20050 Rite Aid_WP-Approval Import Crushed Concrete 20200908

hart
hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via Email
September 2, 2020
NCDEQ — Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646
Attention: Ms. Carolyn Minnich, PG
Re: Soil Management Options
Import of Recycled Crushed Concrete
CAMP North End
Rite Aid & Former Charlotte Army Missile Plant Brownfields Properties
Charlotte, North Carolina
BPN: 20050-16-060 & 11044-07-060
H&H Job No. ATL-003
Dear Carolyn:
1.0 Introduction
On behalf of CAMP Landowner, LP, Hart & Hickman, PC (H&H) would like to request
approval for import and use of recycled crushed concrete as beneficial fill at the CAMP North
End CIP Road Improvement Project (Site). The Site is part of the North Carolina Department of
Environmental Quality (DEQ) Brownfields Program known as the Rite Aid and Former Army
Missile Plant Brownfields Properties.
Recycled crushed concrete is commonly used as a sub -surface structural fill to provide additional
strength to select soils, such as sub -surface soils that may contain elevated moisture levels.
When used, the crushed concrete is generally blended into existing soils until the required
strength characteristics are achieved. For the Site, the crushed concrete is proposed to be used on
an as -needed basis underneath select areas of roadways or around utilities. If used, the crushed
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, INC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Ms. Carolyn Minnich, PG
September 2, 2020
Page 2
concrete will be placed a minimum of 2-ft below grade and covered with existing Site soils,
clean fill, and/or hard surfaces such as asphalt roadways or concrete surfaces.
H&H identified and collected samples of crushed concrete from the following two local facilities
for potential use at the subject Site:
• C&M Recycling (C&M) facility located at 2930 Jeff Adams Drive in Charlotte, NC, and
• DH Griffin Companies (DH Griffin) facility located at 11205 Reames Road, in Charlotte,
NC.
A summary of our crushed concrete sampling activities and results are provided below.
2.0 Sampling Activities
On July 30, 2020, H&H collected a representative sample of crushed concrete from each of the
facilities listed above and submitted them for laboratory analysis for volatile organic compounds
(VOCs) by EPA Method 8260, semi-VOCs (SVOCs) by EPA Method 8270, RCRA Metals by
EPA Methods 6010 & 7471, and hexavalent chromium by EPA Method 7199. The samples
were each collected from a stockpile of crushed concrete at each facility proposed for use as
beneficial fill. Five aliquots were collected from different sections and depths within each
concrete stockpile to provide a representative sample. A grab sample was collected from one
aliquot for VOCs, and the remaining sample was homogenized and composited for SVOCs and
metals. A tabular summary of the crushed concrete results is presented in Table 1. Laboratory
analytical data is attached as Attachment A.
3.0 Sampling Results
Laboratory analytical results from samples collected at the C&M facility indicate VOCs and
SVOCs at concentrations below their respective PSRGs. Arsenic was detected (5.7 mg/kg)
hart hickman
\\hhfs0l\MasterFiles\AAA-Master Projects\ATCO LLC - ATC\ATL-003 CIP\Soil Management\Select Backfill\CAMP NE_BPN SMARTER ENVIRONMENTAL SOLUTIONS
20050-16-060_ 11044-07-060 _Crushed Concrete Import_090220.doc

Ms. Carolyn Minnich, PG
September 2, 2020
Page 3
above its Industrial PSRG (3.0 mg/kg) and selenium was detected (3.5 mg/kg) at a concentration
above its Protection of Groundwater PSRG, but below its Residential PSRG. Hexavalent
chromium (5.9 mg/kg) was detected above its Residential PSRG (0.31 mg/kg), but below its
Industrial PSRG.
Laboratory analytical results from the samples collected at the DH Griffin facility indicate VOCs
and SVOCs at concentrations below PSRGs. However, benzo(a)pyrene, a polycyclic aromatic
hydrocarbon (PAH), was detected as an estimated "J" flag concentration (0.23 J mg/kg) slightly
above its Residential PSRG, and isophorone (0.38 J mg/kg) was detected as an estimated J flag
concentration slight above its Protection of Groundwater PSRG. Arsenic was detected (3.8
mg/kg) slightly above its Industrial PSRG and selenium was detected (3.2 mg/kg) at a
concentration above its Protection of Groundwater PSRG. Hexavalent chromium (3.0 mg/kg)
was detected above its Residential PSRG, (0.31 mg/kg), but at a concentration below its
Industrial PSRG.
H&H compared the detected C&M and DH Griffin facility metals concentrations with site -
specific background concentrations and previous assessment data as summarized in the In -situ
Soil Characterization Report, dated November 6, 2019. The comparison indicated similar
concentrations of arsenic and selenium in the crushed concrete are present in existing Site soils
and the detected concentrations are similar to naturally occurring site -specific background levels.
The low-level benzo(a)pyrene concentrations are similar to detections from previous samples
collected at the Site. The hexavalent chromium concentrations detected in the crushed concrete
proposed for import are slightly higher than the site -specific data, but are below Industrial
PSRGs. Further, based on the proposed use of the crushed concrete as beneficial fill in select
sub -surface areas during construction activities primarily in the roadway areas, the exposure risk
of the hexavalent chromium to workers and Site occupants is considered low.
\\hhfs0l\MasterFiles\AAA-Master Projects\ATCO LLC - ATC\ATL-003 CIP\Soil Management\Select Backfill\CAMP NE_BPN
20050-16-060_ 11044-07-060 _Crushed Concrete Import_090220.doc
Ad
hart hickman
P.
SMARTER ENVIRONMENTAL SOLUTIONS

Ms. Carolyn Minnich, PG
September 2, 2020
Page 4
4.0 Conclusions and Recommendations
As such, H&H is requesting that the DEQ Brownfields Program and the DEQ Solid Waste
Section (SWS) grant approval for both C&M Recycling (located on Jeff Adams Drive) and DH
Griffin (located on Reames Road) as suppliers of recycled crushed concrete to be used as sub-
surface structural fill for select areas at the Site. Provisions for management of soils as indicated
in the DEQ-approved Environmental Management Plan (EMP) will be utilized to import and
manage the crushed concrete from these facilities.
Please let us know if you have any questions or concerns regarding this request.
Very truly yours,
Hart & Hickman, PC
J�
Andrew Besu Trinh, DeSa, PE
Assistant Project Geologist Senior Project Engineer
Table 1 Summary of Crushed Concrete Analytical Data
Attachment A Analytical Laboratory Report
cc: Mr. Matt Ingalls (H&H)
Mr. Scott Carr (Camp North End)
Mr. James Poletti, PE (Blythe Construction)
\\hhfs0l\MasterFiles\AAA-Master Projects\ATCO LLC - ATC\ATL-003 CIP\Soil Management\Select Backfill\CAMP NE_BPN
20050-16-060_ 11044-07-060 _Crushed Concrete Import_090220.doc
Ad
hart hickman
P.
SMARTER ENVIRONMENTAL SOLUTIONS

Table 1 (Page 1 of 1)
Summary of Crushed Concrete Analytical Data
CIP Roadway Improvement Project
CAMP and Rite Aid Brownfields Site
Statesville Ave. and Woodward Ave.
Charlotte, North Carolina
H&H Job No. ATL-003
Sample Material
Select Backfilli2i
Screening Criteria
Site -Specific Background
Metal Concentrations(3)
(mg/kg)
Export Facility
C&M Recycling
DH Griffin
Sample ID
Backfill-CM
Backfill-DH
Health -Based Preliminary Soil Remediation Goals�'I
(mg/kg)
Date
7/30/2020
7/30/2020
Residential
Industrial /
Commercial
Protection of
Groundwater
VOCs by EPA 8260B (mq/kq)
Acetone
0.039
0.012 J
12,000
140,000
25
Naphthalene
<0.00054
0.00097 J
2.1
8.8
0.39
Styrene
0.00068 J
<0.00050
1,200
7,300
1.5
SVOCs by EPA 8270E (mq/kq)
Acenaphthene
<0.014
0.052 J
720
9,000
16
Anthracene
<0.0081
0.12 J
3,600
45,000
1,300
Benzo(a)anthracene
0.044 J
0.30 J
1.1
21
0.35
Benzo(a)pyrene
0.044 J
0.23 J
0.11
2.1
0.12
Benzo(b)fluoranthene
0.069 J
0.32 J
1.1
21
1.2
Benzo(g,h,i)perylene
0.049 J
0.16 J
NE
NE
15,600
Benzo(k)fluoranthene
<0.0077
0.11 J
11
210
12
Benzyl Alcohol
0.20 J
<0.14
1,300
16,000
3.4
Bis(2-Ethylhexyl)phthalate
<0.16
0.46 J
39
160
14
Chrysene
0.054 J
0.29 J
110
2,100
36
Dibenzo(a,h)anthracene
<0.021
0.041 J
0.11
2.1
0.38
Fluoranthene
0.10 J
0.62 J
480
6,000
670
Fluorene
<0.013
0.050 J
480
6,000
110
Indeno(1,2,3-cd)pyrene
0.050 J
0.16 J
1.1
21
3.9
Isophorone
<0.16
0.38 J
570
2,400
0.26
Naphthalene
<0.015
0.040 J
2.1
8.8
0.39
Phenanthrene
0.060 J
0.47 J
NE
NE
134
P rene
0.092 J
0.58 J
360
4,500
440
Metals by EPA 6020B, 7471 B, and
7199 (mq/kg)
Arsenic
5.7
3.8
0.68
3.0
5.8
<2.35 - 5.25
Barium
87 J
78 J
3,100
47,000
580
Cadmium
0.11 J
0.10 J
14
200
3.0
<1.12 - 1.64
Chromium
25
24
NE
NE
NE
23.4 - 70.7
Hexavalent Chromium
5.9
3.0
0.31
6.5
3.8
<2.35 - 2.18J
Trivalent Chromium
19.1
21.0
23,000
350,000
360,000
23.4 - 70.7
Lead
11
12
NE
NE
270
13.3 - 53.4
Mercury
0.025 J
1 0.023 J
1 2.3
9.7
1.0
1 <0.108 - 0.303
Selenium
3.5
1 3.2
1 78
1 1,200
1 2.1
1 <2.41 - 7.77
Silver
0.085 J
1 0.059 J
1 78
1 1,200
1 3.4
Notes:
(1) North Carolina Department of Environmental Quality ((DEQ) Inactive Hazardous Sites Branch (IHSB)
Preliminary Soil Remediation Goals (PSRGs) (July 2020)
(2) Select backfill consists of recycled crushed concrete
(3) Range of site -specific metal background concentrations collected by H&H at the Rite Aid Brownfields site on November 16, 2016
Soil concentration are reported in milligrams per kilogram (mg/kg). Laboratory analytical methods are shown in parentheses.
With the exception of metals, only those compounds detected in at least one sample are shown.
Gray shading indicates an exceedanceif Protection of Groundwater PSRG.
Bold indicates exceedance of Residential PSRG.
Underline indicated exceedance of Industrial PSRG.
VOCs = volatile organic compounds; SVOCs = semi-VOCs; NE = not established; -- = not applicable; NA = not analyzed
CM = C&M Recyling; DH = D. H. Griffin Companies
"J" = compound was detected above the laboratory detection limit but below the laboratory reporting limit
Table 1 (1 of1)
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Attachment A
Analytical Laboratory Report

1 0
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: ATL-003
Lab Submittal Date: 07/30/2020
Work Order: 0070375
Case Narrative
8/28/20 12:21
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this
case narrative.
Narrative Notes:
Method 7199 analysis was subcontracted to Pace/Shealy. Laboratory report is attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a, -.--,I
Angela D. Overcash
Senior Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
M Matrix spike outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
SM Surrogate is outside of the QC limits due to matrix.
SR Surrogate recovery outside of the QC limits.
U Not Detected at the MDL
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

1 Q
Waypoint..
ANALYTICAL
Sample Receipt Summary
08/28/2020
Work Order: 0070375
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
Backfill-CM 0070375-01 Solid
Backfill-DH 0070375-02 Solid
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
07/30/20 11:30 07/30/20 13:07
07/30/20 12:30 07/30/20 13:07
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way poi nt..
ANALYTICAL
Summary of Detections
08/28/2020
Work Order: 0070375
Waypoint ID
Client ID
Parameter
Method
Result
Units
0070375-01
Backfill-CM
Benzo(a)anthracene
8270E
0.044
J
mg/kg dry
0070375-01
Backfill-CM
Benzo(a)pyrene
8270E
0.044
J
mg/kg dry
0070375-01
Backfill-CM
Benzo(b)fluoranthene
8270E
0.069
J
mg/kg dry
0070375-01
Backfill-CM
Benzo(g,h,i)perylene
8270E
0.049
J
mg/kg dry
0070375-01
Backfill-CM
Benzyl alcohol
8270E
0.20
J
mg/kg dry
0070375-01
Backfill-CM
Chrysene
8270E
0.054
J
mg/kg dry
0070375-01
Backfill-CM
Fluoranthene
8270E
0.10
J
mg/kg dry
0070375-01
Backfill-CM
Indeno(1,2,3-cd)pyrene
8270E
0.050
J
mg/kg dry
0070375-01
Backfill-CM
Phenanthrene
8270E
0.060
J
mg/kg dry
0070375-01
Backfill-CM
Pyrene
8270E
0.092
J
mg/kg dry
0070375-01
Backfill-CM
Hexavalent Chromium
7199
5.9
mg/kg dry
0070375-01
Backfill-CM
Mercury
7471E
0.025
J
mg/kg dry
0070375-01
Backfill-CM
Arsenic
6020B
5.7
mg/kg dry
0070375-01
Backfill-CM
Barium
6020E
87
J
mg/kg dry
0070375-01
Backfill-CM
Cadmium
6020E
0.11
J
mg/kg dry
0070375-01
Backfill-CM
Chromium
6020B
25
mg/kg dry
0070375-01
Backfill-CM
Lead
6020E
11
mg/kg dry
0070375-01
Backfill-CM
Selenium
6020B
3.5
mg/kg dry
0070375-01
Backfill-CM
Silver
6020B
0.085
J
mg/kg dry
0070375-01
Backfill-CM
Acetone
8260D
0.039
mg/kg dry
0070375-01
Backfill-CM
Styrene
8260D
0.00068
J
mg/kg dry
0070375-02
Backfill-DH
Acenaphthene
8270E
0.052
J
mg/kg dry
0070375-02
Backfill-DH
Anthracene
8270E
0.12
J
mg/kg dry
0070375-02
Backfill-DH
Benzo(a)anthracene
8270E
0.30
J
mg/kg dry
0070375-02
Backfill-DH
Benzo(a)pyrene
8270E
0.23
J
mg/kg dry
0070375-02
Backfill-DH
Benzo(b)fluoranthene
8270E
0.32
J
mg/kg dry
0070375-02
Backfill-DH
Benzo(g,h,i)perylene
8270E
0.16
J
mg/kg dry
0070375-02
Backfill-DH
Benzo(k)fluoranthene
8270E
0.11
J
mg/kg dry
0070375-02
Backfill-DH
Bis(2-Ethylhexyl)phthalate
8270E
0.46
J
mg/kg dry
0070375-02
Backfill-DH
Chrysene
8270E
0.29
J
mg/kg dry
0070375-02
Backfill-DH
Dibenzo(a,h)anthracene
8270E
0.041
J
mg/kg dry
0070375-02
Backfill-DH
Fluoranthene
8270E
0.62
J
mg/kg dry
0070375-02
Backfill-DH
Fluorene
8270E
0.050
J
mg/kg dry
0070375-02
Backfill-DH
Indeno(1,2,3-cd)pyrene
8270E
0.16
J
mg/kg dry
0070375-02
Backfill-DH
Isophorone
8270E
0.38
J
mg/kg dry
0070375-02
Backfill-DH
Naphthalene
8270E
0.040
J
mg/kg dry
0070375-02
Backfill-DH
Phenanthrene
8270E
0.47
J
mg/kg dry
0070375-02
Backfill-DH
Pyrene
8270E
0.58
J
mg/kg dry
0070375-02
Backfill-DH
Hexavalent Chromium
7199
3.0
mg/kg dry
0070375-02
Backfill-DH
Mercury
7471B
0.023
J
mg/kg dry
0070375-02
Backfill-DH
Arsenic
6020E
3.8
mg/kg dry
0070375-02
Backfill-DH
Barium
6020B
78
J
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

