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HomeMy WebLinkAboutMO-27893_47196_CA_IAR_20200812_Inital Abatement Reportwood. INITIAL ABATEMENT ACTION REPORT 4732 WEST SUGAR CREEK ROAD PARCEL 4732 WEST SUGAR CREEK ROAD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA 28269 PREPARED FOR: CITY OF CHARLOTTE ENVIRONMENTAL SERVICES ENGINEERING AND PROPERTY MANAGMENT 600 EAST FOURTH STREET CHARLOTTE, NORTH CAROLINA 28202 PREPARED BY: WOOD ENVIRONMENT & INFRASTRUCTURE SOLUTIONS, INC. 2801 YORKMONT ROAD, SUITE 100 CHARLOTTE, NORTH CAROLINA 28208 AUGUST 12, 2020 WOOD PROJECT: 1238-20-0028 wood. Wood Environment & Infrastructure Solutions, Inc. 2801 Yorkmont Road, Suite 100 Charlotte, North Carolina 28208 T:704-357-8600 www.woodpic.com August 12, 2020 Ms. Trudy Beverly, LG North Carolina Department of Environmental Quality Mooresville Regional Office UST Section 610 East Center Avenue Mooresville, North Carolina 28115 Subject: Initial Abatement Action Report 4732 West Sugar Creek Road Parcel Charlotte, Mecklenburg County, North Carolina 28269 Wood Project: 1238-20-0028 Dear Ms. Beverly: On behalf of the City of Charlotte (Property Owner), Wood Environment & Infrastructure Solutions, Inc. (Wood) is submitting the enclosed Initial Abatement Action Report for the facility located at 4732 West Sugar Creek Road, Charlotte, Mecklenburg County, North Carolina 28269 (the Site). The report was prepared in general accordance with the North Carolina Department of Environmental Quality (NCDEQ), UST Section Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases (March 1, 2007 version, Change 9, effective February 1, 2019). This report includes a description of the field activities and the results obtained. Sincerely, Wood Environment & Infrastructure Solutions, Inc. Andrew J. Frantz, REM Senior Scientist Enclosure Cc: Mr. Steve Gucciardi, City of Charlotte *&-v1— cae, Helen P. Corley, LG, BCES Principal Hydrogeologist Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 A. SITE INFORMATION 1. Site Identification Date of Report: August 12, 2020 Facility I.D.: N/A UST Incident Number: Pending Site Risk: Pending Site Name: 4732 West Sugar Creek Road Parcel Street Address: 4732 West Sugar Creek Road City: Charlotte Zip Code: 28269 County: Mecklenburg Description of Geographical Data Point: Tank basin Location Method: GPS Latitude: 35.317516" N Longitude:-80.806512" W 2. Information about Contacts Associated with the UST System UST Owner: City of Charlotte Address: 600 East Fourth Street, Charlotte, North Carolina Telephone: 704-651-4366 UST Operator: Clarence and Ulysses Spears Address: 4732 West Sugar Creek Road, Charlotte, North Carolina Telephone: Unknown Property Owner: City of Charlotte Address: 600 East Fourth Street, Charlotte, North Carolina Telephone: 704-651-4366 Property Occupant: Vacant Address: 4732 West Sugar Creek Road, Charlotte, North Carolina Telephone: Consultant: Wood Environment & Infrastructure Solutions, Inc. Address: 2801 Yorkmont Road, Suite 100, Charlotte, North Carolina 28208 Telephone: 704-357-8600 Analytical Laboratory: Waypoint Analytical State Certification No.: 402 Address: 229 Springbrook Road, Charlotte, North Carolina 28224 Telephone: 704-529-6364 Initial Abatement Action Report — 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 3. Information about Release Date Discovered: June 10, 2020 Estimated Quantity of Release: Unknown Cause of Release: Corrosion Source of Release: UST Sizes and Contents of Tanks or Other Containment from which Release Occurred: 250-gallon heating oil UST 4. Certification I, Helen P. Corley, a do certify. knowledg Professional Geologist for Wood Environment & Infrastructure Solutions, Inc., (lhpntained in this report is correct and accurate to the best of my .°� -�C�NS�c' . 9 ! L �F G) ••, Ot 0 (Please affix Stamp'a'riT 566ature) !� d (Dat ) Wood Environment & Infrastructure Solutions, Inc. is licensed to practice geology (C-2478) and engineering (F-1253) in North Carolina. Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 B. EXECUTIVE SUMMARY The Site is Mecklenburg County Tax Parcel 043-106-27, which encompasses approximately 19.42 acres, and is located in a mostly residential area. The City of Charlotte and its tank removal contractor (W.C. Black and Sons, Inc.) mobilized to the Site on June 10, 2020 to remove the 250-gallon heating oil UST. Reportedly, prior to removal, the top of the UST was uncovered by removing the overburden from above the tank. After the tank was uncovered, the liquid was removed from the tank by a vacuum truck. Heating oil and petroleum contact water (PCW) was pumped from the tank into a vacuum truck for off -Site disposal. Following removal of the liquid from the tank, the soils were observed to be impacted (staining and petroleum odor) and stockpiled on plastic. Once the UST was free from the surrounding soil, it was removed from the excavation and placed on plastic. Several areas of corrosion and pitting were observed on the removed UST. On June 11, 2020, Wood personnel mobilized to the Site to collect the UST closure soil samples from the excavation (S-1 and S-2) and one soil sample from the stockpiled soil (S-3) for disposal purposes. The laboratory analytical results identified TPH DRO and TPH GRO concentrations in samples S-1 and S-2, which exceeded the State Action Levels for TPH DRO of 100 milligrams per kilogram (mg/kg) and for TPH GRO of 50 mg/kg. In addition, TPH DRO was identified in sample S-3 at a concentration above State Action Level for TPH DRO. The City of Charlotte requested that Wood personnel return to the Site on July 7, 2020 to oversee petroleum -impacted soil over -excavation from the excavation. PID field screening readings, initially, and the results of the laboratory analyses of sidewall and base confirmation soil samples, eventually, were used to determine that soil over -excavation was complete. Based on the real-time PID screenings, the excavation was extended to an approximate depth of 7.5 feet and to an approximate length and width of 12 feet and 10 feet, respectively. The confirmation sidewall soil samples (SW-1, SW-2, SW-3, and SW-4) were collected from the sidewalls at an approximate depth of 4.5 feet and the confirmation base soil sample (Base) was collected from an approximate depth of 7.5 feet. The analyses of the confirmation soil samples did not identify concentrations of petroleum constituents, which exceeded their respective North Carolina Department of Environmental Quality (NCDEQ) Maximum Soil Contaminant Concentrations (MSCCs). A total of approximately 51.34 tons of petroleum -impacted soil was removed from the excavation and disposed of off -Site. Groundwater or bedrock were not encountered in the excavation. Based on the results of the confirmation soil sampling, Wood recommends no further action in regards to the release from the 250-gallon heating oil UST. Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 C. TABLE OF CONTENTS A. SITE INFORMATION...........................................................................................................i 1. Site Identification..........................................................................................................................................i 2. Information about Contacts Associated with the UST System...........................................................i 3. Information about Release.........................................................................................................................ii 4. Certification...................................................................................................................................................ii B. EXECUTIVE SUMMARY..................................................................................................... iii C. TABLE OF CONTENTS....................................................................................................... iv D. SITE HISTORY AND CHARACTERIZATION.......................................................................1 1. UST Owner/Operator Information...........................................................................................................1 2. UST Information...........................................................................................................................................1 3. Description of the Release..........................................................................................................................1 4. Description of Site Characteristics............................................................................................................1 E. UST CLOSURE REPORT......................................................................................................3 F. INITIAL RESPONSE AND ABATEMENT ACTION..............................................................5 G. EXCAVATION OF CONTAMINATED SOIL.........................................................................6 1. Determination of the Source and Extent of Soil Contamination......................................................6 2. Excavation Process.......................................................................................................................................6 H. CONCLUSIONS AND RECOMMENDATIONS....................................................................7 FIGURES Figure 1 Site Location Map Figure 2 Project Area on USGS Topo Figure 3 Site Map Figure 4 Excavation Layout TABLES Table 1 Site History — UST System Owner/Operator and Other Responsible Party Information Table 2 Site History— UST System and Release Information Table 3 UST Closure Soil Sampling Results Table 4 Summary of UST Confirmation Soil Sampling Results iv Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 APPENDICES Appendix A Photographs Appendix B Tank Disposal Certificate and Liquid/Soil Disposal Manifests Appendix C UST Forms Appendix D Laboratory Analytical Reports and Chain -of -Custody Forms August 12, 2020 v Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 D. SITE HISTORY AND CHARACTERIZATION 1. UST Owner/Operator Information Information regarding ownership and operator of the former UST is provided in Table 1. At the time of this report, the City of Charlotte is the owner of the former UST and Clarence and Ulysses Spears were the operator of the UST. 2. UST Information Information regarding the former UST at the site is provided in Table 2. 3. Description of the Release Following the demolition of the on -Site residence, the 250-gallon heating oil UST was removed on June 10, 2020. During its removal, impacted soil was observed (staining and petroleum odor). The City of Charlotte requested Wood collect samples from the former UST location and the resultant laboratory analyses identified Total Petroleum Hydrocarbon (TPH) Diesel Range Organics (DRO) and Gasoline Range Organics (GRO) concentrations above their respective State Action Levels. 4. Description of Site Characteristics The Site encompasses approximately 19.42 acres, is located in a mostly residential area, and is identified as Mecklenburg County Tax Parcel 043-106-27. A Site Location Map is included as Figure 1, a Topographic Map is included as Figure 2, and the location of the former UST is shown on Figure 3. The site is located within the Piedmont Province. The Piedmont is bounded to the east and southeast by the Atlantic Coastal Plain and to the west by the escarpment of the Blue Ridge Mountains, having a width of 150 to 225 miles (LeGrand 2004). According to the Geologic Map of North Carolina, the Site is underlain by metamorphosed quartz diorite. The Site was formerly occupied by an approximately 2,742-square foot single-family residence constructed in 1938. The UST was located near the northern corner of the former residential building. The surface cover surrounding the area consisted of grass and gravel. The 7.5-minute Derita, North Carolina, United States Geological Survey (USGS) quadrangle, published in 2013 was examined. The elevation at the Project Area ranges from approximately 714 to 766 feet above mean sea level (msl). The topography of the area generally slopes downward to the southeast. Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 The general direction of groundwater flow can be inferred from ground surface elevations and surficial expression of groundwater identified on the Derita, North Carolina USGS topographic quadrangle. Surficial groundwater occurrences generally include permanent lakes, streams, and wetland areas. Based on Wood's review of topographic maps and observations of the Site vicinity, the groundwater flow direction was inferred to be generally to the southeast toward a tributary of Mallard Creek. Wood reviewed the Mecklenburg County Well Information System 4.0 for water -supply wells located in the area surrounding the site. The closest water -supply well identified on the system is located approximately 815 feet to the southwest of the former UST location. 2 Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 E. UST CLOSURE REPORT The City of Charlotte and its tank removal contractor (W.C. Black and Sons, Inc.) mobilized to the Site on June 10, 2020 to remove the 250-gallon heating oil UST. Note, Wood was not on -Site for the removal of the UST. Information regarding the removal of the UST was provided by the City of Charlotte and W.C. Black and Sons, Inc. Reportedly, prior to removal, the top of the UST was uncovered by removing the overburden from above the tank. After the tank was uncovered, liquid was removed from the tank by a vacuum truck. Heating oil and petroleum contact water (PCW) was pumped from the tank into a vacuum truck for off -Site disposal by HAZ-MAT Environmental Services (HAZ-MAT). Following removal of the liquid from the tank, adjacent soils were observed to be impacted (staining and petroleum odor) and were stockpiled on plastic once removed. Once the UST was free from the surrounding soil, it was removed from the excavation and placed on plastic. Several areas of corrosion and pitting were observed on the UST following removal. Since petroleum impacted soils were observed during the UST removal, the excavation was left open to allow for the collection of UST closure soil samples for analytical analyses. On June 11, 2020, Wood personnel mobilized to the Site to collect the UST closure soil samples from the excavation (S-1 and S-2) and one soil sample from the stockpiled soil (S-3) for disposal purposes. Soil samples were collected using a stainless steel hand auger. To minimize the potential for cross -contamination, a new pair of nitrile gloves were donned and the hand auger was decontaminated between sample locations. The soil samples were placed directly into laboratory provided containers, placed in a cooler on ice, and delivered to Waypoint Analytical (Waypoint) in Charlotte, North Carolina. The closure soil samples were analyzed for TPH DRO and TPH GRO via EPA Method 8015C and benzene, toluene, ethylbenzene, and xylenes (BTEX) via EPA Method 8260D. The samples were maintained under a chain -of -custody protocol. The locations of the UST closure soil samples (S-1 and S-2) are depicted on Figure 4. Photographs of the UST closure activities are included in Appendix A. The excavation was left open pending receipt of the analytical results. The laboratory analytical results identified TPH DRO and TPH GRO concentrations in samples S-1 and S-2 exceeding the State Action Level for TPH DRO of 100 milligrams per kilogram (mg/kg) and for TPH GRO of 50 mg/kg. In addition, TPH DRO was identified in sample S-3 at a concentration which exceeded the State Action Level for TPH DRO. Following receipt of the analytical results, on June 18 2020, HAZ-MAT and W.C. Black and Sons, Inc. returned to the site to remove rainwater that had collected in the excavation. The rainwater was pumped from the excavation into a vacuum truck for off -Site disposal by HAZ-MAT. Wood personnel the covered the stockpiles, the UST, and excavation with plastic to keep rainwater from coming into contact with the removed UST and impacted soil. The liquid disposal manifest is included in Appendix B. The Site Investigation Report for Permanent Closure or Change -in -Service of Un-Registered UST (Form UST-2B) is included in Appendix C. The UST closure soil sampling results are summarized on Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 Table 3. The UST closure soil sample laboratory analytical report and chain -of -custody form is included in Appendix D. 4 Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 F. INITIAL RESPONSE AND ABATEMENT ACTION Based on the analytical results of the UST closure soil samples, the City of Charlotte submitted a 24-Hour Release and UST Leak Reporting Form (UST-61 Form). The UST-61 Form is included in Appendix C. The City of Charlotte requested that Wood personnel return to the Site on July 7, 2020 to direct over - excavation of petroleum -impacted soil from the UST excavation. A representative of Wood observed soil excavation and collected samples of soil from the excavator bucket and screened them in the field for volatile organic compounds (VOCs) using a RAE Systems MiniRAE 3000 equipped with a photoionization detector (PID). As the impacted soil was removed from the excavation, W.C. Black and Sons, Inc. personnel placed the soil directly into trucks for off -Site disposal at the Republic Services CMS Landfill facility in Concord, North Carolina. Once the PID screening indicated the petroleum -impacted soil was removed from the excavation, confirmation soil samples were collected from the sidewalls (SW-1, SW-2, SW-3, and SW-4) and from the base (Base) of the excavation for laboratory analyses. Groundwater or bedrock were not encountered in the excavation. The locations of the UST confirmation soil samples are depicted on Figure 4 and the sample depths are provided on Table 4. The confirmation soil samples were collected manually by Wood personnel directly from the excavator bucket. To minimize the potential for cross -contamination, a new pair of nitrile gloves were donned for the collection of each soil sample. The confirmation soil samples were placed directly into laboratory - provided containers, placed in a cooler on ice, and delivered under chain -of -custody protocol to Waypoint for analyses. The confirmation soil samples were analyzed for VOCs via EPA Method 8260D, semi -volatile organic compounds (SVOCs) via EPA Method 8270E, and extractable petroleum hydrocarbons (EPH) and volatile organic compounds (VPH) via the Massachusetts Department of Environmental Protection (MADEP) Method. Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 G. EXCAVATION OF CONTAMINATED SOIL 1. Determination of the Source and Extent of Soil Contamination The source of the soil contamination was observed to be corrosion and pitting present on the former 250- gallon heating oil UST. The PID field screening readings initially and the results of the laboratory analyses of the sidewall and base confirmation soil samples eventually were used to determine when soil over - excavation was complete. Based on the PID screenings, the excavation was extended to an approximate depth of 7.5 feet and to an approximate length and width of 15 feet and 10 feet, respectively. The confirmation sidewall soil samples (SW-1, SW-2, SW-3, and SW-4) were collected from the sidewalls at an approximate depth of 4.5 feet and the confirmation base soil sample (Base) was collected from an approximate depth of 7.5 feet. The analyses of the confirmation soil samples did not identify concentrations of petroleum constituents which exceeded their respective NCDEQ MSCCs as shown on Table 4. The UST confirmation soil sample laboratory analytical report and chain -of -custody form is included in Appendix D. 2. Excavation Process The excavation process is described in Section F of this report. The excavated petroleum -impacted soil was loaded directly into trucks and transported to the Republic Services CMS Landfill facility in Concord, North Carolina. A total of approximately 51.34 tons of soil was transported to the landfill for disposal. Soil disposal manifests are included in Appendix B. Following the receipt of the laboratory analytical results for the confirmation soil samples, the excavation was backfilled by W.C. Black and Sons, Inc. personnel using clean imported fill. H. Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 H. CONCLUSIONS AND RECOMMENDATIONS Concentrations of TPH DRO and GRO were identified in UST closure samples collected following the removal of the former 250-gallon heating oil UST, which led to over -excavation activities. Following over - excavation and off -Site disposal of petroleum -impacted soils, received analytical results of the confirmation soil samples collected from the base and sidewalls of the excavation indicated no constituent concentrations exceeding their respective NCDEQ MSCCs. Groundwater or bedrock were not encountered in the excavation. Based on the results of the confirmation soil sampling, Wood recommends no further action in regards to the release from the 250-gallon heating oil UST. 7 FIGURES 1 MGM v / Rural I l;°aans F°rdl � Fhll Nalore 1 YV,IdI/a 5 Preserve t Lalb -Planmlwn Wars _ - �Natuia Preserve " t may. 1-77 Nemn I� IIII. f�gronai Patty Clta*nyyay , P°'nl Greek 1 I ' Charblte Li = Wuglrs = �! 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Regent Pr f� Ind k�n Trod 0 G°Il C lubf TPC at d,•ed C . 1 Piper Glen � � � `wti at 1�5•fnner F,�• spr,ngn/r� cowry lub Sources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO,'USGS, G°n FAO` NP""S; NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, Esrl`°"'�" b c°"`- ` �� JaFpan; METI, Esri China (Hong Kong), swisstopo, O OpenStreetMap r contributors, and the GIS User Community PREPARED BY: SITE LOCATION MAP LMM N wood• 4732 WEST SUGAR CREEK ROAD DATE: 7/30/2020 CHARLOTTE, NORTH CAROLINA CHECKED BY: s AJF 3 i DATE: 7/30/2020 i Approximate Project Boundary 0 1.5 3 6 PROJECT NO: Miles 1238200028 M FIGURE: 0 1 cpr f �qLm i III iil��iIN ME, •r 'hill a �Man. IMF, �IIII sMWI . • �I� II�II� 'I �I . sEMIM F:\AMEC_Projects\2019\1238-19-0016\MXD\Topo (2).mxd, User: leanna.muroski; Date: 7/30/2020 1:35:39 PM, Checked By; AJF Date: 7/30/2020 F:\AMEC_Projects\2019\1238-19-0016\MXD\BoringLocation plan.mxd, User: leanna.muroski; Date: 7/30/2020 2:53:28 PM, Checked By: AJF Date: 7/30/2020 Document Path: C:\RemoteGIS\WestSugarcrk.mxd PREPARED BY: LMM 7/30/2020; CHECKED BY: AJF 7/30/2020 TABLES Table 1: Site History - UST System Owner/Operator and Other Responsible Party Information UST ID Number 1 Facility ID Number Tlw A Name of Land Owner/UST Owner Dates of Ownership City of Charlotte 12/19/2019 to present Street Address 600 East Fourth Street City State Zip Telephone Number Charlotte NC 28202 704-651-4366 Name of Operator Dates of Operation Clarence and Ulysses Spears Unknown Street Address 4732 West Sugar Creek Road City State Zip Telephone Number Charlotte NC 28269 Unknown Incident Number TBD Table 2: Site History - UST System and Release Information Incident Number/Name: Pending/4732 West Sugar Creek Road Parcel Description Was releaseNCDEQ UST ID Current/Last Previous Capacity Construction Tank of Date Status of associated Dimensions Associated Tank Incident Number Contents Contents (gallons) Details UST with the (feet) Piping and Installed # UST Pumps system? Heating Removed, 1 Heating Oil 250 Steel 3.25 x 4 N/A Unknown Yes TBD Oil 6/2020 Table 3: UST Closure Soil Sample Results Incident Number/Name: Pending/4732 West Sugar Creek Road Parcel Analytical Method 4 TPH by EPA Method 8015 BTEX by EPA Method 8260 Contaminant of Concern 0cl� arc Q) c c Qj � >, X Sample ID Date Collected UST Area Sample Depth (feet) Incident Phase m } w o H S-1 6/11/2020 UST Excavation 3.5 Closure 6,900 240 <0.26 <0.26 0.17 J 2.3 S-2 6/11/2020 UST Excavation 3.5 Closure 15,000 220 <0.28 <0.28 0.17 J 0.25 J S-3 6/11/2020 Stockpile N/A Closure 220 <5.2 <0.0065 <0.0065 <0.0065 <0.020 State Action Level (mg/kg) 100 50 -- -- -- -- Soil to groundwater MSCC (mg/kg) __ -- 0.0056 4.3 4.9 4.6 Residential MSCC (mg/kg) 18 1,200 1,560 3,129 Industrial/Commercial MSCC (mg/kg) __ -- 164 32,000 40,000 81,760 Notes: 1. Sample depths shown in feet below ground surface (bgs) Prepared By/Date: AJF 7/29/20 2. Concentrations are shown in milligrams per kilogram (mg/kg) Checked By/Date: LMM 7/30/20 3. EPA = Environmental Protection Agency 4. TPH = Total Petroleum Hydrocarbons 5. DRO = Diesel Range Organics 6. GRO = Gasoline Range Organics 7. BTEX = Benzene, Toluene, Ethylbenzene, Xylenes 8. J = Indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate 9. MSCCs = North Carolina Department of Environmental Quality (NCDEQ), UST Program, Maximum Soil Contaminant Concentrations, dated April 2012 10. -- = Not Applicable Table 4: Summary of UST Confirmation Soil Sample Results Incident Number/Name: Pending/4732 West Sugar Creek Road Parcel Analytical Method VOC by EPA Method 8260 EPH via MADEP Contaminant of Concern v v v 00 .� V Sample ID Date Collected UST Area Sample Depth (feet) Incident Phase Q U Q z Base 7/7/2020 Base of excavation 7.5 IAA <0.030 0.00094 J 1.7 J Southwestern sidewall SW-1 7/7/2020 of excavation 4.5 IAA <0.029 0.00090 J <32 Southeastern sidewall SW-2 7/7/2020 4.5 IAA 0.015 J 0.00082 J <32 of excavation Northeastern sidewall SW-3 7/7/2020 of excavation 4.5 IAA <0.026 0.00074 J <32 Northwestern sidewall SW-4 7/7/2020 of excavation 4.5 IAA <0.021 <0.010 <32 Soil to groundwater MSCC (mg/kg) 24 0.16 540 Residential MSCC (mg/kg) 14,000 313 1,500 Industrial/Commercial MSCC (mg/kg) 360,000 8,176 40,000 Notes: 1. Sample depths shown in feet below ground surface (bgs) Prepared By/Date: AJF 7/29/20 2. Concentrations are shown in milligrams per kilogram (mg/kg) Checked By/Date: LMM 7/30/20 3. VOC = Volatile Organic Compounds 4. EPH = Extractable Petroleum Hydrocarbons 5. MADEP = Massachusetts Department of Environmental Protection 6. IAA = Initial Abatement Action 7. J = Indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate 8. MSCCs = North Carolina Department of Environmental Quality (NCDEQ), UST Program, Maximum Soil Contaminant Concentrations, dated April 2012 9. Constituents detected in one or more sample shown, see laboratory analytical report for full constituent list let» 4 ►19 ►:Ie1 PHOTOGRAPHS Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 Photograph 1: View of UST following removal, photograph taken June 18, 2020. Photograph 2: View of UST following removal, photograph 1. taken June 18, 2020. Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel August 12, 2020 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 IV hk Photograph 3: View of rainwater in excavation removed on June 18, 2020, photograph taken June 18, 2020. Photograph 4: View of UST, stockpile, and excavation covered with plastic, ,. photograph taken June 19, 2020. r . Initial Abatement Action Report - 4732 West Sugar Creek Road Parcel 4732 West Sugar Creek Road, Charlotte, North Carolina Wood Project: 1238-20-0028 August 12, 2020 Photograph 5: View of excavation covered with plastic following over - excavation, photograph taken July 7, 2020. Photograph 6: View of excavation covered with plastic following over - excavation, photograph taken July 7, 2020. /_1»4►191/:4:j LIQUID/SOIL DISPOSAL MANIFESTS a p#� r MNIV*W& HAZ-MAT ENVIRONMENTAL SERVICES P.O. BOX 37392 • CHARLOTTE, N.C. 28237 (704) 332-5600 FAX (704) 375-7183 NON -HAZARDOUS SPECIAL WASTE Section I. GENERATOR __Pi.te an of section u Manifest No. 88481 P.O. No. Job No. 2J.--.213 I [b GENERATOR LOCATION WORK CONTRACTED BY NAME -j Bill To (If different from information at IeR) ORIGINATING ADDRESS +�J, NAME _ , r► � C MAILING AD E S [jam ADDRE5 + CITY __ ! '� STATEC zip C��ITY STATE _.-_ ZIP J PHONE NO. I�fO Ntt Gr CONTACT NAME _-.... CONTACT NAME _..__ DES. OF WASTE: - -- ------- 0041 7 No. Type Units Quantity Section II.. INVOICE INFORMATION GALLONS DRUMS DESCRIPTION QUANTITY LINE TOTAL -- --.--.-_.----.- _ 1. PETROLEUM CONTACT WATER 2. OFF -SPEC LIGHT OIL, DIESEL OR GAS m _ 3- NON -HAZARDOUS LIQUIDS 4. SEDWENTOR SOLIDS 5. 55-GALLON DRUM REMOVED - SOLID OR EMPTY 8. 55-GALLON DRUM REMOVED- LIQUID 8. 10. ARRIVALTIME: DEPARTURETIME: GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations. GeneratorrCustomer shall reimburse HAZ-MAT its reasonable expenses and charges for handling, analyzing, loading, preparing, transporting, storing or caring for nonconforming or off spec waste, including casts of decontamination and cleaning of equipment. Generator must notify HAi-MAT of any changes to the waste stream prior to shipment. Jr Generator Authorized Agent Name Signature Snom.rnrt Date Section III. TRANSPORTER 7ERfGeneren mmplrrra it Tranep,rcer i.•••r»rlrrerr: T lieu ere E1 HAZ- MAT TRANSPORTER II ENVIRONMENTAL SERVICES P.O. BOX 37392 • CHARLOTTE. N.C. 28237 a- Driver NamelTitle b- Phone No c. Truck No Hazardous Waste Transporter Permits EPA NCD 484613T0 e. Name -__----. f. Address g. Driver Name/Title- h. Phone No. j. Transporter II Permit Nos. i- Truck No. d . �— nrv2rSiGn2[�•e Sh:pmen-Date -.-..---•---------- - Shipment ❑z•m Section IV: FACILITY INFORMATION AND CERTIFICATE OF DISPOSAL Site Name: Haz-Mat Environmental Services a. Phone No- 7D4-332-5600 Physical Address: 21Q Dalton Avenue d- Mailing Address: P-O- Box 37392 Charlotte, N.C-28205 Charlotte, N.C- 28237 e: Discrepancy Indication Space This is to certify that all nm-hazardous mallenal removed from above location has been received and 4 be disposed of in accordance vdh appica6le local, state and feded regulations in the fo" manner: fij tam products are blended into a hers: al reusable fuel tar use in large I burners. (2) Waste waters are to be treated with polymers. pH a*tsters, and a fbtculant then flows through a dissolved air ttation system for prelreatinent separation, then into the CMUD sanitation sewer system under 5012. (3) Sludges from treatment systems are hauled to E.P.A. approved facilities for proper disposal. Manifest and certificate of disposal are on file. (4) Our treatment system operates on a first in, f t basis ptpduct should be proceed within se dais. SIGNATURE OF: FACiLITYAGE NT DATE MONTH bAY YEA ORIGINAL - FINAL T.S.D. • YELLOW - DISPOSER • PINK - f ST IS-D- • GOLD • GENERATOR REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste is asbestos waste, complete Sections I, II, III and IV If waste is NOT asbestos waste, complete Sections I, II and III n GENERATOR (Generator completes la-rl a. Generator's US EPA ID Number b. Manifest Document Number c. Page t of 1 d. Generator's Name and Location: e. Generators Mailing Address: City of Charlotte 4732 W sugar Creek Rd Charlotte, NC 28269 g. Phone: f. Phone: If owner of the generating facility differs from the generator, provide: h. Owners Name: I. Owner's Phone No.: I. Waste Profile # k. Exp. Data I. Waste Shipping Name and In. Comamers I n. Total o. Unit Description uuantrty WWoI No. T e 5010 20 8134 soil I ^1 I L BILL TO: City of Charlotte 70055 S , p GENERATOR'S CERTIFICATION: I hereby certl y that the an material Is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been property described, destined and pa ism oper condithm fortransportetion according to applicable regulations; AND, dthis waste is a treatment residue of a previously restricted rdous was a subj ct to a Land Disposal Restrictions. I canny and warrant that the waste has been treated In accordance with the r uirements of C, n is no ger a rdou seas tlefnetl b 0 CFR 261. . Genera or AutnOnZed Agent Name Print . Signature Ir. Da e n locucmroi wniyietes ue-u anrrt lenspo ter corr p sees c-ef a.Transporter's Name and Address: reo b. Phone: c. Driver Name(Pring tl Sionature _ _ Data III. DESTINATION Ir7enerafnr rmmnlafe Illa-r and rtaellnnfinn sao mninfne tun -mot a. Disposal Facility and Site Address : c. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NO 28027 b. Phone: 704-782-20N I herby carfiffeffildithe,above rallied material has base a e the be knowledge the fiemoolnu is true and accurate. e. Name cIsIhorized A ant ri f. Si nature IV. ASBESTOS (Generator completes IVa-f and Operator complete IVg-i) a. Operators Name and Address: b. Phone: e. Responsible Agency Name and Address: d. Phone: e. Special Handling Instructions and Additional Information: I . Friable 0 Non-Fdable D Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are in all respects In proper Condition for transport by highway according to applicable international and national governmental to ulations. .Operator's Name and Tit Print h. Si nature 1. Date 'Operator refers to the company which owns leases,operates,controls, or supervises the facility being demolished or renovated, or the demolition or &tvREPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST f`, SERVICES, INC. If waste is asbestos waste, complete Sections I, II, III and IV nq If waste is NOT asbestos waste, complete Sections I, II and III 1. GENERATOR !Generator COMDletes la-r1 In (� 1 a. Generators US EPA ID Number In. Manifest Document Number C. Page 1 of 1 d. Generator's Name and Location: e. Generators Mailing Address: City of Charlotte 4732 W sugar Creek Rd Charlotte, NC 28269 g. Phone: I. Phone: If owner of the generating facility differs from the genemtor, provide: h. Owners Name: I. Owners Phone No.: j. Waste Profile V k. Esp. Date I. Waste Shipping Name and m. Containers n. Total o. Unit Desui tion No. T Quantity WI/Vol 5010 20 6134 soil BILL TO: City of Charlotte 70055 GENERATORS CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly desuibad classified and pa in proper condition far transportation according to applicable regulations; AND, ifthis waste is a treatment residue of a previously restricted ste s bject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements of FR 268 a [an Ion waste as defined b 40 CFR 261. . Generator Autho!'etl ent Name not nature k D r �n toenelawl wnlpletes ua-D aria I ransporter completes nc-e) a. Transporters Name antl Adtlaress: TBD I.* ('� iJ /I1� V'dAAr.. l,P✓ -LGrI b. Phone: S� S LC ant c. Ume! Name (Print tl Slanature Date III. DESTINATNIM `r�enaratnr nlafn him_e 11—+i—finn cue .... .,iefe.. uu ..% a. Disposal Fatality and Site Address: c. US EPA Number tl. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-2004 I hem .7Ay [hat the above named materiel has been a tad nd to the best of knowledge the foregoing is true and accurate. - - d e.Na a fA rizedA ent Pdn[ f.Sl nature ale IV. N36CDI VJ RieneratOr COrnmetes iva-t antl UDemmir coMnlBte iva-o a. Operators Name and Address: b. Phone: c. Responsible Agency Name and Address: d. Phone: e. Special Handling Instructions and Additional Information: f. 0 Friable El Non -Friable El Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are in all respects in proper condition for transport by highway according to applicable international and national governmental regulations. . Operators Name and TRIe Print h. Signature 1 1. Date 'Operator refers to the company which owns leases operates, controls or supervises the facility being demolished or renovated or the demolition or k ..,.. REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste is asbestos waste, complete Sections I, ll, III and IV If waste Is NOT asbestos waste, complete Sections I, II and III GENERATOR (Generator completes la-r) A. Generator's US EPA ID Number b. Manifest Document Number Q ge 1,61 7 d. Generators Name and Location: City of Charlotte e. Generators Mailing Acidosis: 4732 W sugar Creek Rd Charlotte, NC 28269 g. Phone: I. Phone: If owner of the generating facility differs from the generator, provide: In. Owners Name: 1. Owners Phone No.: j. Waste Profile # k. Exp. Date I. Waste Shipping Name and m. Containers n. ToGI o. Unit Description No. T Quantity WWol 5010208134 soil BILL TO: City of Charlotte 70055 GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined CFR any applicable state law, has been described, classified and packaged, and is in proper for oncoming to p a re u This applicable regulations; AND, waste is a treatment residue Restion of a previously restricted h subject to the Land Disposal Restrictions. I certfy and warrant that me waste has the Land Disposal if a been treated in accordance with the requirements of 4 and no to m waste as de8netl b 40 CFR 261. dance O J . Generator Aulho A ant ame Print nature I, Da[e TBD S�tJ`� V�WvO 'T QZJ" III_ DERTINOTIDN /fiPnPmtnr rY1TnIPtp lllnl and noctiniatlrm Sltp rrlmrlli IIld_nI a. Disposal Facility and Site Address: c. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concom, NC 28027 b. Phone: 704-7 -2004 I herb certat bo na material has been a e d t he b s[ knowletl a the foregoing is We and accurate. T e. Name of Authorized Agent (filimilli n re V I 1 9. Date IV. ASBESTOS (Generator completes IVa-f and Operator complete IVg-i) a. Operators Name and Address: b. Phone: C. Responsible Agency Name and Address: d. Phone: e. Special Handling Instructions and Additional Information: 1.0 Friable ❑ Non -Friable ❑ Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are In all respects in proper Condition for transport by highway according to applicable International and national govennnental regulations. . Operators Name and Titie Print In. Signal I. Oate *Operator refers to the Company which owns, leases operates, controls or supervises the facility being demolished or mnovatetl or the demol@ion or APPENDIX C UST FORMS UST-2 6 Site Investigation Report for Permanent Closure or Change -in - Service of UN -REGISTERED UST Return completed form to: STATE USE ONLY❑ NC DEQ / DWM / UST SECTION Facility ID E 1646 MAIL SERVICE CENTER RALEIGH, NC 27699-1646 ATTN: REGISTRATION & PERMITTING Date Received phone 1919E1707-8171 fa0[919E1715-1117 hftpltlwww.wastenotnc.org/ INSTRUCTIONS (READ THIS FIRST 1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site ChecksuTank Closure and Initial Response and Abatement. The guidelines can be obtained at http //de .nc.gov/about/divisions/waste-management/waste- management-permit-guidance/underground-storage-tanks-section. 2. Permanent closureoComplete all sections of this form. 3. Change-in-servicedWhere UST systems will be converted from storing a regulated substance to a non -regulated substance complete sections I IIAIIdVCand VI. 4. For more than 5 un-registered UST systemsCattach additional forms as needed. 5. Un-Registered USTs may be subject to unpaid fees and late penalties. 6. REGISTERED LISTS use Form UST-2A. I. OWNERSHIP OF TANKS II. LOCATION OF TANKS Owner Name [Corporation ulndividualEPublic AgencyDor Other Entity Facility Name or Company City of Charlotte 4732 West Sugar Creek Road Street Address Facility ID ❑ df known❑ 600 East Fourth Street N/A City County Street Address Charlotte Mecklenburg 4732 West Sugar Creek Road State Dip Code City County Elip Code NC 28202 Charlotte Mecklenburg 28269 Phone Number Phone Number 704-651-4366 N/A III. CONTACT PERSONNEL Contact for FacilityLi Cbb Title❑ Phone O0 Doug Pierotti Env. Services Mngr. 704-651-4366 Closure Contractor Name❑ Closure Contractor Company❑ Address[] Phone ❑ Jason Black WC Black & Sons, Inc. 5108 Cheviot Rd, 704-597-5954 Charlotte, NC Primary Consultant Name❑ Primary Consultant Company❑ Address❑ Phone ❑ Helen Corley Wood 2801 Yorkmont Rd, 704-357-8600 Charlotte, NC IV. UST INFORMATION FOR UN -REGISTERED UST SYSTEMS V. EXCAVATION CONDITION REGISTERED USTs use Form UST-2A. Tank ID Silk in Last Last Permanent Method of Permanent Closure❑ Change -in- Notable No. Gallons Contents Use Close Date Indicate REMOVED or enter fill Service Water in Free product odoror visible soil Date materialasuch as foam/ Date eD avation contaminatio concrete/ sand n Yes No Yes No Yes No 1 250 Heating Oil Ukn 6/10/2020 Removed 6/10/2020 ❑ ® ❑ ® ® ❑ ❑ ❑ ❑ ❑ 1 ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ VI. CERTIFICATION I certify under penalty of law that I have personally ermined and am familiar with the information submitted in this and all attached documents and that based on my inouiry of those individuals immediately responsible for obtaining the information El believe that the submitted information is true accurate and complete. Print name and official title of owner or ownerls authoriCed representative Andrew Frantz, Senior Scientist for Wood (Owener's Authorized Representative Signature Date Signed 7/30/2020 NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL ❑UALITYEDIVISION OF WASTE MANAGEMENTEUST SECTION UST-61 24-Hour Release and UST Leak Reporting Form. For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release (DWM USE ONLY) Suspected Contamination? (Y/N) Facility ID Number Incident # Risk (H,I,L,U) Confirmed GW Contamination? (Y/N) Date Leak Discovered Received On Received By Confirmed Soil Contamination ?(Y/N) Comm/Non-Commercial? Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) Reg/Non-regulated? Region Free Product? (Y/N) If Yes, State Greatest Thickness INCIDENT DESCRIPTION Incident Name: Address: County: Regional Office (circle one): Asheville, Mooresville, Fayetteville, City/Town: Zip Code: Raleigh, Washington, Wilmington, Winston-Salem Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by: ❑GPS Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors) ❑Topographic map ❑GIS Address matching ❑Other ❑ Unknown Describe location: HOW RELEASE WAS DISCOVERED (Release code) (Check one) ❑Release Detection Equipment or Methods ❑Visual/Odor ❑Groundwater Contamination ❑During UST Closure/Removal ❑Water in Tank ❑Surface Water Contamination ❑Property Transfer ❑Water Supply Well Contamination ❑Other (specify) SOURCE OF CONTAMINATION Source of Release Cause of Release Type of Release Product Type Released (Check primary source) (Check primary cause) (Check one) (Check primary product type released) ❑ Tank ❑ Spill ❑ Petroleum ❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil ❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend ❑ Dispenser ❑Heating Oil ❑ Vegetable Oil 100% Corrosion Both ❑❑ ❑ Other Petroleum ❑ E10 - E20 ❑ Submersible Turbine Pump ❑Physical/Mechanical ❑ Delivery Problem Location Products Damage ❑ E21 - E84 (Check one) Metals ❑ ❑ Install Problem ❑ E85 - E99 ❑ Spill Bucket ❑ Other Inorganics ❑ Other [-]Facility ❑Ethanol 100% ❑ Other ❑ Other Organics ❑ Unknown ❑Residence ❑ E01 - E09 ❑ Unknown ❑Other Definitions presented on reverse Definitions presented on reverse Ownership 1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining UST Form 61 (02/19) Page 1 of 2 IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected Water Supply Wells Contaminated: 1. 2. 3. (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) UST Owner/Company UST SYSTEM OWNER Point of Contact Address City State Zip Code Telephone Number UST SYSTEM OPERATOR UST Operator/Company Address City State Zip Code Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address City State Zip Code Telephone Number Draw Sketch of Area (showing two major road intersections) or Attach Map Person Reporting Incident Company Telephone Number Title Address Date UST Form 61 (02/19) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined APPENDIX D LABORATORY ANALYTICAL REPORTS AND CHAIN -OF -CUSTODY FORMS Case Narrative Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Chart) David Hanley 2801 Yorkmont Rd. #100 Charlotte, NC 28208 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: West Sugar Creek UST Lab Submittal Date: 06/11/2020 Work Order: 0060930 6/16/20 15:40 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL a,j Angela D. Overcash Senior Project Manager Data Qualifiers Key Reference: DO Surrogates diluted out. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). M Matrix spike outside of the control limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 12 Sample Receipt Summary Way� nt 06/16/2020 poiA Work Order: 0060930 NALYTICAL Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received S-1 0060930-01 Solid 06/11/20 12:00 06/11/20 14:00 S-2 0060930-02 Solid 06/11/20 12:10 06/11/20 14:00 S-3 0060930-03 Solid 06/11/20 12:30 06/11/20 14:00 Samples were received in good condition at 5.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 12 WayPAoi nt . NALYTICAL Summary of Detections 06/1693 0 Work Order: 00600 Waypoint ID Client ID Parameter Method Result Units 0060930-01 S-1 Diesel Range Organics `8015C 6900 mg/kg dry 0060930-01 S-1 Gasoline Range Organics '8015C 240 mg/kg dry 0060930-01 S-1 Ethylbenzene 8260D 0.17 J mg/kg dry 0060930-01 S-1 m,p-Xylenes 8260D 2.2 mg/kg dry 0060930-01 S-1 o-Xylene 8260D 0.041 J mg/kg dry 0060930-01 S-1 Xylenes, total 8260D 2.3 mg/kg dry 0060930-02 S-2 Diesel Range Organics '8015C 15000 mg/kg dry 0060930-02 S-2 Gasoline Range Organics `8015C 220 mg/kg dry 0060930-02 S-2 Ethylbenzene 8260D 0.17 J mg/kg dry 0060930-02 S-2 m,p-Xylenes 8260D 0.25 J mg/kg dry 0060930-02 S-2 Xylenes, total 8260D 0.25 J mg/kg dry 0060930-03 S-3 Diesel Range Organics '8015C 220 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 12 � Laboratory Report • Waynt. 06/16/2020 PA ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: S-1 Attn: David Hanley Sample ID: 0060930-01 2801 Yorkmont Rd. #100 Work Order: 0060930 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 06/11/20 12:00 Time Submitted: 06/11/20 14:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 6900 mg/kg dry 470 160 50 *8015C 6/12/20 13:21 ZRC POF0917 Surrogate Recovery Control Limits o-Terphenyl 0 % 31-123 DO Gasoline Range Organics by GC/FID Gasoline Range Organics 240 mg/kg dry 59 16 500 *8015C 6/12/20 15:22 TBL POF0918 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 90 % 50-137 General Chemistry Parameters % Solids 74.4 % by 0.100 0.100 1 *SM2540 G 6/12/20 7:50 EDV POF0914 Weight Volatile Organic Compounds by GUMS (Medium Level) Benzene BRL mg/kg dry 0.26 0.041 50 8260D 6/16/20 10:42 TBL POF0974 Ethylbenzene 0.17 J mg/kg dry 0.26 0.040 50 8260D 6/16/20 10:42 TBL POF0974 m,p-Xylenes 2.2 mg/kg dry 0.53 0.068 50 8260D 6/16/20 10:42 TBL POF0974 o-Xylene 0.041 J mg/kg dry 0.26 0.028 50 8260D 6/16/20 10:42 TBL POF0974 Toluene BRL mg/kg dry 0.26 0.042 50 8260D 6/16/20 10:42 TBL POF0974 Xylenes, total 2.3 mg/kg dry 0.79 0.095 50 8260D 6/16/20 10:42 TBL POF0974 Surrogate Recovery Control Limits 4-Bromofluorobenzene 83 % 70-130 Dibromofluoromethane 97 % 70-130 Toluene-d8 79 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 12 � Laboratory Report • Waynt. 06/16/2020 PA ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: S-2 Attn: David Hanley Sample ID: 0060930-02 2801 Yorkmont Rd. #100 Work Order: 0060930 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 06/11/20 12:10 Time Submitted: 06/11/20 14:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 15000 mg/kg dry 940 320 100 *8015C 6/12/20 15:12 ZRC POF0917 Surrogate Recovery Control Limits o-Terphenyl 0 % 31-123 DO Gasoline Range Organics by GC/FID Gasoline Range Organics 220 mg/kg dry 59 16 500 *8015C 6/12/20 14:54 TBL POF0918 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 110 % 50-137 General Chemistry Parameters % Solids 74.3 % by 0.100 0.100 1 *SM2540 G 6/12/20 7:50 EDV POF0914 Weight Volatile Organic Compounds by GUMS (Medium Level) Benzene BRL mg/kg dry 0.28 0.043 50 8260D 6/16/20 11:42 TBL POF0974 Ethylbenzene 0.17 J mg/kg dry 0.28 0.042 50 8260D 6/16/20 11:42 TBL POF0974 m,p-Xylenes 0.25 J mg/kg dry 0.55 0.071 50 8260D 6116/20 11:42 TBL POF0974 o-Xylene BRL mg/kg dry 0.28 0.029 50 8260D 6/16/20 11:42 TBL POF0974 Toluene BRL mg/kg dry 0.28 0.044 50 8260D 6/16/20 11:42 TBL POF0974 Xylenes, total 0.25 J mg/kg dry 0.83 0.099 50 8260D 6116/20 11:42 TBL POF0974 Surrogate Recovery Control Limits 4-Bromofluorobenzene 107 % 70-130 Dibromofluoromethane 96 % 70-130 Toluene-d8 106 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 12 � Laboratory Report • Waynt. 06/16/2020 PA ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: S-3 Attn: David Hanley Sample ID: 0060930-03 2801 Yorkmont Rd. #100 Work Order: 0060930 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 06/11/20 12:30 Time Submitted: 06/11/20 14:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 220 mg/kg dry 44 15 5 *8015C 6/12/20 15:49 ZRC POF0917 Surrogate Recovery Control Limits o-Terphenyl 61 % 31-123 Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/kg dry 5.2 1.4 50 *8015C 6/12/20 14:26 TBL POF0918 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 109 % 50-137 General Chemistry Parameters % Solids 80.0 % by 0.100 0.100 1 *SM2540 G 6/12/20 7:50 EDV POF0914 Weight Volatile Organic Compounds by GUMS Benzene BRL mg/kg dry 0.0065 0.0010 1 8260D 6/16/20 10:12 TBL POF0972 Ethylbenzene BRL mg/kg dry 0.0065 0.00098 1 8260D 6/16/20 10:12 TBL POF0972 m,p-Xylenes BRL mg/kg dry 0.013 0.0017 1 8260D 6/16/20 10:12 TBL POF0972 o-Xylene BRL mg/kg dry 0.0065 0.00069 1 8260D 6/16/20 10:12 TBL POF0972 Toluene BRL mg/kg dry 0.0065 0.0010 1 8260D 6/16/20 10:12 TBL POF0972 Xylenes, total BRL mg/kg dry 0.020 0.0023 1 8260D 6/16/20 10:12 TBL POF0972 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 70-130 Dibromofluoromethane 103 % 84-123 Toluene-d8 114 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 12 Waypo�nt ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: David Hanley 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch POF0972 - 5035 Reporting Result Limit Units Level II QC Report 6/16/20 Work Order: 0060930 Time Submitted: 6/11/2020 2:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (POF0972-BLK1) Prepared & Analyzed: 06/16/20 Benzene BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet Toluene 0.00152 0.0050 mg/kg wet J Surrogate:4-Bromofluorobenzene 55.7 ug/L 50.00 111 70-130 Surrogate: Dibromofluoromethane 50.0 ug/L 50.00 100 84-123 Surrogate: Toluene-d8 38.0 ug/L 50.00 76 76-129 LCS (POF0972-BS1) Prepared &Analyzed: 06/16/20 Benzene 0.0445 0.0050 mg/kg wet 0.05000 89 74-127 Ethylbenzene 0.0527 0.0050 mg/kg wet 0.05000 105 74-128 m,p-Xylenes 0.113 0.010 mg/kg wet 0.1000 113 75-124 o-Xylene 0.0441 0.0050 mg/kg wet 0.05000 88 74-126 Toluene 0.0572 0.0050 mg/kg wet 0.05000 114 71-129 Surrogate:4-Bromofluorobenzene 51.4 ug/L 50.00 103 70-130 Surrogate: Dibromofluoromethane 50.2 ug/L 50.00 100 84-123 Surrogate: Toluene-d8 60.0 ug/L 50.00 120 76-129 Matrix Spike (POF0972-MS1) Source: 0060930-03 Prepared & Analyzed: 06/16/20 Benzene 0.0473 0.0062 mg/kg dry 0.06248 BRL 76 60-135 Ethylbenzene 0.0435 0.0062 mg/kg dry 0.06248 BRL 70 44-144 m,p-Xylenes 0.0817 0.012 mg/kg dry 0.1250 BRL 65 36-148 o-Xylene 0.0403 0.0062 mg/kg dry 0.06248 BRL 64 43-143 Toluene 0.0483 0.0062 mg/kg dry 0.06248 BRL 77 57-135 Surrogate:4-Bromofluorobenzene 48.6 ug/L 50.00 97 70-130 Surrogate: Dibromofluoromethane 50.5 ug/L 50.00 101 84-123 Surrogate: Toluene-d8 38.1 ug/L 50.00 76 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 12 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: David Hanley 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 6/16/20 Work Order: 0060930 Time Submitted: 6/11/2020 2:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POF0972 - 5035 Matrix Spike Dup (POF0972-MSD1) Source: 0060930-03 Prepared & Analyzed: 06/16/20 Benzene 0.0445 0.0062 mg/kg dry 0.06248 BRL 71 60-135 6 20 Ethylbenzene 0.0387 0.0062 mg/kg dry 0.06248 BRL 62 44-144 12 19 m,p-Xylenes 0.0776 0.012 mg/kg dry 0.1250 BRL 62 36-148 5 20 o-Xylene 0.0372 0.0062 mg/kg dry 0.06248 BRL 60 43-143 8 17 Toluene 0.0438 0.0062 mg/kg dry 0.06248 BRL 70 57-135 10 22 Surrogate:4-Bromofluorobenzene 52.0 ug/L 50.00 104 70-130 Surrogate: Dibromofluoromethane 49.9 ug/L 50.00 100 84-123 Surrogate: Toluene-d8 52.6 ug/L 50.00 105 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 12 Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: David Hanley 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control Reporting Analyte Result Limit Units Batch POF0974 - 5035 Level II QC Report 6/16/20 Work Order: 0060930 Time Submitted: 6/11/2020 2:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (POF0974-BLK1) Prepared & Analyzed: 06/16/20 Benzene BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate:4-Bromofluorobenzene 55.7 ug/L 50.00 111 70-130 Surrogate: Dibromofluoromethane 50.0 ug/L 50.00 100 70-130 Surrogate: Toluene-d8 38.0 ug/L 50.00 76 70-130 LCS (POF0974-BS1) Prepared &Analyzed: 06/16/20 Benzene 0.0445 0.0050 mg/kg wet 0.05000 89 74-123 Ethylbenzene 0.0527 0.0050 mg/kg wet 0.05000 105 69-125 m,p-Xylenes 0.113 0.010 mg/kg wet 0.1000 113 64-125 o-Xylene 0.0441 0.0050 mg/kg wet 0.05000 88 69-121 Toluene 0.0572 0.0050 mg/kg wet 0.05000 114 74-122 Xylenes, total 0.157 0.015 mg/kg wet 0.1500 105 74-126 Surrogate:4-Bromofluorobenzene 51.4 ug/L 50.00 103 70-130 Surrogate: Dibromofluoromethane 50.2 ug/L 50.00 100 70-130 Surrogate: Toluene-d8 57.6 ug/L 50.00 115 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 12 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: David Hanley 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Gasoline Range Organics by GC/FID - Quality Control Level II QC Report 6/16/20 Work Order: 0060930 Time Submitted: 6/11/2020 2:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POF0918 - 5030B Blank (POF0918-BLK1) Gasoline Range Organics Surrogate: a,a,a-Trifluorotoluene LCS(POF0918-BS1) Gasoline Range Organics Surrogate: a,a,a-Trifluorotoluene Matrix Spike (POF0918-MS1) Gasoline Range Organics Surrogate: a,a,a-Trifluorotoluene Matrix Spike Dup (POF0918-MSD1 Gasoline Range Organics Surrogate: a,a,a-Trifluorotoluene Prepared & Analyzed: 06/12/20 BRL 5.0 mg/kg wet 6.20 mg/kg wet 5.000 124 50-137 Prepared & Analyzed: 06/12/20 54.8 5.0 mg/kg wet 50.00 110 41-138 6.00 mg/kg wet 5.000 120 50-137 Source: 0060930-03 Prepared & Analyzed: 06/12/20 113 6.2 mg/kg dry 62.48 BRL 181 41-138 7.56 mg/kg dry 6.248 121 50-137 Source: 0060930-03 Prepared & Analyzed: 06/12/20 95.4 6.2 mg/kg dry 62.48 BRL 153 41-138 7.25 mg/kg dry 6.248 116 50-137 17 34 M M This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 12 ® Level II QC Report Waynt. � 6/16/20 poi ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Work Order: 0060930 Attn: David Hanley Time Submitted: 6/11/2020 2:00:00PM 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Diesel Range Organics by GC/FID - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POF0917 - 3546 Blank (POF0917-BLK1) Prepared: 06/11/20 Analyzed: 06/12/20 Diesel Range Organics BRL 7.0 mg/kg wet Surrogate: o-Terphenyl 0.911 mg/kg wet 1.333 68 31-123 LCS (POF0917-BS1) Prepared: 06/11/20 Analyzed: 06/12/20 Diesel Range Organics 65.3 7.0 mg/kg wet 66.67 98 46-126 Surrogate: o-Terphenyl 1.12 mg/kg wet 1.333 84 31-123 LCS Dup (POF0917-BSD1) Prepared: 06/11/20 Analyzed: 06/12/20 Diesel Range Organics 64.0 7.0 mg/kg wet 66.67 96 46-126 2 20 Surrogate: o-Terphenyl 1.10 mg/kg wet 1.333 82 31-123 Sample Extraction Data Prep Method: 3546 Lab Number Batch Initial Final Date/Time 0060930-01 POF0917 30 g 1 mL 06/11/20 16:00 0060930-02 POF0917 30 g 1 mL 06/11/20 16:00 0060930-03 POF0917 30 g 1 mL 06/11/20 16:00 Prep Method: 5030E Lab Number Batch Initial Final Date/Time 0060930-01 POF0918 5.7 mL 5 mL 06/12/20 10:03 0060930-02 POF0918 5.7 mL 5 mL 06/12/20 10:03 0060930-03 POF0918 5.97 mL 5 mL 06/12/20 10:03 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 0060930-01 POF0914 30 g 30 g 06/11/20 15:10 0060930-02 POF0914 30 g 30 g 06/11/20 15:10 0060930-03 POF0914 30 g 30 g 06/11/20 15:10 Prep Method: 5035 Lab Number Batch Initial Final Date/Time 0060930-03 POF0972 4.8 g 5 mL 06/16/20 8:07 Prep Method: 5035 Lab Number Batch Initial Final Date/Time 0060930-01 POF0974 6.36 g 5 mL 06/16/20 8:58 0060930-01 POF0974 6.36 g 5 mL 06/16/20 8:58 0060930-02 POF0974 6.1 g 5 mL 06/16/20 8:58 0060930-02 POF0974 6.1 g 5 mL 06/16/20 8:58 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 12 C*❑❑zo O z D 1 ❑ y x D z 0 ❑ m 0 Cl) z m 0 O ° N m m 9' "'❑❑0 D 011 0❑ a z cr N g. -i� 0 m n �g CID ❑ ❑ o m oar Q ; 11 ❑ 2$ m 0 G] r2 ❑ N N m n �l v d ❑❑a) z 0 Q r ❑ 0 S o m r i CD ❑ ❑ I n> ❑CA .. a 0 c❑❑Gld o z 0 � m ° 0 N ° ° m 0 N ❑ N Co r N 0 _ ❑ ❑ z a 0 rn N ❑ o o - O X O Z D r e N C (n Q� 0 3 3 -o a g' ai �a 7 3 :� � fO m o ` O S d O1 3 O = oi c �e c .d a o ' N (0c 'a CID 7 a S CO CCO _ d =olrt mm 0 a a dd 'f3 5 N n O � �o d �o ID S O 01 a No. S �CID S y <W D ma N � 0 N N a D 3 C� m .. N � c M a Q a CID 0 n 3 m N 3 T VJ fA ID a I 9 3 O nm m l _ \ =30 C1`� c-r-im� C e v"I �m J1 �zy3 e .