MO-9532_40967_CA_IAR_20200710_IAA Report

IAA
INITIAL ABATEMENT ACTION
REPORT
With
(Non -Regulated UST Removal)
Post -Excavation Soil Contamination Assessment Report
Site:
John Adams Property
934 W. Mallard Creek Church Road
Charlotte, NC
Mecklenburg County
Prepared by:
INENCO, Inc.
132 W. Statesville Ave.
Mooresville, NC
July 2020

IAA REPORT
John Adams Property
94 W. Mallard Creek Church Roach
Charlotte, NC
This report was prepared by IN NCO, Inc.
North Carolina professional Corporation Rcgistmtion 9: -1140
This report was prepared by wd wader the directian of Ryon Osborne, a Pr-ofessional Engineer
for III NCO, Inc. 1 do certify that the information contained in this report is conwt and
accurate to the best of my knowledge
*1iyt1111jdI,,
26:�3
SEAL
1 t
yan R. Osbom:, PE'
sul rlg Project 1atger
orth Carolina Frafe ional Engineer License No. 2 923
Je �
Date

A. Site Identification
General Information
-Ownership of Property
John Adams
600 Morris Street
Charlotte, NC 28202
704-376-4328
-Ownership of UST
Same
*Laboratory
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
NC Lab: 37706
-Engineering Consultant
INENCO, Inc.
132 W. Statesville Ave.
Mooresville, NC 28115
[phone]
Contact: Ryan R. Osborne, PE
Information about Release
*Site Information
Single-family home
934 W. Mallard Creek Church Road
Charlotte, NC
Mecklenburg County
Location: northeast corner of Mallard Creek
Church Road and John Adams
road. UST was located in the side
yard.
3 5 ° 1 V 02" Latitude
80' 5 F 25" Longitude (via Google Earth at UST)
*Contractor (First half)
CERT,Inc.
PO Box 681016
Charlotte, NC 28216
[phone]
Contact: Lee Shank
*Contractor (Second half)
Piedmont Grading and Wrecking
3652 Beatties Ford Rd (20.93 mi)
Charlotte, NC 28216-3212
[phone]
Contact: Wayne Kerr
As part of the Phase I ESA for the redevelopment of the property, a tank was discovered. As
the removal of the 285 gallon home heating oil UST proceeded, a release of the contents of
the tank was evident. A soil sample was taken and delivered to the laboratory indicated a
release. A report of the release was made to the NC DEQ via a UST Form 61 "24 hour"
report emailed to NC DEQ on 3/25/19. The cause of the release is suspected to be the
deterioration of the UST. The amount of the release is unknown.
IAA Report 934 W. Mallard Creek Church Road Page 1

B. Site History and Characterization
UST Owner/Operator Information
The property is owned by John and Catherine Adams. Apparently at some point in the
former home's past it was heated via a fuel oil fired furnace. At the time of this report, it is
unknown as to when the UST was last used.
UST Information
ID #
Last
Previous
Capacity
p
Construction
Tank
Piping and
Date
Status of
Release
Contents
Contents
Details
Dimensions
Pumps
Installed
UST
Discovered
Heating
Single Walle
emoved
1
Oil
Same
285 gal
Carbon teel
36"dia x 66" C p2per
Unk*
3 % 3/19
Yes
* Exact date of tank installation unknown
Non -UST Information
There was no indication at the subject site of an aboveground tank or any other non -UST
source of the discovered contamination. There are no known releases from any non -UST
sources.
Release Information
During the removal of the tanks, a confirmation sample was collected for laboratory analysis.
These activities showed that a release had occurred. The presence of the release was also
evident when the soil removal project commenced.
Site Characterization Information
The property is a single-family residence in a residential area. The predominant soil type at
the site was brown sandy silt. The surface topography at the UST location sloped slightly
toward the west and north. The local area and topography are illustrated in Figure 1, Aerial
Photograph and Figure 2, the USGS map.
The site is located in Charlotte city limits and along with the surrounding properties appears
to utilize municipally supplied water and sewer and/or have access to municipal water and
sewer. The house did utilize a water well at some point in its existence. During the time of
this project the well was abandoned by a certified well contractor.
Summary of Initial Abatement
The UST was discovered as part of the Phase I ESA. The tank was removed on 3/13/19. A
soil sample was collected and analyzed with the results indicating a release of the UST's
contents. A 24-Hour Release and UST Leak Reporting Form was sent to the NC DEQ on
3/25/19. The contaminated soil was excavated in two phases.
C. Site Check Report
This section is not applicable.
IAA Report 934 W. Mallard Creek Church Road Page 2

D. UST Closure (Non -Regulated)
Removal of UST Residuals
It is unknown if residuals were removed from the UST prior to its removal.
UST Removal and Assessment Procedures
The UST was removed by CERT on 3/13/19 utilizing a small trackhoe. A soil sample was
collected by CERT during this removal and sent to a certified laboratory for analysis.
UST Disposal
The UST was disposed of soon after the time that the tank was removed. The tank was
disposed of by CERT through Auto Parts U Pull and Scrap Metal of Charlotte. A copy of the
Certificate of Disposal is included in Appendix E.
UST Closure Site Investigation
UST Closure Field Screening
No field screening was conducted during the UST removal aside for visual and olfactory
screening.
UST Release Confirmation Samples
A single release confirmation sample was collected from the open excavation. Quality
control measures are documented by the laboratory in their analytical report in Appendix B.
UST Release Confirmation Sample Results
The results of the soil sampling confirmed that contamination was present and that a release
had occurred. Laboratory results of the sample indicated 11.9 mg/kg Gasoline Range
Organic (GRO) compounds and 2120 mg/kg Diesel Range Organic (DRO). A 24-Hour
Release and UST Leak Reporting Form was sent to the NC DEQ. The laboratory reports for
these results are located in Appendix B.
UST Closure Conclusions
The operation of the UST caused a release of its contents as documented in these assessment
activities. Initial abatement actions were initiated as documented in this report.
E. Free Product Investigation and Recovery Report
No free product was discovered; therefore, this section is not applicable.
F. Groundwater and Surface Water Investigation
Groundwater was not discovered during the excavations. An assessment of groundwater at
the site was conducted outside of this UST removal project and is attached as Appendix G.
This report indicates a groundwater impact.
IAA Report 934 W. Mallard Creek Church Road Page 3

G. Initial Response and Abatement Action
Abatement activities took place after the discovery and is documented in following sections.
H. Excavation of Contaminated Soil
Over -Excavation Activities
Phase 1 of Over -Excavation
After removal of the UST, on 4/9/2019 soil excavation commenced in an effort to remove
soil to the extent of contamination. Soil checks using the PID and olfactory clues were used
to guide the excavation. The overall final dimensions of the excavation were approximately
20 feet by 22 feet by 18 feet deep. The removed soil was placed directly into trucks for
disposal. The excavation was sampled via the trackhoe with a sample labeled Bottom taken
from the floor of the tank pit area beneath the former location of each UST at a depth of
about 18 feet. Soil samples were labeled West Wall, South Wall, North Wall, and East Wall
and were taken from the area of the wall where it seemed during the excavation activities that
contamination would be most likely to be present. Each of these samples was collected from
a depth of approximately 16' feet below land surface. The soil samples were checked for the
presence of constituents found by EPA Methods 8260, 8270 and MADEP EPH & VPH. The
location of each sample along with the overall excavation is illustrated in Figure 3. All
samples were collected as previously described. Neither groundwater nor bedrock was
encountered during this phase of the over -excavation activities. This phase of the excavation
was backfilled in April of 2019.
Phase 2 of Over -Excavation
The size of the Phase 1 excavation was dictated by the presence of the house east of the UST
area. The results for Phase I indicated that the East wall of the excavation contained
additional contamination (under the house). After demolition of the house, on 5/13/2020 soil
excavation continued with PID and olfactory clues used as a guide. The previous excavation
served as the western boundary of the additional excavation and the pit was expanded to the
east. The final dimensions of the new portion of the excavation were approximately 11 feet
(to the east) by 26 feet (north to south) by 18 feet deep. Soil samples were collected from
each of the three new faces of the excavation. These soil samples were labeled North Wall 2,
South Wall 2, and East Wall 2 and taken from the area of the wall where it seemed during the
closure activities that contamination would be most likely to be present. Each of these
samples was collected from a depth of approximately 16' feet below land surface. The soil
samples were checked for the presence of constituents found by EPA Methods 8260, 8270
and MADEP EPH & VPH. The location of each sample along with the overall excavation is
illustrated in Figure 3. All samples were collected as previously described. Neither
groundwater nor bedrock was encountered during this phase of the over -excavation activities.
Over -Excavation Soil Removal /Disposal
Disposal of the contaminated soil took place on 4/9&l 1/2019 and 5/8/2020. Nineteen
covered dump truck loads were transported to Environmental Soils, Inc. in Lattimore, NC. A
summary of these activities is shown in the following table. The Disposal Manifests are
included as Appendix C.
IAA Report 934 W. Mallard Creek Church Road Page 4