0
Way poi nt .
ANALYTICAL
Summary of Detections
08/28/2020
Work Order: 0070375
Waypoint ID
Client ID
Parameter
Method
Result
Units
0070375-02
Backfill-DH
Cadmium
6020E
0.10 J
mg/kg dry
0070375-02
Backfill-DH
Chromium
6020B
24
mg/kg dry
0070375-02
Backfill-DH
Lead
6020B
12
mg/kg dry
0070375-02
Backfill-DH
Selenium
6020E
3.2
mg/kg dry
0070375-02
Backfill-DH
Silver
6020E
0.059 J
mg/kg dry
0070375-02
Backfill-DH
Acetone
8260D
0.012 J
mg/kg dry
0070375-02
Backfill-DH
Naphthalene
8260D
0.00097 J
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• Laboratory Report
`A Imo\ /N A i N� 08/28/2020
/e1►MIvia lEdIe11
Hart & Hickman (Charlotte) Project: ATL-003 Client Sample ID: Backfill-CM
Attn: Andrew Besu Sample ID: 0070375-01
2923 South Tryon St. Ste 100 Work Order: 0070375
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 07/30/20 11:30
Time Submitted: 07/30/20 13:07
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
89.2
% by
0.100
0.100
1
SM2540 G
8/5/20 10:52
EDV
POH0033
Weight
Semivolatile Organic Compounds
by GC/MS
1,2,4-Trichlorobenzene
0.13 U
mg/kg dry
0.73
0.13
1
8270E
8/5/20 18:09
JMV
POH0039
1,2-Dichlorobenzene
0.12 U
mg/kg dry
0.73
0.12
1
8270E
8/5/20 18:09
JMV
POH0039
1,3-Dichlorobenzene
0.11 U
mg/kg dry
0.73
0.11
1
8270E
8/5/20 18:09
JMV
POH0039
1,4-Dichlorobenzene
0.11 U
mg/kg dry
0.36
0.11
1
8270E
8/5/20 18:09
JMV
POH0039
1-Methyl naphthalene
0.011 U
mg/kg dry
0.73
0.011
1
8270E
8/5/20 18:09
JMV
POH0039
2,4,5-Trichlorophenol
0.15 U
mg/kg dry
0.73
0.15
1
8270E
8/5/20 18:09
JMV
POH0039
2,4,6-Trichlorophenol
0.18 U
mg/kg dry
0.73
0.18
1
8270E
8/5/20 18:09
JMV
POH0039
2,4-Dichlorophenol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:09
JMV
POH0039
2,4-Dimethylphenol
0.15 U
mg/kg dry
0.36
0.15
1
8270E
8/5/20 18:09
JMV
POH0039
2,4-Dinitrophenol
0.43 U
mg/kg dry
1.7
0.43
1
8270E
8/5/20 18:09
JMV
POH0039
2,4-Dinitrotoluene
0.19 U
mg/kg dry
0.73
0.19
1
8270E
8/5/20 18:09
JMV
POH0039
2,6-Dinitrotoluene
0.19 U
mg/kg dry
0.73
0.19
1
8270E
8/5/20 18:09
JMV
POH0039
2-Chloronaphthalene
0.18 U
mg/kg dry
0.73
0.18
1
8270E
8/5/20 18:09
JMV
POH0039
2-Chlorophenol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:09
JMV
POH0039
2-Methyl naphthalene
0.014 U
mg/kg dry
0.73
0.014
1
8270E
8/5/20 18:09
JMV
POH0039
2-Methylphenol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:09
JMV
POH0039
2-Nitrophenol
0.12 U
mg/kg dry
0.73
0.12
1
8270E
8/5/20 18:09
JMV
POH0039
3,3'-Dichlorobenzidine
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:09
JMV
POH0039
3/4-Methyl phenol
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:09
JMV
POH0039
4,6-Dinitro-2-methylphenol
0.40 U
mg/kg dry
1.7
0.40
1
8270E
8/5/20 18:09
JMV
POH0039
4-Bromophenyl phenyl ether
0.17 U
mg/kg dry
0.73
0.17
1
8270E
8/5/20 18:09
JMV
POH0039
4-Chloro-3-methylphenol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:09
JMV
POH0039
4-Chloroaniline
0.088 U
mg/kg dry
0.36
0.088
1
8270E
8/5/20 18:09
JMV
POH0039
4-Chlorophenyl phenyl ether
0.22 U
mg/kg dry
1.1
0.22
1
8270E
8/5/20 18:09
JMV
POH0039
4-Nitrophenol
0.18 U
mg/kg dry
0.73
0.18
1
8270E
8/5/20 18:09
JMV
POH0039
Acenaphthene
0.017 U
mg/kg dry
0.73
0.017
1
8270E
8/5/20 18:09
JMV
POH0039
Acenaphthylene
0.014 U
mg/kg dry
0.73
0.014
1
8270E
8/5/20 18:09
JMV
POH0039
Anthracene
0.0081 U
mg/kg dry
0.73
0.0081
1
8270E
8/5/20 18:09
JMV
POH0039
Azobenzene
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:09
JMV
POH0039
Benzo(a)anthracene
0.044 J
mg/kg dry
0.73
0.0087
1
8270E
8/5/20 18:09
JMV
POH0039
Benzo(a)pyrene
0.044 J
mg/kg dry
0.73
0.0065
1
8270E
8/5/20 18:09
JMV
POH0039
Benzo(b)fluoranthene
0.069 J
mg/kg dry
0.73
0.0067
1
8270E
8/5/20 18:09
JMV
POH0039
Benzo(g,h,i)perylene
0.049 J
mg/kg dry
0.73
0.0072
1
8270E
815120 18:09
JMV
POH0039
Benzo(k)fluoranthene
0.0077 U
mg/kg dry
0.73
0.0077
1
8270E
8/5/20 18:09
JMV
POH0039
Benzoic Acid
0.60 U
mg/kg dry
2.2
0.60
1
8270E
8/5/20 18:09
JMV
POH0039
Benzyl alcohol
0.20 J
mg/kg dry
0.73
0.14
1
8270E
815120 18:09
JMV
POH0039
bis(2-Chloroethoxy)methane
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:09
JMV
POH0039
Bis(2-Chloroethyl)ether
0.12 U
mg/kg dry
0.73
0.12
1
8270E
8/5/20 18:09
JMV
POH0039
Bis(2-chloroisopropyl)ether
0.13 U
mg/kg dry
0.36
0.13
1
8270E
8/5/20 18:09
JMV
POH0039
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• Laboratory Report
08/28/2020
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003 Client Sample ID: Backfill-CM
Attn: Andrew Besu Sample ID: 0070375-01
2923 South Tryon St. Ste 100 Work Order: 0070375
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 07/30/20 11:30
Time Submitted: 07/30/20 13:07
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:09
JMV
POH0039
Butyl benzyl phthalate
0.13 U
mg/kg dry
0.36
0.13
1
8270E
8/5/20 18:09
JMV
POH0039
Chrysene
0.054 J
mg/kg dry
0.73
0.0086
1
8270E
8/5/20 18:09
JMV
POH0039
Dibenzo(a,h)anthracene
0.021 U
mg/kg dry
0.73
0.021
1
8270E
8/5/20 18:09
JMV
POH0039
Dibenzofuran
0.20 U
mg/kg dry
0.73
0.20
1
8270E
8/5/20 18:09
JMV
POH0039
Diethyl phthalate
0.19 U
mg/kg dry
0.73
0.19
1
8270E
8/5/20 18:09
JMV
POH0039
Dimethyl phthalate
0.17 U
mg/kg dry
0.73
0.17
1
8270E
8/5/20 18:09
JMV
POH0039
Di-n-butyl phthalate
0.18 U
mg/kg dry
0.73
0.18
1
8270E
8/5/20 18:09
JMV
POH0039
Di-n-octyl phthalate
0.19 U
mg/kg dry
0.36
0.19
1
8270E
8/5/20 18:09
JMV
POH0039
Fluoranthene
0.10 J
mg/kg dry
0.73
0.0083
1
8270E
8/5/20 18:09
JMV
POH0039
Fluorene
0.013 U
mg/kg dry
0.73
0.013
1
8270E
8/5/20 18:09
JMV
POH0039
Hexachlorobenzene
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:09
JMV
POH0039
Hexachlorobutadiene
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:09
JMV
POH0039
Hexachlorocyclopentadiene
0.25 U
mg/kg dry
0.73
0.25
1
8270E
8/5/20 18:09
JMV
POH0039
Hexachloroethane
0.11 U
mg/kg dry
0.73
0.11
1
8270E
8/5/20 18:09
JMV
POH0039
Indeno(1,2,3-cd)pyrene
0.050 J
mg/kg dry
0.73
0.021
1
8270E
8/5/20 18:09
JMV
POH0039
Isophorone
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:09
JMV
POH0039
Naphthalene
0.015 U
mg/kg dry
0.73
0.015
1
8270E
8/5/20 18:09
JMV
POH0039
Nitrobenzene
0.15 U
mg/kg dry
0.36
0.15
1
8270E
8/5/20 18:09
JMV
POH0039
N-Nitroso-di-n-propylamine
0.17 U
mg/kg dry
0.73
0.17
1
8270E
8/5/20 18:09
JMV
POH0039
N-Nitrosodiphenylamine
0.20 U
mg/kg dry
0.73
0.20
1
8270E
8/5/20 18:09
JMV
POH0039
Pentachlorophenol
0.46 U
mg/kg dry
1.1
0.46
1
8270E
8/5/20 18:09
JMV
POH0039
Phenanthrene
0.060 J
mg/kg dry
0.73
0.0079
1
8270E
8/5/20 18:09
JMV
POH0039
Phenol
0.12 U
mg/kg dry
0.73
0.12
1
8270E
8/5/20 18:09
JMV
POH0039
Pyrene
0.092 J
mg/kg dry
0.73
0.011
1
8270E
8/5/20 18:09
JMV
POH0039
Pyridine
0.070 U
mg/kg dry
0.36
0.070
1
8270E
8/5/20 18:09
JMV
POH0039
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
19 %
39-132
SM
2-Fluorobiphenyl
69 %
44-115
2-Fluorophenol
9 %
35-115
SM
Nitrobenzene-d5
40 %
37-122
Phenol-d5
43 %
34-121
Terphenyl-d14
77 %
54-127
Subcontracted Analyses
Hexavalent Chromium
Total Metals
5.9
mg/kg dry
1.1
0.22
0.894
7199
8125/20 18:08
SCD
POH0417
Mercury
0.025 J
mg/kg dry
0.056
0.017
1
7471B
8/4/20 13:25
EDV
POH0026
Arsenic
5.7
mg/kg dry
1.1
0.094
10
6020B
8/3/20 18:31
JAB
POH0004
Barium
87 J
mg/kg dry
110
4.0
10
6020B
813120 18:31
JAB
POH0004
Cadmium
0.11 J
mg/kg dry
0.56
0.041
10
6020B
8/3/20 18:31
JAB
POH0004
Chromium
25
mg/kg dry
11
2.7
10
6020B
8/3/20 18:31
JAB
POH0004
Lead
11
mg/kg dry
1.1
0.085
10
6020B
8/3/20 18:31
JAB
POH0004
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• Laboratory Report
08/28/2020
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003 Client Sample ID: Backfill-CM
Attn: Andrew Besu Sample ID: 0070375-01
2923 South Tryon St. Ste 100 Work Order: 0070375
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 07/30/20 11:30
Time Submitted: 07/30/20 13:07
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Selenium
3.5
mg/kg dry
1.1
0.26
10
6020B
813120 18:31
JAB
POH0004
Silver
0.085 J
mg/kg dry
0.56
0.057
10
6020B
8/3/20 18:31
JAB
POH0004
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
0.00065 U
mg/kg dry
0.0053
0.00065
1
8260D
7/31/20 12:13
TBL
POG0472
1,1,1-Trichloroethane
0.00078 U
mg/kg dry
0.0053
0.00078
1
8260D
7/31/20 12:13
TBL
POG0472
1,1,2,2-Tetrachloroethane
0.00039 U
mg/kg dry
0.0053
0.00039
1
8260D
7/31/20 12:13
TBL
POG0472
1,1,2-Trichloroethane
0.00057 U
mg/kg dry
0.0053
0.00057
1
8260D
7/31/20 12:13
TBL
POG0472
1,1-Dichloroethane
0.00096 U
mg/kg dry
0.0053
0.00096
1
8260D
7/31/20 12:13
TBL
POG0472
1,1-Dichloroethylene
0.00097 U
mg/kg dry
0.0053
0.00097
1
8260D
7/31/20 12:13
TBL
POG0472
1,1-Dichloropropylene
0.00082 U
mg/kg dry
0.0053
0.00082
1
8260D
7/31/20 12:13
TBL
POG0472
1,2,3-Trichlorobenzene
0.00076 U
mg/kg dry
0.011
0.00076
1
8260D
7/31/20 12:13
TBL
POG0472
1,2,3-Trichloropropane
0.00060 U
mg/kg dry
0.0053
0.00060
1
8260D
7/31/20 12:13
TBL
POG0472
1,2,4-Trichlorobenzene
0.00051 U
mg/kg dry
0.011
0.00051
1
8260D
7/31/20 12:13
TBL
POG0472
1,2,4-Trimethyl benzene
0.00056 U
mg/kg dry
0.0053
0.00056
1
8260D
7/31/20 12:13
TBL
POG0472
1,2-Dibromoethane
0.00048 U
mg/kg dry
0.0053
0.00048
1
8260D
7/31/20 12:13
TBL
POG0472
1,2-Dichlorobenzene
0.00059 U
mg/kg dry
0.0053
0.00059
1
8260D
7/31/20 12:13
TBL
POG0472
1,2-Dichloroethane
0.00063 U
mg/kg dry
0.0053
0.00063
1
8260D
7/31/20 12:13
TBL
POG0472
1,2-Dichloropropane
0.00080 U
mg/kg dry
0.0053
0.00080
1
8260D
7/31/20 12:13
TBL
POG0472
1,3,5-Trimethyl benzene
0.00067 U
mg/kg dry
0.0053
0.00067
1
8260D
7/31/20 12:13
TBL
POG0472
1,3-Dichlorobenzene
0.00066 U
mg/kg dry
0.0053
0.00066
1
8260D
7/31/20 12:13
TBL
POG0472
1,3-Dichloropropane
0.00044 U
mg/kg dry
0.0053
0.00044
1
8260D
7/31/20 12:13
TBL
POG0472
1,4-Dichlorobenzene
0.00067 U
mg/kg dry
0.0053
0.00067
1
8260D
7/31/20 12:13
TBL
POG0472
2,2-Dichloropropane
0.00066 U
mg/kg dry
0.0053
0.00066
1
8260D
7/31/20 12:13
TBL
POG0472
2-Chlorotoluene
0.00071 U
mg/kg dry
0.0053
0.00071
1
8260D
7/31/20 12:13
TBL
POG0472
4-Chlorotoluene
0.00060 U
mg/kg dry
0.0053
0.00060
1
8260D
7/31/20 12:13
TBL
POG0472
4-Isopropyltoluene
0.0013 U
mg/kg dry
0.0053
0.0013
1
8260D
7/31/20 12:13
TBL
POG0472
Acetone
0.039
mg/kg dry
0.021
0.0014
1
8260D
7/31/20 12:13
TBL
POG0472
Benzene
0.00083 U
mg/kg dry
0.0053
0.00083
1
8260D
7/31/20 12:13
TBL
POG0472
Bromobenzene
0.00074 U
mg/kg dry
0.0053
0.00074
1
8260D
7/31/20 12:13
TBL
POG0472
Bromochloromethane
0.00087 U
mg/kg dry
0.0053
0.00087
1
8260D
7/31/20 12:13
TBL
POG0472
Bromodichloromethane
0.00050 U
mg/kg dry
0.0053
0.00050
1
8260D
7/31/20 12:13
TBL
POG0472
Bromoform
0.00041 U
mg/kg dry
0.0053
0.00041
1
8260D
7/31/20 12:13
TBL
POG0472
Bromomethane
0.0026 U
mg/kg dry
0.011
0.0026
1
8260D
7/31/20 12:13
TBL
POG0472
Carbon Tetrachloride
0.0010 U
mg/kg dry
0.0053
0.0010
1
8260D
7/31/20 12:13
TBL
POG0472
Chlorobenzene
0.00083 U
mg/kg dry
0.0053
0.00083
1
8260D
7/31/20 12:13
TBL
POG0472
Chloroethane
0.0010 U
mg/kg dry
0.011
0.0010
1
8260D
7/31/20 12:13
TBL
POG0472
Chloroform
0.00065 U
mg/kg dry
0.0053
0.00065
1
8260D
7/31/20 12:13
TBL
POG0472
Chloromethane
0.0016 U
mg/kg dry
0.011
0.0016
1
8260D
7/31/20 12:13
TBL
POG0472
cis-1,2-Dichloroethylene
0.00083 U
mg/kg dry
0.0053
0.00083
1
8260D
7/31/20 12:13
TBL
POG0472
cis-1,3-Dichloropropylene
0.00052 U
mg/kg dry
0.0053
0.00052
1
8260D
7/31/20 12:13
TBL
POG0472
Dibromochloromethane
0.00036 U
mg/kg dry
0.0053
0.00036
1
8260D
7/31/20 12:13
TBL
POG0472
Dichlorodifluoromethane
0.0015 U
mg/kg dry
0.011
0.0015
1
8260D
7/31/20 12:13
TBL
POG0472
Ethylbenzene
0.00080 U
mg/kg dry
0.0053
0.00080
1
8260D
7/31/20 12:13
TBL
POG0472
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• Laboratory Report
08/28/2020
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003 Client Sample ID: Backfill-CM
Attn: Andrew Besu Sample ID: 0070375-01
2923 South Tryon St. Ste 100 Work Order: 0070375
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 07/30/20 11:30
Time Submitted: 07/30/20 13:07
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Isopropyl Ether
0.00078 U
mg/kg dry
0.0053
0.00078
1
8260D
7/31/20 12:13
TBL
POG0472
Isopropylbenzene (Cumene)
0.00062 U
mg/kg dry
0.0053
0.00062
1
8260D
7/31/20 12:13
TBL
POG0472
m,p-Xylenes
0.0014 U
mg/kg dry
0.011
0.0014
1
8260D
7/31/20 12:13
TBL
P0O0472
Methyl Butyl Ketone (2-Hexanone)
0.00037 U
mg/kg dry
0.021
0.00037
1
8260D
7/31/20 12:13
TBL
P0O0472
Methyl Ethyl Ketone (2-Butanone)
0.0012 U
mg/kg dry
0.021
0.0012
1
8260D
7/31/20 12:13
TBL
P0O0472
Methyl Isobutyl Ketone
0.00043 U
mg/kg dry
0.021
0.00043
1
8260D
7/31/20 12:13
TBL
P0O0472
Methylene Chloride
0.00086 U
mg/kg dry
0.0053
0.00086
1
8260D
7/31/20 12:13
TBL
P0O0472
Methyl-tert-Butyl Ether
0.00074 U
mg/kg dry
0.0053
0.00074
1
8260D
7/31/20 12:13
TBL
P0O0472
Naphthalene
0.00054 U
mg/kg dry
0.011
0.00054
1
8260D
7/31/20 12:13
TBL
P0O0472
n-Butylbenzene
0.00050 U
mg/kg dry
0.0053
0.00050
1
8260D
7/31/20 12:13
TBL
P0O0472
n-Propylbenzene
0.00077 U
mg/kg dry
0.0053
0.00077
1
8260D
7/31/20 12:13
TBL
P0O0472
o-Xylene
0.00056 U
mg/kg dry
0.0053
0.00056
1
8260D
7/31/20 12:13
TBL
POG0472
sec-Butylbenzene
0.00057 U
mg/kg dry
0.0053
0.00057
1
8260D
7/31/20 12:13
TBL
POG0472
Styrene
0.00068 J
mg/kg dry
0.0053
0.00051
1
8260D
7/31/20 12:13
TBL
POG0472
tert-Butylbenzene
0.00063 U
mg/kg dry
0.0053
0.00063
1
8260D
7/31/20 12:13
TBL
P0O0472
Tetrachloroethylene
0.00096 U
mg/kg dry
0.0053
0.00096
1
8260D
7/31/20 12:13
TBL
POG0472
Toluene
0.00085 U
mg/kg dry
0.0053
0.00085
1
8260D
7/31/20 12:13
TBL
POG0472
trans-1,2-Dichloroethylene
0.0010 U
mg/kg dry
0.0053
0.0010
1
8260D
7/31/20 12:13
TBL
POG0472
trans-1,3-Dichloropropylene
0.00045 U
mg/kg dry
0.0053
0.00045
1
8260D
7/31/20 12:13
TBL
P0O0472
Trichloroethylene
0.0010 U
mg/kg dry
0.0053
0.0010
1
8260D
7/31/20 12:13
TBL
P0O0472
Trichlorofluoromethane
0.0014 U
mg/kg dry
0.011
0.0014
1
8260D
7/31/20 12:13
TBL
P0O0472
Vinyl acetate
0.00058 U
mg/kg dry
0.011
0.00058
1
8260D
7/31/20 12:13
TBL
P0O0472
Vinyl chloride
0.0011 U
mg/kg dry
0.011
0.0011
1
8260D
7/31/20 12:13
TBL
P0O0472
Xylenes, total
0.0019 U
mg/kg dry
0.016
0.0019
1
8260D
7/31/20 12:13
TBL
P0O0472
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
105 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
102 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

