4406_ROSCANS_2005

North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section - 1636 Mail
Service Center - Raleigh, NC 27699-1639 - Phone No. [phone]
WELL ABANDONMENT RECORD WELL CONTRACTOR 'di e- C)Ue-r- .—DU.Vr.l I--7--
WELL CONTRACTOR CERT�ION ii _ �5 Y
• WELL USE (Cheek Applicable Box): Residential ❑ Municipal ❑ Industrial 0 Agricultural ❑ Monitoring t$
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show a sketch of the location on back of form.)
Nearest Town: (1 ,, �CountyIF
(Road Name and Number, Community, Subdivision, Lot No.)
s.OW��NEk-:C+C��Ciia_t_«�
4. ADDRESS:Rt'i
5. TOPOGRAPHY: draw, slope, hilltop, valle flat ,
6. TOTAL DEPTH:_ Ci (circle one)
DIAMETER `I
7. CASING REMOVED:
fit diameter
�ISI1vl EcrloN: �}�"i-� �;>t Y
(Amount of 70% hypochlorite used:)
9. SEALING MATERIAL:
Lleat C =- = Sand (ement
bads of cement _9 _ bags of cement
gallons of water gallons of water
0111a
Type material
:mount
10. EXPLAIN METHOD EMPLACEMENT OF MATERIAL.
i i . DATE WELL ABANDONED Q - i
Quadrarlgle No.
WELL DIAGRAM: Draw a detailed sketch of the
well showing total depth, depth and diameter of
screens remaining in the well, gravel interval,
intervals of casing perforations, and depths and
types of fill materials used.
qoI
i do hereby certify that this well was abandoned in accordance with 15A NCAC 2C, well construction
standards, and that a copy of the record has been provided to the well owner.
Signature of'person abandoning the well Date
`w'LLL LOCA"rION: Draw a location sketch on the reverse of this sheet, showing the direction and distance
of the well to at least two (2) nearby reference points such as roads, intersections and
streams. Identify roads with State Highway road identification numbers.
: Ubrrtit original to the Division of Water Quality, Groundwater Section, one copy to the owner within 30 days
from completion of abandonment.
GW•30 Revised 12/99

IV. TV
E ii�

BLUE RIDGE
PAPER PRODUCTS INC.
November 28, 2005
Mr. James Patterson
North Carolina Department of Environment
And Natural Resources
2090 US Highway 70
Swannanoa, North Carolina 28778
Re: Chemical analysis of Canton Mill process wastes.
Dear Mr. Patterson:
Attached is laboratory analysis related to the latest sampling of Canton Mill process
wastes, including wastewater treatment plant sludge, lime mud, slaker grits, precoat filter
dregs, boiler fly ash, and boiler cinders. The analysis is in accordance with Permit
Number 44-06, Area A East, and 15A NCAC 13B, Section .103(d).
Samples were collected on November 2, 2005. Each sample was analyzed by TCLP for
RCRA metals, volatile organics, and semi -volatile organics (excluding herbicides and
pesticides). In addition, the sludge and lime were tested for reactive cyanide and reactive
sulfide. All samples were found to be well within the RCRA standards for each of the
tested parameters. The laboratory results confirm that none of the Canton Mill process
wastes are RCRA hazardous wastes.
Please call me at 828-646-2028 if you have questions or comments.
Sincerely,
im Giauque
Attachments
Copy: Paul Dickens
Bob Williams (Letter Only)
tile:patterson 112805.doc
175 Main Street • P.O. Box 4000 • Canton, North Carolina 28716
Phone: [phone]
Raising Your Expectations

ace Analytical °
www.pacelabs.com
November 15, 2005
Mr. Jim Giauque
Blue Ridge Paper Products
Main Street
PO Box 4000
Canton, NC 28716
RE: Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Dear Mr. Giauque:
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: 704, 875, 9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828,254.7176
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 2, 2005. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincer
c
Lorri Patton
[e-mail]
Project Manager
Enclosures
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ACCORD
In I
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

aceAnalytical °
www.pacelabs.com
Solid results are reported on a dry weight basis
Lab Sample No: 926293432
Client Sample ID: WWTP SLUDGE
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 26078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651-001 Date Collected: 11/02/05 09:45
Matrix: Soil Date Received: 11/02/05 14:13
Parameters Results Units Report Limit Analyzed By CAS No. Qua] RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/08/05 14:00 11/08/05 14:00
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
NO
mg/l
0.025
11/11/05
17:09
ALV
7440-38-2
Barium
1.5
mg/l
0.025
11/11/05
17:09
ALV
7440-39.3
Cadmium
ND
mg/l
0.0050
11/11/05
17:09
ALV
7440-43-9
Chromium
NO
mg/l
0.010
11/11/05
17:09
ALV
7440-47-3
Lead
0.026
mg/l
0.025
11/11/05
17:09
ALV
7439-92-1
Selenium
0.045
mg/l
0.025
11/11/05
17:09
ALV
7782-49-2
Silver
0.012
mg/l
0.010
11/11/05
17:09
ALV
7440-22-4
Date Digested
11/10/05 10:00
11/10/05
10:00
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
0.00022
mg/l
0.00020
11/10/05
07:00
SHB
7439-97-6
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
NO
mg/l
0.75
11/12/05
18:23
BET
106-46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/12/05
18:23
BET
121-14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
11/12/05
18:23
BET
87-68.3
Hexachlorobenzene
NO
mg/l
0.013
11/12/05
18:23
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
11/12/05
18:23
BET
67-72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.050
11/12/05
18:23
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/12/05
18:23
BET
Nitrobenzene
NO
mg/l
0.20
11/12/05
18:23
BET
98-95.3
Pentachlorophenol
NO
mg/l
10.
11/12/05
18:23
BET
87.86-5
Pyridine
NO
mg/l
0.50
11/12/05
18:23
BET
110-86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
11/12/05
18:23
BET
95.95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
11/12/05
18:23
BET
88-06-2
Nitrobenzene-d5 (S)
62
Y.
11/12/05
18:23
BET
4165-60-0
2-Fluorobiphenyl (S)
59
Y.
11/12/05
18:23
BET
321.60-8
Terphenyl-d14 (S)
90
i
11/12/05
18:23
BET
1718-51-0
Phenol-d5 (S)
24
Y.
11/12/05
18:23
BET
4165-62-2
2-Fluorophenol (S)
33
Y.
11/12/05
18:23
BET
367.12-4
2,4,6-Tribromophenol (S)
98
Y.
11/12/05
18:23
BET
118-79-6
Date Extracted
11/09/05
11/09/05
Date: 11/15/05
Page: 1 of 29
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc
99030
without the written consent of Pace Analytical Services, Inc.
Sc
99006
FL NELAP
E87648
SO N ACCOgp9
.=.:
FL NELAP
E87627

