6002_Mecklenburg_HolbrooksRoad_MSWLF_Sept2020GW_FID1456548_20201005

IDENR USE ONLY: I I ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Holbrooks Road Landfill 15401 Holbrooks Road 60-02 .0500 September 15-16, 2020,
September 22, 2020
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑X
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data
Surface water monitoring data ❑
Notification attached?
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC S01id Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G.
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
Project Manager
980-314-3855
�Hrea toae� i eiepnone ivumoer
Affix NC Licensed/ Professional Geologist Seal
PE Firm License Number (if applicable effective May 1,
Revised 6/2009

MECKLENBURU COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
October 5, 2020
Jaclynne Drummond
North Carolina Department of Environment
and Natural Resources
Division of Waste Management
2090 US Highway 70
Swannanoa, NC 28778
Subject: Holbrooks Road Landfill Permit 60-02
Semi-annual Monitoring Results
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Holbrooks Road Landfill in September 15-16, 2020 in accordance with the approved
sample and analysis plan dated March 27, 2003. This report details the results of that
monitoring event. Laboratory analytical data, field -measured data table of values
exceeding 2L standards and landfill gas monitoring data is contained on the electronic
data deliverable submittal.
Samples were collected from fourteen (14) monitoring wells (HRW-7, HRW-8, HRW-
9R, HRW-10, HRW-11 R, HRW-12, HRW-13, HRW-14, HRW-15, HRW-16, HRW-17,
HRW48, HRW-19, HRW-20, and HRW-21) and three (3) surface -water sampling
locations (HRSW-2, HRSW-3 and HRSW-4). Samples were analyzed for metals and
volatile organic compounds ("VOCs") listed in Appendix I of 40 CFR Part
258.54 "Detection monitoring program". Samples were also analyzed for 1,4-Dioxane
as required as of July 1, 2018. Field measurements of temperature, pH, and specific
conductivity were made at each sampling location using a calibrated instrument.
Additionally, measurements of dissolved oxygen were made at each surface -water
sampling location.
The electronic data deliverable package containing the monitoring data is labeled to
reflect the units used for reporting. Surface water standards listed are the water quality
standards established for freshwater classification for aquatic life as outlined in 15A
NCAC 2B "Classification and Water Quality Standards Applicable to Surface Waters of
North Carolina". Groundwater standards listed are the standards outlined in 15A NCAC
2L "Classification of Water Quality Standards applicable to the Groundwaters of North
Carolina". If the sample is reported in parts per billion, then the standard is also reported
in parts per billion.
PEOPLE •PRIDE PROGRESS •PARTNERSHIP
2145 Suttle Ave •Charlotte, North Carolina 28208 • [phone]
www.wipeoutwastea com

Page 2
Surface -water samples:
No VOCs were detected in any of the samples collected from the three surface -water
sampling locations (HRSW-2, HRSW-4 and HRSW-3). Barium was detected in all three
sampling locations below the 2B standards at 56.6, 47.7 and 50.5 ug/l, respectively.
Copper was detected in HRSW-2 and HRSW-3 below the 2 B standards at 6 and 5.7 ug/l,
respectively. Vanadium was detected in all three sampling locations at 10. 1, 7.3 and 8.9
ug/l, respectively. The stream was turbid in appearance, likely from construction adjacent
to the landfill. All field -measured parameters were within the established regulatory
limits. The following table summarizes field -measured parameters for surface water
samples.
Sample Location
Temp.
°C
pH
S.U.
Specific Conductivity
ms/cm
Dissolved Oxygen
mg/1
HRSW-2 upstream
22.3
7.2
0.275
8.35
HRSW-4 mid -stream
21.9
7.3
0.274
8.46
HRSW-3 downstream
21.5
T4
0.290
7.99
Groundwater samples:
Metals were detected in various wells above the 21 standard. The following table
summarizes metals detection for groundwater samples.
Well ID
As
ug/1
Ba
ug/1
Cd
ug/l
Cr
ug/1
Co
ug/1
Cu
ug/l
Pb
ug/l
Ni
ug/1
Sb
ug/1
Se
ug/1
Vn
ug/1
Zn
ug/l
HRW-7
-----
203
4.4
-----
-----
6.5
-----
-----
-----
-----
14.2
13.4
HRW-8
-----
171
-----
6.0
25.8
13.0
-----
-----
-----
-----
26.5
12.8
HRW-9R
-----
568
-----
2092
19.6
143
5.2
1209
-----
-----
120
56.4
HRW40
-----
237
-----
-----
-----
-----
-----
14.1
-----
-----
-----
-----
HRW41R
-----
385
-----
-----
16.6
-----
-----
53.5
-----
-----
15.2
-----
HRW42
-----
820
2.0
-----
58.8
134
-----
170
-----
----
10.8
-----
HRW4 3
-----
160
-----
13.8
6.6
19.5
5.2
9.1
-----
-----
22.3
21.3
HRW44
-----
33.0
-----
-----
-----
-----
-----
-----
-----
-----
7.9
-----
HRW4 5
-----
143
-----
15.4
12.0
101
7.9
5.8
-----
-----
80.1
44.0
HRW46
-----
152
-----
7.8
-----
22.6
-----
5.4
-----
-----
32.7
17.4
HRW47
-----
58.8
-----
-----
-----
-----
-----
-----
-----
-----
5.1
-----
HRW4 8
-----
318
-----
-----
6.8
-----
-----
8.7
-----
-----
2092
-----
HRW49
-----
87.8
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-20
-----
104
-----
-----
-----
-----
-----
-----
-----
-----
6.9
-----
HRW-21
-----
66.1
-----
-----
-----
-----
-----
-----
-----
-----
6.1
-----
2L Std.
10
700
2
10
1
100
15
100
1
20
0.3
1,000
Note: Results shown in bold exceed the 2L standard.

VOCs were detected in eight monitoring wells; HRW-7, HRW-9R, HRW-10, HRW-11R,
HRW-12, HRW-14, HRW-18 and HRW-20. 1,4-Dioxane was detected above the 21
standard in 5 monitoring wells.
The following table summarizes VOC detections.
Well ID
Volatile Constituent
Concentration
2L Standard
u /1
(u /1)
HRW-7
Benzene
196
1
cis- 1,2-Dichloroethene
8.8
70
Trichloroethene
1.8
3
HRW-9R
Chlorobenzene
1.3
50
Chloroethane
6.7
3000
1,2-Dichorobenzene
2.4
20
1,4-Dichlorobenzene
3.1
6
l,I-Dichloroethane
14.3
6
1,2-Dichloroethane
1.9
0.4
cis- 1,2-Dichloroethane
31.7
70
1,2-Dichloropropane
2.1
0.6
1,4-Dioxane
8.9
3
HRW40
Chloroethane
2.7
3000
1,4-Dioxane
10.3
3
HRW41R
1,4-Dioxane
163
3
HRW42
Benzene
1.0
1
Chloroethane
2.2
3000
1,1-Dichloroethane
7.7
6
1,4-Dioxane
181
3
HRW44
Tetrachloroethene
1.4
M
HRW4 8
Benzene
1.6
1
Chloroethane
2.4
3 000
1,1-Dichloroethane
30.5
6
cis -I, 2-Dichloroethene
2.3
70
1,2-Dichloropropane
497
0.6
Vinyl Chloride
12.7
0.03
1,4-Dioxane
6.8
3
HRW-20
1,1-Dichloroethane
5.4
6
Note: Results shown in bold exceed the 2L standard.

Page 4
Measurements of pH were more acidic than the 2L standard range of 6.5 to 8.5 standard
units at locations HRW-7, HRW4, HRW-11R, HRW-13, HRW-16, HRW47 and HRW-
20. Field- measured parameters for groundwater samples are summarized in the
following table.
Sample Location
Tem . °C
PH
Specific Conductivity ms/cm
HRW-7
1994
6.1
0.729
HRW4
16.7
5.8
0.211
HRW-9R
15.7
6.7
1.308
HRW-10
18.7
6.6
0.888
HRW41R
17.9
6A
2.176
HRW4 2
15.7
6.5
2.172
HRW4 3
18.2
6.1
0.394
HRW44
15.6
6.5
0.206
HRW-15
16.0
6.4
0.249
HRW-16
18.2
5.8
0.176
HRW47
16.3
6.7
0.202
HRW-18
17.6
6.3
1.475
HRW49
16.2
6.3
0.337
HRW-20
16.0
6.0
0.344
HRW-21
17A
6.5
0.489
Note: Results shown in bold are outside of the 21, standard range of 6.5 - 8.5 S.U.
Please contact me at amber.grzymslci(a�,mecklenbur cg ountync.�ov or [phone] if
you have any questions regarding this report.
Ste:
187�"
Sincerely,
Amber R. Grzymski, P.G.
Project Manager
Solid Waste Services

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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 29, 2020
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 15, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92495550001 6002-HRW7
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495550002 6002-HRW18
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495550003 6002-HRW19
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495550004 6002-HRW20
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495550005 6002-HRW21
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495550006 TRIP BLANK
EPA 8260D
SAS
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW7
Lab ID: 92495550001 Collected:
09/15/20
10:59
Received: 09/15/20 13:55 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:41
7440-38-2
Barium
203
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:41
7440-41-7
Cadmium
4.4
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:41
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7440-48-4
Copper
6.5
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7439-92-1
Nickel
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:41
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:41
7440-28-0
Vanadium
14.2
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:41
7440-62-2
Zinc
13.4
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:41
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/24/20 01:11
09/24/20 17:15
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 16:14
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 16:14
107-13-1
Benzene
1.6
ug/L
1.0
1
09/24/20 16:14
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 16:14
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 16:14
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 16:14
75-25-2 IK,v2
Bromomethane
ND
ug/L
2.0
1
09/24/20 16:14
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 16:14
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 16:14
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 16:14
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 16:14
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/24/20 16:14
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 16:14
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 16:14
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 16:14
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 16:14
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 16:14
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 16:14
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 16:14
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 16:14
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 16:14
110-57-6 v2
1,1-Dichloroethane
ND
ug/L
1.0
1
09/24/20 16:14
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 16:14
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW7 Lab ID: 92495550001 Collected: 09/15/20 10:59 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:14
75-35-4
cis-1,2-Dichloroethene
8.8
ug/L
1.0
1
09/24/20 16:14
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:14
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:14
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:14
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/24/20 16:14
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/24/20 16:14
591-78-6
lodomethane
ND
ug/L
20.0
1
09/24/20 16:14
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/24/20 16:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/24/20 16:14
108-10-1
Styrene
ND
ug/L
1.0
1
09/24/20 16:14
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:14
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:14
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/24/20 16:14
127-18-4
Toluene
ND
ug/L
1.0
1
09/24/20 16:14
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:14
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:14
79-00-5
Trichloroethene
1.8
ug/L
1.0
1
09/24/20 16:14
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/24/20 16:14
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/24/20 16:14
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/24/20 16:14
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/24/20 16:14
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/24/20 16:14
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/24/20 16:14
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/24/20 16:14
95-47-6
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
09/24/20 16:14
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
09/24/20 16:14
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
09/24/20 16:14
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/17/20 17:42
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
94
%
50-150
1
09/17/20 17:42
17060-07-0
Toluene-d8 (S)
101
%
50-150
1
09/17/20 17:42
2037-26-5
Date: 09/29/2020 12:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW18
Lab ID: 92495550002 Collected:
09/15/20
10:42
Received: 09/15/20 13:55 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:44
7440-38-2
Barium
318
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:44
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:44
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7440-47-3
Cobalt
6.8
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7440-48-4
Copper
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7439-92-1
Nickel
8.7
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:44
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:44
7440-28-0
Vanadium
20.2
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:44
7440-62-2
Zinc
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:44
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/24/20 01:11
09/24/20 17:18
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 16:49
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 16:49
107-13-1
Benzene
1.6
ug/L
1.0
1
09/24/20 16:49
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 16:49
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 16:49
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 16:49
75-25-2 IK,v2
Bromomethane
ND
ug/L
2.0
1
09/24/20 16:49
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 16:49
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 16:49
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 16:49
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 16:49
108-90-7
Chloroethane
2.4
ug/L
1.0
1
09/24/20 16:49
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 16:49
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 16:49
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 16:49
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 16:49
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 16:49
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 16:49
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 16:49
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 16:49
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 16:49
110-57-6 v2
1,1-Dichloroethane
30.5
ug/L
1.0
1
09/24/20 16:49
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 16:49
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW18 Lab ID: 92495550002 Collected: 09/15/20 10:42 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:49
75-35-4
cis-1,2-Dichloroethene
2.3
ug/L
1.0
1
09/24/20 16:49
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:49
156-60-5
1,2-Dichloropropene
4.7
ug/L
1.0
1
09/24/20 16:49
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:49
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:49
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/24/20 16:49
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/24/20 16:49
591-78-6
lodomethane
ND
ug/L
20.0
1
09/24/20 16:49
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/24/20 16:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/24/20 16:49
108-10-1
Styrene
ND
ug/L
1.0
1
09/24/20 16:49
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:49
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:49
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/24/20 16:49
127-18-4
Toluene
ND
ug/L
1.0
1
09/24/20 16:49
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:49
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:49
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/24/20 16:49
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/24/20 16:49
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/24/20 16:49
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/24/20 16:49
108-05-4
Vinyl chloride
12.7
ug/L
1.0
1
09/24/20 16:49
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/24/20 16:49
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/24/20 16:49
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/24/20 16:49
95-47-6
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
09/24/20 16:49
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
09/24/20 16:49
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
09/24/20 16:49
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
6.8
ug/L
2.0
1
09/17/20 19:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
104
%
50-150
1
09/17/20 19:17
17060-07-0
Toluene-d8 (S)
100
%
50-150
1
09/17/20 19:17
2037-26-5
Date: 09/29/2020 12:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW19 Lab ID: 92495550003 Collected: 09/15/20 10:09 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 17:45
09/25/20 01:29
7440-38-2
Barium
87.8
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 17:45
09/25/20 01:29
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/23/20 17:45
09/25/20 01:29
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7440-47-3 P8
Cobalt
ND
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7440-48-4
Copper
ND
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7439-92-1
Nickel
ND
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 17:45
09/25/20 01:29
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 17:45
09/25/2018:40
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/23/20 17:45
09/25/20 01:29
7440-62-2
Zinc
ND
ug/L
10.0
1
09/23/20 17:45
09/25/20 01:29
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
Date: 09/29/2020 12:40 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND
ug/L
0.10
1
09/24/20 01:11 09/24/20 17:22
7440-28-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
09/24/2016:31
67-64-1
ND
ug/L
10.0
1
09/24/2016:31
107-13-1
ND
ug/L
1.0
1
09/24/2016:31
71-43-2
ND
ug/L
1.0
1
09/24/2016:31
74-97-5
ND
ug/L
1.0
1
09/24/2016:31
75-27-4
ND
ug/L
1.0
1
09/24/2016:31
75-25-2 IK,v2
ND
ug/L
2.0
1
09/24/2016:31
74-83-9 v2
ND
ug/L
5.0
1
09/24/2016:31
78-93-3
ND
ug/L
2.0
1
09/24/2016:31
75-15-0
ND
ug/L
1.0
1
09/24/2016:31
56-23-5
ND
ug/L
1.0
1
09/24/2016:31
108-90-7
ND
ug/L
1.0
1
09/24/2016:31
75-00-3
ND
ug/L
5.0
1
09/24/2016:31
67-66-3
ND
ug/L
1.0
1
09/24/2016:31
74-87-3
ND
ug/L
5.0
1
09/24/2016:31
96-12-8
ND
ug/L
1.0
1
09/24/2016:31
124-48-1
ND
ug/L
1.0
1
09/24/2016:31
106-93-4
ND
ug/L
1.0
1
09/24/2016:31
74-95-3
ND
ug/L
1.0
1
09/24/2016:31
95-50-1
ND
ug/L
1.0
1
09/24/2016:31
106-46-7
ND
ug/L
1.0
1
09/24/2016:31
110-57-6 v2
ND
ug/L
1.0
1
09/24/2016:31
75-34-3
ND
ug/L
1.0
1
09/24/2016:31
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW19 Lab ID: 92495550003 Collected: 09/15/20 10:09 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:31
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:31
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:31
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:31
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:31
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:31
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/24/20 16:31
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/24/20 16:31
591-78-6
lodomethane
ND
ug/L
20.0
1
09/24/20 16:31
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/24/20 16:31
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/24/20 16:31
108-10-1
Styrene
ND
ug/L
1.0
1
09/24/20 16:31
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:31
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:31
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/24/20 16:31
127-18-4
Toluene
ND
ug/L
1.0
1
09/24/20 16:31
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:31
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:31
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/24/20 16:31
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/24/20 16:31
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/24/20 16:31
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/24/20 16:31
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/24/20 16:31
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/24/20 16:31
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/24/20 16:31
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/24/20 16:31
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/24/20 16:31
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
09/24/20 16:31
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
09/24/20 16:31
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/17/20 18:01
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
50-150
1
09/17/20 18:01
17060-07-0
Toluene-d8 (S)
101
%
50-150
1
09/17/20 18:01
2037-26-5
Date: 09/29/2020 12:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW20
Lab ID: 92495550004 Collected:
09/15/20
10:26
Received: 09/15/20 13:55 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:48
7440-38-2
Barium
104
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:48
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:48
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7440-48-4
Copper
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7439-92-1
Nickel
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:48
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:48
7440-28-0
Vanadium
6.9
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:48
7440-62-2
Zinc
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:48
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/24/20 01:11
09/24/20 17:26
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 15:56
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 15:56
107-13-1
Benzene
ND
ug/L
1.0
1
09/24/20 15:56
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 15:56
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 15:56
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 15:56
75-25-2 IK,v2
Bromomethane
ND
ug/L
2.0
1
09/24/20 15:56
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 15:56
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 15:56
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 15:56
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 15:56
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/24/20 15:56
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 15:56
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 15:56
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 15:56
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 15:56
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 15:56
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 15:56
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 15:56
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 15:56
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 15:56
110-57-6 v2
1,1-Dichloroethane
5.4
ug/L
1.0
1
09/24/20 15:56
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 15:56
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW20 Lab ID: 92495550004 Collected: 09/15/20 10:26 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/29/2020 12:40 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
101
%
96
%
105
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
97 %
101 %
1.0
1
09/24/20 15:56
75-35-4
1.0
1
09/24/20 15:56
156-59-2
1.0
1
09/24/20 15:56
156-60-5
1.0
1
09/24/20 15:56
78-87-5
1.0
1
09/24/20 15:56
10061-01-5
1.0
1
09/24/20 15:56
10061-02-6
1.0
1
09/24/20 15:56
100-41-4
5.0
1
09/24/20 15:56
591-78-6
20.0
1
09/24/20 15:56
74-88-4
5.0
1
09/24/20 15:56
75-09-2
5.0
1
09/24/20 15:56
108-10-1
1.0
1
09/24/20 15:56
100-42-5
1.0
1
09/24/20 15:56
630-20-6
1.0
1
09/24/20 15:56
79-34-5
1.0
1
09/24/20 15:56
127-18-4
1.0
1
09/24/20 15:56
108-88-3
1.0
1
09/24/20 15:56
71-55-6
1.0
1
09/24/20 15:56
79-00-5
1.0
1
09/24/20 15:56
79-01-6
1.0
1
09/24/20 15:56
75-69-4
1.0
1
09/24/20 15:56
96-18-4
2.0
1
09/24/20 15:56
108-05-4
1.0
1
09/24/20 15:56
75-01-4
1.0
1
09/24/20 15:56
1330-20-7
2.0
1
09/24/20 15:56
179601-23-1
1.0
1
09/24/20 15:56
95-47-6
70-130 1
70-130 1
70-130 1
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/24/20 15:56 460-00-4
09/24/20 15:56 17060-07-0
09/24/20 15:56 2037-26-5
[I)r7/Ir/%��ITI E 3%�IfIE��C�;SQI
09/ 17/20 18:20 17060-07-0
09/17/2018:20 2037-26-5
Page 11 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW21
Lab ID: 92495550005 Collected:
09/15/20
09:45
Received: 09/15/20 13:55 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:51
7440-38-2
Barium
66.1
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:51
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:51
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7440-48-4
Copper
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7439-92-1
Nickel
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:51
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:51
7440-28-0
Vanadium
6.1
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:51
7440-62-2
Zinc
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:51
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/24/20 01:11
09/24/20 17:30
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 15:38
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 15:38
107-13-1
Benzene
ND
ug/L
1.0
1
09/24/20 15:38
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 15:38
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 15:38
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 15:38
75-25-2 IK,v2
Bromomethane
ND
ug/L
2.0
1
09/24/20 15:38
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 15:38
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 15:38
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 15:38
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 15:38
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/24/20 15:38
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 15:38
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 15:38
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 15:38
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 15:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 15:38
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 15:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 15:38
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 15:38
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 15:38
110-57-6 v2
1,1-Dichloroethane
ND
ug/L
1.0
1
09/24/20 15:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 15:38
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: 6002-HRW21 Lab ID: 92495550005 Collected: 09/15/20 09:45 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/29/2020 12:40 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
102
%
99
%
105
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
95 %
102 %
1.0
1
09/24/20 15:38
75-35-4
1.0
1
09/24/20 15:38
156-59-2
1.0
1
09/24/20 15:38
156-60-5
1.0
1
09/24/20 15:38
78-87-5
1.0
1
09/24/20 15:38
10061-01-5
1.0
1
09/24/20 15:38
10061-02-6
1.0
1
09/24/20 15:38
100-41-4
5.0
1
09/24/20 15:38
591-78-6
20.0
1
09/24/20 15:38
74-88-4
5.0
1
09/24/20 15:38
75-09-2
5.0
1
09/24/20 15:38
108-10-1
1.0
1
09/24/20 15:38
100-42-5
1.0
1
09/24/20 15:38
630-20-6
1.0
1
09/24/20 15:38
79-34-5
1.0
1
09/24/20 15:38
127-18-4
1.0
1
09/24/20 15:38
108-88-3
1.0
1
09/24/20 15:38
71-55-6
1.0
1
09/24/20 15:38
79-00-5
1.0
1
09/24/20 15:38
79-01-6
1.0
1
09/24/20 15:38
75-69-4
1.0
1
09/24/20 15:38
96-18-4
2.0
1
09/24/20 15:38
108-05-4
1.0
1
09/24/20 15:38
75-01-4
1.0
1
09/24/20 15:38
1330-20-7
2.0
1
09/24/20 15:38
179601-23-1
1.0
1
09/24/20 15:38
95-47-6
70-130 1
70-130 1
70-130 1
(r�13i
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/24/20 15:38 460-00-4
09/24/20 15:38 17060-07-0
09/24/20 15:38 2037-26-5
1I11-71r0kil§iE 3R rMf aS4Qi
09/ 17/20 18:39 17060-07-0
09/17/2018:39 2037-26-5
Page 13 of 29