Soil Manifest
Table
Manifest No.
Date
Truck no.
Tare Weight
lbs.
Gross Weight
lbs.
Net Weight
lbs.
42598
4/9/2019
D3
25420
46340
20920
42599
4/9/2019
D9
28720
57900
29180
46084
4/9/2019
CGG2
26580
46480
19900
46085
4/9/2019
10
38680
74340
35660
52093
4/9/2019
D3
25420
48280
22860
42600
4/9/2019
D9
28720
54040
25320
53388
4/9/2019
D8
28420
49240
20820
46143
4/11/2019
D4
27580
60120
32540
46144
4/11/2019
D9
28720
59320
30600
46145
4/11/2019
D8
28420
63500
35080
46146
4/11/2019
D4
27580
68100
40520
46147
4/11/2019
D9
28720
59320
30600
46148
4/11/2019
D3
25420
58340
32920
46149
4/11/2019
D8
28420
70940
42520
46150
4/11/2019
D9
28720
53520
24800
53420
5/8/2020
D9
28660
77460
48800
53421
5/8/2020
D 11
29040
80620
51580
53422
5/8/2020
54
35720
92480
56760
53423
5/8/2020
K20
30480
83780
53300
Total: 654680 lbs.
327.34 Tons
Over -Excavation Stockpile Sample Results
Impacted soil was loaded directly onto trucks for disposal. No stockpile sampling was
performed.
Over -Excavation Sample Results
Bottom
After the removal of the affected soil (a total of about 327 tons), a sample was collected
along the floor of the excavation in the shadow of the former UST location at a depth of
about 18 feet. This sample was denoted Bottom. The laboratory results indicated no results
above Soil -to -Groundwater Maximum Soil Contaminant Concentrations (MSCCs). All
results are quantified in Table 1, Soil Sample Results. Sample locations are illustrated in
Figure 3.
South Wall
Additionally, a sample was collected from along each of the excavation walls at the wall's
approximate lateral center at a depth of 16' feet. Both the north and south walls were
sampled in different sections during each separate phase of the excavation. The Phase I
sample collected along the south side of the Phase I excavation was denoted South Wall
sample. The laboratory results indicated no results above Soil -to -Groundwater Maximum
Soil Contaminant Concentrations (MSCCs). The Phase 2 sample collected along the south
IAA Report 934 W. Mallard Creek Church Road Page 5

side of the Phase 2 excavation was denoted South Wall 2 sample. The laboratory results
indicated no results above Soil -to -Groundwater Maximum Soil Contaminant Concentrations
(MSCCs).
West Wall
The sample collected along the west wall of the excavation was denoted West Wall sample.
The laboratory results indicated no results above Soil -to -Groundwater Maximum Soil
Contaminant Concentrations (MSCCs).
North Wall
The Phase 1 sample collected along the north side of the Phase 1 excavation was denoted
North Wall sample. The laboratory results indicated no results above Soil -to -Groundwater
Maximum Soil Contaminant Concentrations (MSCCs). The Phase 2 sample collected along
the north side of the Phase 2 excavation was denoted North Wall 2 sample. The laboratory
results indicated no results above Soil -to -Groundwater Maximum Soil Contaminant
Concentrations (MSCCs).
East Wall
The sample collected along the east wall of the Phase 1 excavation was denoted East Wall
sample. This sample indicated results above Soil -to -Groundwater Maximum Soil
Contaminant Concentrations (MSCCs). For this reason, the excavation was expanded. The
Phase 2 sample collected along the new east side of the Phase 2 excavation was denoted East
Wall 2 sample. The laboratory results indicated no results above Soil -to -Groundwater
Maximum Soil Contaminant Concentrations (MSCCs).
I. Conclusions and Recommendations
The primary source (UST system) of the contamination and the secondary source (affected
soil) of contamination have been removed from the site. Based on this, the property should
be subject to "no further action". Additional work was performed on the site to assess the
groundwater as directed by the prospective purchaser of the property. The sampling took
place in December of 2019, but knowledge of the work along with a copy of the report of this
sampling was given to INENCO after the soil removal fieldwork was completed in June of
2020. This report is attached and shows a groundwater impact exceeding 2L Standards. It is
the authors opinion that the anomaly of clean soil samples (May) and the presence of
groundwater contamination (December) could be explained by seasonal groundwater
fluctuations.
IAA Report 934 W. Mallard Creek Church Road Page 6

Limitations
These environmental services have been performed for the exclusive use of the client for the specific
application to this project. The specifications and operating procedures utilized in the performance of
these services are in accordance with generally accepted engineering principles. No other warranty,
expressed or implied, is made. Although we cannot be responsible for the accuracy of the data
supplied by others, we have no reason to suspect that any of the information provided is inaccurate
unless it has been otherwise noted. Our observations are based upon conditions readily visible at the
site at the time of our site visit(s). Chemical analyses were performed on selected soil samples to
determine the presence and/or concentrations of potential contaminants. Selection of specific EPA
test methods for chemical analyses was based upon (1) information supplied by the client (owner)
concerning the raw materials, products, and/or wastes which may have been handled or generated
within the scope of this project, and (2) the guidelines provided by the NC DEQ. Conclusions
presented in this report are based upon the services described, not on scientific research, tasks or
procedures beyond the scope of described services; nor, beyond the time and/or budgetary constraints
imposed by the client. INENCO, Inc., by virtue of providing the services described in this report,
does not assume the responsibility of the person(s) in charge of the site.

TABLES

INENCO, INC Soil Sample Results Table 1
132 W. Statesville Ave. Initial Abatement Action Report
Mooresville, NC 28115
704-662-8192 Adams Property
934 West Mallard Creek Church Road
Charlotte, NC
UST Release Confirmation Samples
Sample Date: 3/13/19
Sample Depth: 6'
GRO 11.9
DRO 2120
Phase t Post Excavation Samples
Sample Date: 4/9/19 1 4/9/19 1 4/11/19 1 4/11/19 1 4/11/19
Sample Depth: 1 16' 1 16' 1 16' 1 16' 1 18'
Q-1.11MH-1 North Wall I South Wall I North Wall I East Wall I Bottom
Maximum Soil Contaminant Concentrations
Soil-to-GW Residential Industrial / Commercial
EPA Method 8260
n-Butylbenzene
ND
ND
ND
0.0815
ND
4.3
626
16350
sec-Butylbenzene
ND
ND
ND
0.131
ND
3.3
626
16350
Isopropylbenzene
ND
ND
ND
0.03
ND
1.7
1564
40880
Naphthalene
ND
ND
ND
0.066
ND
0.16
313
8176
1,3,5-Trimethylbenzene
ND
I ND
ND
0.786
ND
8.3
782
20440
1,2,4-Trimethylbenzene
ND
ND
ND
0.561
ND
8.5
782
20440
Xylenes
ND
ND
ND
0.05
ND
4.6
3129
81760
EPA Method 8270
Fluorene
ND
ND
ND
0.385
ND
47
620
16400
1-Methylnaphthalene
ND
ND
ND
2.51
ND
0.004
20
100
2-Methylnaphthalene
ND
ND
ND
3.51
ND
3.6
63
1635
MADEP Methods
C5-C8 Aliphatics
ND
ND
ND
8.5
ND
68
939
24528
C9-C18 Aliphatics
ND
ND
ND
669.6
ND
540
1500
40000
C19-C36 Aliphatics
ND
ND
ND
ND
ND
immobile
1 31000
1 810000
C9-C22 Aromatics
ND
ND
ND
399.8
ND
34
1 469
1 12264
Phase 2 Post Excavation Samples
Sample Date:
Sample Depth:
Sample ID#;
5/8/20
5/8/20
5/8/20
Maximum Soil Contaminant Concentrations
16'
16'
16'
Soil-to-GW
Residential
Industrial /Commercial
North Wall 2
East Wall
South Wall
EPA Method 8260
ND
ND
ND
---
---
---
EPA Method 8270
ND
ND
ND
---
---
---
MADEP Methods
ND
ND
ND
---
---
---
All results in mg/kg ND = not detected *** = No MSCC Listed = Exceeds Soil -to -Groundwater MSCCS
468 = Exceeds Residential MSCCS

FIGURES

FIGURE 1
USGS 7.5 MIN TOPOGRAPHY MAP T
John Adams Property
934 West Mallard Creek Church Road
Charlotte, NC
frl-�
L-
Jp1tn A&MIL 01 0.7 003 0A 0. 5 0 b 4 7 0 8 0 7 10 11 1 7 1 3 krn
ViGSBd
0.1 012 RA DA 0.5 0.5 47 a9ml
CipfTopo Seal■ 1112970 I inch - 1Wd fm �•
SURFACE WATER SHOWN IN BLUE
INENCO, Inc.
132 W. STATESVILLE AVE.
MOORESVILLE, NC 28115

FIGURE 2
AERIAL SITE LOCATION
PHOTOGRAPH
John Adams Property
934 West Mallard Creek Church Road
Charlotte, NC
INENCO, Inc.
132 W. STATESVILLE AVE.
4r NIOORESVILLE, NC 28115