aceAnalytical °
www.pacelabs.com
Lab Sample No: 926293432
Client Sample ID: WWTP SLUDGE
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: 704,875.9092
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828,252.4618
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651-001 Date Collected: 11/02/05 09:45
Matrix: Soil Date Received: 11/02/05 14:13
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qua] RegLmt
GUMS Vol ati l es
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
ND
mg/l
0.0050
11/12/05
00:46
DLK
71-43.2
2-Butanone (MEK)
NO
mg/l
0.10
11/12/05
00:46
DLK
78-93-3
Carbon tetrachloride
ND
mg/l
0.0050
11/12/05
00:46
DLK
56-23-5
Chlorobenzene
NO
mg/l
0.0050
11/12/05
00:46
DLK
108-90-7
Chloroform
ND
mg/l
0.0050
11/12/05
00:46
DLK
67-66-3
1,4-Dichlorobenzene
ND
mg/l
0.0050
11/12/05
00:46
DLK
106-46-7
1,2-Dichloroethane
NO
mg/l
0.0050
11/12/05
00:46
DLK
107.06-2
1,1-Dichloroethene
ND
mg/l
0.0050
11/12/05
00:46
DLK
75.35.4
Tetrachloroethene
ND
mg/l
0.0050
11/12/05
00:46
DLK
127.18-4
Trichloroethene
ND
mg/l
0.0050
11/12/05
00:46
DLK
79.01-6
Vinyl chloride
NO
mg/l
0.0050
11/12/05
00:46
DLK
75-01-4
Toluene-d8 (S)
89
Y.
11/12/05
00:46
DLK
2037-26-5
4-Bromofluorobenzene (S)
78
Y.
11/12/05
00:46
DLK
460-00-4
Dibromofluoromethane (S)
75
Y.
11/12/05
00:46
DLK
1868-53-7 1
1,2-Dichloroethane-d4 (S)
69
Y.
11/12/05
00:46
DLK
17060-07-0 1
Date: 11/15/05
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 " ACCOR
Page: 2 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

KaceAnalyfical@
www.pacelabs.com
Lab Sample No: 926293457
Client Sample ID: LIME MUD
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651-002 Date Collected: 11/02/05 08:30
Matrix: Soil Date Received: 11/02/05 14:13
Parameters Results Units Report Limit Analyzed By CAS No. Qual Re9Lmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/08/05 14:00 11/08/05 14:00
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010 / EPA
6010
Arsenic
NO
mg/l
0.025
11/11/05
17:13
ALV
7440-38-2
Barium
0.32
mg/l
0.025
11/11/05
17:13
ALV
7440.39-3
Cadmium
NO
mg/l
0.0050
11/11/05
17:13
ALV
7440-43-9
Chromium
NO
mg/l
0.010
11/11/05
17:13
ALV
7440-47-3
Lead
NO
mg/l
0.025
11/11/05
17:13
ALV
7439-92-1
Selenium
NO
mg/l
0.025
11/11/05
17:13
ALV
7782-49-2
Silver
0.013
mg/l
0.010
11/11/05
17:13
ALV
7440-22-4
Date Digested
11/10/05 10:00
11/10/05
10:00
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
11/10/05
07:00
SHB
7439-97-6
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510 / EPA
8270
1,4-Dichlorobenzene
NO
mg/l
0.75
11/12/05
18:59
BET
106.46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/12/05
18:59
BET
121-14-2
Hexachloro-1,3-butadiene
NO
mg/1
0.050
11/12/05
18:59
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
11/12/05
18:59
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
11/12/05
18:59
BET
67.72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.050
11/12/05
18:59
BET
95.48.7
3&4-Methylphenol
NO
mg/l
0.010
11/12/05
18:59
BET
Nitrobenzene
NO
mg/l
0.20
11/12/05
18:59
BET
98-95-3
Pentachlorophenol
NO
mg/l
10.
11/12/05
18:59
BET
87-86-5
Pyridine
NO
mg/l
0.50
11/12/05
18:59
BET
110.86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
11/12/05
18:59
BET
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
11/12/05
18:59
BET
88-06.2
Nitrobenzene-d5 (S)
73
Z
11/12/05
18:59
BET
4165-60-0
2-Fluorobiphenyl (S)
59
Y.
11/12/05
18:59
BET
321-60-8
Terphenyl-d14 (S)
85
%
11/12/05
18:59
BET
1718-51.0
Phenol-d5 (S)
29
Y.
11/12/05
18:59
BET
4165.62-2
2-Fluorophenol (S)
40
Y.
11/12/05
18:59
BET
367.12-4
2,4,6-Tribromophenol (S)
97
Y.
11/12/05
18:59
BET
118-79-6
Date Extracted
11/09/05
11/09/05
Date: 11/15/05
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 37712 without the written consent of Pace Analytical Services, Inc.
99030
FL NELAP E87648 "a
Page: 3 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical
www.pacelabs.com
Lab Sample No: 926293457
Client Sample ID: LIME MUD
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: 704.875, 9092
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651.002 Date Collected: 11/02/05 08:30
Matrix: Soil Date Received: 11/02/05 14:13
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
GUMS Vol ati l es
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
NO
mg/l
0.0050
11/11/05
00:19
DLK
71-43-2
2-Butanone (MEK)
NO
mg/l
0.10
11/11/05
00:19
DLK
78-93-3
Carbon tetrachloride
NO
mg/l
0.0050
11/11/05
00:19
DLK
56.23-5
Chlorobenzene
ND
mg/l
0.0050
11/11/05
00:19
DLK
108.90-7
Chloroform
NO
mg/l
0.0050
11/11/05
00:19
DLK
67-66-3
1,4-Dichlorobenzene
ND
mg/l
0.0050
11/11/05
00:19
DLK
106-46-7
1,2-Dichloroethane
NO
mg/l
0.0050
11/11/05
00:19
DLK
107-06.2
1,1-Dichloroethene
ND
mg/l
0.0050
11/11/05
00:19
DLK
75-35.4
Tetrachloroethene
NO
mg/l
0.0050
11/11/05
00:19
DLK
127-18.4
Trichloroethene
ND
mg/l
0.0050
11/11/05
00:19
DLK
79-01-6
Vinyl chloride
NO
mg/l
0.0050
11/11/05
00:19
DLK
75-01.4
Toluene-d8 (S)
90
%
11/11/05
00:19
DLK
2037-26-5
4-Bromofluorobenzene (S)
56
%
11/11/05
00:19
DLK
460.00-4 1
Dibromofluoromethane (S)
0
%
11/11/05
00:19
DLK
1868-53-7 1
1,2-Dichloroethane-d4 (S)
106
%
11/11/05
00:19
DLK
17060-07-0
Date: 11/15/05
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 37712 without the written consent of Pace Analytical Services, Inc.
99030
N ACC
FL NELAP E87648
Page: 4 of 29
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

�laneAnalyticale
www.pacelabs.com
Lab Sample No: 926293481
Client Sample ID: SLAKER GRITS
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651-003 Date Collected: 11/02/05 10:05
Matrix: Soil Date Received: 11/02/05 14:13
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/08/05 14:00 11/08/05 14:00
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
ND
mg/l
0.025
11/11/05
17:17
ALV
7440.38-2
Barium
0.43
mg/l
0.025
11/11/05
17:17
ALV
7440-39-3
Cadmium
ND
mg/l
0.0050
11/11/05
17:17
ALV
7440-43-9
Chromium
ND
mg/l
0.010
11/11/05
17:17
ALV
7440-47-3
Lead
ND
mg/l
0.025
11/11/05
17:17
ALV
7439-92-1
Selenium
ND
mg/l
0.025
11/11/05
17:17
ALV
7782-49-2
Silver
ND
mg/l
0.010
11/11/05
17:17
ALV
7440-22.4
Date Digested
11/10/05 10:00
11/10/05
10:00
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
11/10/05
07:00
SHB
7439-97-6
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
11/12/05
19:35
BET
106-46.7
2,4-Dinitrotoluene
ND
mg/l
0.013
11/12/05
19:35
BET
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
11/12/05
19:35
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
11/12/05
19:35
BET
118-74-1
Hexachloroethane
ND
mg/l
0.30
11/12/05
19:35
BET
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/l
0.050
11/12/05
19:35
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/12/05
19:35
BET
Nitrobenzene
ND
mg/l
0.20
11/12/05
19:35
BET
98-95-3
Pentachlorophenol
ND
mg/l
10.
11/12/05
19:35
BET
87-86.5
Pyridine
ND
mg/l
0.50
11/12/05
19:35
BET
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
11/12/05
19:35
BET
95-95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
11/12/05
19:35
BET
88-06-2
Nitrobenzene-d5 (S)
46
%
11/12/05
19:35
BET
4165-60-0
2-Fluorobiphenyl (S)
43
%
11/12/05
19:35
BET
321-60-8
Terphenyl-d14 (S)
77
%
11/12/05
19:35
BET
1718-51-0
Phenol-d5 (S)
19
%
11/12/05
19:35
BET
4165-62-2
2-Fluorophenol (S)
24
i
11/12/05
19:35
BET
367.12.4
2,4,6-Tribromophenol (S)
85
i
11/12/05
19:35
BET
118-79.6
Date Extracted
11/09/05
11/09/05
Date: 11/15/05
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
N A!0,
FL NELAP E87648 �o.. _oy
Page: 5 of 29
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

