4406_ROSCANS_2004

ace Analytical °
www.pacelabs.com
November 24, 2004
Mr. Jim Giaque
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
RE: Lab Project Number: 9281250
Client Project ID: Process Material 2004
Dear Mr. Giaque:
III DEC 1 2004
BLUE RIDGE PAPER PRODUCTS INC
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828.252,4618
Enclosed are the analytical results for sample(s) received by the laboratory on November 10, 2004. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
If you have any questions concerning this report please feel free to contact me.
Since y,
Lor i Patton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 N p��ogo
SC Environmental 99030
FI NIRAP FRUAR
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
rl Kim nn r-ri,

Pace Analytical Services, Inc.
2225 Riverside Drive
Analytical o Asheville, NC 28804
Phone: 828,254.7176
www. pacelabs. com Fax: 828.252, 4618
Lab Project Number: 9281250
Client Project ID: Process Materi-al 2004
Solid results are reported on a dry weight basis
Lab Sample No: 924956410
Client Sample ID: WWTP SLUDGE
Parameters
Metals
Trace ICP Metals, TCLP Leach,
Date Digested
Project Sample Number: 9281250-001 Date Collected: 11/10/04 12:10
Matrix: Other Date Received: 11/10/04 16:14
Results Units Report Limit Analyzed By CAS No. Qua] RegLmt
Method: EPA 6010
11/12/04 04:30
11/12/04 04:30
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
0.037
mg/l
0.025
11/16/04
11:26
ALV
7440.38-2
Barium
0.78
mg/l
0.025
11/16/04
11:26
ALV
7440-39-3
Cadmium
NO
mg/l
0.0050
11/16/04
11:26
ALV
7440-43.9
Chromium
0.013
mg/l
0.010
11/16/04
11:26
ALV
7440-47-3
Lead
0.041
mg/l
0.025
11/16/04
11:26
ALV
7439.92-1
Selenium
0.035
mg/l
0.025
11/16/04
11:26
ALV
7782.49-2
Silver
1.9
mg/l
0,010
11/16/04
11:26
ALV
7440-22-4
Date Digested
11/15/04 01:30
11/15/04
01:30
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
ND
mg/l
0.00020
11/15/04
03:15
ALV
7439-97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
60.8
Y.
11/12/04
14:54
EDF
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510 /
EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
11/21/04
07:11
BET
106-46.7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/21/04
07:11
BET
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
11/21/04
07:11
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
11/21/04
07:11
BET
118-74-1
Hexachloroethane
ND
mg/1
0.30
11/21/04
07:11
BET
67-72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.050
11/21/04
07:11
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/21/04
07:11
BET
Nitrobenzene
ND
mg/l
0.20
11/21/04
07:11
BET
98-95-3
Pentachlorophenol
NO
mg/l
10.
11/21/04
07:11
BET
87-86-5
Pyridine
ND
mg/l
0.50
11/21/04
07:11
BET
110-86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
11/21/04
07:11
BET
95-95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
11/21/04
07:11
BET
88-06-2
Nitrobenzene-d5 (S)
58
%
11/21/04
07:11
BET
4165-60-0
2-Fluorobiphenyl (S)
67
%
11/21/04
07:11
BET
321.60-8
Terphenyl-d14 (S)
69
%
11/21/04
07:11
BET
1718-51-0
Date: 11/24/04
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI AIFI AD GA7FAA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACCp
�n`p�alr
Page: 1 of 30
Charlotte Certification IN
NC Wastewater
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NC Drinking Water
37706
SC
99006
M AIGI AD
GR7907

aceAnalytical °
www. pace/ahs. com
Lab Sample No: 924956410
Client Sample ID: WWTP SLUDGE
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Materi-al 2004
Project Sample Number: 9281250-001 Date Collected: 11/10/04 12:10
Matrix: Other Date Received: 11/10/04 16:14
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
Phenol-d5 (S)
20
%
11/21/04
07:11
BET
4165.62-2
2-Fluorophenol (S)
36
i
11/21/04
07:11
BET
367-12-4.
2,4,6-Tribromophenol (S)
94
Y.
11/21/04
07:11
BET
Date Extracted
11/16/04
11/16/04
GUMS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
NO
mg/l
0.0050
11/22/04
17:59
MSF
71-43-2
2-Butanone (MEK)
NO
mg/l
0.10
11/22/04
17:59
MSF
78-93-3
Carbon tetrachloride
NO
mg/l
0.0050
11/22/04
17:59
MSF
56-23-5
Chlorobenzene
NO
mg/l
0.0050
11/22/04
17:59
MSF
108-90-7
Chloroform
0.045
mg/l
0.0050
11/22/04
17:59
MSF
67-66.3
1,2-Dichloroethane
NO
mg/l
0.0050
11/22/04
17:59
MSF
107.06-2
1,1-Dichloroethene
NO
mg/l
0.0050
11/22/04
17:59
MSF
75-35.4
Tetrachloroethene
NO
mg/l
0.0050
11/22/04
17:59
MSF
127-18-4
Trichloroethene
0.014
mg/l
0.0050
11/22/04
17:59
MSF
79-01-6
Vinyl chloride
NO
mg/l
0.0050
11/22/04
17:59
MSF
75.01-4
Toluene-d8 (S)
82
i
11/22/04
17:59
MSF
2037-26-5
4-Bromofluorobenzene (S)
66
i
11/22/04
17:59
MSF
460-00-4 1
Dibromofluoromethane (S)
61
i
11/22/04
17:59
MSF
1868-53-7 1
1,2-Dichloroethane-d4 (S)
48
i
11/22/04
17:59
MSF
17060-07.0 1
Date: 11/24/04
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 N ACCpq
SC Environmental 99030
CI KIGI AD 1:R7FAR
Page: 2 of 30
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
CI KI CI AD
.C47r-n7

9
aceAnalytical°
www.pacelabs.com
Lab Sample No: 924956493
Client Sample ID: LIME MUD
Parameters
Metals
Trace ICP Metals, TCLP Leach.
Date Digested
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Materi-al 2004
Project Sample Number: 9281250.002 Date Collected: 11/10/04 12:32
Matrix: Other Date Received: 11/10/04 16:14
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Method: EPA 6010
11/16/04 06:30
11/16/04 06:30
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic'
ND
mg/l
0.025
11/23/04
17:12
ALV
7440-38-2
Barium
0.68
mg/l
0.025
11/23/04
17:12
ALV
7440-39-3
Cadmium
ND
mg/l
0.0050
11/23/04
17:12
ALV
7440-43-9
Chromium
NO
mg/l
0.010
11/23/04
17:12
ALV
7440-47-3
Lead
ND
mg/l
0.025
11/23/04
17:12
ALV
7439-92-1
Selenium
NO
mg/l
0.025
11/23/04
17:12
ALV
7782-49-2
Silver
NO
mg/l
0.010
11/23/04
17:12
ALV
7440-22-4
Date Digested
11/17/04 03:45
11/17/04
03:45
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
11/17/04
04:24
ALV
7439-97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
29.8
Y.
11/12/04
14:54
EDF
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
11/21/04
07:46
BET
106-46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/21/04
07:46
BET
121-14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
11/21/04
07:46
BET
87-68-3
Hexachlorobenzene
ND
mg/l
0.013
11/21/04
07:46
BET
118-74-1
Hexachloroethane
ND
mg/l
0.30
11/21/04
07:46
BET
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/l
0.050
11/21/04
07:46
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/21/04
07:46
BET
Nitrobenzene
ND
mg/l
0.20
11/21/04
07:46
BET
98-95-3
Pentachlorophenol
NO
mg/l
10.
11/21/04
07:46
BET
87-86-5
Pyridine
ND
mg/l
0.50
11/21/04
07:46
BET
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
11/21/04
07:46
BET
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
11/21/04
07:46
BET
88-06-2
Nitrobenzene-d5 (S)
52
Y.
11/21/04
07:46
BET
4165-60-0
2-Fluorobiphenyl (S)
62
Y.
11/21104
07:46
BET
321-60-8
Terphenyl-d14 (S)
78
Y.
11/21/04
07:46
BET
1718-51-0
Phenol-d5 (S)
21
%
11/21/04
07:46
BET
4165-62-2
Date: 11/24/04
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
GI AIGI AD
PA79AR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACCQ
Page: 3 of 30
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
CI AI CI AD .CQ7C77

aceAnalytical °
www.pacelabs.com
Lab Sample No: 924956493
Client Sample ID: LIME MUD
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Project Sample Number: 9281250-002 Date Collected: 11/10/04 12:32
Matrix: Other Date Received: 11/10/04 16:14
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
2-Fluorophenol (S) 42 % 11/21/04 07:46 BET 367-12-4
2,4,6-Tribromophenol (S) 94 % 11/21/04 07:46 BET
Date Extracted 11/16/04 11/16/04
GUMS Vol ati l es
Volatile' -Organics, TCLP Leach
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Date: 11/24/04
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
CI AICI AD
CQ762AQ
Method:
EPA 8260
NO
mg/l
0.0050
11/22/04
18:16
MSF
71-43-2
NO
mg/l
0.10
11/22/04
18:16
MSF
78-93-3
NO
mg/l
0.0050
11/22/04
18:16
MSF
56-23-5
ND
mg/l
0.0050
11/22/04
18:16
MSF
108.90-7
NO
mg/l
0.0050
11/22/04
18:16
MSF
67-66-3
ND
mg/l
0.0050
11/22/04
18:16
MSF
107-06-2
NO
mg/l
0.0050
11/22/04
18:16
MSF
75-35-4
ND
mg/l
0.0050
11/22/04
18:16
MSF
127.18-4
NO
mg/l
0.0050
11/22/04
18:16
MSF
79-01-6
ND
mg/l
0.0050
11/22/04
18:16
MSF
75-01-4
98
i
11/22/04
18:16
MSF
2037-26-5
89
%
11/22/04
18:16
MSF
460-00-4
0
i
11/22/04
18:16
MSF
1868-53-7
79
i
11/22/04
18:16
MSF
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCOH
1
Page: 4 of 30
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
CI RICI AD
C47CO7

Pace Analytical Services, Inc.
Analytical o
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254,7176
www.pacelabs.com
Fax., 828.252.4618
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Lab Sample No: 924956584 Project Sample Number: 9281250-003 Date Collected: 11/10/04 12:40
Client Sample ID: SLAKER GRITS Matrix: Other Date Received: 11/10/04 16:14
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/16/04 06:30 11/16/04 06:30
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic'
NO
mg/l
0.025
11/23/04
17:16
ALV
7440-38-2
Barium
0.48
mg/l
0.025
11/23/04
17:16
ALV
7440-39.3
Cadmium
NO
mg/l
0.0050
11/23/04
17:16
ALV
7440-43-9
Chromium
NO
mg/l
0.010
11/23/04
17:16
ALV
7440-47-3
Lead
NO
mg/l
0.025
11/23/04
17:16
ALV
7439-92-1
Selenium
0.033
mg/l
0.025
11/23/04
17:16
ALV
7782-49-2
Silver
NO
mg/l
0.010
11/23/04
17:16
ALV
7440-22-4
Date Digested
11/17/04 03:45
11/17/04
03:45
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
11/17/04
04:24
ALV
7439-97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
12.8
Y.
11/12/04
14:54
EDF
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
NO
mg/l
0.75
11/21/04
08:21
BET
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
11/21/04
08:21
BET
121-14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
11/21/04
08:21
BET
87.68-3
Hexachlorobenzene
ND
mg/l
0,013
11/21/04
08:21
BET
118-74-1
Hexachloroethane
ND
mg/l
0.30
11/21/04
08:21
BET
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/l
0.050
11/21/04
08:21
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/21/04
08:21
BET
Nitrobenzene
NO
mg/l
0.20
11/21/04
08:21
BET
98-95-3
Pentachlorophenol
ND
mg/l
10.
11/21/04
08:21
BET
87-86.5
Pyridine
ND
mg/l
0.50
11/21/04
08:21
BET
110-86-1.
2,4,5-Trichlorophenol
ND
mg/l
40.
11/21/04
08:21
BET
95.95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
11/21/04
08:21
BET
88-06.2
Nitrobenzene-d5 (S)
60
%
11/21/04
08:21
BET
4165-60-0
2-Fluorobiphenyl (S)
75
%
11/21/04
08:21
BET
321.60-8
Terphenyl-d14 (S)
83
%
11/21/04
08:21
BET
1718-51-0
Phenol-d5 (S)
25
Y.
11/21/04
08:21
BET
4165-62-2
Date: 11/24/04
Page: 5 of 30
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
N ���oR
NC Drinking Water
37706
SC Environmental 99030
r^ TT^^,`
Sc
99006
GI NGI AD P079AR
•�F-'lN�£.
CI KI CI AD
C07c77

