MO-9583_47014_CA_LSA_20200812_Phase I LSA

SUMMIT
FNC.INF.F174NC:. I ABORATORV. TE$TINC
August 12, 2020
Ms. Trudy Beverly, L.G.
NCDEQ
Underground Storage Tank Section
610 East Center Ave
Mooresville, NC 28115
SUMMIT Engineering, Laboratory & Testing, P.C.
3575 Centre Circle
Fort Mill, South Carolina 29715
www.SUMMIT-companies.com
Phone: [phone]
Fax: [phone]
Subject: Limited Site Assessment
Curry Vail LLC Properties
2547 & 2553 Vail Avenue
Charlotte, Mecklenburg County, North Carolina
SUMMIT Project No. 1820.E0004
Dear Ms. Beverly:
SUMMIT ENGINEERING, LABRATORY & TESTING, P.C. (SUMMIT) is pleased to submit the following
Limited Site Assessment report on behalf of Curry Vail LLC for 2547 and 2553 Vail Avenue in
Charlotte, North Carolina.
This report includes a description of the methodology of our investigation and a summary of our
findings and conclusions. If you have any questions regarding our assessment of the subject
property or our conclusions, please do not hesitate to call us at [phone].
Sincerely,
SUMMIT���I�r�
SEAL. Tr -
Patrick W. Lowery, LG Michael D. Zavislak, NRC -EAC, Ck PC 033ROP. i
Senior Environmental Manager Environmental Department Managers,:. •A
NC LG No: 2421 »'Z4 G'1Nt 4!t
+ ID 1\i�
SUMMIT NC Engineering Firm License No. C-2530 # �
ENGINEERING* LABORATORY • TESTING
3575 Centre Circle Drive I Fort Mill, Souwh Carolina 29715 i (704) 504 - 1717 1 (704) 504 - 1125 (Fax)
W1 W.EAUMMIT-COMPANIES. OM

SUMMIT
ENGINEERING• LABORATORY. TESTING
LIMITED SITE ASSESSMENT
CURRY VAIL LLC PROPERTIES
INCIDENT #s 47013 & 47014
CHARLOTTE
MECKLENBURG COUNTY
NORTH CAROLINA
SUMMIT PROJECT NO. 1820.E0004
Prepared For:
North Carolina Department of Environmental Quality
Underground Storage Tank Section
Corrective Action Branch
610 East Center Ave
Mooresville, NC 28115
Prepared By:
SUMMIT ENGINEERING, LABRATORY & TESTING, P.C.
3575 Centre Circle
Fort Mill, South Carolina 29715
704-504-1717
August 12, 2020
EN INEERIIN ,& LABORATORY • TESTIN
3575 Centre Circle Drive I Fort Mill, Sowh Carolina 29715 1 (704) 5D4 - 1717 1 (704) 504 - 1125 (Fax)
WW . UMMIT- MPANIES. M

Limited Phase II ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY..............................................................................................................4
2.0 SITE HISTORY AND CHARACTERIZATION...................................................................................6
2.1 UST OWNERSHIP: .................................................................................................................. 6
2.2 UST INFORMATION: .............................................................................................................. 6
2.3 AST SYSTEMS, SPILLS AND NON -UST PETROLEUM RELEASE INFORMATION: ..................... 6
2.4 RELEASE INFORMATION: ....................................................................................................... 6
2.5 SITE CHARACTERISTICS: ........................................................................................................ 7
2.6 ASSESSMENT, INITIAL ABATEMENT, CORRECTIVE ACTION SUMMARY: ............................. 10
3.0 RISK CLASSIFICATION...............................................................................................................13
4.0
RECEPTOR INFORMATION.......................................................................................................15
4.1
WATER SUPPLY WELLS........................................................................................................15
4.2
PUBLIC WATER SUPPLIES....................................................................................................15
4.3
SURFACE WATER.................................................................................................................15
4.4
WELLHEAD PROTECTION AREAS.........................................................................................15
4.5
DEEP AQUIFERS IN COASTAL PLAIN....................................................................................15
4.6
SUBSURFACE STRUCTURES.................................................................................................15
5.0
LAND USE................................................................................................................................16
5.1
PROPERTY OWNERS & OCCUPANTS...................................................................................16
5.2 SENSITIVE LAND USE FEATURES.........................................................................................16
6.0 SITE GEOLOGY AND HYDROGEOLOGY....................................................................................17
7.0 SAMPLING RESULTS.................................................................................................................18
7.1 PHASE I INVESTIGATION......................................................................................................18
7.2 PHASE II INVESTIGATION.....................................................................................................18
8.0 CONCLUSIONS AND RECOMMENDATIONS.............................................................................19
9.0 FREE PRODUCT INVESTIGATION.............................................................................................20
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Limited Phase II ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 12, 2020
APPENDICES
Appendix I: FIGURES
•
1—Topographic Map
•
2 — Site Boundary Map
•
3 — Sampling Location Plan
•
4 — Sensitive Receptor Map
•
5 — Water Supply Well Key
•
6 — Adjoining Properties Map Key
•
7 — Land Use Map
Appendix II:
B TABLES
•
B-1 Site History— USYT/AST Information
•
B-2 Site History — Owner/Operator
•
B-3 Soil Sample Analytical Results
•
B-4 Groundwater Sample Results
•
B-6 Adjoining Parcel Ownership
•
B-7 Well Construction Information
•
B-8 Not Used
•
B-9 Groundwater Elevations
•
B-10 Land Use
Appendix III:
DEQ CORRESPONDANCE
Appendix IV:
DEED & PROPERTY INFORMATION
Appendix V:
ANALYTICAL RESULTS
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Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 1Z 2020
Limited Site Assessment Report
A. Site Information
1. Site Identification
Date of Report: August 12, 2020
Facility I.D.: Unknown Incident Number: Unknown
-Site Name: Curry Vail LLC Properties
Site Street Address: 2547 & 2553 Vail Avenue
City/Town: Charlotte Zip Code: 28207 County: Mecklenburg
Description of Geographical Data Point (e.g., dispenser): Heating Oil UST Basin
Location Method (GPS, topographical map, other): GIS Address Matching
Latitude (decimal degrees): 35.203538 Longitude (decimal degrees):-80.813895
2. Information about Contacts Associated with the Release
—UST/AST Owner: Curry Vail LLC
Address: Unknown Tel: 1001 Berkeley Avenue
-UST/AST Operator: Owner never operated USTs
Address: Unknown Tel: Unknown
-Other Person Associated with Release: N/A
Address: Tel:
Property Owner: Curry Vail LLC
Address: 1001 Berkeley Ave., Charlotte, NC 28207 Tel: [phone]
Property Occupant: Residential Tenants
Address: Tel:
Consultant/Contractor: SUMMIT Engineering, Laboratory & Testing, PC
Address: 3575 Centre Circle Drive, Ft. Mill, SC 29715 Tel: [phone]
Analytical Laboratory: PACE Analytical, Inc. State Certification No.329
Address: 106 Vantage Point Drive, W. Columbia, SC 29172 Tel: [phone]
3. Information about Release
-Date Discovered: March 30, 2020
Estimated Quantity of Release: Unknown
Cause of Release: Leaking Heating Oil USTs (2-tanks)
Source of Release: Heating Oil USTs
Sizes and Contents of Tank or Other Containment from which the Release Occurred: USTs are in
ground but are assumed to be 500-gallon steel tanks
4. Certification (The title page must display the seal and signature of the certifying P.E. or L.G. and the
name and certification number of the company or corporation [See 15A NCAC 2L .0103(e).])
I, Michael Zavislak, a Professional Engineer for SUMMIT ELT, PC, di try r i6fprmation contained in this
report is correct and accurate to the best of my knowledge. �� • • . �� =�,
4 SEAL
61 IN
SUMMIT ELT, PC is licensed to practice engineering in North CarolinQrwlel ber of the
company or corporation is C-2530
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Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
1.0 EXECUTIVE SUMMARY
SUMMIT was retained to complete due diligence services of the Curry Vail LLC Properties, in
Charlotte, North Carolina. The subject properties were utilized for residential purposes with two
(2) brick duplex buildings reportedly constructed in 1954. The current owner, Mr. Harold Curry
purchased the properties in 1973. The due diligence assessment, identified the presence of a
heating oil UST associated with each building (2 USTs). Mr. Curry indicated that he was aware of
the heating oil USTs, however the USTs were not in operation, and remained out of service during
his ownership.
On March 12, 2020, SUMMIT personnel completed a hand auger boring adjacent to each UST. The
borings were completed to 8 ft below ground surface (bgs). The soil borings conducted at the end
of each UST exhibited soil staining, petroleum odors and positive detections on field screening
equipment. A 24-hour Release Notification (UST-61) was submitted to DEQ on March 30, 2020.
On July 13, 2020, SUMMIT conducted a limited assessment of USTs to determine the vertical and
lateral extent of soil impacts related to these USTs. A GeoProbe contractor, Midsouth
Environmental, was utilized to complete the soil borings. A small low clearance GeoProbe machine
was utilized due to clearance and UST access issues. Soil samples were collected from beneath
each UST. UST#1, located at 2547 Vail Avenue, displayed slight impacts to the eastern end of the
UST. Soil sample SB-5 was collected from a depth of 8 ft bgs, beneath the eastern end of the UST.
The soil sample analysis reported no detections for VOC, SVOC, EPH/VPH. UST#2, located at 2553
Vail Avenue, displayed moderate to heavy impacts at the eastern end of the UST. The soil boring
SB-4 was extended to a depth of 16 ft bgs where refusal was encountered. Refusal was believed to
occurred on partially weathered rock. Soils collected from depth indicated petroleum impacts.
Soil Sample SB-4 analysis confirmed petroleum impacts with Naphthalene and VPH exceeding the
established regulatory Soil to Groundwater MSCC. The residential MSCC was not exceeded.
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Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
On July 29, 2020, SUMMIT conducted this field work of this Limited Site Assessment (LSA) for Tank
#2, incident 47014. Clean soils were encountered under Tank #1 and therefore no LSA was
conducted for incident 47013. In accordance with LSA guidance, one (1) temporary monitoring
well was installed at the site. Due to low clearance and UST basin access issues with the property,
the LSA well was installed downgradient of the UST in as close as possible to the source area. The
temporary well was installed to a depth of 25 ft bgs. Groundwater analytical results reported the
presence of Chloroform, Caprolactam, Diethyl ph ha late, Dimethyl phthalate, Di-n-butyl phthalate
and Bis(2-Ethylhexl)phthate at concentrations below the 2L groundwater standards. Soil sample
SS-0, collected from the surface interval reported the detections of SVOCs and VPH at
concentrations below Soil to Groundwater and Residential MSCCs. Soil samples from the 5, 10 and
15 ft bgs intervals did not report any detections.
It should be noted that the perspective purchaser of the property is planning to complete tank
removals, Initial Abatement Actions with clean closure. Due to site logistics, tank removals cannot
occur until the site buildings are demolished.
Based on the results of this assessment, SUMMIT concludes the release related to Tank # 1 at 2547
Vail Avenue is limited to an area along the eastern end of the UST. Soil borings and confirmatory
soil samples indicate that the release has not impacted the soils beneath the UST at 8 ft bgs.
SUMMIT concludes the release from Tank #2, impacted the soils down to the partially weathered
rock interface at 16 ft bgs, however groundwater collected from the LSA well did not identify
impacts above 2L Standards. Therefore, with limited receptors, county wide restrictions on water
supply wells and reported analysis, SUMMIT recommends issuing the releases a Low Risk
classification.
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Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
2.0 SITE HISTORY AND CHARACTERIZATION
2.1 UST Ownership:
Details regarding ownership of the USTs is provided in Table B-2.
2.2 UST Information:
Details regarding the USTs is provided in Table B-1. The USTs are inground at the time of the LSA.
Based on size assessed from the surface, it appears that the USTs are approximately 500 gallon
sized USTs. USTs were out of service and were reported to be out of service prior to 1973.
2.3 AST Systems, Spills and Non -UST Petroleum Release Information:
Information regarding ASTs and Non -UST Petroleum releases is unknown at the time of this report.
2.4 Release Information:
SUMMIT completed hand auger borings adjacent to the USTs on March 12, 2020. Soils collected
adjacent to the eastern ends of the tanks exhibited petroleum odors and staining. A 24-Hr Release
Report (UST-61) was submitted to NCDEQ on March 30, 2020 for review and consideration of a
release. The source of the release was USTs that were formerly operated on -site. July 13, 2020 a
limited assessment was conducted utilizing a geoprobe. Soils were collected from 4 borings
surrounding each side of the USTs. Soils collected from the eastern ends exhibited petroleum
odors and staining. The soil impacts at UST#1 appeared to subside at 8 ft bgs. A confirmation soil
sample was collected as SB-5 at 8 ft bgs. The soil impacts at UST#2 extended to 16 ft bgs where
boring refusal was encountered. SB-4 was collected from the 16 ft bgs interval to determine if
compounds were above regulatory standards. Naphthalene and VPH exceeded the Soil to
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Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 12, 2020
Groundwater MCSS in SB-4. Based on the exceedances, this LSA was performed on July 29, 2020.
Collected groundwater from TMW-1 did not report any exceedances of the 2L groundwater
standards.
2.5 Site Characteristics:
Site Characteristics
The approximate 0.5-acre subject property is comprised of Mecklenburg Tax Parcel Nos. 12712105
and 12712104 and is located at 2547 and 2553 Vail Avenue, Charlotte, Mecklenburg County, North
Carolina. The subject property is developed with two brick multi -story residential duplex
structures. According to the Mecklenburg County POLARIS GIS website, the owner of the subject
tax parcel is listed as Curry Vail LLC, 1001 Berkeley Avenue, Charlotte, NC 28203. Refer to the Site
Location Map shown in Figure 1 for the location of the subject property.
Site Vicinity Characteristics
The vicinity is residential. A vicinity map is provided as Figure 3.
Direction
Address/Occupied By/Use
Topographic Position Relative
to Property
North
2542 Deacon Ave/Common Area for Elizabeth
Glen Townhome Development
Downgradient
East
Downgradient
South
2601 Vail Ave/Multi-Family Apartments
Crossgradient
West
2554-2556 Vail Ave/ Single Family Residential
Upgradient
Water Supply
Water supply is provided to the site by municipal services. No potable or irrigation wells were
observed on the subject property or adjoining properties. Adjoining properties appear to be
provided water by municipal services.
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Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
Topography
The United States Geological Survey (USGS) "Charlotte East" 7.5 minute topographic quadrangle
map was reviewed. According to the contour lines on the topographic map, the elevation of the
subject site ranges from approximately 650 feet to approximately 640 feet above Mean Sea Level
(MSL). The contour lines indicate the general direction of downward slope is to the east towards
unnamed tributaries of Briar Creek that flows south. Refer to Figure 1 in Appendix II of this report.
Vegetation
The site is developed with two (2) residential duplexes. Hardwood trees and shrub vegetation
overhang the site building and driveways. The backyard was grassed with large hardwood trees
were noted along the northeastern boundary of the subject property.
Surface Water
A unnamed tributary of Briar Creek bounds the site to the east/northeast. Water was flowing at
the time of this LSA.
Wells
No water supply wells were observed on the subject property.
Buildings
The site contains two (2) brick residential duplex buildings. 2547 Vail Avenue was reported to be a
1,850 SF, 2-story brick duplex building constructed on a basement foundation. 2553 Vail Avenue
was reported to be a 1,850 SF, 2-story brick duplex building constructed on a basement foundation.
The structures were constructed in the 1950s.
Surface Cover
With the exception of the site structures, no impervious surface coverings were noted. Grass
yards, trees and shrubs cover the undeveloped portions of the property. A gravel parking aera is
noted off of Vail Avenue.
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Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
Soil Type
The Mecklenburg County Soil Survey indicates that soils at the site are classified as Cecil sandy clay
loam.
Depth to and Nature of Bedrock
The property is located in Mecklenburg County, North Carolina, which is located in the south-
central Piedmont Physiographic Province. The Piedmont Province generally consists of well-
rounded hills and ridges which are dissected by a well -developed system of draws and streams.
The Piedmont Province is predominantly underlain by metamorphic rock (formed by heat, pressure
and/or chemical action) and igneous rock (formed directly from molten material) which were
initially formed during the Precambrian and Paleozoic eras. The volcanic and sedimentary rocks
deposited in the Piedmont Province during the Precambrian era were the host from the
metamorphism and were changed to gneiss and schist. The more recent Paleozoic era had periods
of igneous emplacement, with at least episodes of regional metamorphism resulting in the
majority of the rock types seen today.
The topography and relief of the Piedmont Province has developed from differential weathering of
the igneous and metamorphic rock. Ridges and hills have been developed on the more easily
weathered and erodible rock. Because of the continued chemical and physical weathering, the
rocks in the Piedmont Province are now generally covered with a mantle of soil that has weathered
in place from the parent bedrock. These soils vary in thickness and are referred to as residuum or
residual soils. The residuum is typically finer grained and has higher clay content near the surface
because of the advanced weathering. Similarly, the soils typically become coarser grained with
increasing depth because of decreased weathering. As the weathering decreases, the residual soils
generally retain the overall appearance, texture, gradation and foliations of the parent rock.
Soil boring refusal was encountered a various depths during assessment of soil impacts. Based on
the assessment, Bedrock was presumed to be encountered in boring SB-4 at a depth of 16 ft bgs.
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Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
The LSA well was installed at a downgradient location from the UST source area. Rock was not
encountered in the LSA well in the upper 25 ft bgs.
Depth to Groundwater
Following temporary well installation for this LSA, the well was gauged for the presence of
groundwater. TMW-1 was gauged directly following installation and following a 30-minute
equilibrium time. During installation, the Field Geologist indicated that the water table is
encountered between 20 and 25 feet bgs. Water table elevations were observed to rise following
equilibrium time, indicating a semi -confided groundwater table condition. The following Depth to
Water readings were recorded prior to sampling:
Well ID
DTW @ Install
DTW @ Sampling
TMW-1
20.2'
18.5'
Depth to Water (DTW) is recorded as feet below the ground surface (bgs).
2.6 Assessment, Initial Abatement, Corrective Action Summary:
SUMMIT was retained to complete due diligence services of the Curry Vail LLC Properties, in
Charlotte, North Carolina. The subject properties were utilized for residential purposes with two
(2) brick duplex building reportedly constructed in 1954. The current owner, Mr. Harold Curry
purchased the properties in 1973. The due diligence assessment, identified the presence of a
heating oil UST associated with each building (2 USTs). Mr. Curry indicated that he was aware of
the heating oil USTs, however the USTs were not in operation, and remained out of service during
his ownership.
On March 12, 2020, SUMMIT personnel completed a hand auger boring adjacent to each UST. The
borings were completed to 8 ft below ground surface (bgs). The soil borings conducted at the end
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Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
of each UST exhibited soil staining, petroleum odors and positive detections on field screening
equipment. A 24-hour Release Notification (UST-61) was submitted to DEQ on March 30, 2020.
On July 13, 2020, SUMMIT conducted a limited assessment of USTs to determine the vertical and
lateral extent of soil impacts related to these USTs. A GeoProbe contractor, Midsouth
Environmental, was utilized to complete the soil borings. A small low clearance GeoProbe machine
was utilized due to clearance and UST access issues. Soil samples were collected from beneath
each UST. UST#1, located at 2547 Vail Avenue, displayed slight impacts to the eastern end of the
UST. Soil sample SB-5 was collected from a depth of 8 ft bgs, beneath the eastern end of the UST.
The soil sample analysis reported no detections for VOC, SVOC, EPH/VPH. UST#2, located at 2553
Vail Avenue, displayed moderate to heavy impacts at the eastern end of the UST. The soil boring
SB-4 was extended to a depth of 16 ft bgs where refusal was encountered. Refusal was believed to
occurred on partially weathered rock. Soils collected from depth indicated petroleum impacts.
Soil Sample SB-4 analysis confirmed petroleum impacts with Naphthalene and VPH exceeding the
established regulatory Soil to Groundwater MSCC. The residential MSCC was not exceeded.
On July 29, 2020, SUMMIT conducted this field work of this Limited Site Assessment (LSA) for Tank
#2, incident 47014. Clean soils were encountered under Tank #1 and therefore no LSA was
conducted for incident 47013. In accordance with LSA guidance, one (1) temporary monitoring
well was installed at the site. Due to low clearance and UST basin access issues with the property,
the LSA well was installed downgradient of the UST in as close as possible to the source area. The
temporary well was installed to a depth of 25 ft bgs. Groundwater analytical results reported the
presence of Chloroform, Caprolactam, Diethyl ph ha late, Dimethyl phthalate, Di-n-butyl phthalate
and Bis(2-Ethylhexl)phthate at concentrations below the 2L groundwater standards. Soil sample
SS-0, collected from the surface interval reported the detections of SVOCs and VPH at
concentrations below Soil to Groundwater and Residential MSCCs. Soil samples from the 5, 10 and
15 ft bgs intervals did not report any detections.
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Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 12, 2020
No Initial Abatement Actions have occurred at this time. It should be noted that the perspective
purchaser of the property is planning to complete tank removals, Initial Abatement Actions with
clean closure. Due to site logistics, tank removals cannot occur until the site buildings are
demolished.
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Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 12, 2020
3.0 RISK CLASSIFICATION
Part I — Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non -drinking purposes?
NO
2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release?
NO
3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water,
filling swimming pools) located within 250 feet of the source area of the release?
NO
4. Does groundwater within 500 feet of the source area of the release have the potential for future use (there
is no other source of water supply other than the groundwater)?
NO
5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined
space or pose any other serious threat to public health, public safety or the environment?
NO
6. Are there any other factors that would cause the release to pose an imminent danger to public health,
public safety, or the environment?
NO
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release?
YES
8. Is the source area of the release located within a approved or planned wellhead protection area as defined in
42 USC 300h-7(e)?
NO
Is the release located in the Coastal Plain physiographic region as designated on a map entitled "Geology of
North Carolina" published by the Department in 1985?
NO
10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels
(See Table 2.) established by the Department?
NO
Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or temporary)?
YES-4 residential rental apartments.
2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church,
nursing home, or other place of public assembly?
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Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 12, 2020
7 o]
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial
(e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage,
etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped?
NO
4. Do children visit the property?
NO
Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or
both)?
YES
5. Do pavement, buildings, or other structures cap the contaminated soil?
NO
6. What is the zoning status of the property?
Zoning: R22-MF (CD) — Residential Multifamily — 22 Units per Acre Conditional Zoning
7. Is the use of the property likely to change in the next 20 years?
NO — Property will be used for residential purposes.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property
containing source area of the release):
1. What is the distance from the source area of the release to the nearest primary or secondary residence
(permanent or temporary)?
2545 Vail Ave — 50 ft North — Duplex Residence - Crossgradient
2548/2552 Vail Ave —110 ft West — Single Family Homes - Upgradient
2. What is the distance from the source area of the release to the nearest school, daycare center, hospital,
playground, park, recreation area, church, nursing home or other place of public assembly?
> 1500 feet currently.
3. What is the zoning status of properties in the surrounding area?
Zoning: R22-MF(CD) — Residential Multifamily
4. Briefly characterize the use and activities of the land in the surrounding area.
Residential Single Family and Multi -Family
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Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 12, 2020
4.0 RECEPTOR INFORMATION
4.1 Water Supply Wells
The area surrounding the property was walked and observed from public roads. No Water Supply
wells were observed within 1500 feet of the property. All observed properties appear to be
connected to municipal water supply.
4.2 Public Water Supplies
The Town of Charlotte receives water from the City of Charlotte, NC. Water supply is generated
from Lake Norman and the Catawba River. A water main is located along Main Street, the sites
northern boundary.
4.3 Surface Water
No surface water was observed within 500 feet of the subject property. See Table B-5 and receptor
map, Figure 4
4.4 Wellhead Protection Areas
The area of the UST release is not located within a wellhead protection area.
4.5 Deep Aquifers in Coastal Plain
The subject site is not located in the Coastal Plain.
4.6 Subsurface Structures
The subject site structures are constructed with crawl space foundations. Based on the lack of
free product observed at the property, the risk of an explosion hazard is considered low.
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels —Phase I UST\LSA\1820.E0004 Vail Ave - LSA.doc

Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 12, 2020
5.0 LAND USE
5.1 Property Owners & Occupants
Please refer to Table B-6 and Figure 6.
5.2 Sensitive Land Use Features
Sensitive receptions were identified within 1,500 feet of the property and are listed in Table B-10.
The approximate locations of the sensitive receptors are shown on Figure 4.
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels —Phase I UST\LSA\1820.E0004 Vail Ave - LSA.doc

Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 12, 2020
6.0 SITE GEOLOGY AND HYDROGEOLOGY
Borings SB-1 through SB-8, competed adjacent to the USTs (4 borings per UST) typically
encountered six (6) inches of surface material followed by tan/brown/white fine to medium
grained sandy silts to termination depths of 8 to 16 feet bgs. The LSA well typically encountered
brown fine sandy Clay and clayey fine grained sands to termination depths of 25 feet bgs. During
well installation, the Field Geologist indicated that the water table was encountered between 20
and 25 feet bgs. Water table elevations were observed to rise following equilibrium time,
indicating a semi -confided groundwater table condition. The following Depth to Water readings
were recorded prior to sampling:
Well ID
DTW @ Install
DTW @ Sampling
TMW-1
20.2'
18.5'
Depth to Water (DTW) is recorded as feet below the ground surface (bgs). A southwest
groundwater flow direction was concluded based on depth to groundwater readings and surface
topography.
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels —Phase I UST\LSA\1820.E0004 Vail Ave - LSA.doc

Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
7.0 SAMPLING RESULTS
7.1 Phase I Investigation
SUMMIT conducted a limited soil assessment of the two (2) USTs located on the Curry Vail LLC
property. Four (4) soil borings were advanced besides each UST to estimate the lateral and vertical
extent of petroleum impacts previously identified by hand auger borings. The intent of the
assessment was to identify the clean margins of soil to help estimate costs associated with Initial
Abatement Actions during tank closure. The assessment of UST#1 established clean margins with
soil impacts concentrated to the eastern end of the UST. A soil sample collected from 8 ft bgs,
below impacted soils did not report detections above Soil to Groundwater MCSS and Residential
MCSS. The assessment of UST#2 identified impacted soils extending from the UST basin to the
assumed top of rock interface at 16 ft bgs. A soil sample collected from the 16 ft bgs interval
reported Naphthalene and VPH above Soil to Groundwater MCSS and below Residential MCSS.
Due to limitations to access and height restrictions at the UST basin, SUMMIT installed a
temporary monitoring well downgradient of the source area as close as possible to the source are
of UST#2. Soil samples were collected at the 0, 5, 10 and 15 ft intervals in accordance with LSA
Guidance. Soil sample SS-0 (0-2' bgs) identified low concentrations of PAHs and VPH below Soil to
Groundwater MCSS and Residential MCSS. No other soil detection was reported in the LSA well
TMW-1. Groundwater was encountered at 18 ft bgs. Analytical results reported low level SVOC
detections below NC 2L groundwater standards.
7.2 Phase II Investigation
Based on the results of this investigation, a Phase II Investigation was not conducted at this time.
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels —Phase I UST\LSA\1820.E0004 Vail Ave - LSA.doc

Limited Phase 11 ESA — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
8.0 CONCLUSIONS AND RECOMMENDATIONS
The subject property, Curry Vail LLC contains two (2) home heating oil USTs associated with duplex
buildings, located at 2547 Vaile Avenue (UST#1) and 2553 Vail Avenue (UST#2). Limited
assessment of UST #1 (incident 47013) confirmed that the petroleum impacts were limited to soil
impacts with confirmation soil samples collected from 8 ft bgs at the UST basin indicating no
detections. Limited assessment of UST#2 identified soil impacts extending to 16 ft bgs where
boring refusal was encountered on apparent rock materials. A soil sample from 16 ft bgs reported
exceedances of Naphthalene and VPH above Soil to Groundwater MCSSs.
As a result of soil boring refusal on rock material with soil sample exceedances, a LSA was
conducted for UST#2. A temporary monitoring well was installed downgradient of the source area
of UST #2 as access to the UST basin and height clearance issues would not allow installation at the
source area. Soil samples collected reported minimal SVOC (PAHs) and VPH detections at the 0-2
ft bgs soil sample. No other detections were reported in the 5, 10 or 15 ft bgs samples.
Groundwater analysis of sample GW-1 from TMW-1 did not identify any compounds above NC 2L
Groundwater standards.
SUMMIT concludes that the releases associated with the two (2) USTs located on the Curry Vail LLC
properties have not impacted the groundwater or nearby unnamed tributary of the Briar Creek.
Based on the lack of additional receptors, SUMMIT recommends the issuance of a Low Risk
Classification for the identified releases.
The prospective purchaser of the property intends to complete clean closure and Initial Abatement
Actions.
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels —Phase I UST\LSA\1820.E0004 Vail Ave - LSA.doc

Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 1Z 2020
9.0 FREE PRODUCT INVESTIGATION
No Free Product was observed at the subject property during the completion of this LSA.
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels —Phase I UST\LSA\1820.E0004 Vail Ave - LSA.doc

Limited Phase 11 ESA — Curry Vail LLC Properties
Charlotte, North Carolina
SUMMIT Project No. 1820.E0004
August 1Z 2020
APPENDIX
FIGURES
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels —Phase I UST\LSA\1820.E0004 Vail Ave - LSA.doc

J OYA 1.14-0cps a ■J M§I�IC27 [C
I
1
fF
.�Rosenaorit
ti
1
dlCAN
I
rti '
1 ,
dl
-5-
1 �
1+ Boundaries are appr<
Prepared For: N
VAIL AVENUE PARCEL
2547-2555 Vail Avenue
Charlotte, North Carolina 28204
Figure 1
Topographic Map
3/24/2020
Drawn By:
N.r
Not to Scale

17
� �
� �
\
\ �
. �
i Heating O|
\
US #1 O \
/ 47013
\
/ Heating Oil
2 US #
47014
0E00e21 E02 ,Nw: %
¥
� m
m
Sore Drawn SUMMIT
Prepared B mate Pe08/20
Site Boundary Map Checked B mate M£0 20
Curry Vail LLC Properties Curry Vail
2 4 a5 5 Vail Avenue c e
-SUMMIT Charlotte, NC A Shown
Figure 2

KEY
40 Soil Boring
® Temporary Monitoring Well
tN
Source: Drawn by SUMMIT
//AA&
SUMMIT
i
i
,' ♦ Un-named Tributary
' f6' C k
� o rear ree
B-5 2549 2551 Vail Ave
Incident # 470143 .'
#1
e
� d
TMW-1
�
�
SS-0, 5, 10, 15
' UST#2
S B-4
2553 & 2555 Vail Ave
Incident # 47014
Sampling Location Plan
Curry Vail LLC Properties
2549-2555 Vail Avenue
Charlotte, NC
Curry Vail LLC
Prepared By\Date: PL/08/20
Checked By\Date: MZ/08/20
Scale
Not to Scale
Figure 3

N
1
Source: Mecklenburg County Polaris
SUMMIT
Curry Vail LLC
source
� 9Sv'{�o
Scale
1,500-Foot Radius
Prepared By\Date: PL/08/20
Checked By\Date: MZ/08/20
Sensitive Receptor Map
Curry Vail Properties
2549-2555 Vail Avenue
Charlotte, NC
Not to Scale
Figure 4

1,500-Foot Radius
. i jows
PPark 11 pDeveloped
I Source: Mecklenburg County Well Information System 4.0
SUMMIT
Curry Vail LLC
Scale
A
14
Ct
Prepared ByXDate: PL/07/20
Checked By\Date: MZ/07/20
Water Supply Well Key
Curry Vail Properties
2549-2555 Vail Avenue
Charlotte, NC
Not to Scale
Figure 5

17
� �
� �
\
\ �
. �
�� \
\ 2 �
----- -__ Co-
7 \
6
\
5
4 \
�
0E00e21 E02 ,Nw: %
¥
� m
Sore Drawn SUMMIT
Prepared B mate Pe08/20
Adjoining Properties Map Key ChekdBmke M£0820
//Aa& Curry Vail LLC Properties Curry Vail
2 4 a5 5 Vail Avenue c e
-SUMMIT Charlotte, NC A Shown
Figure 6

Zoning - R22-MF
0{ f
0 0.0051.01 0.02 Miles
I
Source: Drawn by SUMMIT
//Aa&
SUMMIT
Zoning - R22-MF
Land Use Map
Curry Vail LLC Properties
2549-2555 Vail Avenue
Charlotte, NC
i
Zoning - 0-2(CD)
i'
i
Curry Vail LLC
Prepared By\Date: PL/08/20
Checked By\Date: MZ/08/20
Scale
As Shown
Figure 7

Limited Site Assessment — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
APPENDIX II
B TABLES
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels_ Phase I USTTSA\Appendix II - B Tables.rtf

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: 8/12/20 Incident Number and Name: 47014/47013 Curry Vail LLC
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
S stem?
1
Heating Oil
500
Single
Out of
Unknown
Unknown
Unknown
YES
Wall Steel
Service
2
Heating Oil
500
Single
Unknown
Unknown
Unknown
Out of
YES
Wall Steel
Service
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
cident
Nn
Material
Date of
Description of Release
umber
Released
Release
47013
Heating Oil
03/30/20
Due Diligence Assessment for future development identified soil impacts adjacent to UST.
Additional Assessment identified soil impacts at 16' bgs. LSA completed for risk class.
47014
Heating Oil
3/30/200
Due Diligence Assessment for future development identified soil impacts adjacent to UST.
Additional Assessment did not identify soil impact below tank basin.
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
* * * Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)
Change 2

Appendix B
Reporting Tables
Table B-2: Site History - UST/AST Owner/Operator and Other Responsible
Party Information
Revision Date: 8/12/20 Incident Number and Name: 47013/47014 Curry Vail
UST ID Number
Unknown
Facility ID Number
Non -Commercial
Name of Owner
Dates of Operation
mm/dd/ to mm/dd/
Curry Vail LLC
Unknown — DID NOT OPERATE USTs —
Purchased property in 1973
Street Address
1001 Berkeley Avenue
city
State
Zip
Telephone Number
Charlotte
NC
28203
Name of Operator
Dates of Operation
mm/dd/ to mm/dd/
Unknown
1953 until Unknown
Street Address
2547 & 2553 Vail Avenue
city
State
Zip
Telephone Number
Charlotte
NC
Incident Number
47013/47014
Name of Other Responsible Party
Dates of Release(s)
mm/dd/ to mm/dd/
Duplexes constructed in 1953. Current owner
purchased in 1973. They had knowledge of
USTs but never filled them.
Street Address
city
State
I Zip
Tele hone Number
Add additional records for all owners, operators and responsible parties as necessary.