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: TRIP BLANK Lab ID: 92495550006 Collected: 09/15/20 09:08 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 17:06
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 17:06
107-13-1
Benzene
ND
ug/L
1.0
1
09/24/20 17:06
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 17:06
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 17:06
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 17:06
75-25-2 IK,v2
Bromomethane
ND
ug/L
2.0
1
09/24/20 17:06
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 17:06
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 17:06
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 17:06
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 17:06
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/24/20 17:06
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 17:06
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 17:06
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 17:06
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 17:06
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 17:06
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 17:06
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 17:06
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 17:06
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 17:06
110-57-6 v2
1,1-Dichloroethane
ND
ug/L
1.0
1
09/24/20 17:06
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 17:06
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
09/24/20 17:06
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 17:06
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 17:06
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/24/20 17:06
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 17:06
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 17:06
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/24/20 17:06
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/24/20 17:06
591-78-6
lodomethane
ND
ug/L
20.0
1
09/24/20 17:06
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/24/20 17:06
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/24/20 17:06
108-10-1
Styrene
ND
ug/L
1.0
1
09/24/20 17:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 17:06
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 17:06
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/24/20 17:06
127-18-4
Toluene
ND
ug/L
1.0
1
09/24/20 17:06
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/24/20 17:06
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/24/20 17:06
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/24/20 17:06
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/24/20 17:06
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/24/20 17:06
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/24/20 17:06
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/24/20 17:06
75-01-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM
without
the written consent of Pace Analytical Services, LLC.
Page 14 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
Sample: TRIP BLANK
Parameters
Lab ID: 92495550006 Collected: 09/15/20 09:08
Results Units Report Limit DF
Received: 09/15/20 13:55 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
09/24/20 17:06
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
09/24/20 17:06
179601-23-1
o-Xylene
ND ug/L
1.0
1
09/24/20 17:06
95-47-6
Surrogates
4-Bromofluorobenzene (S)
102 %
70-130
1
09/24/20 17:06
460-00-4
1,2-Dichloroethane-d4 (S)
101 %
70-130
1
09/24/20 17:06
17060-07-0
Toluene-d8 (S)
103 %
70-130
1
09/24/20 17:06
2037-26-5
Date: 09/29/2020 12:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
QC Batch: 568135 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495550001, 92495550002, 92495550004, 92495550005
METHOD BLANK: 3010387 Matrix: Water
Associated Lab Samples: 92495550001, 92495550002, 92495550004, 92495550005
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
09/24/20 06:50
10.0
09/24/20 06:50
5.0
09/24/20 06:50
1.0
09/24/20 06:50
1.0
09/24/20 06:50
5.0
09/24/20 06:50
5.0
09/24/20 06:50
5.0
09/24/20 06:50
5.0
09/24/20 06:50
5.0
09/24/20 06:50
10.0
09/24/20 06:50
5.0
09/24/20 06:50
10.0
09/24/20 06:50
5.0
09/24/20 06:50
10.0
09/24/20 06:50
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3010388
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
500
100
80-120
Arsenic
ug/L
500
503
101
80-120
Barium
ug/L
500
488
98
80-120
Beryllium
ug/L
500
486
97
80-120
Cadmium
ug/L
500
492
98
80-120
Chromium
ug/L
500
494
99
80-120
Cobalt
ug/L
500
501
100
80-120
Copper
ug/L
500
503
101
80-120
Lead
ug/L
500
500
100
80-120
Nickel
ug/L
500
499
100
80-120
Selenium
ug/L
500
490
98
80-120
Silver
ug/L
250
246
98
80-120
Thallium
ug/L
500
486
97
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
496
99
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Landfill (Permit # 6
92495550
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3010389
3010390
MS
MSD
92495379001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
513
509
103
102
75-125
1
Arsenic
ug/L
ND
500
500
524
525
105
105
75-125
0
Barium
ug/L
107
500
500
601
598
99
98
75-125
1
Beryllium
ug/L
ND
500
500
499
496
100
99
75-125
1
Cadmium
ug/L
ND
500
500
512
513
102
103
75-125
0
Chromium
ug/L
26.2
500
500
536
535
102
102
75-125
0
Cobalt
ug/L
ND
500
500
507
504
101
101
75-125
1
Copper
ug/L
6.3
500
500
517
515
102
102
75-125
0
Lead
ug/L
ND
500
500
511
508
102
101
75-125
1
Nickel
ug/L
5.3
500
500
510
511
101
101
75-125
0
Selenium
ug/L
5.6J
500
500
536
535
106
106
75-125
0
Silver
ug/L
ND
250
250
252
251
101
100
75-125
0
Thallium
ug/L
ND
500
500
496
493
99
99
75-125
1
Vanadium
ug/L
ND
500
500
519
519
104
104
75-125
0
Zinc
ug/L
ND
500
500
516
515
103
102
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
QC Batch: 568444 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495550003
METHOD BLANK: 3011850
Associated Lab Samples: 92495550003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Antimony
ug/L
ND
5.0
09/25/20 00:58
Arsenic
ug/L
ND
10.0
09/25/20 00:58
Barium
ug/L
ND
5.0
09/25/20 00:58
Beryllium
ug/L
ND
1.0
09/25/20 00:58
Cadmium
ug/L
ND
1.0
09/25/20 00:58
Chromium
ug/L
5.9
5.0
09/25/2018:27 P8
Cobalt
ug/L
ND
5.0
09/25/20 00:58
Copper
ug/L
ND
5.0
09/25/20 00:58
Lead
ug/L
ND
5.0
09/25/20 00:58
Nickel
ug/L
ND
5.0
09/25/20 00:58
Selenium
ug/L
ND
10.0
09/25/20 00:58
Silver
ug/L
ND
5.0
09/25/20 00:58
Thallium
ug/L
ND
10.0
09/25/2018:27
Vanadium
ug/L
ND
5.0
09/25/20 00:58
Zinc
ug/L
ND
10.0
09/25/20 00:58
LABORATORY CONTROL SAMPLE:
Parameter
3011851
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
459
92
80-120
Arsenic
ug/L
500
456
91
80-120
Barium
ug/L
500
510
102
80-120
Beryllium
ug/L
500
476
95
80-120
Cadmium
ug/L
500
479
96
80-120
Chromium
ug/L
500
510
102
80-120
Cobalt
ug/L
500
471
94
80-120
Copper
ug/L
500
510
102
80-120
Lead
ug/L
500
471
94
80-120
Nickel
ug/L
500
485
97
80-120
Selenium
ug/L
500
456
91
80-120
Silver
ug/L
250
248
99
80-120
Thallium
ug/L
500
472
94
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
461
92
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Landfill (Permit # 6
92495550
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3011852
3011853
MS
MSD
92494408001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
472
475
94
95
75-125
1
Arsenic
ug/L
ND
500
500
480
487
96
97
75-125
1
Barium
ug/L
68.8
500
500
591
600
104
106
75-125
1
Beryllium
ug/L
ND
500
500
492
494
98
99
75-125
0
Cadmium
ug/L
ND
500
500
505
506
101
101
75-125
0
Chromium
ug/L
ND
500
500
536
540
107
108
75-125
1
Cobalt
ug/L
18.1
500
500
503
503
97
97
75-125
0
Copper
ug/L
42.8
500
500
563
565
104
104
75-125
0
Lead
ug/L
ND
500
500
487
492
97
98
75-125
1
Nickel
ug/L
ND
500
500
502
504
100
100
75-125
1
Selenium
ug/L
ND
500
500
506
503
101
101
75-125
1
Silver
ug/L
ND
250
250
257
257
103
103
75-125
0
Thallium
ug/L
ND
500
500
451
450
90
90
75-125
0
Vanadium
ug/L
8.2
500
500
529
529
104
104
75-125
0
Zinc
ug/L
48.2
500
500
527
530
96
96
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
QC Batch: 568571 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495550001, 92495550002, 92495550003, 92495550004, 92495550005
METHOD BLANK: 3012601
Matrix:
Water
Associated Lab Samples: 92495550001, 92495550002, 92495550003, 92495550004, 92495550005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.10
09/24/2015:37
LABORATORY CONTROL SAMPLE:
3012602
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
9.8
98 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3012603 3012604
MS MSD
92494865009 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.0 9.8 100 98 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 29

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
QC Batch: 568556 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495550001, 92495550002, 92495550003, 92495550004, 92495550005, 92495550006
METHOD BLANK: 3012539 Matrix: Water
Associated Lab Samples: 92495550001, 92495550002, 92495550003, 92495550004, 92495550005, 92495550006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 14:28
1,1,1-Trichloroethane
ug/L
ND
1.0
09/24/20 14:28
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 14:28
1,1,2-Trichloroethane
ug/L
ND
1.0
09/24/20 14:28
1,1-Dichloroethane
ug/L
ND
1.0
09/24/20 14:28
1,1-Dichloroethene
ug/L
ND
1.0
09/24/20 14:28
1,2,3-Trichloropropane
ug/L
ND
1.0
09/24/20 14:28
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
09/24/20 14:28
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/24/20 14:28
1,2-Dichlorobenzene
ug/L
ND
1.0
09/24/20 14:28
1,2-Dichloroethane
ug/L
ND
1.0
09/24/20 14:28
1,2-Dichloropropane
ug/L
ND
1.0
09/24/20 14:28
1,4-Dichlorobenzene
ug/L
ND
1.0
09/24/20 14:28
2-Butanone (MEK)
ug/L
ND
5.0
09/24/20 14:28
2-Hexanone
ug/L
ND
5.0
09/24/20 14:28
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/24/20 14:28
Acetone
ug/L
ND
25.0
09/24/20 14:28
Acrylonitrile
ug/L
ND
10.0
09/24/20 14:28
Benzene
ug/L
ND
1.0
09/24/20 14:28
Bromochloromethane
ug/L
ND
1.0
09/24/20 14:28
Bromodichloromethane
ug/L
ND
1.0
09/24/20 14:28
Bromoform
ug/L
ND
1.0
09/24/20 14:28
Bromomethane
ug/L
ND
2.0
09/24/20 14:28
Carbon disulfide
ug/L
ND
2.0
09/24/20 14:28
Carbon tetrachloride
ug/L
ND
1.0
09/24/20 14:28
Chlorobenzene
ug/L
ND
1.0
09/24/20 14:28
Chloroethane
ug/L
ND
1.0
09/24/20 14:28
Chloroform
ug/L
ND
5.0
09/24/20 14:28
Chloromethane
ug/L
ND
1.0
09/24/20 14:28
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 14:28
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 14:28
Dibromochloromethane
ug/L
ND
1.0
09/24/20 14:28
Dibromomethane
ug/L
ND
1.0
09/24/20 14:28
Ethylbenzene
ug/L
ND
1.0
09/24/20 14:28
lodomethane
ug/L
ND
20.0
09/24/20 14:28
m&p-Xylene
ug/L
ND
2.0
09/24/20 14:28
Methylene Chloride
ug/L
ND
5.0
09/24/20 14:28
o-Xylene
ug/L
ND
1.0
09/24/20 14:28
Styrene
ug/L
ND
1.0
09/24/20 14:28
Tetrachloroethene
ug/L
ND
1.0
09/24/20 14:28
IK,v2
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 29

leAnalyiical
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
METHOD BLANK: 3012539 Matrix: Water
Associated Lab Samples: 92495550001, 92495550002, 92495550003, 92495550004, 92495550005, 92495550006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
09/24/20 14:28
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 14:28
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 14:28
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/24/20 14:28 v2
Trichloroethene
ug/L
ND
1.0
09/24/20 14:28
Trichlorofluoromethane
ug/L
ND
1.0
09/24/20 14:28
Vinyl acetate
ug/L
ND
2.0
09/24/20 14:28
Vinyl chloride
ug/L
ND
1.0
09/24/20 14:28
Xylene (Total)
ug/L
ND
1.0
09/24/20 14:28
1,2-Dichloroethane-d4 (S)
%
94
70-130
09/24/20 14:28
4-Bromofluorobenzene (S)
%
101
70-130
09/24/20 14:28
Toluene-d8 (S)
%
105
70-130
09/24/20 14:28
LABORATORY CONTROL SAMPLE: 3012540
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
44.5
89
70-130
1,1,1-Trichloroethane
ug/L
50
50.0
100
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.5
101
70-130
1,1,2-Trichloroethane
ug/L
50
51.4
103
70-130
1,1-Dichloroethane
ug/L
50
48.0
96
70-130
1,1-Dichloroethene
ug/L
50
49.0
98
70-130
1,2,3-Trichloropropane
ug/L
50
48.7
97
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
42.8
86
70-130
1,2-Dibromoethane (EDB)
ug/L
50
55.2
110
70-130
1,2-Dichlorobenzene
ug/L
50
46.9
94
70-130
1,2-Dichloroethane
ug/L
50
46.0
92
70-130
1,2-Dichloropropane
ug/L
50
50.2
100
70-130
1,4-Dichlorobenzene
ug/L
50
48.3
97
70-130
2-Butanone (MEK)
ug/L
100
101
101
64-135
2-Hexanone
ug/L
100
103
103
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
98.1
98
70-130
Acetone
ug/L
100
105
105
61-157
Acrylonitrile
ug/L
250
245
98
61-143
Benzene
ug/L
50
48.4
97
70-130
Bromochloromethane
ug/L
50
51.9
104
70-130
Bromodichloromethane
ug/L
50
44.2
88
70-130
Bromoform
ug/L
50
40.8
82
70-130lK,v3
Bromomethane
ug/L
50
34.8
70
38-130 v3
Carbon disulfide
ug/L
50
51.5
103
68-130
Carbon tetrachloride
ug/L
50
49.6
99
70-130
Chlorobenzene
ug/L
50
47.6
95
70-130
Chloroethane
ug/L
50
39.9
80
37-142
Chloroform
ug/L
50
47.7
95
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
LABORATORY CONTROL SAMPLE:
Parameter
3012540
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
36.5
cis-1,2-Dichloroethene
ug/L
50
48.1
cis-1,3-Dichloropropene
ug/L
50
54.4
Dibromochloromethane
ug/L
50
45.2
Dibromomethane
ug/L
50
50.9
Ethylbenzene
ug/L
50
47.4
lodomethane
ug/L
100
99.0
m&p-Xylene
ug/L
100
94.6
Methylene Chloride
ug/L
50
47.0
o-Xylene
ug/L
50
47.0
Styrene
ug/L
50
50.3
Tetrachloroethene
ug/L
50
46.5
Toluene
ug/L
50
47.6
trans-1,2-Dichloroethene
ug/L
50
49.3
trans- 1,3-Dichloropropene
ug/L
50
45.9
trans-1,4-Dichloro-2-butene
ug/L
50
59.4
Trichloroethene
ug/L
50
49.2
Trichlorofluoromethane
ug/L
50
44.3
Vinyl acetate
ug/L
100
120
Vinyl chloride
ug/L
50
43.2
Xylene (Total)
ug/L
150
142
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
73
48-130
96
70-130
109
70-130
90
70-130
102
70-130
95
70-130
99
40-130
95
70-130
94
67-132
94
70-131
101
70-130
93
69-130
95
70-130
99
70-130
92
70-130
119
35-189 v3
98
70-130
89
63-130
120
55-143
86
70-131
94
70-130
95
70-130
99
70-130
97
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3012541
MS
92496293007 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3012542
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.7
19.3
104
97
73-134
7
1,1,1-Trichloroethane
ug/L
ND
20
20
21.9
21.0
110
105
82-143
4
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.6
20.9
103
105
70-136
1
1,1,2-Trichloroethane
ug/L
ND
20
20
21.5
21.0
108
105
70-135
3
1,1-Dichloroethane
ug/L
ND
20
20
21.7
20.5
109
103
70-139
6
1,1-Dichloroethene
ug/L
ND
20
20
26.1
24.7
130
124
70-154
5
1,2,3-Trichloropropane
ug/L
ND
20
20
21.9
20.3
109
101
71-137
8
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
18.6
17.2
93
86
65-134
8
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
20.3
19.8
102
99
70-137
3
1,2-Dichlorobenzene
ug/L
ND
20
20
20.6
19.2
103
96
70-133
7
1,2-Dichloroethane
ug/L
ND
20
20
20.6
19.3
103
97
70-137
6
1,2-Dichloropropane
ug/L
ND
20
20
21.3
21.0
106
105
70-140
1
1,4-Dichlorobenzene
ug/L
ND
20
20
20.7
19.3
103
96
70-133
7
2-Butanone (MEK)
ug/L
ND
40
40
43.8
39.5
110
99
60-139
10
2-Hexanone
ug/L
ND
40
40
42.7
39.8
107
100
65-138
7
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
41.5
39.6
104
99
65-135
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 29

