4406_ROSCANS_2002

Re
�•
BLUE RIDGE �a-
PAPER PRODUCTS INC.
January 4, 2002
Mr. James Patterson
North Carolina Department of Environment
And Natural Resources
852 Merriman Ave.
Asheville, North Carolina 28804
Re: Chemical and physical analysis of Canton Mill process wastes.
Dear Mr. Patterson:
Attached is laboratory analysis related to the latest sampling of Canton Mill process
wastes, including wastewater treatment plant sludge, lime mud, slaker grits, precoat filter
dregs, boiler fly ash, and boiler cinders. The analysis is in accordance with Permit
Number 44-06, Area A East, and 15A NCAC 13B, Section .103(d).
Samples were collected on November 6, 2001. Each sample was analyzed by TCLP for
RCRA metals, volatile organics, and semi volatile organics (excluding herbicides and
pesticides). In addition, the sludge and lime were tested for reactive cyanide and reactive
sulfide. No samples were found to be in excess of RCRA standards for the tested
parameters.
Please call me at 828-646-2028 if you have questions or comments.
Sincerely,
eez-,Z , 2
1m Giauque
Z
Attachments
Copy: Derric Brown
file:patterson010402.doc
175 Main Street • P.O. Box 4000
Canton, North Carolina 28716 • Phone: [phone]
Raising Your Expectations

ace Analytical m
www.pacelabs.com
November 30, 2001
Mr. Jim Giaque
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
RE: Lab Project Number: 9324726
Client Project ID: PROCESS WASTES
Dear Mr. Giaque:
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 6, 2001. Results reported
herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
t
Walter Miller
[e-mail]
Project Manager
Enclosures
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N All
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

aceAnalytical"A
www.pacelabs.com
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
Attn: Mr. Jim Giaque
Phone: [phone]
Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax. [phone]
Lab Project Number: 9324726
Client Project ID: PROCESS WASTES
Lab Sample No: 931036909 Project Sample Number: 9324726-001 Date Collected: 11/06/01 13:35
Client Sample ID: WWTP SLUDGE Matrix: Soil Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Reg Limit
Metals
RCRA Metals, ICP, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
ND
mg/l
0.50
11/20/01
09:12
TRW
7440-38-2
Barium
0.91
mg/l
0.10
11/20/01
09:12
TRW
7440-39-3
Cadmium
NO
mg/l
0.010
11/20/01
09:12
TRW
7440-43-9
Chromium
ND
mg/l
0.020
11/20/01
09:12
TRW
7440-47-3
Lead
ND
mg/l
0.10
11/20/01
09:12
TRW
7439.92-1
Selenium
ND
mg/l
0.10
11120101.09:12
TRW
7782-49-2
Silver
ND
mg/l
0.050
11/20/01
09:12
TRW
7440-22-4
Date Digested
11/20/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 1311 / EPA 7470
Date Digested 11/14/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 7470 / EPA 7470
Mercury ND mg/l .0.00020 11/21/01
Wet Chemistry
Percent Moisture Method: % Moisture
Percent Moisture 60.2 % 11/09/01
Date: 11/30/01
TRW 7439-97-6
AAB
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
`:�Co'4
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

aceAnalyticalm
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9324726
Client Project ID: PROCESS WASTES
Lab Sample No: 931036917 Project Sample Number: 9324726.002
Client Sample ID: LIME MUD Matrix: Soil
Parameters
Results
Units
Report Limit
Analyzed
Metals
RCRA Metals, ICP, TCLP Leach.
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
NO
mg/l
0.50
11/20/01
09:14
TRW
Barium
0.67
mg/l
0.10
11/20/01
09:14
TRW
Cadmium
ND
mg/l
0.010
11/20/01
09:14
TRW
Chromium
ND
mg/l
0.020
11/20/01
09:14
TRW
Lead
ND
mg/l
0.10
11/20/01
09:14
TRW
Selenium
NO
mg/l
0.10
11/20/01
09:14
TRW
Silver
NO
mg/l
0.050
11/20/01
09:14
TRW
Date Digested
11/20/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 1311 / EPA 7470
Date Digested 11/14/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 7470 / EPA 7470
Mercury ND mg/l 0.00020 11/21/01
Wet Chemistry
Percent Moisture
Percent Moisture
Date: 11/30/01
Method: % Moisture
34.3 %
11/09/61
Date Collected: 11/06/01 13:45
Date Received: 11/06/01 16:38
CAS No. Ftnote Reg Limit
7440-38-2
7440.39-3
7440-43.9
7440-47.3
7439.92-1
7782-49-2
7440-22-4
TRW 7439-97-6
AAB
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
�p ACC0*
Page: 2
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Analytical m Asheville, NC 28801
Phone: [phone]
www.pacelabs.com Fax: [phone]
Lab Project Number: 9324726
Client Project ID: PROCESS WASTES
Lab Sample No: 931036925 Project Sample Number: 9324726-003 Date Collected: 11/06/01 00:00
Client Sample ID: SLAKER GRITS Matrix: Soil Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Reg Limit
Metals
RCRA Metals, ICP, TCLP Leach.
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
ND
mg/1
0.50
11/20/01
09:16
TRW
7440-38-2
Barium
0.74
mg/l
0.10
11/20/01
09:16
TRW
7440-39-3
Cadmium
NO
mg/l
0.010
11/20/01
09:16
TRW
7440-43-9
Chromium
NO
mg/l
0.020
11/20/01
09:16
TRW
7440-47-3
Lead
NO
mg/l
0.10
11/20/01
09:16
TRW
7439-92.1
Selenium
NO
mg/l
0.10
11/20/01
09:16
TRW
7782-49.2
Silver
NO
mg/l
0.050
11/20/01
09:16
TRW
7440-22-4
Date Digested
11/20/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 1311 / EPA 7470
Date Digested 11/14/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 7470 / EPA 7470
Mercury NO mg/l 0.00020 11/21/01
Wet Chemistry
Percent Moisture Method: % Moisture
Percent Moisture 11.8 % 11/09/01
Date: 11/30/01
TRW 7439-97.6
AAB
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
,N �CCOB\
Page: 3
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

Pace Analytical Services, Inc.
54 Ravenscroft Drive
ace Analytical " Asheville, NC 28801
Phone: [phone]
www.pacelabs.com Fax., 828.254.4618
Lab Project Number: 9324726
Client Project ID: PROCESS WASTES
Lab Sample No: 931036933 Project Sample Number: 9324726.004 Date Collected: 11/06/01 13:54
Client Sample ID: PRECOAT FILTER DREGS Matrix: Soil Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Reg Limit
Metals
RCRA Metals, ICP, TCLP Leach.
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
ND
mg/l
0.50
11/20/01
09:18
TRW
7440-38-2
Barium
0.51
mg/l
0.10
11/20/01
09:18
TRW
7440-39-3
Cadmium
ND
mg/l
0.010
11/20/01
09:18
TRW
7440.43-9
Chromium
ND
mg/l
0.020
11/20/01
09:18
TRW
7440-47-3
Lead
ND
mg/l
0.10
11/20/01
09:18
TRW
7439-92-1
Selenium
ND
mg/l
0.10
11/20/01
09:18
TRW
7782-49-2
Silver
NO
mg/l
0.050
11/20/01
09:18
TRW
7440.22-4
Date Digested
11/20/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 1311 / EPA 7470
Date Digested 11/14/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 7470 / EPA 7470
Mercury NO mg/l 0.00020 11/21/01
Wet Chemistry
Percent Moisture Method: % Moisture
Percent Moisture 47.4 % 11/09/01
Date: 11/30/01
TRW 7439.97-6
AAB
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
,N ACCOA
W
F
Page: 4
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

Pace Analytical Services, Inc.
Analytical"' A Rshevilleille,, NC
Drive
� A28801
Phone: [phone]
www.pacelabs.com Fax: [phone]
Lab Project Number: 9324726
Client Project ID: PROCESS WASTES
Lab Sample No: 931036941 Project Sample Number: 9324726.005 Date Collected: 11/06/01 14:05
Client Sample ID: FLY ASH Matrix: Soil Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Reg Limit
Metals
RCRA Metals, ICP, TCLP Leach.
Prep/Method:
EPA 3010
/ EPA 6010
Arsenic
ND
mg/l
0.50
11/20/01
09:21
TRW
7440-38.2
Barium
0.22
mg/l
0.10
11/20/01
09:21
TRW
7440-39-3
Cadmium
0.042
mg/l
0.010
11/20/01
09:21
TRW
7440-43-9
Chromium
ND
mg/l
0.020
11/20/01
09:21
TRW
7440-47-3
Lead
ND
mg/l
0.10
11/20/01
09:21
TRW
7439-92-1
Selenium
ND
mg/l
0.10
11/20/01
09:21
TRW
7782-49-2
Silver
ND
mg/l
0.050
11/20/01
09:21
TRW
7440.22-4
Date Digested
11/20/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 1311 / EPA 7470
Date Digested 11/14/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 7470 / EPA 7470
Mercury NO mg/l 0.00020 11/21/01
Wet Chemistry
Percent Moisture Method: % Moisture
Percent Moisture 34.6 % 11/09/01
Date: 11/30/01
TRW 7439-97-6
AAB
Laborato[y Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
N ACCOR
Page: 5
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