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 8/12/20 Incident Number and Name: Curry Vail LLC 47013/47014 Facility ID#: NA
Analytical Method (e.g., VOC by EPA 8260)
4
8260
8260
8260
8260
8260
8260
8270
8270
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
N
ID
Collected
Area
Depth
Phase
r
y
(m/dd/yy)
(eg.
(ft BGS)
(Closure
NCd
°
a
Tank pit
20Day,
C"
o
0
1)
LSA,
0
o
�
s.
a�i
N
N
etc.
o
Top of
SB-4
07/13/20
Rock
16
LSA
.011
.006
.15
.240
.079
.05
.21
.31
ND
ND
Tank #2
SB-5
07/13/20
Tank #1
8
LSA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Basin
SS-0
7/29/20
LWell0-2
LSA
ND
ND
ND
ND
ND
ND
ND
ND
0.017
0.026
SS-5
7/29/20
LSA
A
5-7
LSA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SS-10
7/29/20
LSA
10-12
LSA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SS-15
7/29/20
LSA
15-17
LSA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Minimum Reporting Limit (mg/kg)
.007
.002
.002
.002
.002
.003
.019
.012
.003
.003
Soil to groundwater MSCC (mg/kg)
24
NA
4.9
1.7
NA
4.6
11
940
0.35
0.096
Residential MSCC (mg/kg)
1400
NA
1560
1564
NA
3129
469
4600
0.88
0.088
Industrial/Commercial MSCC (mg/kg)
360000
NA
4000
40880
NA
81760
12264
122000
8
0.78
ft. BGS = feet below ground surface Results must be reported in mg/kg. mg/kg =milligrams per kilogr
Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 8/12/20 Incident Number and Name: Curry Vail LLC 47013/47014 2 Facility ID#: NA
Analytical Method (e.g., VOC by EPA 8260)
4
8270
8270
8270
8270
8270
8270
8270
8270
8270
8270
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
;
M
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
N
1)
LSA,
N
N
N
Y
Y
etc.)U
Top of
SB-4
07/13/20
Rock
16
LSA
ND
ND
ND
.73
ND
0.037 J
0.45
ND
2.8
0.63
Tank #2
SB-5
07/13/20
Tank #1
8
LSA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Basin
SS-0
7/29/20
LWell0-2
LSA
J
ND
0.012 J
ND
ND
J
ND
ND
.03
.0111
.009
.009
SS-5
7/29/20
LSA
A
5-7
LSA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SS-10
7/29/20
LSA
10-12
LSA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SS-15
7/29/20
LSA
15-17
LSA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Minimum Reporting Limit (mg/kg)
.003
.003
.007
.12
.002
.009
.013
.005
.023
.022
Soil to groundwater MSCC (mg/kg)
1.2
6400
12
NA
39
290
47
3.4
3.6
0.16
Residential MSCC (mg/kg)
0.88
469
9
NA
88
620
620
0.88
63
313
Industrial/Commercial MSCC (mg/kg)
8
12264
78
NA
780
16400
16400
8
1635
8176
ft. BGS = feet below ground surface Results must be reported in mg/kg. mg/kg =milligrams per kilogram
Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 8/12/20 Incident Number and Name: Curry Vail LLC 47013/47014 Facility ID#: NA
Analytical Method (e.g., VOC by EPA 8260)
EPH
EPH
EPH
EPH
4
8270
8270
VPH
VPH
VPH
VPH
Contaminant of Concern 4
.2
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
Q
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
�,
0
U
o U
1
LSA,
Q
U
v
U r
etc.)
Top of
SB-4
07/13/20
Rock
16
LSA
13
0.22
6.0
230
52
322
Tank #2
SB-5
07/13/20
Tank #1
8
LSA
ND
ND
ND
ND
ND
ND
Basin
SS-0
7/29/20
LSA
A
0-2
LSA
ND
ND
ND
ND
ND
1.4 J
SS-5
7/29/20
LSA
5-7
LSA
ND
ND
ND
ND
ND
ND
SS-10
7/29/20
LSA
10-12
LSA
ND
ND
ND
ND
ND
ND
SS-15
7/29/20
LSA
15-17
LSA
ND
ND
ND
ND
ND
ND
Minimum Reporting Limit (mg/kg)
.017
.012
0.81
0.011
0.011
0.011
Soil to groundwater MSCC (mg/kg)
56
270
68
540
NA
31
Residential MSCC (mg/kg)
469
469
939
1500
31000
469
Industrial/Commercial MSCC (mg/kg)
12264
12264
24528
40000
810000
12264
ft. BGS = feet below ground surface Results must be reported in mg/kg. mg/kg =milligrams per kilogram
Change 2

Appendix B
Reporting Tables
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 8/12/20 Incident Number and Name: Curry Vail LLC 47013/47014 Facility ID#: NA
Analytical Method (e.g., VOC by SM600013) or
Field Measurement (FM)4
8260
8270
8270
8270
8270
8270
Contaminant of Concern/ Field Measurement->
Well or
SW ID
Date
Collected
(n /dd/yy)
Sample
ID
Incident
Phase
(Closure,
20Da
LSA, etc.)
°cc
°
U E
A
y
Q p.
_
t
y
A p.
� 4
y
W M p.
TMW-2
7/29/20
GW-1
LSA
0.97 J
39
1.7 J
0.28
0.45 J
2.5 J
Minimum Reporting Limit (ug/1)
0.40
3.6
0.19
0.19
0.42
0.38
2L Standard (ug/1)
70
4000
6000
NA
700
3
GCL (ug/1)
7000
NA
NA
NA
NA
170
NC 2B Standard or EPA National Criteria
(ug/1)
NA
NA
NA
NA
NA
NA
Field measurement parameters include temperature, pH, dissolved oxygen, specific conductivity, Eh, and alkalinity
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
Results for contaminants must be reported in ug/1
µg/1=micrograms per liter GCL = gross contamination level
Change 2

Appendix B
Reporting Tables
Table B-5: Public and Private Water Supply Well and Other Receptor Information
Revision Date: 8/12/20 Incident Number and Name: 47013/47014 Facility ID#: NA
Public and Private Water Supply Wells
Well #
Well Owner/ User
(indicate which)
Address
Phone Number
Latitude/
Longitude *
(decimal
degrees)
Well
Use
Well
Depth
(ft
BGS)
**
Type
of
Well
Well
Casing
Depth (ft.
BGS )
Well
Screen
Interval
`x to y ft.
BGS)
Distance
from
source
area of
release
(ft.)
o
p �
NONE
Other Receptors
(Other public water supplies, reservoirs, supply lines, surface water bodies, wellhead protection areas, recharge areas for deep aquifers, subsurface structures)
Latitude/ Longitude of
Up or
Distance from
Receptor
Description
Location
*
any significant point(s)
Contact
Phone
Usage
down-
source area of
ID
(describe to left)
Number
gradient
release (ft.)
decimal de rees
1
Tributary to Briar
NE
35.203575/-80.813718
Surfac
down
98
Creek
e water
* The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells or replication of sampling points.
** Ft BGS = feet below ground surface
Change 2

Appendix B
Reporting Tables
Table B-6: Property Owners/ Occupants
Revision Date: 08/12/20 Incident No. and Name: Vail Curry LLC 47013/47014
Tax Parcel
Number/
Map ID
Owner/ Occupant Name
(Last, First MI)
Address
1
Fowler, James
401 Hawthorne Lane Unit 110 PMB 259, Charlotte,
NC 28204
2
Elizabeth Glen Townhome
Association CIO Cusick Community
Management
8008 Corporate Center Drive, Suite 100, Charlotte, NC
28226
3
WR Norwood Family, LLC
1229 Rama Road, Charlotte, NC 28211
4
Klopotowski, Jason
2556 Vail Ave, Charlotte, NC 28207
5
Isiguen, Dennis
2552 Vail Ave, Charlotte, NC 28207
6
Smith, Carly
2548 Vail Ave, Charlotte, NC 28207
7
Lee, Alexander
2544 Vail Ave, Charlotte, NC 28207
Change 2

Appendix B
Reporting Tables
Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 08/12/20 Incident Number and Name: Curry Vail LLC 47013/47014 Facility ID#:
Well
ID
Date
Installed
(m/dd/yy)
Date
Water
Level
Measured
m/dd/
Well
Casing
Diameter
(in.)
Well
Casing
Depth
(ft.
BGS
Screened
Interval
(x to y
ft. BGS)
Depth
of Well
(ft.
BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
ft.
Free
Product
Thickness
** (ft.)
Groundwater
Elevation*
(ft.)
Latitude/
Longitude
(decimal
degrees)***
TMW
-1
07/29/20
07/29/20
1"
15
15 to 25
20\5
0
18
0
35.2038/-
80.8138
ft BGS = feet below ground
* Reference Point for Elevation Measurements , Assumed Elevation: ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
*** The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.
10 Change 2

Appendix G
Contaminant Sources Other than USTs
Table B-8A: Free Product Recovery Information
Revision Date: Incident Number and Name: Facilitv ID#:
Date
(m/dd/yy)
Well
ID #
Product
yp (gas
Type
diesel'
etc.)
Free
Product
Recover*
Method
Product
Thickness
before
Recovery
inches
Product
Thickness
after
Recovery
inches
Amount of
Vaporized
Product
Amount of
Liquid
(Water
and
Product(gallons)
Amount
of Liquid
Product
Total
Amount of
Product
Recovered
(Present all calculations in an attachment)
* Bailing, Skimming, Aggressive Fluid Vapor Recovery, Mobile Multiphase Extraction, etc,
Table B-813: Cumulative Volume of Free Product Recovered from Site
Date of Recovery
Event (m/dd/yy)
Total Volume Recovered from Site During
Current Recovery Event (gallons)
Cumulative Total of Volume Recovered to Date
from All Recovery Events (gallons)
11 Change

Appendix G
Contaminant Sources Other than USTs
Table B-9: Current and Historical Groundwater Elevations and Free Product Thickness
Revision Date: 08/12/20 Incident Number and Name: Curry Vail 47013 & 47014 Facility ID#:
Well ID
#
Date
Screened Interval
(top of screen,
bottom of screen)
Depth to Water*
Uncorrected
(feet)
Free
Product
Thickness
feet
Depth to Water*
Corrected
for Free Product
Thickness feet
Top of
Casing
Elevation
MSL
Groundwater
Surface
Elevation
MSL
TMW-1
7/29/20
15 - 25
18.2
NA
18.2
640
621.8
*Depth to Water is measured from Top of Casing
12 Change 2

Limited Site Assessment — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
APPENDIX III
DEQ CORRESPONDANCE
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels _Phase I UST\LSA\Appendix III - DEQ Correspondance.rtf

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
Curry Vail LLC
Attn: Harold D. Curry
1001 Berkeley Avenue
Charlotte, North Carolina 28203
Dear Mr. Curry:
NORTH CAROLINA
Environmental Quality
April 20, 2020
Re: Notice of Regulatory Requirements
NCGS 14313-279.9 and 14313-279.11
Notice of Residual Petroleum
Curry Vail LLC
2547 Vail Avenue, Charlotte
Mecklenburg County
Incident Number: 47013
Risk Classification: Unknown
The 24 Hour Release and UST Leak Reporting Form received by the Underground Storage
Tank (UST) Section, Division of Waste Management, Mooresville Regional Office on March 30,
2020 has been reviewed. The 24-Hour Release and UST Leak Reporting Form documents visual
staining and petroleum odors in soil adjacent to the home heating oil UST System from the above
referenced facility. The site has an unknown risk classification.
North Carolina General Statute (NCGS) 143B-279.9 and 143B-279.11 require a Notice of
Residual Petroleum (Notice) to be filed with the Register of Deeds in Mecklenburg County, where
the release is located, when a release from an underground storage tank has not been remediated to
below "unrestricted use standards". The Notice is required either prior to conveyance of a
contaminated property or prior to receiving a Notice of No Further Action. "Unrestricted use
standards" for groundwater are the groundwater quality standards and interim standards contained in
Title 15A NCAC 2L .0202, and "unrestricted use standards" for soil are the residential maximum soil
contaminant concentrations (MSCCs) established in Title 15A NCAC 2L .0411.
The Notice must be prepared in accordance with the attached instructions and format. It must
contain a legal description of the property containing the source of contamination and legal
descriptions of any other properties which you own (or control) which are contaminated by the
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1699

release. The Notice must also include appropriate land use restrictions for these properties. In
addition, the Notice must identify all other properties (adjacent, adjoining, downgradient, etc.) on
which contamination is known to exist at the time the Notice is prepared. Provide proof of consent
from the current property owner if you are filing the Notice on their behalf.
The Notice must be sent to this regional office of the UST Section for approval and
notarization. The approved and notarized Notice must then be filed by you with the Register of
Deeds, and a certified copy of the filed Notice must be submitted to this office within 30 days of its
return to you.
Failure to comply with this letter is a violation of North Carolina law and may result in the
assessment of civil penalties and/or the use of other enforcement mechanisms available to the state.
If you have any questions regarding the actions or the rules mentioned in this letter, please contact
me by email at Trudy.Beverlykncdenr.aov or telephone at [phone].
Sincerely,
116A`P, ;6"�-
Trudy Beverly, L.G.
Hydrogeologist
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ
Attachment: Instructions and Form for Notice of Residual Petroleum with Alternate Land
Use Restriction
https://deg.nc. gov/about/divisions/waste-management/ust/forms
cc: Brett Morris & Shawna Caldwell, Mecklenburg County Environmental Health, Groundwater
& Wastewater Services (via email)
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1644

INSTRUCTIONS FOR PREPARING A 'NOTICE OF RESIDUAL PETROLEUM' REFERENCING
ALTERNATE LAND USE RESTRICTIONS (FOR EXISTING RESIDENCES ONLY) FOR FILING
The following is a list of instructions to assist in the preparation and filing of a Notice of Residual
Petroleum
1. The Notice shall be prepared in accordance with the format provided in these instructions and shall
include reference to the appropriate alternate land use restrictions. (REWORDING OF THE NOTICE IS
NOT RECOMMENDED AND WILL SUBSTANTIALLYDELAYAPPROVAL.)
2. The Notice shall include a description that would be sufficient as a description in an instrument of
conveyance of the (i) real property on which the source of contamination is located and (ii) any real
property on which contamination is located at the time the remedial action plan is approved and that was
owned or controlled by any owner or operator of the underground storage tank or other responsible party
at the time the discharge or release of petroleum is discovered or reported or at any time thereafter.
3. The Notice shall also identify the location (legal description) of any residual petroleum on other real
property on which contamination is known to exist at the time the Notice is prepared and that is a result of
the release.
4. The Notice shall reference any restrictions on the current or future use of the real property that are
imposed by the Secretary to protect public health, the environment, or users of the property.
5. (IF REQUIRED BYDEPARTMENT OF ENVIRONMENTAL QUALITY.) If the contamination is
located on more than one parcel or tract of land, the Department may require that the owner, operator, or
other person responsible for the discharge or release prepare a composite map or plat that shows all
parcels or tracts.
If the contamination is located on one parcel or tract of land, the owner, operator, or other person
responsible for the discharge or release may prepare a map or plat that delineates the contamination but is
not required to do so.
When the Department has approved a map or plat, it shall be recorded in the office of the register of
deeds and shall be incorporated into the Notice by reference.
Any map or plat shall be prepared and certified by a professional land surveyor, shall meet the
requirements of G.S. 47-30 and any requirements of the county Register of Deeds, and shall be submitted
to the Department for approval. The plat shall include: (ALL CONTENTS OF THE PLAT MUST BE
DRA WN IN INDELIBLE INK)
a. Property lines, north arrow, scale, bearings and distances as appearing on the deed;
b. With respect to permanently surveyed benchmarks, location and dimensions of areas of the
property where contamination is known to exist in
® groundwater at a concentration exceeding the standard or interim standard established in 15A
NCAC 2L .0202 and/or
soil at a concentration exceeding the residential maximum soil contaminant concentration
established in 15A NCAC 2L .0411.
c. The printed name(s) and title(s) and properly notarized signature(s) of individual(s) with authority
to legally bind the responsible party(ies) (i.e., responsible party(ies), an individual with power of
attorney for the responsible party(ies), officer of a corporation, etc.) (PRINTED TEXT,
SIGNATURES, AND NOTARY SEALS, AS WITH ALL MARKINGS ON THE PLAT, MUST
BE MADE IN INDELIBLE INK);
Revised February 7, 2019

d. The following language: "The areas of contamination depicted upon the map are approximations
derived from the best available information at the time of filing.";
e. The following language, for use by the Department, positioned in the upper left corner of the plat:
"Approved for the purposes of N.C.G.S. 14313-279.9 and 143B-279.11
(signature of Regional Supervisor)
, Regional Supervisor
(printed name of Regional Supervisor)
Regional Office
UST Section
Division of Waste Management
Department of Environment Quality
NORTH CAROLINA
COUNTY
I certify that the following person(s) personally appeared before me this day, each
acknowledging to me that he or she signed the foregoing document: (printedfull
name of Regional Supervisor)
Date:
(signature of Notary Public)
(Official Seal)
(printed or typed name of Notary Public)
Notary Public
My commission expires:
f. Surveyor's certification and seal (using a permanent ink stamp).
6. The signed and notarized Notice (with all indicated attachments) shall be sent to the appropriate UST
Section Regional Office.
7. After the Department approves, notarizes and returns the Notice, the responsible party shall, within
thirty (30) days of its return:
a. File approved Notice in the County Register of Deeds' office of the county or counties in which
the site is located; and
b. Send to the appropriate UST Section Regional Office, a certified copy of the Notice affixed with
the seal of the Register of Deeds and reflecting the book(s) and page number(s) where recorded
and a copy of the page(s) in the grantor index where the Notice is referenced.
Revised February 7, 2019
2

NOTICE OF RESIDUAL PETROLEUM
County, North Carolina
(site name)
The property that is the subject of this Notice (hereinafter referred to as the "Site")
contains residual petroleum and is an Underground Storage Tank (UST) incident under North
Carolina's Statutes and Regulations, which consist of N.C.G.S. 143-215.94 and regulations adopted
thereunder. This Notice is part of a remedial action for the Site that has been approved by the
Secretary (or his/her delegate) of the North Carolina Department of Environment Quality (or its
successor in function), as authorized by N.C.G.S. Section 14313-279.9 and 143B-279.11. The North
Carolina Department of Environment Quality shall hereinafter be referred to as "DEQ".
NOTICE
Petroleum product was released and/or discharged at the Site. Petroleum constituents remain
on the site, but are not a danger to public health and the environment, provided that the
restrictions described herein, and any other measures required by DEQ pursuant to N.C.G.S.
Sections 143B-279.9 and 14313-279.11, are strictly complied with. This "Notice of Residual
Petroleum" is composed of a description of the property, the location of the residual petroleum, and the
land use restrictions on the Site. The Notice has been approved and notarized by DEQ pursuant to
N.C.G.S. Sections 143B-279.9 and 143B-279.11 and has/shall be recorded at the
Register of Deeds' office Book , Page
(name of county)
Any map or plat required by DEQ has been/shall be recorded at the Register of
(name of county)
Deeds' office Book , Page , and has been/shall be incorporated into the Notice by this reference.
Source Property
of
is the owner in fee
(owner's name) (city & state of homeowner)
simple of all or a portion of the Site, which is located in the County of , State of North
Carolina, and is known and legally described as:
Revised February 7, 2019

(Insert Real Property Description Here for Source Property)
Additional Affected Property Also Subject to Restrictions
of is the owner in fee simple of a portion of
(owner's name) (city & state of owner)
the Site, which is located in the County of , State of North Carolina. Petroleum
contamination is located on this property at the time this Notice is approved. This property was also
owned or controlled by the underground storage tank owner or operator or another party responsible for
the petroleum discharge or release at the time the discharge or release was discovered or reported, or at
any time thereafter. This property is known and legally described as:
(Insert Real Property Description Here for Additional Properties Owned or Controlled by Any Owner or
Operator of the Underground Storage Tank or Other Responsible Party, if Applicable)
Additional Affected Property Not Subject to Restrictions
Additionally residual petroleum is also located on the following property. The following
property is not subject to land use restrictions pursuant to N.C.G.S. Section 143B-279.9(b). The
following property is known and legally described as:
(Insert Legal Description of Other Real Property Affected by Residual Petroleum Not Owned or
Controlled by Any Owner or Operator of the Underground Storage Tank or Other Responsible Party, if
Applicable)
For protection of public health and the environment, the following land use restrictions required
by N.C.G.S. Section 143B-279.9(b) shall apply to all of the above -described real property. These
restrictions shall continue in effect as long as residual petroleum remains on the site in excess of
unrestricted use standards and cannot be amended or cancelled unless and until the County
Register of Deed receives and records the written concurrence of the Secretary (or his/her delegate) of
Revised February 7, 2019
2

DEQ (or its successor in function).
[Restrictions apply to activities on, over, or under the land. Choose one or more of the following as
appropriate.]
Soil: Alternate]) Soil containing residual petroleum, above applicable regulatory
standard(s), remains on the site at/within/etc. (Description of specific location on
the site of remaining petroleum contaminated soil). No soil shall be excavated or
disturbed, within _ feet of (Description of specific location on the site of remaining
petroleum contaminated soil), except to remediate the soil in accordance with all
applicable state and federal statutes, regulations and guidelines.
Alternate 2) Soil containing residual petroleum above applicable regulatory
standard(s) remains on the site in the area identified in Figure 1, Attachment A
(Refer to extent of contamination as diagrammed in an existing report and attach
copy of that figure(s)). No soil shall be excavated or disturbed within 3 feet of the
area identified in Figure 1, Attachment A except to remediate the soil in accordance
with all applicable state and federal statutes, regulations and guidelines.
Groundwater: Groundwater from the site is prohibited from use as a water supply. Water supply wells
of any kind shall not be installed or operated on the site.
ENFORCEMENT
The above land use restriction(s) shall be enforced by any owner, operator, or other party
responsible for the Site. The above land use restriction(s) may also be enforced by DEQ through any of
the remedies provided by law or by means of a civil action, and may also be enforced by any unit of local
government having jurisdiction over any part of the Site. Any attempt to cancel this Notice without the
approval of DEQ (or its successor in function) shall be subject to enforcement by DEQ to the full extent
of the law. Failure by any party required or authorized to enforce any of the above restriction(s) shall in
no event be deemed a waiver of the right to do so thereafter as to the same violation or as to one occurring
prior or subsequent thereto.
IN WITNESS WHEREOF, has caused this Notice to be executed pursuant to
N.C.G.S. Sections 14313-279.9 and 14313-279.11, this day of , 20_
(name of responsible party if agent is signing)
(signature of responsible party, attorney or other agent if there is one)
(title of agent for responsible party if there is one)
Signatory's name typed or printed:
(Note to be deleted on final document: Preparer of document must assure that the correct
acknowledgement is used and complies with changes effective October 1, 2006)
Choice One: Instrument signed by one person
Revised February 7, 2019

NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
I certify that the following person(s) personally appeared before me this day, each acknowledging to me
that he or she signed the foregoing document:
Date:
(Official Seal)
expires:
Choice Two: Acknowledge by attorney in fact
NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
I, , a Notary Public for said County and State, do hereby certify that
, attorney in fact for , personally appeared before me this day, and being by
me duly sworn, says that he executed the foregoing and annexed instrument for and in behalf of the said
, and that his authority to execute and acknowledge said instrument is contained in an instrument duly
executed, acknowledged, and recorded in the office of in the County of
, State of , on the day of , 20and
that this instrument was executed under and by virtue of the authority given by said instrument granting
him power of attorney.
I do further certify that the said acknowledged the due execution of the
foregoing and annexed instrument for the purposes therein expressed for and in behalf of the said
WITNESS my hand and official seal, this the day of , 20
(Official Seal)
expires:
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
Choice Three: Conveying security interest in personal property of a corporation
NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
Revised February 7, 2019
4

a Notary Public for said County and State, do hereby certify that
personally came before me this day and acknowledged that he is
of and acknowledged, on behalf of , the grantor
the due execution of the foregoing instrument.
WITNESS my hand and official seal, this the day of 120
(Official Seal)
expires:
Approved for the purposes of N.C.G.S. 14313-279.11
(signature of Regional Supervisor)
, Regional Supervisor
(printed name of Regional Supervisor)
Regional Office
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
UST Section
Division of Waste Management
Department of Environment Quality
NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
I certify that the following person(s) personally appeared before me this day, each acknowledging to me
that he or she signed the foregoing document: (full printed name of Regional Supervisor)
Date:
(Official Seal)
expires:
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
Revised February 7, 2019

Beverly, Trudy
From: Beverly, Trudy
Sent: Monday, April 20, 2020 10:02 AM
To: Caldwell, Shawna; Morris, Brett L.
Subject: Curry Vail LLC - UST Incident #47013 — Notice of Regulatory Requirements
Attachments: MO-9582_47013_G_NORR_20200420_Notice of Regulatory Requirements.pdf
Please see the attached Notice of Regulatory Requirements for Curry Vail LLC located at 2547 Vail Avenue, Charlotte,
Mecklenburg County, North Carolina (Incident #47013).
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
L31 UU�,�UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenr. og_v
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https:Hdeq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hgps:Hdeq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deu.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://deq.nc.gov/about/divisions/waste-mana2ement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httas://files.ne.izov/nede(ifWaste%2OManagement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policy.ildf
htips:Hfiles.nc. gov/ncdeq/Waste°/`20Mana2ement/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.doex

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
Curry Vail LLC
Attn: Harold D. Curry
1001 Berkeley Avenue
Charlotte, North Carolina 28203
Dear Mr. Curry:
NORTH CAROLINA
Environmental Quality
April 20, 2020
Re: Notice of Regulatory Requirements
NCGS 14313-279.9 and 14313-279.11
Notice of Residual Petroleum
Curry Vail LLC 2
2553 Vail Avenue, Charlotte
Mecklenburg County
Incident Number: 47014
Risk Classification: Unknown
The 24 Hour Release and UST Leak Reporting Form received by the Underground Storage
Tank (UST) Section, Division of Waste Management, Mooresville Regional Office on March 30,
2020 has been reviewed. The 24-Hour Release and UST Leak Reporting Form documents visual
staining and petroleum odors in soil adjacent to the home heating oil UST System from the above
referenced facility. The site has an unknown risk classification.
North Carolina General Statute (NCGS) 143B-279.9 and 143B-279.11 require a Notice of
Residual Petroleum (Notice) to be filed with the Register of Deeds in Mecklenburg County, where
the release is located, when a release from an underground storage tank has not been remediated to
below "unrestricted use standards". The Notice is required either prior to conveyance of a
contaminated property or prior to receiving a Notice of No Further Action. "Unrestricted use
standards" for groundwater are the groundwater quality standards and interim standards contained in
Title 15A NCAC 2L .0202, and "unrestricted use standards" for soil are the residential maximum soil
contaminant concentrations (MSCCs) established in Title 15A NCAC 2L .0411.
The Notice must be prepared in accordance with the attached instructions and format. It must
contain a legal description of the property containing the source of contamination and legal
descriptions of any other properties which you own (or control) which are contaminated by the
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1699

release. The Notice must also include appropriate land use restrictions for these properties. In
addition, the Notice must identify all other properties (adjacent, adjoining, downgradient, etc.) on
which contamination is known to exist at the time the Notice is prepared. Provide proof of consent
from the current property owner if you are filing the Notice on their behalf.
The Notice must be sent to this regional office of the UST Section for approval and
notarization. The approved and notarized Notice must then be filed by you with the Register of
Deeds, and a certified copy of the filed Notice must be submitted to this office within 30 days of its
return to you.
Failure to comply with this letter is a violation of North Carolina law and may result in the
assessment of civil penalties and/or the use of other enforcement mechanisms available to the state.
If you have any questions regarding the actions or the rules mentioned in this letter, please contact
me by email at Trudy.Beverlykncdenr.aov or telephone at [phone].
Sincerely,
116A`P, ;6"�-
Trudy Beverly, L.G.
Hydrogeologist
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ
Attachment: Instructions and Form for Notice of Residual Petroleum with Alternate Land
Use Restriction
https://deg.nc. gov/about/divisions/waste-management/ust/forms
cc: Brett Morris & Shawna Caldwell, Mecklenburg County Environmental Health, Groundwater
& Wastewater Services (via email)
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1644

