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HomeMy WebLinkAboutMO-4471_14645_CA_MRP_20200528_Groundwater Monitoring Letter Report;ETC May 28, 2020 7606 Whitehall Executive Dr. Suite 800 Charlotte, NC 28273 Tel: 704-529-3200 Fax: 704-529-3272 www.atcassociates.com N.C. Enaineerina License No. C-1598 Ms. Trudy Beverly North Carolina Department of Environmental Quality Mooresville Regional Office Division of Waste Management - Underground Storage Tank Section 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 Re: Groundwater Monitoring Update Letter Report Circle K Store No. 8387 Phillips 66 Company RM No. 2751 8425 Highway 49 North Mt. Pleasant, Cabarrus County, North Carolina 28124 Facility ID No. 0-004529 NCDEQ Incident No. 14645 Risk Classification: High (380D) ATC Project No. P662751014 Dear Ms. Beverly: On behalf of Phillips 66 Company (P66), ATC Associates of North Carolina, P.C., (ATC) has performed environmental consulting services for the Circle K Store No. 8387 (Phillips 66 Risk Management [RM] No. 2751) facility. The site is located at 8425 Highway 49 North, Mt. Pleasant, North Carolina. The property consists of an active single -story convenience store building and retail gasoline distribution system, which includes three underground storage tanks (USTs), dispensing pumps, and associated piping. The site is mostly covered by asphalt and concrete pavement with landscaped areas located on the northern part of the property. Figure I shows the site location on a topographic map, and a site map showing the locations of the monitoring wells and remediation wells is included as Figure 2. ATC is pleased to submit this report documenting sampling results for site monitoring wells to monitor the results of prior installation of Regenesis Oxygen Releasing Compound Advanced Filter Socks® (ORC socks) in select monitoring wells at the site. Background An initial round of ORC socks were installed in wells GWO 1, GW04, GW05 and GW 14D on January 5, 2018. Previous groundwater monitoring events had indicated the presence of ethylene dibromide (EDB) in wells GWO1, GW04 and GW05 at concentrations slightly above the North Carolina Title 15A, NCAC, Subchapter 2L, Part .0202 Standards (2L Standards). ORC socks were installed in well GW 14D due to a historical presence of MTBE at concentrations that were NCDEQ Phillips 66 RM No. 2751 Ms. Trudy Beverly May 28, 2020 Incident: 14645 Page 2 near the 2L Standard. Groundwater monitoring conducted in 2018 after the installation of the ORC socks showed that EDB concentrations in wells GWO1, GW04 and GW05 had decreased to concentrations below the 2L Standard. However, benzene concentrations in well GW02 increased to above the 2L Standard. Therefore, on January 3, 2019, ATC installed ORC socks in well GW02. On December 12, 2020, ATC replaced ORC socks in wells GWOI, GW02, GW04, GW05, and GW 14D. This report present the results of groundwater monitoring conducted on April 1, 2020 to monitor ORC progress and natural attenuation of residual impact at the site. Groundwater Monitoring On March 31, 2020, 16 site monitoring wells (GWO1, GW02, GW03A, GW04, GW05, GW06, GW07, GWO8, GW09D, GW 10, GW 11, GW 12, GW 13D, GW 14D, GW 15, and GW 15D) were gauged for depth to groundwater and checked for the presence of light non -aqueous phase liquid (LNAPL) prior to sample collection. An oil/water interface probe was used to gauge each well. No LNAPL was present at the time of gauging and sampling. Since the nearby municipal water supply well (WSW) is not in operation, ATC did not collect a WSW sample. Groundwater elevations were then calculated based on top of casing (TOC) elevations, which are referenced to an arbitrary on -site benchmark of 100.00 feet. Well construction details for site monitoring wells are summarized in Table 1. The locations of the monitoring wells are shown in Figure 2, and the groundwater elevation data are summarized in Table 2. Based on the results of the depth to groundwater measurements, the groundwater flow direction was generally to the south and southeast, consistent with previous site information. A groundwater elevation contour map is included as Figure 3. Upon completion of the well gauging activities, groundwater samples were collected from 15 site monitoring wells (GWO1, GW02, GW03A, GW04, GW05, GW06, GW07, GWO8, GW09D, GW 10, GW 12, GW 13D, GW 14D, GW 15, and GW 15D) on A, 2020. Monitoring well GW 11 was unable to be sampled due to an insufficient amount of groundwater within the well. The groundwater samples were collected in laboratory supplied, preserved containers; placed on ice; and shipped in accordance with chain -of -custody protocol to North Carolina -accredited laboratory, SGS Acutest Laboratories, in Orlando, Florida. The groundwater samples were analyzed by EPA Method 6200B for volatile organic compounds including the following petroleum constituents: benzene, toluene, ethylbenzene, total xylenes (BTEX), methyl tertiary butyl ether (MTBE), isopropyl ether (IPE), ethylene dibromide (EDB) and naphthalene. The laboratory report for the April 2020, sampling event is included in Appendix A. Current groundwater analytical results are summarized in Table 3, and historical groundwater analytical results are compiled in Table 4. The groundwater analytical results were compared to the North Carolina 2L Standards and the Gross Contamination Levels (GCLs). Groundwater analytical results indicate the following: • LNAPL was not identified in the gauged and sampled monitoring wells during the event; • The GCLs were not exceeded for any analyzed compound during the event; NCDEQ As. Trudy Beverly Incident: 14645 Phillips 66 RM No. 2751 May 28, 2020 Page 3 • The groundwater sample collected from monitoring well GW02 contained a benzene concentration of 1.2 micrograms per liter (ug/L), exceeding the North Carolina 2L Standard of 1.0 ug/L; • Other petroleum related chemical constituents were detected in the sampled wells, however, at concentrations below their respective 2L Standards, Groundwater analytical results indicate that the ORC socks have been successful in reducing petroleum hydrocarbon concentrations in site wells. Based on the results of the Apri12020, groundwater sampling event, ATC recommends continued quarterly groundwater sampling events to monitor remedial progress of the xemedial socks and ongoing natural attenuation. If you have any questions or require additional information, please callus at (704) 529-3200. Sincerely, ATC Associates of North Carolina, P.C. Project Manager cc: Mr. Ed Kuhn, Contract Program Manager for Phillips 66 v FIGURES D(M SITE)"/ � D - 1000 FOOT RADIUS o I f D J( ) � - ,0 j t D Dc D LATITUDE N 35' 24' 39" LONGITUDE W 80' 26' 06" UTM COORDINATES: ZONE 17 551275E 3918556N 0 2,000 4,000 NOTE: MAP PRODUCED USING 7.5 MINUTE MOUNT PLEASANT, NORTH CAROLINA 2010 USGS QUADRANGLES APPROXIMATE SCALE IN FEET TITLE FIGURE 1 . SITE LOCATION MAP PHILLIPS 66 RM # 2751 tTc 8425 HIGHWAY 49 NORTH MOUNT PLEASANT, NORTH CAROLINA ASSOCIATES OF NORTH CAROLINA, P.C. Charlotte, Nate Carolina 28273 (704) 529-3200 FAX (704) 529-4272 CAD FILE RMR2751 topo_20110722 PREP. BY AD REV. BY FL AS SHOWN DATE 2.3.16 PROJECT NO. 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PLEASANT, NORTH CAROLINA Well Type Well Diameter (inches) Slot Size (inches) Total Well Depth (feet) Screen Interval (feet) Top of Casing Elevation GWO1 II 2 0.020 30 10-30 95.55 GW02 II 2 0.020 28 8-28 97.07 GW03A II 2 0.010 30 3-30 96.89 GW04 II 2 0.020 30 10-30 95.58 GW05 II 2 0.020 27.5 7.5-27.5 96.05 GW06 II 2 0.010 25 5-25 97.37 GW07 II 2 0.010 20 5-20 96.02 GW08 II 2 0.010 17.5 5-17.5 96.18 GW09D III 2 0.020 45.5 40.5-45.5 95.49 GW 10 II 2 0.010 20 5-20 93.90 GW11 11 2 0.010 30 5-30 99.08 GW 12 II 2 0.010 24 4-24 97.51 GW13D III 2 0.010 75 70-75 95.89 GW 14D III 2 0.010 76 71-76 96.93 GW15 11 2 0.010 30 5-30 96.29 GW 15D III 2 0.010 85 70-85 96.24 VWO1 II 4 0.010 14 4-14 95.84 SW-1 supply 6.25 NA 445 NA 154.36 SW-2 Sun* 6.25 NA 453 NA 145.06 WSW-1 supply 6.25 NA 435 NA 99.87 WSW-2 I Su 1 6.25 NA 387 NA 114.85 Notes: 1. Elevations are referenced to an arbitrary on -site benchmark of 100.00 feet. 2. NA = Not Available. 3. Total well depths measured from top of casing. 4. Monitoring well GW03A replaced GW03. 5. Monitoring wells GWl 1 and GW12 were installed on March 23, 2004. 6. Monitoring wells GW13D, G1413, GW15, and GW15D were installed on March 1-2, 2005. 7. Supply well construction information is based on information given from owners/users. Page 1 of 1 TABLE2 HISTORICAL GROUNDWATER ELEVATION DATA CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Monitoring Well Gauging Date Top of Casing Elevation (feet) Depth to Water (feet) Groundwater Elevation (feet) Temperatureo C Conductivity (mS/em) DO (mg/L) pH ORP GWO1 7/9/2008 95.55 10.99 84.56 12/16/2008 13.85 81.70 6/10/2009 7.74 87.81 12/29/2009 6.45 89.10 6/29/2010 8.20 87.35 3/15/2011 6.81 88.74 6/8/2011 8.10 87.45 19.85 0.372 3.06 6.34 114.8 12/7/2011 7.95 87.60 19.97 0.49 2.05 1 6.53 159.7 3/22/2012 8.32 87.23 20.67 0.459 1.23 6.99 217.4 6/7/2012 10.38 85.17 12/11/2012 11.46 84.09 21.06 0.527 3.34 6.37 59 3/11/2013 9.12 86.43 6/27/2013 7.72 87.83 9/30/2013 13.11 82.44 12/19/2013 8.40 87.15 5/28/2014 7.11 88.44 12/9/2014 8.75 86.80 6/29/2015 11.34 84.21 12/28/2015 6.34 89.21 3/22/2016 7.16 88.39 7/6/2016 7.79 87.76 9/14/2016 8.21 87.34 12/28/2016 9.70 85.85 3/21/2017 7.93 87.62 7/26/2017 8.60 86.95 1/12/2018 8.14 87.41 4/19/2018 6.79 88.76 11/6/2018 9.90 85.65 3/26/2019 12.02 83.53 8/22/2019 14.90 80.65 12/12/2019 15.49 80.06 3/31/2020 13.57 81.98 GW02 7/8/2008 97.07 15.11 81.96 12/16/2008 19.17 77.90 6/9/2009 12.34 84.73 12/28/2009 11.29 85.78 6/29/2010 11.93 85.14 3/15/2011 12.27 84.80 6/9/2011 10.42 86.65 18.92 0.415 2.17 6.5 -104.4 12/7/2011 10.33 1 86.74 20.01 1 0.525 2.2 6.68 1 -92.6 3/22/2012 9.91 87.16 20.35 0.76 3.2 6.92 87.6 6/7/2012 17.28 79.79 12/11/2012 16.71 80.36 18.98 0.557 3.28 6.4 74 3/11/2013 18.50 78.57 6/27/2013 10.05 87.02 10/1/2013 15.29 81.78 12/19/2013 15.21 81.86 5/28/2014 6.79 90.28 - - - - - 12/9/2014 11.28 85.79 6/29/2015 6.12 90.95 12/28/2015 3.70 93.37 7/5/2016 6.05 91.02 9/13/2016 7.25 89.82 12/28/2016 8.14 88.93 3/21/2017 5.70 91.37 7/26/2017 6.25 90.82 1/12/2018 6.95 90.12 4/19/2018 5.44 91.63 11/6/2018 4.90 92.17 3/26/2019 6.11 90.96 8/22/2019 6.52 90.55 12/12/2019 7.62 89.45 3/31/2020 6.76 90.31 Pagel of8 TABLE2 HISTORICAL GROUNDWATER ELEVATION DATA CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Monitoring Well Gauging Date Top of Casing Elevation (feet) Depth to Water (feet) Groundwater Elevation (feet) Temperatureo C Conductivity (mS/cm) DO (mg/L) pH ORP GW03A 7/10/2008 96.89 6.15 90.74 12/16/2008 5.70 91.19 6/10/2009 6.12 90.77 12/29/2009 5.57 91.32 6/29/2010 3.59 93.30 3/15/2011 3.13 93.76 6/9/2011 4.57 92.32 20.11 0.638 2.43 6.77 d233.3 12/7/2011 3.07 93.82 20.14 0.59 1.88 6.79 3/22/2012 3.92 92.97 18.41 0.816 1.51 6.92 6/7/2012 4.07 92.82 12/11/2012 6.74 90.15 20.37 1 0.564 5.02 1 6.34 65 3/11/2013 3.80 93.09 6/27/2013 3.58 93.31 9/30/2013 4.08 92.81 12/19/2013 3.19 93.70 5/28/2014 3.84 93.05 12/9/2014 3.74 93.15 6/29/2015 5.61 91.28 12/28/2015 2.36 94.53 3/22/2016 3.87 93.02 7/6/2016 4.52 92.37 9/14/2016 4.49 92.40 12/28/2016 4.68 92.21 3/21/2017 4.04 92.85 7/26/2017 3.98 92.91 1/12/2018 4.57 92.32 4/19/2018 3.60 93.29 11/6/2018 2.70 94.19 3/26/2019 3.68 93.21 8/22/2019 7.12 89.77 12/12/2019 4.72 92.17 3/31/2020 3.85 93.04 GW04 7/10/2008 95.58 9.46 86.12 12/16/2008 8.92 86.66 6/9/2009 7.17 88.41 12/29/2009 7.23 88.35 6/29/2010 8.61 86.97 3/15/2011 6.81 88.77 6/8/2011 4.22 91.36 19.7 0.418 2.97 7.41 79.6 12/7/2011 6.39 89.19 20.84 1 0.5 2.54 1 6.7 163 3/22/2012 7.00 88.58 20 0.532 1.88 6.94 233.3 6/7/2012 7.94 87.64 12/11/2012 9.75 85.83 20.25 0.508 8.42 6.54 -2 3/11/2013 7.22 88.36 6/27/2013 6.76 88.82 9/30/2013 6.73 88.85 12/19/2013 6.94 88.64 5/28/2014 6.00 89.58 12/9/2014 6.82 88.76 6/29/2015 8.39 87.19 12/28/2015 4.78 90.80 3/22/2016 6.58 89.00 7/6/2016 6.80 88.78 9/14/2016 6.88 88.70 12/28/2016 7.63 87.95 3/21/2017 6.74 88.84 7/26/2017 6.91 88.67 1/12/2018 7.28 88.30 4/19/2018 6.15 89.43 11/6/2018 8.52 87.06 3/26/2019 7.81 87.77 8/22/2019 12.40 83.18 12/12/2019 10.02 85.56 3/31/2020 8.85 86.73 Page 2 of 8 TABLE2 HISTORICAL GROUNDWATER ELEVATION DATA CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Monitoring Well Gauging Date Top of Casing Elevation (feet) Depth to Water (feet) Groundwater Elevation (feet) Temperatureo C Conductivity (mS/cm) DO (mg/L) pH ORP GW05 7/9/2008 96.05 14.48 81.57 12/16/2008 15.73 80.32 6/9/2009 8.91 87.14 12/28/2009 7.59 88.46 6/29/2010 8.80 87.25 3/15/2011 8.63 87.42 6/8/2011 9.03 87.02 18.78 0.316 2.83 8.76 44.7 12/7/2011 9.83 86.22 19.7 0.338 3.4 6.76 161.5 3/22/2012 9.87 86.18 19.72 0.383 2.65 6.06 232 6/7/2012 12.87 83.18 12/11/2012 13.45 82.60 21.46 1 0.316 8.12 1 6.4 16 3/11/2013 10.96 85.09 6/27/2013 9.26 86.79 9/30/2013 9.71 86.34 12/19/2013 10.23 85.82 5/28/2014 7.88 88.17 12/9/2014 9.95 86.10 6/29/2015 10.05 86.00 12/28/2015 7.22 88.83 3/22/2016 7.97 88.08 7/5/2016 8.84 87.21 9/13/2016 9.50 86.55 12/28/2016 11.55 84.50 3/21/2017 9.09 86.96 7/26/2017 9.19 