Pace Analytical Services, Inc.
Analytical m A R , Drive
� Asheville, NC
28801
Phone: [phone]
www.pacelabs.com Fax: [phone]
Lab Project Number: 9324726
Client Project ID: PROCESS WASTES
Lab Sample No: 931036958 Project Sample Number: 9324726-006 Date Collected: 11/06/01 14:15
Client Sample ID: CINDERS Matrix: Soil Date Received: 11/06/01 16:38
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Metals
RCRA Metals, ICP, TCLP Leach. Prep/Method: EPA 3010 / EPA 6010
Arsenic ND mg/l 0.50
Barium 1.9 mg/l 0.10
Cadmium ND mg/l 0.010
Chromium ND mg/l 0.020
Lead NO mg/l 0.10
Selenium NO mg/l 0.10
Silver ND mg/l 0.050
Date Digested
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 1311 / EPA 7470
Date Digested
11/20/01 09:23 TRW 7440-38-2
11/20/01 09:23 TRW 7440-39-3
11/20/01 09:23 TRW 7440.43-9
11/20/01 09:23 TRW 7440-47.3
11/20/01 09:23 TRW 7439-92.1
11/20/01 09:23 TRW 7782-49-2
11/20/01 09:23 TRW 7440-22-4
11/20/01
11/14/01
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 7470 / EPA 7470
Mercury . ND mg/l 0.00020 11/21/01
Wet Chemistry
Percent Moisture Method: % Moisture
Percent Moisture 36.3 % 11/09/01
Date: 11/30/01
TRW 7439-97.6
AAB
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
N �CCOH
r � et
Page: 6
Laboratory Certification IN
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aceAnalyticalm
www.pacelabs.com
PARAMETER
ND Not Detected
NC Not Calculable
Date: 11/30/01
Laboratory Certification IN
NC Wastewater 40
NC Drinking Water 37712
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax. [phone]
Lab Project Number: 9324726
Client Project ID: PROCESS WASTES
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 7
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030
N ACCOA
4F� Off!'

aceAnalytical'"
www.pi3celabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Attn: Mr. Walt Miller
Phone: [phone]
Solid results are reported on a dry weight basis
Pace Analytical Services,. Inc.
900 Gemini Avenue
Houston, TX 77058
Phone: 281,486.1810
Far 281.488.4661
Lab Project Number: 8524299
Client Project ID: Reactives/9324726/Blue Ridge
Lab Sample No: 931036909 Project Sample Number: 8524299-001 Date Collected: 11/06/01 13:35
Client Sample ID: WWTP SLUDGE Matrix: Soil Date Received: 11/06/01 16:38
Parameters Results Unite Report Limit Analyzed CAS No. Ftnote Reg Limit
Wet Chemistry
Cyanide, Reactive Prep/Method: SW-846 7.3.3.2 / SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 0.496 11/12/01 15:30 BBRO 250
Sulfide, Reactive Prep/Method: SW-846 7.3.4.2 / SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 49.6 11/12/01 13:30 BFEB
Date: 11/12/01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
500

aceAna6tical-
www. pacelabscom
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, IX77058
Phone. [phone]
Fax., 281.486.4661
Lab Project Number: 8524299
Client Project ID: Reactives/9324726/Blue Ridge
Lab Sample No: 931036917 Project Sample Number: 8524299-002 Date Collected: 11/06/01 13:45
Client Sample ID: LIME MUD Matrix: Soil Date Received: 11/06/01 16:38
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Wet Chemistry
Cyanide, Reactive Prep/Method: SW-846 7.3.3.2 / SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 0.477 11/12/01 15:30 BBRO 250
Sulfide, Reactive Prep/Method: SW-846 7.3.4.2 / SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 47.7 11/12/01 13:30 HFEB
Date: 11/12/01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 2
500

aceAnaiytical ""
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PARAMETER FOOTNOTES
ND Not Detected
NC Not Calculable
Pace Analytical Services,, Inc.
900 Gemini Avenue
Houston, IX77058
Phone. [phone]
Fax: [phone]
Lab Project Number: 8524299
Client Project ID: Reactives/9324726/Blue Ridge
Date: 11/12/01 Page: 3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

aceAMIJI Cafm
www.pacefabs.com
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, IX77058
Phone: [phone]
Fax:[phone]
QUALITY CONTROL DATA
Lab Project Number: 8524299
Client Project ID: Reactives/9324726/Blue Ridge
QC Batch: 60306 Analysis Method: SW-846 7.3.4.2
QC Batch Method: SW-846 7.3.4.2 Analysis Description: Sulfide, Reactive
Associated Lab Samples: 931036909 931036917
METHOD BLANK: 851719756
Associated Lab Samples: 931036909 931036917
Blank Reporting
Parameter Units Result Limit Footnotes
Sulfide, Reactive mg/kg ND 50.0
LABORATORY CONTROL SAMPLE: 851719757
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Sulfide, Reactive mg/kg 350.7 100.0 28
SAMPLE DUPLICATE: 851719758
Parameter Units
Sulfide, Reactive mg/kg
Date: 11/12/01
851715873 DUP
Result Result M2 Footnotes
ND ND NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 4

aceAnalytical "
www.pacefabs.com
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, 1X 77056
Phone: [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number: 8524299
Client Project ID: Reactives/9324726/Blue Ridge
QC Batch: 60307 Analysis Method: SW-846 7.3.3.2
QC Batch Method: SW-846 7.3.3.2 Analysis Description: Cyanide, Reactive
Associated Lab Samples: 931036909 931036917
METHOD BLANK: 851719762
Associated Lab Samples: 931036909 931036917
Blank Reporting
Parameter Units Result Limit Footnotes
Cyanide, Reactive mg/kg ND 0.500
LABORATORY CONTROL SAMPLE: 851719764
Spike LCS LCS
Parameter IInits Cone, Result Rec Footnotes
Cyanide, Reactive mg/kg 19.4 18.05 93
SAMPLE DUPLICATE: 851719763
Parameter Units
Cyanide, Reactive mg/kg
Date: 11/12/01
851715873 DUP
Result Result RPPD Footnotes
ND ND NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 5

aceAnalytical '"
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QUALITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services,.lnc.
900 Gemini Avenue
Houston, TX 77058
Phone: [phone]
Fax:[phone]
Lab Project Number: 8524299
Client Project ID: Reactives/932472 6 /Blue Ridge
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
LCS (D) Laboratory Control Sample (Duplicate)
MS(D)Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not Detected
NC Not Calculable
RPD Relative Percent Difference
Date: 11/12/01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 6