INSTRUCTIONS FOR PREPARING A 'NOTICE OF RESIDUAL PETROLEUM' REFERENCING
ALTERNATE LAND USE RESTRICTIONS (FOR EXISTING RESIDENCES ONLY) FOR FILING
The following is a list of instructions to assist in the preparation and filing of a Notice of Residual
Petroleum
1. The Notice shall be prepared in accordance with the format provided in these instructions and shall
include reference to the appropriate alternate land use restrictions. (REWORDING OF THE NOTICE IS
NOT RECOMMENDED AND WILL SUBSTANTIALLYDELAYAPPROVAL.)
2. The Notice shall include a description that would be sufficient as a description in an instrument of
conveyance of the (i) real property on which the source of contamination is located and (ii) any real
property on which contamination is located at the time the remedial action plan is approved and that was
owned or controlled by any owner or operator of the underground storage tank or other responsible party
at the time the discharge or release of petroleum is discovered or reported or at any time thereafter.
3. The Notice shall also identify the location (legal description) of any residual petroleum on other real
property on which contamination is known to exist at the time the Notice is prepared and that is a result of
the release.
4. The Notice shall reference any restrictions on the current or future use of the real property that are
imposed by the Secretary to protect public health, the environment, or users of the property.
5. (IF REQUIRED BYDEPARTMENT OF ENVIRONMENTAL QUALITY.) If the contamination is
located on more than one parcel or tract of land, the Department may require that the owner, operator, or
other person responsible for the discharge or release prepare a composite map or plat that shows all
parcels or tracts.
If the contamination is located on one parcel or tract of land, the owner, operator, or other person
responsible for the discharge or release may prepare a map or plat that delineates the contamination but is
not required to do so.
When the Department has approved a map or plat, it shall be recorded in the office of the register of
deeds and shall be incorporated into the Notice by reference.
Any map or plat shall be prepared and certified by a professional land surveyor, shall meet the
requirements of G.S. 47-30 and any requirements of the county Register of Deeds, and shall be submitted
to the Department for approval. The plat shall include: (ALL CONTENTS OF THE PLAT MUST BE
DRA WN IN INDELIBLE INK)
a. Property lines, north arrow, scale, bearings and distances as appearing on the deed;
b. With respect to permanently surveyed benchmarks, location and dimensions of areas of the
property where contamination is known to exist in
® groundwater at a concentration exceeding the standard or interim standard established in 15A
NCAC 2L .0202 and/or
soil at a concentration exceeding the residential maximum soil contaminant concentration
established in 15A NCAC 2L .0411.
c. The printed name(s) and title(s) and properly notarized signature(s) of individual(s) with authority
to legally bind the responsible party(ies) (i.e., responsible party(ies), an individual with power of
attorney for the responsible party(ies), officer of a corporation, etc.) (PRINTED TEXT,
SIGNATURES, AND NOTARY SEALS, AS WITH ALL MARKINGS ON THE PLAT, MUST
BE MADE IN INDELIBLE INK);
Revised February 7, 2019

d. The following language: "The areas of contamination depicted upon the map are approximations
derived from the best available information at the time of filing.";
e. The following language, for use by the Department, positioned in the upper left corner of the plat:
"Approved for the purposes of N.C.G.S. 14313-279.9 and 143B-279.11
(signature of Regional Supervisor)
, Regional Supervisor
(printed name of Regional Supervisor)
Regional Office
UST Section
Division of Waste Management
Department of Environment Quality
NORTH CAROLINA
COUNTY
I certify that the following person(s) personally appeared before me this day, each
acknowledging to me that he or she signed the foregoing document: (printedfull
name of Regional Supervisor)
Date:
(signature of Notary Public)
(Official Seal)
(printed or typed name of Notary Public)
Notary Public
My commission expires:
f. Surveyor's certification and seal (using a permanent ink stamp).
6. The signed and notarized Notice (with all indicated attachments) shall be sent to the appropriate UST
Section Regional Office.
7. After the Department approves, notarizes and returns the Notice, the responsible party shall, within
thirty (30) days of its return:
a. File approved Notice in the County Register of Deeds' office of the county or counties in which
the site is located; and
b. Send to the appropriate UST Section Regional Office, a certified copy of the Notice affixed with
the seal of the Register of Deeds and reflecting the book(s) and page number(s) where recorded
and a copy of the page(s) in the grantor index where the Notice is referenced.
Revised February 7, 2019
2

NOTICE OF RESIDUAL PETROLEUM
County, North Carolina
(site name)
The property that is the subject of this Notice (hereinafter referred to as the "Site")
contains residual petroleum and is an Underground Storage Tank (UST) incident under North
Carolina's Statutes and Regulations, which consist of N.C.G.S. 143-215.94 and regulations adopted
thereunder. This Notice is part of a remedial action for the Site that has been approved by the
Secretary (or his/her delegate) of the North Carolina Department of Environment Quality (or its
successor in function), as authorized by N.C.G.S. Section 14313-279.9 and 143B-279.11. The North
Carolina Department of Environment Quality shall hereinafter be referred to as "DEQ".
NOTICE
Petroleum product was released and/or discharged at the Site. Petroleum constituents remain
on the site, but are not a danger to public health and the environment, provided that the
restrictions described herein, and any other measures required by DEQ pursuant to N.C.G.S.
Sections 143B-279.9 and 14313-279.11, are strictly complied with. This "Notice of Residual
Petroleum" is composed of a description of the property, the location of the residual petroleum, and the
land use restrictions on the Site. The Notice has been approved and notarized by DEQ pursuant to
N.C.G.S. Sections 143B-279.9 and 143B-279.11 and has/shall be recorded at the
Register of Deeds' office Book , Page
(name of county)
Any map or plat required by DEQ has been/shall be recorded at the Register of
(name of county)
Deeds' office Book , Page , and has been/shall be incorporated into the Notice by this reference.
Source Property
of
is the owner in fee
(owner's name) (city & state of homeowner)
simple of all or a portion of the Site, which is located in the County of , State of North
Carolina, and is known and legally described as:
Revised February 7, 2019

(Insert Real Property Description Here for Source Property)
Additional Affected Property Also Subject to Restrictions
of is the owner in fee simple of a portion of
(owner's name) (city & state of owner)
the Site, which is located in the County of , State of North Carolina. Petroleum
contamination is located on this property at the time this Notice is approved. This property was also
owned or controlled by the underground storage tank owner or operator or another party responsible for
the petroleum discharge or release at the time the discharge or release was discovered or reported, or at
any time thereafter. This property is known and legally described as:
(Insert Real Property Description Here for Additional Properties Owned or Controlled by Any Owner or
Operator of the Underground Storage Tank or Other Responsible Party, if Applicable)
Additional Affected Property Not Subject to Restrictions
Additionally residual petroleum is also located on the following property. The following
property is not subject to land use restrictions pursuant to N.C.G.S. Section 143B-279.9(b). The
following property is known and legally described as:
(Insert Legal Description of Other Real Property Affected by Residual Petroleum Not Owned or
Controlled by Any Owner or Operator of the Underground Storage Tank or Other Responsible Party, if
Applicable)
For protection of public health and the environment, the following land use restrictions required
by N.C.G.S. Section 143B-279.9(b) shall apply to all of the above -described real property. These
restrictions shall continue in effect as long as residual petroleum remains on the site in excess of
unrestricted use standards and cannot be amended or cancelled unless and until the County
Register of Deed receives and records the written concurrence of the Secretary (or his/her delegate) of
Revised February 7, 2019
2

DEQ (or its successor in function).
[Restrictions apply to activities on, over, or under the land. Choose one or more of the following as
appropriate.]
Soil: Alternate]) Soil containing residual petroleum, above applicable regulatory
standard(s), remains on the site at/within/etc. (Description of specific location on
the site of remaining petroleum contaminated soil). No soil shall be excavated or
disturbed, within _ feet of (Description of specific location on the site of remaining
petroleum contaminated soil), except to remediate the soil in accordance with all
applicable state and federal statutes, regulations and guidelines.
Alternate 2) Soil containing residual petroleum above applicable regulatory
standard(s) remains on the site in the area identified in Figure 1, Attachment A
(Refer to extent of contamination as diagrammed in an existing report and attach
copy of that figure(s)). No soil shall be excavated or disturbed within 3 feet of the
area identified in Figure 1, Attachment A except to remediate the soil in accordance
with all applicable state and federal statutes, regulations and guidelines.
Groundwater: Groundwater from the site is prohibited from use as a water supply. Water supply wells
of any kind shall not be installed or operated on the site.
ENFORCEMENT
The above land use restriction(s) shall be enforced by any owner, operator, or other party
responsible for the Site. The above land use restriction(s) may also be enforced by DEQ through any of
the remedies provided by law or by means of a civil action, and may also be enforced by any unit of local
government having jurisdiction over any part of the Site. Any attempt to cancel this Notice without the
approval of DEQ (or its successor in function) shall be subject to enforcement by DEQ to the full extent
of the law. Failure by any party required or authorized to enforce any of the above restriction(s) shall in
no event be deemed a waiver of the right to do so thereafter as to the same violation or as to one occurring
prior or subsequent thereto.
IN WITNESS WHEREOF, has caused this Notice to be executed pursuant to
N.C.G.S. Sections 14313-279.9 and 14313-279.11, this day of , 20_
(name of responsible party if agent is signing)
(signature of responsible party, attorney or other agent if there is one)
(title of agent for responsible party if there is one)
Signatory's name typed or printed:
(Note to be deleted on final document: Preparer of document must assure that the correct
acknowledgement is used and complies with changes effective October 1, 2006)
Choice One: Instrument signed by one person
Revised February 7, 2019

NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
I certify that the following person(s) personally appeared before me this day, each acknowledging to me
that he or she signed the foregoing document:
Date:
(Official Seal)
expires:
Choice Two: Acknowledge by attorney in fact
NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
I, , a Notary Public for said County and State, do hereby certify that
, attorney in fact for , personally appeared before me this day, and being by
me duly sworn, says that he executed the foregoing and annexed instrument for and in behalf of the said
, and that his authority to execute and acknowledge said instrument is contained in an instrument duly
executed, acknowledged, and recorded in the office of in the County of
, State of , on the day of , 20and
that this instrument was executed under and by virtue of the authority given by said instrument granting
him power of attorney.
I do further certify that the said acknowledged the due execution of the
foregoing and annexed instrument for the purposes therein expressed for and in behalf of the said
WITNESS my hand and official seal, this the day of , 20
(Official Seal)
expires:
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
Choice Three: Conveying security interest in personal property of a corporation
NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
Revised February 7, 2019
4

a Notary Public for said County and State, do hereby certify that
personally came before me this day and acknowledged that he is
of and acknowledged, on behalf of , the grantor
the due execution of the foregoing instrument.
WITNESS my hand and official seal, this the day of 120
(Official Seal)
expires:
Approved for the purposes of N.C.G.S. 14313-279.11
(signature of Regional Supervisor)
, Regional Supervisor
(printed name of Regional Supervisor)
Regional Office
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
UST Section
Division of Waste Management
Department of Environment Quality
NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
I certify that the following person(s) personally appeared before me this day, each acknowledging to me
that he or she signed the foregoing document: (full printed name of Regional Supervisor)
Date:
(Official Seal)
expires:
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
Revised February 7, 2019

Beverly, Trudy
From: Beverly, Trudy
Sent: Monday, April 20, 2020 10:04 AM
To: Caldwell, Shawna; 'Morris, Brett L.'
Subject: Curry Vail LLC 2 - UST Incident #47014 — Notice of Regulatory Requirements
Attachments: MO-9583_47014_G_NORR_20200420_Notice of Regulatory Requirements.pdf
Please see the attached Notice of Regulatory Requirements for Curry Vail LLC 2 located at 2553 Vail Avenue, Charlotte,
Mecklenburg County, North Carolina (Incident #47014).
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
L31 UU�,�UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenr. og_v
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https:Hdeq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hgps:Hdeq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deu.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://deq.nc.gov/about/divisions/waste-mana2ement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httas://files.ne.izov/nede(ifWaste%2OManagement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policy.ildf
htips:Hfiles.nc. gov/ncdeq/Waste°/`20Mana2ement/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.doex

Limited Site Assessment — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
APPENDIX IV
DEED & PROPERTY INFORMATION
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels _Phase I UST\LSA\Appendix IV -Deed and Prop Info.rtf

Excise Tax $ _0_
Tax Lot No.
Verified by
by _
FOR REGISTRATION JUDITH A. GIBSON
REGISTER OF DEEDS
MECKLENBURG COUNTY, NC
2003 DEC 22 02:17 PM
BK 16696 PG 540-543 FEE,$20.00
INSTRUMENT # 2003304395
11111111 IN 11111111111111111111111111111111
2003304395
Time. Book and
Parcel Identifier No. 127-121-04; 127-121-05
County on the day of , 2003_
Mail after recording to Grantee
This instrument was prepared by W. Chris Parnell
Brief Description for the index 2553 Vail Avenue (127-121-04)
2547 Vail Avenue (127-121-05)
NORTH CAROLINA GENERAL WARRANTY DEED
THIS DEED made December 22nd, 2003, by and between
GRANTOR
CURRY & TROIANO, a North Carolina General
Partnership
Curry Vail LLC
1001 Berkeley Ave.
Charlotte, NC 28203
GRANTEE
Enter in appropriate block for each party: name, address, and, if appropriate, character of entity, e.g., corporation or partnership.
The designation Grantor and Grantee as used herein shall include said parties, their heirs, successors, and assigns, and
shall include singular, plural, masculine, feminine or neuter as required by context.
WITNESSETH, that the Grantor, for a valuable consideration paid by the Grantee, the receipt of which is hereby
acknowledged, has and by these presents does grant, bargain, sell and convey unto the Grantee in fee simple, all that
certain lot or parcel of land situated in the City of , Charlotte Township, Mecklenburg County, North Carolina and more
particularly described as follows:
See Exhibit A attached hereto and made a part hereof.
N.C. Bar Assoc. Form No. 3 ® 1977
Printed by Agreement with the N.C. Bar Assoc.
no0s

The property hereinabove described was acquired by Grantor by instruments recorded in Book 3575,
Page 137 and Book 3561, Page 19.
A map showing the above described property is recorded in Plat Book , Page .
TO HAVE AND TO HOLD the aforesaid lot or parcel of land and all privileges and appurtenances thereto belonging to
the Grantee in fee simple.
And the Grantor covenants with the Grantee, that Grantor is seized of the premises in fee simple, has the right to
convey the same in fee simple, that title is marketable and free and clear of all encumbrances, and that Grantor will
warrant and defend the title against the lawful claims of ail persons whomsoever except for the exceptions hereinafter
stated.
Title to the property hereinabove described is subject to the following exceptions:
Easements and restrictions of record.
Ad valorem property taxes.
IN WITNESS WHEREOF, the Grantor has hereunto set his hand and seal, or if corporate, has caused this instrument to be
signed in its corporate name by its duly authorized officers and its seal to be hereunto affixed by authority of its Board of
Directors, the day and year first above written.
CURRY & TROIANO
BY:
j {SEAL)
(Corporate Name) Z HAL D. CURRY, Gen I Partner
O
kie
By: Z
(SEAL)
U
President
m BY:
ATTEST: N (SEAL!
A. MYCHAEL TROIANO, JR., Genera artner
(SEAL)
Secretary (Corporate Seal)
+Mal!
J�j�s g
J�W ►►'4 NORTH CAROLINA, MecklenburCounty.
`��� 1� ��•���•. �� I, a Notary Public of the County and State aforesaid, certify that Hal D. Curry and A. Michael Troiano. Jr.
���_� •.•' ..� �e personally appeared before me this day and acknowledged the execution of the foregoing instrument. Witness
'+ my hand and official stamp or seal, this 22ndday of December. 2003.
o
to _bq + My commission expires:
• ;� +
1
' A
:0G ,.•��` 5/24/05 Notary Public
SEAL -STAMP NORTH CAROLINA, County.
I, a Notary Public of the County and State aforesaid, certify that personally came before me this day and
' acknowledged that he/she is Secretary of , a North Carolina corporation, and that by authority
z
O duly given and as the act of the corporation, the foregoing instrument was signed in its name by its
z President, sealed with its corporate seal and attested by him/her as its Secretary, Witness my hand
and official stamp or seal, this _ day of 19_
a
J
00 My commission expires:
w
f�
Notary Public
The foregoing Certificateis) of
is/are certified to be correct. This instrument and this certificate are duly registered at the date and in the Book and Page shown on the first page
hereof.
REGISTER OF DEEDS FOR COUNTY
By Deputy/Assistant-Register of Deeds.
N.C. Bar Assoc,. Form No. 3 ® 1977
Printed by Agreement with the N.C. Bar Assoc.
ao03

EXHIBIT A
TRACT I: BEGINNING AT AN IRON STAKE IN THE NORTHEASTERN LINE OF
VAIL AVENUE, SAID PLACE OF BEGINNING BEING 590 FEET IN A
SOUTHEASTERLY DIRECTION MEASURED ALONG SAID NORTHEASTERLY
LINE OF VAIL AVENUE FROM THE POINT OF INTERSECTION OF SAID LINE
OF VAIL AVENUE WITH THE SOUTHEASTERLY LINE OF DOTGER AVENUE,
AND RUNS THENCE NORTH 38-51 EAST 157.3 FEET TO AN IRON STAKE IN A
BRANCH; THENCE SOUTH 21-47 EAST 106.98 FEET TO AN IRON STAKE IN
SAID BRANCH; THENCE SOUTH 55-31 WEST 118.5 FEET TO AN IRON STAKE
IN THE NORTHEASTERLY LINE OF VAIL AVENUE; AND THENCE WITH THE
NORTHEASTERLY LINE OF VAIL AVENUE AND IN A NORTHWESTERLY
DIRECTION 60 FEET TO THE PLACE OF BEGINNING.
BEING THE SAME PROPERTY DESCRIBED IN THE DEED RECORDED IN BOOK
3561, PAGE 19, IN THE MECKLENBURG PUBLIC REGISTRY.
TRACT II: BEGINNING AT AN IRON STAKE IN THE NORTHEASTERLY LINE
OF VAIL AVENUE, SAID PLACE OF BEGINNING BEING 650 FEET IN A
SOUTHEASTERLY DIRECTION MEASURED ALONG SAID NORTHEASTERLY
LINE OF VAIL AVENUE FROM THE POINT OF INTERSECTION OF SAID LINE
OF VAIL AVENUE WITH THE SOUTHEASTERLY LINE OF DOTGER AVENUE,
AND RUNS THENCE N. 55-31 E.118.5 FEET TO AN IRON STAKE IN A BRANCH;
THENCE S. 20-05 E. 127.02 FEET TO AN IRON STAKE; THENCE S. 79-01 W. 112.5
FEET TO AN IRON STAKE IN THE NORTHEASTERLY LINE OF VAIL AVENUE;
AND THENCE WITH THE NORTHEASTERLY LINE OF VAIL AVENUE AND IN A
NORTHWESTERLY DIRECTION 80 FEET TO THE PLACE OF BEGINNING.
BEING THE SAME PROPERTY DESCRIBED IN THE DEED RECORDED IN BOOK
3575, PAGE 137, IN THE MECKLENBURG PUBLIC REGISTRY.

2
tr
JUDITH A. GIBSON
rt
REGISTER OF DEEDS, MECKLENBURG
COUNTY & COURTS OFFICE BUILDING
720 EAST FOURTH STREET
CHARLOTTE, NC 28202
Filed For Registration:
Book:
Document No
Recorder:
12122/2003 02:17 PM
RE 16588 Page: 540-543
2003304395
DEED 4 PGS $20.00
LINDA CASTLEBERRY
State of North Carolina, County of Mecklenburg
The foregoing certificate of DIANE MCGUIRE Notary is certified to be correct. This 22 ND of December 2003
r
JUDITH A. GIBSON, REGISTER OF DEEDS By CX -
DeputylAssistant Register of Deeds
2003304395

STATE OF NORTH CAROLINA
_ M&CKLFrXB1J13G-------- COUNTY
INDIVIDUAL ' DEED
Printed and Far Sale BY.
r•. ;
KALE OFFICE OUTFITTERS, LTD,
Charlotte; N. C. 1973
MAY
PnTb
lllEGJs,rEf OF EEQ
\:J� Made this----------7th MECI` �1bfJRG
5
Xay�---------------------------, A. D. 19 7 3_ by' and between ---------------------
FRANCIS I. PARKER and wife, MARY.B. PARKER,
AND
WILLIAM E. POE and wife, MARY W. POE,
Mecklenburg North Carolina,
of the County of_ _------------- and State of ------- _-�-----------
Part-ies _of the first part, and -------------------------------------------------
CURRY AND, TRO.IAf�TO,
(a North Carolina Partnership)
of the County of___MeckleDhur_c�---------- and State of--- North Carolina, °'
part_-Y-__of the second part:
WITNESSETH, that the said part tes--of the first part, in consideration of ----------------
One Hundred Dollars and other valuable considerations-----`-W-W
to__thETaid by the part__Y_____of the second part, the receipt of which is hereby acknowledged
ha_ ve_'_bargained and sold, and by these presents do ------------ grant, bargain, sell and convey
unto the said--___pn;Zty_ of _the _second_part----------------------------------- and
successors and assigns,
its NNW, all ----- that-Ict_-ar_-par- eL--------------------------
________-_________________________________________________of land, situate, lying and being in
_7e_City _of__Charlotte ���--- Mecklenbur------------ County, State of
North Carolina, and more particularly described as follows:
BEGINNING at an iron stake in the northeasterly line of Vail Avenue,
said place of beginning being 650 feet in a southeasterly
direction measured along said northeasterly line of Vail Avenue
from the point of intersection of said line of Vail Avenue with
the southeasterly line of Dotger Avenue, and runs thence N.
55-31 E. 118.5 feet to an iron stake in a branch; thence S. 20-05
E. 127.02 feet to an iron stake; thence S. 79-01 W. 112.5 feet
to an iron stake in the northeasterly line of Vail Avenue; and
thence with the northeasterly line of Vail Avenue and in a
northwesterly direction 80 feet to the place of BEGINNING. Said
lot being known as 2553-55 Vail Avenue.
Being in all respects the same property conveyed to Francis I.
Parker and William E. Poe by deed of Edwin 0. Clarkson and wife,
Elizabeth Barnhill Clarkson, dated May 24, 1955, and recorded
in Book 1766, page 318 of the Mecklenburg County Registry.
137

MECKLENBURG COUNTY — PROPERTY RECORD CARD PROPERTY SEARCH
PARCEL ID: 12712104 CURRY VAIL LLC
2553 VAIL AV CHARLOTTE NC 1001 BERKELEY AVE
CHARLOTTE NC 28203
KEY INFORMATION
Land Use Code
R100 Neighborhood
Land Use Desc
SINGLE FAMILY RESIDENTIAL Land
Exemption/Deferment
Municipality
Last Sale Date
Fire District
Last Sale Price
- Special District
Legal Description
2553 VAIL AVE
ASSESSMENT DETAILS
2020 Real Estate Assessed Value
Land Value
Building Value
Features
Total
BUILDING (1)
Finished Area
1,850
Year Built
1954
Story
2.0 STORY
Heat
FORCED AIR -
DUCTED
Foundation
CRAWL SPACE
External Wall
FACE BRICK
Full Bath(s)
2
Half Bath(s)
Total (SgFt)
2,130
Total Appraised Value
$563,900
M711
1 LOT
CHARLOTTE
CITY OF CHARLOTTE
NA
Built Use / Style
Fuel
Fireplace(s)
Bedroom(s)
$451,000
$112,700
$200
$563,900
DUPLEX -TRIPLEX
GAS
2
LAND
Use Units Type Neighborhood Assessment
R100 1 LOT M711 $451,000
FEATURES
Year Built Type Quantity Units Value
1954 TERRACE 1 48 $200
VALUE CHANGES
The value change history shows only changes in appraised value; it does not show exemptions, exclusions or deferrals that could
reduce a property's taxable value. If any of these are in effect for a particular tax year, it will be shown on the property tax bill for
that year. It is also possible that some previous value changes might be missing from this list or listed in the wrong order. If you
have any questions, please call the County Assessor's Office at 704-336-7600.
Date of Value Change
Effective for Tax Year
Reason for Change
New Value
01/15/2019
2019
COUNTYWIDE REVALUATION
$563,900
04/15/2014
2011
REVALUATION REVIEW - PEARSON
$261,600
02/04/2011
2011
COUNTYWIDE REVALUATION
$254,300
03/15/2003
2003
COUNTYWIDE REVALUATION
$220,000

12712104
YL,
R�
N
100 ft 14
1
Disclaimer
Mecklenburg County makes every effort to produce the most accurate information possible. No warranties, expressed or implied, are provided for the data
herein, its use or interpretation.

Limited Site Assessment — Curry Vail LLC Properties SUMMIT Project No. 1820.E0004
Charlotte, North Carolina August 12, 2020
APPENDIX V
ANALYTICAL RESULTS
C:\plowery\Documents\2-Projects\1820 Saussy Burbank\1820.82 Vail Avenue Parcels_ Phase I USTTSA\Appendix V - Analytical.rtf

0
aceAnalytical
Report of Analysis
SUMMIT Engineering, Laboratory & Testing, P.C.
3575 Centre Circle
Fort Mill, SC 28715
Attention: Patrick Lowery
Project Name: Vail Avenue
Project Number: 1820.E0004
Lot Number:VG13017
Date Completed:07/31/2020
07/31/2020 5:07 PM
Approved and released by:
Project Manager II: Lucas Odom
pCCgF�
24r�14A
"
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 46

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: VG13017
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
VPH
Surrogate recovery for the following sample was outside control limits: VG13017-001. Evidence of matrix
interference is present; therefore, re -extraction and/or re -analysis was not performed.
VOCs by GC/MS
Isopropylbenzene was reported as an estimated value in sample: VG13017-001 as the result was above
the upper calibration level. The sample was re -analyzed from the medium level (methanol) vial, but was
not reported due to the result being below the LOQ therefore only the low level was reported.
SVOCs by GC/MS
The LCS associated with batch 60855 recovered four compounds above method criteria. No corrective
action is required as the associated samples are non -detect for these compounds.
EPH
Due to matrix interferences, the surrogate associated with sample -001 recovered above method criteria.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 46

PACE ANALYTICAL SERVICES, LLC
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: VG13017
Sample Number Sample ID Matrix Date Sampled Date Received
001 SB-4 Solid 07/13/20201100 07/13/2020
002 SB-5 Solid 07/13/20201200 07/13/2020
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 46