ace Analytical °
www.pacelabs.com
Lab Sample No: 924956584
Client Sample ID: SLAKER GRITS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828,252.4618
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Project Sample Number: 9281250-003 Date Collected: 11/10/04 12:40
Matrix: Other Date Received: 11/10/04 16:14
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2-Fluorophenol (S)
51
Y.
11/21/04
08:21
BET
367-12-4
2,4,6-Tribromophenol (S)
108
Y.
11/21/04
08:21
BET
Date Extracted
11/16/04
11/16/04
GUMS Vol ati l es
Volatile"Organics, TCLP Leach.
Method: EPA
8260
Benzene
NO
mg/l
0.0050
11/22/04
18:34
MSF
71.43-2
2-Butanone (MEK)
NO
mg/l
0.10
11/22/04
18:34
MSF
78.93.3
Carbon tetrachloride
NO
mg/l
0.0050
11/22/04
18:34
MSF
56-23-5
Chlorobenzene
NO
mg/l
0.0050
11/22/04
18:34
MSF
108-90-7
Chloroform
NO
mg/l
0.0050
11/22/04
18:34
MSF
67-66.3
1,2-Dichloroethane
NO
mg/l
0.0050
11/22/04
18:34
MSF
107-06-2
1,1-Dichloroethene
NO
mg/l
0.0050
11/22/04
18:34
MSF
75-35-4
Tetrachloroethene
NO
mg/l
0.0050
11/22/04
18:34
MSF
127-18-4
Trichloroethene
ND
mg/l
0,0050
11/22/04
18:34
MSF
79-01.6
Vinyl chloride
NO
mg/l
0.0050
11/22/04
18:34
MSF
75-01.4
Toluene-d8 (S)
98
Y.
11/22/04
18:34
MSF
2037.26-5
4-Bromofluorobenzene (S)
94
i
11/22/04
18:34
MSF
460-00-4
Dibromofluoromethane (S)
0
i
11/22/04
18:34
MSF
1868-53-7 1
1,2-Dichloroethane-d4 (S)
79
i
11/22/04
18:34
MSF
17060-07-0
Date: 11/24/04
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FI RIM eD
GQ7RAQ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,N AC_Cp
A
W
Page: 6 of 30
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
CI NCI AD .007Gn7

ace Analytical
www.pacelahs.com
Lab Sample No: 924956618
Client Sample ID: PRECOAT FILTER DREGS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Matervi-al 2004
Project Sample Number: 9281250-004 Date Collected: 11/10/04 12:25
Matrix: Other Date Received: 11/10/04 16:14
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/16/04 06:30 11/16/04 06:30
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
NO
mg/l
0.025
11/23/04
17:21
ALV
7440-38-2
Barium
0.70
mg/l
0.025
11/23/04
17:21
ALV
7440.39-3
Cadmium
NO
mg/l
0,0050
11/23/04
17:21
ALV
7440-43-9
Chromium
NO
mg/l
0.010
11/23/04
17:21
ALV
7440.47-3
Lead
NO
mg/l
0.025
11/23/04
17:21
ALV
7439-92-1
Selenium
0.033
mg/l
0.025
11/23/04
17:21
ALV
7782.49-2
Silver
NO
mg/l
0,010
11/23/04
17:21
ALV
7440-22-4
Date Digested
11/17/04 03:45
11/17/04
03:45
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
11/17/04
04:24
ALV
7439-97.6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
55.8
i
11/12/04
14:55
EDF
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
NO
mg/l
0.75
11/21/04
08:56
BET
106-46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/21/04
08:56
BET
121-14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
11/21/04
08:56
BET
87.68-3
Hexachlorobenzene
NO
mg/l
0.013
11/21/04
08:56
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
11/21/04
08:56
BET
67.72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.050
11/21/04
08:56
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/21/04
08:56
BET
Nitrobenzene
NO
mg/l
0.20
11/21/04
08:56
BET
98.95-3
Pentachlorophenol
NO
mg/l
10.
11/21/04
08:56
BET
87-86-5
Pyridine
NO
mg/l
0.50
11/21/04
08:56
BET
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
11/21/04
08:56
BET
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
11/21/04
08:56
BET
88-06.2
Nitrobenzene-d5 (S)
53
%
11/21/04
08:56
BET
4165-60-0
2-Fluorobiphenyl (S)
66
Y.
11/21/04
08:56
BET
321-60-8
Terphenyl-d14 (S)
90
Y.
11/21/04
08:56
BET
1718-51-0
Phenol-d5 (S)
26
%
11/21/04
08:56
BET
4165-62-2
Date: 11/24/04
Page: 7 of 30
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
H R6Cpq
NC Drinking Water
37706
SC Environmental 99030
Sc
99006
FI AIFI AD P.Q7AAA
np �ril�"`£
P hirl AD
Gn7907

aceAnalytical °
www.pacelabs.com
Lab Sample No: 924956618
Client Sample ID: PRECOAT FILTER DREGS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Project Sample Number: 9281250.004 Date Collected: 11/10/04 12:25
Matrix: Other Date Received: 11/10/04 16:14
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.
Qual RegLmt
2-Fluorophenol (S)
46
%
11/21/04
08:56
BET
367-12-4
2,4,6-Tribromophenol (S)
108
%
11/21/04
08:56
BET
Date Extracted
11/16/04
11/16/04
GUMS Volatiles
Volatile"Organics, TCLP Leach.
Method: EPA
8260
Benzene
0.0097
mg/l
0.0050
11/22/04
18:51
MSF
71-43-2
2
2-Butanone (MEK)
NO
mg/l
0.10
11/22/04
18:51
MSF
78-93-3
Carbon tetrachloride
NO
mg/l
0.0050
11/22/04
18:51
MSF
56-23-5
Chlorobenzene
NO
mg/l
0.0050
11/22/04
18:51
MSF
108-90-7
Chloroform
ND
mg/l
0.0050
11/22/04
18:51
MSF
67-66-3
1,2-Dichloroethane
NO
mg/l
0.0050
11/22/04
18:51
MSF
107-06.2
1,1-Dichloroethene
NO
mg/l
0.0050
11/22/04
18:51
MSF
75-35-4
Tetrachloroethene
NO
mg/l
0.0050
11/22/04
18:51
MSF
127-18-4
Trichloroethene
0.062
mg/l
0.0050
11/22/04
18:51
MSF
79.01-6
2
Vinyl chloride
ND
mg/l
0.0050
11/22/04
18:51
MSF
75-01.4
Toluene-d8 (S)
95
%
11/22/04
18:51
MSF
2037.26.5
4-Bromofluorobenzene (S)
89
%
11/22/04
18:51
MSF
460-00.4
Dibromofluoromethane (S)
0
%
11/22/04
18:51
MSF
1868-53-7
1
1,2-Dichloroethane-d4 (S)
183
%
11/22/04
18:51
MSF
17060.07-0
3
Date: 11/24/04
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
SC Environmental 99030rl RIM AD rQ7PAQ
Page: 8 of 30
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
CI KILI Al)
GA7907

aceAnalytical °
www.pacelabs.com
Lab Sample No: 924956642
Client Sample ID: FLYASH
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Project Sample Number: 9281250-005 Date Collected: 11/10/04 13:05
Matrix: Other Date Received: 11/10/04 16:14
Parameters Results Units Report Limit Analyzed By CAS No. Qua] RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/16/04 06:30 11/16/04 06:30
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
0.82
mg/l
0.025
11/23/04
17:25
ALV
7440-38-2
Barium
0.24
mg/l
0.025
11/23/04
17:25
ALV
7440-39-3
Cadmium
ND
mg/l
0.0050
11/23/04
17:25
ALV
7440-43-9
Chromium
NO
mg/l
0.010
11/23/04
17:25
ALV
7440-47-3
Lead
ND
mg/l
0.025
11/23/04
17:25
ALV
7439-92-1
Selenium
0.086
mg/l
0.025
11/23/04
17:25
ALV
7782-49-2
Silver
NO
mg/l
0.010
11/23/04
17:25
ALV
7440-22-4
Date Digested
11/17/04 03:45
11/17/04
03:45
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
ND
mg/l
0.00020
11/17/04
04:24
ALV
7439-97-6
Wet Chemistry
Percent Moisture
Method: Y. Moisture
Percent Moisture
20.4
%
11/12/04
14:55
EDF
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
11/21/04
09:31
BET
106-46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
11/21/04
09:31
BET
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
11/21/04
09:31
BET
87-68-3
Hexachlorobenzene
ND
mg/l
0.013
11/21/04
09:31
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
11/21/04
09:31
BET
67-72-1
2-Methylphenol (o-Cresol)
NO
mg/]
0.050
11/21/04
09:31
BET
95-48-7
3&4-Methylphenol
ND
mg/l
0.010
11/21/04
09:31
BET
Nitrobenzene
ND
mg/l
0.20
11/21/04
09:31
BET
98-95-3
Pentachlorophenol
NO
mg/l
10.
11/21/04
09:31
BET
87-86-5
Pyridine
ND
mg/l
0.50
11/21/04
09:31
BET
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
11/21/04
09:31
BET
95.95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
11/21/04
09:31'BET
88-06-2
Nitrobenzene-d5 (S)
56
Y.
11/21/04
09:31
BET
4165-60-0
2-Fluorobiphenyl (S)
62
i
11/21/04
09:31
BET
321-60-8
Terphenyl-d14 (S)
60
%
11/21/04
09:31
BET
1718-51-0
Phenol-d5 (S)
16
Y.
11/21/04
09:31
BET
4165-62-2
Date: 11/24/04
Page: 9 of 30
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
N ACCOR
NC Drinking Water
37706
SC Environmental
99030
Sc
99006
CI ICI AD
C47FA4
/� /��/�1�
fnpin :�
C1 MCI AD
C07Cn7

ace Analytical °
www.pacelabs.com
Lab Sample No: 924956642
Client Sample ID: FLYASH
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828.252,4618
Lab Project Number: 9281250
Client Project ID: Process Mater-i-al 2004
Project Sample Number: 9281250-005 Date Collected: 11/10/04 13:05
Matrix: Other Date Received: 11/10/04 16:14
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
2-Fluorophenol (S) 27 Y. 11/21/04 09:31 BET 367-12-4
2,4,6-Tribromophenol (S) 86 % 11/21/04 09:31 BET
Date Extracted 11/16/04 11/16/04
GUMS Volatiles
Volatile Organics, TCLP Leach
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Date: 11/24/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI NIGI AP PA79AA
Method:
EPA 8260
NO
mg/l
0.0050
11/22/04
09:46
MSF
71.43.2
ND
mg/l
0.10
11/22/04
09:46
MSF
78.93.3
NO
mg/l
0.0050
11/22/04
09:46
MSF
56-23-5
ND
mg/l
0.0050
11/22/04
09:46
MSF
108-90-7
ND
mg/l
0.0050
11/22/04
09:46
MSF
67-66-3
NO
mg/l
0.0050
11/22/04
09:46
MSF
107-06-2
NO
mg/l
0.0050
11/22/04
09:46
MSF
75.35-4
NO
mg/l
0.0050
11/22/04
09:46
MSF
127-18-4
NO
mg/l
0.0050
11/22/04
09:46
MSF
79-01-6
NO
mg/l
0.0050
11/22/04
09:46
MSF
75.01-4
83
i
11/22/04
09:46
MSF
2037-26-5
104
i
11/22/04
09:46
MSF
460-00-4
0
i
11/22/04
09:46
MSF
1868-53-7 1
0
Y
11/22/04
09:46
MSF
17060-07-0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
0 ,N PCCpRO
Page: 10 of 30
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
CI KI CI AD C470,07