0
Way poi nt.
ANALYTICAL
Hart & Hickman (Charlotte)
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: ATL-003
Sample Matrix: Solid
Laboratory Report
08/28/2020
Client Sample ID: Backfill-DH
Sample ID: 0070375-02
Work Order: 0070375
Time Collected: 07/30/20 12:30
Time Submitted: 07/30/20 13:07
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
88.5
% by
0.100
0.100
1
SM2540 G
8/5/20 10:52
EDV
POH0033
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
0.13 U
mg/kg dry
0.73
0.13
1
8270E
8/5/20 18:32
JMV
POH0039
1,2-Dichlorobenzene
0.12 U
mg/kg dry
0.73
0.12
1
8270E
8/5/20 18:32
JMV
POH0039
1,3-Dichlorobenzene
0.11 U
mg/kg dry
0.73
0.11
1
8270E
8/5/20 18:32
JMV
POH0039
1,4-Dichlorobenzene
0.11 U
mg/kg dry
0.36
0.11
1
8270E
8/5/20 18:32
JMV
POH0039
1-Methyl naphthalene
0.011 U
mg/kg dry
0.73
0.011
1
8270E
8/5/20 18:32
JMV
POH0039
2,4,5-Trichlorophenol
0.15 U
mg/kg dry
0.73
0.15
1
8270E
8/5/20 18:32
JMV
POH0039
2,4,6-Trichlorophenol
0.18 U
mg/kg dry
0.73
0.18
1
8270E
8/5/20 18:32
JMV
POH0039
2,4-Dichlorophenol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:32
JMV
POH0039
2,4-Dimethylphenol
0.15 U
mg/kg dry
0.36
0.15
1
8270E
8/5/20 18:32
JMV
POH0039
2,4-Dinitrophenol
0.43 U
mg/kg dry
1.7
0.43
1
8270E
8/5/20 18:32
JMV
POH0039
2,4-Dinitrotoluene
0.19 U
mg/kg dry
0.73
0.19
1
8270E
8/5/20 18:32
JMV
POH0039
2,6-Dinitrotoluene
0.19 U
mg/kg dry
0.73
0.19
1
8270E
8/5/20 18:32
JMV
POH0039
2-Chloronaphthalene
0.18 U
mg/kg dry
0.73
0.18
1
8270E
8/5/20 18:32
JMV
POH0039
2-Chlorophenol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:32
JMV
POH0039
2-Methyl naphthalene
0.014 U
mg/kg dry
0.73
0.014
1
8270E
8/5/20 18:32
JMV
POH0039
2-Methylphenol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:32
JMV
POH0039
2-Nitrophenol
0.12 U
mg/kg dry
0.73
0.12
1
8270E
8/5/20 18:32
JMV
POH0039
3,3'-Dichlorobenzidine
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:32
JMV
POH0039
3/4-Methyl phenol
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:32
JMV
POH0039
4,6-Dinitro-2-methylphenol
0.40 U
mg/kg dry
1.7
0.40
1
8270E
8/5/20 18:32
JMV
POH0039
4-Bromophenyl phenyl ether
0.17 U
mg/kg dry
0.73
0.17
1
8270E
8/5/20 18:32
JMV
POH0039
4-Chloro-3-methylphenol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:32
JMV
POH0039
4-Chloroaniline
0.088 U
mg/kg dry
0.36
0.088
1
8270E
8/5/20 18:32
JMV
POH0039
4-Chlorophenyl phenyl ether
0.22 U
mg/kg dry
1.1
0.22
1
8270E
8/5/20 18:32
JMV
POH0039
4-Nitrophenol
0.18 U
mg/kg dry
0.73
0.18
1
8270E
8/5/20 18:32
JMV
POH0039
Acenaphthene
0.052 J
mg/kg dry
0.73
0.017
1
8270E
8/5/20 18:32
JMV
POH0039
Acenaphthylene
0.014 U
mg/kg dry
0.73
0.014
1
8270E
8/5/20 18:32
JMV
POH0039
Anthracene
0.12 J
mg/kg dry
0.73
0.0080
1
8270E
8/5/20 18:32
JMV
POH0039
Azobenzene
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:32
JMV
POH0039
Benzo(a)anthracene
0.30 J
mg/kg dry
0.73
0.0087
1
8270E
8/5/20 18:32
JMV
POH0039
Benzo(a)pyrene
0.23 J
mg/kg dry
0.73
0.0065
1
8270E
8/5/20 18:32
JMV
POH0039
Benzo(b)fluoranthene
0.32 J
mg/kg dry
0.73
0.0067
1
8270E
8/5/20 18:32
JMV
POH0039
Benzo(g,hJ)perylene
0.16 J
mg/kg dry
0.73
0.0072
1
8270E
8/5/20 18:32
JMV
POH0039
Benzo(k)fluoranthene
0.11 J
mg/kg dry
0.73
0.0077
1
8270E
8/5/20 18:32
JMV
POH0039
Benzoic Acid
0.60 U
mg/kg dry
2.2
0.60
1
8270E
8/5/20 18:32
JMV
POH0039
Benzyl alcohol
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:32
JMV
POH0039
bis(2-Chloroethoxy)methane
0.14 U
mg/kg dry
0.73
0.14
1
8270E
8/5/20 18:32
JMV
POH0039
Bis(2-Chloroethyl)ether
0.12 U
mg/kg dry
0.73
0.12
1
8270E
8/5/20 18:32
JMV
POH0039
Bis(2-chloroisopropyl)ether
0.13 U
mg/kg dry
0.36
0.13
1
8270E
8/5/20 18:32
JMV
POH0039
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• Laboratory Report
08/28/2020
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003 Client Sample ID: Backfill-DH
Attn: Andrew Besu Sample ID: 0070375-02
2923 South Tryon St. Ste 100 Work Order: 0070375
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 07/30/20 12:30
Time Submitted: 07/30/20 13:07
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthalate
0.46 J
mg/kg dry
0.73
0.16
1
8270E
815120 18:32
JMV
POH0039
Butyl benzyl phthalate
0.13 U
mg/kg dry
0.36
0.13
1
8270E
8/5/20 18:32
JMV
POH0039
Chrysene
0.29 J
mg/kg dry
0.73
0.0086
1
8270E
8/5/20 18:32
JMV
POH0039
Dibenzo(a,h)anthracene
0.041 J
mg/kg dry
0.73
0.021
1
8270E
8/5/20 18:32
JMV
POH0039
Dibenzofuran
0.20 U
mg/kg dry
0.73
0.20
1
8270E
8/5/20 18:32
JMV
POH0039
Diethyl phthalate
0.19 U
mg/kg dry
0.73
0.19
1
8270E
8/5/20 18:32
JMV
POH0039
Dimethyl phthalate
0.17 U
mg/kg dry
0.73
0.17
1
8270E
8/5/20 18:32
JMV
POH0039
Di-n-butyl phthalate
0.18 U
mg/kg dry
0.73
0.18
1
8270E
8/5/20 18:32
JMV
POH0039
Di-n-octyl phthalate
0.19 U
mg/kg dry
0.36
0.19
1
8270E
8/5/20 18:32
JMV
POH0039
Fluoranthene
0.62 J
mg/kg dry
0.73
0.0083
1
8270E
8/5/20 18:32
JMV
POH0039
Fluorene
0.050 J
mg/kg dry
0.73
0.013
1
8270E
8/5/20 18:32
JMV
POH0039
Hexachlorobenzene
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:32
JMV
POH0039
Hexachlorobutadiene
0.16 U
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:32
JMV
POH0039
Hexachlorocyclopentadiene
0.25 U
mg/kg dry
0.73
0.25
1
8270E
8/5/20 18:32
JMV
POH0039
Hexachloroethane
0.11 U
mg/kg dry
0.73
0.11
1
8270E
8/5/20 18:32
JMV
POH0039
Indeno(1,2,3-cd)pyrene
0.16 J
mg/kg dry
0.73
0.020
1
8270E
8/5/20 18:32
JMV
POH0039
Isophorone
0.38 J
mg/kg dry
0.73
0.16
1
8270E
8/5/20 18:32
JMV
POH0039
Naphthalene
0.040 J
mg/kg dry
0.73
0.015
1
8270E
8/5120 18:32
JMV
POH0039
Nitrobenzene
0.15 U
mg/kg dry
0.36
0.15
1
8270E
8/5/20 18:32
JMV
POH0039
N-Nitroso-di-n-propylamine
0.17 U
mg/kg dry
0.73
0.17
1
8270E
8/5/20 18:32
JMV
POH0039
N-Nitrosodiphenylamine
0.20 U
mg/kg dry
0.73
0.20
1
8270E
8/5/20 18:32
JMV
POH0039
Pentachlorophenol
0.46 U
mg/kg dry
1.1
0.46
1
8270E
8/5/20 18:32
JMV
POH0039
Phenanthrene
0.47 J
mg/kg dry
0.73
0.0079
1
8270E
8/5/20 18:32
JMV
POH0039
Phenol
0.12 U
mg/kg dry
0.73
0.12
1
8270E
8/5/20 18:32
JMV
POH0039
Pyrene
0.58 J
mg/kg dry
0.73
0.011
1
8270E
815120 18:32
JMV
POH0039
Pyridine
0.069 U
mg/kg dry
0.36
0.069
1
8270E
8/5/20 18:32
JMV
POH0039
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
32 %
39-132
SM
2-Fluorobiphenyl
65 %
44-115
2-Fluorophenol
13 %
35-115
SM
Nitrobenzene-d5
5 %
37-122
SM
Phenol-d5
40 %
34-121
Terphenyl-d14
75 %
54-127
Subcontracted Analyses
Hexavalent Chromium
3.0
mg/kg dry
1.1
0.23
0.882
7199
8/25/20 18:21
SCD
POH0417
Total Metals
Mercury
0.023 J
mg/kg dry
0.056
0.017
1
7471B
8/4/20 13:39
EDV
POH0026
Arsenic
3.8
mg/kg dry
1.1
0.095
10
6020B
8/3/20 18:51
JAB
POH0004
Barium
78 J
mg/kg dry
110
4.1
10
6020B
8/3/20 18:51
JAB
POH0004
Cadmium
0.10 J
mg/kg dry
0.56
0.042
10
6020B
8/3120 18:51
JAB
POH0004
Chromium
24
mg/kg dry
11
2.7
10
6020B
8/3/20 18:51
JAB
POH0004
Lead
12
mg/kg dry
1.1
0.086
10
6020B
8/3/20 18:51
JAB
POH0004
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• Laboratory Report
08/28/2020
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003 Client Sample ID: Backfill-DH
Attn: Andrew Besu Sample ID: 0070375-02
2923 South Tryon St. Ste 100 Work Order: 0070375
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 07/30/20 12:30
Time Submitted: 07/30/20 13:07
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Selenium
3.2
mg/kg dry
1.1
0.26
10
6020B
813120 18:51
JAB
POH0004
Silver
0.059 J
mg/kg dry
0.56
0.058
10
6020B
8/3/20 18:51
JAB
POH0004
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
0.00063 U
mg/kg dry
0.0051
0.00063
1
8260D
7/31/20 12:43
TBL
POG0472
1,1,1-Trichloroethane
0.00075 U
mg/kg dry
0.0051
0.00075
1
8260D
7/31/20 12:43
TBL
POG0472
1,1,2,2-Tetrachloroethane
0.00037 U
mg/kg dry
0.0051
0.00037
1
8260D
7/31/20 12:43
TBL
POG0472
1,1,2-Trichloroethane
0.00055 U
mg/kg dry
0.0051
0.00055
1
8260D
7/31/20 12:43
TBL
POG0472
1,1-Dichloroethane
0.00093 U
mg/kg dry
0.0051
0.00093
1
8260D
7/31/20 12:43
TBL
POG0472
1,1-Dichloroethylene
0.00094 U
mg/kg dry
0.0051
0.00094
1
8260D
7/31/20 12:43
TBL
POG0472
1,1-Dichloropropylene
0.00079 U
mg/kg dry
0.0051
0.00079
1
8260D
7/31/20 12:43
TBL
POG0472
1,2,3-Trichlorobenzene
0.00074 U
mg/kg dry
0.010
0.00074
1
8260D
7/31/20 12:43
TBL
POG0472
1,2,3-Trichloropropane
0.00058 U
mg/kg dry
0.0051
0.00058
1
8260D
7/31/20 12:43
TBL
POG0472
1,2,4-Trichlorobenzene
0.00049 U
mg/kg dry
0.010
0.00049
1
8260D
7/31/20 12:43
TBL
POG0472
1,2,4-Trimethyl benzene
0.00054 U
mg/kg dry
0.0051
0.00054
1
8260D
7/31/20 12:43
TBL
POG0472
1,2-Dibromoethane
0.00046 U
mg/kg dry
0.0051
0.00046
1
8260D
7/31/20 12:43
TBL
POG0472
1,2-Dichlorobenzene
0.00057 U
mg/kg dry
0.0051
0.00057
1
8260D
7/31/20 12:43
TBL
POG0472
1,2-Dichloroethane
0.00061 U
mg/kg dry
0.0051
0.00061
1
8260D
7/31/20 12:43
TBL
POG0472
1,2-Dichloropropane
0.00077 U
mg/kg dry
0.0051
0.00077
1
8260D
7/31/20 12:43
TBL
POG0472
1,3,5-Trimethyl benzene
0.00065 U
mg/kg dry
0.0051
0.00065
1
8260D
7/31/20 12:43
TBL
POG0472
1,3-Dichlorobenzene
0.00064 U
mg/kg dry
0.0051
0.00064
1
8260D
7/31/20 12:43
TBL
POG0472
1,3-Dichloropropane
0.00043 U
mg/kg dry
0.0051
0.00043
1
8260D
7/31/20 12:43
TBL
POG0472
1,4-Dichlorobenzene
0.00065 U
mg/kg dry
0.0051
0.00065
1
8260D
7/31/20 12:43
TBL
POG0472
2,2-Dichloropropane
0.00064 U
mg/kg dry
0.0051
0.00064
1
8260D
7/31/20 12:43
TBL
POG0472
2-Chlorotoluene
0.00069 U
mg/kg dry
0.0051
0.00069
1
8260D
7/31/20 12:43
TBL
POG0472
4-Chlorotoluene
0.00058 U
mg/kg dry
0.0051
0.00058
1
8260D
7/31/20 12:43
TBL
POG0472
4-Isopropyltoluene
0.0013 U
mg/kg dry
0.0051
0.0013
1
8260D
7/31/20 12:43
TBL
POG0472
Acetone
0.012 J
mg/kg dry
0.021
0.0013
1
8260D
7/31/20 12:43
TBL
POG0472
Benzene
0.00080 U
mg/kg dry
0.0051
0.00080
1
8260D
7/31/20 12:43
TBL
POG0472
Bromobenzene
0.00071 U
mg/kg dry
0.0051
0.00071
1
8260D
7/31/20 12:43
TBL
POG0472
Bromochloromethane
0.00084 U
mg/kg dry
0.0051
0.00084
1
8260D
7/31/20 12:43
TBL
POG0472
Bromodichloromethane
0.00049 U
mg/kg dry
0.0051
0.00049
1
8260D
7/31/20 12:43
TBL
POG0472
Bromoform
0.00040 U
mg/kg dry
0.0051
0.00040
1
8260D
7/31/20 12:43
TBL
POG0472
Bromomethane
0.0025 U
mg/kg dry
0.010
0.0025
1
8260D
7/31/20 12:43
TBL
POG0472
Carbon Tetrachloride
0.0010 U
mg/kg dry
0.0051
0.0010
1
8260D
7/31/20 12:43
TBL
POG0472
Chlorobenzene
0.00080 U
mg/kg dry
0.0051
0.00080
1
8260D
7/31/20 12:43
TBL
POG0472
Chloroethane
0.00098 U
mg/kg dry
0.010
0.00098
1
8260D
7/31/20 12:43
TBL
POG0472
Chloroform
0.00063 U
mg/kg dry
0.0051
0.00063
1
8260D
7/31/20 12:43
TBL
POG0472
Chloromethane
0.0016 U
mg/kg dry
0.010
0.0016
1
8260D
7/31/20 12:43
TBL
POG0472
cis-1,2-Dichloroethylene
0.00081 U
mg/kg dry
0.0051
0.00081
1
8260D
7/31/20 12:43
TBL
POG0472
cis-1,3-Dichloropropylene
0.00051 U
mg/kg dry
0.0051
0.00051
1
8260D
7/31/20 12:43
TBL
POG0472
Dibromochloromethane
0.00034 U
mg/kg dry
0.0051
0.00034
1
8260D
7/31/20 12:43
TBL
POG0472
Dichlorodifluoromethane
0.0014 U
mg/kg dry
0.010
0.0014
1
8260D
7/31/20 12:43
TBL
POG0472
Ethylbenzene
0.00077 U
mg/kg dry
0.0051
0.00077
1
8260D
7/31/20 12:43
TBL
POG0472
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• Laboratory Report
08/28/2020
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003 Client Sample ID: Backfill-DH
Attn: Andrew Besu Sample ID: 0070375-02
2923 South Tryon St. Ste 100 Work Order: 0070375
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 07/30/20 12:30
Time Submitted: 07/30/20 13:07
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Isopropyl Ether
0.00075 U
mg/kg dry
0.0051
0.00075
1
8260D
7/31/20 12:43
TBL
POG0472
Isopropylbenzene (Cumene)
0.00060 U
mg/kg dry
0.0051
0.00060
1
8260D
7/31/20 12:43
TBL
POG0472
m,p-Xylenes
0.0013 U
mg/kg dry
0.010
0.0013
1
8260D
7/31/20 12:43
TBL
P0O0472
Methyl Butyl Ketone (2-Hexanone)
0.00036 U
mg/kg dry
0.021
0.00036
1
8260D
7/31/20 12:43
TBL
P0O0472
Methyl Ethyl Ketone (2-Butanone)
0.0012 U
mg/kg dry
0.021
0.0012
1
8260D
7/31/20 12:43
TBL
P0O0472
Methyl Isobutyl Ketone
0.00042 U
mg/kg dry
0.021
0.00042
1
8260D
7/31/20 12:43
TBL
P0O0472
Methylene Chloride
0.00083 U
mg/kg dry
0.0051
0.00083
1
8260D
7/31/20 12:43
TBL
P0O0472
Methyl-tert-Butyl Ether
0.00072 U
mg/kg dry
0.0051
0.00072
1
8260D
7/31/20 12:43
TBL
P0O0472
Naphthalene
0.00097 J
mg/kg dry
0.010
0.00052
1
8260D
7/31/20 12:43
TBL
POG0472
n-Butylbenzene
0.00048 U
mg/kg dry
0.0051
0.00048
1
8260D
7/31/20 12:43
TBL
P0O0472
n-Propylbenzene
0.00074 U
mg/kg dry
0.0051
0.00074
1
8260D
7/31/20 12:43
TBL
P0O0472
o-Xylene
0.00055 U
mg/kg dry
0.0051
0.00055
1
8260D
7/31/20 12:43
TBL
P0O0472
sec-Butylbenzene
0.00055 U
mg/kg dry
0.0051
0.00055
1
8260D
7/31/20 12:43
TBL
P0O0472
Styrene
0.00050 U
mg/kg dry
0.0051
0.00050
1
8260D
7/31/20 12:43
TBL
P0O0472
tert-Butylbenzene
0.00061 U
mg/kg dry
0.0051
0.00061
1
8260D
7/31/20 12:43
TBL
P0O0472
Tetrachloroethylene
0.00093 U
mg/kg dry
0.0051
0.00093
1
8260D
7/31/20 12:43
TBL
POG0472
Toluene
0.00082 U
mg/kg dry
0.0051
0.00082
1
8260D
7/31/20 12:43
TBL
POG0472
trans-1,2-Dichloroethylene
0.00098 U
mg/kg dry
0.0051
0.00098
1
8260D
7/31/20 12:43
TBL
POG0472
trans-1,3-Dichloropropylene
0.00044 U
mg/kg dry
0.0051
0.00044
1
8260D
7/31/20 12:43
TBL
P0O0472
Trichloroethylene
0.0010 U
mg/kg dry
0.0051
0.0010
1
8260D
7/31/20 12:43
TBL
P0O0472
Trichlorofluoromethane
0.0014 U
mg/kg dry
0.010
0.0014
1
8260D
7/31/20 12:43
TBL
P0O0472
Vinyl acetate
0.00056 U
mg/kg dry
0.010
0.00056
1
8260D
7/31/20 12:43
TBL
P0O0472
Vinyl chloride
0.0010 U
mg/kg dry
0.010
0.0010
1
8260D
7/31/20 12:43
TBL
P0O0472
Xylenes, total
0.0018 U
mg/kg dry
0.015
0.0018
1
8260D
7/31/20 12:43
TBL
P0O0472
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
106 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
104 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Way po Int
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POG0472 - 5035
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:O7:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POG0472-BLK1)
Prepared: 07/30/20 Analyzed: 07/31/20
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way po 0nt_
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POG0472 - 5035
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POG0472-BLK1)
Prepared: 07/30/20 Analyzed: 07/31/20
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
52.3
ug/L
50.00
105
70-130
Surrogate: Dibromofluoromethane
51.5
ug/L
50.00
103
84-123
Surrogate: Toluene-d8
50.6
ug/L
50.00
101
76-129
LCS (POG0472-BS1)
Prepared: 07/30/20 Analyzed:
07/31/20
1,1,1,2-Tetrachloroethane
0.0532
0.0050
mg/kg wet
0.05000
106
72-115
1,1,1-Trichloroethane
0.0476
0.0050
mg/kg wet
0.05000
95
67-131
1,1,2,2-Tetrachloroethane
0.0510
0.0050
mg/kg wet
0.05000
102
56-126
1,1,2-Trichloroethane
0.0482
0.0050
mg/kg wet
0.05000
96
70-133
1,1-Dichloroethane
0.0472
0.0050
mg/kg wet
0.05000
94
74-127
1,1-Dichloroethylene
0.0448
0.0050
mg/kg wet
0.05000
90
67-149
1, 1 -Dichloropropylene
0.0466
0.0050
mg/kg wet
0.05000
93
71-130
1,2,3-Trichlorobenzene
0.0519
0.010
mg/kg wet
0.05000
104
68-130
1,2,3-Trichloropropane
0.0510
0.0050
mg/kg wet
0.05000
102
60-137
1,2,4-Trichlorobenzene
0.0526
0.010
mg/kg wet
0.05000
105
66-125
1,2,4-Trimethylbenzene
0.0524
0.0050
mg/kg wet
0.05000
105
69-129
1,2-Dibromoethane
0.0503
0.0050
mg/kg wet
0.05000
101
70-132
1,2-Dichlorobenzene
0.0508
0.0050
mg/kg wet
0.05000
102
72-123
1,2-Dichloroethane
0.0475
0.0050
mg/kg wet
0.05000
95
68-128
1,2-Dichloropropane
0.0480
0.0050
mg/kg wet
0.05000
96
73-130
1,3,5-Trimethylbenzene
0.0512
0.0050
mg/kg wet
0.05000
102
69-128
1,3-Dichlorobenzene
0.0508
0.0050
mg/kg wet
0.05000
102
71-120
1,3-Dichloropropane
0.0490
0.0050
mg/kg wet
0.05000
98
75-124
1,4-Dichlorobenzene
0.0502
0.0050
mg/kg wet
0.05000
100
71-123
2,2-Dichloropropane
0.0500
0.0050
mg/kg wet
0.05000
100
50-142
2-Chlorotoluene
0.0515
0.0050
mg/kg wet
0.05000
103
67-124
4-Chlorotoluene
0.0515
0.0050
mg/kg wet
0.05000
103
71-126
4-Isopropyltoluene
0.0526
0.0050
mg/kg wet
0.05000
105
68-129
Acetone
0.111
0.020
mg/kg wet
0.1000
ill
29-198
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way po 0nt_
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POG0472 - 5035
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POG0472-BSI)
Prepared: 07/30/20 Analyzed: 07/31/20
Benzene
0.0471
0.0050
mg/kg wet
0.05000
94
74-127
Bromobenzene
0.0506
0.0050
mg/kg wet
0.05000
101
73-125
Bromochloromethane
0.0503
0.0050
mg/kg wet
0.05000
101
72-134
Bromodichloromethane
0.0506
0.0050
mg/kg wet
0.05000
101
75-122
Bromoform
0.0470
0.0050
mg/kg wet
0.05000
94
66-135
Bromomethane
0.0472
0.010
mg/kg wet
0.05000
94
20-180
Carbon Tetrachloride
0.0494
0.0050
mg/kg wet
0.05000
99
64-143
Chlorobenzene
0.0482
0.0050
mg/kg wet
0.05000
96
74-118
Chloroethane
0.0399
0.010
mg/kg wet
0.05000
80
33-149
Chloroform
0.0478
0.0050
mg/kg wet
0.05000
96
73-127
Chloromethane
0.0412
0.010
mg/kg wet
0.05000
82
45-143
cis-1,2-Dichloroethylene
0.0477
0.0050
mg/kg wet
0.05000
95
76-134
cis-1,3-Dichloropropylene
0.0512
0.0050
mg/kg wet
0.05000
102
71-125
Dibromochloromethane
0.0533
0.0050
mg/kg wet
0.05000
107
73-122
Dichlorodifluoromethane
0.0402
0.010
mg/kg wet
0.05000
80
26-146
Ethylbenzene
0.0482
0.0050
mg/kg wet
0.05000
96
74-128
Isopropyl Ether
0.0494
0.0050
mg/kg wet
0.05000
99
59-159
Isopropylbenzene (Cumene)
0.0512
0.0050
mg/kg wet
0.05000
102
68-126
m,p-Xylenes
0.101
0.010
mg/kg wet
0.1000
101
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0622
0.020
mg/kg wet
0.05000
124
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0579
0.020
mg/kg wet
0.05000
116
63-149
Methyl Isobutyl Ketone
0.0522
0.020
mg/kg wet
0.05000
104
57-162
Methylene Chloride
0.0460
0.0050
mg/kg wet
0.05000
92
74-129
Methyl-tert-Butyl Ether
0.0484
0.0050
mg/kg wet
0.05000
97
70-130
Naphthalene
0.0526
0.010
mg/kg wet
0.05000
105
57-157
n-Butylbenzene
0.0528
0.0050
mg/kg wet
0.05000
106
65-135
n-Propylbenzene
0.0514
0.0050
mg/kg wet
0.05000
103
67-130
o-Xylene
0.0495
0.0050
mg/kg wet
0.05000
99
74-126
sec-Butylbenzene
0.0512
0.0050
mg/kg wet
0.05000
102
66-131
Styrene
0.0515
0.0050
mg/kg wet
0.05000
103
77-121
tert-Butyl benzene
0.0514
0.0050
mg/kg wet
0.05000
103
67-132
Tetrachloroethylene
0.0485
0.0050
mg/kg wet
0.05000
97
68-130
Toluene
0.0472
0.0050
mg/kg wet
0.05000
94
71-129
trans- 1,2-Dichloroethylene
0.0465
0.0050
mg/kg wet
0.05000
93
73-132
trans- 1,3-Dichloropropylene
0.0529
0.0050
mg/kg wet
0.05000
106
68-123
Trichloroethylene
0.0488
0.0050
mg/kg wet
0.05000
98
75-133
Trichlorofluoromethane
0.0427
0.010
mg/kg wet
0.05000
85
44-146
Vinyl acetate
0.0545
0.010
mg/kg wet
0.05000
109
85-161
Vinyl chloride
0.0443
0.010
mg/kg wet
0.05000
89
48-147
Xylenes, total
0.150
0.015
mg/kg wet
0.1500
100
74-126
Surrogate:4-Bromofluorobenzene
51.0
ug/L
50.00
102
70-130
Surrogate: Dibromofluoromethane
50.5
ug/L
50.00
101
84-123
Surrogate: Toluene-d8
50.6
ug/L
50.00
101
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way po 0nt_
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POG0472 - 5035
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:OOPM
Spike Source
Level Result %REC
%REC RPD
Limits RPD Limit
Matrix Spike (POG0472-MS1)
Source: 0070375-01
Prepared: 07/30/20 Analyzed: 07/31/20
1,1,1,2-Tetrachloroethane
0.0466
0.0056
mg/kg dry
0.05606
BRL
83
60-120
1,1,1-Trichloroethane
0.0490
0.0056
mg/kg dry
0.05606
BRL
87
52-139
1,1,2,2-Tetrachloroethane
0.00117
0.0056
mg/kg dry
0.05606
BRL
2
39-135
1,1,2-Trichloroethane
0.0273
0.0056
mg/kg dry
0.05606
BRL
49
44-140
1,1-Dichloroethane
0.0498
0.0056
mg/kg dry
0.05606
BRL
89
59-137
1,1-Dichloroethylene
0.0681
0.0056
mg/kg dry
0.05606
BRL
121
54-162
1, 1 -Dichloropropylene
0.0464
0.0056
mg/kg dry
0.05606
BRL
83
55-137
1,2,3-Trichlorobenzene
0.0311
0.011
mg/kg dry
0.05606
BRL
55
34-120
1,2,3-Trichloropropane
0.0481
0.0056
mg/kg dry
0.05606
BRL
86
45-139
1,2,4-Trichlorobenzene
0.0327
0.011
mg/kg dry
0.05606
BRL
58
35-116
1,2,4-Trimethylbenzene
0.0420
0.0056
mg/kg dry
0.05606
BRL
75
38-142
1,2-Dibromoethane
0.0485
0.0056
mg/kg dry
0.05606
BRL
86
49-132
1,2-Dichlorobenzene
0.0417
0.0056
mg/kg dry
0.05606
BRL
74
42-130
1,2-Dichloroethane
0.0486
0.0056
mg/kg dry
0.05606
BRL
87
51-131
1,2-Dichloropropane
0.0492
0.0056
mg/kg dry
0.05606
BRL
88
55-138
1,3,5-Trimethylbenzene
0.0445
0.0056
mg/kg dry
0.05606
BRL
79
44-140
1,3-Dichlorobenzene
0.0409
0.0056
mg/kg dry
0.05606
BRL
73
41-129
1,3-Dichloropropane
0.0492
0.0056
mg/kg dry
0.05606
BRL
88
53-129
1,4-Dichlorobenzene
0.0404
0.0056
mg/kg dry
0.05606
BRL
72
44-134
2,2-Dichloropropane
0.0493
0.0056
mg/kg dry
0.05606
BRL
88
30-147
2-Chlorotoluene
0.0424
0.0056
mg/kg dry
0.05606
BRL
76
46-132
4-Chlorotoluene
0.0424
0.0056
mg/kg dry
0.05606
BRL
76
44-135
4-Isopropyltoluene
0.0390
0.0056
mg/kg dry
0.05606
BRL
70
32-144
Acetone
0.141
0.022
mg/kg dry
0.1121
0.0386
92
34-143
Benzene
0.0463
0.0056
mg/kg dry
0.05606
BRL
83
60-135
Bromobenzene
0.0453
0.0056
mg/kg dry
0.05606
BRL
81
45-135
Bromochloromethane
0.0504
0.0056
mg/kg dry
0.05606
BRL
90
55-136
Bromodichloromethane
0.0398
0.0056
mg/kg dry
0.05606
BRL
71
55-127
Bromoform
0.0408
0.0056
mg/kg dry
0.05606
BRL
73
40-136
Bromomethane
0.0479
0.011
mg/kg dry
0.05606
BRL
85
30-137
Carbon Tetrachloride
0.0478
0.0056
mg/kg dry
0.05606
BRL
85
48-153
Chlorobenzene
0.0446
0.0056
mg/kg dry
0.05606
BRL
80
57-125
Chloroethane
0.0424
0.011
mg/kg dry
0.05606
BRL
76
16-177
Chloroform
0.0505
0.0056
mg/kg dry
0.05606
BRL
90
56-137
Chloromethane
0.0359
0.011
mg/kg dry
0.05606
BRL
64
40-145
cis-1,2-Dichloroethylene
0.0486
0.0056
mg/kg dry
0.05606
BRL
87
58-140
cis-1,3-Dichloropropylene
0.0500
0.0056
mg/kg dry
0.05606
BRL
89
42-135
Dibromochloromethane
0.0464
0.0056
mg/kg dry
0.05606
BRL
83
49-127
Dichlorodifluoromethane
0.0355
0.011
mg/kg dry
0.05606
BRL
63
25-151
Ethylbenzene
0.0456
0.0056
mg/kg dry
0.05606
BRL
81
44-144
Isopropyl Ether
0.0496
0.0056
mg/kg dry
0.05606
BRL
88
51-155
Isopropylbenzene (Cumene)
0.0445
0.0056
mg/kg dry
0.05606
BRL
79
41-140
m,p-Xylenes
0.0916
0.011
mg/kg dry
0.1121
BRL
82
36-148
Methyl Butyl Ketone (2-Hexanone)
0.0618
0.022
mg/kg dry
0.05606
BRL
110
30-147
Methyl Ethyl Ketone (2-Butanone)
0.0631
0.022
mg/kg dry
0.05606
BRL
113
24-160
Methyl Isobutyl Ketone
0.0517
0.022
mg/kg dry
0.05606
BRL
92
25-163
Notes
M,J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Level II QC Report
Way point_G
8/28/20
ANALYTICAL
Hart & Hickman (Charlotte)
Project: ATL-003
Work Order: 0070375
Attn: Andrew Besu
Time Submitted: 7/30/2020 1:07:OOPM
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Reporting
Spike
Source
%REC RPD
Analyte
Result
Limit
Units
Level
Result
%REC
Limits RPD Limit Notes
Batch POG0472 - 5035
Matrix Spike (POG0472-MS1)
Source: 0070375-01
Prepared: 07/30/20 Analyzed: 07/31/20
Methylene Chloride
0.0476
0.0056
mg/kg dry
0.05606
BRL
85
53-144
Methyl-tert-Butyl Ether
0.0479
0.0056
mg/kg dry
0.05606
BRL
85
49-135
Naphthalene
0.0370
0.011
mg/kg dry
0.05606
BRL
66
32-127
n-Butylbenzene
0.0357
0.0056
mg/kg dry
0.05606
BRL
64
23-148
n-Propylbenzene
0.0427
0.0056
mg/kg dry
0.05606
BRL
76
35-144
o-Xylene
0.0448
0.0056
mg/kg dry
0.05606
BRL
80
43-143
sec-Butylbenzene
0.0388
0.0056
mg/kg dry
0.05606
BRL
69
34-144
Styrene
0.0481
0.0056
mg/kg dry
0.05606
0.000680
85
42-132
tert-Butyl benzene
0.0409
0.0056
mg/kg dry
0.05606
BRL
73
36-150
Tetrachloroethylene
0.0427
0.0056
mg/kg dry
0.05606
BRL
76
47-142
Toluene
0.0458
0.0056
mg/kg dry
0.05606
BRL
82
57-135
trans- 1,2-Dichloroethylene
0.0475
0.0056
mg/kg dry
0.05606
BRL
85
58-141
trans- 1,3-Dichloropropylene
0.0471
0.0056
mg/kg dry
0.05606
BRL
84
41-124
Trichloroethylene
0.0906
0.0056
mg/kg dry
0.05606
BRL
162
38-164
Trichlorofluoromethane
0.0434
0.011
mg/kg dry
0.05606
BRL
77
30-157
Vinyl acetate
BRL
0.011
mg/kg dry
0.05606
BRL
61-154 M
Vinyl chloride
0.0434
0.011
mg/kg dry
0.05606
BRL
77
40-156
Xylenes, total
0.136
0.017
mg/kg dry
0.1682
BRL
81
36-148
Surrogate:4-Bromofluorobenzene
51.1
ug/L
50.00
102
70-130
Surrogate: Dibromofluoromethane
25.9
ug/L
50.00
52
84-123 SR
Surrogate: Toluene-d8
51.4
ug/L
50.00
103
76-129
Matrix Spike Dup (POG0472-MSD1)
Source: 0070375-01
Prepared: 07/30/20 Analyzed: 07/31/20
1,1,1,2-Tetrachloroethane
0.0473
0.0056
mg/kg dry
0.05606
BRL
84
60-120
1
15
1,1,1-Trichloroethane
0.0504
0.0056
mg/kg dry
0.05606
BRL
90
52-139
3
21
1,1,2,2-Tetrachloroethane
0.00115
0.0056
mg/kg dry
0.05606
BRL
2
39-135
1
22 M, J
1,1,2-Trichloroethane
0.0267
0.0056
mg/kg dry
0.05606
BRL
48
44-140
2
21
1,1-Dichloroethane
0.0510
0.0056
mg/kg dry
0.05606
BRL
91
59-137
2
21
1,1-Dichloroethylene
0.0713
0.0056
mg/kg dry
0.05606
BRL
127
54-162
5
22
1, 1 -Dichloropropylene
0.0480
0.0056
mg/kg dry
0.05606
BRL
86
55-137
4
19
1,2,3-Trichlorobenzene
0.0309
0.011
mg/kg dry
0.05606
BRL
55
34-120
0.7
41
1,2,3-Trichloropropane
0.0491
0.0056
mg/kg dry
0.05606
BRL
88
45-139
2
25
1,2,4-Trichlorobenzene
0.0326
0.011
mg/kg dry
0.05606
BRL
58
35-116
0.4
62
1,2,4-Trimethylbenzene
0.0440
0.0056
mg/kg dry
0.05606
BRL
78
38-142
5
24
1,2-Dibromoethane
0.0498
0.0056
mg/kg dry
0.05606
BRL
89
49-132
3
15
1,2-Dichlorobenzene
0.0428
0.0056
mg/kg dry
0.05606
BRL
76
42-130
3
21
1,2-Dichloroethane
0.0494
0.0056
mg/kg dry
0.05606
BRL
88
51-131
2
13
1,2-Dichloropropane
0.0496
0.0056
mg/kg dry
0.05606
BRL
89
55-138
0.9
16
1,3,5-Trimethylbenzene
0.0473
0.0056
mg/kg dry
0.05606
BRL
84
44-140
6
29
1,3-Dichlorobenzene
0.0423
0.0056
mg/kg dry
0.05606
BRL
75
41-129
3
24
1,3-Dichloropropane
0.0510
0.0056
mg/kg dry
0.05606
BRL
91
53-129
4
15
1,4-Dichlorobenzene
0.0425
0.0056
mg/kg dry
0.05606
BRL
76
44-134
5
21
2,2-Dichloropropane
0.0517
0.0056
mg/kg dry
0.05606
BRL
92
30-147
5
20
2-Chlorotoluene
0.0449
0.0056
mg/kg dry
0.05606
BRL
80
46-132
6
29
4-Chlorotoluene
0.0449
0.0056
mg/kg dry
0.05606
BRL
80
44-135
6
23
4-Isopropyltoluene
0.0400
0.0056
mg/kg dry
0.05606
BRL
71
32-144
3
22
Acetone
0.142
0.022
mg/kg dry
0.1121
0.0386
92
34-143
0.06
49
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way po 0nt_
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POG0472 - 5035
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (POG0472-MSD1)
Source: 0070375-01
Prepared: 07/30/20 Analyzed: 07/31/20
Benzene
0.0484
0.0056
mg/kg dry
0.05606
BRL
86
60-135
4
20
Bromobenzene
0.0483
0.0056
mg/kg dry
0.05606
BRL
86
45-135
7
25
Bromochloromethane
0.0497
0.0056
mg/kg dry
0.05606
BRL
89
55-136
1
18
Bromodichloromethane
0.0408
0.0056
mg/kg dry
0.05606
BRL
73
55-127
2
17
Bromoform
0.0419
0.0056
mg/kg dry
0.05606
BRL
75
40-136
3
35
Bromomethane
0.0424
0.011
mg/kg dry
0.05606
BRL
76
30-137
12
30
Carbon Tetrachloride
0.0505
0.0056
mg/kg dry
0.05606
BRL
90
48-153
6
23
Chlorobenzene
0.0463
0.0056
mg/kg dry
0.05606
BRL
83
57-125
4
14
Chloroethane
0.0430
0.011
mg/kg dry
0.05606
BRL
77
16-177
1
47
Chloroform
0.0512
0.0056
mg/kg dry
0.05606
BRL
91
56-137
1
18
Chloromethane
0.0366
0.011
mg/kg dry
0.05606
BRL
65
40-145
2
26
cis-1,2-Dichloroethylene
0.0500
0.0056
mg/kg dry
0.05606
BRL
89
58-140
3
28
cis-1,3-Dichloropropylene
0.0520
0.0056
mg/kg dry
0.05606
BRL
93
42-135
4
32
Dibromochloromethane
0.0489
0.0056
mg/kg dry
0.05606
BRL
87
49-127
5
24
Dichlorodifluoromethane
0.0370
0.011
mg/kg dry
0.05606
BRL
66
25-151
4
37
Ethylbenzene
0.0472
0.0056
mg/kg dry
0.05606
BRL
84
44-144
3
19
Isopropyl Ether
0.0510
0.0056
mg/kg dry
0.05606
BRL
91
51-155
3
13
Isopropylbenzene (Cumene)
0.0473
0.0056
mg/kg dry
0.05606
BRL
84
41-140
6
27
m,p-Xylenes
0.0965
0.011
mg/kg dry
0.1121
BRL
86
36-148
5
20
Methyl Butyl Ketone (2-Hexanone)
0.0642
0.022
mg/kg dry
0.05606
BRL
115
30-147
4
42
Methyl Ethyl Ketone (2-Butanone)
0.0642
0.022
mg/kg dry
0.05606
BRL
114
24-160
2
42
Methyl Isobutyl Ketone
0.0520
0.022
mg/kg dry
0.05606
BRL
93
25-163
0.5
44
Methylene Chloride
0.0477
0.0056
mg/kg dry
0.05606
BRL
85
53-144
0.4
14
Methyl-tert-Butyl Ether
0.0485
0.0056
mg/kg dry
0.05606
BRL
87
49-135
1
22
Naphthalene
0.0377
0.011
mg/kg dry
0.05606
BRL
67
32-127
2
44
n-Butylbenzene
0.0368
0.0056
mg/kg dry
0.05606
BRL
66
23-148
3
39
n-Propylbenzene
0.0454
0.0056
mg/kg dry
0.05606
BRL
81
35-144
6
27
o-Xylene
0.0464
0.0056
mg/kg dry
0.05606
BRL
83
43-143
4
17
sec-Butylbenzene
0.0407
0.0056
mg/kg dry
0.05606
BRL
73
34-144
5
28
Styrene
0.0499
0.0056
mg/kg dry
0.05606
0.000680
88
42-132
4
28
tert-Butyl benzene
0.0431
0.0056
mg/kg dry
0.05606
BRL
77
36-150
5
29
Tetrachloroethylene
0.0441
0.0056
mg/kg dry
0.05606
BRL
79
47-142
3
26
Toluene
0.0477
0.0056
mg/kg dry
0.05606
BRL
85
57-135
4
22
trans- 1,2-Dichloroethylene
0.0498
0.0056
mg/kg dry
0.05606
BRL
89
58-141
5
18
trans- 1,3-Dichloropropylene
0.0478
0.0056
mg/kg dry
0.05606
BRL
85
41-124
1
20
Trichloroethylene
0.0936
0.0056
mg/kg dry
0.05606
BRL
167
38-164
3
18
Trichlorofluoromethane
0.0435
0.011
mg/kg dry
0.05606
BRL
78
30-157
0.4
27
Vinyl acetate
BRL
0.011
mg/kg dry
0.05606
BRL
61-154
35
Vinyl chloride
0.0439
0.011
mg/kg dry
0.05606
BRL
78
40-156
1
35
Xylenes, total
0.143
0.017
mg/kg dry
0.1682
BRL
85
36-148
5
20
Surrogate:4-Bromofluorobenzene
52.5
ug/L
50.00
105
70-130
Surrogate: Dibromofluoromethane
25.4
ug/L
50.00
51
84-123
Surrogate: Toluene-d8
51.5
ug/L
50.00
103
76-129
M
M
SR
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