PACE ANALYTICAL SERVICES, LLC
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: VG13017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
SB-4
Solid
Acetone
8260D
10
J
ug/kg
5
001
SB-4
Solid
Cyclohexane
8260D
6.6
ug/kg
5
001
SB-4
Solid
Ethylbenzene
8260D
150
ug/kg
5
001
SB-4
Solid
Isopropylbenzene
8260D
240
E
ug/kg
5
001
SB-4
Solid
Methylcyclohexane
8260D
79
ug/kg
5
001
SB-4
Solid
Xylenes (total)
8260D
50
ug/kg
6
001
SB-4
Solid
Acenaphthene
8270E
210
ug/kg
6
001
SB-4
Solid
Anthracene
8270E
310
ug/kg
6
001
SB-4
Solid
1,1'-Biphenyl
8270E
730
ug/kg
6
001
SB-4
Solid
Fluoranthene
8270E
37
J
ug/kg
7
001
SB-4
Solid
Fluorene
8270E
450
ug/kg
7
001
SB-4
Solid
2-Methylnaphthalene
8270E
2800
ug/kg
7
001
SB-4
Solid
Naphthalene
8270E
630
ug/kg
7
001
SB-4
Solid
Phenanthrene
8270E
1300
ug/kg
8
001
SB-4
Solid
Pyrene
8270E
220
ug/kg
8
001
SB-4
Solid
C11 - C22 Aromatics
MADEP-EPH-
250
mg/kg
8
001
SB-4
Solid
C9 - C18 Aliphatics
MADEP-EPH-
230
mg/kg
8
001
SB-4
Solid
C19 - C36 Aliphatics
MADEP-EPH-
52
mg/kg
8
001
SB-4
Solid
C5 - C8 Aliphatics
MADEP-VPH-
6.0
mg/kg
9
001
SB-4
Solid
C9 - C12 Aliphatics
MADEP-VPH-
92
mg/kg
9
001
SB-4
Solid
C9 - C10 Aromatics
MADEP-VPH-
72
mg/kg
9
(21 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-001
Description: SB-4 Matrix: Solid
Date Sampled:07/13/2020 1100 % Solids: 85.7 07/13/2020 2308
Date Received:07/13/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 07/23/20201533 JM1 61025 5.95
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
10 J
20
7.8
ug/kg
Benzene
71-43-2
8260D
ND
4.9
2.0
ug/kg
Bromodichloromethane
75-27-4
8260D
ND
4.9
2.0
ug/kg
Bromoform
75-25-2
8260D
ND
4.9
2.0
ug/kg
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
4.9
2.9
ug/kg
2-Butanone (MEK)
78-93-3
8260D
ND
20
3.9
ug/kg
Carbon disulfide
75-15-0
8260D
ND
4.9
2.0
ug/kg
Carbon tetrachloride
56-23-5
8260D
ND
4.9
2.0
ug/kg
Chlorobenzene
108-90-7
8260D
ND
4.9
2.0
ug/kg
Chloroethane
75-00-3
8260D
ND
4.9
2.0
ug/kg
Chloroform
67-66-3
8260D
ND
4.9
2.0
ug/kg
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
4.9
2.9
ug/kg
Cyclohexane
110-82-7
8260D
6.6
4.9
2.0
ug/kg
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
4.9
2.0
ug/kg
Dibromochloromethane
124-48-1
8260D
ND
4.9
2.0
ug/kg
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
4.9
2.0
ug/kg
1,2-Dichlorobenzene
95-50-1
8260D
ND
4.9
2.0
ug/kg
1,3-Dichlorobenzene
541-73-1
8260D
ND
4.9
2.0
ug/kg
1,4-Dichlorobenzene
106-46-7
8260D
ND
4.9
2.0
ug/kg
Dichlorodifluoromethane
75-71-8
8260D
ND
4.9
2.9
ug/kg
1,1-Dichloroethane
75-34-3
8260D
ND
4.9
2.0
ug/kg
1,2-Dichloroethane
107-06-2
8260D
ND
4.9
2.0
ug/kg
1,1-Dichloroethene
75-35-4
8260D
ND
4.9
2.0
ug/kg
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
4.9
2.0
ug/kg
trans-1,2-Dichloroethene
156-60-5
8260D
ND
4.9
2.0
ug/kg
1,2-Dichloropropane
78-87-5
8260D
ND
4.9
2.0
ug/kg
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
4.9
2.0
ug/kg
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
4.9
2.0
ug/kg
Ethylbenzene
100-41-4
8260D
150
4.9
2.0
ug/kg
2-Hexanone
591-78-6
8260D
ND
9.8
3.9
ug/kg
Isopropylbenzene
98-82-8
8260D
240 E
4.9
2.0
ug/kg
Methyl acetate
79-20-9
8260D
ND
4.9
2.0
ug/kg
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
4.9
2.0
ug/kg
4-Methyl-2-pentanone
108-10-1
8260D
ND
9.8
3.9
ug/kg
Methylcyclohexane
108-87-2
8260D
79
4.9
2.0
ug/kg
Methylene chloride
75-09-2
8260D
ND
4.9
2.0
ug/kg
Styrene
100-42-5
8260D
ND
4.9
2.0
ug/kg
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
4.9
2.0
ug/kg
Tetrachloroethene
127-18-4
8260D
ND
4.9
2.0
ug/kg
Toluene
108-88-3
8260D
ND
4.9
2.0
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-001
Description: SB-4 Matrix: Solid
Date Sampled:07/13/2020 1100 % Solids: 85.7 07/13/2020 2308
Date Received:07/13/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
1 5035
8260D 1 07/23/20201533 JM1
61025
5.95
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D
ND
4.9
2.0
ug/kg
1
1,2,4-Trichlorobenzene
120-82-1 8260D
ND
4.9
2.0
ug/kg
1
1,1,1-Trichloroethane
71-55-6 8260D
ND
4.9
2.0
ug/kg
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
4.9
2.0
ug/kg
1
Trichloroethene
79-01-6 8260D
ND
4.9
2.0
ug/kg
1
Trichlorofluoromethane
75-69-4 8260D
ND
4.9
2.0
ug/kg
1
Vinyl chloride
75-01-4 8260D
ND
4.9
2.9
ug/kg
1
Xylenes (total)
1330-20-7 8260D
50
9.8
3.9
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
105 47-138
1,2-Dichloroethane-d4
101 53-142
Toluene-d8
N 126 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E 20 07/29/2020 1729 SCD
07/22/2020 1102 60855
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9 8270E
210
62
19
ug/kg
1
Acenaphthylene
208-96-8 8270E
ND
62
22
ug/kg
1
Acetophenone
98-86-2 8270E
ND
300
120
ug/kg
1
Anthracene
120-12-7 8270E
310
62
12
ug/kg
1
Atrazine
1912-24-9 8270E
ND
300
120
ug/kg
1
Benzaldehyde
100-52-7 8270E
ND
300
120
ug/kg
1
Benzo(a)anthracene
56-55-3 8270E
ND
62
14
ug/kg
1
Benzo(a)pyrene
50-32-8 8270E
ND
62
15
ug/kg
1
Benzo(b)fluoranthene
205-99-2 8270E
ND
62
12
ug/kg
1
Benzo(g,h,i)perylene
191-24-2 8270E
ND
62
15
ug/kg
1
Benzo(k)fluoranthene
207-08-9 8270E
ND
62
11
ug/kg
1
1,1'-Biphenyl
92-52-4 8270E
730
300
120
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3 8270E
ND
300
120
ug/kg
1
Butyl benzyl phthalate
85-68-7 8270E
ND
300
120
ug/kg
1
Caprolactam
105-60-2 8270E
ND
300
120
ug/kg
1
Carbazole
86-74-8 8270E
ND
300
120
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1 8270E
ND
300
120
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7 8270E
ND
300
120
ug/kg
1
4-Chloroaniline
106-47-8 8270E
ND
300
120
ug/kg
1
bis(2-Chloroethoxy)methane
111-91-1 8270E
ND
300
120
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-001
Description: SB-4 Matrix: Solid
Date Sampled:07/13/2020 1100 % Solids: 85.7 07/13/2020 2308
Date Received:07/13/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 20 07/29/2020 1729 SCD 07/22/2020 1102 60855
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
300
120
ug/kg
2-Chloronaphthalene
91-58-7
8270E
ND
300
120
ug/kg
2-Chlorophenol
95-57-8
8270E
ND
300
120
ug/kg
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
300
120
ug/kg
Chrysene
218-01-9
8270E
ND
62
10
ug/kg
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
62
12
ug/kg
Dibenzofuran
132-64-9
8270E
ND
300
120
ug/kg
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
300
120
ug/kg
2,4-Dichlorophenol
120-83-2
8270E
ND
300
120
ug/kg
Diethylphthalate
84-66-2
8270E
ND
300
120
ug/kg
Dimethyl phthalate
131-11-3
8270E
ND
300
170
ug/kg
2,4-Dimethylphenol
105-67-9
8270E
ND
300
120
ug/kg
Di-n-butyl phthalate
84-74-2
8270E
ND
300
120
ug/kg
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
1500
580
ug/kg
2,4-Dinitrophenol
51-28-5
8270E
ND
1500
580
ug/kg
2,4-Dinitrotoluene
121-14-2
8270E
ND
620
230
ug/kg
2,6-Dinitrotoluene
606-20-2
8270E
ND
620
230
ug/kg
Di-n-octylphthalate
117-84-0
8270E
ND
300
120
ug/kg
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
1500
580
ug/kg
Fluoranthene
206-44-0
8270E
37 J
62
9.7
ug/kg
Fluorene
86-73-7
8270E
450
62
13
ug/kg
Hexachlorobenzene
118-74-1
8270E
ND
300
120
ug/kg
Hexachlorobutadiene
87-68-3
8270E
ND
300
120
ug/kg
Hexachlorocyclopentadiene
77-47-4
8270E
ND
1500
580
ug/kg
Hexachloroethane
67-72-1
8270E
ND
300
120
ug/kg
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
62
23
ug/kg
Isophorone
78-59-1
8270E
ND
300
120
ug/kg
2-Methylnaphthalene
91-57-6
8270E
2800
62
23
ug/kg
2-Methylphenol
95-48-7
8270E
ND
300
120
ug/kg
3+4-Methylphenol
106-44-5
8270E
ND
620
230
ug/kg
Naphthalene
91-20-3
8270E
630
62
22
ug/kg
2-Nitroaniline
88-74-4
8270E
ND
620
230
ug/kg
3-Nitroaniline
99-09-2
8270E
ND
620
230
ug/kg
4-Nitroaniline
100-01-6
8270E
ND
620
230
ug/kg
Nitrobenzene
98-95-3
8270E
ND
300
120
ug/kg
2-Nitrophenol
88-75-5
8270E
ND
620
230
ug/kg
4-Nitrophenol
100-02-7
8270E
ND
1500
580
ug/kg
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
300
120
ug/kg
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
300
120
ug/kg
Pentachlorophenol
87-86-5
8270E
ND
1500
580
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-001
Description: SB-4 Matrix: Solid
Date Sampled:07/13/2020 1100 % Solids: 85.7 07/13/2020 2308
Date Received:07/13/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E 20 07/29/2020 1729 SCD
07/22/2020 1102 60855
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Phenanthrene
85-01-8 8270E
1300
62
17
ug/kg
1
Phenol
108-95-2 8270E
ND
300
120
ug/kg
1
Pyrene
129-00-0 8270E
220
62
12
ug/kg
1
Pyridine
110-86-1 8270E
ND
300
120
ug/kg
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
300
120
ug/kg
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
300
120
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
71 33-102
2-Fluorophenol
65 35-115
Nitrobenzene-d5
78 22-109
Phenol-d5
60 33-122
Terphenyl-d14
88 41-120
2,4,6-Tribromophenol
62 30-117
MA EPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 07/29/2020 1705 JJG
07/25/2020 1009 61232
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C11 - C22 Aromatics
MADEP-EPH-04
250
11
11
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Bromonaphthalene (fractionation
2) N 167 40-140
2-Fluorobiphenyl (fractionation 1)
N 149 40-140
o - Terphenyl (aromatic)
N 212 40-140
MA EPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 07/29/2020 1332 JJG
07/25/2020 1009 61231
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C9 - C18 Aliphatics
MADEP-EPH-04
230
11
11
mg/kg
1
C19 - C36 Aliphatics
MADEP-EPH-04
52
11
11
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
112 40-140
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-001
Description: SB-4 Matrix: Solid
Date Sampled:07/13/2020 1100 % Solids: 85.7 07/13/2020 2308
Date Received:07/13/2020
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1
1 07/21/20201304 ECB
60720
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C5 - C8 Aliphatics
MADEP-VPH-18- 6.0
4.1
0.81
mg/kg
1
C9 - C12 Aliphatics
MADEP-VPH-18- 92
4.1
0.81
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
N
45 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1
1 07/21/20201304 ECB
60722
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C9 - C10 Aromatics
MADEP-VPH-18- 72
1.4
0.54
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (PID)
81 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-002
Description: SB-5 Matrix: Solid
Date Sampled:07/13/2020 1200 % Solids: 83.0 07/13/2020 2308
Date Received:07/13/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260D 1 07/25/2020 0421 JTH 61221 5.13
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
23
9.4
ug/kg
Benzene
71-43-2
8260D
ND
5.9
2.3
ug/kg
Bromodichloromethane
75-27-4
8260D
ND
5.9
2.3
ug/kg
Bromoform
75-25-2
8260D
ND
5.9
2.3
ug/kg
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
5.9
3.5
ug/kg
2-Butanone (MEK)
78-93-3
8260D
ND
23
4.7
ug/kg
Carbon disulfide
75-15-0
8260D
ND
5.9
2.3
ug/kg
Carbon tetrachloride
56-23-5
8260D
ND
5.9
2.3
ug/kg
Chlorobenzene
108-90-7
8260D
ND
5.9
2.3
ug/kg
Chloroethane
75-00-3
8260D
ND
5.9
2.3
ug/kg
Chloroform
67-66-3
8260D
ND
5.9
2.3
ug/kg
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
5.9
3.5
ug/kg
Cyclohexane
110-82-7
8260D
ND
5.9
2.3
ug/kg
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
5.9
2.3
ug/kg
Dibromochloromethane
124-48-1
8260D
ND
5.9
2.3
ug/kg
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
5.9
2.3
ug/kg
1,2-Dichlorobenzene
95-50-1
8260D
ND
5.9
2.3
ug/kg
1,3-Dichlorobenzene
541-73-1
8260D
ND
5.9
2.3
ug/kg
1,4-Dichlorobenzene
106-46-7
8260D
ND
5.9
2.3
ug/kg
Dichlorodifluoromethane
75-71-8
8260D
ND
5.9
3.5
ug/kg
1,1-Dichloroethane
75-34-3
8260D
ND
5.9
2.3
ug/kg
1,2-Dichloroethane
107-06-2
8260D
ND
5.9
2.3
ug/kg
1,1-Dichloroethene
75-35-4
8260D
ND
5.9
2.3
ug/kg
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
5.9
2.3
ug/kg
trans-1,2-Dichloroethene
156-60-5
8260D
ND
5.9
2.3
ug/kg
1,2-Dichloropropane
78-87-5
8260D
ND
5.9
2.3
ug/kg
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
5.9
2.3
ug/kg
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
5.9
2.3
ug/kg
Ethylbenzene
100-41-4
8260D
ND
5.9
2.3
ug/kg
2-Hexanone
591-78-6
8260D
ND
12
4.7
ug/kg
Isopropylbenzene
98-82-8
8260D
ND
5.9
2.3
ug/kg
Methyl acetate
79-20-9
8260D
ND
5.9
2.3
ug/kg
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
5.9
2.3
ug/kg
4-Methyl-2-pentanone
108-10-1
8260D
ND
12
4.7
ug/kg
Methylcyclohexane
108-87-2
8260D
ND
5.9
2.3
ug/kg
Methylene chloride
75-09-2
8260D
ND
5.9
2.3
ug/kg
Styrene
100-42-5
8260D
ND
5.9
2.3
ug/kg
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
5.9
2.3
ug/kg
Tetrachloroethene
127-18-4
8260D
ND
5.9
2.3
ug/kg
Toluene
108-88-3
8260D
ND
5.9
2.3
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-002
Description: SB-5 Matrix: Solid
Date Sampled:07/13/2020 1200 % Solids: 83.0 07/13/2020 2308
Date Received:07/13/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
2 5035
8260D 1 07/25/2020 0421 JTH
61221
5.13
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D
ND
5.9
2.3
ug/kg
2
1,2,4-Trichlorobenzene
120-82-1 8260D
ND
5.9
2.3
ug/kg
2
1,1,1-Trichloroethane
71-55-6 8260D
ND
5.9
2.3
ug/kg
2
1,1,2-Trichloroethane
79-00-5 8260D
ND
5.9
2.3
ug/kg
2
Trichloroethene
79-01-6 8260D
ND
5.9
2.3
ug/kg
2
Trichlorofluoromethane
75-69-4 8260D
ND
5.9
2.3
ug/kg
2
Vinyl chloride
75-01-4 8260D
ND
5.9
3.5
ug/kg
2
Xylenes (total)
1330-20-7 8260D
ND
12
4.7
ug/kg
2
Run 2 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
108 47-138
1,2-Dichloroethane-d4
82 53-142
Toluene-d8
103 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E 1 07/25/2020 2115 SCD
07/22/2020 1102 60855
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9 8270E
ND
3.2
0.98
ug/kg
1
Acenaphthylene
208-96-8 8270E
ND
3.2
1.1
ug/kg
1
Acetophenone
98-86-2 8270E
ND
15
5.9
ug/kg
1
Anthracene
120-12-7 8270E
ND
3.2
0.60
ug/kg
1
Atrazine
1912-24-9 8270E
ND
15
5.9
ug/kg
1
Benzaldehyde
100-52-7 8270E
ND
15
5.9
ug/kg
1
Benzo(a)anthracene
56-55-3 8270E
ND
3.2
0.70
ug/kg
1
Benzo(a)pyrene
50-32-8 8270E
ND
3.2
0.78
ug/kg
1
Benzo(b)fluoranthene
205-99-2 8270E
ND
3.2
0.59
ug/kg
1
Benzo(g,h,i)perylene
191-24-2 8270E
ND
3.2
0.77
ug/kg
1
Benzo(k)fluoranthene
207-08-9 8270E
ND
3.2
0.57
ug/kg
1
1,1'-Biphenyl
92-52-4 8270E
ND
15
5.9
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3 8270E
ND
15
5.9
ug/kg
1
Butyl benzyl phthalate
85-68-7 8270E
ND
15
5.9
ug/kg
1
Caprolactam
105-60-2 8270E
ND
15
5.9
ug/kg
1
Carbazole
86-74-8 8270E
ND
15
5.9
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1 8270E
ND
15
5.9
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7 8270E
ND
15
5.9
ug/kg
1
4-Chloroaniline
106-47-8 8270E
ND
15
5.9
ug/kg
1
bis(2-Chloroethoxy)methane
111-91-1 8270E
ND
15
5.9
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-002
Description: SB-5 Matrix: Solid
Date Sampled:07/13/2020 1200 % Solids: 83.0 07/13/2020 2308
Date Received:07/13/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 07/25/2020 2115 SCD 07/22/2020 1102 60855
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
15
5.9
ug/kg
2-Chloronaphthalene
91-58-7
8270E
ND
15
5.9
ug/kg
2-Chlorophenol
95-57-8
8270E
ND
15
5.9
ug/kg
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
15
5.9
ug/kg
Chrysene
218-01-9
8270E
ND
3.2
0.53
ug/kg
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
3.2
0.60
ug/kg
Dibenzofuran
132-64-9
8270E
ND
15
5.9
ug/kg
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
15
5.9
ug/kg
2,4-Dichlorophenol
120-83-2
8270E
ND
15
5.9
ug/kg
Diethylphthalate
84-66-2
8270E
ND
15
5.9
ug/kg
Dimethyl phthalate
131-11-3
8270E
ND
15
8.7
ug/kg
2,4-Dimethylphenol
105-67-9
8270E
ND
15
5.9
ug/kg
Di-n-butyl phthalate
84-74-2
8270E
ND
15
5.9
ug/kg
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
79
30
ug/kg
2,4-Dinitrophenol
51-28-5
8270E
ND
79
30
ug/kg
2,4-Dinitrotoluene
121-14-2
8270E
ND
32
12
ug/kg
2,6-Dinitrotoluene
606-20-2
8270E
ND
32
12
ug/kg
Di-n-octylphthalate
117-84-0
8270E
ND
15
5.9
ug/kg
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
79
30
ug/kg
Fluoranthene
206-44-0
8270E
ND
3.2
0.50
ug/kg
Fluorene
86-73-7
8270E
ND
3.2
0.67
ug/kg
Hexachlorobenzene
118-74-1
8270E
ND
15
5.9
ug/kg
Hexachlorobutadiene
87-68-3
8270E
ND
15
5.9
ug/kg
Hexachlorocyclopentadiene
77-47-4
8270E
ND
79
30
ug/kg
Hexachloroethane
67-72-1
8270E
ND
15
5.9
ug/kg
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
3.2
1.2
ug/kg
Isophorone
78-59-1
8270E
ND
15
5.9
ug/kg
2-Methylnaphthalene
91-57-6
8270E
ND
3.2
1.2
ug/kg
2-Methylphenol
95-48-7
8270E
ND
15
5.9
ug/kg
3+4-Methylphenol
106-44-5
8270E
ND
32
12
ug/kg
Naphthalene
91-20-3
8270E
ND
3.2
1.1
ug/kg
2-Nitroaniline
88-74-4
8270E
ND
32
12
ug/kg
3-Nitroaniline
99-09-2
8270E
ND
32
12
ug/kg
4-Nitroaniline
100-01-6
8270E
ND
32
12
ug/kg
Nitrobenzene
98-95-3
8270E
ND
15
5.9
ug/kg
2-Nitrophenol
88-75-5
8270E
ND
32
12
ug/kg
4-Nitrophenol
100-02-7
8270E
ND
79
30
ug/kg
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
15
5.9
ug/kg
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
15
5.9
ug/kg
Pentachlorophenol
87-86-5
8270E
ND
79
30
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-002
Description: SB-5 Matrix: Solid
Date Sampled:07/13/2020 1200 % Solids: 83.0 07/13/2020 2308
Date Received:07/13/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E 1 07/25/2020 2115 SCD
07/22/2020 1102 60855
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Phenanthrene
85-01-8 8270E
ND
3.2
0.85
ug/kg
1
Phenol
108-95-2 8270E
ND
15
5.9
ug/kg
1
Pyrene
129-00-0 8270E
ND
3.2
0.59
ug/kg
1
Pyridine
110-86-1 8270E
ND
15
5.9
ug/kg
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
15
5.9
ug/kg
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
15
5.9
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
76 33-102
2-Fluorophenol
65 35-115
Nitrobenzene-d5
76 22-109
Phenol-d5
64 33-122
Terphenyl-d14
88 41-120
2,4,6-Tribromophenol
65 30-117
MA EPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 07/29/2020 1735 JJG
07/25/2020 1009 61232
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C11 - C22 Aromatics
MADEP-EPH-04
ND
12
12
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Bromonaphthalene (fractionation
2) 83 40-140
2-Fluorobiphenyl (fractionation 1)
79 40-140
o - Terphenyl (aromatic)
75 40-140
MA EPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 07/29/2020 1402 JJG
07/25/2020 1009 61231
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C9 - C18 Aliphatics
MADEP-EPH-04
ND
12
12
mg/kg
1
C19 - C36 Aliphatics
MADEP-EPH-04
ND
12
12
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
90 40-140
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 46

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG13017-002
Description: SB-5 Matrix: Solid
Date Sampled:07/13/2020 1200 % Solids: 83.0 07/13/2020 2308
Date Received:07/13/2020
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 07/21/20201333 ECB
60720
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C5 - C8 Aliphatics
MADEP-VPH-18- ND
4.7
0.93
mg/kg
1
C9 - C12 Aliphatics
MADEP-VPH-18- ND
4.7
0.93
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
130 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 07/21/20201333 ECB
60722
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C9 - C10 Aromatics
MADEP-VPH-18- ND
1.6
0.62
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (PID)
123 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 46

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 46

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ61025-001 Matrix: Solid
Batch: 61025 Prep Method: 5035
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
8.0
ug/kg
07/23/2020 1004
Benzene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Bromodichloromethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Bromoform
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Bromomethane (Methyl bromide)
ND
1
5.0
3.0
ug/kg
07/23/2020 1004
2-Butanone (MEK)
ND
1
20
4.0
ug/kg
07/23/2020 1004
Carbon disulfide
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Carbon tetrachloride
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Chlorobenzene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Chloroethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Chloroform
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Chloromethane (Methyl chloride)
ND
1
5.0
3.0
ug/kg
07/23/2020 1004
Cyclohexane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Dibromochloromethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,2-Dibromoethane (EDB)
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,2-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,3-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,4-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Dichlorodifluoromethane
ND
1
5.0
3.0
ug/kg
07/23/2020 1004
1,1-Dichloroethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,2-Dichloroethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,1-Dichloroethene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
cis- 1,2-Dichloroethene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
trans- 1,2-Dichloroethene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,2-Dichloropropane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
cis- 1,3-Dichloropropene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
trans- 1,3-Dichloropropene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Ethylbenzene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
2-Hexanone
ND
1
10
4.0
ug/kg
07/23/2020 1004
Isopropylbenzene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Methyl acetate
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Methyl tertiary butyl ether (MTBE)
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
4-Methyl-2-pentanone
ND
1
10
4.0
ug/kg
07/23/2020 1004
Methylcyclohexane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Methylene chloride
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Styrene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,1,2,2-Tetrachloroethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Tetrachloroethene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Toluene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,2,4-Trichlorobenzene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,1,1-Trichloroethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
1,1,2-Trichloroethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 46

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ61025-001 Matrix: Solid
Batch: 61025 Prep Method: 5035
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Trichloroethene
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Trichlorofluoromethane
ND
1
5.0
2.0
ug/kg
07/23/2020 1004
Vinyl chloride
ND
1
5.0
3.0
ug/kg
07/23/2020 1004
Xylenes (total)
ND
1
10
4.0
ug/kg
07/23/2020 1004
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 96 47-138
1,2-Dichloroethane-d4 101 53-142
Toluene-d8 83 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 46

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ61025-002
Matrix:
Solid
Batch: 61025
Prep Method:
5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
88
1
88
60-140
07/23/2020 0940
Benzene
50
56
1
111
70-130
07/23/2020 0940
Bromodichloromethane
50
54
1
107
70-130
07/23/2020 0940
Bromoform
50
53
1
107
70-130
07/23/2020 0940
Bromomethane (Methyl bromide)
50
60
1
120
70-130
07/23/2020 0940
2-Butanone (MEK)
100
110
1
113
60-140
07/23/2020 0940
Carbon disulfide
50
55
1
110
70-130
07/23/2020 0940
Carbon tetrachloride
50
58
1
115
70-130
07/23/2020 0940
Chlorobenzene
50
54
1
107
70-130
07/23/2020 0940
Chloroethane
50
61
1
122
70-130
07/23/2020 0940
Chloroform
50
56
1
111
70-130
07/23/2020 0940
Chloromethane (Methyl chloride)
50
58
1
116
60-140
07/23/2020 0940
Cyclohexane
50
56
1
112
70-130
07/23/2020 0940
1,2-Dibromo-3-chloropropane (DBCP)
50
53
1
105
70-130
07/23/2020 0940
Dibromochloromethane
50
53
1
106
70-130
07/23/2020 0940
1,2-Dibromoethane (EDB)
50
53
1
106
70-130
07/23/2020 0940
1,2-Dichlorobenzene
50
51
1
102
70-130
07/23/2020 0940
1,3-Dichlorobenzene
50
52
1
104
70-130
07/23/2020 0940
1,4-Dichlorobenzene
50
52
1
103
70-130
07/23/2020 0940
Dichlorodifluoromethane
50
67
1
133
60-140
07/23/2020 0940
1,1-Dichloroethane
50
56
1
111
70-130
07/23/2020 0940
1,2-Dichloroethane
50
55
1
110
70-130
07/23/2020 0940
1,1-Dichloroethene
50
57
1
115
70-130
07/23/2020 0940
cis- 1,2-Dichloroethene
50
58
1
117
70-130
07/23/2020 0940
trans- 1,2-Dichloroethene
50
58
1
116
70-130
07/23/2020 0940
1,2-Dichloropropane
50
49
1
97
70-130
07/23/2020 0940
cis- 1,3-Dichloropropene
50
51
1
102
70-130
07/23/2020 0940
trans- 1,3-Dichloropropene
50
54
1
108
70-130
07/23/2020 0940
Ethylbenzene
50
55
1
109
70-130
07/23/2020 0940
2-Hexanone
100
110
1
109
70-130
07/23/2020 0940
Isopropylbenzene
50
55
1
109
70-130
07/23/2020 0940
Methyl acetate
50
55
1
110
70-130
07/23/2020 0940
Methyl tertiary butyl ether (MTBE)
50
55
1
110
70-130
07/23/2020 0940
4-Methyl-2-pentanone
100
100
1
102
70-130
07/23/2020 0940
Methylcyclohexane
50
51
1
101
70-130
07/23/2020 0940
Methylene chloride
50
53
1
107
70-130
07/23/2020 0940
Styrene
50
54
1
107
70-130
07/23/2020 0940
1,1,2,2-Tetrachloroethane
50
52
1
104
70-130
07/23/2020 0940
Tetrachloroethene
50
60
1
119
70-130
07/23/2020 0940
Toluene
50
55
1
111
70-130
07/23/2020 0940
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
56
1
111
70-130
07/23/2020 0940
1,2,4-Trichlorobenzene
50
52
1
105
70-130
07/23/2020 0940
1,1,1-Trichloroethane
50
58
1
117
70-130
07/23/2020 0940
1,1,2-Trichloroethane
50
56
1
111
70-130
07/23/2020 0940
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 46

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ61025-002
Matrix:
Solid
Batch: 61025
Prep Method:
5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
50
57
1
114
70-130
07/23/2020 0940
Trichlorofluoromethane
50
61
1
122
70-130
07/23/2020 0940
Vinyl chloride
50
61
1
123
70-130
07/23/2020 0940
Xylenes (total)
100
110
1
109
70-130
07/23/2020 0940
Acceptance
Surrogate
Q % Rec
Limit
Bromofluorobenzene 113 47-138
1,2-Dichloroethane-d4 116 53-142
Toluene-d8 119 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 46

Volatile Organic Compounds by GC/MS - LCSD
Sample ID: VQ61025-003
Matrix: Solid
Batch: 61025
Prep
Method: 5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec % RPD
Limit
Limit
Analysis Date
Acetone
100
73
1
73
18
60-140
20
07/23/2020 1928
Benzene
50
51
1
101
9.3
70-130
20
07/23/2020 1928
Bromodichloromethane
50
51
1
102
5.3
70-130
20
07/23/2020 1928
Bromoform
50
52
1
104
3.0
70-130
20
07/23/2020 1928
Bromomethane (Methyl bromide)
50
53
1
106
12
70-130
20
07/23/2020 1928
2-Butanone (MEK)
100
95
1
95
18
60-140
20
07/23/2020 1928
Carbon disulfide
50
45
1
91
19
70-130
20
07/23/2020 1928
Carbon tetrachloride
50
53
1
106
8.1
70-130
20
07/23/2020 1928
Chlorobenzene
50
52
1
104
2.8
70-130
20
07/23/2020 1928
Chloroethane
50
50
1
101
20
70-130
20
07/23/2020 1928
Chloroform
50
52
1
103
7.4
70-130
20
07/23/2020 1928
Chloromethane (Methyl chloride)
50
38 +
1
75
43
60-140
20
07/23/2020 1928
Cyclohexane
50
44 +
1
87
24
70-130
20
07/23/2020 1928
1,2-Dibromo-3-chloropropane (DBCP)
50
44
1
89
17
70-130
20
07/23/2020 1928
Dibromochloromethane
50
50
1
101
4.5
70-130
20
07/23/2020 1928
1,2-Dibromoethane (EDB)
50
49
1
98
7.7
70-130
20
07/23/2020 1928
1,2-Dichlorobenzene
50
50
1
101
1.5
70-130
20
07/23/2020 1928
1,3-Dichlorobenzene
50
51
1
101
2.3
70-130
20
07/23/2020 1928
1,4-Dichlorobenzene
50
51
1
103
0.68
70-130
20
07/23/2020 1928
Dichlorodifluoromethane
50
53 +
1
105
24
60-140
20
07/23/2020 1928
1,1-Dichloroethane
50
47
1
93
18
70-130
20
07/23/2020 1928
1,2-Dichloroethane
50
56
1
112
2.2
70-130
20
07/23/2020 1928
1,1-Dichloroethene
50
50
1
99
15
70-130
20
07/23/2020 1928
cis- 1,2-Dichloroethene
50
50
1
99
16
70-130
20
07/23/2020 1928
trans- 1,2-Dichloroethene
50
52
1
103
11
70-130
20
07/23/2020 1928
1,2-Dichloropropane
50
48
1
96
1.3
70-130
20
07/23/2020 1928
cis- 1,3-Dichloropropene
50
49
1
99
2.7
70-130
20
07/23/2020 1928
trans- 1,3-Dichloropropene
50
48
1
96
11
70-130
20
07/23/2020 1928
Ethylbenzene
50
52
1
104
4.3
70-130
20
07/23/2020 1928
2-Hexanone
100
90
1
90
18
70-130
20
07/23/2020 1928
Isopropylbenzene
50
48
1
96
13
70-130
20
07/23/2020 1928
Methyl acetate
50
46
1
92
19
70-130
20
07/23/2020 1928
Methyl tertiary butyl ether (MTBE)
50
49
1
97
13
70-130
20
07/23/2020 1928
4-Methyl-2-pentanone
100
99
1
99
2.8
70-130
20
07/23/2020 1928
Methylcyclohexane
50
46
1
93
8.4
70-130
20
07/23/2020 1928
Methylene chloride
50
46
1
93
14
70-130
20
07/23/2020 1928
Styrene
50
53
1
106
1.4
70-130
20
07/23/2020 1928
1,1,2,2-Tetrachloroethane
50
44
1
88
16
70-130
20
07/23/2020 1928
Tetrachloroethene
50
50
1
101
17
70-130
20
07/23/2020 1928
Toluene
50
53
1
106
4.9
70-130
20
07/23/2020 1928
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
47
1
95
16
70-130
20
07/23/2020 1928
1,2,4-Trichlorobenzene
50
46
1
91
13
70-130
20
07/23/2020 1928
1,1,1-Trichloroethane
50
53
1
106
9.7
70-130
20
07/23/2020 1928
1,1,2-Trichloroethane
50
48
1
95
15
70-130
20
07/23/2020 1928
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 46