Analytical'"
www P&Celabs rwm
Pace Analytical Services, Inc.
5d Ravenscroit Drive
Asheville, NC 28801
Attn: Ms. Beverly Grinstead
Phone: [phone]
Solid results are reported on a dry weight basis
Lab Sample No: 931036909
Client Sample ID: WWTP SLUDGE
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
HunISrsville, NC 28078
Phone: [phone]
Fax:[phone]
Lab Project Number: 9227569
Client Project ID: Blue Ridge Paper Prod. 9324726
Project Sample Number: 9227589-001 Date Collected: 11/06/01 13:35
Matrix: Other Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Rea Lim
Metals
volatile Organics, TCLP Leach.
Prep/Method:
EPA 1311
/ EPA 8260
Date Leached
0.00
1.0
11/15/01
CBE
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510
/ EPA 8270
1,d-Dichlorobenzens
ND
mg/l
0.75
1.0
11/21/01
01:17
CWA
106-d6-7
2,4-Dinitrotoluene
ND
mg/l
0.013
1.0
11/21/01
01:17
CWA
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
1.0
11/21/01
01:17
CWA
87-68-3
Hexachlorobenzene
ND
mg/l
0.013
1.0
11/21/01
01:17
CWA
118-74-1
Hexachloroethane
ND
mg/l
0.30
1.0
11/21/01
01:17
CWA
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/l
20.
1.0
11/21/01
01:17
CWA
95-18-7
3E4-Methylphenol
ND
mg/1
20.
1.0
11/21/01
01:17
CWA
Nitrobenzene
ND
mg/l
0.20
1.0
11/21/01
01:17
CWA
98-95-3
Pentachlorophenol
ND
mg/l
10.
1.0
11/21/01
01:17
CWA
87-86-5
Pyridine
ND
mg/l
0.50
1.0
11/21/01
01:17
CWA
110-86-1
2,d,5-Trichlorophenol
ND
mg/l
d0.
1.0
11/21/01
01:17
CWA
95-95-4
2,4,6-Trichlorophenol
ND
mg/1
0.20
1.0
11/21/01
01:17
CWA
88-06-2
Nitrobenzene-d5 (S)
77
%
1.0
11/21/01
01:17
CWA
4165-60-0
2-Fluorobiphenyl (S)
74
%
1.0
11/21/01
01:17
CWA
321-60-8
Terphenyl-d14 (S)
91
%
1.0
11/21/01
01:17
CWA
1718-51-0
Phenol-d6 (S)
43
%
1.0
11/21/01
01:17
CWA
13127-88-3
2-Fluorophenol (S)
56
%
1.0
11/21/01
01:17
CWA
367-12-4
2,4,6-Tribromophenol (S)
93
%
1.0
11/21/01
01:17
CWA
Date Extracted
11/17/01
GC/MS Volatiles
volatile Organics, TCLP Leach.
Prep/Method:
EPA 8260
/ EPA 8260
Benzene
ND
mg/l
0.020
1.0
11/19/01
20:40
RPJ
71-43-2
2-Butanone (MER)
ND
mg/l
0.40
1.0
11/19/01
20:d0
RPJ
78-93-3
Date, 11/21/01
Page: 1
Laboratory Certification IN Laboratory Certification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Analytical w
www..Pacelabs com
Lab Sample No: 931036909
Client Sample ID: WWTP SLUDGE
Parameters
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethane
Tetrachloroethene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Date: 11/21/01
Laboratocy Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
fax:[phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Project Sample Number: 9227589-001 Date Collected: 11/06/01 13:35
Matrix: Other Date Received: 11/06/01 16:38
Results
units
Report Limit
Dilution Analyzed
CAS No. Ftnote Rea Lim
ND
mg/1
0.020
1.0
11/19/01
20:40
RPJ
56-23-5
ND
mg/1
0.020
1.0
11/19/01
20:40
RPJ
108-90-7
ND
mg/1
0.020
1.0
11/19/01
20:40
RPJ
67-66-3
ND
mg/1
0.020
1.0
11/19/01
20:40
RPJ
107-06-2
ND
mg/1
0.020
1.0
11/19/01
20:40
RPJ
75-35-4
ND
mg/1
0.020
1.0
11/19/01
20:40
RPJ
127-18-4
ND
mg/1
0.020
1.0
11/19/01
20:40
RPJ
79-01-6
ND
mg/1
0.020
1.0
11/19/01
20:40
RPJ
75-01-4
98
%
1.0
11/19/01
20:40
RPJ
2037-26-5
91
%
1.0
11/19/01
20:40
RPJ
460-00-4
106
%
1.0
11/19/01
20:40
RPJ
115
%
1.0
11/19/01
20:40
RPJ
17060-07-0
Page: 2
REPORT OF LABORATORY ANALYSIS KYLaboratory Certification IDs
Drinking Water 90090
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Analytical"'
wvnv pacelabs.Com
Lab Sample No: 931036917
Client Sample ID: LIME MUD
Parameters
Metals
Volatile Organics, TCLP Leach
Date Leached
Pace Analytical Services, Inc.
9800 Kincey Avenue, Sulte 100
Huntersville, NC 28078
Phone: [phone]
fax: [phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Project Sample Number: 9227589-002 Date Collected: 11/06/01 13:45
Matrix: Other Date Received: 11/06/01 16:38
Results Units Report Limit Dilution Analyzed CAS No. Ftnots Rea Lim
Prep/Method: EPA 1311 / EPA 8260
0.00 1.0 11/15/01 CBE
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510 /
EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
1.0
11/21/01
01:53
CWA
106-46-7
2,4-Dinitrotoluens
ND
mg/1
0.013
1.0
11/21/01
01:53
CWA
121-14-2
Mexachloro-1,3-butadiene
ND
mg/1
0.050
1.0
11/21/01
01:53
CWA
87-68-3
Bexachlorobenzene
ND
mg/l
0.013
1.0
11/21/01
01:53
CWA
118-74-1
Bexachloroethane
ND
mg/l
0.30
1.0
11/21/01
01:53
CWA
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/1
20.
1.0
11/21/01
01:53
CWA
95-48-7
394-Methylphenol
ND
mg/1
20.
1.0
11/21/01
01:53
CWA
Nitrobenzene
ND
mg/1
0.20
1.0
11/21/01
01:53
CWA
98-95-3
Pentachlorophenol
ND
mg/1
10.
1.0
11/21/01
01:53
CWA
87-86-5
Pyridine
ND
mg/l
0.50
1.0
11/21/01
01:53
CWA
110-86-1
2,4,5-Trichlorophenol
ND
mg/1
40.
1.0
11/21/01
01:53
CWA
95-95-4
2,4,6-Trichlorophenol
ND
mg/1
0.20
1.0
11/21/01
01:53
CWA
88-06-2
Nitrobenzene-d5 (S)
66
%
1.0
11/21/01
01:53
CWA
4165-60-0
2-Fluorobiphenyl (8)
69
%
1.0
11/21/01
01:53
CWA
321-60-8
Terphenyl-dl4 (S)
103
%
1.0
11/21/01
01:53
CWA
1718-51-0
Phenol-d6 (S)
39
%
1.0
11/21/01
01:53
CWA
13127-88-3
2-Fluorophenol (S)
51
%
1.0
11/21/01
01:53
CWA
367-12-4
2,4,6-Tribromophenol (S)
84
%
1.0
11/21/01
01:53
CWA
Date Extracted
11/17/01
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Prep/Method:
EPA 8260 /
EPA 8260
Benzene
ND
mg/1
0.020
1.0
11/19/01
19:44
RPJ
71-43-2
2-Butanone (MER)
ND
mg/l
0.40
1.0
11/19/01
19:44
RPJ
78-93-3
Carbon tetrachloride
ND
mg/l
0.020
1.0
11/19/01
19:44
RPJ
56-23-5
Chlorobenzene
ND
mg/1
0.020
1.0
11/19/01
19:44
RPJ
108-90-7
Chloroform
ND
mg/l
0.020
1.0
11/19/01
19:44
RPJ
67-66-3
1,2-Dichloroethane
ND
mg/l
0.020
1.0
11/19/01
19:44
RPJ
107-06-2
1,1-Dichloroethene
ND
mg/1
0.020
1.0
11/19/01
19:44
RPJ
75-35-4
Tetrachloroethene
ND
mg/1
0.020
1.0
11/19/01
19:44
RPJ
127-18-4
Trichloroethene
ND
mg/1
0.020
1.0
11/19/01
19:44
RPJ
79-01-6
Vinyl chloride
ND
mg/l
0.020
1.0
11/19/01
19:44
RPJ
75-01-4
Date: 11/21/01
Page: 3
Laboratory Certification IN Laboratory Certification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Pvww. paWabsWM
Lab Sample No: 931036917
Client Sample ID: LIME HUD
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Project Sample Number: 9227589-002 Date Collected: 11/06/01 13:45
Matrix: Other Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit Dilution
Analyzed
CAS No. Ftnote Rea Lim
Toluene-d8 (S)
100
%
1.0
11/19/01
19:44
RPJ
2037-26-5
4-Bromofluorobenzene (S)
92
%
1.0
11/19/01
19:44
RPJ
460-00-4
Dibromofluoromethane (S)
304
%
1.0
11/19/01
19:44
RPJ
1,2-Dichloroethane-d4 (S)
lit
%
1.0
11/19/01
19:44
RPJ
17060-07-0
Date: 11/21/01
Page: 4
Laboratory Certification IN Laboratory Certification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Analytical"'
wivwpacelabs.com
Lab Sample No: 931036925
Client Sample ID: SLAKER GRITS
Parameters
Metals
Volatile Organics, TCLP Leach
Date Leached
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax: [phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Project Sample Number: 9227589-003 Date Collected: 11/06/01 00:00
Matrix: Other Date Received: 11/06/01 16:38
Results Units Report Limit Dilution Analyzed CAS No. Ftnote Rea Lim
Prep/Method: EPA 1311 / EPA 8260
0.00 1.0 11/15/01 CBE
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510 /
EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
1.0
11/21/01
02:29
CWA
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
1.0
11/21/01
02:29
CWA
121-14-2
Hexachloro-1,3-butadiene
ND
mg/1
0.050
1.0
11/21/01
02:29
CWA
87-68-3
Hexachlorobenzene
ND
mg/l
0.013
1.0
11/21/01
02:29
CWA
118-74-1
Hexachloroethane
ND
mg/l
0.30
1.0
11/21/01
02:29
CWA
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/1
20.
1.0
11/21/01
02:29
CWA
95-48-7
3&4-Methylphenol
ND
mg/l
20.
1.0
11/21/01
02:29
CWA
Nitrobenzene
ND
mg/l
0.20
1.0
11/21/01
02:29
CWA
98-95-3
Pentachlorophenol
ND
mg/l
10.
1.0
11/21/01
02:29
CWA
87-86-5
Pyridine
ND
mg/l
0.50
1.0
11/21/01
02:29
CWA
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
1.0
11/21/01
02:29
CWA
95-95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
1.0
11/21/01
02:29
CWA
88-06-2
Nitrobenzene-d5 (S)
68
%
1.0
11/21/01
02:29
CWA
4165-60-0
2-Fluorobiphenyl (S)
70
%
1.0
11/21/01
02:29
CWA
321-60-8
Terphenyl-d14 (S)
125
%
1.0
11/21/01
02:29
CWA
1718-51-0
Phenol-d6 (S)
39
%
1.0
11/21/01
02:29
CWA
13127-88-3
2-Fluorophenol (S)
51
%
1.0
11/21/01
02:29
CWA
367-12-4
2,4,6-Tribromophenol (S)
82
%
1.0
11/21/01
02:29
CWA
Date Extracted
11/17/01
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Prep/Method:
EPA 8260 /
EPA 8260
Benzene
ND
mg/l
0.020
1.0
11/19/01
21:08
RPJ
71-43-2
2-Butanone (MEK)
ND
mg/1
0.40
1.0
11/19/01
21:08
RPJ
78-93-3
Carbon tetrachloride
ND
mg/l
0.020
1.0
11/19/01
21:08
RPJ
56-23-5
Chlorobenzene
ND
mg/l
0.020
1.0
11/19/01
21:08
RPJ
108-90-7
Chloroform
ND
mg/1
0.020
1.0
11/19/01
21:08
RPJ
67-66-3
1,2-Dichloroethane
ND
mg/l
0.020
1.0
11/19/01
21:08
RPJ
107-06-2
1,1-Dichloroethene
ND
mg/l
0.020
1.0
11/19/01
21:08
RPJ
75-35-4
Tetrachloroethene
ND
mg/l
0.020
1.0
11/19/01
21:08
RPJ
127-18-4
Trichloroethene
ND
mg/l
0.020
1.0
11/19/01
21:08
RPJ
79-01-6
Vinyl chloride
ND
mg/1
0.020
1.0
11/19/01
21:08
RPJ
75-01-4
Date: 11/21/01
Page: 5
Laboratory Certification IDs Laboratory Certification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