86.86 1/12/2018 9.13 86.92 4/19/2018 8.82 87.23 11/6/2018 11.68 84.37 3/26/2019 16.35 79.70 8/22/2019 16.30 79.75 /12/2019 23.55 72.50 31/2020 P 21.25 74.80 GW06 7/9/2008 97.37 7.5* 89.87 12/10/2008 18.38 78.99 6/10/2009 6.36 91.01 12/28/2009 NM NM 6/29/2010 7.07 90.30 3/15/2011 6.31 91.06 6/8/2011 8.43 88.94 18.56 0.15 2.38 5.28 187.3 12/7/2011 6.66 90.71 18.63 0.15 1.6 1 5.45 167.2 3/22/2012 6.86 90.51 17.23 0.145 3.65 6.37 209.2 6/7/2012 7.75 89.62 12/11/2012 13.77 83.60 20.13 0.144 6.82 4.95 159 3/11/2013 6.36 91.01 6/27/2013 6.56 90.81 9/30/2013 7.98 89.39 12/19/2013 6.54 90.83 5/28/2014 7.55 89.82 12/9/2014 6.34 91.03 6/29/2015 7.98 89.39 12/28/2015 5.86 91.51 3/22/2016 6.79 90.58 7/5/2016 7.94 89.43 9/13/2016 8.16 89.21 12/28/2016 9.01 88.36 3/21/2017 6.75 90.62 7/26/2017 7.82 89.55 1/12/2018 7.90 89.47 4/19/2018 6.52 90.85 11/6/2018 6.82 90.55 3/26/2019 7.09 90.28 8/22/2019 6.98 90.39 12/12/2019 7.19 90.18 3/31/2020 6.93 90.44 Page 3 of 8 TABLE2 HISTORICAL GROUNDWATER ELEVATION DATA CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Monitoring Well Gauging Date Top of Casing Elevation (feet) Depth to Water (feet) Groundwater Elevation (feet) Temperatureo C Conductivity (mS/cm) DO (mg/L) pH ORP GW07 7/10/2008 96.02 8.06 87.96 12/16/2008 7.68 88.34 6/10/2009 5.13 90.89 12/29/2009 5.25 90.77 6/29/2010 5.39 90.63 3/15/2011 5.01 91.01 6/8/2011 5.84 90.18 21.15 0.678 2.85 6.73 d223.1 12/7/2011 5.45 90.57 20.82 0.709 2.46 6.87 3/22/2012 5.97 90.05 19.5 0.663 3.17 7.03 6/7/2012 7.54 88.48 12/11/2012 8.19 87.83 22.61 1 0.669 8.09 1 6.64 -54 3/11/2013 6.90 89.12 6/27/2013 5.15 90.87 9/30/2013 5.83 90.19 12/19/2013 5.56 90.46 5/28/2014 5.06 90.96 12/9/2014 5.71 90.31 6/29/2015 6.68 89.34 12/28/2015 4.40 91.62 3/23/2016 4.24 91.78 7/6/2016 5.70 90.32 9/14/2016 5.49 90.53 12/28/2016 6.65 89.37 3/21/2017 6.04 89.98 7/26/2017 5.85 90.17 1/12/2018 6.55 89.47 4/19/2018 5.23 90.79 11/6/2018 4.42 91.60 3/26/2019 6.91 89.11 8/22/2019 8.40 87.62 12/12/2019 8.54 87.48 rffati 7.80 88.22 GW08 7/9/2008 96.18 8.15 88.03 12/16/2008 8.10 88.08 6/10/2009 6.72 89.46 12/29/2009 6.82 89.36 6/29/2010 7.21 88.97 3/15/2011 6.29 89.89 6/9/2011 5.74 90.44 19.71 0.968 2.88 6.48 -26.9 12/7/2011 5.36 90.82 19.44 0.846 2.53 1 6.42 120.1 3/22/2012 5.75 90.43 19.2 1.109 1.83 6.68 194.6 6/7/2012 7.15 89.03 12/11/2012 7.88 88.30 21.41 0.705 8.32 6.48 47 3/11/2013 5.60 90.58 6/27/2013 5.15 91.03 9/30/2013 5.65 90.53 12/19/2013 5.23 90.95 5/28/2014 5.09 91.09 12/9/2014 5.47 90.71 6/29/2015 6.59 89.59 12/28/2015 5.30 90.88 3/23/2016 5.29 90.89 7/6/2016 5.87 90.31 9/14/2016 6.08 90.10 12/28/2016 6.30 89.88 7/26/2017 5.61 90.57 12/12/2019 9.36 86li2 3/31/2020 8.26 87.92 Page 4 of 8 TABLE2 HISTORICAL GROUNDWATER ELEVATION DATA CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Monitoring Well Gauging Date Top of Casing Elevation (feet) Depth to Water (feet) Groundwater Elevation (feet) Temperatureo C Conductivity (mS/cm) DO (mg/L) pH ORP GW09D 7/9/2008 95.49 10.66 84.83 12/10/2008 16.58 78.91 6/10/2009 7.65 87.84 12/29/2009 6.90 88.59 6/29/2010 12.41 83.08 3/15/2011 4.19 91.30 6/8/2011 7.31 88.18 20.73 0.9 2.84 6.69 d222,6 12/7/2011 7.50 87.99 19.43 0.412 1.24 6.68 3/22/2012 8.20 87.29 24.07 0.019 6.63 6.81 6/7/2012 9.82 85.6712/11/2012 11.01 84.48 20.28 0.464 2.34 6.47 5 3/11/2013 11.10 84.39 6/27/2013 7.27 88.22 - - - - - 9/30/2013 7.92 87.57 12/20/2013 8.15 87.34 5/28/2014 6.59 88.90 12/9/2014 8.16 87.33 6/29/2015 8.60 86.89 12/28/2015 7.06 88.43 7/6/2016 6.78 88.71 9/14/2016 7.79 87.70 12/28/2016 8.71 86.78 8/22/2019 8.75 86.74 /12/2019 13.47 82.02 31/2020 P 13.28 82.21 GW10 7/8/2008 93.90 NM NM 12/8/2008 NM NM 6/10/2009 NM NM 12/28/2009 NM NM 6/29/2010 NM NM 3/15/2011 8.12 85.78 6/8/2011 8.68 85.22 19.44 0.193 2.77 5.72 19.5 12/7/2011 8.96 84.94 21.45 0.23 1 1.5 6.45 1 51.6 3/22/2012 9.25 84.65 20.24 0.258 2.96 6.83 208.9 6/7/2012 10.01 83.89 12/11/2012 11.87 82.03 20.53 0.278 8.31 5.1 86 3/11/2013 9.68 84.22 6/27/2013 8.68 85.22 - - - - - 9/30/2013 9.32 84.58 12/19/2013 9.18 84.72 5/28/2014 7.68 86.22 12/9/2014 NM NM 6/29/2015 9.75 84.15 12/28/2015 5.02 88.88 7/5/2016 8.79 85.11 9/13/2016 9.04 84.86 12/28/2016 10.18 83.72 8/22/2019 14.60 79.30 12/12/2019 20.08 73.82 3/31/2020 15.01 78.89 Page 5 of 8 TABLE2 HISTORICAL GROUNDWATER ELEVATION DATA CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Monitoring Well Gauging Date Top of Casing Elevation (feet) Depth to Water (feet) Groundwater Elevation (feet) Temperatureo C Conductivity (mS/cm) DO (mg/L) pH ORP GWIl 7/9/2008 99.08 19.97 79.11 12/10/2008 24.38 74.70 6/10/2009 13.22 85.86 12/28/2009 NM NM 6/29/2010 11.33 87.75 3/15/2011 12.50 86.58 6/8/2011 13.09 85.99 19.57 0.071 7.34 5.24 203.9 12/7/2011 14.81 84.27 21.02 0.073 4.93 5.14 166.7 3/22/2012 14.25 84.83 20.66 0.092 4.87 5.81 237.2 6/7/2012 14.82 84.26 12/11/2012 Obstructed by Vehicle 3/11/2013 Obstructed by Vehicle 6/27/2013 14.91 84.17 - - - - - 9/30/2013 13.96 85.12 12/19/2013 14.28 84.80 5/28/2014 12.54 86.54 12/9/2014 14.22 84.86 6/29/2015 14.26 84.82 12/28/2015 11.22 87.86 7/5/2016 12.59 86.49 9/13/2016 13.21 85.87 12/28/2016 14.40 84.68 8/22/2019 24.88 74.20 12/12/2019 29.37 69.71 3/31/2020 29.07 70.01 GWl2 7/9/2008 97.51 16.63 80.88 12/8/2008 20.58 76.93 6/10/2009 11.34 86.17 12/28/2009 NM NM 6/29/2010 11.06 86.45 3/15/2011 10.81 86.70 6/8/2011 10.24 87.27 18.36 0.429 2.31 6.4 -16.7 12/7/2011 11.09 86.42 20.24 0.501 1 2.34 6.17 1 101.7 3/22/2012 9.56 87.95 18.15 0.317 9.72 6.02 216.9 6/7/2012 10.28 87.23 12/11/2012 15.04 82.47 20.01 0.504 7.9 6.05 115 3/11/2013 11.44 86.07 6/27/2013 10.85 86.66 - - - - - 9/30/2013 10.97 86.54 12/19/2013 9.47 88.04 5/28/2014 10.78 86.73 12/9/2014 7.81 89.70 6/29/2015 8.97 88.54 12/28/2015 8.99 88.52 7/5/2016 7.79 89.72 9/13/2016 8.75 88.76 12/28/2016 8.18 89.33 8/22/2019 20.20 77.31 12/12/2019 22.56 74.95 3/31/2020 18.78 78.73 Page 6 of 8 TABLE2 HISTORICAL GROUNDWATER ELEVATION DATA CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Monitoring Well Gauging Date Top of Casing Elevation (feet) Depth to Water (feet) Groundwater Elevation (feet) Temperatureo C Conductivity (mS/em) DO (mg/L) pH ORP GW13D 7/8/2008 95.89 6.52 89.37 12/15/2008 5.54 90.35 6/9/2009 3.78 92.11 12/29/2009 3.03 92.86 6/29/2010 8.36 87.53 3/15/2011 4.52 91.37 6/8/2011 7.08 88.81 19.83 0.441 2.24 7.28 -138.7 12/7/2011 3.44 92.45 17.8 0.498 0.83 9.13 1-151.5 12/7/2011 3.44 92.45 19.08 0.498 0.64 8.34 -101.5 12/7/2011 3.44 92.45 19.12 0.482 1.14 7.87 3/22/2012 3.96 91.93 20.32 0.513 0.6 6.83 198.9 6/7/2012 4.51 91.38 12/11/2012 NA NA 18.97 0.521 3.96 6.89 -72 3/11/2013 12.56 83.33 6/27/2013 3.85 92.04 10/1/2013 3.90 91.99 12/20/2013 3.88 92.01 5/28/2014 4.57 91.32 12/9/2014 4.41 91.48 6/29/2015 4.11 91.78 12/28/2015 2.16 93.73 3/23/2016 2.83 93.06 7/5/2016 4.49 91.40 9/13/2016 4.24 91.65 12/28/2016 4.58 91.31 8/22/2019 5.71 90.18 12/12/2019 5.34 90.55 3/31/2020 4.35 91.54 GW14D 7/8/2008 96.93 16.15 80.78 12/15/2008 19.66 77.27 6/9/2009 9.21 87.72 12/28/2009 7.80 89.13 6/29/2010 8.98 87.95 3/15/2011 9.36 87.57 6/9/2011 9.95 86.98 19.77 0.33 1.53 8.49 -232.5 12/7/2011 11.20 1 85.73 13.79 0.244 1 2.43 9.58 12/7/2011 11.20 85.73 17.04 0.427 2.97 8.77 -119.8 12/7/2011 11.20 85.73 17.34 0.401 1.74 8.06 -120.6 3/22/2012 11.57 85.36 19.77 0.509 2.95 7.12 201.6 6/7/2012 13.33 83.60 12/11/2012 14.42 82.51 18.86 0.523 8.29 6.8 50 3/11/2013 12.95 83.98 6/27/2013 11.11 85.82 10/1/2013 10.45 86.48 12/20/2013 11.06 85.87 5/28/2014 8.43 88.50 12/9/2014 11.03 85.90 6/29/2015 10.89 86.04 12/28/2015 8.88 88.05 3/23/2016 8.43 88.50 7/5/2016 9.62 87.31 9/13/2016 10.16 86.77 12/28/2016 12.62 84.31 3/21/2017 10.06 86.87 7/26/2017 9.14 87.79 1/12/2018 9.93 87.00 4/19/2018 8.19 88.74 11/6/2018 8.10 88.83 3/26/2019 22.36 74.57 8/22/2019 22.98 73.95 12/12/2019 29.75 67.18 3/31/2020 28.70 68.23 Page 7 of 8 TABLE2 HISTORICAL GROUNDWATER ELEVATION DATA CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Monitoring Well Gauging Date Top of Casing Elevation (feet) Depth to Water (feet) Groundwater Elevation (feet) Temperature° C Conductivity (MS/CM) DO (mg/L) pH ORP GW15 7/8/2008 96.29 13.04 83.25 12/10/2008 19.36 76.93 6/9/2009 8.84 87.45 12/28/2009 7.19 89.10 6/29/2010 8.07 88.22 3/15/2011 7.54 88.75 6/9/2011 8.61 87.68 18.84 0.144 8.19 5.21 d69.8 12/7/2011 8.07 88.22 18.05 0.147 6.25 8.17 3/22/2012 13.20 83.09 19.29 0.134 8.53 6.6 6/7/2012 15.48 80.81 12/11/2012 13.99 82.30 19.07 1 0.12 8.28 1 6.51 170 3/11/2013 7.73 88.56 6/27/2013 8.04 88.25 10/1/2013 12.91 83.38 12/19/2013 8.68 87.61 5/28/2014 7.19 89.10 12/9/2014 7.53 88.76 6/29/2015 8.34 87.95 12/28/2015 7.68 88.61 3/22/2016 6.24 90.05 7/6/2016 7.57 88.72 9/13/2016 8.41 87.88 12/28/2016 9.18 87.11 3/21/2017 6.93 89.36 7/26/2017 5.71 90.58 1/12/2018 8.02 88.27 4/19/2018 6.49 89.80 11/6/2018 7.81 88.48 3/26/2019 13.26 83.03 8/22/2019 12.73 83.56 12/12/2019 21.05 75.24 3/31/2020 19.58 76.71 GW15D 7/8/2008 96.24 26.56 69.68 12/15/2008 35.10 61.14 6/9/2009 25.83 70.41 12/28/2009 18.66 77.58 6/29/2010 14.00 82.24 3/15/2011 6.21 90.03 6/9/2011 9.00 87.24 20.11 0.513 1.67 8.25 -145 12/7/2011 15.15 81.09 18.89 1 0.409 0.89 1 10.36 -161.2 12/7/2011 15.15 81.09 17.17 0.389 1.1 9.93 -171.4 12/7/2011 15.15 81.09 16.89 0.376 0.97 9.85 -185.4 3/22/2012 15.61 80.63 20.5 0.391 1.02 7.48 178.3 6/7/2012 27.10 69.14 12/11/2012 11.15 85.09 19.08 0.338 8.48 8.35 -35 3/11/2013 11.48 84.76 6/27/2013 6.41 89.83 10/1/2013 NM 12/20/2013 30.88 65.36 - - - - - 5/28/2014 3.67 92.57 12/9/2014 0.79 95.45 6/29/2015 6.44 89.80 12/28/2015 12.26 83.98 7/6/2016 9.14 87.10 9/13/2016 18.34 77.90 12/28/2016 6.85 89.39 3/21/2017 2.80 93.44 7/26/2017 4.20 92.04 1/12/2018 4.36 91.88 4/19/2018 2.35 93.89 11/6/2018 NM 3/26/2019 0.80 95.44 8/22/2019 NA NA 12/12/2019 6.00 90.24 3/31/2020 39.69 56.55 Notes: 1. Elevations are ref enced to an arbitrary on -site benchmark of 100.00 f t. 2. Total well depths measured from top of casing. 3. Depth to water measured from top of casing. 4. NM = Not Measured. 5. -Anomalous depth to groundwater. Page 8 of 8 TABLE 3 CURRENT GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE No. 8387 RM No. 2751 8425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA Sample Sample s s o o o o � E o ^� Location Date 10 A U p u v t u A N 7 o o S. o y F+ U W o w O O W U �% N ..7110 A P? o A A A N u u F. � o o C A O i O c O N ^� Q. CE U �". .--I N --I c CC o. O '};,i 'yw N v� M FQ H W H ri W Z O' U �--i ri .r U I� H H ri ri U CQ A CQ Q NC 2L Standard -T 1 600 600 500 20 70 0.02 6 70 70 50 6 0.4 7 70 100 70 5 3 2,000 400 400 0.03 70 4 0.4 -- 6,000 --- -- GW0l 4/1/20 <0.13 <0.13 <0.13 <0.25 4.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.17 J <1.0 0.18 J 2.6 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW02 4/1/20 1.2 0.19 J 0.15 J 0.89 J 1.1 0.56 <0.13 <0.13 <0.13 0.44 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 2.1 <1.0 <0.13 <0.20 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <5.0 <0.20 GW03A 4/1/20 <0.13 <0.13 <0.13 <0.25 5.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 0.21 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW04 4/1/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 3.8 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW05 4/1/20 <0.13 <0.13 <0.13 <0.25 0.75 0.33 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 <0.20 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW06 4/1/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 <0.20 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW07 4/1/20 <0.13 <0.13 <0.13 <0.25 3.8 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 0.44 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW08 4/1/20 <0.13 <0.13 <0.13 <0.25 6.8 1.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 <0.20 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW09D 4/1/20 <0.13 <0.13 <0.13 <0.25 2.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.19 J <0.13 <0.13 <1.0 0.46 J 10.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW10 4/1/20 <0.13 <0.13 <0.13 <0.25 0.14 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 <0.20 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW11 4/1/20 Not Sampled - Insufficent water to sample GW12 4/1/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 <0.20 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW13D 4/1/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 1.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW14D 4/1/20 <0.13 <0.13 <0.13 <0.25 16.2 0.16J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 0.33J 6.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <5.0 <0.20 GW15 4/1/20 <0.13 <0.13 <0.13 <0.25 0.28J 0.23J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 <0.13 <0.20 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <1.0 <0.20 GW15D 4/1/20 <0.13 <0.13 <0.13 <0.25 8.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.17J <0.13 1 <1.0 <0.13 1 <0.20 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <2.0 <5.0 <0.20 Notes "<" = Not detected at or above the laboratory reporting limit Concentrations are reported in micrograms per liter (µg/l) Concentrations expressed in highlighted, bold print equal or exceed the 2L Standard GCL = Gross Contamination Level J = Estimated value below method reporting limit Page 1 of 1 TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. 