene ND 0.0378 1 01/14/2019 07:09 WG1222614 Benzo(k)fluoranthene ND 0.0378 1 01/14/2019 07:09 WG1222614 Benzo(g,h,i)perylene ND 0.0378 1 01/14/2019 07:09 WG1222614 Benzo(a)pyrene ND 0.0378 1 01/14/2019 07:09 WG1222614 Bis(2-chlorethoxy)methane ND 0.378 1 01/14/2019 07:09 WG1222614 Bis(2-chloroethyl)ether ND 0.378 1 01/14/2019 07:09 WG1222614 Bis(2-chloroisopropyl)ether ND 0.378 1 01/14/2019 07:09 WG1222614 4-Bromophenyl-phenylether ND 0.378 1 01/14/2019 07:09 WG1222614 2-Chloronaphthalene ND 0.0378 1 01/14/2019 07:09 WG1222614 4-Chlorophenyl-phenylether ND 0.378 1 01/14/2019 07:09 WG1222614 Chrysene ND 0.0378 1 01/14/2019 07:09 WG1222614 Dibenz(a,h)anthracene ND 0.0378 1 01/14/2019 07:09 WG1222614 3,3-Dichlorobenzidine ND 0.378 1 01/14/2019 07:09 WG1222614 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 11 of 57 ONE LAB. NATIONWIDE. SB-4 15-16' SAMPLE RESULTS - 02 Collected date/time: 01/08/19 09:50 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Analyte 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene HexachIoro-1,3-butadiene HexachIorocyclopentadiene Hexachloroethane Ind eno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-N itros o d i-n-p ro pyl a mine Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result (dry) mg/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 58.7 53.4 33.0 48.9 52.0 52.6 Qualifier RDL (dry) mg/kg Dilution Analysis date / time Batch 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.0378 1 01/14/2019 07:09 WG1222614 0.0378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 J0 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.0378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.0378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.0378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.0378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 0.378 1 01/14/2019 07:09 WG1222614 12.0-120 0111412019 07:09 WG1222614 10.0-120 0111412019 07:09 WG1222614 10.0-122 0111412019 07:09 WG1222614 15.0-120 0111412019 07:09 WG1222614 10.0-127 0111412019 07:09 WG1222614 10.0-120 0111412019 07:09 WG1222614 FP FTc FS Fn FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 12 of 57 SB-3 16-17' SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 01/08/19 11:15 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 88.3 1 01/14/2019 08:19 WG1222495 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time [Cn] Mercury ND 0.0226 1 01/14/201916:26 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.26 1 01/12/201911:51 WG1222487 Barium 191 0.566 1 01/12/201911:51 WG1222487 7G1 Cadmium ND 0.566 1 01/12/201911:51 WG1222487 Chromium 2.66 1.13 1 01/12/201911:51 WG1222487 Lead 10.6 0.566 1 01/12/201911:51 WG1222487 FAI Selenium ND 2.26 1 01/12/201911:51 WG1222487 Silver ND 1.13 1 01/12/201911:51 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0283 1 01/13/201916:24 WG1222924 Acrylonitrile ND 0.0142 1 01/13/201916:24 WG1222924 Benzene ND 0.00113 1 01/13/201916:24 WG1222924 Bromobenzene ND 0.0142 1 01/13/201916:24 WG1222924 Bromodichloromethane ND 0.00283 1 01/13/201916:24 WG1222924 Bromoform ND J4 0.0283 1 01/13/201916:24 WG1222924 Bromomethane ND 0.0142 1 01/13/201916:24 WG1222924 n-Butylbenzene ND 0.0142 1 01/13/201916:24 WG1222924 sec -Butyl benzene ND 0.0142 1 01/13/201916:24 WG1222924 ter[-Butylbenzene ND 0.00566 1 01/13/201916:24 WG1222924 Carbon tetrachloride ND 0.00566 1 01/13/201916:24 WG1222924 Chlorobenzene ND 0.00283 1 01/13/201916:24 WG1222924 Chlorodibromomethane ND 0.00283 1 01/13/201916:24 WG1222924 Chloroethane ND 0.00566 1 01/13/201916:24 WG1222924 Chloroform ND 0.00283 1 01/13/201916:24 WG1222924 Chloromethane ND 0.0142 1 01/13/201916:24 WG1222924 2-Chlorotoluene ND 0.00283 1 01/13/201916:24 WG1222924 4-Chlorotoluene ND 0.00566 1 01/13/201916:24 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0283 1 01/13/201916:24 WG1222924 1,2-Dibromoethane ND 0.00283 1 01/13/201916:24 WG1222924 Dibromomethane ND 0.00566 1 01/13/201916:24 WG1222924 1,2-Dichlorobenzene ND 0.00566 1 01/13/201916:24 WG1222924 1,3-Dichlorobenzene ND 0.00566 1 01/13/201916:24 WG1222924 1,4-Dichlorobenzene ND 0.00566 1 01/13/201916:24 WG1222924 Dichlorodifluoromethane ND 0.00283 1 01/13/201916:24 WG1222924 1,1-Dichloroethane ND 0.00283 1 01/13/201916:24 WG1222924 1,2-Dichloroethane ND 0.00283 1 01/13/201916:24 WG1222924 1,1-Dichloroethene ND 0.00283 1 01/13/201916:24 WG1222924 cis-1,2-Dichloroethene ND 0.00283 1 01/13/201916:24 WG1222924 trans-1,2-Dichloroethene ND 0.00566 1 01/13/201916:24 WG1222924 1,2-Dichloropropane ND 0.00566 1 01/13/201916:24 WG1222924 1,1-Dichloropropene ND 0.00283 1 01/13/201916:24 WG1222924 1,3-Dichloropropane ND 0.00566 1 01/13/201916:24 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 13 of 57 ONE LAB. NATIONWIDE. SB-3 16-17' SAMPLE RESULTS - 03 Collected date/time: 01/08/19 11:15 L1060257 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00283 1 01/13/201916:24 WG1222924 trans-1,3-Dichloropropene ND 0.00566 1 01/13/201916:24 WG1222924 2,2-Dichloropropane ND 0.00283 1 01/13/201916:24 WG1222924 Di -isopropyl ether ND 0.00113 1 01/13/201916:24 WG1222924 Ethylbenzene ND 0.00283 1 01/13/201916:24 WG1222924 Hexachloro-1,3-butadiene ND 0.0283 1 01/13/201916:24 WG1222924 Isopropylbenzene ND 0.00283 1 01/13/201916:24 WG1222924 p-Isopropyltoluene ND 0.00566 1 01/13/201916:24 WG1222924 2-Butanone (MEK) ND 0.0283 1 01/13/201916:24 WG1222924 Methylene Chloride ND 0.0283 1 01/13/201916:24 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0283 1 01/13/201916:24 WG1222924 Methyl tert-butyl ether ND 0.00113 1 01/13/201916:24 WG1222924 Naphthalene ND 0.0142 1 01/13/201916:24 WG1222924 n-Propylbenzene ND 0.00566 1 01/13/201916:24 WG1222924 Styrene ND 0.0142 1 01/13/201916:24 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00283 1 01/13/201916:24 WG1222924 1,1,2,2-Tetrachloroethane ND 0.00283 1 01/13/201916:24 WG1222924 Tetrachloroethene ND 0.00283 1 01/13/201916:24 WG1222924 Toluene ND 0.00566 1 01/13/201916:24 WG1222924 1,2,3-Trichlorobenzene ND 0.00283 1 01/13/201916:24 WG1222924 1,2,4-Trichlorobenzene ND 0.0142 1 01/13/201916:24 WG1222924 1,1,1-Trichloroethane ND 0.00283 1 01/13/201916:24 WG1222924 1,1,2-Trichloroethane ND 0.00283 1 01/13/201916:24 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00283 1 01/13/201916:24 WG1222924 Trichloroethene ND 0.00113 1 01/13/201916:24 WG1222924 Trichlorofluoromethane ND 0.00283 1 01/13/201916:24 WG1222924 1,2,3-Trichloropropane ND 0.0142 1 01/13/201916:24 WG1222924 1,2,4-Trimethylbenzene ND 0.00566 1 01/13/201916:24 WG1222924 1,3,5-Trimethyl benzene ND 0.00566 1 01/13/201916:24 WG1222924 Vinyl chloride ND 0.00283 1 01/13/201916:24 WG1222924 Xylenes, Total ND 0.00736 1 01/13/201916:24 WG1222924 (S) Toluene-d8 108 75.0-131 011131201916:24 WG1222924 (S) Dibromofluoromethane 93.4 65.0-129 011131201916:24 WG1222924 (S) 4-Bromof/uorobenzene 99.5 67.0-138 011131201916:24 WG1222924 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0377 1 01/14/2019 03:43 WG1222614 Acenaphthylene ND 0.0377 1 01/14/2019 03:43 WG1222614 Anthracene ND 0.0377 1 01/14/2019 03:43 WG1222614 Benzidine ND J4 0.377 1 01/14/2019 03:43 WG1222614 Benzo(a)anth race ne ND 0.0377 1 01/14/2019 03:43 WG1222614 Benzo(b)fluoranthene ND 0.0377 1 01/14/2019 03:43 WG1222614 Benzo(k)fluoranthene ND 0.0377 1 01/14/2019 03:43 WG1222614 Benzo(g,h,i)perylene ND 0.0377 1 01/14/2019 03:43 WG1222614 Benzo(a)pyrene ND 0.0377 1 01/14/2019 03:43 WG1222614 Bis(2-chlorethoxy)methane ND 0.377 1 01/14/2019 03:43 WG1222614 Bis(2-chloroethyl)ether ND 0.377 1 01/14/2019 03:43 WG1222614 Bis(2-chloroisopropyl)ether ND 0.377 1 01/14/2019 03:43 WG1222614 4-Bromophenyl-phenylether ND 0.377 1 01/14/2019 03:43 WG1222614 2-Chloronaphthalene ND 0.0377 1 01/14/2019 03:43 WG1222614 4-Chlorophenyl-phenylether ND 0.377 1 01/14/2019 03:43 WG1222614 Chrysene ND 0.0377 1 01/14/2019 03:43 WG1222614 Dibenz(a,h)anthracene ND 0.0377 1 01/14/2019 03:43 WG1222614 3,3-Dichlorobenzidine ND 0.377 1 01/14/2019 03:43 WG1222614 FP1 FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 14 of 57 ONE LAB. NATIONWIDE. SB-3 16-17' SAMPLE RESULTS - 03 Collected date/time: 01/08/19 11:15 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Analyte 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene HexachIoro-1,3-butadiene HexachIorocyclopentadiene Hexachloroethane Ind eno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-N itros o d i-n-p ro pyl a mine Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result (dry) mg/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 56.4 51.2 51.8 46.1 49.5 50.9 Qualifier RDL (dry) mg/kg Dilution Analysis date / time Batch 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.0377 1 01/14/2019 03:43 WG1222614 0.0377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 J0 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.0377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.0377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.0377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.0377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 0.377 1 01/14/2019 03:43 WG1222614 12.0-120 0111412019 03.43 WG1222614 10.0-120 0111412019 03:43 WG1222614 10.0-122 0111412019 03.43 WG1222614 15.0-120 0111412019 03.43 WG1222614 10.0-127 0111412019 03.43 WG1222614 10.0-120 0111412019 03.43 WG1222614 FP FTc FS Fn FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 15 of 57 T2SW1 16' SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 01/09/19 10:00 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 91.3 1 01/14/2019 08:19 WG1222495 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time [Cn] Mercury ND 0.0219 1 01/14/201916:28 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.19 1 01/12/201911:53 WG1222487 Barium 85.5 0.548 1 01/12/201911:53 WG1222487 �GI Cadmium ND 0.548 1 01/12/201911:53 WG1222487 Chromium 1.66 1.10 1 01/12/201911:53 WG1222487 Lead 2.68 0.548 1 01/12/201911:53 WG1222487 FAI Selenium ND 2.19 1 01/12/201911:53 WG1222487 Silver ND 1.10 1 01/12/201911:53 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0274 1 01/13/201916:43 WG1222924 Acrylonitrile ND 0.0137 1 01/13/201916:43 WG1222924 Benzene ND 0.00110 1 01/13/201916:43 WG1222924 Bromobenzene ND 0.0137 1 01/13/201916:43 WG1222924 Bromodichloromethane ND 0.00274 1 01/13/201916:43 WG1222924 Bromoform ND J4 0.0274 1 01/13/201916:43 WG1222924 Bromomethane ND 0.0137 1 01/13/201916:43 WG1222924 n-Butylbenzene ND 0.0137 1 01/13/201916:43 WG1222924 sec -Butyl benzene ND 0.0137 1 01/13/201916:43 WG1222924 ter[-Butylbenzene ND 0.00548 1 01/13/201916:43 WG1222924 Carbon tetrachloride ND 0.00548 1 01/13/201916:43 WG1222924 Chlorobenzene ND 0.00274 1 01/13/201916:43 WG1222924 Chlorodibromomethane ND 0.00274 1 01/13/201916:43 WG1222924 Chloroethane ND 0.00548 1 01/13/201916:43 WG1222924 Chloroform ND 0.00274 1 01/13/201916:43 WG1222924 Chloromethane ND 0.0137 1 01/13/201916:43 WG1222924 2-Chlorotoluene ND 0.00274 1 01/13/201916:43 WG1222924 4-Chlorotoluene ND 0.00548 1 01/13/201916:43 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0274 1 01/13/201916:43 WG1222924 1,2-Dibromoethane ND 0.00274 1 01/13/201916:43 WG1222924 Dibromomethane ND 0.00548 1 01/13/201916:43 WG1222924 1,2-Dichlorobenzene ND 0.00548 1 01/13/201916:43 WG1222924 1,3-Dichlorobenzene ND 0.00548 1 01/13/201916:43 WG1222924 1,4-Dichlorobenzene ND 0.00548 1 01/13/201916:43 WG1222924 Dichlorodifluoromethane ND 0.00274 1 01/13/201916:43 WG1222924 1,1-Dichloroethane ND 0.00274 1 01/13/201916:43 WG1222924 1,2-Dichloroethane ND 0.00274 1 01/13/201916:43 WG1222924 1,1-Dichloroethene ND 0.00274 1 01/13/201916:43 WG1222924 cis-1,2-Dichloroethene ND 0.00274 1 01/13/201916:43 WG1222924 trans-1,2-Dichloroethene ND 0.00548 1 01/13/201916:43 WG1222924 1,2-Dichloropropane ND 0.00548 1 01/13/201916:43 WG1222924 1,1-Dichloropropene ND 0.00274 1 01/13/201916:43 WG1222924 1,3-Dichloropropane ND 0.00548 1 01/13/201916:43 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 16 of 57 ONE LAB. NATIONWIDE. T2SW1 16' SAMPLE RESULTS - 04 Collected date/time: 01/09/19 10:00 L1060257 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00274 1 01/13/201916:43 WG1222924 trans-1,3-Dichloropropene ND 0.00548 1 01/13/201916:43 WG1222924 2,2-Dichloropropane ND 0.00274 1 01/13/201916:43 WG1222924 Di -isopropyl ether ND 0.00110 1 01/13/201916:43 WG1222924 Ethylbenzene ND 0.00274 1 01/13/201916:43 WG1222924 Hexachloro-1,3-butadiene ND 0.0274 1 01/13/201916:43 WG1222924 Isopropylbenzene ND 0.00274 1 01/13/201916:43 WG1222924 p-Isopropyltoluene ND 0.00548 1 01/13/201916:43 WG1222924 2-Butanone (MEK) ND 0.0274 1 01/13/201916:43 WG1222924 Methylene Chloride ND 0.0274 1 01/13/201916:43 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0274 1 01/13/201916:43 WG1222924 Methyl tert-butyl ether ND 0.00110 1 01/13/201916:43 WG1222924 Naphthalene ND 0.0137 1 01/13/201916:43 WG1222924 n-Propylbenzene ND 0.00548 1 01/13/201916:43 WG1222924 Styrene ND 0.0137 1 01/13/201916:43 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00274 1 01/13/201916:43 WG1222924 1,1,2,2-Tetrachloroethane ND 0.00274 1 01/13/201916:43 WG1222924 Tetrachloroethene ND 0.00274 1 01/13/201916:43 WG1222924 Toluene ND 0.00548 1 01/13/201916:43 WG1222924 1,2,3-Trichlorobenzene ND 0.00274 1 01/13/201916:43 WG1222924 1,2,4-Trichlorobenzene ND 0.0137 1 01/13/201916:43 WG1222924 1,1,1-Trichloroethane ND 0.00274 1 01/13/201916:43 WG1222924 1,1,2-Trichloroethane ND 0.00274 1 01/13/201916:43 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00274 1 01/13/201916:43 WG1222924 Trichloroethene ND 0.00110 1 01/13/201916:43 WG1222924 Trichlorofluoromethane ND 0.00274 1 01/13/201916:43 WG1222924 1,2,3-Trichloropropane ND 0.0137 1 01/13/201916:43 WG1222924 1,2,4-Trimethylbenzene ND 0.00548 1 01/13/201916:43 WG1222924 1,3,5-Trimethyl benzene ND 0.00548 1 01/13/201916:43 WG1222924 Vinyl chloride ND 0.00274 1 01/13/201916:43 WG1222924 Xylenes, Total ND 0.00712 1 01/13/201916:43 WG1222924 (S) Toluene-d8 109 75.0-131 011131201916.43 WG1222924 (S Dibromofluoromethane 92.1 65.0-129 011131201916.43 WG1222924 (S) 4-Bromof/uorobenzene 110 67.0-138 011131201916.43 WG1222924 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0365 1 01/14/2019 04:06 WG1222614 Acenaphthylene ND 0.0365 1 01/14/2019 04:06 WG1222614 Anthracene ND 0.0365 1 01/14/2019 04:06 WG1222614 Benzidine ND J4 0.365 1 01/14/2019 04:06 WG1222614 Benzo(a)anth race ne ND 0.0365 1 01/14/2019 04:06 WG1222614 Benzo(b)fluoranthene ND 0.0365 1 01/14/2019 04:06 WG1222614 Benzo(k)fluoranthene ND 0.0365 1 01/14/2019 04:06 WG1222614 Benzo(g,h,i)perylene ND 0.0365 1 01/14/2019 04:06 WG1222614 Benzo(a)pyrene ND 0.0365 1 01/14/2019 04:06 WG1222614 Bis(2-chlorethoxy)methane ND 0.365 1 01/14/2019 04:06 WG1222614 Bis(2-chloroethyl)ether ND 0.365 1 01/14/2019 04:06 WG1222614 Bis(2-chloroisopropyl)ether ND 0.365 1 01/14/2019 04:06 WG1222614 4-Bromophenyl-phenylether ND 0.365 1 01/14/2019 04:06 WG1222614 2-Chloronaphthalene ND 0.0365 1 01/14/2019 04:06 WG1222614 4-Chlorophenyl-phenylether ND 0.365 1 01/14/2019 04:06 WG1222614 Chrysene ND 0.0365 1 01/14/2019 04:06 WG1222614 Dibenz(a,h)anthracene ND 0.0365 1 01/14/2019 04:06 WG1222614 3,3-Dichlorobenzidine ND 0.365 1 01/14/2019 04:06 WG1222614 FP1 FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 17 of 57 ONE LAB. NATIONWIDE. T2SW1 16' SAMPLE RESULTS - 04 Collected date/time: 01/09/19 10:00 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Analyte 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene HexachIoro-1,3-butadiene HexachIorocyclopentadiene Hexachloroethane Ind eno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-N itros o d i-n-p ro pyl a mine Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result (dry) mg/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 61.6 55.7 56.6 51.1 54.7 55.0 Qualifier RDL (dry) Dilution Analysis Batch mg/kg date / time 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.0365 1 01/14/2019 04:06 WG1222614 0.0365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 J0 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.0365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.0365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.0365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.0365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 0.365 1 01/14/2019 04:06 WG1222614 12.0-120 0111412019 04:06 WG1222614 10.0-120 0111412019 04:06 WG1222614 10.0-122 0111412019 04:06 WG1222614 15.0-120 0111412019 04:06 WG1222614 10.0-127 0111412019 04:06 WG1222614 10.0-120 0111412019 04:06 WG1222614 FP FTc FS Fn FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 18 of 57 T 2 S W 4 16' SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE. Collected date/time: 01/09/19 10:10 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 86.6 1 01/14/2019 07:52 WG1223031 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time [Cn] Mercury ND 0.0231 1 01/14/201916:31 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.31 1 01/12/201911:56 WG1222487 Barium 85.0 0.577 1 01/12/201911:56 WG1222487 7G1 Cadmium ND 0.577 1 01/12/201911:56 WG1222487 Chromium 13.2 1.15 1 01/12/201911:56 WG1222487 Lead 20.1 0.577 1 01/12/201911:56 WG1222487 FAI Selenium ND 2.31 1 01/12/201911:56 WG1222487 Silver ND 1.15 1 01/12/201911:56 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0289 1 01/13/201917:03 WG1222924 Acrylonitrile ND 0.0144 1 01/13/201917:03 WG1222924 Benzene ND 0.00115 1 01/13/201917:03 WG1222924 Bromobenzene ND 0.0144 1 01/13/201917:03 WG1222924 Bromodichloromethane ND 0.00289 1 01/13/201917:03 WG1222924 Bromoform ND J4 0.0289 1 01/13/201917:03 WG1222924 Bromomethane ND 0.0144 1 01/13/201917:03 WG1222924 n-Butylbenzene ND 0.0144 1 01/13/201917:03 WG1222924 sec -Butyl benzene ND 0.0144 1 01/13/201917:03 WG1222924 ter[-Butylbenzene ND 0.00577 1 01/13/201917:03 WG1222924 Carbon tetrachloride ND 0.00577 1 01/13/201917:03 WG1222924 Chlorobenzene ND 0.00289 1 01/13/201917:03 WG1222924 Chlorodibromomethane ND 0.00289 1 01/13/201917:03 WG1222924 Chloroethane ND 0.00577 1 01/13/201917:03 WG1222924 Chloroform ND 0.00289 1 01/13/201917:03 WG1222924 Chloromethane ND 0.0144 1 01/13/201917:03 WG1222924 2-Chlorotoluene ND 0.00289 1 01/13/201917:03 WG1222924 4-Chlorotoluene ND 0.00577 1 01/13/201917:03 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0289 1 01/13/201917:03 WG1222924 1,2-Dibromoethane ND 0.00289 1 01/13/201917:03 WG1222924 Dibromomethane ND 0.00577 1 01/13/201917:03 WG1222924 1,2-Dichlorobenzene ND 0.00577 1 01/13/201917:03 WG1222924 1,3-Dichlorobenzene ND 0.00577 1 01/13/201917:03 WG1222924 1,4-Dichlorobenzene ND 0.00577 1 01/13/201917:03 WG1222924 Dichlorodifluoromethane ND 0.00289 1 01/13/201917:03 WG1222924 1,1-Dichloroethane ND 0.00289 1 01/13/201917:03 WG1222924 1,2-Dichloroethane ND 0.00289 1 01/13/201917:03 WG1222924 1,1-Dichloroethene ND 0.00289 1 01/13/201917:03 WG1222924 cis-1,2-Dichloroethene ND 0.00289 1 01/13/201917:03 WG1222924 trans-1,2-Dichloroethene ND 0.00577 1 01/13/201917:03 WG1222924 1,2-Dichloropropane ND 0.00577 1 01/13/201917:03 WG1222924 1,1-Dichloropropene ND 0.00289 1 01/13/201917:03 WG1222924 1,3-Dichloropropane ND 0.00577 1 01/13/201917:03 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 19 of 57 T 2 S W 4 16' SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE. Collected date/time: 01/09/19 10:10 L1060257 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch FP1 Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00289 1 01/13/201917:03 WG1222924 FTc trans-1,3-Dichloropropene ND 0.00577 1 01/13/201917:03 WG1222924 2,2-Dichloropropane ND 0.00289 1 01/13/201917:03 WG1222924 Di -isopropyl ether ND 0.00115 1 01/13/201917:03 WG1222924 FSS Ethylbenzene ND 0.00289 1 01/13/201917:03 WG1222924 Hexachloro-1,3-butadiene ND 0.0289 1 01/13/201917:03 WG1222924 rCn Isopropylbenzene ND 0.00289 1 01/13/201917:03 WG1222924 p-Isopropyltoluene ND 0.00577 1 01/13/201917:03 WG1222924 2-Butanone (MEK) ND 0.0289 1 01/13/201917:03 WG1222924 Methylene Chloride ND 0.0289 1 01/13/201917:03 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0289 1 01/13/201917:03 WG1222924 Fc Methyl tert-butyl ether ND 0.00115 1 01/13/201917:03 WG1222924 Naphthalene ND 0.0144 1 01/13/201917:03 WG1222924 7 n-Propylbenzene ND 0.00577 1 01/13/201917:03 WG1222924 GI Styrene ND 0.0144 1 01/13/201917:03 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00289 1 01/13/201917:03 WG1222924 FAI 1,1,2,2-Tetrachloroethane ND 0.00289 1 01/13/201917:03 WG1222924 Tetrachloroethene ND 0.00289 1 01/13/201917:03 WG1222924 Toluene ND 0.00577 1 01/13/201917:03 WG1222924 FSC 1,2,3-Trichlorobenzene ND 0.00289 1 01/13/201917:03 WG1222924 1,2,4-Trichlorobenzene ND 0.0144 1 01/13/201917:03 WG1222924 1,1,1-Trichloroethane ND 0.00289 1 01/13/201917:03 WG1222924 1,1,2-Trichloroethane ND 0.00289 1 01/13/201917:03 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00289 1 01/13/201917:03 WG1222924 Trichloroethene ND 0.00115 1 01/13/201917:03 WG1222924 Trichlorofluoromethane ND 0.00289 1 01/13/201917:03 WG1222924 1,2,3-Trichloropropane ND 0.0144 1 01/13/201917:03 WG1222924 1,2,4-Trimethylbenzene ND 0.00577 1 01/13/201917:03 WG1222924 1,3,5-Trimethyl benzene ND 0.00577 1 01/13/201917:03 WG1222924 Vinyl chloride ND 0.00289 1 01/13/201917:03 WG1222924 Xylenes, Total ND 0.00750 1 01/13/201917:03 WG1222924 (S) Toluene-d8 108 75.0-131 01113120191703 WG1222924 (S) Dibromofluoromethane 94.7 65.0-129 011131201917.-03 WG1222924 (S) 4-Bromof/uorobenzene 108 67.0-138 01113120191703 WG1222924 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0384 1 01/14/2019 04:29 WG1222614 Acenaphthylene ND 0.0384 1 01/14/2019 04:29 WG1222614 Anthracene ND 0.0384 1 01/14/2019 04:29 WG1222614 Benzidine ND J4 0.384 1 01/14/2019 04:29 WG1222614 Benzo(a)anth race ne ND 0.0384 1 01/14/2019 04:29 WG1222614 Benzo(b)fluoranthene ND 0.0384 1 01/14/2019 04:29 WG1222614 Benzo(k)fluoranthene ND 0.0384 1 01/14/2019 04:29 WG1222614 Benzo(g,h,i)perylene ND 0.0384 1 01/14/2019 04:29 WG1222614 Benzo(a)pyrene ND 0.0384 1 01/14/2019 04:29 WG1222614 Bis(2-chlorethoxy)methane ND 0.384 1 01/14/2019 04:29 WG1222614 Bis(2-chloroethyl)ether ND 0.384 1 01/14/2019 04:29 WG1222614 Bis(2-chloroisopropyl)ether ND 0.384 1 01/14/2019 04:29 WG1222614 4-Bromophenyl-phenylether ND 0.384 1 01/14/2019 04:29 WG1222614 2-Chloronaphthalene ND 0.0384 1 01/14/2019 04:29 WG1222614 4-Chlorophenyl-phenylether ND 0.384 1 01/14/2019 04:29 WG1222614 Chrysene ND 0.0384 1 01/14/2019 04:29 WG1222614 Dibenz(a,h)anthracene ND 0.0384 1 01/14/2019 04:29 WG1222614 3,3-Dichlorobenzidine ND 0.384 1 01/14/2019 04:29 WG1222614 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 20 of 57 ONE LAB. NATIONWIDE. T2SW4 16' SAMPLE RESULTS - 05 Collected date/time: 01/09/19 10:10 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Analyte 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene HexachIoro-1,3-butadiene HexachIorocyclopentadiene Hexachloroethane Ind eno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-N itros o d i-n-p ro pyl a mine Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result (dry) mg/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 66.8 60.1 41.9 55.3 58.1 59.9 Qualifier RDL (dry) mg/kg Dilution Analysis date / time Batch 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.0384 1 01/14/2019 04:29 WG1222614 0.0384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 J0 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.0384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.0384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.0384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.0384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 0.384 1 01/14/2019 04:29 WG1222614 12.0-120 0111412019 0419 WG1222614 10.0-120 0111412019 04:29 WG1222614 10.0-122 0111412019 04:29 WG1222614 15.0-120 0111412019 04:29 WG1222614 10.0-127 0111412019 04:29 WG1222614 10.0-120 0111412019 04:29 WG1222614 FP FTc FS Fn FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 21 of 57 SAMPLE RESULTS - 06 L1060257 ONE LAB. NATIONWIDE. T2SW3 18' Collected date/time: 01/09/19 10:15 Total Solids by Method 2540 G-2011 Result Analyte Total Solids 93.5 Mercury by Method 7471B Qualifier Dilution Analysis date / time 1 01/14/2019 07:52 Batch WG1223031 Result (dry) Analyte mg/kg Mercury ND Metals (ICP) by Method 6010D Qualifier RDL (dry) Dilution mg/kg 0.0214 1 Analysis date / time 01/14/201916:33 Batch WG1223174 Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Arsenic ND 2.14 1 01/12/201911:59 WG1222487 Barium 72.5 0.535 1 01/12/201911:59 WG1222487 Cadmium ND 0.535 1 01/12/201911:59 WG1222487 Chromium 1.58 1.07 1 01/12/201911:59 WG1222487 Lead 6.59 0.535 1 01/12/201911:59 WG1222487 Selenium ND 2.14 1 01/12/201911:59 WG1222487 Silver ND 1.07 1 01/12/201911:59 WG1222487 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0278 1.04 01/13/201917:23 WG1222924 Acrylonitrile ND 0.0139 1.04 01/13/201917:23 WG1222924 Benzene ND 0.00111 1.04 01/13/201917:23 WG1222924 Bromobenzene ND 0.0139 1.04 01/13/201917:23 WG1222924 Bromodichloromethane ND 0.00278 1.04 01/13/201917:23 WG1222924 Bromoform ND J4 0.0278 1.04 01/13/201917:23 WG1222924 Bromomethane ND 0.0139 1.04 01/13/201917:23 WG1222924 n-Butylbenzene ND 0.0139 1.04 01/13/201917:23 WG1222924 sec -Butyl benzene ND 0.0139 1.04 01/13/201917:23 WG1222924 ter[-Butylbenzene ND 0.00556 1.04 01/13/201917:23 WG1222924 Carbon tetrachloride ND 0.00556 1.04 01/13/201917:23 WG1222924 Chlorobenzene ND 0.00278 1.04 01/13/201917:23 WG1222924 Chlorodibromomethane ND 0.00278 1.04 01/13/201917:23 WG1222924 Chloroethane ND 0.00556 1.04 01/13/201917:23 WG1222924 Chloroform ND 0.00278 1.04 01/13/201917:23 WG1222924 Chloromethane ND 0.0139 1.04 01/13/201917:23 WG1222924 2-Chlorotoluene ND 0.00278 1.04 01/13/201917:23 WG1222924 4-Chlorotoluene ND 0.00556 1.04 01/13/201917:23 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0278 1.04 01/13/201917:23 WG1222924 1,2-Dibromoethane ND 0.00278 1.04 01/13/201917:23 WG1222924 Dibromomethane ND 0.00556 1.04 01/13/201917:23 WG1222924 1,2-Dichlorobenzene ND 0.00556 1.04 01/13/201917:23 WG1222924 1,3-Dichlorobenzene ND 0.00556 1.04 01/13/201917:23 WG1222924 1,4-Dichlorobenzene ND 0.00556 1.04 01/13/201917:23 WG1222924 Dichlorodifluoromethane ND 0.00278 1.04 01/13/201917:23 WG1222924 1,1-Dichloroethane ND 0.00278 1.04 01/13/201917:23 WG1222924 1,2-Dichloroethane ND 0.00278 1.04 01/13/201917:23 WG1222924 1,1-Dichloroethene ND 0.00278 1.04 01/13/201917:23 WG1222924 cis-1,2-Dichloroethene ND 0.00278 1.04 01/13/201917:23 WG1222924 trans-1,2-Dichloroethene ND 0.00556 1.04 01/13/201917:23 WG1222924 1,2-Dichloropropane ND 0.00556 1.04 01/13/201917:23 WG1222924 1,1-Dichloropropene ND 0.00278 1.04 01/13/201917:23 WG1222924 1,3-Dichloropropane ND 0.00556 1.04 01/13/201917:23 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 FP1 FTC FSS 4 Cn Rc F ql FAI FSC PAGE: 22 of 57 ONE LAB. NATIONWIDE. T2SW3 18' SAMPLE RESULTS - 06 Collected date/time: 01/09/19 10:15 L1060257 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00278 1.04 01/13/201917:23 WG1222924 trans-1,3-Dichloropropene ND 0.00556 1.04 01/13/201917:23 WG1222924 2,2-Dichloropropane ND 0.00278 1.04 01/13/201917:23 WG1222924 Di -isopropyl ether ND 0.00111 1.04 01/13/201917:23 WG1222924 Ethylbenzene ND 0.00278 1.04 01/13/201917:23 WG1222924 Hexachloro-1,3-butadiene ND 0.0278 1.04 01/13/201917:23 WG1222924 Isopropylbenzene ND 0.00278 1.04 01/13/201917:23 WG1222924 p-Isopropyltoluene ND 0.00556 1.04 01/13/201917:23 WG1222924 2-Butanone (MEK) ND 0.0278 1.04 01/13/201917:23 WG1222924 Methylene Chloride ND 0.0278 1.04 01/13/201917:23 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0278 1.04 01/13/201917:23 WG1222924 Methyl tert-butyl ether ND 0.00111 1.04 01/13/201917:23 WG1222924 Naphthalene ND 0.0139 1.04 01/13/201917:23 WG1222924 n-Propylbenzene ND 0.00556 1.04 01/13/201917:23 WG1222924 Styrene ND 0.0139 1.04 01/13/201917:23 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00278 1.04 01/13/201917:23 WG1222924 1,1,2,2-Tetrachloroethane ND 0.00278 1.04 01/13/201917:23 WG1222924 Tetrachloroethene ND 0.00278 1.04 01/13/201917:23 WG1222924 Toluene ND 0.00556 1.04 01/13/201917:23 WG1222924 1,2,3-Trichlorobenzene ND 0.00278 1.04 01/13/201917:23 WG1222924 1,2,4-Trichlorobenzene ND 0.0139 1.04 01/13/201917:23 WG1222924 1,1,1-Trichloroethane ND 0.00278 1.04 01/13/201917:23 WG1222924 1,1,2-Trichloroethane ND 0.00278 1.04 01/13/201917:23 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00278 1.04 01/13/201917:23 WG1222924 Trichloroethene ND 0.00111 1.04 01/13/201917:23 WG1222924 Trichlorofluoromethane ND 0.00278 1.04 01/13/201917:23 WG1222924 1,2,3-Trichloropropane ND 0.0139 1.04 01/13/201917:23 WG1222924 1,2,4-Trimethylbenzene ND 0.00556 1.04 01/13/201917:23 WG1222924 1,3,5-Trimethyl benzene ND 0.00556 1.04 01/13/201917:23 WG1222924 Vinyl chloride ND 0.00278 1.04 01/13/201917:23 WG1222924 Xylenes, Total ND 0.00723 1.04 01/13/201917:23 WG1222924 (S Toluene-d8 105 75.0-131 01113120191723 WG1222924 (S Dibromofluoromethane 95.7 65.0-129 011131201917.23 WG1222924 (S 4-Bromof/uorobenzene 96.4 67.0-138 01113120191723 WG1222924 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0356 1 01/14/2019 04:52 WG1222614 Acenaphthylene ND 0.0356 1 01/14/2019 04:52 WG1222614 Anthracene ND 0.0356 1 01/14/2019 04:52 WG1222614 Benzidine ND J4 0.356 1 01/14/2019 04:52 WG1222614 Benzo(a)anth race ne ND 0.0356 1 01/14/2019 04:52 WG1222614 Benzo(b)fluoranthene ND 0.0356 1 01/14/2019 04:52 WG1222614 Benzo(k)fluoranthene ND 0.0356 1 01/14/2019 04:52 WG1222614 Benzo(g,h,i)perylene ND 0.0356 1 01/14/2019 04:52 WG1222614 Benzo(a)pyrene ND 0.0356 1 01/14/2019 04:52 WG1222614 Bis(2-chlorethoxy)methane ND 0.356 1 01/14/2019 04:52 WG1222614 Bis(2-chloroethyl)ether ND 0.356 1 01/14/2019 04:52 WG1222614 Bis(2-chloroisopropyl)ether ND 0.356 1 01/14/2019 04:52 WG1222614 4-Bromophenyl-phenylether ND 0.356 1 01/14/2019 04:52 WG1222614 2-Chloronaphthalene ND 0.0356 1 01/14/2019 04:52 WG1222614 4-Chlorophenyl-phenylether ND 0.356 1 01/14/2019 04:52 WG1222614 Chrysene ND 0.0356 1 01/14/2019 04:52 WG1222614 Dibenz(a,h)anthracene ND 0.0356 1 01/14/2019 04:52 WG1222614 3,3-Dichlorobenzidine ND 0.356 1 01/14/2019 04:52 WG1222614 FP1 FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 23 of 57 ONE LAB. NATIONWIDE. T2SW3 18' SAMPLE RESULTS - 06 Collected date/time: 01/09/19 10:15 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Analyte 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene HexachIoro-1,3-butadiene HexachIorocyclopentadiene Hexachloroethane Ind eno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-N itros o d i-n-p ro pyl a mine Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result (dry) mg/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 61.4 55.4 55.9 50.8 53.0 56.5 Qualifier RDL (dry) Dilution Analysis Batch mg/kg date / time 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.0356 1 01/14/2019 04:52 WG1222614 0.0356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 J0 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.0356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.0356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.0356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.0356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 0.356 1 01/14/2019 04:52 WG1222614 12.0-120 0111412019 04:52 WG1222614 10.0-120 0111412019 04:52 WG1222614 10.0-122 0111412019 04:52 WG1222614 15.0-120 0111412019 04:52 WG1222614 10.0-127 0111412019 04:52 WG1222614 10.0-120 0111412019 04:52 WG1222614 FP FTc FS Fn FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 24 of 57 T2SW2 12' SAMPLE RESULTS - 07 ONE LAB. NATIONWIDE. Collected date/time: 01/09/19 10:25 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 81.1 1 01/14/2019 07:52 WG1223031 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time [Cn] Mercury ND 0.0247 1 01/14/201916:36 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.47 1 01/12/201912:02 WG1222487 Barium 79.2 0.617 1 01/12/201912:02 WG1222487 7G1 Cadmium ND 0.617 1 01/12/201912:02 WG1222487 Chromium 3.70 1.23 1 01/12/201912:02 WG1222487 Lead 14.8 0.617 1 01/12/201912:02 WG1222487 FAI Selenium ND 2.47 1 01/12/201912:02 WG1222487 Silver ND 1.23 1 01/12/201912:02 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0308 1 01/13/201917:42 WG1222924 Acrylonitrile ND 0.0154 1 01/13/201917:42 WG1222924 Benzene ND 0.00123 1 01/13/201917:42 WG1222924 Bromobenzene ND 0.0154 1 01/13/201917:42 WG1222924 Bromodichloromethane ND 0.00308 1 01/13/201917:42 WG1222924 Bromoform ND J4 0.0308 1 01/13/201917:42 WG1222924 Bromomethane ND 0.0154 1 01/13/201917:42 WG1222924 n-Butylbenzene ND 0.0154 1 01/13/201917:42 WG1222924 sec -Butyl benzene ND 0.0154 1 01/13/201917:42 WG1222924 tert-Butylbenzene ND 0.00617 1 01/13/201917:42 WG1222924 Carbon tetrachloride ND 0.00617 1 01/13/201917:42 WG1222924 Chlorobenzene ND 0.00308 1 01/13/201917:42 WG1222924 Chlorodibromomethane ND 0.00308 1 01/13/201917:42 WG1222924 Chloroethane ND 0.00617 1 01/13/201917:42 WG1222924 Chloroform ND 0.00308 1 01/13/201917:42 WG1222924 Chloromethane ND 0.0154 1 01/13/201917:42 WG1222924 2-Chlorotoluene ND 0.00308 1 01/13/201917:42 WG1222924 4-Chlorotoluene ND 0.00617 1 01/13/201917:42 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0308 1 01/13/201917:42 WG1222924 1,2-Dibromoethane ND 0.00308 1 01/13/201917:42 WG1222924 Dibromomethane ND 0.00617 1 01/13/201917:42 WG1222924 1,2-Dichlorobenzene ND 0.00617 1 01/13/201917:42 WG1222924 1,3-Dichlorobenzene ND 0.00617 1 01/13/201917:42 WG1222924 1,4-Dichlorobenzene ND 0.00617 1 01/13/201917:42 WG1222924 Dichlorodifluoromethane ND 0.00308 1 01/13/201917:42 WG1222924 1,1-Dichloroethane ND 0.00308 1 01/13/201917:42 WG1222924 1,2-Dichloroethane ND 0.00308 1 01/13/201917:42 WG1222924 1,1-Dichloroethene ND 0.00308 1 01/13/201917:42 WG1222924 cis-1,2-Dichloroethene ND 0.00308 1 01/13/201917:42 WG1222924 trans-1,2-Dichloroethene ND 0.00617 1 01/13/201917:42 WG1222924 1,2-Dichloropropane ND 0.00617 1 01/13/201917:42 WG1222924 1,1-Dichloropropene ND 0.00308 1 01/13/201917:42 WG1222924 1,3-Dichloropropane ND 0.00617 1 01/13/201917:42 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 25 of 57 ONE LAB. NATIONWIDE. T2SW2 12' SAMPLE RESULTS - 07 Collected date/time: 01/09/19 10:25 L1060257 