Volatile Organic Compounds by GC/MS - LCSD
Sample ID: VQ61025-003
Matrix: Solid
Batch: 61025
Prep
Method: 5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec % RPD
Limit
Limit
Analysis Date
Trichloroethene
50
52
1
103
9.3
70-130
20
07/23/2020 1928
Trichlorofluoromethane
50
52
1
104
16
70-130
20
07/23/2020 1928
Vinyl chloride
50
42 +
1
85
37
70-130
20
07/23/2020 1928
Xylenes (total)
100
100
1
105
4.4
70-130
20
07/23/2020 1928
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 106 47-138
1,2-Dichloroethane-d4 108 53-142
Toluene-d8 109 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 46

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ61221-001 Matrix: Solid
Batch:61221 Prep Method: 5035
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
8.0
ug/kg
07/24/2020 2231
Benzene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Bromodichloromethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Bromoform
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Bromomethane (Methyl bromide)
ND
1
5.0
3.0
ug/kg
07/24/2020 2231
2-Butanone (MEK)
ND
1
20
4.0
ug/kg
07/24/2020 2231
Carbon disulfide
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Carbon tetrachloride
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Chlorobenzene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Chloroethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Chloroform
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Chloromethane (Methyl chloride)
ND
1
5.0
3.0
ug/kg
07/24/2020 2231
Cyclohexane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Dibromochloromethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,2-Dibromoethane (EDB)
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,2-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,3-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,4-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Dichlorodifluoromethane
ND
1
5.0
3.0
ug/kg
07/24/2020 2231
1,1-Dichloroethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,2-Dichloroethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,1-Dichloroethene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
cis- 1,2-Dichloroethene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
trans- 1,2-Dichloroethene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,2-Dichloropropane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
cis- 1,3-Dichloropropene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
trans- 1,3-Dichloropropene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Ethylbenzene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
2-Hexanone
ND
1
10
4.0
ug/kg
07/24/2020 2231
Isopropylbenzene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Methyl acetate
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Methyl tertiary butyl ether (MTBE)
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
4-Methyl-2-pentanone
ND
1
10
4.0
ug/kg
07/24/2020 2231
Methylcyclohexane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Methylene chloride
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Styrene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,1,2,2-Tetrachloroethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Tetrachloroethene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Toluene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,2,4-Trichlorobenzene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,1,1-Trichloroethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
1,1,2-Trichloroethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 46

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ61221-001 Matrix: Solid
Batch:61221 Prep Method: 5035
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Trichloroethene
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Trichlorofluoromethane
ND
1
5.0
2.0
ug/kg
07/24/2020 2231
Vinyl chloride
ND
1
5.0
3.0
ug/kg
07/24/2020 2231
Xylenes (total)
ND
1
10
4.0
ug/kg
07/24/2020 2231
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 111 47-138
1,2-Dichloroethane-d4 84 53-142
Toluene-d8 101 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 46

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ61221-002
Matrix:
Solid
Batch:61221
Prep Method:
5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
120
1
125
60-140
07/24/2020 2132
Benzene
50
53
1
105
70-130
07/24/2020 2132
Bromodichloromethane
50
50
1
100
70-130
07/24/2020 2132
Bromoform
50
53
1
106
70-130
07/24/2020 2132
Bromomethane (Methyl bromide)
50
42
1
84
70-130
07/24/2020 2132
2-Butanone (MEK)
100
120
1
119
60-140
07/24/2020 2132
Carbon disulfide
50
51
1
102
70-130
07/24/2020 2132
Carbon tetrachloride
50
52
1
103
70-130
07/24/2020 2132
Chlorobenzene
50
55
1
110
70-130
07/24/2020 2132
Chloroethane
50
43
1
86
70-130
07/24/2020 2132
Chloroform
50
49
1
98
70-130
07/24/2020 2132
Chloromethane (Methyl chloride)
50
41
1
83
60-140
07/24/2020 2132
Cyclohexane
50
46
1
91
70-130
07/24/2020 2132
1,2-Dibromo-3-chloropropane (DBCP)
50
45
1
91
70-130
07/24/2020 2132
Dibromochloromethane
50
53
1
106
70-130
07/24/2020 2132
1,2-Dibromoethane (EDB)
50
53
1
105
70-130
07/24/2020 2132
1,2-Dichlorobenzene
50
55
1
110
70-130
07/24/2020 2132
1,3-Dichlorobenzene
50
55
1
110
70-130
07/24/2020 2132
1,4-Dichlorobenzene
50
55
1
110
70-130
07/24/2020 2132
Dichlorodifluoromethane
50
47
1
94
60-140
07/24/2020 2132
1,1-Dichloroethane
50
49
1
98
70-130
07/24/2020 2132
1,2-Dichloroethane
50
49
1
97
70-130
07/24/2020 2132
1,1-Dichloroethene
50
52
1
105
70-130
07/24/2020 2132
cis- 1,2-Dichloroethene
50
51
1
102
70-130
07/24/2020 2132
trans- 1,2-Dichloroethene
50
52
1
105
70-130
07/24/2020 2132
1,2-Dichloropropane
50
50
1
100
70-130
07/24/2020 2132
cis- 1,3-Dichloropropene
50
51
1
102
70-130
07/24/2020 2132
trans- 1,3-Dichloropropene
50
51
1
101
70-130
07/24/2020 2132
Ethylbenzene
50
56
1
111
70-130
07/24/2020 2132
2-Hexanone
100
110
1
107
70-130
07/24/2020 2132
Isopropylbenzene
50
55
1
110
70-130
07/24/2020 2132
Methyl acetate
50
44
1
87
70-130
07/24/2020 2132
Methyl tertiary butyl ether (MTBE)
50
48
1
97
70-130
07/24/2020 2132
4-Methyl-2-pentanone
100
91
1
91
70-130
07/24/2020 2132
Methylcyclohexane
50
54
1
108
70-130
07/24/2020 2132
Methylene chloride
50
46
1
91
70-130
07/24/2020 2132
Styrene
50
54
1
108
70-130
07/24/2020 2132
1,1,2,2-Tetrachloroethane
50
48
1
97
70-130
07/24/2020 2132
Tetrachloroethene
50
60
1
120
70-130
07/24/2020 2132
Toluene
50
54
1
108
70-130
07/24/2020 2132
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
53
1
105
70-130
07/24/2020 2132
1,2,4-Trichlorobenzene
50
57
1
115
70-130
07/24/2020 2132
1,1,1-Trichloroethane
50
51
1
101
70-130
07/24/2020 2132
1,1,2-Trichloroethane
50
52
1
105
70-130
07/24/2020 2132
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 46

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ61221-002
Matrix:
Solid
Batch:61221
Prep Method:
5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
50
57
1
114
70-130
07/24/2020 2132
Trichlorofluoromethane
50
45
1
91
70-130
07/24/2020 2132
Vinyl chloride
50
45
1
89
70-130
07/24/2020 2132
Xylenes (total)
100
110
1
110
70-130
07/24/2020 2132
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 111 47-138
1,2-Dichloroethane-d4 92 53-142
Toluene-d8 105 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 46

Volatile Organic Compounds by GC/MS - LCSD
Sample ID: VQ61221-003
Matrix: Solid
Batch:61221
Prep
Method: 5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec % RPD
Limit
Limit
Analysis Date
Acetone
100
120
1
122
2.0
60-140
20
07/24/2020 2155
Benzene
50
52
1
105
0.33
70-130
20
07/24/2020 2155
Bromodichloromethane
50
51
1
101
1.3
70-130
20
07/24/2020 2155
Bromoform
50
54
1
108
1.8
70-130
20
07/24/2020 2155
Bromomethane (Methyl bromide)
50
44
1
89
5.3
70-130
20
07/24/2020 2155
2-Butanone (MEK)
100
120
1
118
0.49
60-140
20
07/24/2020 2155
Carbon disulfide
50
50
1
100
1.1
70-130
20
07/24/2020 2155
Carbon tetrachloride
50
52
1
105
1.6
70-130
20
07/24/2020 2155
Chlorobenzene
50
55
1
110
0.34
70-130
20
07/24/2020 2155
Chloroethane
50
42
1
84
2.2
70-130
20
07/24/2020 2155
Chloroform
50
49
1
99
0.35
70-130
20
07/24/2020 2155
Chloromethane (Methyl chloride)
50
40
1
80
3.9
60-140
20
07/24/2020 2155
Cyclohexane
50
45
1
91
0.56
70-130
20
07/24/2020 2155
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
94
3.0
70-130
20
07/24/2020 2155
Dibromochloromethane
50
53
1
106
0.50
70-130
20
07/24/2020 2155
1,2-Dibromoethane (EDB)
50
53
1
106
0.52
70-130
20
07/24/2020 2155
1,2-Dichlorobenzene
50
55
1
110
0.11
70-130
20
07/24/2020 2155
1,3-Dichlorobenzene
50
55
1
110
0.069
70-130
20
07/24/2020 2155
1,4-Dichlorobenzene
50
55
1
110
0.11
70-130
20
07/24/2020 2155
Dichlorodifluoromethane
50
45
1
91
3.2
60-140
20
07/24/2020 2155
1,1-Dichloroethane
50
49
1
97
0.39
70-130
20
07/24/2020 2155
1,2-Dichloroethane
50
48
1
97
0.52
70-130
20
07/24/2020 2155
1,1-Dichloroethene
50
52
1
104
0.42
70-130
20
07/24/2020 2155
cis- 1,2-Dichloroethene
50
51
1
102
0.46
70-130
20
07/24/2020 2155
trans- 1,2-Dichloroethene
50
53
1
105
0.59
70-130
20
07/24/2020 2155
1,2-Dichloropropane
50
50
1
100
0.59
70-130
20
07/24/2020 2155
cis- 1,3-Dichloropropene
50
51
1
102
0.54
70-130
20
07/24/2020 2155
trans- 1,3-Dichloropropene
50
51
1
102
0.50
70-130
20
07/24/2020 2155
Ethylbenzene
50
55
1
110
1.3
70-130
20
07/24/2020 2155
2-Hexanone
100
110
1
107
0.40
70-130
20
07/24/2020 2155
Isopropylbenzene
50
54
1
109
0.84
70-130
20
07/24/2020 2155
Methyl acetate
50
44
1
89
1.8
70-130
20
07/24/2020 2155
Methyl tertiary butyl ether (MTBE)
50
48
1
96
0.31
70-130
20
07/24/2020 2155
4-Methyl-2-pentanone
100
94
1
94
2.3
70-130
20
07/24/2020 2155
Methylcyclohexane
50
54
1
108
0.48
70-130
20
07/24/2020 2155
Methylene chloride
50
46
1
92
0.50
70-130
20
07/24/2020 2155
Styrene
50
53
1
107
0.77
70-130
20
07/24/2020 2155
1,1,2,2-Tetrachloroethane
50
49
1
97
0.59
70-130
20
07/24/2020 2155
Tetrachloroethene
50
59
1
118
2.0
70-130
20
07/24/2020 2155
Toluene
50
53
1
107
1.2
70-130
20
07/24/2020 2155
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
52
1
103
2.1
70-130
20
07/24/2020 2155
1,2,4-Trichlorobenzene
50
58
1
116
0.90
70-130
20
07/24/2020 2155
1,1,1-Trichloroethane
50
51
1
101
0.052
70-130
20
07/24/2020 2155
1,1,2-Trichloroethane
50
53
1
105
0.60
70-130
20
07/24/2020 2155
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 46

Volatile Organic Compounds by GC/MS - LCSD
Sample ID: VQ61221-003
Matrix: Solid
Batch:61221
Prep
Method: 5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec % RPD
Limit
Limit
Analysis Date
Trichloroethene
50
57
1
113
0.61
70-130
20
07/24/2020 2155
Trichlorofluoromethane
50
45
1
91
0.13
70-130
20
07/24/2020 2155
Vinyl chloride
50
43
1
87
3.0
70-130
20
07/24/2020 2155
Xylenes (total)
100
110
1
108
1.6
70-130
20
07/24/2020 2155
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 109 47-138
1,2-Dichloroethane-d4 93 53-142
Toluene-d8 103 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 46

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ60855-001 Matrix: Solid
Batch: 60855 Prep Method: 3546
Analytical Method: 8270E Prep Date: 07/22/2020 1102
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
2.7
0.83
ug/kg
07/25/2020 1225
Acenaphthylene
ND
1
2.7
0.95
ug/kg
07/25/2020 1225
Acetophenone
ND
1
13
5.0
ug/kg
07/25/2020 1225
Anthracene
ND
1
2.7
0.51
ug/kg
07/25/2020 1225
Atrazine
ND
1
13
5.0
ug/kg
07/25/2020 1225
Benzaldehyde
ND
1
13
5.0
ug/kg
07/25/2020 1225
Benzo(a)anthracene
ND
1
2.7
0.59
ug/kg
07/25/2020 1225
Benzo(a)pyrene
ND
1
2.7
0.66
ug/kg
07/25/2020 1225
Benzo(k)fluoranthene
ND
1
2.7
0.50
ug/kg
07/25/2020 1225
Benzo(g,h,i)perylene
ND
1
2.7
0.65
ug/kg
07/25/2020 1225
Benzo(k)fluoranthene
ND
1
2.7
0.48
ug/kg
07/25/2020 1225
1,1'-Biphenyl
ND
1
13
5.0
ug/kg
07/25/2020 1225
4-Bromophenyl phenyl ether
ND
1
13
5.0
ug/kg
07/25/2020 1225
Butyl benzyl phthalate
ND
1
13
5.0
ug/kg
07/25/2020 1225
Caprolactam
ND
1
13
5.0
ug/kg
07/25/2020 1225
Carbazole
ND
1
13
5.0
ug/kg
07/25/2020 1225
bis (2-Chloro-1-methylethyl) ether
ND
1
13
5.0
ug/kg
07/25/2020 1225
4-Chloro-3-methyl phenol
ND
1
13
5.0
ug/kg
07/25/2020 1225
4-Chloroaniline
ND
1
13
5.0
ug/kg
07/25/2020 1225
bis(2-Chloroethoxy)methane
ND
1
13
5.0
ug/kg
07/25/2020 1225
bis(2-Chloroethyl)ether
ND
1
13
5.0
ug/kg
07/25/2020 1225
2-Chloronaphthalene
ND
1
13
5.0
ug/kg
07/25/2020 1225
2-Chlorophenol
ND
1
13
5.0
ug/kg
07/25/2020 1225
4-Chlorophenyl phenyl ether
ND
1
13
5.0
ug/kg
07/25/2020 1225
Chrysene
ND
1
2.7
0.45
ug/kg
07/25/2020 1225
Dibenzo(a,h)anthracene
ND
1
2.7
0.51
ug/kg
07/25/2020 1225
Dibenzofuran
ND
1
13
5.0
ug/kg
07/25/2020 1225
3,3'-Dichlorobenzidine
ND
1
13
5.0
ug/kg
07/25/2020 1225
2,4-Dichlorophenol
ND
1
13
5.0
ug/kg
07/25/2020 1225
Diethylphthalate
ND
1
13
5.0
ug/kg
07/25/2020 1225
Dimethyl phthalate
ND
1
13
7.4
ug/kg
07/25/2020 1225
2,4-Dimethylphenol
ND
1
13
5.0
ug/kg
07/25/2020 1225
Di-n-butyl phthalate
7.3 J
1
13
5.0
ug/kg
07/25/2020 1225
4,6-Dinitro-2-methyl phenol
ND
1
67
25
ug/kg
07/25/2020 1225
2,4-Dinitrophenol
ND
1
67
25
ug/kg
07/25/2020 1225
2,4-Dinitrotoluene
ND
1
27
10
ug/kg
07/25/2020 1225
2,6-Dinitrotoluene
ND
1
27
10
ug/kg
07/25/2020 1225
Di-n-octylphthalate
ND
1
13
5.0
ug/kg
07/25/2020 1225
bis(2-Ethylhexyl)phthalate
ND
1
67
25
ug/kg
07/25/2020 1225
Fluoranthene
ND
1
2.7
0.42
ug/kg
07/25/2020 1225
Fluorene
ND
1
2.7
0.57
ug/kg
07/25/2020 1225
Hexachlorobenzene
ND
1
13
5.0
ug/kg
07/25/2020 1225
Hexachlorobutadiene
ND
1
13
5.0
ug/kg
07/25/2020 1225
Hexachlorocyclopentadiene
ND
1
67
25
ug/kg
07/25/2020 1225
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 46

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ60855-001 Matrix: Solid
Batch: 60855 Prep Method: 3546
Analytical Method: 8270E Prep Date: 07/22/2020 1102
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Hexachloroethane
ND
1
13
5.0
ug/kg
07/25/20201225
Indeno(1,2,3-c,d)pyrene
ND
1
2.7
1.0
ug/kg
07/25/20201225
Isophorone
ND
1
13
5.0
ug/kg
07/25/20201225
2-Methyl naphthalene
ND
1
2.7
0.99
ug/kg
07/25/20201225
2-Methylphenol
ND
1
13
5.0
ug/kg
07/25/20201225
3+4-Methylphenol
ND
1
27
10
ug/kg
07/25/20201225
Naphthalene
ND
1
2.7
0.97
ug/kg
07/25/20201225
2-Nitroaniline
ND
1
27
10
ug/kg
07/25/20201225
3-Nitroaniline
ND
1
27
10
ug/kg
07/25/20201225
4-Nitroaniline
ND
1
27
10
ug/kg
07/25/20201225
Nitrobenzene
ND
1
13
5.0
ug/kg
07/25/20201225
2-Nitrophenol
ND
1
27
10
ug/kg
07/25/20201225
4-Nitrophenol
ND
1
67
25
ug/kg
07/25/20201225
N-Nitrosodi-n-propylamine
ND
1
13
5.0
ug/kg
07/25/20201225
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
13
5.0
ug/kg
07/25/2020 1225
Pentachlorophenol
ND
1
67
25
ug/kg
07/25/20201225
Phenanthrene
ND
1
2.7
0.72
ug/kg
07/25/20201225
Phenol
ND
1
13
5.0
ug/kg
07/25/20201225
Pyrene
ND
1
2.7
0.50
ug/kg
07/25/20201225
Pyridine
ND
1
13
5.0
ug/kg
07/25/20201225
2,4,5-Trichlorophenol
ND
1
13
5.0
ug/kg
07/25/20201225
2,4,6-Trichlorophenol
ND
1
13
5.0
ug/kg
07/25/20201225
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
90
33-102
2-Fluorophenol
95
35-115
Nitrobenzene-d5
93
22-109
Phenol-d5 122 33-122
Terphenyl-d14 114 41-120
2,4,6-Tribromophenol 88 30-117
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 46

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ60855-002
Matrix:
Solid
Batch: 60855
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 07/22/2020 1102
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q
Dil
% Rec
Limit
Analysis Date
Acenaphthene
130
110
1
84
12-111
07/25/2020 1250
Acenaphthylene
130
120
1
90
44-122
07/25/2020 1250
Acetophenone
130
110
1
86
48-111
07/25/2020 1250
Anthracene
130
120
1
91
16-122
07/25/2020 1250
Atrazine
130
140
1
102
48-116
07/25/2020 1250
Benzaldehyde
130
81
1
61
10-110
07/25/2020 1250
Benzo(a)anthracene
130
130
1
100
40-121
07/25/2020 1250
Benzo(a)pyrene
130
130
1
98
36-114
07/25/2020 1250
Benzo(k)fluoranthene
130
130
1
96
38-123
07/25/2020 1250
Benzo(g,h,i)perylene
130
130
1
97
43-120
07/25/2020 1250
Benzo(k)fluoranthene
130
130
1
98
40-126
07/25/2020 1250
1,1'-Biphenyl
130
110
1
83
49-110
07/25/2020 1250
4-Bromophenyl phenyl ether
130
110
1
83
46-118
07/25/2020 1250
Butyl benzyl phthalate
130
270
N
1
200
46-128
07/25/2020 1250
Caprolactam
130
150
1
112
43-121
07/25/2020 1250
Carbazole
130
130
1
98
47-128
07/25/2020 1250
bis (2-Chloro-1-methylethyl) ether
130
180
N
1
139
31-102
07/25/2020 1250
4-Chloro-3-methyl phenol
130
140
1
103
49-118
07/25/2020 1250
4-Chloroaniline
130
54
1
41
17-106
07/25/2020 1250
bis(2-Chloroethoxy)methane
130
120
1
91
39-108
07/25/2020 1250
bis(2-Chloroethyl)ether
130
140
N
1
107
32-105
07/25/2020 1250
2-Chloronaphthalene
130
110
1
84
31-127
07/25/2020 1250
2-Chlorophenol
130
120
1
93
37-106
07/25/2020 1250
4-Chlorophenyl phenyl ether
130
110
1
85
47-116
07/25/2020 1250
Chrysene
130
130
1
97
41-124
07/25/2020 1250
Dibenzo(a,h)anthracene
130
130
1
95
38-125
07/25/2020 1250
Dibenzofuran
130
120
1
87
45-112
07/25/2020 1250
3,3'-Dichlorobenzidine
130
150
1
109
10-119
07/25/2020 1250
2,4-Dichlorophenol
130
120
1
89
41-113
07/25/2020 1250
Diethylphthalate
130
140
1
105
49-123
07/25/2020 1250
Dimethyl phthalate
130
130
1
98
48-120
07/25/2020 1250
2,4-Dimethylphenol
130
160
1
122
33-123
07/25/2020 1250
Di-n-butyl phthalate
130
140
1
106
51-129
07/25/2020 1250
4,6-Dinitro-2-methyl phenol
130
95
1
71
40-130
07/25/2020 1250
2,4-Dinitrophenol
270
160
1
59
32-115
07/25/2020 1250
2,4-Dinitrotoluene
130
140
1
102
48-124
07/25/2020 1250
2,6-Dinitrotoluene
130
120
1
94
47-125
07/25/2020 1250
Di-n-octylphthalate
130
140
1
104
49-142
07/25/2020 1250
bis(2-Ethylhexyl)phthalate
130
150
1
116
45-128
07/25/2020 1250
Fluoranthene
130
120
1
91
26-133
07/25/2020 1250
Fluorene
130
120
1
90
19-108
07/25/2020 1250
Hexachlorobenzene
130
110
1
84
44-122
07/25/2020 1250
Hexachlorobutadiene
130
100
1
78
33-103
07/25/2020 1250
Hexachlorocyclopentadiene
670
380
1
56
18-121
07/25/2020 1250
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 30 of 46

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ60855-002
Matrix:
Solid
Batch: 60855
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 07/22/2020 1102
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Hexachloroethane
130
120
1
89
30-96
07/25/20201250
Indeno(1,2,3-c,d)pyrene
130
130
1
98
42-123
07/25/20201250
Isophorone
130
140
1
106
41-113
07/25/20201250
2-Methyl naphthalene
130
110
1
86
10-107
07/25/20201250
2-Methylphenol
130
120
1
92
32-107
07/25/20201250
3+4-Methylphenol
130
150
N 1
115
39-108
07/25/20201250
Naphthalene
130
110
1
80
10-112
07/25/20201250
2-Nitroaniline
130
140
1
107
45-123
07/25/20201250
3-Nitroaniline
130
110
1
81
24-127
07/25/20201250
4-Nitroaniline
130
160
1
117
48-127
07/25/20201250
Nitrobenzene
130
130
1
101
33-114
07/25/20201250
2-Nitrophenol
130
120
1
93
35-108
07/25/20201250
4-Nitrophenol
270
190
1
73
18-154
07/25/20201250
N-Nitrosodi-n-propylamine
130
140
1
107
32-115
07/25/20201250
N-Nitrosodiphenylamine (Diphenylamine) 130
130
1
100
53-150
07/25/2020 1250
Pentachlorophenol
270
150
1
56
27-138
07/25/20201250
Phenanthrene
130
120
1
87
16-123
07/25/20201250
Phenol
130
130
1
95
36-108
07/25/20201250
Pyrene
130
140
1
103
34-121
07/25/20201250
Pyridine
130
100
1
77
30-130
07/25/20201250
2,4,5-Trichlorophenol
130
120
1
92
46-122
07/25/20201250
2,4,6-Trichlorophenol
130
110
1
85
38-115
07/25/20201250
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
78
33-102
2-Fluorophenol
77
35-115
Nitrobenzene-d5
93
22-109
Phenol-d5 102 33-122
Terphenyl-d14 100 41-120
2,4,6-Tribromophenol 75 30-117
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 31 of 46

MA EPH (aliphatics) - MB
Sample ID: VQ61231-001 Matrix: Solid
Batch: 61231 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 07/25/2020 1009
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics ND 1 10 10 mg/kg 07/29/2020 1130
C19 - C36 Aliphatics ND 1 10 10 mg/kg 07/29/2020 1130
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 68 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 32 of 46

MA EPH (aliphatics) - LCS
Sample ID: VQ61231-002
Matrix: Solid
Batch: 61231
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 07/25/2020 1009
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg)
Q Dil % Rec
Limit Analysis Date
C9 - C18 Aliphatics
30
21
1 71
40-140 07/29/2020 1200
C19 - C36 Aliphatics
40
36
1 90
40-140 07/29/2020 1200
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 53 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 33 of 46

MA EPH (aliphatics) - LCSD
Sample ID: VQ61231-003
Matrix: Solid
Batch: 61231
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 07/25/2020 1009
Spike
Amount
Result
% Rec
% RPD
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
30
22
1 73 2.4 40-140
25 07/29/2020 1231
C19 - C36 Aliphatics
40
35
1 88 2.0 40-140
25 07/29/2020 1231
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 67 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 34 of 46

MA EPH (aromatics) - MB
Sample ID: VQ61232-001 Matrix: Solid
Batch: 61232 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 07/25/2020 1009
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 10 10 mg/kg 07/29/2020 1503
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 76 40-140
2-Fluorobiphenyl (fractionation 1) 70 40-140
o - Terphenyl (aromatic) 64 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 35 of 46

MA EPH (aromatics) - LCS
Sample ID: VQ61232-002
Matrix: Solid
Batch: 61232
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 07/25/2020 1009
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
85
56
1 66 40-140 07/29/2020 1533
Surrogate
Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2) 84 40-140
2-Fluorobiphenyl (fractionation 1) 83 40-140
o - Terphenyl (aromatic) 75 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 36 of 46

MA EPH (aromatics) - LCSD
Sample ID: VQ61232-003 Matrix: Solid
Batch: 61232 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 07/25/2020 1009
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 85 64 1 75 12 40-140 25 07/29/2020 1603
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 95 40-140
2-Fluorobiphenyl (fractionation 1) 89 40-140
o - Terphenyl (aromatic) 81 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 37 of 46

MADEP VPH (aliphatics) - MB
Sample ID: VQ60720-001 Matrix: Solid
Batch: 60720 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C5 - C8 Aliphatics ND 1 3.8 0.75 mg/kg 07/21/2020 1204
C9 - C12 Aliphatics ND 1 3.8 0.75 mg/kg 07/21/2020 1204
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
113 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 38 of 46

MADEP VPH (aliphatics) - LCS
Sample ID: VQ60720-002 Matrix: Solid
Batch: 60720 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg) Q Dil
% Rec Limit Analysis Date
C5 - C8 Aliphatics
7.5
8.4 1
112 70-130 07/21/2020 1106
C9 - C12 Aliphatics
8.8
10 1
114 70-130 07/21/2020 1106
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
115 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 39 of 46

MADEP VPH (aliphatics) - LCSD
Sample ID: VQ60720-003 Matrix: Solid
Batch: 60720 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
% RPD
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C5 - C8 Aliphatics
7.5
7.8
1 104 7.3 70-130
25 07/21/2020 1135
C9 - C12 Aliphatics
8.8
9.7
1 ill 3.0 70-130
25 07/21/2020 1135
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
112 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 40 of 46

MADEP VPH (aromatics) - MB
Sample ID: VQ60722-001 Matrix: Solid
Batch: 60722 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C10 Aromatics ND 1 1.3 0.50 mg/kg 07/21/2020 1204
Surrogate
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
117 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 46

MADEP VPH (aromatics) - LCS
Sample ID: VQ60722-002 Matrix: Solid
Batch: 60722 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 1.3 1.4 1 112 70-130 07/21/2020 1106
Surrogate
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
117 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 42 of 46

MADEP VPH (aromatics) - LCSD
Sample ID: VQ60722-003 Matrix: Solid
Batch: 60722 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 1.3 1.4 1 112 0.00 70-130 25 07/21/2020 1135
Surrogate
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
117 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 43 of 46

Chain of Custody
and
Miscellaneous Documents
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Page 44 of 46

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 45 of 46

PACE ANALYTICAL SERVICES, LLC
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Page 46 of 46

0
aceAnalytical
Report of Analysis
SUMMIT Engineering, Laboratory & Testing, P.C.
3575 Centre Circle
Fort Mill, SC 28715
Attention: Patrick Lowery
Project Name: Vail Ave.
Project Number: 1820.E0004
Lot Number:VG29053
Date Completed:08/13/2020
08/14/2020 9:44 AM
Approved and released by:
Project Manager II: Lucas Odom
pCCgF�
24r�14A
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ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
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Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 73

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: VG29053
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
VOCs by GC/MS
The continuing calibration verification (CCV) associated with samples VG29053-001 and VG29053-004
recovered Vinyl chloride above the upper control limit. The sample associated with this CCV were non -
detect for the affected analytes; therefore, the data has been reported.
The method blank associated with batch 62263 yielded a "J" value detection for Carbon Disulfide. No
corrective action is required as this is an estimated value recovered below the LOQ. Associated samples
have been qualified with a "B".
SVOCs by GC/MS
The method blank associated with batch 61942 yielded a "J" value detection for four compounds. No
corrective action is required as this is an estimated value recovered below the LOQ. Associated samples
have been qualified with a "B".
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 73

PACE ANALYTICAL SERVICES, LLC
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: VG29053
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
SS-0
Solid
07/29/20201100
07/29/2020
002
SS-5
Solid
07/29/20201110
07/29/2020
003
SS-10
Solid
07/29/20201115
07/29/2020
004
SS-15
Solid
07/29/20201120
07/29/2020
005
GW-1
Aqueous
07/29/20201205
07/29/2020
(5 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 73