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PLEASANT, NORTH CAROLINA �mmmmmaaaaaaasaaaaaaaaaaaaaaa �®mmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa ��mmm®aaaaaaasaaaaaaaaaaaaaaa �ammmmaaaaaaasaaaaaaaaaaaaaaa ��mmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ��mmm®aaaaaaasaaaaaaaaaaaaaaa ��mmm®aaaaaaasaaaaaaaaaaaaaaa ��mmmmaaaaaaasaaaaaaaaaaaaaaa �ammm®aaaaaaasaaaaaaaaaaaaaaa ®����aaaaaaasaaaaaaaaaaaaaaa ®®®®aaaaaaasaaaaaaaaaaaaaaa ����m�aaaaaaasaaaaaaaaaaaaaaa �mm®®aaaaaaasaaaaaaaaaaaaaaa ���aamaaaaaaasaaaaaaaaaaaaaaa �����maaaaaaasaaaaaaaaaaaaaaa ����®aaaaaaasaaaaaaaaaaaaaaa ��omo®aaaaaaasaaaaaaaaaaaaaaa ®���maaaaaaasaaaaaaaaaaaaaaa �mmmmoaaaaaaasaaaaaaaaaaaaaaa �����®aaaaaaasaaaaaaaaaaaaaaa ���®®maaaaaaasaaaaaaaaaaaaaaa TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA iO 71 �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmaaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmoaaaaaaasaaaaaaaaaaaaaaa �mmmmaaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmm®maaaaaaasaaaaaaaaaaaaaaa �momomaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®mmmmmmmammmmmmmmamaaaaa �mmmm®mmmmmmmammmmmmmmamaaaaa ®mmmmmmmmmmmmammmmmmmmamaaaaa ®mmmmmmmmmmmmmmmmmmmmmamaaaaa �mmmm®mmmmmmmmmmmmmmmmmmaaaaa ®mmmm®mmmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmommmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmommmaaaaa �mmmmmmmmmmmmmmmmmmm®mmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmommmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmm®mmmaaaaa �mmmmmmmmmmmmmmmmmmm®mmmaaaaa �mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmm®®mmmmmmmmmmmmmmmmmmammaa �mmm®®mmmmmmmmmmmmmmmmmmammaa ®mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmm®mmmmmmmmmmmmmmmmmmammaa �mmmm®mmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmmm TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm�aaaaaaasaaaaaaaaaaaaaaa ��mmm�aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa ��mmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa ��mmm�aaaaaaasaaaaaaaaaaaaaaa ��mmm�aaaaaaasaaaaaaaaaaaaaaa ��mmm�aaaaaaasaaaaaaaaaaaaaaa ��mmm�aaaaaaasaaaaaaaaaaaaaaa ��mmm�aaaaaaasaaaaaaaaaaaaaaa ��mmm�aaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa ����®®aaaaaaasaaaaaaaaaaaaaaa �momo®aaaaaaasaaaaaaaaaaaaaaa �����®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �����maaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA ®m©mmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �m®®amaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �®mmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mammmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmamaaaaaaasaaaaaaaaaaaaaaa �mmm®®aaaaaaasaaaaaaaaaaaaaaa �momomaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ®mmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa ®mmmmmmmmmmmmamammmmmmamaaaaa �mmmmmommmmmmamammmmmmamaaaaa ®mmmmmmmmmmmmammmmmmmmamaaaaa ®mmmmmmmmmmmmmmmmmmmmmamaaaaa �®mmmm®mmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmommmmmmmmmmmmm®mmmmaaaaa �mmm®mmmmmmmmmmmmmmmmmmmammaa �mmm®mmmmmmmmmmmmmmmmmmmammaa ®mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmm®mmmmmmmmmmmmmmmmmmmmmam �mmm®mmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmmm TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmaaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmaaaaaaaasaaaaaaaaaaaaaaa �mmmmoaaaaaaasaaaaaaaaaaaaaaa �mmm®maaaaaaasaaaaaaaaaaaaaaa �mmmomaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ®mmmmmammmmmmammmmmmmmamaaaaa �mmmm®ammmmmmammmmmmmmamaaaaa ®mmmmmmmmmmmmammmmmmmmamaaaaa ®mmmmmmmmmmmmmmmmmmmmmamaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmm®mmmmmmmmmmmmmmmmmmmammaa �mmm®mmmmmmmmmmmmmmmmmmmammaa ®mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmmmmmmmmmmmmam �mmm®mmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmmm TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA ®©©©�aaaaaaasaaaaaaaaaaaaaaa �ammmmaaaaaaasaaaaaaaaaaaaaaa �mmmm�aaaaaaasaaaaaaaaaaaaaaa ®mma�aaaaaaasaaaaaaaaaaaaaaa �ammm®aaaaaaasaaaaaaaaaaaaaaa ��mmo®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa ��oma®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa ��mmo®aaaaaaasaaaaaaaaaaaaaaa ��mmo�aaaaaaasaaaaaaaaaaaaaaa ��mm®�aaaaaaasaaaaaaaaaaaaaaa ®a0m�aaaaaaasaaaaaaaaaaaaaaa �m��a�aaaaaaasaaaaaaaaaaaaaaa ®m®0�aaaaaaasaaaaaaaaaaaaaaa ��aam�aaaaaaasaaaaaaaaaaaaaaa ��aaa�aaaaaaasaaaaaaaaaaaaaaa �m����aaaaaaasaaaaaaaaaaaaaaa �momo®aaaaaaasaaaaaaaaaaaaaaa �����®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �����oaaaaaaasaaaaaaaaaaaaaaa �����®aaaaaaasaaaaaaaaaaaaaaa TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA �mm®®maaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmammaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �m®®®maaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa mmmm®maaaaaaasaaaaaaaaaaaaaaa �momomaaaaaaasaaaaaaaaaaaaaaa mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ®mmmmm®mmmmmmmmmmmmmmmamaaaaa mmmm®mmmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmammmmmmmmamaaaaa ®mmmmmmmmmmmmmmmmmmmmmamaaaaa mmmm®mmmmmmmmmmmmmmmmmmaaaaa ®mmmm®mmmmmmmmmmmmmmmmmmaaaaa ®mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmm®mmmmmmmmmmmmmmmmmmaaaaa mmmm®mmmmmmmmmmmmmmmmmmaaaaa mmmm©mmmmmmmmmmmmmmmmmmaaaaa mmmm®mmmmmmmmmmmmmmmmmmmammaa mmmm®mmmmmmmmmmmmmmmmmmmammaa mmmm®®mmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmam TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmaamaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmma®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa ®mma®aaaaaaasaaaaaaaaaaaaaaa �mmmamaaaaaaasaaaaaaaaaaaaaaa ®mmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmamaaaaaaasaaaaaaaaaaaaaaa �mamamaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mamm®aaaaaaasaaaaaaaaaaaaaaa mmm®maaaaaaasaaaaaaaaaaaaaaa �mommmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmoaaaaaaasaaaaaaaaaaaaaaa �mmmmaaaaaaaasaaaaaaaaaaaaaaa �mmmmmmmmmmmmammmmmmmmamaaaaa �mmmmmmmmmmmmammmmmmmmamaaaaa ®mmm®mmmmmmmmammmmmmmmamaaaaa ®mmmmommmmmmmmmmmmmm®mmmaaaaa �®m®®mmm®mmmmmmmmmmmmmmmaaaaa ®mmmmommmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmmommaaaaa �mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmmm®mmmmmmmmmmmmmm®mmmaaaaa �mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmmm®mmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmm®mmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmm®mmmmmmmmmmmmmmm®mmmammaa mmm®mmmmmmmmmmmmmmmmmmmammaa mmm®mmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmmmmmmmmmmmmmmmam �mmmm®mmmmmmmmmmmmmmmmmmmmmmm TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA �mmmmoaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmaaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmaaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ®mam®®®mmmmmms��mmmmmmamaaaaa �mmmmmammmmmmammmmmmmmamaaaaa ®mmmmmmmmmmmmammmmmmmmamaaaaa ®mmmmm®mmmmmmmmmmmmmmmmmaaaaa �mmm®m®mmmmmmmmmmmmmmmmmaaaaa ®mmmm®®mmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmmmmmmmmmmmmaaaaa Sig,,dmmmmmmmaaaaa �mmmm®mmmmmmm���� �mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmm®mmmmmmmmmmmmmmmmmmmammaa �mmm®mmmmmmmmmmmmmmmmmmmammaa �mmm®mmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmm��mmmmmmmmmmmmm TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA iO 71 �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmm®maaaaaaasaaaaaaaaaaaaaaa �momooaaaaaaasaaaaaaaaaaaaaaa �mmmm®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa aaaaaaasaaaaaaaaaaaaaaa �mm��maaaaaaasaaaaaaaaaaaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmosmmmmmmmmamaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmm®mmmmmmmmmamaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmm®m��mmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmm®mmmmmmmmmmmmmmmmmmmammaa �mmm®mmmmmmmmmmmmmmmmmmmammaa �mmmmmmmmmmmmmmmm®mmmmmmmmmam �mmmmmaaaaaaaaaaaaaaaaaaaaaaa �mmmmmaaaaaaaaaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmooaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmmmmmmmmmmmammmmmmmmamaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa ®mmmm®mmmmmmmmmmmmmmmmamaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa ®mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa mmmmmmmmmmmmmmmmmmmmmmmaaaaa �mmm®mmmmmmmmmmmmmmmmmmmammaa �mmm®mmmmmmmmmmmmmmmmmmmammaa �mmm®mmmmmmmmmmmmmmmmmmmmmmam �mmmmmmmmmmmmm��mmmmmmmmmmmmm TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA iO 71 ������aaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa ��®���aaaaaaasaaaaaaaaaaaaaaa �momooaaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa �����maaaaaaaaaaaaaaaaaaaaaaa ��o��maaaaaaaaaaaaaaaaaaaaaaa ����®maaaaaaasaaaaaaaaaaaaaaa �momomaaaaaaasaaaaaaaaaaaaaaa �����maaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa �����maaaa�aasaaaaaaaaaaaaaaa TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA iO 71 ©���maaaaaaasaaaaaaaaaaaaaaa �a����aaaaaaasaaaaaaaaaaaaaaa ����®®aaaaaaasaaaaaaaaaaaaaaa �momo�aaaaaaasaaaaaaaaaaaaaaa �����®aaaaaaasaaaaaaaaaaaaaaa �mmmmmaaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa �����maaaaaaasaaaaaaaaaaaaaaa �����maaaaaaasaaaaaaaaaaaaaaa ����®®aaaaaaasaaaaaaaaaaaaaaa �momomaaaaaaasaaaaaaaaaaaaaaa �����maaaaaaasaaaaaaaaaaaaaaa ��mmmmaaaaaaasaaaaaaaaaaaaaaa �����®aaaaaaasaaaaaaaaaaaaaaa �����®aaaaaaasaaaaaaaaaaaaaaa TABLE4 HISTORICAL GROUNDWATER ANALYTICAL RESULTS CIRCLE K STORE N. 8387 RM No, 2751 9425 NORTH CAROLINA HIGHWAY 49 NORTH MT. PLEASANT, NORTH CAROLINA ��m®�®aaaaaaasaaaaaaaaaaaaaaa ���®��aaaaaaasaaaaaaaaaaaaaaa ����o�aaaaaaasaaaaaaaaaaaaaaa ��maomaaaaaaasaaaaaaaaaaaaaaa ��®®®aaaaaaasaaaaaaaaaaaaaaa ®®mm�aaaaaaasaaaaaaaaaaaaaaa ������aaaaaaasaaaaaaaaaaaaaaa ®mm®aaaaaaasaaaaaaaaaaaaaaa ®aaa®aaaaaaasaaaaaaaaaaaaaaa ��ammmaaaaaaasaaaaaaaaaaaaaaa ��®mm�aaaaaaasaaaaaaaaaaaaaaa ��mm®aaaaaaasaaaaaaaaaaaaaaa ��®®m®aaaaaaasaaaaaaaaaaaaaaa ��®�®®aaaaaaasaaaaaaaaaaaaaaa ��m�®maaaaaaasaaaaaaaaaaaaaaa ��o®��aaaaaaasaaaaaaaaaaaaaaa �ama��aaaaaaasaaaaaaaaaaaaaaa Notes: I. mND = Not Detected am above the laboratory detection limit. 2. Conc®trations are reported in mimg—, per liter (ugd) of parts per billion (ppb). 3. Concentrations m bold print and shaded exceed the cm responding NCDEQ Groundwater Quality 2L Standard (NC 2L Standard). Th, NC 2L Standard was rovised on 1-1-10. Data exuedances @om previous semplmg events ere relative to the former 2L 3mndards 4. NCDEQ = North Carolina Department of Enviromnental Quality 5. NA — Not A ly—l. 6. NS = Not Sampled. 7. - = Coastim— previously not reported 8. J= Estimated value below method reporting 1Mh APPENDIX A LABORATORY ANALYTICAL REPORTS ffm Orlando, FL The results set forth herein are provided by SGS North America Inc. a-Hl ydcopy 2. 0 Automated Report Technical Report for ATC Group Services LLC RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC SGS Job Number: FA73985 Sampling Date: 04/01/20 Report to: ATC Group Services LLC. 7606 Whitehall Executive Center Dr. Suite 800 Charlotte, NC 28273 jason.whittle@atcgs.com ATTN: Jason Whittle Total number of pages in report: 82 Ac Fp Test results contained within this data package meet the requirements Caitlin Brice, M. S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about Unauthorized modification of this report is strictly prohibited. how we can serve you better at: Review standard terms at: http://www.sgs.com/en/terms-and-conditions EHS.US.CustomerCare@sgs.com 1 of 82 FA73985 Sections: Table of Contents 1 Section1: Sample Summary................................................................................................... 3 Section2: Summary of Hits.................................................................................................... 5 Section3: Sample Results........................................................................................................ 7 3.1! FA73985-1: GW 01....................................................................................................... 8 3.2 FA73985-2: GW 02....................................................................................................... 11 3.3• FA73985-3: GW 03A.................................................................................................... 14 3.4 FA73985-4: GW 04....................................................................................................... 17 3.5- FA73985-5: GW 05....................................................................................................... 20 3.6 FA73985-6: GW 06....................................................................................................... 23 3.7: FA73985-7: GW 07....................................................................................................... 27 3.8 FA73985-8: GW 08....................................................................................................... 30 3.9: FA73985-9: GW 09D.................................................................................................... 33 3.10: FA73985-10: GW 10................................................................................................... 