leAnalyiical
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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3012541
MS
92496293007 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3012542
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
38.7
35.9
97
90
60-148
8
Acrylonitrile
ug/L
ND
100
100
106
100
106
100
64-147
6
Benzene
ug/L
ND
20
20
21.7
22.0
109
110
70-151
1
Bromochloromethane
ug/L
ND
20
20
22.3
21.6
112
108
70-141
3
Bromodichloromethane
ug/L
ND
20
20
18.5
19.0
92
95
70-138
3
Bromoform
ug/L
ND
20
20
17.3
17.2
87
86
63-130
1
Bromomethane
ug/L
ND
20
20
17.1
15.8
86
79
15-152
8
Carbon disulfide
ug/L
ND
20
20
29.2
27.6
146
138
69-149
6 IH
Carbon tetrachloride
ug/L
ND
20
20
22.3
21.8
111
109
70-143
2
Chlorobenzene
ug/L
ND
20
20
20.8
20.4
104
102
70-138
2
Chloroethane
ug/L
ND
20
20
20.6
19.5
103
98
52-163
6
Chloroform
ug/L
ND
20
20
20.5
20.1
103
101
70-139
2
Chloromethane
ug/L
ND
20
20
16.3
14.7
81
74
41-139
10
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.0
20.3
110
102
70-141
8
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.5
21.8
108
109
70-137
1
Dibromochloromethane
ug/L
ND
20
20
21.2
20.2
106
101
70-134
5
Dibromomethane
ug/L
ND
20
20
22.4
21.1
112
106
70-138
6
Ethylbenzene
ug/L
ND
20
20
20.9
21.2
105
106
66-153
1
lodomethane
ug/L
ND
40
40
48.8
45.6
122
114
20-138
7
m&p-Xylene
ug/L
ND
40
40
41.8
40.0
105
100
69-152
4
Methylene Chloride
ug/L
ND
20
20
21.4
20.9
107
105
42-159
2
o-Xylene
ug/L
ND
20
20
20.5
20.6
102
103
70-148
1
Styrene
ug/L
ND
20
20
21.5
21.0
108
105
70-135
2
Tetrachloroethene
ug/L
ND
20
20
20.2
20.0
101
100
59-143
1
Toluene
ug/L
ND
20
20
20.8
20.5
104
102
59-148
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
22.9
21.3
115
106
70-146
7
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.9
20.3
104
101
70-135
3
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
18.0
17.8
90
89
47-135
1
Trichloroethene
ug/L
ND
20
20
21.9
20.7
109
104
70-147
5
Trichlorofluoromethane
ug/L
ND
20
20
19.2
18.0
96
90
70-148
6
Vinyl acetate
ug/L
ND
40
40
43.8
41.7
109
104
49-151
5
Vinyl chloride
ug/L
ND
20
20
17.6
16.6
88
83
70-156
6
Xylene (Total)
ug/L
ND
60
60
62.3
60.7
104
101
63-158
3
1,2-Dichloroethane-d4 (S)
%
99
95
70-130
4-Bromofluorobenzene (S)
%
98
97
70-130
Toluene-d8(S)
%
97
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/29/2020 12:40 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 29

leAnalyiical
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QUALITY CONTROL DATA
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
QC Batch: 567202 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495550001, 92495550002, 92495550003, 92495550004, 92495550005
METHOD BLANK: 3005681
Matrix:
Water
Associated Lab Samples:
92495550001, 92495550002, 92495550003, 92495550004, 92495550005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/17/20 12:39
1,2-Dichloroethane-d4 (S)
%
96
50-150
09/17/20 12:39
Toluene-d8 (S)
%
100
50-150
09/17/20 12:39
LABORATORY CONTROL SAMPLE: 3005682
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 21.0 105 70-130
1,2-Dichloroethane-d4 (S) % 107 50-150
Toluene-d8 (S) % 100 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3005683
3005684
MS
MSD
92495534003 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 20.1
20.6 91
94
50-150 3
1,2-Dichloroethane-d4 (S)
%
99
106
50-150
Toluene-d8(S)
%
102
101
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
lac,
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QUALIFIERS
Project: Holbrooks Landfill (Permit # 6
Pace Project No.: 92495550
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than
the blank or were below the reporting limit.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Landfill (Permit # 6
92495550
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92495550001
6002-HRW7
EPA 3010A
568135
EPA6010D
568283
92495550002
6002-HRW18
EPA 3010A
568135
EPA6010D
568283
92495550003
6002-HRW19
EPA 3010A
568444
EPA6010D
568548
92495550004
6002-HRW20
EPA 3010A
568135
EPA6010D
568283
92495550005
6002-HRW21
EPA 3010A
568135
EPA6010D
568283
92495550001
6002-HRW7
EPA 3010A
568571
EPA 6020B
568591
92495550002
6002-HRW18
EPA 3010A
568571
EPA 6020B
568591
92495550003
6002-HRW19
EPA 3010A
568571
EPA 6020B
568591
92495550004
6002-HRW20
EPA 3010A
568571
EPA 6020B
568591
92495550005
6002-HRW21
EPA 3010A
568571
EPA 6020B
568591
92495550001
6002-HRW7
EPA 8260D
568556
92495550002
6002-HRW18
EPA 8260D
568556
92495550003
6002-HRW19
EPA 8260D
568556
92495550004
6002-HRW20
EPA 8260D
568556
92495550005
6002-HRW21
EPA 8260D
568556
92495550006
TRIP BLANK
EPA 8260D
568556
92495550001
6002-HRW7
EPA 8260D Mod.
567202
92495550002
6002-HRW18
EPA 8260D Mod.
567202
92495550003
6002-HRW19
EPA 8260D Mod.
567202
92495550004
6002-HRW20
EPA 8260D Mod.
567202
92495550005
6002-HRW21
EPA 8260D Mod.
567202
Date: 09/29/2020 12:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 29

Document Name:
sample Condition Upon Rec
Analytical Document No.:
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑
oecument Revised: February 7, 2018
ipt15CUR I Pase 1 of 2
Issuing Authority:
b Face Carolinas Quailty Office
Huntersville [� Raleigh❑ Mechanicsville❑
simple Condition Client Name: , Project*. Wo## : 92495550
i Upon Receipt M t L , �'� ` �v . , ` Il l Ill ll �Il II 1111� 1 ill
(�FeTJ Ex ❑UPS❑LISPS / lient
Laurier: ❑ °��s,� Commercial ace VL✓ /rs/1G ❑Other: 92495550
o
DatellrltlalsPerson Exam[ningCantents:
Biologital Tissue Frozen?
Packing Material: 0--13ubble Wrap �bble Bags ❑None Other ]Yes ❑No []N/A
Thermometer 92TO61 Type of Ice: et ❑Blue ❑None
OR Gun ID:
Cooler Temp (°Cj: 3 j i Correction Factor: Add/5ubtract ('Cl 0.0 Temp should be above freezingto VC
Gaoler Temp Cortecteti (°Lj: 3 �{ ❑Samples auto( temp cQerla.5ampies on ice, cooling process
has begun
USDA Regulated Soil (' N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, ar 5C (check maps)? Including ngiHawaii and Puerto Rlco)?❑Yes source {InteOrrNtonally,
ONO
Chain of Custody Present?
yes
[]NO,❑NIA
1.
Samples Arrived within Hold Time?
CV,,
❑No
❑NIA
2.
Short Hold Time Analysis (c72 hr.]?
❑Yes
No
[]NIA
3.
Rush Turn Around Time Requested?
[]Yes
No
❑N/A
4,
Sufficient Volurne?
Eq�e�s.
❑No
[]N/A
5.
Cor rect Co nta in er s Used?
Yes
es
❑No
❑No
❑NIA
[]N/A
5-
Pace Containers Used?
es
❑No
❑N/A
7.
Containers Intact?
❑NIA
9.
Dissolved analysis: Samples Field Filtered?
w -
No
Sample Labels N4atch COG?
Yes
❑na
❑NIA
9.
-Includes Date/TimellD/Analyses wrau a.
❑Yes a ❑N/A 10.
Headspace in VGA Vials {>5-6mml? 11.
Trip Blank Present? ©Yes [NO ❑N/A
Trip Blank Custody 5eak Present? ❑Yes CEO ❑NIA
Fleid Date Repulred? ❑yes ❑No
COMMENTS/SAMPLE DISCREPANCY
Lot ID of spit containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date:
Page 28 of 29

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Page 29 of 29

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 28, 2020
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 15, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92495534001 6002-HRW10
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495534002 6002-HRW11R
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495534003 6002-HRW13
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495534004 6002-HRW12
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495534005 6002-HRW17
EPA 6010D
SH1
15
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW10 Lab ID: 92495534001 Collected: 09/15/20 12:32 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:13
7440-38-2
Barium
237
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:13
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:13
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7440-48-4
Copper
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7439-92-1
Nickel
14.1
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:13
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:13
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:13
7440-62-2
Zinc
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:13
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/19/20 01:41
09/21/20 15:13
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 16:39
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 16:39
107-13-1
Benzene
ND
ug/L
1.0
1
09/24/20 16:39
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 16:39
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 16:39
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 16:39
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/24/20 16:39
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 16:39
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 16:39
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 16:39
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 16:39
108-90-7
Chloroethane
2.7
ug/L
1.0
1
09/24/20 16:39
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 16:39
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 16:39
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 16:39
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 16:39
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 16:39
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 16:39
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 16:39
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 16:39
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 16:39
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/24/20 16:39
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 16:39
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW10 Lab ID: 92495534001 Collected: 09/15/20 12:32 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:39
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:39
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:39
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:39
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:39
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:39
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/24/20 16:39
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/24/20 16:39
591-78-6
lodomethane
ND
ug/L
20.0
1
09/24/20 16:39
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/24/20 16:39
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/24/20 16:39
108-10-1
Styrene
ND
ug/L
1.0
1
09/24/20 16:39
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:39
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:39
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/24/20 16:39
127-18-4
Toluene
ND
ug/L
1.0
1
09/24/20 16:39
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:39
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:39
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/24/20 16:39
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/24/20 16:39
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/24/20 16:39
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/24/20 16:39
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/24/20 16:39
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/24/20 16:39
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/24/20 16:39
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/24/20 16:39
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/24/20 16:39
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
09/24/20 16:39
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
09/24/20 16:39
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
10.3
ug/L
2.0
1
09/17/20 18:58
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
108
%
50-150
1
09/17/20 18:58
17060-07-0
Toluene-d8 (S)
100
%
50-150
1
09/17/20 18:58
2037-26-5
Date: 09/28/2020 04:35 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW11R Lab ID: 92495534002 Collected: 09/15/20 11:21 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:16
7440-38-2
Barium
385
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:16
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:16
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7440-47-3
Cobalt
16.6
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7440-48-4
Copper
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7439-92-1
Nickel
53.5
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:16
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:16
7440-28-0
Vanadium
15.2
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:16
7440-62-2
Zinc
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:16
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/19/20 01:41
09/21/20 15:17
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 16:57
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 16:57
107-13-1
Benzene
ND
ug/L
1.0
1
09/24/20 16:57
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 16:57
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 16:57
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 16:57
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/24/20 16:57
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 16:57
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 16:57
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 16:57
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 16:57
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/24/20 16:57
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 16:57
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 16:57
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 16:57
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 16:57
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 16:57
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 16:57
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 16:57
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 16:57
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 16:57
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/24/20 16:57
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 16:57
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW11R Lab ID: 92495534002 Collected: 09/15/20 11:21 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:57
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:57
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 16:57
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:57
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:57
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 16:57
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/24/20 16:57
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/24/20 16:57
591-78-6
lodomethane
ND
ug/L
20.0
1
09/24/20 16:57
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/24/20 16:57
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/24/20 16:57
108-10-1
Styrene
ND
ug/L
1.0
1
09/24/20 16:57
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:57
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 16:57
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/24/20 16:57
127-18-4
Toluene
ND
ug/L
1.0
1
09/24/20 16:57
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:57
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/24/20 16:57
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/24/20 16:57
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/24/20 16:57
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/24/20 16:57
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/24/20 16:57
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/24/20 16:57
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/24/20 16:57
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/24/20 16:57
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/24/20 16:57
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
09/24/20 16:57
460-00-4
1,2-Dichloroethane-d4 (S)
108
%
70-130
1
09/24/20 16:57
17060-07-0
Toluene-d8(S)
103
%
70-130
1
09/24/20 16:57
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
163
ug/L
5.0
2.5
09/17/20 19:36
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
106
%
50-150
2.5
09/17/20 19:36
17060-07-0
Toluene-d8 (S)
100
%
50-150
2.5
09/17/20 19:36
2037-26-5
Date: 09/28/2020 04:35 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW13 Lab ID: 92495534003 Collected: 09/15/20 11:59 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:32
7440-38-2
Barium
160
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:32
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:32
7440-43-9
Chromium
13.8
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7440-47-3
Cobalt
6.6
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7440-48-4
Copper
19.5
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7440-50-8
Lead
5.2
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7439-92-1
Nickel
9.1
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:32
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:32
7440-28-0
Vanadium
22.3
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:32
7440-62-2
Zinc
21.3
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:32
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/19/20 01:41
09/21/20 15:45
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 17:16
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 17:16
107-13-1
Benzene
ND
ug/L
1.0
1
09/24/20 17:16
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 17:16
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 17:16
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 17:16
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/24/20 17:16
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 17:16
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 17:16
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 17:16
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 17:16
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/24/20 17:16
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 17:16
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 17:16
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 17:16
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 17:16
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 17:16
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 17:16
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 17:16
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 17:16
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 17:16
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/24/20 17:16
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 17:16
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW13 Lab ID: 92495534003 Collected: 09/15/20 11:59 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/24/20 17:16
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 17:16
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/24/20 17:16
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/24/20 17:16
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 17:16
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/24/20 17:16
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/24/20 17:16
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/24/20 17:16
591-78-6
lodomethane
ND
ug/L
20.0
1
09/24/20 17:16
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/24/20 17:16
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/24/20 17:16
108-10-1
Styrene
ND
ug/L
1.0
1
09/24/20 17:16
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 17:16
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/24/20 17:16
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/24/20 17:16
127-18-4
Toluene
ND
ug/L
1.0
1
09/24/20 17:16
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/24/20 17:16
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/24/20 17:16
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/24/20 17:16
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/24/20 17:16
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/24/20 17:16
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/24/20 17:16
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/24/20 17:16
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/24/20 17:16
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/24/20 17:16
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/24/20 17:16
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
09/24/20 17:16
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
09/24/20 17:16
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
09/24/20 17:16
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/17/20 17:04
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
50-150
1
09/17/20 17:04
17060-07-0
Toluene-d8 (S)
101
%
50-150
1
09/17/20 17:04
2037-26-5
Date: 09/28/2020 04:35 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW12 Lab ID: 92495534004 Collected: 09/15/20 11:42 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:35
7440-38-2
Barium
820
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:35
7440-41-7
Cadmium
2.0
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:35
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7440-47-3
Cobalt
58.8
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7440-48-4
Copper
134
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7439-92-1
Nickel
170
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:35
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:35
7440-28-0
Vanadium
10.8
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:35
7440-62-2
Zinc
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:35
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/19/20 01:41
09/21/20 15:49
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 17:34
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 17:34
107-13-1
Benzene
1.0
ug/L
1.0
1
09/24/20 17:34
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 17:34
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 17:34
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 17:34
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/24/20 17:34
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 17:34
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 17:34
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 17:34
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 17:34
108-90-7
Chloroethane
2.2
ug/L
1.0
1
09/24/20 17:34
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 17:34
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 17:34
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 17:34
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 17:34
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 17:34
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 17:34
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 17:34
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 17:34
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 17:34
110-57-6
1,1-Dichloroethane
7.7
ug/L
1.0
1
09/24/20 17:34
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 17:34
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 26

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW12 Lab ID: 92495534004 Collected: 09/15/20 11:42 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/28/2020 04:35 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
101
%
107
%
100
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
181 ug/L
105 %
100 %
1.0
1
09/24/20 17:34
75-35-4
1.0
1
09/24/20 17:34
156-59-2
1.0
1
09/24/20 17:34
156-60-5
1.0
1
09/24/20 17:34
78-87-5
1.0
1
09/24/20 17:34
10061-01-5
1.0
1
09/24/20 17:34
10061-02-6
1.0
1
09/24/20 17:34
100-41-4
5.0
1
09/24/20 17:34
591-78-6
20.0
1
09/24/20 17:34
74-88-4
5.0
1
09/24/20 17:34
75-09-2
5.0
1
09/24/20 17:34
108-10-1
1.0
1
09/24/20 17:34
100-42-5
1.0
1
09/24/20 17:34
630-20-6
1.0
1
09/24/20 17:34
79-34-5
1.0
1
09/24/20 17:34
127-18-4
1.0
1
09/24/20 17:34
108-88-3
1.0
1
09/24/20 17:34
71-55-6
1.0
1
09/24/20 17:34
79-00-5
1.0
1
09/24/20 17:34
79-01-6
1.0
1
09/24/20 17:34
75-69-4
1.0
1
09/24/20 17:34
96-18-4
2.0
1
09/24/20 17:34
108-05-4
1.0
1
09/24/20 17:34
75-01-4
1.0
1
09/24/20 17:34
1330-20-7
2.0
1
09/24/20 17:34
179601-23-1
1.0
1
09/24/20 17:34
95-47-6
70-130 1
70-130 1
70-130 1
6111=J!.1
50-150 2.5
50-150 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/24/20 17:34 460-00-4
09/24/20 17:34 17060-07-0
09/24/20 17:34 2037-26-5
[ek7fr/fkilEiF11l.'ul<ifa 4Qi
09/ 17/20 19:55 17060-07-0
09/17/2019:55 2037-26-5
Page 11 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW17 Lab ID: 92495534005 Collected: 09/15/20 12:14 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:38
7440-38-2
Barium
58.8
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:38
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/23/20 02:04
09/24/20 07:38
7440-43-9
Chromium
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7440-48-4
Copper
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7440-50-8
Lead
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7439-92-1
Nickel
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7440-02-0
Selenium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:38
7782-49-2
Silver
ND
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7440-22-4
Thallium
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:38
7440-28-0
Vanadium
5.1
ug/L
5.0
1
09/23/20 02:04
09/24/20 07:38
7440-62-2
Zinc
ND
ug/L
10.0
1
09/23/20 02:04
09/24/20 07:38
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/19/20 01:41
09/21/20 15:52
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/24/20 17:52
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/24/20 17:52
107-13-1
Benzene
ND
ug/L
1.0
1
09/24/20 17:52
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/24/20 17:52
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/20 17:52
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/20 17:52
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/24/20 17:52
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/20 17:52
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/24/20 17:52
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/20 17:52
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/20 17:52
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/24/20 17:52
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/20 17:52
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/20 17:52
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/20 17:52
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/20 17:52
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/20 17:52
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/20 17:52
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 17:52
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/20 17:52
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/24/20 17:52
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/24/20 17:52
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/24/20 17:52
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 26