aeeAna1jfta1TM
www.pacelabscom
Pace Analytical Services, Inc.
9800 Kincey A venue, Suite 100
Huntersville, NC 28078
Phone: [phone]
fax:[phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Lab Sample No: 931036925
Project Sample
Number: 9227589-003
Date Collected: 11/06/01 00:00
Client Sample ID: SLARSR GRITS
Matrix: Other
Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit Dilution
Analyzed
CAS No. Ftnote Rea Lim
Toluene-d8 (S)
104
%
1.0
11/19/01
21:08
RPJ 2037-26-5
4-Bromofluorobenzene (S)
65
%
1.0
11/19/01
21:08
RPJ 460-00-4
Dibromofluoromethane (S)
104
%
1.0
11/19/01
21:08
RPJ
1,2-Dichloroethane-d4 (S)
113
%
1.0
11/19/01
21:08
RPJ 17060-07-0
Date: 11/21/01
Pape: 6
NC Wastewater
Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory v Certification IDS
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical- Huntersville, NC 28078
Phone: [phone]
www pacelabs.com Far: 704.875.9091
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Lab Sample No: 931036933
Project Sample
Number: 9227589=004
Date Collected: 11/06/01 13:54
Client Sample ID: PRECOAT FILTER
DREGS
Matrix: Other
Date
Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Rea Lim
Metals
Volatile Organics, TCLP Leach.
Prep/Method:
EPA 1311 /
EPA 8260
Date Leached
0.00
1.0
11/15/01
CBE
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510 /
EPA 8270
1,4-Dichlorobenzene
ND
mg/l
0.75
1.0
11/21/01
03:06
CWA
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
1.0
11/21/01
03:06
CWA
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
1.0
11/21/01
03:06
CWA
87-68-3
Hexachlorobenzene
ND
mg/l
0.013
1.0
11/21/01
03:06
CWA
118-74-1
Hexachloroethans
ND
mg/1
0.30
1.0
11/21/01
03:06
CWA
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/l
20.
1.0
11/21/01
03:06
CWA
95-48-7
3&4-Methylphenol
ND
mg/l
20.
1.0
11/21/01
03:06
CWA
Nitrobenzene
ND
mg/l
0.20
1.0
11/21/01
03:06
CWA
98-95-3
Pentachlorophenol
ND
mg/l
10.
1.0
11/21/01
03:06
CWA
87-86-5
Pyridine
ND
mg/1
0.50
1.0
11/21/01
03:06
CWA
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
1.0
11/21/01
03:06
CWA
95-95-4
2,4,6-Trichlorophenol
ND
mg/1
0.20
1.0
11/21/01
03:06
CWA
88-06-2
Nitrobenzene-d5 (S)
66
%
1.0
11/21/01
03:06
CWA
4165-60-0
2-Fluorobiphenyl (S)
64
%
1.0
11/21/01
03:06
CWA
321-60-8
Terphenyl-d14 (S)
97
%
1.0
11/21/01
03:06
CWA
1718-51-0
Phenol-d6 (S)
37
%
1.0
11/21/01
03:06
CWA
13127-88-3
2-Fluorophenol (S)
48
%
1.0
11/21/01
03:06
CWA
367-12-4
2,4,6-Tribromophenol (S)
79
%
1.0
11/21/01
03:06
CWA
Date Extracted
11/17/01
GC/MS Volatiles
volatile Organics, TCLP Leach.
Prep/Method:
EPA 8260 /
EPA 8260
Benzene
ND
mg/l
0.020
1.0
11/19/01
18:48
RPJ
71-43-2
2-Butanone (MER)
ND
mg/1
0.40
1.0
11/19/01
18:48
RPJ
78-93-3
Carbon tetrachloride
ND
mg/1
0.020
1.0
11/19/01
18:48
RPJ
56-23-5
Chlorobenzene
ND
mg/l
0.020
1.0
11/19/01
18:48
RPJ
108-90-7
Chloroform
ND
mg/1
0.020
1.0
11/19/01
18:48
RPJ
67-66-3
1,2-Dichloroethane
ND
mg/l
0.020
1.0
11/19/01
18:48
RPJ
107-06-2
1,1-Dichloroethane
ND
mg/1
0.020
1.0
11/19/01
18:48
RPJ
75-35-4
Tetrachloroethene
ND
mg/l
0.020
1.0
11/19/01
18:48
RPJ
127-18-4
Trichloroethene
ND
mg/l
0.020
1.0
11/19/01
18:48
RPJ
79-01-6
Vinyl chloride
ND
mg/l
0.020
1.0
11/19/01
18:48
RPJ
75-01-4
Date: 11/21/01
Page: 7
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Analytical'"
www pacelabsWrn
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NO 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 932d726
Lab Sample No: 931036933
Project Sample
Number: 9227589-004
Date Collected: 11/06/01 13:5d
Client Sample ID: PRECOAT FILTER
DREGS
Matrix: Other
Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit Dilution
Analyzed
CAS No. Ftnote Rea Lim
Toluene-d8 (S)
95
%
1.0
11/19/01
18:48
RPJ 2037-26-5
d-Bromofluorobenzene (S)
88
%
1.0
11/19/01
18:48
RPJ d60-00-4
Dibromofluoromethane (S)
103
%
1.0
11/19/01
18:48
RPJ
1,2-Dichloroethane-di (S)
114
%
1.0
11/19/01
18:48
RPJ 17060-07-0
Date: 11/21/01
Page: 8
Laboratory Certification IDs Laboratory Qertification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

AnalyiicalTM
WWW.Pacetabscom
Lab Sample No: 931036941
Client Sample ID: FLY ASK
Parameters
Metals
volatile Organics, TCLP Leach
Date Leached
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Project Sample Number: 9227589-005 Date Collected: 11/06/01 14:05
Matrix: Other Date Received: 11/06/01 16:38
Results Units Report Limit Dilution Analyzed CAS No. Ftnote Rau Lim
Prep/Method: EPA 1311 / EPA 8260
0.00 1.0 11/15/01 CBE
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510 /
EPA 8270
1,4-Dichlorobenzene
ND
mg/1
0.75
1.0
11/21/01
03:42
CWA
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
1.0
11/21/01
03:42
CWA
121-14-2
Kexachloro-1,3-butadiene
ND
mg/l
0.050
1.0
11/21/01
03:42
CWA
87-68-3
Kexachlorobenzene
ND
mg/l
0.013
1.0
11/21/01
03:42
CWA
118-74-1
Kexachloroethane
ND
mg/l
0.30
1.0
11/21/01
03:d2
CWA
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/1
20.
1.0
11/21/01
03:42
CWA
9548-7
364-Methylphenol
ND
mg/l
20.
1.0
11/21/01
03:42
CWA
Nitrobenzene
ND
mg/l
0.20
1.0
11/21/01
03:42
CWA
98-95-3
Pentachlorophenol
ND
mg/1
10.
1.0
11/21/01
03:42
CWA
87-86-5
Pyridine
ND
mg/l
0.50
1.0
11/21/01
03:42
CWA
110-86-1
2,d,5-Trichlorophenol
ND
mg/l
40.
1.0
11/21/01
03:42
CWA
95-95-d
2,4,6-Trichlorophenol
ND
mg/l
0.20
1.0
11/21/01
03:42
CWA
88-06-2
Nitrobenzene-d5 (S)
72
%
1.0
11/21/01
03:42
CWA
4165-60-0
2-Fluorobiphenyl (S)
70
%
1.0
11/21/01
03:42
CWA
321-60-8
Terphenyl-d14 (3)
84
%
1.0
11/21/01
03:42
CWA
1718-51-0
Phenol-d6 (S)
27
%
1.0
11/21/01
03:42
CWA
13127-88-3
2-Fluorophenol (S)
37
%
1.0
11/21/01
03:42
CWA
367-12-4
2,4,6-Tribromophenoi (S)
71
%
1.0
11/21/01
03:42
CWA
Date Extracted
11/17/01
GC/MS Volatiles
volatile Organics, TCLP Leach.
Prep/method:
EPA 8260 /
EPA 8260
Benzene
ND
mg/l
0.020
1.0
11/19/01
20:12
RPJ
7143-2
2-Butanone (MEK)
ND
mg/l
0.40
1.0
11/19/01
20:12
RPJ
78-93-3
Carbon tetrachloride
ND
mg/l
0.020
1.0
11/19/01
20:12
RPJ
56-23-5
Chlorobenzene
ND
mg/1
0.020
1.0
11/19/01
20:12
RPJ
108-90-7
Chloroform
ND
mg/l
0.020
1.0
11/19/01
20:12
RPJ
67-66-3
1,2-Dichloroethane
ND
mg/l
0.020
1.0
11/19/01
20:12
RPJ
107-06-2
1,1-Dichloroethene
ND
mg/l
0.020
1.0
11/19/01
20:12
RPJ
75-35-4
Tetrachloroethene
ND
mg/l
0.020
1.0
11/19/01
20:12
RPJ
127-16-4
Trichloroethene
ND
mg/1
0.020
1.0
11/19/01
20:12
RPJ
79-01-6
vinyl chloride
ND
mg/l
0.020
1.0
11/19/01
20:12
RPJ
75-01-4
Date: 11/21/01
Page: 0
Laboratory Certification IN Laboratory Certification Ids
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