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00308 1 01/13/201917:42 WG1222924 trans-1,3-Dichloropropene ND 0.00617 1 01/13/201917:42 WG1222924 2,2-Dichloropropane ND 0.00308 1 01/13/201917:42 WG1222924 Di -isopropyl ether ND 0.00123 1 01/13/201917:42 WG1222924 Ethylbenzene ND 0.00308 1 01/13/201917:42 WG1222924 Hexachloro-1,3-butadiene ND 0.0308 1 01/13/201917:42 WG1222924 Isopropylbenzene ND 0.00308 1 01/13/201917:42 WG1222924 p-Isopropyltoluene ND 0.00617 1 01/13/201917:42 WG1222924 2-Butanone (MEK) ND 0.0308 1 01/13/201917:42 WG1222924 Methylene Chloride ND 0.0308 1 01/13/201917:42 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0308 1 01/13/201917:42 WG1222924 Methyl tert-butyl ether ND 0.00123 1 01/13/201917:42 WG1222924 Naphthalene ND 0.0154 1 01/13/201917:42 WG1222924 n-Propylbenzene ND 0.00617 1 01/13/201917:42 WG1222924 Styrene ND 0.0154 1 01/13/201917:42 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00308 1 01/13/201917:42 WG1222924 1,1,2,2-Tetrachloroethane ND 0.00308 1 01/13/201917:42 WG1222924 Tetrachloroethene ND 0.00308 1 01/13/201917:42 WG1222924 Toluene ND 0.00617 1 01/13/201917:42 WG1222924 1,2,3-Trichlorobenzene ND 0.00308 1 01/13/201917:42 WG1222924 1,2,4-Trichlorobenzene ND 0.0154 1 01/13/201917:42 WG1222924 1,1,1-Trichloroethane ND 0.00308 1 01/13/201917:42 WG1222924 1,1,2-Trichloroethane ND 0.00308 1 01/13/201917:42 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00308 1 01/13/201917:42 WG1222924 Trichloroethene ND 0.00123 1 01/13/201917:42 WG1222924 Trichlorofluoromethane ND 0.00308 1 01/13/201917:42 WG1222924 1,2,3-Trichloropropane ND 0.0154 1 01/13/201917:42 WG1222924 1,2,4-Trimethylbenzene ND 0.00617 1 01/13/201917:42 WG1222924 1,3,5-Trimethyl benzene ND 0.00617 1 01/13/201917:42 WG1222924 Vinyl chloride ND 0.00308 1 01/13/201917:42 WG1222924 Xylenes, Total ND 0.00802 1 01/13/201917:42 WG1222924 (S) Toluene-d8 109 75.0-131 01113120191742 WG1222924 (S Dibromofluoromethane 92.2 65.0-129 01113120191742 WG1222924 (S)4-Bromof/uorobenzene 104 67.0-138 01113120191742 WG1222924 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0411 1 01/14/2019 05:15 WG1222614 Acenaphthylene ND 0.0411 1 01/14/2019 05:15 WG1222614 Anthracene ND 0.0411 1 01/14/2019 05:15 WG1222614 Benzidine ND J4 0.411 1 01/14/2019 05:15 WG1222614 Benzo(a)anth race ne ND 0.0411 1 01/14/2019 05:15 WG1222614 Benzo(b)fluoranthene ND 0.0411 1 01/14/2019 05:15 WG1222614 Benzo(k)fluoranthene ND 0.0411 1 01/14/2019 05:15 WG1222614 Benzo(g,h,i)perylene ND 0.0411 1 01/14/2019 05:15 WG1222614 Benzo(a)pyrene ND 0.0411 1 01/14/2019 05:15 WG1222614 Bis(2-chlorethoxy)methane ND 0.411 1 01/14/2019 05:15 WG1222614 Bis(2-chloroethyl)ether ND 0.411 1 01/14/2019 05:15 WG1222614 Bis(2-chloroisopropyl)ether ND 0.411 1 01/14/2019 05:15 WG1222614 4-Bromophenyl-phenylether ND 0.411 1 01/14/2019 05:15 WG1222614 2-Chloronaphthalene ND 0.0411 1 01/14/2019 05:15 WG1222614 4-Chlorophenyl-phenylether ND 0.411 1 01/14/2019 05:15 WG1222614 Chrysene ND 0.0411 1 01/14/2019 05:15 WG1222614 Dibenz(a,h)anthracene ND 0.0411 1 01/14/2019 05:15 WG1222614 3,3-Dichlorobenzidine ND 0.411 1 01/14/2019 05:15 WG1222614 FP1 FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 26 of 57 ONE LAB. NATIONWIDE. T2SW2 12' SAMPLE RESULTS - 07 Collected date/time: 01/09/19 10:25 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Analyte 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene HexachIoro-1,3-butadiene HexachIorocyclopentadiene Hexachloroethane Ind eno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethylamine n-Nitrosodiphenylamine n-N itros o d i-n-p ro pyl a mine Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result (dry) mg/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 64.5 58.3 59.3 51.7 56.1 56.6 Qualifier RDL (dry) Dilution Analysis Batch mg/kg date / time 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.0411 1 01/14/2019 05:15 WG1222614 0.0411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 J0 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.0411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.0411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.0411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.0411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 0.411 1 01/14/2019 05:15 WG1222614 12.0-120 0111412019 05.15 WG1222614 10.0-120 0111412019 05.15 WG1222614 10.0-122 0111412019 05.15 WG1222614 15.0-120 0111412019 05.15 WG1222614 10.0-127 0111412019 05.15 WG1222614 10.0-120 0111412019 05.15 WG1222614 FP FTc FS Fn FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 27 of 57 T1SW4-1 8' SAMPLE RESULTS - 08 ONE LAB. NATIONWIDE. Collected date/time: 01/09/19 15:35 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 86.5 1 01/14/2019 07:52 WG1223031 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time [Cn] Mercury ND 0.0231 1 01/14/201916:38 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.31 1 01/12/201912:04 WG1222487 Barium 55.1 0.578 1 01/12/201912:04 WG1222487 �GI Cadmium ND 0.578 1 01/12/201912:04 WG1222487 Chromium 5.17 1.16 1 01/12/201912:04 WG1222487 Lead 25.7 0.578 1 01/12/201912:04 WG1222487 FAI Selenium ND 2.31 1 01/12/201912:04 WG1222487 Silver ND 1.16 1 01/12/201912:04 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.231 8 01/13/2019 20:20 WG1222924 Acrylonitrile ND 0.116 8 01/13/2019 20:20 WG1222924 Benzene 0.358 0.00925 8 01/13/2019 20:20 WG1222924 Bromobenzene ND 0.116 8 01/13/2019 20:20 WG1222924 Bromodichloromethane ND 0.0231 8 01/13/2019 20:20 WG1222924 Bromoform ND J4 0.231 8 01/13/2019 20:20 WG1222924 Bromomethane ND 0.116 8 01/13/2019 20:20 WG1222924 n-Butylbenzene 9.17 2.89 200 01/15/2019 00:10 WG1223188 sec -Butyl benzene 4.71 0.116 8 01/13/2019 20:20 WG1222924 tert-Butylbenzene ND 0.0463 8 01/13/2019 20:20 WG1222924 Carbon tetrachloride ND 0.0463 8 01/13/2019 20:20 WG1222924 Chlorobenzene ND 0.0231 8 01/13/2019 20:20 WG1222924 Chlorodibromomethane ND 0.0231 8 01/13/2019 20:20 WG1222924 Chloroethane ND 0.0463 8 01/13/2019 20:20 WG1222924 Chloroform ND 0.0231 8 01/13/2019 20:20 WG1222924 Chloromethane ND 0.116 8 01/13/2019 20:20 WG1222924 2-Chlorotoluene ND 0.0231 8 01/13/2019 20:20 WG1222924 4-Chlorotoluene ND 0.0463 8 01/13/2019 20:20 WG1222924 1,2-Dibromo-3-Chloropropane 0.338 0.231 8 01/13/2019 20:20 WG1222924 1,2-Dibromoethane 0.218 0.0231 8 01/13/2019 20:20 WG1222924 Dibromomethane ND 0.0463 8 01/13/2019 20:20 WG1222924 1,2-Dichlorobenzene ND 0.0463 8 01/13/2019 20:20 WG1222924 1,3-Dichlorobenzene ND 0.0463 8 01/13/2019 20:20 WG1222924 1,4-Dichlorobenzene ND 0.0463 8 01/13/2019 20:20 WG1222924 Dichlorodifluoromethane ND 0.0231 8 01/13/2019 20:20 WG1222924 1,1-Dichloroethane ND 0.0231 8 01/13/2019 20:20 WG1222924 1,2-Dichloroethane ND 0.0231 8 01/13/2019 20:20 WG1222924 1,1-Dichloroethene ND 0.0231 8 01/13/2019 20:20 WG1222924 cis-1,2-Dichloroethene ND 0.0231 8 01/13/2019 20:20 WG1222924 trans-1,2-Dichloroethene ND 0.0463 8 01/13/2019 20:20 WG1222924 1,2-Dichloropropane ND 0.0463 8 01/13/2019 20:20 WG1222924 1,1-Dichloropropene ND 0.0231 8 01/13/2019 20:20 WG1222924 1,3-Dichloropropane ND 0.0463 8 01/13/2019 20:20 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 28 of 57 T1 S W4-1 8' SAMPLE Collected date/time: 01/09/19 15:35 Volatile Organic Compounds (GC/MS) by Method 8260B RESULTS - 08 L1060257 ONE LAB. NATIONWIDE. Result (dry) Qualifier RDL (dry) Dilution Analysis Batch FP1 Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.0231 8 01/13/2019 20:20 WG1222924 FTc trans-1,3-Dichloropropene ND 0.0463 8 01/13/2019 20:20 WG1222924 2,2-Dichloropropane ND 0.0231 8 01/13/2019 20:20 WG1222924 Di -isopropyl ether ND 0.00925 8 01/13/2019 20:20 WG1222924 FSS Ethylbenzene 33.2 0.578 200 01/15/2019 00:10 WG1223188 Hexachloro-1,3-butadiene ND 0.231 8 01/13/2019 20:20 WG1222924 rCn Isopropylbenzene 5.37 0.578 200 01/15/2019 00:10 WG1223188 p-Isopropyltoluene 2.51 0.0463 8 01/13/2019 20:20 WG1222924 2-Butanone (MEK) 4.75 0.231 8 01/13/2019 20:20 WG1222924 Methylene Chloride ND 0.231 8 01/13/2019 20:20 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.231 8 01/13/2019 20:20 WG1222924 Fc Methyl tert-butyl ether ND 0.00925 8 01/13/2019 20:20 WG1222924 Naphthalene 14.3 2.89 200 01/15/2019 00:10 WG1223188 7 n-Propylbenzene 16.8 0.0463 8 01/13/2019 20:20 WG1222924 GI Styrene 0.180 0.116 8 01/13/2019 20:20 WG1222924 1,1,1,2-Tetrachloroethane ND 0.0231 8 01/13/2019 20:20 WG1222924 FAI 1,1,2,2-Tetrachloroethane ND 0.0231 8 01/13/2019 20:20 WG1222924 Tetrachloroethene ND 0.0231 8 01/13/2019 20:20 WG1222924 Toluene 50.7 1.16 200 01/15/2019 00:10 WG1223188 F 1,2,3-Trichlorobenzene ND 0.0231 8 01/13/2019 20:20 WG1222924 1,2,4-Trichlorobenzene ND 0.116 8 01/13/2019 20:20 WG1222924 1,1,1-Trichloroethane ND 0.0231 8 01/13/2019 20:20 WG1222924 1,1,2-Trichloroethane ND 0.0231 8 01/13/2019 20:20 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.0231 8 01/13/2019 20:20 WG1222924 Trichloroethene ND 0.00925 8 01/13/2019 20:20 WG1222924 Trichlorofluoromethane ND 0.0231 8 01/13/2019 20:20 WG1222924 1,2,3-Trichloropropane ND 0.116 8 01/13/2019 20:20 WG1222924 1,2,4-Trimethylbenzene 135 1.16 200 01/15/2019 00:10 WG1223188 1,3,5-Trimethyl benzene 41.0 1.16 200 01/15/2019 00:10 WG1223188 Vinyl chloride ND 0.0231 8 01/13/2019 20:20 WG1222924 Xylenes, Total 252 1.50 200 01/15/2019 00:10 WG1223188 (S Toluene-d8 141 11 75.0-131 0111312019 20:20 WG1222924 (S Toluene-d8 ill 75.0-131 0111512019 00:10 WG1223188 (S) Dibromofluoromeftne 97.6 65.0-129 0111312019 20:20 WG1222924 (S Dibromofluoromethane 97.1 65.0-129 0111512019 00:10 WG1223188 (S) 4-Bromofluorobenzene 104 67.0-138 0111312019 20:20 WG1222924 (S 4-Bromofluorobenzene 94.2 67.0-138 0111512019 00:10 WG1223188 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0385 1 01/14/2019 07:32 WG1222614 Acenaphthylene ND 0.0385 1 01/14/2019 07:32 WG1222614 Anthracene ND 0.0385 1 01/14/2019 07:32 WG1222614 Benzidine ND J4 0.385 1 01/14/2019 07:32 WG1222614 Benzo(a)anth race ne ND 0.0385 1 01/14/2019 07:32 WG1222614 Benzo(b)fluoranthene ND 0.0385 1 01/14/2019 07:32 WG1222614 Benzo(k)fluoranthene ND 0.0385 1 01/14/2019 07:32 WG1222614 Benzo(g,h,i)perylene ND 0.0385 1 01/14/2019 07:32 WG1222614 Benzo(a)pyrene ND 0.0385 1 01/14/2019 07:32 WG1222614 Bis(2-chlorethoxy)methane ND 7.70 20 01/14/201911:46 WG1222614 Bis(2-chloroethyl)ether ND 7.70 20 01/14/201911:46 WG1222614 Bis(2-chloroisopropyl)ether ND 7.70 20 01/14/201911:46 WG1222614 4-Bromophenyl-phenylether ND 0.385 1 01/14/2019 07:32 WG1222614 2-Chloronaphthalene ND 0.0385 1 01/14/2019 07:32 WG1222614 4-Chlorophenyl-phenylether ND 0.385 1 01/14/2019 07:32 WG1222614 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 29 of 57 ONE LAB. NATIONWIDE. T1SW4-1 8' SAMPLE RESULTS - 08 Collected date/time: 01/09/19 15:35 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Chrysene ND 0.0385 1 01/14/2019 07:32 WG1222614 Dibenz(a,h)anthracene ND 0.0385 1 01/14/2019 07:32 WG1222614 3,3-Dichlorobenzidine ND 0.385 1 01/14/2019 07:32 WG1222614 2,4-Dinitrotoluene ND 0.385 1 01/14/2019 07:32 WG1222614 2,6-Dinitrotoluene ND 0.385 1 01/14/2019 07:32 WG1222614 Fluoranthene ND 0.0385 1 01/14/2019 07:32 WG1222614 Fluorene 0.160 0.0385 1 01/14/2019 07:32 WG1222614 Hexachlorobenzene ND 0.385 1 01/14/2019 07:32 WG1222614 Hexachloro-1,3-butadiene ND 7.70 20 01/14/201911:46 WG1222614 Hexachlorocyclopentadiene ND J0 0.385 1 01/14/2019 07:32 WG1222614 Hexachloroethane ND 7.70 20 01/14/201911:46 WG1222614 Indeno(1,2,3-cd)pyrene ND 0.0385 1 01/14/2019 07:32 WG1222614 Isophorone ND 7.70 20 01/14/201911:46 WG1222614 Naphthalene 16.3 0.770 20 01/14/201911:46 WG1222614 Nitrobenzene ND 7.70 20 01/14/201911:46 WG1222614 n-Nitrosodimethyla mine ND 7.70 20 01/14/201911:46 WG1222614 n-Nitrosodiphenyla mine ND 0.385 1 01/14/2019 07:32 WG1222614 n-Nitrosodi-n-propylamine ND 7.70 20 01/14/201911:46 WG1222614 Phenanthrene 0.0714 0.0385 1 01/14/2019 07:32 WG1222614 Benzylbutyl phthalate ND 0.385 1 01/14/2019 07:32 WG1222614 Bis(2-ethylhexyl)phthalate ND 0.385 1 01/14/2019 07:32 WG1222614 Di-n-butyl phthalate ND 0.385 1 01/14/2019 07:32 WG1222614 Diethyl phthalate ND 0.385 1 01/14/2019 07:32 WG1222614 Dimethyl phthalate ND 0.385 1 01/14/2019 07:32 WG1222614 Di-n-octyl phthalate ND 0.385 1 01/14/2019 07:32 WG1222614 Pyrene ND 0.0385 1 01/14/2019 07:32 WG1222614 1,2,4-Trichlorobenzene ND 7.70 20 01/14/201911:46 WG1222614 4-ChIoro-3-methyl phenol ND 7.70 20 01/14/201911:46 WG1222614 2-Chorophenol ND 7.70 20 01/14/201911:46 WG1222614 2,4-Dichlorophenol ND 7.70 20 01/14/201911:46 WG1222614 2,4-Dimethylphenol ND 7.70 20 01/14/201911:46 WG1222614 4,6-Dinitro-2-methylphenol ND 0.385 1 01/14/2019 07:32 WG1222614 2,4-Dinitrophenol ND 0.385 1 01/14/2019 07:32 WG1222614 2-Nitrophenol ND 7.70 20 01/14/201911:46 WG1222614 4-Nitrophenol ND 0.385 1 01/14/2019 07:32 WG1222614 Pentachlorophenol ND 0.385 1 01/14/2019 07:32 WG1222614 Phenol ND 7.70 20 01/14/201911:46 WG1222614 2,4,6-Trichlorophenol ND 0.385 1 01/14/2019 07:32 WG1222614 (S 2-F/uorophenol 17.1 12.0-120 0111412019 07.32 WG1222614 (S 2-Fluorophenol 83.2 J7 12.0-120 011141201911.46 WG1222614 (S) Phenol-d5 84.5 10.0-120 0111412019 07.32 WG1222614 (S Phenol-d5 63.0 J7 10.0-120 011141201911.46 WG1222614 (S Nitrobenzene-d5 87.6 10.0-122 0111412019 07.32 WG1222614 (S) Nitrobenzene-d5 96.0 J7 10.0-122 011141201911.46 WG1222614 (S 2-F/uorobipheny/ 46.6 15.0-120 0111412019 07.32 WG1222614 (S 2-Fluorobiphenyl 67.7 J7 15.0-120 011141201911.46 WG1222614 (S)Z4,6-Tribromopheno/ 37.1 J7 10.0-127 011141201911.46 WG1222614 (S) 2,4,6- Tribromophenol 55.1 10.0-127 011141201907.32 WG1222614 (S p-Terphenyl-d14 61.5 J7 10.0-120 011141201911.46 WG1222614 (S) p-Terphenyl-d14 52.2 10.0-120 0111412019 07.32 WG1222614 Sample Narrative: L1060257-08 WG1222614: IS/SURR failed on lower dilution. FP1 FTc FSS 4 Cn Fc 7G1 FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 30 of 57 T1SW2-1 14' SAMPLE RESULTS - 09 ONE LAB. NATIONWIDE. Collected date/time: 01/09/19 15:45 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 86.6 1 01/14/2019 07:52 WG1223031 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time [Cn] Mercury ND 0.0231 1 01/14/201916:41 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.31 1 01/12/201912:07 WG1222487 Barium 167 0.577 1 01/12/201912:07 WG1222487 7G1 Cadmium ND 0.577 1 01/12/201912:07 WG1222487 Chromium 6.97 1.15 1 01/12/201912:07 WG1222487 Lead 17.1 0.577 1 01/12/201912:07 WG1222487 FAI Selenium ND 2.31 1 01/12/201912:07 WG1222487 Silver ND 1.15 1 01/12/201912:07 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0289 1 01/13/201918:01 WG1222924 Acrylonitrile ND 0.0144 1 01/13/201918:01 WG1222924 Benzene ND 0.00115 1 01/13/201918:01 WG1222924 Bromobenzene ND 0.0144 1 01/13/201918:01 WG1222924 Bromodichloromethane ND 0.00289 1 01/13/201918:01 WG1222924 Bromoform ND J4 0.0289 1 01/13/201918:01 WG1222924 Bromomethane ND 0.0144 1 01/13/201918:01 WG1222924 n-Butylbenzene 10.2 0.577 40 01/15/2019 00:31 WG1223188 sec -Butyl benzene 1.49 0.577 40 01/15/2019 00:31 WG1223188 ter[-Butylbenzene ND 0.00577 1 01/13/201918:01 WG1222924 Carbon tetrachloride ND 0.00577 1 01/13/201918:01 WG1222924 Chlorobenzene ND 0.00289 1 01/13/201918:01 WG1222924 Chlorodibromomethane ND 0.00289 1 01/13/201918:01 WG1222924 Chloroethane ND 0.00577 1 01/13/201918:01 WG1222924 Chloroform ND 0.00289 1 01/13/201918:01 WG1222924 Chloromethane ND 0.0144 1 01/13/201918:01 WG1222924 2-Chlorotoluene ND 0.00289 1 01/13/201918:01 WG1222924 4-Chlorotoluene ND 0.00577 1 01/13/201918:01 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0289 1 01/13/201918:01 WG1222924 1,2-Dibromoethane ND 0.00289 1 01/13/201918:01 WG1222924 Dibromomethane ND 0.00577 1 01/13/201918:01 WG1222924 1,2-Dichlorobenzene ND 0.00577 1 01/13/201918:01 WG1222924 1,3-Dichlorobenzene ND 0.00577 1 01/13/201918:01 WG1222924 1,4-Dichlorobenzene ND 0.00577 1 01/13/201918:01 WG1222924 Dichlorodifluoromethane ND 0.00289 1 01/13/201918:01 WG1222924 1,1-Dichloroethane ND 0.00289 1 01/13/201918:01 WG1222924 1,2-Dichloroethane ND 0.00289 1 01/13/201918:01 WG1222924 1,1-Dichloroethene ND 0.00289 1 01/13/201918:01 WG1222924 cis-1,2-Dichloroethene ND 0.00289 1 01/13/201918:01 WG1222924 trans-1,2-Dichloroethene ND 0.00577 1 01/13/201918:01 WG1222924 1,2-Dichloropropane ND 0.00577 1 01/13/201918:01 WG1222924 1,1-Dichloropropene ND 0.00289 1 01/13/201918:01 WG1222924 1,3-Dichloropropane ND 0.00577 1 01/13/201918:01 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 31 of 57 T1SW2-1 14' SAMPLE Collected date/time: 01/09/19 15:45 Volatile Organic Compounds (GC/MS) by Method 8260B RESULTS - 09 L1060257 ONE LAB. NATIONWIDE. Result (dry) Qualifier RDL (dry) Dilution Analysis Batch FP1 Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00289 1 01/13/201918:01 WG1222924 FTc trans-1,3-Dichloropropene ND 0.00577 1 01/13/201918:01 WG1222924 2,2-Dichloropropane ND 0.00289 1 01/13/201918:01 WG1222924 Di -isopropyl ether ND 0.00115 1 01/13/201918:01 WG1222924 FSS Ethylbenzene 4.90 0.115 40 01/15/2019 00:31 WG1223188 Hexachloro-1,3-butadiene ND 0.0289 1 01/13/201918:01 WG1222924 rCn Isopropylbenzene 1.75 0.115 40 01/15/2019 00:31 WG1223188 p-Isopropyltoluene 1.15 0.231 40 01/15/2019 00:31 WG1223188 2-Butanone (MEK) 0.228 0.0289 1 01/13/201918:01 WG1222924 Methylene Chloride ND 0.0289 1 01/13/201918:01 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0289 1 01/13/201918:01 WG1222924 Fc Methyl tert-butyl ether ND 0.00115 1 01/13/201918:01 WG1222924 Naphthalene 14.4 0.577 40 01/15/2019 00:31 WG1223188 n-Propylbenzene 6.97 0.231 40 01/15/2019 00:31 WG1223188 GI Styrene ND 0.0144 1 01/13/201918:01 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00289 1 01/13/201918:01 WG1222924 FAI 1,1,2,2-Tetrachloroethane ND 0.00289 1 01/13/201918:01 WG1222924 Tetrachloroethene ND 0.00289 1 01/13/201918:01 WG1222924 Toluene 0.434 0.00577 1 01/13/2019 18:01 WG1222924 FSC 1,2,3-Trichlorobenzene ND 0.00289 1 01/13/201918:01 WG1222924 1,2,4-Trichlorobenzene ND 0.0144 1 01/13/201918:01 WG1222924 1,1,1-Trichloroethane ND 0.00289 1 01/13/201918:01 WG1222924 1,1,2-Trichloroethane ND 0.00289 1 01/13/201918:01 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00289 1 01/13/201918:01 WG1222924 Trichloroethene ND 0.00115 1 01/13/201918:01 WG1222924 Trichlorofluoromethane ND 0.00289 1 01/13/201918:01 WG1222924 1,2,3-Trichloropropane ND 0.0144 1 01/13/201918:01 WG1222924 1,2,4-Trimethylbenzene 58.2 0.231 40 01/15/2019 00:31 WG1223188 1,3,5-Trimethyl benzene 15.5 0.231 40 01/15/2019 00:31 WG1223188 Vinyl chloride ND 0.00289 1 01/13/201918:01 WG1222924 Xylenes, Total 37.9 0.300 40 01/15/2019 00:31 WG1223188 (S Toluene-d8 128 75.0-131 011131201918:01 WG1222924 (S Toluene-d8 ill 75.0-131 0111512019 0031 WG1223188 (S Dibromofluoromeftne 91.8 65.0-129 011131201918:01 WG1222924 (S Dibromofluoromethane 101 65.0-129 0111512019 00:31 WG1223188 (S) 4-Bromofluorobenzene 104 67.0-138 011131201918:01 WG1222924 (S 4-Bromofluorobenzene 95.4 67.0-138 0111512019 00:31 WG1223188 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0384 1 01/14/2019 05:38 WG1222614 Acenaphthylene ND 0.0384 1 01/14/2019 05:38 WG1222614 Anthracene ND 0.0384 1 01/14/2019 05:38 WG1222614 Benzidine ND J4 0.384 1 01/14/2019 05:38 WG1222614 Benzo(a)anth race ne ND 0.0384 1 01/14/2019 05:38 WG1222614 Benzo(b)fluoranthene ND 0.0384 1 01/14/2019 05:38 WG1222614 Benzo(k)fluoranthene ND 0.0384 1 01/14/2019 05:38 WG1222614 Benzo(g,h,i)perylene ND 0.0384 1 01/14/2019 05:38 WG1222614 Benzo(a)pyrene ND 0.0384 1 01/14/2019 05:38 WG1222614 Bis(2-chlorethoxy)methane ND 7.69 20 01/14/201911:00 WG1222614 Bis(2-chloroethyl)ether ND 7.69 20 01/14/201911:00 WG1222614 Bis(2-chloroisopropyl)ether ND 7.69 20 01/14/201911:00 WG1222614 4-Bromophenyl-phenylether ND 0.384 1 01/14/2019 05:38 WG1222614 2-Chloronaphthalene ND 0.0384 1 01/14/2019 05:38 WG1222614 4-Chlorophenyl-phenylether ND 0.384 1 01/14/2019 05:38 WG1222614 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 32 of 57 ONE LAB. NATIONWIDE. T1SW2-1 14' SAMPLE RESULTS - 09 Collected date/time: 01/09/19 15:45 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Chrysene ND 0.0384 1 01/14/2019 05:38 WG1222614 Dibenz(a,h)anthracene ND 0.0384 1 01/14/2019 05:38 WG1222614 3,3-Dichlorobenzidine ND 0.384 1 01/14/2019 05:38 WG1222614 2,4-Dinitrotoluene ND 0.384 1 01/14/2019 05:38 WG1222614 2,6-Dinitrotoluene ND 0.384 1 01/14/2019 05:38 WG1222614 Fluoranthene ND 0.0384 1 01/14/2019 05:38 WG1222614 Fluorene 0.0627 0.0384 1 01/14/2019 05:38 WG1222614 Hexachlorobenzene ND 0.384 1 01/14/2019 05:38 WG1222614 Hexachloro-1,3-butadiene ND 7.69 20 01/14/201911:00 WG1222614 Hexachlorocyclopentadiene ND J0 0.384 1 01/14/2019 05:38 WG1222614 Hexachloroethane ND 7.69 20 01/14/201911:00 WG1222614 Indeno(1,2,3-cd)pyrene ND 0.0384 1 01/14/2019 05:38 WG1222614 Isophorone ND 7.69 20 01/14/201911:00 WG1222614 Naphthalene 12.1 0.769 20 01/14/201911:00 WG1222614 Nitrobenzene ND 7.69 20 01/14/201911:00 WG1222614 n-Nitrosodimethyla mine ND 7.69 20 01/14/201911:00 WG1222614 n-Nitrosodiphenyla mine ND 0.384 1 01/14/2019 05:38 WG1222614 n-Nitrosodi-n-propylamine ND 7.69 20 01/14/201911:00 WG1222614 Phenanthrene 0.0711 0.0384 1 01/14/2019 05:38 WG1222614 Benzylbutyl phthalate ND 0.384 1 01/14/2019 05:38 WG1222614 Bis(2-ethylhexyl)phthalate ND 0.384 1 01/14/2019 05:38 WG1222614 Di-n-butyl phthalate ND 0.384 1 01/14/2019 05:38 WG1222614 Diethyl phthalate ND 0.384 1 01/14/2019 05:38 WG1222614 Dimethyl phthalate ND 0.384 1 01/14/2019 05:38 WG1222614 Di-n-octyl phthalate ND 0.384 1 01/14/2019 05:38 WG1222614 Pyrene ND 0.0384 1 01/14/2019 05:38 WG1222614 1,2,4-Trichlorobenzene ND 7.69 20 01/14/201911:00 WG1222614 4-ChIoro-3-methyl phenol ND 7.69 20 01/14/201911:00 WG1222614 2-Chorophenol ND 7.69 20 01/14/201911:00 WG1222614 2,4-Dichlorophenol ND 7.69 20 01/14/201911:00 WG1222614 2,4-Dimethylphenol ND 7.69 20 01/14/201911:00 WG1222614 4,6-Dinitro-2-methylphenol ND 0.384 1 01/14/2019 05:38 WG1222614 2,4-Dinitrophenol ND 0.384 1 01/14/2019 05:38 WG1222614 2-Nitrophenol ND 7.69 20 01/14/201911:00 WG1222614 4-Nitrophenol ND 0.384 1 01/14/2019 05:38 WG1222614 Pentachlorophenol ND 0.384 1 01/14/2019 05:38 WG1222614 Phenol ND 7.69 20 01/14/201911:00 WG1222614 2,4,6-Trichlorophenol ND 0.384 1 01/14/2019 05:38 WG1222614 (S) 2-F/uorophenol 55.0 12.0-120 0111412019 0538 WG1222614 (S) 2-Fluorophenol 53.3 J7 12.0-120 011141201911:00 WG1222614 (S) Phenol-d5 34.5 10.0-120 0111412019 0538 WG1222614 (S) Phenol-d5 36.9 J7 10.0-120 011141201911:00 WG1222614 (S) Nitrobenzene-d5 74.8 10.0-122 0111412019 0538 WG1222614 (S) Nitrobenzene-d5 66.2 J7 10.0-122 011141201911:00 WG1222614 (S) 2-F/uorobipheny/ 44.2 15.0-120 0111412019 0538 WG1222614 (S) 2-Fluorobiphenyl 46.4 J7 15.0-120 011141201911:00 WG1222614 (S)2,4,6-Tribromopheno/ 0.000 J7 10.0-127 011141201911:00 WG1222614 (S) 2,4,6- Tribromophenol 46.8 10.0-127 0111412019 05:38 WG1222614 (S) p-Terphenyl-d14 45.4 J7 10.0-120 011141201911:00 WG1222614 (S) p-Terphenyl-d14 45.7 10.0-120 0111412019 05:38 WG1222614 Sample Narrative: L1060257-09 WG1222614: IS/SURR failed on lower dilution. FP1 FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 33 of 57 T1SW3-1 20' SAMPLE RESULTS - 10 ONE LAB. NATIONWIDE. Collected date/time: 01/09/19 15:50 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 94.8 1 01/14/2019 07:52 WG1223031 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time [Cn] Mercury ND 0.0211 1 01/14/201916:44 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.11 1 01/12/201912:10 WG1222487 Barium 104 0.527 1 01/12/201912:10 WG1222487 7G1 Cadmium ND 0.527 1 01/12/201912:10 WG1222487 Chromium 2.74 1.05 1 01/12/201912:10 WG1222487 Lead 14.8 0.527 1 01/12/201912:10 WG1222487 FAI Selenium ND 2.11 1 01/12/201912:10 WG1222487 Silver ND 1.05 1 01/12/201912:10 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0264 1 01/13/201918:21 WG1222924 Acrylonitrile ND 0.0132 1 01/13/201918:21 WG1222924 Benzene ND 0.00105 1 01/13/201918:21 WG1222924 Bromobenzene ND 0.0132 1 01/13/201918:21 WG1222924 Bromodichloromethane ND 0.00264 1 01/13/201918:21 WG1222924 Bromoform ND J4 0.0264 1 01/13/201918:21 WG1222924 Bromomethane ND 0.0132 1 01/13/201918:21 WG1222924 n-Butylbenzene 3.55 0.264 20 01/15/2019 00:51 WG1223188 sec -Butyl benzene 0.619 0.264 20 01/15/2019 00:51 WG1223188 tert-Butylbenzene ND 0.00527 1 01/13/201918:21 WG1222924 Carbon tetrachloride ND 0.00527 1 01/13/201918:21 WG1222924 Chlorobenzene ND 0.00264 1 01/13/201918:21 WG1222924 Chlorodibromomethane ND 0.00264 1 01/13/201918:21 WG1222924 Chloroethane ND 0.00527 1 01/13/201918:21 WG1222924 Chloroform ND 0.00264 1 01/13/201918:21 WG1222924 Chloromethane ND 0.0132 1 01/13/201918:21 WG1222924 2-Chlorotoluene ND 0.00264 1 01/13/201918:21 WG1222924 4-Chlorotoluene ND 0.00527 1 01/13/201918:21 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0264 1 01/13/201918:21 WG1222924 1,2-Dibromoethane ND 0.00264 1 01/13/201918:21 WG1222924 Dibromomethane ND 0.00527 1 01/13/201918:21 WG1222924 1,2-Dichlorobenzene ND 0.00527 1 01/13/201918:21 WG1222924 1,3-Dichlorobenzene ND 0.00527 1 01/13/201918:21 WG1222924 1,4-Dichlorobenzene ND 0.00527 1 01/13/201918:21 WG1222924 Dichlorodifluoromethane ND 0.00264 1 01/13/201918:21 WG1222924 1,1-Dichloroethane ND 0.00264 1 01/13/201918:21 WG1222924 1,2-Dichloroethane ND 0.00264 1 01/13/201918:21 WG1222924 1,1-Dichloroethene ND 0.00264 1 01/13/201918:21 WG1222924 cis-1,2-Dichloroethene ND 0.00264 1 01/13/201918:21 WG1222924 trans-1,2-Dichloroethene ND 0.00527 1 01/13/201918:21 WG1222924 1,2-Dichloropropane ND 0.00527 1 01/13/201918:21 WG1222924 1,1-Dichloropropene ND 0.00264 1 01/13/201918:21 WG1222924 1,3-Dichloropropane ND 0.00527 1 01/13/201918:21 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 34 of 57 T1SW3-1 20' SAMPLE Collected date/time: 01/09/19 15:50 Volatile Organic Compounds (GC/MS) by Method 8260B RESULTS - 10 L1060257 ONE LAB. NATIONWIDE. Result (dry) Qualifier RDL (dry) Dilution Analysis Batch FP1 Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00264 1 01/13/201918:21 WG1222924 2 Tc trans-1,3-Dichloropropene ND 0.00527 1 01/13/201918:21 WG1222924 2,2-Dichloropropane ND 0.00264 1 01/13/201918:21 WG1222924 Di -isopropyl ether ND 0.00105 1 01/13/201918:21 WG1222924 FSS Ethylbenzene 1.55 0.00264 1 01/13/201918:21 WG1222924 Hexachloro-1,3-butadiene ND 0.0264 1 01/13/201918:21 WG1222924 rCn Isopropylbenzene 0.583 0.0527 20 01/15/2019 00:51 WG1223188 p-Isopropyltoluene 0.287 0.105 20 01/15/2019 00:51 WG1223188 2-Butanone (MEK) 0.0449 0.0264 1 01/13/201918:21 WG1222924 Methylene Chloride ND 0.0264 1 01/13/201918:21 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0264 1 01/13/201918:21 WG1222924 Fc Methyl tert-butyl ether ND 0.00105 1 01/13/201918:21 WG1222924 Naphthalene 4.76 0.264 20 01/15/2019 00:51 WG1223188 n-Propylbenzene 2.17 0.00527 1 01/13/201918:21 WG1222924 GI Styrene ND 0.0132 1 01/13/201918:21 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00264 1 01/13/201918:21 WG1222924 FAI 1,1,2,2-Tetrachloroethane ND 0.00264 1 01/13/201918:21 WG1222924 Tetrachloroethene ND 0.00264 1 01/13/201918:21 WG1222924 Toluene 0.0110 0.00527 1 01/13/201918:21 WG1222924 FSC 1,2,3-Trichlorobenzene ND 0.00264 1 01/13/201918:21 WG1222924 1,2,4-Trichlorobenzene ND 0.0132 1 01/13/201918:21 WG1222924 1,1,1-Trichloroethane ND 0.00264 1 01/13/201918:21 WG1222924 1,1,2-Trichloroethane ND 0.00264 1 01/13/201918:21 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00264 1 01/13/201918:21 WG1222924 Trichloroethene ND 0.00105 1 01/13/201918:21 WG1222924 Trichlorofluoromethane ND 0.00264 1 01/13/201918:21 WG1222924 1,2,3-Trichloropropane ND 0.0132 1 01/13/201918:21 WG1222924 1,2,4-Trimethylbenzene 24.4 0.105 20 01/15/2019 00:51 WG1223188 1,3,5-Trimethyl benzene 6.62 0.105 20 01/15/2019 00:51 WG1223188 Vinyl chloride ND 0.00264 1 01/13/201918:21 WG1222924 Xylenes, Total 10.4 0.137 20 01/15/2019 00:51 WG1223188 (S Toluene-d8 ill 75.0-131 011131201918:21 WG1222924 (S Toluene-d8 108 75.0-131 0111512019 00:51 WG1223188 (S Dibromofluoromeftne 94.7 65.0-129 011131201918:21 WG1222924 (S) Dibromofluoromethane 102 65.0-129 0111512019 00:51 WG1223188 (S) 4-Bromofluorobenzene 106 67.0-138 011131201918:21 WG1222924 (S 4-Bromofluorobenzene 94.1 67.0-138 0111512019 00:51 WG1223188 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0351 1 01/14/2019 06:01 WG1222614 Acenaphthylene ND 0.0351 1 01/14/2019 06:01 WG1222614 Anthracene ND 0.0351 1 01/14/2019 06:01 WG1222614 Benzidine ND J4 0.351 1 01/14/2019 06:01 WG1222614 Benzo(a)anth race ne ND 0.0351 1 01/14/2019 06:01 WG1222614 Benzo(b)fluoranthene ND 0.0351 1 01/14/2019 06:01 WG1222614 Benzo(k)fluoranthene ND 0.0351 1 01/14/2019 06:01 WG1222614 Benzo(g,h,i)perylene ND 0.0351 1 01/14/2019 06:01 WG1222614 Benzo(a)pyrene ND 0.0351 1 01/14/2019 06:01 WG1222614 Bis(2-chlorethoxy)methane ND 3.51 10 01/14/201911:23 WG1222614 Bis(2-chloroethyl)ether ND 3.51 10 01/14/201911:23 WG1222614 Bis(2-chloroisopropyl)ether ND 3.51 10 01/14/201911:23 WG1222614 4-Bromophenyl-phenylether ND 0.351 1 01/14/2019 06:01 WG1222614 2-Chloronaphthalene ND 0.0351 1 01/14/2019 06:01 WG1222614 4-Chlorophenyl-phenylether ND 0.351 1 01/14/2019 06:01 WG1222614 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 35 of 57 ONE LAB. NATIONWIDE. T1SW3-1 20' SAMPLE RESULTS - 10 Collected date/time: 01/09/19 15:50 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Chrysene ND 0.0351 1 01/14/2019 06:01 WG1222614 Dibenz(a,h)anthracene ND 0.0351 1 01/14/2019 06:01 WG1222614 3,3-Dichlorobenzidine ND 0.351 1 01/14/2019 06:01 WG1222614 2,4-Dinitrotoluene ND 0.351 1 01/14/2019 06:01 WG1222614 2,6-Dinitrotoluene ND 0.351 1 01/14/2019 06:01 WG1222614 Fluoranthene ND 0.0351 1 01/14/2019 06:01 WG1222614 Fluorene 0.0722 0.0351 1 01/14/2019 06:01 WG1222614 Hexachlorobenzene ND 0.351 1 01/14/2019 06:01 WG1222614 Hexachloro-1,3-butadiene ND 3.51 10 01/14/201911:23 WG1222614 Hexachlorocyclopentadiene ND J0 0.351 1 01/14/2019 06:01 WG1222614 Hexachloroethane ND 3.51 10 01/14/201911:23 WG1222614 Indeno(1,2,3-cd)pyrene ND 0.0351 1 01/14/2019 06:01 WG1222614 Isophorone ND 3.51 10 01/14/201911:23 WG1222614 Naphthalene 6.11 0.351 10 01/14/201911:23 WG1222614 Nitrobenzene ND 3.51 10 01/14/201911:23 WG1222614 n-Nitrosodimethyla mine ND 3.51 10 01/14/201911:23 WG1222614 n-Nitrosodiphenyla mine ND 0.351 1 01/14/2019 06:01 WG1222614 n-Nitrosodi-n-propylamine ND 3.51 10 01/14/201911:23 WG1222614 Phenanthrene 0.0422 0.0351 1 01/14/2019 06:01 WG1222614 Benzylbutyl phthalate ND 0.351 1 01/14/2019 06:01 WG1222614 Bis(2-ethylhexyl)phthalate ND 0.351 1 01/14/2019 06:01 WG1222614 Di-n-butyl phthalate ND 0.351 1 01/14/2019 06:01 WG1222614 Diethyl phthalate ND 0.351 1 01/14/2019 06:01 WG1222614 Dimethyl phthalate ND 0.351 1 01/14/2019 06:01 WG1222614 Di-n-octyl phthalate ND 0.351 1 01/14/2019 06:01 WG1222614 Pyrene ND 0.0351 1 01/14/2019 06:01 WG1222614 1,2,4-Trichlorobenzene ND 3.51 10 01/14/201911:23 WG1222614 4-ChIoro-3-methyl phenol ND 3.51 10 01/14/201911:23 WG1222614 2-Chorophenol ND 3.51 10 01/14/201911:23 WG1222614 2,4-Dichlorophenol ND 3.51 10 01/14/201911:23 WG1222614 2,4-Dimethylphenol ND 3.51 10 01/14/201911:23 WG1222614 4,6-Dinitro-2-methylphenol ND 0.351 1 01/14/2019 06:01 WG1222614 2,4-Dinitrophenol ND 0.351 1 01/14/2019 06:01 WG1222614 2-Nitrophenol ND 3.51 10 01/14/201911:23 WG1222614 4-Nitrophenol ND 0.351 1 01/14/2019 06:01 WG1222614 Pentachlorophenol ND 0.351 1 01/14/2019 06:01 WG1222614 Phenol ND 3.51 10 01/14/201911:23 WG1222614 2,4,6-Trichlorophenol ND 0.351 1 01/14/2019 06:01 WG1222614 (S) 2-F/uorophenol 61.9 12.0-120 0111412019 06:01 WG1222614 (S) 2-Fluorophenol 68.3 12.0-120 011141201911:23 WG1222614 (S) Phenol-d5 54.5 10.0-120 0111412019 06:01 WG1222614 (S) Phenol-d5 48.9 10.0-120 011141201911:23 WG1222614 (S) Nitrobenzene-d5 67.1 10.0-122 0111412019 06:01 WG1222614 (S) Nitrobenzene-d5 72.7 10.0-122 01114120191123 WG1222614 (S) 2-F/uorobipheny/ 47.6 15.0-120 0111412019 06:01 WG1222614 (S) 2-Fluorobiphenyl 60.8 15.0-120 011141201911:23 WG1222614 (S)2,4,6-Tribromopheno/ 29.3 10.0-127 011141201911:23 WG1222614 (S) 2,4,6- Tribromophenol 53.1 10.0-127 0111412019 06:01 WG1222614 (S) p-Terphenyl-d14 51.1 10.0-120 0111412019 06:01 WG1222614 (S) p-Terphenyl-d14 59.9 10.0-120 011141201911:23 WG1222614 Sample Narrative: L1060257-10 WG1222614: IS/SURR failed on lower dilution. FP1 FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 36 of 57 T1SW1 2' SAMPLE RESULTS - 11 ONE LAB. NATIONWIDE. Collected date/time: 01/09/19 16:00 L1060257 Total Solids by Method 2540 G-2011 FP1 Result Qualifier Dilution Analysis Batch Analyte % date /time Total Solids 86.6 1 01/14/201910:02 WG1223079 FTC Mercury by Method 7471B FSS Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 4 CCl Mercury 0.128 0.0231 1 01/14/201916:51 WG1223174 Metals (ICP) by Method 6010D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time 6 QC Arsenic ND 2.31 1 01/12/201912:13 WG1222487 Barium 78.4 0.577 1 01/12/201912:13 WG1222487 7G1 Cadmium ND 0.577 1 01/12/201912:13 WG1222487 Chromium 9.14 1.15 1 01/12/201912:13 WG1222487 Lead 4.36 0.577 1 01/12/201912:13 WG1222487 FAI Selenium ND 2.31 1 01/12/201912:13 WG1222487 Silver ND 1.15 1 01/12/201912:13 WG1222487 FSC Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acetone ND 0.0289 1 01/13/201918:41 WG1222924 Acrylonitrile ND 0.0144 1 01/13/201918:41 WG1222924 Benzene ND 0.00115 1 01/13/201918:41 WG1222924 Bromobenzene ND 0.0144 1 01/13/201918:41 WG1222924 Bromodichloromethane ND 0.00289 1 01/13/201918:41 WG1222924 Bromoform ND J4 0.0289 1 01/13/201918:41 WG1222924 Bromomethane ND 0.0144 1 01/13/201918:41 WG1222924 n-Butylbenzene ND 0.0144 1 01/14/2019 23:09 WG1223188 sec -Butyl benzene ND 0.0144 1 01/14/2019 23:09 WG1223188 ter[-Butylbenzene ND 0.00577 1 01/13/201918:41 WG1222924 Carbon tetrachloride ND 0.00577 1 01/13/201918:41 WG1222924 Chlorobenzene ND 0.00289 1 01/13/201918:41 WG1222924 Chlorodibromomethane ND 0.00289 1 01/13/201918:41 WG1222924 Chloroethane ND 0.00577 1 01/13/201918:41 WG1222924 Chloroform ND 0.00289 1 01/13/201918:41 WG1222924 Chloromethane ND 0.0144 1 01/13/201918:41 WG1222924 2-Chlorotoluene ND 0.00289 1 01/13/201918:41 WG1222924 4-Chlorotoluene ND 0.00577 1 01/13/201918:41 WG1222924 1,2-Dibromo-3-Chloropropane ND 0.0289 1 01/13/201918:41 WG1222924 1,2-Dibromoethane ND 0.00289 1 01/13/201918:41 WG1222924 Dibromomethane ND 0.00577 1 01/13/201918:41 WG1222924 1,2-Dichlorobenzene ND 0.00577 