4406_ROSCANS_2000

k
, Zo �3
NC®ENR
� a
JAMES B. HUNT JR.
GOVERNOR
BILL 14131,MAN
SECRETARY
i v
WIL,L,IAr,j L. MEYER
DIRECTOR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
March 14, 2000
Mr. Jim Giauque
Blue Ridge Paper Products, Inc.
PO Box 4000
Canton, NC 28716
Re: Blue Ridge Paper Products Landfill No. 6 Industrial Waste Landfill
Solid Waste Permit No. 44-06
Part 1: Permit to Construct
Dear Mr. Giauque:
Enclosed is Solid Waste Permit No. 44-06, Part 1: Permit to Construct.
This permit approves construction of Area 6A East, Cell V in addition to
Area 6A West, Cells I and II. This permit also amends the name of the
facility.
If you have any questions or comments, please contact me at
[phone], ext. 259.
Sincerely,
Sherri Coghill
Environmental Engineer
Solid Waste Section
cc: Brent Rockett
Tim Jewett
Jim Patterson
1646 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1646
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

A
NCDENR
JAMES B. HUNT JR.
GOVERNOR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
FACILITY PERMIT NO: 44-06
Part 1-Permit to Construct
Date of Original Issue: January 9, 1992
Amendment Date: March 8, 1999
Modification Date: March 14, 2000
Page 1
INDUSTRIAL SOLID WASTE LANDFILL
BLUE RIDGE PAPER PRODUCTS, INC.
is hereby issued a PERMIT to CONSTRUCT an
INDUSTRIAL SOLID WASTE LANDFILL FACILITY
located on SR 1550 and 1-40, Haywood County, North Carolina, in accordance with
Article 9, Chapter 130A, of the General Statutes of North Carolina and all rules
promulgated thereunder and subject to the conditions set forth in this permit.
Ja es C. Coffey, Supervi
ermitting Branch
Solid Waste Section
1646 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1646
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

FACILITY PERMIT NO: 44-06
Part 1-Permit to Construct
Date of Original Issue: January 9, 1992
Amendment Date: March 8, 1999
Modification Date: March 14, 2000
Page 2
ATTACHMENT 1
Approved Documents
1. Application for Permit to Construct, Landfill No. 6A West, Champion International
Corporation, Canton, NC, prepared by Sevee and Maher Engineers, Inc., revised through
February 24, 1999.
2. Operations Manual, Landfill No. 6A West, Champion International Corporation, Canton, NC,
prepared by Sevee and Maher Engineers, Inc., dated January 1999.
3. Landfill Stability Evaluation for Vertical Expansion, Area 6A East, Blue Ridge Paper
Products, Inc., Canton NC, prepared by Sevee and Maher Engineers, Inc., dated
October 1999.
4. Facility Drawings, Landfill 6, Area A West and Area A West (Alternate), prepared by
Sevee and Maher Engineers, Inc., dated March 8, 2000.

FACILITY PERMIT NO: 44-06
Part 1-Permit to Construct
Date of Original Issue: January 9, 1992
Amendment Date: March 8, 1999
Modification Date: March 14, 2000
Page 3
ATTACHMENT 2
Conditions of Permit to Construct
PART I: INDUSTRIAL WASTE LANDFILL FACILITY
GENERAL CONDITIONS
1. This permit shall be effective upon compliance with 15A NCAC 13B .0204 and when the
certified copy with the page, book number, date of recordation, and Register's seat is
returned to the Solid Waste Section (Section).
2. This permit is subject to review every five years as per 15A NCAC 13B .0201(e), according
to the issuance date of the Permit to Operate. Modifications to the facility may be
required in accordance with rules in effect at the time of review.
3. The approved plans are described in Attachment 1, "Approved Documents", and allows
construction Where discrepancies may exist, the most recent approved submittal and
Conditions of Permit shall govern.
4. The landfill is permitted to receive solid waste generated solely by Blue Ridge Paper
Products, Inc. as described in the approved plan and as defined in 15A NCAC 13B
.0101(36), except where prohibited by North Carolina General Statutes Article 9 of
Chapter 130A, and rules adopted by the Commission for Health Services.
5. This facility is subject to the requirements of at[ applicable sections of the most recent
version of the North Carolina Solid Waste Management Rules, 15A NCAC 13B and the
specific conditions contained herein.
6. This permit is not transferable.
PART II: INDUSTRIAL WASTE LANDFILL UNIT
CONSTRUCTION CONDITIONS
7. The permittee shall conduct a pre -construction meeting, on -site, prior to initiating
construction and shall notify the Solid Waste Section of said meeting. If construction does
not begin within 18 months from the issuance date of this permit, then the permittee
must obtain written approval from the Section prior to construction and comply with any
conditions of said approval.

FACILITY PERMIT NO: 44-06
Part 1-Permit to Construct
Date of Original Issue: January 9, 1992
Amendment Date: March 8, 1999
Modification Date: March 14, 2000
Page 4
8. This permit approves the construction of Cells I and II of Area 6A West and Celt V of Area
6A East. Construction shall be in accordance with the approved plans as described in
Attachment 1, Document 1, "Approved Documents".
9. Additional conditions and revisions of the approved documents or changes during
construction require approval by the North Carolina Solid Waste Section.
10. Any modifications in sedimentation and erosion control activities require approval by the
Land Quality Section. The Section shalt be notified of any sedimentation and erosion
control modifications.
WATER QUALITY MONITORING SYSTEM CONSTRUCTION CONDITIONS
11. The owner's geologist shall examine the cell excavation and note any pertinent geologic
features exposed during the construction process and shalt notify the Solid Waste Section
Hydrogeologist of these findings prior to the placement of any liner materials.
12. The owner's geologist shall be in the field to supervise all well installations. Any
modifications to the approved water quality monitoring plan require approval by the
Section Hydrogeologist. Documentation of all changes to the approved plan shall be
submitted with the well construction records.
13. For each monitoring well constructed, a well construction record, well schematic, boring
tog and a description of well development activities shall be submitted to the Section
within 30 days upon well completion.
PRE -OPERATIVE CONDITIONS
14. Prior to receiving waste, a Permit to Operate, must be obtained from the Solid Waste
Section in accordance with 15A NCAC 13B .0201(b).
15. The following requirements shall be met prior to obtaining a Permit to Operate:
a. Site preparation shall be in accordance with the approved plans, and the conditions
specified herein.
b. Site inspection shall be made by a representative of the Solid Waste Section.
C. A pre -operative meeting shall be held on -site with key landfill personnel and
representatives of the Solid Waste Section.
d. Ground water monitoring wells and surface water sampling locations shall be
sampled prior to issuing the Permit to Operate.
e. CQA documentation as well as a certification by the project engineer that the
landfill was built in accordance with approved plans shall be submitted to the
Section.

BLUE RIDGE
PAPER PRODUCTS INC.
November 1, 2000
Mr. James Patterson
North Carolina Department of Environment
And Natural Resources
59 Woodfin Place
Asheville, North Carolina 28801
Re: Chemical and physical analysis of Canton Mill process wastes.
Dear Mr. Patterson:
Attached is laboratory analysis related to the latest sampling of Canton Mill process
wastes, including wastewater treatment plant sludge, lime mud, slaker grits, precoat filter
dregs, boiler fly ash, and boiler cinders. The analysis is in accordance with Permit
Number 44-06, Area A East, and 15A NCAC 13B, Section .103(d).
Samples were collected on September 28, 2000. Each sample was analyzed by TCLP for
RCRA metals, volatile organics, and semi volatile organics (excluding herbicides and
pesticides). In addition, the sludge, lime, dregs, and grits were tested for reactive cyanide
and reactive sulfide. No samples were found to be in excess of RCRA standards for the
tested parameters.
Please call me at 828-646-2028 if you have questions or comments.
Sincerely,
Jim Giauque
Attachments
Copy: Derric Brown
lile:pattersonl 11.doc
175 Main Street - P.O. Box 4000
Canton, North Carolina 28716 - Phone: [phone]
Raising Your Expectations

dceAnalytical
www.pacelabs.com
October 18, 2000
Mr. Jim Giaque
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
RE: Pace Project Number: 9315593
Client Project ID: Process Waste
Dear Mr. Giaque:
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s)received by the laboratory on September 28, 2000. If you have any
questions concerning this report, please feel free to contact me.
Sincerely,
Walter Miller
Project Manager
Enclosures
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

�(�O�Iacle'Analyticafm
www.pacelabs.com
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
Attn: Mr. Jim Giaque
Phone: [phone]
Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
54 Ravenscrolt Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
DATE: 10/25/00
PAGE: 1
Pace Project Number: 9315593
Client Project ID: Process Waste
Pace Sample No: 93675239 Date Collected: 09/28/00 Matrix: Soil
Client Sample ID: WWTP SLUDGE Date Received: 09/28/00
Parameters Results Units PRL Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ------------------ ----- ---------- ----------
Inorganics Prep
RCRA Metals, ICP, TCLP Leach.
Date Digested
Metals
RCRA Metals, ICP, TCLP Leach.
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Date Digested
Mercury, CVAAS, TCLP Leachate
Mercury
Selenium, AAS Furnace, TCLP
Selenium
Date Digested
Wet Chemistry
Percent Moisture
Percent Moisture
Method: EPA 6010
Method: EPA 6010
ND mg/l 0.5
0.750 mg/t 0.1
NO mg/l 0.01
ND mg/t 0.005
NO mg/l 0.1
NO mg/t 0.05
Method: EPA 7470
NO mg/l 0.0002
Method: EPA 7740
NO mg/l 0.005
Method: % Moisture
67.2
Prep Method: EPA 1311
10/12/00
Prep Method: EPA 3010
10/13/00 TRW 7440-38-2
10/13/00 TRW 7440-39-3
10/13/00 TRW 7440-43-9
10/13/00 TRW 7440-47-3
10/13/00 TRW 7439-92-1
10/13/00 TRW 7440-22-4
10/12/00
Prep Method: EPA 7470
10/17/00 TRW 7439-97-6
Prep Method: EPA 3020
10/11/00 JDA 7782-49-2
10/06/00
Prep Method:
09/29/00 JMS
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IN
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full,
g without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

Pace Analytical Services, Inc.
eAnalytical m 54 RDrive
Ashevilleville,, NC
28801
www.pacelabs.com Phone: [phone], 6
Fax: [phone]
DATE: 10/25/00
PAGE: 2
Pace Project Number: 9315593
Client Project ID: Process Waste
Pace Sample No: 93675247 Date Collected: 09/28/00 Matrix: Soil
Client Sample ID: LIME MUD Date Received: 09/28/00
Parameters Results Units PRL Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ------------------ ----- ---------- ----------
Inorganics Prep
RCRA Metals, ICP, TCLP Leach. Method: EPA 6010
Date Digested
Metals
RCRA Metals, ICP, TCLP Leach.
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Date Digested
Mercury, CVAAS, TCLP Leachate
Mercury
Selenium, AAS Furnace, TCLP
Selenium
Date Digested
Wet Chemistry
Percent Moisture
Percent Moisture
Method: EPA 6010
ND
mg/l
0.5
0.9
mg/l
0.1
ND
mg/l
0.01
ND
mg/t
0.005
NO
mg/l
0.1
ND
mg/l
0.05
Method: EPA 7470
ND
mg/l
0.0002
Method: EPA 7740
NO
mg/l
0.005
Method: % Moisture
35.5
Prep Method: EPA 1311
10/12/00
Prep Method: EPA 3010
10/13/00 TRW 7440-38-2
10/13/00 TRW 7440-39-3
10/13/00 TRW 7440-43-9
10/13/00 TRW 7440-47-3
10/13/00 TRW 7439-92-1
10/13/00 TRW 7440-22-4
10/12/00
Prep Method: EPA 7470
10/17/00 TRW 7439-97-6
Prep Method: EPA 3020
10/11/00 JDA 7782-49-2
10/06/00
Prep Method:
09/29/00 JMS
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full,
g without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