AnalXicaf u
ww►v.Q8W8bs.00m
Lab Sample No: 931036941
Client Sample ID: FLY ASK
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
far.• 704.875.9091
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 932d726
Project Sample Number: 9227589-005 Date Collected: 11/06/01 14:05
Matrix: Other Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit Dilution
Analyzed
CAS No. Ftnote Rea Lim
Toluene-d8 (S)
101
%
1.0
11/19/01
20:12
RPJ
2037-26-5
4-Bromofluorobenzens (S)
92
%
1.0
11/19/01
20:12
RPJ
460-00-4
Dibromofluoromethane (S)
104
%
1.0
11/19/01
20:12
RPJ
1,2-Dichloroethane-d4 (S)
121
%
1.0
11/19/01
20:12
RPJ
17060-07-0 1
Date: 11/31/01
Page: 10
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory_ Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Analytical'"
www Pacelabs com
Lab Sample No: 931036958
Client Sample ID: CINDERS
Parameters
Metals
Volatile Organics•, TCLP Leach.
Date Leached
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Hunters ville, NC28078
Phone, 704.875.9092
fax:[phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Project Sample Number: 9227589-006 Date Collected: 11/06/01 14:15
Matrix: Other Date Received: 11/06/01 16:38
Results Units Report Limit Dilution Analyzed CAS No. Ftnote Rea Lim
Prep/Method: EPA 1311 / EPA 8260
0.00 1.0 11/15/01 CBE
GC/MS Semivolatiles
Semivolatile organics, TCLP
Prep/Method:
EPA 3510 /
EPA 8270
1,4-Dichlorobenzene
ND
mg/1
0.75
1.0.
11/21/01
04:18
CWA
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
1.0
11/21/01
04:18
CWA
121-14-2
Hexachloro-1,3-butadiens
ND
mg/l
0.050
1.0
11/21/01
04:18
CWA
87-68-3
Rexachlorobenzene
ND
mg/l
0.013
1.0
11/21/01
04:18
CWA
118-74-1
Rexachloroethane
ND
mg/l
0.30
1.0
11/21/01
04:18
CWA
67-72-1
2-Methylphenol (o-Cresol)
ND
mg/l
20.
1.0
11/21/01
04:18
CWA
95-48-7
3E4-Methylphenol
ND
mg/l
20.
1.0
11/21/01
04:18
CWA
Nitrobenzene
ND
mg/l
0.20
1.0
11/21/01
01:18
CWA
96-95-3
Pentachlorophenol
ND
mg/l
10.
1.0
11/21/01
01:18
CWA
87-86-5
Pyridine
ND
mg/l
0.50
1.0
11/21/01
04:18
CWA
110-86-1
2,4,5-Trichlorophenol
ND
mg/l
40.
1.0
11/21/01
04:18
CWA
95-95-4
2,4,6-Trichlorophenol
ND
mg/l
0.20
1.0
11/21/01
04:18
CWA
88-06-2
Nitrobenzene-d5 (S)
80
%
1.0
11/21/01
O4:18
CWA
4165-60-0
2-Fluorobiphenyl (S)
75
%
1.0
11/21/01
04:18
CWA
321-60-8
Terphenyl-d14 (S)
124
%
1.0
11/21/01
04:18
CWA
1718-51-0
Phenol-d6 (S)
39
%
1.0
11/21/01
04:18
CWA
13127-88-3
2-Fluorophenol (S)
51
%
1.0
11/21/01
01:18
CWA
367-12-4
2,4,6-Tribromophenol (S)
80
%
1.0
11/21/01
04:18
CWA
Date Extracted
11/17/01
GC/MS Volatiles
Volatile organics, TCLP Leach.
Prep/Method:
EPA 8260 /
EPA 8260
Benzene
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
71-43-2
2-Butanone (MER)
ND
mg/l
0.40
1.0
11/19/01
19:16
RPJ
78-93-3
Carbon tetrachloride
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
56-23-5
Chlorobenzene
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
108-90-7
Chloroform
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
67-66-3
1,2-Dichloroethane
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
107-06-2
1,1-Dichloroethene
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
75-35-4
Tetrachloroethene
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
127-18-4
Trichloroethene
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
79-01-6
Vinyl chloride
ND
mg/l
0.020
1.0
11/19/01
19:16
RPJ
75-01-4
Date: 11/21/01
Page: 11
Laboratory Certification
NC Wastewater
IN
12
REPORT OF LABORATORY ANALYSIS
Laboratory Certification
KY Drinking Water
l�
90090
NC Drinking Water
37706
This report shall not be reproduced, except in full,
VA Drinking Water
213
Sc
99006
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87627

Analytical'*
www pwelabsoom
Lab Sample No: 931036958
Client Sample ID: CINDERS
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Project Sample Number: 9227589-006 Date Collected: 11/06/01 14:15
Matrix: Other Date Received: 11/06/01 16:38
Parameters
Results
Units
Report Limit Dilution Analyzed
CAS No. Ftnote Rau Lim
Toluene-d8 (S)
99
%
1.0 11/19/01
19:16
RPJ
2037-26-5
4-Bromofluorobenzene (S)
86
%
1.0 11/19/01
19:16
RPJ
460-00-4
Dibromofluoromethane (S)
103
%
1.0 11/19/01
19:16
RPJ
1,2-Dichloroethane-d4 (S)
110
%
1.0 11/19/01
19:16
RPJ
17060-07-0
Date: 11/21/01
Page: 12
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Analytical
VAMPacelaftcom
PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax- 704.875.9091
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9321726
ND Not Detected
NC Not Calculable
(S) Surrogate
[1] The surrogate and/or spike recovery was outside acceptance limits.
Date: 11/21/01
Page: 13
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratoryn IDs
Certificatio
NC Wastewater 12 KY Drinking
Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

wtov.pacetabs.com
QC Batch: 49599
QC Batch Method: EPA 3510
Associated Lab Samples:
METHOD BLANK: 921938049
Associated Lab Samples:
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Analysis Method: EPA 8270
Analysis Description: Semivolatile Organics, TCLP
931036909 931036917 931036925 931036933 931036941
931036958
931036909 931036917 931036925 931036933 931036941 931036958
Parameter
Units
1,4-Dichlorobenzene
mg/l
2,4-Dinitrotoluene
mg/l
Hexachloro-1,3-butadiene
mg/l
Hexachlorobenzene
mg/1
Hexachloroethane
mg/l
2-Methylphenol (o-Cresol)
mg/l
3&4-Methylphenol
mg/l
Nitrobenzene
mg/1
Pent achlorophenol
mg/l
Pyridine
mg/l
2,4,5-Trichlorophenol
mg/l
2,4,6-Trichlorophenol
mg/l
Nitrobenzene-d5 (S)
%
2-Fluorobiphenyl (S)
%
Terphenyl-d14 (S)
%
Phenol-d6 (8)
%
2-Fluorophenol (S)
%
2,4,6-Tribromophenol (S)
%
Blank Reporting
Result
Limit Footnotes
ND
0.0008
ND
0.0000
ND
0.0001
ND
0.0000
ND
0.0003
ND
0.020
ND
0.020
ND
0.0002
NO
0.010
ND
0.0005
ND
0.040
ND
0.0002
73
74
103
40
53
81
LABORATORY CONTROL SAMPLE & LCSD: 921938056 921938064
Spike
LCS
LCSD
LCS
LCSD
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
RPD Footnotes
1,4-Dichlorobenzene
mg/l
0.2500
0.1409
0.1590
56
64
12
2,4-Dinitrot oluene
mg/l
0.2500
0.1928
0.1865
77
75
3
Hexachloro-1,3-but adiene
mg/l
0.2500
0.1280
0.1416
51
57
10
Hexachlorobenzene
mg/l
0.2500
0.1985
0.1933
79
77
3
Date: 11/21/01
Page: 11
Laboratory Certification IDs Laboratory Certification I�
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Analytical'"
www.paoelabscom
QC Batch: 49713
QC Batch Method: EPA 6260
Associated Lab Samples:
METHOD BLANK: 921942256
Associated Lab Samples:
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Nuntersville, NC28078
Phone: [phone]
fax:[phone]
QUALITY CONTROL DATA
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Analysis Method: EPA 8260
Analysis Description: Volatile Organics, TCLP Leach.
931036909 931036917 931036925 931036933 931036941
931036958
931036909 931036917 931036925 931036933 931036941 931036958
Parameter
Units
Benzene
mg/l
2-Butanone (MEK)
mg/l
Carbon tetrachloride
mg/l
Chlorobenzene
mg/l
Chloroform
mg/l
1,2-Dichloroethane
mg/l
1,1-Dichloroethene
mg/l
Tetrachloroethene
mg/l
Trichloroethene
mg/1
Vinyl chloride
mg/l
Toluene-d8 (S)
%
4-Bromofluorobenzene (S)
%
Dibromofluoromethane (S)
%
1,2-Dichloroethane-di (S)
%
LABORATORY CONTROL SAMPLE: 921942264
Blank Reporting
Result
Limit Footnotes
ND
0.020
ND
0.40
ND
0.020
ND
0.020
ND
0.020
ND
0.020
ND
0.020
ND
0.020
ND
0.020
NO
0.020
100
90
105
115
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Benzene
mg/l
0.2000
0.1906
95
2-Butanone (MEK)
mg/l
0.4000
0.3408
85
Carbon tetrachloride
mg/1
0.2000
0.2131
107
Chlorobenzene
mg/l
0.2000
0.2126
106
Chloroform
mg/1
0.2000
0.1983
99
1,2-Dichloroethane
mg/l
0.2000
0.1900
95
1,1-Dichloroethene
mg/l
0.2000
0.2043
102
Tetrachloroethene
mg/1
0.2000
0.2467
123
Trichloroethene
mg/l
0.2000
0.1992
100
Date: 11/21/01
Page: 16
Laboratory Certification IDS; Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Analytical
wvnv pacelabs.wM
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone, 704.875.9092
fax: [phone]
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
LABORATORY CONTROL SAMPLE: 921942264
Spike LCS LCS
Parameter Units Cone. Result % Rec Footnotes
Vinyl chloride mg/1 0.2000 0.1914 96
Toluene-d8 (S) 100
4-Bromofluorobenzene (S) 97
Dibromofluoromethane (S) 100
1,2-Dichloroethane-d4 (9) 100
Date: 11/21/01
Pape: 17
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification 1Ds
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