1 01/13/201918:41 WG1222924 1,3-Dichlorobenzene ND 0.00577 1 01/13/201918:41 WG1222924 1,4-Dichlorobenzene ND 0.00577 1 01/13/201918:41 WG1222924 Dichlorodifluoromethane ND 0.00289 1 01/13/201918:41 WG1222924 1,1-Dichloroethane ND 0.00289 1 01/13/201918:41 WG1222924 1,2-Dichloroethane ND 0.00289 1 01/13/201918:41 WG1222924 1,1-Dichloroethene ND 0.00289 1 01/13/201918:41 WG1222924 cis-1,2-Dichloroethene ND 0.00289 1 01/13/201918:41 WG1222924 trans-1,2-Dichloroethene ND 0.00577 1 01/13/201918:41 WG1222924 1,2-Dichloropropane ND 0.00577 1 01/13/201918:41 WG1222924 1,1-Dichloropropene ND 0.00289 1 01/13/201918:41 WG1222924 1,3-Dichloropropane ND 0.00577 1 01/13/201918:41 WG1222924 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 37 of 57 T1SW1 2' SAMPLE RESULTS - 11 Collected date/time: 01/09/19 16:00 L1060257 Volatile Organic Compounds (GC/MS) by Method 8260B ONE LAB. NATIONWIDE. Result (dry) Qualifier RDL (dry) Dilution Analysis Batch FP1 Analyte mg/kg mg/kg date / time cis-1,3-Dichloropropene ND 0.00289 1 01/13/201918:41 WG1222924 FTc trans-1,3-Dichloropropene ND 0.00577 1 01/13/201918:41 WG1222924 2,2-Dichloropropane ND 0.00289 1 01/13/201918:41 WG1222924 Di -isopropyl ether ND 0.00115 1 01/13/201918:41 WG1222924 FSS Ethylbenzene 0.00515 0.00289 1 01/14/2019 23:09 WG1223188 Hexachloro-1,3-butadiene ND 0.0289 1 01/13/201918:41 WG1222924 rCn Isopropylbenzene ND 0.00289 1 01/14/2019 23:09 WG1223188 p-Isopropyltoluene ND 0.00577 1 01/14/2019 23:09 WG1223188 2-Butanone (MEK) ND 0.0289 1 01/13/201918:41 WG1222924 Methylene Chloride ND 0.0289 1 01/13/201918:41 WG1222924 4-Methyl-2-pentanone (MIBK) ND 0.0289 1 01/13/201918:41 WG1222924 Fc Methyl tert-butyl ether ND 0.00115 1 01/13/201918:41 WG1222924 Naphthalene 0.0247 0.0144 1 01/14/2019 23:09 WG1223188 n-Propylbenzene 0.0107 0.00577 1 01/14/2019 23:09 WG1223188 GI Styrene ND 0.0144 1 01/13/201918:41 WG1222924 1,1,1,2-Tetrachloroethane ND 0.00289 1 01/13/201918:41 WG1222924 FAI 1,1,2,2-Tetrachloroethane ND 0.00289 1 01/13/201918:41 WG1222924 Tetrachloroethene ND 0.00289 1 01/13/201918:41 WG1222924 Toluene ND 0.00577 1 01/13/201918:41 WG1222924 FSC 1,2,3-Trichlorobenzene ND 0.00289 1 01/13/201918:41 WG1222924 1,2,4-Trichlorobenzene ND 0.0144 1 01/13/201918:41 WG1222924 1,1,1-Trichloroethane ND 0.00289 1 01/13/201918:41 WG1222924 1,1,2-Trichloroethane ND 0.00289 1 01/13/201918:41 WG1222924 1,1,2-Trichlorotrifluoroethane ND 0.00289 1 01/13/201918:41 WG1222924 Trichloroethene ND 0.00115 1 01/13/201918:41 WG1222924 Trichlorofluoromethane ND 0.00289 1 01/13/201918:41 WG1222924 1,2,3-Trichloropropane ND 0.0144 1 01/13/201918:41 WG1222924 1,2,4-Trimethylbenzene 0.103 0.00577 1 01/14/2019 23:09 WG1223188 1,3,5-Trimethyl benzene 0.0276 0.00577 1 01/14/2019 23:09 WG1223188 Vinyl chloride ND 0.00289 1 01/13/201918:41 WG1222924 Xylenes, Total 0.0479 0.00751 1 01/14/2019 23:09 WG1223188 (S Toluene-d8 108 75.0-131 011131201918.41 WG1222924 (SToluene-d8 114 75.0-131 011141201923:09 WG1223188 (S) Dibromofluoromeftne 93.1 65.0-129 011131201918.41 WG1222924 (S) Dibromofluoromethane 85.5 65.0-129 0111412019 23:09 WG1223188 (S) 4-Bromofluorobenzene 122 67.0-138 011131201918.41 WG1222924 (S4-Bromofluorobenzene 91.2 67.0-138 011141201923:09 WG1223188 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Acenaphthene ND 0.0385 1 01/14/2019 06:24 WG1222614 Acenaphthylene ND 0.0385 1 01/14/2019 06:24 WG1222614 Anthracene ND 0.0385 1 01/14/2019 06:24 WG1222614 Benzidine ND J4 0.385 1 01/14/2019 06:24 WG1222614 Benzo(a)anth race ne ND 0.0385 1 01/14/2019 06:24 WG1222614 Benzo(b)fluoranthene ND 0.0385 1 01/14/2019 06:24 WG1222614 Benzo(k)fluoranthene ND 0.0385 1 01/14/2019 06:24 WG1222614 Benzo(g,h,i)perylene ND 0.0385 1 01/14/2019 06:24 WG1222614 Benzo(a)pyrene ND 0.0385 1 01/14/2019 06:24 WG1222614 Bis(2-chlorethoxy)methane ND 0.385 1 01/14/2019 06:24 WG1222614 Bis(2-chloroethyl)ether ND 0.385 1 01/14/2019 06:24 WG1222614 Bis(2-chloroisopropyl)ether ND 0.385 1 01/14/2019 06:24 WG1222614 4-Bromophenyl-phenylether ND 0.385 1 01/14/2019 06:24 WG1222614 2-Chloronaphthalene ND 0.0385 1 01/14/2019 06:24 WG1222614 4-Chlorophenyl-phenylether ND 0.385 1 01/14/2019 06:24 WG1222614 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 38 of 57 T1SW1 2' SAMPLE RESULTS - 11 Collected date/time: 01/09/19 16:00 L1060257 Semi Volatile Organic Compounds (GC/MS) by Method 8270D ONE LAB. NATIONWIDE. Analyte Chrysene Dibenz(a,h)anthracene 3,3-Dichlorobenzidine 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene Hexachloro-1,3-butadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethyla mine n-Nitrosodiphenyla mine n-N itros o d i-n-p ro pyl a m i n e Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-F/uorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result (dry) Qualifier RDL (dry) Dilution Analysis Batch mg/kg mg/kg date / time ND 0.0385 1 01/14/2019 06:24 WG1222614 ND 0.0385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.0385 1 01/14/2019 06:24 WG1222614 ND 0.0385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND J0 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.0385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.0385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.0385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.0385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 ND 0.385 1 01/14/2019 06:24 WG1222614 61.9 12.0-120 0111412019 06:24 WG1222614 56.1 10.0-120 0111412019 06:24 WG1222614 57.8 10.0-122 0111412019 06:24 WG1222614 52.3 15.0-120 0111412019 06:24 WG1222614 54.4 10.0-127 0111412019 06:24 WG1222614 54.7 10.0-120 0111412019 06:24 WG1222614 Cp FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 39 of 57 WG1222495 QUALITY CONTROL SUMMARY Total Solids by Method 2540 G-2011 1-1060257-01,02,03,04 Method Blank (MB) (MB) R3375765-1 01/14/19 08:19 MB Result MB Qualifier MB MDL MB RDL Analyte % _ % % Total Solids 0.00100 L1060202-11 Original Sample (OS) • Duplicate (DUP) (OS) L1060202-11 01/14/19 08:19 • (DUP) R3375765-3 01/14/19 08:19 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte % % % % Total Solids 69.8 70.0 1 0.321 10 Laboratory Control Sample (LCS) (LCS) R3375765-2 01/14/19 08:19 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte % %_ % % Total Solids 50.0 50.0 100 85.0-115 ONE LAB. NATIONWIDE. — I Cp FTc FSS 4 — Cn FSr — �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 40 of 57 WG1223031 QUALITY CONTROL SUMMARY Total Solids by Method 2540 G-2011 L1060257-05,06,07,08,09,10 Method Blank (MB) (MB) R3375606-1 01/14/19 07:52 MB Result MB Qualifier MB MDL MB RDL Analyte % % % Total Solids 0.00200 L1060597-02 Original Sample (OS) • Duplicate (DUP) (OS) L1060597-02 01/14/19 07:52 • (DUP) R3375606-3 01/14/19 07:52 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte % % % % Total Solids 96.6 96.7 1 0.0781 10 Laboratory Control Sample (LCS) (LCS) R3375606-2 01/14/19 07:52 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte % %_ % % Total Solids 50.0 50.0 100 85.0-115 ONE LAB. NATIONWIDE. — I Cp FTc FSS 4 — Cn FSr — �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 41 of 57 WG1223079 QUALITY CONTROL SUMMARY Total Solids by Method 2540 G-2011 L1060257-11 Method Blank (MB) (MB) R3375768-1 01/14/1910:02 MB Result MB Qualifier MB MDL MB RDL Analyte % % % Total Solids 0.000 L1060448-01 Original Sample (OS) • Duplicate (DUP) (OS) L1060448-01 01/14/19 10:02 • (DUP) R3375768-3 01/14/1910:02 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte % % % % Total Solids 84.4 84.0 1 0.555 10 Laboratory Control Sample (LCS) (LCS) R3375768-2 01/14/1910:02 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte % %_ % % Total Solids 50.0 50.0 100 85.0-115 ONE LAB. NATIONWIDE. — I Cp FTc FSS 4 — Cn FSr — �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 42 of 57 WG1223174 Mercury by Method 7471B Method Blank (MB) (MB) R3375739-1 01/14/1915:50 MB Result Analyte mg/kg Mercury 0.00362 MB Qualifier MB MDL MB RDL mg/kg mg/kg J 0.00280 0.0200 QUALITY CONTROL SUMMARY L1060257-01,02,03,04,05,06,07,08,09,10,11 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375739-2 01/14/19 15:53 • (LCSD) R3375739-3 01/14/1915:55 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Mercury 0.500 0.535 0.519 107 104 80.0-120 3.00 20 L1060470-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1060470-01 01/14/1915:58 • (MS) R3375739-4 01/14/1916:00 • (MSD) R3375739-5 01/14/1916:03 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte mg/kg mg/kg mg/kg mg/kg % % % % Mercury 0.500 0.0111 0.509 0.535 99.7 105 1 75.0-125 4.90 ONE LAB. NATIONWIDE. RPD Limits 20 — I Cp FTc FSS 4 — Cn FSr — �GI — $AI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 43 of 57 WG1222487 QUALITY CONTROL SUMMARY Metals (ICP) by Method 6010D L1060257-01,02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3375351-1 01/12/1911:16 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Arsenic U 0.460 2.00 Barium U 0.170 0.500 Cadmium U 0.0700 0.500 Chromium U 0.140 1.00 Lead U 0.190 0.500 Selenium U 0.620 2.00 Silver U 0.120 1.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. (LCS) R3375351-2 01/12/1911:18 • (LCSD) R3375351-3 01/12/1911:21 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Arsenic 100 98.2 96.8 98.2 96.8 80.0-120 1.41 20 Barium 100 104 102 104 102 80.0-120 1.84 20 Cadmium 100 101 99.0 101 99.0 80.0-120 1.93 20 Chromium 100 99.7 96.8 99.7 96.8 80.0-120 2.94 20 Lead 100 99.3 98.0 99.3 98.0 80.0-120 1.32 20 Selenium 100 101 101 101 101 80.0-120 0.788 20 Silver 20.0 18.9 18.4 94.7 92.1 80.0-120 2.78 20 L1060257-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1060257-01 01/12/1911:23 • (MS) R3375351-6 01/12/1911:31 • (MSD) R3375351-7 01/12/1911:34 Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits (dry) (dry) (dry) Analyte mg/kg mg/kg mg/kg mg/kg % % % % % Arsenic 108 ND 106 98.4 97.8 90.2 1 75.0-125 7.95 20 Barium 108 76.8 179 169 94.5 85.4 1 75.0-125 5.66 20 Cadmium 108 ND 110 102 102 94.6 1 75.0-125 7.66 20 Chromium 108 13.9 122 113 100 91.4 1 75.0-125 7.95 20 Lead 108 4.43 114 106 101 93.9 1 75.0-125 7.09 20 Selenium 108 ND 111 102 102 94.7 1 75.0-125 7.79 20 Silver 21.6 ND 20.3 18.8 93.8 87.2 1 75.0-125 7.27 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 44 of 57 FP1 FTc FSS [Cn] FSr �GI FAI [Sc WG1222924 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1060257-01,02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3375605-3 01/13/1914:34 MB Result Analyte mg/kg Acetone 0.0150 Acrylonitrile U Benzene U Bromobenzene U Bromodichloromethane U Bromoform U Bromomethane U n-Butylbenzene U sec -Butyl benzene U tert-Butylbenzene U Carbon tetrachloride U Chlorobenzene U Chlorodibromomethane U Chloroethane U Chloroform U Chloromethane U 2-Chlorotoluene U 4-Chlorotoluene U 1,2-Dibromo-3-Chloropropane U 1,2-Dibromoethane U Dibromomethane U 1,2-Dichlorobenzene U 1,3-Dichlorobenzene U 1,4-Dichlorobenzene U Dichlorodifluoromethane U 1,1-Dichloroethane U 1,2-Dichloroethane U 1,1-Dichloroethene U cis-1,2-Dichloroethene U trans-1,2-Dichloroethene U 1,2-Dichloropropane U 1,1-Dichloropropene U 1,3-Dichloropropane U cis-1,3-Dichloropropene U trans-1,3-Dichloropropene U 2,2-Dichloropropane U Di -isopropyl ether U Ethylbenzene U Hexachloro-1,3-butadiene U Isopropylbenzene U MB Qualifier J MB MDL mg/kg 0.0137 0.00190 0.000400 0.00105 0.000788 0.00598 0.00370 0.00384 0.00253 0.00155 0.00108 0.000573 0.000450 0.00108 0.000415 0.00139 0.000920 0.00113 0.00510 0.000525 0.00100 0.00145 0.00170 0.00197 0.000818 0.000575 0.000475 0.000500 0.000690 0.00143 0.00127 0.000700 0.00175 0.000678 0.00153 0.000793 0.000350 0.000530 0.0127 0.000863 MB RDL mg/kg 0.0250 0.0125 0.00100 0.0125 0.00250 0.0250 0.0125 0.0125 0.0125 0.00500 0.00500 0.00250 0.00250 0.00500 0.00250 0.0125 0.00250 0.00500 0.0250 0.00250 0.00500 0.00500 0.00500 0.00500 0.00250 0.00250 0.00250 0.00250 0.00250 0.00500 0.00500 0.00250 0.00500 0.00250 0.00500 0.00250 0.00100 0.00250 0.0250 0.00250 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 45 of 57 WG1222924 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1060257-01,02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3375605-3 01/13/1914:34 MB Result Analyte mg/kg p-Isopropyltoluene U 2-Butanone (MEK) U Methylene Chloride 0.0163 4-Methyl-2-pentanone (MIBK) U Methyl tert-butyl ether U Naphthalene U n-Propylbenzene U Styrene U 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U Tetrachloroethene U Toluene U 1,1,2-Trichlorotrifluoroethane U 1,2,3-Trichlorobe nzene U 1,2,4-Trichlorobenzene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichlorofluoromethane U 1,2,3-Trichloropropane U 1,2,4-Trimethylbenzene U 1,3,5-Trimethyl benzene U Vinyl chloride U Xylenes, Total U (S) Toluene-d8 107 (S) Dibromofluoromethane 93.0 (S) 4-Bromof/uorobenzene 101 MB Qualifier MB MDL mg/kg MB RDL mg/kg 0.00233 0.00500 0.0125 0.0250 J 0.00664 0.0250 0.0100 0.0250 0.000295 0.00100 0.00312 0.0125 0.00118 0.00500 0.00273 0.0125 0.000500 0.00250 0.000390 0.00250 0.000700 0.00250 0.00125 0.00500 0.000675 0.00250 0.000625 0.00250 0.00482 0.0125 0.000275 0.00250 0.000883 0.00250 0.000400 0.00100 0.000500 0.00250 0.00510 0.0125 0.00116 0.00500 0.00108 0.00500 0.000683 0.00250 0.00478 0.00650 75.0-131 65.0-129 67.0-138 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375605-1 01/13/1911:52 • (LCSD) R3375605-2 01/13/1912:51 Spike Amount LCS Result LCSD Result Analyte mg/kg mg/kg mg/kg Acetone 0.625 0.688 0.639 Acrylonitrile 0.625 0.840 0.765 Benzene 0.125 0.134 0.127 Bromobenzene 0.125 0.133 0.125 Bromodichloromethane 0.125 0.139 0.136 Bromoform 0.125 0.168 0.161 ACCOUNT: Withers & Ravenel Eng. - Standard LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 110 102 10.0-160 7.44 31 134 122 45.0-153 9.39 22 107 102 70.0-123 5.17 20 106 99.6 73.0-121 6.27 20 ill 108 73.0-121 2.44 20 134 128 64.0-132 J4 4.51 20 PROJECT: SDG: DATE/TIME: PAGE: 02180643.01 L1060257 01/15/19 14:54 46 of 57 FP1 FTc FSS [Cn] FSr �GI FAI [Sc WG1222924 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260B L1060257-01,02,03,04,05,06,07,08,09,10,11 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375605-1 01/13/1911:52 • (LCSD) R3375605-2 01/13/1912:51 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Bromomethane 0.125 0.126 0.123 101 98.1 56.0-147 2.85 20 n-Butylbenzene 0.125 0.121 0.117 96.7 93.4 68.0-135 3.50 20 sec -Butyl benzene 0.125 0.151 0.143 121 115 74.0-130 5.12 20 tert-Butylbenzene 0.125 0.139 0.133 111 106 75.0-127 4.57 20 Carbon tetrachloride 0.125 0.146 0.137 117 110 66.0-128 6.42 20 Chlorobenzene 0.125 0.121 0.119 97.0 94.9 76.0-128 2.14 20 Chlorodibromomethane 0.125 0.142 0.138 114 110 74.0-127 2.92 20 Chloroethane 0.125 0.150 0.143 120 115 61.0-134 4.63 20 Chloroform 0.125 0.130 0.123 104 98.3 72.0-123 5.65 20 Chloromethane 0.125 0.132 0.124 105 98.9 51.0-138 6.34 20 2-Chlorotoluene 0.125 0.146 0.137 116 110 75.0-124 5.79 20 4-Chlorotoluene 0.125 0.140 0.134 112 107 75.0-124 3.98 20 1,2-Dibromo-3-Chloropropane 0.125 0.147 0.143 118 115 59.0-130 2.87 20 1,2-Dibromoethane 0.125 0.134 0.130 107 104 74.0-128 2.82 20 Dibromomethane 0.125 0.144 0.138 115 111 75.0-122 4.31 20 1,2-Dichlorobenzene 0.125 0.134 0.128 107 102 76.0-124 4.42 20 1,3-Dichlorobenzene 0.125 0.135 0.130 108 104 76.0-125 3.98 20 1,4-Dichlorobenzene 0.125 0.122 0.117 97.6 93.5 77.0-121 4.27 20 Dichlorodifluoromethane 0.125 0.126 0.122 101 97.3 43.0-156 3.41 20 1,1-Dichloroethane 0.125 0.140 0.132 112 106 70.0-127 5.93 20 1,2-Dichloroethane 0.125 0.139 0.132 111 105 65.0-131 5.47 20 1,1-Dichloroethene 0.125 0.141 0.134 113 108 65.0-131 4.78 20 cis-1,2-Dichloroethene 0.125 0.138 0.131 110 105 73.0-125 5.24 20 trans-1,2-Dichloroethene 0.125 0.131 0.124 104 99.4 71.0-125 4.99 20 1,2-Dichloropropane 0.125 0.137 0.133 109 106 74.0-125 2.90 20 1,1-Dichloropropene 0.125 0.136 0.132 109 106 73.0-125 2.66 20 1,3-Dichloropropane 0.125 0.137 0.133 110 106 80.0-125 3.27 20 cis-1,3-Dichloropropene 0.125 0.149 0.147 120 118 76.0-127 1.69 20 trans-1,3-Dichloropropene 0.125 0.149 0.146 119 117 73.0-127 2.10 20 2,2-Dichloropropane 0.125 0.138 0.129 111 103 59.0-135 6.67 20 Di -isopropyl ether 0.125 0.152 0.144 122 116 60.0-136 5.24 20 Ethylbenzene 0.125 0.136 0.134 109 107 74.0-126 1.87 20 Hexachloro-1,3-butadiene 0.125 0.111 0.108 88.7 86.2 57.0-150 2.82 20 Isopropylbenzene 0.125 0.129 0.122 103 97.7 72.0-127 5.57 20 p-Isopropyltoluene 0.125 0.140 0.134 112 108 72.0-133 4.26 20 2-Butanone (MEK) 0.625 0.875 0.824 140 132 30.0-160 5.97 24 Methylene Chloride 0.125 0.125 0.118 100 94.1 68.0-123 6.07 20 4-Methyl-2-pentanone (MIBK) 0.625 0.830 0.781 133 125 56.0-143 6.09 20 Methyl tert-butyl ether 0.125 0.154 0.142 123 114 66.0-132 7.91 20 Naphthalene 0.125 0.107 0.0988 85.7 79.1 59.0-130 8.02 20 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 47 of 57 WG1222924 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260B L1060257-01,02,03,04,05,06,07,08,09,10,11 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375605-1 01/13/1911:52 • (LCSD) R3375605-2 01/13/1912:51 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % n-Propylbenzene 0.125 0.132 0.124 106 99.2 74.0-126 6.12 20 Styrene 0.125 0.115 0.109 92.2 87.6 72.0-127 5.17 20 1,1,1,2-Tetrachloroethane 0.125 0.134 0.130 107 104 74.0-129 2.71 20 1,1,2,2-Tetrachloroethane 0.125 0.153 0.142 122 113 68.0-128 7.57 20 Tetrachloroethene 0.125 0.118 0.116 94.2 92.8 70.0-136 1.49 20 Toluene 0.125 0.109 0.106 87.1 84.8 75.0-121 2.68 20 1,1,2-Trichlorotrifluoroethane 0.125 0.137 0.128 110 103 61.0-139 6.83 20 1,2,3-Trichlorobenzene 0.125 0.0828 0.0801 66.2 64.1 59.0-139 3.30 20 1,2,4-Trichlorobenzene 0.125 0.0875 0.0842 70.0 67.4 62.0-137 3.75 20 1,1,1-Trichloroethane 0.125 0.151 0.141 121 113 69.0-126 6.71 20 1,1,2-Trichloroethane 0.125 0.136 0.133 109 106 78.0-123 2.19 20 Trichloroethene 0.125 0.146 0.144 117 115 76.0-126 1.33 20 Trichlorofluoromethane 0.125 0.133 0.127 106 101 61.0-142 4.65 20 1,2,3-Trichloropropane 0.125 0.157 0.147 125 117 67.0-129 6.68 20 1,2,4-Trimethylbenzene 0.125 0.128 0.122 103 97.2 70.0-126 5.36 20 1,3,5-Trimethyl benzene 0.125 0.148 0.141 118 113 73.0-127 4.74 20 Vinyl chloride 0.125 0.101 0.0989 81.0 79.1 63.0-134 2.33 20 Xylenes, Total 0.375 0.394 0.381 105 102 72.0-127 3.35 20 (S) Toluene-d8 96.3 97.8 75.0-131 (S) DibromoFluoromethane 104 101 65.0-129 (S) 4-Bromof/uorobenzene 107 105 67 0-138 ONE LAB. NATIONWIDE. FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 48 of 57 WG1223188 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1060257-08,09,10,11 Method Blank (MB) FP1(MB) R3375802-3 01/14/19 21:16 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg FTc n-Butylbenzene U 0.00384 0.0125 sec -Butyl benzene U 0.00253 0.0125 FSS Ethylbenzene U 0.000530 0.00250 Isopropylbenzene U 0.000863 0.00250 p-Isopropyltoluene U 0.00233 0.00500 rCn Naphthalene U 0.00312 0.0125 n-Propylbenzene U 0.00118 0.00500 FSr Toluene U 0.00125 0.00500 1,2,4-Trimethylbenzene U 0.00116 0.00500 1,3,5-Trimethyl benzene U 0.00108 0.00500 Xylenes, Total U 0.00478 0.00650 (S) Toluene-d8 116 75.0-131 G (S) Dibromofluoromethane 91.0 65.0-129 (S) 4-Bromof/uorobenzene 94.3 67.0-138 rAl Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FSC (LCS) R3375802-1 01/14/1919:33 • (LCSD) R3375802-2 01/14/19 19:54 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % n-Butylbenzene 0.125 0.104 0.0946 83.2 75.7 68.0-135 9.43 20 sec -Butyl benzene 0.125 0.108 0.0980 86.7 78.4 74.0-130 10.1 20 Ethylbenzene 0.125 0.112 0.107 89.2 85.5 74.0-126 4.19 20 Isopropylbenzene 0.125 0.103 0.0955 82.8 76.4 72.0-127 7.99 20 p-Isopropyltoluene 0.125 0.109 0.0991 87.5 79.3 72.0-133 9.85 20 Naphthalene 0.125 0.0937 0.0931 74.9 74.5 59.0-130 0.568 20 n-Propylbenzene 0.125 0.102 0.0929 81.7 74.3 74.0-126 9.49 20 Toluene 0.125 0.119 0.114 95.1 91.5 75.0-121 3.80 20 1,2,4-Trimethylbenzene 0.125 0.104 0.0953 83.4 76.2 70.0-126 9.02 20 1,3,5-Trimethyl benzene 0.125 0.104 0.0949 83.4 76.0 73.0-127 9.36 20 Xylenes, Total 0.375 0.406 0.378 108 101 72.0-127 7.14 20 (S) Toluene-d8 104 103 75.0-131 (S) Dibromofluoromethane 105 105 65.0-129 (S) 4-Bromofluorobenzene 94.9 9t 4 67.0-138 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 49 of 57 WG1222614 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1060257-01,02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3375591-3 01/14/19 03:21 MB Result MB Qualifier Analyte mg/kg Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anth race ne Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(g,h,i)perylene Benzo(a)pyrene B is(2-chlorethoxy)meth a ne Bis(2-ch loroethyl)ether Bis(2-chloroisopropyl)ether 4-Bromophenyl-phenylether 2-Chloronaphthalene 4-Chlorophenyl-phenylether Chrysene Dibenz(a,h)anthracene 3,3-Dichlorobenzidine 2,4-Dinitrotoluene 2,6-Dinitrotoluene Fluoranthene Fluorene Hexachlorobenzene Hexachloro-1,3-butadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene n-Nitrosodimethyla mine n-Nitrosodiphenylamine n-N itros o d i-n-p ro pyl a m i n e Phenanthrene Benzylbutyl phthalate B is(2-ethyl h exyl)phtha I ate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MB MDL mg/kg 0.00642 0.00671 0.00632 0.0637 0.00428 0.00695 0.00582 0.00721 0.00548 0.00770 0.00896 0.00760 0.0114 0.00639 0.00627 0.00555 0.00821 0.0794 0.00607 0.00737 0.00496 0.00682 0.00856 0.0100 0.0587 0.0134 0.00772 0.00522 0.00889 0.00695 0.0647 0.0900 0.00906 0.00528 0.0103 0.0120 0.0109 0.00691 0.00540 0.00907 MB RDL mg/kg 0.0333 0.0333 0.0333 0.333 0.0333 0.0333 0.0333 0.0333 0.0333 0.333 0.333 0.333 0.333 0.0333 0.333 0.0333 0.0333 0.333 0.333 0.333 0.0333 0.0333 0.333 0.333 0.333 0.333 0.0333 0.333 0.0333 0.333 0.333 0.333 0.333 0.0333 0.333 0.333 0.333 0.333 0.333 0.333 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 50 of 57 WG1222614 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1060257-01,02,03,04,05,06,07,08,09,10,11 ONE LAB. NATIONWIDE. Method Blank (MB) (MB) R3375591-3 01/14/19 03:21 MB Result MB Qualifier Analyte mg/kg Pyrene U 1,2,4-Trichlorobenzene U 4-ChIoro-3-methyl phenol U 2-Chlorophenol U 2,4-Dichlorophenol U 2,4-Dimethylphenol U 4,6-Dinitro-2-methylphenol U 2,4-Dinitrophenol U 2-Nitrophenol U 4-Nitrophenol U Pentachlorophenol U Phenol U 2,4,6-Trichlorophenol U (S) Nitrobenzene-d5 61.0 (S) 2-Fluorobiphenyl 54.1 (S) p-Terphenyl-d14 57.1 (S) Phenol-d5 58.6 (S) 2-F/uorophenol 64.7 (S)2,4,6-Tribromopheno/ 54.4 MB MDL mg/kg 0.0123 0.00876 0.00477 0.00831 0.00746 0.0471 0.124 0.0980 0.0130 0.0525 0.0480 0.00695 0.00779 MB RDL mg/kg 0.0333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 10.0-122 15.0-120 10.0-120 10.0-120 12.0-120 10.0-127 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375591-1 01/14/19 02:34 • (LCSD) R3375591-2 01/14/19 02:57 Spike Amount LCS Result LCSD Result Analyte mg/kg mg/kg mg/kg Acenaphthene 0.666 0.468 0.425 Acenaphthylene 0.666 0.478 0.429 Anthracene 0.666 0.467 0.423 Benzidine 0.666 ND ND Benzo(a)anth race ne 0.666 0.468 0.443 Benzo(b)fluoranthene 0.666 0.485 0.452 Benzo(k)fluoranthene 0.666 0.481 0.442 Benzo(g,h,i)perylene 0.666 0.503 0.497 Benzo(a)pyrene 0.666 0.486 0.449 Bis(2-chlorethoxy)methane 0.666 0.376 0.341 Bis(2-chloroethyl)ether 0.666 0.469 0.414 Bis(2-chloroisopropyl)ether 0.666 0.446 0.386 4-Bromophenyl-phenylether 0.666 0.469 0.421 2-Chloronaphthalene 0.666 0.448 0.397 ACCOUNT: Withers & Ravenel Eng. - Standard LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 70.3 63.8 38.0-120 9.63 22 71.8 64.4 40.0-120 10.8 22 70.1 63.5 42.0-120 9.89 20 0.000 0.000 1.00-120 J4 J4 0.000 40 70.3 66.5 44.0-120 5.49 20 72.8 67.9 43.0-120 7.04 22 72.2 66.4 44.0-120 8.45 21 75.5 74.6 43.0-120 1.20 22 73.0 67.4 45.0-120 7.91 20 56.5 51.2 20.0-120 9.76 23 70.4 62.2 16.0-120 12.5 31 67.0 58.0 23.0-120 14.4 30 70.4 63.2 40.0-120 10.8 21 67.3 59.6 35.0-120 12.1 24 PROJECT: SDG: DATE/TIME: PAGE: 02180643.01 L1060257 01/15/19 14:54 51 of 57 FP1 FTc FSS [Cn] FSr �GI FAI [Sc WG1222614 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1060257-01,02,03,04,05,06,07,08,09,10,11 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS) R3375591-1 01/14/19 02:34 • (LCSD) R3375591-2 01/14/19 02:57 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % z TC 4-Chlorophenyl-phenylether 0.666 0.467 0.419 70.1 62.9 40.0-120 10.8 22 Chrysene 0.666 0.478 0.444 71.8 66.7 43.0-120 7.38 20 FSS Dibenz(a,h)anthracene 0.666 0.492 0.485 73.9 72.8 44.0-120 1.43 22 3,3-Dichlorobenzidine 0.666 0.279 0.289 41.9 43.4 28.0-120 3.52 23 2,4-Dinitrotoluene 0.666 0.527 0.471 79.1 70.7 45.0-120 11.2 21 [Cn] 2,6-Dinitrotoluene 0.666 0.481 0.443 72.2 66.5 42.0-120 8.23 21 Fluoranthene 0.666 0.488 0.441 73.3 66.2 44.0-120 10.1 21 FSr Fluorene 0.666 0.473 0.429 71.0 64.4 41.0-120 9.76 22 Hexachlorobenzene 0.666 0.472 0.423 70.9 63.5 39.0-120 10.9 21 Hexachloro-1,3-butadiene 0.666 0.394 0.346 59.2 52.0 15.0-120 13.0 28 Hexachlorocyclopentadiene 0.666 0.468 0.407 70.3 61.1 15.0-120 13.9 31 Hexachloroethane 0.666 0.457 0.403 68.6 60.5 17.0-120 12.6 31 7G1 Indeno(1,2,3-cd)pyrene 0.666 0.497 0.485 74.6 72.8 45.0-120 2.44 21 Isophorone 0.666 0.417 0.372 62.6 55.9 23.0-120 11.4 23 Naphthalene 0.666 0.376 0.337 56.5 50.6 18.0-120 10.9 24 FAI Nitrobenzene 0.666 0.401 0.351 60.2 52.7 17.0-120 13.3 26 n-Nitrosodimethyla mine 0.666 0.472 0.388 70.9 58.3 10.0-125 19.5 33 FSC n-Nitrosodiphenylamine 0.666 0.473 0.416 71.0 62.5 40.0-120 12.8 21 n-Nitrosodi-n-propylamine 0.666 0.492 0.437 73.9 65.6 26.0-120 11.8 27 Phenanthrene 0.666 0.457 0.424 68.6 63.7 42.0-120 7.49 20 Benzylbutyl phthalate 0.666 0.534 0.508 80.2 76.3 40.0-120 4.99 21 Bis(2-ethylhexyl)phthalate 0.666 0.544 0.516 81.7 77.5 41.0-120 5.28 21 Di-n-butyl phthalate 0.666 0.541 0.489 81.2 73.4 43.0-120 10.1 20 Diethyl phthalate 0.666 0.527 0.486 79.1 73.0 43.0-120 8.09 21 Dimethyl phthalate 0.666 0.484 0.440 72.7 66.1 43.0-120 9.52 22 Di-n-octyl phthalate 0.666 0.534 0.508 80.2 76.3 40.0-120 4.99 21 Pyrene 0.666 0.489 0.454 73.4 68.2 41.0-120 7.42 21 1,2,4-Trichlorobenzene 0.666 0.377 0.327 56.6 49.1 17.0-120 14.2 26 4-Chloro-3-methylphenol 0.666 0.419 0.391 62.9 58.7 28.0-120 6.91 20 2-Chlorophenol 0.666 0.472 0.428 70.9 64.3 28.0-120 9.78 28 2,4-Dichlorophenol 0.666 0.405 0.373 60.8 56.0 25.0-120 8.23 21 2,4-Dimethylphenol 0.666 0.388 0.359 58.3 53.9 15.0-120 7.76 26 4,6-Dinitro-2-methylphenol 0.666 0.412 0.378 61.9 56.8 16.0-120 8.61 33 2,4-Dinitrophenol 0.666 0.298 0.285 44.7 42.8 10.0-120 4.46 40 2-Nitrophenol 0.666 0.430 0.382 64.6 57.4 20.0-120 11.8 25 4-Nitrophenol 0.666 0.493 0.467 74.0 70.1 27.0-120 5.42 24 Pentachlorophenol 0.666 0.465 0.425 69.8 63.8 29.0-120 8.99 25 Phenol 0.666 0.464 0.417 69.7 62.6 28.0-120 10.7 27 2,4,6-Trichlorophenol 0.666 0.459 0.418 68.9 62.8 37.0-120 9.35 24 (S) Nitrobenzene-d5 53.5 47.1 10.0-122 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 52 of 57 WG1222614 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1060257-01,02,03,04,05,06,07,08,09,10,11 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. (LCS) R3375591-1 01/14/19 02:34 • (LCSD) R3375591-2 01/14/19 02:57 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % (S) 2-Fluorobipheny/ 57.1 50.2 15.0-120 (S) p-Terphenyl-d14 61.3 55.3 10.0-120 (S) Phenol-d5 61.4 54.4 10.0-120 (S) 2-F/uorophenol 68.3 59.3 12.0-120 (S)2,4,6-Tribromopheno/ 65.0 55.1 10.0-127 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 53 of 57 FP1 FTC FSS [Cn] FSr �GI FAI FSC GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions (dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. RDL (dry) Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. J The identification of the analyte is acceptable; the reported value is an estimate. JO J0: Calibration verification outside of acceptance limits. Result is estimated. J1 Surrogate recovery limits have been exceeded; values are outside upper control limits. J4 The associated batch QC was outside the established quality control range for accuracy. J7 Surrogate recovery cannot be used for control limit evaluation due to dilution. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 54 of 57 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 5 Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T 104704245-17-14 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA ME MT NO OR MN T ID t WI NY SD WY MI NV t NE IA OH PA T f IL Ills WV vA UT T CA�� T KS MO KY N NM O� AR SC T MS AL`7GA T TX * LA T AK q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060257 01/15/19 14:54 55 of 57 mP r'I� y NameJAddres5 - 0vers & Ravenel Eng. i 15 W acKenan Drive l f ory r IN G 27511 Fte M prle�i Wheat Fields Development — VeSCr ipji3On; 919) 469-334Q erP�,l Froyeck u plane:2180643.0 fax r'nllaGt in(print}; SI#ejFariiityli l Billing{ Imfermabon! WITHRAVS - Regular WITHRAVS - Trust Fund WITHRAVS - 6200FULL WITHRAVS - STATE LEAD Ema;I Tv! i'r, II. C lie by{stgnaturel: { Rush? [tab MUST tie NvWledl vvv"1. 1 t + } — Same + 1 WVt oay ,,,,, ,,,,,,, ,, ]no% iataly f TwoiDay ......... pared a n ICE N Y 4j _ Three bay Sample ID C*rnpjGrab MatrU � t . � � U7 - k 4 1 •1' q LP withersraveneh om City/S#a#e ? O , ! [orr#ah,er{ Preservatrre Lab Project it LZ w � o r e� N _ ti m �F E pate Results Needed _ La 0 E a r Ema.l?_No _wes tF v E FAX? Na Yes NU. o d o Date TrrruE Mrs o CO 00 0"O4 tl� :CNInof{uslady pace-I-of�L 1140ESC L.n B &.0 I.E.N C E.S MISS LatwronRO 1�-1�' a%�I� ' MOun1 Mimi. TN 37122 M LJ I ur.:ais,?5arsssa �Pno :EOo-767-585y }- FmK: 615. 