1 I—J/
ace Analytical °
www.pacelabs.com
Lab Sample No: 926293481
Client Sample ID: SLAKER GRITS
Parameters
GUMS Vol ati l es
Volatile Organics, TCLP Leach
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Date: 11/15/05
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828.252,4618
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651-003 Date Collected: 11/02/05 10:05
Matrix: Soil Date Received: 11/02/05 14:13
Results Units Report Limit Analyzed By CAS No. Dual RegLmt
Method:
EPA 8260
ND
mg/l
0.0050
11/11/05
00:38
DLK
71-43-2
ND
mg/l
0.10
11/11/05
00:38
DLK
78-93-3
ND
mg/l
0.0050
11/11/05
00:38
DLK
56-23-5
NO
mg/l
0.0050
11/11/05
00:38
DLK
108-90-7
ND
mg/l
0.0050
11/11/05
00:38
DLK
67-66-3
NO
mg/l
0.0050
11/11/05
00:38
DLK
106.46-7
ND
mg/l
0.0050
11/11/05
00:38
DLK
107-06-2
NO
mg/l
0.0050
11/11/05
00:38
DLK
75-35-4
ND
mg/l
0.0050
11/11/05
00:38
DLK
127-18-4
NO
mg/l
0.0050
11/11/05
00:38
DLK
79.01-6
ND
mg/l
0.0050
11/11/05
00:38
DLK
75-01-4
94
%
11/11/05
00:38
DLK
2037-26.5
93
%
11/11/05
00:38
DLK
460.00.4
0
%
11/11/05
00:38
DLK
1868-53-7
81
%
11/11/05
00:38
DLK
17060.07-0
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
N ACCOR
FL NELAP E87648
1
Page: 6 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

� aceAnalytical °
www.pacelabs.com
Lab Sample No: 926293499
Client Sample ID: PRECOAT FILTER
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone. [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651.004 Date Collected: 11/02/05 08:45
Matrix: Soil Date Received: 11/02/05 14:13
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/08/05 14:00 11/08/05 14:00
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
NO
mg/l
0.025
11/11/05
17:21
ALV
7440-38-2
Barium
0.034
mg/l
0.025
11/11/05
17:21
ALV
7440.39-3
Cadmium
NO
mg/l
0.0050
11/11/05
17:21
ALV
7440-43-9
Chromium
NO
mg/l
0.010
11/11/05
17:21
ALV
7440-47-3
Lead
NO
mg/l
0.025
11/11/05
17:21
ALV
7439-92-1
Selenium
ND
mg/l
0.025
11/11/05
17:21
ALV
7782-49-2
Silver
NO
mg/l
0.010
11/11/05
17:21
ALV
7440-22-4
Date Digested
11/10/05 10:00
11/10/05
10:00
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
ND
mg/l
0.00020
11/10/05
07:00
SHB
7439-97-6
GUMS Serni vol ati l es
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
11/12/05
20:10
BET
106-46.7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/12/05
20:10
BET
121.14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
11/12/05
20:10
BET
87-68.3
Hexachlorobenzene
ND
mg/l
0.013
11/12/05
20:10
BET
118.74-1
Hexachloroethane
NO
mg/l
0.30
11/12/05
20:10
BET
67-72.1
2-Methylphenol (o-Cresol)
ND
mg/l
0.050
11/12/05
20:10
BET
95.48-7
3&4-Methylphenol
NO
mg/l
0.010
11/12/05
20:10
BET
Nitrobenzene
NO
mg/l
0.20
11/12/05
20:10
BET
98.95.3
Pentachlorophenol
ND
mg/l
10.
11/12/05
20:10
BET
87-86-5
Pyridine
NO
mg/l
0.50
11/12/05
20:10
BET
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
11/12/05
20:10
BET
95-95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
11/12/05
20:10
BET
88-06-2
Nitrobenzene-d5 (S)
57
Y.
11/12/05
20:10
BET
4165-60-0
2-Fluorobiphenyl (S)
58
Z
11/12/05
20:10
BET
321-60-8
Terphenyl-d14 (S)
80
i
11/12/05
20:10
BET
1718-51-0
Phenol-d5 (S)
24
i
11/12/05
20:10
BET
4165.62-2
2-Fluorophenol (S)
31
i
11/12/05
20:10
BET
367.12-4
2,4,6-Tribromophenol (S)
92
i
11/12/05
20:10
BET
118.79.6
Date Extracted
11/09/05
11/09/05
Date: 11/15/05 Page: 7 of 29
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
„ AC
COR
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacolabs.com
Lab Sample No: 926293499
Client Sample ID: PRECOAT FILTER
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651-004 Date Collected: 11/02/05 08:45
Matrix: Soil Date Received: 11/02/05 14:13
Parameters
Results
Units
Report Limit
Analyzed
By
GUMS Vol ati l es
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
NO
mg/l
0.10
11/14/05
15:12
DLK
2-Butanone (MEK)
ND
mg/l
2.0
11/14/05
15:12
DLK
Carbon tetrachloride
NO
mg/l
0.10
11/14/05
15:12
DLK
Chlorobenzene
ND
mg/l
0.10
11/14/05
15:12
DLK
Chloroform
ND
mg/l
0.10
11/14/05
15:12
DLK
1,4-Dichlorobenzene
NO
mg/l
0.10
11/14/05
15:12
DLK
1,2-Dichloroethane
ND
mg/l
0.10
11/14/05
15:12
DLK
1,1-Dichloroethene
ND
mg/l
0.10
11/14/05
15:12
DLK
Tetrachloroethene
ND
mg/l
0.10
11/14/05
15:12
DLK
Trichloroethene
NO
mg/l
0.10
11/14/05
15:12
DLK
Vinyl chloride
ND
mg/l
0.10
11/14/05
15:12
DLK
Toluene-d8 (S)
105
Y.
11/14/05
15:12
DLK
4-Bromofluorobenzene (S)
95
%
11/14/05
15:12
DLK
Dibromofluoromethane (S)
131
Y.
11/14/05
15:12
DLK
1,2-Dichloroethane-d4 (S)
130
%
11/14/05
15:12
DLK
Date: 11/15/05
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
O 111 ACCpga
CAS No. Qual RegLmt
71.43-2
78-93-3
56.23-5
108.90-7
67-66-3
106.46-7
107-06-2
75-35-4
127-18-4
79-01-6
75.01-4
2037-26-5
460-00-4
1868-53-7 2,3
17060-07-0
Page: 8 of 29
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