36 3.11: FA73985-11: GW 12................................................................................................... 39 3.12: FA73985-12: GW 13D................................................................................................ 42 3.13: FA73985-13: GW 14D................................................................................................ 45 3.14: FA73985-14: GW 15................................................................................................... 48 3.15: FA73985-15: GW 15D................................................................................................ 51 Section4: Misc. Forms............................................................................................................ 54 4.1: Chain of Custody........................................................................................................... 55 Section 5: MS Volatiles - QC Data Summaries..................................................................... 58 5.1: Method Blank Summary................................................................................................ 59 5.2: Blank Spike Summary................................................................................................... 65 5.3: Matrix Spike/Matrix Spike Duplicate Summary........................................................... 71 Section6: GC Volatiles - QC Data Summaries..................................................................... 77 6.1: Method Blank Summary................................................................................................ 78 6.2: Blank Spike Summary................................................................................................... 79 6.3: Matrix Spike Summary.................................................................................................. 81 6.4: Duplicate Summary....................................................................................................... 82 W, SGS North America Inc. Sample Summary ATC Group Services LLC Job No: FA73985 RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Sample Collected Matrix Client Number Date Time By Received Code Type Sample I D This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA73985-1 04/01/20 14:15 SBAR 04/03/20 AQ Ground Water GW O1 FA73985-2 04/01/20 14:10 SBAR 04/03/20 AQ Ground Water GW 02 FA73985-3 04/01/20 11:30 SBAR 04/03/20 AQ Ground Water GW 03A FA73985-4 04/01/20 12:20 SBAR 04/03/20 AQ Ground Water GW 04 FA73985-5 04/01/20 12:35 SBAR 04/03/20 AQ Ground Water GW 05 FA73985-6 04/01/20 10:25 SBAR 04/03/20 AQ Ground Water GW 06 FA73985-7 04/01/20 14:55 SBAR 04/03/20 AQ Ground Water GW 07 FA73985-8 04/01/20 15:20 SBAR 04/03/20 AQ Ground Water GW 08 FA73985-9 04/01/20 13:45 SBAR 04/03/20 AQ Ground Water GW 09D FA73985-10 04/01/20 10:55 SBAR 04/03/20 AQ Ground Water GW 10 FA73985-11 04/01/20 10:35 SBAR 04/03/20 AQ Ground Water GW 12 FA73985-12 04/01/20 12:30 SBAR 04/03/20 AQ Ground Water GW 13D 6 3 of 82 FA73985 SGS North America Inc. Sample Summary (continued) ATC Group Services LLC Job No: FA73985 RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC ;ample Collected Matrix Client lumber Date Time By Received Code Type Sample I D FA73985-13 04/01/20 13:30 SBAR 04/03/20 AQ Ground Water GW 14D FA73985-14 04/01/20 15:30 SBAR 04/03/20 AQ Ground Water GW 15 FA73985-15 04/01/20 15:05 SBAR 04/03/20 AQ Ground Water GW 15D 6 4of82 FA73985 Summary of Hits Job Number: FA73985 Account: ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Collected: 04/01/20 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA73985-1 GW 01 Isopropylbenzene 0.17 J 0.50 0.13 ug/l SM 6200B Methyl Tert Butyl Ether 4.3 0.50 0.13 ug/l SM 6200B Trichloroethylene 0.18 J 0.50 0.13 ug/l SM 6200B Trichlorofluoromethane 2.6 0.50 0.20 ug/l SM 6200B FA73985-2 GW 02 Benzene 1.2 0.50 0.13 ug/l SM 6200B sec-Butylbenzene 0.44 J 0.50 0.13 ug/l SM 6200B Di -Isopropyl Ether 0.56 0.50 0.13 ug/l SM 6200B Ethylbenzene 0.15 J 0.50 0.13 ug/l SM 6200B Isopropylbenzene 2.1 0.50 0.13 ug/l SM 6200B Methyl Tert Butyl Ether 1.1 0.50 0.13 ug/l SM 6200B n-Propylbenzene 0.46 J 0.50 0.13 ug/l SM 6200B Toluene 0.19 J 0.50 0.13 ug/l SM 6200B m,p-Xylene 0.54 J 1.0 0.13 ug/l SM 6200B o-Xylene 0.35 J 0.50 0.13 ug/l SM 6200B Xylene (total) 0.89 J 1.5 0.25 ug/l SM 6200B FA73985-3 GW 03A Methyl Tert Butyl Ether 5.4 0.50 0.13 ug/l SM 6200B Trichlorofluoromethane 0.21 J 0.50 0.20 ug/1 SM 6200B FA73985-4 GW 04 Trichlorofluoromethane 3.8 0.50 0.20 ug/l SM 6200B FA73985-5 GW 05 Di -Isopropyl Ether 0.33 J 0.50 0.13 ug/l SM 6200B Methyl Tert Butyl Ether 0.75 0.50 0.13 ug/l SM 6200B FA73985-6 GW 06 No hits reported in this sample. FA73985-7 GW 07 Methyl Tert Butyl Ether 3.8 0.50 0.13 ug/l SM 6200B Page 1 of 2 6 5 of 82 FA73985 Summary of Hits Job Number: FA73985 Account: ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Collected: 04/01/20 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA73985-8 GW 08 Di -Isopropyl Ether Methyl Tert Butyl Ether FA73985-9 GW 09D cis- 1, 2-Dichloroethylene Methyl Tert Butyl Ether Trichloroethylene Trichlorofluoromethane FA73985-10 GW 10 Methyl Tert Butyl Ether FA73985-11 GW 12 No hits reported in this sample. FA73985-12 GW 13D Trichlorofluoromethane FA73985-13 GW 14D Di -Isopropyl Ether Methyl Tert Butyl Ether Trichloroethylene Trichlorofluoromethane FA73985-14 GW 15 Di -Isopropyl Ether Methyl Tert Butyl Ether FA73985-15 GW 15D cis-1, 2-Dichloroethylene Methyl Tert Butyl Ether 1.2 0.50 0.13 ug/l SM 6200B 6.8 0.50 0.13 ug/l SM 6200B 0.19 J 0.50 0.13 ug/l SM 6200B 2.3 0.50 0.13 ug/l SM 6200B 0.46 J 0.50 0.13 ug/l SM 6200B 10.4 0.50 0.20 ug/l SM 6200B 0.14 J 0.50 0.13 ug/l SM 6200B 1.2 0.50 0.20 ug/l SM 6200B 0.16 J 0.50 0.13 ug/l SM 6200B 16.2 0.50 0.13 ug/l SM 6200B 0.33 J 0.50 0.13 ug/l SM 6200B 6.5 0.50 0.20 ug/l SM 6200B 0.23 J 0.50 0.13 ug/l SM 6200B 0.28 J 0.50 0.13 ug/l SM 6200B 0.17 J 0.50 0.13 ug/l SM 6200B 8.2 0.50 0.13 ug/1 SM 6200B Page 2 of 2 6 6 of 82 FA73985 i SG$f Orlando, FL im Section 3 Sample Results Report of Analysis 6 7 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW O1 Lab Sample ID: FA73985-1 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102583.1) 1 04/07/20 10:28 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 8 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW O1 Lab Sample ID: FA73985-1 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene 0.17 0.50 0.13 ug/1 J 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 4.3 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene 0.18 0.50 0.13 ug/1 J 75-69-4 Trichlorofluoromethane 2.6 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102% 70-130% 17060-07-0 1,2-Dichloroethane-D4 108% 70-130% 2037-26-5 Toluene-D8 99% 70-130% 460-00-4 4-Bromofluorobenzene 100% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 9 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW O1 Lab Sample ID: FA73985-1 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 j File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111424.D 1 04/06/20 18:55 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 37.4ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.019 0.0094 ug/1 Run# 1 Run# 2 Limits 102% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 10 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 02 Lab Sample ID: FA73985-2 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102584.1) 1 04/07/20 10:51 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene 1.2 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene 0.44 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 J ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 11 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 02 Lab Sample ID: FA73985-2 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether 0.56 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene 0.15 0.50 0.13 ug/1 J 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene 2.1 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 1.1 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene 0.46 0.50 0.13 ug/1 J 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene 0.19 0.50 0.13 ug/1 J 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene 0.54 1.0 0.13 ug/1 J 95-47-6 o-Xylene 0.35 0.50 0.13 ug/1 J 1330-20-7 Xylene (total) 0.89 1.5 0.25 ug/1 J CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104% 70-130% 17060-07-0 1,2-Dichloroethane-D4 109% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 96% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 12 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 02 Lab Sample ID: FA73985-2 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 N File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111425.1) 1 04/06/20 19:11 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 38.0ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0092 ug/1 Run# 1 Run# 2 Limits 97% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound � 13 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 03A Lab Sample ID: FA73985-3 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102585.1) 1 04/07/20 11:13 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 14of82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 03A Lab Sample ID: FA73985-3 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 5.4 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane 0.21 0.50 0.20 ug/1 J 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 108% 70-130% 2037-26-5 Toluene-D8 99% 70-130% 460-00-4 4-Bromofluorobenzene 99% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 15 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 03A Lab Sample ID: FA73985-3 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 w File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111426.D 1 04/06/20 19:26 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 37.9ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0092 ug/1 Run# 1 Run# 2 Limits 99% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 16 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 04 Lab Sample ID: FA73985-4 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102586.1) 1 04/07/20 11:37 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 17 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 04 Lab Sample ID: FA73985-4 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane 3.8 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102% 70-130% 17060-07-0 1,2-Dichloroethane-D4 110% 70-130% 2037-26-5 Toluene-D8 96% 70-130% 460-00-4 4-Bromofluorobenzene 100% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 18 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 04 Lab Sample ID: FA73985-4 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 P File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111429.D 1 04/06/20 20:13 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 38.0ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0092 ug/1 Run# 1 Run# 2 Limits 108% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 19 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 05 Lab Sample ID: FA73985-5 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102587.1) 1 04/07/20 11:59 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 20 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 05 Lab Sample ID: FA73985-5 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether 0.33 0.50 0.13 ug/1 J 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 0.75 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104% 70-130% 17060-07-0 1,2-Dichloroethane-D4 109% 70-130% 2037-26-5 Toluene-D8 98% 70-130% 460-00-4 4-Bromofluorobenzene 97% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 21 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 05 Lab Sample ID: FA73985-5 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 P File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111430.1) 1 04/06/20 20:28 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run #1 38.3 ml 2.0 ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0091 ug/1 Run# 1 Run# 2 Limits 93% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 22 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID: GW 06 Lab Sample ID: FA73985-6 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0221889.1) 1 04/08/20 10:39 AB n/a n/a VA2716 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 23 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 06 Lab Sample ID: FA73985-6 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol a ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 112% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 97% 70-130% Page 2 of 3 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 24 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 06 Lab Sample ID: FA73985-6 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q (a) Associated CCV and BS outside control limits high. Page 3 of 3 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �1%6 25 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 06 Lab Sample ID: FA73985-6 