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
Sample: 6002-HRW17 Lab ID: 92495534005 Collected: 09/15/20 12:14 Received: 09/15/20 13:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/28/2020 04:35 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
102
%
106
%
102
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
94 %
100 %
1.0
1
09/24/20 17:52
75-35-4
1.0
1
09/24/20 17:52
156-59-2
1.0
1
09/24/20 17:52
156-60-5
1.0
1
09/24/20 17:52
78-87-5
1.0
1
09/24/20 17:52
10061-01-5
1.0
1
09/24/20 17:52
10061-02-6
1.0
1
09/24/20 17:52
100-41-4
5.0
1
09/24/20 17:52
591-78-6
20.0
1
09/24/20 17:52
74-88-4
5.0
1
09/24/20 17:52
75-09-2
5.0
1
09/24/20 17:52
108-10-1
1.0
1
09/24/20 17:52
100-42-5
1.0
1
09/24/20 17:52
630-20-6
1.0
1
09/24/20 17:52
79-34-5
1.0
1
09/24/20 17:52
127-18-4
1.0
1
09/24/20 17:52
108-88-3
1.0
1
09/24/20 17:52
71-55-6
1.0
1
09/24/20 17:52
79-00-5
1.0
1
09/24/20 17:52
79-01-6
1.0
1
09/24/20 17:52
75-69-4
1.0
1
09/24/20 17:52
96-18-4
2.0
1
09/24/20 17:52
108-05-4
1.0
1
09/24/20 17:52
75-01-4
1.0
1
09/24/20 17:52
1330-20-7
2.0
1
09/24/20 17:52
179601-23-1
1.0
1
09/24/20 17:52
95-47-6
70-130 1
70-130 1
70-130 1
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/24/20 17:52 460-00-4
09/24/20 17:52 17060-07-0
09/24/20 17:52 2037-26-5
09/ 17/20 17:23 17060-07-0
09/17/2017:23 2037-26-5
Page 13 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
QC Batch: 568135 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495534001, 92495534002, 92495534003, 92495534004, 92495534005
METHOD BLANK: 3010387 Matrix: Water
Associated Lab Samples: 92495534001, 92495534002, 92495534003, 92495534004, 92495534005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
09/24/20 06:50
Arsenic
ug/L
ND
10.0
09/24/20 06:50
Barium
ug/L
ND
5.0
09/24/20 06:50
Beryllium
ug/L
ND
1.0
09/24/20 06:50
Cadmium
ug/L
ND
1.0
09/24/20 06:50
Chromium
ug/L
ND
5.0
09/24/20 06:50
Cobalt
ug/L
ND
5.0
09/24/20 06:50
Copper
ug/L
ND
5.0
09/24/20 06:50
Lead
ug/L
ND
5.0
09/24/20 06:50
Nickel
ug/L
ND
5.0
09/24/20 06:50
Selenium
ug/L
ND
10.0
09/24/20 06:50
Silver
ug/L
ND
5.0
09/24/20 06:50
Thallium
ug/L
ND
10.0
09/24/20 06:50
Vanadium
ug/L
ND
5.0
09/24/20 06:50
Zinc
ug/L
ND
10.0
09/24/20 06:50
LABORATORY CONTROL SAMPLE:
Parameter
3010388
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
500
100
80-120
Arsenic
ug/L
500
503
101
80-120
Barium
ug/L
500
488
98
80-120
Beryllium
ug/L
500
486
97
80-120
Cadmium
ug/L
500
492
98
80-120
Chromium
ug/L
500
494
99
80-120
Cobalt
ug/L
500
501
100
80-120
Copper
ug/L
500
503
101
80-120
Lead
ug/L
500
500
100
80-120
Nickel
ug/L
500
499
100
80-120
Selenium
ug/L
500
490
98
80-120
Silver
ug/L
250
246
98
80-120
Thallium
ug/L
500
486
97
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
496
99
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92495534
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3010389
3010390
MS
MSD
92495379001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
513
509
103
102
75-125
1
Arsenic
ug/L
ND
500
500
524
525
105
105
75-125
0
Barium
ug/L
107
500
500
601
598
99
98
75-125
1
Beryllium
ug/L
ND
500
500
499
496
100
99
75-125
1
Cadmium
ug/L
ND
500
500
512
513
102
103
75-125
0
Chromium
ug/L
26.2
500
500
536
535
102
102
75-125
0
Cobalt
ug/L
ND
500
500
507
504
101
101
75-125
1
Copper
ug/L
6.3
500
500
517
515
102
102
75-125
0
Lead
ug/L
ND
500
500
511
508
102
101
75-125
1
Nickel
ug/L
5.3
500
500
510
511
101
101
75-125
0
Selenium
ug/L
5.6J
500
500
536
535
106
106
75-125
0
Silver
ug/L
ND
250
250
252
251
101
100
75-125
0
Thallium
ug/L
ND
500
500
496
493
99
99
75-125
1
Vanadium
ug/L
ND
500
500
519
519
104
104
75-125
0
Zinc
ug/L
ND
500
500
516
515
103
102
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
QC Batch: 567587 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495534001, 92495534002, 92495534003, 92495534004, 92495534005
METHOD BLANK: 3007979
Matrix:
Water
Associated Lab Samples: 92495534001, 92495534002, 92495534003, 92495534004, 92495534005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.10
09/21/2012:54
LABORATORY CONTROL SAMPLE:
3007980
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
9.7
97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3007981 3007982
MS MSD
92495498002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L 0.26J 10 10 10.2 10.2 100 100 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
QC Batch: 568552 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495534001, 92495534002, 92495534003, 92495534004, 92495534005
METHOD BLANK: 3012534 Matrix: Water
Associated Lab Samples: 92495534001, 92495534002, 92495534003, 92495534004, 92495534005
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 14:30
1,1,1-Trichloroethane
ug/L
ND
1.0
09/24/20 14:30
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 14:30
1,1,2-Trichloroethane
ug/L
ND
1.0
09/24/20 14:30
1,1-Dichloroethane
ug/L
ND
1.0
09/24/20 14:30
1,1-Dichloroethene
ug/L
ND
1.0
09/24/20 14:30
1,2,3-Trichloropropane
ug/L
ND
1.0
09/24/20 14:30
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
09/24/20 14:30
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/24/20 14:30
1,2-Dichlorobenzene
ug/L
ND
1.0
09/24/20 14:30
1,2-Dichloroethane
ug/L
ND
1.0
09/24/20 14:30
1,2-Dichloropropane
ug/L
ND
1.0
09/24/20 14:30
1,4-Dichlorobenzene
ug/L
ND
1.0
09/24/20 14:30
2-Butanone (MEK)
ug/L
ND
5.0
09/24/20 14:30
2-Hexanone
ug/L
ND
5.0
09/24/20 14:30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/24/20 14:30
Acetone
ug/L
ND
25.0
09/24/20 14:30
Acrylonitrile
ug/L
ND
10.0
09/24/20 14:30
Benzene
ug/L
ND
1.0
09/24/20 14:30
Bromochloromethane
ug/L
ND
1.0
09/24/20 14:30
Bromodichloromethane
ug/L
ND
1.0
09/24/20 14:30
Bromoform
ug/L
ND
1.0
09/24/20 14:30
Bromomethane
ug/L
ND
2.0
09/24/20 14:30
Carbon disulfide
ug/L
ND
2.0
09/24/20 14:30
Carbon tetrachloride
ug/L
ND
1.0
09/24/20 14:30
Chlorobenzene
ug/L
ND
1.0
09/24/20 14:30
Chloroethane
ug/L
ND
1.0
09/24/20 14:30
Chloroform
ug/L
ND
5.0
09/24/20 14:30
Chloromethane
ug/L
ND
1.0
09/24/20 14:30
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 14:30
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 14:30
Dibromochloromethane
ug/L
ND
1.0
09/24/20 14:30
Dibromomethane
ug/L
ND
1.0
09/24/20 14:30
Ethylbenzene
ug/L
ND
1.0
09/24/20 14:30
lodomethane
ug/L
ND
20.0
09/24/20 14:30
m&p-Xylene
ug/L
ND
2.0
09/24/20 14:30
Methylene Chloride
ug/L
ND
5.0
09/24/20 14:30
o-Xylene
ug/L
ND
1.0
09/24/20 14:30
Styrene
ug/L
ND
1.0
09/24/20 14:30
Tetrachloroethene
ug/L
ND
1.0
09/24/20 14:30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 26

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
METHOD BLANK: 3012534 Matrix: Water
Associated Lab Samples: 92495534001, 92495534002, 92495534003, 92495534004, 92495534005
Blank Reporting
Parameter Units Result Limit Analyzed
Toluene
ug/L
ND
1.0
09/24/20 14:30
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 14:30
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 14:30
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/24/20 14:30
Trichloroethene
ug/L
ND
1.0
09/24/20 14:30
Trichlorofluoromethane
ug/L
ND
1.0
09/24/20 14:30
Vinyl acetate
ug/L
ND
2.0
09/24/20 14:30
Vinyl chloride
ug/L
ND
1.0
09/24/20 14:30
Xylene (Total)
ug/L
ND
1.0
09/24/20 14:30
1,2-Dichloroethane-d4 (S)
%
106
70-130
09/24/20 14:30
4-Bromofluorobenzene (S)
%
99
70-130
09/24/20 14:30
Toluene-d8 (S)
%
102
70-130
09/24/20 14:30
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3012535
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
55.9
112
70-130
1,1,1-Trichloroethane
ug/L
50
54.2
108
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
54.0
108
70-130
1,1,2-Trichloroethane
ug/L
50
53.2
106
70-130
1,1-Dichloroethane
ug/L
50
51.3
103
70-130
1,1-Dichloroethene
ug/L
50
53.5
107
70-130
1,2,3-Trichloropropane
ug/L
50
52.5
105
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
58.4
117
70-130
1,2-Dibromoethane (EDB)
ug/L
50
58.0
116
70-130
1,2-Dichlorobenzene
ug/L
50
53.2
106
70-130
1,2-Dichloroethane
ug/L
50
50.5
101
70-130
1,2-Dichloropropane
ug/L
50
55.4
111
70-130
1,4-Dichlorobenzene
ug/L
50
52.4
105
70-130
2-Butanone (MEK)
ug/L
100
111
111
64-135
2-Hexanone
ug/L
100
116
116
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
106
106
70-130
Acetone
ug/L
100
105
105
61-157
Acrylonitrile
ug/L
250
273
109
61-143
Benzene
ug/L
50
54.0
108
70-130
Bromochloromethane
ug/L
50
52.3
105
70-130
Bromodichloromethane
ug/L
50
47.9
96
70-130
Bromoform
ug/L
50
57.1
114
70-130
Bromomethane
ug/L
50
46.9
94
38-130
Carbon disulfide
ug/L
50
53.2
106
68-130
Carbon tetrachloride
ug/L
50
52.8
106
70-130
Chlorobenzene
ug/L
50
53.1
106
70-130
Chloroethane
ug/L
50
44.6
89
37-142
Chloroform
ug/L
50
52.5
105
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 26

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
LABORATORY CONTROL SAMPLE:
Parameter
3012535
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
47.9
96
48-130
52.4
105
70-130
58.5
117
70-130
57.2
114
70-130
57.1
114
70-130
52.5
105
70-130
107
107
40-130
103
103
70-130
53.0
106
67-132
53.0
106
70-131
53.6
107
70-130
52.8
106
69-130
52.7
105
70-130
54.3
109
70-130
55.4
111
70-130
59.8
120
35-189
57.8
116
70-130
43.1
86
63-130
119
119
55-143
46.8
94
70-131
156
104
70-130
100
70-130
101
70-130
99
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3012536
MS
92495541007 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3012537
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
18.1
17.5
91
88
73-134
3
1,1,1-Trichloroethane
ug/L
ND
20
20
23.9
23.9
119
119
82-143
0
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.1
20.2
105
101
70-136
4
1,1,2-Trichloroethane
ug/L
ND
20
20
22.9
23.4
114
117
70-135
2
1,1-Dichloroethane
ug/L
ND
20
20
23.4
22.8
117
114
70-139
3
1,1-Dichloroethene
ug/L
ND
20
20
24.5
23.3
123
116
70-154
5
1,2,3-Trichloropropane
ug/L
ND
20
20
20.9
19.9
105
99
71-137
5
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
17.2
17.9
86
89
65-134
4
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
23.0
22.7
115
113
70-137
1
1,2-Dichlorobenzene
ug/L
ND
20
20
21.2
20.7
106
104
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
22.4
22.0
112
110
70-137
1
1,2-Dichloropropane
ug/L
ND
20
20
22.7
23.3
113
116
70-140
3
1,4-Dichlorobenzene
ug/L
ND
20
20
21.2
20.5
106
103
70-133
3
2-Butanone (MEK)
ug/L
ND
40
40
42.8
41.9
107
105
60-139
2
2-Hexanone
ug/L
ND
40
40
38.9
38.4
97
96
65-138
1
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
38.2
39.8
95
100
65-135
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 26

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3012536
MS
92495541007 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3012537
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
43.9
43.0
110
108
60-148
2
Acrylonitrile
ug/L
ND
100
100
109
107
109
107
64-147
2
Benzene
ug/L
ND
20
20
21.8
22.3
109
112
70-151
2
Bromochloromethane
ug/L
ND
20
20
25.4
25.1
127
126
70-141
1
Bromodichloromethane
ug/L
ND
20
20
19.9
20.2
100
101
70-138
1
Bromoform
ug/L
ND
20
20
15.4
15.8
77
79
63-130
2 IK
Bromomethane
ug/L
ND
20
20
7.3
8.9
36
45
15-152
21
Carbon disulfide
ug/L
ND
20
20
25.4
25.1
127
125
69-149
1
Carbon tetrachloride
ug/L
ND
20
20
21.6
22.8
108
114
70-143
6
Chlorobenzene
ug/L
ND
20
20
21.3
20.7
107
103
70-138
3
Chloroethane
ug/L
ND
20
20
22.0
20.8
110
104
52-163
5
Chloroform
ug/L
ND
20
20
23.3
22.9
116
114
70-139
2
Chloromethane
ug/L
ND
20
20
16.8
17.1
84
86
41-139
2
cis-1,2-Dichloroethene
ug/L
ND
20
20
23.4
22.6
117
113
70-141
3
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.2
22.5
111
112
70-137
1
Dibromochloromethane
ug/L
ND
20
20
18.6
18.8
93
94
70-134
1
Dibromomethane
ug/L
ND
20
20
23.8
23.8
119
119
70-138
0
Ethylbenzene
ug/L
ND
20
20
21.9
21.3
110
107
66-153
3
lodomethane
ug/L
ND
40
40
38.9
46.5
97
116
20-138
18
m&p-Xylene
ug/L
ND
40
40
43.7
42.7
109
107
69-152
2
Methylene Chloride
ug/L
ND
20
20
22.2
21.3
111
106
42-159
4
o-Xylene
ug/L
ND
20
20
21.9
21.1
109
105
70-148
4
Styrene
ug/L
ND
20
20
22.3
21.4
112
107
70-135
4
Tetrachloroethene
ug/L
ND
20
20
20.7
20.2
104
101
59-143
2
Toluene
ug/L
ND
20
20
21.9
21.5
110
107
59-148
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.6
23.0
118
115
70-146
3
trans- 1,3-Dichloropropene
ug/L
ND
20
20
17.7
17.7
89
88
70-135
0
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
12.5
14.4
63
72
47-135
14
Trichloroethene
ug/L
ND
20
20
22.5
22.9
113
114
70-147
2
Trichlorofluoromethane
ug/L
ND
20
20
22.9
21.7
115
108
70-148
5
Vinyl acetate
ug/L
ND
40
40
44.7
44.2
112
110
49-151
1
Vinyl chloride
ug/L
ND
20
20
20.9
20.2
105
101
70-156
3
Xylene (Total)
ug/L
ND
60
60
65.6
63.8
109
106
63-158
3
1,2-Dichloroethane-d4 (S)
%
101
99
70-130
4-Bromofluorobenzene (S)
%
106
102
70-130
Toluene-d8(S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
QC Batch: 567202 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495534001, 92495534002, 92495534003, 92495534004, 92495534005
METHOD BLANK: 3005681
Matrix:
Water
Associated Lab Samples:
92495534001, 92495534002, 92495534003, 92495534004, 92495534005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/17/20 12:39
1,2-Dichloroethane-d4 (S)
%
96
50-150
09/17/20 12:39
Toluene-d8 (S)
%
100
50-150
09/17/20 12:39
LABORATORY CONTROL SAMPLE: 3005682
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 21.0 105 70-130
1,2-Dichloroethane-d4 (S) % 107 50-150
Toluene-d8 (S) % 100 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3005683
3005684
MS
MSD
92495534003 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 20.1
20.6 91
94
50-150 3
1,2-Dichloroethane-d4 (S)
%
99
106
50-150
Toluene-d8(S)
%
102
101
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 26

leAnalyiical
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Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Holbrooks Road Landfill (Permi
Pace Project No.: 92495534
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2020 04:35 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 26

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Road Landfill (Permi
92495534
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92495534001
6002-HRW10
EPA 3010A
568135
EPA6010D
568283
92495534002
6002-HRW11 R
EPA 3010A
568135
EPA6010D
568283
92495534003
6002-HRW13
EPA 3010A
568135
EPA6010D
568283
92495534004
6002-HRW12
EPA 3010A
568135
EPA6010D
568283
92495534005
6002-HRW17
EPA 3010A
568135
EPA6010D
568283
92495534001
6002-HRW10
EPA 3010A
567587
EPA6020B
567601
92495534002
6002-HRW11 R
EPA 3010A
567587
EPA 6020B
567601
92495534003
6002-HRW13
EPA 3010A
567587
EPA6020B
567601
92495534004
6002-HRW12
EPA 3010A
567587
EPA6020B
567601
92495534005
6002-HRW17
EPA 3010A
567587
EPA6020B
567601
92495534001
6002-HRW10
EPA 8260D
568552
92495534002
6002-HRW11R
EPA 8260D
568552
92495534003
6002-HRW13
EPA 8260D
568552
92495534004
6002-HRW12
EPA 8260D
568552
92495534005
6002-HRW17
EPA 8260D
568552
92495534001
6002-HRW10
EPA 8260D Mod.
567202
92495534002
6002-HRW11R
EPA 8260D Mod.
567202
92495534003
6002-HRW13
EPA 8260D Mod.
567202
92495534004
6002-HRW12
EPA 8260D Mod.
567202
92495534005
6002-HRW17
EPA 8260D Mod.
567202
Date: 09/28/2020 04:35 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 26