Pace Analytical Services, Inc.
e Analytical "' 54 R , coft Drive
Asheville, NC 28801
www.pacelabs.com Phone: [phone]
Fax: [phone]
DATE: 10/25/00
PAGE: 3
Pace Project Number: 9315593
Client Project ID: Process Waste
Pace Sample No: 93675254 Date Collected: 09/28/00 Matrix: Soil
Client Sample ID: SLAKER GRITS Date Received: 09/28/00
Parameters Results Units PRL Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- --------------- ----------
Inorganics Prep
RCRA Metals, ICP, TCLP Leach.
Date Digested
Metals
RCRA Metals, ICP, TCLP Leach.
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Date Digested
Mercury, CVAAS, TCLP Leachate
Mercury
Selenium, AAS Furnace, TCLP
Selenium
Date Digested
Wet Chemistry
Percent Moisture
Percent Moisture
Method: EPA 6010
Method: EPA 6010
ND
mg/t
0.5
0.51
mg/l
0.1
ND
mg/l
0.01
ND
mg/l
0.005
ND
mg/l
0.1
ND
mg/l
0.05
Method: EPA 7470
ND mg/t 0.0002
Method: EPA 7740
ND mg/l 0.005
Method: % Moisture
11.5
Prep Method: EPA 1311
10/12/00
Prep Method: EPA 3010
10/13/00 TRW 7440-38-2
10/13/00 TRW 7440-39-3
10/13/00 TRW 7440-43-9
10/13/00 TRW 7440-47-3
10/13/00 TRW 7439-92-1
10/13/00 TRW 7440-22-4
10/12/00
Prep Method: EPA 7470
10/17/00 TRW 7439-97-6
Prep Method: EPA 3020
10/11/00 JDA 7782-49-2
10/06/00
Prep Method:
09/29/00 JMS
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full,
g without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

Pace Analytical Services, Inc.
54 Ravenscrolt Drive
Analytical'u Asheville, NC 28801
www.pacelabs.com Phone: [phone]
Fax: [phone]
DATE: 10/25/00
PAGE: 4
Pace Project Number: 9315593
Client Project ID: Process Waste
Pace Sample No: 93675262 Date Collected: 09/28/00 Matrix: Soil
Client Sample ID: PRECOAT FILTER DREGS Date Received: 09/28/00
Parameters Results Units PRL Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- --------------- ----------
Inorganics Prep
RCRA Metals, ICP, TCLP Leach.
Date Digested
Metals
RCRA Metals, ICP, TCLP Leach.
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Date Digested
Mercury, CVAAS, TCLP Leachate
Mercury
Selenium, AAS Furnace, TCLP
Selenium
Date Digested
Wet Chemistry
Percent Moisture
Percent Moisture
Method: EPA 6010
Method: EPA 6010
ND
mg/t
0.5
0.72
mg/l
0.1
ND
mg/L
0.01
ND
mg/l
0.005
ND
mg/l
0.1
0.003
mg/t
0.002
Method: EPA 7470
0.00022 mg/t 0.0002
Method: EPA 7740
ND mg/l 0.005
Method: % Moisture
50.0
Prep Method: EPA 1311
10/12/00
Prep Method: EPA 3010
10/13/00 TRW 7440-38-2
10/13/00 TRW 7440-39-3
10/13/00 TRW 7440-43-9
10/13/00 TRW 7440-47-3
10/13/00 TRW 7439-92-1
10/13/00 TRW 7440-22-4
10/12/00
Prep Method: EPA 7470
10/17/00 TRW 7439-97-6
Prep Method: EPA 3020
10/11/00 JDA 7782-49-2
10/06/00
Prep Method:
09/29/00 JMS
Laboratory Certification IDS REPORT OF LABORATORY ANALYSIS Laboratory Certification IN
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
Analytical � 54 Rville, Drive
Asheville, NC
28801
www.pacelabs.com Phone: [phone]
Fax: [phone]
DATE: 10/25/00
PAGE: 5
Pace Project Number: 9315593
Client Project ID: Process Waste
Pace Sample No: 93675312 Date Collected: 09/28/00 Matrix: Soil
Client Sample ID: FLYASH-TOTAL Date Received: 09/28/00
Parameters Results Units PRL Analyzed Analyst CAS# Footnotes
---------------------------------------------------- ---------- -------- ----- ---------- ----------
Inorganics Prep
RCRA Metals, ICP, TCLP Leach.
Method:
EPA
6010
Date Digested
Metals
RCRA Metals, ICP, TCLP Leach.
Method:
EPA
6010
Arsenic
0.005
mg/t
0.5
Barium
0.22
mg/l
0.1
Cadmium
0.010
mg/t
0.01
Chromium
0.005
mg/l
0.005
Lead
ND
mg/l
0.1
Silver
ND
mg/l
0.05
Date Digested
Mercury, CVAAS, TCLP Leachate
Method:
EPA
7470
Mercury
ND
mg/t
0.0002
Selenium, AAS Furnace, TCLP
Method:
EPA
7740
Selenium
0.026
mg/t
0.005
Date Digested
Wet Chemistry
Percent Moisture
Method:
% Moisture
Percent Moisture
8.9
Prep Method: EPA 1311
10/12/00
Prep Method: EPA 3010
10/13/00 TRW 7440-38-2
10/13/00 TRW 7440-39-3
10/13/00 TRW 7440-43-9
10/13/00 TRW 7440-47-3
10/13/00 TRW 7439-92-1
10/13/00 TRW 7440-22-4
10/12/00
Prep Method: EPA 7470
10/17/00 TRW 7439-97-6
Prep Method: EPA 3020
10/11/00 JDA 7782-49-2
10/06/00
Prep Method:
09/29/00 JMS
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 This report shall not be reproduced, except in full, TN Drinking Water 02980
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

Pace Analytical Services, Inc.
Mnalytical m . As Raven, Asheville
C Drive
AsNC 28801
www.pacelabs.com Phone: [phone]
fax: 828.252,4618
DATE: 10/25/00
PAGE: 6
Pace Project Number: 9315593
Client Project ID: Process Waste
Pace Sample No: 93675320 Date Collected: 09/28/00 Matrix: Soil
Client Sample ID: CINDERS-BB/PG/RC/#4 Date Received: 09/28/00
Parameters Results Units PRL Analyzed Analyst CAS# Footnotes
---------------------------------------------------------------------- ----- ---------- ----------
Inorganics Prep
RCRA Metals, ICP, TCLP Leach
Date Digested
Metals
RCRA Metals, ICP, TCLP Leach.
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Date Digested
Mercury, CVAAS, TCLP Leachate
Mercury
Selenium, AAS Furnace, TCLP
Selenium
Date Digested
Wet Chemistry
Percent Moisture
Percent Moisture
Method: EPA 6010
Method: EPA 6010
ND
mg/1
0.5
1.9
mg/l
0.1
ND
mg/t
0.01
ND
mg/l
0.005
ND
mg/l
0.1
ND
mg/t
0.05
Method: EPA 7470
0.0004 mg/l 0.0002
Method: EPA 7740
ND mg/t 0.005
Method: % Moisture
55.6
Prep Method: EPA 1311
10/12/00
Prep Method: EPA 3010
10/13/00 TRW 7440-38-2
10/13/00 TRW 7440-39-3
10/13/00 TRW 7440-43-9
10/13/00 TRW 7440-47-3
10/13/00 TRW 7439-92-1
10/13/00 TRW 7440-22-4
10/13/00
Prep Method: EPA 7470
10/17/00 TRW 7439-97-6
Prep Method: EPA 3020
10/11/00 JDA 7782-49-2
10/06/00
Prep Method:
09/29/00 JMS
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IN
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscrott Drive
e Analytical m Asheville, NC 28801
www.pacelabs.com Phone: [phone]
Fax: [phone]
DATE: 10/25/00
PAGE: 7
Pace Project Number: 9315593
Client Project 1D: Process Waste
Pace Sample No: 93675338 Date Collected: 09/28/00 Matrix: Soil.
Client Sample ID: CINDERS-RILEY BARK Date Received: 09/28/00
Parameters Results Units PRL Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- ------------------- -------- --------------- ----------
Inorganics Prep
RCRA Metals, ICP, TCLP Leach
Date Digested
Metals
RCRA Metals, ICP, TCLP Leach.
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Date Digested
Mercury, CVAAS, TCLP Leachate
Mercury
Selenium, AAS Furnace, TCLP
Selenium
Date Digested
Wet Chemistry
Percent Moisture
Percent Moisture
Method: EPA 6010
Method: EPA 6010
NO
mg/L
0.5
0.770
mg/l
0.1
0.001
mg/l
0.01
0.006
mg/t
0.005
NO
mg/l
0.1
NO
mg/t
0.05
Method: EPA 7470
NO mg/L 0.0002
Method: EPA 7740
NO mg/t 0.005
Method: % Moisture
25.5
Prep Method: EPA 1311
10/12/00
Prep Method: EPA 3010
10/13/00 TRW 7440-38-2
10/13/00 TRW 7440-39-3
10/13/00 TRW 7440-43-9
10/13/00 TRW 7440-47-3
10/13/00 TRW 7439-92-1
10/13/00 TRW 7440-22-4
10/13/00
Prep Method: EPA 7470
10/17/00 TRW 7439-97-6
Prep Method: EPA 3020
10/11/00 JDA 7782-49-2
10/06/00
Prep Method:
09/29/00 JMS
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IN
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full,
g without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

ace Analytical Tm
www.pacelabs.com
PARAMETER FOOTNOTES
NO Not Detected
NC Not Calculable
PRL Pace Reporting Limit
Pace Analytical Services, Inc.
54 Ravenscrolt Drive
Asheville, NC 28801
Phone: [phone]
DATE: 10/18/00 Fax:[phone]
PAGE: 8
Pace Project Number: 9315593
Client Project ID: Process Waste
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 This report shall not be reproduced, except in full, TN Drinking Water 02980
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

ac e Analytical
www.pacelabs.com
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton. NC 28716
Attn: Mr. Jim Giaque
Phone: [phone]
QC Batch ID: 15247
Analysis Method: X Moisture
Associated Pace Samples:
SAMPLE DUPLICATE: 93677896
Parameter
--------------------- ---------
Percent Moisture
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
QUALITY CONTROL DATA DATE: 10/18/00 Fax:828.252,4618
PAGE: 9
Pace Project Number: 9315593
Client Project ID: Process Waste
QC Batch Method:
Analysis Description: Percent Moisture
93675239 93675247 93675254 93675262 93675312
93675320 93675338
Dup.
Units 93673663 Result RPD
------------------------------ -----
% 41.70 42.00 1
Footnotes
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full,
g without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

ace Analytical m
www.pacelabs.com
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
Attn: Mr. Jim Giaque
Phone: [phone]
QC Batch ID: 15323
Analysis Method: EPA 7740
Associated Pace Samples:
METHOD BLANK: 93680254
Associated Pace Samples:
Pace Analytical Services, Inc.
54 Ravenscroit Drive
Asheville, NC 28801
Phone: [phone]
QUALITY CONTROL DATA DATE: 10/18/00 Fax:[phone]
PAGE: 10
Pace Project Number: 9315593
Client Project ID: Process Waste
QC Batch Method: EPA 3020
Analysis Description: Selenium, AAS Furnace, TCLP
93675239 93675247 93675254 93675262 93675312
93675320 93675338
93675239 93675247 93675254 93675262 93675312 93675320 93675338
Method
Blank
Parameter Units Result PRL Footnotes
------------------------------ ----------.......... ----------..........
Selenium mg/l ND 0.005
MATRIX SPIKE: 93680262 Matrix
Spike Spike Spike
Parameter Units 93675239 Conc. Result X Rec Footnotes
------------------------------ ------------------------------------- -----..........
Selenium mg/l 0.003000 0.0300 0.02240 64.7 1
LABORATORY CONTROL SAMPLE: 93680288
Spike LCS Spike
Parameter Units Conc. Result X Rec Footnotes
------------------------------ --------------------------- ----- ..........
Selenium mg/l 0.0300 0.02820 94.0
SAMPLE DUPLICATE: 93680270
Dup.
Parameter Units 93675239 Result RPD Footnotes
------------------------------ ----------.......... .......... -----..........
Selenium mg/l NO ND NC
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 This report shall not be reproduced, except in full, TN Drinking Water 02980
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