1 0
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POH0039 - 3546
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POH0039-BLK1)
Prepared: 08/04/20 Analyzed: 08/05/20
1,2,4-Trichlorobenzene
BRL
0.66
mg/kg wet
1,2-Dichlorobenzene
BRL
0.66
mg/kg wet
1,3-Dichlorobenzene
BRL
0.66
mg/kg wet
1,4-Dichlorobenzene
BRL
0.33
mg/kg wet
1-Methyl naphthalene
BRL
0.66
mg/kg wet
2,4,5-Trichlorophenol
BRL
0.66
mg/kg wet
2,4,6-Trichlorophenol
BRL
0.66
mg/kg wet
2,4-Dichlorophenol
BRL
0.66
mg/kg wet
2,4-Dimethylphenol
BRL
0.33
mg/kg wet
2,4-Dinitrophenol
BRL
1.5
mg/kg wet
2,4-Dinitrotoluene
BRL
0.66
mg/kg wet
2,6-Dinitrotoluene
BRL
0.66
mg/kg wet
2-Chloronaphthalene
BRL
0.66
mg/kg wet
2-Chlorophenol
BRL
0.66
mg/kg wet
2-Methyl naphthalene
BRL
0.66
mg/kg wet
2-Methylphenol
BRL
0.66
mg/kg wet
2-Nitrophenol
BRL
0.66
mg/kg wet
3,3'-Dichlorobenzidine
BRL
0.66
mg/kg wet
3/4-Methyl phenol
BRL
0.66
mg/kg wet
4,6-Dinitro-2-methylphenol
BRL
1.5
mg/kg wet
4-Bromophenyl phenyl ether
BRL
0.66
mg/kg wet
4-Chloro-3-methylphenol
BRL
0.66
mg/kg wet
4-Chloroaniline
BRL
0.33
mg/kg wet
4-Chlorophenyl phenyl ether
BRL
1.0
mg/kg wet
4-Nitrophenol
BRL
0.66
mg/kg wet
Acenaphthene
BRL
0.66
mg/kg wet
Acenaphthylene
BRL
0.66
mg/kg wet
Anthracene
BRL
0.66
mg/kg wet
Azobenzene
BRL
0.66
mg/kg wet
Benzo(a)anthracene
BRL
0.66
mg/kg wet
Benzo(a)pyrene
BRL
0.66
mg/kg wet
Benzo(b)fluoranthene
BRL
0.66
mg/kg wet
Benzo(g,h,i)perylene
BRL
0.66
mg/kg wet
Benzo(k)fluoranthene
BRL
0.66
mg/kg wet
Benzoic Acid
BRL
2.0
mg/kg wet
Benzyl alcohol
BRL
0.66
mg/kg wet
bis(2-Chloroethoxy)methane
BRL
0.66
mg/kg wet
Bis(2-Chloroethyl)ether
BRL
0.66
mg/kg wet
Bis(2-chloroisopropyl)ether
BRL
0.33
mg/kg wet
Bis(2-Ethylhexyl)phthalate
BRL
0.66
mg/kg wet
Butyl benzyl phthalate
BRL
0.33
mg/kg wet
Chrysene
BRL
0.66
mg/kg wet
Dibenzo(a,h)anthracene
BRL
0.66
mg/kg wet
Dibenzofuran
BRL
0.66
mg/kg wet
Diethyl phthalate
BRL
0.66
mg/kg wet
Dimethyl phthalate
BRL
0.66
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