SOIL TEST RESULTS
Test Method
Sample #1 Description
@Depth
GRO
DRO
Tank Release Confirm
6'
11.9
2120
W
West Wall
16'
<MSCCs See Table 1
S
South Wall
16'
<MSCCs See Table 1
N
North Wall
16'
<MSCCs See Table 1
E
East Wall
16'
>MSCCs See Table 1
B
I Bottom
18'
<MSCCs See Table 1
S2
South Wall 2
16'
<MSCCs See Table 1
N2
North Wall 2
16'
<MSCCs See Table 1
E2
East Wall 2
16'
<MSCCs See Table 1
All Results mg/kg
UST Area Approximate
Over -Excavation
— - — — Property Line
N
Garage
Driveway
I
/
/
/
/
/
/
/
/
/
/
/
/
/
/
Boundary 4—
Phase 2 Ala//ar
1 i 2 / ROaa
I
/
1
B/
I
/
I
I Approximate /
1 Over -Excavation /
I Boundary
I Phase 1 /
I 1 /
O = Soil Sample Locations /
1------------------- ---V
El Well House
(Abandoned)
934
Creek h rt ha//aro
R°aa
Approximate Former
Location of 285 Gallon
Heating Oil UST
SITE PLAN
Sample Locations
Adams Property
934 W. Mallard Cr. Ch. Rd, Charlotte, NC
41j�INENCO, Inc.
132 W. Statesville Ave, Mooresville, NC
SCALE: As Shown IAA Report
5i8i20 FIGURE 3
Boundary 4—
Phase 2 Ala//ar
1 i 2 / ROaa
I
/
1
B/
I
/
I
I Approximate /
1 Over -Excavation /
I Boundary
I Phase 1 /
I 1 /
O = Soil Sample Locations /
1------------------- ---V
El Well House
(Abandoned)
934
Creek h rt ha//aro
R°aa
Approximate Former
Location of 285 Gallon
Heating Oil UST
SITE PLAN
Sample Locations
Adams Property
934 W. Mallard Cr. Ch. Rd, Charlotte, NC
41j�INENCO, Inc.
132 W. Statesville Ave, Mooresville, NC
SCALE: As Shown IAA Report
5i8i20 FIGURE 3

APPENDICES

/_1 a a =1 /:I_1
INENCO's Standard Operating Procedures

INENCO, INC.
132 W. Statesville Ave.
Mooresville, NC 28115
[phone]
Fax: [phone]
INENCO, Inc. has adopted the following as Standard Operating Procedures for all fieldwork
deemed necessary by the UST Section of the NC DEQ:
"UST SECTION GUIDELINES FOR SAMPLING" NC DEQ, Division of Waste Management,
Underground Storage Tank Section, July 15, 2008 Version, Change 3 December 1, 2013.
Providing Environmental Engineering, Technology and Service

»=1LIQOT -M]
Analytical / Laboratory Reports

` aeeArltral
vnxw.r�:ewes (U."
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 19, 2019
Lee Shank
Carolina Environmental Respons
5648 Daphne Drive
Charlotte, NC 28269
RE: Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
Dear Lee Shank:
Enclosed are the analytical results for sample(s) received by the laboratory on March 13, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
t6k --
Amanda Payne
[e-mail]
[phone]
Project Manager
Enclosures
cc: Steve Hamilton, Carolina Environmental Response Team
Cassandra Kisiah, Carolina Environmental Response
Team
N P
A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

aceAnal&al
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 16

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
John Adams: 934 W Mallard
92421086
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92421086001
TANK SAMPLE #1
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 16

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
Lab Sample ID
Method
92421086001
EPA 8015C Modified
EPA 8015C Modified
ASTM D2974-87
SUMMARY OF DETECTION
Client Sample ID
Parameters
TANK SAMPLE #1
Diesel Range Organics(C10-C28)
Gas Range Organics (C6-C10)
Percent Moisture
Result
Units
2120
mg/kg
11.9
mg/kg
31.5
%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit
Analyzed
36.8
03/18/19 20:37
9.1
03/14/19 16:38
0.10
03/13/1916:30
Qualifiers
Page 4 of 16

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
Method: EPA 8015C Modified
Description: 8015 GCS THC-Diesel
Client: Carolina Environmental Response Team
Date: March 19, 2019
General Information:
1 sample was analyzed for EPA 8015C Modified. All samples were received in acceptable condition with any exceptions noted below or
on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 463555
SO: Surrogate recovery outside laboratory control limits.
• MS (Lab ID: 2521858)
• n-Pentacosane (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 463555
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92421090001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2521858)
• Diesel Range Organics(C10-C28)
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 16

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
Method: EPA 8015C Modified
Description: 8015 GCS THC-Diesel
Client: Carolina Environmental Response Team
Date: March 19, 2019
QC Batch: 463555
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 2521859)
• Diesel Range Organics(C10-C28)
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
Method: EPA 8015C Modified
Description: Gasoline Range Organics
Client: Carolina Environmental Response Team
Date: March 19, 2019
General Information:
1 sample was analyzed for EPA 8015C Modified. All samples were received in acceptable condition with any exceptions noted below or
on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 463320
S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-
analysis).
• TANK SAMPLE #1 (Lab ID: 92421086001)
• 4-Bromofluorobenzene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 7 of 16

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
Sample: TANK SAMPLE #1
Lab ID: 92421086001 Collected: 03/13/19 12:45 Received: 03/13/19 13:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
2120 mg/kg 36.8 5 03/15/19 12:06 03/18/19 20:37
Surrogates
n-Pentacosane (S)
91 % 33-129 5 03/15/19 12:06 03/18/19 20:37 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Gas Range Organics (C6-C10)
11.9 mg/kg 9.1 1 03/14/19 14:56 03/14/19 16:38
Surrogates
4-Bromofluorobenzene (S)
202 % 63-130 1 03/14/19 14:56 03/14/19 16:38 460-00-4 S2
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
31.5 % 0.10 1 03/13/19 16:30
REPORT OF LABORATORY ANALYSIS
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Date: 03/19/2019 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

rr
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
QC Batch: 463320 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030B Analysis Description: Gasoline Range Organics
Associated Lab Samples: 92421086001
METHOD BLANK: 2520925 Matrix: Solid
Associated Lab Samples: 92421086001
Blank Reporting
Parameter Units Result Limit Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 03/14/19 12:21
4-Bromofluorobenzene (S) % 107 63-130 03/14/19 12:21
Qualifiers
LABORATORY CONTROL SAMPLE:
2520926
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
49.7 50.0
101
70-130
4-Bromofluorobenzene (S)
%
117
63-130
MATRIX SPIKE SAMPLE:
2520928
2615975001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 54.9
60.0
109
40-155
4-Bromofluorobenzene (S)
%
101
63-130
SAMPLE DUPLICATE: 2521543
Parameter
Gas Range Organics (C6-C10)
4-Bromofluorobenzene (S)
92421248001 Dup
Units Result Result
mg/kg ND ND
111 104
RPD Qualifiers
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/19/2019 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

rr
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
QC Batch: 463555 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92421086001
METHOD BLANK: 2521856 Matrix: Solid
Associated Lab Samples: 92421086001
Blank Reporting
Parameter Units Result Limit Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 03/15/19 17:37
n-Pentacosane (S) % 66 33-129 03/15/19 17:37
Qualifiers
LABORATORY CONTROL SAMPLE:
2521857
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
66.4 56.6
85
43-130
n-Pentacosane(S)
%
74
33-129
MATRIX SPIKE SAMPLE:
2521858
92421090001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
45.5 81.3
9.1
-45
10-130 M1
n-Pentacosane(S)
%
8
33-129 SO
SAMPLE DUPLICATE: 2521859
Parameter
Diesel Range Organics(C10-C28)
n-Pentacosane(S)
92421090002 Dup
Units Result Result
mg/kg 25.4 16.4
% 68 66
RPD Qualifiers
43 D6
6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
QC Batch: 463119 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92421086001
SAMPLE DUPLICATE: 2519958
92420892001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 15.4 15.7 2
SAMPLE DUPLICATE: 2519959
92421002001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 0.79 0.65 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: John Adams: 934 W Mallard
Pace Project No.: 92421086
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
SO Surrogate recovery outside laboratory control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
REPORT OF LABORATORY ANALYSIS
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Date: 03/19/2019 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
John Adams: 934 W Mallard
92421086
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92421086001
TANK SAMPLE #1
EPA 3546
463555 EPA 8015C Modified
463786
92421086001
TANK SAMPLE #1
EPA 5030B
463320 EPA 8015C Modified
463343
92421086001
TANK SAMPLE #1
ASTM D2974-87
463119
REPORT OF LABORATORY ANALYSIS
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Date: 03/19/2019 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 16

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Page 14 of 16

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16 of 16

aeeArltral
vww.r�:ewes (U."
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
May 02, 2019
Lee Shank
Carolina Environmental Respons
5648 Daphne Drive
Charlotte, NC 28269
RE: Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Dear Lee Shank:
Enclosed are the analytical results for sample(s) received by the laboratory on April 11, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
t6k --
Amanda Payne
[e-mail]
[phone]
Project Manager
Enclosures
cc: Steve Hamilton, Carolina Environmental Response Team
Cassandra Kisiah, Carolina Environmental Response
Team
N P
A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 1 of 49