aceAnalytical'm
www.pacelabs.com
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
Attn: Mr. Jim Giaque
Phone: [phone]
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
QUALITY CONTROL DATA DATE: 10/18/00 Fax:[phone]
PAGE: 12
Pace Project Number: 9315593
Client Project ID: Process Waste
QC Batch ID: 15548 QC Batch Method: EPA 7470
Analysis Method: EPA 7470 Analysis Description: Mercury, CVAAS, TCLP Leachate
Associated Pace Samples: 93675239 93675247 93675254 93675262 93675312
93675320 93675338
METHOD BLANK: 93690618
Associated Pace Samples:
93675239 93675247 93675254 93675262 93675312 93675320 93675338
Method
Blank
Parameter Units Result PRL Footnotes
------------------------------ ---------- .......... ----------..........
Mercury mg/l ND 0.0002
LABORATORY CONTROL SAMPLE: 93690642
Spike LCS Spike
Parameter Units Conc. Result % Rec Footnotes
------------------------------ --------------------------- ----- ----------
Mercury mg/l 0.0050 0.005430 109
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravensctott Drive
e Analytical m Asheville, NC 28801
www.pacelabs.com Phone: 828,254.7176
DATE: 10/18/00 Fax:[phone]
PAGE: 13
Pace Project Number: 9315593
Client Project ID: Process Waste
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate X Rec and RPD values.
NO Not Detected
NC Not Calculable
PRL Pace Reporting Limit
RPD Relative Percent Difference
El) Due to matrix interference the matrix spike and/or matrix spike duplicate do not provide reliable values. Sample
results for this QC batch accepted based on LCS and/or LCSD X Recovery and/or RPD values.
Laboratory Certification IDS REPORT OF LABORATORY ANALYSIS Laboratory Certification IN
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

aceAnalytical "
www.pacelabs.com
Mr. Jim Giaque
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
702103/CHAMPION INT
Client Reference: Process Waste
Pace Project No: 9315593
Quantity U/M Description
ANALYTICAL Charges:
7.00
ea
7.00
ea
7.00
ea
7.00
ea
7.00
ea
7.00
ea
7.00
ea
7.00
ea
7:00
ea
7.00
ea
4.00
ea
4.00
ea
7.00
ea
7.00
ea
7.00
ea
C03226
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
54 Ravenscroft Drive
je, W801
10/lfbo0e: 828.254.7176
Fax: [phone]
Pace Analytical Services, Inc.
NW 8922
P.O. Box 1450
Minneapolis, MN 55485-8922
Walter Miller Due Upon Receipt 1
Method Matrix Price Total
Percent Moisture
X Moisture
Soil
Acid Digestion
Soil
60.00
Silver
EPA
6010
Soil
10.00
Arsenic
EPA
6010
Soil
10.00
Barium
EPA
6010
Soil
10.00
Cadmium
EPA
6010
Soil
10.00
Chromium
EPA
6010
Soil
10.00
Lead
EPA
6010
Soil
10.00
Mercury, CVAAS, TCLP Leachate
EPA
7470
Soil
28.00
Selenium, AAS Furnace, TCLP
EPA
7740
Soil
12.00
Reactive Cyanide
Soil
50.00
Reactive Sulfide
Soil
50.00
Sample Preparation
Soil
70.00
Volatile Organics, EPA 8260
Soil
100.00
Semi -Vol. Organics. EPA 8270
Soil
250.00
ANALYTICAL SUBTOTAL:
TOTAL INVOICE AMOUNT:
N/C
$ 420.00
$ 70.00
$ 70.00
$ 70.00
$ 70.00
$ 70.00
$ 70.00
$ 196.00
$ 84.00
$ 200.00
$ 200.00
$ 490.00
$ 700.00
$ 1750.00
$ 4460.00
--------------
$ 4460.00
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 This report shA"R%7iId%tFffid, except in full, TN Drinking Water 02980
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. SC Environmental 99030

- aceAnalyticalrm
www.pacelabs.com
Mr. Jim Giaque
Blue Ridge Paper Products Inc.
Main St.
PO Box 4000
Canton, NC 28716
54 Ravenscroft Drive Pace Analytical Services, Inc.
Asheville, NC 28801 ****,h5t&nn"0-0rive
Phone: [phone]&ville, NC28801
Fax: [phone] Phone:[phone]
Far 828.252.4618
702103/CHAMPION INT C03226 Walter Miller
The above charges are for the following samples:
Spl# Description/Client ID Received
93675239
WWTP SLUDGE
09/28/00
93675247
LIME MUD
09/28/00
93675254
SLAKER GRITS
09/28/00
93675262
PRECOAT FILTER DREGS
09/28/00
93675312
FLYASH-TOTAL
09/28/00
93675320
CINDERS-BB/PG/RC/#4
09/28/00
93675338
CINDERS-RILEY BARK
09/28/00
Pace Analytical Services, Inc.
NW 8922
P.O. Box 1450
Minneapolis, MN 55485.8922
Due Upon Receipt 2
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

(��a'cie'A na lyticalTM
Blue Ridge Paper Products, Inc.
P. 0. Box 4000
Canton, NC 28716
Attn: Mr. Jim Giaque
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
fax: 704.875, 9091
DATE: 10/11/00
PAGE: 1
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Solid results are reported on a dry weight basis
Pace Sample No: 93675239 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: WWTP SLUDGE Date Received: 09/28/00
Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ------------------ -------- --------------- ----------
Inorganics Prep
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method: EPA
1311
Date Leached
0.00
1.00
10/06/00
DLH
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method:
EPA
8260
Vinyl Chloride
ND
mg/t
0.02
1.00
10/11/00
CBD
75-01-4
1,1-Dichloroethene
ND
mg/t
0.02
1.00
10/11/00
CBD
75-35-4
2-Butanone
ND
mg/l
0.4
1.00
10/11/00
CBD
78-93-3
Chloroform
ND
mg/l
0.02
1.00
10/11/00
CBD
67-66-3
1,2-Dichloroethane
ND
mg/l
0.02
1.00
10/11/00
CBD
107-06-2
Carbon Tetrachloride
ND
mg/1
0.02
1.00
10/11/00
CBD
56-23-5
Benzene
ND
mg/l
0.02
1.00
10/11/00
CBD
71-43-2
Trichloroethene
ND
mg/t
0.02
1.00
10/11/00
CBD
79-01-6
Tetrachloroethene
ND
mg/t
0.02
1.00
10/11/00
CBD
127-18-4
Chlorobenzene
ND
mg/1
0.02
1.00
10/11/00
CBD
108-90-7
Dibromofluoromethane (S)
105
%
1.00
10/11/00
CBD
1868-53-7
1,2-Dichloroethane-d4 (S)
102
%
1.00
10/11/00
CBD
17060-07-0
Toluene-d8 (S)
98
%
1.00
10/11/00
CBD
2037-26-5
4-Bromofluorobenzene (S)
98
%
1.00
10/11/00
CBD
460-00-4
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Method: EPA 8270
Prep Method:
EPA
3510
Pyridine
ND
mg/l
0.5
1.00
10/11/00
DHJ
110-86-1
1,4-Dichlorobenzene
ND
mg/l
0.75
1.00
10/11/00
DHJ
106-46-7
2-Methylphenol
ND
mg/l
20
1.00
10/11/00
DHJ
95-48-7
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical Phone:
NC 28078
Phone: [phone]
Fax [phone]
DATE: 10/11/00
PAGE: 2
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675239 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: WWTP SLUDGE Date Received: 09/28/00
Parameters
---------------------------------
Results
----------
Units
---------
PRL
----------
App. DF
--------
Analyzed
--------
Analyst CAS# Footnotes
----- ---------- ----------
Hexachloroethane
ND
mg/l
0.3
1.00
10/11/00
DHJ
67-72-1
3&4-Methylphenol
ND
mg/l
20
1.00
10/11/00
DHJ
Nitrobenzene
ND
mg/l
0.2
1.00
10/11/00
DHJ
98-95-3
Hexachloro-1,3-butadiene
ND
mg/t
0.05
1.00
10/11/00
DHJ
87-68-3
2,4,6-Trichlorophenol
ND
mg/l
0.2
1.00
10/11/00
DHJ
88-06-2
2,4,5-Trichlorophenol
ND
mg/l
40
1.00
10/11/00
DHJ
95-95-4
2,4-Dinitrotoluene
ND
mg/t
0.013
1.00
10/11/00
DHJ
121-14-2
Hexachlorobenzene
ND
mg/l
0.013
1.00
10/11/00
DHJ
118-74-1
Pentachlorophenol
ND
mg/l
10
1.00
10/11/00
DHJ
87-86-5
Nitrobenzene-d5 (S)
75
%
1.00
10/11/00
DHJ
4165-60-0
2-Fluorobiphenyl (S)
57
%
1.00
10/11/00
DHJ
321-60-8
Terphenyl-d14 (S)
76
%
1.00
10/11/00
DHJ
1718-51-0
Phenol-c16 (S)
28
%
1.00
10/11/00
DHJ
13127-88-3
2-Fluorophenol (S)
41
%
1.00
10/11/00
DHJ
367-12-4
2,4,6-Tribromophenol (S)
101
%
1.00
10/11/00
DHJ
118-79-6
Date Extracted
10/10/00
Laboratory Certification IN Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
o. Analytical m Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 3
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675247 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: LIME MUD Date Received: 09/28/00
Parameters Results Units PRL App. OF Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ------------------ -------- ----- ---------- ----------
Inorganics Prep
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method: EPA
1311
Date Leached
0.00
1.00
10/06/00
DLH
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method: EPA
8260
Vinyl Chloride
ND
mg/t
0.02
1.00
10/11/00
CBD
75-01-4
1,1-Dichloroethene
ND
mg/t
0.02
1.00
10/11/00
CBD
75-35-4
2-Butanone
NO
mg/t
0.4
1.00
10/11/00
CBD
78-93-3
Chloroform
NO
mg/t
0.02
1.00
10/11/00
CBD
67-66-3
1,2-Dichloroethane
ND
mg/l
0.02
1.00
10/11/00
CBD
107-06-2
Carbon Tetrachloride
ND
mg/l
0.02
1.00
10/11/00
CBD
56-23-5
Benzene
ND
mg/t
0.02
1.00
10/11/00
CBD
71-43-2
Trichloroethene
NO
mg/t
0.02
1.00
10/11/00
CBD
79-01-6
Tetrachtoroethene
NO
mg/t
0.02
1.00
10/11/00
CBD
127-18-4
Chlorobenzene
ND
mg/t
0.02
1.00
10/11/00
CBD
108-90-7
Dibromofluoromethane (S)
107
%
1.00
10/11/00
CBD
1868-53-7
1,2-Dichloroethane-d4 (S)
103
%
1.00
10/11/00
CBD
17060-07-0
Toluene-d8 (S)
99
%
1.00
10/11/00
CBD
2037-26-5
4-Bromofluorobenzene (S)
96
%
1.00
10/11/00
CBD
460-00-4
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Method: EPA 8270
Prep Method:
EPA
3510
Pyridine
ND
mg/l
0.5
1.00
10/10/00
DHJ
110-86-1
1,4-Dichlorobenzene
ND
mg/t
0.75
1.00
10/10/00
DHJ
106-46-7
2-Methylphenot
NO
mg/t
20
1.00
10/10/00
DHJ
95-48-7
Hexachloroethane
NO
mg/l
0.3
1.00
10/10/00
DHJ
67-72-1
3&4-Methylphenot
ND
mg/l
20
1.00
10/10/00
DHJ
Nitrobenzene
NO
mg/l
0.2
1.00
10/10/00
DHJ
98-95-3
Hexachloro-1,3-butadiene
ND
mg/l
0.05
1.00
10/10/00
DHJ
87-68-3
2,4,6-Trichlorophenol
ND
mg/t
0.2
1.00
10/10/00
DHJ
88-06-2
2,4,5-Trichlorophenol
ND
mg/l
40
1.00
10/10/00
DHJ
95-95-4
2,4-Dinitrotoluene
ND
mg/l
0.013
1.00
10/10/00
DHJ
121-14-2
Hexachlorobenzene
ND
mg/l
0.013
1.00
10/10/00
DHJ
118-74-1
Pentachlorophenol
ND
mg/l
10
1.00
10/10/00
DHJ
87-86-5
Nitrobenzene-d5 (S)
48
%
1.00
10/10/00
DHJ
4165-60-0
Laboratory Certification IDS REPORT OF LABORATORY ANALYSIS Laboratory Certification IDS
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Mnalytical m Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 4
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675247 Date Collected: 09/28/00 Matrix: Other
Client sample ID: LIME MUD Date Received: 09/28/00
Parameters
---------------------------------
Results
----------
Units PRL
--------- ----------
App. DF
Analyzed
Analyst CAS# ' Footnotes
---------- ----------
2-Fluorobiphenyl (S)
43
%
--------
1.00
--------
10/10/00
-----
DHJ 321-60-8 1
Terphenyl-dl4 (S)
55
%
1.00
10/10/00
DHJ 1718-51-0
Phenol-d6 (S)
18
%
1.00
10/10/00
DHJ 13127-88-3
2-Fluorophenol (S)
31
%
1.00
10/10/00
DHJ 367-12-4
2,4,6-Tribromophenol (S)
72
%
1.00
10/10/00
DHJ 118-79-6
Date Extracted
10/10/00
Laboratory Certification IN Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
AA ianlytical m Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 5
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675254 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: SLAKER GRITS Date Received: 09/28/00
Parameters
---------------------------------
Results Units
---------- ---------
PRL
----------
App. OF
--------
Analyzed
--------
Analyst CAS# Footnotes
----- ---------- ----------
Inorganics Prep
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method: EPA
1311
Date Leached
0.00
1.00
10/06/00
DLH
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method:
EPA
8260
Vinyl Chloride
ND
mg/t
0.02
1.00
10/11/00
CBD
75-01-4
1,1-Dichloroethene
NO
mg/t
0.02
1.00
10/11/00
CBD
75-35-4
2-Butanone
ND
mg/l
0.4
1.00
10/11/00
CBD
78-93-3
Chloroform
NO
mg/l
0.02
1.00
10/11/00
CBD
67-66-3
1,2-Dichloroethane
ND
mg/l
0.02
1.00
10/11/00
CBD
107-06-2
Carbon Tetrachloride
NO
mg/l
0.02
1.00
10/11/00
CBD
56-23-5
Benzene
ND
mg/l
0.02
1.00
10/11/00
CBD
71-43-2
Trichloroethene
NO
mg/t
0.02
1.00
10/11/00
CBD
79-01-6
Tetrachloroethene
ND
mg/l
0.02
1.00
10/11/00
CBD
127-18-4
Chlorobenzene
ND
mg/t
0.02
1.00
10/11/00
CBD
108-90-7
Dibromoftuoromethane (S)
104
%
1.00
10/11/00
CBD
1868-53-7
1,2-Dichloroethane-d4 (S)
101
%
1.00
10/11/00
CBD
17060-07-0
Toluene-d8 (S)
101
%
1.00
10/11/00
CBD
2037-26-5
4-Bromofluorobenzene (S)
97
%
1.00
10/11/00
CBD
460-00-4
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Method: EPA 8270
Prep Method: EPA
3510
Pyridine
ND
mg/l
0.5
1.00
10/10/00
DHJ
110-86-1
1,4-Dichlorobenzene
NO
mg/t
0.75
1.00
10/10/00
DHJ
106-46-7
2-Methylphenot
ND
mg/t
20
1.00
10/10/00
DHJ
95-48-7
Hexachloroethane
NO
mg/l
0.3
1.00
10/10/00
DHJ
67-72-1
3&4-Methylphenot
NO
mg/t
20
1.00
10/10/00
DHJ
Nitrobenzene
NO
mg/l
0.2
1.00
10/10/00
DHJ
98-95-3
Hexachloro-1,3-butadiene
NO
mg/l
0.05
1.00
10/10/00
DHJ
87-68-3
2,4,6-Trichlorophenol
NO
mg/l
0.2
1.00
10/10/00
DHJ
88-06-2
2,4,5-Trichlorophenol
NO
mg/t
40
1.00
10/10/00
DHJ
95-95-4
2,4-Dinitrotoluene
NO
mg/t
0.013
1.00
10/10/00
DHJ
121-14-2
Hexachlorobenzene
NO
mg/l
0.013
1.00
10/10/00
DHJ
118-74-1
Pentachlorophenol
NO
mg/l
10
1.00
10/10/00
DHJ
87-86-5
Nitrobenzene-d5 (S)
52
%
1.00
10/10/00
DHJ
4165-60-0
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