1 0
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POH0039 - 3546
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POH0039-BLK1)
Prepared: 08/04/20 Analyzed: 08/05/20
Di-n-butyl phthalate
BRL
0.66
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.66
mg/kg wet
Fluorene
BRL
0.66
mg/kg wet
Hexachlorobenzene
BRL
0.66
mg/kg wet
Hexachlorobutadiene
BRL
0.66
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.66
mg/kg wet
Hexachloroethane
BRL
0.66
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.66
mg/kg wet
Isophorone
BRL
0.66
mg/kg wet
Naphthalene
BRL
0.66
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.66
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.66
mg/kg wet
Pentachlorophenol
BRL
1.0
mg/kg wet
Phenanthrene
BRL
0.66
mg/kg wet
Phenol
BRL
0.66
mg/kg wet
Pyrene
BRL
0.66
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
3.36
mg/kg wet
3.317
101
39-132
Surrogate: 2-Fluorobiphenyl
1.28
mg/kg wet
1.658
77
44-115
Surrogate: 2-Fluorophenol
2.63
mg/kg wet
3.317
79
35-115
Surrogate: Nitrobenzene-d5
1.18
mg/kg wet
1.658
71
37-122
Surrogate: Phenol-d5
2.66
mg/kg wet
3.317
80
34-121
Surrogate: Terphenyl-d14
1.49
mg/kg wet
1.658
90
54-127
LCS (POH0039-BSI)
Prepared: 08/04/20 Analyzed: 08/05/20
1,2,4-Trichlorobenzene
1.12
0.66
mg/kg wet
1.663
67
34-118
1,2-Dichlorobenzene
1.01
0.66
mg/kg wet
1.663
61
33-117
1,3-Dichlorobenzene
0.980
0.66
mg/kg wet
1.663
59
30-115
1,4-Dichlorobenzene
0.970
0.33
mg/kg wet
1.663
58
31-115
1-Methyl naphthalene
1.22
0.66
mg/kg wet
1.663
73
40-119
2,4,5-Trichlorophenol
1.38
0.66
mg/kg wet
1.663
83
62-124
2,4,6-Trichlorophenol
1.34
0.66
mg/kg wet
1.663
80
39-126
2,4-Dichlorophenol
1.29
0.66
mg/kg wet
1.663
77
40-122
2,4-Dimethylphenol
1.46
0.33
mg/kg wet
1.663
88
30-127
2,4-Dinitrophenol
0.751
1.5
mg/kg wet
1.663
45
27-129 J
2,4-Dinitrotoluene
1.30
0.66
mg/kg wet
1.663
78
48-126
2,6-Dinitrotoluene
1.29
0.66
mg/kg wet
1.663
77
46-124
2-Chloronaphthalene
1.16
0.66
mg/kg wet
1.663
70
41-114
2-Chlorophenol
1.18
0.66
mg/kg wet
1.663
71
34-121
2-Methyl naphthalene
1.17
0.66
mg/kg wet
1.663
70
38-122
2-Methylphenol
1.21
0.66
mg/kg wet
1.663
73
32-122
2-Nitrophenol
1.21
0.66
mg/kg wet
1.663
73
36-123
3,3'-Dichlorobenzidine
1.45
0.66
mg/kg wet
1.663
87
22-121
3/4-Methyl phenol
1.06
0.66
mg/kg wet
1.663
64
34-119
4,6-Dinitro-2-methylphenol
1.16
1.5
mg/kg wet
1.663
70
29-132 J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