aceAnal&al
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
934 W. MALLARD CREEK CH. RD
92425107
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92425107001
WEST WALL
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 8270E
PKS
74
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92425107002
SOUTH WALL
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 8270E
PKS
74
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92425107003
NORTH WALL
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 8270E
PKS
74
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92425107004
EAST WALL
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 8270E
PKS
74
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92425107005
BOTTOM
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 8270E
PKS
74
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Lab Sample ID
Method
Client Sample ID
Parameters
92425107001
WEST WALL
ASTM D2974-87
Percent Moisture
92425107002
SOUTH WALL
ASTM D2974-87
Percent Moisture
92425107003
NORTH WALL
ASTM D2974-87
Percent Moisture
92425107004
EAST WALL
MADEP EPH
Aliphatic (C09-C18)
MADEP EPH
Aromatic (C11-C22)
MADEP VPH
Aliphatic (C05-008)
MADEP VPH
Aliphatic (C09-C12)
MADEP VPH
Aliphatic(C09-C12) Adjusted
MADEP VPH
Aromatic (C09-C10)
EPA 8270E
Fluorene
EPA 8270E
1-Methylnaphthalene
EPA 8270E
2-Methylnaphthalene
EPA 8260D
n-Butylbenzene
EPA 8260D
sec-Butylbenzene
EPA 8260D
Isopropylbenzene (Cumene)
EPA 8260D
Naphthalene
EPA 8260D
1,2,4-Trimethylbenzene
EPA 8260D
1,3,5-Trimethylbenzene
EPA 8260D
Xylene (Total)
EPA 8260D
m&p-Xylene
ASTM D2974-87
Percent Moisture
92425107005
BOTTOM
ASTM D2974-87
Percent Moisture
Result Units Report Limit Analyzed
10.6
%
0.10
04/11 /19 18:14
19.6
%
0.10
04/11 /19 18:14
13.4
%
0.10
04/11 /19 18:15
595
mg/kg
225
04/24/19 08:28
N2
368
mg/kg
45.0
04/24/19 08:28
N2
8.5
mg/kg
2.7
04/12/19 03:17
N2
74.6
mg/kg
2.7
04/12/19 03:17
N2
42.8
mg/kg
2.7
04/12/19 03:17
N2
31.8
mg/kg
2.7
04/12/19 03:17
N2
385
ug/kg
375
04/12/19 22:09
2510
ug/kg
375
04/12/19 22:09
3510
ug/kg
751
04/15/1918:55
81.5
ug/kg
4.2
04/16/1919:04
L2
131
ug/kg
4.2
04/16/1919:04
L2
30.0
ug/kg
4.2
04/16/1919:04
L2
66.0
ug/kg
4.2
04/16/1919:04
L2
561
ug/kg
105
04/17/19 20:24
L2
78.6
ug/kg
4.2
04/16/1919:04
L2
50.0
ug/kg
8.4
04/16/1919:04
LS
50.0
ug/kg
8.4
04/16/1919:04
L2
11.2
%
0.10
04/11 /19 18:15
8.6
%
0.10
04/11 /19 18:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 4 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Method: MADEP EPH
Description: MADEP EPH NC Soil
Client: Carolina Environmental Response Team
Date: May 02, 2019
General Information:
5 samples were analyzed for MADEP EPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 470727
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
• EAST WALL (Lab ID: 92425107004)
• Nonatriacontane (S)
S5: Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
• EAST WALL (Lab ID: 92425107004)
• 2-Bromonaphthalene (S)
• 2-Fluorobiphenyl (S)
• o-Terphenyl (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Method: MADEP VPH
Description: VPH NC Soil
Client: Carolina Environmental Response Team
Date: May 02, 2019
General Information:
5 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP VPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 468890
S5: Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
• EAST WALL (Lab ID: 92425107004)
• 4-Bromofluorobenzene (FID) (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Method: EPA 8270E
Description: 8270E MSSV Microwave
Client: Carolina Environmental Response Team
Date: May 02, 2019
General Information:
5 samples were analyzed for EPA 8270E. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Method: EPA 8260D
Description: 8260D/5035A Volatile Organics
Client: Carolina Environmental Response Team
Date: May 02, 2019
General Information:
5 samples were analyzed for EPA 8260D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 469508
S5: Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
• EAST WALL (Lab ID: 92425107004)
• 4-Bromofluorobenzene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: 469508
P2: Re -extraction or re -analysis could not be performed due to insufficient sample amount.
• WEST WALL (Lab ID: 92425107001)
• Toluene-d8 (S)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Method: EPA 8260D
Description: 8260D/5035A Volatile Organics
Client: Carolina Environmental Response Team
Date: May 02, 2019
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: WEST WALL
Lab ID: 92425107001
Collected: 04/09/19
12:15
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
11.2
1
04/22/19 08:58
04/23/19 20:23
N2
Aliphatic (C19-C36)
ND
mg/kg
11.2
1
04/22/19 08:58
04/23/19 20:23
N2
Aromatic (C11-C22)
ND
mg/kg
11.2
1
04/22/19 08:58
04/23/19 20:23
N2
Surrogates
Nonatriacontane (S)
46
%
40-140
1
04/22/19 08:58
04/23/19 20:23
7194-86-7
o-Terphenyl (S)
68
%
40-140
1
04/22/19 08:58
04/23/19 20:23
84-15-1
2-Fluorobiphenyl (S)
70
%
40-140
1
04/22/19 08:58
04/23/19 20:23
321-60-8
2-Bromonaphthalene (S)
79
%
40-140
1
04/22/19 08:58
04/23/19 20:23
580-13-2
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-008)
ND
mg/kg
2.5
1
04/11/19 17:38
04/11/19 19:55
N2
Aliphatic (C09-C12)
ND
mg/kg
2.5
1
04/11/19 17:38
04/11/19 19:55
N2
Aliphatic(C09-C12)Adjusted
ND
mg/kg
2.5
1
04/11/19 17:38
04/11/19 19:55
N2
Aromatic (C09-C10)
ND
mg/kg
2.5
1
04/11/19 17:38
04/11/19 19:55
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
96
%
70-130
1
04/11/19 17:38
04/11/19 19:55
460-00-4
4-Bromofluorobenzene (PID) (S)
95
%
70-130
1
04/11/19 17:38
04/11/19 19:55
460-00-4
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
83-32-9
Acenaphthylene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
208-96-8
Aniline
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
62-53-3
Anthracene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
120-12-7
Benzo(a)anthracene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
56-55-3
Benzo(a)pyrene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
207-08-9
Benzoic Acid
ND
ug/kg
1860
1
04/12/19 10:06
04/12/19 20:36
65-85-0
v1
Benzyl alcohol
ND
ug/kg
744
1
04/12/19 10:06
04/12/19 20:36
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
101-55-3
Butylbenzylphthalate
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
744
1
04/12/19 10:06
04/12/19 20:36
59-50-7
4-Chloroaniline
ND
ug/kg
1860
1
04/12/19 10:06
04/12/19 20:36
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
111-44-4
2-Chloronaphthalene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
91-58-7
2-Chlorophenol
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
7005-72-3
Chrysene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
53-70-3
Dibenzofuran
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1860
1
04/12/19 10:06
04/12/19 20:36
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: WEST WALL Lab ID: 92425107001 Collected: 04/09/19 12:15 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
120-83-2
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
84-66-2
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
105-67-9
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
131-11-3
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
84-74-2
ND
ug/kg
744
1
04/12/19 10:06
04/12/19 20:36
534-52-1
ND
ug/kg
1860
1
04/12/19 10:06
04/12/19 20:36
51-28-5
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
121-14-2
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
606-20-2
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
117-84-0
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
117-81-7
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
206-44-0
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
86-73-7
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
87-68-3
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
118-74-1
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
77-47-4
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
67-72-1
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
193-39-5
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
78-59-1
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
90-12-0
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
91-57-6
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
95-48-7
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
15831-10-4
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
91-20-3
ND
ug/kg
1860
1
04/12/19 10:06
04/12/19 20:36
88-74-4
ND
ug/kg
1860
1
04/12/19 10:06
04/12/19 20:36
99-09-2
ND
ug/kg
744
1
04/12/19 10:06
04/12/19 20:36
100-01-6
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
98-95-3
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
88-75-5
ND
ug/kg
1860
1
04/12/19 10:06
04/12/19 20:36
100-02-7
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
62-75-9
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
621-64-7
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
86-30-6
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
108-60-1
ND
ug/kg
1860
1
04/12/19 10:06
04/12/19 20:36
87-86-5
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
85-01-8
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
108-95-2
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
129-00-0
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
120-82-1
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
95-95-4
ND
ug/kg
372
1
04/12/19 10:06
04/12/19 20:36
88-06-2
60
%
23-110
1
04/12/19 10:06
04/12/19 20:36
4165-60-0
57
%
30-110
1
04/12/19 10:06
04/12/19 20:36
321-60-8
60
%
28-110
1
04/12/19 10:06
04/12/19 20:36
1718-51-0
60
%
22-110
1
04/12/19 10:06
04/12/19 20:36
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: WEST WALL
Lab ID: 92425107001
Collected: 04/09/19
12:15
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)
59
%
13-110
1
04/12/19 10:06
04/12/19 20:36
367-12-4
2,4,6-Tribromophenol (S)
67
%
27-110
1
04/12/19 10:06
04/12/19 20:36
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
2410
25
04/15/19 18:39
04/17/19 19:59
67-64-1
L2
Benzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
71-43-2
L2
Bromobenzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
108-86-1
L2
Bromochloromethane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
74-97-5
L2
Bromodichloromethane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
75-27-4
L2
Bromoform
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
75-25-2
L2
Bromomethane
ND
ug/kg
241
25
04/15/19 18:39
04/17/19 19:59
74-83-9
L2
2-Butanone (MEK)
ND
ug/kg
2410
25
04/15/19 18:39
04/17/19 19:59
78-93-3
L2
n-Butylbenzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
104-51-8
L2
sec-Butylbenzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
135-98-8
L2
tert-Butyl benzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
98-06-6
L2
Carbon tetrachloride
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
56-23-5
L2
Chlorobenzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
108-90-7
L2
Chloroethane
ND
ug/kg
241
25
04/15/19 18:39
04/17/19 19:59
75-00-3
L2
Chloroform
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
67-66-3
L2
Chloromethane
ND
ug/kg
241
25
04/15/19 18:39
04/17/19 19:59
74-87-3
L2
2-Chlorotoluene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
95-49-8
L2
4-Chlorotoluene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