aceAnalytical"
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 6
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675254 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: SLAKER GRITS Date Received: 09/28/00
Parameters
---------------------------------
Results
Units PRL
App. DF
Analyzed
Analyst
CAS# Footnotes
2-Fluorobiphenyl (S)
----------
45
--------- ----------
%
--------
1.00
--------
10/10/00
-----
DHJ
---------- ----------
321-60-8
Terphenyl-d14 (S)
60
%
1.00
10/10/00
DHJ
1718-51-0
Phenol-d6 (S)
19
%
1.00
10/10/00
DHJ
13127-88-3
2-Fluorophenol (S)
34
%
1.00
10/10/00
DHJ
367-12-4
2,4,6-Tribromophenol (S)
75
%
1.00
10/10/00
DHJ
118-79-6
Date Extracted
10/10/00
Laboratory Certification IDs Laboratory Certification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
ace Analytical'" Huntersville. NC 28078
Phone: [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 7
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675262 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: PRECOAT FILTER DREGS Date Received: 09/28/00
Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes
---------------------------------------------------------------------- -------- ----- ---------- ----------
Inorganics Prep
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method: EPA
1311
Date Leached
0.00
1.00
10/06/00
DLH
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method:
EPA
8260
Vinyl Chloride
ND
mg/t
0.02
1.00
10/11/00
CBD
75-01-4
1,1-Dichloroethene
ND
mg/l
0.02
1.00
10/11/00
CBD
75-35-4
2-Butanone
ND
mg/t
0.4
1.00
10/11/00
CBD
78-93-3
Chloroform
ND
mg/l
0.02
1.00
10/11/00
CBD
67-66-3
1,2-Dichtoroethane
ND
mg/l
0.02
1.00
10/11/00
CBD
107-06-2
Carbon Tetrachloride
ND
mg/l
0.02
1.00
10/11/00
CBD
56-23-5
Benzene
ND
mg/l
0.02
1.00
10/11/00
CBD
71-43-2
Trichloroethene
ND
mg/1
0.02
1.00
10/11/00
CBD
79-01-6
Tetrachloroethene
ND
mg/t
0.02
1.00
10/11/00
CBD
127-18-4
Chlorobenzene
ND
mg/l
0.02
1.00
10/11/00
CBD
108-90-7
Dibromofluoromethane (S)
104
%
1.00
10/11/00
CBD
1868-53-7
1,2-Dichloroethane-d4 (S)
102
%
1.00
10/11/00
CBD
17060-07-0
Toluene-d8 (S)
100
%
1.00
10/11/00
CBD
2037-26-5
4-Bromofluorobenzene (S)
98
%
1.00
10/11/00
CBD
460-00-4
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Method: EPA 8270
Prep Method:
EPA
3510
Pyridine
ND
mg/l
0.5
1.00
10/10/00
DHJ
110-86-1
1,4-Dichlorobenzene
ND
mg/t
0.75
1.00
10/10/00
DHJ
106-46-7
2-Methylphenol
ND
mg/l
20
1.00
10/10/00
DHJ
95-48-7
Hexachloroethane
ND
mg/t
0.3
1.00
10/10/00
DHJ
67-72-1
3&4-Methylphenol
ND
mg/l
20
1.00
10/10/00
DHJ
Nitrobenzene
NO
mg/l
0.2
1.00
10/10/00
DHJ
98-95-3
Hexachloro-1,3-butadiene
ND
mg/l
0.05
1.00
10/10/00
DHJ
87-68-3
2,4,6-Trichlorophenol
ND
mg/t
0.2
1.00
10/10/00
DHJ
88-06-2
2,4,5-Trichlorophenol
ND
mg/l
40
1.00
10/10/00
DHJ
95-95-4
2,4-Dinitrototuene
ND
mg/t
0.013
1.00
10/10/00
DHJ
121-14-2
Hexachlorobenzene
ND
mg/l
0.013
1.00
10/10/00
DHJ
118-74-1
Pentachlorophenol
ND
mg/l
10
1.00
10/10/00
DHJ
87-86-5
Nitrobenzene-d5 (S)
51
%
1.00
10/10/00
DHJ
4165-60-0
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