75R. 5056) l 1- �- E065 Acctnum. WITHRAVS Rmlog,rr; �- Wagner CoBler= Shipped via: RemL+�mnt.m.,ane Sampc C gab e.F,j 0� 6 -- �' 1S t31 1 4 to 10 Ali% - I-CirP4tn avatar - asteWaer�li rn nTkl`gVRaF2T-[rtls- Hold tt R r flow _ ❑thu ,q hod by : {Signs) a) mate; Time; Reo[±ived by: i S' —u•el - f mples returned via, I] UPS GdrrdItIOFk= (lab use only) L - 5 I ❑ fpdF.r L'1 1rWF ❑ hed by cur Date: Time: Rem ti. 4rl t J. C� „-Jr rgmp-�2 #C g[/4r* + V 9 COC Seal Intact: _ Y N NA R elr W6 - Tinier For lab by- CElignature I [ate; Timm pH Checked: Nick O �FaceAnalXical o National Center for Testing & Innovation r Ad ANALYTICAL REPORT January 15, 2019 Withers & Ravenel Eng. - Standard Sample Delivery Group: L1060264 Samples Received: 01/11/2019 Project Number: 02180643.01 Description: Wheat Fields Development Report To: Laura Elliott 115 MacKenan Drive Cary, NC 27511 Entire Report Reviewed By: 4�41 Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. V F# 4 + � k dk_ U I & 4b TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1 Fn Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 FS MW-1 L1060264-01 5 [Cn] MW-3 L1060264-02 8 MW-4 L1060264-03 11 FSr MW-5 L1060264-04 14 Qc: Quality Control Summary 17 RC Volatile Organic Compounds (GC/MS) by Method 8260B 17 GI Semi Volatile Organic Compounds (GC/MS) by Method 8270D 25 GI: Glossary of Terms 30 rAl Al: Accreditations & Locations 31 Sc: Sample Chain of Custody 32 FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 2 of 33 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time MW-1 L1060264-01 GW Laura Elliott 01/10/1915:05 01/11/1908:45 FP1 Method Batch Dilution Preparation Analysis Analyst date/time date/time FTC Volatile Organic Compounds (GC/MS) by Method 8260B WG1222574 50 01/12/19 03:02 01/12/19 03:02 JHH Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222625 1 01/14/19 06:48 01/14/1916:35 LEA Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222625 10 01/14/19 06:48 01/15/19 01:18 AO Collected by Collected date/time Received date/time [Cn] MW-3 L1060264-02 GW Laura Elliott 01/10/1914:30 01/11/1908:45 Method Batch Dilution Preparation Analysis Analyst FSr date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260E WG1222574 1 01/12/19 03:22 01/12/19 03:22 JHH 6 QC Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222625 1 01/14/19 06:48 01/14/1916:58 LEA 7G1 Collected by Collected date/time Received date/time MW-4 L1060264-03 GW Laura Elliott 01/10/1913:10 01/11/1908:45 FAI Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG1222574 1 01/12/19 03:42 01/12/19 03:42 JHH FSC Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222625 1 01/14/19 06:48 01/14/1917:22 LEA Collected by Collected date/time Received date/time MW-5 L1060264-04 GW Laura Elliott 01/10/1911:35 01/11/1908:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260E WG1223190 1 01/14/1916:29 01/14/1916:29 DWR Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1222625 1 01/14/19 06:48 01/14/1917:46 LEA ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 3 of 33 CASE NARRATIVE ONE LAB. NATIONWIDE. FP1 All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. FSr FC-1 4�j �GI Heather J Wagner FAI Project Manager FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 4 of 33 M W-1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 01/10/19 15:05 L1060264 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch u Analyte ug/I ug/I date /time Acetone ND 2500 50 01/12/2019 03:02 WG1222574 FTc Acrolein ND J4 2500 50 01/12/2019 03:02 WG1222574 Acrylonitrile ND J4 500 50 01/12/2019 03:02 WG1222574 F Benzene 501 50.0 50 01/12/2019 03:02 WG1222574 Bromobenzene ND 50.0 50 01/12/2019 03:02 WG1222574 Bromodichloromethane ND 50.0 50 01/12/2019 03:02 WG1222574 rCn Bromoform ND 50.0 50 01/12/2019 03:02 WG1222574 Bromomethane ND 250 50 01/12/2019 03:02 WG1222574 n-Butylbenzene ND 50.0 50 01/12/2019 03:02 WG1222574 sec -Butyl benzene ND 50.0 50 01/12/2019 03:02 WG1222574 ter[-Butylbenzene ND 50.0 50 01/12/2019 03:02 WG1222574 Fc Carbon tetrachloride ND 50.0 50 01/12/2019 03:02 WG1222574 Chlorobenzene ND 50.0 50 01/12/2019 03:02 WG1222574 Fq Chlorodibromomethane ND 50.0 50 01/12/2019 03:02 WG1222574 Chloroethane ND 250 50 01/12/2019 03:02 WG1222574 Chloroform ND 250 50 01/12/2019 03:02 WG1222574 FAI Chloromethane ND 125 50 01/12/2019 03:02 WG1222574 2-Chlorotoluene ND 50.0 50 01/12/2019 03:02 WG1222574 F 4-Chlorotoluene ND 50.0 50 01/12/2019 03:02 WG1222574 1,2-Dibromo-3-Chloropropane ND J4 250 50 01/12/2019 03:02 WG1222574 1,2-Dibromoethane ND 50.0 50 01/12/2019 03:02 WG1222574 Dibromomethane ND 50.0 50 01/12/2019 03:02 WG1222574 1,2-Dichlorobenzene ND 50.0 50 01/12/2019 03:02 WG1222574 1,3-Dichlorobenzene ND 50.0 50 01/12/2019 03:02 WG1222574 1,4-Dichlorobenzene ND 50.0 50 01/12/2019 03:02 WG1222574 Dichlorodifluoromethane ND 250 50 01/12/2019 03:02 WG1222574 1,1-Dichloroethane ND 50.0 50 01/12/2019 03:02 WG1222574 1,2-Dichloroethane ND 50.0 50 01/12/2019 03:02 WG1222574 1,1-Dichloroethene ND 50.0 50 01/12/2019 03:02 WG1222574 cis-1,2-Dichloroethene ND 50.0 50 01/12/2019 03:02 WG1222574 trans-1,2-Dichloroethene ND 50.0 50 01/12/2019 03:02 WG1222574 1,2-Dichloropropane ND 50.0 50 01/12/2019 03:02 WG1222574 1,1-Dichloropropene ND 50.0 50 01/12/2019 03:02 WG1222574 1,3-Dichloropropane ND 50.0 50 01/12/2019 03:02 WG1222574 cis-1,3-Dichloropropene ND 50.0 50 01/12/2019 03:02 WG1222574 trans-1,3-Dichloropropene ND 50.0 50 01/12/2019 03:02 WG1222574 2,2-Dichloropropane ND 50.0 50 01/12/2019 03:02 WG1222574 Di -isopropyl ether ND 50.0 50 01/12/2019 03:02 WG1222574 Ethylbenzene 2180 50.0 50 01/12/2019 03:02 WG1222574 Hexachloro-1,3-butadiene ND 50.0 50 01/12/2019 03:02 WG1222574 Isopropylbenzene 89.8 50.0 50 01/12/2019 03:02 WG1222574 p-Isopropyltoluene ND 50.0 50 01/12/2019 03:02 WG1222574 2-Butanone (MEK) ND 500 50 01/12/2019 03:02 WG1222574 Methylene Chloride ND 250 50 01/12/2019 03:02 WG1222574 4-Methyl-2-pentanone (MIBK) ND 500 50 01/12/2019 03:02 WG1222574 Methyl tert-butyl ether ND 50.0 50 01/12/2019 03:02 WG1222574 Naphthalene 581 250 50 01/12/2019 03:02 WG1222574 n-Propylbenzene 232 50.0 50 01/12/2019 03:02 WG1222574 Styrene ND 50.0 50 01/12/2019 03:02 WG1222574 1,1,1,2-Tetrachloroethane ND 50.0 50 01/12/2019 03:02 WG1222574 1,1,2,2-Tetrachloroethane ND 50.0 50 01/12/2019 03:02 WG1222574 1,1,2-Trichlorotrifluoroethane ND 50.0 50 01/12/2019 03:02 WG1222574 Tetrachloroethene ND 50.0 50 01/12/2019 03:02 WG1222574 Toluene 6220 50.0 50 01/12/2019 03:02 WG1222574 1,2,3-Trichlorobenzene ND 50.0 50 01/12/2019 03:02 WG1222574 1,2,4-Trichlorobenzene ND 50.0 50 01/12/2019 03:02 WG1222574 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 5 of 33 ONE LAB. NATIONWIDE. MW-1 SAMPLE RESULTS - 01 Collected date/time: 01/10/19 15:05 L1060264 Volatile Organic Compounds (GC/MS) by Method 8260B Result Analyte ug/I 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethylbenzene 1600 1,2,3-Trimethyl benzene 429 1,3,5-Trimethyl benzene 434 Vinyl chloride ND Xylenes, Total 11000 (S) Toluene-d8 108 (S) Dibromofluoromethane 101 (S) 4-Bromofluorobenzene 106 Semi Volatile Organic Compounds Qualifier RDL Dilution Analysis ug/I date / time 50.0 50 01/12/2019 03:02 50.0 50 01/12/2019 03:02 50.0 50 01/12/2019 03:02 250 50 01/12/2019 03:02 125 50 01/12/2019 03:02 50.0 50 01/12/2019 03:02 50.0 50 01/12/2019 03:02 50.0 50 01/12/2019 03:02 50.0 50 01/12/2019 03:02 150 50 01/12/2019 03:02 80.0-120 0111212019 03.02 75.0-120 0111212019 03.02 77.0-126 0111212019 03.02 (GC/MS) by Method 8270D Batch WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acenaphthene ND 1.00 1 01/14/201916:35 WG1222625 Acenaphthylene ND 1.00 1 01/14/201916:35 WG1222625 Anthracene ND 1.00 1 01/14/201916:35 WG1222625 Benzidine ND J3 10.0 1 01/14/201916:35 WG1222625 Benzo(a)anth race ne ND 1.00 1 01/14/201916:35 WG1222625 Benzo(b)fluoranthene ND 1.00 1 01/14/201916:35 WG1222625 Benzo(k)fluoranthene ND 1.00 1 01/14/201916:35 WG1222625 Benzo(g,h,i)perylene ND 1.00 1 01/14/201916:35 WG1222625 Benzo(a)pyrene ND 1.00 1 01/14/201916:35 WG1222625 Bis(2-chlorethoxy)methane ND 10.0 1 01/14/201916:35 WG1222625 Bis(2-chloroethyl)ether ND 10.0 1 01/14/201916:35 WG1222625 Bis(2-chloroisopropyl)ether ND 10.0 1 01/14/201916:35 WG1222625 4-Bromophenyl-phenylether ND 10.0 1 01/14/201916:35 WG1222625 2-Chloronaphthalene ND 1.00 1 01/14/201916:35 WG1222625 4-Chlorophenyl-phenylether ND 10.0 1 01/14/201916:35 WG1222625 Chrysene ND 1.00 1 01/14/201916:35 WG1222625 Dibenz(a,h)anthracene ND 1.00 1 01/14/201916:35 WG1222625 3,3-Dichlorobenzidine ND 10.0 1 01/14/201916:35 WG1222625 2,4-Dinitrotoluene ND 10.0 1 01/14/201916:35 WG1222625 2,6-Dinitrotoluene ND 10.0 1 01/14/201916:35 WG1222625 Fluoranthene ND 1.00 1 01/14/201916:35 WG1222625 Fluorene ND 1.00 1 01/14/201916:35 WG1222625 Hexachlorobenzene ND 1.00 1 01/14/201916:35 WG1222625 Hexachloro-1,3-butadiene ND 10.0 1 01/14/201916:35 WG1222625 Hexachlorocyclopentadiene ND 10.0 1 01/14/201916:35 WG1222625 Hexachloroethane ND 10.0 1 01/14/201916:35 WG1222625 Indeno(1,2,3-cd)pyrene ND 1.00 1 01/14/201916:35 WG1222625 Isophorone ND 10.0 1 01/14/201916:35 WG1222625 Naphthalene 273 10.0 10 01/15/2019 01:18 WG1222625 Nitrobenzene ND 10.0 1 01/14/201916:35 WG1222625 n-Nitrosodimethyla mine ND 10.0 1 01/14/201916:35 WG1222625 n-Nitrosodiphenyla mine ND 10.0 1 01/14/201916:35 WG1222625 n-Nitrosodi-n-propylamine ND 10.0 1 01/14/201916:35 WG1222625 Phenanthrene ND 1.00 1 01/14/201916:35 WG1222625 Benzylbutyl phthalate ND 3.00 1 01/14/201916:35 WG1222625 Bis(2-ethylhexyl)phthalate ND 3.00 1 01/14/201916:35 WG1222625 Di-n-butyl phthalate ND 3.00 1 01/14/201916:35 WG1222625 Diethyl phthalate ND 3.00 1 01/14/201916:35 WG1222625 Dimethyl phthalate ND 3.00 1 01/14/201916:35 WG1222625 ACCOUNT: PROJECT: SDG: DATE/TIME: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 Fp FTc FS Fn Fc F, FAI [Sc PAGE: 6 of 33 M W-1 Collected date/time: 01/10/19 15:05 Semi Volatile Organic Compounds SAMPLE RESULTS - 01 L1060264 (GC/MS) by Method 8270D ONE LAB. NATIONWIDE. Result Qualifier RDL Dilution Analysis Batch FP1 Analyte ug/I ug/I date / time Di-n-octyl phthalate ND 3.00 1 01/14/201916:35 WG1222625 FTc Pyrene ND 1.00 1 01/14/201916:35 WG1222625 1,2,4-Trichlorobenzene ND 10.0 1 01/14/201916:35 WG1222625 4-ChIoro-3-methylphenol ND 10.0 1 01/14/201916:35 WG1222625 FSS 2-Chorophenol ND 10.0 1 01/14/201916:35 WG1222625 2,4-Dichlorophenol ND 10.0 1 01/14/201916:35 WG1222625 rCn 2,4-Dimethylphenol 11.9 10.0 1 01/14/201916:35 WG1222625 4,6-Dinitro-2-methylphenol ND 10.0 1 01/14/201916:35 WG1222625 2,4-Dinitrophenol ND 10.0 1 01/14/201916:35 WG1222625 2-Nitrophenol ND 10.0 1 01/14/201916:35 WG1222625 4-Nitrophenol ND 10.0 1 01/14/201916:35 WG1222625 Fc Pentachlorophenol ND 10.0 1 01/14/201916:35 WG1222625 Phenol ND 10.0 1 01/14/201916:35 WG1222625 2,4,6-Trichlorophenol ND 10.0 1 01/14/201916:35 WG1222625 GI (S 2-F/uorophenol 57.7 10.0-120 01114120191635 WG1222625 (S2-Fluorophenol 57.7 10.0-120 0111512019 01:18 WG1222625 FAI (S) Phenol-d5 19.0 10.0-120 0111512019 01:18 WG1222625 (S Phenol-d5 25.3 10.0-120 011141201916.35 WG1222625 (S) Nitrobenzene-d5 53.5 10.0-127 011141201916:35 WG1222625 FSC (S Nitrobenzene-d5 47.7 10.0-127 0111512019 01:18 WG1222625 (S) 2-F/uorobipheny/ 53.3 10.0-130 01114120191635 WG1222625 (S 2-Fluorobiphenyl 48.5 10.0-130 0111512019 01:18 WG1222625 (S)2,4,6-Tribromopheno/ 40.5 10.0-155 0111512019 01:18 WG1222625 (52,4,6-Tribromopheno/ 63.2 10.0-155 01114120191635 WG1222625 (S) p-Terphenyl-d14 57.5 10.0-128 01114120191635 WG1222625 (S p-Terphenyl-d14 51.4 10.0-128 0111512019 01:18 WG1222625 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 7 of 33 MW-3 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 01/10/19 14:30 L1060264 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch u Analyte ug/I ug/I date /time Acetone ND 50.0 1 01/12/2019 03:22 WG1222574 FTc Acrolein ND J4 50.0 1 01/12/2019 03:22 WG1222574 Acrylonitrile ND J4 10.0 1 01/12/2019 03:22 WG1222574 F Benzene ND 1.00 1 01/12/2019 03:22 WG1222574 Bromobenzene ND 1.00 1 01/12/2019 03:22 WG1222574 Bromodichloromethane ND 1.00 1 01/12/2019 03:22 WG1222574 rCn Bromoform ND 1.00 1 01/12/2019 03:22 WG1222574 Bromomethane ND 5.00 1 01/12/2019 03:22 WG1222574 n-Butylbenzene ND 1.00 1 01/12/2019 03:22 WG1222574 sec -Butyl benzene ND 1.00 1 01/12/2019 03:22 WG1222574 ter[-Butylbenzene ND 1.00 1 01/12/2019 03:22 WG1222574 Fc Carbon tetrachloride ND 1.00 1 01/12/2019 03:22 WG1222574 Chlorobenzene ND 1.00 1 01/12/2019 03:22 WG1222574 Fq Chlorodibromomethane ND 1.00 1 01/12/2019 03:22 WG1222574 Chloroethane ND 5.00 1 01/12/2019 03:22 WG1222574 Chloroform ND 5.00 1 01/12/2019 03:22 WG1222574 FAI Chloromethane ND 2.50 1 01/12/2019 03:22 WG1222574 2-Chlorotoluene ND 1.00 1 01/12/2019 03:22 WG1222574 F 4-Chlorotoluene ND 1.00 1 01/12/2019 03:22 WG1222574 1,2-Dibromo-3-Chloropropane ND J4 5.00 1 01/12/2019 03:22 WG1222574 1,2-Dibromoethane ND 1.00 1 01/12/2019 03:22 WG1222574 Dibromomethane ND 1.00 1 01/12/2019 03:22 WG1222574 1,2-Dichlorobenzene ND 1.00 1 01/12/2019 03:22 WG1222574 1,3-Dichlorobenzene ND 1.00 1 01/12/2019 03:22 WG1222574 1,4-Dichlorobenzene ND 1.00 1 01/12/2019 03:22 WG1222574 Dichlorodifluoromethane ND 5.00 1 01/12/2019 03:22 WG1222574 1,1-Dichloroethane ND 1.00 1 01/12/2019 03:22 WG1222574 1,2-Dichloroethane ND 1.00 1 01/12/2019 03:22 WG1222574 1,1-Dichloroethene ND 1.00 1 01/12/2019 03:22 WG1222574 cis-1,2-Dichloroethene ND 1.00 1 01/12/2019 03:22 WG1222574 trans-1,2-Dichloroethene ND 1.00 1 01/12/2019 03:22 WG1222574 1,2-Dichloropropane ND 1.00 1 01/12/2019 03:22 WG1222574 1,1-Dichloropropene ND 1.00 1 01/12/2019 03:22 WG1222574 1,3-Dichloropropane ND 1.00 1 01/12/2019 03:22 WG1222574 cis-1,3-Dichloropropene ND 1.00 1 01/12/2019 03:22 WG1222574 trans-1,3-Dichloropropene ND 1.00 1 01/12/2019 03:22 WG1222574 2,2-Dichloropropane ND 1.00 1 01/12/2019 03:22 WG1222574 Di -isopropyl ether ND 1.00 1 01/12/2019 03:22 WG1222574 Ethylbenzene ND 1.00 1 01/12/2019 03:22 WG1222574 Hexachloro-1,3-butadiene ND 1.00 1 01/12/2019 03:22 WG1222574 Isopropylbenzene ND 1.00 1 01/12/2019 03:22 WG1222574 p-Isopropyltoluene ND 1.00 1 01/12/2019 03:22 WG1222574 2-Butanone (MEK) ND 10.0 1 01/12/2019 03:22 WG1222574 Methylene Chloride ND 5.00 1 01/12/2019 03:22 WG1222574 4-Methyl-2-pentanone (MIBK) ND 10.0 1 01/12/2019 03:22 WG1222574 Methyl tert-butyl ether ND 1.00 1 01/12/2019 03:22 WG1222574 Naphthalene ND 5.00 1 01/12/2019 03:22 WG1222574 n-Propylbenzene ND 1.00 1 01/12/2019 03:22 WG1222574 Styrene ND 1.00 1 01/12/2019 03:22 WG1222574 1,1,1,2-Tetrachloroethane ND 1.00 1 01/12/2019 03:22 WG1222574 1,1,2,2-Tetrachloroethane ND 1.00 1 01/12/2019 03:22 WG1222574 1,1,2-Trichlorotrifluoroethane ND 1.00 1 01/12/2019 03:22 WG1222574 Tetrachloroethene ND 1.00 1 01/12/2019 03:22 WG1222574 Toluene ND 1.00 1 01/12/2019 03:22 WG1222574 1,2,3-Trichlorobenzene ND 1.00 1 01/12/2019 03:22 WG1222574 1,2,4-Trichlorobenzene ND 1.00 1 01/12/2019 03:22 WG1222574 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 8 of 33 ONE LAB. NATIONWIDE. MW-3 SAMPLE RESULTS - 02 Collected date/time: 01/10/19 14:30 L1060264 Volatile Organic Compounds (GC/MS) by Method 8260B Result Analyte ug/I 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethylbenzene ND 1,2,3-Trimethyl benzene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND Xylenes, Total ND (S) Toluene-d8 104 (S) Dibromofluoromethane 105 (S) 4-Bromofluorobenzene 101 Semi Volatile Organic Compounds Qualifier RDL Dilution Analysis ug/I date / time 1.00 1 01/12/2019 03:22 1.00 1 01/12/2019 03:22 1.00 1 01/12/2019 03:22 5.00 1 01/12/2019 03:22 2.50 1 01/12/2019 03:22 1.00 1 01/12/2019 03:22 1.00 1 01/12/2019 03:22 1.00 1 01/12/2019 03:22 1.00 1 01/12/2019 03:22 3.00 1 01/12/2019 03:22 80.0-120 0111212019 0312 75.0-120 0111212019 0312 77.0-126 0111212019 0312 (GC/MS) by Method 8270D Batch WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acenaphthene ND 1.00 1 01/14/201916:58 WG1222625 Acenaphthylene ND 1.00 1 01/14/201916:58 WG1222625 Anthracene ND 1.00 1 01/14/201916:58 WG1222625 Benzidine ND J3 10.0 1 01/14/201916:58 WG1222625 Benzo(a)anth race ne ND 1.00 1 01/14/201916:58 WG1222625 Benzo(b)fluoranthene ND 1.00 1 01/14/201916:58 WG1222625 Benzo(k)fluoranthene ND 1.00 1 01/14/201916:58 WG1222625 Benzo(g,h,i)perylene ND 1.00 1 01/14/201916:58 WG1222625 Benzo(a)pyrene ND 1.00 1 01/14/201916:58 WG1222625 Bis(2-chlorethoxy)methane ND 10.0 1 01/14/201916:58 WG1222625 Bis(2-chloroethyl)ether ND 10.0 1 01/14/201916:58 WG1222625 Bis(2-chloroisopropyl)ether ND 10.0 1 01/14/201916:58 WG1222625 4-Bromophenyl-phenylether ND 10.0 1 01/14/201916:58 WG1222625 2-Chloronaphthalene ND 1.00 1 01/14/201916:58 WG1222625 4-Chlorophenyl-phenylether ND 10.0 1 01/14/201916:58 WG1222625 Chrysene ND 1.00 1 01/14/201916:58 WG1222625 Dibenz(a,h)anthracene ND 1.00 1 01/14/201916:58 WG1222625 3,3-Dichlorobenzidine ND 10.0 1 01/14/201916:58 WG1222625 2,4-Dinitrotoluene ND 10.0 1 01/14/201916:58 WG1222625 2,6-Dinitrotoluene ND 10.0 1 01/14/201916:58 WG1222625 Fluoranthene ND 1.00 1 01/14/201916:58 WG1222625 Fluorene ND 1.00 1 01/14/201916:58 WG1222625 Hexachlorobenzene ND 1.00 1 01/14/201916:58 WG1222625 Hexachloro-1,3-butadiene ND 10.0 1 01/14/201916:58 WG1222625 Hexachlorocyclopentadiene ND 10.0 1 01/14/201916:58 WG1222625 Hexachloroethane ND 10.0 1 01/14/201916:58 WG1222625 Indeno(1,2,3-cd)pyrene ND 1.00 1 01/14/201916:58 WG1222625 Isophorone ND 10.0 1 01/14/201916:58 WG1222625 Naphthalene ND 1.00 1 01/14/201916:58 WG1222625 Nitrobenzene ND 10.0 1 01/14/201916:58 WG1222625 n-Nitrosodimethyla mine ND 10.0 1 01/14/201916:58 WG1222625 n-Nitrosodiphenyla mine ND 10.0 1 01/14/201916:58 WG1222625 n-Nitrosodi-n-propylamine ND 10.0 1 01/14/201916:58 WG1222625 Phenanthrene ND 1.00 1 01/14/201916:58 WG1222625 Benzylbutyl phthalate ND 3.00 1 01/14/201916:58 WG1222625 Bis(2-ethylhexyl)phthalate ND 3.00 1 01/14/201916:58 WG1222625 Di-n-butyl phthalate ND 3.00 1 01/14/201916:58 WG1222625 Diethyl phthalate ND 3.00 1 01/14/201916:58 WG1222625 Dimethyl phthalate ND 3.00 1 01/14/201916:58 WG1222625 ACCOUNT: PROJECT: SDG: DATE/TIME: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 Fp FTc FS Fn N Fc F, FAI [Sc PAGE: 9 of 33 MW-3 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 01/10/19 14:30 L1060264 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result Qualifier RDL Dilution Analysis Batch FP1 Analyte ug/I ug/I date / time Di-n-octyl phthalate ND 3.00 1 01/14/201916:58 WG1222625 FTc Pyrene ND 1.00 1 01/14/201916:58 WG1222625 1,2,4-Trichlorobenzene ND 10.0 1 01/14/201916:58 WG1222625 4-ChIoro-3-methylphenol ND 10.0 1 01/14/201916:58 WG1222625 FSS 2-Chlorophenol ND 10.0 1 01/14/201916:58 WG1222625 2,4-Dichlorophenol ND 10.0 1 01/14/201916:58 WG1222625 rCn 2,4-Dimethylphenol ND 10.0 1 01/14/201916:58 WG1222625 4,6-Dinitro-2-methylphenol ND 10.0 1 01/14/201916:58 WG1222625 2,4-Dinitrophenol ND 10.0 1 01/14/201916:58 WG1222625 2-Nitrophenol ND 10.0 1 01/14/201916:58 WG1222625 4-Nitrophenol ND 10.0 1 01/14/201916:58 WG1222625 Fc Pentachlorophenol ND 10.0 1 01/14/201916:58 WG1222625 Phenol ND 10.0 1 01/14/201916:58 WG1222625 2,4,6-Trichlorophenol ND 10.0 1 01/14/201916:58 WG1222625 GI (S) 2-F/uorophenol 35.3 10.0-120 011141201916:58 WG1222625 (S Phenol-d5 19.9 10.0-120 011141201916:58 WG1222625 FAI (S) Nitrobenzene-d5 49.8 10.0-127 011141201916:58 WG1222625 (S 2-Fluorobiphenyl 53.3 10.0-130 011141201916:58 WG1222625 (S)Z4,6-Tribromopheno/ 44.7 10.0-155 011141201916:58 WG1222625 FSC (S p-Terphenyl-d14 54.4 10.0-128 011141201916:58 WG1222625 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 10 of 33 MW-4 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 01/10/19 13:10 L1060264 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch u Analyte ug/I ug/I date /time Acetone ND 50.0 1 01/12/2019 03:42 WG1222574 FTc Acrolein ND J4 50.0 1 01/12/2019 03:42 WG1222574 Acrylonitrile ND J4 10.0 1 01/12/2019 03:42 WG1222574 F Benzene ND 1.00 1 01/12/2019 03:42 WG1222574 Bromobenzene ND 1.00 1 01/12/2019 03:42 WG1222574 Bromodichloromethane ND 1.00 1 01/12/2019 03:42 WG1222574 rCn Bromoform ND 1.00 1 01/12/2019 03:42 WG1222574 Bromomethane ND 5.00 1 01/12/2019 03:42 WG1222574 n-Butylbenzene ND 1.00 1 01/12/2019 03:42 WG1222574 sec -Butyl benzene ND 1.00 1 01/12/2019 03:42 WG1222574 ter[-Butylbenzene ND 1.00 1 01/12/2019 03:42 WG1222574 Fc Carbon tetrachloride ND 1.00 1 01/12/2019 03:42 WG1222574 Chlorobenzene ND 1.00 1 01/12/2019 03:42 WG1222574 Fq Chlorodibromomethane ND 1.00 1 01/12/2019 03:42 WG1222574 Chloroethane ND 5.00 1 01/12/2019 03:42 WG1222574 Chloroform ND 5.00 1 01/12/2019 03:42 WG1222574 FAI Chloromethane ND 2.50 1 01/12/2019 03:42 WG1222574 2-Chlorotoluene ND 1.00 1 01/12/2019 03:42 WG1222574 F 4-Chlorotoluene ND 1.00 1 01/12/2019 03:42 WG1222574 1,2-Dibromo-3-Chloropropane ND J4 5.00 1 01/12/2019 03:42 WG1222574 1,2-Dibromoethane ND 1.00 1 01/12/2019 03:42 WG1222574 Dibromomethane ND 1.00 1 01/12/2019 03:42 WG1222574 1,2-Dichlorobenzene ND 1.00 1 01/12/2019 03:42 WG1222574 1,3-Dichlorobenzene ND 1.00 1 01/12/2019 03:42 WG1222574 1,4-Dichlorobenzene ND 1.00 1 01/12/2019 03:42 WG1222574 Dichlorodifluoromethane ND 5.00 1 01/12/2019 03:42 WG1222574 1,1-Dichloroethane ND 1.00 1 01/12/2019 03:42 WG1222574 1,2-Dichloroethane ND 1.00 1 01/12/2019 03:42 WG1222574 1,1-Dichloroethene ND 1.00 1 01/12/2019 03:42 WG1222574 cis-1,2-Dichloroethene ND 1.00 1 01/12/2019 03:42 WG1222574 trans-1,2-Dichloroethene ND 1.00 1 01/12/2019 03:42 WG1222574 1,2-Dichloropropane ND 1.00 1 01/12/2019 03:42 WG1222574 1,1-Dichloropropene ND 1.00 1 01/12/2019 03:42 WG1222574 1,3-Dichloropropane ND 1.00 1 01/12/2019 03:42 WG1222574 cis-1,3-Dichloropropene ND 1.00 1 01/12/2019 03:42 WG1222574 trans-1,3-Dichloropropene ND 1.00 1 01/12/2019 03:42 WG1222574 2,2-Dichloropropane ND 1.00 1 01/12/2019 03:42 WG1222574 Di -isopropyl ether ND 1.00 1 01/12/2019 03:42 WG1222574 Ethylbenzene ND 1.00 1 01/12/2019 03:42 WG1222574 Hexachloro-1,3-butadiene ND 1.00 1 01/12/2019 03:42 WG1222574 Isopropylbenzene ND 1.00 1 01/12/2019 03:42 WG1222574 p-Isopropyltoluene ND 1.00 1 01/12/2019 03:42 WG1222574 2-Butanone (MEK) ND 10.0 1 01/12/2019 03:42 WG1222574 Methylene Chloride ND 5.00 1 01/12/2019 03:42 WG1222574 4-Methyl-2-pentanone (MIBK) ND 10.0 1 01/12/2019 03:42 WG1222574 Methyl tert-butyl ether ND 1.00 1 01/12/2019 03:42 WG1222574 Naphthalene ND 5.00 1 01/12/2019 03:42 WG1222574 n-Propylbenzene ND 1.00 1 01/12/2019 03:42 WG1222574 Styrene ND 1.00 1 01/12/2019 03:42 WG1222574 1,1,1,2-Tetrachloroethane ND 1.00 1 01/12/2019 03:42 WG1222574 1,1,2,2-Tetrachloroethane ND 1.00 1 01/12/2019 03:42 WG1222574 1,1,2-Trichlorotrifluoroethane ND 1.00 1 01/12/2019 03:42 WG1222574 Tetrachloroethene ND 1.00 1 01/12/2019 03:42 WG1222574 Toluene ND 1.00 1 01/12/2019 03:42 WG1222574 1,2,3-Trichlorobenzene ND 1.00 1 01/12/2019 03:42 WG1222574 1,2,4-Trichlorobenzene ND 1.00 1 01/12/2019 03:42 WG1222574 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 11 of 33 ONE LAB. NATIONWIDE. MW-4 SAMPLE RESULTS - 03 Collected date/time: 01/10/19 13:10 L1060264 Volatile Organic Compounds (GC/MS) by Method 8260B Result Analyte ug/I 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethylbenzene ND 1,2,3-Trimethyl benzene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND Xylenes, Total ND (S) Toluene-d8 105 (S) Dibromofluoromethane 104 (S) 4-Bromofluorobenzene 104 Semi Volatile Organic Compounds Qualifier RDL Dilution Analysis ug/I date / time 1.00 1 01/12/2019 03:42 1.00 1 01/12/2019 03:42 1.00 1 01/12/2019 03:42 5.00 1 01/12/2019 03:42 2.50 1 01/12/2019 03:42 1.00 1 01/12/2019 03:42 1.00 1 01/12/2019 03:42 1.00 1 01/12/2019 03:42 1.00 1 01/12/2019 03:42 3.00 1 01/12/2019 03:42 80.0-120 0111212019 03:42 75.0-120 0111212019 03.42 77.0-126 0111212019 03:42 (GC/MS) by Method 8270D Batch WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 WG1222574 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acenaphthene ND 1.00 1 01/14/201917:22 WG1222625 Acenaphthylene ND 1.00 1 01/14/201917:22 WG1222625 Anthracene ND 1.00 1 01/14/201917:22 WG1222625 Benzidine ND J3 10.0 1 01/14/201917:22 WG1222625 Benzo(a)anth race ne ND 1.00 1 01/14/201917:22 WG1222625 Benzo(b)fluoranthene ND 1.00 1 01/14/201917:22 WG1222625 Benzo(k)fluoranthene ND 1.00 1 01/14/201917:22 WG1222625 Benzo(g,h,i)perylene ND 1.00 1 01/14/201917:22 WG1222625 Benzo(a)pyrene ND 1.00 1 01/14/201917:22 WG1222625 Bis(2-chlorethoxy)methane ND 10.0 1 01/14/201917:22 WG1222625 Bis(2-chloroethyl)ether ND 10.0 1 01/14/201917:22 WG1222625 Bis(2-chloroisopropyl)ether ND 10.0 1 01/14/201917:22 WG1222625 4-Bromophenyl-phenylether ND 10.0 1 01/14/201917:22 WG1222625 2-Chloronaphthalene ND 1.00 1 01/14/201917:22 WG1222625 4-Chlorophenyl-phenylether ND 10.0 1 01/14/201917:22 WG1222625 Chrysene ND 1.00 1 01/14/201917:22 WG1222625 Dibenz(a,h)anthracene ND 1.00 1 01/14/201917:22 WG1222625 3,3-Dichlorobenzidine ND 10.0 1 01/14/201917:22 WG1222625 2,4-Dinitrotoluene ND 10.0 1 01/14/201917:22 WG1222625 2,6-Dinitrotoluene ND 10.0 1 01/14/201917:22 WG1222625 Fluoranthene ND 1.00 1 01/14/201917:22 WG1222625 Fluorene ND 1.00 1 01/14/201917:22 WG1222625 Hexachlorobenzene ND 1.00 1 01/14/201917:22 WG1222625 Hexachloro-1,3-butadiene ND 10.0 1 01/14/201917:22 WG1222625 Hexachlorocyclopentadiene ND 10.0 1 01/14/201917:22 WG1222625 Hexachloroethane ND 10.0 1 01/14/201917:22 WG1222625 Indeno(1,2,3-cd)pyrene ND 1.00 1 01/14/201917:22 WG1222625 Isophorone ND 10.0 1 01/14/201917:22 WG1222625 Naphthalene ND 1.00 1 01/14/201917:22 WG1222625 Nitrobenzene ND 10.0 1 01/14/201917:22 WG1222625 n-Nitrosodimethyla mine ND 10.0 1 01/14/201917:22 WG1222625 n-Nitrosodiphenyla mine ND 10.0 1 01/14/201917:22 WG1222625 n-Nitrosodi-n-propylamine ND 10.0 1 01/14/201917:22 WG1222625 Phenanthrene ND 1.00 1 01/14/201917:22 WG1222625 Benzylbutyl phthalate ND 3.00 1 01/14/201917:22 WG1222625 Bis(2-ethylhexyl)phthalate ND 3.00 1 01/14/201917:22 WG1222625 Di-n-butyl phthalate ND 3.00 1 01/14/201917:22 WG1222625 Diethyl phthalate ND 3.00 1 01/14/201917:22 WG1222625 Dimethyl phthalate ND 3.00 1 01/14/201917:22 WG1222625 ACCOUNT: PROJECT: SDG: DATE/TIME: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 Fp FTc FS Fn N Fc F, FAI [Sc PAGE: 12 of 33 MW-4 SAMPLE RESULTS - 03 Collected date/time: 01/10/19 13:10 L1060264 Semi Volatile Organic Compounds (GC/MS) by Method 8270D ONE LAB. NATIONWIDE. Analyte Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result Qualifier RDL Dilution Analysis ug/I ug/I date / time ND 3.00 1 01/14/201917:22 ND 1.00 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 ND 10.0 1 01/14/201917:22 32.3 10.0-120 011141201917.22 19.6 10.0-120 011141201917.22 42.2 10.0-127 011141201917.22 42.2 10.0-130 011141201917.22 38.8 10.0-155 011141201917.22 54.6 10.0-128 011141201917.22 Batch WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 Cp FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 13 of 33 MW-5 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 01/10/19 11:35 L1060264 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch u Analyte ug/I ug/I date /time Acetone ND 50.0 1 01/14/201916:29 WG1223190 FTc Acrolein ND J4 50.0 1 01/14/201916:29 WG1223190 Acrylonitrile ND 10.0 1 01/14/201916:29 WG1223190 F Benzene ND 1.00 1 01/14/201916:29 WG1223190 Bromobenzene ND 1.00 1 01/14/201916:29 WG1223190 Bromodichloromethane ND 1.00 1 01/14/201916:29 WG1223190 rCn Bromoform ND 1.00 1 01/14/201916:29 WG1223190 Bromomethane ND 5.00 1 01/14/201916:29 WG1223190 n-Butylbenzene ND 1.00 1 01/14/201916:29 WG1223190 sec -Butyl benzene ND 1.00 1 01/14/201916:29 WG1223190 ter[-Butylbenzene ND 1.00 1 01/14/201916:29 WG1223190 Fc Carbon tetrachloride ND 1.00 1 01/14/201916:29 WG1223190 Chlorobenzene ND 1.00 1 01/14/201916:29 WG1223190 Fq Chlorodibromomethane ND 1.00 1 01/14/201916:29 WG1223190 Chloroethane ND 5.00 1 01/14/201916:29 WG1223190 Chloroform ND 5.00 1 01/14/201916:29 WG1223190 FAI Chloromethane ND J4 2.50 1 01/14/201916:29 WG1223190 2-Chlorotoluene ND 1.00 1 01/14/201916:29 WG1223190 F 4-Chlorotoluene ND 1.00 1 01/14/201916:29 WG1223190 1,2-Dibromo-3-Chloropropane ND 5.00 1 01/14/201916:29 WG1223190 1,2-Dibromoethane ND 1.00 1 01/14/201916:29 WG1223190 Dibromomethane ND 1.00 1 01/14/201916:29 WG1223190 1,2-Dichlorobenzene ND 1.00 1 01/14/201916:29 WG1223190 1,3-Dichlorobenzene ND 1.00 1 01/14/201916:29 WG1223190 1,4-Dichlorobenzene ND 1.00 1 01/14/201916:29 WG1223190 Dichlorodifluoromethane ND 5.00 1 01/14/201916:29 WG1223190 1,1-Dichloroethane ND 1.00 1 01/14/201916:29 WG1223190 1,2-Dichloroethane ND 1.00 1 01/14/201916:29 WG1223190 1,1-Dichloroethene ND 1.00 1 01/14/201916:29 WG1223190 cis-1,2-Dichloroethene ND 1.00 1 01/14/201916:29 WG1223190 trans-1,2-Dichloroethene ND 1.00 1 01/14/201916:29 WG1223190 1,2-Dichloropropane ND 1.00 1 01/14/201916:29 WG1223190 1,1-Dichloropropene ND 1.00 1 01/14/201916:29 WG1223190 1,3-Dichloropropane ND 1.00 1 01/14/201916:29 WG1223190 cis-1,3-Dichloropropene ND 1.00 1 01/14/201916:29 WG1223190 trans-1,3-Dichloropropene ND 1.00 1 01/14/201916:29 WG1223190 2,2-Dichloropropane ND 1.00 1 01/14/201916:29 WG1223190 Di -isopropyl ether ND 1.00 1 01/14/201916:29 WG1223190 Ethylbenzene ND 1.00 1 01/14/201916:29 WG1223190 Hexachloro-1,3-butadiene ND 1.00 1 01/14/201916:29 WG1223190 Isopropylbenzene ND 1.00 1 01/14/201916:29 WG1223190 p-Isopropyltoluene ND 1.00 1 01/14/201916:29 WG1223190 2-Butanone (MEK) ND 10.0 1 01/14/201916:29 WG1223190 Methylene Chloride ND 5.00 1 01/14/201916:29 WG1223190 4-Methyl-2-pentanone (MIBK) ND J4 10.0 1 01/14/201916:29 WG1223190 Methyl tert-butyl ether ND 1.00 1 01/14/201916:29 WG1223190 Naphthalene ND 5.00 1 01/14/201916:29 WG1223190 n-Propylbenzene ND 1.00 1 01/14/201916:29 WG1223190 Styrene ND 1.00 1 01/14/201916:29 WG1223190 1,1,1,2-Tetrachloroethane ND 1.00 1 01/14/201916:29 WG1223190 1,1,2,2-Tetrachloroethane ND 1.00 1 01/14/201916:29 WG1223190 1,1,2-Trichlorotrifluoroethane ND 1.00 1 01/14/201916:29 WG1223190 Tetrachloroethene ND 1.00 1 01/14/201916:29 WG1223190 Toluene ND 1.00 1 01/14/201916:29 WG1223190 1,2,3-Trichlorobenzene ND 1.00 1 01/14/201916:29 WG1223190 1,2,4-Trichlorobenzene ND 1.00 1 01/14/201916:29 WG1223190 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 14 of 33 ONE LAB. NATIONWIDE. MW-5 SAMPLE RESULTS - 04 Collected date/time: 01/10/19 11:35 L1060264 Volatile Organic Compounds (GC/MS) by Method 8260B Result Analyte ug/I 1,1,1-Trichloroethane ND 1,1,2-Trichloroethane ND Trichloroethene ND Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethylbenzene ND 1,2,3-Trimethyl benzene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND Xylenes, Total ND (S) Toluene-d8 113 (S) Dibromofluoromethane 89.4 (S)4-Bromofluorobenzene 102 Semi Volatile Organic Compounds Qualifier RDL Dilution Analysis ug/I date / time 1.00 1 01/14/201916:29 1.00 1 01/14/201916:29 1.00 1 01/14/201916:29 5.00 1 01/14/201916:29 2.50 1 01/14/201916:29 1.00 1 01/14/201916:29 1.00 1 01/14/201916:29 1.00 1 01/14/201916:29 1.00 1 01/14/201916:29 3.00 1 01/14/201916:29 80.0-120 011141201916:29 75.0-120 011141201916:29 77.0-126 011141201916:29 (GC/MS) by Method 8270D Batch WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 WG1223190 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acenaphthene ND 1.00 1 01/14/201917:46 WG1222625 Acenaphthylene ND 1.00 1 01/14/201917:46 WG1222625 Anthracene ND 1.00 1 01/14/201917:46 WG1222625 Benzidine ND J3 10.0 1 01/14/201917:46 WG1222625 Benzo(a)anth race ne ND 1.00 1 01/14/201917:46 WG1222625 Benzo(b)fluoranthene ND 1.00 1 01/14/201917:46 WG1222625 Benzo(k)fluoranthene ND 1.00 1 01/14/201917:46 WG1222625 Benzo(g,h,i)perylene ND 1.00 1 01/14/201917:46 WG1222625 Benzo(a)pyrene ND 1.00 1 01/14/201917:46 WG1222625 Bis(2-chlorethoxy)methane ND 10.0 1 01/14/201917:46 WG1222625 Bis(2-chloroethyl)ether ND 10.0 1 01/14/201917:46 WG1222625 Bis(2-chloroisopropyl)ether ND 10.0 1 01/14/201917:46 WG1222625 4-Bromophenyl-phenylether ND 10.0 1 01/14/201917:46 WG1222625 2-Chloronaphthalene ND 1.00 1 01/14/201917:46 WG1222625 4-Chlorophenyl-phenylether ND 10.0 1 01/14/201917:46 WG1222625 Chrysene ND 1.00 1 01/14/201917:46 WG1222625 Dibenz(a,h)anthracene ND 1.00 1 01/14/201917:46 WG1222625 3,3-Dichlorobenzidine ND 10.0 1 01/14/201917:46 WG1222625 2,4-Dinitrotoluene ND 10.0 1 01/14/201917:46 WG1222625 2,6-Dinitrotoluene ND 10.0 1 01/14/201917:46 WG1222625 Fluoranthene ND 1.00 1 01/14/201917:46 WG1222625 Fluorene ND 1.00 1 01/14/201917:46 WG1222625 Hexachlorobenzene ND 1.00 1 01/14/201917:46 WG1222625 Hexachloro-1,3-butadiene ND 10.0 1 01/14/201917:46 WG1222625 Hexachlorocyclopentadiene ND 10.0 1 01/14/201917:46 WG1222625 Hexachloroethane ND 10.0 1 01/14/201917:46 WG1222625 Indeno(1,2,3-cd)pyrene ND 1.00 1 01/14/201917:46 WG1222625 Isophorone ND 10.0 1 01/14/201917:46 WG1222625 Naphthalene ND 1.00 1 01/14/201917:46 WG1222625 Nitrobenzene ND 10.0 1 01/14/201917:46 WG1222625 n-Nitrosodimethyla mine ND 10.0 1 01/14/201917:46 WG1222625 n-Nitrosodiphenyla mine ND 10.0 1 01/14/201917:46 WG1222625 n-Nitrosodi-n-propylamine ND 10.0 1 01/14/201917:46 WG1222625 Phenanthrene ND 1.00 1 01/14/201917:46 WG1222625 Benzylbutyl phthalate ND 3.00 1 01/14/201917:46 WG1222625 Bis(2-ethylhexyl)phthalate ND 3.00 1 01/14/201917:46 WG1222625 Di-n-butyl phthalate ND 3.00 1 01/14/201917:46 WG1222625 Diethyl phthalate ND 3.00 1 01/14/201917:46 WG1222625 Dimethyl phthalate ND 3.00 1 01/14/201917:46 WG1222625 ACCOUNT: PROJECT: SDG: DATE/TIME: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 Fp FTc FS Fn N Fc F, FAI [Sc PAGE: 15 of 33 MW-5 SAMPLE RESULTS - 04 Collected date/time: 01/10/19 11:35 L1060264 Semi Volatile Organic Compounds (GC/MS) by Method 8270D ONE LAB. NATIONWIDE. Analyte Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene 4-Ch I oro-3-m ethyl phenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Di n itro-2-methyl phen of 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol (S) 2-F/uorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 2,4,6-Tribromophenol (S) p-Terphenyl-d14 Result Qualifier RDL Dilution Analysis ug/I ug/I date / time ND 3.00 1 01/14/201917:46 ND 1.00 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 ND 10.0 1 01/14/201917:46 34.7 10.0-120 011141201917.46 20.2 10.0-120 011141201917.46 48.5 10.0-127 011141201917:46 51.4 10.0-130 011141201917.46 41.0 10.0-155 011141201917.46 53.2 10.0-128 011141201917.46 Batch WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 WG1222625 Cp FTc FSS 4 Cn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 16 of 33 WG1222574 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1060264-01,02,03 Method Blank (MB) (MB) R3375607-4 01/11/19 21:24 MB Result Analyte ug/I Acetone U Acrolein U Acrylonitrile U Benzene U Bromobenzene U Bromodichloromethane U Bromoform U Bromomethane U n-Butylbenzene U sec -Butyl benzene U tert-Butylbenzene U Carbon tetrachloride U Chlorobenzene U Chlorodibromomethane U Chloroethane U Chloroform U Chloromethane U 2-Chlorotoluene U 4-Chlorotoluene U 1,2-Dibromo-3-Chloropropane U 1,2-Dibromoethane U Dibromomethane U 1,2-Dichlorobenzene U 1,3-Dichlorobenzene U 1,4-Dichlorobenzene U Dichlorodifluoromethane U 1,1-Dichloroethane U 1,2-Dichloroethane U 1,1-Dichloroethene U cis-1,2-Dichloroethene U trans-1,2-Dichloroethene U 1,2-Dichloropropane U 1,1-Dichloropropene U 1,3-Dichloropropane U cis-1,3-Dichloropropene U trans-1,3-Dichloropropene U 2,2-Dichloropropane U Di -isopropyl ether U Ethylbenzene U Hexachloro-1,3-butadiene U MB Qualifier MB MDL MB RDL ug/I ug/I 10.0 50.0 8.87 50.0 1.87 10.0 0.331 1.00 0.352 1.00 0.380 1.00 0.469 1.00 0.866 5.00 0.361 1.00 0.365 1.00 0.399 1.00 0.379 1.00 0.348 1.00 0.327 1.00 0.453 5.00 0.324 5.00 0.276 2.50 0.375 1.00 0.351 1.00 1.33 5.00 0.381 1.00 0.346 1.00 0.349 1.00 0.220 1.00 0.274 1.00 0.551 5.00 0.259 1.00 0.361 1.00 0.398 1.00 0.260 1.00 0.396 1.00 0.306 1.00 0.352 1.00 0.366 1.00 0.418 1.00 0.419 1.00 0.321 1.00 0.320 1.00 0.384 1.00 0.256 1.00 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 17 of 33 WG1222574 Volatile Organic Compounds (GC/MS) by Method 8260B Method Blank (MB) (MB) R3375607-4 01/11/19 21:24 MB Result Analyte ug/I Isopropylbenzene U p-Isopropyltoluene U 2-Butanone (MEK) U Methylene Chloride U 4-Methyl-2-pentanone (MIBK) U Methyl tert-butyl ether U Naphthalene U n-Propylbenzene U Styrene U 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U Tetrachloroethene U Toluene U 1,1,2-Trichlorotrifluoroethane U 1,2,3-Trichlorobenzene U 1,2,4-Trichlorobenzene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichlorofluoromethane U 1,2,3-Trichloropropane U 1,2,3-Trimethyl benzene U 1,2,4-Trimethylbenzene U 1,3,5-Trimethyl benzene U Vinyl chloride U Xylenes, Total U (S) Toluene-d8 105 (S) Dibromofluoromethane 101 (S) 4-Bromof/uorobenzene 102 MB Qualifier MB MDL MB RDL ug/I ug/I QUALITY CONTROL SUMMARY L1060264-01,02,03 0.326 1.00 0.350 1.00 3.93 10.0 1.00 5.00 2.14 10.0 0.367 1.00 1.00 5.00 0.349 1.00 0.307 1.00 0.385 1.00 0.130 1.00 0.372 1.00 0.412 1.00 0.303 1.00 0.230 1.00 0.355 1.00 0.319 1.00 0.383 1.00 0.398 1.00 1.20 5.00 0.807 2.50 0.321 1.00 0.373 1.00 0.387 1.00 0.259 1.00 1.06 3.00 80.0-120 75.0-120 77.0-126 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375607-1 01/11/1919:44 • (LCSD) R3375607-2 01/11/19 20:04 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits Analyte ug/I ug/I ug/I % % % Acetone 125 158 168 Acrolein 125 238 233 Acrylonitrile 125 187 189 Benzene 25.0 24.1 24.7 127 191 150 96.5 134 186 151 99.0 19.0-160 10.0-160 55.0-149 70.0-123 LCS Qualifier LCSD Qualifier RPD 5.99 J4 J4 2.43 J4 J4 0.792 2.51 RPD Limits 27 26 20 20 ONE LAB. NATIONWIDE. FP1 FTc FSS 4 Cn FSr �GI FAI [Sc ACCOUNT: PROJECT: SDG: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 DATE/TIME: 01/15/19 15:06 PAGE: 18 of 33 WG1222574 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260B L1060264-01,02,03 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375607-1 01/11/1919:44 • (LCSD) R3375607-2 01/11/19 20:04 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I Bromobenzene 25.0 24.7 24.8 Bromodichloromethane 25.0 24.6 24.8 Bromoform 25.0 28.2 28.1 Bromomethane 25.0 23.4 24.6 n-Butylbenzene 25.0 26.6 27.6 sec -Butyl benzene 25.0 25.5 26.3 tert-Butylbenzene 25.0 25.9 26.1 Carbon tetrachloride 25.0 23.6 23.9 Chlorobenzene 25.0 26.6 26.0 Chlorodibromomethane 25.0 26.4 25.8 Chloroethane 25.0 33.1 32.7 Chloroform 25.0 25.3 25.2 Chloromethane 25.0 23.4 24.0 2-Chlorotoluene 25.0 26.7 27.0 4-Chlorotoluene 25.0 25.7 26.2 1,2-Dibromo-3-Chloropropane 25.0 37.4 39.3 1,2-Dibromoethane 25.0 27.1 26.5 Dibromomethane 25.0 25.8 25.9 1,2-Dichlorobenzene 25.0 25.9 26.2 1,3-Dichlorobenzene 25.0 24.6 25.0 1,4-Dichlorobenzene 25.0 26.0 24.8 Dichlorodifluoromethane 25.0 34.7 35.4 1,1-Dichloroethane 25.0 24.9 24.6 1,2-Dichloroethane 25.0 25.1 24.7 1,1-Dichloroethene 25.0 28.1 27.6 cis-1,2-Dichloroethene 25.0 25.3 25.1 trans-1,2-Dichloroethene 25.0 26.9 26.7 1,2-Dichloropropane 25.0 25.7 25.5 1,1-Dichloropropene 25.0 26.3 26.1 1,3-Dichloropropane 25.0 24.9 24.7 cis-1,3-Dichloropropene 25.0 27.0 26.8 trans-1,3-Dichloropropene 25.0 28.4 28.0 2,2-Dichloropropane 25.0 24.4 24.0 Di -isopropyl ether 25.0 25.1 24.6 Ethylbenzene 25.0 26.6 26.3 Hexachloro-1,3-butadiene 25.0 26.9 28.1 Isopropylbenzene 25.0 26.9 27.6 p-Isopropyltoluene 25.0 26.7 26.5 2-Butanone (MEK) 125 179 185 Methylene Chloride 25.0 24.1 23.9 ACCOUNT: Withers & Ravenel Eng. - Standard LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 98.9 99.3 73.0-121 0.427 20 98.5 99.1 75.0-120 0.645 20 113 112 68.0-132 0.267 20 93.7 98.4 10.0-160 4.90 25 106 110 73.0-125 3.68 20 102 105 75.0-125 3.20 20 104 105 76.0-124 0.939 20 94.5 95.5 68.0-126 1.05 20 106 104 80.0-121 1.97 20 106 103 77.0-125 2.19 20 132 131 47.0-150 1.25 20 101 101 73.0-120 0.334 20 93.5 95.9 41.0-142 2.55 20 107 108 76.0-123 1.22 20 103 105 75.0-122 2.01 20 150 157 58.0-134 J4 J4 4.81 20 108 106 80.0-122 1.94 20 103 104 80.0-120 0.175 20 103 105 79.0-121 1.21 20 98.3 100 79.0-120 1.77 20 104 99.2 79.0-120 4.73 20 139 142 51.0-149 1.92 20 99.6 98.4 70.0-126 1.26 20 100 98.9 70.0-128 1.40 20 113 111 71.0-124 1.80 20 101 100 73.0-120 0.779 20 108 107 73.0-120 0.775 20 103 102 77.0-125 0.858 20 105 104 74.0-126 0.701 20 99.6 98.9 80.0-120 0.704 20 108 107 80.0-123 0.848 20 114 112 78.0-124 1.52 20 97.7 95.8 58.0-130 2.01 20 100 98.3 58.0-138 2.25 20 106 105 79.0-123 0.959 20 107 112 54.0-138 4.54 20 108 110 76.0-127 2.39 20 107 106 76.0-125 0.507 20 143 148 44.0-160 3.77 20 96.4 95.8 67.0-120 0.661 20 PROJECT: SDG: DATE/TIME: PAGE: 02180643.01 L1060264 01/15/19 15:06 19 of 33 FP1 FTC FSS [Cn] FSr �GI FAI FSC WG1222574 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260B L1060264-01,02,03 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375607-1 01/11/1919:44 • (LCSD) R3375607-2 01/11/19 20:04 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I 4-Methyl-2-pentanone (MIBK) 125 164 163 Methyl tert-butyl ether 25.0 24.6 24.3 Naphthalene 25.0 31.3 32.8 n-Propylbenzene 25.0 26.5 27.1 Styrene 25.0 28.5 29.1 1,1,1,2-Tetrachloroethane 25.0 26.0 26.2 1,1,2,2-Tetrachloroethane 25.0 28.6 28.2 Tetrachloroethene 25.0 27.3 27.5 Toluene 25.0 24.9 24.8 1,1,2-Trichlorotrifluoroethane 25.0 27.2 27.6 1,2,3-Trichlorobenzene 25.0 31.2 33.2 1,2,4-Trichlorobenzene 25.0 26.5 29.2 1,1,1-Trichloroethane 25.0 25.1 25.1 1,1,2-Trichloroethane 25.0 26.1 25.8 Trichloroethene 25.0 25.9 26.4 Trichlorofluoromethane 25.0 27.4 27.3 1,2,3-Trichloropropane 25.0 32.0 31.7 1,2,3-Trimethylbenzene 25.0 25.4 24.4 1,2,4-Trimethylbenzene 25.0 24.5 24.7 1,3,5-Trimethyl benzene 25.0 26.0 26.0 Vinyl chloride 25.0 26.6 26.6 Xylenes, Total 75.0 78.8 78.0 (S) Toluene-d8 (S) DibromoFluoromethane (S) 4-Bromof/uorobenzene LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 131 131 68.0-142 0.685 20 98.5 97.2 68.0-125 1.41 20 125 131 54.0-135 4.74 20 106 108 77.0-124 2.25 20 114 116 73.0-130 1.94 20 104 105 75.0-125 0.704 20 115 113 65.0-130 1.62 20 109 110 72.0-132 0.742 20 99.5 99.4 79.0-120 0.117 20 109 110 69.0-132 1.46 20 125 133 50.0-138 6.36 20 106 117 57.0-137 9.48 20 101 100 73.0-124 0.219 20 104 103 80.0-120 1.02 20 104 106 78.0-124 1.97 20 110 109 59.0-147 0.188 20 128 127 73.0-130 0.790 20 102 97.6 77.0-120 4.05 20 98.1 99.0 76.0-121 0.836 20 104 104 76.0-122 0.229 20 106 106 67.0-131 0.0884 20 105 104 79.0-123 1.02 20 107 104 80.0-120 101 100 75.0-120 103 108 77.0-126 ONE LAB. NATIONWIDE. FP1 FTC FSS 4 Cn FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 20 of 33 WG1223190 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1060264-04 Method Blank (MB) (MB) R3375787-2 01/14/1915:50 MB Result Analyte ug/I Acetone U Acrolein U Acrylonitrile U Benzene U Bromobenzene U Bromodichloromethane U Bromoform U Bromomethane U n-Butylbenzene U sec -Butyl benzene U tert-Butylbenzene U Carbon tetrachloride U Chlorobenzene U Chlorodibromomethane U Chloroethane U Chloroform U Chloromethane U 2-Chlorotoluene U 4-Chlorotoluene U 1,2-Dibromo-3-Chloropropane U 1,2-Dibromoethane U Dibromomethane U 1,2-Dichlorobenzene U 1,3-Dichlorobenzene U 1,4-Dichlorobenzene U Dichlorodifluoromethane U 1,1-Dichloroethane U 1,2-Dichloroethane U 1,1-Dichloroethene U cis-1,2-Dichloroethene U trans-1,2-Dichloroethene U 1,2-Dichloropropane U 1,1-Dichloropropene U 1,3-Dichloropropane U cis-1,3-Dichloropropene U trans-1,3-Dichloropropene U 2,2-Dichloropropane U Di -isopropyl ether U Ethylbenzene U Hexachloro-1,3-butadiene U MB Qualifier MB MDL MB RDL ug/I ug/I 10.0 50.0 8.87 50.0 1.87 10.0 0.331 1.00 0.352 1.00 0.380 1.00 0.469 1.00 0.866 5.00 0.361 1.00 0.365 1.00 0.399 1.00 0.379 1.00 0.348 1.00 0.327 1.00 0.453 5.00 0.324 5.00 0.276 2.50 0.375 1.00 0.351 1.00 1.33 5.00 0.381 1.00 0.346 1.00 0.349 1.00 0.220 1.00 0.274 1.00 0.551 5.00 0.259 1.00 0.361 1.00 0.398 1.00 0.260 1.00 0.396 1.00 0.306 1.00 0.352 1.00 0.366 1.00 0.418 1.00 0.419 1.00 0.321 1.00 0.320 1.00 0.384 1.00 0.256 1.00 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 21 of 33 WG1223190 Volatile Organic Compounds (GC/MS) by Method 8260B Method Blank (MB) (MB) R3375787-2 01/14/1915:50 MB Result Analyte ug/I Isopropylbenzene U p-Isopropyltoluene U 2-Butanone (MEK) U Methylene Chloride U 4-Methyl-2-pentanone (MIBK) U Methyl tert-butyl ether U Naphthalene U n-Propylbenzene U Styrene U 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U Tetrachloroethene U Toluene U 1,1,2-Trichlorotrifluoroethane U 1,2,3-Trichlorobenzene U 1,2,4-Trichlorobenzene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichlorofluoromethane U 1,2,3-Trichloropropane U 1,2,3-Trimethyl benzene U 1,2,4-Trimethylbenzene U 1,3,5-Trimethyl benzene U Vinyl chloride U Xylenes, Total U (S) Toluene-d8 114 (S)Dibromofluoromethane 875 (S) 4-Bromof/uorobenzene 101 MB Qualifier MB MDL MB RDL ug/I ug/I Laboratory Control Sample (LCS) QUALITY CONTROL SUMMARY L1060264-04 0.326 1.00 0.350 1.00 3.93 10.0 1.00 5.00 2.14 10.0 0.367 1.00 1.00 5.00 0.349 1.00 0.307 1.00 0.385 1.00 0.130 1.00 0.372 1.00 0.412 1.00 0.303 1.00 0.230 1.00 0.355 1.00 0.319 1.00 0.383 1.00 0.398 1.00 1.20 5.00 0.807 2.50 0.321 1.00 0.373 1.00 0.387 1.00 0.259 1.00 1.06 3.00 80.0-120 75.0-120 77.0-126 (LCS) R3375787-1 01/14/1914:51 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I % % Acetone 125 182 145 19.0-160 Acrolein 125 245 196 10.0-160 J4 Acrylonitrile 125 183 146 55.0-149 Benzene 25.0 21.0 83.8 70.0-123 ONE LAB. NATIONWIDE. FP1 FTC FSS 4 Cn FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 22 of 33 WG1223190 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1060264-04 Laboratory Control Sample (LCS) FP1(LCS) R3375787-1 01/14/1914:51 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I % % z TC Bromobenzene 25.0 23.7 94.7 73.0-121 Bromodichloromethane 25.0 22.6 90.5 75.0-120 FSS Bromoform 25.0 23.0 91.8 68.0-132 Bromomethane 25.0 28.2 113 10.0-160 n-Butylbenzene 25.0 21.8 87.1 73.0-125 [Cn] sec -Butyl benzene 25.0 21.7 86.8 75.0-125 tert-Butylbenzene 25.0 23.1 92.3 76.0-124 FSr Carbon tetrachloride 25.0 21.7 86.7 68.0-126 Chlorobenzene 25.0 27.3 109 80.0-121 Chlorodibromomethane 25.0 25.9 104 77.0-125 Chloroethane 25.0 25.7 103 47.0-150 Chloroform 25.0 23.2 92.8 73.0-120 7G1 Chloromethane 25.0 37.1 148 41.0-142 J4 2-Chlorotoluene 25.0 23.1 92.2 76.0-123 4-Chlorotoluene 25.0 23.2 92.7 75.0-122 FAI 1,2-Dibromo-3-Chloropropane 25.0 25.4 102 58.0-134 1,2-Dibromoethane 25.0 25.3 101 80.0-122 FSC Dibromomethane 25.0 23.4 93.7 80.0-120 1,2-Dichlorobenzene 25.0 24.7 99.0 79.0-121 1,3-Dichlorobenzene 25.0 24.2 96.8 79.0-120 1,4-Dichlorobenzene 25.0 23.7 94.9 79.0-120 Dichlorodifluoromethane 25.0 29.7 119 51.0-149 1,1-Dichloroethane 25.0 27.3 109 70.0-126 1,2-Dichloroethane 25.0 25.9 104 70.0-128 1,1-Dichloroethene 25.0 22.7 90.7 71.0-124 cis-1,2-Dichloroethene 25.0 22.9 91.7 73.0-120 trans-1,2-Dichloroethene 25.0 23.7 94.6 73.0-120 1,2-Dichloropropane 25.0 27.7 111 77.0-125 1,1-Dichloropropene 25.0 22.9 91.6 74.0-126 1,3-Dichloropropane 25.0 25.9 104 80.0-120 cis-1,3-Dichloropropene 25.0 25.7 103 80.0-123 trans-1,3-Dichloropropene 25.0 26.4 106 78.0-124 2,2-Dichloropropane 25.0 20.9 83.6 58.0-130 Di -isopropyl ether 25.0 34.5 138 58.0-138 Ethylbenzene 25.0 26.5 106 79.0-123 Hexachloro-1,3-butadiene 25.0 21.4 85.6 54.0-138 Isopropylbenzene 25.0 23.3 93.0 76.0-127 p-Isopropyltoluene 25.0 23.7 94.7 76.0-125 2-Butanone (MEK) 125 186 149 44.0-160 Methylene Chloride 25.0 21.8 87.1 67.0-120 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 23 of 33 WG1223190 Volatile Organic Compounds (GC/MS) by Method 8260B Laboratory Control Sample (LCS) QUALITY CONTROL SUMMARY L1060264-04 (LCS) R3375787-1 01/14/1914:51 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I % % 4-Methyl-2-pentanone (MIBK) 125 197 158 68.0-142 J4 Methyl tert-butyl ether 25.0 23.5 94.2 68.0-125 Naphthalene 25.0 24.2 96.9 54.0-135 n-Propylbenzene 25.0 22.6 90.4 77.0-124 Styrene 25.0 23.9 95.8 73.0-130 1,1,1,2-Tetrachloroethane 25.0 26.8 107 75.0-125 1,1,2,2-Tetrachloroethane 25.0 23.9 95.4 65.0-130 Tetrachloroethene 25.0 26.7 107 72.0-132 Toluene 25.0 24.1 96.5 79.0-120 1,1,2-Trichlorotrifluoroethane 25.0 22.3 89.2 69.0-132 1,2,3-Trichlorobenzene 25.0 24.4 97.4 50.0-138 1,2,4-Trichlorobenzene 25.0 23.3 93.1 57.0-137 1,1,1-Trichloroethane 25.0 22.3 89.3 73.0-124 1,1,2-Trichloroethane 25.0 26.7 107 80.0-120 Trichloroethene 25.0 25.3 101 78.0-124 Trichlorofluoromethane 25.0 24.7 99.0 59.0-147 1,2,3-Trichloropropane 25.0 24.7 98.7 73.0-130 1,2,3-Trimethylbenzene 25.0 23.1 92.2 77.0-120 1,2,4-Trimethylbenzene 25.0 22.6 90.5 76.0-121 1,3,5-Trimethyl benzene 25.0 22.4 89.6 76.0-122 Vinyl chloride 25.0 29.5 118 67.0-131 Xylenes, Total 75.0 78.4 105 79.0-123 (S) Toluene-d8 110 80.0-120 (S) DibromoFluoromethane 91.2 75.0-120 (S) 4-Bromof/uorobenzene 101 77.0-126 ONE LAB. NATIONWIDE. FP1 FTC FSS 4 Cn FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 24 of 33 WG1222625 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 8270D 1-1060264-01,02,03,04 Method Blank (MB) FP1(MB) R3375725-3 01/14/1915:23 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I 2 TC Acenaphthene U 0.316 1.00 Acenaphthylene U 0.309 1.00 FSS Anthracene U 0.291 1.00 Benzidine U 4.32 10.0 Benzo(a)anthracene U 0.0975 1.00 [Cn] Benzo(b)fluoranthene U 0.0896 1.00 Benzo(k)fluoranthene U 0.355 1.00 FSr Benzo(g,h,i)perylene U 0.161 1.00 Benzo(a)pyrene U 0.340 1.00 Bis(2-chlorethoxy)methane U 0.329 10.0 Bis(2-chloroethyl)ether U 1.62 10.0 Bis(2-chloroisopropyl)ether U 0.445 10.0 7G� 4-Bromophenyl-phenylether U 0.335 10.0 2-Chloronaphthalene U 0.330 1.00 4-Chlorophenyl-phenylether U 0.303 10.0 FAI Chrysene U 0.332 1.00 Dibenz(a,h)anthracene U 0.279 1.00 FSC 3,3-Dichlorobenzidine U 2.02 10.0 2,4-Dinitrotoluene U 1.65 10.0 2,6-Dinitrotoluene U 0.279 10.0 Fluoranthene U 0.310 1.00 Fluorene U 0.323 1.00 Hexachlorobenzene U 0.341 1.00 Hexachloro-1,3-butadiene U 0.329 10.0 Hexachlorocyclopentadiene U 2.33 10.0 Hexachloroethane U 0.365 10.0 Indeno(1,2,3-cd)pyrene U 0.279 1.00 Isophorone U 0.272 10.0 Naphthalene U 0.372 1.00 Nitrobenzene U 0.367 10.0 n-Nitrosodimethyla mine U 1.26 10.0 n-Nitrosodiphenylamine U 1.19 10.0 n-Nitrosodi-n-propylamine U 0.403 10.0 Phenanthrene U 0.366 1.00 Benzylbutyl phthalate U 0.275 3.00 Bis(2-ethylhexyl)phthalate U 0.709 3.00 Di-n-butyl phthalate U 0.266 3.00 Diethyl phthalate U 0.282 3.00 Dimethyl phthalate U 0.283 3.00 Di-n-octyl phthalate U 0.278 3.00 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 25 of 33 WG1222625 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 8270D 1-1060264-01,02,03,04 Method Blank (MB) FP1(MB) R3375725-3 01/14/1915:23 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I FTc Pyrene U 0.330 1.00 1,2,4-Trichlorobenzene U 0.355 10.0 FSS 4-ChIoro-3-methyl phenol U 0.263 10.0 2-Chlorophenol U 0.283 10.0 2-Nitrophenol U 0.320 10.0 rCn 4-Nitrophenol U 2.01 10.0 Pentachlorophenol U 0.313 10.0 FSr Phenol U 0.334 10.0 2,4,6-Trichlorophenol U 0.297 10.0 2,4-Dichlorophenol U 0.284 10.0 2,4-Dimethylphenol U 0.264 10.0 4,6-Dinitro-2-methylphenol U 2.62 10.0 7G1 2,4-Dinitrophenol U 3.25 10.0 (S) Nitrobenzene-d5 50.5 10.0-127 (S)2-Fluorobipheny/ 50.8 10.0-130 FAI (S) p-Terphenyl-d14 58.6 10.0-128 (S) Phenol-d5 20.3 10.0-120 [Sc (S) 2-F/uorophenol 35.9 10.0-120 (S)2,4,6-Tribromopheno/ 38.1 10.0-155 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375725-1 01/14/1914:36 • (LCSD) R3375725-2 01/14/1914:59 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % Acenaphthene 50.0 36.4 36.4 72.8 72.8 41.0-120 0.000 22 Acenaphthylene 50.0 35.8 36.0 71.6 72.0 43.0-120 0.557 22 Anthracene 50.0 36.2 35.3 72.4 70.6 45.0-120 2.52 20 Benzidine 50.0 9.34 19.4 18.7 38.8 1.00-120 J3 70.0 36 Benzo(a)anth race ne 50.0 35.7 34.2 71.4 68.4 47.0-120 4.29 20 Benzo(b)fluoranthene 50.0 34.7 34.2 69.4 68.4 46.0-120 1.45 20 Benzo(k)fluoranthene 50.0 36.0 34.6 72.0 69.2 46.0-120 3.97 21 Benzo(g,h,i)perylene 50.0 36.8 35.7 73.6 71.4 48.0-121 3.03 20 Benzo(a)pyrene 50.0 37.2 36.4 74.4 72.8 47.0-120 2.17 20 Bis(2-chlorethoxy)methane 50.0 31.1 31.5 62.2 63.0 33.0-120 1.28 24 Bis(2-chloroethyl)ether 50.0 33.4 33.9 66.8 67.8 23.0-120 1.49 33 Bis(2-chloroisopropyl)ether 50.0 32.9 33.8 65.8 67.6 28.0-120 2.70 31 4-Bromophenyl-phenylether 50.0 36.8 37.1 73.6 74.2 45.0-120 0.812 20 2-Chloronaphthalene 50.0 34.6 34.7 69.2 69.4 37.0-120 0.289 25 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 26 of 33 WG1222625 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1060264-01,02,03,04 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS) R3375725-1 01/14/1914:36 • (LCSD) R3375725-2 01/14/1914:59 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % 2 TC 4-Chlorophenyl-phenylether 50.0 36.8 36.8 73.6 73.6 44.0-120 0.000 20 Chrysene 50.0 37.6 36.1 75.2 72.2 48.0-120 4.07 20 FSS Dibenz(a,h)anthracene 50.0 37.6 36.3 75.2 72.6 47.0-120 3.52 20 3,3-Dichlorobenzidine 50.0 38.8 37.7 77.6 75.4 44.0-120 2.88 20 2,4-Dinitrotoluene 50.0 40.6 39.4 81.2 78.8 49.0-124 3.00 20 [Cn] 2,6-Dinitrotoluene 50.0 37.8 37.6 75.6 75.2 46.0-120 0.531 21 Fluoranthene 50.0 38.7 38.3 77.4 76.6 51.0-120 1.04 20 FSr Fluorene 50.0 36.5 36.0 73.0 72.0 47.0-120 1.38 20 Hexachlorobenzene 50.0 36.7 36.5 73.4 73.0 44.0-120 0.546 20 Hexachloro-1,3-butadiene 50.0 31.7 32.5 63.4 65.0 19.0-120 2.49 32 Hexachlorocyclopentadiene 50.0 28.9 29.3 57.8 58.6 15.0-120 1.37 31 Hexachloroethane 50.0 31.7 33.3 63.4 66.6 15.0-120 4.92 37 7G1 Indeno(1,2,3-cd)pyrene 50.0 36.6 35.3 73.2 70.6 49.0-122 3.62 20 Isophorone 50.0 33.0 32.7 66.0 65.4 36.0-120 0.913 23 Naphthalene 50.0 30.2 31.1 60.4 62.2 27.0-120 2.94 27 FAI Nitrobenzene 50.0 31.7 32.6 63.4 65.2 27.0-120 2.80 29 n-Nitrosodimethyla mine 50.0 21.6 21.8 43.2 43.6 10.0-120 0.922 40 FSC n-Nitrosodiphenylamine 50.0 37.3 36.8 74.6 73.6 47.0-120 1.35 20 n-Nitrosodi-n-propylamine 50.0 35.4 36.7 70.8 73.4 31.0-120 3.61 28 Phenanthrene 50.0 35.8 35.5 71.6 71.0 46.0-120 0.842 20 Benzylbutyl phthalate 50.0 40.9 39.0 81.8 78.0 43.0-121 4.76 20 Bis(2-ethylhexyl)phthalate 50.0 39.7 38.7 79.4 77.4 43.0-122 2.55 20 Di-n-butyl phthalate 50.0 40.2 39.1 80.4 78.2 49.0-121 2.77 20 Diethyl phthalate 50.0 39.1 38.2 78.2 76.4 48.0-122 2.33 20 Dimethyl phthalate 50.0 38.0 37.5 76.0 75.0 48.0-120 1.32 20 Di-n-octyl phthalate 50.0 43.2 41.2 86.4 82.4 42.0-125 4.74 20 Pyrene 50.0 38.6 37.8 77.2 75.6 47.0-120 2.09 20 1,2,4-Trichlorobenzene 50.0 30.8 31.4 61.6 62.8 24.0-120 1.93 29 4-Chloro-3-methylphenol 50.0 35.8 34.1 71.6 68.2 40.0-120 4.86 21 2-Chlorophenol 50.0 32.6 33.4 65.2 66.8 25.0-120 2.42 35 2,4-Dichlorophenol 50.0 34.5 34.3 69.0 68.6 36.0-120 0.581 26 2,4-Dimethylphenol 50.0 32.3 32.4 64.6 64.8 33.0-120 0.309 26 4,6-Dinitro-2-methylphenol 50.0 51.4 50.2 103 100 38.0-138 2.36 25 2,4-Dinitrophenol 50.0 40.5 37.3 81.0 74.6 10.0-120 8.23 39 2-Nitrophenol 50.0 36.8 37.0 73.6 74.0 31.0-120 0.542 29 4-Nitrophenol 50.0 15.9 14.7 31.8 29.4 10.0-120 7.84 33 Pentachlorophenol 50.0 33.9 31.8 67.8 63.6 23.0-120 6.39 25 Phenol 50.0 14.9 14.5 29.8 29.0 10.0-120 2.72 36 2,4,6-Trichlorophenol 50.0 37.9 37.5 75.8 75.0 42.0-120 1.06 23 (S) Nitrobenzene-d5 51.4 53.1 10.0-127 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 27 of 33 WG1222625 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1060264-01,02,03,04 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3375725-1 01/14/1914:36 • (LCSD) R3375725-2 01/14/1914:59 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I (S) 2-Fluorobiphenyl (S) p-Terphenyl-d14 (S) Phenol-d5 (S) 2-F/uorophenol (S) 2,4,6-Tribromophenol LCS Rec. LCSD Rec. Rec. Limits 59.3 58.9 10.0-130 63.5 60.1 10.0-128 23.4 23.1 10.0-120 39.8 38.9 10.0-120 59.5 57.0 10.0-155 L1059019-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1059019-01 01/14/19 22:31 • (MS) R3375725-4 01/14/19 22:55 • (MSD) R3375725-5 01/14/19 23:19 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte ug/I ug/I ug/I ug/I % % Acenaphthene 50.0 ND 34.3 34.0 68.6 68.0 Acenaphthylene 50.0 ND 33.6 32.7 67.2 65.4 Anthracene 50.0 ND 34.3 32.8 68.6 65.6 Benzidine 50.0 ND 4.40 NO 8.80 0.000 Benzo(a)anth race ne 50.0 ND 33.7 32.9 67.4 65.8 Benzo(b)fluoranthene 50.0 ND 36.6 33.9 73.2 67.8 Benzo(k)fluoranthene 50.0 ND 35.5 31.8 71.0 63.6 Benzo(g,h,i)perylene 50.0 ND 37.0 34.0 74.0 68.0 Benzo(a)pyrene 50.0 ND 35.4 34.0 70.8 68.0 Bis(2-chlorethoxy)methane 50.0 ND 31.4 30.5 62.8 61.0 Bis(2-chloroethyl)ether 50.0 ND 31.9 30.4 63.8 60.8 Bis(2-chloroisopropyl)ether 50.0 ND 30.9 30.1 61.8 60.2 4-Bromophenyl-phenylether 50.0 ND 35.4 34.9 70.8 69.8 2-Chloronaphthalene 50.0 ND 32.7 32.2 65.4 64.4 4-Chlorophenyl-phenylether 50.0 ND 36.0 35.0 72.0 70.0 Chrysene 50.0 ND 35.8 34.6 71.6 69.2 Dibenz(a,h)anthracene 50.0 ND 38.1 34.6 76.2 69.2 3,3-Dichlorobenzidine 50.0 ND 25.9 15.3 51.8 30.6 2,4-Dinitrotoluene 50.0 ND 38.7 37.9 77.4 75.8 2,6-Dinitrotoluene 50.0 ND 36.2 35.2 72.4 70.4 Fluoranthene 50.0 ND 37.3 36.5 74.6 73.0 Fluorene 50.0 ND 34.8 34.2 69.6 68.4 Hexachlorobenzene 50.0 ND 35.2 34.7 70.4 69.4 Hexachloro-1,3-butadiene 50.0 ND 32.6 29.1 65.2 58.2 Hexachlorocyclopentadiene 50.0 ND 31.7 30.8 63.4 61.6 Hexachloroethane 50.0 ND 31.1 25.7 62.2 51.4 Indeno(1,2,3-cd)pyrene 50.0 ND 37.2 33.9 74.4 67.8 Isophorone 50.0 ND 33.1 32.0 66.2 64.0 LCS Qualifier LCSD Qualifier RPD RPD Limits Dilution Rec. Limits MS Qualifier MSD Qualifier zo.u-ILu 31.0-121 36.0-120 1.00-120 39.0-120 37.0-120 37.0-120 37.0-123 37.0-120 17.0-120 14.0-120 18.0-120 37.0-120 29.0-120 36.0-120 38.0-120 36.0-121 10.0-134 39.0-125 36.0-120 41.0-121 37.0-120 35.0-122 12.0-120 10.0-120 10.0-120 38.0-125 21.0-120 J3 J6 J3 RPD RPD Limits 0.878 25 2.71 25 4.47 23 200 37 2.40 23 7.66 23 11.0 26 8.45 25 4.03 24 2.91 31 4.82 33 2.62 34 1.42 24 1.54 28 2.82 23 3.41 23 9.63 24 51.5 30 2.09 25 2.80 27 2.17 22 1.74 24 1.43 24 11.3 34 2.88 33 19.0 40 9.28 24 3.38 27 FP1 FTC FSS [Cn] s Sr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 28 of 33 WG1222625 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1060264-01,02,03,04 L1O59019-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1059019-01 01/14/19 22:31 • (MS) R3375725-4 01/14/19 22:55 • (MSD) R3375725-5 01/14/19 23:19 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits Analyte ug/I ug/I ug/I ug/I % % % Naphthalene 50.0 ND 31.8 29.9 63.6 59.8 1 10.0-120 Nitrobenzene 50.0 ND 32.4 31.8 64.8 63.6 1 12.0-120 n-Nitrosodimethyla mine 50.0 ND 23.3 21.3 46.6 42.6 1 10.0-120 n-Nitrosodiphenyla mine 50.0 ND 5.43 6.17 10.9 12.3 1 37.0-120 n-Nitrosodi-n-propylamine 50.0 ND 33.1 31.8 66.2 63.6 1 16.0-120 Phenanthrene 50.0 ND 34.2 33.3 68.4 66.6 1 33.0-120 Benzylbutyl phthalate 50.0 ND 38.8 37.0 77.6 74.0 1 34.0-126 Bis(2-ethylhexyl)phthalate 50.0 ND 37.6 36.6 75.2 73.2 1 33.0-126 Di-n-butyl phthalate 50.0 ND 38.3 37.1 76.6 74.2 1 35.0-128 Diethyl phthalate 50.0 ND 37.6 36.3 75.2 72.6 1 39.0-125 Dimethyl phthalate 50.0 ND 36.8 35.3 73.6 70.6 1 37.0-120 Di-n-octyl phthalate 50.0 ND 39.9 38.9 79.8 77.8 1 25.0-135 Pyrene 50.0 ND 36.6 36.2 73.2 72.4 1 39.0-120 1,2,4-Trichlorobenzene 50.0 ND 32.0 29.3 64.0 58.6 1 15.0-120 4-ChIoro-3-methyl phenol 50.0 ND 33.6 33.7 67.2 67.4 1 26.0-120 2-Chlorophenol 50.0 ND 27.7 27.3 55.4 54.6 1 18.0-120 2,4-Dichlorophenol 50.0 ND 32.8 33.6 65.6 67.2 1 19.0-120 2,4-Dimethylphenol 50.0 ND 30.1 25.1 60.2 50.2 1 15.0-120 4,6-Dinitro-2-methylphenol 50.0 ND 47.8 48.0 95.6 96.0 1 10.0-144 2,4-Dinitrophenol 50.0 ND 41.7 44.1 83.4 88.2 1 10.0-120 2-Nitrophenol 50.0 ND 36.1 36.9 72.2 73.8 1 20.0-120 4-Nitrophenol 50.0 ND 14.7 15.2 29.4 30.4 1 10.0-120 Pentachlorophenol 50.0 ND 34.5 36.3 69.0 72.6 1 10.0-128 Phenol 50.0 ND 14.1 13.3 28.2 26.6 1 10.0-120 2,4,6-Trichlorophenol 50.0 ND 33.2 35.3 66.4 70.6 1 26.0-120 (S) Nitrobenzene-d5 53.1 51.9 10.0-127 (S) 2-Fluorobiphenyl 54.4 54.2 10.0-130 (S) p-Terphenyl-d14 60.1 58.2 10.0-128 (S) Phenol-d5 22.4 20.9 10.0-120 (S) 2-F/uorophenol 37.6 35.5 10.0-120 (S)2,4,6-Tribromopheno/ 57.5 56.5 10.0-155 ONE LAB. NATIONWIDE. MS Qualifier MSD Qualifier RPD RPD Limits 6.16 31 1.87 30 8.97 40 J6 J6 12.8 24 4.01 30 2.67 22 4.75 24 2.70 25 3.18 23 3.52 24 4.16 24 2.54 26 1.10 22 8.81 31 0.297 27 1.45 34 2.41 27 18.1 28 0.418 39 5.59 40 2.19 30 3.34 40 5.08 37 5.84 40 6.13 31 FP1 FTc FSS [Cn] FSr �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 29 of 33 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. FP1 FTC FSS [Cn] FSr 6 QC FAI FSC Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Withers & Ravenel Eng. - Standard 02180643.01 L1060264 01/15/19 15:06 30 of 33 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T 104704245-17-14 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. 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ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 October 22, 2019 Laura Elliott Withers & Ravenel- Greensboro 424 Gallimore Dairy Road, Suite C Greensboro, NC 27409 Project Location: Wake Forest, NC Client Job Number: Project Number: 02180643.01 Laboratory Work Order Number: 19JO915 Enclosed are results of analyses for samples received by the laboratory on October 11, 2019. If you have any questions concerning this report, please feel free to contact me. Sincerely, �11 �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Withers & Ravenel- Greensboro REPORT DATE: 10/22/2019 424 Gallimore Dairy Road, Suite C Greensboro, NC 27409 PURCHASE ORDER NUMBER: 02180643.01 ATTN: Laura Elliott PROJECT NUMBER: 02180643.01 ANALYTICAL SUMMARY WORK ORDER NUMBER: 19JO915 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Wake Forest, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB SV-1 19JO915-01 Soil Gas EPA TO-15 SV-2 19JO915-02 Soil Gas EPA TO-15 SV-3 19JO915-03 Soil Gas EPA TO-15 SV-4 19JO915-04 Soil Gas EPA TO-15 SV-5 19JO915-05 Soil Gas EPA TO-15 SV-6 19JO915-06 Soil Gas EPA TO-15 SV-7 19JO915-07 Soil Gas EPA TO-15 SV-8 19JO915-08 Soil Gas EPA TO-15 SV-9 19JO915-09 Soil Gas EPA TO-15 Duplicate 19JO915-10 Soil Gas EPA TO-15 Unused Can/Reg #2294/4324 19JO915-11 Soil Gas Page 2 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. REVISED REPORT - 10/22/2019 - Updated Chain of Custody included with final report. EPA TO-15 Qualifications: Laboratory fortified blank /laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. Analyte & Samples(s) Qualified: 1,2,4-Trichlorobenzene B243570-BS1,B243587-BS1 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: Naphthalene 19J0915-01[SV--1], 19J0915-02[SV-2], 19J0915-03[SV-3], 19J0915-04[SV-4],B243587-BS1 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: 1,2,4-Trichlorobenzene B243587-BS1 Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in house limits of 50-150%. Analyte & Samples(s) Qualified: Ethanol, Isopropanol, Naphthalene 19J0915-05[SV-5], 19J0915-06[SV-6], 19J0915-07[SV-7], 19J0915-08[SV-8], 19J0915-09[SV-9], 19J0915-10[Duplicate], B243570-BLKI, B243570-BS1, B243570-DUPI, 19J0915-01[SV-1], 19J0915-02[SV-2], 19J0915-03[SV-3], 19J0915-04[SV-4], B243587-BSI The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Tod E. Kopyscinski Laboratory Director Page 3 of 48 icon-tes w . ANALYTICAL LABORATORY Project Location: Wake Forest, NC Date Received: 10/11/2019 Field Sample #: SV-1 Sample ID: 19JO915-01 Sample Matrix: Soil Gas Sampled: 10/10/2019 16:50 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Work Order: 19JO915 Sub Description/Location: Initial Vacuum(in Hg): -29.5 Canister ID: 2305 Final Vacuum(in Hg): -5 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.9 Flow Controller ID: 4328 Flow Controller Type: Fixed -Orifice Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results ILL MDL Dilution Analyzed Analyst Acetone 400 40 14 950 95 33 20 10/18/19 8:57 BRF Benzene 1.8 0.20 0.082 5.8 0.64 0.26 4 10/16/19 20:21 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/16/19 20:21 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/16/19 20:21 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/16/19 20:21 BRF Bromomethane ND 0.20 0.14 ND 0.78 0.53 4 10/16/19 20:21 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/16/19 20:21 BRF 2-Butanone (MEK) 9.2 8.0 0.37 27 24 1.1 4 10/16/19 20:21 BRF Carbon Disulfide 4.3 2.0 0.14 13 6.2 0.43 4 10/16/19 20:21 BRF Carbon Tetrachloride 0.084 0.20 0.065 J 0.53 1.3 0.41 4 10/16/19 20:21 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/16/19 20:21 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/16/19 20:21 BRF Chloroform 0.45 0.20 0.074 2.2 0.98 0.36 4 10/16/19 20:21 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/16/19 20:21 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/16/19 20:21 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/16/19 20:21 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/16/19 20:21 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/16/19 20:21 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/16/19 20:21 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/16/19 20:21 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/16/19 20:21 BRF 1, 1 -Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/16/19 20:21 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/16/19 20:21 BRF 1, 1 -Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/16/19 20:21 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/16/19 20:21 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/16/19 20:21 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/16/19 20:21 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/16/19 20:21 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/16/19 20:21 BRF 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/16/19 20:21 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/16/19 20:21 BRF Ethanol 32 8.0 3.6 61 15 6.7 4 10/16/19 20:21 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/16/19 20:21 BRF Ethylbenzene 0.27 0.20 0.12 1.2 0.87 0.50 4 10/16/19 20:21 BRF 4-Ethyltoluene 0.18 0.20 0.12 J 0.90 0.98 0.60 4 10/16/19 20:21 BRF Heptane 1.1 0.20 0.12 4.5 0.82 0.48 4 10/16/19 20:21 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/16/19 20:21 BRF Hexane 11 8.0 0.35 39 28 1.2 4 10/16/19 20:21 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/16/19 20:21 BRF Isopropanol ND 8.0 0.37 ND 20 0.90 4 10/16/19 20:21 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/16/19 20:21 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/16/19 20:21 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 10/16/19 20:21 BRF Naphthalene 0.31 0.20 0.15 Z-01, V-35 1.6 1.0 0.80 4 10/16/19 20:21 BRF Propene 150 8.0 0.37 260 14 0.64 4 10/16/19 20:21 BRF Styrene ND 0.20 0.12 ND 0.85 0.53 4 10/16/19 20:21 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/16/19 20:21 BRF Page 4 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -29.5 Field Sample #: SV-1 Canister ID: 2305 Final Vacuum(in Hg): -5 Sample ID: 19JO915-01 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.9 Sample Matrix: Soil Gas Flow Controller ID: 4328 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 16:50 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.11 ND 1.4 0.75 4 10/16/19 20:21 BRF Tetrahydrofuran ND 0.20 0.20 ND 0.59 0.59 4 10/16/19 20:21 BRF Toluene 1.4 0.20 0.10 5.3 0.75 0.39 4 10/16/19 20:21 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/16/19 20:21 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.075 ND 1.1 0.41 4 10/16/19 20:21 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/16/19 20:21 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/16/19 20:21 BRF Trichlorofluoromethane (Freon 11) 0.26 0.80 0.15 J 1.4 4.5 0.85 4 10/16/19 20:21 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/16/19 20:21 BRF 1,2,4-Trimethylbenzene 0.96 0.20 0.13 4.7 0.98 0.63 4 10/16/19 20:21 BRF 1,3,5-Trimethylbenzene 0.21 0.20 0.13 1.0 0.98 0.62 4 10/16/19 20:21 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/16/19 20:21 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/16/19 20:21 BRF m&p-Xylene 0.98 0.40 0.23 4.3 1.7 1.00 4 10/16/19 20:21 BRF o-Xylene 0.48 0.20 0.12 2.1 0.87 0.54 4 10/16/19 20:21 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene(1) 109 70-130 10/18/19 8:57 4-Bromofluorobenzene (1) 108 70-130 10/16/19 20:21 Page 5 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SV-2 Canister ID: 2299 Final Vacuum(in Hg): -5 Sample ID: 19JO915-02 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.9 Sample Matrix: Soil Gas Flow Controller ID: 4340 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 15:55 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 730 80 28 1700 190 66 40 10/18/19 9:25 BRF Benzene 3.6 0.20 0.082 12 0.64 0.26 4 10/16/19 21:02 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/16/19 21:02 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/16/19 21:02 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/16/19 21:02 BRF Bromomethane ND 0.20 0.14 ND 0.78 0.53 4 10/16/19 21:02 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/16/19 21:02 BRF 2-Butanone (MEK) 9.5 8.0 0.37 28 24 1.1 4 10/16/19 21:02 BRF Carbon Disulfide 5.2 2.0 0.14 16 6.2 0.43 4 10/16/19 21:02 BRF Carbon Tetrachloride ND 0.20 0.065 ND 1.3 0.41 4 10/16/19 21:02 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/16/19 21:02 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/16/19 21:02 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/16/19 21:02 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/16/19 21:02 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/16/19 21:02 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/16/19 21:02 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/16/19 21:02 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/16/19 21:02 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/16/19 21:02 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/16/19 21:02 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/16/19 21:02 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/16/19 21:02 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/16/19 21:02 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/16/19 21:02 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/16/19 21:02 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/16/19 21:02 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/16/19 21:02 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/16/19 21:02 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/16/19 21:02 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/16/19 21:02 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/16/19 21:02 BRF Ethanol 49 8.0 3.6 92 15 6.7 4 10/16/19 21:02 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/16/19 21:02 BRF Ethylbenzene 0.48 0.20 0.12 2.1 0.87 0.50 4 10/16/19 21:02 BRF 4-Ethyltoluene 0.28 0.20 0.12 1.4 0.98 0.60 4 10/16/19 21:02 BRF Heptane 7.3 0.20 0.12 30 0.82 0.48 4 10/16/19 21:02 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/16/19 21:02 BRF Hexane 55 8.0 0.35 190 28 1.2 4 10/16/19 21:02 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/16/19 21:02 BRF Isopropanol ND 8.0 0.37 ND 20 0.90 4 10/16/19 21:02 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/16/19 21:02 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/16/19 21:02 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 10/16/19 21:02 BRF Naphthalene 0.46 0.20 0.15 V-35, Z-01 2.4 1.0 0.80 4 10/16/19 21:02 BRF Propene 660 80 3.7 1100 140 6.4 40 10/18/19 9:25 BRF Styrene ND 0.20 0.12 ND 0.85 0.53 4 10/16/19 21:02 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/16/19 21:02 BRF Page 6 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SV-2 Canister ID: 2299 Final Vacuum(in Hg): -5 Sample ID: 19JO915-02 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.9 Sample Matrix: Soil Gas Flow Controller ID: 4340 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 15:55 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.11 ND 1.4 0.75 4 10/16/19 21:02 BRF Tetrahydrofuran ND 0.20 0.20 ND 0.59 0.59 4 10/16/19 21:02 BRF Toluene 2.4 0.20 0.10 9.0 0.75 0.39 4 10/16/19 21:02 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/16/19 21:02 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.075 ND 1.1 0.41 4 10/16/19 21:02 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/16/19 21:02 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/16/19 21:02 BRF Trichlorofluoromethane (Freon 11) 0.26 0.80 0.15 J 1.5 4.5 0.85 4 10/16/19 21:02 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/16/19 21:02 BRF 1,2,4-Trimethylbenzene ND 0.20 0.13 ND 0.98 0.63 4 10/16/19 21:02 BRF 1,3,5-Trimethylbenzene 0.31 0.20 0.13 1.5 0.98 0.62 4 10/16/19 21:02 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/16/19 21:02 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/16/19 21:02 BRF m&p-Xylene 1.6 0.40 0.23 7.1 1.7 1.00 4 10/16/19 21:02 BRF o-Xylene 0.71 0.20 0.12 3.1 0.87 0.54 4 10/16/19 21:02 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene(1) 110 70-130 10/18/19 9:25 4-Bromofluorobenzene(1) 108 70-130 10/16/19 21:02 Page 7 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: SV-3 Canister ID: 2244 Final Vacuum(in Hg): -5 Sample ID: 19JO915-03 Canister Size: 1 liter Receipt Vacuum(in Hg): -6 Sample Matrix: Soil Gas Flow Controller ID: 4138 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 14:55 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 400 40 14 940 95 33 20 10/18/19 9:52 BRF Benzene 0.78 0.20 0.082 2.5 0.64 0.26 4 10/16/19 21:42 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/16/19 21:42 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/16/19 21:42 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/16/19 21:42 BRF Bromomethane ND 0.20 0.14 ND 0.78 0.53 4 10/16/19 21:42 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/16/19 21:42 BRF 2-Butanone (MEK) 6.9 8.0 0.37 J 20 24 1.1 4 10/16/19 21:42 BRF Carbon Disulfide 5.2 2.0 0.14 16 6.2 0.43 4 10/16/19 21:42 BRF Carbon Tetrachloride 0.068 0.20 0.065 J 0.43 1.3 0.41 4 10/16/19 21:42 