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111431.1) 1 04/06/20 20:44 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 37.4ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.019 0.0094 ug/1 Run# 1 Run# 2 Limits 106% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 26 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 07 Lab Sample ID: FA73985-7 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102589.1) 1 04/07/20 12:45 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 27 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 07 Lab Sample ID: FA73985-7 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 3.8 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 111% 70-130% 2037-26-5 Toluene-D8 98% 70-130% 460-00-4 4-Bromofluorobenzene 99% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 28 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 07 Lab Sample ID: FA73985-7 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 P File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111432.1) 1 04/06/20 20:59 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run #1 38.1 ml 2.0 ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0092 ug/1 Run# 1 Run# 2 Limits 91% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 29 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 08 Lab Sample ID: FA73985-8 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102590.1) 1 04/07/20 13:08 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound w i" 01 30 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 08 Lab Sample ID: FA73985-8 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether 1.2 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 6.8 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104% 70-130% 17060-07-0 1,2-Dichloroethane-D4 112% 70-130% 2037-26-5 Toluene-D8 99% 70-130% 460-00-4 4-Bromofluorobenzene 100% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound w 00 01 31 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 08 Lab Sample ID: FA73985-8 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 w File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111433.1) 1 04/06/20 21:15 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run #1 37.8 ml 2.0 ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.019 0.0093 ug/1 Run# 1 Run# 2 Limits 103% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound � 32 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 09D Lab Sample ID: FA73985-9 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102595.1) 1 04/07/20 15:01 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene 0.19 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 J ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 33 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 09D Lab Sample ID: FA73985-9 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 2.3 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene 0.46 0.50 0.13 ug/1 J 75-69-4 Trichlorofluoromethane 10.4 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 108% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 98% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 34 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 09D Lab Sample ID: FA73985-9 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 P File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111434.1) 1 04/06/20 21:30 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 37.9ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0092 ug/1 Run# 1 Run# 2 Limits 103% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 35 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 10 Lab Sample ID: FA73985-10 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102596.1) 1 04/07/20 15:24 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 36 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 10 Lab Sample ID: FA73985-10 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 0.14 0.50 0.13 ug/1 J 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 108% 70-130% 2037-26-5 Toluene-D8 98% 70-130% 460-00-4 4-Bromofluorobenzene 99% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 37 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 10 Lab Sample ID: FA73985-10 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111435.1) 1 04/06/20 21:46 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 37.6ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.019 0.0093 ug/1 Run# 1 Run# 2 Limits 92% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 38 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 12 Lab Sample ID: FA73985-11 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102597.1) 1 04/07/20 15:47 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 39 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 12 Lab Sample ID: FA73985-11 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 110% 70-130% 2037-26-5 Toluene-D8 96% 70-130% 460-00-4 4-Bromofluorobenzene 100% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 40 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 12 Lab Sample ID: FA73985-11 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111436.1) 1 04/06/20 22:01 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run #1 38.1 ml 2.0 ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0092 ug/1 Run# 1 Run# 2 Limits 106% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 41 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 13D Lab Sample ID: FA73985-12 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102598.1) 1 04/07/20 16:09 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 42 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 13D Lab Sample ID: FA73985-12 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane 1.2 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 110% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 100% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 43 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 13D Lab Sample ID: FA73985-12 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111437.D 1 04/06/20 22:17 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run #1 37.5 ml 2.0 ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.019 0.0093 ug/1 Run# 1 Run# 2 Limits 88% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 44 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 14D Lab Sample ID: FA73985-13 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102599.1) 1 04/07/20 16:32 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 45 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 14D Lab Sample ID: FA73985-13 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether 0.16 0.50 0.13 ug/1 J 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 16.2 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene 0.33 0.50 0.13 ug/1 J 75-69-4 Trichlorofluoromethane 6.5 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 111% 70-130% 2037-26-5 Toluene-D8 102% 70-130% 460-00-4 4-Bromofluorobenzene 98% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 46 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 14D Lab Sample ID: FA73985-13 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111438.1) 1 04/06/20 22:32 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 37.7ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.019 0.0093 ug/1 Run# 1 Run# 2 Limits 110% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 47 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 15 Lab Sample ID: FA73985-14 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102600.1) 1 04/07/20 16:55 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 48 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 15 Lab Sample ID: FA73985-14 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether 0.23 0.50 0.13 ug/1 J 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 0.28 0.50 0.13 ug/1 J 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104% 70-130% 17060-07-0 1,2-Dichloroethane-D4 112% 70-130% 2037-26-5 Toluene-D8 99% 70-130% 460-00-4 4-Bromofluorobenzene 96% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 49 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 15 Lab Sample ID: FA73985-14 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111441.1) 1 04/06/20 23:19 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run #1 38.5 ml 2.0 ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0091 ug/1 Run# 1 Run# 2 Limits 75% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 50 of 82 FA73985 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID: GW 15D Lab Sample ID: FA73985-15 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E102601.1) 1 04/07/20 17:18 AB n/a n/a VE2282 Run #2 Purge Volume Run # 1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/1 71-43-2 Benzene ND 0.50 0.13 ug/1 108-86-1 Bromobenzene ND 0.50 0.13 ug/1 74-97-5 Bromochloromethane ND 0.50 0.13 ug/1 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/1 75-25-2 Bromoform ND 0.50 0.13 ug/1 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/1 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/1 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/1 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/1 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/1 108-90-7 Chlorobenzene ND 0.50 0.13 ug/1 75-00-3 Chloroethane ND 0.50 0.20 ug/1 67-66-3 Chloroform ND 0.50 0.13 ug/1 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/1 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/1 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/1 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/1 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/1 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/1 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/1 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/1 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/1 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/1 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/1 156-59-2 cis-1,2-Dichloroethylene 0.17 0.50 0.13 ug/1 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/1 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/1 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/1 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/1 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/1 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 J ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 51 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 15D Lab Sample ID: FA73985-15 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: SM 6200B Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC VOA List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/1 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/1 64-17-5 Ethyl Alcohol ND 100 65 ug/1 100-41-4 Ethylbenzene ND 0.50 0.13 ug/1 591-78-6 2-Hexanone ND 5.0 1.0 ug/1 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/1 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/1 74-83-9 Methyl Bromide ND 0.50 0.20 ug/1 74-87-3 Methyl Chloride ND 0.50 0.20 ug/1 75-09-2 Methylene Chloride ND 2.0 1.0 ug/1 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/1 1634-04-4 Methyl Tert Butyl Ether 8.2 0.50 0.13 ug/1 91-20-3 Naphthalene ND 0.50 0.13 ug/1 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/1 100-42-5 Styrene ND 0.50 0.13 ug/1 630-20-6 1, 1, 1,2-Tetrachloroethane ND 0.50 0.13 ug/1 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/1 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/1 108-88-3 Toluene ND 0.50 0.13 ug/1 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/1 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/1 79-00-5 1, 1, 2-Trichloroethane ND 0.50 0.13 ug/1 79-01-6 Trichloroethylene ND 0.50 0.13 ug/1 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/1 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/1 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/1 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/1 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/1 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/1 m,p-Xylene ND 1.0 0.13 ug/1 95-47-6 o-Xylene ND 0.50 0.13 ug/1 1330-20-7 Xylene (total) ND 1.5 0.25 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104% 70-130% 17060-07-0 1,2-Dichloroethane-D4 112% 70-130% 2037-26-5 Toluene-D8 99% 70-130% 460-00-4 4-Bromofluorobenzene 98% 70-130% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 52 of 82 FA73985 SGS North America Inc. Report of Analysis Client Sample ID: GW 15D Lab Sample ID: FA73985-15 Date Sampled: 04/01/20 Matrix: AQ - Ground Water Date Received: 04/03/20 Method: EPA 504.1 EPA 504.1 Percent Solids: n/a Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 DD111442.D 1 04/06/20 23:34 KB 04/06/20 14:22 OP79697 GDD3206 Run #2 Initial Volume Final Volume Run#1 38.0ml 2.0ml Run #2 CAS No. Compound 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene Result RL MDL Units Q ND 0.018 0.0092 ug/1 Run# 1 Run# 2 Limits 74% 63-137% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 53 of 82 FA73985 ffm Orlando, FL Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 6 54 of 82 FA73985 cc 1%1..a+}h A . Tnn _ (irllonrin CAI L604e Chain of Custody V - sI -� N#O?JV ✓ PAGE A OF Z- sn$ 4405 Vineland tined, Sui. C-15 Orland" FI32811 TEL.407425fi700 FAX: 407425-0707 SGS - ORLANDO Quote # SKIFF # Client / Reporting Information Project Information _ i Anal ical Information- -; Matrix Codes Company Name: /I Y[ /.i (_ 1�1t� 5 X�d• Protect Name: q M G-7 r, i '5 �% -3 `I� 1j z 7 - _ ` U I•rl G� Water Ing CW- Ground Water WW - Water SW-Surrace Water SO -Soil SO SL-Sludge 01-011 LIQ - Other Liquid AIR-AirSam SOL Other Solid Address: 7 t t'�T % COL alb Gxc f� D- Street ?i.J H b( r'il`l) z.w City: 611 to t� State: zip: '> 1N N(<, OZ7.i r N % �. lY%t %riUVtru1� C Project Contac(•, Email: J (17 LIh w1c :TS a -4 is,R7. ro'act# Q / 6L Z7J1 Phone #: 776r�- 5;; - .3Z-00 Fax# Sampler(s) Name(s)(Printed) ter 1:/01 Client Purchase Order# SGS Orlando Sample # Field ID / Point of Collection COLL MON CON-NER-O""' - LAB USE ONLY DATE TIME sAnv+Leo ar. x rmALx aF eoTrLEs w e E z �, F to i N/1 ZJ 1415 5 8 X >C h 6L✓-(,Uj A N/1/i4: li 30 66 (:w LJ '-Ul N/i/ZJ rL3S 5 Gw r ?