aceAnalyticalm
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 8
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675262 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: PRECOAT FILTER DREGS Date Received: 09/28/00
Parameters
---------------------------------
Results
----------
Units PRL
App. DF
Analyzed
Analyst CAS# Footnotes
2-Fluorobiphenyl (S)
47
--------- ----------
%
--------
1.00
--------
10/10/00
----- ---------- ----------
DHJ 321-60-8
Terphenyl-d14 (S)
62
%
1.00
10/10/00
DHJ 1718-51-0
Phenol-d6 (S)
19
%
1.00
10/10/00
DHJ 13127-88-3
2-Fluorophenol (S)
30
%
1.00
10/10/00
DHJ 367-12-4
2,4,6-Tribromophenol (S)
71
%
1.00
10/10/00
DHJ 118-79-6
Date Extracted
10/10/00
Laboratory Certification IN REPORT -OF LABORATORY ANALYSIS Laboratory Certification IDs
.
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
SC 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical m Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
DATE: 10/11/00
PAGE: 9
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675312 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: FLYASH-TOTAL Date Received: 09/28/00
Parameters
---------------------------------
Results Units
-------------------
PRL
----------
App. DF
--------
Analyzed
--------
Analyst CAS# Footnotes
----- ---------- ----------
Inorganics Prep
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method: EPA
1311
Date Leached
0.00
1.00
10/07/00
KSB
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method:
EPA
8260
Vinyl Chloride
ND
mg/l
0.02
1.00
10/11/00
CBD
75-01-4
1,1-Dichloroethene
NO
mg/l
0.02
1.00
10/11/00
CBD
75-35-4
2-Butanone
ND
mg/l
0.4
1.00
10/11/00
CBD
78-93-3
Chloroform
ND
mg/l
0.02
1.00
10/11/00
CBD
67-66-3
1,2-Dichloroethane
ND
mg/l
0.02
1.00
10/11/00
CBD
107-06-2
Carbon Tetrachloride
NO
mg/t
0.02
1.00
10/11/00
CBD
56-23-5
Benzene
ND
mg/l
0.02
1.00
10/11/00
CBD
71-43-2
Trichloroethene
ND
mg/L
0.02
1.00
10/11/00
CBD
79-01-6
Tetrachloroethene
ND
mg/l
0.02
1.00
10/11/00
CBD
127-18-4
Chlorobenzene
ND
mg/t
0.02
1.00
10/11/00
CBD
108-90-7
Dibromofluoromethane (S)
108
%
1.00
10/11/00
CBD
1868-53-7
1,2-Dichloroethane-d4 (S)
106
%
1.00
10/11/00
CBD
17060-07-0
Toluene-d8 (S)
100
%
1.00
10/11/00
CBD
2037-26-5
4-Bromofluorobenzene (S)
97
%
1.00
10/11/00
CBD
460-00-4
GC/MS Semivolatiles
Semivolatite Organics, TCLP
Method: EPA 8270
Prep Method: EPA
3510
Pyridine
NO
mg/L
0.5
1.00
10/10/00
DHJ
110-86-1
1,4-Dichlorobenzene
ND
mg/l
0.75
1.00
10/10/00
DHJ
106-46-7
2-Methylphenol
NO
mg/t
20
1.00
10/10/00
DHJ
95-48-7
Hexachloroethane
ND
mg/t
0.3
1.00
10/10/00
DHJ
67-72-1
3&4-Methylphenot
NO
mg/t
20
1.00
10/10/00
DHJ
Nitrobenzene
ND
mg/t
0.2
1.00
10/10/00
DHJ
98-95-3
Hexachloro-1,3-butadiene
NO
mg/l
0.05
1.00
10/10/00
DHJ
87-68-3
2,4,6-Trichlorophenol
NO
mg/l
0.2
1.00
10/10/00
DHJ
88-06-2
2,4,5-Trichlorophenol
NO
mg/t
40
1.00
10/10/00
DHJ
95-95-4
2,4-Dinitrotoluene
ND
mg/l
0.013
1.00
10/10/00
DHJ
121-14-2
Hexachlorobenzene
NO
mg/t
0.013
1.00
10/10/00
DHJ
118-74-1
Pentachlorophenol
ND
mg/l
10
1.00
10/10/00
DHJ
87-86-5
Nitrobenzene-d5 (S)
55
%
1.00
10/10/00
DHJ
4165-60-0
Laboratory Certification IDS REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Analytical m Hunters ville, NC 28078
Phone:[phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 10
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675312 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: FLYASH-TOTAL Date Received: 09/28/00
Parameters
---------------------------------
Results
----------
Units PRL
App. DF
Analyzed
Analyst
CAS# Footnotes
2-Fluorobiphenyl (S)
47
--------- ----------
%
--------
1.00
--------
10/10/00
-----
DHJ
---------- ----------
321-60-8
Terphenyl-dl4 (S)
61
%
1.00
10/10/00
DHJ
1718-51-0
Phenol-d6 (S)
19
%
1.00
10/10/00
DHJ
13127-88-3
2-Fluorophenol (S)
33
%
1.00
10/10/00
DHJ
367-12-4
2,4,6-Tribromophenol (S)
70
%
1.00
10/10/00
DHJ
118-79-6
Date Extracted
10/10/00
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical m Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 11
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675320 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: CINDERS-BB/PG/RC/#4 Date Received: 09/28/00
Parameters
---------------------------------
Results Units
---------- ---------
PRL
----------
App. DF
--------
Analyzed
--------
Analyst CAS# Footnotes
--------------- ----------
Inorganics Prep
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method:
EPA
1311
Date Leached
0.00
1.00
10/07/00
KSB
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method:
EPA
8260
Vinyl Chloride
ND
mg/l
0.02
1.00
10/11/00
CBD
75-01-4
1,1-Dichloroethene
ND
mg/t
0.02
1.00
10/11/00
CBD
75-35-4
2-Butanone
ND
mg/t
0.4
1.00
10/11/00
CBD
78-93-3
Chloroform
ND
mg/l
0.02
1.00
10/11/00
CBD
67-66-3
1,2-Dichloroethane
NO
mg/l
0.02
1.00
10/11/00
CBD
107-06-2
Carbon Tetrachloride
ND
mg/t
0.02
1.00
10/11/00
CBD
56-23-5
Benzene
ND
mg/l
0.02
1.00
10/11/00
CBD
71-43-2
Trichloroethene
ND
mg/1
0.02
1.00
10/11/00
CBD
79-01-6
Tetrachloroethene
ND
mg/l
0.02
1.00
10/11/00
CBD
127-18-4
Chlorobenzene
ND
mg/t
0.02
1.00
10/11/00
CBD
108-90-7
Dibromofluoromethane (S)
104
%
1.00
10/11/00
CBD
1868-53-7
1,2-Dichloroethane-d4 (S)
103
%
1.00
10/11/00
CBD
17060-07-0
Toluene-d8 (S)
98
%
1.00
10/11/00
CBD
2037-26-5
4-BromofLuorobenzene (S)
100
%
1.00
10/11/00
CBD
460-00-4
GC/MS Semivolatiles
Semivolatile Organics, TCLP
Method: EPA 8270
Prep Method: EPA
3510
Pyridine
NO
mg/t
0.5
1.00
10/10/00
DHJ
110-86-1
1,4-Dichlorobenzene
ND
mg/1
0.75
1.00
10/10/00
DHJ
106-46-7
2-Methylphenol
ND
mg/l
20
1.00
10/10/00
DHJ
95-48-7
Hexachloroethane
ND
mg/1
0.3
1.00
10/10/00
DHJ
67-72-1
3&4-Methylphenol
ND
mg/1
20
1.00
10/10/00
DHJ
Nitrobenzene
ND
mg/l
0.2
1.00
10/10/00
DHJ
98-95-3
Hexachloro-1,3-butadiene
ND
mg/l
0.05
1.00
10/10/00
DHJ
87-68-3
2,4,6-Trichlorophenot
ND
mg/l
0.2
1.00
10/10/00
DHJ
88-06-2
2,4,5-Trichlorophenot
ND
mg/l
40
1.00
10/10/00
DHJ
95-95-4
2,4-Dinitrotoluene
ND
mg/l
0.013
1.00
10/10/00
DHJ
121-14-2
Hexachlorobenzene
ND
mg/l
0.013
1.00
10/10/00
DHJ
118-74-1
Pentachlorophenol
ND
mg/1
10
1.00
10/10/00
DHJ
87-86-5
Nitrobenzene-d5 (S)
61
%
1.00
10/10/00
DHJ
4165-60-0
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

(���a'c-eAnalyticalTM
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone. [phone]
Fax, 704.875.9091
DATE: 10/11/00
PAGE: 12
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675320 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: CINDERS-BB/PG/RC/#4 Date Received: 09/28/00
Parameters
---------------------------------
Results
----------
Units PRL
App. DF
Analyzed
Analyst
CAS# Footnotes
2-Fluorobiphenyt (S)
60
-------------------
%
--------
1.00
--------
10/10/00
-----
DHJ
--------------------
321-60-8
TerphenyL-dl4 (S)
85
%
1.00
10/10/00
DHJ
1718-51-0
PhenoL-d6 (S)
22
%
1.00
10/10/00
DHJ
13127-88-3
2-FLuorophenoL (S)
36
%
1.00
10/10/00
DHJ
367-12-4
2,4,6-TribromophenoL (S)
81
%
1.00
10/10/00
DHJ
118-79-6
Date Extracted
10/10/00
Laboratory Certification IN Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
SC 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical T Huntersville, NC 28078
Phone. [phone]
Fax:[phone]
DATE: 10/11/00
PAGE: 13
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Pace Sample No: 93675338 Date Collected: 09/28/00 Matrix: Other
Client Sample ID: CINDERS-RILEY BARK Date Received: 09/28/00
Parameters
---------------------------------
Results Units
---------- ---------
PRL
----------
App. DF
--------
Analyzed
--------
Analyst CAS# Footnotes
--------------- ----------
Inorganics Prep
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method: EPA
1311
Date Leached
0.00
1.00
10/07/00
KSB
GC/MS Volatiles
Volatile Organics, TCLP Leach.
Method: EPA 8260
Prep Method:
EPA
8260
Vinyl Chloride
ND
mg/l
0.02
1.00
10/11/00
CBD
75-01-4
1,1-Dichloroethene
ND
mg/l
0.02
1.00
10/11/00
CBD
75-35-4
2-Butanone
ND
mg/l
0.4
1.00
10/11/00
CBD
78-93-3
Chloroform
ND
mg/t
0.02
1.00
10/11/00
CBD
67-66-3
1,2-Dichloroethane
ND
mg/t
0.02
1.00
10/11/00
CBD
107-06-2
Carbon Tetrachloride
ND
mg/l
0.02
1.00
10/11/00
CBD
56-23-5
Benzene
ND
mg/l
0.02
1.00
10/11/00
CBD
71-43-2
Trichloroethene
ND
mg/l
0.02
1.00
10/11/00
CBD
79-01-6
Tetrachloroethene
ND
mg/t
0.02
1.00
10/11/00
CBD
127-18-4
Chlorobenzene
ND
mg/t
0.02
1.00
10/11/00
CBD
108-90-7
Dibromofluoromethane (S)
103
%
1.00
10/11/00
CBD
1868-53-7
1,2-Dichloroethane-d4 (S)
102
%
1.00
10/11/00
CBD
17060-07-0
Toluene-d8 (S)
99
%
1.00
10/11/00
CBD
2037-26-5
4-Bromofluorobenzene (S)
96
%
1.00
10/11/00
CBD
460-00-4
GC/MS Semivolati Les
Semivolatile Organics, TCLP
Method: EPA 8270
Prep Method:
EPA
3510
Pyridine
ND
mg/l
0.5
1.00
10/11/00
DHJ
110-86-1
1,4-Dichlorobenzene
ND
mg/t
0.75
1.00
10/11/00
DHJ
106-46-7
2-Methylphenol
ND
mg/t
20
1.00
10/11/00
DHJ
95-48-7
Hexachloroethane
NO
mg/l
0.3
1.00
10/11/00
DHJ
67-72-1
3&4-Methylphenol
ND
mg/l
20
1.00
10/11/00
DHJ
Nitrobenzene
ND
mg/l
0.2
1.00
10/11/00
DHJ
98-95-3
Hexachloro-1,3-butadiene
ND
mg/l
0.05
1.00
10/11/00
DHJ
87-68-3
2,4,6-Trichlorophenol
ND
mg/1
0.2
1.00
10/11/00
DHJ
88-06-2
2,4,5-Trichlorophenol
ND
mg/l
40
1.00
10/11/00
DHJ
95-95-4
2,4-Dinitrotoluene
ND
mg/1
0.013
1.00
10/11/00
DHJ
121-14-2
Hexachlorobenzene
ND
mg/l
0.013
1.00
10/11/00
DHJ
118-74-1
Pentachlorophenol
ND
mg/1
10
1.00
10/11/00
DHJ
87-86-5
Nitrobenzene-d5 (S)
56
%
1.00
10/11/00
DHJ
4165-60-0
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification INNC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

aceAnalyticaf"
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone. [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 14
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
'ace Sample No: 93675338 Date Collected: 09/28/00 Matrix: Other
:Bent Sample ID: CINDERS-RILEY BARK Date Received: 09/28/00
- 'arameters
---------------------------------
Results
----------
Units PRL
--------- ----------
App. DF
Analyzed
--------
Analyst
-----
CAS# Footnotes
--------------------
2-Fluorobiphenyl (S)
52
%
--------
1.00
10/11/00
DHJ
321-60-8
Terphenyl-d14 (S)
66
Y
1.00
10/11/00
DHJ
1718-51-0
Phenol-d6 (S)
22
%
1.00
10/11/00
DHJ
13127-88-3
2-Fluorophenol (S)
36
Y
1.00
10/11/00
DHJ
367-12-4
_ 2,4,6-Tribromophenol (S)
78
Y
1.00
10/11/00
DHJ
118-79-6
Date Extracted
10/10/00
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
SC 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical m Huntersville, NC 28078
Phone:[phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 15
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
PARAMETER FOOTNOTES
NO Not Detected
NC Not Calculable
PRL Pace Reporting Limit
(S) Surrogate
App. DF Applied Dilution Factor
L1) Base/neutral surrogate recovery outside of control Limits. The data was accepted based on valid recovery of remaining
two base/neutral surrogates.
Laboratory Certification IN LaboratoryCertification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking ater 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