aceAnalytical
www.pacelabs.com
Lab Sample No: 924956667
Client Sample ID: CINDERS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828.252,4618
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Project Sample Number: 9281250-006 Date Collected: 11/10/04 13:25
Matrix: Other Date Received: 11/10/04 16:14
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 11/16/04 06:30 11/16/04 06:30
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
NO
mg/l
0.025
11/23/04
17:30
ALV
7440-38-2
Barium
0.36
mg/l
0.025
11/23/04
17:30
ALV
7440.39.3
Cadmium
NO
mg/l
0.0050
11/23/04
17:30
ALV
7440-43-9
Chromium
0.012
mg/l
0.010
11/23/04
17:30
ALV
7440-47-3
Lead
NO
mg/l
0.025
11/23/04
17:30
ALV
7439-92-1
Selenium
NO
mg/l
0.025
11/23/04
17:30
ALV
7782-49-2
Silver
NO
mg/l
0.010
11/23/04
17:30
ALV
7440.22.4
Date Digested
11/17/04 03:45
11/17/04
03:45
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
11/17/04
04:24
ALV
7439-97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
28.6
%
11/12/04
14:55
EDF
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
11/21/04
10:06
BET
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
11/21/04
10:06
BET
121.14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
11/21/04
10:06
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
11/21/04
10:06
BET
118-74-1
Hexachloroethane
ND
mg/l
0.30
11/21/04
10:06
BET
67-72-1
2-Methylphenol (o-Cresol)
NO
mg/1
0.050
11/21/04
10:06
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
11/21/04
10:06
BET
Nitrobenzene
ND
mg/l
0.20
11/21/04
10:06
BET
98.95-3
Pentachlorophenol
NO
mg/l
10.
11/21/04
10:06
BET
87.86-5
Pyridine
NO
mg/l
0.50
11/21/04
10:06
BET
110.86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
11/21/04
10:06
BET
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
11/21/04
10:06
BET
88.06-2
Nitrobenzene-d5 (S)
61
%
11/21/04
10:06
BET
4165.60-0
2-Fluorobiphenyl (S)
66
Y.
11/21104
10:06
BET
321-60-8
Terphenyl-d14 (S)
62
Y.
11/21/04
10:06
BET
1718-51-0
Phenol-d5 (S)
21
%
11/21/04
10:06
BET
4165-62-2
Date: 11/24/04
Page: 11 of 30
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
NC Drinking Water
37706
SC Environmental
99030
W;'`, a��°IF
Sc
99006
CI NCI AD
CR7RAQ
t¢';1 IP��I ,=.
CI KICI AD
207G77

aceAnalytical °
www.pacelabs.com
Lab Sample No: 924956667
Client Sample ID: CINDERS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828,254.7176
Fax [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Project Sample Number: 9281250-006 Date Collected: 11/10/04 13:25
Matrix: Other Date Received: 11/10/04 16:14
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
2-Fluorophenol (S) 40 Y. 11/21/04 10:06 BET 367-12-4
2,4,6-Tribromophenol (S) Ill % 11/21/04 10:06 BET
Date Extracted 11/16/04 11/16/04
GUMS Volatiles
Volatile Organics, TCLP Leach
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Date: 11/24/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Method: EPA
8260
0.033
mg/l
0.0050
11/22/04
10:04
MSF
71-43.2 2
ND
mg/l
0.10
11/22/04
10:04
MSF
78-93-3
NO
mg/l
0.0050
11/22/04
10:04
MSF
56-23.5
ND
mg/l
0.0050
11/22/04
10:04
MSF
108-90-7
0.013
mg/1
0.0050
11/22/04
10:04
MSF
67-66.3 2
NO
mg/l
0.0050
11/22/04
10:04
MSF
107-06-2
NO
mg/l
0.0050
11/22/04
10:04
MSF
75-35.4
0,0096
mg/l
0.0050
11/22/04
10:04
MSF
127-18-4 2
0.053
mg/l
0.0050
11/22/04
10:04
MSF
79-01-6 2
NO
mg/l
0.0050
11/22/04
10:04
MSF
75-01-4
64
%
11/22/04
10:04
MSF
2037.26-5 1
83
%
11/22/04
10:04
MSF
460-00-4
105
5.1
11/22/04
10:04
MSF
1868-53.7
56
%
11/22/04
10:04
MSF
17060.07-0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N �CCOA
�rto�'rMf
Page: 12 of 30
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC99006 1. ,r ^^ --

aceAnalytical
www.pacelabs.com
QC Batch: 114923
QC Batch Method: EPA 3510
Associated Lab Samples: 924956410
924956667
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
QUALITY CONTROL DATA Phone: Fax828.25
Fax- 828.252,42.4618
8
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Analysis Method: EPA 8270
Analysis Description: Semivolatile Organics, TCLP
924956493 924956584 924956618 924956642
METHOD BLANK: 924976418
Associated Lab Samples: 924956410 924956493 924956584 924956618 924956642 924956667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
1,4-Dichlorobenzene
mg/l
NO
0.75
2,4-Dinitrotoluene
mg/l
NO
0.013
Hexachloro-1,3-butadiene
mg/l
NO
0.050
Hexachlorobenzene
mg/l
ND
0.013
Hexachloroethane
mg/l
NO
0.30
2-Methylphenol (o-Cresol)
mg/l
NO
0.050
3&4- Methyl phenol
mg/l
NO
0.010
Nitrobenzene
mg/l
NO
0.20
Pentachlorophenol
mg/l
ND
10.
Pyridine
mg/l
NO
0.50
2,4,5-Trichlorophenol
mg/l
ND
40.
2,4,6-Trichlorophenol
mg/l
NO
0.20
Nitrobenzene-d5 (S)
%
58
2-Fluorobiphenyl (S)
Z
68
Terphenyl-d14 (S)
a
80
Phenol-d5 (S)
%
22
2-Fluorophenol (S)
i
45
2,4,6-Tribromophenol (S)
i
103
LABORATORY CONTROL SAMPLE: 924976426
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Z Rec Footnotes
1,4-Dichlorobenzene
mg/l
0.2500
0.1146
46
2,4-Dinitrotoluene
mg/l
0.2500
0.1973
79
Hexachloro-1,3-butadiene
mg/l
0.2500
0.1512
60
Hexachlorobenzene
mg/l
0.2500
0.2239
90
Hexachloroethane
mg/l
0.2500
0.0973
39
2-Methylphenol (o-Cresol)
mg/1
0.2500
0.0681
27
Date: 11/24/04
Asheville Certification IN
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
CI RICI AD
CQ7RAQ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
'N ACCpq
Page: 15 of 30
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
CI AICI AD C07C07

Pace Analytical Services, Inc.
aceAnalytical ® Asheville,
Riverside Drive
Asheville, NC 28804
www.pacelabs.com QUALITY CONTROL DATA Phone: Fax828.25
Fax: [phone]
4618
Lab Project Number: 9281250
Client Project ID: Process Material 2004
LABORATORY CONTROL SAMPLE: 924976426
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
3&4-Methylphenol
mg/l
0.2500
0.0611
24
Nitrobenzene
mg/l
0.2500
0.1219
49
Pentachlorophenol
mg/l
0.2500
0.2425
97
Pyridine
mg/l
0.2500
0.0425
17
2,4,5-Trichlorophenol
mg/l
0.2500
0.1577
63
2,4,6-Trichlorophenol
mg/l
0.2500
0.1616
65
Nitrobenzene-d5 (S)
56
2-Fluorobiphenyl (S)
70
Terphenyl-d14 (S)
85
Phenol-d5 (S)
16
2-Fluorophenol (S)
25
2,4,6-Tribromophenol (S)
106
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 924976434 924976442
924956410
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result %
Rec %
Rec
RPD Footnotes
1,4-Dichlorobenzene
mg/l
0
0.2500
0.1385
0.1333
55
53
4
2,4-Dinitrotoluene
mg/l
0
0.2500
0.2141
0.2070
86
83
3
Hexachloro-1,3-butadiene
mg/l
0
0.2500
0.1753
0.1696
70
68
3
Hexachlorobenzene
mg/l
0
0.2500
0.2314
0.2269
93
91
2
Hexachloroethane
mg/l
0
0.2500
0.1180
0.1184
47
47
0
2-Methylphenol (o-Cresol)
mg/l
0
0.2500
0.0813
0.0376
32
15
73 1
3&4-Methylphenol
mg/l
0
0.5000
0.0550
0.0328
11
7
51
Nitrobenzene
mg/l
0
0.2500
0.1402
0.1355
56
54
3
Pentachlorophenol
mg/l
0
0.2500
0.2817
0.2609
113
104
8
Pyridine
mg/l
0
0.2500
0.0780
0.0746
31
30
5
2,4,5-Trichlorophenol
mg/1
0
0.2500
0.2173
0.1649
87
66
27
2,4,6-Trichlorophenol
mg/l
0
0.2500
0.1959
0.1481
78
59
28
Nitrobenzene-d5 (S)
61
58
2-Fluorobiphenyl (S)
76
78
Terphenyl-d14 (S)
73
78
Phenol-d5 (S)
19
10
2-Fluorophenol (S)
29
14
2,4,6-Tribromophenol (S)
104
79
Date: 11/24/04 Page: 16 of 30
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
NC Drinking Water 37712 N ACCCq� NC Drinking Water 37706
l�'�t. CT q,,,
SC Environmental 99030 W �°F Sc 99006
'/ 4 r, •,r, nn rn-inn-.

Pace Analytical Services, Inc.
Analytical o Asheville,
ie,NCRiverside Drive
� Asheville, NC 28804
7176
www.pace►abs.com QUALITY CONTROL DATA Phone: Fax[phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
SAMPLE DUPLICATE: 924976459
Parameter
Units
1,4-Dichlorobenzene
mg/l
2,4-Dinitrotoluene
mg/l
Hexachloro-1,3-butadiene
mg/l
Hexachlorbbenzene
mg/l
Hexachloroethane
mg/l
2-Methylphenol (o-Cresol)
mg/l
3&4- Methyl phenol
mg/l
Nitrobenzene
mg/l
Pentachlorophenol
mg/l
Pyridine
mg/l
2,4,5-Trichlorophenol
mg/l
2,4,6-Trichlorophenol
mg/l
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
i
Terphenyl-d14 (S)
Z
Phenol-d5 (S)
i
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Y
Date: 11/24/04
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
n Ain An ro7ed0
924956493
DUP
Result
Result
RPD Footnotes
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
ND
ND
NC
52
55
62
64
78
82
21
21
42
39
94
96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N �CCOA
Page: 17 of 30
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
rn KIM An r07067

Pace Analytical Services, Inc.
Analytical0 Riverside Drive
� Ashe Asheville, NC 28804
7176
www.pacelahs.com QUALITY CONTROL DATA Phone:828.25
Fax:[phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
QC Batch: 115548
QC Batch Method: EPA 8260
Associated Lab Samples: 924956410
924956667
Analysis Method: EPA 8260
Analysis Description: Volatile Organics, TCLP Leach.
924956493 924956584 924956618 924956642
METHOD BLANK: 925007080
Associated Lab Samples: 924956410 924956493 924956584 924956618 924956642 924956667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Benzene
mg/l
NO
0.0050
2-Butanone (MEK)
mg/l
ND
0.10
Carbon tetrachloride
mg/l
ND
0.0050
Chlorobenzene
mg/l
NO
0.0050
Chloroform
mg/l
ND
0.0050
1,2-Dichloroethane
mg/l
ND
0.0050
1,1-Dichloroethene
mg/l
ND
0.0050
Tetrachloroethene
mg/l
NO
0.0050
Trichloroethene
mg/l
ND
0.0050
Vinyl chloride
mg/l
ND
0.0050
Toluene-d8 (S)
%
97
4-Bromofluorobenzene (S)
%
96
Dibromofluoromethane (S)
%
96
1,2-Dichloroethane-d4 (S)
%
93
LABORATORY CONTROL SAMPLE: 925007098
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Benzene
mg/l
0.0500
0.0493
99
2-Butanone (MEK)
mg/l
0.1000
0,0907
91
Carbon tetrachloride
mg/l
0.0500
0.0519
104
Chlorobenzene
mg/l
0.0500
0.0502
100
Chloroform
mg/l
0.0500
0.0503
101
1,2-Dichloroethane
mg/l
0.0500
0.0476
95
1,1-Dichloroethene
mg/l
0.0500
0.0525
105
Tetrachloroethene
mg/l
0.0500
0.0491
98
Trichloroethene
mg/l
0.0500
0.0486
97
Vinyl chloride
mg/l
0.0500
0.0528
106
Date: 11/24/04
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
CI RICI An 17070A0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
% !O
Page: 18 of 30
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
CI MCI An CO7067

Pace Analytical Services, Inc.
,Analytical ® Asheville,
Riverside Drive
] Asheville, NC 28804
www.pacelabs.com QUALITY CONTROL DATA Phone: Fax828.25
Fax: [phone]
4618
Lab Project Number: 9281250
Client Project ID: Process Material 2004
LABORATORY CONTROL SAMPLE: 925007098
Parameter Units
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Date: 11/24/04
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
ri eiri nn rn�reo
Spike LCS LCS
Conc. Result i Rec Footnotes
97
100
102
94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
e
Page: 19 of 30
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
rl IUrl An rn7 n,

Pace Analytical Services, Inc.
Analytical ® Asheville,
ill,, NC Drive
� Asheville, NC 28804
www.pacelabs.com QUALITY CONTROL DATA Phoneax.828.25828.252..4 18
Fax: 818
Lab Project Number: 9281250
Client Project ID: Process Material 2004
QC Batch: 114822 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: Mercury, CVAAS, TCLP Leachate
Associated Lab Samples: 924956410
METHOD BLANK: 924972649
Associated Lab Samples: 924956410
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/l NO 0.0002
LABORATORY CONTROL SAMPLE: 924972656
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Mercury mg/l 0.0025 0.0027 107
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 924972664 924972672
924957731 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Mercury mg/l 0 0.0025 0.0025 0.0025 99 102 3
Date: 11/24/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
CI AIM A❑ CO -MA 0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N RC�p
�iF'1A fir:£.
Page: 20 of 30
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
rI AI CI An
99006
Ca7r/17