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Page 26 of 26

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 29, 2020
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 16, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92495813001 6002-HRW8
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
PM1
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495813002 6002-HRW9
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495813003 6002-HRW16
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
PM1
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495813004 6002-HRW14
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
PM1
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495813005 6002-HRW15
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495813006 Trip Blank
EPA 8260D
PM1
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW8 Lab ID: 92495813001 Collected: 09/16/20 12:50 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:58
7440-38-2
Barium
171
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 20:58
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 20:58
7440-43-9
Chromium
6.0
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7440-47-3
Cobalt
25.8
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7440-48-4
Copper
13.0
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7440-50-8
Lead
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7439-92-1
Nickel
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7440-02-0
Selenium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:58
7782-49-2
Silver
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7440-22-4
Thallium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:58
7440-28-0
Vanadium
26.5
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:58
7440-62-2
Zinc
12.8
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:58
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/25/20 01:08
09/28/20 01:03
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 02:24
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 02:24
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 02:24
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 02:24
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 02:24
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 02:24
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 02:24
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 02:24
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 02:24
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 02:24
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/25/20 02:24
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/25/20 02:24
75-00-3
Chloroform
ND
ug/L
5.0
1
09/25/20 02:24
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 02:24
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 02:24
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 02:24
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 02:24
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 02:24
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 02:24
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 02:24
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 02:24
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/25/20 02:24
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/25/20 02:24
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW8 Lab ID: 92495813001 Collected: 09/16/20 12:50 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:24
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:24
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:24
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:24
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:24
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:24
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/25/20 02:24
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/25/20 02:24
591-78-6
lodomethane
ND
ug/L
20.0
1
09/25/20 02:24
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/25/20 02:24
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/25/20 02:24
108-10-1
Styrene
ND
ug/L
1.0
1
09/25/20 02:24
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 02:24
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 02:24
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/25/20 02:24
127-18-4
Toluene
ND
ug/L
1.0
1
09/25/20 02:24
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/25/20 02:24
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/25/20 02:24
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/25/20 02:24
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/25/20 02:24
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/25/20 02:24
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/25/20 02:24
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/25/20 02:24
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/25/20 02:24
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/25/20 02:24
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/25/20 02:24
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/25/20 02:24
460-00-4
1,2-Dichloroethane-d4 (S)
108
%
70-130
1
09/25/20 02:24
17060-07-0
Toluene-d8 (S)
94
%
70-130
1
09/25/20 02:24
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/18/20 05:43
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
102
%
50-150
1
09/18/20 05:43
17060-07-0
Toluene-d8 (S)
101
%
50-150
1
09/18/20 05:43
2037-26-5
Date: 09/29/2020 09:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW9
Lab ID: 92495813002 Collected:
09/16/20
12:12
Received: 09/16/20 14:23 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:01
7440-38-2
Barium
568
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 21:01
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 21:01
7440-43-9
Chromium
20.2
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7440-47-3
Cobalt
19.6
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7440-48-4
Copper
143
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7440-50-8
Lead
5.2
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7439-92-1
Nickel
12.9
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7440-02-0
Selenium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:01
7782-49-2
Silver
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7440-22-4
Thallium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:01
7440-28-0
Vanadium
120
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:01
7440-62-2
Zinc
56.4
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:01
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
0.15
ug/L
0.10
1
09/25/20 01:08
09/28/20 01:07
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 08:31
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 08:31
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 08:31
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 08:31
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 08:31
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 08:31
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 08:31
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 08:31
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 08:31
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 08:31
56-23-5
Chlorobenzene
1.3
ug/L
1.0
1
09/25/20 08:31
108-90-7
Chloroethane
6.7
ug/L
1.0
1
09/25/20 08:31
75-00-3 IL,v2
Chloroform
ND
ug/L
5.0
1
09/25/20 08:31
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 08:31
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 08:31
96-12-8 L1
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 08:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 08:31
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 08:31
74-95-3
1,2-Dichlorobenzene
2.4
ug/L
1.0
1
09/25/20 08:31
95-50-1
1,4-Dichlorobenzene
3.1
ug/L
1.0
1
09/25/20 08:31
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 08:31
110-57-6
1,1-Dichloroethane
14.3
ug/L
1.0
1
09/25/20 08:31
75-34-3
1,2-Dichloroethane
1.9
ug/L
1.0
1
09/25/20 08:31
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW9 Lab ID: 92495813002 Collected: 09/16/20 12:12 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/25/20 08:31
75-35-4
cis-1,2-Dichloroethene
31.7
ug/L
1.0
1
09/25/20 08:31
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 08:31
156-60-5
1,2-Dichloropropene
2.1
ug/L
1.0
1
09/25/20 08:31
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 08:31
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 08:31
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/25/20 08:31
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/25/20 08:31
591-78-6
lodomethane
ND
ug/L
20.0
1
09/25/20 08:31
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/25/20 08:31
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/25/20 08:31
108-10-1
Styrene
ND
ug/L
1.0
1
09/25/20 08:31
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 08:31
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 08:31
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/25/20 08:31
127-18-4
Toluene
ND
ug/L
1.0
1
09/25/20 08:31
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/25/20 08:31
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/25/20 08:31
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/25/20 08:31
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/25/20 08:31
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/25/20 08:31
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/25/20 08:31
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/25/20 08:31
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/25/20 08:31
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/25/20 08:31
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/25/20 08:31
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
09/25/20 08:31
460-00-4
1,2-Dichloroethane-d4 (S)
92
%
70-130
1
09/25/20 08:31
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
09/25/20 08:31
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
8.9
ug/L
2.0
1
09/18/20 06:40
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
114
%
50-150
1
09/18/20 06:40
17060-07-0
Toluene-d8 (S)
98
%
50-150
1
09/18/20 06:40
2037-26-5
Date: 09/29/2020 09:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW16 Lab ID: 92495813003 Collected: 09/16/20 11:39 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:04
7440-38-2
Barium
152
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 21:04
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 21:04
7440-43-9
Chromium
7.8
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7440-48-4
Copper
22.6
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7440-50-8
Lead
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7439-92-1
Nickel
5.4
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7440-02-0
Selenium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:04
7782-49-2
Silver
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7440-22-4
Thallium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:04
7440-28-0
Vanadium
32.7
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:04
7440-62-2
Zinc
17.4
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:04
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/25/20 01:08
09/28/20 01:18
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 02:42
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 02:42
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 02:42
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 02:42
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 02:42
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 02:42
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 02:42
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 02:42
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 02:42
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 02:42
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/25/20 02:42
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/25/20 02:42
75-00-3
Chloroform
ND
ug/L
5.0
1
09/25/20 02:42
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 02:42
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 02:42
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 02:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 02:42
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 02:42
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 02:42
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 02:42
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 02:42
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/25/20 02:42
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/25/20 02:42
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW16 Lab ID: 92495813003 Collected: 09/16/20 11:39 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:42
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:42
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:42
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:42
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:42
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/25/20 02:42
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/25/20 02:42
591-78-6
lodomethane
ND
ug/L
20.0
1
09/25/20 02:42
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/25/20 02:42
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/25/20 02:42
108-10-1
Styrene
ND
ug/L
1.0
1
09/25/20 02:42
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 02:42
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 02:42
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/25/20 02:42
127-18-4
Toluene
ND
ug/L
1.0
1
09/25/20 02:42
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/25/20 02:42
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/25/20 02:42
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/25/20 02:42
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/25/20 02:42
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/25/20 02:42
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/25/20 02:42
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/25/20 02:42
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/25/20 02:42
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/25/20 02:42
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/25/20 02:42
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
09/25/20 02:42
460-00-4
1,2-Dichloroethane-d4 (S)
108
%
70-130
1
09/25/20 02:42
17060-07-0
Toluene-d8 (S)
96
%
70-130
1
09/25/20 02:42
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/17/20 23:45
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
50-150
1
09/17/20 23:45
17060-07-0
Toluene-d8 (S)
99
%
50-150
1
09/17/20 23:45
2037-26-5
Date: 09/29/2020 09:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW14 Lab ID: 92495813004 Collected: 09/16/20 11:13 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:07
7440-38-2
Barium
33.0
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 21:07
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 21:07
7440-43-9
Chromium
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7440-48-4
Copper
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7440-50-8
Lead
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7439-92-1
Nickel
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7440-02-0
Selenium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:07
7782-49-2
Silver
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7440-22-4
Thallium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:07
7440-28-0
Vanadium
7.9
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:07
7440-62-2
Zinc
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:07
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/25/20 01:08
09/28/20 01:22
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 07:48
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 07:48
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 07:48
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 07:48
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 07:48
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 07:48
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 07:48
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 07:48
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 07:48
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 07:48
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/25/20 07:48
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/25/20 07:48
75-00-3
Chloroform
ND
ug/L
5.0
1
09/25/20 07:48
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 07:48
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 07:48
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 07:48
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 07:48
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 07:48
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 07:48
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 07:48
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 07:48
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/25/20 07:48
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/25/20 07:48
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW14 Lab ID: 92495813004 Collected: 09/16/20 11:13 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/29/2020 09:45 AM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
97
%
107
%
94
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
102 %
101 %
1.0
1
09/25/20 07:48
75-35-4
1.0
1
09/25/20 07:48
156-59-2
1.0
1
09/25/20 07:48
156-60-5
1.0
1
09/25/20 07:48
78-87-5
1.0
1
09/25/20 07:48
10061-01-5
1.0
1
09/25/20 07:48
10061-02-6
1.0
1
09/25/20 07:48
100-41-4
5.0
1
09/25/20 07:48
591-78-6
20.0
1
09/25/20 07:48
74-88-4
5.0
1
09/25/20 07:48
75-09-2
5.0
1
09/25/20 07:48
108-10-1
1.0
1
09/25/20 07:48
100-42-5
1.0
1
09/25/20 07:48
630-20-6
1.0
1
09/25/20 07:48
79-34-5
1.0
1
09/25/20 07:48
127-18-4
1.0
1
09/25/20 07:48
108-88-3
1.0
1
09/25/20 07:48
71-55-6
1.0
1
09/25/20 07:48
79-00-5
1.0
1
09/25/20 07:48
79-01-6
1.0
1
09/25/20 07:48
75-69-4
1.0
1
09/25/20 07:48
96-18-4
2.0
1
09/25/20 07:48
108-05-4
1.0
1
09/25/20 07:48
75-01-4
1.0
1
09/25/20 07:48
1330-20-7
2.0
1
09/25/20 07:48
179601-23-1
1.0
1
09/25/20 07:48
95-47-6
70-130 1
70-130 1
70-130 1
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/25/20 07:48 460-00-4
09/25/20 07:48 17060-07-0
09/25/20 07:48 2037-26-5
[ek7iE:7f��eIeI:7[eY�if��c?�;SQiI
09/18/20 06:02 17060-07-0
09/18/20 06:02 2037-26-5
Page 11 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW15
Lab ID: 92495813005 Collected:
09/16/20
11:26
Received: 09/16/20 14:23 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:17
7440-38-2
Barium
143
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 21:17
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 21:17
7440-43-9
Chromium
15.4
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7440-47-3
Cobalt
12.0
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7440-48-4
Copper
101
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7440-50-8
Lead
7.9
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7439-92-1
Nickel
5.8
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7440-02-0
Selenium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:17
7782-49-2
Silver
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7440-22-4
Thallium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:17
7440-28-0
Vanadium
80.1
ug/L
5.0
1
09/24/20 01:35
09/25/20 21:17
7440-62-2
Zinc
44.0
ug/L
10.0
1
09/24/20 01:35
09/25/20 21:17
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/25/20 01:08
09/28/20 01:25
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 06:23
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 06:23
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 06:23
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 06:23
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 06:23
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 06:23
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 06:23
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 06:23
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 06:23
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 06:23
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/25/20 06:23
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/25/20 06:23
75-00-3 IL,v2
Chloroform
ND
ug/L
5.0
1
09/25/20 06:23
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 06:23
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 06:23
96-12-8 L1
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 06:23
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 06:23
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 06:23
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 06:23
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 06:23
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 06:23
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/25/20 06:23
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/25/20 06:23
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: 6002-HRW15 Lab ID: 92495813005 Collected: 09/16/20 11:26 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/29/2020 09:45 AM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
95
%
89
%
102
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
100 %
101 %
1.0
1
09/25/20 06:23
75-35-4
1.0
1
09/25/20 06:23
156-59-2
1.0
1
09/25/20 06:23
156-60-5
1.0
1
09/25/20 06:23
78-87-5
1.0
1
09/25/20 06:23
10061-01-5
1.0
1
09/25/20 06:23
10061-02-6
1.0
1
09/25/20 06:23
100-41-4
5.0
1
09/25/20 06:23
591-78-6
20.0
1
09/25/20 06:23
74-88-4
5.0
1
09/25/20 06:23
75-09-2
5.0
1
09/25/20 06:23
108-10-1
1.0
1
09/25/20 06:23
100-42-5
1.0
1
09/25/20 06:23
630-20-6
1.0
1
09/25/20 06:23
79-34-5
1.0
1
09/25/20 06:23
127-18-4
1.0
1
09/25/20 06:23
108-88-3
1.0
1
09/25/20 06:23
71-55-6
1.0
1
09/25/20 06:23
79-00-5
1.0
1
09/25/20 06:23
79-01-6
1.0
1
09/25/20 06:23
75-69-4
1.0
1
09/25/20 06:23
96-18-4
2.0
1
09/25/20 06:23
108-05-4
1.0
1
09/25/20 06:23
75-01-4
1.0
1
09/25/20 06:23
1330-20-7
2.0
1
09/25/20 06:23
179601-23-1
1.0
1
09/25/20 06:23
95-47-6
70-130 1
70-130 1
70-130 1
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/25/20 06:23 460-00-4
09/25/20 06:23 17060-07-0
09/25/20 06:23 2037-26-5
[ek71E:Wil11I-VA=iPaS4 N
09/18/20 06:21 17060-07-0
09/18/20 06:21 2037-26-5
Page 13 of 37

leAnalyiical
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ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: Trip Blank
Lab ID: 92495813006 Collected:
09/16/20
09:21
Received: 09/16/20 14:23 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 00:36
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 00:36
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 00:36
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 00:36
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 00:36
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 00:36
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 00:36
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 00:36
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 00:36
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 00:36
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/25/20 00:36
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/25/20 00:36
75-00-3
Chloroform
ND
ug/L
5.0
1
09/25/20 00:36
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 00:36
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 00:36
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 00:36
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 00:36
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 00:36
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 00:36
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 00:36
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 00:36
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/25/20 00:36
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/25/20 00:36
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
09/25/20 00:36
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 00:36
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 00:36
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/25/20 00:36
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 00:36
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 00:36
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/25/20 00:36
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/25/20 00:36
591-78-6
lodomethane
ND
ug/L
20.0
1
09/25/20 00:36
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/25/20 00:36
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/25/20 00:36
108-10-1
Styrene
ND
ug/L
1.0
1
09/25/20 00:36
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 00:36
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 00:36
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/25/20 00:36
127-18-4
Toluene
ND
ug/L
1.0
1
09/25/20 00:36
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/25/20 00:36
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/25/20 00:36
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/25/20 00:36
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/25/20 00:36
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/25/20 00:36
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/25/20 00:36
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/25/20 00:36
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 37