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/16/19 21:42 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/16/19 21:42 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/16/19 21:42 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/16/19 21:42 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/16/19 21:42 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/16/19 21:42 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/16/19 21:42 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/16/19 21:42 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/16/19 21:42 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/16/19 21:42 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/16/19 21:42 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/16/19 21:42 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/16/19 21:42 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/16/19 21:42 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/16/19 21:42 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/16/19 21:42 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/16/19 21:42 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/16/19 21:42 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/16/19 21:42 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/16/19 21:42 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/16/19 21:42 BRF Ethanol 14 8.0 3.6 26 15 6.7 4 10/16/19 21:42 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/16/19 21:42 BRF Ethylbenzene 0.26 0.20 0.12 1.1 0.87 0.50 4 10/16/19 21:42 BRF 4-Ethyltoluene 0.27 0.20 0.12 1.3 0.98 0.60 4 10/16/19 21:42 BRF Heptane 0.49 0.20 0.12 2.0 0.82 0.48 4 10/16/19 21:42 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/16/19 21:42 BRF Hexane 15 8.0 0.35 53 28 1.2 4 10/16/19 21:42 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/16/19 21:42 BRF Isopropanol ND 8.0 0.37 ND 20 0.90 4 10/16/19 21:42 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/16/19 21:42 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/16/19 21:42 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 10/16/19 21:42 BRF Naphthalene 0.44 0.20 0.15 V-35, Z-01 2.3 1.0 0.80 4 10/16/19 21:42 BRF Propene ND 8.0 0.37 ND 14 0.64 4 10/16/19 21:42 BRF Styrene 0.18 0.20 0.12 J 0.75 0.85 0.53 4 10/16/19 21:42 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/16/19 21:42 BRF Page 8 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: SV-3 Canister ID: 2244 Final Vacuum(in Hg): -5 Sample ID: 19JO915-03 Canister Size: 1 liter Receipt Vacuum(in Hg): -6 Sample Matrix: Soil Gas Flow Controller ID: 4138 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 14:55 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.11 ND 1.4 0.75 4 10/16/19 21:42 BRF Tetrahydrofuran ND 0.20 0.20 ND 0.59 0.59 4 10/16/19 21:42 BRF Toluene 1.0 0.20 0.10 3.9 0.75 0.39 4 10/16/19 21:42 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/16/19 21:42 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.075 ND 1.1 0.41 4 10/16/19 21:42 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/16/19 21:42 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/16/19 21:42 BRF Trichlorofluoromethane (Freon 11) 0.25 0.80 0.15 J 1.4 4.5 0.85 4 10/16/19 21:42 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/16/19 21:42 BRF 1,2,4-Trimethylbenzene 1.5 0.20 0.13 7.3 0.98 0.63 4 10/16/19 21:42 BRF 1,3,5-Trimethylbenzene 0.30 0.20 0.13 1.5 0.98 0.62 4 10/16/19 21:42 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/16/19 21:42 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/16/19 21:42 BRF m&p-Xylene 1.2 0.40 0.23 5.2 1.7 1.00 4 10/16/19 21:42 BRF o-Xylene 0.59 0.20 0.12 2.6 0.87 0.54 4 10/16/19 21:42 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene(1) 110 70-130 10/18/19 9:52 4-Bromofluorobenzene(1) 107 70-130 10/16/19 21:42 Page 9 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: SV-4 Canister ID: 2241 Final Vacuum(in Hg): -5 Sample ID: 19JO915-04 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.3 Sample Matrix: Soil Gas Flow Controller ID: 4139 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 14:00 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 390 40 14 930 95 33 20 10/18/19 10:20 BRF Benzene 0.45 0.20 0.082 1.4 0.64 0.26 4 10/16/19 22:23 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/16/19 22:23 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/16/19 22:23 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/16/19 22:23 BRF Bromomethane ND 0.20 0.14 ND 0.78 0.53 4 10/16/19 22:23 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/16/19 22:23 BRF 2-Butanone (MEK) 4.6 8.0 0.37 J 14 24 1.1 4 10/16/19 22:23 BRF Carbon Disulfide 0.65 2.0 0.14 J 2.0 6.2 0.43 4 10/16/19 22:23 BRF Carbon Tetrachloride ND 0.20 0.065 ND 1.3 0.41 4 10/16/19 22:23 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/16/19 22:23 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/16/19 22:23 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/16/19 22:23 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/16/19 22:23 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/16/19 22:23 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/16/19 22:23 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/16/19 22:23 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/16/19 22:23 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/16/19 22:23 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/16/19 22:23 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/16/19 22:23 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/16/19 22:23 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/16/19 22:23 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/16/19 22:23 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/16/19 22:23 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/16/19 22:23 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/16/19 22:23 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/16/19 22:23 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/16/19 22:23 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/16/19 22:23 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/16/19 22:23 BRF Ethanol 13 8.0 3.6 25 15 6.7 4 10/16/19 22:23 BRF Ethyl Acetate 0.79 0.20 0.15 2.8 0.72 0.54 4 10/16/19 22:23 BRF Ethylbenzene 0.25 0.20 0.12 1.1 0.87 0.50 4 10/16/19 22:23 BRF 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 10/16/19 22:23 BRF Heptane 0.24 0.20 0.12 0.97 0.82 0.48 4 10/16/19 22:23 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/16/19 22:23 BRF Hexane ND 8.0 0.35 ND 28 1.2 4 10/16/19 22:23 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/16/19 22:23 BRF Isopropanol 4.7 8.0 0.37 J 12 20 0.90 4 10/16/19 22:23 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/16/19 22:23 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/16/19 22:23 BRF 4-Methyl-2-pentanone (MIBK) 0.15 0.20 0.10 J 0.61 0.82 0.43 4 10/16/19 22:23 BRF Naphthalene 0.28 0.20 0.15 V-35, Z-01 1.5 1.0 0.80 4 10/16/19 22:23 BRF Propene ND 8.0 0.37 ND 14 0.64 4 10/16/19 22:23 BRF Styrene 0.14 0.20 0.12 J 0.61 0.85 0.53 4 10/16/19 22:23 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/16/19 22:23 BRF Page 10 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: SV-4 Canister ID: 2241 Final Vacuum(in Hg): -5 Sample ID: 19JO915-04 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.3 Sample Matrix: Soil Gas Flow Controller ID: 4139 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 14:00 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.11 ND 1.4 0.75 4 10/16/19 22:23 BRF Tetrahydrofuran ND 0.20 0.20 ND 0.59 0.59 4 10/16/19 22:23 BRF Toluene 0.96 0.20 0.10 3.6 0.75 0.39 4 10/16/19 22:23 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/16/19 22:23 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.075 ND 1.1 0.41 4 10/16/19 22:23 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/16/19 22:23 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/16/19 22:23 BRF Trichlorofluoromethane (Freon 11) 0.23 0.80 0.15 J 1.3 4.5 0.85 4 10/16/19 22:23 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.16 0.80 0.15 J 1.2 6.1 1.2 4 10/16/19 22:23 BRF 1,2,4-Trimethylbenzene 1.1 0.20 0.13 5.3 0.98 0.63 4 10/16/19 22:23 BRF 1,3,5-Trimethylbenzene 0.22 0.20 0.13 1.1 0.98 0.62 4 10/16/19 22:23 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/16/19 22:23 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/16/19 22:23 BRF m&p-Xylene 1.0 0.40 0.23 4.4 1.7 1.00 4 10/16/19 22:23 BRF o-Xylene 0.50 0.20 0.12 2.2 0.87 0.54 4 10/16/19 22:23 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 110 70-130 10/18/19 10:20 4-Bromofluorobenzene (1) 108 70-130 10/16/19 22:23 Page 11 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: SV-5 Canister ID: 2236 Final Vacuum(in Hg): -5 Sample ID: 19JO915-05 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.6 Sample Matrix: Soil Gas Flow Controller ID: 4229 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 13:06 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 120 8.0 2.8 290 19 6.6 4 10/17/19 17:26 BRF Benzene 2.3 0.20 0.082 7.5 0.64 0.26 4 10/17/19 17:26 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/17/19 17:26 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/17/19 17:26 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/17/19 17:26 BRF Bromomethane ND 2.0 0.14 ND 7.8 0.53 4 10/17/19 17:26 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/17/19 17:26 BRF 2-Butanone (MEK) 3.3 8.0 0.37 J 9.8 24 1.1 4 10/17/19 17:26 BRF Carbon Disulfide 17 2.0 0.14 52 6.2 0.43 4 10/17/19 17:26 BRF Carbon Tetrachloride ND 0.20 0.065 ND 1.3 0.41 4 10/17/19 17:26 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/17/19 17:26 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/17/19 17:26 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/17/19 17:26 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/17/19 17:26 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/17/19 17:26 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/17/19 17:26 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/17/19 17:26 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/17/19 17:26 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/17/19 17:26 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/17/19 17:26 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/17/19 17:26 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/17/19 17:26 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/17/19 17:26 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/17/19 17:26 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/17/19 17:26 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/17/19 17:26 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/17/19 17:26 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/17/19 17:26 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/17/19 17:26 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/17/19 17:26 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/17/19 17:26 BRF Ethanol ND 8.0 3.6 Z-01 ND 15 6.7 4 10/17/19 17:26 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/17/19 17:26 BRF Ethylbenzene 0.58 0.20 0.12 2.5 0.87 0.50 4 10/17/19 17:26 BRF 4-Ethyltoluene 0.79 0.20 0.12 3.9 0.98 0.60 4 10/17/19 17:26 BRF Heptane 8.3 0.20 0.12 34 0.82 0.48 4 10/17/19 17:26 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/17/19 17:26 BRF Hexane ND 8.0 0.35 ND 28 1.2 4 10/17/19 17:26 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/17/19 17:26 BRF Isopropanol ND 8.0 0.37 Z-01 ND 20 0.90 4 10/17/19 17:26 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/17/19 17:26 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/17/19 17:26 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 10/17/19 17:26 BRF Naphthalene 0.46 0.20 0.15 Z-01 2.4 1.0 0.80 4 10/17/19 17:26 BRF Propene ND 8.0 0.37 ND 14 0.64 4 10/17/19 17:26 BRF Styrene ND 0.20 0.12 ND 0.85 0.53 4 10/17/19 17:26 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/17/19 17:26 BRF Page 12 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: SV-5 Canister ID: 2236 Final Vacuum(in Hg): -5 Sample ID: 19JO915-05 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.6 Sample Matrix: Soil Gas Flow Controller ID: 4229 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 13:06 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.11 ND 1.4 0.75 4 10/17/19 17:26 BRF Tetrahydrofuran ND 0.20 0.20 ND 0.59 0.59 4 10/17/19 17:26 BRF Toluene 2.3 0.20 0.10 8.6 0.75 0.39 4 10/17/19 17:26 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/17/19 17:26 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.075 ND 1.1 0.41 4 10/17/19 17:26 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/17/19 17:26 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/17/19 17:26 BRF Trichlorofluoromethane (Freon 11) ND 0.80 0.15 ND 4.5 0.85 4 10/17/19 17:26 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/17/19 17:26 BRF 1,2,4-Trimethylbenzene 1.1 0.20 0.13 5.2 0.98 0.63 4 10/17/19 17:26 BRF 1,3,5-Trimethylbenzene 0.30 0.20 0.13 1.5 0.98 0.62 4 10/17/19 17:26 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/17/19 17:26 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/17/19 17:26 BRF m&p-Xylene 1.5 0.40 0.23 6.6 1.7 1.00 4 10/17/19 17:26 BRF o-Xylene 0.59 0.20 0.12 2.6 0.87 0.54 4 10/17/19 17:26 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 112 70-130 10/17/19 17:26 Page 13 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SV-6 Canister ID: 2257 Final Vacuum(in Hg): -5 Sample ID: 19JO915-06 Canister Size: 1 liter Receipt Vacuum(in Hg): -5 Sample Matrix: Soil Gas Flow Controller ID: 4321 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 11:28 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 19 8.0 2.8 46 19 6.6 4 10/17/19 17:55 BRF Benzene 1.2 0.20 0.082 4.0 0.64 0.26 4 10/17/19 17:55 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/17/19 17:55 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/17/19 17:55 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/17/19 17:55 BRF Bromomethane ND 2.0 0.14 ND 7.8 0.53 4 10/17/19 17:55 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/17/19 17:55 BRF 2-Butanone (MEK) 1.0 8.0 0.37 J 3.1 24 1.1 4 10/17/19 17:55 BRF Carbon Disulfide 5.2 2.0 0.14 16 6.2 0.43 4 10/17/19 17:55 BRF Carbon Tetrachloride ND 0.20 0.065 ND 1.3 0.41 4 10/17/19 17:55 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/17/19 17:55 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/17/19 17:55 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/17/19 17:55 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/17/19 17:55 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/17/19 17:55 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/17/19 17:55 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/17/19 17:55 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/17/19 17:55 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/17/19 17:55 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/17/19 17:55 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/17/19 17:55 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/17/19 17:55 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/17/19 17:55 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/17/19 17:55 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/17/19 17:55 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/17/19 17:55 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/17/19 17:55 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/17/19 17:55 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/17/19 17:55 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/17/19 17:55 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/17/19 17:55 BRF Ethanol ND 8.0 3.6 Z-01 ND 15 6.7 4 10/17/19 17:55 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/17/19 17:55 BRF Ethylbenzene 0.36 0.20 0.12 1.5 0.87 0.50 4 10/17/19 17:55 BRF 4-Ethyltoluene 0.52 0.20 0.12 2.6 0.98 0.60 4 10/17/19 17:55 BRF Heptane 0.47 0.20 0.12 1.9 0.82 0.48 4 10/17/19 17:55 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/17/19 17:55 BRF Hexane ND 8.0 0.35 ND 28 1.2 4 10/17/19 17:55 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/17/19 17:55 BRF Isopropanol 1.8 8.0 0.37 Z-01, J 4.5 20 0.90 4 10/17/19 17:55 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/17/19 17:55 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/17/19 17:55 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 10/17/19 17:55 BRF Naphthalene ND 0.20 0.15 ND 1.0 0.80 4 10/17/19 17:55 BRF Propene ND 8.0 0.37 ND 14 0.64 4 10/17/19 17:55 BRF Styrene ND 0.20 0.12 ND 0.85 0.53 4 10/17/19 17:55 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/17/19 17:55 BRF Page 14 of 48 icon-tes w . ANALYTICAL LABORATORY Project Location: Wake Forest, NC Date Received: 10/11/2019 Field Sample #: SV-6 Sample ID: 19JO915-06 Sample Matrix: Soil Gas Sampled: 10/ 10/2019 11:28 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2257 Canister Size: 1 liter Flow Controller ID: 4321 Sample Type: 10 min Work Order: 19JO915 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.15 0.20 0.11 J 1.0 1.4 0.75 4 10/17/19 17:55 BRF Tetrahydrofuran ND 0.20 0.20 ND 0.59 0.59 4 10/17/19 17:55 BRF Toluene 1.4 0.20 0.10 5.2 0.75 0.39 4 10/17/19 17:55 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/17/19 17:55 BRF 1, 1, 1 -Trichloroethane 0.092 0.20 0.075 J 0.50 1.1 0.41 4 10/17/19 17:55 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/17/19 17:55 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/17/19 17:55 BRF Trichlorofluoromethane (Freon 11) 0.36 0.80 0.15 J 2.0 4.5 0.85 4 10/17/19 17:55 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/17/19 17:55 BRF 1,2,4-Trimethylbenzene 0.65 0.20 0.13 3.2 0.98 0.63 4 10/17/19 17:55 BRF 1,3,5-Trimethylbenzene 0.26 0.20 0.13 1.3 0.98 0.62 4 10/17/19 17:55 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/17/19 17:55 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/17/19 17:55 BRF m&p-Xylene 0.95 0.40 0.23 4.1 1.7 1.00 4 10/17/19 17:55 BRF o-Xylene 0.50 0.20 0.12 2.2 0.87 0.54 4 10/17/19 17:55 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 114 % REC Limits 70-130 10/17/19 17:55 Page 15 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: SV-7 Canister ID: 2338 Final Vacuum(in Hg): -5 Sample ID: 19JO915-07 Canister Size: 1 liter Receipt Vacuum(in Hg): -6 Sample Matrix: Soil Gas Flow Controller ID: 4262 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 12:10 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 50 8.0 2.8 120 19 6.6 4 10/17/19 18:24 BRF Benzene 1.9 0.20 0.082 6.1 0.64 0.26 4 10/17/19 18:24 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/17/19 18:24 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/17/19 18:24 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/17/19 18:24 BRF Bromomethane ND 2.0 0.14 ND 7.8 0.53 4 10/17/19 18:24 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/17/19 18:24 BRF 2-Butanone (MEK) 2.4 8.0 0.37 J 7.1 24 1.1 4 10/17/19 18:24 BRF Carbon Disulfide 13 2.0 0.14 42 6.2 0.43 4 10/17/19 18:24 BRF Carbon Tetrachloride 0.18 0.20 0.065 J 1.2 1.3 0.41 4 10/17/19 18:24 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/17/19 18:24 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/17/19 18:24 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/17/19 18:24 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/17/19 18:24 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/17/19 18:24 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/17/19 18:24 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/17/19 18:24 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/17/19 18:24 BRF 1,3-Dichlorobenzene 0.32 0.20 0.10 1.9 1.2 0.62 4 10/17/19 18:24 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/17/19 18:24 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/17/19 18:24 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/17/19 18:24 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/17/19 18:24 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/17/19 18:24 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/17/19 18:24 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/17/19 18:24 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/17/19 18:24 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/17/19 18:24 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/17/19 18:24 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/17/19 18:24 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/17/19 18:24 BRF Ethanol 7.5 8.0 3.6 Z-01, J 14 15 6.7 4 10/17/19 18:24 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/17/19 18:24 BRF Ethylbenzene 0.44 0.20 0.12 1.9 0.87 0.50 4 10/17/19 18:24 BRF 4-Ethyltoluene 0.84 0.20 0.12 4.1 0.98 0.60 4 10/17/19 18:24 BRF Heptane 3.8 0.20 0.12 16 0.82 0.48 4 10/17/19 18:24 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/17/19 18:24 BRF Hexane ND 8.0 0.35 ND 28 1.2 4 10/17/19 18:24 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/17/19 18:24 BRF Isopropanol 5.2 8.0 0.37 Z-01, J 13 20 0.90 4 10/17/19 18:24 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/17/19 18:24 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/17/19 18:24 BRF 4-Methyl-2-pentanone (MIBK) 0.39 0.20 0.10 1.6 0.82 0.43 4 10/17/19 18:24 BRF Naphthalene 0.56 0.20 0.15 Z-01 2.9 1.0 0.80 4 10/17/19 18:24 BRF Propene ND 8.0 0.37 ND 14 0.64 4 10/17/19 18:24 BRF Styrene ND 0.20 0.12 ND 0.85 0.53 4 10/17/19 18:24 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/17/19 18:24 BRF Page 16 of 48 icon-tes w . ANALYTICAL LABORATORY Project Location: Wake Forest, NC Date Received: 10/11/2019 Field Sample #: SV-7 Sample ID: 19JO915-07 Sample Matrix: Soil Gas Sampled: 10/ 10/2019 12:10 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2338 Canister Size: 1 liter Flow Controller ID: 4262 Sample Type: 10 min Work Order: 19JO915 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.19 0.20 0.11 J 1.3 1.4 0.75 4 10/17/19 18:24 BRF Tetrahydrofuran 0.58 0.20 0.20 1.7 0.59 0.59 4 10/17/19 18:24 BRF Toluene 1.7 0.20 0.10 6.4 0.75 0.39 4 10/17/19 18:24 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/17/19 18:24 BRF 1, 1, 1 -Trichloroethane 0.10 0.20 0.075 J 0.55 1.1 0.41 4 10/17/19 18:24 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/17/19 18:24 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/17/19 18:24 BRF Trichlorofluoromethane (Freon 11) ND 0.80 0.15 ND 4.5 0.85 4 10/17/19 18:24 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/17/19 18:24 BRF 1,2,4-Trimethylbenzene 1.0 0.20 0.13 5.1 0.98 0.63 4 10/17/19 18:24 BRF 1,3,5-Trimethylbenzene 0.38 0.20 0.13 1.9 0.98 0.62 4 10/17/19 18:24 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/17/19 18:24 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/17/19 18:24 BRF m&p-Xylene 1.3 0.40 0.23 5.5 1.7 1.00 4 10/17/19 18:24 BRF o-Xylene 0.63 0.20 0.12 2.7 0.87 0.54 4 10/17/19 18:24 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 113 % REC Limits 70-130 10/17/19 18:24 Page 17 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: SV-8 Canister ID: 2319 Final Vacuum(in Hg): -5 Sample ID: 19JO915-08 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.7 Sample Matrix: Soil Gas Flow Controller ID: 4337 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 10:32 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 10 8.0 2.8 25 19 6.6 4 10/17/19 18:53 BRF Benzene 2.3 0.20 0.082 7.2 0.64 0.26 4 10/17/19 18:53 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/17/19 18:53 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/17/19 18:53 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/17/19 18:53 BRF Bromomethane ND 2.0 0.14 ND 7.8 0.53 4 10/17/19 18:53 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/17/19 18:53 BRF 2-Butanone (MEK) 1.2 8.0 0.37 J 3.7 24 1.1 4 10/17/19 18:53 BRF Carbon Disulfide 16 2.0 0.14 49 6.2 0.43 4 10/17/19 18:53 BRF Carbon Tetrachloride ND 0.20 0.065 ND 1.3 0.41 4 10/17/19 18:53 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/17/19 18:53 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/17/19 18:53 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/17/19 18:53 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/17/19 18:53 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/17/19 18:53 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/17/19 18:53 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/17/19 18:53 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/17/19 18:53 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/17/19 18:53 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/17/19 18:53 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/17/19 18:53 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/17/19 18:53 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/17/19 18:53 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/17/19 18:53 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/17/19 18:53 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/17/19 18:53 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/17/19 18:53 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/17/19 18:53 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/17/19 18:53 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/17/19 18:53 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/17/19 18:53 BRF Ethanol ND 8.0 3.6 Z-01 ND 15 6.7 4 10/17/19 18:53 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/17/19 18:53 BRF Ethylbenzene 0.62 0.20 0.12 2.7 0.87 0.50 4 10/17/19 18:53 BRF 4-Ethyltoluene 0.58 0.20 0.12 2.9 0.98 0.60 4 10/17/19 18:53 BRF Heptane 2.5 0.20 0.12 10 0.82 0.48 4 10/17/19 18:53 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/17/19 18:53 BRF Hexane ND 8.0 0.35 ND 28 1.2 4 10/17/19 18:53 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/17/19 18:53 BRF Isopropanol 1.4 8.0 0.37 Z-01, J 3.3 20 0.90 4 10/17/19 18:53 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/17/19 18:53 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/17/19 18:53 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 10/17/19 18:53 BRF Naphthalene 0.41 0.20 0.15 Z-01 2.2 1.0 0.80 4 10/17/19 18:53 BRF Propene ND 8.0 0.37 ND 14 0.64 4 10/17/19 18:53 BRF Styrene ND 0.20 0.12 ND 0.85 0.53 4 10/17/19 18:53 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/17/19 18:53 BRF Page 18 of 48 icon-tes w . ANALYTICAL LABORATORY Project Location: Wake Forest, NC Date Received: 10/11/2019 Field Sample #: SV-8 Sample ID: 19JO915-08 Sample Matrix: Soil Gas Sampled: 10/ 10/2019 10:32 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2319 Canister Size: 1 liter Flow Controller ID: 4337 Sample Type: 10 min Work Order: 19JO915 Initial Vacuum(in Hg): -28.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -4.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.20 0.20 0.11 J 1.3 1.4 0.75 4 10/17/19 18:53 BRF Tetrahydrofuran ND 0.20 0.20 ND 0.59 0.59 4 10/17/19 18:53 BRF Toluene 2.6 0.20 0.10 9.7 0.75 0.39 4 10/17/19 18:53 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/17/19 18:53 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.075 ND 1.1 0.41 4 10/17/19 18:53 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/17/19 18:53 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/17/19 18:53 BRF Trichlorofluoromethane (Freon 11) ND 0.80 0.15 ND 4.5 0.85 4 10/17/19 18:53 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/17/19 18:53 BRF 1,2,4-Trimethylbenzene 0.71 0.20 0.13 3.5 0.98 0.63 4 10/17/19 18:53 BRF 1,3,5-Trimethylbenzene 0.26 0.20 0.13 1.3 0.98 0.62 4 10/17/19 18:53 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/17/19 18:53 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/17/19 18:53 BRF m&p-Xylene 1.6 0.40 0.23 6.7 1.7 1.00 4 10/17/19 18:53 BRF o-Xylene 0.67 0.20 0.12 2.9 0.87 0.54 4 10/17/19 18:53 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 109 % REC Limits 70-130 10/17/19 18:53 Page 19 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: SV-9 Canister ID: 202 Final Vacuum(in Hg): -5 Sample ID: 19JO915-09 Canister Size: 1 liter Receipt Vacuum(in Hg): -5 Sample Matrix: Soil Gas Flow Controller ID: 4310 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 17:50 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 330 80 28 780 190 66 40 10/17/19 22:24 BRF Benzene 9.8 0.20 0.082 31 0.64 0.26 4 10/17/19 19:22 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/17/19 19:22 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/17/19 19:22 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/17/19 19:22 BRF Bromomethane ND 2.0 0.14 ND 7.8 0.53 4 10/17/19 19:22 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/17/19 19:22 BRF 2-Butanone (MEK) ND 8.0 0.37 ND 24 1.1 4 10/17/19 19:22 BRF Carbon Disulfide 18 2.0 0.14 55 6.2 0.43 4 10/17/19 19:22 BRF Carbon Tetrachloride 0.14 0.20 0.065 J 0.91 1.3 0.41 4 10/17/19 19:22 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/17/19 19:22 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/17/19 19:22 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/17/19 19:22 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/17/19 19:22 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/17/19 19:22 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/17/19 19:22 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/17/19 19:22 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/17/19 19:22 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/17/19 19:22 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/17/19 19:22 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/17/19 19:22 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/17/19 19:22 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/17/19 19:22 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/17/19 19:22 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/17/19 19:22 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/17/19 19:22 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/17/19 19:22 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/17/19 19:22 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/17/19 19:22 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/17/19 19:22 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/17/19 19:22 BRF Ethanol 8.5 8.0 3.6 Z-01 16 15 6.7 4 10/17/19 19:22 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/17/19 19:22 BRF Ethylbenzene 1.4 0.20 0.12 6.0 0.87 0.50 4 10/17/19 19:22 BRF 4-Ethyltoluene 0.81 0.20 0.12 4.0 0.98 0.60 4 10/17/19 19:22 BRF Heptane 26 0.20 0.12 110 0.82 0.48 4 10/17/19 19:22 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/17/19 19:22 BRF Hexane ND 8.0 0.35 ND 28 1.2 4 10/17/19 19:22 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/17/19 19:22 BRF Isopropanol ND 8.0 0.37 Z-01 ND 20 0.90 4 10/17/19 19:22 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/17/19 19:22 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/17/19 19:22 BRF 4-Methyl-2-pentanone (MIBK) 0.78 0.20 0.10 3.2 0.82 0.43 4 10/17/19 19:22 BRF Naphthalene 0.47 0.20 0.15 Z-01 2.5 1.0 0.80 4 10/17/19 19:22 BRF Propene 880 80 3.7 1500 140 6.4 40 10/17/19 22:24 BRF Styrene ND 0.20 0.12 ND 0.85 0.53 4 10/17/19 19:22 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/17/19 19:22 BRF Page 20 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: SV-9 Canister ID: 202 Final Vacuum(in Hg): -5 Sample ID: 19JO915-09 Canister Size: 1 liter Receipt Vacuum(in Hg): -5 Sample Matrix: Soil Gas Flow Controller ID: 4310 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 17:50 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.89 0.20 0.11 6.0 1.4 0.75 4 10/17/19 19:22 BRF Tetrahydrofuran ND 0.20 0.20 ND 0.59 0.59 4 10/17/19 19:22 BRF Toluene 7.1 0.20 0.10 27 0.75 0.39 4 10/17/19 19:22 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/17/19 19:22 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.075 ND 1.1 0.41 4 10/17/19 19:22 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/17/19 19:22 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/17/19 19:22 BRF Trichlorofluoromethane (Freon 11) ND 0.80 0.15 ND 4.5 0.85 4 10/17/19 19:22 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/17/19 19:22 BRF 1,2,4-Trimethylbenzene 0.98 0.20 0.13 4.8 0.98 0.63 4 10/17/19 19:22 BRF 1,3,5-Trimethylbenzene 0.33 0.20 0.13 1.6 0.98 0.62 4 10/17/19 19:22 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/17/19 19:22 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/17/19 19:22 BRF m&p-Xylene 2.6 0.40 0.23 11 1.7 1.00 4 10/17/19 19:22 BRF o-Xylene 1.2 0.20 0.12 5.1 0.87 0.54 4 10/17/19 19:22 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 106 70-130 10/17/19 22:24 4-Bromofluorobenzene (1) 109 70-130 10/17/19 19:22 Page 21 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: Duplicate Canister ID: 2300 Final Vacuum(in Hg): -5 Sample ID: 19JO915-10 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Soil Gas Flow Controller ID: 4310 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 17:50 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 550 80 28 1300 190 66 40 10/17/19 22:53 BRF Benzene 8.9 0.20 0.082 28 0.64 0.26 4 10/17/19 19:50 BRF Benzyl chloride ND 0.20 0.052 ND 1.0 0.27 4 10/17/19 19:50 BRF Bromodichloromethane ND 0.20 0.074 ND 1.3 0.49 4 10/17/19 19:50 BRF Bromoform ND 0.20 0.090 ND 2.1 0.93 4 10/17/19 19:50 BRF Bromomethane ND 2.0 0.14 ND 7.8 0.53 4 10/17/19 19:50 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 10/17/19 19:50 BRF 2-Butanone (MEK) ND 8.0 0.37 ND 24 1.1 4 10/17/19 19:50 BRF Carbon Disulfide 19 2.0 0.14 60 6.2 0.43 4 10/17/19 19:50 BRF Carbon Tetrachloride 0.14 0.20 0.065 J 0.88 1.3 0.41 4 10/17/19 19:50 BRF Chlorobenzene ND 0.20 0.098 ND 0.92 0.45 4 10/17/19 19:50 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 10/17/19 19:50 BRF Chloroform ND 0.20 0.074 ND 0.98 0.36 4 10/17/19 19:50 BRF Chloromethane ND 0.40 0.14 ND 0.83 0.28 4 10/17/19 19:50 BRF Cyclohexane ND 0.20 0.14 ND 0.69 0.49 4 10/17/19 19:50 BRF Dibromochloromethane ND 0.20 0.066 ND 1.7 0.57 4 10/17/19 19:50 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.078 ND 1.5 0.60 4 10/17/19 19:50 BRF 1,2-Dichlorobenzene ND 0.20 0.096 ND 1.2 0.58 4 10/17/19 19:50 BRF 1,3-Dichlorobenzene ND 0.20 