106-43-4
L2
1,2-Dibromo-3-chloropropane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
96-12-8
L2
Dibromochloromethane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
124-48-1
L2
1,2-Dibromoethane (EDB)
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
106-93-4
L2
Dibromomethane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
74-95-3
L2
1,2-Dichlorobenzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
95-50-1
L2
1,3-Dichlorobenzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
541-73-1
L2
1,4-Dichlorobenzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
106-46-7
L2
Dichlorodifluoromethane
ND
ug/kg
241
25
04/15/19 18:39
04/17/19 19:59
75-71-8
L2
1,1-Dichloroethane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
75-34-3
L2
1,2-Dichloroethane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
107-06-2
L2
1,1-Dichloroethene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
75-35-4
L2
cis-1,2-Dichloroethene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
156-59-2
L2
trans-1,2-Dichloroethene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
156-60-5
L2
1,2-Dichloropropane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
78-87-5
L2
1,3-Dichloropropane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
142-28-9
L2
2,2-Dichloropropane
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
594-20-7
L2
1,1-Dichloropropene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
563-58-6
L2
cis-1,3-Dichloropropene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
10061-01-5
L2
trans- 1,3-Dichloropropene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
10061-02-6
L2
Diisopropyl ether
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
108-20-3
L2
Ethylbenzene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
100-41-4
L2
Hexachloro-1,3-butadiene
ND
ug/kg
120
25
04/15/19 18:39
04/17/19 19:59
87-68-3
L2
2-Hexanone
ND
ug/kg
1200
25
04/15/19 18:39
04/17/19 19:59
591-78-6
L2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: WEST WALL Lab ID: 92425107001 Collected: 04/09/19 12:15 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
98-82-8
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
99-87-6
L2
ND
ug/kg
482
25
04/15/1918:39
04/17/1919:59
75-09-2
L2
ND
ug/kg
1200
25
04/15/1918:39
04/17/1919:59
108-10-1
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
1634-04-4
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
91-20-3
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
103-65-1
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
100-42-5
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
630-20-6
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
79-34-5
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
127-18-4
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
108-88-3
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
87-61-6
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
120-82-1
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
71-55-6
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
79-00-5
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
79-01-6
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
75-69-4
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
96-18-4
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
95-63-6
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
108-67-8
L2
ND
ug/kg
1200
25
04/15/1918:39
04/17/1919:59
108-05-4
L2
ND
ug/kg
241
25
04/15/1918:39
04/17/1919:59
75-01-4
L2
ND
ug/kg
241
25
04/15/1918:39
04/17/1919:59
1330-20-7
LS
ND
ug/kg
241
25
04/15/1918:39
04/17/1919:59
179601-23-1
L2
ND
ug/kg
120
25
04/15/1918:39
04/17/1919:59
95-47-6
L2
110
%
70-130
25
04/15/1918:39
04/17/1919:59
2037-26-5
P2
103
%
70-130
25
04/15/1918:39
04/17/1919:59
460-00-4
100
%
70-132
25
04/15/1918:39
04/17/1919:59
17060-07-0
Analytical Method: ASTM D2974-87
10.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
04/11/19 18:14
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: SOUTH WALL
Lab ID: 92425107002
Collected: 04/09/19
12:30
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
12.4
1
04/22/19 08:58
04/23/19 20:51
N2
Aliphatic (C19-C36)
ND
mg/kg
12.4
1
04/22/19 08:58
04/23/19 20:51
N2
Aromatic (C11-C22)
ND
mg/kg
12.4
1
04/22/19 08:58
04/23/19 20:51
N2
Surrogates
Nonatriacontane (S)
63
%
40-140
1
04/22/19 08:58
04/23/19 20:51
7194-86-7
o-Terphenyl (S)
109
%
40-140
1
04/22/19 08:58
04/23/19 20:51
84-15-1
2-Fluorobiphenyl (S)
130
%
40-140
1
04/22/19 08:58
04/23/19 20:51
321-60-8
2-Bromonaphthalene (S)
137
%
40-140
1
04/22/19 08:58
04/23/19 20:51
580-13-2
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-008)
ND
mg/kg
3.3
1
04/11/19 17:38
04/11/19 20:25
N2
Aliphatic (C09-C12)
ND
mg/kg
3.3
1
04/11/19 17:38
04/11/19 20:25
N2
Aliphatic(C09-C12)Adjusted
ND
mg/kg
3.3
1
04/11/19 17:38
04/11/19 20:25
N2
Aromatic (C09-C10)
ND
mg/kg
3.3
1
04/11/19 17:38
04/11/19 20:25
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
97
%
70-130
1
04/11/19 17:38
04/11/19 20:25
460-00-4
4-Bromofluorobenzene (PID) (S)
96
%
70-130
1
04/11/19 17:38
04/11/19 20:25
460-00-4
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
83-32-9
Acenaphthylene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
208-96-8
Aniline
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
62-53-3
Anthracene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
120-12-7
Benzo(a)anthracene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
56-55-3
Benzo(a)pyrene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
207-08-9
Benzoic Acid
ND
ug/kg
2070
1
04/12/19 10:06
04/12/19 21:07
65-85-0
v1
Benzyl alcohol
ND
ug/kg
829
1
04/12/19 10:06
04/12/19 21:07
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
101-55-3
Butylbenzylphthalate
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
829
1
04/12/19 10:06
04/12/19 21:07
59-50-7
4-Chloroaniline
ND
ug/kg
2070
1
04/12/19 10:06
04/12/19 21:07
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
111-44-4
2-Chloronaphthalene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
91-58-7
2-Chlorophenol
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
7005-72-3
Chrysene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
53-70-3
Dibenzofuran
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2070
1
04/12/19 10:06
04/12/19 21:07
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: SOUTH WALL Lab ID: 92425107002 Collected: 04/09/19 12:30 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
120-83-2
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
84-66-2
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
105-67-9
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
131-11-3
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
84-74-2
ND
ug/kg
829
1
04/12/19 10:06
04/12/19 21:07
534-52-1
ND
ug/kg
2070
1
04/12/19 10:06
04/12/19 21:07
51-28-5
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
121-14-2
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
606-20-2
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
117-84-0
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
117-81-7
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
206-44-0
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
86-73-7
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
87-68-3
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
118-74-1
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
77-47-4
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
67-72-1
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
193-39-5
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
78-59-1
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
90-12-0
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
91-57-6
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
95-48-7
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
15831-10-4
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
91-20-3
ND
ug/kg
2070
1
04/12/19 10:06
04/12/19 21:07
88-74-4
ND
ug/kg
2070
1
04/12/19 10:06
04/12/19 21:07
99-09-2
ND
ug/kg
829
1
04/12/19 10:06
04/12/19 21:07
100-01-6
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
98-95-3
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
88-75-5
ND
ug/kg
2070
1
04/12/19 10:06
04/12/19 21:07
100-02-7
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
62-75-9
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
621-64-7
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
86-30-6
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
108-60-1
ND
ug/kg
2070
1
04/12/19 10:06
04/12/19 21:07
87-86-5
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
85-01-8
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
108-95-2
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
129-00-0
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
120-82-1
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
95-95-4
ND
ug/kg
414
1
04/12/19 10:06
04/12/19 21:07
88-06-2
63
%
23-110
1
04/12/19 10:06
04/12/19 21:07
4165-60-0
57
%
30-110
1
04/12/19 10:06
04/12/19 21:07
321-60-8
55
%
28-110
1
04/12/19 10:06
04/12/19 21:07
1718-51-0
63
%
22-110
1
04/12/19 10:06
04/12/19 21:07
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: SOUTH WALL
Lab ID: 92425107002
Collected: 04/09/19
12:30
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)
63
%
13-110
1
04/12/19 10:06
04/12/19 21:07
367-12-4
2,4,6-Tribromophenol (S)
70
%
27-110
1
04/12/19 10:06
04/12/19 21:07
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D
Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
2530
25
04/15/19 18:39
04/16/19 17:00
67-64-1
L2
Benzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
71-43-2
L2
Bromobenzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
108-86-1
L2
Bromochloromethane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
74-97-5
L2
Bromodichloromethane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
75-27-4
L2
Bromoform
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
75-25-2
L2
Bromomethane
ND
ug/kg
253
25
04/15/19 18:39
04/16/19 17:00
74-83-9
L2
2-Butanone (MEK)
ND
ug/kg
2530
25
04/15/19 18:39
04/16/19 17:00
78-93-3
L2
n-Butylbenzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
104-51-8
L2
sec-Butylbenzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
135-98-8
L2
tert-Butyl benzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
98-06-6
L2
Carbon tetrachloride
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
56-23-5
L2
Chlorobenzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
108-90-7
L2
Chloroethane
ND
ug/kg
253
25
04/15/19 18:39
04/16/19 17:00
75-00-3
L2,v1
Chloroform
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
67-66-3
L2
Chloromethane
ND
ug/kg
253
25
04/15/19 18:39
04/16/19 17:00
74-87-3
L2
2-Chlorotoluene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
95-49-8
L2
4-Chlorotoluene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
106-43-4
L2
1,2-Dibromo-3-chloropropane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
96-12-8
L2
Dibromochloromethane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
124-48-1
L2
1,2-Dibromoethane (EDB)
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
106-93-4
L2
Dibromomethane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
74-95-3
L2
1,2-Dichlorobenzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