�laneAnalyticalo
www.pacelabs.com
Lab Sample No: 926293507
Client Sample ID: FLYASH
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: 704.875, 9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651-005 Date Collected: 11/02/05 09:15
Matrix: Soil Date Received: 11/02/05 14:13
Parameters Results Units Report Limit Analyzed By CAS No. Qua] RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/08/05 14:00 11/08/05 14:00
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
ND
mg/l
0.025
11/11/05
17:24
ALV
7440-38-2
Barium
0.22
mg/l
0.025
11/11/05
17:24
ALV
7440-39-3
Cadmium
NO
mg/l
0.0050
11/11/05
17:24
ALV
7440-43-9
Chromium
NO
mg/l
0.010
11/11/05
17:24
ALV
7440-47-3
Lead
ND
mg/l
0.025
11/11/05
17:24
ALV
7439-92-1
Selenium
NO
mg/l
0.025
11/11/05
17:24
ALV
7782-49-2
Silver
NO
mg/l
0.010
11/11/05
17:24
ALV
7440-22-4
Date Digested
11/10/05 10:00
11/10/05
10:00
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
ND
mg/l
0.00020
11/10/05
07:00
SHB
7439-97-6
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
NO
mg/l
0.75
11/12/05
20:46
BET
106.46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/12/05
20:46
BET
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
11/12/05
20:46
BET
87-68.3
Hexachlorobenzene
NO
mg/l
0.013
11/12/05
20:46
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
11/12/05
20:46
BET
67-72.1
2-Methylphenol (o-Cresol)
NO
mg/l
0.050
11/12/05
20:46
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/12/05
20:46
BET
Nitrobenzene
NO
mg/l
0.20
11/12/05
20:46
BET
98-95-3
Pentachlorophenol
NO
mg/l
10.
11/12/05
20:46
BET
87-86-5
Pyridine
NO
mg/l
0.50
11/12/05
20:46
BET
110-86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
11/12/05
20:46
BET
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
11/12/05
20:46
BET
88-06-2
Nitrobenzene-d5 (S)
71
Y.
11/12/05
20:46
BET
4165-60-0
2-Fluorobiphenyl (S)
61
i
11/12/05
20:46
BET
321-60-8
Terphenyl-d14 (S)
81
i
11/12/05
20:46
BET
1718-51-0
Phenol-d5 (S)
26
i
11/12/05
20:46
BET
4165-62-2
2-Fluorophenol (S)
37
%
11/12/05
20:46
BET
367-12-4
2,4,6-Tribromophenol (S)
94
%
11/12/05
20:46
BET
118-79-6
Date Extracted
11/09/05
11/09/05
Date: 11/15/05
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
a N ACCpRO
W
Page: 9 of 29
Charlotte Certification IN
NC Wastewater 12
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SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 926293507
Client Sample ID: FLYASH
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: 704.875, 9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651.005 Date Collected: 11/02/05 09:15
Matrix: Soil Date Received: 11/02/05 14:13
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.
Qual RegLmt
GUMS Vol ati l es
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
NO
mg/l
0.10
11/14/05
14:52
DLK
71.43-2
2-Butanone (MEK)
NO
mg/l
2.0
11/14/05
14:52
DLK
78-93.3
Carbon tetrachloride
ND
mg/l
0.10
11/14/05
14:52
DLK
56-23-5
Chlorobenzene
NO
mg/l
0.10
11/14/05
14:52
DLK
108-90-7
Chloroform
ND
mg/l
0.10
11/14/05
14:52
DLK
67-66-3
1,4-Dichlorobenzene
NO
mg/l
0.10
11/14/05
14:52
DLK
106-46-7
1,2-Dichloroethane
NO
mg/l
0.10
11/14/05
14:52
DLK
107-06-2
1,1-Dichloroethene
ND
mg/l
0.10
11/14/05
14:52
DLK
75.35-4
Tetrachloroethene
NO
mg/l
0.10
11/14/05
14:52
DLK
127-18-4
Trichloroethene
NO
mg/l
0.10
11/14/05
14:52
DLK
79-01-6
Vinyl chloride
NO
mg/l
0.10
11/14/05
14:52
DLK
75-01-4
Toluene-d8 (S)
94
%
11/14/05
14:52
DLK
2037-26-5
4-Bromofluorobenzene (S)
58
Y.
11/14/05
14:52
DLK
460-00-4
4
Dibromofluoromethane (S)
224
Z
11/14/05
14:52
DLK
1868-53-7
3,4
1,2-Dichloroethane-d4 (S)
205
i
11/14/05
14:52
DLK
17060.07-0
4
Date: 11/15/05
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,p nCCpRo
�,Iho1�r�
Page: 10 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

�lacmnalyfical@
www.pacelabs.com
Lab Sample No: 926293515
Client Sample ID: CINDERS
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: 704,875.9092
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651.006 Date Collected: 11/02/05 09:05
Matrix: Soil Date Received: 11/02/05 14:13
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/08/05 14:00 11/08/05 14:00
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
0.82
mg/l
0.025
11/11/05
17:28
ALV
7440-38-2
Barium
0.28
mg/l
0,025
11/11/05
17:28
ALV
7440-39-3
Cadmium
0.016
mg/l
0.0050
11/11/05
17:28
ALV
7440-43-9
Chromium
0.010
mg/l
0.010
11/11/05
17:28
ALV
7440-47-3
Lead
ND
mg/l
0.025
11/11/05
17:28
ALV
7439-92-1
Selenium
0.10
mg/l
0.025
11/11/05
17:28
ALV
7782-49-2
Silver
NO
mg/l
0.010
11/11/05
17:28
ALV
7440-22-4
Date Digested
11/10/05 10:00
11/10/05
10:00
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
11/10/05
07:00
SHB
7439-97-6
GUMS Senlivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
NO
mg/l
0.75
11/12/05
21:22
BET
106-46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/12/05
21:22
BET
121-14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
11/12/05
21:22
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
11/12/05
21:22
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
11/12/05
21:22
BET
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/l
0.050
11/12/05
21:22
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/12/05
21:22
BET
Nitrobenzene
ND
mg/l
0.20
11/12/05
21:22
BET
98-95.3
Pentachlorophenol
NO
mg/l
10.
11/12/05
21:22
BET
87-86-5
Pyridine
ND
mg/l
0.50
11/12/05
21:22
BET
110.86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
11/12/05
21:22
BET
95-95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
11/12/05
21:22
BET
88.06-2
Nitrobenzene-d5 (S)
62
i
11/12/05
21:22
BET
4165-60-0
2-Fluorobiphenyl (S)
48
i
11/12/05
21:22
BET
321.60-8
Terphenyl-d14 (S)
80
i
11/12/05
21:22
BET
1718-51-0
Phenol-d5 (S)
25
i
11/12/05
21:22
BET
4165-62.2
2-Fluorophenol (S)
35
i
11/12/05
21:22
BET
367.12.4
2,4,6-Tribromophenol (S)
89
i
11/12/05
21:22
BET
118-79.6
Date Extracted
11/09/05
11/09/05
Date: 11/15/05
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACCCA
On
Page: 11 of 29
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Lab Sample No: 926293515
Client Sample ID: CINDERS
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254,7176
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Project Sample Number: 92106651-006 Date Collected: 11/02/05 09:05
Matrix: Soil Date Received: 11/02/05 14:13
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.Qua] RegLmt
GUMS Vol ati l es
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
NO
mg/l
0.0050
11/11/05
DLK
71-43-2
2-Butanone (MEK)
ND
mg/1
0.10
11/11/05
DLK
78-93-3
Carbon tetrachloride
ND
mg/l
0.0050
11/11/05
DLK
56-23.5
Chlorobenzene
NO
mg/l
0.0050
11/11/05
DLK
108-90-7
Chloroform
ND
mg/l
0.0050
11/11/05
DLK
67-66-3
1,4-Dichlorobenzene
NO
mg/l
0.0050
11/11/05
DLK
106-46-7
1,2-Dichloroethane
ND
mg/l
0.0050
11/11/05
DLK
107-06-2
1,1-Dichloroethene
NO
mg/l
0.0050
11/11/05
DLK
75.35.4
Tetrachloroethene
NO
mg/l
0.0050
11/11/05
DLK
127-18-4
Trichloroethene
NO
mg/l
0.0050
11/11/05
DLK
79.01.6
Vinyl chloride
NO
mg/l
0.0050
11/11/05
DLK
75-01-4
Toluene-d8 (S)
83
Y.
11/11/05
DLK
2037-26-5
4-Bromofluorobenzene (S)
44
Y.
11/11/05
DLK
460.00-4 1
Dibromofluoromethane (S)
103
i
11/11/05
DLK
1868-53-7
1,2-Dichloroethane-d4 (S)
57
%
11/11/05
DLK
17060-07-0 1
Date: 11/15/05 Page: 12 of 29
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc
99030
without the written consent of Pace Analytical Services, Inc.
SC
99006
FL NELAP
E87648
to` N AiiCCOgg9y
FL NELAP
E87627
t^►�'11nP �

�laneAnalyfical°
www, pacelahs. com
PARAMETER FOOTNOTES
Method 9071E modified to use ASE.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
[1] Low surrogate recovery was confirmed as a matrix effect by a second analysis.
[21 The surrogate recovery was above the QC recovery limit. The sample was not re -extracted since no target
analytes were detected in the sample.
[31 The sample was diluted to reduce matrix interference, resulting in elevated reporting limits.
[41 The surrogate recovery was outside QC acceptance limits due to matrix interference.
Date: 11/15/05
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCaRo
a —
Page: 14 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

� ace Analytical °
www.pacelabs.com
QC Batch: 139864
QC Batch Method: EPA 3510
Associated Lab Samples:
METHOD BLANK: 926321605
Associated Lab Samples:
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: 704.875, 9091
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
926293432 926293457 926293481
926293515
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828,254.7176
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
EPA 8270
Semivolatile Organics, TCLP
926293499 926293507
926293432 926293457 926293481 926293499 926293507 926293515
Parameter
Units
1,4-Dichlorobenzene
mg/l
2,4-Dinitrotoluene
mg/l
Hexachloro-1,3-butadiene
mg/l
Hexachlorobenzene
mg/l
Hexachloroethane
mg/l
2-Methylphenol (o-Cresol)
mg/l
3&4-Methylphenol
mg/l
Nitrobenzene
mg/l
Pentachlorophenol
mg/l
Pyridine
mg/l
2,4,5-Trichlorophenol
mg/l
2,4,6-Trichlorophenol
mg/l
Nitrobenzene-d5 (S)
%
2-Fluorobiphenyl (S)
i
Terphenyl-d14 (S)
i
Phenol-d5 (S)
2-Fluorophenol (S)
i
2,4,6-Tribromophenol (S)
2
LABORATORY CONTROL SAMPLE: 926208075
Blank
Result
Reporting
Limit Footnotes
NO
0.75
NO
0.013
ND
0.050
NO
0.013
NO
0.30
NO
0.050
NO
0.010
NO
0.20
NO
10.
NO
0.50
NO
40.
NO
0.20
64
56
75
25
37
82
Spike
LCS
LCS
Parameter
Units
Cone.
Result
a Rec
1,4-Dichlorobenzene
mg/l
0.2500
0.1315
53
2,4-Dinitrotoluene
mg/l
0.2500
0.1805
72
Hexachloro-1,3-butadiene
mg/l
0.2500
0.1185
47
Hexachlorobenzene
mg/l
0.2500
0.2089
84
Hexachloroethane
mg/l
0.2500
0.1142
46
2-Methylphenol (o-Cresol)
mg/l
0.2500
0.1621
65
Date: 11/15/05
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Fnnf-nnffnc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
O \11_ ACCOq�9
Page: 15 of 29
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Anal vtical o Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926208075
Spike
LCS
LCS
Parameter
Units
Conc.
Result
i Rec
3&4-Methylphenol
mg/l
0.2500
0.1535
61
Nitrobenzene
mg/l
0.2500
0.1831
73
Pentachlorophenol
mg/1
0,2500
0.2020
81
Pyridine
mg/l
0.2500
0.2111
84
2,4,5-Trichlorophenol
mg/1
0.2500
0.1970
79
2,4,6-Trichlorophenol
mg/1
0.2500
0.1878
75
Nitrobenzene-d5 (S)
78
2-Fluorobiphenyl (S)
77
Terphenyl-d14 (S)
81
Phenol-d5 (S)
28
2-Fluorophenol (S)
42
2,4,6-Tribromophenol (S)
89
LABORATORY CONTROL SAMPLE: 926267220
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec
1,4-Dichlorobenzene
mg/l
0.2500
0.0916
37
2,4-Dinitrotoluene
mg/l
0.2500
0.1683
67
Hexachloro-1,3-butadiene
mg/l
0.2500
0.0643
26
Hexachlorobenzene
mg/l
0.2500
0.1684
67
Hexachloroethane
mg/l
0.2500
0.0677
27
2-Methylphenol (o-Cresol)
mg/l
0.2500
0.1418
57
3&4-Methylphenol
mg/l
0.2500
0,1262
50
Nitrobenzene
mg/l
0.2500
0.1336
53
Pentachlorophenol
mg/l
0.2500
0.1869
75
Pyridine
mg/l
0.2500
0.0785
31
2,4,5-Trichlorophenol
mg/l
0.2500
0.1811
72
2,4,6-Trichlorophenol
mg/l
0.2500
0.1768
71
Nitrobenzene-d5 (S)
55
2-Fluorobiphenyl (S)
62
Terphenyl-d14 (S)
89
Phenol-d5 (S)
25
2-Fluorophenol (S)
34
2,4,6-Tribromophenol (S)
86
Date: 11/15/05
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Footnotes
Footnotes
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
Page: 16 of 29
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Nuntersville, NC 28078 Asheville, NC 28804
828.254.7176
:Analytical o Phone: Fax., 7004,875.9091 4.875.9092 Ph Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926290370
Spike
LCS
LCS
Parameter
Units
Conc.
Result
i Rec
1,4-Dichlorobenzene
mg/l
0.2500
0.0903
36
2,4-Dinitrotoluene
mg/l
0.2500
0.1485
59
Hexachloro-1,3-butadiene
mg/l
0.2500
0.0914
36
Hexachlorobenzene
mg/l
0.2500
0.1654
66
Hexachloroethane
mg/l
0.2500
0.0805
32
2-Methylphenol (o-Cresol)
mg/l
0.2500
0.1353
54
3&4-Methylphenol
mg/l
0.2500
0.1309
52
Nitrobenzene
mg/l
0.2500
0.1367
55
Pentachlorophenol
mg/l
0.2500
0.1581
63
Pyridine
mg/l
0.2500
0.1083
43
2,4,5-Trichlorophenol
mg/l
0.2500
0.1703
68
2,4,6-Trichlorophenol
mg/l
0.2500
0.1655
66
Nitrobenzene-d5 (S)
75.
2-Fluorobiphenyl (S)
75
Terphenyl-d14 (S)
80
Phenol-d5 (S)
37
2-Fluorophenol (S)
49
2,4,6-Tribromophenol (S)
97
LABORATORY CONTROL SAMPLE: 926321613
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y. Rec
1,4-Dichlorobenzene
mg/l
0.2500
0.0950
38
2,4-Dinitrotoluene
mg/l
0.2500
0.1561
62
Hexachloro-1,3-butadiene
mg/l
0.2500
0.0985
39
Hexachlorobenzene
mg/l
0.2500
0.1811
72
Hexachloroethane
mg/1
0.2500
0.0822
33
2-Methylphenol (o-Cresol)
mg/l
0.2500
0.1461
58
3&4-Methylphenol
mg/l
0.2500
0.1330
53
Nitrobenzene
mg/l
0.2500
0.1656
66
Pentachlorophenol
mg/l
0.2500
0.1829
73