aceAnalyticaf'
Blue Ridge Paper Products, Inc.
P. 0. Box 4000
Canton, NC 28716
Attn: Mr. Jim Giaque
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: 704.875.,9091
QUALITY CONTROL DATA DATE: 10/11/00
PAGE: 16
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
QC Batch ID: 32158 QC Batch Method: EPA 8260
Analysis Method: EPA 8260 Analysis Description: Volatile Organics, TCLP Leach.
Associated Pace Samples: 93675239 93675247 93675254 93675262 93675312
93675338
METHOD BLANK: 921255923
Associated Pace Samples:
93675239
93675247
93675254 93675262
Method
Blank
Parameter
------------------------------
Units
Result
PRL Footnotes
Vinyl Chloride
----------
mg/t
----------
NO
---------- ----------
0.02
1,1-Dichloroethene
mg/t
ND
0.02
2-Butanone
mg/l
ND
0.4
Chloroform
mg/l
NO
0.02
1,2-Dichloroethane
mg/t
NO
0.02
Carbon Tetrachloride
mg/t
ND
0.02
Benzene
mg/l
ND
0.02
Trichloroethene
mg/l
ND
0.02
Tetrachioroethene
mg/t
NO
0.02
Chlorobenzene
mg/t
NO
0.02
Dibromofluoromethane (S)
Y
105
1,2-Dichloroethane-d4 (S)
%
107
Toluene-d8 (S)
%
98
4-Bromofluorobenzene (S)
%
96
METHOD BLANK: 921257184
Associated Pace Samples:
93675312 93675338
Method
Blank
Parameter Units Result PRL Footnotes
------------------------------ ---------- ---------- ---------- ----------
Vinyl Chloride mg/l ND 0.02
Laboratory Certification IDs Laboratory Certification IDS
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
AAnalytical Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 10/11/00
PAGE: 17
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
METHOD BLANK: 921257184
Associated Pace Samples:
93675312
93675338
Method
Blank
Parameter
------------------------------
Units
Result
PRL Footnotes
-
1,1-Dichloroethene
----------
mg/l
----------
ND
---------- ----------
0.02
2-Butanone
mg/l
ND
0.4
Chloroform
mg/l
ND
0.02
1,2-Dichloroethane
mg/l
ND
0.02
Carbon Tetrachloride
mg/l
ND
0.02
Benzene
mg/l
ND
0.02
Trichloroethene
mg/l
ND
0.02
Tetrachloroethene
mg/l
ND
0.02
Chlorobenzene
mg/l
ND
0.02
Dibromofluoromethane (S)
%
104
1,2-Dichloroethane-d4 (S)
%
104
Toluene-d8 (S)
%
99
4-Bromofluorobenzene (S)
%
99
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
921257168 921257176
Matrix
Matrix
Spike
Spike
Spike
Spike
Sp. Dup.
Dup
Parameter
------------------------------
Units
93673663
Conc.
Result
% Rec
Result
% Rec
RPD Footnotes
Vinyl Chloride
----------
mg/l
----------
0
-------
0.2000
----------
0.2152
-----
108
----------
0.1836
-----
91.8
----- ----------
16
1,1-Dichloroethene
mg/t
0
0.2000
0.2960
148
0.2537
127
15
2-Butanone
mg/l
0
0.4000
0.1789
44.7
0.1594
39.8
12
Chloroform
mg/l
0
0.2000
0.2091
104
0.1897
94.9
10
1,2-Dichloroethane
mg/t
0
0.2000
0.1997
99.8
0.1836
91.8
8
Carbon Tetrachloride
mg/l
0
0.2000
0.2289
114
0.1966
98.3
15
Benzene
mg/l
0
0.2000
0.2231
112
0.1974
98.7
12
Trichloroethene
mg/l
0
0.2000
0.2026
101
0.1795
89.8
12
Tetrachloroethene
mg/l
0
0.2000
0.1582
79.1
0.1393
69.6
13
Chlorobenzene
mg/l
0
0.2000
0.2029
101
0.1790
89.5
12
Dibromofluoromethane (S)
101
99
1,2-Dichloroethane-d4 (S)
105
103
Toluene-d8 (S)
98
98
4-Bromofluorobenzene (S)
100
100
Laboratory Certification IN Laboratory Certification IDS
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
Analytical Hunt 9800KiAvenue, Suite 100
0 Huntersville, NC 2807878
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 10/11/00
PAGE: 18
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
LABORATORY CONTROL SAMPLE: 921226270
Spike
LCS
Parameter
Units
Conc.
Result
------------------------------
Vinyl Chloride
----------
mg/l
-------
0.2000
----------
0.08494
1,1-Dichloroethene
mg/l
0.2000
0.1560
2-Butanone
mg/l
0.4000
0.3384
Chloroform
mg/l
0.2000
0.1783
1,2-Dichloroethane
mg/l
0.2000
0.1795
Carbon Tetrachloride
mg/L
0.2000
0.1748
Benzene
mg/l
0.2000
0.1738
Trichloroethene
mg/l
0.2000
0.1575
Tetrachloroethene
mg/l
0.2000
0.1987
Chlorobenzene
mg/L
0.2000
0.1515
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
LABORATORY CONTROL SAMPLE: 921232179
Spike
LCS
Parameter
Units
Conc.
Result
------------------------------
Vinyl Chloride
----------
mg/t
-------
0.2000
----------
0.1580
1,1-Dichloroethene
mg/l
0.2000
0.1699
2-Butanone
mg/l
0.4000
0.2905
Chloroform
mg/l
0.2000
0.1569
1,2-Dichloroethane
mg/l
0.2000
0.1458
Carbon Tetrachloride
mg/L
0.2000
0.1646
Benzene
mg/l
0.2000
0.1601
Trichloroethene
mg/t
0.2000
0.1589
Tetrachloroethene
mg/l
0.2000
0.1511
Chlorobenzene
mg/t
0.2000
0.1425
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
SAMPLE DUPLICATE: 921228623
Spike
Y Rec Footnotes
---------------
42.5 1
78.0
84.6
89.1
89.7
87.4
86.9
78.8
99.4
75.7
106
118
103
98
Spike
Rec Footnotes
79.0
85.0
72.6
78.5
72.9
82.3
80.0
79.5
75.5
71.3
101
107
100
96
Dup.
Parameter Units 921208229 Result RPD Footnotes
------------------------------ -------------------- ---------- ----- ----------
Vinyl Chloride mg/l ND ND NC
Laboratory Certification IN Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Mnalytical m Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 10/11/00
PAGE: 19
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
SAMPLE DUPLICATE: 921228623
Dup.
Parameter
------------------------------
Units
921208229
Result
RPD Footnotes
1,1-Dichtoroethene
----------
mg/l
----------
ND
----------
ND
----- ----------
NC
2-Butanone
mg/l
ND
NO
NC
Chloroform
mg/t
NO
ND
NC
1,2-Dichloroethane
mg/l
ND
ND
NC
Carbon Tetrachloride
mg/t
ND
NO
NC
Benzene
mg/l
0.02500
0.02500
3
Trichloroethene
mg/l
ND
ND
NC
Tetrachloroethene
mg/l
ND
NO
NC
Chlorobenzene
mg/t
NO
ND
NC
Dibromofluoromethane (S)
%
103
101
0
1,2-Dichloroethane-d4 (S)
%
112
ill
0
Toluene -dB (S)
%
106
106
0
4-Bromofluorobenzene (S)
%
90
92
0
Laboratory Certification IN Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

aceAnalytical"
Blue Ridge Paper Products, Inc.
P. 0. Box 4000
Canton, NC 28716
Attn: Mr. Jim Giaque
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY -CONTROL DATA DATE: 10/11/00
PAGE: 20
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
QC Batch ID: 32287 QC Batch Method: EPA 3510
Analysis Method: EPA 8270 Analysis Description: Semivotatile Organics, TCLP
Associated Pace Samples: 93675239 93675247 93675254 93675262 93675312
93675320 93675338
METHOD BLANK: 921255378
Associated Pace Samples:
Parameter
Pyridine
1,4-Dichlorobenzene
2-Methylphenol
Hexachloroethane
3&4-Methylphenol
Nitrobenzene
Hexachloro-1,3-butadiene
2,4,6-TrichlorophenoL
2,4,5-Trichlorophenol
2,4-Dinitrotoluene
Hexachtorobenzene
PentachlorophenoL
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-dl4 (S)
Phenol-d6 (S)
2-FLuorophenol (S)
2,4,6-Tribromophenol (S)
93675239
Units
mg/t
mg/t
mg/t
mg/t
mg/l
mg/L
mg/t
mg/l
mg/t
mg/t
mg/l
mg/t
%
93675247
Method
Blank
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
65
60
94
23
38
84
93675254 93675262 93675312
PRL
0.0005
0.00075
0.02
0.0003
0.02
0.0002
0.00005
0.0002
0.04
0.000013
0.000013
0.01
Footnotes
93675320 93675338
Laboratory Certification IN Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical Huntersville, NC 28078
Phone.' 704.875.9092
Fax: [phone]
QUALITY CONTROL DATA DATE: 10/11/00
PAGE: 21
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
MATRIX SPIKE: 921230959 Matrix
Spike Spike Spike
Parameter Units 921222162 Conc. Result % Rec Footnotes
------------------------------
Pyridine
----------
mg/L
----------
0
-------
0.5000
----------
0.1136
----- ----------
22.7
1,4-Dichlorobenzene
mg/L
0
0.5000
0.1759
35.2
2-Methylphenol
mg/l
0
0.5000
0.1356
27.1
Hexachloroethane
mg/l
0
0.5000
0.1500
30.0 2
3&4-Methylphenol
mg/L
0
1.000
0.1303
13.0
Nitrobenzene
mg/L
0
0.5000
0.2175
43.5
Hexachloro-1,3-butadiene
mg/l
0
0.5000
0.1766
35.3
2,4,6-Trichlorophenol
mg/L
0
0.5000
0.2406
48.1
2,4,5-Trichlorophenol
mg/L
0
0.5000
0.1870
37.4
2,4-Dinitrotoluene
mg/l
0
0.5000
0.2023
40.5
Hexachlorobenzene
mg/l
0
0.5000
0.2175
43.5
Pentachlorophenol
mg/L
0
0.5000
0.2341
46.8
Nitrobenzene-d5 (S)
80
2-Fluorobiphenyl (S)
92
Terphenyl-d14 (S)
70
Phenol-d6 (S)
26
2-FLuorophenol (S)
24
2,4,6-Tribromophenol (S)
100
LABORATORY CONTROL SAMPLE: 921230942
Spike
LCS
Spike
Parameter
------------------------------
Units
Conc.
Result
% Rec Footnotes
Pyridine
----------
mg/l
-------
0.5000
----------
0.07528
----- ---------
15.1
1,4-Dichlorobenzene
mg/t
0.5000
0.09641
19.3
2-Methylphenol
mg/L
0.5000
0.1203
24.1
Hexachloroethane
mg/l
0.5000
0.09107
18.2 2
3&4-Methylphenol
mg/l
0.5000
0.1089
21.8
Nitrobenzene
mg/l
0.5000
0.1429
28.6
Hexachloro-1,3-butadiene
mg/L
0.5000
0.08494
17.0
2,4,6-Trichlorophenol
mg/l
0.5000
0.1596
31.9
2,4,5-Trichlorophenol
mg/t
0.5000
0.1583
31.7
2,4-Dinitrotoluene
mg/L
0.5000
0.1758
35.2
Hexachlorobenzene
mg/L
0.5000
0.1614
32.3
Pentachlorophenol
mg/t
0.5000
0.1493
29.9
Nitrobenzene-d5 (S)
59
2-Fluorobiphenyl (S)
63
Terphenyl-d14 (S)
66
Phenol-d6 (S)
19
2-Fluorophenol (S)
25
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDS
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical ', Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 10/11/00
PAGE: 22
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
LABORATORY CONTROL SAMPLE: 921
Spike LCS Spike
Parameter Units Conc. Result % Rec Footnotes
------------------------------ ---------- ----------------- ---------------
2,4,6-Tribromophenol (S) 76
SAMPLE DUPLICATE: 921249793
Parameter Units
Pyridine
mg/t
1,4-Dichlorobenzene
mg/L
2-Methylphenol
mg/1
Hexachloroethane
mg/t
3&4-Methylphenol
mg/L
Nitrobenzene
mg/l
HexachIoro-1,3-butadiene
mg/l
2,4,6-Trichlorophenot
mg/l
2,4,5-Trichlorophenot
mg/L
2,4-Dinitrotoluene
mg/l
HexachLorobenzene
mg/L
PentachlorophenoL
mg/t
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyt-d14 (S)
PhenoL-d6 (S)
2-FLuorophenoL (S)
2,4,6-Tribromophenol (S)
Dup.
93670636 Result
ND
ND
ND
NO
ND
ND
ND
ND
ND
NO
NO
ND
ND
NO
NO
NO
ND
ND
NO
NO
ND
ND
NO
NO
51
38
45
36
49
39
19
19
13
21
36
43
RPD
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
0
0
0
0
0
0
Footnotes
3
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