95-50-1
L2
1,3-Dichlorobenzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
541-73-1
L2
1,4-Dichlorobenzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
106-46-7
L2
Dichlorodifluoromethane
ND
ug/kg
253
25
04/15/19 18:39
04/16/19 17:00
75-71-8
L2
1,1-Dichloroethane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
75-34-3
L2
1,2-Dichloroethane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
107-06-2
L2
1,1-Dichloroethene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
75-35-4
L2
cis-1,2-Dichloroethene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
156-59-2
L2
trans-1,2-Dichloroethene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
156-60-5
L2
1,2-Dichloropropane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
78-87-5
L2
1,3-Dichloropropane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
142-28-9
L2
2,2-Dichloropropane
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
594-20-7
L2
1,1-Dichloropropene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
563-58-6
L2
cis-1,3-Dichloropropene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
10061-01-5
L2
trans- 1,3-Dichloropropene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
10061-02-6
L2
Diisopropyl ether
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
108-20-3
L2
Ethylbenzene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
100-41-4
L2
Hexachloro-1,3-butadiene
ND
ug/kg
126
25
04/15/19 18:39
04/16/19 17:00
87-68-3
L2
2-Hexanone
ND
ug/kg
1260
25
04/15/19 18:39
04/16/19 17:00
591-78-6
L2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: SOUTH WALL Lab ID: 92425107002 Collected: 04/09/19 12:30 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
98-82-8
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
99-87-6
L2
ND
ug/kg
505
25
04/15/1918:39
04/16/1917:00
75-09-2
L2
ND
ug/kg
1260
25
04/15/1918:39
04/16/1917:00
108-10-1
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
1634-04-4
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
91-20-3
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
103-65-1
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
100-42-5
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
630-20-6
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
79-34-5
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
127-18-4
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
108-88-3
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
87-61-6
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
120-82-1
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
71-55-6
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
79-00-5
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
79-01-6
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
75-69-4
L2,v1
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
96-18-4
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
95-63-6
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
108-67-8
L2
ND
ug/kg
1260
25
04/15/1918:39
04/16/1917:00
108-05-4
L2
ND
ug/kg
253
25
04/15/1918:39
04/16/1917:00
75-01-4
L2
ND
ug/kg
253
25
04/15/1918:39
04/16/1917:00
1330-20-7
LS
ND
ug/kg
253
25
04/15/1918:39
04/16/1917:00
179601-23-1
L2
ND
ug/kg
126
25
04/15/1918:39
04/16/1917:00
95-47-6
L2
107
%
70-130
25
04/15/1918:39
04/16/1917:00
2037-26-5
97
%
70-130
25
04/15/1918:39
04/16/1917:00
460-00-4
101
%
70-132
25
04/15/1918:39
04/16/1917:00
17060-07-0
Analytical Method: ASTM D2974-87
19.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
04/11/19 18:14
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: NORTH WALL
Lab ID: 92425107003
Collected: 04/11/19
09:30
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
11.5
1
04/22/19 08:58
04/23/19 21:18
N2
Aliphatic (C19-C36)
ND
mg/kg
11.5
1
04/22/19 08:58
04/23/19 21:18
N2
Aromatic (C11-C22)
ND
mg/kg
11.5
1
04/22/19 08:58
04/23/19 21:18
N2
Surrogates
Nonatriacontane (S)
46
%
40-140
1
04/22/19 08:58
04/23/19 21:18
7194-86-7
o-Terphenyl (S)
61
%
40-140
1
04/22/19 08:58
04/23/19 21:18
84-15-1
2-Fluorobiphenyl (S)
69
%
40-140
1
04/22/19 08:58
04/23/19 21:18
321-60-8
2-Bromonaphthalene (S)
71
%
40-140
1
04/22/19 08:58
04/23/19 21:18
580-13-2
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
ND
mg/kg
2.7
1
04/11/19 17:38
04/11/19 20:54
N2
Aliphatic (C09-C12)
ND
mg/kg
2.7
1
04/11/19 17:38
04/11/19 20:54
N2
Aliphatic(C09-C12)Adjusted
ND
mg/kg
2.7
1
04/11/19 17:38
04/11/19 20:54
N2
Aromatic (C09-C10)
ND
mg/kg
2.7
1
04/11/19 17:38
04/11/19 20:54
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
98
%
70-130
1
04/11/19 17:38
04/11/19 20:54
460-00-4
4-Bromofluorobenzene (PID) (S)
97
%
70-130
1
04/11/19 17:38
04/11/19 20:54
460-00-4
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
83-32-9
Acenaphthylene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
208-96-8
Aniline
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
62-53-3
Anthracene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
120-12-7
Benzo(a)anthracene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
56-55-3
Benzo(a)pyrene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
207-08-9
Benzoic Acid
ND
ug/kg
1910
1
04/12/19 10:06
04/12/19 21:38
65-85-0
v1
Benzyl alcohol
ND
ug/kg
764
1
04/12/19 10:06
04/12/19 21:38
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
101-55-3
Butylbenzylphthalate
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
764
1
04/12/19 10:06
04/12/19 21:38
59-50-7
4-Chloroaniline
ND
ug/kg
1910
1
04/12/19 10:06
04/12/19 21:38
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
111-44-4
2-Chloronaphthalene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
91-58-7
2-Chlorophenol
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
7005-72-3
Chrysene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
53-70-3
Dibenzofuran
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1910
1
04/12/19 10:06
04/12/19 21:38
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: NORTH WALL Lab ID: 92425107003 Collected: 04/11/19 09:30 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
120-83-2
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
84-66-2
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
105-67-9
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
131-11-3
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
84-74-2
ND
ug/kg
764
1
04/12/19 10:06
04/12/19 21:38
534-52-1
ND
ug/kg
1910
1
04/12/19 10:06
04/12/19 21:38
51-28-5
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
121-14-2
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
606-20-2
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
117-84-0
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
117-81-7
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
206-44-0
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
86-73-7
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
87-68-3
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
118-74-1
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
77-47-4
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
67-72-1
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
193-39-5
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
78-59-1
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
90-12-0
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
91-57-6
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
95-48-7
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
15831-10-4
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
91-20-3
ND
ug/kg
1910
1
04/12/19 10:06
04/12/19 21:38
88-74-4
ND
ug/kg
1910
1
04/12/19 10:06
04/12/19 21:38
99-09-2
ND
ug/kg
764
1
04/12/19 10:06
04/12/19 21:38
100-01-6
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
98-95-3
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
88-75-5
ND
ug/kg
1910
1
04/12/19 10:06
04/12/19 21:38
100-02-7
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
62-75-9
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
621-64-7
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
86-30-6
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
108-60-1
ND
ug/kg
1910
1
04/12/19 10:06
04/12/19 21:38
87-86-5
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
85-01-8
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
108-95-2
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
129-00-0
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
120-82-1
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
95-95-4
ND
ug/kg
382
1
04/12/19 10:06
04/12/19 21:38
88-06-2
54
%
23-110
1
04/12/19 10:06
04/12/19 21:38
4165-60-0
53
%
30-110
1
04/12/19 10:06
04/12/19 21:38
321-60-8
57
%
28-110
1
04/12/19 10:06
04/12/19 21:38
1718-51-0
54
%
22-110
1
04/12/19 10:06
04/12/19 21:38
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: NORTH WALL
Lab ID: 92425107003
Collected: 04/11/19
09:30
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)
53
%
13-110
1
04/12/19 10:06
04/12/19 21:38
367-12-4
2,4,6-Tribromophenol (S)
61
%
27-110
1
04/12/19 10:06
04/12/19 21:38
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D
Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
107
1
04/15/19 18:35
04/16/19 14:57
67-64-1
L2
Benzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
71-43-2
L2
Bromobenzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
108-86-1
L2
Bromochloromethane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
74-97-5
L2
Bromodichloromethane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
75-27-4
L2
Bromoform
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
75-25-2
L2
Bromomethane
ND
ug/kg
10.7
1
04/15/19 18:35
04/16/19 14:57
74-83-9
L2
2-Butanone (MEK)
ND
ug/kg
107
1
04/15/19 18:35
04/16/19 14:57
78-93-3
L2
n-Butylbenzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
104-51-8
L2
sec-Butylbenzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
135-98-8
L2
tert-Butyl benzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
98-06-6
L2
Carbon tetrachloride
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
56-23-5
L2
Chlorobenzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
108-90-7
L2
Chloroethane
ND
ug/kg
10.7
1
04/15/19 18:35
04/16/19 14:57
75-00-3
L2,v1
Chloroform
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
67-66-3
L2
Chloromethane
ND
ug/kg
10.7
1
04/15/19 18:35
04/16/19 14:57
74-87-3
L2
2-Chlorotoluene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
95-49-8
L2
4-Chlorotoluene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
106-43-4
L2
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
96-12-8
L2
Dibromochloromethane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
124-48-1
L2
1,2-Dibromoethane (EDB)
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
106-93-4
L2
Dibromomethane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
74-95-3
L2
1,2-Dichlorobenzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
95-50-1
L2
1,3-Dichlorobenzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
541-73-1
L2
1,4-Dichlorobenzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
106-46-7
L2
Dichlorodifluoromethane
ND
ug/kg
10.7
1
04/15/19 18:35
04/16/19 14:57
75-71-8
L2
1,1-Dichloroethane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
75-34-3
L2
1,2-Dichloroethane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
107-06-2
L2