�>C C1 -C) . W/(/Zo i2LL 5 P /YIaJ- CJ$ GI 1 v 1 riGiJ Sri GL✓ c K � h vl (w--U i 0 ! "` 50 Caw S x < �x C t - v S -( 6/ i 1 1 X% rL,/-I) —^ J- I L•f,G#1—l',k. Turnaround Time Business da s '[]COMMERCIAL Data Deliverable Information�%, ,.. 1` - *o , "} , Comments I Remarks 70 Day (Business) Approved By: I Date: 7 Day y Day � (, . 3 Day RUSH 2 Day RUSH t Day RUSH Other Ruah TIA Data Available VIA Emall or Lablink "A" (RESULTS ONLY) ❑COMMERCIAL "B" (RESULTS PLUS QC) ❑REDTI (EPA LEVEL 3) ❑FULLTI(EPA LEVEL 4) ❑EDO'S 'r\(7, �C.'/'i-' S - L.:tl✓�� �- u + LABEL VERIFICATK))V._._--...- - Sam le Cusfotl must be documented be ow eat ime sam les thane ossession, includin courier dative . a .. Relinquished bl!y SamplerlAffllla/t1oln / 1 /t �-itJ✓1 I� /y%Gl / 17�L Data Time:){ IT) /(/�-J Received Iliatlon% Z 2 •' r ✓ A0 : G Relinqui By/Afflll -on 3 z _ D.�at/e Ime 7 Z / Received By/Affll lio_n/ 4 �•P o" Relinquished by/Affiliation r 5 1�.. Date Time: Recei - d y/Affiliali �1 �Li 6 ( 03 Relinquished /Afflllaaon 7 ate Time: Received By/Affiliation 6 Lab Use Only: Cooler Temueralure (a' Celsius (,or—'edl:. _ hft : /vrww. ORLD-SNTr-0001-03-FORM-COC (1) Rev 031318 FA73985: Chain of Custody Page 1 of 3 6 55 of 82 FA73985 SGS North America Inc - Orlando Sc;§ Chain of Custody 4405VinelandRmd. Roilsr.H rbd"d" Fl ?Rll SGS - ORLANDO JOB# . PAGE OF TEL4074256700 FAX: 407-425-0707 SGS - ORLANDO Quote # SKIFF # Client I Reporting Information Project Information �_' ,K'. Analytical Information - •' Matrix Codes CompanyName: 4fC ta�OV /1 Y'Vd Project Name:LAV QM 7 S l � rJ \} — `.� fn j'� �'h - nn ng Water OW - Ground water ater w-Surfar SW -surface Water SO - soil SL-Sludge LIQ - Other Liquid AIR - Air SOL-Other Solid r Address: '406 wh ,1CAJI I/k(. (.7 r ]'r I/ I^ Street -1 kp N 7`i 1'lw , I"1 9 NU City: (, )tvipf-FG State: NL ZIP' 63%73 �y M 41 f�", p�C- <iWl N�- Project Contact: Email: ':>o---,, wh,Vl"le 5a.S- 1,6:fkt 6ti'C r,-/ Project# P66 ZT51 ��7 Phone#: I la V Fax# Sampler(s) Name(s�(Printed) Sampler 1:Sam ler2: ir• Client Purchase Order # 3 S Orlando Sam le # Field ID I Point of Collection illy COLLEOTNN CONTAINERNFORMATpN WE 7M sAuxEo —e. rOTALx of eornes g z 1 $ $ x ; - FLAB USE ONLY VL 1 15 D ) 100 S C, G w !jkj I I I]c I (' irw 1530 Gt r, Y :� „ „..;; Turnaround Time ( Business days) „" u� ^. r. " .. • ;;i. Data Delivarable Information , i `%ri.: ,? :" ` „�u - " Comments / Remarks,' 10 Day (Business) Approved By:l Dale: 7Da Day 5j'�1" 3 Day RUSH 2 Day RUSH 1 Day RUSH Other Rush TIA Data Available VIA Email or Labllnk COMMERCIAL "A" (RESULTS ONLY) COMMERCIAL"B"(RESULTS PLUS QC) []REDT1 (EPA LEVEL 3) E]FULLTI (EPA LEVEL 4) []EDD'S / - \�•r zYj t i .i-'"'J'"O•)� >_ ample Custody must be documented bel Tpossession, Including courier Relmqu''11l'�shed�by Sampler/Affiliation l l rWl I( Date Timeu(6tx) Received Illa/ti/oy� YL 2 G -� ."�/// Relinquis/h/e�BylAffili on 3 CG. Dat ime: 4 7S Received By/Affiliation 4 T Relinquished b/Affiliation- $ Date Time: Recet tl /Affilia' �yt S elinquished By/Affiliation 7 Data Time: Received By/Affiliation g Lab Use Onl : Cooler Tem erature (s) Celsius (corre ed): MID, sgs.com/en/torms-and-aqadilioL ORLD-SMT-0001-03-FORM-COC (1) Rev 031318 FA73985: Chain of Custody Page 2 of 3 dsill 56 of 82 FA73985 Job Number: FA73985 Client: AT Date / Time Received: 4/3/2020 9:45:00 AM [Therm ID: IR 1;ler Temps (Raw Measured) °C: Cooler 1: (3.4); Cooler Temps (Corrected) °C: Cooler 1: (2.6); Cooler Information Y or N 1. Custody Seals Present ❑.I ❑ 2. Custody Seals Intact ❑d ❑ 3. Temp criteria achieved ❑d ❑ 4. Cooler temp verification IR Gun 5. Cooler media Ice(Bag SGS Sample Receipt Summary C Project: RM 2751 livery Method: FED EX Airbill #'s: 1001893363010003281100100963780112 ;rm CF: -0.8; # of Coolers: 1 Sample Information Y or N N/A 1. Sample labels present on bottles W ❑ 2. Samples preserved properly ❑d ❑ 3. Sufficient volume/containers recvd for analysis: W ❑ 4. Condition of sample Intact 5. Sample recvd within HT 0 ❑ 6. Dates/Times/IDs on COC match Sample Label 0 ❑ Trio Blank Information Y or N N/A 7. VOCs have headspace ❑ ❑.i ❑ 1. Trip Blank present / cooler ❑ ❑,i [ 8. Bottles received for unspecified tests ❑ ❑d 2. Trip Blank listed on COC ❑ ❑d [ 9. Compositing instructions clear ❑ ❑ k 10. Voa Soil Kits/Jars received past 48hrs? ❑ ❑ ❑,/ W or S N/A 11. % Solids Jar received? ❑ ❑ 0 3. Type Of TB Received ❑ ❑ W 12. Residual Chlorine Present? ❑ ❑ ❑,� Misc. Information Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: Test Strip Lot #s: pH 0-3 230315 pH 10-12 219813A Other: (Specify) Residual Chlorine Test Strip Lot #: Comments shoot Rev. Dale 05/24/17 Technician: SHAYLAP Date: 4/3/2020 9:45:00 AM Reviewer: Date: FA73985: Chain of Custody Page 3 of 3 A 0 6 57 of 82 FA73985 Orlando, FL MS Volatiles QC Data Summaries 60 i Section 5 Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries 6 58 of 82 FA73985 Method Blank Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2282-MB E102581.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-1 1, FA73985-12, FA73985-13, FA73985-14, FA73985-15 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/l 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis- 1, 2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans- 1, 2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/l 64-17-5 Ethyl Alcohol ND 100 65 ug/l 100-41-4 Ethlbenzene ND 0.50 0.13 ug/l 6 59 of 82 FA73985 Method Blank Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 2 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2282-MB E102581.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 CAS No. Compound Result RL MDL Units Q 591-78-6 2-Hexanone ND 5.0 1.0 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1, 1, 1, 2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1, 2,3 -Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total) ND 1.5 0.25 ug/l CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 101% 70-130% 17060-07-0 1,2-Dichloroethane-D4 108% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 6 60 of 82 FA73985 Method Blank Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 3 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2282-MB E102581.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 CAS No. Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 97% 70-130% � 61 of 82 FA73985 Method Blank Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2716-MB A0221888.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: Method: SM 6200B FA73985-6 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 2.0 ug/l 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 78-93-3 2-Butanone (MEK) ND 2.5 1.3 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1, 1 -Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1, 1 -Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis- 1, 2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans- 1, 2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1, 1 -Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis- 1, 3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans- 1, 3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di -Isopropyl Ether ND 0.50 0.13 ug/l 64-17-5 Ethyl Alcohol ND 100 65 ug/l 100-41-4 Ethlbenzene ND 0.50 0.13 ug/l 6 62 of 82 FA73985 Method Blank Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 2 of 3 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl TA2716-MB A0221888.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: Method: SM 6200B FA73985-6 CAS No. Compound Result RL MDL Units Q 591-78-6 2-Hexanone ND 5.0 1.0 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 108-10-1 4-Methyl-2-pentanone (MIBK) ND 2.5 1.3 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1, 1, 1, 2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1, 1, 1 -Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1, 2,3 -Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total) ND 1.5 0.25 ug/l CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 100% 70-130% 17060-07-0 1,2-Dichloroethane-D4 109% 70-130% 2037-26-5 Toluene-D8 102% 70-130% 6 63 of 82 FA73985 Method Blank Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 3 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2716-MB A0221888.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: Method: SM 6200B FA73985-6 CAS No. Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 99% 70-130% 6 64 of 82 FA73985 Blank Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2282-BS E102579.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-1 1, FA73985-12, FA73985-13, FA73985-14, FA73985-15 Spike BSP BSP CAS No. Compound ug/1 ug/l % Limits 67-64-1 Acetone 50 53.1 106 70-130 71-43-2 Benzene 10 9.9 99 70-130 108-86-1 Bromobenzene 10 9.1 91 70-130 74-97-5 Bromochloromethane 10 9.2 92 70-130 75-27-4 Bromodichloromethane 10 9.6 96 70-130 75-25-2 Bromoform 10 8.2 82 70-130 78-93-3 2-Butanone (MEK) 50 47.5 95 70-130 104-51-8 n-Butylbenzene 10 10.1 101 70-130 135-98-8 sec-Butylbenzene 10 10.2 102 70-130 98-06-6 tert-Butylbenzene 10 9.8 98 70-130 56-23-5 Carbon Tetrachloride 10 11.2 112 70-130 108-90-7 Chlorobenzene 10 9.5 95 70-130 75-00-3 Chloroethane 10 9.7 97 60-140 67-66-3 Chloroform 10 9.5 95 70-130 95-49-8 o-Chlorotoluene 10 9.4 94 70-130 106-43-4 p-Chlorotoluene 10 9.5 95 70-130 124-48-1 Dibromochloromethane 10 8.9 89 70-130 106-93-4 1,2-Dibromoethane 10 9.2 92 70-130 75-71-8 Dichlorodifluoromethane 10 7.9 79 60-140 95-50-1 1,2-Dichlorobenzene 10 9.3 93 70-130 541-73-1 1,3-Dichlorobenzene 10 9.5 95 70-130 106-46-7 1,4-Dichlorobenzene 10 9.2 92 70-130 75-34-3 1, 1 -Dichloroethane 10 9.9 99 70-130 107-06-2 1,2-Dichloroethane 10 9.9 99 70-130 75-35-4 1, 1 -Dichloroethylene 10 10.7 107 70-130 156-59-2 cis- 1, 2-Dichloroethylene 10 9.5 95 70-130 156-60-5 trans- 1, 2-Dichloroethylene 10 10.1 101 70-130 78-87-5 1,2-Dichloropropane 10 9.5 95 70-130 142-28-9 1,3-Dichloropropane 10 9.0 90 70-130 594-20-7 2,2-Dichloropropane 10 10.6 106 70-130 563-58-6 1, 1 -Dichloropropene 10 10.6 106 70-130 10061-01-5 cis- 1, 3-Dichloropropene 10 9.4 94 70-130 10061-02-6 trans- 1, 3-Dichloropropene 10 9.5 95 70-130 108-20-3 Di -Isopropyl Ether 10 9.8 98 70-130 64-17-5 Ethyl Alcohol 500 539 108 70-130 100-41-4 Ethlbenzene 10 9.9 99 70-130 * = Outside of Control Limits. 6 65 of 82 FA73985 Blank Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 2 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2282-BS E102579.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 Spike BSP BSP CAS No. Compound ug/1 ug/l % Limits 591-78-6 2-Hexanone 50 44.7 89 70-130 98-82-8 Isopropylbenzene 10 10 100 70-130 99-87-6 p-Isopropyltoluene 10 10 100 70-130 74-83-9 Methyl Bromide 10 9.4 94 60-140 74-87-3 Methyl Chloride 10 9.7 97 60-140 75-09-2 Methylene Chloride 10 9.5 95 70-130 108-10-1 4-Methyl-2-pentanone (MIBK) 50 51.9 104 70-130 1634-04-4 Methyl Tert Butyl Ether 10 10.2 102 70-130 91-20-3 Naphthalene 10 9.0 90 70-130 103-65-1 n-Propylbenzene 10 9.7 97 70-130 100-42-5 Styrene 10 9.5 95 70-130 630-20-6 1, 1, 1, 2-Tetrachloroethane 10 10.3 103 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130 127-18-4 Tetrachloroethylene 10 9.5 95 70-130 108-88-3 Toluene 10 9.7 97 70-130 87-61-6 1,2,3-Trichlorobenzene 10 8.8 88 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.2 92 70-130 71-55-6 1, 1, 1 -Trichloroethane 10 10.4 104 70-130 79-00-5 1,1,2-Trichloroethane 10 9.3 93 70-130 79-01-6 Trichloroethylene 10 9.8 98 70-130 75-69-4 Trichlorofluoromethane 10 11.5 115 60-140 96-18-4 1, 2,3 -Trichloropropane 10 9.0 90 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.4 94 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.7 97 70-130 108-05-4 Vinyl Acetate 50 52.9 106 70-130 75-01-4 Vinyl Chloride 10 9.8 98 60-140 m,p-Xylene 20 19.8 99 70-130 95-47-6 o-Xylene 10 9.6 96 70-130 1330-20-7 Xylene (total) 30 29.4 98 70-130 CAS No. Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 110% 70-130% 2037-26-5 Toluene-D8 100% 70-130% * = Outside of Control Limits. 6 66 of 82 FA73985 Blank Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 3 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2282-BS E102579.