Pace Analytical Services, Inc.
Analytical Riverside Drive
� Ashe Asheville, NC 28804
www.pacelabs.com QUALITY CONTROL DATA Phone: Fax[phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
QC Batch: 115008 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: Mercury, CVAAS, TCLP Leachate
Associated Lab Samples: 924956493 924956584 924956618 924956642 924956667
METHOD BLANK: 924979925
Associated Lab Samples: 924956493 924956584 924956618 924956642 924956667
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/l NO 0.0002
LABORATORY CONTROL SAMPLE: 924979933
Parameter
Mercury
Spike LCS LCS
Units Conc. Result Y Rec Footnotes
mg/l 0.0025 0.0026 102
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 924980451 924980469
924970742 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Mercury mg/l 0 0.0025 0.0026 0.0027 103 108 5
Date: 11/24/04
Page: 21 of 30
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
NC Drinking Water 37712 N ACCOgO NC Drinking Water 37706
SC Environmental 99030 Sc 99006

ace Analytical
www.pacelahs.com
QC Batch: 114715
QC Batch Method: EPA 3010
Associated Lab Samples: 924956410
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
7176
QUALITY CONTROL DATA Phone: Fax[phone]
Fax.' 828.252.4618
Lab Project Number: 9281250
Client Project ID: Process Material 2004
Analysis Method: EPA 6010
Analysis Description: Trace ICP Metals, TCLP Leach.
METHOD BLANK: 924966344
Associated Lab Samples:
924956410
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Arsenic
mg/l
NO
0.025
Barium
mg/l
NO
0.025
Cadmium
mg/l
ND
0.0050
Chromium
mg/l
NO
0.010
Lead
mg/l
NO
0.025
Selenium
mg/l
ND
0.025
Silver
mg/l
NO
0.010
LABORATORY CONTROL SAMPLE: 924966351
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Arsenic
mg/l
2.500
2.460
98
Barium
mg/l
2.500
2.475
99
Cadmium
mg/1
2.500
2.360
94
Chromium
mg/l
2.500
2.360
94
Lead
mg/l
2.500
2.385
95
Selenium
mg/l
2.500
2.425
97
Silver
mg/l
2.500
2.370
95
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 924966369 924966377
924956295
Parameter
Units
Result
Arsenic
mg/l
0.06100
Barium
mg/l
0.04510
Cadmium
mg/l
0.00050
Chromium
mg/l
0.05250
Lead
mg/l
0.03230
Date: 11/24/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030^
Spike
MS
MSD
MS
MSD
.
Conc.
Result
Result
% Rec %
Rec
RPD Footnotes
2.500
2.670
2.575
104
101
4
2.500
2.575
2.500
101
98
3
2.500
2.375
2.295
95
92
3
2.500
2.385
2.305
93
90
3
2.500
2.480
2.395
98
94
3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,
,N �CCCN
pqy
(Yti�J,
Page: 22 of 30
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006,

Pace Analytical Services, Inc.
2225 Riverside Drive
3Analytical ® Asheville, NC 28804
www.pacelabs.com QUALITY CONTROL DATA Phone: Fax[phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 924966369 924966377
924956295
Spike
MS
MSD
MS
MSD
Parameter Units Result
Conc.
Result
Result
% Rec %
Rec .RPD Footnotes
Selenium mg/l 0.05200
2.500
2.705
2.605
106
102 4
Silver mg/l 0.00131
2.500
2.475
2.390
99
96 3
SAMPLE DUPLICATE: 924966385
924956246
DUP
Parameter
Units
Result
Result
RPD Footnotes
Arsenic
mg/l
5.000
5.100
3
Barium
mg/l
0.04100
0.04200
4
Cadmium
mg/l
ND
ND
NC
Chromium
mg/l
ND
ND
NC
Lead
mg/l
ND
ND
NC
Selenium
mg/l
0.07600
0.08600
13
Silver
mg/l
ND
0.01200
0
Date: 11/24/04
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 o N Atgggo
SC Environmental 99030 /��,/`yF
CI hirl AD C07CA0 '�F�11d';f
Page: 23 of 30
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
r. r.." - --n'

Pace Analytical Services, Inc.
2225 Riverside Drive
:.)Analytical® Asheville, NC 28804
www.pacelabs.com QUALITY CONTROL DATA Phone::
Fax::828.252,4618.4618
4.7176
Lab Project Number: 9281250
Client Project ID: Process Material 2004
QC Batch: 115013
QC Batch Method: EPA 3010
Associated Lab Samples:
METHOD BLANK: 924980121
Associated Lab Samples:
Analysis Method: EPA 6010
Analysis Description: Trace ICP Metals, TCLP Leach.
924956493 924956584 924956618 924956642 924956667
924956493 924956584 924956618 924956642 924956667
Parameter
Units
Arsenic
mg/l
Barium
mg/l
Cadmium
mg/l
Chromium
mg/l
Lead
mg/l
Selenium
mg/l
Silver
mg/l
LABORATORY CONTROL SAMPLE: 924980139
Blank
Reporting
Result
Limit Footnotes
ND
0.025
ND
0.025
NO
0.0050
ND
0.010
NO
0.025
NO
0.025
ND
0.010
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Arsenic
mg/l
2.500
2.475
99
Barium
mg/l
2.500
2.605
104
Cadmium
mg/l
2.500
2.405
96
Chromium
mg/l
2.500
2.440
98
Lead
mg/l
2.500
2.440
98
Selenium
mg/l
2.500
2.440
98
Silver
mg/l
2.500
2.490
100
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 924980295 924980303
924970742
Spike
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
Arsenic
mg/l
0.02070
2.500
2.500
2.525
Barium
mg/l
0.04970
2.500
2.680
2.690
Cadmium
mg/l
0.00378
2.500
2.365
2.365
Chromium
mg/l
0.00300
2.500
2.415
2.395
Lead
mg/l
0.03090
2.500
2.475
2.470
Date: 11/24/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,N ACCON
MS MSD
Rec % Rec
RPD Footnotes
99 100
1
105 106
0
94 94
0
96 96
1
98 98
0
Page: 26 of 30
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006 1. .r ^^ ,

Pace Analytical Services, Inc.
2225 Riverside Drive
Analytical® Asheville, NC 28804
4.7176
www.pacelahs.com QUALITY CONTROL DATA Phone: Fax828.252,4618
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 924980295 924980303
924970742
Spike
MS
MSD
MS
MSD
Parameter Units
Result
Conc.
Result
Result
Y. Rec %
Rec RPD Footnotes
Selenium mg/l
0.02630
2.500
2.525
2.525
100
100 0
Silver mg/l
0.00500
2.500
2.555
2.565
102
102 0
Date: 11/24/04
Page: 27 of 30
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
NC Drinking Water 37712 N NC Drinking Water 37706
Rp
SC Environmental 99030 W°j`f~a` F Sc 99006

Pace Analytical Services, Inc.
2225 Riverside Drive
Analytical o Asheville, NC 28804
www.pace/abs.com Phone: [phone]
Fax: [phone]
Lab Project Number: 9281250
Client Project ID: Process Material 2004
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S) Surrogate
[1] RPD value was outside control limits, however both percent recoveries were acceptable. Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data.
[21 The calculated RPD was outside QC acceptance limits.
Date: 11/24/04
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
SC Environmental 99030
Page: 30 of 30
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006—

PRECISION PETROLEUM LABS, INC.
5915 Star Lane Houston, TX. 77057
Ph.713-680-9425 Fax:[phone]
CERTIFICATE OF AN.A.LYSIS
COMPANY: PACE ANALYTICAL
INVOICE No.: 25028
LAB REFERENCE No.: 2004-11-250 wig,? =7A41C
PRODUCT Ill: 924956410 PROJECT 9281250
DATE RECEIVED: 11-12-2004
AUTHORIZED BY: LORRI PATTON
TEST
METHOD
MET140D
DETECTION
LIMIT RESULTS
Reactive Cyanides, PPM S.W. 9010
0.01 BDL
Reactive Sulfides, PPM S.W. 9030
1.0 BDL
BDL ! BELOW DETECTION LIMIT
PRECISION PETROLEVU LAMS, INUS RESPONSIBILITY FOR THE ABOVE ANALYSIS,
OPINIONS OR INTERPRETATIONS 19 LINUTED TO THE INVOICE A,)IOUNT.

PRECISION PETROLEUM LABS, INC.
5915 Star Lane Houston, TX. 77057
Ph.713-680-9425 Fax:[phone]
COMPANY:
INVOICE No,:
LAB REFERENCE No.:
PRODUCT ID:
DATE RECEIVED:
AUTHORIZED BY:
Reactive Cyanides, PPM
Reactive Sulfides, PPM
CERTIFICATE OF ,ANALYSIS
PACE ANALYTICAL
25028
2004-11-251
924956493 PROJECT 9281250
11 - 12-2004
LORRIPATTON
TEST
METHOD
METHOD
DETECTION
LIMIT RESULTS
S.W.9010
0.01 BDL
S.W. 9030
1.0 BDL
BDL T BELOW DETECTION LIMIT
PRECISION PETROLEUM LAB$, ..N; US RESPONSIBILITY FOR THE ABOVE ANALYSIS,
OPiNIO\S OR INTERPRETATIONS [$ LIMITED TO THE IiN'VOIC=E AMOUNT.

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BLUE RIDGE
PAPER PRODUCTS INC.
January 5, 2004
Mr. James Patterson
North Carolina Department of Environment
And Natural Resources
59 Woodfin Place
Asheville, North Carolina 28801
Re: Chemical and physical analysis of Canton Mill process wastes.
Dear Mr. Patterson:
Attached is laboratory analysis related to the latest sampling of Canton Mill process
wastes, including wastewater treatment plant sludge, lime mud, slaker grits, precoat filter
dregs, boiler fly ash, and boiler cinders. The analysis is in accordance with Permit
Number 44-06, Area A East, and 15A NCAC 13B, Section .103(d).
Samples were collected on December 10, 2003. Each sample was analyzed by TCLP for
RCRA metals, volatile organics, and semi -volatile organics (excluding herbicides and
pesticides). In addition, the sludge and lime were tested for reactive cyanide and reactive
sulfide. No samples were found to be in excess of RCRA standards for the tested
parameters.
Please call me at 828-646-2028 if you have questions or comments.
Sincerely,
�L— J' Giauque 7
Attachments
Copy: Daryl Whitt
file:patterson010504.doc
175 Main Street • P.O. Box 4000
Canton, North Carolina 28716 • Phone: [phone]
Raising Your Expectations

aceAnalytical °
www.pacelabs.com
December 24, 2003
Mr. Jim Giaque
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
RE: Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Dear Mr. Giaque:
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Enclosed are the analytical results for sample(s) received by the laboratory on December 10, 2003. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
If you have any questions concerning this report please feel free to contact me.
Si nceye`ly.
.-�--•.,-fig, ) 3
,",torri Patton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 N ACCpgO
SC Environmental 99030
FL NELAP E87648 ne�c
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FI NPI AP
FR7A97

aceAnalytical °
www.pacelabs.com
Solid results are reported on a dry weight basis
Lab Sample No: 923619811
Client Sample ID: WWTP SLUDGE
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562-001 Date Collected: 12/10/03 09:50
Matrix: Other Date Received: 12/10/03 17:08
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 12/12/03 12/12/03
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
NO
mg/l
0.025
12/24/03
02:04
LBG
7440-38-2
Barium
1.1
mg/l
0.025
12/24/03
02:04
LBG
7440.39-3
Cadmium
NO
mg/l
0.0050
12/24/03
02:04
LBG
7440-43-9
Chromium
NO
mg/l
0.010
12/24/03
02:04
LBG
7440-47-3
Lead
NO
mg/l
0.015
12/24/03
02:04
LBG
7439-92-1
Selenium
NO
mg/l
0.025
12/24/03
02:04
LBG
7782.49-2
Silver
ND
mg/l
0.010
12/24/03
02:04
LBG
7440-22-4
Date Digested
12/17/03
12/17/03
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
12/17/03
LBG
7439.97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
68.2
%
12/12/03
15:26
EDF
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
12/19/03
18:46
BET
106-46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
12/19/03
18:46
BET
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
12/19/03
18:46
BET
87.68-3
Hexachlorobenzene
NO
mg/l
0.013
12/19/03
18:46
BET
118-74.1
Hexachloroethane
NO
mg/l
0.30
12/19/03
18:46
BET
67.72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.010
12/19/03
18:46
BET
95-48.7
3&4-Methylphenol
NO
mg/l
0.010
12/19/03
18:46
BET
Nitrobenzene
NO
mg/l
0.20
12/19/03
18:46
BET
98-95.3
Pentachlorophenol
NO
mg/l
10.
12/19/03
18:46
BET
87.86-5
Pyridine
ND
mg/l
0.50
12/19/03
18:46
BET
110-86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
12/19/03
18:46
BET
95-95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
12/19/03
18:46
BET
88-06.2
Nitrobenzene-d5 (S)
59
%
12/19/03
18:46
BET
4165-60-0
2-Fluorobiphenyl (S)
49
%
12/19/03
18:46
BET
321-60-8
Terphenyl-d14 (S)
60
%
12/19/03
18:46
BET
1718-51-0
Date: 12/24/03
Page: 1 of 28
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
\N. ACCpg04
NC Drinking Water
37706
SC Environmental
99030
E�
W ; Fa yF
Sc
99006
FI NFI AP
FR764R
'nPl r4
PI N191 AP
Gu7997