aceAnalytical'"
WWW.PWWabS.COM
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax.- 704.875.9091
Lab Project Number: 9227589
Client Project ID: Blue Ridge Paper Prod. 9324726
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
LCS (D) Laboratory Control Sample (Duplicate)
NS(D)Natrix Spike (Duplicate)
DUP Sample Duplicate
ND Not Detected
NC Not Calculable
RPD Relative Percent Difference
(S) Surrogate
Date: 11/21/01
Page: 18
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking
Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

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North Carolina
Department of Environment and Natural Resources
F •
Division of Waste Management
MichaelF. Easley, Governor NCDENR
William G. Ross Jr., Secretary
Dexter R. Matthews, Director
February 6, 2002
Mr. Jim Giauque
Blue Ridge Paper Products, Inc.
Main Street
Canton, NC 28716
Re: Blue Ridge Paper Products, Inc.
Solid Waste Permit No. 44-06
Part 2: Permit to Operate
Dear Mr. Giauque:
The Solid Waste Section has determined that Blue Ridge Paper Products, Inc. has met
the pre -operative conditions of Solid Waste Permit No. 44-06, Part 1: Permit to Construct.
Enclosed is Solid Waste Permit No. 44-06, Part 2: Permit to Operate.
If you have any questions or comments, please contact me at [phone], ext. 259.
Sincerely,
Sherri Coghill
Environmental Engineer
Solid Waste Section
cc: Brent Rockett, DWM
Tim Jewett, DWM
Jim Patterson, DWM
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ FAX: [phone] \ Internet: www.enr.state.nc.us
AN EQUAL OPPORTUNITY \ AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED / 10% POST CONSUMER PAPER

North Carolina
Department of Environment and Natural Resources
Division of Waste Management
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Dexter R. Matthews, Director
February 6, 2002
Mr. Jim Giauque
Blue Ridge Paper Products, Inc.
Main Street
Canton, NC 28716
Re: Blue Ridge Paper Products, Inc.
Solid Waste Permit No. 44-06
Pa t 2: Permit to Operate
aC�C�A co .
Dear Mr. Glauque:
ern
NCDENR
The Solid Waste Section has determined that Blue Ridge Paper Products, Inc. has met
the pre -operative conditions of Solid Waste Permit No. 44-06, Part 1: Permit to Construct.
Enclosed is Solid Waste Permit No. 44-06, Part 2: Permit to Operate.
If you have any questions or comments, please contact me at [phone], ext. 259.
Sincerely,
C
Sherri Coghill
Environmental Engineer
Solid Waste Section
cc: Brent Rockett, DWM
Tim Jewett, DWM
Jim Patterson, DWM
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ FAX: [phone] \ Internet: www.enr.state.nc.us
AN EQUAL OPPORTUNITY \ AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED / 10% POST CONSUMER PAPER

North Carolina
Department of Environment and Natural Resources
Division of Waste Management A���
Michael F. Easley, Governor NCDENR
William G. Ross Jr., Secretar
y
Dexter R. Matthews, Director
INDUSTRIAL SOLID WASTE LANDFILL
PERMIT
BLUE RIDGE PAPER PRODUCTS, INC.
is hereby issued a PERMIT to OPERATE an
INDUSTRIAL SOLID WASTE LANDFILL FACILITY
located on SR 1550 and 1-40, Haywood County, North Carolina, in accordance with Article 9,
Chapter 130A, of the General Statutes of North Carolina and all rules promulgated thereunder
and subject to the conditions set forth in this permit. The facility is located and described by
the legal description of the site or the property map contained within the approved
application.
C C_
aPtidWastce
C. Coffey, Acting Chief
Section
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ FAX: [phone] \ Internet: www.enr.state.nc.us
AN EQUAL OPPORTUNITY \ AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED / 10% POST CONSUMER PAPER

FACILITY PERMIT NO: 44-06
Part 2-Permit to Operate
Date of Original Issue (Phase 1, Area 6A East): April 29, 1994
Amendment Date (Phase 2, Area 6A West): February 5, 2002
Page 2
ATTACHMENT 3
Approved Documents
PART I: INDUSTRIAL LANDFILL FACILITY
PART II: INDUSTRIAL LANDFILL UNIT
Area 6A West
1. Construction Documentation, Cell 6A-West Construction, Blue Ridge Paper Products,
Inc., Canton, NC, Volumes I and II, prepared by Sevee It Maher Engineers, Inc., dated
January, 2001, submitted March 29, 2001.
2. Response to NCDENR Comments, Landfill No. 6, Area A -West, submitted by Blue Ridge
Paper Products, Inc., January 10, 2002.

FACILITY PERMIT NO: 44-06
Part 2-Permit to Operate
Date of Original Issue (Phase 1, Area 6A East): April 29, 1994
Amendment Date (Phase 2, Area 6A West): February 5, 2002
Page 3
ATTACHMENT 4
Conditions of Permit to Operate
PART I: INDUSTRIAL LANDFILL FACILITY
GENERAL CONDITIONS
1. This permit shall be reviewed, pursuant to 15A NCAC 1313.0201(e), five (5) years from the
issuance date of this permit to operate or the latest amendment.
2. In the event of conflicts between this Permit to Operate and previously issued conditions,
the conditions of this Permit to Operate shall supersede previously issued conditions.
3. Additional conditions and revision of the approved documents or changes during the
operation of the landfill require approval by the North Carolina Solid Waste Section.
PART II: INDUSTRIAL LANDFILL UNIT
OPERATIONAL CONDITIONS
4. This permit approves the operation of Landfill No. 6A West as well as the on -site
environmental management and protection facilities as described in the approved plans.
5. The solid waste management units within this facility shalt conform to all operating
requirements described in the approved plans, 15A NCAC 13B .0506, and the conditions
specified herein:
a. Closure or partial closure of any MSWLF unit shall be in accordance with the
Closure Plans described in the approved plans. Final Closure Plans shall be
submitted to the Division at least 90 days prior to implementation. The
Section may require a modification to closure cap design should
performance of the approved liner and leachate collection system prove
ineffective in maintaining less than one foot of leachate head on the base
liner system. Periodic measurement of leachate head may be required.
b. Wastewater treatment sludges may be codisposed in accordance with
approved plans.
6. Ground water quality at this facility is subject to the "Classifications and Water Quality
Standards Applicable To The Groundwater of North Carolina", 15A NCAC 2L. This includes,
but is not limited to provisions for detection monitoring, assessment, and corrective
action. Compliance will be determined with ground water monitoring at the landfill.
MONITORING AND REPORTING
7. Water quality monitoring at this unit shall be as described in the approved monitoring
plan.
8. A readily accessible unobstructed path shall be cleared and maintained so that four-wheel
drive vehicles may access monitoring well locations at all times.