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
Sample: Trip Blank
Parameters
Lab ID: 92495813006 Collected: 09/16/20 09:21
Results Units Report Limit DF
Received: 09/16/20 14:23 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
09/25/20 00:36
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
09/25/20 00:36
179601-23-1
o-Xylene
ND ug/L
1.0
1
09/25/20 00:36
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
1
09/25/20 00:36
460-00-4
1,2-Dichloroethane-d4 (S)
102 %
70-130
1
09/25/20 00:36
17060-07-0
Toluene-d8 (S)
95 %
70-130
1
09/25/20 00:36
2037-26-5
Date: 09/29/2020 09:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
QC Batch: 568568 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495813001, 92495813002, 92495813003, 92495813004, 92495813005
METHOD BLANK: 3012589 Matrix: Water
Associated Lab Samples: 92495813001, 92495813002, 92495813003, 92495813004, 92495813005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
09/25/20 20:26
Arsenic
ug/L
ND
10.0
09/25/20 20:26
Barium
ug/L
ND
5.0
09/25/20 20:26
Beryllium
ug/L
ND
1.0
09/25/20 20:26
Cadmium
ug/L
ND
1.0
09/25/20 20:26
Chromium
ug/L
ND
5.0
09/25/20 20:26
Cobalt
ug/L
ND
5.0
09/25/20 20:26
Copper
ug/L
ND
5.0
09/25/20 20:26
Lead
ug/L
ND
5.0
09/25/20 20:26
Nickel
ug/L
ND
5.0
09/25/20 20:26
Selenium
ug/L
ND
10.0
09/25/20 20:26
Silver
ug/L
ND
5.0
09/25/20 20:26
Thallium
ug/L
ND
10.0
09/25/20 20:26
Vanadium
ug/L
ND
5.0
09/25/20 20:26
Zinc
ug/L
ND
10.0
09/25/20 20:26
LABORATORY CONTROL SAMPLE:
Parameter
3012590
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
472
94
80-120
Arsenic
ug/L
500
465
93
80-120
Barium
ug/L
500
504
101
80-120
Beryllium
ug/L
500
507
101
80-120
Cadmium
ug/L
500
475
95
80-120
Chromium
ug/L
500
489
98
80-120
Cobalt
ug/L
500
474
95
80-120
Copper
ug/L
500
498
100
80-120
Lead
ug/L
500
472
94
80-120
Nickel
ug/L
500
481
96
80-120
Selenium
ug/L
500
465
93
80-120
Silver
ug/L
250
241
96
80-120
Thallium
ug/L
500
471
94
80-120
Vanadium
ug/L
500
483
97
80-120
Zinc
ug/L
500
458
92
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Road Landfill
92495813
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3012591
3012592
MS
MSD
92495794001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
489
494
98
99
75-125
1
Arsenic
ug/L
ND
500
500
499
505
100
101
75-125
1
Barium
ug/L
56.6
500
500
585
585
106
106
75-125
0
Beryllium
ug/L
ND
500
500
532
532
106
106
75-125
0
Cadmium
ug/L
ND
500
500
506
510
101
102
75-125
1
Chromium
ug/L
ND
500
500
512
516
102
103
75-125
1
Cobalt
ug/L
ND
500
500
494
498
99
99
75-125
1
Copper
ug/L
6.0
500
500
525
530
104
105
75-125
1
Lead
ug/L
ND
500
500
496
502
99
100
75-125
1
Nickel
ug/L
ND
500
500
501
504
100
101
75-125
1
Selenium
ug/L
ND
500
500
518
525
103
105
75-125
2
Silver
ug/L
ND
250
250
250
252
100
101
75-125
1
Thallium
ug/L
ND
500
500
491
493
98
99
75-125
0
Vanadium
ug/L
10.1
500
500
517
520
101
102
75-125
0
Zinc
ug/L
ND
500
500
491
496
97
98
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
QC Batch: 568898 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495813001, 92495813002, 92495813003, 92495813004, 92495813005
METHOD BLANK: 3014112
Matrix:
Water
Associated Lab Samples: 92495813001, 92495813002, 92495813003, 92495813004, 92495813005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.10
09/27/20 20:33
LABORATORY CONTROL SAMPLE:
3014113
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
10.1
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3014114 3014115
MS MSD
92494939003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.2 10.3 102 103 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
QC Batch: 568862 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495813001, 92495813003, 92495813006
METHOD BLANK: 3013939 Matrix:
Associated Lab Samples: 92495813001, 92495813003, 92495813006
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1,1-Trichloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1,2-Trichloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1-Dichloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1-Dichloroethene
ug/L
ND
1.0
09/24/20 23:24
1,2,3-Trichloropropane
ug/L
ND
1.0
09/24/20 23:24
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
09/24/20 23:24
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/24/20 23:24
1,2-Dichlorobenzene
ug/L
ND
1.0
09/24/20 23:24
1,2-Dichloroethane
ug/L
ND
1.0
09/24/20 23:24
1,2-Dichloropropane
ug/L
ND
1.0
09/24/20 23:24
1,4-Dichlorobenzene
ug/L
ND
1.0
09/24/20 23:24
2-Butanone (MEK)
ug/L
ND
5.0
09/24/20 23:24
2-Hexanone
ug/L
ND
5.0
09/24/20 23:24
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/24/20 23:24
Acetone
ug/L
ND
25.0
09/24/20 23:24
Acrylonitrile
ug/L
ND
10.0
09/24/20 23:24
Benzene
ug/L
ND
1.0
09/24/20 23:24
Bromochloromethane
ug/L
ND
1.0
09/24/20 23:24
Bromodichloromethane
ug/L
ND
1.0
09/24/20 23:24
Bromoform
ug/L
ND
1.0
09/24/20 23:24
Bromomethane
ug/L
ND
2.0
09/24/20 23:24
Carbon disulfide
ug/L
ND
2.0
09/24/20 23:24
Carbon tetrachloride
ug/L
ND
1.0
09/24/20 23:24
Chlorobenzene
ug/L
ND
1.0
09/24/20 23:24
Chloroethane
ug/L
ND
1.0
09/24/20 23:24
Chloroform
ug/L
ND
5.0
09/24/20 23:24
Chloromethane
ug/L
ND
1.0
09/24/20 23:24
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 23:24
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 23:24
Dibromochloromethane
ug/L
ND
1.0
09/24/20 23:24
Dibromomethane
ug/L
ND
1.0
09/24/20 23:24
Ethylbenzene
ug/L
ND
1.0
09/24/20 23:24
lodomethane
ug/L
ND
20.0
09/24/20 23:24
m&p-Xylene
ug/L
ND
2.0
09/24/20 23:24
Methylene Chloride
ug/L
ND
5.0
09/24/20 23:24
o-Xylene
ug/L
ND
1.0
09/24/20 23:24
Styrene
ug/L
ND
1.0
09/24/20 23:24
Tetrachloroethene
ug/L
ND
1.0
09/24/20 23:24
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
METHOD BLANK: 3013939 Matrix:
Associated Lab Samples: 92495813001, 92495813003, 92495813006
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
09/24/20 23:24
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 23:24
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 23:24
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/24/20 23:24
Trichloroethene
ug/L
ND
1.0
09/24/20 23:24
Trichlorofluoromethane
ug/L
ND
1.0
09/24/20 23:24
Vinyl acetate
ug/L
ND
2.0
09/24/20 23:24
Vinyl chloride
ug/L
ND
1.0
09/24/20 23:24
Xylene (Total)
ug/L
ND
1.0
09/24/20 23:24
1,2-Dichloroethane-d4 (S)
%
106
70-130
09/24/20 23:24
4-Bromofluorobenzene (S)
%
98
70-130
09/24/20 23:24
Toluene-d8 (S)
%
94
70-130
09/24/20 23:24
LABORATORY CONTROL SAMPLE:
Parameter
3013940
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.1
106
70-130
1,1,1-Trichloroethane
ug/L
50
48.8
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.9
106
70-130
1,1,2-Trichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethane
ug/L
50
49.3
99
70-130
1,1-Dichloroethene
ug/L
50
49.5
99
70-130
1,2,3-Trichloropropane
ug/L
50
54.6
109
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.1
108
70-130
1,2-Dibromoethane (EDB)
ug/L
50
52.5
105
70-130
1,2-Dichlorobenzene
ug/L
50
51.7
103
70-130
1,2-Dichloroethane
ug/L
50
47.3
95
70-130
1,2-Dichloropropane
ug/L
50
48.0
96
70-130
1,4-Dichlorobenzene
ug/L
50
52.4
105
70-130
2-Butanone (MEK)
ug/L
100
101
101
64-135
2-Hexanone
ug/L
100
112
112
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
103
103
70-130
Acetone
ug/L
100
102
102
61-157
Acrylonitrile
ug/L
250
262
105
61-143
Benzene
ug/L
50
49.6
99
70-130
Bromochloromethane
ug/L
50
49.6
99
70-130
Bromodichloromethane
ug/L
50
44.8
90
70-130
Bromoform
ug/L
50
54.6
109
70-130
Bromomethane
ug/L
50
38.4
77
38-130 v3
Carbon disulfide
ug/L
50
52.9
106
68-130
Carbon tetrachloride
ug/L
50
45.4
91
70-130
Chlorobenzene
ug/L
50
51.0
102
70-130
Chloroethane
ug/L
50
41.4
83
37-142
Chloroform
ug/L
50
51.0
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
LABORATORY CONTROL SAMPLE:
Parameter
3013940
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
46.7
93
48-130
49.8
100
70-130
52.2
104
70-130
53.8
108
70-130
49.9
100
70-130
49.4
99
70-130
106
106
40-130
98.6
99
70-130
48.7
97
67-132
50.5
101
70-131
53.5
107
70-130
48.6
97
69-130
48.8
98
70-130
51.4
103
70-130
51.2
102
70-130
64.0
128
35-189
48.2
96
70-130
40.0
80
63-130
111
111
55-143
44.2
88
70-131
149
99
70-130
90
70-130
102
70-130
99
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3013941
MS
92495794003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3013942
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
19.2
20.4
96
102
73-134
6
1,1,1-Trichloroethane
ug/L
ND
20
20
20.2
21.1
101
106
82-143
5
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.3
19.7
97
98
70-136
2
1,1,2-Trichloroethane
ug/L
ND
20
20
18.5
19.4
92
97
70-135
5
1,1-Dichloroethane
ug/L
ND
20
20
19.7
20.1
98
100
70-139
2
1,1-Dichloroethene
ug/L
ND
20
20
21.4
21.3
107
106
70-154
1
1,2,3-Trichloropropane
ug/L
ND
20
20
18.0
18.9
90
94
71-137
5
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
19.1
19.6
96
98
65-134
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
18.9
20.5
95
102
70-137
8
1,2-Dichlorobenzene
ug/L
ND
20
20
19.3
19.4
96
97
70-133
0
1,2-Dichloroethane
ug/L
ND
20
20
19.9
20.2
100
101
70-137
1
1,2-Dichloropropane
ug/L
ND
20
20
19.7
20.4
99
102
70-140
4
1,4-Dichlorobenzene
ug/L
ND
20
20
19.9
20.7
100
104
70-133
4
2-Butanone (MEK)
ug/L
ND
40
40
43.4
46.1
108
115
60-139
6
2-Hexanone
ug/L
ND
40
40
42.4
42.8
106
107
65-138
1
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
39.0
39.2
97
98
65-135
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC.
Page 21 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3013941
MS
92495794003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3013942
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
41.8
39.9
105
100
60-148
5
Acrylonitrile
ug/L
ND
100
100
102
102
102
102
64-147
0
Benzene
ug/L
ND
20
20
20.3
20.6
102
103
70-151
1
Bromochloromethane
ug/L
ND
20
20
19.2
19.0
96
95
70-141
1
Bromodichloromethane
ug/L
ND
20
20
16.6
17.6
83
88
70-138
6
Bromoform
ug/L
ND
20
20
17.9
18.3
89
92
63-130
3
Bromomethane
ug/L
ND
20
20
10.4
11.8
52
59
15-152
13 v3
Carbon disulfide
ug/L
ND
20
20
19.2
18.7
96
93
69-149
3
Carbon tetrachloride
ug/L
ND
20
20
20.3
20.7
101
104
70-143
2
Chlorobenzene
ug/L
ND
20
20
19.7
20.4
99
102
70-138
3
Chloroethane
ug/L
ND
20
20
20.6
20.3
103
101
52-163
1
Chloroform
ug/L
ND
20
20
19.9
19.5
99
98
70-139
2
Chloromethane
ug/L
ND
20
20
17.3
18.1
86
90
41-139
5
cis-1,2-Dichloroethene
ug/L
ND
20
20
19.8
20.4
99
102
70-141
3
cis-1,3-Dichloropropene
ug/L
ND
20
20
19.9
20.4
99
102
70-137
3
Dibromochloromethane
ug/L
ND
20
20
18.8
20.1
94
100
70-134
6
Dibromomethane
ug/L
ND
20
20
18.9
20.3
95
101
70-138
7
Ethylbenzene
ug/L
ND
20
20
19.5
20.1
97
100
66-153
3
lodomethane
ug/L
ND
40
40
29.8
39.2
75
98
20-138
27
m&p-Xylene
ug/L
ND
40
40
38.8
40.2
97
100
69-152
3
Methylene Chloride
ug/L
ND
20
20
21.1
20.8
105
104
42-159
1
o-Xylene
ug/L
ND
20
20
19.4
19.7
97
99
70-148
2
Styrene
ug/L
ND
20
20
19.7
20.5
99
102
70-135
4
Tetrachloroethene
ug/L
ND
20
20
19.7
20.5
98
103
59-143
4
Toluene
ug/L
ND
20
20
19.3
19.3
96
96
59-148
0
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.4
20.8
102
104
70-146
2
trans- 1,3-Dichloropropene
ug/L
ND
20
20
18.8
19.5
94
97
70-135
3
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
17.8
18.7
89
94
47-135
5
Trichloroethene
ug/L
ND
20
20
19.8
20.3
99
102
70-147
3
Trichlorofluoromethane
ug/L
ND
20
20
18.6
18.0
93
90
70-148
4
Vinyl acetate
ug/L
ND
40
40
42.6
44.6
106
111
49-151
5
Vinyl chloride
ug/L
ND
20
20
17.2
17.3
86
87
70-156
1
Xylene (Total)
ug/L
ND
60
60
58.2
59.9
97
100
63-158
3
1,2-Dichloroethane-d4 (S)
%
105
106
70-130
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8(S)
%
98
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
QC Batch: 568865 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495813004
METHOD BLANK: 3013948
Associated Lab Samples: 92495813004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 23:42
1,1,1-Trichloroethane
ug/L
ND
1.0
09/24/20 23:42
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 23:42
1,1,2-Trichloroethane
ug/L
ND
1.0
09/24/20 23:42
1,1-Dichloroethane
ug/L
ND
1.0
09/24/20 23:42
1,1-Dichloroethene
ug/L
ND
1.0
09/24/20 23:42
1,2,3-Trichloropropane
ug/L
ND
1.0
09/24/20 23:42
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
09/24/20 23:42
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/24/20 23:42
1,2-Dichlorobenzene
ug/L
ND
1.0
09/24/20 23:42
1,2-Dichloroethane
ug/L
ND
1.0
09/24/20 23:42
1,2-Dichloropropane
ug/L
ND
1.0
09/24/20 23:42
1,4-Dichlorobenzene
ug/L
ND
1.0
09/24/20 23:42
2-Butanone (MEK)
ug/L
ND
5.0
09/24/20 23:42
2-Hexanone
ug/L
ND
5.0
09/24/20 23:42
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/24/20 23:42
Acetone
ug/L
ND
25.0
09/24/20 23:42
Acrylonitrile
ug/L
ND
10.0
09/24/20 23:42
Benzene
ug/L
ND
1.0
09/24/20 23:42
Bromochloromethane
ug/L
ND
1.0
09/24/20 23:42
Bromodichloromethane
ug/L
ND
1.0
09/24/20 23:42
Bromoform
ug/L
ND
1.0
09/24/20 23:42
Bromomethane
ug/L
ND
2.0
09/24/20 23:42 v2
Carbon disulfide
ug/L
ND
2.0
09/24/20 23:42
Carbon tetrachloride
ug/L
ND
1.0
09/24/20 23:42
Chlorobenzene
ug/L
ND
1.0
09/24/20 23:42
Chloroethane
ug/L
ND
1.0
09/24/20 23:42
Chloroform
ug/L
ND
5.0
09/24/20 23:42
Chloromethane
ug/L
ND
1.0
09/24/20 23:42
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 23:42
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 23:42
Dibromochloromethane
ug/L
ND
1.0
09/24/20 23:42
Dibromomethane
ug/L
ND
1.0
09/24/20 23:42
Ethylbenzene
ug/L
ND
1.0
09/24/20 23:42
lodomethane
ug/L
ND
20.0
09/24/20 23:42
m&p-Xylene
ug/L
ND
2.0
09/24/20 23:42
Methylene Chloride
ug/L
ND
5.0
09/24/20 23:42
o-Xylene
ug/L
ND
1.0
09/24/20 23:42
Styrene
ug/L
ND
1.0
09/24/20 23:42
Tetrachloroethene
ug/L
ND
1.0
09/24/20 23:42
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC.
Page 23 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
METHOD BLANK: 3013948
Associated Lab Samples: 92495813004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
09/24/20 23:42
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 23:42
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 23:42
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/24/20 23:42
Trichloroethene
ug/L
ND
1.0
09/24/20 23:42
Trichlorofluoromethane
ug/L
ND
1.0
09/24/20 23:42
Vinyl acetate
ug/L
ND
2.0
09/24/20 23:42
Vinyl chloride
ug/L
ND
1.0
09/24/20 23:42
Xylene (Total)
ug/L
ND
1.0
09/24/20 23:42
1,2-Dichloroethane-d4 (S)
%
106
70-130
09/24/20 23:42
4-Bromofluorobenzene (S)
%
99
70-130
09/24/20 23:42
Toluene-d8 (S)
%
95
70-130
09/24/20 23:42
LABORATORY CONTROL SAMPLE:
Parameter
3013949
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.1
100
70-130
1,1,1-Trichloroethane
ug/L
50
46.7
93
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.6
103
70-130
1,1,2-Trichloroethane
ug/L
50
47.9
96
70-130
1,1-Dichloroethane
ug/L
50
46.7
93
70-130
1,1-Dichloroethene
ug/L
50
46.7
93
70-130
1,2,3-Trichloropropane
ug/L
50
52.6
105
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
56.1
112
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.4
101
70-130
1,2-Dichlorobenzene
ug/L
50
49.4
99
70-130
1,2-Dichloroethane
ug/L
50
47.3
95
70-130
1,2-Dichloropropane
ug/L
50
45.6
91
70-130
1,4-Dichlorobenzene
ug/L
50
49.6
99
70-130
2-Butanone (MEK)
ug/L
100
101
101
64-135
2-Hexanone
ug/L
100
111
111
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
103
103
70-130
Acetone
ug/L
100
105
105
61-157
Acrylonitrile
ug/L
250
261
105
61-143
Benzene
ug/L
50
46.5
93
70-130
Bromochloromethane
ug/L
50
48.7
97
70-130
Bromodichloromethane
ug/L
50
43.6
87
70-130
Bromoform
ug/L
50
52.4
105
70-130
Bromomethane
ug/L
50
38.6
77
38-130 v3
Carbon disulfide
ug/L
50
50.0
100
68-130
Carbon tetrachloride
ug/L
50
44.1
88
70-130
Chlorobenzene
ug/L
50
48.5
97
70-130
Chloroethane
ug/L
50
38.2
76
37-142
Chloroform
ug/L
50
48.9
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
LABORATORY CONTROL SAMPLE:
Parameter
3013949
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
44.1
88
48-130
47.3
95
70-130
50.2
100
70-130
51.4
103
70-130
48.7
97
70-130
46.2
92
70-130
99.9
100
40-130
92.8
93
70-130
46.9
94
67-132
47.0
94
70-131
50.6
101
70-130
46.0
92
69-130
45.9
92
70-130
48.3
97
70-130
49.6
99
70-130
62.1
124
35-189
44.6
89
70-130
38.3
77
63-130
109
109
55-143
41.7
83
70-131
140
93
70-130
92
70-130
101
70-130
98
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3013950
MS
92494865022 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3013951
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.2
20.9
106
104
73-134
2
1,1,1-Trichloroethane
ug/L
ND
20
20
21.1
20.9
106
105
82-143
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.4
20.1
102
101
70-136
1
1,1,2-Trichloroethane
ug/L
ND
20
20
20.3
19.7
101
99
70-135
3
1,1-Dichloroethane
ug/L
ND
20
20
20.0
20.0
100
100
70-139
0
1,1-Dichloroethene
ug/L
ND
20
20
20.6
20.7
103
103
70-154
1
1,2,3-Trichloropropane
ug/L
ND
20
20
19.5
19.6
97
98
71-137
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.1
20.2
106
101
65-134
5
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.0
20.7
105
103
70-137
1
1,2-Dichlorobenzene
ug/L
ND
20
20
20.9
20.1
104
100
70-133
4
1,2-Dichloroethane
ug/L
ND
20
20
20.4
20.0
102
100
70-137
2
1,2-Dichloropropane
ug/L
ND
20
20
21.0
20.2
105
101
70-140
4
1,4-Dichlorobenzene
ug/L
ND
20
20
21.5
20.8
107
104
70-133
3
2-Butanone (MEK)
ug/L
ND
40
40
48.0
45.2
120
113
60-139
6
2-Hexanone
ug/L
ND
40
40
44.1
43.5
110
109
65-138
1
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
41.6
40.3
104
101
65-135
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC.
Page 25 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3013950
MS
92494865022 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3013951
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
40.2
41.4
101
103
60-148
3
Acrylonitrile
ug/L
ND
100
100
104
103
104
103
64-147
1
Benzene
ug/L
ND
20
20
21.3
20.9
106
104
70-151
2
Bromochloromethane
ug/L
ND
20
20
19.5
20.1
98
100
70-141
3
Bromodichloromethane
ug/L
ND
20
20
18.5
17.9
93
90
70-138
3
Bromoform
ug/L
ND
20
20
18.7
19.0
93
95
63-130
2
Bromomethane
ug/L
ND
20
20
13.0
13.6
65
68
15-152
5 v3
Carbon disulfide
ug/L
ND
20
20
19.1
19.3
96
96
69-149
1
Carbon tetrachloride
ug/L
ND
20
20
20.2
20.8
101
104
70-143
3
Chlorobenzene
ug/L
ND
20
20
20.7
20.8
104
104
70-138
0
Chloroethane
ug/L
ND
20
20
20.3
19.1
101
96
52-163
6
Chloroform
ug/L
ND
20
20
19.6
19.6
98
98
70-139
0
Chloromethane
ug/L
ND
20
20
18.3
18.1
91
90
41-139
1
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.6
20.3
103
101
70-141
2
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.1
20.4
106
102
70-137
3
Dibromochloromethane
ug/L
ND
20
20
20.5
20.1
102
100
70-134
2
Dibromomethane
ug/L
ND
20
20
20.7
19.4
104
97
70-138
6
Ethylbenzene
ug/L
ND
20
20
20.7
20.2
103
101
66-153
2
lodomethane
ug/L
ND
40
40
42.1
41.6
105
104
20-138
1
m&p-Xylene
ug/L
ND
40
40
41.6
40.5
104
101
69-152
3
Methylene Chloride
ug/L
ND
20
20
20.4
20.2
102
101
42-159
1
o-Xylene
ug/L
ND
20
20
20.3
20.4
101
102
70-148
1
Styrene
ug/L
ND
20
20
21.3
20.8
106
104
70-135
2
Tetrachloroethene
ug/L
ND
20
20
19.9
19.7
100
99
59-143
1
Toluene
ug/L
ND
20
20
20.0
19.5
100
98
59-148
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.6
21.4
108
107
70-146
1
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.1
19.9
101
99
70-135
1
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
19.6
19.8
98
99
47-135
1
Trichloroethene
ug/L
ND
20
20
20.9
20.7
105
104
70-147
1
Trichlorofluoromethane
ug/L
ND
20
20
17.9
18.4
89
92
70-148
3
Vinyl acetate
ug/L
ND
40
40
44.8
43.3
112
108
49-151
4
Vinyl chloride
ug/L
ND
20
20
17.7
18.3
89
91
70-156
3
Xylene (Total)
ug/L
ND
60
60
61.9
61.0
103
102
63-158
2
1,2-Dichloroethane-d4 (S)
%
104
103
70-130
4-Bromofluorobenzene (S)
%
98
100
70-130
Toluene-d8(S)
%
96
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC.
Page 26 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
QC Batch: 568867 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495813002, 92495813005
METHOD BLANK: 3013960
Associated Lab Samples: 92495813002, 92495813005
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/25/20 03:57
1,1,1-Trichloroethane
ug/L
ND
1.0
09/25/20 03:57
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/25/20 03:57
1,1,2-Trichloroethane
ug/L
ND
1.0
09/25/20 03:57
1,1-Dichloroethane
ug/L
ND
1.0
09/25/20 03:57
1,1-Dichloroethene
ug/L
ND
1.0
09/25/20 03:57
1,2,3-Trichloropropane
ug/L
ND
1.0
09/25/20 03:57
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
09/25/20 03:57
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/25/20 03:57
1,2-Dichlorobenzene
ug/L
ND
1.0
09/25/20 03:57
1,2-Dichloroethane
ug/L
ND
1.0
09/25/20 03:57
1,2-Dichloropropane
ug/L
ND
1.0
09/25/20 03:57
1,4-Dichlorobenzene
ug/L
ND
1.0
09/25/20 03:57
2-Butanone (MEK)
ug/L
ND
5.0
09/25/20 03:57
2-Hexanone
ug/L
ND
5.0
09/25/20 03:57
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/25/20 03:57
Acetone
ug/L
ND
25.0
09/25/20 03:57
Acrylonitrile
ug/L
ND
10.0
09/25/20 03:57
Benzene
ug/L
ND
1.0
09/25/20 03:57
Bromochloromethane
ug/L
ND
1.0
09/25/20 03:57
Bromodichloromethane
ug/L
ND
1.0
09/25/20 03:57
Bromoform
ug/L
ND
1.0
09/25/20 03:57
Bromomethane
ug/L
ND
2.0
09/25/20 03:57
Carbon disulfide
ug/L
ND
2.0
09/25/20 03:57
Carbon tetrachloride
ug/L
ND
1.0
09/25/20 03:57
Chlorobenzene
ug/L
ND
1.0
09/25/20 03:57
Chloroethane
ug/L
ND
1.0
09/25/20 03:57 IL,v2
Chloroform
ug/L
ND
5.0
09/25/20 03:57
Chloromethane
ug/L
ND
1.0
09/25/20 03:57
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/25/20 03:57
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/25/20 03:57
Dibromochloromethane
ug/L
ND
1.0
09/25/20 03:57
Dibromomethane
ug/L
ND
1.0
09/25/20 03:57
Ethylbenzene
ug/L
ND
1.0
09/25/20 03:57
lodomethane
ug/L
ND
20.0
09/25/20 03:57
m&p-Xylene
ug/L
ND
2.0
09/25/20 03:57
Methylene Chloride
ug/L
ND
5.0
09/25/20 03:57
o-Xylene
ug/L
ND
1.0
09/25/20 03:57
Styrene
ug/L
ND
1.0
09/25/20 03:57
Tetrachloroethene
ug/L
ND
1.0
09/25/20 03:57
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
METHOD BLANK: 3013960
Associated Lab Samples: 92495813002, 92495813005
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
09/25/20 03:57
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/25/20 03:57
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/25/20 03:57
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/25/20 03:57
Trichloroethene
ug/L
ND
1.0
09/25/20 03:57
Trichlorofluoromethane
ug/L
ND
1.0
09/25/20 03:57
Vinyl acetate
ug/L
ND
2.0
09/25/20 03:57
Vinyl chloride
ug/L
ND
1.0
09/25/20 03:57
Xylene (Total)
ug/L
ND
1.0
09/25/20 03:57
1,2-Dichloroethane-d4 (S)
%
94
70-130
09/25/20 03:57
4-Bromofluorobenzene (S)
%
96
70-130
09/25/20 03:57
Toluene-d8 (S)
%
99
70-130
09/25/20 03:57
LABORATORY CONTROL SAMPLE: 3013961
Qualifiers
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
70-130
1,1,1-Trichloroethane
ug/L
50
49.4
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.8
104
70-130
1,1,2-Trichloroethane
ug/L
50
50.9
102
70-130
1,1-Dichloroethane
ug/L
50
49.7
99
70-130
1,1-Dichloroethene
ug/L
50
49.6
99
70-130
1,2,3-Trichloropropane
ug/L
50
53.4
107
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
71.8
144
70-130 L1
1,2-Dibromoethane (EDB)
ug/L
50
52.2
104
70-130
1,2-Dichlorobenzene
ug/L
50
50.1
100
70-130
1,2-Dichloroethane
ug/L
50
46.6
93
70-130
1,2-Dichloropropane
ug/L
50
50.0
100
70-130
1,4-Dichlorobenzene
ug/L
50
48.8
98
70-130
2-Butanone (MEK)
ug/L
100
99.3
99
64-135
2-Hexanone
ug/L
100
104
104
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
104
104
61-157
Acrylonitrile
ug/L
250
264
106
61-143
Benzene
ug/L
50
48.9
98
70-130
Bromochloromethane
ug/L
50
52.1
104
70-130
Bromodichloromethane
ug/L
50
45.9
92
70-130
Bromoform
ug/L
50
51.5
103
70-130
Bromomethane
ug/L
50
41.3
83
38-130
Carbon disulfide
ug/L
50
47.8
96
68-130
Carbon tetrachloride
ug/L
50
47.8
96
70-130
Chlorobenzene
ug/L
50
49.0
98
70-130
Chloroethane
ug/L
50
28.9
58
37-142 IL,v3
Chloroform
ug/L
50
47.7
95
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 37