aceAnalytical °
www.pacelabs.com
Lab Sample No: 923619811
Client Sample ID: WWTP SLUDGE
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562.001 Date Collected: 12/10/03 09:50
Matrix: Other Date Received: 12/10/03 17:08
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.
Qual Re Lmt
Phenol-d5 (S)
23
%
12/19/03
18:46
BET
4165-62-2
2-Fluorophenol (S)
28
%
12/19/03
18:46
BET
367-12-4
2,4,6-Tribromophenol (S)
51
%
12/19/03
18:46
BET
Date Extracted
12/18/03
12/18/03
GUMS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
ND
mg/l
0.010
12/18/03
20:57
RWS
71-43-2
2-Butanone (MEK)
NO
mg/l
0.010
12/18/03
20:57
RWS
78.93-3
Carbon tetrachloride
NO
mg/l
0.010
12/18/03
20:57
RWS
56-23-5
Chlorobenzene
ND
mg/l
0.010
12/18/03
20:57
RWS
108-90-7
Chloroform
0.030
mg/l
0.010
12/18/03
20:57
RWS
67-66-3
1
1,2-Dichloroethane
NO
mg/l
0.010
12/18/03
20:57
RWS
107-06-2
1,1-Dichloroethene
ND
mg/l
0.010
12/18/03
20:57
RWS
75-35-4
Tetrachloroethene
NO
mg/l
0.010
12/18/03
20:57
RWS
127-18-4
Tri chl oroethene
ND
mg/l
0.010
12/18/03
20:57
RWS
79-01-6
Vinyl chloride
NO
mg/l
0.010
12/18/03
20:57
RWS
75.01-4
Toluene-d8 (S)
58
%
12/18/03
20:57
RWS
2037-26-5
2
4-Bromofluorobenzene (S)
39
%
12/18/03
20:57
RWS
460-00-4
2
Dibromofluoromethane (S)
152
%
12/18/03
20:57
RWS
1868-53-7
3
1,2-Dichloroethane-d4 (S)
113
%
12/18/03
20:57
RWS
17060.07-0
Date: 12/24/03
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI NPI AP FR7AAR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCOA
� nPI;Jr f
Page: 2 of 28
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
CI RIP[ AP
GQ7F')7

Pace Analytical Services, Inc.
2225 Riverside Drive
.,Analytical o Asheville, NC 28804
Phone: [phone]
www. pace/abs. cnm Fax. [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Lab Sample No: 923619829 Project Sample Number: 9255562-002 Date Collected: 12/10/03 10:00
Client Sample ID: LIME MUD Matrix: Other Date Received: 12/10/03 17:08
Parameters Results Units Report Limit _ Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 12/12/03 12/12/03
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
NO
mg/l
0.025
12/24/03 02:08 LBG
7440-38-2
Barium
0.45
mg/l
0.025
12/24/03
02:08 LBG
7440.39-3
Cadmium
NO
mg/l
0.0050
12/24/03
02:08 LBG
7440-43-9
Chromium
ND
mg/l
0.010
12/24/03
02:08 LBG
7440.47-3
Lead
ND
mg/l
0.015
12/24/03
02:08 LBG
7439.92-1
Selenium
NO
mg/l
0.025
12/24/03
02:08 LBG
7782-49-2
Silver
NO
mg/l
0.010
12/24/03
02:08 LBG
7440.22-4
Date Digested
12/17/03
12/17/03
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
12/17/03
LBG
7439.97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
40.9
%
12/12/03
15:27 EDF
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
12/19/03
19:17 BET
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
12/19/03
19:17 BET
121-14.2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
12/19/03
19:17 BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
12/19/03
19:17 BET
118-74-1
Hexachloroethane
ND
mg/l
0.30
12/19/03
19:17 BET
67-72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.010
12/19/03
19:17 BET
95.48-7
3&4-Methylphenol
NO
mg/l
0.010
12/19/03
19:17 BET
Nitrobenzene
NO
mg/l
0.20
12/19/03
19:17 BET
98.95-3
Pentachlorophenol
NO
mg/1
10.
12/19/03
19:17 BET
87-86.5
Pyridine
NO
mg/l
0.50
12/19/03
19:17 BET
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
12/19/03
19:17 BET
95.95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
12/19/03
19:17 BET
88-06.2
Nitrobenzene-d5 (S)
57
Y.
12/19/03
19:17 BET
4165-60-0
2-Fluorobiphenyl (S)
51
%
12/19/03
19:17 BET
321-60-8
Terphenyl-d14 (S)
68
2
12/19/03
19:17 BET
1718-51-0
Phenol-d5 (S)
25
%
12/19/03
19:17 BET
4165-62-2
Date: 12/24/03
Page: 3 of 28
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN
This report shall not be reproduced, except in full,
Charlotte Certification IDs
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
N AIF?
NC Drinking Water
37706
SC Environmental
99030
�' -R�'' F
Sc
99006
FL NELAP
F87648
`ne� C£
FI RIP1 AP
FR7F97

aceAnalytical °
www.pacelabs.com
Lab Sample No: 923619829
Client Sample ID: LIME MUD
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828.252, 4618
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562-002 Date Collected: 12/10/03 10:00
Matrix: Other Date Received: 12/10/03 17:08
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2-Fluorophenol (S)
31
i
12/19/03
19:17
BET
367-12-4
2,4,6-Tribromophenol (S)
58
i
12/19/03
19:17
BET
Date Extracted
12/18/03
12/18/03
GUMS Vol ati l es
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
ND
mg/l
0.010
12/18/03
21:14
RWS
71-43.2
2-Butanone (MEK)
NO
mg/l
0.010
12/18/03
21:14
RWS
78-93-3
Carbon tetrachloride
NO
mg/l
0.010
12/18/03
21:14
RWS
56-23-5
Chlorobenzene
NO
mg/l
0.010
12/18/03
21:14
RWS
108.90-7
Chloroform
NO
mg/l
0.010
12/18/03
21:14
RWS
67-66-3
1,2-Dichloroethane
ND
mg/l
0.010
12/18/03
21:14
RWS
107-06-2
1,1-Dichloroethene
ND
mg/l
0.010
12/18/03
21:14
RWS
75-35-4
Tetrachloroethene
NO
mg/l
0.010
12/18/03
21:14
RWS
127-18-4
Trichloroethene
NO
mg/l
0.010
12/18/03
21:14
RWS
79-01-6
Vinyl chloride
NO
mg/l
0.010
12/18/03
21:14
RWS
75-01-4
Toluene-d8 (S)
95
Y.
12/18/03
21:14
RWS
2037-26-5
4-Bromofluorobenzene (S)
86
i
12/18/03
21:14
RWS
460-00.4
Dibromofluoromethane (S)
0
i
12/18/03
21:14
RWS
1868.53-7 2
1,2-Dichloroethane-d4 (S)
70
%
12/18/03
21:14
RWS
17060-07-0 2
Date: 12/24/03
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 N ACCpgO
SC Environmental 99030
FI NIFI AP FR7AAR
Page: 4 of 28
Charlotte Certification IDs
NC Wastewater
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NC Drinking Water
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Sc
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FI NGI Op
PP7r)7

ace Analytical °
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Lab Sample No: 923619852
Client Sample ID: SLAKER GRITS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562.003 Date Collected: 12/10/03 10:15
Matrix: Other Date Received: 12/10/03 17:08
Parameters Results Units Report Limit Analyzed By CAS No. Qual Re Lmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 12/12/03 12/12/03
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
ND
mg/l
0.025
12/24/03
02:13 LBG
7440-38-2
Barium
0.41
mg/l
0.025
12/24/03
02:13
LBG
7440-39-3
Cadmium
ND
mg/l
0.0050
12/24/03
02:13
LBG
7440-43.9
Chromium
ND
mg/l
0.010
12/24/03
02:13
LBG
7440-47-3
Lead
NO
mg/l
0.015
12/24/03
02:13
LBG
7439-92-1
Selenium
ND
mg/l
0.025
12/24/03
02:13
LBG
7782-49-2
Silver
ND
mg/l
0.010
12/24/03
02:13
LBG
7440.22-4
Date Digested
12/17/03
12/17/03
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
ND
mg/l
0.00020
12/17/03
LBG
7439-97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
25.4
%
12/12/03
15:28
EDF
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
12/19/03
19:48
BET
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
12/19/03
19:48
BET
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
12/19/03
19:48
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
12/19/03
19:48
BET
118-74-1
Hexachloroethane
ND
mg/l
0.30
12/19/03
19:48
BET
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/l
0.010
12/19/03
19:48
BET
95-48-7
3&4-Methylphenol
ND
mg/l
0.010
12/19/03
19:48
BET
Nitrobenzene
ND
mg/l
0.20
12/19/03
19:48
BET
98-95-3
Pentachlorophenol
NO
mg/l
10.
12/19/03
19:48
BET
87.86-5
Pyridine
ND
mg/l
0.50
12/19/03
19:48
BET
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
12/19/03
19:48
BET
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
12/19/03
19:48
BET
88-06-2
Nitrobenzene-d5 (S)
52
%
12/19/03
19:48
BET
4165-60.0
2-Fluorobiphenyl (S)
45
%
12/19/03
19:48
BET
321-60-8
Terphenyl-d14 (S)
72
%
12/19/03
19:48
BET
1718.51-0
Phenol-d5 (S)
12
%
12/19/03
19:48
BET
4165-62.2
Date: 12/24/03
Page: 5 of 28
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
N A��oa
NC Drinking Water
37706
SC Environmental
FI NFI AP
99030
FR7R4R
� net c
SC
99006
FI RIP1 LAP
FR7R97

aceAnalytical °
www.pacelabs.com
Lab Sample No: 923619852
Client Sample ID: SLAKER GRITS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254,7176
Fax [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562-003 Date Collected: 12/10/03 10:15
Matrix: Other Date Received: 12/10/03 17:08
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.Qua] Re9Lmt
2-Fluorophenol (S)
13
%
12/19/03
19:48
BET
367-12-4
2,4,6-Tribromophenol (S)
51
%
12/19/03
19:48
BET
Date Extracted
12/18/03
12/18/03
GUMS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
NO
mg/l
0.010
12/18/03
21:30
RWS
71-43-2
2-Butanone (MEK)
ND
mg/l
0.010
12/18/03
21:30
RWS
78-93.3
Carbon tetrachloride
ND
mg/l
0.010
12/18/03
21:30
RWS
56-23-5
Chlorobenzene
NO
mg/l
0.010
12/18/03
21:30
RWS
108-90-7
Chloroform
NO
mg/l
0.010
12/18/03
21:30
RWS
67-66-3
1,2-Dichloroethane
NO
mg/l
0.010
12/18/03
21:30
RWS
107-06-2
1,1-Dichloroethene
NO
mg/l
0.010
12/18/03
21:30
RWS
75-35-4
Tetrachloroethene
NO
mg/l
0.010
12/18/03
21:30
RWS
127-18-4
Trichloroethene
NO
mg/l
0.010
12/18/03
21:30
RWS
79.01.6
Vinyl chloride
ND
mg/l
0.010
12/18/03
21:30
RWS
75-01-4
Toluene-d8 (S)
98
%
12/18/03
21:30
RWS
2037-26-5
4-Bromofluorobenzene (S)
92
%
12/18/03
21:30
RWS
460-00-4
Dibromofluoromethane (S)
0
%
12/18/03
21:30
RWS
1868-53-7 2
1,2-Dichloroethane-d4 (S)
76
Y.
12/18/03
21:30
RWS
17060-07-0 2
Date: 12/24/03
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI NIFI AP PR7AAR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 6 of 28
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
GI NFI AD
G97F')7