0.10 ND 1.2 0.62 4 10/17/19 19:50 BRF 1,4-Dichlorobenzene ND 0.20 0.12 ND 1.2 0.73 4 10/17/19 19:50 BRF Dichlorodifluoromethane (Freon 12) ND 0.20 0.087 ND 0.99 0.43 4 10/17/19 19:50 BRF 1,1-Dichloroethane ND 0.20 0.061 ND 0.81 0.25 4 10/17/19 19:50 BRF 1,2-Dichloroethane ND 0.20 0.076 ND 0.81 0.31 4 10/17/19 19:50 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 10/17/19 19:50 BRF cis-1,2-Dichloroethylene ND 0.20 0.082 ND 0.79 0.32 4 10/17/19 19:50 BRF trans-1,2-Dichloroethylene ND 0.20 0.081 ND 0.79 0.32 4 10/17/19 19:50 BRF 1,2-Dichloropropane ND 0.20 0.071 ND 0.92 0.33 4 10/17/19 19:50 BRF cis- 1,3 -Dichloropropene ND 0.20 0.070 ND 0.91 0.32 4 10/17/19 19:50 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.073 ND 0.91 0.33 4 10/17/19 19:50 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 10/17/19 19:50 BRF 1,4-Dioxane ND 2.0 1.3 ND 7.2 4.6 4 10/17/19 19:50 BRF Ethanol ND 8.0 3.6 Z-01 ND 15 6.7 4 10/17/19 19:50 BRF Ethyl Acetate ND 0.20 0.15 ND 0.72 0.54 4 10/17/19 19:50 BRF Ethylbenzene 1.3 0.20 0.12 5.5 0.87 0.50 4 10/17/19 19:50 BRF 4-Ethyltoluene 0.81 0.20 0.12 4.0 0.98 0.60 4 10/17/19 19:50 BRF Heptane 21 0.20 0.12 87 0.82 0.48 4 10/17/19 19:50 BRF Hexachlorobutadiene ND 0.20 0.092 ND 2.1 0.98 4 10/17/19 19:50 BRF Hexane ND 8.0 0.35 ND 28 1.2 4 10/17/19 19:50 BRF 2-Hexanone (MBK) ND 0.20 0.12 ND 0.82 0.48 4 10/17/19 19:50 BRF Isopropanol ND 8.0 0.37 Z-01 ND 20 0.90 4 10/17/19 19:50 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.10 ND 0.72 0.36 4 10/17/19 19:50 BRF Methylene Chloride ND 2.0 0.24 ND 6.9 0.84 4 10/17/19 19:50 BRF 4-Methyl-2-pentanone (MIBK) 0.56 0.20 0.10 2.3 0.82 0.43 4 10/17/19 19:50 BRF Naphthalene 0.50 0.20 0.15 Z-01 2.6 1.0 0.80 4 10/17/19 19:50 BRF Propene 1100 80 3.7 1800 140 6.4 40 10/17/19 22:53 BRF Styrene ND 0.20 0.12 ND 0.85 0.53 4 10/17/19 19:50 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.089 ND 1.4 0.61 4 10/17/19 19:50 BRF Page 22 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wake Forest, NC Sample Description/Location: Work Order: 19JO915 Date Received: 10/11/2019 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: Duplicate Canister ID: 2300 Final Vacuum(in Hg): -5 Sample ID: 19JO915-10 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Soil Gas Flow Controller ID: 4310 Flow Controller Type: Fixed -Orifice Sampled: 10/10/2019 17:50 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.92 0.20 0.11 6.3 1.4 0.75 4 10/17/19 19:50 BRF Tetrahydroforan ND 0.20 0.20 ND 0.59 0.59 4 10/17/19 19:50 BRF Toluene 6.6 0.20 0.10 25 0.75 0.39 4 10/17/19 19:50 BRF 1,2,4-Trichlorobenzene ND 0.20 0.14 ND 1.5 1.0 4 10/17/19 19:50 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.075 ND 1.1 0.41 4 10/17/19 19:50 BRF 1,1,2-Trichloroethane ND 0.20 0.082 ND 1.1 0.45 4 10/17/19 19:50 BRF Trichloroethylene ND 0.20 0.081 ND 1.1 0.43 4 10/17/19 19:50 BRF Trichlorofluoromethane (Freon 11) ND 0.80 0.15 ND 4.5 0.85 4 10/17/19 19:50 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 10/17/19 19:50 BRF 1,2,4-Trimethylbenzene 0.98 0.20 0.13 4.8 0.98 0.63 4 10/17/19 19:50 BRF 1,3,5-Trimethylbenzene 0.32 0.20 0.13 1.6 0.98 0.62 4 10/17/19 19:50 BRF Vinyl Acetate ND 4.0 0.12 ND 14 0.44 4 10/17/19 19:50 BRF Vinyl Chloride ND 0.20 0.13 ND 0.51 0.32 4 10/17/19 19:50 BRF m&p-Xylene 2.4 0.40 0.23 10 1.7 1.00 4 10/17/19 19:50 BRF o-Xylene 1.1 0.20 0.12 4.6 0.87 0.54 4 10/17/19 19:50 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene(1) 108 70-130 10/17/19 22:53 4-Bromofluorobenzene(1) 124 70-130 10/17/19 19:50 Page 23 of 48 icon-tes w . ANALYTICAL LABORATORY Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID] 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. Sample Extraction Data Pre-Dil Pre-Dil Pressure Pre Initial Final Batch Dilution Dilution mL mL 413/525-2332 Default Injection mL Actual Injection mL Date 19J0915-01RE1 [SV--1] B243570 1.5 1 N/A 1000 400 30 10/17/19 19J0915-02RE1[SV--2] B243570 1.5 1 N/A 1000 400 15 10/17/19 19J0915-03RE1[SV--3] B243570 1.5 1 N/A 1000 400 30 10/17/19 19J0915-04RE1[SV--4] B243570 1.5 1 N/A 1000 400 30 10/17/19 19J0915-05 [SV-5] B243570 1.5 1 N/A 1000 400 150 10/17/19 19J0915-06 [SV-6] B243570 1.5 1 N/A 1000 400 150 10/17/19 19J0915-07 [SV-7] B243570 1.5 1 N/A 1000 400 150 10/17/19 19J0915-08[SV-8] B243570 1.5 1 N/A 1000 400 150 10/17/19 19J0915-09 [SV-9] B243570 1.5 1 N/A 1000 400 150 10/17/19 19J0915-09RE1[SV--9] B243570 1.5 1 N/A 1000 400 15 10/17/19 19J0915-10 [Duplicate] B243570 1.5 1 N/A 1000 400 150 10/17/19 19J0915-IOREI [Duplicate] B243570 1.5 1 N/A 1000 400 15 10/17/19 Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID] Batch Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL Date 19J0915-01 [SV-1] B243587 1.5 1 N/A 1000 400 150 10/16/19 19J0915-02 [SV-2] B243587 1.5 1 N/A 1000 400 150 10/16/19 19J0915-03 [SV-3] B243587 1.5 1 N/A 1000 400 150 10/16/19 19J0915-04[SV-4] B243587 1.5 1 N/A 1000 400 150 10/16/19 Page 24 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD malyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B243570 - TO-15 Prep Blank (B243570-BLK1) Prepared & Analyzed: 10/17/19 Acetone ND 1.4 Benzene ND 0.035 Benzyl chloride ND 0.035 Bromodichloromethane ND 0.035 Bromoform ND 0.035 Bromomethane ND 0.035 1,3-Butadiene ND 0.035 2-Butanone (MEK) ND 1.4 Carbon Disulfide ND 0.35 Carbon Tetrachloride ND 0.035 Chlorobenzene ND 0.035 Chloroethane ND 0.035 Chloroform ND 0.035 Chloromethane ND 0.070 Cyclohexane ND 0.035 Dibromochloromethane ND 0.035 1,2-Dibromoethane (EDB) ND 0.035 1,2-Dichlorobenzene ND 0.035 1,3-Dichlorobenzene ND 0.035 114-Dichlorobenzene ND 0.035 Dichlorodifluoromethane (Freon 12) ND 0.035 1,1-Dichloroethane ND 0.035 1,2-Dichloroethane ND 0.035 1,1-Dichloroethylene ND 0.035 cis-1,2-Dichloroethylene ND 0.035 trans-1,2-Dichloroethylene ND 0.035 1,2-Dichloropropane ND 0.035 cis- 1,3 -Dichloropropene ND 0.035 trans- l,3-Dichloropropene ND 0.035 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.035 (Freon 114) 1,4-Dioxane ND 0.35 Ethanol ND 1.4 Z-01 Ethyl Acetate ND 0.035 Ethylbenzene ND 0.035 4-Ethyltoluene ND 0.035 Heptane ND 0.035 Hexachlorobutadiene ND 0.035 Hexane ND 1.4 2-Hexanone (MBK) ND 0.035 Isopropanol ND 1.4 Z-01 Methyl tert-Butyl Ether (MTBE) ND 0.035 Methylene Chloride ND 0.35 4-Methyl-2-pentanone (MIBK) ND 0.035 Naphthalene ND 0.035 Propene ND 1.4 Styrene ND 0.035 Page 25 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B243570 - TO-15 Prep Blank (B243570-BLKI) Prepared & Analyzed: 10/17/19 1,1,2,2-Tetrachloroethane ND 0.035 Tetrachloroethylene ND 0.035 Tetrahydrofuran ND 0.035 Toluene ND 0.035 1,2,4-Trichlorobenzene ND 0.035 1, 1, 1 -Trichloroethane ND 0.035 1,1,2-Trichloroethane ND 0.035 Trichloroethylene ND 0.035 Trichlorofluoromethane (Freon 11) ND 0.14 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.14 113) 1,2,4-Trimethylbenzene ND 0.035 1,3,5-Trimethylbenzene ND 0.035 Vinyl Acetate ND 0.70 Vinyl Chloride ND 0.035 m&p-Xylene ND 0.070 o-Xylene ND 0.035 Surrogate: 4-Bromofluorobenzene (1) LCS (B243570-BS1) 8.90 8.00 111 Prepared & Analyzed: 10/17/19 70-130 Acetone 3.69 5.00 73.8 70-130 Benzene 3.81 5.00 76.3 70-130 Benzyl chloride 5.15 5.00 103 70-130 Bromodichloromethane 3.75 5.00 75.0 70-130 Bromoform 4.89 5.00 97.9 70-130 Bromomethane 4.49 5.00 89.7 70-130 1,3-Butadiene 3.52 5.00 70.3 70-130 2-Butanone (MEK) 3.60 5.00 72.1 70-130 Carbon Disulfide 4.06 5.00 81.2 70-130 Carbon Tetrachloride 3.73 5.00 74.6 70-130 Chlorobenzene 4.07 5.00 81.4 70-130 Chloroethane 4.53 5.00 90.6 70-130 Chloroform 4.00 5.00 80.0 70-130 Chloromethane 4.25 5.00 85.0 70-130 Cyclohexane 3.80 5.00 76.0 70-130 Dibromochloromethane 4.13 5.00 82.6 70-130 1,2-Dibromoethane (EDB) 4.20 5.00 83.9 70-130 1,2-Dichlorobenzene 5.58 5.00 112 70-130 1,3-Dichlorobenzene 5.24 5.00 105 70-130 1,4-Dichlorobenzene 5.19 5.00 104 70-130 Dichlorodifluoromethane (Freon 12) 4.16 5.00 83.2 70-130 1,1-Dichloroethane 3.87 5.00 77.4 70-130 1,2-Dichloroethane 3.80 5.00 75.9 70-130 1, 1 -Dichloroethylene 3.82 5.00 76.5 70-130 cis-1,2-Dichloroethylene 3.78 5.00 75.6 70-130 trans-1,2-Dichloroethylene 3.70 5.00 73.9 70-130 1,2-Dichloropropane 3.67 5.00 73.3 70-130 Page 26 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B243570 - TO-15 Prep LCS (B243570-BS1) Prepared & Analyzed: 10/17/19 cis-1,3-Dichloropropene 3.69 5.00 73.9 70-130 trans-1,3-Dichloropropene 4.25 5.00 85.1 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 3.80 5.00 76.0 70-130 (Freon 114) 1,4-Dioxane 4.55 5.00 91.0 70-130 Ethanol 3.40 5.00 68.1 * 70-130 Z-01 Ethyl Acetate 3.92 5.00 78.5 70-130 Ethylbenzene 4.05 5.00 80.9 70-130 4-Ethyltoluene 4.37 5.00 87.4 70-130 Heptane 3.50 5.00 70.1 70-130 Hexachlorobutadiene 5.78 5.00 116 70-130 Hexane 4.23 5.00 84.5 70-130 2-Hexanone (MBK) 3.57 5.00 71.5 70-130 Isopropanol 3.29 5.00 65.9 * 70-130 Z-01 Methyl tert-Butyl Ether (MTBE) 3.72 5.00 74.4 70-130 Methylene Chloride 3.67 5.00 73.3 70-130 4-Methyl-2-pentanone (MIBK) 3.63 5.00 72.6 70-130 Naphthalene 6.54 5.00 131 * 70-130 Z-01 Propene 3.50 5.00 70.0 70-130 Styrene 4.56 5.00 91.3 70-130 1,1,2,2-Tetrachloroethane 4.40 5.00 88.0 70-130 Tetrachloroethylene 4.31 5.00 86.2 70-130 Tetrahydrofuran 3.86 5.00 77.2 70-130 Toluene 3.91 5.00 78.1 70-130 1,2,4-Trichlorobenzene 6.99 5.00 140 * 70-130 L-01 1, 1, 1 -Trichloroethane 3.55 5.00 70.9 70-130 1,1,2-Trichloroethane 4.24 5.00 84.7 70-130 Trichloroethylene 3.88 5.00 77.7 70-130 Trichlorofluoromethane (Freon 11) 3.96 5.00 79.2 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 3.93 5.00 78.6 70-130 113) 1,2,4-Trimethylbenzene 4.39 5.00 87.8 70-130 1,3,5-Trimethylbenzene 4.19 5.00 83.8 70-130 Vinyl Acetate 3.54 5.00 70.7 70-130 Vinyl Chloride 3.85 5.00 77.1 70-130 m&p-Xylene 8.15 10.0 81.5 70-130 o-Xylene 3.97 5.00 79.3 70-130 Surrogate: 4-Bromofluorobenzene (1) 9.43 8.00 118 70-130 Page 27 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD knalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B243570 - TO-15 Prep Duplicate (B243570-DUPI) Source: 19JO915-06 Prepared & Analyzed: 10/17/19 Acetone 21 8.0 49 19 19 7.37 25 Benzene 1.3 0.20 4.0 0.64 1.2 0.960 25 Benzyl chloride ND 0.20 ND 1.0 ND 25 Bromodichloromethane ND 0.20 ND 1.3 ND 25 Bromoform ND 0.20 ND 2.1 ND 25 Bromomethane ND 0.20 ND 0.78 ND 25 1,3-Butadiene ND 0.20 ND 0.44 ND 25 2-Butanone (MEK) 1.1 8.0 3.1 24 1.0 1.53 25 J Carbon Disulfide 5.7 2.0 18 6.2 5.2 10.2 25 Carbon Tetrachloride ND 0.20 ND 1.3 ND 25 Chlorobenzene ND 0.20 ND 0.92 ND 25 Chloroethane ND 0.20 ND 0.53 ND 25 Chloroform 0.24 0.20 1.2 0.98 ND 25 Chloromethane ND 0.40 ND 0.83 ND 25 Cyclohexane ND 0.20 ND 0.69 ND 25 Dibromochloromethane ND 0.20 ND 1.7 ND 25 1,2-Dibromoethane (EDB) ND 0.20 ND 1.5 ND 25 1,2-Dichlorobenzene ND 0.20 ND 1.2 ND 25 1,3-Dichlorobenzene ND 0.20 ND 1.2 ND 25 1,4-Dichlorobenzene ND 0.20 ND 1.2 ND 25 Dichlorodifluoromethane (Freon 12) ND 0.20 ND 0.99 ND 25 1,1-Dichloroethane ND 0.20 ND 0.81 ND 25 1,2-Dichloroethane ND 0.20 ND 0.81 ND 25 1,1-Dichloroethylene ND 0.20 ND 0.79 ND 25 cis-1,2-Dichloroethylene ND 0.20 ND 0.79 ND 25 trans-1,2-Dichloroethylene ND 0.20 ND 0.79 ND 25 1,2-Dichloropropane ND 0.20 ND 0.92 ND 25 cis-1,3-Dichloropropene ND 0.20 ND 0.91 ND 25 trans- 1, 3 -Dichloropropene ND 0.20 ND 0.91 ND 25 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.20 ND 1.4 ND 25 (Freon 114) 1,4-Dioxane ND 2.0 ND 7.2 ND 25 Ethanol 4.3 8.0 8.1 15 ND 25 Z-01, J Ethyl Acetate ND 0.20 ND 0.72 ND 25 Ethylbenzene 0.37 0.20 1.6 0.87 0.36 3.31 25 4-Ethyltoluene 0.55 0.20 2.7 0.98 0.52 4.48 25 Heptane 0.59 0.20 2.4 0.82 0.47 23.4 25 Hexachlorobutadiene ND 0.20 ND 2.1 ND 25 Hexane ND 8.0 ND 28 ND 25 2-Hexanone (MBK) ND 0.20 ND 0.82 ND 25 Isopropanol 1.8 8.0 4.4 20 1.8 1.55 25 Z-01, J Methyl tert-Butyl Ether (MTBE) ND 0.20 ND 0.72 ND 25 Methylene Chloride ND 2.0 ND 6.9 ND 25 4-Methyl-2-pentanone (MIBK) ND 0.20 ND 0.82 ND 25 Naphthalene ND 0.20 ND 1.0 ND 25 Z-01 Propene ND 8.0 ND 14 ND 25 Styrene ND 0.20 ND 0.85 ND 25 Page 28 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B243570 - TO-15 Prep Duplicate (B243570-DUPI) Source: 19JO915-06 Prepared & Analyzed: 10/17/19 1,1,2,2-Tetrachloroethane ND 0.20 ND 1.4 ND 25 Tetrachloroethylene 0.13 0.20 0.90 1.4 0.15 14.1 25 J Tetrahydrofuran ND 0.20 ND 0.59 ND 25 Toluene 1.4 0.20 5.2 0.75 1.4 0.290 25 1,2,4-Trichlorobenzene ND 0.20 ND 1.5 ND 25 1, 1, 1 -Trichloroethane 0.10 0.20 0.57 1.1 0.092 12.2 25 J 1,1,2-Trichloroethane ND 0.20 ND 1.1 ND 25 Trichloroethylene ND 0.20 ND 1.1 ND 25 Trichlorofluoromethane (Freon 11) 0.38 0.80 2.1 4.5 0.36 5.41 25 J 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.80 ND 6.1 ND 25 113) 1,2,4-Trimethylbenzene 0.67 0.20 3.3 0.98 0.65 3.02 25 1,3,5-Trimethylbenzene 0.26 0.20 1.3 0.98 0.26 0.00 25 Vinyl Acetate ND 4.0 ND 14 ND 25 Vinyl Chloride ND 0.20 ND 0.51 ND 25 m&p-Xylene 1.0 0.40 4.3 1.7 0.95 5.34 25 o-Xylene 0.53 0.20 2.3 0.87 0.50 4.65 25 Surrogate: 4-Bromofluorobenzene (1) 8.61 8.00 108 70-130 Batch B243587 - TO-15 Prep Blank (B243587-BLKI) Prepared & Analyzed: 10/16/19 Acetone ND 1.4 Benzene ND 0.035 Benzyl chloride ND 0.035 Bromodichloromethane ND 0.035 Bromoform ND 0.035 Bromomethane ND 0.035 1,3-Butadiene ND 0.035 2-Butanone (MEK) ND 1.4 Carbon Disulfide ND 0.35 Carbon Tetrachloride ND 0.035 Chlorobenzene ND 0.035 Chloroethane ND 0.035 Chloroform ND 0.035 Chloromethane ND 0.070 Cyclohexane ND 0.035 Dibromochloromethane ND 0.035 1,2-Dibromoethane (EDB) ND 0.035 1,2-Dichlorobenzene ND 0.035 1,3-Dichlorobenzene ND 0.035 1,4-Dichlorobenzene ND 0.035 Dichlorodifluoromethane (Freon 12) ND 0.035 1,1-Dichloroethane ND 0.035 1,2-Dichloroethane ND 0.035 1, 1 -Dichloroethylene ND 0.035 cis-1,2-Dichloroethylene ND 0.035 Page 29 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B243587 - TO-15 Prep Blank (B243587-BLKI) Prepared & Analyzed: 10/16/19 trans-1,2-Dichloroethylene ND 0.035 1,2-Dichloropropane ND 0.035 cis- 1,3 -Dichloropropene ND 0.035 trans- l,3-Dichloropropene ND 0.035 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.035 (Freon 114) 1,4-Dioxane ND 0.35 Ethanol ND 1.4 Ethyl Acetate ND 0.035 Ethylbenzene ND 0.035 4-Ethyltoluene ND 0.035 Heptane ND 0.035 Hexachlorobutadiene ND 0.035 Hexane ND 1.4 2-Hexanone (MBK) ND 0.035 Isopropanol ND 1.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 Methylene Chloride ND 0.35 4-Methyl-2-pentanone (MIBK) ND 0.035 Naphthalene ND 0.035 Propene ND 1.4 Styrene ND 0.035 1,1,2,2-Tetrachloroethane ND 0.035 Tetrachloroethylene ND 0.035 Tetrahydrofuran ND 0.035 Toluene ND 0.035 1,2,4-Trichlorobenzene ND 0.035 1, 1, 1 -Trichloroethane ND 0.035 1,1,2-Trichloroethane ND 0.035 Tichloroethylene ND 0.035 Trichlorofluoromethane (Freon 11) ND 0.14 1,1,2-Tichloro-1,2,2-trifluoroethane (Freon ND 0.14 113) 1,2,4-Trimethylbenzene ND 0.035 1,3,5-Trimethylbenzene ND 0.035 Vinyl Acetate ND 0.70 Vinyl Chloride ND 0.035 m&p-Xylene ND 0.070 o-Xylene ND 0.035 Surrogate: 4-Bromofluorobenzene (1) 8.75 8.00 109 70-130 Page 30 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B243587 - TO-15 Prep LCS (B243587-BS1) Prepared & Analyzed: 10/16/19 Acetone 5.66 5.00 113 70-130 Benzene 4.65 5.00 93.1 70-130 Benzyl chloride 5.78 5.00 116 70-130 Bromodichloromethane 4.49 5.00 89.8 70-130 Bromoform 4.85 5.00 97.0 70-130 Bromomethane 4.29 5.00 85.9 70-130 1,3-Butadiene 4.34 5.00 86.9 70-130 2-Butanone (MEK) 4.59 5.00 91.9 70-130 Carbon Disulfide 4.36 5.00 87.2 70-130 Carbon Tetrachloride 4.31 5.00 86.1 70-130 Chlorobenzene 4.44 5.00 88.7 70-130 Chloroethane 4.32 5.00 86.5 70-130 Chloroform 4.05 5.00 81.0 70-130 Chloromethane 4.06 5.00 81.3 70-130 Cyclohexane 3.99 5.00 79.9 70-130 Dibromochloromethane 4.44 5.00 88.7 70-130 1,2-Dibromoethane (EDB) 4.38 5.00 87.7 70-130 1,2-Dichlorobenzene 5.66 5.00 113 70-130 1,3-Dichlorobenzene 5.40 5.00 108 70-130 1,4-Dichlorobenzene 5.54 5.00 111 70-130 Dichlorodifluoromethane(Freon 12) 3.89 5.00 77.7 70-130 1,1-Dichloroethane 4.18 5.00 83.7 70-130 1,2-Dichloroethane 4.00 5.00 79.9 70-130 1,1-Dichloroethylene 4.10 5.00 82.0 70-130 cis-1,2-Dichloroethylene 4.04 5.00 80.7 70-130 trans-1,2-Dichloroethylene 4.09 5.00 81.9 70-130 1,2-Dichloropropane 4.15 5.00 83.1 70-130 cis-1,3-Dichloropropene 4.25 5.00 85.0 70-130 trans- 1, 3 -Dichloropropene 4.53 5.00 90.6 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 4.19 5.00 83.9 70-130 (Freon 114) 1,4-Dioxane 6.27 5.00 125 70-130 Ethanol 5.54 5.00 ill 70-130 Ethyl Acetate 4.28 5.00 85.7 70-130 Ethylbenzene 4.47 5.00 89.3 70-130 4-Ethyltoluene 4.98 5.00 99.7 70-130 Heptane 4.68 5.00 93.6 70-130 Hexachlorobutadiene 5.43 5.00 109 70-130 Hexane 4.38 5.00 87.6 70-130 2-Hexanone (MBK) 5.18 5.00 104 70-130 Isopropanol 5.01 5.00 100 70-130 Methyl tert-Butyl Ether (MTBE) 3.90 5.00 78.1 70-130 Methylene Chloride 4.01 5.00 80.2 70-130 4-Methyl-2-pentanone (MIBK) 5.34 5.00 107 70-130 Naphthalene 7.25 5.00 145 * 70-130 Z-01, V-35 Propene 4.21 5.00 84.1 70-130 Styrene 4.44 5.00 88.9 70-130 Page 31 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B243587 - TO-15 Prep LCS (B243587-BS1) Prepared & Analyzed: 10/16/19 1,1,2,2-Tetrachloroethane 5.00 5.00 100 70-130 Tetrachloroethylene 4.25 5.00 85.0 70-130 Tetrahydrofuran 4.60 5.00 92.0 70-130 Toluene 4.40 5.00 87.9 70-130 1,2,4-Trichlorobenzene 7.06 5.00 141 * 70-130 L-01, V-3( 1, 1, 1 -Trichloroethane 4.04 5.00 80.8 70-130 1,1,2-Trichloroethane 4.52 5.00 90.4 70-130 Trichloroethylene 4.51 5.00 90.3 70-130 Trichlorofluoromethane (Freon 11) 4.69 5.00 93.8 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 4.06 5.00 81.2 70-130 113) 1,2,4-Trimethylbenzene 5.43 5.00 109 70-130 1,3,5-Trimethylbenzene 5.12 5.00 102 70-130 Vinyl Acetate 4.72 5.00 94.4 70-130 Vinyl Chloride 4.25 5.00 84.9 70-130 m&p-Xylene 9.72 10.0 97.2 70-130 o-Xylene 4.70 5.00 94.1 70-130 Surrogate: 4-Bromofluorobenzene (1) 8.77 8.00 110 70-130 Page 32 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-01 Laboratory fortified blank /laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. V-35 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is estimated. V-36 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Z-01 Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in house limits of 50-150%. Page 33 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYST TPH Thomas P. Hnitecki RLF Rebecca Faust KKM Kerry K. McGee BRF Brittany R. Fisk Page 34 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S038528-ICV1) Lab File ID: B1920819.D Analyzed: 07/27/19 19:24 Bromochloromethane (1) 144000 5.05 141846 5.054 102 60 - 140 -0.0040 +/-0.50 1,4-Difluorobenzene (1) 338979 6.264 331570 6.268 102 60 - 140 -0.0040 +/-0.50 Chlorobenzene-d5(1) 300441 9.857 293128 9.861 102 60-140 -0.0040 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S039721-ICV1) Lab File ID: G1923934.13 Analyzed: 08/28/19 12:54 Bromochloromethane (1) 443826 8.54 448077 8.54 99 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1177845 10.32 1185200 10.32 99 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1032941 14.697 1038060 14.697 100 60-140 0.0000 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q Calibration Check (SO41606-CCVI) Lab File ID: B1929004.D Analyzed: 10/17/19 13:10 Bromochloromethane (1) 158008 5.049 141846 5.054 111 60 - 140 -0.0050 +/-0.50 1,4-Difluorobenzene (1) 391181 6.263 331570 6.268 118 60 - 140 -0.0050 +/-0.50 Chlorobenzene-d5(1) 359482 9.856 293128 9.861 123 60-140 -0.0050 +/-0.50 LCS (B243570-BS1 ) Lab File ID: B1929005.D Analyzed: 10/17/19 13:41 Bromochloromethane (1) 154013 5.049 158008 5.049 97 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 371949 6.263 391181 6.263 95 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 325568 9.856 359482 9.856 91 60-140 0.0000 +/-0.50 Blank (B243570-BLK1) Lab File ID: B 1929008.13 Analyzed: 10/17/19 15:20 Bromochloromethane (1) 151723 5.049 158008 5.049 96 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 350087 6.263 391181 6.263 89 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 317060 9.856 359482 9.856 88 60-140 0.0000 +/-0.50 SV-5 (19J0915-05 ) Lab File ID: B1929009.D Analyzed: 10/17/19 17:26 Bromochloromethane (1) 168337 5.05 158008 5.049 107 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene (1) 406307 6.263 391181 6.263 104 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 364335 9.857 359482 9.856 101 60-140 0.0010 +/-0.50 SV-6 (19J0915-06 ) Lab File ID: B1929010.D Analyzed: 10/17/19 17:55 Bromochloromethane (1) 157074 5.049 158008 5.049 99 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 428651 6.263 391181 6.263 110 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 376351 9.856 359482 9.856 105 60-140 0.0000 +/-0.50 Page 35 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q SV-7 (19J0915-07) Lab File ID: B 192901 LD Analyzed: 10/17/19 18:24 Bromochloromethane (1) 168728 5.05 158008 5.049 107 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene (1) 444784 6.264 391181 6.263 114 60 - 140 0.0010 +/-0.50 Chlorobenzene-d5(1) 395531 9.857 359482 9.856 110 60-140 0.0010 +/-0.50 SV-8 (19J0915-08) Lab File ID: B1929012.D Analyzed: 10/17/19 18:53 Bromochloromethane (1) 181314 5.048 158008 5.049 115 60 - 140 -0.0010 +/-0.50 1,4-Difluorobenzene (1) 450669 6.268 391181 6.263 115 60 - 140 0.0050 +/-0.50 Chlorobenzene-d5(1) 393300 9.855 359482 9.856 109 60-140 -0.0010 +/-0.50 SV-9 (19J0915-09) Lab File ID: B1929013.D Analyzed: 10/17/19 19:22 Bromochloromethane (1) 190843 5.054 158008 5.049 121 60 - 140 0.0050 +/-0.50 1,4-Difluorobenzene (1) 464947 6.268 391181 6.263 119 60 - 140 0.0050 +/-0.50 Chlorobenzene-d5(1) 421122 9.855 359482 9.856 117 60-140 -0.0010 +/-0.50 Duplicate (19J0915-10) Lab File ID: B1929014.D Analyzed: 10/17/19 19:50 Bromochloromethane (1) 190496 5.048 158008 5.049 121 60 - 140 -0.0010 +/-0.50 1,4-Difluorobenzene (1) 504889 6.268 391181 6.263 129 60 - 140 0.0050 +/-0.50 Chlorobenzene-d5(1) 454297 9.855 359482 9.856 126 60-140 -0.0010 +/-0.50 Duplicate (B243570-DUP1) Lab File ID: B1929017.D Analyzed: 10/17/19 21:57 Bromochloromethane (1) 173272 5.049 158008 5.049 110 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 391019 6.269 391181 6.263 100 60 - 140 0.0060 +/-0.50 Chlorobenzene-d5(1) 350440 9.856 359482 9.856 97 60-140 0.0000 +/-0.50 SV-9 (19J0915-09RE1) Lab File ID: B1929018.D Analyzed: 10/17/19 22:24 Bromochloromethane (1) 164684 5.053 158008 5.049 104 60 - 140 0.0040 +/-0.50 1,4-Difluorobenzene (1) 375310 6.267 391181 6.263 96 60 - 140 0.0040 +/-0.50 Chlorobenzene-d5(1) 332725 9.854 359482 9.856 93 60-140 -0.0020 +/-0.50 Duplicate (19J0915-10REl) Lab File ID: B1929019.D Analyzed: 10/17/19 22:53 Bromochloromethane (1) 167292 5.055 158008 5.049 106 60 - 140 0.0060 +/-0.50 1,4-Difluorobenzene (1) 389898 6.269 391181 6.263 100 60 - 140 0.0060 +/-0.50 Chlorobenzene-d5(1) 351783 9.856 359482 9.856 98 60-140 0.0000 +/-0.50 SV-1 (19J0915-OIRE1) Lab File ID: B1929022.D Analyzed: 10/18/19 08:57 Bromochloromethane (1) 180016 5.043 158008 5.049 114 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene (1) 430551 6.262 391181 6.263 110 60 - 140 -0.0010 +/-0.50 Chlorobenzene-d5(1) 379565 9.856 359482 9.856 106 60-140 0.0000 +/-0.50 SV-2 (19J0915-02RE1) Lab File ID: B1929023.D Analyzed: 10/18/19 09:25 Bromochloromethane (1) 173058 5.052 158008 5.049 110 60 - 140 0.0030 +/-0.50 1,4-Difluorobenzene (1) 418324 6.266 391181 6.263 107 60 - 140 0.0030 +/-0.50 Chlorobenzene-d5(1) 373319 9.853 359482 9.856 104 60-140 -0.0030 +/-0.50 Page 36 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q SV-3 (19J0915-03RE1) Lab File ID: B1929024.D Analyzed: 10/18/19 09:52 Bromochloromethane (1) 164128 5.048 158008 5.049 104 60 - 140 -0.0010 +/-0.50 1,4-Difluorobenzene (1) 408427 6.268 391181 6.263 104 60 - 140 0.0050 +/-0.50 Chlorobenzene-d5(1) 362686 9.855 359482 9.856 101 60-140 -0.0010 +/-0.50 SV-4 (19J0915-04RE1) Lab File ID: B1929025.D Analyzed: 10/18/19 10:20 Bromochloromethane (1) 162800 5.054 158008 5.049 103 60 - 140 0.0050 +/-0.50 1,4-Difluorobenzene (1) 406789 6.268 391181 6.263 104 60 - 140 0.0050 +/-0.50 Chlorobenzene-d5(1) 358665 9.855 359482 9.856 100 60-140 -0.0010 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q Calibration Check (SO41612-CCV1) Lab File ID: G1928904.13 Analyzed: 10/16/19 11:46 Bromochloromethane (1) 329837 8.54 448077 8.54 74 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 785602 10.32 1185200 10.32 66 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 677019 14.691 1038060 14.697 65 60-140 -0.0060 +/-0.50 LCS (B243587-BS1 ) Lab File ID: G1928905.13 Analyzed: 10/16/19 12:26 Bromochloromethane (1) 340225 8.54 329837 8.54 103 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 796303 10.314 785602 10.32 101 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 729382 14.691 677019 14.691 108 60-140 0.0000 +/-0.50 Blank (B243587-BLK1) Lab File ID: G1928914.13 Analyzed: 10/16/19 19:41 Bromochloromethane (1) 339459 8.546 329837 8.54 103 60 - 140 0.0060 +/-0.50 1,4-Difluorobenzene (1) 755562 10.32 785602 10.32 96 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 697637 14.697 677019 14.691 103 60-140 0.0060 +/-0.50 SV-1 (19J0915-01) Lab File ID: G1928915.13 Analyzed: 10/16/19 20:21 Bromochloromethane (1) 349889 8.54 329837 8.54 106 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 793972 10.32 785602 10.32 101 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 743150 14.697 677019 14.691 110 60-140 0.0060 +/-0.50 SV-2 (19J0915-02 ) Lab File ID: G1928916.13 Analyzed: 10/16/19 21:02 Bromochloromethane (1) 359340 8.539 329837 8.54 109 60 - 140 -0.0010 +/-0.50 1,4-Difluorobenzene (1) 818925 10.32 785602 10.32 104 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 759711 14.697 677019 14.691 112 60-140 0.0060 +/-0.50 SV-3 (19J0915-03 ) Lab File ID: G1928917.1) Analyzed: 10/16/19 21:42 Bromochloromethane (1) 357463 8.54 329837 8.54 108 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 814459 10.32 785602 10.32 104 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 753145 14.691 677019 14.691 ill 60-140 0.0000 +/-0.50 Page 37 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q SV-4 (19,10915-04) Lab File ID: G1928918.D Analyzed: 10/16/19 22:23 Bromochloromethane (1) 346188 8.54 329837 8.54 105 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 793020 10.32 785602 10.32 101 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 740049 14.697 677019 14.691 109 60-140 0.0060 +/-0.50 Page 38 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S041606-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 4.05 1.061501 0.8602096 -19.0 30 Benzene A 5.00 4.31 0.8735206 0.75283 -13.8 30 Benzyl chloride A 5.00 4.22 0.6996465 0.5905564 -15.6 30 Bromodichloromethane A 5.00 4.30 0.6034027 0.5189986 -14.0 30 Bromoform A 5.00 5.01 0.5598351 0.5613989 0.3 30 Bromomethane L 5.00 5.46 0.7671881 0.6555415 9.3 30 1,3-Butadiene A 5.00 4.15 0.5165437 0.4290112 -16.9 30 2-Butanone (MEK) A 5.00 4.05 1.510652 1.223847 -19.0 30 Carbon Disulfide A 5.00 4.52 1.951102 1.765521 -9.5 30 Carbon Tetrachloride A 5.00 4.31 0.4907439 0.4234316 -13.7 30 Chlorobenzene A 5.00 4.35 0.7671143 0.6670131 -13.0 30 Chloroethane A 5.00 5.12 0.3286624 0.33655 2.4 30 Chloroform A 5.00 4.61 1.338096 1.234662 -7.7 30 Chloromethane L 5.00 4.84 0.7600805 0.5964964 -3.2 30 Cyclohexane A 5.00 4.35 0.3968377 0.3449861 -13.1 30 Dibromochloromethane A 5.00 4.42 0.6131759 0.5422692 -11.6 30 1,2-Dibromoethane(EDB) A 5.00 4.39 0.5188831 0.4555889 -12.2 30 1,2-Dichlorobenzene A 5.00 5.14 0.5529051 0.5684936 2.8 30 1,3-Dichlorobenzene A 5.00 4.97 0.6156422 0.6119872 -0.6 30 1,4-Dichlorobenzene A 5.00 4.92 0.6222462 0.6117246 -1.7 30 Dichlorodifluoromethane (Freon 12) A 5.00 4.97 1.496329 1.48675 -0.6 30 1,1-Dichloroethane A 5.00 4.46 1.161609 1.037183 -10.7 30 1,2-Dichloroethane A 5.00 4.41 0.7744181 0.6835097 -11.7 30 1,1-Dichloroethylene A 5.00 4.54 0.9609644 0.8734343 -9.1 30 cis-1,2-Dichloroethylene A 5.00 4.46 0.8593978 0.767151 -10.7 30 trans-1,2-Dichloroethylene A 5.00 4.35 0.9369909 0.815827 -12.9 30 1,2-Dichloropropane A 5.00 4.24 0.3089133 0.2621804 -15.1 30 cis- 1,3 -Dichloropropene A 5.00 4.34 0.5065485 0.4396083 -13.2 30 trans- l,3-Dichloropropene A 5.00 4.55 0.3948445 0.3592894 -9.0 30 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 1 A 5.00 4.69 1.85497 1.739173 -6.2 30 1,4-Dioxane A 5.00 4.99 0.1503196 0.1499746 -0.2 30 Ethanol L 5.00 4.47 0.2361095 0.1906536 -10.6 30 Ethyl Acetate A 5.00 4.70 0.2359238 0.2217812 -6.0 30 Ethylbenzene A 5.00 4.34 1.254903 1.089813 -13.2 30 4-Ethyltoluene A 5.00 4.46 1.170616 1.044338 -10.8 30 Heptane A 5.00 4.07 0.2735238 0.2226079 -18.6 30 Hexachlorobutadiene A 5.00 5.36 0.3591407 0.3851809 7.3 30 Hexane L 5.00 4.98 0.492452 0.4011544 -0.4 30 Page 39 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S041606-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone(MBK) A 5.00 3.71 0.7409122 0.5499113 -25.8 30 Isopropanol L 5.00 4.72 1.490308 1.134596 -5.5 30 Methyl tert-Butyl Ether (MTBE) A 5.00 4.28 1.846042 1.578472 -14.5 30 Methylene Chloride A 5.00 4.24 0.8402594 0.7122171 -15.2 30 4-Methyl-2-pentanone (MI13K) A 5.00 4.08 0.7161798 0.5844701 -18.4 30 Naphthalene A 5.00 5.23 0.6049938 0.6327816 4.6 30 Propene A 5.00 4.14 0.5842939 0.4838135 -17.2 30 Styrene A 5.00 4.80 0.6473158 0.6221218 -3.9 30 1,1,2,2-Tetrachloroethane A 5.00 4.49 0.7674959 0.6889157 -10.2 30 Tetrachloroethylene A 5.00 4.62 0.4931961 0.4557269 -7.6 30 Tetrahydroforan A 5.00 4.20 0.8848512 0.7432738 -16.0 30 Toluene A 5.00 4.17 0.9917029 0.8265404 -16.7 30 1,2,4-Trichlorobenzene A 5.00 5.64 0.2985806 0.3368625 12.8 30 1, 1, 1 -Trichloroethane A 5.00 4.24 0.4929082 0.4180203 -15.2 30 1,1,2-Trichloroethane A 5.00 4.48 0.3379477 0.3030716 -10.3 30 Trichloroethylene A 5.00 4.35 0.357385 0.311054 13.0 30 Trichlorofluoromethane(Freon 11) A 5.00 4.56 1.428406 1.30204 -8.8 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 4.65 1.290004 1.199848 -7.0 30 1,2,4-Trimethylbenzene A 5.00 4.45 0.8903904 0.7926784 -11.0 30 1,3,5-Trimethylbenzene A 5.00 4.38 0.9344044 0.8175452 -12.5 30 Vinyl Acetate A 5.00 3.76 1.947711 1.466721 -24.7 30 Vinyl Chloride A 5.00 4.48 0.6970639 0.625062 -10.3 30 m&p-Xylene A 10.0 8.70 0.9303396 0.8092377 -13.0 30 o-Xylene A 5.00 4.19 0.9311699 0.7795083 -16.3 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 40 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S041612-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 4.59 0.9996126 0.9170881 -8.3 30 Benzene A 5.00 4.25 0.8362378 0.7109982 -15.0 30 Benzyl chloride A 5.00 5.63 0.7444344 0.8379582 12.6 30 Bromodichloromethane A 5.00 4.14 0.6360305 0.5268989 -17.2 30 Bromoform A 5.00 4.81 0.4550491 0.4375464 -3.8 30 Bromomethane A 5.00 4.06 0.5413212 0.4400477 -18.7 30 1,3-Butadiene A 5.00 4.04 0.5071688 0.4095114 -19.3 30 2-Butanone (MEK) A 5.00 4.00 1.437726 1.150178 -20.0 30 Carbon Disulfide A 5.00 4.01 1.922763 1.542187 -19.8 30 Carbon Tetrachloride A 5.00 4.10 0.5343296 0.4384999 -17.9 30 Chlorobenzene A 5.00 4.41 0.8157002 0.7192968 -11.8 30 Chloroethane A 5.00 4.11 0.3245753 0.2665365 -17.9 30 Chloroform A 5.00 3.80 1.505338 1.1449 -23.9 30 Chloromethane A 5.00 3.88 0.6578021 0.5098955 -22.5 30 Cyclohexane A 5.00 3.74 0.3926285 0.2933577 -25.3 30 Dibromochloromethane A 5.00 4.45 0.5907777 0.5255604 -11.0 30 1,2-Dibromoethane (EDB) A 5.00 4.32 0.5578998 0.4816881 -13.7 30 1,2-Dichlorobenzene A 5.00 5.31 0.5031563 0.534723 6.3 30 1,3-Dichlorobenzene A 5.00 5.22 0.5826651 0.6079215 4.3 30 1,4-Dichlorobenzene A 5.00 5.28 0.565436 0.5968163 5.5 30 Dichlorodifluoromethane (Freon 12) A 5.00 3.54 1.564405 1.108698 -29.1 30 1,1-Dichloroethane A 5.00 3.80 1.326073 1.008159 -24.0 30 1,2-Dichloroethane A 5.00 3.75 0.9846894 0.738013 -25.1 30 1,1-Dichloroethylene A 5.00 3.79 1.147818 0.8700152 -24.2 30 cis-1,2-Dichloroethylene A 5.00 3.82 0.9602326 0.7337394 -23.6 11 30 trans-1,2-Dichloroethylene A 5.00 3.85 0.9932025 0.7653574 -22.9 30 1,2-Dichloropropane A 5.00 3.88 0.3549055 0.2753557 -22.4 30 cis-1,3-Dichloropropene A 5.00 4.12 0.5059353 0.4174165 -17.5 30 trans-1,3-Dichloropropene A 5.00 4.08 0.4295861 0.3508016 -18.3 30 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 1 A 5.00 4.19 1.520134 1.274855 -16.1 30 1,4-Dioxane A 5.00 4.61 0.1214858 0.1119773 -7.8 30 Ethanol A 5.00 5.14 0.1645103 0.1689368 2.7 30 Ethyl Acetate A 5.00 4.24 0.2335069 0.1981536 -15.1 30 Ethylbenzene A 5.00 4.40 1.37273 1.206553 -12.1 30 4-Ethyltoluene A 5.00 4.82 1.267281 1.221288 -3.6 30 Heptane A 5.00 4.42 0.2655831 0.2350605 -11.5 30 Hexachlorobutadiene 4 5.00 5.25 0.2909596 0.3054922 5.0 30 Hexane L 5.00 4.18 0.8819918 0.7066957 -16.5 30 Page 41 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S041612-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 4.46 0.6314745 0.5630566 -10.8 30 Isopropanol A 5.00 4.42 0.9582604 0.8474295 -11.6 30 Methyl tert-Butyl Ether (MTBE) A 5.00 3.66 1.920089 1.404767 -26.8 30 Methylene Chloride A 5.00 3.82 0.8859416 0.6767318 -23.6 30 4-Methyl-2-pentanone (MI13K) A 5.00 4.60 0.6252441 0.5748723 -8.1 30 Naphthalene A 5.00 6.46 0.6346751 0.8193235 29.1 30 Propene A 5.00 3.96 0.6073756 0.4803779 -20.9 30 Styrene A 5.00 4.51 0.7335872 0.6621876 -9.7 30 1,1,2,2-Tetrachloroethane A 5.00 4.77 0.7522962 0.7170706 -4.7 30 Tetrachloroethylene A 5.00 4.24 0.4346519 0.36833 -15.3 30 Tetrahydroforan A 5.00 3.86 0.2760485 0.213269 -22.7 30 Toluene A 5.00 4.29 1.096404 0.940178 -14.2 30 1,2,4-Trichlorobenzene A 5.00 6.39 0.2705311 0.3457203 27.8 30 1, 1, 1 -Trichloroethane A 5.00 3.99 0.5629167 0.4490376 -20.2 30 1,1,2-Trichloroethane A 5.00 4.44 0.3731061 0.3316988 -11.1 30 Trichloroethylene A 5.00 4.16 0.3587167 0.2982029 16.9 30 Trichlorofluoromethane (Freon 11) A 5.00 4.38 1.298228 1.13841 -12.3 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 3.87 1.350265 1.045297 -22.6 30 1,2,4-Trimethylbenzene A 5.00 5.12 0.9531808 0.9761546 2.4 30 1,3,5-Trimethylbenzene A 5.00 4.98 1.026356 1.02192 -0.4 30 Vinyl Acetate A 5.00 4.31 2.0403 1.759356 -13.8 30 Vinyl Chloride A 5.00 4.04 0.6780775 0.5485473 -19.1 30 m&p-Xylene A 1 10.0 9.58 0.9941566 0.9528808 -4.2 30 o-Xylene A 1 5.00 4.63 1.04101 0.9642435 -7.4 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 42 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Acetone Benzene Benzyl chloride Bromodichloromethane Bromoform Bromomethane 1,3-Butadiene 2-Butanone (MEK) Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Cyclohexane Dibromochloromethane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane (Freon 12) 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethylene cis-1,2-Dichloroethylene trans- l,2-Dichloro ethylene 1,2-Dichloropropane cis- 1,3 -Dichloropropene trans- 1, 3 -Dichloropropene 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 1,4-Dioxane Ethanol Ethyl Acetate Ethylbenzene 4-Ethyltoluene Heptane Hexachlorobutadiene Hexane 2-Hexanone (MBK) Isopropanol Methyl tart -Butyl Ether (MTBE) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Naphthalene Propene Styrene 1,1,2,2-Tetrachloroethane Certifications AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH NY,ME,NH AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH,VA Page 43 of 48 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA TO-15 in Air Tetrachloroethylene AIHA,FL,NJ,NY,ME,NH,VA Tetrahydrofuran AIHA Toluene AIHA,FL,NJ,NYM E,NH,VA 1,2,4-Trichlorobenzene AIHA,NJ,NY,ME,NH,VA 1, 1, 1 -Trichloroethane AIHA,FL,NJ,NY,ME,NH,VA 1,1,2-Trichloroethane AIHA,FL,NJ,NY,ME,NH,VA Trichloroethylene AIHA,FL,NJ,NY,ME,NH,VA Trichlorofluoromethane (Freon 11) AIHA,NY,ME,NH 1,1,2-Trichloro-1,2,2-ttifluoroethane (Freon 113) AIHA,NJ,NY,ME,NH,VA 1,2,4-Trimethylbenzene AIHA,NJ,NY,ME,NH 1,3,5-Trimethylbenzene AIHA,NJ,NY,ME,NH Vinyl Acetate AIHA,FLNJ,NY,ME,NH,VA Vinyl Chloride AIHA,FLNJ,NY,ME,NH,VA m&p-Xylene AIHA,FL,NJ,NY,ME,NH,VA o-Xylene AIHA,FL,NJ,NY,ME,NH,VA The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2017 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2020 CT Connecticut Department of Publilc Health PH-0567 09/30/2021 NY New York State Department of Health 10899 NELAP 04/l/2020 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2020 RI Rhode Island Department of Health LA000112 12/30/2019 NC North Carolina Div. of Water Quality 652 12/31/2019 NJ New Jersey DEP MA007 NELAP 06/30/2020 FL Florida Department of Health E871027 NELAP 06/30/2020 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2020 ME State of Maine 2011028 06/9/2021 VA Commonwealth of Virginia 460217 12/14/2019 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2020 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2020 NC-DW North Carolina Department of Health 25703 07/31/2020 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2020 Page 44 of 48 7a 61 O — R GS y N ::r fij Cep 4 F- sue, H Eno :: c a �g+ ' _ R-. ems +� (V 4 t`1 yp^���g Q a w ¢ 0 s yu uQr� A Exam gg C3 pca¢ttso.