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
LABORATORY CONTROL SAMPLE:
Parameter
3013961
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
41.0
82
48-130
48.7
97
70-130
51.6
103
70-130
51.2
102
70-130
49.7
99
70-130
48.5
97
70-130
107
107
40-130
95.8
96
70-130
47.2
94
67-132
48.7
97
70-131
50.4
101
70-130
48.3
97
69-130
48.7
97
70-130
49.3
99
70-130
49.7
99
70-130
47.6
95
35-189
51.0
102
70-130
38.8
78
63-130
110
110
55-143
41.8
84
70-131
145
96
70-130
88
70-130
100
70-130
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3013962
MS
92496293015 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3013963
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
17.3
17.0
86
85
73-134
2
1,1,1-Trichloroethane
ug/L
ND
20
20
18.2
17.2
91
86
82-143
5
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
17.7
17.2
88
86
70-136
3
1,1,2-Trichloroethane
ug/L
ND
20
20
17.7
17.1
88
85
70-135
4
1,1-Dichloroethane
ug/L
ND
20
20
17.9
17.6
90
88
70-139
2
1,1-Dichloroethene
ug/L
ND
20
20
19.1
19.1
95
95
70-154
0
1,2,3-Trichloropropane
ug/L
ND
20
20
17.8
17.3
89
86
71-137
3
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
25.4
23.8
127
119
65-134
7
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
17.2
17.4
86
87
70-137
1
1,2-Dichlorobenzene
ug/L
ND
20
20
17.0
16.3
85
81
70-133
4
1,2-Dichloroethane
ug/L
ND
20
20
16.9
16.6
84
83
70-137
2
1,2-Dichloropropane
ug/L
ND
20
20
18.0
17.3
90
87
70-140
4
1,4-Dichlorobenzene
ug/L
ND
20
20
16.8
16.2
84
81
70-133
4
2-Butanone (MEK)
ug/L
ND
40
40
33.8
33.1
85
83
60-139
2
2-Hexanone
ug/L
ND
40
40
35.5
34.2
89
86
65-138
4
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
34.4
33.0
86
83
65-135
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC.
Page 29 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3013962
MS
92496293015 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3013963
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
36.6
35.3
91
88
60-148
4
Acrylonitrile
ug/L
ND
100
100
89.7
86.8
90
87
64-147
3
Benzene
ug/L
ND
20
20
18.1
17.1
91
86
70-151
6
Bromochloromethane
ug/L
ND
20
20
17.7
17.7
88
89
70-141
0
Bromodichloromethane
ug/L
ND
20
20
16.5
15.2
82
76
70-138
8
Bromoform
ug/L
ND
20
20
16.7
16.5
84
83
63-130
1
Bromomethane
ug/L
ND
20
20
15.2
15.5
76
78
15-152
2
Carbon disulfide
ug/L
ND
20
20
17.9
17.6
89
88
69-149
2
Carbon tetrachloride
ug/L
ND
20
20
18.7
17.5
93
88
70-143
6
Chlorobenzene
ug/L
ND
20
20
17.4
17.0
87
85
70-138
2
Chloroethane
ug/L
ND
20
20
14.6
13.8
73
69
52-163
61L,v3
Chloroform
ug/L
ND
20
20
16.8
16.9
84
85
70-139
0
Chloromethane
ug/L
ND
20
20
15.3
14.4
76
72
41-139
6
cis-1,2-Dichloroethene
ug/L
ND
20
20
17.6
17.2
88
86
70-141
2
cis-1,3-Dichloropropene
ug/L
ND
20
20
18.6
17.8
93
89
70-137
4
Dibromochloromethane
ug/L
ND
20
20
17.0
17.0
85
85
70-134
0
Dibromomethane
ug/L
ND
20
20
17.8
16.9
89
85
70-138
5
Ethylbenzene
ug/L
ND
20
20
17.4
17.2
87
86
66-153
1
lodomethane
ug/L
ND
40
40
34.9
33.3
87
83
20-138
5
m&p-Xylene
ug/L
ND
40
40
34.4
33.4
86
83
69-152
3
Methylene Chloride
ug/L
ND
20
20
17.8
17.3
89
86
42-159
3
o-Xylene
ug/L
ND
20
20
17.3
16.8
87
84
70-148
3
Styrene
ug/L
ND
20
20
17.0
16.7
85
83
70-135
2
Tetrachloroethene
ug/L
ND
20
20
17.9
17.5
90
87
59-143
2
Toluene
ug/L
ND
20
20
18.0
16.7
90
84
59-148
8
trans-1,2-Dichloroethene
ug/L
ND
20
20
18.2
17.8
91
89
70-146
2
trans- 1,3-Dichloropropene
ug/L
ND
20
20
17.9
17.3
90
87
70-135
3
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
16.1
16.1
80
80
47-135
0
Trichloroethene
ug/L
ND
20
20
18.9
17.9
94
89
70-147
6
Trichlorofluoromethane
ug/L
ND
20
20
17.2
16.9
86
85
70-148
2
Vinyl acetate
ug/L
ND
40
40
36.8
36.1
92
90
49-151
2
Vinyl chloride
ug/L
ND
20
20
15.5
15.3
78
76
70-156
2
Xylene (Total)
ug/L
ND
60
60
51.7
50.2
86
84
63-158
3
1,2-Dichloroethane-d4 (S)
%
91
92
70-130
4-Bromofluorobenzene (S)
%
98
99
70-130
Toluene-d8(S)
%
102
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC.
Page 30 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
QC Batch: 567203 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495813001, 92495813002, 92495813004, 92495813005
METHOD BLANK: 3005695
Matrix:
Water
Associated Lab Samples:
92495813001, 92495813002, 92495813004, 92495813005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/18/20 00:20
1,2-Dichloroethane-d4 (S)
%
100
50-150
09/18/20 00:20
Toluene-d8 (S)
%
102
50-150
09/18/20 00:20
LABORATORY CONTROL SAMPLE: 3005696
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.3 96 70-130
1,2-Dichloroethane-d4 (S) % 102 50-150
Toluene-d8(S) % 102 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3005697
3005698
MS
MSD
7342517002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.5
19.2 98
96
50-150 1
1,2-Dichloroethane-d4 (S)
%
96
98
50-150
Toluene-d8(S)
%
102
101
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
QC Batch: 567204 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495813003
METHOD BLANK: 3005714
Matrix:
Water
Associated Lab Samples: 92495813003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/17/20 16:35
1,2-Dichloroethane-d4 (S)
%
94
50-150
09/17/20 16:35
Toluene-d8 (S)
%
124
50-150
09/17/20 16:35
LABORATORY CONTROL SAMPLE: 3005715
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.9 100 70-130
1,2-Dichloroethane-d4 (S) % 95 50-150
Toluene-d8 (S) % 97 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3005716
3005717
MS
MSD
92495813003 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 20.9
21.4 104
107
50-150 2
1,2-Dichloroethane-d4 (S)
%
104
102
50-150
Toluene-d8(S)
%
101
101
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Holbrooks Road Landfill
Pace Project No.: 92495813
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:45 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Road Landfill
92495813
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92495813001
6002-HRW8
EPA 3010A
568568
EPA6010D
568581
92495813002
6002-HRW9
EPA 3010A
568568
EPA6010D
568581
92495813003
6002-HRW16
EPA 3010A
568568
EPA6010D
568581
92495813004
6002-HRW14
EPA 3010A
568568
EPA6010D
568581
92495813005
6002-HRW15
EPA 3010A
568568
EPA6010D
568581
92495813001
6002-HRW8
EPA 3010A
568898
EPA 6020B
568913
92495813002
6002-HRW9
EPA 3010A
568898
EPA 6020B
568913
92495813003
6002-HRW16
EPA 3010A
568898
EPA 6020B
568913
92495813004
6002-HRW14
EPA 3010A
568898
EPA 6020B
568913
92495813005
6002-HRW15
EPA 3010A
568898
EPA 6020B
568913
92495813001
6002-HRW8
EPA 8260D
568862
92495813002
6002-HRW9
EPA 8260D
568867
92495813003
6002-HRW16
EPA 8260D
568862
92495813004
6002-HRW14
EPA 8260D
568865
92495813005
6002-HRW15
EPA 8260D
568867
92495813006
Trip Blank
EPA 8260D
568862
92495813001
6002-HRW8
EPA 8260D Mod.
567203
92495813002
6002-HRW9
EPA 8260D Mod.
567203
92495813003
6002-HRW16
EPA 8260D Mod.
567204
92495813004
6002-HRW14
EPA 8260D Mod.
567203
92495813005
6002-HRW15
EPA 8260D Mod.
567203
Date: 09/29/2020 09:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 34 of 37

Document Name:
Document Revised: February 7, W18
aceAnal�tical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh[] Mechanicsville❑
SampleClient Name: m WO# : 92495813
—Upon Receipt
(_ h Project #;
'�'' �'It
Courier:
emmercial [—]Fed Ex
x ❑UPS ❑
❑ f� Other: 92495813
Packing Material: ❑Bubble wrap []Bubble Bags None ❑ Other
Thermometer; -QIR Gun !D: 92TO61 Type of Ice: I
it ❑aloe
�
Cooler Temp (°C): ' - J Correction Factor: Add/Subtract (°C) 0.0
Cooler Temp Corrected (°C):
Date/InitlaNPerson Examining
Biological Tlssu Frozen?
❑None v
[]Yes ' ❑No 7N/A q I P ) �
Temp should be above freezing to 6°C
❑Samples out of temp criteria. 5amples on ice, cooling process
has begun
USDA Regulated Soil (E N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source )internationally,
I71yes nNo e W . A »a Dig aim n r7V.. r In1.,
Camments/Discrepancy:
Chain of Custody Present?
yes
[]NO
[]N/A
1.
Samples Arrived within Hold Time?
QVes
❑No
❑N/A
2,
Short Hold Time Analysis (<72 hr.)?
❑Yes
No
❑N/A
I
Rush Turn Around Time Requested?
❑Yes
fnNo
[]NIA
4.
Sufficient Volume?
OYes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
_.❑fes
Yes
[]NO
❑No
❑N/A
❑N/A
6.
Containers Intact?
12yes
ONO
❑N/A
7,
Dissolved analysis: Samples Field Filtered?
❑Yes
❑Vo
El N/A
8.
Sample Labels Match CDC?
Yes
[]NO
❑N/A
4.
Includes Date/Time/ID/Analysis Matrix:
J
LZ
Headspace in VOA Vials (>S-6mm)?
Dyes
No
01/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
(—]Yes
❑yes
i❑No —t!JN/A
❑No —TIN/A
11.
COMMENTS/SAMPLEDISCREPANCY p I Field Date Required? []Yes ❑No
A
JOC
Lot iD of spilt containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
project Manager SRF Review:
Date/Time:
Pate:
Date:
Page 35 of 37

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Document Name:
Document Revised: February 7, 2018
a
aCBARaIytlCal
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev,06
Pace Carolinas Quality Office
*Check mark top half of box If pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"*Bottom half of box Is to list number of bottle
Project tf Wp# : 92495813
PM: MWB Due Date: 09/30/20
CLIENT: 92—MECK CO
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
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added
Lot d
Note: Whenever there is a discrepancy affecting North Carolina carnpliance samples, a copy of this Form will be sentto the North Carolina MEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, incorrect containers.
Page 37 of 37