Pyridine
mg/l
0.2500
0.0950
38
2,4,5-Trichlorophenol
mg/l
0.2500
0.1810
72
2,4,6-Trichlorophenol
mg/l
0.2500
0.1807
72
Nitrobenzene-d5 (S)
75
Date: 11/15/05
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Footnotes
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
AC 07'
� I �1i1�^i�•.£
Page: 17 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Anal vocal o Phone: [phone] Phone: [phone]
o. Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926321613
Parameter
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Spike LCS LCS
Units Conc. Result i Rec
66
79
30
41
82
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926208083 926208091
Parameter
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol (o-Cresol)
3&4-Methylphenol
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 11/15/05
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Footnotes
926195348
Spike
MS
MSD
MS
MSD
Units
Result
Conc,
Result
Result Y.
Rec %
Rec
RPD Footnotes
mg/l
0
0.2500
0.1059
0.1226
42
49
15
mg/l
0
0.2500
0.1725
0.1871
69
75
8
mg/l
0
0.2500
0.1015
0.1228
41
49
19
mg/l
0
0.2500
0.1975
0.2207
79
88
11
mg/l
0
0.2500
0.0888
0.1070
36
43
19
mg/l
0
0.2500
0.1495
0,1664
60
66
11
mg/l
0
0.2500
0.1471
0.1632
59
65
10
mg/l
0
0.2500
0.1624
0.1870
65
75
14
mg/l
0
0.2500
0.2026
0.2198
81
88
8
mg/l
0
0.2500
0.2319
0.2701
93
108
15
mg/l
0
0.2500
0.1967
0.2206
79
88
11
mg/l
0
0.2500
0.1815
0.2028
73
81
11
70
80
73
83
80
85
26
29
34
40
87
95
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACC.,,O
Page: 18 of 29
Charlotte Certification_ IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Anal vocal ° Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
QC Batch: 142540 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: Volatile Organics, TCLP Leach.
Associated Lab Samples: 926293432 926293457 926293481 926293515
METHOD BLANK: 926332131
Associated Lab Samples: 926293432 926293457 926293481 926293515
Parameter
Units
Benzene
mg/l
2-Butanone (MEK)
mg/l
Carbon tetrachloride
mg/l
Chlorobenzene
mg/l
Chloroform
mg/l
1,4-Dichlorobenzene
mg/l
1,2-Dichloroethane
mg/l
1,1-Dichloroethene
mg/l
Tetrachloroethene
mg/l
Tri chl oroethene
mg/l
Vinyl chloride
mg/l
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
LABORATORY CONTROL SAMPLE: 926332149
Parameter
Units
Benzene
mg/l
2-Butanone (MEK)
mg/l
Carbon tetrachloride
mg/l
Chlorobenzene
mg/l
Chloroform
mg/l
1,4-Dichlorobenzene
mg/l
1,2-Dichloroethane
mg/l
1,1-Dichloroethene
mg/l
Tetrachloroethene
mg/l
Trichloroethene
mg/l
Date: 11/15/05
Blank
Reporting
Result
Limit Footnotes
NO
0.0050
NO
0.10
ND
0.0050
ND
0.0050
ND
0.0050
ND
0.0050
NO
0.0050
NO
0.0050
NO
0.0050
ND
0.0050
ND
0.0050
98
95
116
111
Spike LCS LCS
Conc. Result % Rec Footnotes
0.0500 0.0459 92
0.1000 0.0888 89
0.0500 0.0477 95
0.0500 0.0490 98
0.0500 0.0507 101
0.0500 0.0459 92
0.0500 0.0485 97
0.0500 0.0501 100
0.0500 0.0469 94
0.0500 0.0474 95
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
37712 This report shall not be reproduced, except in full,
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
SC 99030
37712
FL NELAP E87648 N ^�C�R
4 0,..
Page: 19 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical o Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
LABORATORY CONTROL SAMPLE: 926332149
Spike LCS LCS
Parameter
Units Conc. Result % Rec Footnotes
Vinyl chloride
mg/l 0.0500 0.0422 84
Toluene-d8 (S)
96
4-Bromofluorobenzene (S)
102
Dibromofluoromethane (S)
105
1,2-Dichloroethane-d4 (S)
97
Date: 11/15/05
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712
37712
This report shall not be reproduced, except in full,
SC 99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
N AC�NRO
Page: 20 of 29
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical o Phone: [phone] Phone: [phone]
Fax., 704.875.9091 Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
QC Batch: 142704 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: Volatile Organics, TCLP Leach.
Associated Lab Samples: 926293499 926293507
METHOD BLANK: 926339250
Associated Lab Samples: 926293499 926293507
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Benzene
mg/l
NO
0.0050
2-Butanone (MEK)
mg/1
NO
0.10
Carbon tetrachloride
mg/l
NO
0.0050
Chlorobenzene
mg/l
NO
0.0050
Chloroform
mg/1
NO
0.0050
1,4-Dichlorobenzene
mg/l
NO
0.0050
1,2-Dichloroethane
mg/l
NO
0.0050
1,1-Dichloroethene
mg/1
NO
0.0050
Tetrachloroethene
mg/l
NO
0.0050
Trichloroethene
mg/l
NO
0.0050
Vinyl chloride
mg/l
NO
0.0050
Toluene-d8 (S)
Y.
99
4-Bromofluorobenzene (S)
i
96
Dibromofluoromethane (S)
%
104
1,2-Dichloroethane-d4 (S)
i
102
LABORATORY CONTROL SAMPLE: 926339268
Parameter
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Date: 11/15/05
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Sc 99030
FL NELAP E87648
Spike
LCS
LCS
Units
Conc.
Result
Y. Rec
mg/1
0.0500
0.0414
83
mg/l
0.1000
0.0749
75
mg/l
0.0500
0.0448
90
mg/l
0.0500
0.0425
85
mg/l
0.0500
0.0429
86
mg/l
0.0500
0.0439
88
mg/l
0.0500
0.0402
80
mg/l
0.0500
0.0471
94
mg/l
0.0500
0.0431
86
mg/l
0.0500
0.0439
88
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
„1 ACCOF
Page: 21 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