-J Z °$daaLsN °Fa E u E d ~' N a cam► 6 Gt —1! N K.1 x yrEl 0 a y gss vEQ�� 0 Lab Receipt Pressure �` �� `fir o Final Pressure U cc L.n Js � } Ln Initial Pressure �+ e u c cn Ev ~ : O W CL -, Q 0 ❑ ❑ Of M 1 x E N a _91 r- N J N r G r= Q y. .-�- d R ¢ 6 a Cz _ ❑ ❑ ❑ V i �f) v 7 Qii W_ qL CL Cr LJ El �j, M Lt1 Cr R V S nF m v n.' Cn 2 ❑ ❑ ❑ El El El r Q Un 0 ca o U l lC E [ E C aui❑❑ q 'pro o Us c E E c— E 5 r ""` E E N «.. g G% ✓ \� j� t a -.per' ii � , V + �e !�' m aE 4s e!• M C ° .a✓ / t xa E ��&.'. L °. ► i a lRS f j 6Ea ..? U• Amp 'Y1 IIA p R t tO E C LM YJ qi Q1 1J 2n x u c C Vie m 7S,.... Z N c a a y u cs a E y^ ¢ rL . n i ri u° cn c° ax s a Page 45 of 48 ¢^p /f C: l a s a� � Vro .W C !02-0 0 0 Ry o JOmy 2� m inJ� a Ua 5 Ln ❑ El Cc h° of y4a�omo Cn CN aLab Receipt Pressure E Final Pressure 0 S Initial Pressure 1=0 LLJQ 0 sEl mw a (A H q 3 j... ® CAA a� v a a o a L7 a c.3 0 � d:. ❑ ❑ � C C O C � v d rs o a C q+g y ZS 41 Q a3 ❑ ❑ ❑ U C CL r n ~ El ^a in n m m E cy in_ O U LU LLLLJ K C ,.... u ❑ ❑ ❑ m L LO 3n c c E E E E E E ,y N U N @j + E WO en Y .L1 O r✓ E a1 W Tr Y Y„� C CU x 7—nV"• � .. Tj T Sz p ' 'CS -a) '0 , R5 4 C. - Cl- CL C3 N ` - '' O 9 a7 aJ C! a7 C7 U Page 46 of 48 10/14/2019 Track your package or shipment with FedEx Tracking 776701289801 ' 3 Delivered Monday 10/14/2019 at 1- 4 pm DELIVERED Signed for by: WWASENSKI GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM TO Raleigh, NC US Fast Longrr,eadov,, iv'A OS Multiple -piece Shipment % Piece shipment . .. . TRACKING NUMBER ;SHIPPER. , SHIPPER. STATE .. .. SWiA HATE STATUS...: DEI ltfERY RATE -..DESTINATION/RECIPIENT.. CITY, STATE 776701288562 DURHAM, NC 10/11/2019 10/ 14i,D19 EAS7 LONGMEADOW, MA (rrlaSter) 776701288871 DURHAM, NC 10/11/2019 10/14/2019 EAST LONGiMEADOW, MA ; 776701289157 DURHAN4, NC 10/11/2019 10/14/2019 EAST LONGMEADOW, MA 776701289205 DOREIA',4, NC 10/11/2019 10/14/2019 EAST LON&VEADOW, MA 776701289238 DURHAM, NC 10/11/2019 10/14/2019 EAST LONGMEADOW, MA 776701269411 DURH,� M, NC 10/11/2019 10; i4r2019 EAST LC?iJGMEADOIN, NA 7767012898C"l DURHAM, NC 1C/11/2019 10/14/2W 9 EAST LONGMEADOW, MA Shipment Facts TRACKING NUMBER SERVICE 776701289801 FedEx Ground REFERENCE 80 https://www.fedex.com/apps/fedextrackl?action=track&trackingnumber=7767012898Ol&cntry_code=us&locale=en_US Page 47 of 48 Client---W_ Received By Et , T Date How were the samples In Cooler received? In Box Were samples within Temperature By Gun # Compliance? 2-6°C By Blank # Was Custody Seal Intact? Was COC Relinquished ? i Are there any loose caps/valves on any samples? Is COC in ink/ Legible? �ittt t Time _ l On Ice No Ice Ambient Melted Ice Actual I emp - Actual Temp - Were Samples Tampered with? Does Chain Agree With Samples? E Did COC Include all Client i Analysis j Sampler Name R Pertinent Information? Project ID's 1 Collection Dates/Times Are Sample Labels filled out and legible? Are there Rushes? � Samples are received within holding time? 7 Proper Media Used? 7 Individually Certified Cans? Are there Trip Blanks? F-- Is there enough Volume? i Who was notified? Page 48 of 48 Appendix E EPA Risk Calculator Input and Output Forms North Carolina Department of Environmental Quality Risk Calculator Version Date: February 2018 Basis: November 2017 EPA RSL Table Site Name: Wheat Fields Development Site Address: 1009 Forestville Road, Wake Forest, Wake County, NC DEQ Section: Brownfields Site ID: 22051-19-092 Exposure Unit ID: Submittal Date: 10/28/2019 Prepared By: Laura Elliott, P.G., WithersRavenel, Inc. Reviewed B Brian Bellis, P.G., WithersRavenel, Inc. North Carolina DEQ Risk Calculator Complete Exposure Pathways Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Note: Risk output will only be calculated for complete exposure pathways. Receptor Pathway Check box if pathway complete PRIMARY PATHWAYS Resident Soil Combined Pathways ❑ Groundwater Combined Pathways ❑ Non -Residential Worker Soil Combined Pathways 0 Groundwater Combined Pathways 0 Construction Worker Soil Combined Pathways 0 User Defined Soil Combined Pathways ❑ Surface Water Combined Pathways ❑ VAPOR INTRUSION PATHWAYS Resident Groundwater to Indoor Air 0 Soil Gas to Indoor Air 0 Indoor Air ❑ Non -Residential Worker Groundwater to Indoor Air 0 Soil Gas to Indoor Air 0 Indoor Air ❑ CONTAMINANT MIGRATION PATHWAYS Protection of Groundwater Use Source Soil 0 Source Groundwater 0 Protection of Surface Water Source Soil 0 Source Groundwater 0 North Carolina DEQ Risk Calculator Summary of Risk Assessment Output Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: PRIMARY CALCULATORS Receptor Pathway CarcinogenicRisk Hazard Index Risk exceeded? Resident Soil Combined Pathways 1.2E-04 1.3E+00 YES Groundwater Combined Pathways* 6.IE-03 2.2E+02 YES Non -Residential Worker Soil Combined Pathways 1.1E-05 2.5E-01 NO Groundwater Combined Pathways* 1.5E-03 5.3E+01 YES Construction Worker Soil Combined Pathways 5.5E-06 4.6E-01 NO User Defined Soil Combined Pathways NC NC NC Surface Water Combined Pathways* NC NC NC RL VAPOR INTRUSION CALCULATORS qr Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Resident Groundwater to Indoor Air 1.1E-03 4.6E+01 YES Soil Gas to Indoor Air 4.4E-06 1.2E-01 NO Indoor Air NC NC NC Non -Residential Worker Groundwater to Indoor Air 2.4E-04 1.1E+01 YES Soil Gas to Indoor Air 3.4E-07 9.2E-03 NO Indoor Air NC NC NC CONTAMINANT MIGRATION CALCULATORS Pathway Source Target POE Concentrations Exceeded? Protection of Groundwater Use Source Soil Exceedence of 2L at POE? YES Source Groundwater Exceedence of 2L at POE? YES Protection of Surface Water Source Soil Exceedence of 213 at POE? NO Source Groundwater I Exceedence of 213 at POE? NO Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 213 Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. North Carolina DEQ Risk Calculator Exposure Factors and Target Risks Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Exposure Parameter Default Value Site Specific Value Justification General Target Cancer Risk (individual) 1.0E-06 1.0E-06 Target Cancer Risk (cumulative) 1.0E-04 1.0E-04 Target Hazard Index (individual) 2.0E-01 2.0E-01 Target Hazard Index (cumulative) 1.0E+40 1.0E+00 Residential Child Lifetime (LT) (years) 70 70 Body Weight(BW) (kg) 15 15 Exposure Duration (ED) (yr) 6 6 Exposure Frequency (EF) (d/yr) 350 350 Exposure Time (ET) (hr) 24 24 Skin Surface Area - Soil Exposure (SAg) (cm2) 2373 2373 Soil Adherence Factor (AF) (mg/cm2) 0.2 0.2 Soil Ingestion Rate (IRS) (mg/day) 200 200 Skin Surface Area - Water Exposure (SA,) (cm2) 6365 6365 Water Ingestion Rate (IRW) (L/d) 0.78 0.78 Water Exposure Time (ET,_) (hr/event) 0.54 0.54 Water Event Frequency (EV) (events/day) 1 1 Residential Adult Lifetime (LT) (years) 70 70 Body Weight(BW) (kg) 80 80 Exposure Duration (ED) (yr) 20 20 Exposure Frequency (EF) (d/yr) 350 350 Exposure Time (ET) (hr) 24 24 Skin Surface Area - Soil Exposure (SAg) (cm) 6032 6032 Soil Adherence Factor (AF) (mg/cm2) 0.07 0.07 Soil Ingestion Rate (IRS) (mg/day) 100 100 Skin Surface Area - Water Exposure (SA,) (Cm 2) 19652 19652 Water Ingestion Rate (IRW) (L/d) 2.5 2.5 Water Exposure Time (ET,_) (hr/event) 0.71 0.71 Water Event Frequency (EV) (events/day) 1 1 Non -Residential Worker Lifetime (LT) (years) 70 70 Body Weight(BW) (kg) 80 80 Exposure Duration (ED) (yr) 25 25 Exposure Frequency (EF) (d/yr) 250 250 Exposure Time (ET) (hr) 8 8 Skin Surface Area - Soil Exposure (SAs) (cm) 3527 3527 Soil Adherence Factor (AF) (mg/cm2) 0.12 0.12 Soil Ingestion Rate (IR) (mg/day) 100 100 Skin Surface Area - Water Exposure (SA,) (Cm 2) 19652 19652 Water Ingestion Rate (IRW) (L/d) 0.83 0.83 Water Exposure Time (ET,_) (hr/event) 0.67 0.67 Water Event Frequency (EV) (events/day) 1 1 Construction Worker Lifetime (LT) (years) 70 70 Body Weight(BW) (kg) 80 80 Working Weeks (EW) (wk/yr) 50 50 Exposure Duration (ED) (yr) 1 1 Exposure Frequency (EF) (d/yr) 250 250 Exposure Time (ET) (hr) 8 8 Skin Surface Area - Soil Exposure (SAs) (Cm 2) 3527 3527 Soil Adherence Factor (AF) (mg/cm2) 0.3 0.3 Soil Ingestion Rate (IR) (mg/day) 330 330 North Carolina DEQ Risk Calculator Exposure Factors and Target Risks Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Exposure Parameter North Default Value Site Specific Value Justification User Defined Child Recreator Trespasser Lifetime (LT) (years) 70 NA Averaging Time (AT) (days/yr) 365 NA 365 Body Weight (BW) (kg) 15 NA 15 Exposure Duration 0-2 (ED) (yr) 2 NA 2 Exposure Duration 2-6 (ED) (yr) 4 NA 4 Exposure Frequency (EF) (d/yr) 195 NA 195 Exposure Time (ET) (hr) 2 NA 2 Skin Surface Area -Soil Exposure (SAg) (cm) 2373 NA 2373 Soil Adherence Factor (AF) (mg/cm2) 0.2 NA 0.2 Soil Ingestion Rate (IRS) (mg/day) 200 NA 200 Skin Surface Area -Water Exposure (SA,) (Cm Z) 6365 NA 6365 Water Ingestion Rate (IRW) (L/hr) 0.12 NA 0.12 Water Exposure Time (ET,_) (hr/event) 2 NA 2 Water Event Frequency (EV) (events/day) 1 NA 1 User Defined Adult Recreator Trespasser Lifetime (LT) (years) 70 70 70 Body Weight(BW) (kg) 80 45 80 Exposure Duration 6-16 (ED) (yr) 10 10 10 Exposure Duration 16-26 (ED) (yr) 10 0 ] 0 Exposure Frequency (EF) (d/yr) 195 90 195 Exposure Time (ET) (hr) 2 2 2 Skin Surface Area -Soil Exposure (SAs) (Cm Z) 6032 6032 6032 Soil Adherence Factor (AF) (mg/cm) 0.07 0.2 0.07 Soil Ingestion Rate (IRS) (mg/day) 100 200 100 Skin Surface Area -Water Exposure (SA,) (cm) 19652 19652 19652 Water Ingestion Rate (IRW) (LAu) 0.071 0.071 0.071 Water Exposure Time (ET_j (hr/event) 2 2 2 Water Event Frequency (EV) (events/day) 1 1 1 Carolina DEQ Risk Calculator Contaminant Migration Parameters Version Date: February 2015 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Provide justification for the contaminant migration parameters used. Site Specific Parameter Default Value Justification Value Distance to Protection of Groundwater Point of 0 250 Approximate distance from UST #1 to on -site water supply well. Exposure (POE,) (feet) Distance to Protection of Surface Water Point of 0 500 Approximate distance from UST #1 to nearest surface water body to Exposure (POE„,) (feet) northeast of site Depth to Base of Affected Soils (d,) (cm) 1244 1244 Length of Affected Soil Site -specific Parallel to Assumed GW Flow value required 1,500 Assume —50 feet Direction (L) (cm) Aerial extent of soil contamination (AJ (acres) (Note minimum acceptable value is 0.5 and 0.5 0.5 maximum acceptable value is 500.) Fraction of Vegetative Cover 0.5 0.5 (V) (unitless) 0.15 (soil to outdoor air 0.15 pathway) Water Filled Sol Porosity (0„,) (unitless) 0.3 (soil to groundwater 0.3 pathway) 0.28 (soil to outdoor air 0.28 pathway) Air Filled Soil Porosity (0a) (unitless) 0.13 (soil to groundwater 0.13 pathway) Total Soil Porosity (n) 0.43 0.43 (unitless) Dry Soil Bulk Density (py) (g/cm3) 1.5 1.5 North Carolina DEQ Risk Calculator Contaminant Migration Parameters Version Date: February 2015 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Provide justification for the contaminant migration parameters used. Parameter Default Value Site Specific Justification Value Net Infiltration Rate (I) 66 66 (c-/Yr) 0.006 (soil to outdoor air 0.006 pathway) Fraction Organic Carbon (foc) limitless) 0.002 (soil leaching to 0.002 groundwater pathway) Aquifer Hydraulic Site -specific 8.64 Based on an average K or 1 x 10-4 cm/sec for Piedmont saprolite Conductivity (I) (cm/d) value required Hydraulic Gradient (i) Site -specific 0.010 Typical hydraulic gradient in the Piedmont, and close to that measured at (unitless) value required the site (-0.012) Average Groundwater Temperature (Ts,„) (°C) 25 25 Aquifer Thickness (d,) (cm) Site -specific 1,500 Assume —50 feet value required Groundwater Source Site -specific 300 Assume —10 feet Thickness (S,) (cm) value required Groundwater Source Width Site -specific 1,500 Assume —50 feet (Sw) (cm) value required Plume Thickness at GW/SW Site -specific 300 Assume —10 ft Discharge (Ssw) (cm) value required Plume Width at GW/SW Site -specific 300 Assume —10 feet Discharge (W,,) (cm) value required Surface Water Flowrate at GW/SW Dischara g (Qsw) Site -specific 1,200,000,000 Conversion of 0.5 cubic feet per second (assumed) to cm3/day s (cm /d) value required North Carolina DEQ Risk Calculator don Date: February 2018 s: November 2017 EPA RSL Table ID: 22051-19-092 Exposure Point Concentration (mg/kg) Justification for Exposure Point Concentration CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 0.0293 Highest Concentration 67-64-1 Acetone mg/kg 191 Highest Concentration 7440-39-3 Barium m 0.358 Highest Concentration 71-43-2 Benzene m 10.2 Highest Concentration 104-51-8 But lbenzene, n- m 4.71 Highest Concentration 135-98-8 Butylbenzene, sec- m 13.9 Highest Concentration 7440-47-3 Chromium, Total m 5.37 Highest Concentration 98-82-8 Cumene — /kg 0.338 Highest Concentration 96-12-8 Dibromo-3-chloro ro ane, 1,2- mg/kg 0.218 Higbest Concentration 106-93-4 Dibromoethane, 1,2- mg/kg 33.2 Higbest Concentration 100-41-4 Ethylbenzene — /kg 25.7 Highest Concentration 7439-92-1 —Lead and Compounds mg/kg 0.128 Highest Concentration 7439-97-6 Mercury (elemental) mg/kg 4.75 Highest Concentration 78-93-3 Methyl Ethyl Ketone (2-Butanone) mg/kg 0.16 Highest Concentration 86-73-7 —Fluorene m 16.3 Highest Concentration 91-20-3 —Naphthalene mg/kg 16.8 Highest Concentration 103-65-1 Propylbenzene mg/kg 0.18 Higbest Concentration 100-42-5 Styrene mg/kg 50.7 Higbest Concentration 108-88-3 Toluene mg/kg 135 Highest Concentration 95-63-6 Trimeth lbenzene, 1,2,4- mg/kg 41 Higbest Concentration 108-67-8 Trimeth lbenzene, 1,3,5- mg/kg 212 Highest Concentration 1330-20-7 X lens m Note: No surficial soil samples were collected. Therefore highest concentrations detected in subsurface soils was used to simulate worse than expected conditions. North Carolina DED Risk Calculator Exposure Point Concentrations Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Subsurface Soil Exposure Point Concentration Table Exposure Point Concentration (mg/kg) Justification For Exposure Point Concentration CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/I I) Rationale for Selection or Deletion 0.0293 Highest Concentration 67-64-1 Acetone mg/kg 191 Highest Concentration 7440-39-3 Barium mg/kg 0.358 Highest Concentration 7143-2 Benzene mg/kg 10.2 Highest Concentration 104-51-8 Butylbenzene, n- mg/kg 4.71 Highest Concentration 135-98-8 Bu ]benzene, sec- mg/kg 13.9 Highest Concentration 7440-47-3 Chromium, Total mg/kg 5.37 Highest Concentration 98-82-8 Cumene mg/kg 0.338 Highest Concentration 96-12-8 Dibromo-3-chloropropane, 1,2- mg/kg 0.218 Hi est Concentration 106-934 Dibromoethane, 1,2- mg/kg 33.2 Highest Concentration 100414 Ethylbenzene mg/kg 25.7 Hi est Concentration 7439-92-1 Lead and Compounds mg/kg 0.128 Highest Concentration 7439-97-6 _Mercury (elemental) mg/kg 4.75 Hi est Concentration 78-93-3 Methyl Ethyl Ketone (2-Butanone mg/kg 0.16 Highest Concentration 86-73-7 —Fluorene mg/kg 16.3 Highest Concentration 91-20-3 —Naphthalene mg/kg 16.8 Highest Concentration 103-65-1 Propyl benzene mg/kg 0.18 Highest Concentration 10042-5 Styrene mg/kg 50.7 Highest Concentration 108-88-3 Toluene mg/kg 135 Highest Concentration 95-63-6 Trimeth ]benzene, 1,2,4- mg/kg 41 Highest Concentration 108-67-8 Trimethylbenzene, 1,3,5- mg/kg 252 Highest Concentration 1330-20-7 X lenes mg/kg North Carolina DEQ Risk Calculator Exposure Point Concentrations Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Groundwater Exposure Point Concentration Table Minimum Maximum Location of Range of Concentration Screening Potential Potential Exposure Point Concentration (ug/L) Justification for Exposure Point Concentration CAS Number Chemical Concentration (Qualifier) Concentration (Qualifier) Units Maximum Concentration Detection Frequency Detection Limits Used for Screening Background Value Toxicity Value (Screening Level) ARAR/TBC Value ARAR/TBC Source COPC Flag (y/N) Rationale for Selection or Deletion 501 Highest Recent Concentration 71-43-2 Benzene ug/L 89.8 Highest Recent Concentration 98-82-8 Cumene ug/L 11.9 Highest Recent Concentration 105-67-9 Dimeth 1 henol, 2,4- ug/L 2180 Highest Recent Concentration 100-41-4 Ethylbenzene ug/L 581 Highest Recent Concentration 91-20-3 —Naphthalene ug/L 232 Highest Recent Concentration 103-65-1 Propyl benzene ug/L 6220 Highest Recent Concentration 108-88-3 Toluene ug/L 429 Highest Recent Concentration 526-73-8 Trimethylbenzene, 1,2,3- ug/L 1600 Highest Recent Concentration 95-63-6 Trimethylbenzene, 1,2,4- u /L 434 Highest Recent Concentration 108-67-8 Trimethylbenzene, 1,3,5- ug/L 11000 Highest Recent Concentration 1330-20-7 X lenes ug/L North Carolina DEC Risk Calculator Exposure Point Concentrations Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Soil Gas Exposure Point Concentration Table Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. Exposure Point Minimum Maximum Location of Range of Concentration Screening Potential Potential Rationale for Concentration Justification for Exposure Point CAS Number Chemical Concentration Concentration Units Maximum Detection Detection Used for Background Toxicity Value ARAR/TBC ARAR/'I'BC COPC Flag Selection or s (ug/m) Concentration (Qualifier) (Qualifier) Concentration Frequency Limits Screening Value (Screening Value Source (Y/I� Deletion bevel) (n/c) 1700 Highest Concentration 67-64-1 Acetone ug/m3 31 Highest Concentration 71-43-2 Benzene ug/ms 60 Highest Concentration 75-15-0 Carbon Disulfide 119/m3 1.2 Highest Concentration 56-23-5 Carbon Tetrachloride ug/ms 2.2 Highest Concentration 67-66-3 Chloroform 119/m3 2.8 Highest Concentration 141-78-6 Ethyl Acetate ug/ms 6 Highest Concentration 100-41-4 Eth lbenzene 119/m3 110 Highest Concentration 142-82-5 Heptane, N- ug/ms 190 Highest Concentration 110-54-3 Hexane, N- 119/m3 13 Highest Concentration 67-63-0 Isopropanol ug/ms 28 Highest Concentration 78-93-3 Methyl Ethyl Ketone (2-Butanone) 119/m3 3.2 Highest Concentration 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) ug/ms 2.9 Highest Concentration 91-20-3 —Naphthalene 119/m3 1800 Highest Concentration 115-07-1 Propylene ug/ms 0.75 Highest Concentration 100-42-5 Styrene 119/m3 6.3 Highest Concentration 127-18-4 Tertachloroethylene ug/ms 27 Highest Concentration 108-88-3 Toluene 119/m3 1.2 Highest Concentration 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- ug/ms 0.55 Highest Concentration 71-55-6 Trichloroethane, 1,1,1- 119/m3 2 Highest Concentration 75-69-4 Trichlorofluoromethane ug/ms 7.3 Highest Concentration 95-63-6 Trimeth lbenzene, 1,2,4- 119/m3 1.9 Highest Concentration 108-67-8 Trimethylbenzene, 1,3,5- ug/ms 11 Highest Concentration 106-42-3 X lene, P- 119/m3 11 Highest Concentration 108-38-3 Xylene, m- ug/ms 5.1 Highest Concentration 95-47-6 X lene, o- 119/m3 North Carolina DED Risk CalGllalor Summary of Risk Assessment Output Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: PRIMARY CALCULATORS Receptor Pathway CarcinogenicRisk Hazard Index Risk exceeded? Resident Soil Combined Pathways 1.2E-04 1.3E+00 YES Groundwater Combined Pathways* 6.IE-03 2.2E+02 YES Non -Residential Worker Soil Combined Pathways 1.1E-05 2.5E-01 NO Groundwater Combined Pathways* 1.5E-03 5.3E+01 YES Construction Worker Soil Combined Pathways 5.5E-06 4.6E-01 NO User Defined Soil Combined Pathways NC NC NC Surface Water Combined Pathways* NC NC NC RL VAPOR INTRUSION CALCULATORS qr Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Resident Groundwater to Indoor Air 1.1E-03 4.6E+01 YES Soil Gas to Indoor Air 4.4E-06 1.2E-01 NO Indoor Air NC NC NC Non -Residential Worker Groundwater to Indoor Air 2.4E-04 1.1E+01 YES Soil Gas to Indoor Air 3.4E-07 9.2E-03 NO Indoor Air NC NC NC CONTAMINANT MIGRATION CALCULATORS Pathway Source Target POE Concentrations Exceeded? Protection of Groundwater Use Source Soil Exceedence of 2L at POE? YES Source Groundwater Exceedence of 2L at POE? YES Protection of Surface Water Source Soil Exceedence of 213 at POE? NO Source Groundwater I Exceedence of 213 at POE? NO Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 213 Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. North Carolina DEQ Risk Calculator N— Carolina DEO Rlak Calculabr Noh� Carolina OEp Rlsk Calculabr DEQ Risk Calculator- Primar -tion-Residential Worker Groundwater Combined Path.vays Version Date: February 2018 Basis: November 2017 EPA RSL Table t 1 Site lD: 22051-19-092 E o re Unit ID: * - Note that inhalation on this calculator refers to inhalation associated with tapwater use, not inhalation associated with vapor inmission from subsurface groundwater sources. ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is nor possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA Action Level of15 µg/L. Cumulative: 1.5E-03 5.3E+01 CABit Chemical Name: Ingestion Concentration (ug/L) Dermal Concentration (ugiL) Inhalation Concentration (ugiL)* Ingestion Carcinogenic Risk Dermal Carcinogenic Risk Inhalation Carcinogenic Risk Calculated Carcinogenic Risk Ingestion Hard Quotient Demral Hazard Quotient inhalation Hazard Quotient Calculated Non- Carcinogenic Hazard Quotient 7143-2 Benzene 501 501 501 7. 3.0E-05 1.6F1114 2.6E-04 8.9E-01 3.8E-01 1.9E+00 3.2E+00 98-82-8 Cumene 89.8 89.8 89.8 6.4E-03 2.2E-02 2.6E-02 5.4E-02 105-67-9 Dimethylphenol, 2,4- 11.9 11.9 11.9 4.2E-03 1.8E-03 6.0E-03 100-41-4 Eth benzene 2180 2180 2180 6.1)'r05 1.0E-04 2.2E-04 3.9E-04 1.5E-01 2.6E-01 2.5E-01 6.7E-01 91-20-3 -Naphthalene 581 581 581 8.1E-04 8.1E-04 2.1E-01 3.8E-01 2.2E+01 2.3E+01 103-65-1 Pro benzene 232 232 232 1.6E-02 5.8E-02 2.6E-02 1.0E-01 108-88-3 Toluene 6220 6220 6220 5.5E-01 5.4E-01 1.4E-01 1.2E+00 526-73-8 Trimeth benzene, 1,2,3- 429 429 429 3.0E-01 1.0E+00 6.2E-01 2.2E+00 95-63-6 Trimethylbenzene, 1,2,4- 1600 1600 1600 1.1E+00 3.7E+00 3.0E+00 7.9E+00 108-67-8 Trimeth benzene, 1,3,5- 434 434 434 3.1E-01 7.2E-01 6.3E-01 1.9E+00 1330-20-7 Xylene 11000 11000 11000 3.9E-01 6.7E-01 1.3E+01 1.4E+O1 Air Date: February 2018 ID: 22051-19-092 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. CAS # Chemical Name: Groundwater Concentration (uP�) Calculated Indoor Air Concentration (ug/m') Target Indoor Air Conc. for Carcinogens ® TCR = 1E-06 Target Indoor Air Conc. for Non-Cazcinogers ® TEIQ = 0.2 Calculated Carcinogenic Rrsk Calculated Non - Carcinogenic Hazazd Quotient 71-43-2 Benzene 501 113.6774511 3.6E-01 6.3E+00 3.2E-04 3.6E+00 104-51-8 Bu Ibenzene,n- 135-98-8 But Ibenzene,sec- 98-82-8 Cumene 89.8 42.21995492 8.3E+01 1.0E-01 100-41-4 Eth (benzene 2180 702.305748 1.1E+00 2.1E+02 6.3E-04 6.7E-01 91-20-3 -Naphthalene 581 10.4513766 8.3E-02 6.3E-01 1.3E-04 3.3E+00 103-65-1 Pro (benzene 232 99.5911736 2.1E+02 9.5E-02 100-42-5 S ene 2.1E+02 108-88-3 Toluene 6220 1688.503592 1.0E+03 3.2E-01 95-63-6 Trimeth (benzene, 1,2,4- 1600 402.94352 1.3E+01 6.4E+00 108-67-8 Trimeth (benzene, 1,3,5- 434 155.6083564 1.3E+01 2.5E+00 1330-20-7 X Imes 11000 2981.6028 2.1E+01 2.9E+01 Cumulative: I 1.1E-03 4.6E+O1 DEQ Risk Calculator -Prima -Construction Worker Soil Combined Pa[hwa s Output Version Date: February 2018 Basis: November 2017 EPA RSL Table Site lD: 22051-19-092 Es os re Unit ID: * -Note that inhalation on this calculator refers to outdoor inhalation ofvolatiles andparticulates, not indoor inhalation associated with vapor intrusion. **-Note that the EPA has no consensus on reference dose or cancer slopefactor valussforlead, thereforeitis notpossible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of800 mg/kg forcommerciallindustrial soil. Cumulative: 5.5E-06 4.6E-01 CAS # Chemical Name: Ingestion Concentration (mg/kg) Dermal Concentration (mg/kg) Inhalation Concentration (mg/kg)* Ingestion Carcinogenic Risk Derrnal Carcinogenic Risk Inhalation Carcinogenic Risk Calculated Carcinogenic Risk Ingestion Hazard Quotient Dermal Hazard Quotient Inhalation Hazard Quotient Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 0.0293 0.0293 0.0293 1.2E-07 7440-39-3 Barium 191 191 191 2.8E-03 8.6E-03 1.1E-02 71-43-2 Benzene 0.358 0.358 0.358 7.9E-10 1.1E-08 1.2E-08 1.1E-04 1.3E-03 1.4E-03 104-51-8 Bu benzene, n- 10.2 10.2 10.2 3.0E-04 3.0E-04 135-98-8 Butylbenzeue, sec- 4.71 4.71 4.71 1.4E-04 1.4E-04 7440-47-3 Chromium, Total 13.9 13.9 13.9 2.8E-07 3.6E-06 3.9E-06 8.2E-03 1.0E-02 1.9E-02 98-82-8 Cumeue 5.37 5.37 5.37 4.0E-05 1.0E-02 1.0E-02 96-12-8 Dibromo-3-chloro ro tine, 1,2- 0.338 0.338 0.338 1.1E-08 9.3E-07 9.4E-07 5.0E-04 5.6E-03 6.1E-03 106-93-4 Dibromoethane, 1,2- 0.218 0.218 0.218 1.8E-08 2.2E-07 2.4E-07 7.1E-05 1.3E-02 1.3E-02 100-41-4 Eth benzene 33.2 33.2 33.2 1.5E-08 2.1E-07 2.3E-07 2.0E-03 6.9E-04 2.6E-03 7439-92-1 -Lead and Compounds 25.7 25.7 25.7 6L** 4SL** 6L** 7439-97-6 -Mercury elemental 0.128 0.128 0.128 1.3E-02 1.3E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone) 4.75 4.75 4.75 7.0E-06 4.1E-04 4.2E-04 86-73-7 -Fluorene 0.16 0.16 0.16 1.2E-06 4.9E-07 1.7E-06 91-20-3 -Naphthalene 16.3 16.3 16.3 1.8E-07 1.8E-07 8.0E-05 3.3E-05 13E-01 1.3E-01 103-65-1 Pro lbenzene 16.8 16.8 16.8 5.0E-04 3.0E-03 100-42-5 Styrene 0.18 0.18 0.18 2.7E-06 9.5E-06 108-88-3 Toluene 50.7 50.7 50.7 1.9E-04 2.7E-03 95-63-6 TrimeNylbeuzeue, 1,2,4- 135 135 135 9.9E-03 M1.2E-01 1.0E-01 108-67-8 7}inreW benzene, 1,3,5- 41 41 41 3.0E-03 3.6E-02 1330-20-7 Xylene 252 252 252 1.9E-03 1.2E-01 Date: February 2018 November 2017 EPA RSL Table Site ID: 22051-19-092 Exposure Unit ID: Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m3 CAS # Chemical Name: Soil Gas Concentration s (ug/m) Calculated Indoor Air Concentration Co (ug/ms) Target Indoor Air Conc. for Carcinogens @ TCR = 1 E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 1700 51 6.5E+03 1.6E-03 71-43-2 Benzene 31 0.93 3.6E-01 6.3E+00 2.6E-06 3.0E-02 75-15-0 Carbon Disulfide 60 1.8 1.5E+02 2.5E-03 56-23-5 Carbon Tetrachloride 1.2 0.036 4.7E-01 2.1E+01 7.7E-08 3.5E-04 67-66-3 Chloroform 2.2 0.066 1.2E-01 2.0E+01 5.4E-07 6.5E-04 141-78-6 Ethyl Acetate 2.8 0.084 1.5E+01 1.2E-03 100-41-4 Eth lbenzene 6 0.18 1.1E+00 2.1E+02 1.6E-07 1.7E-04 142-82-5 Heptane, N- 110 3.3 8.3E+01 7.9E-03 110-54-3 Hexane, N- 190 5.7 1.5E+02 7.8E-03 67-63-0 Iso ro anol 0.39 4.2E+01 1.9E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.84 1.0E+03 1.6E-04 108-10-1 Methyl Isobu1Ketone(4-meth 1-2- entanone) ;3.2 0.096 6.3E+02 3.1E-05 91-20-3 -Na hthalene 0.087 8.3E-02 6.3E-01 1.1E-06 2.8E-02 115-07-1 Pro lene 54 6.3E+02 1.7E-02 100-42-5 Styrene 0.75 0.0225 2.1E+02 2.2E-05 127-18-4 Tetrachloroethylene 6.3 0.189 1.1E+01 8.3E+00 1.8E-08 4.5E-03 108-88-3 Toluene 27 0.81 1.0E+03 1.6E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 1.2 0.036 1.0E+03 6.9E-06 71-55-6 Trichloroethane, 1,1,1- 0.55 0.0165 1.0E+03 3.2E-06 75-69-4 Trichlorofluoromethane 2 0.06 95-63-6 Trimeth lbenzene, 1,2,4- 7.3 0.219 1.3E+01 3.5E-03 108-67-8 Trimeth lbenzene, 1,3,5- 1.9 0.057 1.3E+01 9.1E-04 106-42-3 X lene,P- 11 0.33 2.1E+01 3.2E-03 108-38-3 X lene, m- 11 0.33 2.1E+01 3.2E-03 95-47-6 X lene, o- 5.1 0.153 2.1E+01 1.5E-03 Cumulative: I 4.4E-06 I 1.2E-0 l North Carolina DEQ Risk Calculator North Carolina DEQ Risk Calculator DEQ Risk Calculator - Contaminant Migration - Soil Source to Groundwater POE - Forward Mode 1 Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Distance to Groundwater POE 250 feet Notes: This is a 1-D model and should be used as a screening tool. NM= Not modeled because contaminant migration parameters have not been entered. CAS # Chemical Name: Source Soil Concentration (mg/kg) 2L StandardGroundwater (µgo) Concentration at POE (µg/L) Concentration Exceeds 2L Standard? 67-64-1 Acetone 0.0293 6000 6.5E-01 NO 7440-39-3 Barium 191 700 2.1E+01 NO 71-43-2 Benzene 0.358 1 3.2E+00 YES 104-51-8 Butylbenzene, n- 10.2 70 1.4E+01 NO 135-98-8 Butylbenzene, sec- 4.71 70 7.4E+00 NO 7440-47-3 Chromium, Total 13.9 10 3.3E+00 NO 98-82-8 Cumene 5.37 70 1.5E+01 NO 96-12-8 Dibromo-3-chloropropane, 1,2- 0.338 0.04 3.6E+00 YES 106-934 Dibromoethane, 1,2- 0.218 0.02 3.5E+00 YES 100414 Ethylbenzene 33.2 600 1.4E+02 NO 7439-92-1 Lead and Compounds 25.7 15 1.3E-01 NO 7439-97-6 -Mercury(elemental) 0.128 1 1.1E-02 NO 78-93-3 Methyl Ethyl Ketone (2-Butanone) 4.75 4000 1.0E+02 NO 86-73-7 -Fluorene 0.16 300 3.9E-02 NO 91-20-3 -Naphthalene 16.3 6 2.3E+01 YES 103-65-1 Propyl benzene 16.8 70 4.1E+01 NO 10042-5 Styrene 0.18 70 7.5E-01 NO 108-88-3 Toluene 50.7 600 3.4E+02 NO 95-63-6 Trimethylbenzene, 1,2,4- 135 400 4.3E+02 YES 108-67-8 Trimethylbenzene, 1,3,5- 41 400 1.3E+02 NO 1330-20-7 Xylenes 252 500 1.2E+03 YES North Carolina DEQ Risk Calculator DEQ Risk Calculator - Contaminant Migration - Groundwater Source to Groundwater POE - Forward Mode 1 Version Date: February 2018 Basis: November 2017 EPA RSL Table A ID: 22051-19-092 Distance to Groundwater POE 250 feet Notes: This is a 1-D model and should be used as a screening tool. NM= Not modeled because contaminant migration parameters have not been entered. CAS # Chemical Name: Source Groundwater Concentration (ug/L) 2L Standard (µme) Groundwater Concentration at POE (µg/L) Concentration Exceeds 2L Standard? 71-43-2 Benzene 501 1 4.6E+01 YES 104-51-8 Butylbenzene,n- 70 135-98-8 Butylbenzene,see- 70 98-82-8 Cumene 89.8 70 8.2E+00 NO 100414 Ethylbenzene 2180 600 2.0E+02 NO 91-20-3 —Naphthalene 581 6 5.3E+01 YES 103-65-1 Propylbenzene 232 70 2.1E+01 NO 10042-5 Styrene 70 108-88-3 Toluene 6220 600 5.7E+02 NO 95-63-6 Trimethylbenzene, 1,2,4- 1600 400 1.5E+02 NO 108-67-8 Trimethylbenzene, 1,3,5- 434 400 4.0E+01 NO 1330-20-7 Xylenes 11000 500 1.0E+03 YES North Carolina DEQ Risk Calculator DEQ Risk Calculator - Contaminant Migration - Soil Source to Surface Water POE - Forward Mode 1 Version Date: February 2018 Basis: November 2017 EPA RSL Table J016 ID: 22051-19-092 Distance to Surface Water POE 500 feet Notes: This is a 1-D model and should be used as a screening tool. NM= Not modeled because contaminant migration parameters have not been entered. CAS # Chemical Name: Source Soil Concentration (mg/kg) 213 Standard (µgo) Surface Water Concentration at POE (µg/L) Concentration Exceeds 2 B Standard? 67-64-1 Acetone 0.0293 1.1E-06 NA 7440-39-3 Barium 191 3.6E-05 NA 71-43-2 Benzene 0.358 5.4E-06 NA 104-51-8 Butylbenzene, n- 10.2 2.4E-05 NA 135-98-8 Butylbenzene, sec- 4.71 1.2E-05 NA 7440-47-3 Chromium, Total 13.9 5.6E-06 NA 98-82-8 Cumene 5.37 2.5E-05 NA 96-12-8 Dibromo-3-chloropropane, 1,2- 0.338 6.0E-06 NA 106-934 Dibromoethane, 1,2- 0.218 5.9E-06 NA 100414 Ethylbenzene 33.2 2.3E-04 NA 7439-92-1 Lead and Compounds 25.7 2.2E-07 NA 7439-97-6 Mercury (elemental) 0.128 1.9E-08 NA 78-93-3 Methyl Ethyl Ketone (2-Butanone) 4.75 1.7E-04 NA 86-73-7 -Fluorene 0.16 6.6E-08 NA 91-20-3 -Naphthalene 16.3 3.8E-05 NA 103-65-1 Propyl benzene 16.8 6.9E-05 NA 10042-5 Styrene 0.18 1.3E-06 NA 108-88-3 Toluene 50.7 5.6E-04 NA 95-63-6 Trimethylbenzene, 1,2,4- 135 7.1E-04 NA 108-67-8 1 Trimethylbenzene, 1,3,5- 41 2.2E-04 NA 1330-20-7 1 Xylenes 252 2.0E-03 NA NA = Not applicable because no 213 Standard entered. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Contaminant Migration - Groundwater Source to Surface Water POE - Forward Mode Version Date: February 2018 Basis: November 2017 EPA RSL Table Site ID: 22051-19-092 Distance to Surface Water POE 500 feet Notes: This is a 1-D model and should be used as a screening tool. NM= Not modeled because contaminant migration parameters have not been entered. CAS # Chemical Name: Source Groundwater Concentration (ug/L) 2B Standard (µme) Surface Water Concentration at POE (µg/L) Concentration Exceeds 2B Standard? 7143-2 Benzene 501 7.7E-05 NA 104-51-8 Butylbenzene,n- 135-98-8 Butylbenzene,sec- 98-82-8 Cumene 89.8 1.4E-05 NA 100-41-4 Ethylbenzene 2180 3.3E-04 NA 91-20-3 —Naphthalene 581 8.9E-05 NA 103-65-1 Propyl benzene 232 3.6E-05 NA 100-42-5 Styrene 108-88-3 Toluene 6220 9.6E-04 NA 95-63-6 Trimethylbenzene, 1,2,4- 1600 2.5E-04 NA 108-67-8 Trimethylbenzene, 1,3,5- 434 6.7E-05 NA 1330-20-7 Xylenes 11000 1.7E-03 NA NA = Not applicable because no 2B Standard entered. North Carolina DEQ Risk Calculator