1 0
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POH0039 - 3546
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POH0039-BS1)
Prepared: 08/04/20 Analyzed: 08/05/20
4-Bromophenyl phenyl ether
1.24
0.66
mg/kg wet
1.663
75
46-124
4-Chloro-3-methylphenol
1.29
0.66
mg/kg wet
1.663
78
45-122
4-Chloroaniline
1.09
0.33
mg/kg wet
1.663
66
17-106
4-Chlorophenyl phenyl ether
1.22
1.0
mg/kg wet
1.663
73
45-121
4-Nitrophenol
1.38
0.66
mg/kg wet
1.663
83
30-132
Acenaphthene
1.19
0.66
mg/kg wet
1.663
72
40-123
Acenaphthylene
1.23
0.66
mg/kg wet
1.663
74
32-132
Anthracene
1.28
0.66
mg/kg wet
1.663
77
47-123
Azobenzene
1.17
0.66
mg/kg wet
1.663
71
39-125
Benzo(a)anthracene
1.38
0.66
mg/kg wet
1.663
83
49-126
Benzo(a)pyrene
1.42
0.66
mg/kg wet
1.663
86
45-129
Benzo(b)fluoranthene
1.36
0.66
mg/kg wet
1.663
82
45-132
Benzo(g,h,i)perylene
1.41
0.66
mg/kg wet
1.663
85
43-134
Benzo(k)fluoranthene
1.35
0.66
mg/kg wet
1.663
81
47-132
Benzoic Acid
BRL
2.0
mg/kg wet
1.663
10-83
Benzyl alcohol
1.20
0.66
mg/kg wet
1.663
72
29-122
bis(2-Chloroethoxy)methane
1.09
0.66
mg/kg wet
1.663
65
36-121
Bis(2-Chloroethyl)ether
0.897
0.66
mg/kg wet
1.663
54
31-120
Bis(2-chloroisopropyl)ether
0.880
0.33
mg/kg wet
1.663
53
33-131
Bis(2-Ethylhexyl)phthalate
1.50
0.66
mg/kg wet
1.663
90
51-133
Butyl benzyl phthalate
1.36
0.33
mg/kg wet
1.663
82
48-132
Chrysene
1.31
0.66
mg/kg wet
1.663
79
50-124
Dibenzo(a,h)anthracene
0.942
0.66
mg/kg wet
1.663
57
45-134
Dibenzofuran
1.17
0.66
mg/kg wet
1.663
70
44-120
Diethyl phthalate
1.18
0.66
mg/kg wet
1.663
71
50-124
Dimethyl phthalate
1.19
0.66
mg/kg wet
1.663
72
48-124
Di-n-butyl phthalate
1.30
0.66
mg/kg wet
1.663
78
51-128
Di-n-octyl phthalate
1.42
0.33
mg/kg wet
1.663
85
45-140
Fluoranthene
1.27
0.66
mg/kg wet
1.663
76
50-127
Fluorene
1.26
0.66
mg/kg wet
1.663
76
43-125
Hexachlorobenzene
1.23
0.66
mg/kg wet
1.663
74
45-122
Hexachlorobutadiene
1.24
0.66
mg/kg wet
1.663
75
32-123
Hexachlorocyclopentadiene
1.12
0.66
mg/kg wet
1.663
67
32-117
Hexachloroethane
0.964
0.66
mg/kg wet
1.663
58
28-117
Indeno(1,2,3-cd)pyrene
1.55
0.66
mg/kg wet
1.663
93
45-133
Isophorone
0.937
0.66
mg/kg wet
1.663
56
30-122
Naphthalene
1.14
0.66
mg/kg wet
1.663
68
35-123
Nitrobenzene
1.00
0.33
mg/kg wet
1.663
60
34-122
N-Nitroso-di-n-propylamine
1.08
0.66
mg/kg wet
1.663
65
36-120
N-Nitrosodiphenylamine
1.47
0.66
mg/kg wet
1.663
88
38-127
Pentachlorophenol
1.46
1.0
mg/kg wet
1.663
88
25-133
Phenanthrene
1.25
0.66
mg/kg wet
1.663
75
50-121
Phenol
1.17
0.66
mg/kg wet
1.663
70
34-121
Pyrene
1.45
0.66
mg/kg wet
1.663
87
47-127
Pyridine
0.694
0.33
mg/kg wet
1.663
42
10-60
Surrogate: 2,4,6-Tribromophenol
2.87
mg/kg wet
3.327
86
39-132
L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