aceAnalyticalTM
Blue Ridge Paper Products, Inc.
P. 0. Box 4000
Canton, NC 28716
Attn: Mr. Jim Giaque
QC Batch ID: 32938
Analysis Method: EPA 8260
Associated Pace Samples: 93675320
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: 704.875, 9092
Fax: 704, 875.9091
QUALITY CONTROL DATA DATE: 10/11/00
PAGE: 23
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
QC Batch Method: EPA 8260
Analysis Description: Volatile Organics, TCLP Leach.
METHOD BLANK: 921257192
Associated Pace Samples:
93675320
Method
Blank
Parameter
------------------------------
Units
Result
PRL Footnotes
Vinyl Chloride
----------
mg/l
----------
ND
---------- ----------
0.02
1,1-Dichloroethene
mg/l
ND
0.02
2-Butanone
mg/t
NO
0.4
Chloroform
mg/l
ND
0.02
1,2-Dichloroethane
mg/l
ND
0.02
Carbon Tetrachloride
mg/l
NO
0.02
Benzene
mg/L
ND
0.02
Trichloroethene
mg/l
NO
0.02
TetrachLoroethene
mg/l
ND
0.02
Chlorobenzene
mg/L
ND
0.02
Dibromofluoromethane (S)
%
104
1,2-Dichloroethane-d4 (S)
%
104
Toluene-d8 (S)
%
99
4-Bromofluorobenzene (S)
%
99
LABORATORY CONTROL SAMPLE: 921257200
Spike
LCS
Spike
Parameter
------------------------------
Units
Conc.
Result
% Rec Footnotes
Vinyl Chloride
----------
mg/l
-------
0.2000
----------
0.1784
----- ----------
89.2
1,1-Dichloroethene
mg/l
0.2000
0.2502
125
2-Butanone
mg/t
0.4000
0.2892
72.3
Chloroform
mg/t
0.2000
0.1766
88.3
1,2-Dichloroethane
mg/l
0.2000
0.1698
84.9
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDS
S NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Analytical Huntersville, NC 28078
Phone: [phone]
Fax [phone]
LABORATORY CONTROL SAMPLE: 921257200
Parameter Units
Carbon Tetrachloride
mg/t
Benzene
mg/l
Trichloroethene
mg/t
Tetrachloroethene
mg/t
Ch.lorobenzene
mg/l
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
SAMPLE DUPLICATE: 921257218
QUALITY. CONTROL DATA DATE: 10/11/00
PAGE: 24
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
Spike
LCS
Spike
Conc.
-------
Result
----------
% Rec Footnotes
0.2000
0.1932
---------------
96.6
0.2000
0.1867
93.3
0.2000
0.2250
113
0.2000
0.2703
135 2
0.2000
0.1688
84.4
100
104
100
101
Dup.
Parameter
------------------------------
Units
93675320
Result
RPD Footnotes
Vinyl Chloride
----------
mg/l
----------
NO
----------
NO
----- ----------
NC
1,1-Dichloroethene
mg/l
ND
NO
NC
2-Butanone
mg/l
NO
NO
NC
Chloroform
mg/l
NO
NO
NC
1,2-Dichloroethane
mg/l
NO
NO
NC
Carbon Tetrachloride
mg/l
ND
NO
NC
Benzene
mg/l
NO
NO
NC
Trichloroethene
mg/l
NO
NO
NC
Tetrachloroethene
mg/t
ND
NO
NC
Chlorobenzene
mg/l
NO
NO
NC
Dibromofluoromethane (S)
%
104
103
0
1,2-Dichloroethane-d4 (S)
%
103
101
0
Toluene -dB (S)
%
98
99
0
4-Bromofluorobenzene (S)
%
100
98
0
Laboratory Certification IN Laboratory Certification IDS
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
9Analyticafm Hunters ville, NC28078
Phone: [phone]
Fax: [phone]
DATE: 10/11/00
PAGE: 25
Pace Project Number: 9217435
Client Project ID: Blue Ridge-9315593
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
ND Not Detected
NC Not Calculable
PRL Pace Reporting Limit
RPD Relative Percent Difference
(S) Surrogate
Ill The surrogate and/or spike recovery was outside acceptance limits.
[21 Recovery falls outside of QC limits, however, this compound is not found in the associated samples.
(31 Base/neutral surrogate recovery outside of control limits. The data was accepted based on valid recovery of remaining
two base/neutral surrogates.
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laborat� Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, TN UST List
Sc 99006 without the written consent of Pace Analytical Services, Inc. VA Drinking Water 213

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BLUE RIDGE PAPER PRODUCTS, INC.
CANTON MILL — LANDFILL 6, AREA A WEST
PRE -CONSTRUCTION MEETING — JUNE 8, 2000
1. Introduction
• Meeting Purpose
2. General Site Orientation
• History
• Area 6A East Operation
• Area 6A West Permit
3. Area 6A West Construction Features
• Liner Components
• Leachate Drainage system
• Interior Dike
• Access Roads
4. Roles and Responsibilities
• Construction Management Organization
• Respective Duties During Construction
5. Schedule
6. Followup/Other Issues

PERMIT NUMBER 44-06
AREA A WEST
GENERAL PERMIT REQUIREMENTS
Basic PRE -CONSTRUCTION and PRE -OPERATIVE requirements of the Landfill 6 A
West Construction Permit include the following:
PRE -CONSTRUCTION REQUIREMENTS
1. Part I, Section 1 - Must record permit in Haywood County, NC, and submit
certified copy to Solid Waste Section (SWS).
2. Part II, Section 7 - Conduct pre -construction meeting on site and notify SWS
of same.
3. Part II, Section 11 - Owner's geologist is to examine cell excavation and note
pertinent geologic features.
PRE -OPERATIVE REQUIREMENTS
1. Part II, Section 15 - Prior to operation:
• (b) Site to be inspected by SWS representative.
(c) Pre -operative meeting to be held on -site with key landfill personnel
and representative(s) of SWS.
• (d) Sample monitoring wells and surface sites.
A (e) Submit CQA documentation and engineer's certfication to SWS.
file:6awrep.doc

LAW
Maya, 1999 ' r'NNG:BB Grow `f'e,,�
Mr. Guy Cote
Sevee & Maher Engineers, Inc.
4 Blanchard Road
Cumberland Center, Maine 04021
Subject: Report of Observed Geologic Features
Excavated Landfill Cell 6A-West
Champion International, Inc - Canton, North Carolina
LAW Project 30300-9-0313.03.800
Dear Mr. Cote:
As requested, observation of the exposed landfill foundation was performed on the subject project by Law
Engineering and Environmental Services, Inc.on April 22. 1999. The purpose of the observation was to
document site Qeology relative to landfill liner performance. According to site personnel, the final base
grade was achieved by excavating overburden material to the extent possible by mechanical equipment
(ripping).
The landfill foundation consists of several areas of exposed rock surfaces (interpreted to be parent bedrock).
The rock appears to be generally similar at all locations and classified (from visual examination) as biotite-
muscovite gneiss described as light to medium gray, medium to coarse grained, foliated and composed of
orthoclase, quartz, biotite, hornblende, muscovite and other minor accessory minerals including garnet. All
locations are hard to very hard with very slight weathering to fresh surface exposures.
No evidence of solution features, dike intrusions, sills, sinkholes, faults or other related features were
observed in the bedrock. Apart from the bedrock, the exposed soil is residual material that generally retains
the parent rock structure and texture. The rock and soil types encountered at the site are consistent with
those described in the pre -construction geotechnical report and geologic literature for the area.
Based on observations discussed above, the foundation for Landfill Cell 6A-West appears to be in
substantial compliance in that no oeoioQic features were observed that could adversely impact the
x _ performance of the landfill liner. ~
Please contact the undersigned at 704-357-8600 if you have any questions regarding this submittal.
Sincerely,
LAW ENGINEERING AN N SERVICES, INC.
SEAL
(liff Lundgren, P.G. 1359 s Stephen E. Blevins, P.
Senior GeologistGF000G�S �k'c Principal
Registered N.C. No. 1359 ,�'•.,� 9. ' ''�O ��•`
LAVA! Engineering and Environmental Services inc
:�, Ycrk.M. . aca- • Ch- - tiC 2°2Sc

BLUE RIDGE PAPER PRODUCTS, INC.
CANTON MILL — LANDFILL 6, AREA A WEST
PRE -CONSTRUCTION MEETING — JUNE 8, 2000
,sign Engineer
-SME Guy Cot
-SME PE On
General Organization
BRPP, Inc. (Owner
-E&N Bill vonVitzthume
-EOIIS Jim Giauque
-Materials Lynn Sellars
:CC (Gen. Cont.)
-Tom Davis
-Derrick Dockery
Bryant Electric
(Excavation/Directional GSE (Liner
Boring) Installation)
-Randv Smith I
Inc. (Pipe Fabrication

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PAPER PRODUCTS !',jc.
To: Distribution
From: Jim Giauque
Date: May 23, 2000
Subject: Landfill 6A West Pre -construction
Meeting
A pre -construction meeting for the Blue Ridge Paper Products, Inc., Landfill Number 6,
Area A West, Permit Number 44-06, will be held Thursday, June 8, 2000, at the landfill
site, beginning at 1:00 PM, as required by Attachment 2, Part II of the construction
permit.
Area construction, liner fabrication, drainage/leachate system, quality control, safety and
other pertinent information will be discussed.
Please plan for your representative(s) to participate. Should you have questions, call me
at 828-646-2028.
JimGiauque
Dist: Andy Apostolopoulos
Derric Brown
Guy Cote (Sevee & Maher Eng.) (Information only)
Tom Davis (RCC)
Derrick Dockery (RCC)
Lynn Sellars
Matt Shiplet (RCC)
Bill vonVitzthume
Bob Williams
Copy: Sherri Coghill (NC DEHNR, SWS)
Jim Patterson (NC DEHNR, SWS)
file:precon.doc
175 Main Street • P.O. Box 4000
Canton, North Carolina 28716 • Phone: [phone]
Raising Your Expectations

NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Solid waste Management
Solid waste Section
SOLID WASTE MANAGEMENT FACILITY EVALUATION REPORT
Type of Facility. ! 'if'�t ,� F�,l ��:: Permit # County
Name of Faci I ity ;' )Vu-, r\1{�C,i, T hi�U ' ��iY.)R t l �- Location �j � ) 5 � ~� , 1. �, f (f'►\
Date of Last Evaluation 1 11J 1. 0
I. Permit Conditions Followed 4—Yes No N/A
A. Specific Condition(s) Viol
II. Operational Requirements Followed Yes No
15A N.C. Admin. Code 13B Section a c' j L) 95
A. Specific Violation(s) by number and letter.
III. other Violations of Rule or
IV. Evaluator's Comments
V. Continuation Page Required? Yes
No Receiving Signature
a
Evaluation Date Solid Waste Section i
DENNR 3793 (Part I White: Facility Part II Canary: -Central Office Part III Pintas Regional Office)
Solid Waste Section (Review 7/94) -

NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Solid Waste Management
Solid Waste Section
SOLID WASTE KUACflENT FACILITY EVALUATION REPORT
Type of Facility 1`Permit ll County.
Name of Facility i rl k s A; h;�'(i Location
Date of Last Evaluation
I. Permit Conditions Followed Yes No N/A
A. Specific Condition(s) Violated
II. Operational Requirements Followed Yes No
15A N.C. AcImin. Code 13B Section
A. Specific Violations) by number and letter.
III. other Violations of Rule or Law
IV. Evaluator's
V. Continuation Page Required?
Yes No Receiving Signature
Evaluation Date Solid Waste Section
DEHNR 3793 (Part I White: Facility Part II Canary: Central Office Part III Pink: Regional Office)
Solid Waste Section (Review 7/94)

NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Solid Waste Management
Solid Waste Section
SOLID WASTE NAMAGE14ENT FACILITY EVALUATION REPORT
Type of Facility. 11" 0 r 1111 Permit X county
Name of Facility Location '�)fZ 1571,5, (.,L/ r)- .4jj
Date of Last Evaluation
I. Permit Conditions Followed Yes No N/A
A. Specific Condition(s) Violated
11. Operational Requirements Followed Yes No
15A N.C. Admin. Code 138 Section
A. Specific Violation(s) by number and Letter.
A/I
III. Other Violations of Rule or Law
IV. Evaluator's Comments 3 Zj (_.'
V. Continuation Page Required? —Yes No Receiving Signature —
Evaluation Date Solid Waste Section
DEHNR 3793 (Part I White: Facility Part 11 Canary: Central Office Part III Pink: Regional Office)
Solid Waste Section (Review 7/94)

NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Solid waste Management
Solid waste Section
SOLID WASTE MAMAGEIENT FACILITY EVALUATION REPORT
Type of Facility. Permit # County.
! �'; j )
Name of Facility ; ,�f l%< < f /�i,1,;` Location
Date of Last Evaluation
I. Permit Conditions Followed Yes No N/A
A. Specific Condition(s) Violated
II. Operational Requirements Followed Yes No
15A N-C_ Agin. Code 138 Section
A_ Specific Violation(s) by number and Letter.
III_ Other Violations of Rule or Law
IV. Evaluator's
V. Continuation Page Required?
Yes No Receiving Signature
Evaluation Date Solid Waste Section
DEHNR 3793 (Part I White: Facility Part II Canary: Central Office Part III Pink: Regional Office)
Solid Waste Section (Review 7/94)

mK,� �
=�
NCDENR
.LAMES B. HUNT JR.
GOVERNOR
BILL HOLMAN
SECRETARY
WILLIAM L. MEYER.
DIRECTOR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL }RESOURCES
DIVISION OF WASTE MANAGEMENT
RECEIVED
N.C. Dept. of EHiNA
MAR 17 2000
Winston-Salem
March 14, 2000
Mr. Jim Giauque
Blue Ridge Paper Products, Inc.
PO Box 4000
Canton, NC 28716
Re: Blue Ridge Paper Products Landfill No. 6 Industrial Waste Landfill
Solid Waste Permit No. 44-06
Part 1: Permit to ConstructW�� C�w�
Dear Mr. Giauque:
Enclosed is Solid Waste Permit No. 44-06, Part 1: Permit to Construct.
This permit approves construction of Area 6A East, Cell V in addition to
Area 6A West, Cells I and ll. This permit also amends the name of the
facility.
If you have any questions or comments, please contact me at
[phone], ext. 259.
Sincerely,
Sherri Coghill
Environmental Engineer
Solid Waste Section
cc: ►Brent Rockett
Tim Jewett
Jim Patterson
M<:A'M6K�+GyF
1646 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1646
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX 91 9-71 S-3605
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
NCDENR DIVISION OF WASTE MANAGEMENT
located on SR 1550 and 1-40, Haywood County, North Carolina, in accordance with
Article 9, Chapter 130A, of the General Statutes of North Carolina and all rules
promulgated thereunder and subject to the conditions set forth in this permit.
J es C. Coffey, Supervi
ermitting Branch
Solid Waste Section
i
1�,
L dtF�EAbR,f�h, '�
1646 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1646
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

FACILITY PERMIT NO: 44-06
Part 1-Permit to Construct
Date of Original Issue: January 9, 1992
Amendment Date: March 8, 1999
Modification Date: March 14, 2000
Page 2
ATTACHMENT 1
Approved Documents
1. Application for Permit to Construct, Landfill No. 6A West, Champion International
Corporation, Canton, NC, prepared by Sevee and Maher Engineers, Inc., revised through
February 24, 1999.
2. Operations Manual, Landfill No. 6A West, Champion International Corporation, Canton, NC,
prepared by Sevee and Maher Engineers, Inc., dated January 1999.
3. Landfill Stability Evaluation for Vertical Expansion, Area 6A East, Blue Ridge Paper
Products, Inc., Canton NC, prepared by Sevee and Maher Engineers, Inc., dated
October 1999.
4. Facility Drawings, Landfill 6, Area A West and Area A West (Alternate), prepared by
Sevee and Maher Engineers, Inc., dated March 8, 2000.

FACILITY PERMIT NO: 44-06
Part 1-Permit to Construct
Date of Original Issue: January 9, 1992
Amendment Date: March 8, 1999
Modification Date: March 14, 2000
Page 3
ATTACHMENT 2
Conditions of Permit to Construct
PART I: INDUSTRIAL WASTE LANDFILL FACILITY
GENERAL CONDITIONS
1. This permit shall be effective upon compliance with 15A NCAC 13B .0204 and when the
certified copy with the page, book number, date of recordation, and Register's seal is
returned to the Solid Waste Section (Section).
2. This permit is subject to review every five years as per 15A NCAC 13B .0201(e), according
to the issuance date of the Permit to Operate. Modifications to the facility may be
required in accordance with rules in effect at the time of review.
3. The approved plans are described in Attachment 1, "Approved Documents", and allows
construction Where discrepancies may exist, the most recent approved submittal and
Conditions of Permit shall govern.
4. The landfill is permitted to receive solid waste generated solely by Blue Ridge Paper
Products, Inc. as described in the approved plan and as defined in 15A NCAC 13B
.0101(36), except where prohibited by North Carolina General Statutes Article 9 of
Chapter 130A, and rules adopted by the Commission for Health Services.
5. This facility is subject to the requirements of all applicable sections of the most recent
version of the North Carolina Solid Waste Management Rules, 15A NCAC 13B and the
specific conditions contained herein.
6. This permit is not transferable.
PART II: INDUSTRIAL WASTE LANDFILL UNIT
CONSTRUCTION CONDITIONS
7. The permittee shall conduct a pre -construction meeting, on -site, prior to initiating
construction and shall notify the Solid Waste Section of said meeting. If construction does
not begin within 18 months from the issuance date of this permit, then the permittee
must obtain written approval from the Section prior to construction and comply with any
conditions of said approval.

FACILITY PERMIT NO: 44-06
Part 1-Permit to Construct
Date of Original Issue: January 9, 1992
Amendment Date: March 8, 1999
Modification Date: March 14, 2000
Page 4
8. This permit approves the construction of Cells I and II of Area 6A West and Cell V of Area
6A East. Construction shall be in accordance with the approved plans as described in
Attachment 1, Document 1, "Approved Documents".
9. Additional conditions and revisions of the approved documents or changes during
construction require approval by the North Carolina Solid Waste Section.
10. Any modifications in sedimentation and erosion control activities require approval by the
Land Quality Section. The Section shall be notified of any sedimentation and erosion
control modifications.
WATER QUALITY MONITORING SYSTEM CONSTRUCTION CONDITIONS
11. The owner's geologist shall examine the cell excavation and note any pertinent geologic
features exposed during the construction process and shall notify the Solid Waste Section
Hydrogeologist of these findings prior to the placement of any liner materials.
12. The owner's geologist shall be in the field to supervise all well installations. Any
modifications to the approved water quality monitoring plan require approval by the
Section Hydrogeologist. Documentation of all changes to the approved plan shall be
submitted with the well construction records.
13. For each monitoring well constructed, a well construction record, well schematic, boring
log and a description of well development activities shall be submitted to the Section
within 30 days upon well completion.
PRE -OPERATIVE CONDITIONS
14. Prior to receiving waste, a Permit to Operate, must be obtained from the Solid Waste
Section in accordance with 15A NCAC 13B .0201(b).
15. The following requirements shall be met prior to obtaining a Permit to Operate:
a. Site preparation shall be in accordance with the approved plans, and the conditions
specified herein.
b. Site inspection shall be made by a representative of the Solid Waste Section.
C. A pre -operative meeting shall be held on -site with key landfill personnel and
representatives of the Solid Waste Section.
d. Ground water monitoring wells and surface water sampling locations shall be
sampled prior to issuing the Permit to Operate.
e. CQA documentation as well as a certification by the project engineer that the
landfill was built in accordance with approved plans shall be submitted to the
Section.

NOTES:
1. PLAN COMPILED FROM AERIAL PHOTOGRAAwETRIC NAPPING
DATED ANY 1996, PERFORMED BY AMERICAN
GEOGRAPHIC DATA INC., OF W%.VING'ON N.C..
2. PLANS COMPILED IN THIS MAWR SHOULD BE FIELD VERIFIED
PRIOR TO CONSTRUCTION.
3. SITE CCW ITIONS WIVE CHANGED SINCE THE COMPILATION
OF THIS PLAN DUE TO CURRENT EXCAVATION WORK.
4. GRID IS BASED ON NORTH CAROL INA STATE PLANE
COORDINATE SYSTEM BASED ON NAGS 1983.
5, VERTICAL DATUM IS BASED CN NGVO 1929.
6. EX:STINO GRADE CONTOUR INTERVAL IS 10 FEET.
7. PROPERTY LIKE AND AREAS D AND E BOUNDARY WERE DIGITIZED
FROM LAW ENGINEERING DRAWING DATED JANUARY 14. 1984.
2-FWAIERb ELEI-Mar
710N
WELL t0-uta r-95• 22-FeD-96. 6. 6-#by-96. 24-Jul-97
NW -IA 2710.35 2709.46 RN 2711.72 2712.55
MA-2 2593.63 2592.35 2591.78 2593.58 2593.87
104-3A 2575.77 2575..64 257548 25785
4
7 2 2571 38A4-4 2571.39 2571W4
A-5A 254341 254364 N2543.02 2542.49
MW-5 253932 2537.8A 25377.35
Mh7
2540.39 2539.90 NA 2539.79 2539.69
MN-8 W 2586.20 Nd 25g4.18 2583.43
M,H3 2651.53 2652. 20 NN 2652. 47 2651.89
MA-10 2644. 63 264c. 43 NM 2645.23 NUMn-1J 2632.9E 2632. 25 NM 2631 .95 2630.92
AOH 12 2536.67 2535 08 2534.72 2534.61 N4
1,06-13 2540.71 2540.24 2539.92 2539.82 NM
MN-14 2654. 4' 2655.38 N+ 2656.18 2550.65
MW-15 2683.70 2683.73 N4 2683.83 2680.67
P-9701A N/A N/A N/A N/A 2547.31
P-97078 N/A N/A N/A N/A 2656.48
P-9702A N/A N/A N/A N/A 2664.64
P-97028 N/A N/A N/A N/A 2649.85
P-9703A N/A - N/A N/A N/A 2694.88
P-9703B N/A N/A N/A N/A 2715 Ag
17-'f N,'A N/A > N/: 255'�
N''A
v. �q N/A NIA N. N/A 26f_ :.
NA Nat M•a,ured CHAMPION INTERNATIONAL CORP.
N/A Pi•zomaer not �mta1l•a until June 1997 tx uR°`'+► CANTON, NORTH CAROL I NA
El eInfo-, .apr a„ed ,n fee: 'Grow ,ea lev... LANDFILL NO. 6A WEST CONSTRUCTION
• info•met;on obtained fnom "Groundrater ana Sur •oc• water A„ of ement 1D8Y9
for LDna!f11 No. 6' and 'Grountl..ater ono Surfoce water A-,*s"nt
for Lona. No. 6 �na,a :1', Dr•por •d Dy Roy F. weeton, InC.
EfE� SITE LOCATION PLAN
DESIGN BY: CJB
DRAWN BY: CJB
j TSEVEE & MAHER ENGINEERS, INC. CHECKED BY: GI•C
10/31/971 SUBMITTED TO NCDEHNR CCN$ULT!NG ENGINEERS GATE: 8/2t /96
$UBNI TTCO TO HCDEHNR Ci;M,6ERLAND, MAINE IFICLD VK_ LOCA1.
._, 1

NOTES
=•v�''S is '' %�j ' ,/.--� �� ,
��!i/// ji'�'�,�n✓---- _ 1. PLAN COMPILED FROM AERIAL PFgiOORATR IC MAPPING ,V,E
DATED MAY 1996. PERFORMED BY Ad.ERICAN
/%� /rr�'�j/�'/�=•'� GEOGRAPHIC DATA INC.. OF WILMINGTON N.C..
2. PLANS COAPILEO 1N THIS MOWER SHOULD BE FIELD VERIFIED
PRIOR TO CONSTRUCTION.
3. SITE CONDITIONS MAY OAVE CWWGEO SINCE THE CO%e ILATiCN
OF THIS PLAN.
4. GRID IS BASED ON NORTH CAROLINA STATE PLANE
COORDINATE SYSTEM BASED ON NAGS 1963.
/ i' i/�%�,i• 1 3. VERTICAL DATUM IS BASED ON NGVD 1929.
6. CONTOUR INTERVAL 1S 2 FEET. ..
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ko so tzorccr I
1/9t/97
3UBMITTW TO NCOCXNR
12/5/"
SUBMITTED TO CLIENT
_
8/28/"
SUBMITTED TO CLIENT
@/Maros
SUBMITTED TO CLIENT
REV.
BY
DATE
I STATUS
C r0
CHAMPION INTERNATIONAL CORP.
CANTON, NORTH CAROL INA
LANDFILL NO. 6A WEST CONSTRUCTION
EXISTING CONDITIONS PLAN
I
SEVEE do MAHER ENGINEERS, INC.
CONSULTING ENGINEERS
"+nERtAND, MAINE
:
DESIGN BYjo
DRAWN BY: CJB
CHECKED NY: M-C
DATE: 6/28
rIELD BK
ISCA C