FACILITY PERMIT NO: 44-06
Part 2-Permit to Operate
Date of Original Issue (Phase 1, Area 6A East): April 29, 1994
Amendment Date (Phase 2, Area 6A West): February 5, 2002
Page 4
9. A field log book which details all development, sampling, repair, and all other pertinent
activities associated with each monitoring well and all sampling activities associated with
each surface water and leachate sampling location shall be kept as part of the permanent
facility record.
10. Records of all ground water, surface water, leachate, and underdrain analytical data shall
be kept as part of the permanent facility record.
11. Ground water monitoring wells, surface water sampling locations and the underdrain at
6A East must be sampled at least semi-annually according to the specifications outlined
in the approved water quality monitoring plan and the current policies and guidelines of
the Section in effect at the time of sampling.
12. Reports of the analytical data for each water quality sampling event shall be submitted
to the Section within 60 days of the respective sampling event. Analytical data shall be
submitted in a manner prescribed by the Section.
13. The four independent samples which comprise the initial baseline sampling event shall be
collected from each ground water monitoring well and the report shall be submitted to
the Section within six months after issuance of the Permit to Operate.
14. Untreated leachate shall be sampled and analyzed at least semi-annually concurrently
with the ground and surface water sampling. The leachate shall be analyzed for the same
constituents as the ground and surface water and also for pH, specific conductance, BOD,
COD, phosphate, nitrate and sulfate. Test results shall be submitted to the Section along
with ground and surface water test results.
15. On or before August 1 of each year, the permittee shall report the amount of waste
received (in tons) at this facility and disposed of in the landfill units to the Solid Waste
Section, on forms prescribed by the Section. This report shall include the following
information:
a. The reporting period shall be for the previous year, beginning July 1 and ending on
June 30.
b. The amount of waste received and landfilled in tons, compiled on a monthly basis
by county or transfer station of origin and by specific waste type if diverted to a
specific unit within the permitted facility; and
C. The completed report shall be forwarded to the Regional Waste Management
Specialist for the facility. A copy of the completed report shall be forwarded to the
County Manager of each county from which waste was received.

UNIT TYPE::(check ali thatapply to this.audit withsamePermit number) .
Lined
LCID
YW
Transfer
Compost
SLAS
COUNTY: Haywood
MSWLF
PERMIT NO.: 44-06
Closed
HHW
white
Incin
T&P
FIRM
MSWLF
goods
.FILE TYPE: COMPLIANCE
CDLF
TireT&P/
Tire
Industrial
x
DEMO
SDTF
Collection
Monofill
Landfill
-
Date of Audit: 01 /25/02
Date of Last Audit: 10/26/01
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque, Environmental Engineer
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque, Environmental Engineer
Blue Ridge Paper Products, Inc.
175 Main Street
P.O. Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, N.C. Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active
PURPOSE OF AUDIT:
Semi-annual comprehensive industrial landfill audit.
NOTICE OF VIOLATIONS) (citation and explanation):
No violations observed.
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such
further relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A
OTHER COMMENTS /SUGGESTIONS:
Operation looks good.

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
Please contact me if you have any questions or concerns regarding this audit report.
(signature) Phone: [phone].
R ' nal Representative
Distribution: original signed copy to facility -- signed copy to compliance officer — e-mail or copy to super
Delivered on : O1/31/02 by hand delivery X US Mail Certified No. r I

revised 0711210212. PM.
' FACILITY COMPLIANCE AUBIT REPORT
AIM
DIVISIon. of Waste Management;
NCDENR Sol><d Waste Section'
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
UNIT TYPE (el
Lined LC1D
MSWLF
Closed EIHW
MS WLF
CDLF Tire T&P /
Collection
Y W
Transfer
Compost
SLAS
White
Incin
T&P
FIRM
roods
Tire
Industrial
X
DEMO
SDTF
onofill
Landfill
Date of Audit: 07/09/02
Date of Last Audit: 04/23/02
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc
175 Main Street
P.O. Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, N.C. Solid Waste Section
Jim Giauque, Blue Ridge Paper Products
STATUS OF PERMIT:
Active
PURPOSE OF AUDIT:
Inspection of industrial landfill.
NOTICE OF VIOLATIONS) (citation and explanation):
N/A
,AUNTY: Haywood
'ERMIT NO.: 44-06
ILE>TYPE COMPLIANCE
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such
further relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A
OTHER COMMENTS /SUGGESTIONS:
A good-looking operation.

Please contact me if you have any questions or concerns regarding this audit report.
(signature) Phone: [phone].
Regional Representative
Distribution: original signed copy to facility -- signed copy to compliance officer — e-mail or copy to super
Delivered on : 07/15/02 by hand delivery X US Mail Certified No. u

low
revrsed:07f12/02 12.48 PM
FACILITY COMPLIANCE AtTDIT REPQRT
® Division of Was#e Manageme>nt ,
NCDENR Solid Waste Sect>fon.
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
UNIT TYRE. (check alT that apply. to liis audit with same Permit number
Lined LCID YW Transfer Compost SLAS COUNTY: Haywood
MS WLF
Closed HHW White Incin T&P FIRM PERMIT NO 44 06
MS WLF goods
CDLF TireT&P/ Tire Industrial X DEMO SDTF FILETYPE::-COMPLIANCE
Collection Monofill Landfill
Date of Audit: 07/09/02 Date of Last Audit: 04/23/02
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc
175 Main Street
P.O. Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, N.C. Solid Waste Section
Jim Giauque, Blue Ridge Paper Products
STATUS OF PERMIT:
Active
PURPOSE OF AUDIT:
Inspection of industrial landfill.
NOTICE OF VIOLATIONS) (citation and explanation):
N/A
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such
further relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A
OTHER COMMENTS /SUGGESTIONS:
A good-looking operation.

Please contact me if you have any questions or concerns regarding this audit report.
(signature) Phone: [phone].
qo'Tgionalb'presentative
Distribution: original signed copy to facility -- signed copy to compliance officer — e-mail or copy to super
Delivered on : 07/15/02 by hand delivery X US Mail Certified No. jj

_ r FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
NCDENk g
Solid Waste Section
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Date of Audit: 10/22/02
Date of Last Audit: 07/09/02
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
P.O. Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, N.C. Solid Waste Section
Jim Giauque, Blue Ridge Paper Products
STATUS OF PERMIT:
Permit amendment date - February 5, 2002
PURPOSE OF AUDIT:
Inspection of industrial landfill.
NOTICE OF VIOLATIONS) (citation and explanation):
No violations noted.
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such
further relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A
OTHER COMMENTS /SUGGESTIONS:
Blue Ridge Paper Products is still using processed C and D material from the Haywood County C and D treatment and
processing facility as a bulking agent for the wastewater treatment plant sludge.

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
Please contact me if you have any questions or concerns regarding this audit report.
(;�� (signature) Phone: [phone].
Regional Representative
Distribution: original signed cony to facility -- signed copy to compliance officer e-mail or coat/ to super
Delivered on : 10/31/02 by hand delivery X US Mail Certified NoJ I

CDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
UNIT TYPE: (check all that apply to this audit with samePermit number),
Lined
LCID
YW
Transfer
Compost
SLAB
COUNTY: Haywood.
MSWLF
PERMIT NO.: 44-06
Closed
HHW
white
Incin
T&P
FIRM
MSWLF
goods
FILE TYPE: COMPLIANCE
CDLF
TireT&P/
Tire
Industrial
X
DEMO
sDTF
Collection
Monofill
Landfill
Date of Audit: 10/22/02
Date of Last Audit: 07/09/02
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque
Blue Ridge Paper Products, Inc.
P.O. Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, N.C. Solid Waste Section
Jim Giauque, Blue Ridge Paper Products
STATUS OF PERMIT:
Permit amendment date - February 5, 2002
PURPOSE OF AUDIT:
Inspection of industrial landfill.
NOTICE OF VIOLATIONS) (citation and explanation):
No violations noted.
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such
further relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A
OTHER COMMENTS /SUGGESTIONS:
Blue Ridge Paper Products is still using processed C and D material from the Haywood County C and D treatment and
processing facility as a bulking agent for the wastewater treatment plant sludge.

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
Please contact me if you have any questions or concerns regarding this audit report.
(signature) Phone: [phone].
Regional Representative
Distribution: original signed copy to facility -- signed copy to compliance officer e-mail or copy to super
Delivered on : 10/31/02 by hand delivery X US Mail Certified No. f 1

1
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT ANO NATURAL RESOURCES
revised 04122102 2:17 PM
FACILITY COMPLIANCE AUDITf REPORT
Division of Waste Management
Solid Waste Section
UNIT TYPE: (check all that apply
to this audit with: same. Permit number
Lined
LCID
YW
Transfer
Compost
SLAS
COUNTY: 'Haywood
MSWLF
PERMIT NO.: 44-08-TP
Closed
HEW
White
Incin
T&P
X
FIRM
MS WLF
goods
-
FILE TYPE: COMPLIANCE
CDLF
TireT&P/
Tire
Industrial
DEMO
sDTF
Collection
Monofill
Landfill
Date of Audit: 04/19/02
Date of Last Audit: 01/25/02
FACILITY NAME AND ADDRESS:
Haywood County Municipal Waste Processing Facility
278 Recycle Drive
Clyde, NC 28721
FACILITY CONTACT NAME AND PHONE NUMBER:
Bobby Cogdill, Haywood County Solid Waste Director
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
N/A
AUDIT PARTICIPANTS:
Jim Patterson, N.C. Solid Waste Section
Linda Clark, Haywood County Solid Waste
Department
STATUS OF PERMIT:
Active
PURPOSE OF AUDIT:
Inspection of waste treatment and processing facility.
NOTICE OF VIOLATIONS) (citation and explanation):
No violations noted.
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such
further relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audit):
N/A
OTHER COMMENTS /SUGGESTIONS:
Operation looks good.