—.911111.
� ace Analytical °
www.pacelahs.com
LABORATORY CONTROL SAMPLE: 926339268
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Spike LCS LCS
Parameter Units
Conc. Result Y. Rec Footnotes
Vinyl chloride mg/l
0.0500 0.0367 73
Toluene-d8 (S)
99
4-Bromofluorobenzene (S)
100
Dibromofluoromethane (S)
95
1,2-Dichloroethane-d4 (S)
95
Date: 11/15/05
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
Sc 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACCpgO
Page: 22 of 29
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical � Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
QC Batch: 142371 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: Mercury, CVAAS, TCLP Leachate
Associated Lab Samples: 926293432 926293457 926293481 926293499 926293507
926293515
METHOD BLANK: 926326091
Associated Lab Samples: 926293432 926293457 926293481 926293499 926293507 926293515
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/l NO 0.0002
LABORATORY CONTROL SAMPLE: 926326109
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Mercury mg/l 0.0025 0.0028 111
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926326117 926326125
926293432 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Mercury mg/l 0.00022 0.0025 0.0065 0.0068 249 264 6 1,1
Date: 11/15/05
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
ry ACCOR
Page: 23 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
?Analytical o Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92106651
Client Project
ID: 2005
Process Waste Profile
QC Batch: 141714
Analysis Method: EPA 6010
QC Batch Method: EPA 3050
Analysis
Description: Metals, Trace ICP
Associated Lab Samples:
926293556
METHOD BLANK: 926295858
Associated Lab Samples:
926293556
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Arsenic
mg/kg
NO
0.50
Cadmium
mg/kg
NO
0.10
Chromium
mg/kg
NO
0.20
Lead
mg/kg
NO
0.50
LABORATORY CONTROL SAMPLE:
926295866
Spike
LCS LCS
Parameter
Units
Conc.
Result i Rec Footnotes
Arsenic
mg/kg
50.00
51.20 102
Cadmium
mg/kg
50.00
50.70 101
Chromium
mg/kg
50.00
51.00 102
Lead
mg/kg
50.00
51.20 102
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
926295874 926295882
926289729
Spike MS MSD
MS
MSD
Parameter
Units
Result
Conc. Result Result
% Rec Y.
Rec
RPD Footnotes
Arsenic
mg/kg
0.6911
60.29 61.61 59.89
101
102
3
Cadmium
mg/kg
0
60.29 61.25 59.89
102
103
2
Chromium
mg/kg
0.6588
60.29 62.58 61.28
103
105
2
Lead
mg/kg
6.365
60.29 68.97 66.26
104
103
4
SAMPLE DUPLICATE: 926295890
Parameter Units
Arsenic mg/kg
Date: 11/15/05
926289737 DUP
Result Result RPD Footnotes
3.700 4.300 13
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 37712 without the written consent of Pace Analytical Services, Inc.
99030
FL NELAP E87648 ApR
Page: 24 of 29
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
AnalyticalO Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
SAMPLE DUPLICATE: 926295890
Parameter
Cadmium
Chromium
Lead
Date: 11/15/05
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
926289737
DUP
Units
Result
Result
RPD
mg/kg
ND
ND
NC
mg/kg
7.500
8.500
13
mg/kg
48.00
43.00
11
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
PCCRR
Page: 25 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

lacmnalytical °
www.pacelabs.com
QC Batch: 142364
QC Batch Method: EPA 3010
Associated Lab Samples:
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
2225 Riverside Drive
Huntersville, NC 28078
Asheville, NC 28804
Phone: [phone]
Phone: 828,254.7176
Fax: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Analysis Method: EPA 6010
Analysis Description: Trace ICP Metals, TCLP Leach.
926293432 926293457 926293481 926293499 926293507
926293515
METHOD BLANK: 926325762
Associated Lab Samples: 926293432 926293457 926293481 926293499 926293507 926293515
Parameter
Units
Arsenic
mg/l
Barium
mg/l
Cadmium
mg/l
Chromium
mg/l
Lead
mg/l
Selenium
mg/l
Silver
mg/l
LABORATORY CONTROL SAMPLE: 926325770
Blank
Reporting
Result
Limit Footnotes
NO
0.025
ND
0.025
ND
0.0050
NO
0.010
ND
0.025
ND
0.025
NO
0.010
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Arsenic
mg/l
2.500
2.470
99
Barium
mg/l
2.500
2.535
101
Cadmium
mg/l
2.500
2.455
98
Chromium
mg/l
2.500
2.510
100
Lead
mg/l
2.500
2.480
99
Selenium
mg/l
2.500
2.490
100
Silver
mg/l
2.500
2.530
101
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926325788 926325796
926293432
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
% Rec %
Rec
RPD Footnotes
Arsenic
mg/l
0.02120
2.500
2.545
2.580
101
102
1
Barium
mg/l
1.475
2.500
4.150
3.995
107
101
4
Cadmium
mg/l
0
2.500
2.365
2.410
95
96
2
Chromium
mg/l
0.00294
2.500
2.410
2.450
96
98
2
Date: 11/15/05
Page: 26 of 29
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc
99030
without the written consent of Pace Analytical Services, Inc.
Sc
99006
FL NELAP
E87648
0 ;- -90
,� . " A°°°p
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical o Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
926325788 926325796
926293432 Spike
MS
MSD
MS
MSD
Parameter
Units
Result Conc.
Result
Result
% Rec %
Rec
RPD Footnotes
Lead
mg/l
0.02575 2.500
2.475
2.510
98
99
1
Selenium
mg/l
0.04540 2.500
2.625
2.670
103
105
2
Silver
mg/l
0.01225 2.500
2.550
2.575
102
102
1
Date: 11/15/05 Page: 27 of 29
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc
99030
without the written consent of Pace Analytical Services, Inc.
Sc
99006
FL NELAP
E87648
FL NELAP
E87627
Irveln^.�

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28076
llaceAnalyficafo Phone: [phone]
Fax: 704.875.909
www.pacelahs.com QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
QC Batch: 142034 Analysis Method: Y. Moisture
QC Batch Method: Analysis Description: Percent Moisture
Associated Lab Samples: 926293556
SAMPLE DUPLICATE: 926310483
926309154 DUP
Parameter Units Result Result RPD Footnotes
Percent Moisture o 12.30 12.50 1
Date: 11/15/05 Page: 28 of 29
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACFoRO
F
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.paceiabs.com
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828,252.4618
Lab Project Number: 92106651
Client Project ID: 2005 Process Waste Profile
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate i Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S) Surrogate
Ell The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
Date: 11/15/05
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
�N ACCON
o
Page: 29 of 29
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

PRECISION PETROLEUM LABS, INC.
5915 Star Lane Houston, TX. 77057
Ph.713-680-9425 Fax:[phone]
COMPANY:
INVOICE No.:
LAB REFERENCE No
PRODUCT ID:
DATE RECEIVED:
AUTHORIZED BY:
Reactive Cyanides, PPM
Reactive Sulfides, PPM
CERTIFICATE OF ANALYSIS
PACE ANALYTICAL
28212
2005-11-119
926293432 WWTP SLUDGE 11-02-2005
11-03-2005
LORRIPATTON
BDL = BELOW DETECTION LIMIT
TEST
METHOD
METHOD
DETECTION
LIMIT RESULTS
S.W.9010
0.01 BDL
S.W. 9030
1.0 BDL
PRECISION PETROLEUM LABS, INC.'S RESPONSIBILITY FOR THE ABOVE ANALYSIS,
OPINIONS OR INTERPRETATIONS IS LIMITED TO THE INVOICE AMOUNT.

y 1 �
PRECISION PETROLEUM LABS, INC.
5915 Star Lane Houston, TX. 77057
Ph.713-680-9425 Fax:[phone]
COMPANY:
INVOICE No.:
LAB REFERENCE No
PRODUCT ID:
DATE RECEIVED:
AUTHORIZED BY:
Reactive Cyanides, PPM
Reactive Sulfides, PPM
CERTIFICATE OF ANALYSIS
PACE ANALYTICAL
28212
2005-11-120
926293457 LIME MUD 11-02-2005
11-03-2005
LORRIPATTON
BDL = BELOW DETECTION LIMIT
TEST
METHOD
METHOD
DETECTION
LIMIT RESULTS
S.W.9010
0.01 BDL
S.W. 9030
1.0 BDL
PRECISION PETROLEUM LABS, INC.'s RESPONSIBILITY FOR THE ABOVE ANALYSIS,
OPINIONS OR INTERPRETATIONS IS LIMITED TO THE INVOICE AMOUNT.