--.-� C cm D mooX X A > cn m m-0 pm � D m 0 z D z m � 0O (A m �., v --I IN m m n Z \D f/J 0 D I � fn IM A \ c m —, v M m D N �Ool o cn cn m m 'a ;D 0 m m G o v O O .0 10 p .= M a m c 3 0 = y Da o g Z 71 H = .3. 7 < v N N n ca =v N� CD z m y x m A m C pa g°a0m �` Aa N Lmnr r■ C =r : 2 • x,A �40 r Q A� e . zo {� - 1 'r C 3 3 0 n c I, m " su m10 .30 a m zm ID_.@ m p A z CD ID a m m M) av M) ar ; d N T M. N Z j A is v W 0-3Qo p m zR.z. O m 2 Z N O ❑ N M w zo D N cD m N W rA Q a n w rrmc- o v oz�N y ❑� C0� 5L a G 1Im a R 0�mY- lil co d a F ❑ 0� p CL G 01� fn N M r a m ,113 v a N m z n 0 O F y O r m m z m �°, � a r Oz O n �m N O z z m r 300ai`-' O-o V 3 m�0® r 0 z 1 2 ni O�ODIm GAccD 0- am �� �a J Q mS n J d Case Narrative Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Chart) Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: West Sugar Creek UST Lab Submittal Date: 07/07/2020 Work Order: 0070067 7/14/20 12:08 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL a,j Angela D. Overcash Senior Project Manager Data Qualifiers Key Reference: CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. M Matrix spike outside of the control limits. SR Surrogate recovery outside of the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 36 Sample Receipt Summary Way� nt 07/14/2020 poiA Work Order: 0070067 NALYTICAL Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received Base 0070067-01 Solid 07/07/20 14:00 07/07/20 15:40 SW-1 0070067-02 Solid 07/07/20 13:55 07/07/20 15:40 SW-2 0070067-03 Solid 07/07/20 13:45 07/07/20 15:40 SW-3 0070067-04 Solid 07/07/20 13:40 07/07/20 15:40 SW-4 0070067-05 Solid 07/07/20 13:45 07/07/20 15:40 Samples were received in good condition at 4.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 36 Summary of Detections WayPAoi t 07/14067 n/2020 . Work Order: 007067 NALYTICAL Waypoint ID Client ID Parameter Method Result Units 0070067-01 Base C9-CI8 Aliphatics MADEP EPH 1.7 J mg/kg dry 0070067-01 Base Naphthalene 8260D 0.00094 J mg/kg dry 0070067-02 SW-1 Naphthalene 8260D 0.00090 J mg/kg dry 0070067-03 SW-2 Acetone 8260D 0.015 J mg/kg dry 0070067-03 SW-2 Naphthalene 8260D 0.00082 J mg/kg dry 0070067-04 SW-3 Naphthalene 8260D 0.00074 J mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: Base Attn: Andrew Frantz Sample ID: 0070067-01 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 14:00 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics 1.7 J mg/kg dry 32 1.6 1 MADEP EPH 7/10/20 16:24 ZRC POG0106 C19-C36 Aliphatics BRL mg/kg dry 32 5.3 1 MADEP EPH 7/10/20 16:24 ZRC POG0106 C11-C22 Aromatics BRL CCV mg/kg dry 32 8.6 1 MADEP EPH 7/10/20 16:24 ZRC POG0106 Surrogate Recovery Control Limits 1-Chlorooctadecane 68 % 40-140 o-Terphenyl 73 % 40-140 2-Fluorobiphenyl 85 % 40-140 2-Bromonaphthalene 91 % 40-140 General Chemistry Parameters Solids 78.5 % by 0.100 0.100 1 SM2540 G 7/13/20 10:11 EDV POG0129 Weight Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.84 0.15 1 8270E 7/10/20 14:52 JMV POG0105 1,2-Dichlorobenzene BRL mg/kg dry 0.84 0.14 1 8270E 7/10/20 14:52 JMV POG0105 1,3-Dichlorobenzene BRL mg/kg dry 0.84 0.12 1 8270E 7/10/20 14:52 JMV POG0105 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.13 1 8270E 7/10/20 14:52 JMV POG0105 1-Methyl naphthalene BRL mg/kg dry 0.84 0.013 1 8270E 7/10/20 14:52 JMV POG0105 2,4,5-Trichlorophenol BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 14:52 JMV POG0105 2,4,6-Trichlorophenol BRL mg/kg dry 0.84 0.20 1 8270E 7/10/20 14:52 JMV POG0105 2,4-Dichlorophenol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 14:52 JMV POG0105 2,4-Dimethylphenol BRL mg/kg dry 0.42 0.17 1 8270E 7/10/20 14:52 JMV POG0105 2,4-Dinitrophenol BRL mg/kg dry 1.9 0.49 1 8270E 7/10/20 14:52 JMV POG0105 2,4-Dinitrotoluene BRL mg/kg dry 0.84 0.22 1 8270E 7/10/20 14:52 JMV POG0105 2,6-Dinitrotoluene BRL mg/kg dry 0.84 0.22 1 8270E 7/10/20 14:52 JMV POG0105 2-Chloronaphthalene BRL mg/kg dry 0.84 0.20 1 8270E 7/10/20 14:52 JMV POG0105 2-Chlorophenol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 14:52 JMV POG0105 2-Methyl naphthalene BRL mg/kg dry 0.84 0.016 1 8270E 7/10/20 14:52 JMV POG0105 2-Methylphenol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 14:52 JMV POG0105 2-Nitrophenol BRL mg/kg dry 0.84 0.14 1 8270E 7/10/20 14:52 JMV POG0105 3,3'-Dichlorobenzidine BRL mg/kg dry 0.84 0.17 1 8270E 7/10/20 14:52 JMV POG0105 3/4-Methyl phenol BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 14:52 JMV POG0105 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.9 0.46 1 8270E 7/10/20 14:52 JMV POG0105 4-Bromophenyl phenyl ether BRL mg/kg dry 0.84 0.20 1 8270E 7/10/20 14:52 JMV POG0105 4-Chloro-3-methylphenol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 14:52 JMV POG0105 4-Chloroaniline BRL mg/kg dry 0.42 0.10 1 8270E 7/10/20 14:52 JMV POG0105 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.3 0.26 1 8270E 7/10/20 14:52 JMV POG0105 4-Nitrophenol BRL mg/kg dry 0.84 0.21 1 8270E 7/10/20 14:52 JMV POG0105 Acenaphthene BRL mg/kg dry 0.84 0.019 1 8270E 7/10/20 14:52 JMV POG0105 Acenaphthylene BRL mg/kg dry 0.84 0.017 1 8270E 7/10/20 14:52 JMV POG0105 Anthracene BRL mg/kg dry 0.84 0.0093 1 8270E 7/10/20 14:52 JMV POG0105 Azobenzene BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 14:52 JMV POG0105 Benzo(a)anthracene BRL mg/kg dry 0.84 0.010 1 8270E 7/10/20 14:52 JMV POG0105 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 36 • � PA Waynt. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Project: West Sugar Creek UST Sample Matrix: Solid Laboratory Report 07/14/2020 Client Sample ID: Base Sample ID: 0070067-01 Work Order: 0070067 Time Collected: 07/07/20 14:00 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(a)pyrene BRL mg/kg dry 0.84 0.0075 1 8270E 7/10/20 14:52 JMV POG0105 Benzo(b)fluoranthene BRL mg/kg dry 0.84 0.0077 1 8270E 7/10/20 14:52 JMV POG0105 Benzo(g,h,i)perylene BRL mg/kg dry 0.84 0.0083 1 8270E 7/10/20 14:52 JMV POG0105 Benzo(k)fluoranthene BRL mg/kg dry 0.84 0.0089 1 8270E 7/10/20 14:52 JMV POG0105 Benzoic Acid BRL mg/kg dry 2.5 0.70 1 8270E 7/10/20 14:52 JMV POG0105 Benzyl alcohol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 14:52 JMV POG0105 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 14:52 JMV POG0105 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.84 0.13 1 8270E 7/10/20 14:52 JMV POG0105 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.15 1 8270E 7/10/20 14:52 JMV POG0105 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.84 0.19 1 8270E 7/10/20 14:52 JMV POG0105 Butyl benzyl phthalate BRL mg/kg dry 0.42 0.14 1 8270E 7/10/20 14:52 JMV POG0105 Chrysene BRL mg/kg dry 0.84 0.0099 1 8270E 7/10/20 14:52 JMV POG0105 Dibenzo(a,h)anthracene BRL mg/kg dry 0.84 0.024 1 8270E 7/10/20 14:52 JMV POG0105 Dibenzofuran BRL mg/kg dry 0.84 0.23 1 8270E 7/10/20 14:52 JMV POG0105 Diethyl phthalate BRL mg/kg dry 0.84 0.22 1 8270E 7/10/20 14:52 JMV POG0105 Dimethyl phthalate BRL mg/kg dry 0.84 0.20 1 8270E 7/10/20 14:52 JMV POG0105 Di-n-butyl phthalate BRL mg/kg dry 0.84 0.21 1 8270E 7/10/20 14:52 JMV POG0105 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.22 1 8270E 7/10/20 14:52 JMV POG0105 Fluoranthene BRL mg/kg dry 0.84 0.0095 1 8270E 7/10/20 14:52 JMV POG0105 Fluorene BRL mg/kg dry 0.84 0.014 1 8270E 7/10/20 14:52 JMV POG0105 Hexachlorobenzene BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 14:52 JMV POG0105 Hexachlorobutadiene BRL mg/kg dry 0.84 0.19 1 8270E 7/10/20 14:52 JMV POG0105 Hexachlorocyclopentadiene BRL mg/kg dry 0.84 0.29 1 8270E 7/10/20 14:52 JMV POG0105 Hexachloroethane BRL mg/kg dry 0.84 0.13 1 8270E 7/10/20 14:52 JMV POG0105 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.84 0.024 1 8270E 7/10/20 14:52 JMV POG0105 Isophorone BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 14:52 JMV POG0105 Naphthalene BRL mg/kg dry 0.84 0.018 1 8270E 7/10/20 14:52 JMV POG0105 Nitrobenzene BRL mg/kg dry 0.42 0.18 1 8270E 7/10/20 14:52 JMV POG0105 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.84 0.19 1 8270E 7/10/20 14:52 JMV POG0105 N-Nitrosodiphenylamine BRL mg/kg dry 0.84 0.23 1 8270E 7/10/20 14:52 JMV POG0105 Pentachlorophenol BRL mg/kg dry 1.3 0.53 1 8270E 7/10/20 14:52 JMV POG0105 Phenanthrene BRL mg/kg dry 0.84 0.0091 1 8270E 7/10/20 14:52 JMV POG0105 Phenol BRL mg/kg dry 0.84 0.14 1 8270E 7/10/20 14:52 JMV POG0105 Pyrene BRL mg/kg dry 0.84 0.012 1 8270E 7/10/20 14:52 JMV POG0105 Pyridine BRL mg/kg dry 0.42 0.080 1 8270E 7/10/20 14:52 JMV POG0105 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 82 % 39-132 2-Fluorobiphenyl 71 % 44-115 2-Fluorophenol 78 % 35-115 Nitrobenzene-d5 68 % 37-122 Phenol-d5 79 % 34-121 Terphenyl-d14 72 % 54-127 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: Base Attn: Andrew Frantz Sample ID: 0070067-01 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 14:00 Time Submitted: 07/07/20 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0076 0.00092 1 8260D 7/8/20 13:12 TBL POG0082 1,1,1-Trichloroethane BRL mg/kg dry 0.0076 0.0011 1 8260D 7/8/20 13:12 TBL POG0082 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0076 0.00055 1 8260D 7/8/20 13:12 TBL POG0082 1,1,2-Trichloro-1,2,2-trifluoroethane BRL mg/kg dry 0.015 0.0013 1 8260D 7/8/20 13:12 TBL POG0082 1,1,2-Trichloroethane BRL mg/kg dry 0.0076 0.00082 1 8260D 7/8/20 13:12 TBL POG0082 1,1-Dichloroethane BRL mg/kg dry 0.0076 0.0014 1 8260D 7/8/20 13:12 TBL POG0082 1,1-Dichloroethylene BRL mg/kg dry 0.0076 0.0014 1 8260D 7/8/20 13:12 TBL POG0082 1,1-Dichloropropylene BRL mg/kg dry 0.0076 0.0012 1 8260D 7/8/20 13:12 TBL POG0082 1,2,3-Trichlorobenzene BRL mg/kg dry 0.015 0.0011 1 8260D 7/8/20 13:12 TBL POG0082 1,2,3-Trichloropropane BRL mg/kg dry 0.0076 0.00086 1 8260D 7/8/20 13:12 TBL POG0082 1,2,4-Trichlorobenzene BRL mg/kg dry 0.015 0.00072 1 8260D 7/8/20 13:12 TBL POG0082 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0076 0.00080 1 8260D 7/8/20 13:12 TBL POG0082 1,2-Dibromoethane BRL mg/kg dry 0.0076 0.00068 1 8260D 7/8/20 13:12 TBL POG0082 1,2-Dichlorobenzene BRL mg/kg dry 0.0076 0.00084 1 8260D 7/8/20 13:12 TBL POG0082 1,2-Dichloroethane BRL mg/kg dry 0.0076 0.00090 1 8260D 7/8/20 13:12 TBL POG0082 1,2-Dichloropropane BRL mg/kg dry 0.0076 0.0011 1 8260D 7/8/20 13:12 TBL POG0082 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0076 0.00095 1 8260D 7/8/20 13:12 TBL POG0082 1,3-Dichlorobenzene BRL mg/kg dry 0.0076 0.00094 1 8260D 7/8/20 13:12 TBL POG0082 1,3-Dichloropropane BRL mg/kg dry 0.0076 0.00063 1 8260D 7/8/20 13:12 TBL POG0082 1,4-Dichlorobenzene BRL mg/kg dry 0.0076 0.00096 1 8260D 7/8/20 13:12 TBL POG0082 2,2-Dichloropropane BRL mg/kg dry 0.0076 0.00094 1 8260D 7/8/20 13:12 TBL POG0082 2-Chlorotoluene BRL mg/kg dry 0.0076 0.0010 1 8260D 7/8/20 13:12 TBL POG0082 4-Chlorotoluene BRL mg/kg dry 0.0076 0.00086 1 8260D 7/8/20 13:12 TBL POG0082 4-Isopropyltoluene BRL mg/kg dry 0.0076 0.0019 1 8260D 7/8/20 13:12 TBL POG0082 Acetone BRL mg/kg dry 0.030 0.0019 1 8260D 7/8/20 13:12 TBL POG0082 Benzene BRL mg/kg dry 0.0076 0.0012 1 8260D 7/8/20 13:12 TBL POG0082 Bromobenzene BRL mg/kg dry 0.0076 0.0011 1 8260D 7/8/20 13:12 TBL POG0082 Bromochloromethane BRL mg/kg dry 0.0076 0.0012 1 8260D 7/8/20 13:12 TBL POG0082 Bromodichloromethane BRL mg/kg dry 0.0076 0.00072 1 8260D 7/8/20 13:12 TBL POG0082 Bromoform BRL mg/kg dry 0.0076 0.00059 1 8260D 7/8/20 13:12 TBL POG0082 Bromomethane BRL mg/kg dry 0.015 0.0037 1 8260D 7/8/20 13:12 TBL POG0082 Carbon Tetrachloride BRL mg/kg dry 0.0076 0.0015 1 8260D 7/8/20 13:12 TBL POG0082 Chlorobenzene BRL mg/kg dry 0.0076 0.0012 1 8260D 7/8/20 13:12 TBL POG0082 Chloroethane BRL mg/kg dry 0.015 0.0014 1 8260D 7/8/20 13:12 TBL POG0082 Chloroform BRL mg/kg dry 0.0076 0.00093 1 8260D 7/8/20 13:12 TBL POG0082 Chloromethane BRL mg/kg dry 0.015 0.0023 1 8260D 7/8/20 13:12 TBL POG0082 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0076 0.0012 1 8260D 7/8/20 13:12 TBL POG0082 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0076 0.00075 1 8260D 7/8/20 13:12 TBL POG0082 Dibromochloromethane BRL mg/kg dry 0.0076 0.00051 1 8260D 7/8/20 13:12 TBL POG0082 Dichlorodifluoromethane BRL mg/kg dry 0.015 0.0021 1 8260D 7/8/20 13:12 TBL POG0082 Ethylbenzene BRL mg/kg dry 0.0076 0.0011 1 8260D 7/8/20 13:12 TBL POG0082 Isopropyl Ether BRL mg/kg dry 0.0076 0.0011 1 8260D 7/8/20 13:12 TBL POG0082 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0076 0.00088 1 8260D 7/8/20 13:12 TBL POG0082 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: Base Attn: Andrew Frantz Sample ID: 0070067-01 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 14:00 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID m,p-Xylenes BRL mg/kg dry 0.015 0.0019 1 8260D 7/8/20 13:12 TBL POG0082 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.030 0.00052 1 8260D 7/8/20 13:12 TBL POG0082 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.030 0.0018 1 8260D 7/8/20 13:12 TBL POG0082 Methyl Isobutyl Ketone BRL mg/kg dry 0.030 0.00062 1 8260D 7/8/20 13:12 TBL POG0082 Methylene Chloride BRL mg/kg dry 0.0076 0.0012 1 8260D 7/8/20 13:12 TBL POG0082 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0076 0.0011 1 8260D 7/8/20 13:12 TBL POG0082 Naphthalene 0.00094 J mg/kg dry 0.015 0.00076 1 8260D 7/8/20 13:12 TBL POG0082 n-Butylbenzene BRL mg/kg dry 0.0076 0.00071 1 8260D 7/8/20 13:12 TBL POG0082 n-Propylbenzene BRL mg/kg dry 0.0076 0.0011 1 8260D 7/8/20 13:12 TBL POG0082 o-Xylene BRL mg/kg dry 0.0076 0.00081 1 8260D 7/8/20 13:12 TBL POG0082 sec-Butylbenzene BRL mg/kg dry 0.0076 0.00082 1 8260D 7/8/20 13:12 TBL POG0082 Styrene BRL mg/kg dry 0.0076 0.00073 1 8260D 7/8/20 13:12 TBL POG0082 tert-Butylbenzene BRL mg/kg dry 0.0076 0.00090 1 8260D 7/8/20 13:12 TBL POG0082 Tetrachloroethylene BRL mg/kg dry 0.0076 0.0014 1 8260D 7/8/20 13:12 TBL POG0082 Toluene BRL mg/kg dry 0.0076 0.0012 1 8260D 7/8/20 13:12 TBL POG0082 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0076 0.0014 1 8260D 7/8/20 13:12 TBL POG0082 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0076 0.00065 1 8260D 7/8/20 13:12 TBL POG0082 Trichloroethylene BRL mg/kg dry 0.0076 0.0015 1 8260D 7/8/20 13:12 TBL POG0082 Trichlorofluoromethane BRL mg/kg dry 0.015 0.0020 1 8260D 7/8/20 13:12 TBL POG0082 Vinyl acetate BRL mg/kg dry 0.015 0.00082 1 8260D 7/8/20 13:12 TBL POG0082 Vinyl chloride BRL mg/kg dry 0.015 0.0015 1 8260D 7/8/20 13:12 TBL POG0082 Xylenes, total BRL mg/kg dry 0.023 0.0027 1 8260D 7/8/20 13:12 TBL POG0082 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 94 % 84-123 Toluene-d8 89 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 16 3.2 100 MADEP VPH 7/8/20 14:32 TBL POG0081 C9-Cl2 Aliphatics BRL mg/kg dry 16 1.4 100 MADEP VPH 7/8/20 14:32 TBL POG0081 C9-Cl0 Aromatics BRL mg/kg dry 16 1.5 100 MADEP VPH 7/8/20 14:32 TBL POG0081 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 116 % 70-130 2,5-Dibromotoluene (FID) 123 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-1 Attn: Andrew Frantz Sample ID: 0070067-02 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:55 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics BRL mg/kg dry 32 1.6 1 MADEP EPH 7/10/20 17:00 ZRC POG0106 C19-C36 Aliphatics BRL mg/kg dry 32 5.4 1 MADEP EPH 7/10/20 17:00 ZRC POG0106 C11-C22 Aromatics BRL CCV mg/kg dry 32 8.7 1 MADEP EPH 7/10/20 17:00 ZRC POG0106 Surrogate Recovery Control Limits 1-Chlorooctadecane 66 % 40-140 o-Terphenyl 66 % 40-140 2-Fluorobiphenyl 75 % 40-140 2-Bromonaphthalene 44 % 40-140 General Chemistry Parameters % Solids 78.1 % by 0.100 0.100 1 SM2540 G 7113/20 10:11 EDV POG0129 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.84 0.15 1 8270E 7/10/20 15:15 JMV POG0105 1,2-Dichlorobenzene BRL mg/kg dry 0.84 0.14 1 8270E 7/10/20 15:15 JMV POG0105 1,3-Dichlorobenzene BRL mg/kg dry 0.84 0.12 1 8270E 7/10/20 15:15 JMV POG0105 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.13 1 8270E 7/10/20 15:15 JMV POG0105 1-Methyl naphthalene BRL mg/kg dry 0.84 0.013 1 8270E 7/10/20 15:15 JMV POG0105 2,4,5-Trichlorophenol BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 15:15 JMV POG0105 2,4,6-Trichlorophenol BRL mg/kg dry 0.84 0.20 1 8270E 7/10/20 15:15 JMV POG0105 2,4-Dichlorophenol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 15:15 JMV POG0105 2,4-Dimethylphenol BRL mg/kg dry 0.42 0.18 1 8270E 7/10/20 15:15 JMV POG0105 2,4-Dinitrophenol BRL mg/kg dry 1.9 0.49 1 8270E 7/10/20 15:15 JMV POG0105 2,4-Dinitrotoluene BRL mg/kg dry 0.84 0.22 1 8270E 7/10/20 15:15 JMV POG0105 2,6-Dinitrotoluene BRL mg/kg dry 0.84 0.22 1 8270E 7/10/20 15:15 JMV POG0105 2-Chloronaphthalene BRL mg/kg dry 0.84 0.21 1 8270E 7/10/20 15:15 JMV POG0105 2-Chlorophenol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 15:15 JMV POG0105 2-Methyl naphthalene BRL mg/kg dry 0.84 0.016 1 8270E 7/10/20 15:15 JMV POG0105 2-Methylphenol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 15:15 JMV POG0105 2-Nitrophenol BRL mg/kg dry 0.84 0.14 1 8270E 7/10/20 15:15 JMV POG0105 3,3'-Dichlorobenzidine BRL mg/kg dry 0.84 0.17 1 8270E 7/10/20 15:15 JMV POG0105 3/4-Methyl phenol BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 15:15 JMV POG0105 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.9 0.47 1 8270E 7/10/20 15:15 JMV POG0105 4-Bromophenyl phenyl ether BRL mg/kg dry 0.84 0.20 1 8270E 7/10/20 15:15 JMV POG0105 4-Chloro-3-methylphenol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 15:15 JMV POG0105 4-Chloroaniline BRL mg/kg dry 0.42 0.10 1 8270E 7/10/20 15:15 JMV POG0105 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.3 0.26 1 8270E 7/10/20 15:15 JMV POG0105 4-Nitrophenol BRL mg/kg dry 0.84 0.21 1 8270E 7/10/20 15:15 JMV POG0105 Acenaphthene BRL mg/kg dry 0.84 0.019 1 8270E 7/10/20 15:15 JMV POG0105 Acenaphthylene BRL mg/kg dry 0.84 0.017 1 8270E 7/10/20 15:15 JMV POG0105 Anthracene BRL mg/kg dry 0.84 0.0093 1 8270E 7/10/20 15:15 JMV POG0105 Azobenzene BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 15:15 JMV POG0105 Benzo(a)anthracene BRL mg/kg dry 0.84 0.010 1 8270E 7/10/20 15:15 JMV POG0105 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 36 • � PA Waynt. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Project: West Sugar Creek UST Sample Matrix: Solid Laboratory Report 07/14/2020 Client Sample ID: SW-1 Sample ID: 0070067-02 Work Order: 0070067 Time Collected: 07/07/20 13:55 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(a)pyrene BRL mg/kg dry 0.84 0.0075 1 8270E 7/10/20 15:15 JMV POG0105 Benzo(b)fluoranthene BRL mg/kg dry 0.84 0.0078 1 8270E 7/10/20 15:15 JMV POG0105 Benzo(g,h,i)perylene BRL mg/kg dry 0.84 0.0083 1 8270E 7/10/20 15:15 JMV POG0105 Benzo(k)fluoranthene BRL mg/kg dry 0.84 0.0090 1 8270E 7/10/20 15:15 JMV POG0105 Benzoic Acid BRL mg/kg dry 2.6 0.70 1 8270E 7/10/20 15:15 JMV POG0105 Benzyl alcohol BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 15:15 JMV POG0105 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.84 0.16 1 8270E 7/10/20 15:15 JMV POG0105 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.84 0.14 1 8270E 7/10/20 15:15 JMV POG0105 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.15 1 8270E 7/10/20 15:15 JMV POG0105 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.84 0.19 1 8270E 7/10/20 15:15 JMV POG0105 Butyl benzyl phthalate BRL mg/kg dry 0.42 0.15 1 8270E 7/10/20 15:15 JMV POG0105 Chrysene BRL mg/kg dry 0.84 0.010 1 8270E 7/10/20 15:15 JMV POG0105 Dibenzo(a,h)anthracene BRL mg/kg dry 0.84 0.024 1 8270E 7/10/20 15:15 JMV POG0105 Dibenzofuran BRL mg/kg dry 0.84 0.23 1 8270E 7/10/20 15:15 JMV POG0105 Diethyl phthalate BRL mg/kg dry 0.84 0.22 1 8270E 7/10/20 15:15 JMV POG0105 Dimethyl phthalate BRL mg/kg dry 0.84 0.20 1 8270E 7/10/20 15:15 JMV POG0105 Di-n-butyl phthalate BRL mg/kg dry 0.84 0.21 1 8270E 7/10/20 15:15 JMV POG0105 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.22 1 8270E 7/10/20 15:15 JMV POG0105 Fluoranthene BRL mg/kg dry 0.84 0.0096 1 8270E 7/10/20 15:15 JMV POG0105 Fluorene BRL mg/kg dry 0.84 0.015 1 8270E 7/10/20 15:15 JMV POG0105 Hexachlorobenzene BRL mg/kg dry 0.84 0.19 1 8270E 7/10/20 15:15 JMV POG0105 Hexachlorobutadiene BRL mg/kg dry 0.84 0.19 1 8270E 7/10/20 15:15 JMV POG0105 Hexachlorocyclopentadiene BRL mg/kg dry 0.84 0.29 1 8270E 7/10/20 15:15 JMV POG0105 Hexachloroethane BRL mg/kg dry 0.84 0.13 1 8270E 7/10/20 15:15 JMV POG0105 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.84 0.024 1 8270E 7/10/20 15:15 JMV POG0105 Isophorone BRL mg/kg dry 0.84 0.18 1 8270E 7/10/20 15:15 JMV POG0105 Naphthalene BRL mg/kg dry 0.84 0.018 1 8270E 7/10/20 15:15 JMV POG0105 Nitrobenzene BRL mg/kg dry 0.42 0.18 1 8270E 7/10/20 15:15 JMV POG0105 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.84 0.19 1 8270E 7/10/20 15:15 JMV POG0105 N-Nitrosodiphenylamine BRL mg/kg dry 0.84 0.23 1 8270E 7/10/20 15:15 JMV POG0105 Pentachlorophenol BRL mg/kg dry 1.3 0.54 1 8270E 7/10/20 15:15 JMV POG0105 Phenanthrene BRL mg/kg dry 0.84 0.0092 1 8270E 7/10/20 15:15 JMV POG0105 Phenol BRL mg/kg dry 0.84 0.14 1 8270E 7/10/20 15:15 JMV POG0105 Pyrene BRL mg/kg dry 0.84 0.012 1 8270E 7/10/20 15:15 JMV POG0105 Pyridine BRL mg/kg dry 0.42 0.081 1 8270E 7/10/20 15:15 JMV POG0105 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 83 % 39-132 2-Fluorobiphenyl 68 % 44-115 2-Fluorophenol 73 % 35-115 Nitrobenzene-d5 64 % 37-122 Phenol-d5 73 % 34-121 Terphenyl-d14 76 % 54-127 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-1 Attn: Andrew Frantz Sample ID: 0070067-02 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:55 Time Submitted: 07/07/20 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0073 0.00089 1 8260D 7/8/20 10:43 TBL POG0082 1,1,1-Trichloroethane BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0073 0.00053 1 8260D 7/8/20 10:43 TBL POG0082 1,1,2-Trichloro-1,2,2-trifluoroethane BRL mg/kg dry 0.015 0.0013 1 8260D 7/8/20 10:43 TBL POG0082 1,1,2-Trichloroethane BRL mg/kg dry 0.0073 0.00078 1 8260D 7/8/20 10:43 TBL POG0082 1,1-Dichloroethane BRL mg/kg dry 0.0073 0.0013 1 8260D 7/8/20 10:43 TBL POG0082 1,1-Dichloroethylene BRL mg/kg dry 0.0073 0.0013 1 8260D 7/8/20 10:43 TBL POG0082 1,1-Dichloropropylene BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 1,2,3-Trichlorobenzene BRL mg/kg dry 0.015 0.0010 1 8260D 7/8/20 10:43 TBL POG0082 1,2,3-Trichloropropane BRL mg/kg dry 0.0073 0.00082 1 8260D 7/8/20 10:43 TBL POG0082 1,2,4-Trichlorobenzene BRL mg/kg dry 0.015 0.00069 1 8260D 7/8/20 10:43 TBL POG0082 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0073 0.00077 1 8260D 7/8/20 10:43 TBL POG0082 1,2-Dibromoethane BRL mg/kg dry 0.0073 0.00065 1 8260D 7/8/20 10:43 TBL POG0082 1,2-Dichlorobenzene BRL mg/kg dry 0.0073 0.00081 1 8260D 7/8/20 10:43 TBL POG0082 1,2-Dichloroethane BRL mg/kg dry 0.0073 0.00086 1 8260D 7/8/20 10:43 TBL POG0082 1,2-Dichloropropane BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0073 0.00091 1 8260D 7/8/20 10:43 TBL POG0082 1,3-Dichlorobenzene BRL mg/kg dry 0.0073 0.00090 1 8260D 7/8/20 10:43 TBL POG0082 1,3-Dichloropropane BRL mg/kg dry 0.0073 0.00061 1 8260D 7/8/20 10:43 TBL POG0082 1,4-Dichlorobenzene BRL mg/kg dry 0.0073 0.00092 1 8260D 7/8/20 10:43 TBL POG0082 2,2-Dichloropropane BRL mg/kg dry 0.0073 0.00090 1 8260D 7/8/20 10:43 TBL POG0082 2-Chlorotoluene BRL mg/kg dry 0.0073 0.00097 1 8260D 7/8/20 10:43 TBL POG0082 4-Chlorotoluene BRL mg/kg dry 0.0073 0.00083 1 8260D 7/8/20 10:43 TBL POG0082 4-Isopropyltoluene BRL mg/kg dry 0.0073 0.0018 1 8260D 7/8/20 10:43 TBL POG0082 Acetone BRL mg/kg dry 0.029 0.0019 1 8260D 7/8/20 10:43 TBL POG0082 Benzene BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 Bromobenzene BRL mg/kg dry 0.0073 0.0010 1 8260D 7/8/20 10:43 TBL POG0082 Bromochloromethane BRL mg/kg dry 0.0073 0.0012 1 8260D 7/8/20 10:43 TBL POG0082 Bromodichloromethane BRL mg/kg dry 0.0073 0.00069 1 8260D 7/8/20 10:43 TBL POG0082 Bromoform BRL mg/kg dry 0.0073 0.00056 1 8260D 7/8/20 10:43 TBL POG0082 Bromomethane BRL mg/kg dry 0.015 0.0036 1 8260D 7/8/20 10:43 TBL POG0082 Carbon Tetrachloride BRL mg/kg dry 0.0073 0.0014 1 8260D 7/8/20 10:43 TBL POG0082 Chlorobenzene BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 Chloroethane BRL mg/kg dry 0.015 0.0014 1 8260D 7/8/20 10:43 TBL POG0082 Chloroform BRL mg/kg dry 0.0073 0.00089 1 8260D 7/8/20 10:43 TBL POG0082 Chloromethane BRL mg/kg dry 0.015 0.0022 1 8260D 7/8/20 10:43 TBL POG0082 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0073 0.00072 1 8260D 7/8/20 10:43 TBL POG0082 Dibromochloromethane BRL mg/kg dry 0.0073 0.00049 1 8260D 7/8/20 10:43 TBL POG0082 Dichlorodifluoromethane BRL mg/kg dry 0.015 0.0020 1 8260D 7/8/20 10:43 TBL POG0082 Ethylbenzene BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 Isopropyl Ether BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0073 0.00085 1 8260D 7/8/20 10:43 TBL POG0082 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-1 Attn: Andrew Frantz Sample ID: 0070067-02 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:55 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID m,p-Xylenes BRL mg/kg dry 0.015 0.0019 1 8260D 7/8/20 10:43 TBL POG0082 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.029 0.00050 1 8260D 7/8/20 10:43 TBL POG0082 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.029 0.0017 1 8260D 7/8/20 10:43 TBL POG0082 Methyl Isobutyl Ketone BRL mg/kg dry 0.029 0.00059 1 8260D 7/8/20 10:43 TBL POG0082 Methylene Chloride BRL mg/kg dry 0.0073 0.0012 1 8260D 7/8/20 10:43 TBL POG0082 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0073 0.0010 1 8260D 7/8/20 10:43 TBL POG0082 Naphthalene 0.00090 J mg/kg dry 0.015 0.00073 1 8260D 7/8/20 10:43 TBL POG0082 n-Butylbenzene BRL mg/kg dry 0.0073 0.00068 1 8260D 7/8/20 10:43 TBL POG0082 n-Propylbenzene BRL mg/kg dry 0.0073 0.0011 1 8260D 7/8/20 10:43 TBL POG0082 o-Xylene BRL mg/kg dry 0.0073 0.00077 1 8260D 7/8/20 10:43 TBL POG0082 sec-Butylbenzene BRL mg/kg dry 0.0073 0.00078 1 8260D 7/8/20 10:43 TBL POG0082 Styrene BRL mg/kg dry 0.0073 0.00070 1 8260D 7/8/20 10:43 TBL POG0082 tert-Butylbenzene BRL mg/kg dry 0.0073 0.00086 1 8260D 7/8/20 10:43 TBL POG0082 Tetrachloroethylene BRL mg/kg dry 0.0073 0.0013 1 8260D 7/8/20 10:43 TBL POG0082 Toluene BRL mg/kg dry 0.0073 0.0012 1 8260D 7/8/20 10:43 TBL POG0082 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0073 0.0014 1 8260D 7/8/20 10:43 TBL POG0082 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0073 0.00062 1 8260D 7/8/20 10:43 TBL POG0082 Trichloroethylene BRL mg/kg dry 0.0073 0.0014 1 8260D 7/8/20 10:43 TBL POG0082 Trichlorofluoromethane BRL mg/kg dry 0.015 0.0020 1 8260D 7/8/20 10:43 TBL POG0082 Vinyl acetate BRL mg/kg dry 0.015 0.00079 1 8260D 7/8/20 10:43 TBL POG0082 Vinyl chloride BRL mg/kg dry 0.015 0.0014 1 8260D 7/8/20 10:43 TBL POG0082 Xylenes, total BRL mg/kg dry 0.022 0.0026 1 8260D 7/8/20 10:43 TBL POG0082 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 70-130 Dibromofluoromethane 93 % 84-123 Toluene-d8 91 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 23 4.6 100 MADEP VPH 7/8/20 15:01 TBL POG0081 C9-Cl2 Aliphatics BRL mg/kg dry 23 2.1 100 MADEP VPH 7/8/20 15:01 TBL POG0081 C9-Cl0 Aromatics BRL mg/kg dry 23 2.2 100 MADEP VPH 7/8/20 15:01 TBL POG0081 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 121 % 70-130 2,5-Dibromotoluene (FID) 125 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-2 Attn: Andrew Frantz Sample ID: 0070067-03 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:45 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics BRL mg/kg dry 32 1.6 1 MADEP EPH 7/10/20 17:36 ZRC POG0106 C19-C36 Aliphatics BRL mg/kg dry 32 5.4 1 MADEP EPH 7/10/20 17:36 ZRC POG0106 C11-C22 Aromatics BRL CCV mg/kg dry 32 8.8 1 MADEP EPH 7/10/20 17:36 ZRC POG0106 Surrogate Recovery Control Limits 1-Chlorooctadecane 66 % 40-140 o-Terphenyl 65 % 40-140 2-Fluorobiphenyl 71 % 40-140 2-Bromonaphthalene 39 % 40-140 SR General Chemistry Parameters % Solids 76.0 % by 0.100 0.100 1 SM2540 G 7113/20 10:11 EDV POG0129 Weight Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.87 0.15 1 8270E 7/10/20 15:38 JMV POG0105 1,2-Dichlorobenzene BRL mg/kg dry 0.87 0.14 1 8270E 7/10/20 15:38 JMV POG0105 1,3-Dichlorobenzene BRL mg/kg dry 0.87 0.13 1 8270E 7/10/20 15:38 JMV POG0105 1,4-Dichlorobenzene BRL mg/kg dry 0.43 0.14 1 8270E 7/10/20 15:38 JMV POG0105 1-Methyl naphthalene BRL mg/kg dry 0.87 0.013 1 8270E 7/10/20 15:38 JMV POG0105 2,4,5-Trichlorophenol BRL mg/kg dry 0.87 0.18 1 8270E 7/10/20 15:38 JMV POG0105 2,4,6-Trichlorophenol BRL mg/kg dry 0.87 0.21 1 8270E 7/10/20 15:38 JMV POG0105 2,4-Dichlorophenol BRL mg/kg dry 0.87 0.17 1 8270E 7/10/20 15:38 JMV POG0105 2,4-Dimethylphenol BRL mg/kg dry 0.43 0.18 1 8270E 7/10/20 15:38 JMV POG0105 2,4-Dinitrophenol BRL mg/kg dry 2.0 0.51 1 8270E 7/10/20 15:38 JMV POG0105 2,4-Dinitrotoluene BRL mg/kg dry 0.87 0.23 1 8270E 7/10/20 15:38 JMV POG0105 2,6-Dinitrotoluene BRL mg/kg dry 0.87 0.22 1 8270E 7/10/20 15:38 JMV POG0105 2-Chloronaphthalene BRL mg/kg dry 0.87 0.21 1 8270E 7/10/20 15:38 JMV POG0105 2-Chlorophenol BRL mg/kg dry 0.87 0.17 1 8270E 7/10/20 15:38 JMV POG0105 2-Methyl naphthalene BRL mg/kg dry 0.87 0.017 1 8270E 7/10/20 15:38 JMV POG0105 2-Methylphenol BRL mg/kg dry 0.87 0.17 1 8270E 7/10/20 15:38 JMV POG0105 2-Nitrophenol BRL mg/kg dry 0.87 0.14 1 8270E 7/10/20 15:38 JMV POG0105 3,3'-Dichlorobenzidine BRL mg/kg dry 0.87 0.17 1 8270E 7/10/20 15:38 JMV POG0105 3/4-Methyl phenol BRL mg/kg dry 0.87 0.19 1 8270E 7/10/20 15:38 JMV POG0105 4,6-Dinitro-2-methylphenol BRL mg/kg dry 2.0 0.48 1 8270E 7/10/20 15:38 JMV POG0105 4-Bromophenyl phenyl ether BRL mg/kg dry 0.87 0.20 1 8270E 7/10/20 15:38 JMV POG0105 4-Chloro-3-methylphenol BRL mg/kg dry 0.87 0.17 1 8270E 7/10/20 15:38 JMV POG0105 4-Chloroaniline BRL mg/kg dry 0.43 0.11 1 8270E 7/10/20 15:38 JMV POG0105 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.3 0.27 1 8270E 7/10/20 15:38 JMV POG0105 4-Nitrophenol BRL mg/kg dry 0.87 0.21 1 8270E 7/10/20 15:38 JMV POG0105 Acenaphthene BRL mg/kg dry 0.87 0.020 1 8270E 7/10/20 15:38 JMV POG0105 Acenaphthylene BRL mg/kg dry 0.87 0.017 1 8270E 7/10/20 15:38 JMV POG0105 Anthracene BRL mg/kg dry 0.87 0.0096 1 8270E 7/10/20 15:38 JMV POG0105 Azobenzene BRL mg/kg dry 0.87 0.19 1 8270E 7/10/20 15:38 JMV POG0105 Benzo(a)anthracene BRL mg/kg dry 0.87 0.010 1 8270E 7/10/20 15:38 JMV POG0105 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 0f 36 • � PA Waynt. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Project: West Sugar Creek UST Sample Matrix: Solid Laboratory Report 07/14/2020 Client Sample ID: SW-2 Sample ID: 0070067-03 Work Order: 0070067 Time Collected: 07/07/20 13:45 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(a)pyrene BRL mg/kg dry 0.87 0.0078 1 8270E 7/10/20 15:38 JMV POG0105 Benzo(b)fluoranthene BRL mg/kg dry 0.87 0.0080 1 8270E 7/10/20 15:38 JMV POG0105 Benzo(g,h,i)perylene BRL mg/kg dry 0.87 0.0085 1 8270E 7/10/20 15:38 JMV POG0105 Benzo(k)fluoranthene BRL mg/kg dry 0.87 0.0092 1 8270E 7/10/20 15:38 JMV POG0105 Benzoic Acid BRL mg/kg dry 2.6 0.72 1 8270E 7/10/20 15:38 JMV POG0105 Benzyl alcohol BRL mg/kg dry 0.87 0.16 1 8270E 7/10/20 15:38 JMV POG0105 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.87 0.17 1 8270E 7/10/20 15:38 JMV POG0105 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.87 0.14 1 8270E 7/10/20 15:38 JMV POG0105 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.43 0.16 1 8270E 7/10/20 15:38 JMV POG0105 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.87 0.20 1 8270E 7/10/20 15:38 JMV POG0105 Butyl benzyl phthalate BRL mg/kg dry 0.43 0.15 1 8270E 7/10/20 15:38 JMV POG0105 Chrysene BRL mg/kg dry 0.87 0.010 1 8270E 7/10/20 15:38 JMV POG0105 Dibenzo(a,h)anthracene BRL mg/kg dry 0.87 0.025 1 8270E 7/10/20 15:38 JMV POG0105 Dibenzofuran BRL mg/kg dry 0.87 0.23 1 8270E 7/10/20 15:38 JMV POG0105 Diethyl phthalate BRL mg/kg dry 0.87 0.22 1 8270E 7/10/20 15:38 JMV POG0105 Dimethyl phthalate BRL mg/kg dry 0.87 0.21 1 8270E 7/10/20 15:38 JMV POG0105 Di-n-butyl phthalate BRL mg/kg dry 0.87 0.22 1 8270E 7/10/20 15:38 JMV POG0105 Di-n-octyl phthalate BRL mg/kg dry 0.43 0.22 1 8270E 7/10/20 15:38 JMV POG0105 Fluoranthene BRL mg/kg dry 0.87 0.0099 1 8270E 7/10/20 15:38 JMV POG0105 Fluorene BRL mg/kg dry 0.87 0.015 1 8270E 7/10/20 15:38 JMV POG0105 Hexachlorobenzene BRL mg/kg dry 0.87 0.19 1 8270E 7/10/20 15:38 JMV POG0105 Hexachlorobutadiene BRL mg/kg dry 0.87 0.20 1 8270E 7/10/20 15:38 JMV POG0105 Hexachlorocyclopentadiene BRL mg/kg dry 0.87 0.30 1 8270E 7/10/20 15:38 JMV POG0105 Hexachloroethane BRL mg/kg dry 0.87 0.14 1 8270E 7/10/20 15:38 JMV POG0105 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.87 0.024 1 8270E 7/10/20 15:38 JMV POG0105 Isophorone BRL mg/kg dry 0.87 0.19 1 8270E 7/10/20 15:38 JMV POG0105 Naphthalene BRL mg/kg dry 0.87 0.018 1 8270E 7/10/20 15:38 JMV POG0105 Nitrobenzene BRL mg/kg dry 0.43 0.18 1 8270E 7/10/20 15:38 JMV POG0105 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.87 0.20 1 8270E 7/10/20 15:38 JMV POG0105 N-Nitrosodiphenylamine BRL mg/kg dry 0.87 0.24 1 8270E 7/10/20 15:38 JMV POG0105 Pentachlorophenol BRL mg/kg dry 1.3 0.55 1 8270E 7/10/20 15:38 JMV POG0105 Phenanthrene BRL mg/kg dry 0.87 0.0095 1 8270E 7/10/20 15:38 JMV POG0105 Phenol BRL mg/kg dry 0.87 0.14 1 8270E 7/10/20 15:38 JMV POG0105 Pyrene BRL mg/kg dry 0.87 0.013 1 8270E 7/10/20 15:38 JMV POG0105 Pyridine BRL mg/kg dry 0.43 0.083 1 8270E 7/10/20 15:38 JMV POG0105 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 86 % 39-132 2-Fluorobiphenyl 72 % 44-115 2-Fluorophenol 80 % 35-115 Nitrobenzene-d5 69 % 37-122 Phenol-d5 80 % 34-121 Terphenyl-d14 81 % 54-127 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 0f 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-2 Attn: Andrew Frantz Sample ID: 0070067-03 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:45 Time Submitted: 07/07/20 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0069 0.00084 1 8260D 7/8/20 11:13 TBL POG0082 1,1,1-Trichloroethane BRL mg/kg dry 0.0069 0.0010 1 8260D 7/8/20 11:13 TBL POG0082 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0069 0.00050 1 8260D 7/8/20 11:13 TBL POG0082 1,1,2-Trichloro-1,2,2-trifluoroethane BRL mg/kg dry 0.014 0.0012 1 8260D 7/8/20 11:13 TBL POG0082 1,1,2-Trichloroethane BRL mg/kg dry 0.0069 0.00075 1 8260D 7/8/20 11:13 TBL POG0082 1,1-Dichloroethane BRL mg/kg dry 0.0069 0.0012 1 8260D 7/8/20 11:13 TBL POG0082 1,1-Dichloroethylene BRL mg/kg dry 0.0069 0.0013 1 8260D 7/8/20 11:13 TBL POG0082 1,1-Dichloropropylene BRL mg/kg dry 0.0069 0.0011 1 8260D 7/8/20 11:13 TBL POG0082 1,2,3-Trichlorobenzene BRL mg/kg dry 0.014 0.00099 1 8260D 7/8/20 11:13 TBL POG0082 1,2,3-Trichloropropane BRL mg/kg dry 0.0069 0.00079 1 8260D 7/8/20 11:13 TBL POG0082 1,2,4-Trichlorobenzene BRL mg/kg dry 0.014 0.00066 1 8260D 7/8/20 11:13 TBL POG0082 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0069 0.00073 1 8260D 7/8/20 11:13 TBL POG0082 1,2-Dibromoethane BRL mg/kg dry 0.0069 0.00062 1 8260D 7/8/20 11:13 TBL POG0082 1,2-Dichlorobenzene BRL mg/kg dry 0.0069 0.00077 1 8260D 7/8/20 11:13 TBL POG0082 1,2-Dichloroethane BRL mg/kg dry 0.0069 0.00082 1 8260D 7/8/20 11:13 TBL POG0082 1,2-Dichloropropane BRL mg/kg dry 0.0069 0.0010 1 8260D 7/8/20 11:13 TBL POG0082 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0069 0.00087 1 8260D 7/8/20 11:13 TBL POG0082 1,3-Dichlorobenzene BRL mg/kg dry 0.0069 0.00086 1 8260D 7/8/20 11:13 TBL POG0082 1,3-Dichloropropane BRL mg/kg dry 0.0069 0.00058 1 8260D 7/8/20 11:13 TBL POG0082 1,4-Dichlorobenzene BRL mg/kg dry 0.0069 0.00088 1 8260D 7/8/20 11:13 TBL POG0082 2,2-Dichloropropane BRL mg/kg dry 0.0069 0.00086 1 8260D 7/8/20 11:13 TBL POG0082 2-Chlorotoluene BRL mg/kg dry 0.0069 0.00093 1 8260D 7/8/20 11:13 TBL POG0082 4-Chlorotoluene BRL mg/kg dry 0.0069 0.00079 1 8260D 7/8/20 11:13 TBL POG0082 4-Isopropyltoluene BRL mg/kg dry 0.0069 0.0017 1 8260D 7/8/20 11:13 TBL POG0082 Acetone 0.015 J mg/kg dry 0.028 0.0018 1 8260D 7/8/20 11:13 TBL POG0082 Benzene BRL mg/kg dry 0.0069 0.0011 1 8260D 7/8/20 11:13 TBL POG0082 Bromobenzene BRL mg/kg dry 0.0069 0.00096 1 8260D 7/8/20 11:13 TBL POG0082 Bromochloromethane BRL mg/kg dry 0.0069 0.0011 1 8260D 7/8/20 11:13 TBL POG0082 Bromodichloromethane BRL mg/kg dry 0.0069 0.00066 1 8260D 7/8/20 11:13 TBL POG0082 Bromoform BRL mg/kg dry 0.0069 0.00053 1 8260D 7/8/20 11:13 TBL POG0082 Bromomethane BRL mg/kg dry 0.014 0.0034 1 8260D 7/8/20 11:13 TBL POG0082 Carbon Tetrachloride BRL mg/kg dry 0.0069 0.0014 1 8260D 7/8/20 11:13 TBL POG0082 Chlorobenzene BRL mg/kg dry 0.0069 0.0011 1 8260D 7/8/20 11:13 TBL POG0082 Chloroethane BRL mg/kg dry 0.014 0.0013 1 8260D 7/8/20 11:13 TBL POG0082 Chloroform BRL mg/kg dry 0.0069 0.00085 1 8260D 7/8/20 11:13 TBL POG0082 Chloromethane BRL mg/kg dry 0.014 0.0021 1 8260D 7/8/20 11:13 TBL POG0082 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0069 0.0011 1 8260D 7/8/20 11:13 TBL POG0082 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0069 0.00068 1 8260D 7/8/20 11:13 TBL POG0082 Dibromochloromethane BRL mg/kg dry 0.0069 0.00046 1 8260D 7/8/20 11:13 TBL POG0082 Dichlorodifluoromethane BRL mg/kg dry 0.014 0.0019 1 8260D 7/8/20 11:13 TBL POG0082 Ethylbenzene BRL