1,1-Dichloroethene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
75-35-4
L2
cis-1,2-Dichloroethene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
156-59-2
L2
trans-1,2-Dichloroethene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
156-60-5
L2
1,2-Dichloropropane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
78-87-5
L2
1,3-Dichloropropane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
142-28-9
L2
2,2-Dichloropropane
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
594-20-7
L2
1,1-Dichloropropene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
563-58-6
L2
cis-1,3-Dichloropropene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
10061-01-5
L2
trans- 1,3-Dichloropropene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
10061-02-6
L2
Diisopropyl ether
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
108-20-3
L2
Ethylbenzene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
100-41-4
L2
Hexachloro-1,3-butadiene
ND
ug/kg
5.4
1
04/15/19 18:35
04/16/19 14:57
87-68-3
L2
2-Hexanone
ND
ug/kg
53.6
1
04/15/19 18:35
04/16/19 14:57
591-78-6
L2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: NORTH WALL Lab ID: 92425107003 Collected: 04/11/19 09:30 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
98-82-8
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
99-87-6
L2
ND
ug/kg
21.5
1
04/15/1918:35
04/16/1914:57
75-09-2
L2
ND
ug/kg
53.6
1
04/15/1918:35
04/16/1914:57
108-10-1
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
1634-04-4
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
91-20-3
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
103-65-1
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
100-42-5
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
630-20-6
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
79-34-5
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
127-18-4
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
108-88-3
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
87-61-6
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
120-82-1
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
71-55-6
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
79-00-5
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
79-01-6
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
75-69-4
L2,v1
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
96-18-4
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
95-63-6
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
108-67-8
L2
ND
ug/kg
53.6
1
04/15/1918:35
04/16/1914:57
108-05-4
L2
ND
ug/kg
10.7
1
04/15/1918:35
04/16/1914:57
75-01-4
L2
ND
ug/kg
10.7
1
04/15/1918:35
04/16/1914:57
1330-20-7
LS
ND
ug/kg
10.7
1
04/15/1918:35
04/16/1914:57
179601-23-1
L2
ND
ug/kg
5.4
1
04/15/1918:35
04/16/1914:57
95-47-6
L2
106
%
70-130
1
04/15/1918:35
04/16/1914:57
2037-26-5
96
%
70-130
1
04/15/1918:35
04/16/1914:57
460-00-4
91
%
70-132
1
04/15/1918:35
04/16/1914:57
17060-07-0
Analytical Method: ASTM D2974-87
13.4 % 0.10 1
REPORT OF LABORATORY ANALYSIS
04/11/19 18:15
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: EAST WALL
Lab ID: 92425107004
Collected: 04/11/19
10:30
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
595
mg/kg
225
20
04/22/19 08:58
04/24/19 08:28
N2
Aliphatic (C19-C36)
ND
mg/kg
225
20
04/22/19 08:58
04/24/19 08:28
N2
Aromatic (C11-C22)
368
mg/kg
45.0
4
04/22/19 08:58
04/24/19 08:28
N2
Surrogates
Nonatriacontane (S)
0
%
40-140
20
04/22/19 08:58
04/24/19 08:28
7194-86-7
S4
o-Terphenyl (S)
142
%
40-140
4
04/22/19 08:58
04/24/19 08:28
84-15-1
S5
2-Fluorobiphenyl (S)
224
%
40-140
4
04/22/19 08:58
04/24/19 08:28
321-60-8
S5
2-Bromonaphthalene (S)
955
%
40-140
4
04/22/19 08:58
04/24/19 08:28
580-13-2
S5
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
8.5
mg/kg
2.7
1
04/11/19 17:38
04/12/19 03:17
N2
Aliphatic (C09-C12)
74.6
mg/kg
2.7
1
04/11/19 17:38
04/12/19 03:17
N2
Aliphatic(C09-C12) Adjusted
42.8
mg/kg
2.7
1
04/11/19 17:38
04/12/19 03:17
N2
Aromatic (C09-C10)
31.8
mg/kg
2.7
1
04/11/19 17:38
04/12/19 03:17
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
153
%
70-130
1
04/11/19 17:38
04/12/19 03:17
460-00-4
S5
4-Bromofluorobenzene (PID) (S)
ill
%
70-130
1
04/11/19 17:38
04/12/19 03:17
460-00-4
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
83-32-9
Acenaphthylene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
208-96-8
Aniline
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
62-53-3
Anthracene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
120-12-7
Benzo(a)anthracene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
56-55-3
Benzo(a)pyrene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
207-08-9
Benzoic Acid
ND
ug/kg
1880
1
04/12/19 10:06
04/12/19 22:09
65-85-0
vl
Benzyl alcohol
ND
ug/kg
751
1
04/12/19 10:06
04/12/19 22:09
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
101-55-3
Butylbenzylphthalate
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
751
1
04/12/19 10:06
04/12/19 22:09
59-50-7
4-Chloroaniline
ND
ug/kg
1880
1
04/12/19 10:06
04/12/19 22:09
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
111-44-4
2-Chloronaphthalene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
91-58-7
2-Chlorophenol
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
7005-72-3
Chrysene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
53-70-3
Dibenzofuran
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1880
1
04/12/19 10:06
04/12/19 22:09
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: EAST WALL Lab ID: 92425107004 Collected: 04/11/19 10:30 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
120-83-2
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
84-66-2
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
105-67-9
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
131-11-3
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
84-74-2
ND
ug/kg
751
1
04/12/19 10:06
04/12/19 22:09
534-52-1
ND
ug/kg
1880
1
04/12/19 10:06
04/12/19 22:09
51-28-5
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
121-14-2
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
606-20-2
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
117-84-0
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
117-81-7
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
206-44-0
385
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
86-73-7
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
87-68-3
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
118-74-1
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
77-47-4
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
67-72-1
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
193-39-5
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
78-59-1
2510
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
90-12-0
3510
ug/kg
751
2
04/12/19 10:06
04/15/1918:55
91-57-6
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
95-48-7
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
15831-10-4
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
91-20-3
ND
ug/kg
1880
1
04/12/19 10:06
04/12/19 22:09
88-74-4
ND
ug/kg
1880
1
04/12/19 10:06
04/12/19 22:09
99-09-2
ND
ug/kg
751
1
04/12/19 10:06
04/12/19 22:09
100-01-6
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
98-95-3
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
88-75-5
ND
ug/kg
1880
1
04/12/19 10:06
04/12/19 22:09
100-02-7
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
62-75-9
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
621-64-7
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
86-30-6
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
108-60-1
ND
ug/kg
1880
1
04/12/19 10:06
04/12/19 22:09
87-86-5
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
85-01-8
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
108-95-2
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
129-00-0
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
120-82-1
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
95-95-4
ND
ug/kg
375
1
04/12/19 10:06
04/12/19 22:09
88-06-2
66
%
23-110
1
04/12/19 10:06
04/12/19 22:09
4165-60-0
54
%
30-110
1
04/12/19 10:06
04/12/19 22:09
321-60-8
73
%
28-110
1
04/12/19 10:06
04/12/19 22:09
1718-51-0
65
%
22-110
1
04/12/19 10:06
04/12/19 22:09
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: EAST WALL
Lab ID: 92425107004
Collected: 04/11/19
10:30
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)
66
%
13-110
1
04/12/19 10:06
04/12/19 22:09
367-12-4
2,4,6-Tribromophenol (S)
81
%
27-110
1
04/12/19 10:06
04/12/19 22:09
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D
Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
83.6
1
04/15/19 18:35
04/16/19 19:04
67-64-1
L2
Benzene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
71-43-2
L2
Bromobenzene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
108-86-1
L2
Bromochloromethane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
74-97-5
L2
Bromodichloromethane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
75-27-4
L2
Bromoform
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
75-25-2
L2
Bromomethane
ND
ug/kg
8.4
1
04/15/19 18:35
04/16/19 19:04
74-83-9
L2
2-Butanone (MEK)
ND
ug/kg
83.6
1
04/15/19 18:35
04/16/19 19:04
78-93-3
L2
n-Butylbenzene
81.5
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
104-51-8
L2
sec-Butylbenzene
131
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
135-98-8
L2
tert-Butyl benzene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
98-06-6
L2
Carbon tetrachloride
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
56-23-5
L2
Chlorobenzene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
108-90-7
L2
Chloroethane
ND
ug/kg
8.4
1
04/15/19 18:35
04/16/19 19:04
75-00-3
L2,v1
Chloroform
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
67-66-3
L2
Chloromethane
ND
ug/kg
8.4
1
04/15/19 18:35
04/16/19 19:04
74-87-3
L2
2-Chlorotoluene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
95-49-8
L2
4-Chlorotoluene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
106-43-4
L2
1,2-Dibromo-3-chloropropane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
96-12-8
L2
Dibromochloromethane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
124-48-1
L2
1,2-Dibromoethane (EDB)
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
106-93-4
L2
Dibromomethane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
74-95-3
L2
1,2-Dichlorobenzene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
95-50-1
L2
1,3-Dichlorobenzene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
541-73-1
L2
1,4-Dichlorobenzene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
106-46-7
L2
Dichlorodifluoromethane
ND
ug/kg
8.4
1
04/15/19 18:35
04/16/19 19:04
75-71-8
L2
1,1-Dichloroethane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
75-34-3
L2
1,2-Dichloroethane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
107-06-2
L2
1,1-Dichloroethene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
75-35-4
L2
cis-1,2-Dichloroethene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
156-59-2
L2
trans-1,2-Dichloroethene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
156-60-5
L2
1,2-Dichloropropane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
78-87-5
L2