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 CAS No. Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 96% 70-130% * = Outside of Control Limits. 6 67 of 82 FA73985 Blank Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2716-BS A0221886.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: Method: SM 6200B FA73985-6 CAS No. Compound Spike BSP BSP ug/1 ug/l % Limits 67-64-1 Acetone 50 53.9 108 70-130 71-43-2 Benzene 10 9.4 94 70-130 108-86-1 Bromobenzene 10 9.6 96 70-130 74-97-5 Bromochloromethane 10 8.6 86 70-130 75-27-4 Bromodichloromethane 10 9.3 93 70-130 75-25-2 Bromoform 10 9.4 94 70-130 78-93-3 2-Butanone (MEK) 50 52.2 104 70-130 104-51-8 n-Butylbenzene 10 9.9 99 70-130 135-98-8 sec-Butylbenzene 10 10.1 101 70-130 98-06-6 tert-Butylbenzene 10 9.7 97 70-130 56-23-5 Carbon Tetrachloride 10 10.6 106 70-130 108-90-7 Chlorobenzene 10 9.5 95 70-130 75-00-3 Chloroethane 10 7.9 79 60-140 67-66-3 Chloroform 10 9.5 95 70-130 95-49-8 o-Chlorotoluene 10 10.3 103 70-130 106-43-4 p-Chlorotoluene 10 10.0 100 70-130 124-48-1 Dibromochloromethane 10 9.4 94 70-130 106-93-4 1,2-Dibromoethane 10 9.3 93 70-130 75-71-8 Dichlorodifluoromethane 10 7.7 77 60-140 95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130 541-73-1 1,3-Dichlorobenzene 10 9.8 98 70-130 106-46-7 1,4-Dichlorobenzene 10 9.6 96 70-130 75-34-3 1, 1 -Dichloroethane 10 9.8 98 70-130 107-06-2 1,2-Dichloroethane 10 9.4 94 70-130 75-35-4 1, 1 -Dichloroethylene 10 10.7 107 70-130 156-59-2 cis- 1, 2-Dichloroethylene 10 9.3 93 70-130 156-60-5 trans- 1, 2-Dichloroethylene 10 9.8 98 70-130 78-87-5 1,2-Dichloropropane 10 9.4 94 70-130 142-28-9 1,3-Dichloropropane 10 9.2 92 70-130 594-20-7 2,2-Dichloropropane 10 10.7 107 70-130 563-58-6 1, 1 -Dichloropropene 10 10.3 103 70-130 10061-01-5 cis- 1, 3-Dichloropropene 10 8.7 87 70-130 10061-02-6 trans- 1, 3-Dichloropropene 10 9.7 97 70-130 108-20-3 Di -Isopropyl Ether 10 9.5 95 70-130 64-17-5 Ethyl Alcohol 500 1150 230* 70-130 100-41-4 Ethlbenzene 10 10.1 101 70-130 * = Outside of Control Limits. 6 68 of 82 FA73985 Blank Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 2 of 3 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl TA2716-BS A0221886.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: FA73985-6 Spike BSP BSP CAS No. Compound ug/1 ug/l % Limits 591-78-6 2-Hexanone 50 48.5 97 70-130 98-82-8 Isopropylbenzene 10 9.9 99 70-130 99-87-6 p-Isopropyltoluene 10 9.5 95 70-130 74-83-9 Methyl Bromide 10 8.6 86 60-140 74-87-3 Methyl Chloride 10 9.3 93 60-140 75-09-2 Methylene Chloride 10 8.9 89 70-130 108-10-1 4-Methyl-2-pentanone (MIBK) 50 48.0 96 70-130 1634-04-4 Methyl Tert Butyl Ether 10 8.9 89 70-130 91-20-3 Naphthalene 10 7.7 77 70-130 103-65-1 n-Propylbenzene 10 10.2 102 70-130 100-42-5 Styrene 10 8.8 88 70-130 630-20-6 1, 1, 1, 2-Tetrachloroethane 10 9.9 99 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 9.9 99 70-130 127-18-4 Tetrachloroethylene 10 10.5 105 70-130 108-88-3 Toluene 10 9.6 96 70-130 87-61-6 1,2,3-Trichlorobenzene 10 8.7 87 70-130 120-82-1 1,2,4-Trichlorobenzene 10 8.6 86 70-130 71-55-6 1, 1, 1 -Trichloroethane 10 10.3 103 70-130 79-00-5 1,1,2-Trichloroethane 10 9.6 96 70-130 79-01-6 Trichloroethylene 10 9.7 97 70-130 75-69-4 Trichlorofluoromethane 10 8.9 89 60-140 96-18-4 1, 2,3 -Trichloropropane 10 9.6 96 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.2 92 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.6 96 70-130 108-05-4 Vinyl Acetate 50 49.4 99 70-130 75-01-4 Vinyl Chloride 10 7.8 78 60-140 m,p-Xylene 20 20.8 104 70-130 95-47-6 o-Xylene 10 9.9 99 70-130 1330-20-7 Xylene (total) 30 30.6 102 70-130 CAS No. Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 100% 70-130% 17060-07-0 1,2-Dichloroethane-D4 108% 70-130% 2037-26-5 Toluene-D8 102% 70-130% * = Outside of Control Limits. Method: SM 6200B 6 69 of 82 FA73985 Blank Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 3 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2716-BS A0221886.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: Method: SM 6200B FA73985-6 CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene * = Outside of Control Limits. BSP Limits 98% 70-130% 6 70 of 82 FA73985 Matrix Spike/Matrix Spike Duplicate Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA73985-lMS E102591.1) 5 04/07/20 AB n/a n/a VE2282 FA73985-1MSD E102592.1) 5 04/07/20 AB n/a n/a VE2282 FA73985-1 E102583.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-1 1, FA73985-12, FA73985-13, FA73985-14, FA73985-15 FA73985-1 Spike MS MS Spike MSD MSD Limits CAS No. Compound ug/l Q ug/l ug/l % ug/l ug/l % RPD Rec/RPD 67-64-1 Acetone ND 250 245 98 250 261 104 6 70-130/20 71-43-2 Benzene ND 50 49.2 98 50 48.3 97 2 70-130/20 108-86-1 Bromobenzene ND 50 44.8 90 50 43.7 87 2 70-130/20 74-97-5 Bromochloromethane ND 50 44.3 89 50 42.8 86 3 70-130/20 75-27-4 Bromodichloromethane ND 50 46.4 93 50 45.4 91 2 70-130/20 75-25-2 Bromoform ND 50 36.6 73 50 34.7 69* 5 70-130/20 78-93-3 2-Butanone (MEK) ND 250 214 86 250 227 91 6 70-130/20 104-51-8 n-Butylbenzene ND 50 51.6 103 50 48.4 97 6 70-130/20 135-98-8 sec-Butylbenzene ND 50 51.8 104 50 49.3 99 5 70-130/20 98-06-6 tert-Butylbenzene ND 50 50.1 100 50 47.8 96 5 70-130/20 56-23-5 Carbon Tetrachloride ND 50 57.9 116 50 55.2 110 5 70-130/20 108-90-7 Chlorobenzene ND 50 46.8 94 50 45.5 91 3 70-130/20 75-00-3 Chloroethane ND 50 50.2 100 50 52.9 106 5 60-140/20 67-66-3 Chloroform ND 50 47.9 96 50 46.6 93 3 70-130/20 95-49-8 o-Chlorotoluene ND 50 47.8 96 50 45.5 91 5 70-130/20 106-43-4 p-Chlorotoluene ND 50 47.0 94 50 46.0 92 2 70-130/20 124-48-1 Dibromochloromethane ND 50 40.7 81 50 40.8 82 0 70-130/20 106-93-4 1,2-Dibromoethane ND 50 43.0 86 50 41.8 84 3 70-130/20 75-71-8 Dichlorodifluoromethane ND 50 42.2 84 50 41.4 83 2 60-140/20 95-50-1 1,2-Dichlorobenzene ND 50 47.2 94 50 45.0 90 5 70-130/20 541-73-1 1,3-Dichlorobenzene ND 50 48.3 97 50 46.4 93 4 70-130/20 106-46-7 1,4-Dichlorobenzene ND 50 46.4 93 50 44.7 89 4 70-130/20 75-34-3 1, 1 -Dichloroethane ND 50 51.2 102 50 48.9 98 5 70-130/20 107-06-2 1,2-Dichloroethane ND 50 49.8 100 50 47.7 95 4 70-130/20 75-35-4 1, 1 -Dichloroethylene ND 50 54.6 109 50 52.7 105 4 70-130/20 156-59-2 cis- 1, 2-Dichloroethylene ND 50 46.8 94 50 45.9 92 2 70-130/20 156-60-5 trans- 1, 2-Dichloroethylene ND 50 51.9 104 50 50.1 100 4 70-130/20 78-87-5 1,2-Dichloropropane ND 50 46.9 94 50 46.2 92 2 70-130/20 142-28-9 1,3-Dichloropropane ND 50 43.2 86 50 42.5 85 2 70-130/20 594-20-7 2,2-Dichloropropane ND 50 52.9 106 50 49.7 99 6 70-130/20 563-58-6 1, 1 -Dichloropropene ND 50 53.4 107 50 51.1 102 4 70-130/20 10061-01-5 cis- 1, 3-Dichloropropene ND 50 41.4 83 50 40.2 80 3 70-130/20 10061-02-6 trans- 1, 3-Dichloropropene ND 50 44.8 90 50 43.4 87 3 70-130/20 108-20-3 Di -Isopropyl Ether ND 50 49.8 100 50 48.0 96 4 70-130/20 64-17-5 Ethyl Alcohol ND 2500 2470 99 2500 2280 91 8 70-130/20 100-41-4 Ethlbenzene ND 50 49.7 99 50 47.6 95 4 70-130/20 * = Outside of Control Limits. 01 71 of 82 FA73985 CAS No. 591-78-6 98-82-8 99-87-6 74-83-9 74-87-3 75-09-2 108-10-1 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 95-47-6 1330-20-7 CAS No. Matrix Spike/Matrix Spike Duplicate Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 2 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA73985-lMS E102591.1) 5 04/07/20 AB n/a n/a VE2282 FA73985-1MSD E102592.1) 5 04/07/20 AB n/a n/a VE2282 FA73985-1 E102583.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-1 1, FA73985-12, FA73985-13, FA73985-14, FA73985-15 FA73985-1 Spike MS MS Spike MSD MSD Limits Compound ug/l Q ug/l ug/l % ug/l ug/l % RPD Rec/RPD 2-Hexanone ND 250 206 82 250 214 86 4 70-130/20 Isopropylbenzene 0.17 J 50 50.3 100 50 48.9 97 3 70-130/20 p-Isopropyltoluene ND 50 50.1 100 50 48.2 96 4 70-130/20 Methyl Bromide ND 50 49.1 98 50 46.8 94 5 60-140/20 Methyl Chloride ND 50 49.8 100 50 49.6 99 0 60-140/20 Methylene Chloride ND 50 54.0 108 50 51.1 102 6 70-130/20 4-Methyl-2-pentanone (MIBK) ND 250 242 97 250 251 100 4 70-130/20 Methyl Tert Butyl Ether 4.3 50 53.4 98 50 52.2 96 2 70-130/20 Naphthalene ND 50 42.8 86 50 39.9 80 7 70-130/20 n-Propylbenzene ND 50 49.6 99 50 47.1 94 5 70-130/20 Styrene ND 50 26.7 53* 50 20.8 42* 25* 70-130/20 1, 1, 1, 2-Tetrachloroethane ND 50 52.0 104 50 49.7 99 5 70-130/20 1,1,2,2-Tetrachloroethane ND 50 47.6 95 50 46.0 92 3 70-130/20 Tetrachloroethylene ND 50 46.8 94 50 45.1 90 4 70-130/20 Toluene ND 50 48.4 97 50 46.7 93 4 70-130/20 1,2,3-Trichlorobenzene ND 50 42.4 85 50 39.7 79 7 70-130/20 1,2,4-Trichlorobenzene ND 50 44.0 88 50 41.2 82 7 70-130/20 1, 1, 1 -Trichloroethane ND 50 53.7 107 50 51.2 102 5 70-130/20 1,1,2-Trichloroethane ND 50 45.4 91 50 43.6 87 4 70-130/20 Trichloroethylene 0.18 J 50 48.4 96 50 46.2 92 5 70-130/20 Trichlorofluoromethane 2.6 50 64.4 124 50 61.4 118 5 60-140/20 1, 2,3 -Trichloropropane ND 50 45.3 91 50 43.4 87 4 70-130/20 1,2,4-Trimethylbenzene ND 50 47.4 95 50 45.6 91 4 70-130/20 1, 3,5 -Trimethylbenzene ND 50 49.4 99 50 46.8 94 5 70-130/20 Vinyl Acetate ND 250 198 79 250 187 75 6 70-130/20 Vinyl Chloride ND 50 50.4 101 50 49.9 100 1 60-140/20 m,p-Xylene ND 100 99.0 99 100 96.2 96 3 70-130/20 o-Xylene ND 50 48.5 97 50 46.6 93 4 70-130/20 Xylene (total) ND 150 147 98 150 143 95 3 70-130/20 Surrogate Recoveries MS 1868-53-7 Dibromofluoromethane 105% 17060-07-0 1,2-Dichloroethane-D4 114% 2037-26-5 Toluene-D8 100% * = Outside of Control Limits. MSD FA73985-1 Limits 104% 102% 70-130% 112% 108% 70-130% 100% 99% 70-130% 6 72 of 82 FA73985 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA73985-lMS E102591.1) 5 04/07/20 AB n/a n/a VE2282 FA73985-1MSD E102592.1) 5 04/07/20 AB n/a n/a VE2282 FA73985-1 E102583.1) 1 04/07/20 AB n/a n/a VE2282 The QC reported here applies to the following samples: Method: SM 6200B FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 CAS No. Surrogate Recoveries MS MSD FA73985-1 Limits 460-00-4 4-Bromofluorobenzene 97% 97% 100% 70-130% * = Outside of Control Limits. 6 73 of 82 FA73985 Matrix Spike/Matrix Spike Duplicate Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA73985-6MS A0221896.1) 5 04/08/20 AB n/a n/a VA2716 FA73985-6MSD A0221897.1) 5 04/08/20 AB n/a n/a VA2716 FA73985-6 A0221889.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: FA73985-6 CAS No. Compound FA73985-6 Spike MS ug/l Q ug/l ug/l Method: SM 6200B MS Spike MSD MSD Limits % ug/l ug/l % RPD Rec/RPD 67-64-1 Acetone ND 250 248 99 250 241 96 3 70-130/20 71-43-2 Benzene ND 50 50.2 100 50 49.5 99 1 70-130/20 108-86-1 Bromobenzene ND 50 52.0 104 50 52.0 104 0 70-130/20 74-97-5 Bromochloromethane ND 50 45.9 92 50 45.2 90 2 70-130/20 75-27-4 Bromodichloromethane ND 50 48.4 97 50 47.9 96 1 70-130/20 75-25-2 Bromoform ND 50 47.4 95 50 46.0 92 3 70-130/20 78-93-3 2-Butanone (MEK) ND 250 239 96 250 244 98 2 70-130/20 104-51-8 n-Butylbenzene ND 50 52.8 106 50 52.0 104 2 70-130/20 135-98-8 sec-Butylbenzene ND 50 54.6 109 50 53.7 107 2 70-130/20 98-06-6 tert-Butylbenzene ND 50 52.9 106 50 52.8 106 0 70-130/20 56-23-5 Carbon Tetrachloride ND 50 54.0 108 50 53.3 107 1 70-130/20 108-90-7 Chlorobenzene ND 50 50.2 100 50 50.2 100 0 70-130/20 75-00-3 Chloroethane ND 50 41.6 83 50 53.8 108 26* 60-140/20 67-66-3 Chloroform ND 50 49.1 98 50 48.4 97 1 70-130/20 95-49-8 o-Chlorotoluene ND 50 55.6 111 50 55.6 111 0 70-130/20 106-43-4 p-Chlorotoluene ND 50 55.0 110 50 53.9 108 2 70-130/20 124-48-1 Dibromochloromethane ND 50 47.9 96 50 47.1 94 2 70-130/20 106-93-4 1,2-Dibromoethane ND 50 50.4 101 50 49.8 100 1 70-130/20 75-71-8 Dichlorodifluoromethane ND 50 37.6 75 50 42.4 85 12 60-140/20 95-50-1 1,2-Dichlorobenzene ND 50 50.1 100 50 50.0 100 0 70-130/20 541-73-1 1,3-Dichlorobenzene ND 50 53.0 106 50 52.0 104 2 70-130/20 106-46-7 1,4-Dichlorobenzene ND 50 50.6 101 50 50.4 101 0 70-130/20 75-34-3 1, 1 -Dichloroethane ND 50 51.2 102 50 50.3 101 2 70-130/20 107-06-2 1,2-Dichloroethane ND 50 47.0 94 50 46.0 92 2 70-130/20 75-35-4 1, 1 -Dichloroethylene ND 50 54.0 108 50 53.2 106 1 70-130/20 156-59-2 cis- 1, 2-Dichloroethylene ND 50 50.1 100 50 49.1 98 2 70-130/20 156-60-5 trans- 1, 2-Dichloroethylene ND 50 50.9 102 50 50.4 101 1 70-130/20 78-87-5 1,2-Dichloropropane ND 50 49.1 98 50 48.3 97 2 70-130/20 142-28-9 1,3-Dichloropropane ND 50 48.7 97 50 47.8 96 2 70-130/20 594-20-7 2,2-Dichloropropane ND 50 54.1 108 50 55.9 112 3 70-130/20 563-58-6 1, 1 -Dichloropropene ND 50 55.6 ill 50 54.0 108 3 70-130/20 10061-01-5 cis- 1, 3-Dichloropropene ND 50 43.0 86 50 42.8 86 0 70-130/20 10061-02-6 trans- 1, 3-Dichloropropene ND 50 48.5 97 50 49.7 99 2 70-130/20 108-20-3 Di -Isopropyl Ether ND 50 49.0 98 50 47.7 95 3 70-130/20 64-17-5 Ethyl Alcohol ND 2500 5270 211* 2500 4080 163* 25* 70-130/20 100-41-4 Ethlbenzene ND 50 53.8 108 50 53.0 106 1 70-130/20 * = Outside of Control Limits. 01 74 of 82 FA73985 Matrix Spike/Matrix Spike Duplicate Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 2 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA73985-6MS A0221896.1) 5 04/08/20 AB n/a n/a VA2716 FA73985-6MSD A0221897.1) 5 04/08/20 AB n/a n/a VA2716 FA73985-6 A0221889.