mg/kg dry 0.0069 0.0010 1 8260D 7/8/20 11:13 TBL POG0082 Isopropyl Ether BRL mg/kg dry 0.0069 0.0010 1 8260D 7/8/20 11:13 TBL POG0082 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0069 0.00080 1 8260D 7/8/20 11:13 TBL POG0082 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 0f 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-2 Attn: Andrew Frantz Sample ID: 0070067-03 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:45 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID m,p-Xylenes BRL mg/kg dry 0.014 0.0018 1 8260D 7/8/20 11:13 TBL POG0082 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.028 0.00048 1 8260D 7/8/20 11:13 TBL POG0082 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.028 0.0016 1 8260D 7/8/20 11:13 TBL POG0082 Methyl Isobutyl Ketone BRL mg/kg dry 0.028 0.00056 1 8260D 7/8/20 11:13 TBL POG0082 Methylene Chloride BRL mg/kg dry 0.0069 0.0011 1 8260D 7/8/20 11:13 TBL POG0082 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0069 0.00097 1 8260D 7/8/20 11:13 TBL POG0082 Naphthalene 0.00082 J mg/kg dry 0.014 0.00070 1 8260D 7/8/20 11:13 TBL POG0082 n-Butylbenzene BRL mg/kg dry 0.0069 0.00065 1 8260D 7/8/20 11:13 TBL POG0082 n-Propylbenzene BRL mg/kg dry 0.0069 0.0010 1 8260D 7/8/20 11:13 TBL POG0082 o-Xylene BRL mg/kg dry 0.0069 0.00074 1 8260D 7/8/20 11:13 TBL POG0082 sec-Butylbenzene BRL mg/kg dry 0.0069 0.00075 1 8260D 7/8/20 11:13 TBL POG0082 Styrene BRL mg/kg dry 0.0069 0.00067 1 8260D 7/8/20 11:13 TBL POG0082 tert-Butylbenzene BRL mg/kg dry 0.0069 0.00082 1 8260D 7/8/20 11:13 TBL POG0082 Tetrachloroethylene BRL mg/kg dry 0.0069 0.0013 1 8260D 7/8/20 11:13 TBL POG0082 Toluene BRL mg/kg dry 0.0069 0.0011 1 8260D 7/8/20 11:13 TBL POG0082 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0069 0.0013 1 8260D 7/8/20 11:13 TBL POG0082 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0069 0.00059 1 8260D 7/8/20 11:13 TBL POG0082 Trichloroethylene BRL mg/kg dry 0.0069 0.0013 1 8260D 7/8/20 11:13 TBL POG0082 Trichlorofluoromethane BRL mg/kg dry 0.014 0.0019 1 8260D 7/8/20 11:13 TBL POG0082 Vinyl acetate BRL mg/kg dry 0.014 0.00075 1 8260D 7/8/20 11:13 TBL POG0082 Vinyl chloride BRL mg/kg dry 0.014 0.0014 1 8260D 7/8/20 11:13 TBL POG0082 Xylenes, total BRL mg/kg dry 0.021 0.0025 1 8260D 7/8/20 11:13 TBL POG0082 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 95 % 84-123 Toluene-d8 90 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 17 3.3 100 MADEP VPH 7/8/20 15:31 TBL POG0081 C9-Cl2 Aliphatics BRL mg/kg dry 17 1.5 100 MADEP VPH 7/8/20 15:31 TBL POG0081 C9-Cl0 Aromatics BRL mg/kg dry 17 1.6 100 MADEP VPH 7/8/20 15:31 TBL POG0081 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 119 % 70-130 2,5-Dibromotoluene (FID) 126 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 0f 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-3 Attn: Andrew Frantz Sample ID: 0070067-04 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:40 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics BRL mg/kg dry 32 1.6 1 MADEP EPH 7/10/20 18:12 ZRC POG0106 C19-C36 Aliphatics BRL mg/kg dry 32 5.4 1 MADEP EPH 7/10/20 18:12 ZRC POG0106 C11-C22 Aromatics BRL CCV mg/kg dry 32 8.8 1 MADEP EPH 7/10/20 18:12 ZRC POG0106 Surrogate Recovery Control Limits 1-Chlorooctadecane 61 % 40-140 o-Terphenyl 67 % 40-140 2-Fluorobiphenyl 83 % 40-140 2-Bromonaphthalene 88 % 40-140 General Chemistry Parameters % Solids 77.8 % by 0.100 0.100 1 SM2540 G 7113/20 10:11 EDV POG0129 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.85 0.15 1 8270E 7/10/20 16:01 JMV POG0105 1,2-Dichlorobenzene BRL mg/kg dry 0.85 0.14 1 8270E 7/10/20 16:01 JMV POG0105 1,3-Dichlorobenzene BRL mg/kg dry 0.85 0.12 1 8270E 7/10/20 16:01 JMV POG0105 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.13 1 8270E 7/10/20 16:01 JMV POG0105 1-Methyl naphthalene BRL mg/kg dry 0.85 0.013 1 8270E 7/10/20 16:01 JMV POG0105 2,4,5-Trichlorophenol BRL mg/kg dry 0.85 0.18 1 8270E 7/10/20 16:01 JMV POG0105 2,4,6-Trichlorophenol BRL mg/kg dry 0.85 0.21 1 8270E 7/10/20 16:01 JMV POG0105 2,4-Dichlorophenol BRL mg/kg dry 0.85 0.17 1 8270E 7/10/20 16:01 JMV POG0105 2,4-Dimethylphenol BRL mg/kg dry 0.42 0.18 1 8270E 7/10/20 16:01 JMV POG0105 2,4-Dinitrophenol BRL mg/kg dry 1.9 0.50 1 8270E 7/10/20 16:01 JMV POG0105 2,4-Dinitrotoluene BRL mg/kg dry 0.85 0.22 1 8270E 7/10/20 16:01 JMV POG0105 2,6-Dinitrotoluene BRL mg/kg dry 0.85 0.22 1 8270E 7/10/20 16:01 JMV POG0105 2-Chloronaphthalene BRL mg/kg dry 0.85 0.21 1 8270E 7/10/20 16:01 JMV POG0105 2-Chlorophenol BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:01 JMV POG0105 2-Methyl naphthalene BRL mg/kg dry 0.85 0.016 1 8270E 7/10/20 16:01 JMV POG0105 2-Methylphenol BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:01 JMV POG0105 2-Nitrophenol BRL mg/kg dry 0.85 0.14 1 8270E 7/10/20 16:01 JMV POG0105 3,3'-Dichlorobenzidine BRL mg/kg dry 0.85 0.17 1 8270E 7/10/20 16:01 JMV POG0105 3/4-Methyl phenol BRL mg/kg dry 0.85 0.18 1 8270E 7/10/20 16:01 JMV POG0105 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.9 0.47 1 8270E 7/10/20 16:01 JMV POG0105 4-Bromophenyl phenyl ether BRL mg/kg dry 0.85 0.20 1 8270E 7/10/20 16:01 JMV POG0105 4-Chloro-3-methylphenol BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:01 JMV POG0105 4-Chloroaniline BRL mg/kg dry 0.42 0.10 1 8270E 7/10/20 16:01 JMV POG0105 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.3 0.26 1 8270E 7/10/20 16:01 JMV POG0105 4-Nitrophenol BRL mg/kg dry 0.85 0.21 1 8270E 7/10/20 16:01 JMV POG0105 Acenaphthene BRL mg/kg dry 0.85 0.019 1 8270E 7/10/20 16:01 JMV POG0105 Acenaphthylene BRL mg/kg dry 0.85 0.017 1 8270E 7/10/20 16:01 JMV POG0105 Anthracene BRL mg/kg dry 0.85 0.0094 1 8270E 7/10/20 16:01 JMV POG0105 Azobenzene BRL mg/kg dry 0.85 0.18 1 8270E 7/10/20 16:01 JMV POG0105 Benzo(a)anthracene BRL mg/kg dry 0.85 0.010 1 8270E 7/10/20 16:01 JMV POG0105 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 0f 36 • � PA Waynt. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Project: West Sugar Creek UST Sample Matrix: Solid Laboratory Report 07/14/2020 Client Sample ID: SW-3 Sample ID: 0070067-04 Work Order: 0070067 Time Collected: 07/07/20 13:40 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(a)pyrene BRL mg/kg dry 0.85 0.0076 1 8270E 7/10/20 16:01 JMV POG0105 Benzo(b)fluoranthene BRL mg/kg dry 0.85 0.0078 1 8270E 7/10/20 16:01 JMV POG0105 Benzo(g,h,i)perylene BRL mg/kg dry 0.85 0.0083 1 8270E 7/10/20 16:01 JMV POG0105 Benzo(k)fluoranthene BRL mg/kg dry 0.85 0.0090 1 8270E 7/10/20 16:01 JMV POG0105 Benzoic Acid BRL mg/kg dry 2.6 0.70 1 8270E 7/10/20 16:01 JMV POG0105 Benzyl alcohol BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:01 JMV POG0105 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:01 JMV POG0105 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.85 0.14 1 8270E 7/10/20 16:01 JMV POG0105 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.15 1 8270E 7/10/20 16:01 JMV POG0105 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.85 0.19 1 8270E 7/10/20 16:01 JMV POG0105 Butyl benzyl phthalate BRL mg/kg dry 0.42 0.15 1 8270E 7/10/20 16:01 JMV POG0105 Chrysene BRL mg/kg dry 0.85 0.010 1 8270E 7/10/20 16:01 JMV POG0105 Dibenzo(a,h)anthracene BRL mg/kg dry 0.85 0.024 1 8270E 7/10/20 16:01 JMV POG0105 Dibenzofuran BRL mg/kg dry 0.85 0.23 1 8270E 7/10/20 16:01 JMV POG0105 Diethyl phthalate BRL mg/kg dry 0.85 0.22 1 8270E 7/10/20 16:01 JMV POG0105 Dimethyl phthalate BRL mg/kg dry 0.85 0.20 1 8270E 7/10/20 16:01 JMV POG0105 Di-n-butyl phthalate BRL mg/kg dry 0.85 0.21 1 8270E 7/10/20 16:01 JMV POG0105 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.22 1 8270E 7/10/20 16:01 JMV POG0105 Fluoranthene BRL mg/kg dry 0.85 0.0096 1 8270E 7/10/20 16:01 JMV POG0105 Fluorene BRL mg/kg dry 0.85 0.015 1 8270E 7/10/20 16:01 JMV POG0105 Hexachlorobenzene BRL mg/kg dry 0.85 0.19 1 8270E 7/10/20 16:01 JMV POG0105 Hexachlorobutadiene BRL mg/kg dry 0.85 0.19 1 8270E 7/10/20 16:01 JMV POG0105 Hexachlorocyclopentadiene BRL mg/kg dry 0.85 0.29 1 8270E 7/10/20 16:01 JMV POG0105 Hexachloroethane BRL mg/kg dry 0.85 0.13 1 8270E 7/10/20 16:01 JMV POG0105 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.85 0.024 1 8270E 7/10/20 16:01 JMV POG0105 Isophorone BRL mg/kg dry 0.85 0.18 1 8270E 7/10/20 16:01 JMV POG0105 Naphthalene BRL mg/kg dry 0.85 0.018 1 8270E 7/10/20 16:01 JMV POG0105 Nitrobenzene BRL mg/kg dry 0.42 0.18 1 8270E 7/10/20 16:01 JMV POG0105 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.85 0.19 1 8270E 7/10/20 16:01 JMV POG0105 N-Nitrosodiphenylamine BRL mg/kg dry 0.85 0.23 1 8270E 7/10/20 16:01 JMV POG0105 Pentachlorophenol BRL mg/kg dry 1.3 0.54 1 8270E 7/10/20 16:01 JMV POG0105 Phenanthrene BRL mg/kg dry 0.85 0.0092 1 8270E 7/10/20 16:01 JMV POG0105 Phenol BRL mg/kg dry 0.85 0.14 1 8270E 7/10/20 16:01 JMV POG0105 Pyrene BRL mg/kg dry 0.85 0.012 1 8270E 7/10/20 16:01 JMV POG0105 Pyridine BRL mg/kg dry 0.42 0.081 1 8270E 7/10/20 16:01 JMV POG0105 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 85 % 39-132 2-Fluorobiphenyl 73 % 44-115 2-Fluorophenol 80 % 35-115 Nitrobenzene-d5 69 % 37-122 Phenol-d5 78 % 34-121 Terphenyl-d14 75 % 54-127 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 0f 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-3 Attn: Andrew Frantz Sample ID: 0070067-04 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:40 Time Submitted: 07/07/20 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0065 0.00079 1 8260D 7/8/20 11:43 TBL POG0082 1,1,1-Trichloroethane BRL mg/kg dry 0.0065 0.00095 1 8260D 7/8/20 11:43 TBL POG0082 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0065 0.00047 1 8260D 7/8/20 11:43 TBL POG0082 1,1,2-Trichloro-1,2,2-trifluoroethane BRL mg/kg dry 0.013 0.0011 1 8260D 7/8/20 11:43 TBL POG0082 1,1,2-Trichloroethane BRL mg/kg dry 0.0065 0.00070 1 8260D 7/8/20 11:43 TBL POG0082 1,1-Dichloroethane BRL mg/kg dry 0.0065 0.0012 1 8260D 7/8/20 11:43 TBL POG0082 1,1-Dichloroethylene BRL mg/kg dry 0.0065 0.0012 1 8260D 7/8/20 11:43 TBL POG0082 1,1-Dichloropropylene BRL mg/kg dry 0.0065 0.0010 1 8260D 7/8/20 11:43 TBL POG0082 1,2,3-Trichlorobenzene BRL mg/kg dry 0.013 0.00093 1 8260D 7/8/20 11:43 TBL POG0082 1,2,3-Trichloropropane BRL mg/kg dry 0.0065 0.00074 1 8260D 7/8/20 11:43 TBL POG0082 1,2,4-Trichlorobenzene BRL mg/kg dry 0.013 0.00062 1 8260D 7/8/20 11:43 TBL POG0082 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0065 0.00069 1 8260D 7/8/20 11:43 TBL POG0082 1,2-Dibromoethane BRL mg/kg dry 0.0065 0.00058 1 8260D 7/8/20 11:43 TBL POG0082 1,2-Dichlorobenzene BRL mg/kg dry 0.0065 0.00072 1 8260D 7/8/20 11:43 TBL POG0082 1,2-Dichloroethane BRL mg/kg dry 0.0065 0.00077 1 8260D 7/8/20 11:43 TBL POG0082 1,2-Dichloropropane BRL mg/kg dry 0.0065 0.00097 1 8260D 7/8/20 11:43 TBL POG0082 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0065 0.00081 1 8260D 7/8/20 11:43 TBL POG0082 1,3-Dichlorobenzene BRL mg/kg dry 0.0065 0.00081 1 8260D 7/8/20 11:43 TBL POG0082 1,3-Dichloropropane BRL mg/kg dry 0.0065 0.00054 1 8260D 7/8/20 11:43 TBL POG0082 1,4-Dichlorobenzene BRL mg/kg dry 0.0065 0.00082 1 8260D 7/8/20 11:43 TBL POG0082 2,2-Dichloropropane BRL mg/kg dry 0.0065 0.00081 1 8260D 7/8/20 11:43 TBL POG0082 2-Chlorotoluene BRL mg/kg dry 0.0065 0.00087 1 8260D 7/8/20 11:43 TBL POG0082 4-Chlorotoluene BRL mg/kg dry 0.0065 0.00074 1 8260D 7/8/20 11:43 TBL POG0082 4-Isopropyltoluene BRL mg/kg dry 0.0065 0.0016 1 8260D 7/8/20 11:43 TBL POG0082 Acetone BRL mg/kg dry 0.026 0.0017 1 8260D 7/8/20 11:43 TBL POG0082 Benzene BRL mg/kg dry 0.0065 0.0010 1 8260D 7/8/20 11:43 TBL POG0082 Bromobenzene BRL mg/kg dry 0.0065 0.00090 1 8260D 7/8/20 11:43 TBL POG0082 Bromochloromethane BRL mg/kg dry 0.0065 0.0011 1 8260D 7/8/20 11:43 TBL POG0082 Bromodichloromethane BRL mg/kg dry 0.0065 0.00062 1 8260D 7/8/20 11:43 TBL POG0082 Bromoform BRL mg/kg dry 0.0065 0.00050 1 8260D 7/8/20 11:43 TBL POG0082 Bromomethane BRL mg/kg dry 0.013 0.0032 1 8260D 7/8/20 11:43 TBL POG0082 Carbon Tetrachloride BRL mg/kg dry 0.0065 0.0013 1 8260D 7/8/20 11:43 TBL POG0082 Chlorobenzene BRL mg/kg dry 0.0065 0.0010 1 8260D 7/8/20 11:43 TBL POG0082 Chloroethane BRL mg/kg dry 0.013 0.0012 1 8260D 7/8/20 11:43 TBL POG0082 Chloroform BRL mg/kg dry 0.0065 0.00079 1 8260D 7/8/20 11:43 TBL POG0082 Chloromethane BRL mg/kg dry 0.013 0.0020 1 8260D 7/8/20 11:43 TBL POG0082 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0065 0.0010 1 8260D 7/8/20 11:43 TBL POG0082 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0065 0.00064 1 8260D 7/8/20 11:43 TBL POG0082 Dibromochloromethane BRL mg/kg dry 0.0065 0.00043 1 8260D 7/8/20 11:43 TBL POG0082 Dichlorodifluoromethane BRL mg/kg dry 0.013 0.0018 1 8260D 7/8/20 11:43 TBL POG0082 Ethylbenzene BRL mg/kg dry 0.0065 0.00097 1 8260D 7/8/20 11:43 TBL POG0082 Isopropyl Ether BRL mg/kg dry 0.0065 0.00095 1 8260D 7/8/20 11:43 TBL POG0082 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0065 0.00075 1 8260D 7/8/20 11:43 TBL POG0082 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 0f 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-3 Attn: Andrew Frantz Sample ID: 0070067-04 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:40 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID m,p-Xylenes BRL mg/kg dry 0.013 0.0017 1 8260D 7/8/20 11:43 TBL POG0082 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.026 0.00045 1 8260D 7/8/20 11:43 TBL POG0082 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.026 0.0015 1 8260D 7/8/20 11:43 TBL POG0082 Methyl Isobutyl Ketone BRL mg/kg dry 0.026 0.00053 1 8260D 7/8/20 11:43 TBL POG0082 Methylene Chloride BRL mg/kg dry 0.0065 0.0010 1 8260D 7/8/20 11:43 TBL POG0082 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0065 0.00091 1 8260D 7/8/20 11:43 TBL POG0082 Naphthalene 0.00074 J mg/kg dry 0.013 0.00065 1 8260D 7/8/20 11:43 TBL POG0082 n-Butylbenzene BRL mg/kg dry 0.0065 0.00061 1 8260D 7/8/20 11:43 TBL POG0082 n-Propylbenzene BRL mg/kg dry 0.0065 0.00094 1 8260D 7/8/20 11:43 TBL POG0082 o-Xylene BRL mg/kg dry 0.0065 0.00069 1 8260D 7/8/20 11:43 TBL POG0082 sec-Butylbenzene BRL mg/kg dry 0.0065 0.00070 1 8260D 7/8/20 11:43 TBL POG0082 Styrene BRL mg/kg dry 0.0065 0.00063 1 8260D 7/8/20 11:43 TBL POG0082 tert-Butylbenzene BRL mg/kg dry 0.0065 0.00077 1 8260D 7/8/20 11:43 TBL POG0082 Tetrachloroethylene BRL mg/kg dry 0.0065 0.0012 1 8260D 7/8/20 11:43 TBL POG0082 Toluene BRL mg/kg dry 0.0065 0.0010 1 8260D 7/8/20 11:43 TBL POG0082 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0065 0.0012 1 8260D 7/8/20 11:43 TBL POG0082 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0065 0.00055 1 8260D 7/8/20 11:43 TBL POG0082 Trichloroethylene BRL mg/kg dry 0.0065 0.0013 1 8260D 7/8/20 11:43 TBL POG0082 Trichlorofluoromethane BRL mg/kg dry 0.013 0.0017 1 8260D 7/8/20 11:43 TBL POG0082 Vinyl acetate BRL mg/kg dry 0.013 0.00070 1 8260D 7/8/20 11:43 TBL POG0082 Vinyl chloride BRL mg/kg dry 0.013 0.0013 1 8260D 7/8/20 11:43 TBL POG0082 Xylenes, total BRL mg/kg dry 0.019 0.0023 1 8260D 7/8/20 11:43 TBL POG0082 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 70-130 Dibromofluoromethane 95 % 84-123 Toluene-d8 90 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 15 2.9 100 MADEP VPH 7/8/20 16:00 TBL POG0081 C9-Cl2 Aliphatics BRL mg/kg dry 15 1.3 100 MADEP VPH 7/8/20 16:00 TBL POG0081 C9-Cl0 Aromatics BRL mg/kg dry 15 1.4 100 MADEP VPH 7/8/20 16:00 TBL POG0081 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 122 % 70-130 2,5-Dibromotoluene (FID) 127 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-4 Attn: Andrew Frantz Sample ID: 0070067-05 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:45 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics BRL mg/kg dry 32 1.6 1 MADEP EPH 7/10/20 18:49 ZRC POG0106 C19-C36 Aliphatics BRL mg/kg dry 32 5.4 1 MADEP EPH 7/10/20 18:49 ZRC POG0106 C11-C22 Aromatics BRL CCV mg/kg dry 32 8.8 1 MADEP EPH 7/10/20 18:49 ZRC POG0106 Surrogate Recovery Control Limits 1-Chlorooctadecane 68 % 40-140 o-Terphenyl 70 % 40-140 2-Fluorobiphenyl 84 % 40-140 2-Bromonaphthalene 92 % 40-140 General Chemistry Parameters % Solids 77.0 % by 0.100 0.100 1 SM2540 G 7113/20 10:11 EDV POG0129 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.85 0.15 1 8270E 7/10/20 16:23 JMV POG0105 1,2-Dichlorobenzene BRL mg/kg dry 0.85 0.14 1 8270E 7/10/20 16:23 JMV POG0105 1,3-Dichlorobenzene BRL mg/kg dry 0.85 0.13 1 8270E 7/10/20 16:23 JMV POG0105 1,4-Dichlorobenzene BRL mg/kg dry 0.43 0.13 1 8270E 7/10/20 16:23 JMV POG0105 1-Methyl naphthalene BRL mg/kg dry 0.85 0.013 1 8270E 7/10/20 16:23 JMV POG0105 2,4,5-Trichlorophenol BRL mg/kg dry 0.85 0.18 1 8270E 7/10/20 16:23 JMV POG0105 2,4,6-Trichlorophenol BRL mg/kg dry 0.85 0.21 1 8270E 7/10/20 16:23 JMV POG0105 2,4-Dichlorophenol BRL mg/kg dry 0.85 0.17 1 8270E 7/10/20 16:23 JMV POG0105 2,4-Dimethylphenol BRL mg/kg dry 0.43 0.18 1 8270E 7/10/20 16:23 JMV POG0105 2,4-Dinitrophenol BRL mg/kg dry 1.9 0.50 1 8270E 7/10/20 16:23 JMV POG0105 2,4-Dinitrotoluene BRL mg/kg dry 0.85 0.23 1 8270E 7/10/20 16:23 JMV POG0105 2,6-Dinitrotoluene BRL mg/kg dry 0.85 0.22 1 8270E 7/10/20 16:23 JMV POG0105 2-Chloronaphthalene BRL mg/kg dry 0.85 0.21 1 8270E 7/10/20 16:23 JMV POG0105 2-Chlorophenol BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:23 JMV POG0105 2-Methyl naphthalene BRL mg/kg dry 0.85 0.017 1 8270E 7/10/20 16:23 JMV POG0105 2-Methylphenol BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:23 JMV POG0105 2-Nitrophenol BRL mg/kg dry 0.85 0.14 1 8270E 7/10/20 16:23 JMV POG0105 3,3'-Dichlorobenzidine BRL mg/kg dry 0.85 0.17 1 8270E 7/10/20 16:23 JMV POG0105 3/4-Methyl phenol BRL mg/kg dry 0.85 0.19 1 8270E 7/10/20 16:23 JMV POG0105 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.9 0.47 1 8270E 7/10/20 16:23 JMV POG0105 4-Bromophenyl phenyl ether BRL mg/kg dry 0.85 0.20 1 8270E 7/10/20 16:23 JMV POG0105 4-Chloro-3-methylphenol BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:23 JMV POG0105 4-Chloroaniline BRL mg/kg dry 0.43 0.10 1 8270E 7/10/20 16:23 JMV POG0105 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.3 0.26 1 8270E 7/10/20 16:23 JMV POG0105 4-Nitrophenol BRL mg/kg dry 0.85 0.21 1 8270E 7/10/20 16:23 JMV POG0105 Acenaphthene BRL mg/kg dry 0.85 0.020 1 8270E 7/10/20 16:23 JMV POG0105 Acenaphthylene BRL mg/kg dry 0.85 0.017 1 8270E 7/10/20 16:23 JMV POG0105 Anthracene BRL mg/kg dry 0.85 0.0094 1 8270E 7/10/20 16:23 JMV POG0105 Azobenzene BRL mg/kg dry 0.85 0.18 1 8270E 7/10/20 16:23 JMV POG0105 Benzo(a)anthracene BRL mg/kg dry 0.85 0.010 1 8270E 7/10/20 16:23 JMV POG0105 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 0f 36 • � PA Waynt. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Project: West Sugar Creek UST Sample Matrix: Solid Laboratory Report 07/14/2020 Client Sample ID: SW-4 Sample ID: 0070067-05 Work Order: 0070067 Time Collected: 07/07/20 13:45 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(a)pyrene BRL mg/kg dry 0.85 0.0076 1 8270E 7/10/20 16:23 JMV POG0105 Benzo(b)fluoranthene BRL mg/kg dry 0.85 0.0079 1 8270E 7/10/20 16:23 JMV POG0105 Benzo(g,h,i)perylene BRL mg/kg dry 0.85 0.0084 1 8270E 7/10/20 16:23 JMV POG0105 Benzo(k)fluoranthene BRL mg/kg dry 0.85 0.0091 1 8270E 7/10/20 16:23 JMV POG0105 Benzoic Acid BRL mg/kg dry 2.6 0.71 1 8270E 7/10/20 16:23 JMV POG0105 Benzyl alcohol BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:23 JMV POG0105 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.85 0.16 1 8270E 7/10/20 16:23 JMV POG0105 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.85 0.14 1 8270E 7/10/20 16:23 JMV POG0105 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.43 0.15 1 8270E 7/10/20 16:23 JMV POG0105 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.85 0.19 1 8270E 7/10/20 16:23 JMV POG0105 Butyl benzyl phthalate BRL mg/kg dry 0.43 0.15 1 8270E 7/10/20 16:23 JMV POG0105 Chrysene BRL mg/kg dry 0.85 0.010 1 8270E 7/10/20 16:23 JMV POG0105 Dibenzo(a,h)anthracene BRL mg/kg dry 0.85 0.025 1 8270E 7/10/20 16:23 JMV POG0105 Dibenzofuran BRL mg/kg dry 0.85 0.23 1 8270E 7/10/20 16:23 JMV POG0105 Diethyl phthalate BRL mg/kg dry 0.85 0.22 1 8270E 7/10/20 16:23 JMV POG0105 Dimethyl phthalate BRL mg/kg dry 0.85 0.20 1 8270E 7/10/20 16:23 JMV POG0105 Di-n-butyl phthalate BRL mg/kg dry 0.85 0.21 1 8270E 7/10/20 16:23 JMV POG0105 Di-n-octyl phthalate BRL mg/kg dry 0.43 0.22 1 8270E 7/10/20 16:23 JMV POG0105 Fluoranthene BRL mg/kg dry 0.85 0.0097 1 8270E 7/10/20 16:23 JMV POG0105 Fluorene BRL mg/kg dry 0.85 0.015 1 8270E 7/10/20 16:23 JMV POG0105 Hexachlorobenzene BRL mg/kg dry 0.85 0.19 1 8270E 7/10/20 16:23 JMV POG0105 Hexachlorobutadiene BRL mg/kg dry 0.85 0.19 1 8270E 7/10/20 16:23 JMV POG0105 Hexachlorocyclopentadiene BRL mg/kg dry 0.85 0.29 1 8270E 7/10/20 16:23 JMV POG0105 Hexachloroethane BRL mg/kg dry 0.85 0.13 1 8270E 7/10/20 16:23 JMV POG0105 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.85 0.024 1 8270E 7/10/20 16:23 JMV POG0105 Isophorone BRL mg/kg dry 0.85 0.18 1 8270E 7/10/20 16:23 JMV POG0105 Naphthalene BRL mg/kg dry 0.85 0.018 1 8270E 7/10/20 16:23 JMV POG0105 Nitrobenzene BRL mg/kg dry 0.43 0.18 1 8270E 7/10/20 16:23 JMV POG0105 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.85 0.20 1 8270E 7/10/20 16:23 JMV POG0105 N-Nitrosodiphenylamine BRL mg/kg dry 0.85 0.23 1 8270E 7/10/20 16:23 JMV POG0105 Pentachlorophenol BRL mg/kg dry 1.3 0.54 1 8270E 7/10/20 16:23 JMV POG0105 Phenanthrene BRL mg/kg dry 0.85 0.0093 1 8270E 7/10/20 16:23 JMV POG0105 Phenol BRL mg/kg dry 0.85 0.14 1 8270E 7/10/20 16:23 JMV POG0105 Pyrene BRL mg/kg dry 0.85 0.012 1 8270E 7/10/20 16:23 JMV POG0105 Pyridine BRL mg/kg dry 0.43 0.082 1 8270E 7/10/20 16:23 JMV POG0105 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 87 % 39-132 2-Fluorobiphenyl 75 % 44-115 2-Fluorophenol 80 % 35-115 Nitrobenzene-d5 72 % 37-122 Phenol-d5 80 % 34-121 Terphenyl-d14 74 % 54-127 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 0f 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-4 Attn: Andrew Frantz Sample ID: 0070067-05 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:45 Time Submitted: 07/07/20 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0052 0.00063 1 8260D 7/8/20 12:13 TBL POG0082 1,1,1-Trichloroethane BRL mg/kg dry 0.0052 0.00076 1 8260D 7/8/20 12:13 TBL POG0082 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0052 0.00038 1 8260D 7/8/20 12:13 TBL POG0082 1,1,2-Trichloro-1,2,2-trifluoroethane BRL mg/kg dry 0.010 0.00090 1 8260D 7/8/20 12:13 TBL POG0082 1,1,2-Trichloroethane BRL mg/kg dry 0.0052 0.00056 1 8260D 7/8/20 12:13 TBL POG0082 1,1-Dichloroethane BRL mg/kg dry 0.0052 0.00093 1 8260D 7/8/20 12:13 TBL POG0082 1,1-Dichloroethylene BRL mg/kg dry 0.0052 0.00095 1 8260D 7/8/20 12:13 TBL POG0082 1,1-Dichloropropylene BRL mg/kg dry 0.0052 0.00080 1 8260D 7/8/20 12:13 TBL POG0082 1,2,3-Trichlorobenzene BRL mg/kg dry 0.010 0.00074 1 8260D 7/8/20 12:13 TBL POG0082 1,2,3-Trichloropropane BRL mg/kg dry 0.0052 0.00059 1 8260D 7/8/20 12:13 TBL POG0082 1,2,4-Trichlorobenzene BRL mg/kg dry 0.010 0.00049 1 8260D 7/8/20 12:13 TBL POG0082 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0052 0.00055 1 8260D 7/8/20 12:13 TBL POG0082 1,2-Dibromoethane BRL mg/kg dry 0.0052 0.00046 1 8260D 7/8/20 12:13 TBL POG0082 1,2-Dichlorobenzene BRL mg/kg dry 0.0052 0.00058 1 8260D 7/8/20 12:13 TBL POG0082 1,2-Dichloroethane BRL mg/kg dry 0.0052 0.00062 1 8260D 7/8/20 12:13 TBL POG0082 1,2-Dichloropropane BRL mg/kg dry 0.0052 0.00078 1 8260D 7/8/20 12:13 TBL POG0082 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0052 0.00065 1 8260D 7/8/20 12:13 TBL POG0082 1,3-Dichlorobenzene BRL mg/kg dry 0.0052 0.00064 1 8260D 7/8/20 12:13 TBL POG0082 1,3-Dichloropropane BRL mg/kg dry 0.0052 0.00043 1 8260D 7/8/20 12:13 TBL POG0082 1,4-Dichlorobenzene BRL mg/kg dry 0.0052 0.00066 1 8260D 7/8/20 12:13 TBL POG0082 2,2-Dichloropropane BRL mg/kg dry 0.0052 0.00065 1 8260D 7/8/20 12:13 TBL POG0082 2-Chlorotoluene BRL mg/kg dry 0.0052 0.00069 1 8260D 7/8/20 12:13 TBL POG0082 4-Chlorotoluene BRL mg/kg dry 0.0052 0.00059 1 8260D 7/8/20 12:13 TBL POG0082 4-Isopropyltoluene BRL mg/kg dry 0.0052 0.0013 1 8260D 7/8/20 12:13 TBL POG0082 Acetone BRL mg/kg dry 0.021 0.0013 1 8260D 7/8/20 12:13 TBL POG0082 Benzene BRL mg/kg dry 0.0052 0.00081 1 8260D 7/8/20 12:13 TBL POG0082 Bromobenzene BRL mg/kg dry 0.0052 0.00072 1 8260D 7/8/20 12:13 TBL POG0082 Bromochloromethane BRL mg/kg dry 0.0052 0.00085 1 8260D 7/8/20 12:13 TBL POG0082 Bromodichloromethane BRL mg/kg dry 0.0052 0.00049 1 8260D 7/8/20 12:13 TBL POG0082 Bromoform BRL mg/kg dry 0.0052 0.00040 1 8260D 7/8/20 12:13 TBL POG0082 Bromomethane BRL mg/kg dry 0.010 0.0025 1 8260D 7/8/20 12:13 TBL POG0082 Carbon Tetrachloride BRL mg/kg dry 0.0052 0.0010 1 8260D 7/8/20 12:13 TBL POG0082 Chlorobenzene BRL mg/kg dry 0.0052 0.00081 1 8260D 7/8/20 12:13 TBL POG0082 Chloroethane BRL mg/kg dry 0.010 0.00099 1 8260D 7/8/20 12:13 TBL POG0082 Chloroform BRL mg/kg dry 0.0052 0.00063 1 8260D 7/8/20 12:13 TBL POG0082 Chloromethane BRL mg/kg dry 0.010 0.0016 1 8260D 7/8/20 12:13 TBL POG0082 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0052 0.00081 1 8260D 7/8/20 12:13 TBL POG0082 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0052 0.00051 1 8260D 7/8/20 12:13 TBL POG0082 Dibromochloromethane BRL mg/kg dry 0.0052 0.00035 1 8260D 7/8/20 12:13 TBL POG0082 Dichlorodifluoromethane BRL mg/kg dry 0.010 0.0015 1 8260D 7/8/20 12:13 TBL POG0082 Ethylbenzene BRL mg/kg dry 0.0052 0.00078 1 8260D 7/8/20 12:13 TBL POG0082 Isopropyl Ether BRL mg/kg dry 0.0052 0.00076 1 8260D 7/8/20 12:13 TBL POG0082 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0052 0.00060 1 8260D 7/8/20 12:13 TBL POG0082 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 0f 36 Laboratory Report IR A i • . 0 07/14/2020 - -ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Client Sample ID: SW-4 Attn: Andrew Frantz Sample ID: 0070067-05 2801 Yorkmont Rd. #100 Work Order: 0070067 Charlotte, NC 28208 Sample Matrix: Solid Time Collected: 07/07/20 13:45 Time Submitted: 07/07/20 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID m,p-Xylenes BRL mg/kg dry 0.010 0.0013 1 8260D 7/8/20 12:13 TBL POG0082 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.021 0.00036 1 8260D 7/8/20 12:13 TBL POG0082 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.021 0.0012 1 8260D 7/8/20 12:13 TBL POG0082 Methyl Isobutyl Ketone BRL mg/kg dry 0.021 0.00042 1 8260D 7/8/20 12:13 TBL POG0082 Methylene Chloride BRL mg/kg dry 0.0052 0.00084 1 8260D 7/8/20 12:13 TBL POG0082 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0052 0.00073 1 8260D 7/8/20 12:13 TBL POG0082 Naphthalene BRL mg/kg dry 0.010 0.00052 1 8260D 7/8/20 12:13 TBL POG0082 n-Butylbenzene BRL mg/kg dry 0.0052 0.00048 1 8260D 7/8/20 12:13 TBL POG0082 n-Propylbenzene BRL mg/kg dry 0.0052 0.00075 1 8260D 7/8/20 12:13 TBL POG0082 o-Xylene BRL mg/kg dry 0.0052 0.00055 1 8260D 7/8/20 12:13 TBL POG0082 sec-Butylbenzene BRL mg/kg dry 0.0052 0.00056 1 8260D 7/8/20 12:13 TBL POG0082 Styrene BRL mg/kg dry 0.0052 0.00050 1 8260D 7/8/20 12:13 TBL POG0082 tert-Butylbenzene BRL mg/kg dry 0.0052 0.00062 1 8260D 7/8/20 12:13 TBL POG0082 Tetrachloroethylene BRL mg/kg dry 0.0052 0.00094 1 8260D 7/8/20 12:13 TBL POG0082 Toluene BRL mg/kg dry 0.0052 0.00082 1 8260D 7/8/20 12:13 TBL POG0082 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0052 0.00099 1 8260D 7/8/20 12:13 TBL POG0082 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0052 0.00044 1 8260D 7/8/20 12:13 TBL POG0082 Trichloroethylene BRL mg/kg dry 0.0052 0.0010 1 8260D 7/8/20 12:13 TBL POG0082 Trichlorofluoromethane BRL mg/kg dry 0.010 0.0014 1 8260D 7/8/20 12:13 TBL POG0082 Vinyl acetate BRL mg/kg dry 0.010 0.00056 1 8260D 7/8/20 12:13 TBL POG0082 Vinyl chloride BRL mg/kg dry 0.010 0.0010 1 8260D 7/8/20 12:13 TBL POG0082 Xylenes, total BRL mg/kg dry 0.016 0.0019 1 8260D 7/8/20 12:13 TBL POG0082 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 96 % 84-123 Toluene-d8 89 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 18 3.6 100 MADEP VPH 7/8/20 16:30 TBL POG0081 C9-C12 Aliphatics BRL mg/kg dry 18 1.6 100 MADEP VPH 7/8/20 16:30 TBL POG0081 C9-Cl0 Aromatics BRL mg/kg dry 18 1.7 100 MADEP VPH 7/8/20 16:30 TBL POG0081 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 117 % 70-130 2,5-Dibromotoluene (FID) 124 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 0f 36 Waypo�nt ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch POG0082 - 5035 Reporting Result Limit Units Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (POG0082-BLK1) Prepared & Analyzed: 07/08/20 Benzene BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet Surrogate:4-Bromofluorobenzene 50.0 ug/L 50.00 100 70-130 Surrogate: Dibromofluoromethane 47.6 ug/L 50.00 95 84-123 Surrogate: Toluene-d8 45.4 ug/L 50.00 91 76-129 LCS (POG0082-BS1) Prepared &Analyzed: 07/08/20 Benzene 0.0555 0.0050 mg/kg wet 0.05000 ill 74-127 Ethylbenzene 0.0498 0.0050 mg/kg wet 0.05000 100 74-128 m,p-Xylenes 0.103 0.010 mg/kg wet 0.1000 103 75-124 o-Xylene 0.0510 0.0050 mg/kg wet 0.05000 102 74-126 Toluene 0.0551 0.0050 mg/kg wet 0.05000 110 71-129 Surrogate:4-Bromofluorobenzene 49.0 ug/L 50.00 98 70-130 Surrogate: Dibromofluoromethane 47.8 ug/L 50.00 96 84-123 Surrogate: Toluene-d8 44.6 ug/L 50.00 89 76-129 Matrix Spike (POG0082-MS1) Source: 0070067-02 Prepared & Analyzed: 07/08/20 Benzene 0.0643 0.0064 mg/kg dry 0.06405 BRL 100 60-135 Ethylbenzene 0.0606 0.0064 mg/kg dry 0.06405 BRL 95 44-144 m,p-Xylenes 0.124 0.013 mg/kg dry 0.1281 BRL 97 36-148 o-Xylene 0.0585 0.0064 mg/kg dry 0.06405 BRL 91 43-143 Toluene 0.0665 0.0064 mg/kg dry 0.06405 BRL 104 57-135 Surrogate:4-Bromofluorobenzene 48.8 ug/L 50.00 98 70-130 Surrogate: Dibromofluoromethane 47.1 ug/L 50.00 94 84-123 Surrogate: Toluene-d8 44.5 ug/L 50.00 89 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:40:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POG0082 - 5035 Matrix Spike Dup (POG0082-MSD1) Source: 0070067-02 Prepared & Analyzed: 07/08/20 Benzene 0.0684 0.0064 mg/kg dry 0.06405 BRL 107 60-135 6 20 Ethylbenzene 0.0647 0.0064 mg/kg dry 0.06405 BRL 101 44-144 6 19 m,p-Xylenes 0.132 0.013 mg/kg dry 0.1281 BRL 103 36-148 6 20 o-Xylene 0.0621 0.0064 mg/kg dry 0.06405 BRL 97 43-143 6 17 Toluene 0.0696 0.0064 mg/kg dry 0.06405 BRL 109 57-135 5 22 Surrogate:4-Bromofluorobenzene 48.4 ug/L 50.00 97 70-130 Surrogate: Dibromofluoromethane 47.0 ug/L 50.00 94 84-123 Surrogate: Toluene-d8 44.4 ug/L 50.00 89 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Semivolatile Organic Compounds by GC/MS - Quality Control Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:4O:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POG0105 - 3546 Blank (POG0105-BLK1) 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1-Methyl naphthalene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methyl naphthalene 2-Methylphenol 2-Nitrophenol 3,3'-Dichlorobenzidine 3/4-Methyl phenol 4,6-Dinitro-2-methylphenol 4-Bromophenyl phenyl ether 4-C h loro-3-methyl phenol 4-Chloroaniline 4-Chlorophenyl phenyl ether 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Azobenzene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy)methane B is(2-Ch loroethyl )ether Bis(2-chloroisopropyl)ether Bis(2-Ethylhexyl)phthalate Butyl benzyl phthalate Chrysene Dibenzo(a,h)anthracene Dibenzofuran Diethyl phthalate Dimethyl phthalate BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 1.5 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 1.5 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 1.0 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 2.0 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet Prepared: 07/09/20 Analyzed: 07/10/20 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 36 ® Level II QC Report Waynt. � 7/14/20 poi ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Work Order: 0070067 Attn: Andrew Frantz Time Submitted: 7/7/2020 3:4O:OOPM 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POG0105 - 3546 Blank (POG0105-BLK1) Prepared: 07/09/20 Analyzed: 07/10/20 Di-n-butyl phthalate BRL 0.66 mg/kg wet Di-n-octyl phthalate BRL 0.33 mg/kg wet Fluoranthene BRL 0.66 mg/kg wet Fluorene BRL 0.66 mg/kg wet Hexachlorobenzene BRL 0.66 mg/kg wet Hexachlorobutadiene BRL 0.66 mg/kg wet Hexachlorocyclopentadiene BRL 0.66 mg/kg wet Hexachloroethane BRL 0.66 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.66 mg/kg wet Isophorone BRL 0.66 mg/kg wet Naphthalene BRL 0.66 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylamine BRL 0.66 mg/kg wet N-Nitrosodiphenylamine BRL 0.66 mg/kg wet Pentachlorophenol BRL 1.0 mg/kg wet Phenanthrene BRL 0.66 mg/kg wet Phenol BRL 0.66 mg/kg wet Pyrene BRL 0.66 mg/kg wet Pyridine BRL 0.33 mg/kg wet Surrogate: 2,4,6-Tribromophenol 2.70 mg/kg wet 3.333 81 39-132 Surrogate: 2-Fluorobiphenyl 1.26 mg/kg wet 1.667 76 44-115 Surrogate: 2-Fluorophenol 2.73 mg/kg wet 3.333 82 35-115 Surrogate: Nitrobenzene-d5 1.17 mg/kg wet 1.667 70 37-122 Surrogate: Phenol-d5 2.72 mg/kg wet 3.333 82 34-121 Surrogate: Terphenyl-04 1.26 mg/kg wet 1.667 76 54-127 LCS (POG0105-BS1) Prepared: 07/09/20 Analyzed: 07/10/20 1,2,4-Trichlorobenzene 0.913 0.66 mg/kg wet 1.667 55 34-118 1,2-Dichlorobenzene 0.820 0.66 mg/kg wet 1.667 49 33-117 1,3-Dichlorobenzene 0.758 0.66 mg/kg wet 1.667 45 30-115 1,4-Dichlorobenzene 0.766 0.33 mg/kg wet 1.667 46 31-115 1-Methyl naphthalene 1.08 0.66 mg/kg wet 1.667 65 40-119 2,4,5-Trichlorophenol 1.23 0.66 mg/kg wet 1.667 74 62-124 2,4,6-Trichlorophenol 1.17 0.66 mg/kg wet 1.667 70 39-126 2,4-Dichlorophenol 1.10 0.66 mg/kg wet 1.667 66 40-122 2,4-Dimethylphenol 1.33 0.33 mg/kg wet 1.667 80 30-127 2,4-Dinitrophenol 1.06 1.5 mg/kg wet 1.667 64 27-129 J 2,4-Dinitrotoluene 1.29 0.66 mg/kg wet 1.667 78 48-126 2,6-Dinitrotoluene 1.24 0.66 mg/kg wet 1.667 75 46-124 2-Chloronaphthalene 1.07 0.66 mg/kg wet 1.667 64 41-114 2-Chlorophenol 1.05 0.66 mg/kg wet 1.667 63 34-121 2-Methyl naphthalene 1.04 0.66 mg/kg wet 1.667 63 38-122 2-Methylphenol 1.13 0.66 mg/kg wet 1.667 68 32-122 2-Nitrophenol 1.01 0.66 mg/kg wet 1.667 60 36-123 3,3'-Dichlorobenzidine 1.28 0.66 mg/kg wet 1.667 77 22-121 3/4-Methyl phenol 1.01 0.66 mg/kg wet 1.667 61 34-119 4,6-Dinitro-2-methylphenol 1.18 1.5 mg/kg wet 1.667 71 29-132 J This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 0f 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch POG0105 - 3546 Reporting Result Limit Units Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:4O:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (POG0105-BSI) Prepared: 07/09/20 Analyzed: 07/10/20 4-Bromophenyl phenyl ether 1.16 0.66 mg/kg wet 1.667 70 46-124 4-Chloro-3-methyl phenol 1.23 0.66 mg/kg wet 1.667 74 45-122 4-Chloroaniline 0.976 0.33 mg/kg wet 1.667 59 17-106 4-Chlorophenyl phenyl ether 1.12 1.0 mg/kg wet 1.667 67 45-121 4-Nitrophenol 1.10 0.66 mg/kg wet 1.667 66 30-132 Acenaphthene 1.12 0.66 mg/kg wet 1.667 67 40-123 Acenaphthylene 1.17 0.66 mg/kg wet 1.667 70 32-132 Anthracene 1.27 0.66 mg/kg wet 1.667 76 47-123 Azobenzene 1.23 0.66 mg/kg wet 1.667 74 39-125 Benzo(a)anthracene 1.22 0.66 mg/kg wet 1.667 73 49-126 Benzo(a)pyrene 1.37 0.66 mg/kg wet 1.667 82 45-129 Benzo(b)fluoranthene 1.24 0.66 mg/kg wet 1.667 75 45-132 Benzo(g,h,i)perylene 1.30 0.66 mg/kg wet 1.667 78 43-134 Benzo(k)fluoranthene 1.31 0.66 mg/kg wet 1.667 79 47-132 Benzoic Acid 0.709 2.0 mg/kg wet 1.667 43 10-83 Benzyl alcohol 1.06 0.66 mg/kg wet 1.667 64 29-122 bis(2-Chloroethoxy)methane 0.998 0.66 mg/kg wet 1.667 60 36-121 Bis(2-Chloroethyl)ether 0.860 0.66 mg/kg wet 1.667 52 31-120 Bis(2-chloroisopropyl)ether 0.827 0.33 mg/kg wet 1.667 50 33-131 Bis(2-Ethylhexyl)phthalate 1.35 0.66 mg/kg wet 1.667 81 51-133 Butyl benzyl phthalate 1.28 0.33 mg/kg wet 1.667 77 48-132 Chrysene 1.21 0.66 mg/kg wet 1.667 73 50-124 Dibenzo(a,h)anthracene 0.738 0.66 mg/kg wet 1.667 44 45-134 Dibenzofuran 1.11 0.66 mg/kg wet 1.667 67 44-120 Diethyl phthalate 1.17 0.66 mg/kg wet 1.667 70 50-124 Dimethyl phthalate 1.21 0.66 mg/kg wet 1.667 72 48-124 Di-n-butyl phthalate 1.33 0.66 mg/kg wet 1.667 80 51-128 Di-n-octyl phthalate 1.39 0.33 mg/kg wet 1.667 83 45-140 Fluoranthene 1.26 0.66 mg/kg wet 1.667 76 50-127 Fluorene 1.20 0.66 mg/kg wet 1.667 72 43-125 Hexachlorobenzene 1.15 0.66 mg/kg wet 1.667 69 45-122 Hexachlorobutadiene 0.922 0.66 mg/kg wet 1.667 55 32-123 Hexachlorocyclopentadiene 0.873 0.66 mg/kg wet 1.667 52 32-117 Hexachloroethane 0.748 0.66 mg/kg wet 1.667 45 28-117 Indeno(1,2,3-cd)pyrene 1.39 0.66 mg/kg wet 1.667 84 45-133 Isophorone 0.860 0.66 mg/kg wet 1.667 52 30-122 Naphthalene 0.983 0.66 mg/kg wet 1.667 59 35-123 Nitrobenzene 0.883 0.33 mg/kg wet 1.667 53 34-122 N-Nitroso-di-n-propylamine 1.01 0.66 mg/kg wet 1.667 60 36-120 N-Nitrosodiphenylamine 1.45 0.66 mg/kg wet 1.667 87 38-127 Pentachlorophenol 1.30 1.0 mg/kg wet 1.667 78 25-133 Phenanthrene 1.24 0.66 mg/kg wet 1.667 74 50-121 Phenol 1.13 0.66 mg/kg wet 1.667 68 34-121 Pyrene 1.31 0.66 mg/kg wet 1.667 79 47-127 Pyridine 0.495 0.33 mg/kg wet 1.667 30 10-60 Surrogate: 2,4,6-Tribromophenol 2.52 mg/kg wet 3.333 76 39-132 J L This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 0f 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch POG0105 - 3546 Reporting Result Limit Units Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:4O:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (POG0105-BSI) Prepared: 07/09/20 Analyzed: 07/10/20 Surrogate: 2-Fluorobiphenyl 1.02 mg/kg wet 1.667 61 44-115 Surrogate: 2-Fluorophenol 2.12 