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
Please contact me if you have any questions or concerns regarding this audit report.
(signature) Phone: [phone].
Regional Representative
Distribution_ original signed copv to facilitv -- signed copy to compliance officer — e-mail or cony to super
Delivered on : 04/25/02 by I I hand delivery I X I US Mail I I Certified No. l_1

�'
- .revised 01/29/02 2: 06 PM
•
AP
FACILITY COMPLIANCE AUDIT REPORT
®
Division of Waste Management
NCDENRlido
Waste Section
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT ANo NATURAL RESOURCES
UNIT TYPE: (check all that apply to this audit with same Permit number
Lined
LCID
YW
Transfer
Compost
SLAS
COUNTY: .
MSWLF
,Haywood
Closed
HHW
White
Incin
UP
FIRM
PERMIT NO.: 44-06
MSWLF
goods
CDLF
Tire UP /
Tire
Industrial
x
DEMO
SDTF
FILE TYPE: COMPLIANCE
Collection
Monofill
Landfill
Date of Audit: 01 /25/02
Date of Last Audit: 10/26/01
FACILITY NAME AND ADDRESS:
Blue Ridge Paper Products Industrial Landfill
State Road 1550
Canton, NC 28716
FACILITY CONTACT NAME AND PHONE NUMBER:
Jim Giauque, Environmental Engineer
Telephone: [phone]
FACILITY CONTACT ADDRESS (IF DIFFERENT):
Jim Giauque, Environmental Engineer
Blue Ridge Paper Products, Inc.
175 Main Street
P.O. Box 4000
Canton, NC 28716
AUDIT PARTICIPANTS:
Jim Patterson, N.C. Solid Waste Section
Jim Giauque, Blue Ridge Paper Products, Inc.
STATUS OF PERMIT:
Active
PURPOSE OF AUDIT:
Semi-annual comprehensive industrial landfill audit.
NOTICE OF VIOLATIONS) (citation and explanation):
No violations observed.
You are hereby advised that, pursuant to N.C.G.S. 130A-22, an administrative penalty of up to $5,000 per day may be assessed for each
violation of the Solid Waste Statute or Regulations. If the violation(s) noted here continue, you may be subject to enforcement actions
including penalties, injunction from operation of a solid waste management facility or a solid waste collection service and any such
further relief as may be necessary to achieve compliance with the North Carolina Solid Waste Management Act and Rules.
STATUS OF PAST NOTED VIOLATIONS (List all noted last audiit):
N/A
OTHER COMMENTS /SUGGESTIONS:
Operation looks good.

FACILITY COMPLIANCE AUDIT REPORT
Division of Waste Management
Solid Waste Section
Page 2 of 2
Please contact me if you have any questions or concerns regarding this audit report.
112 a4�� (signature) Phone: [phone].
R nal Representative
Distribution: original signed copy to facility -- signed copy to compliance officer — e-mail or copy to super
Delivered on : 01/31/02 by hand delivery X US Mail Certified No. f I

North Carolina
Department of Environment and Natural Resources
Division of Waste Management .� ► ®�
Michael F. Easley, Governor®���
William G. Ross Jr., Secretary
Dexter R. Matthews, Director
l
INDUSTRIAL SOLID WASTE LANDFILL
PERMIT
BLUE RIDGE PAPER PRODUCTS, INC.
is hereby issued a PERMIT to OPERATE an
INDUSTRIAL SOLID WASTE LANDFILL FACILITY
located on SR 1550 and 1-40, Haywood County, North Carolina, in accordance with Article 9,
Chapter 130A, of the General Statutes of North Carolina and all rules promulgated thereunder
and subject to the conditions set forth in this permit. The facility is located and described by
the legal description of the site or the property map contained within the approved
application.
a/Yr,e
C—
a es C. Coffey, Acting Chi
lid Waste Section
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ FAX: [phone] \ Internet: www.enr.state.nc.us
AN EQUAL OPPORTUNITY \ AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED / 10% POST CONSUMER PAPER

FACILITY PERMIT NO: 44-06
Part 2-Permit to Operate
Date of Original Issue (Phase 1, Area 6A East): April 29, 1994
Amendment Date (Phase 2, Area 6A West): February 5, 2002
Page 2
ATTACHMENT
Approved Documents
PART I: INDUSTRIAL LANDFILL FACILITY
PART II: INDUSTRIAL LANDFILL UNIT
Area 6A West
1. Construction Documentation, Cell 6A-West Construction, Blue Ridge Paper Products,
Inc., Canton, NC, Volumes I and II, prepared by Sevee Ft Maher Engineers, Inc., dated
January, 2001, submitted March 29, 2001.
2. Response to NCDENR Comments, Landfill No. 6, Area A -West, submitted by Blue Ridge
Paper Products, Inc., January 10, 2002.

FACILITY PERMIT NO: 44-06
Part 2-Permit to Operate
Date of Original Issue (Phase 1, Area 6A East): April 29, 1994
Amendment Date (Phase 2, Area 6A West): February 5, 2002
Page 3
ATTACHMENT 4
Conditions of Permit to Operate
PART I: INDUSTRIAL LANDFILL FACILITY
GENERAL CONDITIONS
1. This permit shall be reviewed, pursuant to 15A NCAC 1313.0201(e), five (5) years from the
issuance date of this permit to operate or the latest amendment.
2. In the event of conflicts between this Permit to Operate and previously issued conditions,
the conditions of this Permit to Operate shall supersede previously issued conditions.
3. Additional conditions and revision of the approved documents or changes during the
operation of the landfill require approval by the North Carolina Solid Waste Section.
PART II: INDUSTRIAL LANDFILL UNIT
OPERATIONAL CONDITIONS
4. This permit approves the operation of Landfill No. 6A West as well as the on -site
environmental management and protection facilities as described in the approved plans.
5. The solid waste management units within this facility shall conform to all operating
requirements described in the approved plans, 15A NCAC 13B .0506, and the conditions
specified herein:
a. Closure or partial closure of any MSWLF unit shall be in accordance with the
Closure Plans described in the approved plans. Final Closure Plans shalt be
submitted to the Division at least 90 days prior to implementation. The
Section may require a modification to closure cap design should
performance of the approved liner and leachate collection system prove
ineffective in maintaining less than one foot of leachate head on the base
liner system. Periodic measurement of leachate head may be required.
b. Wastewater treatment sludges may be codisposed in accordance with
approved plans.
6. Ground water quality at this facility is subject to the "Classifications and Water Quality
Standards Applicable To The Groundwater of North Carolina", 15A NCAC 2L. This includes,
but is not limited to provisions for detection monitoring, assessment, and corrective
action. Compliance will be determined with ground water monitoring at the landfill.
MONITORING AND REPORTING
7. Water quality monitoring at this unit shall be as described in the approved monitoring
plan.
8. A readily accessible unobstructed path shall be cleared and maintained so that four-wheel
drive vehicles may access monitoring well locations at all times.

FACILITY PERMIT NO: 44-06
Part 2-Permit to Operate
Date of Original Issue (Phase 1, Area 6A East): April 29, 1994
Amendment Date (Phase 2, Area 6A West): February 5, 2002
Page 4
9. A field log book which details all development, sampling, repair, and all other pertinent
activities associated with each monitoring well and all sampling activities associated with
each surface water and leachate sampling location shall be kept as part of the permanent
facility record.
10. Records of all ground water, surface water, leachate, and underdrain analytical data shall
be kept as part of the permanent facility record.
11. Ground water monitoring wells, surface water sampling locations and the underdrain at
6A East must be sampled at least semi-annually according to the specifications outlined
in the approved water quality monitoring plan and the current policies and guidelines of
the Section in effect at the time of sampling. }
12. Reports of the analytical data for each water quality sampling event shall be submitted
to the Section within 60 days of the respective sampling event. Analytical data shall be
submitted in a manner prescribed by the Section.
13. The four independent samples which comprise the initial baseline sampling event shall be
collected from each ground water monitoring well and the report shalt be submitted to
the Section within six months after issuance of the Permit to Operate.
14. Untreated leachate shall be sampled and analyzed at least semi-annually concurrently
with the ground and surface water sampling. The leachate shall be analyzed for the same
constituents as the ground and surface water and also for pH, specific conductance, BOD,
COD, phosphate, nitrate and sulfate. Test results shall be submitted to the Section along
with ground and surface water test results.
15. On or before August 1 of each year, the permittee shall report the amount of waste
received (in tons) at this facility and disposed of in the landfill units to the Solid Waste
Section, on forms prescribed by the Section. This report shall include the following
information:
a. The reporting period shall be for the previous year, beginning July 1 and ending on
June 30.
b. The amount of waste received and landfitled in tons, compiled on a monthly basis
by county or transfer station of origin and by specific waste type if diverted to a
specific unit within the permitted facility; and
C. The completed report shall be forwarded to the Regional Waste Management
Specialist for the facility. A copy of the completed report shall be forwarded to the
County Manager of each county from which waste was received.