aceAnalytical °
www.paceiabs.com
Lab Sample No: 923619878
Client Sample ID: PRECOAT FILTER DREGS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562-004 Date Collected: 12/10/03 10:05
Matrix: Other Date Received: 12/10/03 17:08
Parameters Results Units Report Limit Analyzed By CAS No. Qual Reg
Lmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 12/12/03 12/12/03
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
NO
mg/l
0.025
12/24/03 02:17
LBG
7440-38-2
Barium
2.1
mg/l
0.025
12/24/03
02:17
LBG
7440-39-3
Cadmium
NO
mg/l
0.0050
12/24/03
02:17
LBG
7440-43.9
Chromium
NO
mg/l
0.010
12/24/03
02:17
LBG
7440-47-3
Lead
ND
mg/l
0.015
12/24/03
02:17
LBG
7439-92-1
Selenium
0.042
mg/l
0.025
12/24/03
02:17
LBG
7782-49-2
Silver
NO
mg/l
0.010
12/24/03
02:17
LBG
7440-22-4
Date Digested
12/17/03
12/17/03
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
ND
mg/l
0.00020
12/17/03
LBG
7439.97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
65.5
%
12/12/03
15:29
EDF
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
NO
mg/l
0.75
12/19/03
20:20
BET
106-46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
12/19/03
20:20
BET
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
12/19/03
20:20
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
12/19/03
20:20
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
12/19/03
20:20
BET
67.72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.010
12/19/03
20:20
BET
95-48.7
3&4-Methylphenol
NO
mg/l
0.010
12/19/03
20:20
BET
Nitrobenzene
NO
mg/l
0.20
12/19/03
20:20
BET
98-95.3
Pentachlorophenol
NO
mg/l
10,
12/19/03
20:20
BET
87.86-5
Pyridine
ND
mg/l
0.50
12/19/03
20:20
BET
110-86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
12/19/03
20:20
BET
95.95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
12/19/03
20:20
BET
88-06-2
Nitrobenzene-d5 (S)
64
Y.
12/19/03
20:20
BET
4165-60-0
2-Fluorobiphenyl (S)
61
Y.
12/19/03
20:20
BET
321.60-8
Terphenyl-d14 (S)
77
Y.
12/19/03
20:20
BET
1718-51-0
Phenol-d5 (S)
28
i
12/19/03
20:20
BET
4165-62-2
Date: 12/24/03
Page: 7 of 28
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater 12
NC Drinking Water
37712
N A��agO
NC Drinking Water 37706
SC Environmental
99030
Sc 99006
FI NFI AP
PA76AR
� nP��r,£
GI KIM AD GQ7r )7

aceAnalytical °
www.pacelabs.com
Lab Sample No: 923619878
Client Sample ID: PRECOAT FILTER DREGS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562-004 Date Collected: 12/10/03 10:05
Matrix: Other Date Received: 12/10/03 17:08
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.
Qual RegLmt
2-Fluorophenol (S)
35
Z
12/19/03
20:20
BET
367-12-4
2,4,6-Tribromophenol
(S)
53
i
12/19/03
20:20
BET
Date Extracted
12/18/03
12/18/03
GUMS Vol ati l es
Volatile Organics, TCLP
Leach.
Method: EPA
8260
Benzene
NO
mg/l
0.010
12/18/03
21:46
RWS
71-43-2
2-Butanone (MEK)
NO
mg/l
0.010
12/18/03
21:46
RWS
78.93-3
Carbon tetrachloride
NO
mg/l
0.010
12/18/03
21:46
RWS
56.23-5
Chlorobenzene
NO
mg/l
0.010
12/18/03
21:46
RWS
108-90.7
Chloroform
NO
mg/l
0.010
12/18/03
21:46
RWS
67-66-3
1,2-Dichloroethane
NO
mg/l
0.010
12/18/03
21:46
RWS
107-06-2
1,1-Dichloroethene
NO
mg/l
0.010
12/18/03
21:46
RWS
75-35-4
Tetrachloroethene
NO
mg/l
0.010
12/18/03
21:46
RWS
127-18-4
Trichloroethene
ND
mg/l
0.010
12/18/03
21:46
RWS
79-01-6
Vinyl chloride
NO
mg/l
0.010
12/18/03
21:46
RWS
75-01.4
Toluene-d8 (S)
51
Y.
12/18/03
21:46
RWS
2037-26.5
2
4-Bromofluorobenzene
(S)
0
%
12/18/03
21:46
RWS
460-00-4
2
Dibromofluoromethane
(S)
0
%
12/18/03
21:46
RWS
1868-53-7
2
1,2-Dichloroethane-d4
(S)
278
i
12/18/03
21:46
RWS
17060-07-0
3
Date: 12/24/03
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 „ ACCCR
SC Environmental 99030
Page: 8 of 28
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FI RIFI DP FR7F97
FL NELAP F876419

ace Analytical °
www.pacelabs.com
Lab Sample No: 923619886
Client Sample ID: FLY ASH
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562-005 Date Collected: 12/10/03 10:10
Matrix: Other Date Received: 12/10/03 17:08
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 12/12/03 12/12/03
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010 / EPA
6010
Arsenic
1.1
mg/l
0.025
12/24/03
02:22
LBG
7440-38-2
Barium
0.13
mg/l
0.025
12/24/03
02:22
LBG
7440-39-3
Cadmium
0.013
mg/l
0.0050
12/24/03
02:22
LBG
7440-43-9
Chromium
NO
mg/l
0.010
12/24/03
02:22
LBG
7440-47-3
Lead
NO
mg/l
0.015
12/24/03
02:22
LBG
7439.92-1
Selenium
0.044
mg/l
0.025
12/24/03
02:22
LBG
7782-49-2
Silver
NO
mg/l
0.010
12/24/03
02:22
LBG
7440-22-4
Date Digested
12/17/03
12/17/03
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
NO
mg/l
0.00020
12/17/03
LBG
7439-97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
25.2
Z
12/12/03
15:30
EDF
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510 / EPA
8270
1,4-Dichlorobenzene
NO
mg/l
0.75
12/19/03
20:52
BET
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
12/19/03
20:52
BET
121.14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
12/19/03
20:52
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
12/19/03
20:52
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
12/19/03
20:52
BET
67-72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.010
12/19/03
20:52
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
12/19/03
20:52
BET
Nitrobenzene
NO
mg/l
0.20
12/19/03
20:52
BET
98-95-3
Pentachlorophenol
NO
mg/l
10.
12/19/03
20:52
BET
87-86-5
Pyridine
NO
mg/l
0.50
12/19/03
20:52
BET
110-86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
12/19/03
20:52
BET
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
12/19/03
20:52
BET
88-06-2
Nitrobenzene-d5 (S)
69
i
12/19/03
20:52
BET
4165-60-0
2-Fluorobiphenyl (S)
63
i
12/19/03
20:52
BET
321-60.8
Terphenyl-d14 (S)
72
i
12/19/03
20:52
BET
1718-51-0
Phenol-d5 (S)
27
i
12/19/03
20:52
BET
4165-62-2
Date: 12/24/03
Page: 9 of 28
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
N ACCOH0
-
NC Drinking Water
37706
SC Environmental
99030
\ �� '...
99
n`e
Sc
99006
FI NIFI AP
FR7AAR
¢ r£
ri nirl AD
GP7r)7

aceAnalytical °
www.pacelahs.com
Lab Sample No: 923619886
Client Sample ID: FLY ASH
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562-005 Date Collected: 12/10/03 10:10
Matrix: Other Date Received: 12/10/03 17:08
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
2-Fluorophenol (S)
34
i
12/19/03
20:52
BET
367-12-4
2,4,6-Tribromophenol (S)
57
i
12/19/03
20:52
BET
Date Extracted
12/18/03
12/18/03
GUMS Vol ati l es
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
ND
mg/l
0.010
12/24/03
07:36
BCK
71-43.2
2-Butanone (MEK)
ND
mg/l
0.010
12/24/03
07:36
BCK
78-93-3
Carbon tetrachloride
NO
mg/l
0.010
12/24/03
07:36
BCK
56-23-5
Chlorobenzene
ND
mg/l
0.010
12/24/03
07:36
BCK
108-90-7
Chloroform
NO
mg/l
0.010
12/24/03
07:36
BCK
67-66-3
1,2-Dichloroethane
NO
mg/l
0.010
12/24/03
07:36
BCK
107-06-2
1,1-Dichloroethene
ND
mg/l
0.010
12/24/03
07:36
BCK
75-35-4
Tetrachloroethene
ND
mg/l
0.010
12/24/03
07:36
BCK
127-18-4
Trichloroethene
ND
mg/l
0.010
12/24/03
07:36
BCK
79-01-6
Vinyl chloride
NO
mg/l
0.010
12/24/03
07:36
BCK
75-01.4
Toluene-d8 (S)
104
i
12/24/03
07:36
BCK
2037.26-5
4-Bromofluorobenzene (S)
100
i
12/24/03
07:36
BCK
460-00-4
Dibromofluoromethane (S)
88
i
12/24/03
07:36
BCK
1868.53-7
1,2-Dichloroethane-d4 (S)
76
q
12/24/03
07:36
BCK
17060.07-0 2
Date: 12/24/03
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FI NFI AP
FR7A4R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
`�� \N AC�pRo9C
��r1re��cf
Page: 10 of 28
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FI NIP[ AP FR7R)7

Pace Analytical Services, Inc.
2225 Riverside Drive
?Analytical o Asheville, NC 28804
Phone: 828.254, 7176
www.pacelabs.com Fax [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Lab Sample No: 923619894 Project Sample Number: 9255562-006 Date Collected: 12/10/03 10:25
Client Sample ID: CINDERS Matrix: Other Date Received: 12/10/03 17:08
Parameters Results Units Report Limit Analyzed By CAS No. Qual Re9Lmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 12/12/03 12/12/03
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
NO
mg/l
0.025
12/24/03
02:26
LBG
7440-38-2
Barium
0.22
mg/l
0.025
12/24/03
02:26
LBG
7440.39-3
Cadmium
NO
mg/l
0.0050
12/24/03
02:26
LBG
7440-43-9
Chromium
NO
mg/l
0.010
12/24/03
02:26
LBG
7440-47-3
Lead
NO
mg/l
0.015
12/24/03
02:26
LBG
7439.92-1
Selenium
NO
mg/l
0.025
12/24/03
02:26
LBG
7782.49-2
Silver
NO
mg/l
0.010
12/24/03
02:26
LBG
7440.22-4
Date Digested
12/17/03
12/17/03
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Mercury
ND
mg/l
0.00020
12/17/03
LBG
7439.97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
39.0
%
12/12/03
15:31
EDF
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,4-Dichlorobenzene
NO
mg/l
0.75
12/19/03
21:23
BET
106-46-7
2,4-Dinitrotoluene
NO
mg/l
0.013
12/19/03
21:23
BET
121-14-2
Hexachloro-1,3-butadiene
NO
mg/l
0.050
12/19/03
21:23
BET
87-68.3
Hexachlorobenzene
NO
mg/l
0.013
12/19/03
21:23
BET
118-74-1
Hexachloroethane
ND
mg/l
0.30
12/19/03
21:23
BET
67.72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.010
12/19/03
21:23
BET
95-48-7
3&4-Methylphenol
ND
mg/l
0.010
12/19/03
21:23
BET
Nitrobenzene
NO
mg/l
0.20
12/19/03
21:23
BET
98-95.3
Pentachlorophenol
NO
mg/l
10.
12/19/03
21:23
BET
87.86-5
Pyridine
NO
mg/l
0.50
12/19/03
21:23
BET
110-86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
12/19/03
21:23
BET
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
12/19/03
21:23
BET
88-06.2
Nitrobenzene-d5 (S)
53
Y.
12/19/03
21:23
BET
4165.60-0
2-Fluorobiphenyl (S)
47
%
12/19/03
21:23
BET
321-60-8
Terphenyl-d14 (S)
75
%
12/19/03
21:23
BET
1718-51-0
Phenol-d5 (S)
20
%
12/19/03
21:23
BET
4165-62-2
Date: 12/24/03
Page: 11 of 28
REPORT OF LABORATORY ANALYSIS
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This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
.��oRo
NC Drinking Water
37706
SC Environmental 99030
Sc
99006
FL NELAP FR7A4.9
ne r_
FI AIFI AP
GQ7a)7

aceAnalytical °
www.pacelabs.com
Lab Sample No: 923619894
Client Sample ID: CINDERS
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828,254.7176
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Project Sample Number: 9255562-006 Date Collected: 12/10/03 10:25
Matrix: Other Date Received: 12/10/03 17:08
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.
Qual RegLmt
2-Fluorophenol (S)
28
%
12/19/03
21:23
BET
367-12-4
2,4,6-Tribromophenol
(S)
55
%
12/19/03
21:23
BET
Date Extracted
12/18/03
12/18/03
GUMS Vol ati l es
Volatile Organics, TCLP Leach.
Method: EPA
8260
Benzene
ND
mg/l
0.010
12/18/03
22:19
RWS
71-43-2
2-Butanone (MEK)
NO
mg/l
0.010
12/18/03
22:19
RWS
78-93-3
Carbon tetrachloride
ND
mg/l
0.010
12/18/03
22:19
RWS
56-23-5
Chlorobenzene
NO
mg/l
0.010
12/18/03
22:19
RWS
108-90-7
Chloroform
ND
mg/l
0.010
12/18/03
22:19
RWS
67-66.3
1,2-Dichloroethane
NO
mg/l
0.010
12/18/03
22:19
RWS
107-06-2
1,1-Dichloroethene
ND
mg/l
0.010
12/18/03
22:19
RWS
75.35-4
Tetrachloroethene
ND
mg/l
0.010
12/18/03
22:19
RWS
127-18-4
Trichloroethene
NO
mg/l
0.010
12/18/03
22:19
RWS
79.01.6
Vinyl chloride
ND
mg/l
0.010
12/18/03
22:19
RWS
75-01-4
Toluene-d8 (S)
66
i
12/18/03
22:19
RWS
2037-26-5
2
4-Bromofluorobenzene
(S)
25
%
12/18/03
22:19
RWS
460-00-4
2
Dibromofluoromethane
(S)
62
i
12/18/03
22:19
RWS
1868-53-7
2
1,2-Dichloroethane-d4
(S)
37
i
12/18/03
22:19
RWS
17060.07.0
2
Date: 12/24/03
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 N A��ogo
SC Environmental 99030
Page: 12 of 28
Charlotte Certification IN
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NC Drinking Water
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SC
99006
GI hirl AP
rP7r97
FI NIFI AP FURAR