1 0
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POH0039 - 3546
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:O7:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POH0039-BS1)
Prepared: 08/04/20 Analyzed: 08/05/20
Surrogate: 2-Fluorobiphenyl
1.16
mg/kg wet
1.663
70
44-115
Surrogate: 2-Fluorophenol
2.27
mg/kg wet
3.327
68
35-115
Surrogate: Nitrobenzene-d5
1.05
mg/kg wet
1.663
63
37-122
Surrogate: Phenol-d5
2.24
mg/kg wet
3.327
67
34-121
Surrogate: Terphenyl-d14
1.33
mg/kg wet
1.663
80
54-127
Matrix Spike (POH0039-MS1)
Source: 0070375-02
Prepared:
08/04/20 Analyzed: 08/05/20
1,2,4-Trichlorobenzene
1.48
0.74
mg/kg dry
1.878
BRL
79
34-118
1,2-Dichlorobenzene
1.29
0.74
mg/kg dry
1.878
BRL
69
33-117
1,3-Dichlorobenzene
1.24
0.74
mg/kg dry
1.878
BRL
66
30-115
1,4-Dichlorobenzene
1.23
0.37
mg/kg dry
1.878
BRL
65
31-115
1-Methyl naphthalene
1.58
0.74
mg/kg dry
1.878
BRL
84
40-119
2,4,5-Trichlorophenol
0.525
0.74
mg/kg dry
1.878
BRL
28
45-121
MI, J
2,4,6-Trichlorophenol
0.377
0.74
mg/kg dry
1.878
BRL
20
39-126
MI, J
2,4-Dichlorophenol
0.398
0.74
mg/kg dry
1.878
BRL
21
40-122
MI, J
2,4-Dimethylphenol
1.60
0.37
mg/kg dry
1.878
BRL
85
30-127
2,4-Dinitrophenol
BRL
1.7
mg/kg dry
1.878
BRL
27-129
MI
2,4-Dinitrotoluene
0.222
0.74
mg/kg dry
1.878
BRL
12
48-126
MI, J
2,6-Dinitrotoluene
0.267
0.74
mg/kg dry
1.878
BRL
14
46-124
MI, J
2-Chloronaphthalene
1.45
0.74
mg/kg dry
1.878
BRL
77
41-114
2-Chlorophenol
0.295
0.74
mg/kg dry
1.878
BRL
16
34-121
MI, J
2-Methyl naphthalene
1.55
0.74
mg/kg dry
1.878
BRL
83
38-122
2-Methylphenol
0.856
0.74
mg/kg dry
1.878
BRL
46
32-122
2-Nitrophenol
0.174
0.74
mg/kg dry
1.878
BRL
9
36-123
MI, J
3,3'-Dichlorobenzidine
1.47
0.74
mg/kg dry
1.878
BRL
78
22-121
3/4-Methyl phenol
1.04
0.74
mg/kg dry
1.878
BRL
55
34-119
4,6-Dinitro-2-methylphenol
BRL
1.7
mg/kg dry
1.878
BRL
29-132
MI
4-Bromophenyl phenyl ether
1.51
0.74
mg/kg dry
1.878
BRL
80
46-124
4-Chloro-3-methylphenol
0.843
0.74
mg/kg dry
1.878
BRL
45
45-122
4-Chloroaniline
1.27
0.37
mg/kg dry
1.878
BRL
68
17-106
4-Chlorophenyl phenyl ether
1.48
1.1
mg/kg dry
1.878
BRL
79
45-121
4-Nitrophenol
0.768
0.74
mg/kg dry
1.878
BRL
41
30-132
Acenaphthene
1.50
0.74
mg/kg dry
1.878
0.0525
77
40-123
Acenaphthylene
1.50
0.74
mg/kg dry
1.878
BRL
80
32-132
Anthracene
1.60
0.74
mg/kg dry
1.878
0.123
78
47-123
Azobenzene
1.44
0.74
mg/kg dry
1.878
BRL
77
39-125
Benzo(a)anthracene
1.88
0.74
mg/kg dry
1.878
0.295
84
49-126
Benzo(a)pyrene
1.91
0.74
mg/kg dry
1.878
0.227
89
45-129
Benzo(b)fluoranthene
1.88
0.74
mg/kg dry
1.878
0.321
83
45-132
Benzo(g,h,i)perylene
1.80
0.74
mg/kg dry
1.878
0.161
87
43-134
Benzo(k)fluoranthene
1.68
0.74
mg/kg dry
1.878
0.107
84
47-132
Benzoic Acid
BRL
2.3
mg/kg dry
1.878
BRL
10-83
MI
Benzyl alcohol
0.226
0.74
mg/kg dry
1.878
BRL
12
29-122
MI, J
bis(2-Chloroethoxy)methane
1.06
0.74
mg/kg dry
1.878
BRL
56
36-121
Bis(2-Chloroethyl)ether
1.07
0.74
mg/kg dry
1.878
BRL
57
31-120
Bis(2-chloroisopropyl)ether
1.31
0.37
mg/kg dry
1.878
BRL
70
33-131
Bis(2-Ethylhexyl)phthalate
1.79
0.74
mg/kg dry
1.878
0.465
70
51-133
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Level II QC Report
Waypo i nt .0 8/28/20
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003 Work Order: 0070375
Attn: Andrew Besu Time Submitted: 7/30/2020 1:07:OOPM
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting
Spike
Source
%REC RPD
Analyte
Result
Limit
Units
Level
Result
%REC
Limits RPD Limit
Notes
Batch POH0039 - 3546
Matrix Spike (POH0039-MS1)
Source: 0070375-02
Prepared:
08/04/20
Analyzed:
08/05/20
Butyl benzyl phthalate
0.272
0.37
mg/kg dry
1.878
BRL
14
48-132
MI, J
Chrysene
1.79
0.74
mg/kg dry
1.878
0.289
80
50-124
Dibenzo(a,h)anthracene
1.20
0.74
mg/kg dry
1.878
0.0407
62
45-134
Dibenzofuran
1.46
0.74
mg/kg dry
1.878
BRL
78
44-120
Diethyl phthalate
0.201
0.74
mg/kg dry
1.878
BRL
11
50-124
MI, J
Dimethyl phthalate
BRL
0.74
mg/kg dry
1.878
BRL
48-124
MI
Di-n-butyl phthalate
0.389
0.74
mg/kg dry
1.878
BRL
21
51-128
MI, J
Di-n-octyl phthalate
0.916
0.37
mg/kg dry
1.878
BRL
49
45-140
Fluoranthene
1.95
0.74
mg/kg dry
1.878
0.621
71
50-127
Fluorene
1.49
0.74
mg/kg dry
1.878
0.0495
77
43-125
Hexachlorobenzene
1.47
0.74
mg/kg dry
1.878
BRL
78
45-122
Hexachlorobutadiene
1.61
0.74
mg/kg dry
1.878
BRL
86
32-123
Hexachlorocyclopentadiene
BRL
0.74
mg/kg dry
1.878
BRL
32-117
MI
Hexachloroethane
BRL
0.74
mg/kg dry
1.878
BRL
28-117
MI
Indeno(1,2,3-cd)pyrene
2.02
0.74
mg/kg dry
1.878
0.164
99
45-133
Isophorone
1.29
0.74
mg/kg dry
1.878
0.376
49
30-122
Naphthalene
1.51
0.74
mg/kg dry
1.878
0.0404
78
35-123
Nitrobenzene
0.994
0.37
mg/kg dry
1.878
BRL
53
34-122
N-Nitroso-di-n-propylamine
1.47
0.74
mg/kg dry
1.878
BRL
78
36-120
N-Nitrosodiphenylamine
1.80
0.74
mg/kg dry
1.878
BRL
96
38-127
Pentachlorophenol
1.21
1.1
mg/kg dry
1.878
BRL
65
25-133
Phenanthrene
1.81
0.74
mg/kg dry
1.878
0.469
71
50-121
Phenol
0.152
0.74
mg/kg dry
1.878
BRL
8
34-121
MI, J
Pyrene
2.17
0.74
mg/kg dry
1.878
0.578
85
47-127
Pyridine
0.827
0.37
mg/kg dry
1.878
BRL
44
20-150
Surrogate: 2,4,6-Tribromophenol
0.752
mg/kg dry
3.756
20
39-132
SM
Surrogate: 2-Fluorobiphenyl
1.38
mg/kg dry
1.878
73
44-115
Surrogate: 2-Fluorophenol
0.565
mg/kg dry
3.756
15
35-115
Ml
Surrogate: Nitrobenzene-d5
0.982
mg/kg dry
1.878
52
37-122
Surrogate: Phenol-d5
1.58
mg/kg dry
3.756
42
34-121
Surrogate: Terphenyl-d14
1.58
mg/kg dry
1.878
84
54-127
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way po 0nt_
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch POH0039 - 3546
Matrix Spike Dup (POH0039-MSD1)
Source: 0070375-02
Prepared: 08/04/20 Analyzed: 08/05/20
1,2,4-Trichlorobenzene
1.39
0.73
mg/kg dry
1.832
BRL
76
34-118
6
20
1,2-Dichlorobenzene
1.23
0.73
mg/kg dry
1.832
BRL
67
33-117
4
20
1,3-Dichlorobenzene
1.18
0.73
mg/kg dry
1.832
BRL
64
30-115
5
20
1,4-Dichlorobenzene
1.17
0.36
mg/kg dry
1.832
BRL
64
31-115
5
20
1-Methyl naphthalene
1.54
0.73
mg/kg dry
1.832
BRL
84
40-119
3
20
2,4,5-Trichlorophenol
0.527
0.73
mg/kg dry
1.832
BRL
29
45-121
0.5
35
MI, J
2,4,6-Trichlorophenol
0.342
0.73
mg/kg dry
1.832
BRL
19
39-126
10
20
MI, J
2,4-Dichlorophenol
0.401
0.73
mg/kg dry
1.832
BRL
22
40-122
0.7
20
MI, J
2,4-Dimethylphenol
1.51
0.36
mg/kg dry
1.832
BRL
82
30-127
6
20
2,4-Dinitrophenol
BRL
1.6
mg/kg dry
1.832
BRL
27-129
20
MI
2,4-Dinitrotoluene
0.214
0.73
mg/kg dry
1.832
BRL
12
48-126
4
20
MI, J
2,6-Dinitrotoluene
0.308
0.73
mg/kg dry
1.832
BRL
17
46-124
14
20
MI, J
2-Chloronaphthalene
1.38
0.73
mg/kg dry
1.832
BRL
75
41-114
5
20
2-Chlorophenol
0.398
0.73
mg/kg dry
1.832
BRL
22
34-121
30
20
D, MI, J
2-Methyl naphthalene
1.52
0.73
mg/kg dry
1.832
BRL
83
38-122
2
20
2-Methylphenol
0.848
0.73
mg/kg dry
1.832
BRL
46
32-122
0.9
20
2-Nitrophenol
0.161
0.73
mg/kg dry
1.832
BRL
9
36-123
8
20
MI, J
3,3'-Dichlorobenzidine
1.46
0.73
mg/kg dry
1.832
BRL
80
22-121
0.6
20
3/4-Methyl phenol
0.964
0.73
mg/kg dry
1.832
BRL
53
34-119
7
20
4,6-Dinitro-2-methylphenol
BRL
1.6
mg/kg dry
1.832
BRL
29-132
20
MI
4-Bromophenyl phenyl ether
1.46
0.73
mg/kg dry
1.832
BRL
79
46-124
4
20
4-Chloro-3-methylphenol
0.836
0.73
mg/kg dry
1.832
BRL
46
45-122
0.8
20
4-Chloroaniline
1.19
0.36
mg/kg dry
1.832
BRL
65
17-106
6
20
4-Chlorophenyl phenyl ether
1.40
1.1
mg/kg dry
1.832
BRL
77
45-121
6
20
4-Nitrophenol
0.790
0.73
mg/kg dry
1.832
BRL
43
30-132
3
20
Acenaphthene
1.61
0.73
mg/kg dry
1.832
0.0525
85
40-123
7
20
Acenaphthylene
1.45
0.73
mg/kg dry
1.832
BRL
79
32-132
3
20
Anthracene
1.96
0.73
mg/kg dry
1.832
0.123
100
47-123
20
20
D
Azobenzene
1.38
0.73
mg/kg dry
1.832
BRL
75
39-125
4
20
Benzo(a)anthracene
2.50
0.73
mg/kg dry
1.832
0.295
120
49-126
28
20
D
Benzo(a)pyrene
2.33
0.73
mg/kg dry
1.832
0.227
115
45-129
20
20
D
Benzo(b)fluoranthene
2.55
0.73
mg/kg dry
1.832
0.321
122
45-132
30
20
D
Benzo(g,h,i)perylene
2.11
0.73
mg/kg dry
1.832
0.161
106
43-134
16
20
Benzo(k)fluoranthene
1.81
0.73
mg/kg dry
1.832
0.107
93
47-132
7
20
Benzoic Acid
BRL
2.2
mg/kg dry
1.832
BRL
10-83
20
MI
Benzyl alcohol
1.67
0.73
mg/kg dry
1.832
BRL
91
29-122
152
20
D
bis(2-Chloroethoxy)methane
1.10
0.73
mg/kg dry
1.832
BRL
60
36-121
4
20
Bis(2-Chloroethyl)ether
1.11
0.73
mg/kg dry
1.832
BRL
61
31-120
3
20
Bis(2-chloroisopropyl)ether
1.26
0.36
mg/kg dry
1.832
BRL
69
33-131
4
20
Bis(2-Ethylhexyl)phthalate
1.72
0.73
mg/kg dry
1.832
0.465
69
51-133
4
20
Butyl benzyl phthalate
0.290
0.36
mg/kg dry
1.832
BRL
16
48-132
6
20
MI, J
Chrysene
2.35
0.73
mg/kg dry
1.832
0.289
112
50-124
27
20
D
Dibenzo(a,h)anthracene
1.19
0.73
mg/kg dry
1.832
0.0407
63
45-134
0.8
20
Dibenzofuran
1.52
0.73
mg/kg dry
1.832
BRL
83
44-120
4
20
Diethyl phthalate
0.229
0.73
mg/kg dry
1.832
BRL
13
50-124
13
20
MI, J
Dimethyl phthalate
BRL
0.73
mg/kg dry
1.832
BRL
48-124
20
MI
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

1 0
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: ATL-003
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting
Analyte Result Limit Units
Batch POH0039 - 3546
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:O7:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (POH0039-MSD1)
Source: 0070375-02
Prepared: 08/04/20 Analyzed: 08/05/20
Di-n-butyl phthalate
0.427
0.73
mg/kg dry
1.832
BRL
23
51-128
9
20
MI, J
Di-n-octyl phthalate
0.889
0.36
mg/kg dry
1.832
BRL
49
45-140
3
20
Fluoranthene
3.28
0.73
mg/kg dry
1.832
0.621
145
50-127
51
20
D, MI
Fluorene
1.67
0.73
mg/kg dry
1.832
0.0495
89
43-125
11
20
Hexachlorobenzene
1.41
0.73
mg/kg dry
1.832
BRL
77
45-122
4
20
Hexachlorobutadiene
1.49
0.73
mg/kg dry
1.832
BRL
81
32-123
8
20
Hexachlorocyclopentadiene
BRL
0.73
mg/kg dry
1.832
BRL
32-117
20
MI
Hexachloroethane
BRL
0.73
mg/kg dry
1.832
BRL
28-117
20
MI
Indeno(1,2,3-cd)pyrene
2.32
0.73
mg/kg dry
1.832
0.164
118
45-133
14
20
Isophorone
1.18
0.73
mg/kg dry
1.832
0.376
44
30-122
9
20
Naphthalene
1.55
0.73
mg/kg dry
1.832
0.0404
83
35-123
3
20
Nitrobenzene
0.930
0.36
mg/kg dry
1.832
BRL
51
34-122
7
20
N-Nitroso-di-n-propylamine
1.42
0.73
mg/kg dry
1.832
BRL
78
36-120
4
20
N-Nitrosodiphenylamine
1.72
0.73
mg/kg dry
1.832
BRL
94
38-127
4
20
Pentachlorophenol
1.24
1.1
mg/kg dry
1.832
BRL
67
25-133
2
20
Phenanthrene
3.20
0.73
mg/kg dry
1.832
0.469
149
50-121
56
20
D, MI
Phenol
0.145
0.73
mg/kg dry
1.832
BRL
8
34-121
4
20
MI, J
Pyrene
3.28
0.73
mg/kg dry
1.832
0.578
148
47-127
41
20
MI
Pyridine
0.759
0.36
mg/kg dry
1.832
BRL
41
20-150
9
60
Surrogate: 2,4,6-Tribromophenol
0.695
mg/kg dry
3.665
19
39-132
SM
Surrogate: 2-Fluorobiphenyl
1.34
mg/kg dry
1.832
73
44-115
Surrogate: 2-Fluorophenol
0.494
mg/kg dry
3.665
13
35-115
Ml
Surrogate: Nitrobenzene-d5
0.923
mg/kg dry
1.832
50
37-122
Surrogate: Phenol-d5
1.48
mg/kg dry
3.665
40
34-121
Surrogate: Terphenyl-d14
1.50
mg/kg dry
1.832
82
54-127
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

1 0
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte)
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Total Metals - Quality Control
Analyte
Batch POH0004 - 3050B
Project: ATL-003
Reporting
Result Limit Units
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:07:00PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POH0004-BLK1)
Prepared & Analyzed: 08/03/20
Arsenic
BRL
1.0
mg/kg wet
Barium
BRL
100
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Chromium
BRL
10
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Silver
BRL
0.50
mg/kg wet
LCS (POH0004-BS1)
Prepared &Analyzed: 08/03/20
Arsenic
12.0
1.0
mg/kg wet
12.50 96
80-120
Barium
12.3
100
mg/kg wet
12.50 98
80-120
J
Cadmium
12.9
0.50
mg/kg wet
12.50 103
80-120
Chromium
12.7
10
mg/kg wet
12.50 102
80-120
Lead
13.2
1.0
mg/kg wet
12.50 106
80-120
Selenium
12.9
1.0
mg/kg wet
12.50 103
80-120
Silver
5.10
0.50
mg/kg wet
5.000 102
80-120
Matrix Spike (POH0004-MS1)
Source: 0070375-01
Prepared & Analyzed: 08/03/20
Arsenic
18.6
1.1
mg/kg dry
14.02 5.72 92
75-125
Barium
107
110
mg/kg dry
14.02 87.4 139
75-125
M, J
Cadmium
14.3
0.56
mg/kg dry
14.02 0.107 101
75-125
Chromium
40.6
11
mg/kg dry
14.02 25.4 108
75-125
Lead
26.7
1.1
mg/kg dry
14.02 11.1 111
75-125
Selenium
16.9
1.1
mg/kg dry
14.01 3.52 95
75-125
Silver
5.65
0.56
mg/kg dry
5.606 0.0852 99
75-125
Matrix Spike Dup (POH0004-MSD1)
Source: 0070375-01
Prepared & Analyzed: 08/03/20
Arsenic
18.9
1.1
mg/kg dry
14.02 5.72 94
75-125
2
20
Barium
96.2
110
mg/kg dry
14.02 87.4 63
75-125
11
20 M, J
Cadmium
14.1
0.56
mg/kg dry
14.02 0.107 100
75-125
1
20
Chromium
41.6
11
mg/kg dry
14.02 25.4 116
75-125
2
20
Lead
25.3
1.1
mg/kg dry
14.02 11.1 101
75-125
5
20
Selenium
16.4
1.1
mg/kg dry
14.01 3.52 92
75-125
3
20
Silver
5.66
0.56
mg/kg dry
5.606 0.0852 100
75-125
0.3
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