mg/kg wet 3.333 64 35-115 Surrogate: Nitrobenzene-d5 0.903 mg/kg wet 1.667 54 37-122 Surrogate: Phenol-d5 2.14 mg/kg wet 3.333 64 34-121 Surrogate: Terphenyl-d14 1.16 mg/kg wet 1.667 70 54-127 Matrix Spike (POG0105-MS1) Source: 0070067-01 Prepared: 07/09/20 Analyzed: 07/10/20 1,2,4-Trichlorobenzene 1.34 0.84 mg/kg dry 2.121 BRL 63 34-118 1,2-Dichlorobenzene 1.28 0.84 mg/kg dry 2.121 BRL 60 33-117 1,3-Dichlorobenzene 1.21 0.84 mg/kg dry 2.121 BRL 57 30-115 1,4-Dichlorobenzene 1.23 0.42 mg/kg dry 2.121 BRL 58 31-115 1-Methyl naphthalene 1.51 0.84 mg/kg dry 2.121 BRL 71 40-119 2,4,5-Trichlorophenol 1.75 0.84 mg/kg dry 2.121 BRL 83 45-121 2,4,6-Trichlorophenol 1.74 0.84 mg/kg dry 2.121 BRL 82 39-126 2,4-Dichlorophenol 1.61 0.84 mg/kg dry 2.121 BRL 76 40-122 2,4-Dimethylphenol 1.90 0.42 mg/kg dry 2.121 BRL 90 30-127 2,4-Dinitrophenol 1.99 1.9 mg/kg dry 2.121 BRL 94 27-129 2,4-Dinitrotoluene 1.71 0.84 mg/kg dry 2.121 BRL 81 48-126 2,6-Dinitrotoluene 1.71 0.84 mg/kg dry 2.121 BRL 80 46-124 2-Chloronaphthalene 1.48 0.84 mg/kg dry 2.121 BRL 70 41-114 2-Chlorophenol 1.61 0.84 mg/kg dry 2.121 BRL 76 34-121 2-Methyl naphthalene 1.47 0.84 mg/kg dry 2.121 BRL 69 38-122 2-Methylphenol 1.70 0.84 mg/kg dry 2.121 BRL 80 32-122 2-Nitrophenol 1.56 0.84 mg/kg dry 2.121 BRL 74 36-123 3,3'-Dichlorobenzidine 1.47 0.84 mg/kg dry 2.121 BRL 69 22-121 3/4-Methyl phenol 1.53 0.84 mg/kg dry 2.121 BRL 72 34-119 4,6-Dinitro-2-methylphenol 1.70 1.9 mg/kg dry 2.121 BRL 80 29-132 4-Bromophenyl phenyl ether 1.56 0.84 mg/kg dry 2.121 BRL 74 46-124 4-Chloro-3-methylphenol 1.74 0.84 mg/kg dry 2.121 BRL 82 45-122 4-Chloroaniline 1.38 0.42 mg/kg dry 2.121 BRL 65 17-106 4-Chlorophenyl phenyl ether 1.51 1.3 mg/kg dry 2.121 BRL 71 45-121 4-Nitrophenol 1.65 0.84 mg/kg dry 2.121 BRL 78 30-132 Acenaphthene 1.53 0.84 mg/kg dry 2.121 BRL 72 40-123 Acenaphthylene 1.61 0.84 mg/kg dry 2.121 BRL 76 32-132 Anthracene 1.64 0.84 mg/kg dry 2.121 BRL 77 47-123 Azobenzene 1.68 0.84 mg/kg dry 2.121 BRL 79 39-125 Benzo(a)anthracene 1.51 0.84 mg/kg dry 2.121 BRL 71 49-126 Benzo(a)pyrene 1.71 0.84 mg/kg dry 2.121 BRL 81 45-129 Benzo(b)fluoranthene 1.58 0.84 mg/kg dry 2.121 BRL 75 45-132 Benzo(g,h,i)perylene 1.68 0.84 mg/kg dry 2.121 BRL 79 43-134 Benzo(k)fluoranthene 1.67 0.84 mg/kg dry 2.121 BRL 79 47-132 Benzoic Acid 1.67 2.5 mg/kg dry 2.121 BRL 79 10-83 Benzyl alcohol 1.69 0.84 mg/kg dry 2.121 BRL 80 29-122 bis(2-Chloroethoxy)methane 1.49 0.84 mg/kg dry 2.121 BRL 70 36-121 Bis(2-Chloroethyl)ether 1.34 0.84 mg/kg dry 2.121 BRL 63 31-120 Bis(2-chloroisopropyl)ether 1.27 0.42 mg/kg dry 2.121 BRL 60 33-131 Bis(2-Ethylhexyl)phthalate 1.66 0.84 mg/kg dry 2.121 BRL 78 51-133 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 0f 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch POG0105 - 3546 Reporting Result Limit Units Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike (POG0105-MS1) Source: 0070067-01 Prepared: 07/09/20 Analyzed: 07/10/20 Butyl benzyl phthalate 1.63 0.42 mg/kg dry 2.121 BRL 77 48-132 Chrysene 1.52 0.84 mg/kg dry 2.121 BRL 72 50-124 Dibenzo(a,h)anthracene 1.06 0.84 mg/kg dry 2.121 BRL 50 45-134 Dibenzofuran 1.53 0.84 mg/kg dry 2.121 BRL 72 44-120 Diethyl phthalate 1.56 0.84 mg/kg dry 2.121 BRL 73 50-124 Dimethyl phthalate 1.64 0.84 mg/kg dry 2.121 BRL 77 48-124 Di-n-butyl phthalate 1.74 0.84 mg/kg dry 2.121 BRL 82 51-128 Di-n-octyl phthalate 1.77 0.42 mg/kg dry 2.121 BRL 84 45-140 Fluoranthene 1.63 0.84 mg/kg dry 2.121 BRL 77 50-127 Fluorene 1.63 0.84 mg/kg dry 2.121 BRL 77 43-125 Hexachlorobenzene 1.56 0.84 mg/kg dry 2.121 BRL 73 45-122 Hexachlorobutadiene 1.40 0.84 mg/kg dry 2.121 BRL 66 32-123 Hexachlorocyclopentadiene 1.31 0.84 mg/kg dry 2.121 BRL 62 32-117 Hexachloroethane 1.19 0.84 mg/kg dry 2.121 BRL 56 28-117 Indeno(1,2,3-cd)pyrene 1.85 0.84 mg/kg dry 2.121 BRL 87 45-133 Isophorone 1.26 0.84 mg/kg dry 2.121 BRL 59 30-122 Naphthalene 1.44 0.84 mg/kg dry 2.121 BRL 68 35-123 Nitrobenzene 1.35 0.42 mg/kg dry 2.121 BRL 64 34-122 N-Nitroso-di-n-propylamine 1.49 0.84 mg/kg dry 2.121 BRL 70 36-120 N-Nitrosodiphenylamine 1.95 0.84 mg/kg dry 2.121 BRL 92 38-127 Pentachlorophenol 1.92 1.3 mg/kg dry 2.121 BRL 90 25-133 Phenanthrene 1.63 0.84 mg/kg dry 2.121 BRL 77 50-121 Phenol 1.70 0.84 mg/kg dry 2.121 BRL 80 34-121 Pyrene 1.65 0.84 mg/kg dry 2.121 BRL 78 47-127 Pyridine 0.330 0.42 mg/kg dry 2.121 BRL 16 20-150 Surrogate: 2,4,6-Tribromophenol 3.50 mg/kg dry 4.242 83 39-132 Surrogate: 2-Fluorobiphenyl 1.39 mg/kg dry 2.121 66 44-115 Surrogate: 2-Fluorophenol 3.29 mg/kg dry 4.242 78 35-115 Surrogate: Nitrobenzene-d5 1.37 mg/kg dry 2.121 65 37-122 Surrogate: Phenol-d5 3.25 mg/kg dry 4.242 77 34-121 Surrogate: Terphenyl-04 1.42 mg/kg dry 2.121 67 54-127 M,J This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 0f 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch POG0105 - 3546 Reporting Result Limit Units Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:4O:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike Dup (POG0105-MSD1) Source: 0070067-01 Prepared: 07/09/20 Analyzed: 07/10/20 1,2,4-Trichlorobenzene 1.11 0.84 mg/kg dry 2.119 BRL 52 34-118 18 20 1,2-Dichlorobenzene 1.05 0.84 mg/kg dry 2.119 BRL 49 33-117 20 20 1,3-Dichlorobenzene 0.994 0.84 mg/kg dry 2.119 BRL 47 30-115 20 20 1,4-Dichlorobenzene 1.01 0.42 mg/kg dry 2.119 BRL 47 31-115 20 20 1-Methyl naphthalene 1.31 0.84 mg/kg dry 2.119 BRL 62 40-119 14 20 2,4,5-Trichlorophenol 1.58 0.84 mg/kg dry 2.119 BRL 75 45-121 10 35 2,4,6-Trichlorophenol 1.49 0.84 mg/kg dry 2.119 BRL 70 39-126 15 20 2,4-Dichlorophenol 1.35 0.84 mg/kg dry 2.119 BRL 64 40-122 17 20 2,4-Dimethylphenol 1.59 0.42 mg/kg dry 2.119 BRL 75 30-127 18 20 2,4-Dinitrophenol 1.72 1.9 mg/kg dry 2.119 BRL 81 27-129 15 20 2,4-Dinitrotoluene 1.64 0.84 mg/kg dry 2.119 BRL 77 48-126 4 20 2,6-Dinitrotoluene 1.58 0.84 mg/kg dry 2.119 BRL 75 46-124 8 20 2-Chloronaphthalene 1.30 0.84 mg/kg dry 2.119 BRL 61 41-114 13 20 2-Chlorophenol 1.33 0.84 mg/kg dry 2.119 BRL 63 34-121 19 20 2-Methyl naphthalene 1.25 0.84 mg/kg dry 2.119 BRL 59 38-122 16 20 2-Methylphenol 1.41 0.84 mg/kg dry 2.119 BRL 67 32-122 19 20 2-Nitrophenol 1.26 0.84 mg/kg dry 2.119 BRL 60 36-123 21 20 3,3'-Dichlorobenzidine 1.59 0.84 mg/kg dry 2.119 BRL 75 22-121 8 20 3/4-Methyl phenol 1.27 0.84 mg/kg dry 2.119 BRL 60 34-119 19 20 4,6-Dinitro-2-methylphenol 1.63 1.9 mg/kg dry 2.119 BRL 77 29-132 4 20 4-Bromophenyl phenyl ether 1.46 0.84 mg/kg dry 2.119 BRL 69 46-124 7 20 4-Chloro-3-methylphenol 1.53 0.84 mg/kg dry 2.119 BRL 72 45-122 13 20 4-Chloroaniline 1.21 0.42 mg/kg dry 2.119 BRL 57 17-106 13 20 4-Chlorophenyl phenyl ether 1.43 1.3 mg/kg dry 2.119 BRL 67 45-121 5 20 4-Nitrophenol 1.54 0.84 mg/kg dry 2.119 BRL 73 30-132 7 20 Acenaphthene 1.40 0.84 mg/kg dry 2.119 BRL 66 40-123 9 20 Acenaphthylene 1.46 0.84 mg/kg dry 2.119 BRL 69 32-132 10 20 Anthracene 1.59 0.84 mg/kg dry 2.119 BRL 75 47-123 3 20 Azobenzene 1.54 0.84 mg/kg dry 2.119 BRL 72 39-125 9 20 Benzo(a)anthracene 1.49 0.84 mg/kg dry 2.119 BRL 70 49-126 1 20 Benzo(a)pyrene 1.70 0.84 mg/kg dry 2.119 BRL 80 45-129 0.8 20 Benzo(b)fluoranthene 1.60 0.84 mg/kg dry 2.119 BRL 75 45-132 1 20 Benzo(g,h,i)perylene 1.67 0.84 mg/kg dry 2.119 BRL 79 43-134 0.7 20 Benzo(k)fluoranthene 1.67 0.84 mg/kg dry 2.119 BRL 79 47-132 0.3 20 Benzoic Acid 1.32 2.5 mg/kg dry 2.119 BRL 62 10-83 24 20 Benzyl alcohol 1.39 0.84 mg/kg dry 2.119 BRL 66 29-122 19 20 bis(2-Chloroethoxy)methane 1.20 0.84 mg/kg dry 2.119 BRL 57 36-121 22 20 Bis(2-Chloroethyl)ether 1.12 0.84 mg/kg dry 2.119 BRL 53 31-120 18 20 Bis(2-chloroisopropyl)ether 1.04 0.42 mg/kg dry 2.119 BRL 49 33-131 19 20 Bis(2-Ethylhexyl)phthalate 1.65 0.84 mg/kg dry 2.119 BRL 78 51-133 0.5 20 Butyl benzyl phthalate 1.62 0.42 mg/kg dry 2.119 BRL 76 48-132 0.7 20 Chrysene 1.52 0.84 mg/kg dry 2.119 BRL 72 50-124 0.3 20 Dibenzo(a,h)anthracene 1.21 0.84 mg/kg dry 2.119 BRL 57 45-134 13 20 Dibenzofuran 1.41 0.84 mg/kg dry 2.119 BRL 66 44-120 9 20 Diethyl phthalate 1.51 0.84 mg/kg dry 2.119 BRL 71 50-124 3 20 Dimethyl phthalate 1.52 0.84 mg/kg dry 2.119 BRL 72 48-124 7 20 J 7 J D, J t) This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 0f 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Batch POG0105 - 3546 Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike Dup (POG0105-MSD1) Source: 0070067-01 Prepared: 07/09/20 Analyzed: 07/10/20 Di-n-butyl phthalate 1.66 0.84 mg/kg dry 2.119 BRL 78 51-128 5 20 Di-n-octyl phthalate 1.77 0.42 mg/kg dry 2.119 BRL 83 45-140 0.3 20 Fluoranthene 1.58 0.84 mg/kg dry 2.119 BRL 75 50-127 3 20 Fluorene 1.55 0.84 mg/kg dry 2.119 BRL 73 43-125 6 20 Hexachlorobenzene 1.45 0.84 mg/kg dry 2.119 BRL 68 45-122 7 20 Hexachlorobutadiene 1.16 0.84 mg/kg dry 2.119 BRL 55 32-123 19 20 Hexachlorocyclopentadiene 1.11 0.84 mg/kg dry 2.119 BRL 53 32-117 16 20 Hexachloroethane 0.973 0.84 mg/kg dry 2.119 BRL 46 28-117 20 20 Indeno(1,2,3-cd)pyrene 1.86 0.84 mg/kg dry 2.119 BRL 88 45-133 0.3 20 Isophorone 1.04 0.84 mg/kg dry 2.119 BRL 49 30-122 19 20 Naphthalene 1.21 0.84 mg/kg dry 2.119 BRL 57 35-123 17 20 Nitrobenzene 1.10 0.42 mg/kg dry 2.119 BRL 52 34-122 20 20 N-Nitroso-di-n-propylamine 1.25 0.84 mg/kg dry 2.119 BRL 59 36-120 18 20 N-Nitrosodiphenylamine 1.81 0.84 mg/kg dry 2.119 BRL 85 38-127 7 20 Pentachlorophenol 1.83 1.3 mg/kg dry 2.119 BRL 86 25-133 5 20 Phenanthrene 1.56 0.84 mg/kg dry 2.119 BRL 74 50-121 4 20 Phenol 1.42 0.84 mg/kg dry 2.119 BRL 67 34-121 18 20 Pyrene 1.64 0.84 mg/kg dry 2.119 BRL 77 47-127 0.5 20 Pyridine 0.303 0.42 mg/kg dry 2.119 BRL 14 20-150 9 60 Surrogate: 2,4,6-Tribromophenol 3.31 mg/kg dry 4.239 78 39-132 Surrogate: 2-Fluorobiphenyl 1.25 mg/kg dry 2.119 59 44-115 Surrogate: 2-Fluorophenol 2.58 mg/kg dry 4.239 61 35-115 Surrogate: Nitrobenzene-d5 1.11 mg/kg dry 2.119 52 37-122 Surrogate: Phenol-d5 2.69 mg/kg dry 4.239 63 34-121 Surrogate: Terphenyl-d14 1.42 mg/kg dry 2.119 67 54-127 M,J This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control Analyte Batch POG0081 - MADEP VPH (S Reporting Result Limit Units Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:4O:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (POG0081-BLK1) Prepared &Analyzed: 07/08/20 C5-C8 Aliphatics BRL 5.0 mg/kg wet C9-C12 Aliphatics BRL 5.0 mg/kg wet C9-Cl0 Aromatics BRL 5.0 mg/kg wet Surrogate: 2,5-Dibromotoluene (PID) 10700 ug/L 10000 107 70-130 Surrogate: 2,5-Dibromotoluene (FID) 11200 ug/L 10000 112 70-130 LCS (POG0081-BS1) Prepared &Analyzed: 07/08/20 C5-C8 Aliphatics 28.4 5.0 mg/kg wet 32.00 89 70-130 C9-Cl0 Aromatics 10.7 5.0 mg/kg wet 10.67 100 70-130 C9-C12 Aliphatic 37.4 5.0 mg/kg wet 32.00 117 70-130 Surrogate: 2,5-Dibromotoluene (PID) 10300 ug/L 10000 103 70-130 Surrogate: 2,5-Dibromotoluene (FID) 10700 ug/L 10000 107 70-130 LCS Dup (POG0081-BSD1) Prepared &Analyzed: 07/08/20 C5-C8 Aliphatics 29.3 5.0 mg/kg wet 32.00 92 70-130 3 50 C9-Cl0 Aromatics 10.7 5.0 mg/kg wet 10.67 100 70-130 0.2 50 C9-C12 Aliphatic 38.2 5.0 mg/kg wet 32.00 119 70-130 2 50 Surrogate: 2,5-Dibromotoluene (PID) 10400 ug/L 10000 104 70-130 Surrogate: 2,5-Dibromotoluene (FID) 11100 ug/L 10000 111 70-130 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 36 (2) Waypoint. ANALYTICAL Wood Environ. & Infrastructure Solutions (Ch Project: West Sugar Creek UST Attn: Andrew Frantz 2801 Yorkmont Rd. #100 Charlotte, NC 28208 Extractable Petroleum Hydrocarbons by GC/FID - Quality Control Level II QC Report 7/14/20 Work Order: 0070067 Time Submitted: 7/7/2020 3:4O:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POG0106 - 3546 Blank (POG0106-BLK1) Prepared: 07/09/20 Analyzed: 07/10/20 C9-C18 Aliphatics BRL 25 mg/kg wet C19-C36 Aliphatics BRL 25 mg/kg wet C1 1-C22 Aromatics BRL 25 mg/kg wet Surrogate: 1-Chlorooctadecane 1.39 mg/kg wet 2.000 70 40-140 Surrogate: o-Terphenyl 1.47 mg/kg wet 2.000 73 40-140 Surrogate: 2-Fluorobiphenyl 3.06 mg/kg wet 4.000 76 40-140 Surrogate: 2-Bromonaphthalene 3.08 mg/kg wet 4.000 77 40-140 LCS (POG0106-BS1) Prepared: 07/09/20 Analyzed: 07/10/20 C9-C18 Aliphatics 44.8 25 mg/kg wet 60.00 75 40-140 C19-C36 Aliphatics 80.0 25 mg/kg wet 80.00 100 40-140 C11-C22 Aromatics 186 25 mg/kg wet 170.0 110 40-140 Surrogate: 1-Chlorooctadecane 1.32 mg/kg wet 2.000 66 40-140 Surrogate: o-Terphenyl 1.37 mg/kg wet 2.000 69 40-140 Surrogate: 2-Fluorobiphenyl 3.38 mg/kg wet 4.000 84 40-140 Surrogate: 2-Bromonaphthalene 3.59 mg/kg wet 4.000 90 40-140 Matrix Spike (POG0106-MS1) Source: 0070067-02 Prepared: 07/09/20 Analyzed: 07/10/20 C9-Cl8 Aliphatics 62.1 32 mg/kg dry 76.78 BRL 81 40-140 C19-C36 Aliphatics 116 32 mg/kg dry 102.4 BRL 113 40-140 C11-C22 Aromatics 268 32 mg/kg dry 217.5 BRL 123 40-140 Surrogate: 1-Chlorooctadecane 1.73 mg/kg dry 2.559 68 40-140 Surrogate: o-Terphenyl 1.80 mg/kg dry 2.559 70 40-140 Surrogate: 2-Fluorobiphenyl 4.30 mg/kg dry 5.118 84 40-140 Surrogate: 2-Bromonaphthalene 4.48 mg/kg dry 5.118 88 40-140 Matrix Spike Dup (POG0106-MSD1) Source: 0070067-02 Prepared: 07/09/20 Analyzed: 07/10/20 C9-C18 Aliphatics 57.3 32 mg/kg dry 76.70 BRL 75 40-140 8 50 C19-C36 Aliphatics 112 32 mg/kg dry 102.3 BRL 109 40-140 4 50 C11-C22 Aromatics 250 32 mg/kg dry 217.3 BRL 115 40-140 7 50 Surrogate: 1-Chlorooctadecane 1.62 mg/kg dry 2.557 64 40-140 Surrogate: o-Terphenyl 1.61 mg/kg dry 2.557 63 40-140 Surrogate: 2-Fluorobiphenyl 3.78 mg/kg dry 5.113 74 40-140 Surrogate: 2-Bromonaphthalene 4.04 mg/kg dry 5.113 79 40-140 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 36 Sample Extraction Data Prep Method: 3546 Lab Number Batch Initial Final Date/Time 0070067-01 POG0106 10.1 g 2 mL 07/09/20 10:30 0070067-02 POG0106 10.06 g 2 mL 07/09/20 10:30 0070067-03 POG0106 10.22 g 2 mL 07/09/20 10:30 0070067-04 POG0106 10.01 g 2 mL 07/09/20 10:30 0070067-05 POG0106 10.08 g 2 mL 07/09/20 10:30 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 0070067-01 POG0129 30 g 30 g 07/10/20 13:00 0070067-02 POG0129 30 g 30 g 07/10/20 13:00 0070067-03 POG0129 30 g 30 g 07/10/20 13:00 0070067-04 POG0129 30 g 30 g 07/10/20 13:00 0070067-05 POG0129 30 g 30 g 07/10/20 13:00 Prep Method: 3546 Lab Number Batch Initial Final Date/Time 0070067-01 POG0105 30.09 g 1 mL 07/09/20 10:30 0070067-02 POG0105 30.05 g 1 mL 07/09/20 10:30 0070067-03 POG0105 30.01 g 1 mL 07/09/20 10:30 0070067-04 POG0105 30.07 g 1 mL 07/09/20 10:30 0070067-05 POG0105 30.09 g 1 mL 07/09/20 10:30 Prep Method: 5035 Lab Number Batch Initial Final DatelTime 0070067-01 POG0082 4.21 g 5 mL 07/08/20 10:38 0070067-02 POG0082 4.41 g 5 mL 07/08/20 10:38 0070067-03 POG0082 4.76 g 5 mL 07/08/20 10:38 0070067-04 POG0082 4.96 g 5 mL 07/08/20 10:38 0070067-05 POG0082 6.27 g 5 mL 07/08/20 10:38 Prep Method: MADEP VPH (S) Lab Number Batch Initial Final Date/Time 0070067-01 POG0081 5.86 g 16 mL 07/08/20 10:37 0070067-02 POG0081 4.11 g 16 mL 07/08/20 10:37 0070067-03 POG0081 5.85 g 16 mL 07/08/20 10:37 0070067-04 POG0081 6.57 g 16 mL 07/08/20 10:37 0070067-05 POG0081 5.35 g 16 mL 07/08/20 10:37 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 0f 36 O ❑ v M n P?❑❑G D Z;t n n C a ❑� cr N CD n 0 rr u A u z m �.❑ ❑a z n C r II ❑ CO) n r< 3 rr r a❑❑X ❑.. ca D 0 �❑❑a O z� .. n Z CD ❑ 'T O nG CG m 3 c°,❑❑ n za n r N ❑ r H co) r N n =❑❑C CD Z a n IV Ul ❑ca -� a 0 ° In Cl)m , ^ N cn m m `8 a M M 3 c c. v] 3 r r �• 7 m m 'S 7 C (/? y M 0 0 f�D N ro' fo v3 3. 3 N .M i -9 z-n N I O Nn x c c 3 10 m m 1 :rd `G m 30 ,' p z n �' m_ N SN "� N Em D _ '� r o D £ LC rL a z ` �' ° r> �O o an ° is M� nm c H R U c Q Uzi, m VI,`� � i 0 Z. < v0 W -S'0 �'^ �) c-1m3 �z1m . 1C ��.w „ V �v m '"yam »a $ y Z� w• 3 O N CA o �° 0 +� c> a O- � cR ry S O n-4 Q `s O -i 0 G)�r� m p' X cv �GcZ �m ; a co �� M• m r2 c 'm 3° 0 1- —0. .. W a x m C, N D m - S ` o n m m m' t7 M z m�mL v m -p y �In D m e m 7 II mXCL0 � � � mo m a D. 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A 3 Z M r N 3 o D D M m 3 co N T z CD In v D r z z S o n M m O m ' z p +c> Q O o z i n Ot O 7 A ; o O D CI. 0 G Ot C rt 3 0c N w Z H 0) 7� � M A ca u z �o D ar TC '` D rip zo k � CO) � CL O D O C N m /� a ♦/ N CD fA CND a .O► rir 2 N C N O N Q' any m �� z Ot N 0N y 0 C CD CD • O 0 •.e C(0)— 3 � Jam° J! m 2 Poo CD 2. o N - n m y P 0 °� a n O fD 5) r n 40 o So v cn D �• 7• � ,ZWM r p a WMa y m np M- w,§ X-z 2 2 R Z r = m �v�r,��o<� �N 2 Z D a Q M m m C L ^� I I�\1 I`U) C5 ° ! o z 6 Page 36 of 36 Beverly, Trudy From: Beverly, Trudy Sent: Wednesday, August 12, 2020 12:42 PM To: Frantz, Andrew J Cc: Gucciardi, Steve; Pierotti, Doug; Corley, Helen Subject: RE: [External] 4732 W Sugar Creek Rd Parcel - IAA Report Good Afternoon Andrew, Received. No need to mail a paper copy. We switched to electronic report submittals in March. Have a great day, Trudy Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mille Regional Office irvrc,� on, Mooresville g 704.235.2182 (Office) Trudy.Beverlykncdenr. ov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: ht_pt s:Hdeg.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https://deg.nc.aov/about/divisions/waste-mana2ement/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httos://deo.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-mans File Review Procedures: htlps://deg.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): httos: //deq.nc. gov/about/divisions/waste-manai4ement/laserfiche Document Submittal & UST File Names for Laserfiche Policies: httns://files.ne.izov/nedeafWaste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policy.odf https:Hfiles.nc.gov/ncdeq/Waste%20Management/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Frantz, Andrew J [mailto:andrew.frantz@woodplc.com] Sent: Wednesday, August 12, 2020 12:32 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Cc: Gucciardi, Steve <sgucciardi@ci.charlotte.nc.us>; Pierotti, Doug <dpierotti@ci.charlotte.nc.us>; Corley, Helen <helen.corley@woodplc.com> Subject: [External] 4732 W Sugar Creek Rd Parcel - IAA Report CAUTION:I email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to c. ov Good Afternoon Trudy, Attached is the IAA report for the heating oil UST that was removed from the 4732 W Sugar Creek Rd Parcel in Charlotte. A paper copy of the report will be on its way in a few days as we are still working remotely. Hope everything is well and let us know if you have any questions. Thanks, Andrew J. Frantz, REM Senior Environmental Scientist Direct: (704) 357-5542 Mobile: (704) 519-9230 www.woodpic.com This message is the property of John Wood Group PLC and/or its subsidiaries and/or affiliates and is intended only for the named recipient(s). Its contents (including any attachments) may be confidential, legally privileged or otherwise protected from disclosure by law. Unauthorized use, copying, distribution or disclosure of any of it may be unlawful and is strictly prohibited. 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