Pace Analytical Services, Inc.
2225 Riverside Drive
3.Analytical o Asheville, NC 28804
Phone: 828.254,7176
www.pacelahs.com Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
PARAMETER FOOTNOTES
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
Ill The reported result may be biased high due to matrix interference with the internal standard. This was
confirmed by reanalysis of the sample.
[21 Low surrogate recovery was confirmed as a matrix effect by a second analysis.
[31 High surrogate recovery was confirmed as a matrix effect by a second analysis.
Date: 12/24/03
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
PI NFI AP FR7642
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N kC o,
Page: 14 of 29
Charlotte Certification IN
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37706
SC
99006
FI NIP[ lip
PA7R)7

ace Analytical °
www.pace►abs.com QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
QC Batch: 87389 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: Semivolatile Organics, TCLP
Associated Lab Samples: 923619811 923619829 923619852 923619878 923619886
923619894
METHOD BLANK: 923645717
Associated Lab Samples: 923619811 923619829 923619852 923619878 923619886 923619894
Parameter
Units
1,4-Dichlorobenzene
mg/l
2,4-Dinitrotoluene
mg/l
Hexachloro-1,3-butadiene
mg/l
Hexachlorobenzene
mg/l
Hexachloroethane
mg/l
2-Methylphenol (o-Cresol)
mg/l
3&4-Methylphenol
mg/l
Nitrobenzene
mg/l
Pentachlorophenol
mg/l
Pyridine
mg/l
2,4,5-Trichlorophenol
mg/l
2,4,6-Trichlorophenol
mg/l
Nitrobenzene-d5 (S)
%
2-Fluorobiphenyl (S)
i
Terphenyl-d14 (S)
i
Phenol-d5 (S)
i
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
i
LABORATORY CONTROL SAMPLE: 923639348
Blank
Reporting
Result
Limit Footnotes
ND
0.75
ND
0.013
NO
0.050
ND
0.013
ND
0.30
NO
0.010
ND
0.010
NO
0.20
ND
10.
NO
0.50
ND
40.
NO
0.20
58
51
72
21
29
54
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
1,4-Dichlorobenzene
mg/l
0.2500
0.1209
48
2,4-Dinitrotoluene
mg/l
0.2500
0.2152
86
Hexachloro-1,3-butadiene
mg/l
0.2500
0.1024
41
Hexachlorobenzene
mg/l
0.2500
0.2024
81
Hexachloroethane
mg/l
0.2500
0.1216
49
2-Methylphenol (o-Cresol)
mg/l
0.2500
0.1296
52
Date: 12/24/03
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
A NFI AP FR7649
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\ O N ACCpgO9 c
r� \
��nP�ac
Page: 15 of 28
Charlotte Certification IN
NC Wastewater 12
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Fi Kirl AP Gu7r97

aceAnalytical °
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 923639348
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y. Rec
3&4- Methyl phenol
mg/1
0.2500
0.1265
51
Nitrobenzene
mg/l
0.2500
0.1311
52
Pentachlorophenol
mg/l
0.2500
0.2541
102
Pyridine
mg/l
0.2500
0.0767
31
2,4,5-Trichlorophenol
mg/1
0.2500
0.1999
80
2,4,6-Trichlorophenol
mg/l
0.2500
0.1993
80
Nitrobenzene-d5 (S)
53
2-Fluorobiphenyl (S)
71
Terphenyl-d14 (S)
86
Phenol-d5 (S)
24
2-Fluorophenol (S)
32
2,4,6-Tribromophenol (S)
91
LABORATORY CONTROL SAMPLE: 923645725
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec
1,4-Dichlorobenzene
mg/l
0.2500
0.1254
50
2,4-Dinitrotoluene
mg/l
0.2500
0.1981
79
Hexachloro-1,3-butadiene
mg/l
0.2500
0.1106
44
Hexachlorobenzene
mg/l
0.2500
0.1847
74
Hexachloroethane
mg/l
0.2500
0.1243
50
2-Methylphenol (o-Cresol)
mg/l
0.2500
0.1386
55
3&4-Methylphenol
mg/l
0.2500
0.1356
54
Nitrobenzene
mg/l
0.2500
0.1559
62
Pentachlorophenol
mg/l
0.2500
0.2338
94
Pyridine
mg/l
0.2500
0.0970
39
2,4,5-Trichlorophenol
mg/l
0.2500
0.1788
72
2,4,6-Trichlorophenol
mg/l
0.2500
0.1859
74
Nitrobenzene-d5 (S)
61
2-Fluorobiphenyl (S)
65
Terphenyl-d14 (S)
80
Phenol-d5 (S)
27
2-Fluorophenol (S)
36
2,4,6-Tribromophenol (S)
80
Date: 12/24/03
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI AIFI AP FR71;dR
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828.252, 4618
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Footnotes
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,N ACCOR
Page: 16 of 28
Charlotte Certification IN
NC Wastewater 12
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SC 99006
FI AIFI OP rA7r)7

Pace Analytical Services, Inc.
2225 Riverside Drive
3Analytical o Asheville, NC 28804
Phone: [phone]
www.pace►ahs.com QUALITY CONTROL DATA Fax:[phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
MATRIX SPIKE: 923639355
923629661
Spike
MS
MS
Parameter
Units
Result
Conc.
Result i
Rec Footnotes
1,4-Dichlorobenzene
mg/l
0
0.2500
0.1441
58
2,4-Dinitrotoluene
mg/1
0
0.2500
0,2231
89
Hexachloro-1,3-butadiene
mg/l
0
0.2500
0.1201
48
Hexachlorobenzene
mg/l
0
0.2500
0.2076
83
Hexachloroethane
mg/l
0
0.2500
0.1423
57
2-Methylphenol (o-Cresol)
mg/l
0
0.2500
0.1432
57
3&4-Methylphenol
mg/l
0
0.5000
0.1333
27
Nitrobenzene
mg/l
0
0.2500
0.1371
55
Pentachlorophenol
mg/l
0
0.2500
0.3710
148 1
Pyridine
mg/l
0
0.2500
0.0811
32
2,4,5-Trichlorophenol
mg/l
0
0.2500
0.2150
86
2,4,6-Trichlorophenol
mg/l
0
0.2500
0.2155
86
Nitrobenzene-d5 (S)
56
2-Fluorobiphenyl (S)
70
Terphenyl-d14 (S)
86
Phenol-d5 (S)
27
2-Fluorophenol (S)
34
2,4,6-Tribromophenol (S)
102
Date: 12/24/03
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 0 \N. ACp0g0
SC Environmental 99030
FL NELAP F876419 ` nef c4
Page: 17 of 28
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FI NIPI AP
GR7A97

aceAnalytical °
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
QC Batch: 87812 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: Volatile Organics, TCLP Leach.
Associated Lab Samples: 923619811 923619829 923619852 923619878 923619894
METHOD BLANK: 923661326
Associated Lab Samples: 923619811 923619829 923619852 923619878 923619894
Parameter
Units
Benzene
mg/l
2-Butanone (MEK)
mg/l
Carbon tetrachloride
mg/l
Chlorobenzene
mg/l
Chloroform
mg/l
1,2-Dichloroethane
mg/l
1,1-Dichloroethene
mg/l
Tetrachloroethene
mg/l
Trichloroethene
mg/l
Vinyl chloride
mg/l
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
i
1,2-Dichloroethane-d4 (S)
i
LABORATORY CONTROL SAMPLE: 923661334
Blank
Reporting
Result
Limit Footnotes
ND
0.010
NO
0.010
NO
0.010
NO
0.010
NO
0.010
NO
0.010
ND
0.010
NO
0.010
NO
0.010
ND
0.010
102
95
94
105
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Benzene
mg/l
0.0500
0.0502
100
2-Butanone (MEK)
mg/l
0.1000
0.0819
82
Carbon tetrachloride
mg/l
0.0500
0.0426
85
Chlorobenzene
mg/l
0.0500
0.0467
93
Chloroform
mg/l
0.0500
0.0468
94
1,2-Dichloroethane
mg/l
0.0500
0.0513
103
1.1-Dichloroethene
mg/l
0.0500
0.0478
96
Tetrachloroethene
mg/l
0.0500
0.0451
90
Trichloroethene
mg/l
0.0500
0.0490
98
Vinyl chloride
mg/l
0.0500
0.0449
90
Toluene-d8 (S)
101
Date: 12/24/03
Asheville Certification IN
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
F1 NFL AP
FR7RAR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
„ ACCOR
Page: 18 of 28
Charlotte Certification IN
NC Wastewater 12
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SC 99006
ri AIM AD GR7a)7

aceAnalytical °
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 923661334
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828.252,4618
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Spike LCS LCS
Parameter Units Conc. Result Y. Rec Footnotes
4-Bromofluorobenzene (S) 93
Dibromofluoromethane (S) 91
1.2-Dichloroethane-d4 (S) 104
Date: 12/24/03
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI NIFI AP FA79AR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
�p ACCpq
Page: 19 of 28
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Gi K1r1 AP GQ7r07

aceAnalytical °
www.pacelahs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254,7176
Fax., 828.252, 4618
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
QC Batch: 87888 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: Volatile Organics, TCLP Leach.
Associated Lab Samples: 923619886
METHOD BLANK: 923666200
Associated Lab Samples: 923619886
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Benzene
mg/l
ND
0.010
2-Butanone (MEK)
mg/l
ND
0.010
Carbon tetrachloride
mg/l
ND
0.010
Chlorobenzene
mg/l
ND
0.010
Chloroform
mg/l
ND
0.010
1,2-Dichloroethane
mg/l
ND
0.010
1,1-Dichloroethene
mg/l
NO
0.010
Tetrachloroethene
mg/l
ND
0.010
Trichloroethene
mg/l
ND
0.010
Vinyl chloride
mg/l
ND
0.010
Toluene-d8 (S)
%
104
4-Bromofluorobenzene (S)
i
103
Dibromofluoromethane (S)
i
97
1,2-Dichloroethane-d4 (S)
Y.
88
LABORATORY CONTROL SAMPLE: 923666218
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Benzene
mg/l
0.0500
0.0466
93
2-Butanone (MEK)
mg/l
0.1000
0.1116
112
Carbon tetrachloride
mg/l
0.0500
0.0412
82
Chlorobenzene
mg/l
0.0500
0.0462
92
Chloroform
mg/l
0.0500
0.0423
85
1,2-Dichloroethane
mg/l
0.0500
0.0389
78
1,1-Dichloroethene
mg/l
0.0500
0.0463
93
Tetrachloroethene
mg/1
0.0500
0.0471
94
Trichloroethene
mg/l
0.0500
0.0451
90
Vinyl chloride
mg/l
0,0500
0.0456
91
Toluene-d8 (S)
107
Date: 12/24/03
Asheville Certification IN
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FI NFI AP
FR764R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
ACCpRO
,1' 44 C
n:e[Art
Page: 20 of 28
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FI NIP1 OP FR7r,97