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 29, 2020
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 16, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92495794001 6002-HRSW2
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
PM1
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495794002 6002-HRSW3
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
PM1
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
92495794003 6002-HRSW4
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
PM1
52
PASI-C
EPA 8260D Mod.
CL
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Sample: 6002-HRSW2 Lab ID: 92495794001 Collected: 09/16/20 09:43 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:39
7440-38-2
Barium
56.6
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 20:39
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 20:39
7440-43-9
Chromium
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7440-48-4
Copper
6.0
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7440-50-8
Lead
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7439-92-1
Nickel
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7440-02-0
Selenium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:39
7782-49-2
Silver
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7440-22-4
Thallium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:39
7440-28-0
Vanadium
10.1
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:39
7440-62-2
Zinc
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:39
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/25/20 01:08
09/28/20 00:52
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 01:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 01:30
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 01:30
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 01:30
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 01:30
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 01:30
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 01:30
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 01:30
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 01:30
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 01:30
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/25/20 01:30
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/25/20 01:30
75-00-3
Chloroform
ND
ug/L
5.0
1
09/25/20 01:30
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 01:30
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 01:30
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 01:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 01:30
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 01:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 01:30
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 01:30
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 01:30
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/25/20 01:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/25/20 01:30
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Sample: 6002-HRSW2 Lab ID: 92495794001 Collected: 09/16/20 09:43 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/25/20 01:30
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 01:30
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 01:30
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/25/20 01:30
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 01:30
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 01:30
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/25/20 01:30
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/25/20 01:30
591-78-6
lodomethane
ND
ug/L
20.0
1
09/25/20 01:30
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/25/20 01:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/25/20 01:30
108-10-1
Styrene
ND
ug/L
1.0
1
09/25/20 01:30
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 01:30
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 01:30
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/25/20 01:30
127-18-4
Toluene
ND
ug/L
1.0
1
09/25/20 01:30
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/25/20 01:30
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/25/20 01:30
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/25/20 01:30
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/25/20 01:30
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/25/20 01:30
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/25/20 01:30
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/25/20 01:30
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/25/20 01:30
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/25/20 01:30
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/25/20 01:30
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/25/20 01:30
460-00-4
1,2-Dichloroethane-d4 (S)
109
%
70-130
1
09/25/20 01:30
17060-07-0
Toluene-d8 (S)
94
%
70-130
1
09/25/20 01:30
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/18/20 04:46
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
101
%
50-150
1
09/18/20 04:46
17060-07-0
Toluene-d8 (S)
101
%
50-150
1
09/18/20 04:46
2037-26-5
Date: 09/29/2020 09:44 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Sample: 6002-HRSW3 Lab ID: 92495794002 Collected: 09/16/20 10:32 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:51
7440-38-2
Barium
50.5
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 20:51
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 20:51
7440-43-9
Chromium
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7440-48-4
Copper
5.7
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7440-50-8
Lead
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7439-92-1
Nickel
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7440-02-0
Selenium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:51
7782-49-2
Silver
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7440-22-4
Thallium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:51
7440-28-0
Vanadium
8.9
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:51
7440-62-2
Zinc
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:51
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/25/20 01:08
09/28/20 00:55
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 01:48
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 01:48
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 01:48
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 01:48
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 01:48
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 01:48
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 01:48
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 01:48
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 01:48
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 01:48
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/25/20 01:48
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/25/20 01:48
75-00-3
Chloroform
ND
ug/L
5.0
1
09/25/20 01:48
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 01:48
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 01:48
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 01:48
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 01:48
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 01:48
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 01:48
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 01:48
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 01:48
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/25/20 01:48
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/25/20 01:48
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Sample: 6002-HRSW3 Lab ID: 92495794002 Collected: 09/16/20 10:32 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/25/20 01:48
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 01:48
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 01:48
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/25/20 01:48
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 01:48
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 01:48
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/25/20 01:48
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/25/20 01:48
591-78-6
lodomethane
ND
ug/L
20.0
1
09/25/20 01:48
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/25/20 01:48
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/25/20 01:48
108-10-1
Styrene
ND
ug/L
1.0
1
09/25/20 01:48
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 01:48
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 01:48
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/25/20 01:48
127-18-4
Toluene
ND
ug/L
1.0
1
09/25/20 01:48
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/25/20 01:48
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/25/20 01:48
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/25/20 01:48
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/25/20 01:48
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/25/20 01:48
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/25/20 01:48
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/25/20 01:48
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/25/20 01:48
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/25/20 01:48
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/25/20 01:48
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
09/25/20 01:48
460-00-4
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
09/25/20 01:48
17060-07-0
Toluene-d8 (S)
94
%
70-130
1
09/25/20 01:48
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/18/20 05:05
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
103
%
50-150
1
09/18/20 05:05
17060-07-0
Toluene-d8 (S)
103
%
50-150
1
09/18/20 05:05
2037-26-5
Date: 09/29/2020 09:44 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Sample: 6002-HRSW4 Lab ID: 92495794003 Collected: 09/16/20 10:11 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:54
7440-38-2
Barium
47.7
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 20:54
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/24/20 01:35
09/25/20 20:54
7440-43-9
Chromium
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7440-48-4
Copper
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7440-50-8
Lead
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7439-92-1
Nickel
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7440-02-0
Selenium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:54
7782-49-2
Silver
ND
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7440-22-4
Thallium
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:54
7440-28-0
Vanadium
7.3
ug/L
5.0
1
09/24/20 01:35
09/25/20 20:54
7440-62-2
Zinc
ND
ug/L
10.0
1
09/24/20 01:35
09/25/20 20:54
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
09/25/20 01:08
09/28/20 00:59
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/25/20 02:06
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/25/20 02:06
107-13-1
Benzene
ND
ug/L
1.0
1
09/25/20 02:06
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/25/20 02:06
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/25/20 02:06
75-27-4
Bromoform
ND
ug/L
1.0
1
09/25/20 02:06
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/25/20 02:06
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/25/20 02:06
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/25/20 02:06
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/25/20 02:06
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/25/20 02:06
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/25/20 02:06
75-00-3
Chloroform
ND
ug/L
5.0
1
09/25/20 02:06
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/25/20 02:06
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/25/20 02:06
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/25/20 02:06
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/25/20 02:06
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/25/20 02:06
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 02:06
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/25/20 02:06
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/25/20 02:06
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/25/20 02:06
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/25/20 02:06
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
Sample: 6002-HRSW4 Lab ID: 92495794003 Collected: 09/16/20 10:11 Received: 09/16/20 14:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:06
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:06
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/25/20 02:06
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:06
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:06
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/25/20 02:06
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/25/20 02:06
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/25/20 02:06
591-78-6
lodomethane
ND
ug/L
20.0
1
09/25/20 02:06
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/25/20 02:06
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/25/20 02:06
108-10-1
Styrene
ND
ug/L
1.0
1
09/25/20 02:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 02:06
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/25/20 02:06
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/25/20 02:06
127-18-4
Toluene
ND
ug/L
1.0
1
09/25/20 02:06
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/25/20 02:06
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/25/20 02:06
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/25/20 02:06
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/25/20 02:06
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/25/20 02:06
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/25/20 02:06
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/25/20 02:06
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/25/20 02:06
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/25/20 02:06
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/25/20 02:06
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
09/25/20 02:06
460-00-4
1,2-Dichloroethane-d4 (S)
107
%
70-130
1
09/25/20 02:06
17060-07-0
Toluene-d8 (S)
95
%
70-130
1
09/25/20 02:06
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/18/20 05:24
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
100
%
50-150
1
09/18/20 05:24
17060-07-0
Toluene-d8 (S)
102
%
50-150
1
09/18/20 05:24
2037-26-5
Date: 09/29/2020 09:44 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
QC Batch: 568568 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495794001, 92495794002, 92495794003
METHOD BLANK: 3012589 Matrix: Water
Associated Lab Samples: 92495794001, 92495794002, 92495794003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
09/25/20 20:26
10.0
09/25/20 20:26
5.0
09/25/20 20:26
1.0
09/25/20 20:26
1.0
09/25/20 20:26
5.0
09/25/20 20:26
5.0
09/25/20 20:26
5.0
09/25/20 20:26
5.0
09/25/20 20:26
5.0
09/25/20 20:26
10.0
09/25/20 20:26
5.0
09/25/20 20:26
10.0
09/25/20 20:26
5.0
09/25/20 20:26
10.0
09/25/20 20:26
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3012590
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
472
94
80-120
Arsenic
ug/L
500
465
93
80-120
Barium
ug/L
500
504
101
80-120
Beryllium
ug/L
500
507
101
80-120
Cadmium
ug/L
500
475
95
80-120
Chromium
ug/L
500
489
98
80-120
Cobalt
ug/L
500
474
95
80-120
Copper
ug/L
500
498
100
80-120
Lead
ug/L
500
472
94
80-120
Nickel
ug/L
500
481
96
80-120
Selenium
ug/L
500
465
93
80-120
Silver
ug/L
250
241
96
80-120
Thallium
ug/L
500
471
94
80-120
Vanadium
ug/L
500
483
97
80-120
Zinc
ug/L
500
458
92
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Road Landfill
92495794
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3012591
3012592
MS
MSD
92495794001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
489
494
98
99
75-125
1
Arsenic
ug/L
ND
500
500
499
505
100
101
75-125
1
Barium
ug/L
56.6
500
500
585
585
106
106
75-125
0
Beryllium
ug/L
ND
500
500
532
532
106
106
75-125
0
Cadmium
ug/L
ND
500
500
506
510
101
102
75-125
1
Chromium
ug/L
ND
500
500
512
516
102
103
75-125
1
Cobalt
ug/L
ND
500
500
494
498
99
99
75-125
1
Copper
ug/L
6.0
500
500
525
530
104
105
75-125
1
Lead
ug/L
ND
500
500
496
502
99
100
75-125
1
Nickel
ug/L
ND
500
500
501
504
100
101
75-125
1
Selenium
ug/L
ND
500
500
518
525
103
105
75-125
2
Silver
ug/L
ND
250
250
250
252
100
101
75-125
1
Thallium
ug/L
ND
500
500
491
493
98
99
75-125
0
Vanadium
ug/L
10.1
500
500
517
520
101
102
75-125
0
Zinc
ug/L
ND
500
500
491
496
97
98
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
QC Batch: 568898 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92495794001, 92495794002, 92495794003
METHOD BLANK: 3014112
Matrix:
Water
Associated Lab Samples: 92495794001, 92495794002, 92495794003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.10
09/27/20 20:33
LABORATORY CONTROL SAMPLE:
3014113
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
10.1
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3014114 3014115
MS MSD
92494939003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.2 10.3 102 103 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
QC Batch: 568862 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495794001, 92495794002, 92495794003
METHOD BLANK: 3013939 Matrix:
Associated Lab Samples: 92495794001, 92495794002, 92495794003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1,1-Trichloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1,2-Trichloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1-Dichloroethane
ug/L
ND
1.0
09/24/20 23:24
1,1-Dichloroethene
ug/L
ND
1.0
09/24/20 23:24
1,2,3-Trichloropropane
ug/L
ND
1.0
09/24/20 23:24
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
09/24/20 23:24
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/24/20 23:24
1,2-Dichlorobenzene
ug/L
ND
1.0
09/24/20 23:24
1,2-Dichloroethane
ug/L
ND
1.0
09/24/20 23:24
1,2-Dichloropropane
ug/L
ND
1.0
09/24/20 23:24
1,4-Dichlorobenzene
ug/L
ND
1.0
09/24/20 23:24
2-Butanone (MEK)
ug/L
ND
5.0
09/24/20 23:24
2-Hexanone
ug/L
ND
5.0
09/24/20 23:24
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/24/20 23:24
Acetone
ug/L
ND
25.0
09/24/20 23:24
Acrylonitrile
ug/L
ND
10.0
09/24/20 23:24
Benzene
ug/L
ND
1.0
09/24/20 23:24
Bromochloromethane
ug/L
ND
1.0
09/24/20 23:24
Bromodichloromethane
ug/L
ND
1.0
09/24/20 23:24
Bromoform
ug/L
ND
1.0
09/24/20 23:24
Bromomethane
ug/L
ND
2.0
09/24/20 23:24
Carbon disulfide
ug/L
ND
2.0
09/24/20 23:24
Carbon tetrachloride
ug/L
ND
1.0
09/24/20 23:24
Chlorobenzene
ug/L
ND
1.0
09/24/20 23:24
Chloroethane
ug/L
ND
1.0
09/24/20 23:24
Chloroform
ug/L
ND
5.0
09/24/20 23:24
Chloromethane
ug/L
ND
1.0
09/24/20 23:24
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 23:24
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 23:24
Dibromochloromethane
ug/L
ND
1.0
09/24/20 23:24
Dibromomethane
ug/L
ND
1.0
09/24/20 23:24
Ethylbenzene
ug/L
ND
1.0
09/24/20 23:24
lodomethane
ug/L
ND
20.0
09/24/20 23:24
m&p-Xylene
ug/L
ND
2.0
09/24/20 23:24
Methylene Chloride
ug/L
ND
5.0
09/24/20 23:24
o-Xylene
ug/L
ND
1.0
09/24/20 23:24
Styrene
ug/L
ND
1.0
09/24/20 23:24
Tetrachloroethene
ug/L
ND
1.0
09/24/20 23:24
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
METHOD BLANK: 3013939 Matrix:
Associated Lab Samples: 92495794001, 92495794002, 92495794003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
09/24/20 23:24
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/24/20 23:24
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/24/20 23:24
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/24/20 23:24
Trichloroethene
ug/L
ND
1.0
09/24/20 23:24
Trichlorofluoromethane
ug/L
ND
1.0
09/24/20 23:24
Vinyl acetate
ug/L
ND
2.0
09/24/20 23:24
Vinyl chloride
ug/L
ND
1.0
09/24/20 23:24
Xylene (Total)
ug/L
ND
1.0
09/24/20 23:24
1,2-Dichloroethane-d4 (S)
%
106
70-130
09/24/20 23:24
4-Bromofluorobenzene (S)
%
98
70-130
09/24/20 23:24
Toluene-d8 (S)
%
94
70-130
09/24/20 23:24
LABORATORY CONTROL SAMPLE:
Parameter
3013940
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.1
106
70-130
1,1,1-Trichloroethane
ug/L
50
48.8
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.9
106
70-130
1,1,2-Trichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethane
ug/L
50
49.3
99
70-130
1,1-Dichloroethene
ug/L
50
49.5
99
70-130
1,2,3-Trichloropropane
ug/L
50
54.6
109
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.1
108
70-130
1,2-Dibromoethane (EDB)
ug/L
50
52.5
105
70-130
1,2-Dichlorobenzene
ug/L
50
51.7
103
70-130
1,2-Dichloroethane
ug/L
50
47.3
95
70-130
1,2-Dichloropropane
ug/L
50
48.0
96
70-130
1,4-Dichlorobenzene
ug/L
50
52.4
105
70-130
2-Butanone (MEK)
ug/L
100
101
101
64-135
2-Hexanone
ug/L
100
112
112
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
103
103
70-130
Acetone
ug/L
100
102
102
61-157
Acrylonitrile
ug/L
250
262
105
61-143
Benzene
ug/L
50
49.6
99
70-130
Bromochloromethane
ug/L
50
49.6
99
70-130
Bromodichloromethane
ug/L
50
44.8
90
70-130
Bromoform
ug/L
50
54.6
109
70-130
Bromomethane
ug/L
50
38.4
77
38-130 v3
Carbon disulfide
ug/L
50
52.9
106
68-130
Carbon tetrachloride
ug/L
50
45.4
91
70-130
Chlorobenzene
ug/L
50
51.0
102
70-130
Chloroethane
ug/L
50
41.4
83
37-142
Chloroform
ug/L
50
51.0
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
LABORATORY CONTROL SAMPLE:
Parameter
3013940
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
46.7
93
48-130
49.8
100
70-130
52.2
104
70-130
53.8
108
70-130
49.9
100
70-130
49.4
99
70-130
106
106
40-130
98.6
99
70-130
48.7
97
67-132
50.5
101
70-131
53.5
107
70-130
48.6
97
69-130
48.8
98
70-130
51.4
103
70-130
51.2
102
70-130
64.0
128
35-189
48.2
96
70-130
40.0
80
63-130
111
111
55-143
44.2
88
70-131
149
99
70-130
90
70-130
102
70-130
99
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3013941
MS
92495794003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3013942
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
19.2
20.4
96
102
73-134
6
1,1,1-Trichloroethane
ug/L
ND
20
20
20.2
21.1
101
106
82-143
5
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.3
19.7
97
98
70-136
2
1,1,2-Trichloroethane
ug/L
ND
20
20
18.5
19.4
92
97
70-135
5
1,1-Dichloroethane
ug/L
ND
20
20
19.7
20.1
98
100
70-139
2
1,1-Dichloroethene
ug/L
ND
20
20
21.4
21.3
107
106
70-154
1
1,2,3-Trichloropropane
ug/L
ND
20
20
18.0
18.9
90
94
71-137
5
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
19.1
19.6
96
98
65-134
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
18.9
20.5
95
102
70-137
8
1,2-Dichlorobenzene
ug/L
ND
20
20
19.3
19.4
96
97
70-133
0
1,2-Dichloroethane
ug/L
ND
20
20
19.9
20.2
100
101
70-137
1
1,2-Dichloropropane
ug/L
ND
20
20
19.7
20.4
99
102
70-140
4
1,4-Dichlorobenzene
ug/L
ND
20
20
19.9
20.7
100
104
70-133
4
2-Butanone (MEK)
ug/L
ND
40
40
43.4
46.1
108
115
60-139
6
2-Hexanone
ug/L
ND
40
40
42.4
42.8
106
107
65-138
1
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
39.0
39.2
97
98
65-135
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC.
Page 15 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3013941
MS
92495794003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3013942
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
41.8
39.9
105
100
60-148
5
Acrylonitrile
ug/L
ND
100
100
102
102
102
102
64-147
0
Benzene
ug/L
ND
20
20
20.3
20.6
102
103
70-151
1
Bromochloromethane
ug/L
ND
20
20
19.2
19.0
96
95
70-141
1
Bromodichloromethane
ug/L
ND
20
20
16.6
17.6
83
88
70-138
6
Bromoform
ug/L
ND
20
20
17.9
18.3
89
92
63-130
3
Bromomethane
ug/L
ND
20
20
10.4
11.8
52
59
15-152
13 v3
Carbon disulfide
ug/L
ND
20
20
19.2
18.7
96
93
69-149
3
Carbon tetrachloride
ug/L
ND
20
20
20.3
20.7
101
104
70-143
2
Chlorobenzene
ug/L
ND
20
20
19.7
20.4
99
102
70-138
3
Chloroethane
ug/L
ND
20
20
20.6
20.3
103
101
52-163
1
Chloroform
ug/L
ND
20
20
19.9
19.5
99
98
70-139
2
Chloromethane
ug/L
ND
20
20
17.3
18.1
86
90
41-139
5
cis-1,2-Dichloroethene
ug/L
ND
20
20
19.8
20.4
99
102
70-141
3
cis-1,3-Dichloropropene
ug/L
ND
20
20
19.9
20.4
99
102
70-137
3
Dibromochloromethane
ug/L
ND
20
20
18.8
20.1
94
100
70-134
6
Dibromomethane
ug/L
ND
20
20
18.9
20.3
95
101
70-138
7
Ethylbenzene
ug/L
ND
20
20
19.5
20.1
97
100
66-153
3
lodomethane
ug/L
ND
40
40
29.8
39.2
75
98
20-138
27
m&p-Xylene
ug/L
ND
40
40
38.8
40.2
97
100
69-152
3
Methylene Chloride
ug/L
ND
20
20
21.1
20.8
105
104
42-159
1
o-Xylene
ug/L
ND
20
20
19.4
19.7
97
99
70-148
2
Styrene
ug/L
ND
20
20
19.7
20.5
99
102
70-135
4
Tetrachloroethene
ug/L
ND
20
20
19.7
20.5
98
103
59-143
4
Toluene
ug/L
ND
20
20
19.3
19.3
96
96
59-148
0
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.4
20.8
102
104
70-146
2
trans- 1,3-Dichloropropene
ug/L
ND
20
20
18.8
19.5
94
97
70-135
3
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
17.8
18.7
89
94
47-135
5
Trichloroethene
ug/L
ND
20
20
19.8
20.3
99
102
70-147
3
Trichlorofluoromethane
ug/L
ND
20
20
18.6
18.0
93
90
70-148
4
Vinyl acetate
ug/L
ND
40
40
42.6
44.6
106
111
49-151
5
Vinyl chloride
ug/L
ND
20
20
17.2
17.3
86
87
70-156
1
Xylene (Total)
ug/L
ND
60
60
58.2
59.9
97
100
63-158
3
1,2-Dichloroethane-d4 (S)
%
105
106
70-130
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8(S)
%
98
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
QC Batch: 567203 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92495794001, 92495794002, 92495794003
METHOD BLANK: 3005695
Matrix:
Water
Associated Lab Samples:
92495794001, 92495794002, 92495794003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/18/20 00:20
1,2-Dichloroethane-d4 (S)
%
100
50-150
09/18/20 00:20
Toluene-d8 (S)
%
102
50-150
09/18/20 00:20
LABORATORY CONTROL SAMPLE: 3005696
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.3 96 70-130
1,2-Dichloroethane-d4 (S) % 102 50-150
Toluene-d8(S) % 102 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3005697
3005698
MS
MSD
7342517002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.5
19.2 98
96
50-150 1
1,2-Dichloroethane-d4 (S)
%
96
98
50-150
Toluene-d8(S)
%
102
101
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 22

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Holbrooks Road Landfill
Pace Project No.: 92495794
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/29/2020 09:44 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Road Landfill
92495794
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92495794001
6002-HRSW2
EPA 3010A
568568
EPA 6010D
568581
92495794002
6002-HRSW3
EPA 3010A
568568
EPA 6010D
568581
92495794003
6002-HRSW4
EPA 3010A
568568
EPA 6010D
568581
92495794001
6002-HRSW2
EPA 3010A
568898
EPA 6020B
568913
92495794002
6002-HRSW3
EPA 3010A
568898
EPA 6020B
568913
92495794003
6002-HRSW4
EPA 3010A
568898
EPA 6020B
568913
92495794001
6002-HRSW2
EPA 8260D
568862
92495794002
6002-HRSW3
EPA 8260D
568862
92495794003
6002-HRSW4
EPA 8260D
568862
92495794001
6002-HRSW2
EPA 8260D Mod.
567203
92495794002
6002-HRSW3
EPA 8260D Mod.
567203
92495794003
6002-HRSW4
EPA 8260D Mod.
567203
Date: 09/29/2020 09:44 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 22

Document Name:
Document Revised: February 7, 2018
aceAnalytica!
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvilleo Raleigh❑ Mechanicsville[]
SampleClient Name: J� r IP WO# 92495794
Upon Receipt I IVY � ri1 Project q:
Courier: ❑Fed Ex[]UPS ❑USPS ❑Client 11111111
IN I
III
111111
❑ Commercial Pace ❑Other:
92495794
'netnA. Canl y�.� I —I Rrocanf7 l7Yat A INn Seals Intact? I IYes F-A, A_ rI
Date/Initials Person Examining
Packing Material: []Bubble Wrap ❑Bubble Bags None ❑ Other Biological Tissue Frozen? q
Thermometer: ❑Yes ❑No
92T061 type of Ice. et ❑slue [—]None
�/A
�
JR Gun ID:
W
Cooler Temp (°Cj: ( 1 [ Correction Factor: Add/Subtract CC) 0.0 Temp should be above freezing to 6•C
Cooler Temp Corrected (•tj: r ❑Samples out of temp criteria. Samples on ice, cooling process
7 has tegun
USDA Regulated Soil [V N/A, water sample)
Did samples originate in ✓ quarantine zone within the united States: CA, NY, or SC (check maps}? Did samples originate from a foreign source ilnternationally,
I—IInrludinu Hawall and Pupnn RIrn171 {Yes nNo
L—J �.._
Comments/Disc re panty:
Chain of Custody Present?
wes
No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
❑N/A
2,
Short Hold Time Analysis (02 hr.j?
❑Yes
C7fNo
[]NIA
3.
Rush Turn Around Time Requested?
❑Yes
eNo
❑N/A
4.
Sufficient Volume?
Eyes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
,Y es
/ fifes
[:]No❑N/A
[]NO
[]NIA
6.
Containers Intact?
L2YeS
❑No
[]NIA
7
Dissolved analysis: Samples Field Filtered?
❑Yes
❑s4a
[:]N/A
R.
Sample Labels Match COC?
Yes
-[]No
❑NIA
9.
-includes Date/Time/ID/Analysis Matrix:
Head space in VOA Vials (>5-6mm)?
❑Yes
EfNo
C /A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Des
�No
/dNo
' N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Lot ID of split containers:
Date:
Date:
Field Data Required? ❑Yes [:]No
Page 20 of 22

Document Name:
Document Revised: February 7, 2018
m
�dce Analytrcaf
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev,06
Pace Carolinas Quaiity Office
*Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
*'"Bottom half of box is to list number of bottle
Project # W4# : 92495794
PM: MWB Due Date: 09/30/20
CLIENT: 92-MECK CO
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pH upon receipt
Date preservation adjusted
Time preservation
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Lot 11
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office {Le.
Out of hold. Incorrect preservative, out of temp, incorrect containers.
Page 21 of 22

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Page 22 of 22