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: FA73985-6 CAS No. Compound FA73985-6 Spike MS ug/l Q ug/l ug/l Method: SM 6200B MS Spike MSD MSD Limits % ug/l ug/l % RPD Rec/RPD 591-78-6 2-Hexanone ND 250 220 88 250 228 91 4 70-130/20 98-82-8 Isopropylbenzene ND 50 53.7 107 50 53.1 106 1 70-130/20 99-87-6 p-Isopropyltoluene ND 50 52.5 105 50 51.5 103 2 70-130/20 74-83-9 Methyl Bromide ND 50 46.3 93 50 52.8 106 13 60-140/20 74-87-3 Methyl Chloride ND 50 42.5 85 50 45.5 91 7 60-140/20 75-09-2 Methylene Chloride ND 50 44.8 90 50 43.2 86 4 70-130/20 108-10-1 4-Methyl-2-pentanone (MIBK) ND 250 221 88 250 228 91 3 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 50 46.9 94 50 47.7 95 2 70-130/20 91-20-3 Naphthalene ND 50 43.0 86 50 40.9 82 5 70-130/20 103-65-1 n-Propylbenzene ND 50 55.7 111 50 54.9 110 1 70-130/20 100-42-5 Styrene ND 50 48.1 96 50 47.7 95 1 70-130/20 630-20-6 1, 1, 1, 2-Tetrachloroethane ND 50 51.4 103 50 50.7 101 1 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 50 51.8 104 50 51.2 102 1 70-130/20 127-18-4 Tetrachloroethylene ND 50 55.5 111 50 55.1 110 1 70-130/20 108-88-3 Toluene ND 50 51.7 103 50 51.1 102 1 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 50 45.1 90 50 43.8 88 3 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 50 46.4 93 50 44.7 89 4 70-130/20 71-55-6 1, 1, 1 -Trichloroethane ND 50 53.8 108 50 53.0 106 1 70-130/20 79-00-5 1,1,2-Trichloroethane ND 50 50.1 100 50 49.9 100 0 70-130/20 79-01-6 Trichloroethylene ND 50 50.7 101 50 50.7 101 0 70-130/20 75-69-4 Trichlorofluoromethane ND 50 43.8 88 50 50.9 102 15 60-140/20 96-18-4 1, 2,3 -Trichloropropane ND 50 50.5 101 50 50.1 100 1 70-130/20 95-63-6 1,2,4-Trimethylbenzene ND 50 49.9 100 50 49.5 99 1 70-130/20 108-67-8 1, 3,5 -Trimethylbenzene ND 50 52.6 105 50 51.9 104 1 70-130/20 108-05-4 Vinyl Acetate ND 250 235 94 250 243 97 3 70-130/20 75-01-4 Vinyl Chloride ND 50 39.9 80 50 45.3 91 13 60-140/20 m,p-Xylene ND 100 112 112 100 ill ill 1 70-130/20 95-47-6 o-Xylene ND 50 54.3 109 50 53.7 107 1 70-130/20 1330-20-7 Xylene (total) ND 150 166 ill 150 164 109 1 70-130/20 CAS No. Surrogate Recoveries MS MSD FA73985-6 Limits 1868-53-7 Dibromofluoromethane 97% 97% 103% 70-130% 17060-07-0 1,2-Dichloroethane-D4 99% 98% 112% 70-130% 2037-26-5 Toluene-D8 101% 101% 101% 70-130% * = Outside of Control Limits. 6 75 of 82 FA73985 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA73985-6MS A0221896.1) 5 04/08/20 AB n/a n/a VA2716 FA73985-6MSD A0221897.1) 5 04/08/20 AB n/a n/a VA2716 FA73985-6 A0221889.1) 1 04/08/20 AB n/a n/a VA2716 The QC reported here applies to the following samples: Method: SM 6200B FA73985-6 CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene * = Outside of Control Limits. MS MSD FA73985-6 Limits 101% 101% 97% 70-130% 6 76 of 82 FA73985 i SG$ Orlando, FL MW Section 6 GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries 0 6 77 of 82 FA73985 Method Blank Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP79697-MB DD111423.D 1 04/06/20 KB 04/06/20 OP79697 GDD3206 The QC reported here applies to the following samples: Method: EPA 504.1 FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-6, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 CAS No. Compound Result RL MDL Units Q 106-93-4 1,2-Dibromoethane ND 0.020 0.010 ug/1 CAS No. Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 112% 63-137% 6 78 of 82 FA73985 Blank Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl )P79697-BS DD111421.D 1 04/06/20 KB 04/06/20 OP79697 GDD3206 The QC reported here applies to the following samples: Method: EPA 504.1 FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-6, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 Spike BSP BSP CAS No. Compound ug/l ug/l % Limits 106-93-4 1,2-Dibromoethane 0.25 0.30 120 70-130 CAS No. Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 126% 63-137% * = Outside of Control Limits. 6 79 of 82 FA73985 Blank Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl )P79697-BS2 DD111422.D 1 04/06/20 KB 04/06/20 OP79697 GDD3206 The QC reported here applies to the following samples: Method: EPA 504.1 FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-6, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 Spike BSP BSP CAS No. Compound ug/l ug/l % Limits 106-93-4 1,2-Dibromoethane 0.25 0.27 108 70-130 CAS No. Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 112% 63-137% * = Outside of Control Limits. 6 80 of 82 FA73985 Matrix Spike Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl )P79697-MS DD111443.D 1 04/06/20 KB 04/06/20 OP79697 GDD3206 'A73985-12 DD111437.D 1 04/06/20 KB 04/06/20 OP79697 GDD3206 The QC reported here applies to the following samples: Method: EPA 504.1 FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-6, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 FA73985-12 Spike MS MS CAS No. Compound ug/1 Q ug/l ug/l % Limits 106-93-4 1,2-Dibromoethane ND 0.231 0.22 95 70-130 CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene * = Outside of Control Limits. MS FA73985-12 Limits 101% 88% 63-137% 6 81 of 82 FA73985 Duplicate Summary Job Number: FA73985 Account: ATCNCC ATC Group Services LLC Project: RM 2751; 8425 Hwy 49 N, Mt Pleasant, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl )P79697-DUP DD111444.D 1 04/07/20 KB 04/06/20 OP79697 GDD3206 'A73985-13 DD111438.D 1 04/06/20 KB 04/06/20 OP79697 GDD3206 The QC reported here applies to the following samples: Method: EPA 504.1 FA73985-1, FA73985-2, FA73985-3, FA73985-4, FA73985-5, FA73985-6, FA73985-7, FA73985-8, FA73985-9, FA73985-10, FA73985-11, FA73985-12, FA73985-13, FA73985-14, FA73985-15 FA73985-13 DUP CAS No. Compound ug/1 Q ug/l Q RPD Limits 106-93-4 1,2-Dibromoethane ND ND nc 25 CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene * = Outside of Control Limits. DUP FA73985-13 Limits 108% 110% 63-137% 6 82 of 82 FA73985 Beverly, Trudy From: Jason Whittle <jason.whittle@atcgs.com> Sent: Friday, August 21, 2020 10:51 AM To: Beverly, Trudy; Brittney Windsand Cc: Tesa Graff Subject: RE: [External] RE: RM 2751- Report for submittal- Incident 14645 External e aW111111111111111Lclick links or open attachments unless you verify. Send all suspicious email as an attachment to �llllllbort.spamftc.gov Thank you Trudy. I apologize for the inconvenience. Have a great weekend. -Jake From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Friday, August 21, 2020 10:44 AM To: Brittney Windsand <brittney.windsand@atcgs.com>; Jason Whittle <jason.whittle@atcgs.com> Cc: Tesa Graff <tesa.graff@atcgs.com> Subject: RE: [External] RE: RM 2751- Report for submittal- Incident 14645 Brittney — Thank you for the tracking information. Jason — The UST Section no longer requires a hard copy as of March 2020. We are still working remotely due to Covid concerns. You should always get a received email response from me when you submit a report for review by email. I'll get the report reviewed by the end of next week and email you an acknowledgement of report receipt letter or NORR. Have a great weekend, Trudy opf 5Q�xk_., Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management ,::5:-D E North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office Ikparmr�e ment�l6w 704.235.2182 (Office) Trudy. B everlykncdenr. g ov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-proeram INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httDs:Hdeu.ne. aov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaaement-eis-mans File Review Procedures: https:Hdcq.nc. gov/about/divisions/waste-manaaement/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): httns://deo.nc. aov/about/divisions/waste-manaeement/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https:Hfiles.ne.gov/ncdeg[Waste%20Management/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.pdf https:Hfiles.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%20filc%20names%20for%2OLaserfiche.docx From: Brittney Windsand[mailto:brittney.windsand@atcgs.com] Sent: Friday, August 21, 2020 10:15 AM To: Jason Whittle <jason.whittle@atcgs.com>; Beverly, Trudy <trudy.beverly@ncdenr.gov> Cc: Tesa Graff <tesa.graff@atcgs.com> Subject: [External] RE: RM 2751- Report for Submittal- Incident 14645 External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to kort.spam@nc.gov Hello, here is the tracking information for RM2751 Tracking - Internet Explorer idicn:trac1c tkrarknumL. E- u565547i1jI20 52$&cntry_codezus&language=en8tcticnttvpe:fhist IRACKANOTHDIR SHIPMENT 770565547009 Delivered Tuesday 222 t 1 :1 am DELIV ER ED Signed for by: D JEi EFERE Fit F;_4i F*xf Fiml k--4 - F=_d - F,s<f F---{I FROM ATC GROUP SERVICES INC Victoria Poole 7606 Whr tehall Executive Center Dr. Suite 600 CHARLOTTE, INC US 28273 7D4 529-320%% Travel HW y GET STATUS UPDATES OBTAIN PROOF OF DELIVERY Shipment Facts TO DEQ - Df, Trudy 81 610 East Ce Su ite MOORESVILLE 704 529-: 9 Brittney Windsand I PROJECT ASSISTANT I ATC Group Services LLC Direct +1 704 529 3200 ETC 7606 Whitehall Executive Center Drive Suite 800 1 Charlotte, NC 28273 brittney.windsand(�batcgs.com I www.atcaroupservices.com This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not reflect the views or opinions of ATC. From: Jason Whittle <lason.whittle@atcgs.com> Sent: Friday, August 21, 2020 10:11 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Cc: Tesa Graff <tesa.graff@atcgs.com>; Brittney Windsand <brittney.windsand@atcgs.com> Subject: FW: RM 2751- Report for submittal- Incident 14645 Sorry Trudy, I usually email these reports and did not in this case? I have internal email correspondence below that shows the approximate hard copy mail date. We will see if we can find the FedEx tracking number and delivery information. From: Jason Whittle Sent: Thursday, May 28, 2020 8:15 AM To: Brittney Windsand <brittney.windsand@atcgs.com> Subject: RM 2751- Report for submittal Good Morning Brittney, Can you prep the attached report for submittal? Project number is: P66 2751015 It can ship slowest cheapest way FedEx overnight to MRO. Thanks. Jason (Jake) Whittle, CHMM I PROJECT MANAGER I ATC Group Services LLC +1 704 972 4082 1 +1 704 236 5323 mobile 7606 Whitehall Exec. Center Dr., Suite 800 1 Charlotte, NC 28273 +1 704 529 3272 fax I iason.whittle@atcassociates.com I www.atcgroupservices.com This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not reflect the views or opinions of ATC. Beverly, Trudy From: Beverly, Trudy Sent: Friday, August 21, 2020 10:44 AM To: Jason Whittle Cc: Tesa Graff; Brittney Windsand Subject: RE: [External] M-4471_14645 - Report Receipt Confirmation- May 2020 Received. Trudy From: Jason Whittle [mailto:jason.whittle@atcgs.com] Sent: Friday, August 21, 2020 10:13 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Cc: Tesa Graff <tesa.graff@atcgs.com>; Brittney Windsand <brittney.windsand@atcgs.com> Subject: RE: [External] M-4471_14645 - Report Receipt Confirmation- May 2020 External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to report.spam@nc.gov Sorry, Here's the final version with stamp/seal. From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Friday, August 21, 2020 10:08 AM To: Jason Whittle <jason.whittle@atcgs.com> Cc: Tesa Graff <tesa.graff@atcgs.com> Subject: RE: [External] M-4471_14645 - Report Receipt Confirmation- May 2020 The copy that you just emailed is not signed and stamped by a licensed geologist or professional engineer. Trudy From: Beverly, Trudy Sent: Friday, August 21, 2020 10:05 AM To: Jason Whittle <lason.whittle@atcgs.com> Cc: Tesa Graff <tesa.graff@atcgs.com> Subject: RE: [External] M-4471_14645 - Report Receipt Confirmation- May 2020 Jason, I don't have any record of the report being submitted in my email. The UST section transitioned to electronic submittals in March 2020. What day did you send the report so that I can recheck my emails? Trudy Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy.BeverlyL&ncdenr. gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httDs://deu.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-maps File Review Procedures: https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): httns://deu.nc. gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https:Hfiles.nc.gov/ncdeci/W aste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.pdf https:Hfiles.nc.gov/ncdeq/Waste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%2Ofor%2OLaserficlie.do From: Jason Whittle [mailto:iason.whittle@atcgs.com] Sent: Friday, August 21, 2020 9:58 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Cc: Tesa Graff <tesa.graff@atcgs.com> Subject: [External] M-4471_14645 - Report Receipt Confirmation- May 2020 External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to kort.spam@nc.gov Hi Trudy, We are working on a Trust Fund claim and are in need of a report receipt and approval date for the attached report submitted in May. It may have been sent to me but I cannot locate it. Do you have a record of this information you can send us? Thanks, -Jake Jason (Jake) Whittle, CHMM I PROJECT MANAGER I ATC Group Services LLC +1 704 972 4082 i +1 704 236 5323 mobile 7606 Whitehall Exec. Center Dr., Suite 800 1 Charlotte, NC 28273 +1 704 529 3272 fax I jason.whittle@atcassociates.com I www.atcgroupservices.com This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not reflect the views or opinions of ATC.