PACE ANALYTICAL SERVICES, LLC
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: VG29053
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
SS-0
Solid
Benzo(a)anthracene
8270E
17
ug/kg
6
001
SS-0
Solid
Benzo(a)pyrene
8270E
26
ug/kg
6
001
SS-0
Solid
Benzo(b)fluoranthene
8270E
30
ug/kg
6
001
SS-0
Solid
Benzo(g,h,i)perylene
8270E
11
J
ug/kg
6
001
SS-0
Solid
Benzo(k)fluoranthene
8270E
9.0
J
ug/kg
6
001
SS-0
Solid
Chrysene
8270E
12
J
ug/kg
7
001
SS-0
Solid
Fluoranthene
8270E
16
ug/kg
7
001
SS-0
Solid
Indeno(1,2,3-c,d)pyrene
8270E
9.8
J
ug/kg
7
001
SS-0
Solid
Pyrene
8270E
23
ug/kg
8
001
SS-0
Solid
C9 - C10 Aromatics
MADEP-VPH-
1.4
J
mg/kg
9
005
GW-1
Aqueous
Chloroform
8260D
0.97
J
ug/L
19
005
GW-1
Aqueous
Caprolactam
8270E
39
B
ug/L
20
005
GW-1
Aqueous
Diethylphthalate
8270E
1.7
BJ
ug/L
21
005
GW-1
Aqueous
Dimethyl phthalate
8270E
0.28
J
ug/L
21
005
GW-1
Aqueous
Di-n-butyl phthalate
8270E
0.45
J
ug/L
21
005
GW-1
Aqueous
bis(2-Ethylhexyl)phthalate
8270E
2.5
BJ
ug/L
21
(16 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-001
Description: SS-0 Matrix: Solid
Date Sampled:07/29/2020 1100 % Solids: 87.3 07/30/2020 0022
Date Received:07/29/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 08/03/20201520 JM1 62131 5.55
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
21
8.3
ug/kg
Benzene
71-43-2
8260D
ND
5.2
2.1
ug/kg
Bromodichloromethane
75-27-4
8260D
ND
5.2
2.1
ug/kg
Bromoform
75-25-2
8260D
ND
5.2
2.1
ug/kg
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
5.2
3.1
ug/kg
2-Butanone (MEK)
78-93-3
8260D
ND
21
4.1
ug/kg
Carbon disulfide
75-15-0
8260D
ND
5.2
2.1
ug/kg
Carbon tetrachloride
56-23-5
8260D
ND
5.2
2.1
ug/kg
Chlorobenzene
108-90-7
8260D
ND
5.2
2.1
ug/kg
Chloroethane
75-00-3
8260D
ND
5.2
2.1
ug/kg
Chloroform
67-66-3
8260D
ND
5.2
2.1
ug/kg
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
5.2
3.1
ug/kg
Cyclohexane
110-82-7
8260D
ND
5.2
2.1
ug/kg
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
5.2
2.1
ug/kg
Dibromochloromethane
124-48-1
8260D
ND
5.2
2.1
ug/kg
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
5.2
2.1
ug/kg
1,2-Dichlorobenzene
95-50-1
8260D
ND
5.2
2.1
ug/kg
1,3-Dichlorobenzene
541-73-1
8260D
ND
5.2
2.1
ug/kg
1,4-Dichlorobenzene
106-46-7
8260D
ND
5.2
2.1
ug/kg
Dichlorodifluoromethane
75-71-8
8260D
ND
5.2
3.1
ug/kg
1,1-Dichloroethane
75-34-3
8260D
ND
5.2
2.1
ug/kg
1,2-Dichloroethane
107-06-2
8260D
ND
5.2
2.1
ug/kg
1,1-Dichloroethene
75-35-4
8260D
ND
5.2
2.1
ug/kg
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
5.2
2.1
ug/kg
trans-1,2-Dichloroethene
156-60-5
8260D
ND
5.2
2.1
ug/kg
1,2-Dichloropropane
78-87-5
8260D
ND
5.2
2.1
ug/kg
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
5.2
2.1
ug/kg
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
5.2
2.1
ug/kg
Ethylbenzene
100-41-4
8260D
ND
5.2
2.1
ug/kg
2-Hexanone
591-78-6
8260D
ND
10
4.1
ug/kg
Isopropylbenzene
98-82-8
8260D
ND
5.2
2.1
ug/kg
Methyl acetate
79-20-9
8260D
ND
5.2
2.1
ug/kg
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
5.2
2.1
ug/kg
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
4.1
ug/kg
Methylcyclohexane
108-87-2
8260D
ND
5.2
2.1
ug/kg
Methylene chloride
75-09-2
8260D
ND
5.2
2.1
ug/kg
Styrene
100-42-5
8260D
ND
5.2
2.1
ug/kg
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
5.2
2.1
ug/kg
Tetrachloroethene
127-18-4
8260D
ND
5.2
2.1
ug/kg
Toluene
108-88-3
8260D
ND
5.2
2.1
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-001
Description: SS-0 Matrix: Solid
Date Sampled:07/29/2020 1100 % Solids: 87.3 07/30/2020 0022
Date Received:07/29/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
1 5035
8260D 1 08/03/20201520 JM1
62131
5.55
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D
ND
5.2
2.1
ug/kg
1
1,2,4-Trichlorobenzene
120-82-1 8260D
ND
5.2
2.1
ug/kg
1
1,1,1-Trichloroethane
71-55-6 8260D
ND
5.2
2.1
ug/kg
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
5.2
2.1
ug/kg
1
Trichloroethene
79-01-6 8260D
ND
5.2
2.1
ug/kg
1
Trichlorofluoromethane
75-69-4 8260D
ND
5.2
2.1
ug/kg
1
Vinyl chloride
75-01-4 8260D
ND
5.2
3.1
ug/kg
1
Xylenes (total)
1330-20-7 8260D
ND
10
4.1
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
112 47-138
1,2-Dichloroethane-d4
117 53-142
Toluene-d8
115 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E 5 08/07/2020 1941 SCD
07/30/2020 1900 61838
2 3546
8270E 5 08/08/2020 1530 SCD
08/07/2020 2039 62822
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9 8270E
ND
15
4.6
ug/kg
1
Acenaphthylene
208-96-8 8270E
ND
15
5.3
ug/kg
1
Acetophenone
98-86-2 8270E
ND
73
28
ug/kg
1
Anthracene
120-12-7 8270E
ND
15
2.9
ug/kg
1
Atrazine
1912-24-9 8270E
ND
73
28
ug/kg
1
Benzaldehyde
100-52-7 8270E
ND
73
28
ug/kg
1
Benzo(a)anthracene
56-55-3 8270E
17
15
3.3
ug/kg
1
Benzo(a)pyrene
50-32-8 8270E
26
15
3.7
ug/kg
1
Benzo(b)fluoranthene
205-99-2 8270E
30
15
2.8
ug/kg
1
Benzo(g,h,i)perylene
191-24-2 8270E
11 J
15
3.6
ug/kg
1
Benzo(k)fluoranthene
207-08-9 8270E
9.0 J
15
2.7
ug/kg
1
1,1'-Biphenyl
92-52-4 8270E
ND
73
28
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3 8270E
ND
73
28
ug/kg
1
Butyl benzyl phthalate
85-68-7 8270E
ND
73
28
ug/kg
1
Caprolactam
105-60-2 8270E
ND
73
28
ug/kg
1
Carbazole
86-74-8 8270E
ND
73
28
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1 8270E
ND
73
28
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7 8270E
ND
73
28
ug/kg
1
4-Chloroaniline
106-47-8 8270E
ND
73
28
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-001
Description: SS-0 Matrix: Solid
Date Sampled:07/29/2020 1100 % Solids: 87.3 07/30/2020 0022
Date Received:07/29/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 08/07/2020 1941 SCD 07/30/2020 1900 61838
2 3546 8270E 5 08/08/2020 1530 SCD 08/07/2020 2039 62822
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
73
28
ug/kg
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
73
28
ug/kg
2-Chloronaphthalene
91-58-7
8270E
ND
73
28
ug/kg
2-Chlorophenol
95-57-8
8270E
ND
73
28
ug/kg
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
73
28
ug/kg
Chrysene
218-01-9
8270E
12 J
15
2.5
ug/kg
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
15
2.9
ug/kg
Dibenzofuran
132-64-9
8270E
ND
73
28
ug/kg
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
73
28
ug/kg
2,4-Dichlorophenol
120-83-2
8270E
ND
73
28
ug/kg
Diethylphthalate
84-66-2
8270E
ND
73
28
ug/kg
Dimethyl phthalate
131-11-3
8270E
ND
73
41
ug/kg
2,4-Dimethylphenol
105-67-9
8270E
ND
73
28
ug/kg
Di-n-butyl phthalate
84-74-2
8270E
ND
73
28
ug/kg
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
380
140
ug/kg
2,4-Dinitrophenol
51-28-5
8270E
ND
380
140
ug/kg
2,4-Dinitrotoluene
121-14-2
8270E
ND
150
56
ug/kg
2,6-Dinitrotoluene
606-20-2
8270E
ND
150
56
ug/kg
Di-n-octylphthalate
117-84-0
8270E
ND
73
28
ug/kg
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
370
140
ug/kg
Fluoranthene
206-44-0
8270E
16
15
2.3
ug/kg
Fluorene
86-73-7
8270E
ND
15
3.2
ug/kg
Hexachlorobenzene
118-74-1
8270E
ND
73
28
ug/kg
Hexachlorobutadiene
87-68-3
8270E
ND
73
28
ug/kg
Hexachlorocyclopentadiene
77-47-4
8270E
ND
370
140
ug/kg
Hexachloroethane
67-72-1
8270E
ND
73
28
ug/kg
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
9.8 J
15
5.6
ug/kg
Isophorone
78-59-1
8270E
ND
73
28
ug/kg
2-Methylnaphthalene
91-57-6
8270E
ND
15
5.5
ug/kg
2-Methylphenol
95-48-7
8270E
ND
73
28
ug/kg
3+4-Methylphenol
106-44-5
8270E
ND
150
56
ug/kg
Naphthalene
91-20-3
8270E
ND
15
5.4
ug/kg
2-Nitroaniline
88-74-4
8270E
ND
150
56
ug/kg
3-Nitroaniline
99-09-2
8270E
ND
150
56
ug/kg
4-Nitroaniline
100-01-6
8270E
ND
150
56
ug/kg
Nitrobenzene
98-95-3
8270E
ND
73
28
ug/kg
2-Nitrophenol
88-75-5
8270E
ND
150
56
ug/kg
4-Nitrophenol
100-02-7
8270E
ND
370
140
ug/kg
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
73
28
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-001
Description: SS-0 Matrix: Solid
Date Sampled:07/29/2020 1100 % Solids: 87.3 07/30/2020 0022
Date Received:07/29/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E 5 08/07/2020 1941 SCD
07/30/2020 1900
61838
2 3546
8270E 5 08/08/2020 1530 SCD
08/07/2020 2039
62822
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E
ND
73
28
ug/kg
1
Pentachlorophenol
87-86-5 8270E
ND
370
140
ug/kg
1
Phenanthrene
85-01-8 8270E
ND
15
4.0
ug/kg
1
Phenol
108-95-2 8270E
ND
73
28
ug/kg
1
Pyrene
129-00-0 8270E
23
15
2.8
ug/kg
1
Pyridine
110-86-1 8270E
ND
73
28
ug/kg
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
73
28
ug/kg
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
73
28
ug/kg
1
Run 1 Acceptance Run
2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery
Limits
2-Fluorobiphenyl
65 33-102 70
33-102
2-Fluorophenol
55 35-115 66
35-115
Nitrobenzene-d5
64 22-109 59
22-109
Phenol-d5
63 33-122 72
33-122
Terphenyl-d14
70 41-120 81
41-120
2,4,6-Tribromophenol
54 30-117 59
30-117
MA EPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/12/2020 2019 JJG
08/03/2020 1348
62125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C11 - C22 Aromatics
MADEP-EPH-04
ND
11
11
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) 74 40-140
2-Fluorobiphenyl (fractionation 1)
71 40-140
o - Terphenyl (aromatic)
70 40-140
MA EPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/12/2020 1949 JJG
08/03/2020 1348
62124
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C9 - C18 Aliphatics
MADEP-EPH-04
ND
11
11
mg/kg
1
C19 - C36 Aliphatics
MADEP-EPH-04
ND
11
11
mg/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated
result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-001
Description: SS-0 Matrix: Solid
Date Sampled:07/29/2020 1100 % Solids: 87.3 07/30/2020 0022
Date Received:07/29/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
46 40-140
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201622 ECB
62147
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C5 - C8 Aliphatics
MADEP-VPH-18- ND
5.5
1.1
mg/kg
1
C9 - C12 Aliphatics
MADEP-VPH-18- ND
5.5
1.1
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
124 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201622 ECB
62150
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C9 - C10 Aromatics
MADEP-VPH-18- 1.4 J
1.8
0.73
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (PID)
125 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-002
Description: SS-5 Matrix: Solid
Date Sampled:07/29/2020 1110 % Solids: 87.2 07/30/2020 0022
Date Received:07/29/2020
MA EPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/08/2020 0100 JJG
08/03/2020 1348 62125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C11 - C22 Aromatics
MADEP-EPH-04
ND
11
11
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) 91 40-140
2-Fluorobiphenyl (fractionation 1)
87 40-140
o - Terphenyl (aromatic)
82 40-140
MA EPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/07/2020 2059 JJG
08/03/2020 1348 62124
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C9 - C18 Aliphatics
MADEP-EPH-04
ND
11
11
mg/kg
1
C19 - C36 Aliphatics
MADEP-EPH-04
ND
11
11
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
60 40-140
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201651 ECB
62147
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C5 - C8 Aliphatics
MADEP-VPH-18-
ND
4.0
0.81
mg/kg
1
C9 - C12 Aliphatics
MADEP-VPH-18-
ND
4.0
0.81
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
125 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201651 ECB
62150
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C9 - C10 Aromatics
MADEP-VPH-18-
ND
1.3
0.54
mg/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG29053-002
Description: SS-5 Matrix: Solid
Date Sampled:07/29/2020 1110 % Solids: 87.2 07/30/2020 0022
Date Received:07/29/2020
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID) 117 70-130
LOCI = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-003
Description: SS-10 Matrix: Solid
Date Sampled:07/29/2020 1115 % Solids: 86.1 07/30/2020 0022
Date Received:07/29/2020
MA EPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/08/2020 0130 JJG
08/03/2020 1348 62125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C11 - C22 Aromatics
MADEP-EPH-04
ND
11
11
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) 83 40-140
2-Fluorobiphenyl (fractionation 1)
81 40-140
o - Terphenyl (aromatic)
78 40-140
MA EPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/07/2020 2129 JJG
08/03/2020 1348 62124
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C9 - C18 Aliphatics
MADEP-EPH-04
ND
11
11
mg/kg
1
C19 - C36 Aliphatics
MADEP-EPH-04
ND
11
11
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
47 40-140
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201720 ECB
62147
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C5 - C8 Aliphatics
MADEP-VPH-18-
ND
4.0
0.79
mg/kg
1
C9 - C12 Aliphatics
MADEP-VPH-18-
ND
4.0
0.79
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
128 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201720 ECB
62150
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C9 - C10 Aromatics
MADEP-VPH-18-
ND
1.3
0.53
mg/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VG29053-003
Description: SS-10 Matrix: Solid
Date Sampled:07/29/2020 1115 % Solids: 86.1 07/30/2020 0022
Date Received:07/29/2020
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID) 127 70-130
LOCI = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-004
Description: SS-15 Matrix: Solid
Date Sampled:07/29/2020 1120 % Solids: 82.6 07/30/2020 0022
Date Received:07/29/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 08/03/20201544 JM1 62131 6.51
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
19
7.4
ug/kg
Benzene
71-43-2
8260D
ND
4.7
1.9
ug/kg
Bromodichloromethane
75-27-4
8260D
ND
4.7
1.9
ug/kg
Bromoform
75-25-2
8260D
ND
4.7
1.9
ug/kg
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
4.7
2.8
ug/kg
2-Butanone (MEK)
78-93-3
8260D
ND
19
3.7
ug/kg
Carbon disulfide
75-15-0
8260D
ND
4.7
1.9
ug/kg
Carbon tetrachloride
56-23-5
8260D
ND
4.7
1.9
ug/kg
Chlorobenzene
108-90-7
8260D
ND
4.7
1.9
ug/kg
Chloroethane
75-00-3
8260D
ND
4.7
1.9
ug/kg
Chloroform
67-66-3
8260D
ND
4.7
1.9
ug/kg
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
4.7
2.8
ug/kg
Cyclohexane
110-82-7
8260D
ND
4.7
1.9
ug/kg
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
4.7
1.9
ug/kg
Dibromochloromethane
124-48-1
8260D
ND
4.7
1.9
ug/kg
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
4.7
1.9
ug/kg
1,2-Dichlorobenzene
95-50-1
8260D
ND
4.7
1.9
ug/kg
1,3-Dichlorobenzene
541-73-1
8260D
ND
4.7
1.9
ug/kg
1,4-Dichlorobenzene
106-46-7
8260D
ND
4.7
1.9
ug/kg
Dichlorodifluoromethane
75-71-8
8260D
ND
4.7
2.8
ug/kg
1,1-Dichloroethane
75-34-3
8260D
ND
4.7
1.9
ug/kg
1,2-Dichloroethane
107-06-2
8260D
ND
4.7
1.9
ug/kg
1,1-Dichloroethene
75-35-4
8260D
ND
4.7
1.9
ug/kg
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
4.7
1.9
ug/kg
trans-1,2-Dichloroethene
156-60-5
8260D
ND
4.7
1.9
ug/kg
1,2-Dichloropropane
78-87-5
8260D
ND
4.7
1.9
ug/kg
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
4.7
1.9
ug/kg
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
4.7
1.9
ug/kg
Ethylbenzene
100-41-4
8260D
ND
4.7
1.9
ug/kg
2-Hexanone
591-78-6
8260D
ND
9.3
3.7
ug/kg
Isopropylbenzene
98-82-8
8260D
ND
4.7
1.9
ug/kg
Methyl acetate
79-20-9
8260D
ND
4.7
1.9
ug/kg
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
4.7
1.9
ug/kg
4-Methyl-2-pentanone
108-10-1
8260D
ND
9.3
3.7
ug/kg
Methylcyclohexane
108-87-2
8260D
ND
4.7
1.9
ug/kg
Methylene chloride
75-09-2
8260D
ND
4.7
1.9
ug/kg
Styrene
100-42-5
8260D
ND
4.7
1.9
ug/kg
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
4.7
1.9
ug/kg
Tetrachloroethene
127-18-4
8260D
ND
4.7
1.9
ug/kg
Toluene
108-88-3
8260D
ND
4.7
1.9
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-004
Description: SS-15 Matrix: Solid
Date Sampled:07/29/2020 1120 % Solids: 82.6 07/30/2020 0022
Date Received:07/29/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
1 5035
8260D 1 08/03/20201544 JM1
62131
6.51
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D
ND
4.7
1.9
ug/kg
1
1,2,4-Trichlorobenzene
120-82-1 8260D
ND
4.7
1.9
ug/kg
1
1,1,1-Trichloroethane
71-55-6 8260D
ND
4.7
1.9
ug/kg
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
4.7
1.9
ug/kg
1
Trichloroethene
79-01-6 8260D
ND
4.7
1.9
ug/kg
1
Trichlorofluoromethane
75-69-4 8260D
ND
4.7
1.9
ug/kg
1
Vinyl chloride
75-01-4 8260D
ND
4.7
2.8
ug/kg
1
Xylenes (total)
1330-20-7 8260D
ND
9.3
3.7
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
114 47-138
1,2-Dichloroethane-d4
116 53-142
Toluene-d8
117 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E 1 08/07/2020 1440 SCD
07/30/2020 1900 61838
2 3546
8270E 1 08/08/2020 1555 SCD
08/07/2020 2039 62822
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9 8270E
ND
3.1
0.97
ug/kg
1
Acenaphthylene
208-96-8 8270E
ND
3.1
1.1
ug/kg
1
Acetophenone
98-86-2 8270E
ND
15
5.8
ug/kg
1
Anthracene
120-12-7 8270E
ND
3.1
0.59
ug/kg
1
Atrazine
1912-24-9 8270E
ND
15
5.8
ug/kg
1
Benzaldehyde
100-52-7 8270E
ND
15
5.8
ug/kg
1
Benzo(a)anthracene
56-55-3 8270E
ND
3.1
0.69
ug/kg
1
Benzo(a)pyrene
50-32-8 8270E
ND
3.1
0.77
ug/kg
1
Benzo(b)fluoranthene
205-99-2 8270E
ND
3.1
0.58
ug/kg
1
Benzo(g,h,i)perylene
191-24-2 8270E
ND
3.1
0.76
ug/kg
1
Benzo(k)fluoranthene
207-08-9 8270E
ND
3.1
0.56
ug/kg
1
1,1'-Biphenyl
92-52-4 8270E
ND
15
5.8
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3 8270E
ND
15
5.8
ug/kg
1
Butyl benzyl phthalate
85-68-7 8270E
ND
15
5.8
ug/kg
1
Caprolactam
105-60-2 8270E
ND
15
5.8
ug/kg
1
Carbazole
86-74-8 8270E
ND
15
5.8
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1 8270E
ND
15
5.8
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7 8270E
ND
15
5.8
ug/kg
1
4-Chloroaniline
106-47-8 8270E
ND
15
5.8
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-004
Description: SS-15 Matrix: Solid
Date Sampled:07/29/2020 1120 % Solids: 82.6 07/30/2020 0022
Date Received:07/29/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 08/07/2020 1440 SCD 07/30/2020 1900 61838
2 3546 8270E 1 08/08/2020 1555 SCD 08/07/2020 2039 62822
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
15
5.8
ug/kg
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
15
5.8
ug/kg
2-Chloronaphthalene
91-58-7
8270E
ND
15
5.8
ug/kg
2-Chlorophenol
95-57-8
8270E
ND
15
5.8
ug/kg
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
15
5.8
ug/kg
Chrysene
218-01-9
8270E
ND
3.1
0.52
ug/kg
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
3.1
0.59
ug/kg
Dibenzofuran
132-64-9
8270E
ND
15
5.8
ug/kg
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
15
5.8
ug/kg
2,4-Dichlorophenol
120-83-2
8270E
ND
15
5.8
ug/kg
Diethylphthalate
84-66-2
8270E
ND
15
5.8
ug/kg
Dimethyl phthalate
131-11-3
8270E
ND
15
8.6
ug/kg
2,4-Dimethylphenol
105-67-9
8270E
ND
15
5.8
ug/kg
Di-n-butyl phthalate
84-74-2
8270E
ND
15
5.8
ug/kg
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
81
30
ug/kg
2,4-Dinitrophenol
51-28-5
8270E
ND
81
30
ug/kg
2,4-Dinitrotoluene
121-14-2
8270E
ND
31
12
ug/kg
2,6-Dinitrotoluene
606-20-2
8270E
ND
31
12
ug/kg
Di-n-octylphthalate
117-84-0
8270E
ND
15
5.8
ug/kg
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
78
29
ug/kg
Fluoranthene
206-44-0
8270E
ND
3.1
0.49
ug/kg
Fluorene
86-73-7
8270E
ND
3.1
0.66
ug/kg
Hexachlorobenzene
118-74-1
8270E
ND
15
5.8
ug/kg
Hexachlorobutadiene
87-68-3
8270E
ND
15
5.8
ug/kg
Hexachlorocyclopentadiene
77-47-4
8270E
ND
78
29
ug/kg
Hexachloroethane
67-72-1
8270E
ND
15
5.8
ug/kg
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
3.1
1.2
ug/kg
Isophorone
78-59-1
8270E
ND
15
5.8
ug/kg
2-Methylnaphthalene
91-57-6
8270E
ND
3.1
1.2
ug/kg
2-Methylphenol
95-48-7
8270E
ND
15
5.8
ug/kg
3+4-Methylphenol
106-44-5
8270E
ND
31
12
ug/kg
Naphthalene
91-20-3
8270E
ND
3.1
1.1
ug/kg
2-Nitroaniline
88-74-4
8270E
ND
31
12
ug/kg
3-Nitroaniline
99-09-2
8270E
ND
31
12
ug/kg
4-Nitroaniline
100-01-6
8270E
ND
31
12
ug/kg
Nitrobenzene
98-95-3
8270E
ND
15
5.8
ug/kg
2-Nitrophenol
88-75-5
8270E
ND
31
12
ug/kg
4-Nitrophenol
100-02-7
8270E
ND
78
29
ug/kg
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
15
5.8
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-004
Description: SS-15 Matrix: Solid
Date Sampled:07/29/2020 1120 % Solids: 82.6 07/30/2020 0022
Date Received:07/29/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E 1 08/07/2020 1440 SCD
07/30/2020 1900
61838
2 3546
8270E 1 08/08/2020 1555 SCD
08/07/2020 2039
62822
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E
ND
15
5.8
ug/kg
1
Pentachlorophenol
87-86-5 8270E
ND
78
29
ug/kg
1
Phenanthrene
85-01-8 8270E
ND
3.1
0.84
ug/kg
1
Phenol
108-95-2 8270E
ND
15
5.8
ug/kg
1
Pyrene
129-00-0 8270E
ND
3.1
0.58
ug/kg
1
Pyridine
110-86-1 8270E
ND
15
5.8
ug/kg
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
15
5.8
ug/kg
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
15
5.8
ug/kg
1
Run 1 Acceptance Run
2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery
Limits
2-Fluorobiphenyl
65 33-102 82
33-102
2-Fluorophenol
69 35-115 89
35-115
Nitrobenzene-d5
67 22-109 74
22-109
Phenol-d5
69 33-122 96
33-122
Terphenyl-d14
80 41-120 85
41-120
2,4,6-Tribromophenol
61 30-117 74
30-117
MA EPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/08/2020 0200 JJG
08/03/2020 1348
62125
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C11 - C22 Aromatics
MADEP-EPH-04
ND
11
11
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) 70 40-140
2-Fluorobiphenyl (fractionation 1)
68 40-140
o - Terphenyl (aromatic)
63 40-140
MA EPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/07/2020 2200 JJG
08/03/2020 1348
62124
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
C9 - C18 Aliphatics
MADEP-EPH-04
ND
11
11
mg/kg
1
C19 - C36 Aliphatics
MADEP-EPH-04
ND
11
11
mg/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated
result <
LOQ and > DL
H = Out of holding time W
= Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-004
Description: SS-15 Matrix: Solid
Date Sampled:07/29/2020 1120 % Solids: 82.6 07/30/2020 0022
Date Received:07/29/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
50 40-140
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201748 ECB
62147
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C5 - C8 Aliphatics
MADEP-VPH-18- ND
4.6
0.93
mg/kg
1
C9 - C12 Aliphatics
MADEP-VPH-18- ND
4.6
0.93
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
124 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201748 ECB
62150
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C9 - C10 Aromatics
MADEP-VPH-18- ND
1.5
0.62
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (PID)
115 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-005
Description: GW-1 Matrix: Aqueous
Date Sampled:07/29/2020 1205
Date Received:07/29/2020
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/04/20201231 TML 62263
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
0.97 J
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
Cyclohexane
110-82-7
8260D
ND
1.0
0.40
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,3-Dichlorobenzene
541-73-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
Dichlorodifluoromethane
75-71-8
8260D
ND
2.0
0.60
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans-1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Isopropylbenzene
98-82-8
8260D
ND
1.0
0.40
ug/L
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
1.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-005
Description: GW-1 Matrix: Aqueous
Date Sampled:07/29/2020 1205
Date Received:07/29/2020
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 08/04/20201231 TML
62263
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1 8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6 8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
104 70-130
1,2-Dichloroethane-d4
101 70-130
Toluene-d8
100 70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E 1 08/04/2020 1755 SCD
07/31/2020 1622 61942
2 3520C
8270E 5 08/05/2020 1813 SCD
07/31/2020 1622 61942
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9 8270E
ND
0.16
0.040
ug/L
1
Acenaphthylene
208-96-8 8270E
ND
0.16
0.040
ug/L
1
Acetophenone
98-86-2 8270E
ND
0.80
0.23
ug/L
1
Anthracene
120-12-7 8270E
ND
0.16
0.040
ug/L
1
Atrazine
1912-24-9 8270E
ND
0.80
0.20
ug/L
1
Benzaldehyde
100-52-7 8270E
ND
4.0
0.27
ug/L
1
Benzo(a)anthracene
56-55-3 8270E
ND
0.16
0.040
ug/L
1
Benzo(a)pyrene
50-32-8 8270E
ND
0.16
0.040
ug/L
1
Benzo(b)fluoranthene
205-99-2 8270E
ND
0.16
0.040
ug/L
1
Benzo(g,h,i)perylene
191-24-2 8270E
ND
0.16
0.040
ug/L
1
Benzo(k)fluoranthene
207-08-9 8270E
ND
0.16
0.040
ug/L
1
1,1'-Biphenyl
92-52-4 8270E
ND
0.80
0.21
ug/L
1
4-Bromophenyl phenyl ether
101-55-3 8270E
ND
0.80
0.15
ug/L
1
Butyl benzyl phthalate
85-68-7 8270E
ND
4.0
0.21
ug/L
1
Caprolactam
105-60-2 8270E
39 B
20
3.6
ug/L
2
Carbazole
86-74-8 8270E
ND
0.80
0.040
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1 8270E
ND
0.80
0.17
ug/L
1
4-Chloro-3-methyl phenol
59-50-7 8270E
ND
0.80
0.26
ug/L
1
4-Chloroaniline
106-47-8 8270E
ND
0.80
0.13
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result
< LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-005
Description: GW-1 Matrix: Aqueous
Date Sampled:07/29/2020 1205
Date Received:07/29/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/04/2020 1755 SCD 07/31/2020 1622 61942
2 3520C 8270E 5 08/05/2020 1813 SCD 07/31/2020 1622 61942
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.80
0.060
ug/L
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.80
0.16
ug/L
2-Chloronaphthalene
91-58-7
8270E
ND
0.80
0.15
ug/L
2-Chlorophenol
95-57-8
8270E
ND
0.80
0.15
ug/L
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.80
0.16
ug/L
Chrysene
218-01-9
8270E
ND
0.16
0.040
ug/L
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.16
0.040
ug/L
Dibenzofuran
132-64-9
8270E
ND
0.80
0.16
ug/L
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
0.81
ug/L
2,4-Dichlorophenol
120-83-2
8270E
ND
0.80
0.19
ug/L
Diethylphthalate
84-66-2
8270E
1.7
BJ
4.0
0.19
ug/L
Dimethyl phthalate
131-11-3
8270E
0.28
J
4.0
0.18
ug/L
2,4-Dimethylphenol
105-67-9
8270E
ND
0.80
0.15
ug/L
Di-n-butyl phthalate
84-74-2
8270E
0.45
J
4.0
0.42
ug/L
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
4.0
0.89
ug/L
2,4-Dinitrophenol
51-28-5
8270E
ND
4.0
1.3
ug/L
2,4-Dinitrotoluene
121-14-2
8270E
ND
1.6
0.36
ug/L
2,6-Dinitrotoluene
606-20-2
8270E
ND
1.6
0.34
ug/L
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.48
ug/L
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
2.5
BJ
4.0
0.38
ug/L
Fluoranthene
206-44-0
8270E
ND
0.16
0.040
ug/L
Fluorene
86-73-7
8270E
ND
0.16
0.040
ug/L
Hexachlorobenzene
118-74-1
8270E
ND
0.80
0.15
ug/L
Hexachlorobutadiene
87-68-3
8270E
ND
0.80
0.17
ug/L
Hexachlorocyclopentadiene
77-47-4
8270E
ND
4.0
1.1
ug/L
Hexachloroethane
67-72-1
8270E
ND
0.80
0.17
ug/L
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.16
0.040
ug/L
Isophorone
78-59-1
8270E
ND
0.80
0.22
ug/L
2-Methylnaphthalene
91-57-6
8270E
ND
0.16
0.040
ug/L
2-Methylphenol
95-48-7
8270E
ND
0.80
0.21
ug/L
3+4-Methylphenol
106-44-5
8270E
ND
1.6
0.46
ug/L
Naphthalene
91-20-3
8270E
ND
0.16
0.040
ug/L
2-Nitroaniline
88-74-4
8270E
ND
1.6
0.66
ug/L
3-Nitroaniline
99-09-2
8270E
ND
1.6
0.15
ug/L
4-Nitroaniline
100-01-6
8270E
ND
1.6
1.3
ug/L
Nitrobenzene
98-95-3
8270E
ND
0.80
0.17
ug/L
2-Nitrophenol
88-75-5
8270E
ND
1.6
0.44
ug/L
4-Nitrophenol
100-02-7
8270E
ND
4.0
2.1
ug/L
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.80
0.28
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-005
Description: GW-1 Matrix: Aqueous
Date Sampled:07/29/2020 1205
Date Received:07/29/2020
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 3520C
8270E 1 08/04/2020 1755 SCD 07/31/2020 1622
61942
2 3520C
8270E 5 08/05/2020 1813 SCD 07/31/2020 1622
61942
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E ND
0.80
0.50
ug/L
1
Pentachlorophenol
87-86-5 8270E ND
4.0
1.3
ug/L
1
Phenanthrene
85-01-8 8270E ND
0.16
0.040
ug/L
1
Phenol
108-95-2 8270E ND
0.80
0.19
ug/L
1
Pyrene
129-00-0 8270E ND
0.16
0.040
ug/L
1
2,4,5-Trichlorophenol
95-95-4 8270E ND
0.80
0.19
ug/L
1
2,4,6-Trichlorophenol
88-06-2 8270E ND
0.80
0.22
ug/L
1
Run 1 Acceptance Run 2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
2-Fluorobiphenyl
65 37-129 55 37-129
2-Fluorophenol
33 24-127 26 24-127
Nitrobenzene-d5
66 38-127 54 38-127
Phenol-d5
57 28-128 32 28-128
Terphenyl-d14
88 10-148 67 10-148
2,4,6-Tribromophenol
79 35-144 55 35-144
MADEP EPH (aliphatics) - Unfractionated
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/11/2020 1449 JJG 08/03/2020 1535
63151
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C19 - C36 Aliphatics - Unfractionated MADEP-EPH-04 ND
100
100
ug/L
1
C9 - C18 Aliphatics - Unfractionated
MADEP-EPH-04 ND
100
100
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic) - Unfractionated 43 40-140
MADEP EPH (aromatics) - Unfractionated
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 MADEP-EPH-
MADEP-EPH-04 1 08/11/2020 1449 JJG 08/03/2020 1535
63154
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C11 - C22 Aromatics - Unfractionated MADEP-EPH-04 ND
100
100
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated
result
< LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 73