1 0
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte)
Attn: Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Total Metals - Quality Control
Analyte
Project: ATL-003
Level II QC Report
8/28/20
Work Order: 0070375
Time Submitted: 7/30/2020 1:O7:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POH0004 - 3050B
Post Spike (POH0004-PS1)
Source: 0070375-01
Prepared & Analyzed: 08/03/20
Arsenic
115
ug/L
100.0 20.4 95
80-120
Barium
403
ug/L
100.0 312 92
80-120
Cadmium
99.2
ug/L
100.0 0.383 99
80-120
Chromium
188
ug/L
100.0 90.6 98
80-120
Lead
139
ug/L
100.0 39.6 99
80-120
Selenium
111
ug/L
100.0 12.5 99
80-120
Silver
101
ug/L
100.0 0.304 100
80-120
Batch POH0026 - 7471 B
Blank (POH0026-BLK1)
Prepared & Analyzed: 08/04/20
Mercury
BRL
0.050 mg/kg wet
LCS (POH0026-BS1)
Prepared &Analyzed: 08/04/20
Mercury
0.418
0.050 mg/kg wet
0.4167 100
80-120
Matrix Spike (POH0026-MS1)
Source: 0070375-01
Prepared & Analyzed: 08/04/20
Mercury
0.500
0.056 mg/kg dry
0.4672 0.0246 102
80-120
Matrix Spike Dup (POH0026-MSD1)
Source: 0070375-01
Prepared & Analyzed: 08/04/20
Mercury
0.499
0.056 mg/kg dry
0.4672 0.0246 102
80-120 0.2 20
Post Spike (POH0026-PS1)
Source: 0070375-01
Prepared & Analyzed: 08/04/20
Mercury
5.61
ug/L
5.000 0.263 107
85-115
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
0070375-01
POH0033
30 g
30 g
08/04/20 14:46
0070375-02
POH0033
30 g
30 g
08/04/20 14:46
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
0070375-01
POH0039
30.47 g
1 mL
08/04/20 11:00
0070375-02
POH0039
30.8 g
1 mL
08/04/20 11:00
Prep Method: *** DEFAULT PREP ***
Lab Number
Batch
Initial
Final
Date/Time
0070375-01
POH0417
100 g
100 mL
08/21/20 12:10
0070375-02
POH0417
100 g
100 mL
08/21/20 12:10
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
0070375-01
POH0004
2 g
50 mL
08/03/20 7:41
0070375-02
POH0004
2 g
50 mL
08/03/20 7:41
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/Time
0070375-01
POH0026
0.6 g
50 mL
08/04/20 11:31
0070375-02
POH0026
0.6 g
50 mL
08/04/20 11:31
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date/Time
0070375-01
POG0472
5.28 g
5 mL
07/31/20 9:09
0070375-02
POG0472
5.5 g
5 mL
07/31/20 9:09
Subcontracted Analyses
The following analyses
were subcontracted to Pace Analytical
Services, LLC (Shealy)
Lab Number
Analysis
0070375-01
Hexavalent Chromium by 7199 (Sub)
0070375-02
Hexavalent Chromium by 7199 (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint.
ANALYTICAL
449 Springbrook Road • Charlotte, INC 21217
Phone [phone] •Fax• 704i152&0409
Client Company Name: 14-,+,
_A Plc,*,n
Report To/Contact Name: ,-GW V
Reporting Address: j • Tr y.
CHAIN OF CUSTODY RECORD
PAGE 1 of l QUOTE O TOENSURE PROPER BILLING:
Project Name: A L -003
Short Hold Analysis (Yes) (I�o UST Project: (Yes) go
"Please ATTACH any project specific reporting (QC LEVEL 1 11 III IV)
provisions and/or Q Requirements t.
Invoice To: atCovht�PA,,ry94�,411 -Ckri.eVP).Co_,--1
Address: I I
YES NO
NIA
Samples INTACT upon arrival?
K
Received ON WET ICE?
?�
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
lC
VOLATILES rec'd WIOUT HEADSPACE?
PROPER CONTAINERS used?
,
TEMP: Therm ID: Te is Observed 3. v °C /Corr,
`33C
Phone: Z2 'T --0 9 o v%ov L Fax (Ye H Purchase Order No.IBl,iing Reference
Email Address: Cl es- �Q I P-L Yrl g � , e0)" Requested Due Date U 1 Day ❑ 2 Days ❑ 3 Days L7 4 Days Days
Woro Mdust Be
EDD Type: PDFJ�_ ExcelOther "Working Days" ❑ 6-9 Days ❑ Standard 10 days J Rush Approved
7'L - O 0 pp
Site Location Name: �_ Samples received after 14:00 will be processed next business day.
TO BE FILLEDIN BY CLIENTISAMPLING PERSONNEL
Certification: NELAC FL NC )(
SC OTHER NIA
Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT)
Water Chlorinated: YES— NOi
Sample Iced Upon Collection: YES_. NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER, OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSIS REQUESTED
E7
rlr UU �Opv ��¢ t' [>\� REMARKS
�J �rZlhJ 4 `0 ��
//
ID NO.
*TYPE
SEE BELOW
NO.
SIZE
BotcC
ao
1130
sari
G o�
5
"`so �a:o s.
x
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"IM ov t1ol D
01
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J*),30
Soy'[
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X
X
�
719 1 ONddinD
�Z
Sampler's Signature Sampled By (Print Name) Jot �7'1'tp LO*-Z- Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be LAB UsE= ONLY
submitted In writing to the Waypoint Analytical Project Manager. There will be charges for any changes after analyses have been initialized.
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Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LAaoRATORy, COC Group No,
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
t ?o Mileage:
j
❑ Fed Ex O UPS 7 Hand -delivered J Waypoint Analytical Field Service ❑ Ddier 00
7
NPDES: UST: TER
GROLID FILL OTHER:
D SWATER: O
❑ N1CK
NCU ❑ SC NC JI SCTE'
NCB ❑ SC I ❑❑ NCN ❑ SC ❑ NC a SC I NC ❑ SC
❑ NC ❑ SC I ❑❑ NC ❑ SC lu
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aceAnalytical
Report of Analysis
Waypoint Analytical
PO Box 240543
Charlotte, NC 28224
Attention: Angela Overcash
Project Name: 0070375
Lot Number:VH2O064
Date Completed:08/26/2020
C Z' r, I - (714- —
08/28/2020 11:59 AM
Approved and released by:
Project Manager II: Lucas Odom
A&B
ANSf NalfO�kT*iG�1yfM� $CBrP
A C C R E D I T E D
FETING LAROPATOMW
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Waypoint Analytical
Lot Number: VH2O064
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: VH2O064
Sample Number Sample ID Matrix Date Sampled Date Received
001 Backfill-CM Solid 07/30/20201130 08/20/2020
002 Backfill-DH Solid 07/30/20201230 08/20/2020
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

PACE ANALYTICAL SERVICES,
LLC
Detection Summary
Waypoint Analytical
Lot Number: VH2O064
Sample Sample ID
Matrix Parameter Method
Result Q Units Page
001 Backfill-CM
002 Backfill-DH
Solid Hexavalent Chromium 7199
Solid Hexavalent Chromium 7199
5.9 mg/kg 5
3.0 mg/kg 6
(2 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Client: Waypoint Analytical Laboratory ID: VH2O064-001
Description: Backfill-CM Matrix: Solid
Date Sampled:07/30/2020 1130 % Solids: 89.7 08/21/2020 0050
Date Received:08/20/2020
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 3060A (Hexavalent C) 7199 1 08/25/2020 1808 AMR 08/21/2020 1343 64298
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexavalent Chromium
18540-29-9 7199 5.9 1.1 0.22 mg/kg 2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client: Waypoint Analytical Laboratory ID: VH2O064-002
Description: Backfill-DH Matrix: Solid
Date Sampled:07/30/2020 1230 % Solids: 87.9 08/21/2020 0050
Date Received:08/20/2020
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 3060A (Hexavalent C) 7199 1 08/25/2020 1821 AMR 08/21/2020 1343 64298
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexavalent Chromium
18540-29-9 7199 3.0 1.1 0.23 mg/kg 2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
wI
Ah1ALYTiCAL
S><iWONTRACT ORDER
14
w6fiaadon: NELACT�SACP
a lain# 2knnlysical VC. z SC Other
0070375 - - —
SLNDlilfl oitAmn}`r 1 ECE1V1XGLALIQRATfiTk'i'-
1'lappointAna. uti al
Priee P lalybuid Service3, LLC (Shealy)
R, 0- Box 29fl543
106 WvMge Point )give
Chw[OM-,NC 25221-0543
WMC:elum�ia, 5C 29172
Phone: 812D-52M364
P} artc ;(8D3) 791-970U
Pax' 7%14-525.64-79
7aa: M 3) 67? {Y75
PraJera Mara""; A.-i�*cla D, Oumltsh Nccd v day TAT
Amply s 11ur J P.Ineg Laboratory IR
Odor menu
5arnpp; ID: UII'ii1375 Ul Sollu 40rolded:071JW2(p 11:M Backfill-CM
Pernwdeml i�jl7a "?T'Dr]U=t7 tSV 19 Q7111i IZ3Q
i+
4.2w--w2gf')',F 6 Iq2,,--
Sarupiv ]1)- 4E70375-02 Solid KAMPIC&Or- 3Q12Q 12;34 Saek1116D11
Aetiavalenl tvons;uui by F1ik1 ll-f +:M 12:34
r nnl uxxrs sNi7liee.-
cJor' l
aNd
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
:31isrry Lnrimmmamtpl 6mrkv% :nc.
1]fl4WrbMLXumper, Mf'041SC- u
Slir"Ple Receipt Checklist (SRC r-7cvlive UKLK F,r2r3uLx
Client: WAYPOINT C.`ooler 1 er-LcO by/date: AILD { N1 0? i)20 Lull 9'I12�0{r
Meads c*freceipt: m fiN1ST C�licnt © UPS Q FedE, OEl:er:
[0 Yef 7 No 1. W�;rc custady seals preseu[ uu the cagier?
Yes Nu LIA 2. If .i,sN�d seals �atr reser,r, �,verc Hye irtatct and unbroken?
pH Strip ID: 1�A _ Chlorine Svip Ti). NA Tested ; }tHU
Original u7nporature upon rcacipt l Derived (COEItm;w(),le,nperaturo tipal Mv6pt %cholid SAfairCup ID: 20-1342
2.0 {2.0 C hFA {NA NA ?A'A ¢C NA ?NA aC
Lmethod: ZTe:t4wrature Blank L]Agaimi Botdos [I{ Crutl .ID: 5 1R Gn-1 Corr"an Factor: 0 °C
Metlxxl of caolarlt: 0 Wet loa LJ lce R lCkg 0 Dry Tra None
Yens Q Nor ®NA if tc,nperatnrc or uuy t unlrr eaedcd t.0°C, vva Fmjewt Is+ianager �afed'7
PM was NuliE'Lcd by: phorte I email { Cwx-ripface (circ'e aafej
Yes ❑ -) 21NA d_ Js the cornnemial caat`ar's peckin Alip attached to ih-s form?
❑ TI5 WC3-e pj)RGF cust.3cy FM-nopchtres (relinquishcxvrcrrived) follovicd?
ff Yes N 0 6. W:!rc sample 1D.4 li sted 0n the COC r?
® Yes ❑ Ne 7. Wise sample IDs li sted on all sainp [t cap ine ? -
Yes T j—N—G 8. "AlEts eolh tian date & time fisted an tine C.002
❑ Yes ❑ 1Vn 9, Was 1201[cctiork date & tune listt:d on al[-;aMpic c-artaivcn ?
❑ Yes ❑ No 10. D rd all oantainwr label hifbi a3w ior_ (ID, &tr, time) ggrcc with the COC?
Yes —ff No i i_ Were tuts to be performed Ilstbd on the C0C7
m Yet ❑ No 12. DId a]I auv.ples ar. ire: in the fur, ooatainers far each Jv5# andlnr itl food condilkm
{unbmken, li4s on, ctc.)F
YPI: ❑ No 13. Wei Mloq K9re swrlplr. volume available19 � -
Yt:w DNo 1$.Wtrt:aJlvm1csrcccivedtivit{,in:�#Ileh�ldingtitnta,r[R=tp�rs,kvhichevaloamesfir5�?
�ca No IN, WEL'e an :la: IL:s cal-Minefs,rnissing'excess (circle one) samples Nat IisteJ ❑n C{ a
�J Yes ❑ �� ! NA ld_ For VOA and R9K-177-jurnph:s, were babbles presrtt[ `"pea siz$" (Ya1 air nmm in diameter)
In ally ML [he V0A v[als?
ElYes Na NA ] 7, V�'ere z11 I ItC]u'mc lafrtstt-ietu sitMpJc� Jrmived al. a pH of <2?
Yes N ®NA I ki, Were all cyaltide wmiles rr+xivud at a p, i 12 and suI�tde samples jruvivcd a. aEl
❑ Yes ,
❑ Na A !9. cre all allnlicalsle N +'fKNlcyaril �plrcna ?525 (- ,Brae/]+) MELIPIM ;rec a residual
Ch lckrh Le?
❑ Ycs ❑ n HA 20. W111 client rernarksirmticsts (i.e_ requ,4sted Jiha6ns, IviS?,MSD design, ti-DM, eta...)
cxurectly uanscribcd f xin the COC into the coil]nlerrt sectiotL in LtMS'?
t�la 21. %Vas this uote number liF.teti an t]]v ountainer labc]? Ir sty, rote g NA
r2Mp12 PrWacrvatin0 Want be mrlPlutvd for any swnpl48) incorrectly u,rRervr..d or with hum:[space.)
is nple(S NA were reoei4%d incorrectly pros wrvsd and were adjusted according[,
n ,sample receiving with NA mL of circle one: US043 HNO3, HC1, NaON using Sit # -NA
'i mt, of preservation NA T m oro tlsan 9310 pre%—Htive it flooded, pl-mm note in the com rm!Tits bejuw,
;) NA WOM receiYEN I with bubblcs -#6
rnm m diameter.
Cs) hTl1 _ wcfc rece [wd with €92 C > OS rrtg{L (If # 19 is � o) and were
accorrlin lv ilt "J [.tplo receiving v+'ikh suditutt lhiosulfate (N,r2S2O.,) with Sliaary [L)- NA
har-Me. labels applied by..AHD
C[1ro rrttmnty
Date, MW2020
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
Sent Via E-mail
Mr. Scott Carr
ATCO
Camp North End
300 Camp Road
Charlotte, North Carolina 28206
scott&camp.nc
NORTH CAROLINA
Environmental Quality
September 8, 2020
Subject: Brownfields Soil Management Options- Import Approval
Camp North End
Rite Aid & Former Charlotte Army Missile Plant Brownfields Properties
Charlotte, Mecklenburg County
Brownfields Project No. 20050-16-060 & 11044-07-060
Dear Mr. Carr:
The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received
a request to import and use recycle crushed concrete as beneficial fill at the Camp North End
(CNE) Brownfields Property. DEQ Brownfields reviewed the analytical data provided in the Soil
Management Options: Import of Recycled Crushed Concrete letter report dated September 2, 2020
prepared by Hart & Hickman and additional project information in the Environmental
Management Plan (EMP) approved and dated (revised) March 28, 2019.
Based on our review of the data, DEQ Brownfields approved the import of crushed concrete from
the two facilities: C&M Recycling facility located at 2930 Jeff Adams Drive, Charlotte, NC and
DH Griffin Companies located at 11205 Reames Road, Charlotte, NC. Note that imported
concrete should be from stockpiles that were previously sampled as part of assessment activities.
All import must be conducted under a DEQ Brownfields approved EMP. If unanticipated impacts
are identified during import process, please refer to the EMP for further actions and cease transfer
until appropriate characterization can be completed. In addition, in accordance with the CNE
EMP, an annual Redevelopment Summary Report will be submitted to DEQ Brownfields. Details
related to the disposition of this import including but not limited to, total volume, general
description of field screening efforts, etc. should be included with the Redevelopment Summary
Report.
NORTHCAROLINAD_E Q��
Oepriament of Environmental Quality
North Carolina Department of Environmental Quality I Division of Waste Management
217 West Jones Street 1 1646 Mail Service Center I Raleigh, North Carolina 27699-1646
919.707.8200

September 8, 2020
Page 2
Please be advised that this approval does not waive any applicable requirement to obtain any
necessary permits, licenses or certifications which may be required from other state or local
entities. If you have questions about this correspondence or require additional information, please
feel free to contact Jordan Thompson by phone at 704-223-6549 or by email at
j ordan. thomp s ongnc deny. gov.
Sincerely,
a ez ,
Jordan Thompson
Interim Supervisor
Brownfields Property Management Unit
ec: Matt Ingalls, Hart & Hickman, PC
Doug Pierotti, City of Charlotte, dpierotti&ci.charlotte.nc.us
Jim Keenan, ATCO, jim&keenanps.com
Carolyn Minnich, DEQ