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FACILIT4' COMPLIANGE A.VD►IT REPORT ,
NCDENRDivision of WasteManabement
.... .... . .......
Soled Wash Section
NORTH GROUNA DEPARTMENT OF
E.IRONMENTAND NATURAL RESOURCES ;
Date of Audit: 10/18/05 Date of Last Audit: 7/12/05
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
PO Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, NCDENR, Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active - Permit Amendment issued February 5, 2002
PURPOSE OF AUDIT:
Inspection of Industrial Landfill
NOTICE OF VIOLATION(S) (citation and explanation):
None
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such further
relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A

.. .._.................
FACILITY COMPLIANCE ALIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
OTHER COMMENTS /SUGGESTIONS:
(1) Areas that have settled in the inactive cells are being filled with soil.
(2) Eroded areas on slopes have been repaired and seeded. Grass looks good.
/�P ease contact me if you have any questions or concerns regarding this audit report.
1
Phone: [phone]
Regional Representative/)=VMS
Mailed on : 28 October 2005 by Hand delivery X US Mail Certified No. L j
Distribution: original signed copy to facility — signed coov to compliance officer — email or copv to supervisor
CC: Mark Poindexter, NCDENR, Division of Waste Management
Brent Rockett, NCDENR, Solid Waste Section

Ei
_ _ '��► FACILITYCOMPLI NCEAUDIT.REPORT
NCDENA'`� ® Division ofMaste 1VlanagemeA
R Solid Waste Section
NORTH C.AROLINA DEPARTMENT OF . ' .:
ENVIRONMENTANO NATURAL RESOURCES r W
IF
Date of Audit: 7/12/05 Date of Last Audit: 4/12/05
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
PO Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, NCDENR, Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active - Permit Amendment issued February 5, 2002
PURPOSE OF AUDIT:
Inspection of Industrial Landfill
(NOTICE OF VIOLATIONS) (citation and explanation):
None
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such further
relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A

Please contact me if you have any questions or concerns regarding this audit report.
C���`�_�/r•" Phone: [phone]
v Regional Representative/WiIIS
Mailed on : 19 July 2005 by Hand delivery X US Mail Certified No. Lj
Distribution: orieinal signed copy to facility — signed copy to compliance officer — email or copy to supervisor
CC: Mark Poindexter, NCDENR, Division of Waste Management
Brent Rockett, NCDENR, Solid Waste Section

E-13A
sK EL
NCDENR
NCRT CAROLINA DEPARTMENT OF
ENVIRONMENT ANO NATURAL RESOURCES
Date of Audit: 7/12/05 Date of Last Audit: 4/12/05
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
PO Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, NCDENR, Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active - Permit Amendment issued February 5, 2002
PURPOSE OF AUDIT:
Inspection of Industrial Landfill
NOTICE OF VIOLATIONS) (citation and explanation):
None
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such further
relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List atl noted last audit):
N/A

FACILITY COMPLIANCE AUDIT REPORT <
Division of Waste Management
Solid Waste `Section
Page 2 of 2
OTHER COMN ENTS /SUGGESTIONS:
(1) Add soil to the areas that have settled in the inactive cell south of the active area.
(2) Operation looks good.
Please contact me if you have any questions or concerns regarding this audit report.
cz&' Phone: [phone]
Regional RepresentativelTRIIS
Mailed on : 19 July 2005 by Hand delivery Y liS Mail Certified No. [_]
Distribution: original signed copy to facility — signed copy to compliance officer — email or copv to supervisor
CC: Mark Poindexter, NCDENR, Division of Waste Management
Brent Rockett, NCDENR, Solid Waste Section

NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
UNIT' TYPE:.
(check all that apply to this
audit with same Permit number
Lined
LCID
YW
Transfer
Compost
SLAS
COUNTY: HAYWOOD
MS WLF
PERMIT NO.: 44-06
Closed
HHW
White
Incin
T&P
FIRM
MSWLF
goods
FILE TYPE: "' COMPLIANCE
CDLF
TireT&P/
Tire
Industrial
X
DEMO
SDTF
Collection
Monofill
Landfill
.'
Date of Audit: 4/12/05
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc
PO Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, NCDENR, Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active - Permit Amendment issued February 5, 2002
PURPOSE OF AUDIT:
Inspection of Industrial Landfill
NOTICE OF VIOLATIONS) (citation and explanation):
None
Date of Last Audit: 1/27/05
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such further
relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
OTHER COMMENTS /SUGGESTIONS:
(1) Fertilizer and lime need to be applied to grass on landfill cap.
(2) The closed out unlined disposal area south of the active landfill has settled in areas causing impoundment of surface
water. The low areas need to be filled with soil, then seeded.
:;:
contact me if you have any questions or concerns regarding this audit report.
Phone: [phone]
Regional Representative/WMS
Mailed on: 15 April 2005 by Hand delivery X US Mail Certified No. L j
Distribution: original siened copv to facilitv — sinned copy to compliance officer — email or copy to supervisor
CC: Mark Poindexter, NCDENR, Division of Waste Management
Brent Rockett, NCDENR, Solid Waste Section

,�MAGJ*a
NCDENR
NORTH CAROIINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
UNITTYPE: (check all that_apply to this
audit with same Permit number)
Lined
LCID
YW
Transfer
Compost
SLAS
COUNTY: HAYWOOD
MSWLF
PERMIT NO.: 44-06
Closed
HHW
White
lncin
T&P
FIRM
MSWLF
goods
FILE TYPE: COMPLIANCE
CDLF
Tire UP /
Tire
Industrial
X
DEMO
SDTF
Collection
Monofill
Landfill
Date of Audit: 1/27/05
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc
PO Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, NCDENR, Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active - Permit Amendment issued February 5, 2002
PURPOSE OF AUDIT:
Inspection of Industrial Landfill
NOTICE OF VIOLATIONS) (citation and explanation):
None
Date of Last Audit: 11/3/04
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such further
relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
OTHER COMMENTS /SUGGESTIONS:
(1) Landfill looks good!
f
e contact me if you have any questions or concerns regarding this audit report.
+ Phone: 82S-296-4500
Regional Representative/WiLIS
Mailed on : 2 February 2005 by Hand delivery X US Mail Certified No. jI
Distribution: original shined copy to facility — signed copy to compliance officer — email or copy to supervisor
CC: Mark Poindexter, NCDENR, Division of Waste Management
Brent Rockett, NCDENR, Solid Waste Section