Client:SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: VG29053-005
Description: GW-1 Matrix: Aqueous
Date Sampled:07/29/2020 1205
Date Received:07/29/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
o - Terphenyl (aromatic) - Unfractionated 71 40-140
2-Fluorobiphenyl (fractionation 1)
89 40-140
2-Bromonaphthalene (fractionation 2) 97 40-140
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201456 ECB
62146
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C5 - C8 Aliphatics
MADEP-VPH-18- ND
75
15
ug/L
1
C9 - C12 Aliphatics
MADEP-VPH-18- ND
75
15
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
114 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-18-2.1 1 08/03/20201456 ECB
62149
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
C9 - C10 Aromatics
MADEP-VPH-18- ND
25
5.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (PID)
111 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 73

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 73

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ62131-001 Matrix: Solid
Batch: 62131 Prep Method: 5035
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
8.0
ug/kg
08/03/2020 1027
Benzene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Bromodichloromethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Bromoform
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Bromomethane (Methyl bromide)
ND
1
5.0
3.0
ug/kg
08/03/2020 1027
2-Butanone (MEK)
ND
1
20
4.0
ug/kg
08/03/2020 1027
Carbon disulfide
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Carbon tetrachloride
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Chlorobenzene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Chloroethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Chloroform
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Chloromethane (Methyl chloride)
ND
1
5.0
3.0
ug/kg
08/03/2020 1027
Cyclohexane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Dibromochloromethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,2-Dibromoethane (EDB)
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,2-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,3-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,4-Dichlorobenzene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Dichlorodifluoromethane
ND
1
5.0
3.0
ug/kg
08/03/2020 1027
1,1-Dichloroethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,2-Dichloroethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,1-Dichloroethene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
cis- 1,2-Dichloroethene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
trans- 1,2-Dichloroethene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,2-Dichloropropane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
cis- 1,3-Dichloropropene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
trans- 1,3-Dichloropropene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Ethylbenzene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
2-Hexanone
ND
1
10
4.0
ug/kg
08/03/2020 1027
Isopropylbenzene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Methyl acetate
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Methyl tertiary butyl ether (MTBE)
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
4-Methyl-2-pentanone
ND
1
10
4.0
ug/kg
08/03/2020 1027
Methylcyclohexane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Methylene chloride
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Styrene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,1,2,2-Tetrachloroethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Tetrachloroethene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Toluene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,2,4-Trichlorobenzene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,1,1-Trichloroethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
1,1,2-Trichloroethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 73

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ62131-001 Matrix: Solid
Batch: 62131 Prep Method: 5035
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Trichloroethene
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Trichlorofluoromethane
ND
1
5.0
2.0
ug/kg
08/03/2020 1027
Vinyl chloride
ND
1
5.0
3.0
ug/kg
08/03/2020 1027
Xylenes (total)
ND
1
10
4.0
ug/kg
08/03/2020 1027
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 110 47-138
1,2-Dichloroethane-d4 107 53-142
Toluene-d8 115 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 73

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ62131-002
Matrix:
Solid
Batch: 62131
Prep Method:
5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
100
1
103
60-140
08/03/2020 1004
Benzene
50
55
1
111
70-130
08/03/2020 1004
Bromodichloromethane
50
53
1
106
70-130
08/03/2020 1004
Bromoform
50
53
1
106
70-130
08/03/2020 1004
Bromomethane (Methyl bromide)
50
59
1
118
70-130
08/03/2020 1004
2-Butanone (MEK)
100
100
1
102
60-140
08/03/2020 1004
Carbon disulfide
50
59
1
117
70-130
08/03/2020 1004
Carbon tetrachloride
50
58
1
117
70-130
08/03/2020 1004
Chlorobenzene
50
54
1
108
70-130
08/03/2020 1004
Chloroethane
50
59
1
118
70-130
08/03/2020 1004
Chloroform
50
53
1
106
70-130
08/03/2020 1004
Chloromethane (Methyl chloride)
50
57
1
114
60-140
08/03/2020 1004
Cyclohexane
50
52
1
105
70-130
08/03/2020 1004
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
95
70-130
08/03/2020 1004
Dibromochloromethane
50
52
1
103
70-130
08/03/2020 1004
1,2-Dibromoethane (EDB)
50
51
1
102
70-130
08/03/2020 1004
1,2-Dichlorobenzene
50
51
1
102
70-130
08/03/2020 1004
1,3-Dichlorobenzene
50
54
1
107
70-130
08/03/2020 1004
1,4-Dichlorobenzene
50
52
1
103
70-130
08/03/2020 1004
Dichlorodifluoromethane
50
56
1
111
60-140
08/03/2020 1004
1,1-Dichloroethane
50
53
1
106
70-130
08/03/2020 1004
1,2-Dichloroethane
50
51
1
102
70-130
08/03/2020 1004
1,1-Dichloroethene
50
59
1
117
70-130
08/03/2020 1004
cis- 1,2-Dichloroethene
50
53
1
106
70-130
08/03/2020 1004
trans- 1,2-Dichloroethene
50
57
1
114
70-130
08/03/2020 1004
1,2-Dichloropropane
50
52
1
103
70-130
08/03/2020 1004
cis- 1,3-Dichloropropene
50
53
1
106
70-130
08/03/2020 1004
trans- 1,3-Dichloropropene
50
50
1
101
70-130
08/03/2020 1004
Ethylbenzene
50
55
1
110
70-130
08/03/2020 1004
2-Hexanone
100
93
1
93
70-130
08/03/2020 1004
Isopropylbenzene
50
53
1
106
70-130
08/03/2020 1004
Methyl acetate
50
47
1
93
70-130
08/03/2020 1004
Methyl tertiary butyl ether (MTBE)
50
52
1
103
70-130
08/03/2020 1004
4-Methyl-2-pentanone
100
95
1
95
70-130
08/03/2020 1004
Methylcyclohexane
50
52
1
104
70-130
08/03/2020 1004
Methylene chloride
50
50
1
99
70-130
08/03/2020 1004
Styrene
50
54
1
107
70-130
08/03/2020 1004
1,1,2,2-Tetrachloroethane
50
47
1
95
70-130
08/03/2020 1004
Tetrachloroethene
50
59
1
117
70-130
08/03/2020 1004
Toluene
50
56
1
112
70-130
08/03/2020 1004
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
56
1
112
70-130
08/03/2020 1004
1,2,4-Trichlorobenzene
50
53
1
105
70-130
08/03/2020 1004
1,1,1-Trichloroethane
50
58
1
116
70-130
08/03/2020 1004
1,1,2-Trichloroethane
50
50
1
100
70-130
08/03/2020 1004
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 73

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ62131-002
Matrix:
Solid
Batch: 62131
Prep Method:
5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
50
58
1
116
70-130
08/03/2020 1004
Trichlorofluoromethane
50
59
1
118
70-130
08/03/2020 1004
Vinyl chloride
50
62
1
124
70-130
08/03/2020 1004
Xylenes (total)
100
110
1
110
70-130
08/03/2020 1004
Acceptance
Surrogate
Q % Rec
Limit
Bromofluorobenzene 108 47-138
1,2-Dichloroethane-d4 104 53-142
Toluene-d8 115 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 73

Volatile Organic Compounds by GC/MS - Duplicate
Sample ID: VG29053-001DU Matrix: Solid
Batch: 62131 Prep Method: 5035
Analytical Method: 8260D
Sample
Amount
Result
% RPD
Parameter
(ug/kg)
(ug/kg) Q
Dil
% RPD
Limit
Analysis Date
Acetone
ND
ND
1
0.00
20
08/03/2020 2028
Benzene
ND
ND
1
0.00
20
08/03/2020 2028
Bromodichloromethane
ND
ND
1
0.00
20
08/03/2020 2028
Bromoform
ND
ND
1
0.00
20
08/03/2020 2028
Bromomethane (Methyl bromide)
ND
ND
1
0.00
20
08/03/2020 2028
2-Butanone (MEK)
ND
ND
1
0.00
20
08/03/2020 2028
Carbon disulfide
ND
ND
1
0.00
20
08/03/2020 2028
Carbon tetrachloride
ND
ND
1
0.00
20
08/03/2020 2028
Chlorobenzene
ND
ND
1
0.00
20
08/03/2020 2028
Chloroethane
ND
ND
1
0.00
20
08/03/2020 2028
Chloroform
ND
ND
1
0.00
20
08/03/2020 2028
Chloromethane (Methyl chloride)
ND
ND
1
0.00
20
08/03/2020 2028
Cyclohexane
ND
ND
1
0.00
20
08/03/2020 2028
1,2-Dibromo-3-chloropropane (DBCP)
ND
ND
1
0.00
20
08/03/2020 2028
Dibromochloromethane
ND
ND
1
0.00
20
08/03/2020 2028
1,2-Dibromoethane (EDB)
ND
ND
1
0.00
20
08/03/2020 2028
1,2-Dichlorobenzene
ND
ND
1
0.00
20
08/03/2020 2028
1,3-Dichlorobenzene
ND
ND
1
0.00
20
08/03/2020 2028
1,4-Dichlorobenzene
ND
ND
1
0.00
20
08/03/2020 2028
Dichlorodifluoromethane
ND
ND
1
0.00
20
08/03/2020 2028
1,1-Dichloroethane
ND
ND
1
0.00
20
08/03/2020 2028
1,2-Dichloroethane
ND
ND
1
0.00
20
08/03/2020 2028
1,1-Dichloroethene
ND
ND
1
0.00
20
08/03/2020 2028
cis- 1,2-Dichloroethene
ND
ND
1
0.00
20
08/03/2020 2028
trans- 1,2-Dichloroethene
ND
ND
1
0.00
20
08/03/2020 2028
1,2-Dichloropropane
ND
ND
1
0.00
20
08/03/2020 2028
cis- 1,3-Dichloropropene
ND
ND
1
0.00
20
08/03/2020 2028
trans- 1,3-Dichloropropene
ND
ND
1
0.00
20
08/03/2020 2028
Ethylbenzene
ND
ND
1
0.00
20
08/03/2020 2028
2-Hexanone
ND
ND
1
0.00
20
08/03/2020 2028
Isopropylbenzene
ND
ND
1
0.00
20
08/03/2020 2028
Methyl acetate
ND
ND
1
0.00
20
08/03/2020 2028
Methyl tertiary butyl ether (MTBE)
ND
ND
1
0.00
20
08/03/2020 2028
4-Methyl-2-pentanone
ND
ND
1
0.00
20
08/03/2020 2028
Methylcyclohexane
ND
ND
1
0.00
20
08/03/2020 2028
Methylene chloride
ND
ND
1
0.00
20
08/03/2020 2028
Styrene
ND
ND
1
0.00
20
08/03/2020 2028
1,1,2,2-Tetrachloroethane
ND
ND
1
0.00
20
08/03/2020 2028
Tetrachloroethene
ND
ND
1
0.00
20
08/03/2020 2028
Toluene
ND
ND
1
0.00
20
08/03/2020 2028
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
ND
1
0.00
20
08/03/2020 2028
1,2,4-Trichlorobenzene
ND
ND
1
0.00
20
08/03/2020 2028
1,1,1-Trichloroethane
ND
ND
1
0.00
20
08/03/2020 2028
1,1,2-Trichloroethane
ND
ND
1
0.00
20
08/03/2020 2028
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 73

Volatile Organic Compounds by GC/MS - Duplicate
Sample ID: VG29053-001DU
Matrix:
Solid
Batch: 62131
Prep Method:
5035
Analytical Method: 8260D
Sample
Amount
Result
% RPD
Parameter
(ug/kg)
(ug/kg) Q
Dil
% RPD
Limit
Analysis Date
Trichloroethene
ND
ND
1
0.00
20
08/03/2020 2028
Trichlorofluoromethane
ND
ND
1
0.00
20
08/03/2020 2028
Vinyl chloride
ND
ND
1
0.00
20
08/03/2020 2028
Xylenes (total)
ND
ND
1
0.00
20
08/03/2020 2028
Acceptance
Surrogate
Q % Rec
Limit
Bromofluorobenzene 111 47-138
1,2-Dichloroethane-d4 107 53-142
Toluene-d8 112 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 73

Volatile Organic Compounds by GC/MS - MS
Sample ID: VG29053-004MS
Matrix:
Solid
Batch: 62131
Prep Method:
5035
Analytical Method: 8260D
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
(ug/kg)
Q
Dil
% Rec
Limit
Analysis Date
Acetone
ND
100
57
N
1
57
70-130
08/03/2020 2051
Benzene
ND
50
50
1
99
70-130
08/03/2020 2051
Bromodichloromethane
ND
50
52
1
103
70-130
08/03/2020 2051
Bromoform
ND
50
48
1
95
70-130
08/03/2020 2051
Bromomethane (Methyl bromide)
ND
50
58
1
114
70-130
08/03/2020 2051
2-Butanone (MEK)
ND
100
82
1
81
70-130
08/03/2020 2051
Carbon disulfide
ND
50
52
1
104
70-130
08/03/2020 2051
Carbon tetrachloride
ND
50
48
1
96
70-130
08/03/2020 2051
Chlorobenzene
ND
50
47
1
93
70-130
08/03/2020 2051
Chloroethane
ND
50
51
1
101
70-130
08/03/2020 2051
Chloroform
ND
50
54
1
106
70-130
08/03/2020 2051
Chloromethane (Methyl chloride)
ND
50
53
1
106
60-140
08/03/2020 2051
Cyclohexane
ND
50
47
1
94
70-130
08/03/2020 2051
1,2-Dibromo-3-chloropropane (DBCP)
ND
50
41
1
82
70-130
08/03/2020 2051
Dibromochloromethane
ND
50
49
1
98
70-130
08/03/2020 2051
1,2-Dibromoethane (EDB)
ND
50
49
1
96
70-130
08/03/2020 2051
1,2-Dichlorobenzene
ND
50
45
1
89
70-130
08/03/2020 2051
1,3-Dichlorobenzene
ND
50
46
1
91
70-130
08/03/2020 2051
1,4-Dichlorobenzene
ND
50
46
1
91
70-130
08/03/2020 2051
Dichlorodifluoromethane
ND
50
48
1
95
60-140
08/03/2020 2051
1,1-Dichloroethane
ND
50
51
1
102
70-130
08/03/2020 2051
1,2-Dichloroethane
ND
50
54
1
107
70-130
08/03/2020 2051
1,1-Dichloroethene
ND
50
51
1
102
70-130
08/03/2020 2051
cis- 1,2-Dichloroethene
ND
50
54
1
108
70-130
08/03/2020 2051
trans- 1,2-Dichloroethene
ND
50
52
1
104
70-130
08/03/2020 2051
1,2-Dichloropropane
ND
50
50
1
98
70-130
08/03/2020 2051
cis- 1,3-Dichloropropene
ND
50
50
1
100
70-130
08/03/2020 2051
trans- 1,3-Dichloropropene
ND
50
47
1
92
70-130
08/03/2020 2051
Ethylbenzene
ND
50
46
1
92
70-130
08/03/2020 2051
2-Hexanone
ND
100
69
N
1
69
70-130
08/03/2020 2051
Isopropylbenzene
ND
50
42
1
84
70-130
08/03/2020 2051
Methyl acetate
ND
50
68
N
1
134
70-130
08/03/2020 2051
Methyl tertiary butyl ether (MTBE)
ND
50
53
1
106
70-130
08/03/2020 2051
4-Methyl-2-pentanone
ND
100
88
1
88
70-130
08/03/2020 2051
Methylcyclohexane
ND
50
48
1
95
70-130
08/03/2020 2051
Methylene chloride
ND
50
52
1
103
70-130
08/03/2020 2051
Styrene
ND
50
47
1
94
70-130
08/03/2020 2051
1,1,2,2-Tetrachloroethane
ND
50
45
1
89
70-130
08/03/2020 2051
Tetrachloroethene
ND
50
45
1
90
70-130
08/03/2020 2051
Toluene
ND
50
49
1
98
70-130
08/03/2020 2051
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
50
51
1
101
70-130
08/03/2020 2051
1,2,4-Trichlorobenzene
ND
50
41
1
82
70-130
08/03/2020 2051
1,1,1-Trichloroethane
ND
50
49
1
97
70-130
08/03/2020 2051
1,1,2-Trichloroethane
ND
50
48
1
96
70-130
08/03/2020 2051
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 73

Volatile Organic Compounds by GC/MS - MS
Sample ID: VG29053-004MS
Matrix:
Solid
Batch: 62131
Prep Method:
5035
Analytical Method: 8260D
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
ND
50
49
1
97
70-130
08/03/2020 2051
Trichlorofluoromethane
ND
50
48
1
96
70-130
08/03/2020 2051
Vinyl chloride
ND
50
54
1
108
70-130
08/03/2020 2051
Xylenes (total)
ND
100
95
1
95
70-130
08/03/2020 2051
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 103 47-138
1,2-Dichloroethane-d4 113 53-142
Toluene-d8 110 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 73

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ62263-001 Matrix: Aqueous
Batch: 62263 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
08/04/2020 1033
Benzene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Bromodichloromethane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Bromoform
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
08/04/2020 1033
2-Butanone (MEK)
ND
1
10
2.0
ug/L
08/04/2020 1033
Carbon disulfide
0.50 J
1
1.0
0.40
ug/L
08/04/2020 1033
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Chlorobenzene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Chloroethane
ND
1
2.0
0.40
ug/L
08/04/2020 1033
Chloroform
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
08/04/2020 1033
Cyclohexane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Dibromochloromethane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,3-Dichlorobenzene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Dichlorodifluoromethane
ND
1
2.0
0.60
ug/L
08/04/2020 1033
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Ethylbenzene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
2-Hexanone
ND
1
10
2.0
ug/L
08/04/2020 1033
Isopropylbenzene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Methyl acetate
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Methyl tertiary butyl ether (MTBE)
ND
1
1.0
0.40
ug/L
08/04/2020 1033
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
08/04/2020 1033
Methylcyclohexane
ND
1
5.0
0.40
ug/L
08/04/2020 1033
Methylene chloride
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Styrene
ND
1
1.0
0.41
ug/L
08/04/2020 1033
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Tetrachloroethene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Toluene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
1.0
0.42
ug/L
08/04/2020 1033
1,2,4-Trichlorobenzene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 73

Volatile Organic Compounds by GC/MS - MB
Sample ID: VQ62263-001 Matrix: Aqueous
Batch: 62263 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Trichloroethene
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Vinyl chloride
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Xylenes (total)
ND
1
1.0
0.40
ug/L
08/04/2020 1033
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 93 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 73

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ62263-002
Matrix:
Aqueous
Batch: 62263
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
110
1
112
60-140
08/04/2020 0940
Benzene
50
51
1
102
70-130
08/04/2020 0940
Bromodichloromethane
50
53
1
106
70-130
08/04/2020 0940
Bromoform
50
43
1
86
70-130
08/04/2020 0940
Bromomethane (Methyl bromide)
50
55
1
110
70-130
08/04/2020 0940
2-Butanone (MEK)
100
110
1
113
70-130
08/04/2020 0940
Carbon disulfide
50
48
1
96
70-130
08/04/2020 0940
Carbon tetrachloride
50
53
1
106
70-130
08/04/2020 0940
Chlorobenzene
50
49
1
99
70-130
08/04/2020 0940
Chloroethane
50
57
1
114
70-130
08/04/2020 0940
Chloroform
50
49
1
98
70-130
08/04/2020 0940
Chloromethane (Methyl chloride)
50
58
1
116
60-140
08/04/2020 0940
Cyclohexane
50
52
1
103
70-130
08/04/2020 0940
1,2-Dibromo-3-chloropropane (DBCP)
50
46
1
92
70-130
08/04/2020 0940
Dibromochloromethane
50
45
1
90
70-130
08/04/2020 0940
1,2-Dibromoethane (EDB)
50
51
1
102
70-130
08/04/2020 0940
1,2-Dichlorobenzene
50
50
1
100
70-130
08/04/2020 0940
1,3-Dichlorobenzene
50
50
1
100
70-130
08/04/2020 0940
1,4-Dichlorobenzene
50
48
1
97
70-130
08/04/2020 0940
Dichlorodifluoromethane
50
65
1
131
60-140
08/04/2020 0940
1,1-Dichloroethane
50
51
1
102
70-130
08/04/2020 0940
1,2-Dichloroethane
50
50
1
99
70-130
08/04/2020 0940
1,1-Dichloroethene
50
54
1
108
70-130
08/04/2020 0940
cis- 1,2-Dichloroethene
50
52
1
104
70-130
08/04/2020 0940
trans- 1,2-Dichloroethene
50
53
1
107
70-130
08/04/2020 0940
1,2-Dichloropropane
50
52
1
104
70-130
08/04/2020 0940
cis- 1,3-Dichloropropene
50
50
1
100
70-130
08/04/2020 0940
trans- 1,3-Dichloropropene
50
47
1
94
70-130
08/04/2020 0940
Ethylbenzene
50
53
1
105
70-130
08/04/2020 0940
2-Hexanone
100
110
1
112
70-130
08/04/2020 0940
Isopropylbenzene
50
55
1
110
70-130
08/04/2020 0940
Methyl acetate
50
53
1
106
70-130
08/04/2020 0940
Methyl tertiary butyl ether (MTBE)
50
51
1
102
70-130
08/04/2020 0940
4-Methyl-2-pentanone
100
110
1
108
70-130
08/04/2020 0940
Methylcyclohexane
50
54
1
108
70-130
08/04/2020 0940
Methylene chloride
50
49
1
98
70-130
08/04/2020 0940
Styrene
50
55
1
111
70-130
08/04/2020 0940
1,1,2,2-Tetrachloroethane
50
50
1
101
70-130
08/04/2020 0940
Tetrachloroethene
50
50
1
101
70-130
08/04/2020 0940
Toluene
50
51
1
102
70-130
08/04/2020 0940
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
45
1
90
70-130
08/04/2020 0940
1,2,4-Trichlorobenzene
50
52
1
103
70-130
08/04/2020 0940
1,1,1-Trichloroethane
50
53
1
106
70-130
08/04/2020 0940
1,1,2-Trichloroethane
50
49
1
98
70-130
08/04/2020 0940
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 73

Volatile Organic Compounds by GC/MS - LCS
Sample ID: VQ62263-002
Matrix:
Aqueous
Batch: 62263
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
50
47
1
94
70-130
08/04/2020 0940
Trichlorofluoromethane
50
54
1
107
70-130
08/04/2020 0940
Vinyl chloride
50
61
1
122
70-130
08/04/2020 0940
Xylenes (total)
100
110
1
107
70-130
08/04/2020 0940
Acceptance
Surrogate
Q % Rec
Limit
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 96 70-130
Toluene-d8 100 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 36 of 73

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ61838-001 Matrix: Solid
Batch: 61838 Prep Method: 3546
Analytical Method: 8270E Prep Date: 07/30/2020 1900
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
2.7
0.83
ug/kg
08/07/2020 1121
Acenaphthylene
ND
1
2.7
0.95
ug/kg
08/07/2020 1121
Acetophenone
ND
1
13
5.0
ug/kg
08/07/2020 1121
Anthracene
ND
1
2.7
0.51
ug/kg
08/07/2020 1121
Atrazine
ND
1
13
5.0
ug/kg
08/07/2020 1121
Benzaldehyde
ND
1
13
5.0
ug/kg
08/07/2020 1121
Benzo(a)anthracene
ND
1
2.7
0.59
ug/kg
08/07/2020 1121
Benzo(a)pyrene
ND
1
2.7
0.66
ug/kg
08/07/2020 1121
Benzo(k)fluoranthene
ND
1
2.7
0.50
ug/kg
08/07/2020 1121
Benzo(g,h,i)perylene
ND
1
2.7
0.65
ug/kg
08/07/2020 1121
Benzo(k)fluoranthene
ND
1
2.7
0.48
ug/kg
08/07/2020 1121
1,1'-Biphenyl
ND
1
13
5.0
ug/kg
08/07/2020 1121
4-Bromophenyl phenyl ether
ND
1
13
5.0
ug/kg
08/07/2020 1121
Butyl benzyl phthalate
ND
1
13
5.0
ug/kg
08/07/2020 1121
Caprolactam
ND
1
13
5.0
ug/kg
08/07/2020 1121
Carbazole
ND
1
13
5.0
ug/kg
08/07/2020 1121
bis (2-Chloro-1-methylethyl) ether
ND
1
13
5.0
ug/kg
08/07/2020 1121
4-Chloro-3-methyl phenol
ND
1
13
5.0
ug/kg
08/07/2020 1121
4-Chloroaniline
ND
1
13
5.0
ug/kg
08/07/2020 1121
bis(2-Chloroethoxy)methane
ND
1
13
5.0
ug/kg
08/07/2020 1121
bis(2-Chloroethyl)ether
ND
1
13
5.0
ug/kg
08/07/2020 1121
2-Chloronaphthalene
ND
1
13
5.0
ug/kg
08/07/2020 1121
2-Chlorophenol
ND
1
13
5.0
ug/kg
08/07/2020 1121
4-Chlorophenyl phenyl ether
ND
1
13
5.0
ug/kg
08/07/2020 1121
Chrysene
ND
1
2.7
0.45
ug/kg
08/07/2020 1121
Dibenzo(a,h)anthracene
ND
1
2.7
0.51
ug/kg
08/07/2020 1121
Dibenzofuran
ND
1
13
5.0
ug/kg
08/07/2020 1121
3,3'-Dichlorobenzidine
ND
1
13
5.0
ug/kg
08/07/2020 1121
2,4-Dichlorophenol
ND
1
13
5.0
ug/kg
08/07/2020 1121
Diethylphthalate
ND
1
13
5.0
ug/kg
08/07/2020 1121
Dimethyl phthalate
ND
1
13
7.4
ug/kg
08/07/2020 1121
2,4-Dimethylphenol
ND
1
13
5.0
ug/kg
08/07/2020 1121
Di-n-butyl phthalate
ND
1
13
5.0
ug/kg
08/07/2020 1121
2,4-Dinitrotoluene
ND
1
27
10
ug/kg
08/07/2020 1121
2,6-Dinitrotoluene
ND
1
27
10
ug/kg
08/07/2020 1121
Di-n-octylphthalate
ND
1
13
5.0
ug/kg
08/07/2020 1121
bis(2-Ethylhexyl)phthalate
ND
1
67
25
ug/kg
08/07/2020 1121
Fluoranthene
ND
1
2.7
0.42
ug/kg
08/07/2020 1121
Fluorene
ND
1
2.7
0.57
ug/kg
08/07/2020 1121
Hexachlorobenzene
ND
1
13
5.0
ug/kg
08/07/2020 1121
Hexachlorobutadiene
ND
1
13
5.0
ug/kg
08/07/2020 1121
Hexachlorocyclopentadiene
ND
1
67
25
ug/kg
08/07/2020 1121
Hexachloroethane
ND
1
13
5.0
ug/kg
08/07/2020 1121
Indeno(1,2,3-c,d)pyrene
ND
1
2.7
1.0
ug/kg
08/07/2020 1121
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 37 of 73

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ61838-001 Matrix: Solid
Batch: 61838 Prep Method: 3546
Analytical Method: 8270E Prep Date: 07/30/2020 1900
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Isophorone
ND
1
13
5.0
ug/kg
08/07/20201121
2-Methyl naphthalene
ND
1
2.7
0.99
ug/kg
08/07/20201121
2-Methylphenol
ND
1
13
5.0
ug/kg
08/07/20201121
3+4-Methylphenol
ND
1
27
10
ug/kg
08/07/20201121
Naphthalene
ND
1
2.7
0.97
ug/kg
08/07/20201121
2-Nitroaniline
ND
1
27
10
ug/kg
08/07/20201121
3-Nitroaniline
ND
1
27
10
ug/kg
08/07/20201121
4-Nitroaniline
ND
1
27
10
ug/kg
08/07/20201121
Nitrobenzene
ND
1
13
5.0
ug/kg
08/07/20201121
2-Nitrophenol
ND
1
27
10
ug/kg
08/07/20201121
4-Nitrophenol
ND
1
67
25
ug/kg
08/07/20201121
N-Nitrosodi-n-propylamine
ND
1
13
5.0
ug/kg
08/07/20201121
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
13
5.0
ug/kg
08/07/2020 1121
Pentachlorophenol
ND
1
67
25
ug/kg
08/07/20201121
Phenanthrene
ND
1
2.7
0.72
ug/kg
08/07/20201121
Phenol
ND
1
13
5.0
ug/kg
08/07/20201121
Pyrene
ND
1
2.7
0.50
ug/kg
08/07/20201121
Pyridine
ND
1
13
5.0
ug/kg
08/07/20201121
2,4,5-Trichlorophenol
ND
1
13
5.0
ug/kg
08/07/20201121
2,4,6-Trichlorophenol
ND
1
13
5.0
ug/kg
08/07/20201121
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
60
33-102
2-Fluorophenol
57
35-115
Nitrobenzene-d5
61
22-109
Phenol-d5 63 33-122
Terphenyl-d14 78 41-120
2,4,6-Tribromophenol 48 30-117
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 38 of 73