aceAnalytical °
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 923666218
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Spike LCS LCS
Parameter Units Conc. Result Y. Rec Footnotes
4-Bromofluorobenzene (S) 105
Dibromofluoromethane (S) 101
1,2-Dichloroethane-d4 (S) 87
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 923666226 923666234
923636245
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result %
Rec %
Rec
RPD Footnotes
Benzene
mg/l
0
0.0500
0.0458
0.0485
92
97
6
2-Butanone (MEK)
mg/l
0
0.1000
0.1188
0.0950
119
95
22
Carbon tetrachloride
mg/l
0
0.0500
0.0357
0.0395
71
79
10
Chlorobenzene
mg/l
0
0.0500
0.0434
0.0465
87
93
7
Chloroform
mg/l
0
0.0500
0.0404
0.0421
81
84
4
1,2-Dichloroethane
mg/l
0
0.0500
0.0388
0.0392
78
78
1
1,1-Dichloroethene
mg/l
0
0.0500
0.0437
0.0505
87
101
14
Tetrachloroethene
mg/l
0
0.0500
0.0392
0.0443
78
89
12
Trichloroethene
mg/l
0
0.0500
0.0412
0.0450
82
90
9
Vinyl chloride
mg/l
0
0.0500
0.0425
0.0473
85
95
11
Toluene-d8 (S)
101
100
4-Bromofluorobenzene (S)
99
93
Dibromofluoromethane (S)
101
97
1,2-Dichloroethane-d4 (S)
92
94
Date: 12/24/03 Page: 21 of 28
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI NFI AP FR7RAR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\�O \11_AC�pgO9c
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
P1 NGI AP PP7a')7

aceAnalytical °
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 87381
QC Batch Method: EPA 7470
Associated Lab Samples: 923619811
923619894
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254, 7176
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Analysis Method: EPA 7470
Analysis Description: Mercury, CVAAS, TCLP Leachate
923619829 923619852 923619878 923619886
METHOD BLANK: 923639082
Associated Lab Samples: 923619811 923619829 923619852 923619878 923619886 923619894
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/l NO 0.0002
LABORATORY CONTROL SAMPLE: 923639090
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Mercury mg/l 0.0050 0.0049 98
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 923639108 923639116
923619852 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Mercury mg/l 0 0.0050 0.0041 0.0050 82 100 20
Date: 12/24/03
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI NIFI AP FR7F;AR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCCH
��O o4C
Page: 22 of 28
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
rl hirl AD
rP7F77

Pace Analytical Services, Inc.
2225 Riverside Drive
?Analytical o Asheville, NC 28804
Phone: [phone]
www.pacelabs.com QUALITY CONTROL DATA Fax, 828.252,4618
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
QC Batch: 87040 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: Metals, Trace ICP
Associated Lab Samples: 923619928
METHOD BLANK: 923625677
Associated Lab Samples: 923619928
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Arsenic
mg/kg
NO
0.50
Cadmium
mg/kg
ND
0.10
Chromium
mg/kg
NO
0.20
Lead
mg/kg
ND
0.50
LABORATORY CONTROL SAMPLE: 923625685
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Arsenic
mg/kg
50.00
49.10
98
Cadmium
mg/kg
50.00
48.30
97
Chromium
mg/kg
50.00
48.00
96
Lead
mg/kg
50.00
47.00
94
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 923625693 923625701
923620041
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
% Rec %
Rec
RPD Footnotes
Arsenic
mg/kg
3.979
55.42
56.31
53.29
94
92
6
Cadmium
mg/kg
0
55.42
47.66
46.25
86
87
3
Chromium
mg/kg
22.61
55.42
85.90
70.13
114
89
20
Lead
mg/kg
7.626
55.42
58.30
57.13
91
93
2
SAMPLE DUPLICATE: 923625719
923620066 DUP
Parameter Units Result Result RPD Footnotes
Arsenic mg/kg 2.800 3.700 28
Date: 12/24/03 Page: 23 of 28
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
N. ACCOR�9
NC Drinking Water
37706
SC Environmental
99030
to
t- :'ye
Sc
99006
FL NELAP
F87648
` ner c
R NIFI AP
GR7a)7

ace Analytical °
www.pacelabs.com
SAMPLE DUPLICATE: 923625719
Parameter
Units
Cadmium
mg/kg
Chromium
mg/kg
Lead
mg/kg
Date: 12/24/03
Asheville Certification IDs
NO Wastewater 40
NO Drinking Water 37712
SC Environmental 99030
FI NIFI AP FR7AAR
QUALITY CONTROL DATA
923620066 DUP
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Result
Result
RPD
ND
NO
NC
12.00
16.00
27
17.00
25.00
35
Footnotes
2
2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,1 AC�pgo
Page: 24 of 28
Charlotte Certification IDs
NO Wastewater 12
NO Drinking Water 37706
SC 99006
ri NIFI AP FAW97

aceAnalytical °
www.pacelahs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254, 7176
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
QC Batch: 87343 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: Trace ICP Metals, TCLP Leach.
Associated Lab Samples: 923619811 923619829 923619852 923619878 923619886
923619894
METHOD BLANK: 923636625
Associated Lab Samples: 923619811 923619829 923619852 923619878 923619886 923619894
Parameter
Units
Arsenic
mg/l
Barium
mg/l
Cadmium
mg/l
Chromium
mg/l
Lead
mg/l
Selenium
mg/l
Silver
mg/l
LABORATORY CONTROL SAMPLE: 923636633
Blank
Reporting
Result
Limit Footnotes
ND
0.025
ND
0.025
ND
0.0050
ND
0.010
ND
0.015
NO
0.025
ND
0.010
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Y. Rec Footnotes
Arsenic
mg/l
2.500
2.475
99
Barium
mg/l
2.500
2.560
102
Cadmium
mg/l
2.500
2.450
98
Chromium
mg/l
2.500
2.395
96
Lead
mg/l
2.500
2.445
98
Selenium
mg/l
2.500
2.445
98
Silver
mg/l
2.500
2.455
98
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 923636641 923636658
923619811
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
% Rec %
Rec
RPD Footnotes
Arsenic
mg/l
0
2.500
2.705
2.520
108
101
7
Barium
mg/l
1.095
2.500
3.810
3.520
109
97
8
Cadmium
mg/l
0
2.500
2.545
2.395
102
96
6
Chromium
mg/l
0
2.500
2.465
2.325
99
93
6
Date: 12/24/03
Page: 25 of 28
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IDs
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
,t L�ORp
NC Drinking Water
37706
SC Environmental 99030
��' '"
Sc
99006
FI NIR AP FR7RdR
`onP� 4
GI KIM AD
GQ7ao7

aceAnalytical °
www.pacelabs.com
QUALITY CONTROL DATA
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 923636641 923636658
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
923619811
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
% Rec %
Rec
RPD Footnotes
Lead
mg/l
0
2.500
2.540
2.405
102
96
5
Selenium
mg/l
0.02265
2.500
2.685
2.530
106
100
6
Silver
mg/l
0
2.500
2.595
2.460
104
98
5
Date: 12/24/03
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 A��oRo
SC Environmental 99030 E�` ip
FI NFI AP FR7R4R . `hplA '
Page: 26 of 28
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
ri NFI AP r:P7F')7

Analytical °
www.pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828,254.7176
Fax., 828.252.4618
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
QC Batch: 87106 Analysis Method: % Moisture
QC Batch Method: Analysis Description: Percent Moisture
Associated Lab Samples: 923619811 923619829 923619852 923619878 923619886
923619894 923619928
SAMPLE DUPLICATE: 923628283
Parameter Units
Percent Moisture %
Date: 12/24/03
Asheville_ Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI NIFI AP P97RAR
923626899 DUP
Result Result RPD Footnotes
24.30 24.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N PCCaq
nPhr4
Page: 27 of 28
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
ri IUGI AP
GR7R')7

aceAnalytical °
www.pacelabs.com
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9255562
Client Project ID: PROCESS MATERIALS 2003
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S) Surrogate
[1] Recovery falls outside of QC limits, however, this compound is not found in the associated samples.
[21 The calculated RPD was outside QC acceptance limits.
Date: 12/24/03
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
F87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\�� N_..A000AO4 c
°ne��c4
Page: 28 of 28
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
PI RIP[ AP FR7R97

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FACILITY ITS' COMPLIANCE AUDIT REPORT
NCDENR Division of Waste Management
Solid Waste Section
NORTH CAROLINA DEPARTMENT OF - - - -
ENVIRONMENT AND NATURAL RESOURCES - - - - - -
Date of Audit: 11/3/04
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
_FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
PO Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, NCDENR, Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active - Permit Amendment issued February 5, 2002
PURPOSE OF AUDIT:
Inspection of Industrial Landfill
NOTICE OF VIOLATIONS) (citation and explanation):
None
Date of Last Audit: 7/30/04
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such further
relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A

FACILITY COMPLIAN( 1, AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
OTHER COMMENTS /SUGGESTIONS:
(1) Erosion from recent storms has been repaired.
4act;Regional
ntme if you have any questions or concerns regarding this audit report.
IV —Phone: [phone]
Representative/WiVS
Mailed on : 5 November 2004 by Hand delivery X US Mail Certified No. Lj
Distribution: original signed copy to facility — signed copy to compliance officer — email or copy to supervisor
CC: Brent Rockett
DENR — Solid Waste Section
585 Waughtown Street
Winston-Salem, NC 27107
Mark Poindexter
Division of Waste Mgt.
Solid Waste Section
401 Oberlin Road
Raleigh, NC 27605

NCDENR
NORTH CAROUI DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
UNIT TYPE': (check all that apply to this
`audit with same Permit number
Lined
LCID
YW
Transfer
Compost
SLAS
COUNTY: HAYWOOD .
MSWLF
PERMIT NO.: 44-06
Closed
HHW
White
Incin
UP
FIRM
MSWLF
goods
.
FILE TYPE: COMPLIANCE
CDLF
Tire UP!
Tire
Industrial
X
DEMO
SDTF
Collection
Monofill
Landfill
-
Date of Audit: 7/30/04
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
PO Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, NCDENR, Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active - Permit Amendment issued February 5, 2002
PURPOSE OF AUDIT:
Inspection of Industrial Landfill
NOTICE OF VIOLATIONS) (citation and explanation):
None
Date of Last Audit: 4/27/04
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such further
relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
OTHER COMMENTS /SUGGESTIONS:
None
Please contact me if you have any questions or concerns regarding this audit report.
Phone: [phone]
Regional Representative/ S
Mailed on : 2 August 2004 by hand delivery X US Mail Certified No. j,j
Distribution: original signed copy to facili — signed copy to compliance officer — email or copy to supervisor
CC: Brent Rockett Mark Poindexter
DENR — Solid Waste Section Division of Waste Mgt.
585 Waughtown Street Solid Waste Section
Winston-Salem, NC 27107 401 Oberlin Road
Raleigh, NC 27605

AEa
NCDENR
NCRTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
UNIT TYPE: (check all that apply to this
audit with same Pen -nit number)
Lined
LCID
YW
Transfer
Compost
SLAS
COUNTY: HAYWOOD
�fSWLF
PERMIT NO.: 44-06
Closed
HHW
White
mein
T&1
FIRM
NISWLF
goods
FILE TYPE: COMPLIANCE
CDLF
Tire TIV e
Collection
Tire
Monofill
Industrial
Landfill
X
DEMO
SDTF
Date of Audit: 4/27/04
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
PO Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERINIIT:
Permit Amendment issued February 5, 2002
PURPOSE OF AUDIT:
Inspection of Industrial Landfill
F
None
Date of Last Audit: 1 /7/04
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such further
relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A

NCDENR
Noes- CAAOW . 00ft'" oor or
Ept e M Vcmo MMUM e. RftMm:C7
Date of Audit: 01/07/04
FACILITY COMPLIANCE AUDIT REPORT
Division of. Waste Management
Solid Waste Section
Date of Last Audit: 10/28/03
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
P.O. Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, N.C. Solid Waste Section
Jim Giauque and Daryl Whitt, Blue Ridge Paper
Products
STATUS OF PERMIT:
Permit amendment February 5, 2002.
PURPOSE OF AUDIT:
Inspection of industrial landfill.
NOTICE OF VIOLATIONS) (citation and explanation):
None
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such
further relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
OTHER COMMENTS /SUGGESTIONS:
0 Repair erosion on landfill slopes when weather permits.
Please contact me if you have any questions or concerns regarding this audit report.
G (signature) Phone: [phone].
Regional Representative
Distribution: original siLmed copy to facility -- signed copy to compliance officer — e-mail or copv to super
Delivered on : 01/08/04 by I I hand delivery I X I US Mail I I Certified No. lI
cc: Mark Poindexter
Brent Rockett