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ61838-002
Matrix:
Solid
Batch: 61838
Prep Method:
3546
Analytical Method: 8270E
Prep Date:
07/30/2020 1900
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
130
97
1
73
12-111
08/07/2020 1300
Acenaphthylene
130
110
1
84
44-122
08/07/2020 1300
Acetophenone
130
110
1
85
48-111
08/07/2020 1300
Anthracene
130
120
1
87
16-122
08/07/2020 1300
Atrazine
130
140
1
103
48-116
08/07/2020 1300
Benzaldehyde
130
110
1
82
10-110
08/07/2020 1300
Benzo(a)anthracene
130
130
1
95
40-121
08/07/2020 1300
Benzo(a)pyrene
130
120
1
91
36-114
08/07/2020 1300
Benzo(k)fluoranthene
130
110
1
86
38-123
08/07/2020 1300
Benzo(g,h,i)perylene
130
140
1
109
43-120
08/07/2020 1300
Benzo(k)fluoranthene
130
120
1
92
40-126
08/07/2020 1300
1,1'-Biphenyl
130
100
1
77
49-110
08/07/2020 1300
4-Bromophenyl phenyl ether
130
100
1
76
46-118
08/07/2020 1300
Butyl benzyl phthalate
130
160
1
121
46-128
08/07/2020 1300
Caprolactam
130
140
1
104
43-121
08/07/2020 1300
Carbazole
130
120
1
87
47-128
08/07/2020 1300
bis (2-Chloro-1-methylethyl) ether
130
110
1
85
31-102
08/07/2020 1300
4-Chloro-3-methyl phenol
130
100
1
76
49-118
08/07/2020 1300
4-Chloroaniline
130
54
1
41
17-106
08/07/2020 1300
bis(2-Chloroethoxy)methane
130
98
1
74
39-108
08/07/2020 1300
bis(2-Chloroethyl)ether
130
110
1
81
32-105
08/07/2020 1300
2-Chloronaphthalene
130
100
1
75
31-127
08/07/2020 1300
2-Chlorophenol
130
110
1
79
37-106
08/07/2020 1300
4-Chlorophenyl phenyl ether
130
99
1
75
47-116
08/07/2020 1300
Chrysene
130
120
1
87
41-124
08/07/2020 1300
Dibenzo(a,h)anthracene
130
130
1
101
38-125
08/07/2020 1300
Dibenzofuran
130
100
1
76
45-112
08/07/2020 1300
3,3'-Dichlorobenzidine
130
140
1
102
10-119
08/07/2020 1300
2,4-Dichlorophenol
130
100
1
75
41-113
08/07/2020 1300
Diethylphthalate
130
110
1
84
49-123
08/07/2020 1300
Dimethyl phthalate
130
110
1
83
48-120
08/07/2020 1300
2,4-Dimethylphenol
130
160
1
119
33-123
08/07/2020 1300
Di-n-butyl phthalate
130
120
1
92
51-129
08/07/2020 1300
2,4-Dinitrotoluene
130
120
1
92
48-124
08/07/2020 1300
2,6-Dinitrotoluene
130
120
1
89
47-125
08/07/2020 1300
Di-n-octylphthalate
130
130
1
101
49-142
08/07/2020 1300
bis(2-Ethylhexyl)phthalate
130
150
1
110
45-128
08/07/2020 1300
Fluoranthene
130
110
1
80
26-133
08/07/2020 1300
Fluorene
130
100
1
75
19-108
08/07/2020 1300
Hexachlorobenzene
130
100
1
76
44-122
08/07/2020 1300
Hexachlorobutadiene
130
85
1
64
33-103
08/07/2020 1300
Hexachlorocyclopentadiene
670
490
1
73
18-121
08/07/2020 1300
Hexachloroethane
130
100
1
76
30-96
08/07/2020 1300
Indeno(1,2,3-c,d)pyrene
130
130
1
101
42-123
08/07/2020 1300
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 73

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ61838-002
Matrix:
Solid
Batch: 61838
Prep Method:
3546
Analytical Method: 8270E
Prep Date:
07/30/2020 1900
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Isophorone
130
130
1
96
41-113
08/07/20201300
2-Methyl naphthalene
130
100
1
76
10-107
08/07/20201300
2-Methylphenol
130
120
1
92
32-107
08/07/20201300
3+4-Methylphenol
130
130
1
99
39-108
08/07/20201300
Naphthalene
130
95
1
71
10-112
08/07/20201300
2-Nitroaniline
130
130
1
96
45-123
08/07/20201300
3-Nitroaniline
130
99
1
75
24-127
08/07/20201300
4-Nitroaniline
130
130
1
100
48-127
08/07/20201300
Nitrobenzene
130
110
1
86
33-114
08/07/20201300
2-Nitrophenol
130
93
1
70
35-108
08/07/20201300
4-Nitrophenol
270
150
1
55
18-154
08/07/20201300
N-Nitrosodi-n-propylamine
130
130
1
94
32-115
08/07/20201300
N-Nitrosodiphenylamine (Diphenylamine) 130
120
1
87
53-150
08/07/2020 1300
Pentachlorophenol
270
110
1
40
27-138
08/07/20201300
Phenanthrene
130
100
1
77
16-123
08/07/20201300
Phenol
130
110
1
85
36-108
08/07/20201300
Pyrene
130
130
1
99
34-121
08/07/20201300
Pyridine
130
130
1
99
30-130
08/07/20201300
2,4,5-Trichlorophenol
130
77
1
58
46-122
08/07/20201300
2,4,6-Trichlorophenol
130
92
1
69
38-115
08/07/20201300
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
74
33-102
2-Fluorophenol
77
35-115
Nitrobenzene-d5
75
22-109
Phenol-d5 91 33-122
Terphenyl-d14 93 41-120
2,4,6-Tribromophenol 66 30-117
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 73

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ61942-001 Matrix: Aqueous
Batch: 61942 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 07/31/2020 1622
Parameter
Result
Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Acenaphthylene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Acetophenone
ND
1
0.80
0.23
ug/L
08/04/2020 1029
Anthracene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Atrazine
ND
1
0.80
0.20
ug/L
08/04/2020 1029
Benzaldehyde
ND
1
4.0
0.27
ug/L
08/04/2020 1029
Benzo(a)anthracene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Benzo(a)pyrene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Benzo(k)fluoranthene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Benzo(g,h,i)perylene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Benzo(k)fluoranthene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
1,1'-Biphenyl
ND
1
0.80
0.21
ug/L
08/04/2020 1029
4-Bromophenyl phenyl ether
ND
1
0.80
0.15
ug/L
08/04/2020 1029
Butyl benzyl phthalate
0.53
J
1
4.0
0.21
ug/L
08/04/2020 1029
Caprolactam
3.5
J
1
4.0
0.71
ug/L
08/04/2020 1029
Carbazole
ND
1
0.80
0.040
ug/L
08/04/2020 1029
bis (2-Chloro-1-methylethyl) ether
ND
1
0.80
0.17
ug/L
08/04/2020 1029
4-Chloro-3-methyl phenol
ND
1
0.80
0.26
ug/L
08/04/2020 1029
4-Chloroaniline
ND
1
0.80
0.13
ug/L
08/04/2020 1029
bis(2-Chloroethoxy)methane
ND
1
0.80
0.060
ug/L
08/04/2020 1029
bis(2-Chloroethyl)ether
ND
1
0.80
0.16
ug/L
08/04/2020 1029
2-Chloronaphthalene
ND
1
0.80
0.15
ug/L
08/04/2020 1029
2-Chlorophenol
ND
1
0.80
0.15
ug/L
08/04/2020 1029
4-Chlorophenyl phenyl ether
ND
1
0.80
0.16
ug/L
08/04/2020 1029
Chrysene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Dibenzo(a,h)anthracene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Dibenzofuran
ND
1
0.80
0.16
ug/L
08/04/2020 1029
3,3'-Dichlorobenzidine
ND
1
4.0
0.81
ug/L
08/04/2020 1029
2,4-Dichlorophenol
ND
1
0.80
0.19
ug/L
08/04/2020 1029
Diethylphthalate
0.30
J
1
4.0
0.19
ug/L
08/04/2020 1029
Dimethyl phthalate
ND
1
4.0
0.18
ug/L
08/04/2020 1029
2,4-Dimethylphenol
ND
1
0.80
0.15
ug/L
08/04/2020 1029
Di-n-butyl phthalate
ND
1
4.0
0.42
ug/L
08/04/2020 1029
4,6-Dinitro-2-methyl phenol
ND
1
4.0
0.89
ug/L
08/04/2020 1029
2,4-Dinitrophenol
ND
1
4.0
1.3
ug/L
08/04/2020 1029
2,4-Dinitrotoluene
ND
1
1.6
0.36
ug/L
08/04/2020 1029
2,6-Dinitrotoluene
ND
1
1.6
0.34
ug/L
08/04/2020 1029
Di-n-octylphthalate
ND
1
4.0
0.48
ug/L
08/04/2020 1029
bis(2-Ethylhexyl)phthalate
1.4
J
1
4.0
0.38
ug/L
08/04/2020 1029
Fluoranthene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Fluorene
ND
1
0.16
0.040
ug/L
08/04/2020 1029
Hexachlorobenzene
ND
1
0.80
0.15
ug/L
08/04/2020 1029
Hexachlorobutadiene
ND
1
0.80
0.17
ug/L
08/04/2020 1029
Hexachlorocyclopentadiene
ND
1
4.0
1.1
ug/L
08/04/2020 1029
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 73

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ61942-001 Matrix: Aqueous
Batch: 61942 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 07/31/2020 1622
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Hexachloroethane
ND
1
0.80
0.17
ug/L
08/04/20201029
Indeno(1,2,3-c,d)pyrene
ND
1
0.16
0.040
ug/L
08/04/20201029
Isophorone
ND
1
0.80
0.22
ug/L
08/04/20201029
2-Methyl naphthalene
ND
1
0.16
0.040
ug/L
08/04/20201029
2-Methylphenol
ND
1
0.80
0.21
ug/L
08/04/20201029
3+4-Methylphenol
ND
1
1.6
0.46
ug/L
08/04/20201029
Naphthalene
ND
1
0.16
0.040
ug/L
08/04/20201029
2-Nitroaniline
ND
1
1.6
0.66
ug/L
08/04/20201029
3-Nitroaniline
ND
1
1.6
0.15
ug/L
08/04/20201029
4-Nitroaniline
ND
1
1.6
1.3
ug/L
08/04/20201029
Nitrobenzene
ND
1
0.80
0.17
ug/L
08/04/20201029
2-Nitrophenol
ND
1
1.6
0.44
ug/L
08/04/20201029
4-Nitrophenol
ND
1
4.0
2.1
ug/L
08/04/20201029
N-Nitrosodi-n-propylamine
ND
1
0.80
0.28
ug/L
08/04/20201029
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
0.80
0.50
ug/L
08/04/2020 1029
Pentachlorophenol
ND
1
4.0
1.3
ug/L
08/04/20201029
Phenanthrene
ND
1
0.16
0.040
ug/L
08/04/20201029
Phenol
ND
1
0.80
0.19
ug/L
08/04/20201029
Pyrene
ND
1
0.16
0.040
ug/L
08/04/20201029
2,4,5-Trichlorophenol
ND
1
0.80
0.19
ug/L
08/04/20201029
2,4,6-Trichlorophenol
ND
1
0.80
0.22
ug/L
08/04/20201029
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 61 37-129
2-Fluorophenol 29 24-127
Nitrobenzene-d5 68 38-127
Phenol-d5 60 28-128
Terphenyl-d 14 85 10-148
2,4,6-Tribromophenol 59 35-144
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 42 of 73

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ61942-002
Matrix:
Aqueous
Batch: 61942
Prep Method:
3520C
Analytical Method: 8270E
Prep Date:
07/31/2020 1622
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
8.0
4.7
1
59
30-122
08/04/2020 1054
Acenaphthylene
8.0
5.3
1
66
30-130
08/04/2020 1054
Acetophenone
8.0
8.0
1
100
52-125
08/04/2020 1054
Anthracene
8.0
6.1
1
76
30-123
08/04/2020 1054
Atrazine
8.0
7.3
1
92
25-121
08/04/2020 1054
Benzaldehyde
8.0
5.4
1
67
20-115
08/04/2020 1054
Benzo(a)anthracene
8.0
6.6
1
83
40-125
08/04/2020 1054
Benzo(a)pyrene
8.0
6.0
1
74
40-128
08/04/2020 1054
Benzo(k)fluoranthene
8.0
5.9
1
74
30-130
08/04/2020 1054
Benzo(g,h,i)perylene
8.0
7.3
1
92
30-130
08/04/2020 1054
Benzo(k)fluoranthene
8.0
6.9
1
86
30-130
08/04/2020 1054
1,1'-Biphenyl
8.0
4.8
1
61
42-120
08/04/2020 1054
4-Bromophenyl phenyl ether
8.0
5.0
1
62
30-124
08/04/2020 1054
Butyl benzyl phthalate
8.0
7.8
1
97
54-135
08/04/2020 1054
Caprolactam
8.0
11
1
137
44-152
08/04/2020 1054
Carbazole
8.0
5.8
1
72
45-101
08/04/2020 1054
bis (2-Chloro-1-methylethyl) ether
8.0
7.7
1
96
42-124
08/04/2020 1054
4-Chloro-3-methyl phenol
8.0
5.3
1
66
30-123
08/04/2020 1054
4-Chloroaniline
8.0
3.7
1
47
12-157
08/04/2020 1054
bis(2-Chloroethoxy)methane
8.0
4.7
1
59
44-127
08/04/2020 1054
bis(2-Chloroethyl)ether
8.0
7.3
1
91
46-120
08/04/2020 1054
2-Chloronaphthalene
8.0
4.7
1
58
46-100
08/04/2020 1054
2-Chlorophenol
8.0
5.5
1
68
50-117
08/04/2020 1054
4-Chlorophenyl phenyl ether
8.0
4.8
1
60
30-121
08/04/2020 1054
Chrysene
8.0
6.1
1
76
30-130
08/04/2020 1054
Dibenzo(a,h)anthracene
8.0
6.9
1
86
30-130
08/04/2020 1054
Dibenzofuran
8.0
4.8
1
60
30-118
08/04/2020 1054
3,3'-Dichlorobenzidine
8.0
4.2
1
53
10-126
08/04/2020 1054
2,4-Dichlorophenol
8.0
4.4
1
55
30-121
08/04/2020 1054
Diethylphthalate
8.0
6.3
1
79
40-125
08/04/2020 1054
Dimethyl phthalate
8.0
5.7
1
71
40-127
08/04/2020 1054
2,4-Dimethylphenol
8.0
6.0
1
75
20-125
08/04/2020 1054
Di-n-butyl phthalate
8.0
6.9
1
86
40-127
08/04/2020 1054
4,6-Dinitro-2-methyl phenol
8.0
5.8
1
73
56-128
08/04/2020 1054
2,4-Dinitrophenol
16
9.7
1
61
11-126
08/04/2020 1054
2,4-Dinitrotoluene
8.0
6.4
1
80
59-127
08/04/2020 1054
2,6-Dinitrotoluene
8.0
5.9
1
73
59-126
08/04/2020 1054
Di-n-octylphthalate
8.0
6.8
1
85
50-136
08/04/2020 1054
bis(2-Ethylhexyl)phthalate
8.0
8.8
1
110
56-128
08/04/2020 1054
Fluoranthene
8.0
5.5
1
69
40-128
08/04/2020 1054
Fluorene
8.0
4.8
1
60
30-124
08/04/2020 1054
Hexachlorobenzene
8.0
4.9
1
61
30-125
08/04/2020 1054
Hexachlorobutadiene
8.0
3.5
1
44
24-110
08/04/2020 1054
Hexachlorocyclopentadiene
40
16
1
41
16-96
08/04/2020 1054
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 43 of 73

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ61942-002
Matrix:
Aqueous
Batch: 61942
Prep Method:
3520C
Analytical Method: 8270E
Prep Date:
07/31/2020 1622
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Hexachloroethane
8.0
4.0
1
50
31-110
08/04/20201054
Indeno(1,2,3-c,d)pyrene
8.0
6.7
1
84
30-130
08/04/20201054
Isophorone
8.0
6.3
1
79
57-123
08/04/20201054
2-Methyl naphthalene
8.0
4.5
1
56
40-132
08/04/20201054
2-Methylphenol
8.0
9.4
1
117
56-119
08/04/20201054
3+4-Methylphenol
8.0
8.5
1
107
53-119
08/04/20201054
Naphthalene
8.0
4.4
1
55
30-130
08/04/20201054
2-Nitroaniline
8.0
6.1
1
76
60-124
08/04/20201054
3-Nitroaniline
8.0
4.5
1
56
43-123
08/04/20201054
4-Nitroaniline
8.0
5.1
1
64
30-135
08/04/20201054
Nitrobenzene
8.0
5.5
1
69
51-122
08/04/20201054
2-Nitrophenol
8.0
5.0
1
63
51-118
08/04/20201054
4-Nitrophenol
16
11
1
70
53-130
08/04/20201054
N-Nitrosodi-n-propylamine
8.0
8.8
1
110
54-127
08/04/20201054
N-Nitrosodiphenylamine (Diphenylamine) 8.0
5.6
1
70
30-123
08/04/2020 1054
Pentachlorophenol
16
9.3
1
58
42-131
08/04/20201054
Phenanthrene
8.0
5.0
1
62
40-123
08/04/20201054
Phenol
8.0
6.1
1
77
49-117
08/04/20201054
Pyrene
8.0
6.8
1
84
40-126
08/04/20201054
2,4,5-Trichlorophenol
8.0
4.6
1
58
30-123
08/04/20201054
2,4,6-Trichlorophenol
8.0
5.0
1
62
30-125
08/04/20201054
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 55 37-129
2-Fluorophenol 38 24-127
Nitrobenzene-d5 61 38-127
Phenol-d5 81 28-128
Terphenyl-d 14 77 10-148
2,4,6-Tribromophenol 59 35-144
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 44 of 73

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ62822-001 Matrix: Solid
Batch: 62822 Prep Method: 3546
Analytical Method: 8270E Prep Date: 08/07/2020 2039
Parameter Result Q Dil LOQ DL Units Analysis Date
4,6-Dinitro-2-methyl phenol ND 1 67 25 ug/kg 08/08/20201351
2,4-Dinitrophenol ND 1 67 25 ug/kg 08/08/20201351
Surrogate
Acceptance
Q % Rec Limit
2-Fluorobiphenyl
73
33-102
2-Fluorophenol
95
35-115
Nitrobenzene-d5
79
22-109
Phenol-d5
113
33-122
Terphenyl-d14
90
41-120
2,4,6-Tribromophenol
72
30-117
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 45 of 73

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ62822-002
Matrix:
Solid
Batch: 62822
Prep Method:
3546
Analytical Method: 8270E
Prep Date:
08/07/2020 2039
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit Analysis Date
4,6-Dinitro-2-methyl phenol
130
95
1
71
40-130 08/08/20201416
2,4-Dinitrophenol
270
100
1
38
32-115 08/08/20201416
Surrogate
Q % Rec
Acceptance
Limit
2-Fluorobiphenyl
67
33-102
2-Fluorophenol
93
35-115
Nitrobenzene-d5
80
22-109
Phenol-d5
103
33-122
Terphenyl-d14
86
41-120
2,4,6-Tribromophenol
79
30-117
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 46 of 73

MA EPH (aliphatics) - MB
Sample ID: VQ62124-001 Matrix: Solid
Batch: 62124 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/03/2020 1348
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics ND 1 10 10 mg/kg 08/07/2020 1856
C19 - C36 Aliphatics ND 1 10 10 mg/kg 08/07/2020 1856
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 51 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 47 of 73

MA EPH (aliphatics) - LCS
Sample ID: VQ62124-002
Matrix:
Solid
Batch: 62124
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/03/2020 1348
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg)
Q Dil
% Rec
Limit Analysis Date
C9 - C18 Aliphatics
30
14
1
48
40-140 08/07/2020 1927
C19 - C36 Aliphatics
40
25
1
62
40-140 08/07/2020 1927
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 52 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 48 of 73

MA EPH (aliphatics) - LCSD
Sample ID: VQ62124-003
Matrix:
Solid
Batch: 62124
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/03/2020 1348
Spike
Amount
Result
% Rec
% RPD
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec
% RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
30
15
1 50
3.9 40-140
25 08/07/2020 1958
C19 - C36 Aliphatics
40
27
1 68
9.2 40-140
25 08/07/2020 1958
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 56 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 49 of 73

MA EPH (aromatics) - MB
Sample ID: VQ62125-001 Matrix: Solid
Batch: 62125 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/03/2020 1348
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 10 10 mg/kg 08/07/2020 2300
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 82 40-140
2-Fluorobiphenyl (fractionation 1) 79 40-140
o - Terphenyl (aromatic) 73 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 50 of 73

MA EPH (aromatics) - LCS
Sample ID: VQ62125-002
Matrix:
Solid
Batch: 62125
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/03/2020 1348
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg) Q
Dil
% Rec Limit Analysis Date
C11 - C22 Aromatics
85
52
1
61 40-140 08/07/2020 2330
Acceptance
Surrogate
Q % Rec
Limit
2-Bromonaphthalene (fractionation 2) 84 40-140
2-Fluorobiphenyl (fractionation 1) 81 40-140
o - Terphenyl (aromatic) 78 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 51 of 73

MA EPH (aromatics) - LCSD
Sample ID: VQ62125-003 Matrix: Solid
Batch: 62125 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/03/2020 1348
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 85 57 1 67 10 40-140 25 08/08/2020 0000
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 90 40-140
2-Fluorobiphenyl (fractionation 1) 86 40-140
o - Terphenyl (aromatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 52 of 73

MADEP EPH (aliphatics) - Unfractionated - MB
Sample ID: VQ63151-001 Matrix: Aqueous
Batch: 63151 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/03/2020 1535
Parameter Result Q Dil LOQ DL Units Analysis Date
C19 - C36 Aliphatics - Unfractionated ND 1 100 100 ug/L 08/11/2020 1318
C9 - C18 Aliphatics - Unfractionated ND 1 100 100 ug/L 08/11/2020 1318
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 50 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 53 of 73

MADEP EPH (aliphatics) - Unfractionated - LCS
Sample ID: VQ63151-002
Matrix:
Aqueous
Batch: 63151
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/03/2020 1535
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit Analysis Date
C19 - C36 Aliphatics - Unfractionated
900
690
1
77
40-140 08/11/2020 1348
C9 - C18 Aliphatics - Unfractionated
650
410
1
63
40-140 08/11/2020 1348
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 72 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 54 of 73

MADEP EPH (aliphatics) - Unfractionated - LCSD
Sample ID: VQ63151-003
Matrix:
Aqueous
Batch: 63151
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/03/2020 1535
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
% RPD Limit
Limit Analysis Date
C19 - C36 Aliphatics - Unfractionated
900
660
1 73
5.2 40-140
25 08/11/2020 1419
C9 - C18 Aliphatics - Unfractionated
650
350
1 55
14 40-140
25 08/11/2020 1419
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 64 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 55 of 73

MADEP EPH (aromatics) - Unfractionated - MB
Sample ID: VQ63154-001 Matrix: Aqueous
Batch: 63154 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/03/2020 1535
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics - Unfractionated ND 1 100 100 ug/L 08/11/2020 1318
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) - Unfractionated
63
40-140
2-Fluorobiphenyl (fractionation 1)
78
40-140
2-Bromonaphthalene (fractionation 2)
84
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 56 of 73

MADEP EPH (aromatics) - Unfractionated - LCS
Sample ID: VQ63154-002
Matrix:
Aqueous
Batch: 63154
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/03/2020 1535
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec Limit Analysis Date
C11 - C22 Aromatics - Unfractionated
1400
830
1
60 40-140 08/11/2020 1348
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) - Unfractionated
76
40-140
2-Fluorobiphenyl (fractionation 1)
95
40-140
2-Bromonaphthalene (fractionation 2)
104
40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 57 of 73

MADEP EPH (aromatics) - Unfractionated - LCSD
Sample ID: VQ63154-003
Matrix:
Aqueous
Batch: 63154
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/03/2020 1535
Spike
Amount
Result
% Rec % RPD
Parameter
(ug/L)
(ug/L) Q Dil % Rec
% RPD Limit Limit Analysis Date
C11 - C22 Aromatics - Unfractionated
1400
770 1 55
8.4 40-140 25 08/11/2020 1419
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) - Unfractionated
67
40-140
2-Fluorobiphenyl (fractionation 1)
86
40-140
2-Bromonaphthalene (fractionation 2)
94
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 58 of 73

MADEP VPH (aliphatics) - MB
Sample ID: VQ62146-001 Matrix: Aqueous
Batch: 62146 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C5 - C8 Aliphatics ND 1 75 15 ug/L 08/03/2020 1233
C9 - C12 Aliphatics ND 1 75 15 ug/L 08/03/2020 1233
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
120 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 59 of 73

MADEP VPH (aliphatics) - LCS
Sample ID: VQ62146-002
Matrix:
Aqueous
Batch: 62146
Prep Method:
VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit Analysis Date
C5 - C8 Aliphatics
150
160
1
107
70-130 08/03/2020 1136
C9 - C12 Aliphatics
180
180
1
103
70-130 08/03/2020 1136
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
106 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 60 of 73

MADEP VPH (aliphatics) - LCSD
Sample ID: VQ62146-003
Matrix: Aqueous
Batch: 62146
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD
Limit
Limit Analysis Date
C5 - C8 Aliphatics
150
160
1 105 1.3
70-130
25 08/03/2020 1204
C9 - C12 Aliphatics
180
180
1 102 0.73
70-130
25 08/03/2020 1204
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
111 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 61 of 73

MADEP VPH (aliphatics) - MB
Sample ID: VQ62147-001 Matrix: Solid
Batch: 62147 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C5 - C8 Aliphatics ND 1 3.8 0.75 mg/kg 08/03/2020 1428
C9 - C12 Aliphatics ND 1 3.8 0.75 mg/kg 08/03/2020 1428
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
118 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 62 of 73

MADEP VPH (aliphatics) - LCS
Sample ID: VQ62147-002
Matrix: Solid
Batch: 62147
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg)
Q Dil % Rec
Limit Analysis Date
C5 - C8 Aliphatics
7.5
8.0
1 107
70-130 08/03/2020 1330
C9 - C12 Aliphatics
8.8
10
1 114
70-130 08/03/2020 1330
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
116 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 63 of 73

MADEP VPH (aliphatics) - LCSD
Sample ID: VQ62147-003
Matrix: Solid
Batch: 62147
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
% RPD
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec % RPD
Limit
Limit Analysis Date
C5 - C8 Aliphatics
7.5
8.2
1 110 2.1
70-130
25 08/03/2020 1359
C9 - C12 Aliphatics
8.8
10
1 117 2.0
70-130
25 08/03/2020 1359
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
120 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 64 of 73

MADEP VPH (aromatics) - MB
Sample ID: VQ62149-001 Matrix: Aqueous
Batch: 62149 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C10 Aromatics ND 1 25 5.0 ug/L 08/03/2020 1233
Surrogate
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
116 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 65 of 73

MADEP VPH (aromatics) - LCS
Sample ID: VQ62149-002 Matrix: Aqueous
Batch: 62149 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 25 25 1 102 70-130 08/03/2020 1136
Surrogate
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
104 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 66 of 73

MADEP VPH (aromatics) - LCSD
Sample ID: VQ62149-003 Matrix: Aqueous
Batch: 62149 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 25 26 1 103 1.2 70-130 25 08/03/2020 1204
Surrogate
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
107 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 67 of 73

MADEP VPH (aromatics) - MB
Sample ID: VQ62150-001 Matrix: Solid
Batch: 62150 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C10 Aromatics ND 1 1.3 0.50 mg/kg 08/03/2020 1428
Surrogate
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
117 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 68 of 73

MADEP VPH (aromatics) - LCS
Sample ID: VQ62150-002 Matrix: Solid
Batch: 62150 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 1.3 1.4 1 112 70-130 08/03/2020 1330
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
112 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 69 of 73

MADEP VPH (aromatics) - LCSD
Sample ID: VQ62150-003 Matrix: Solid
Batch: 62150 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 1.3 1.4 1 112 0.00 70-130 25 08/03/2020 1359
Surrogate
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
125 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 70 of 73

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 71 of 73

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 72 of 73

PACE ANALYTICAL SERVICES, LLC
Shrnlg ErMroaws 4l S:n ice4 ins
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SnmpJe€(s) MA _ %veer, rrL:cived urLTi; TRC � 0.5 mgrL (If f IY is pro) aasd woFe
adjusted a€ppr6;ngly J:s sample resMM!ltg v.'id3 sodium thi❑sulfate (Na3, Q3) `ith t;:tealy In: NA
SR barkade Ialeels Hit -flied by' ZMG late; 07129.2020
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 73 of 73

Beverly, Trudy
From: Beverly, Trudy
Sent: Wednesday, August 19, 2020 3:13 PM
To: Patrick Lowery
Subject: RE: [External] Phase I LSA - Incident #s 47013 & 47014 - Curry Vail LLC
Received.
Trudy
Trudy Beverly, L.G.
D
IE �1
Hydrogeologist, Division of Waste Management
_ North Carolina Department of Environmental Quality
Q�
LF Pa.rI n. of Lnorun,w 0MOT ` UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hgps:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deu.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
ht_pt s://deq.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
htt2s://deg.nc.gov/about/divisions/waste-mana2ement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.eov/nedea/Waste%2OMana2ement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc.gov/ncdeg/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Patrick Lowery [mailto:[e-mail]]
Sent: Wednesday, August 19, 2020 3:05 PM
To: Beverly, Trudy <[e-mail]>
Subject: [External] Phase I LSA - Incident #s 47013 & 47014 - Curry Vail LLC
• External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
llllllllllllllll�nc.gov
Trudy,
Please find attached a copy of the LSA completed for the Curry Vail LLC properties. These parcels were side by side and
each contained a heating oil UST. We completed an assessment of each UST for the perspective purchaser and found
that clean soils beneath the UST at 2547 Vail Ave (47013). At 2553 Vail Ave (47014), impacted soils were encountered to
a depth of 16 ft where probe refusal was encountered. A LSA well was installed for this incident. The well was located
as close as possible to the UST basin, but due to clearance and access issues, the LSA well was installed —25ft
downgradient of the source area.
Please let me know if you have any questions.
Thank you,
Patrick

II -AL -
SUMMIT
PATRICK W. LOWERY, P.G.
Senior Environmental Manager
[e-mail]
Columbia Office • 101 Rice Bent Way, Unit 9 • Columbia, SC 29229
803.708.7945 Office • 803.708.7946 Fax • 803.230.5087 Cell
www.summit-companies.com
Charlotte -HQ • Raleigh • Columbia • Greenville • Charleston