1,3-Dichloropropane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
142-28-9
L2
2,2-Dichloropropane
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
594-20-7
L2
1,1-Dichloropropene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
563-58-6
L2
cis-1,3-Dichloropropene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
10061-01-5
L2
trans- 1,3-Dichloropropene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
10061-02-6
L2
Diisopropyl ether
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
108-20-3
L2
Ethylbenzene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
100-41-4
L2
Hexachloro-1,3-butadiene
ND
ug/kg
4.2
1
04/15/19 18:35
04/16/19 19:04
87-68-3
L2
2-Hexanone
ND
ug/kg
41.8
1
04/15/19 18:35
04/16/19 19:04
591-78-6
L2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: EAST WALL Lab ID: 92425107004 Collected: 04/11/19 10:30 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
30.0
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
98-82-8
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
99-87-6
L2
ND
ug/kg
16.7
1
04/15/1918:35
04/16/1919:04
75-09-2
L2
ND
ug/kg
41.8
1
04/15/1918:35
04/16/1919:04
108-10-1
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
1634-04-4
L2
66.0
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
91-20-3
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
103-65-1
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
100-42-5
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
630-20-6
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
79-34-5
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
127-18-4
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
108-88-3
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
87-61-6
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
120-82-1
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
71-55-6
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
79-00-5
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
79-01-6
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
75-69-4
L2,v1
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
96-18-4
L2
561
ug/kg
105
25
04/15/19 18:35
04/17/19 20:24
95-63-6
L2
78.6
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
108-67-8
L2
ND
ug/kg
41.8
1
04/15/1918:35
04/16/1919:04
108-05-4
L2
ND
ug/kg
8.4
1
04/15/1918:35
04/16/1919:04
75-01-4
L2
50.0
ug/kg
8.4
1
04/15/1918:35
04/16/1919:04
1330-20-7
LS
50.0
ug/kg
8.4
1
04/15/1918:35
04/16/1919:04
179601-23-1
L2
ND
ug/kg
4.2
1
04/15/1918:35
04/16/1919:04
95-47-6
L2
113
%
70-130
1
04/15/1918:35
04/16/1919:04
2037-26-5
241
%
70-130
1
04/15/1918:35
04/16/1919:04
460-00-4
S5
102
%
70-132
1
04/15/1918:35
04/16/1919:04
17060-07-0
Analytical Method: ASTM D2974-87
11.2 % 0.10 1
REPORT OF LABORATORY ANALYSIS
04/11/19 18:15
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: BOTTOM
Lab ID: 92425107005
Collected: 04/11/19
11:00
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
10.9
1
04/22/19 08:58
04/23/19 22:13
N2
Aliphatic (C19-C36)
ND
mg/kg
10.9
1
04/22/19 08:58
04/23/19 22:13
N2
Aromatic (C11-C22)
ND
mg/kg
10.9
1
04/22/19 08:58
04/23/19 22:13
N2
Surrogates
Nonatriacontane (S)
41
%
40-140
1
04/22/19 08:58
04/23/19 22:13
7194-86-7
o-Terphenyl (S)
79
%
40-140
1
04/22/19 08:58
04/23/19 22:13
84-15-1
2-Fluorobiphenyl (S)
89
%
40-140
1
04/22/19 08:58
04/23/19 22:13
321-60-8
2-Bromonaphthalene (S)
92
%
40-140
1
04/22/19 08:58
04/23/19 22:13
580-13-2
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-008)
ND
mg/kg
2.4
1
04/11/19 17:38
04/12/19 01:20
N2
Aliphatic (C09-C12)
ND
mg/kg
2.4
1
04/11/19 17:38
04/12/19 01:20
N2
Aliphatic(C09-C12) Adjusted
ND
mg/kg
2.4
1
04/11/19 17:38
04/12/19 01:20
N2
Aromatic (C09-C10)
ND
mg/kg
2.4
1
04/11/19 17:38
04/12/19 01:20
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
101
%
70-130
1
04/11/19 17:38
04/12/19 01:20
460-00-4
4-Bromofluorobenzene (PID) (S)
100
%
70-130
1
04/11/19 17:38
04/12/19 01:20
460-00-4
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
83-32-9
Acenaphthylene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
208-96-8
Aniline
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
62-53-3
Anthracene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
120-12-7
Benzo(a)anthracene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
56-55-3
Benzo(a)pyrene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
207-08-9
Benzoic Acid
ND
ug/kg
1820
1
04/12/19 10:06
04/12/19 22:40
65-85-0
v1
Benzyl alcohol
ND
ug/kg
727
1
04/12/19 10:06
04/12/19 22:40
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
101-55-3
Butylbenzylphthalate
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
727
1
04/12/19 10:06
04/12/19 22:40
59-50-7
4-Chloroaniline
ND
ug/kg
1820
1
04/12/19 10:06
04/12/19 22:40
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
111-44-4
2-Chloronaphthalene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
91-58-7
2-Chlorophenol
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
7005-72-3
Chrysene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
53-70-3
Dibenzofuran
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1820
1
04/12/19 10:06
04/12/19 22:40
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: BOTTOM Lab ID: 92425107005 Collected: 04/11/19 11:00 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
120-83-2
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
84-66-2
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
105-67-9
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
131-11-3
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
84-74-2
ND
ug/kg
727
1
04/12/19 10:06
04/12/19 22:40
534-52-1
ND
ug/kg
1820
1
04/12/19 10:06
04/12/19 22:40
51-28-5
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
121-14-2
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
606-20-2
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
117-84-0
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
117-81-7
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
206-44-0
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
86-73-7
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
87-68-3
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
118-74-1
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
77-47-4
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
67-72-1
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
193-39-5
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
78-59-1
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
90-12-0
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
91-57-6
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
95-48-7
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
15831-10-4
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
91-20-3
ND
ug/kg
1820
1
04/12/19 10:06
04/12/19 22:40
88-74-4
ND
ug/kg
1820
1
04/12/19 10:06
04/12/19 22:40
99-09-2
ND
ug/kg
727
1
04/12/19 10:06
04/12/19 22:40
100-01-6
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
98-95-3
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
88-75-5
ND
ug/kg
1820
1
04/12/19 10:06
04/12/19 22:40
100-02-7
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
62-75-9
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
621-64-7
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
86-30-6
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
108-60-1
ND
ug/kg
1820
1
04/12/19 10:06
04/12/19 22:40
87-86-5
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
85-01-8
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
108-95-2
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
129-00-0
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
120-82-1
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
95-95-4
ND
ug/kg
364
1
04/12/19 10:06
04/12/19 22:40
88-06-2
58
%
23-110
1
04/12/19 10:06
04/12/19 22:40
4165-60-0
57
%
30-110
1
04/12/19 10:06
04/12/19 22:40
321-60-8
62
%
28-110
1
04/12/19 10:06
04/12/19 22:40
1718-51-0
61
%
22-110
1
04/12/19 10:06
04/12/19 22:40
13127-88-3
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: BOTTOM
Lab ID: 92425107005
Collected: 04/11/19
11:00
Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)
59
%
13-110
1
04/12/19 10:06
04/12/19 22:40
367-12-4
2,4,6-Tribromophenol (S)
75
%
27-110
1
04/12/19 10:06
04/12/19 22:40
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D
Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
102
1
04/15/19 18:35
04/16/19 15:22
67-64-1
L2
Benzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
71-43-2
L2
Bromobenzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
108-86-1
L2
Bromochloromethane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
74-97-5
L2
Bromodichloromethane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
75-27-4
L2
Bromoform
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
75-25-2
L2
Bromomethane
ND
ug/kg
10.2
1
04/15/19 18:35
04/16/19 15:22
74-83-9
L2
2-Butanone (MEK)
ND
ug/kg
102
1
04/15/19 18:35
04/16/19 15:22
78-93-3
L2
n-Butylbenzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
104-51-8
L2
sec-Butylbenzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
135-98-8
L2
tert-Butyl benzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
98-06-6
L2
Carbon tetrachloride
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
56-23-5
L2
Chlorobenzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
108-90-7
L2
Chloroethane
ND
ug/kg
10.2
1
04/15/19 18:35
04/16/19 15:22
75-00-3
L2,v1
Chloroform
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
67-66-3
L2
Chloromethane
ND
ug/kg
10.2
1
04/15/19 18:35
04/16/19 15:22
74-87-3
L2
2-Chlorotoluene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
95-49-8
L2
4-Chlorotoluene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
106-43-4
L2
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
96-12-8
L2
Dibromochloromethane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
124-48-1
L2
1,2-Dibromoethane (EDB)
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
106-93-4
L2
Dibromomethane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
74-95-3
L2
1,2-Dichlorobenzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
95-50-1
L2
1,3-Dichlorobenzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
541-73-1
L2
1,4-Dichlorobenzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
106-46-7
L2
Dichlorodifluoromethane
ND
ug/kg
10.2
1
04/15/19 18:35
04/16/19 15:22
75-71-8
L2
1,1-Dichloroethane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
75-34-3
L2
1,2-Dichloroethane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
107-06-2
L2
1,1-Dichloroethene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
75-35-4
L2
cis-1,2-Dichloroethene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
156-59-2
L2
trans-1,2-Dichloroethene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
156-60-5
L2
1,2-Dichloropropane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
78-87-5
L2
1,3-Dichloropropane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
142-28-9
L2
2,2-Dichloropropane
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
594-20-7
L2
1,1-Dichloropropene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
563-58-6
L2
cis-1,3-Dichloropropene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
10061-01-5
L2
trans- 1,3-Dichloropropene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
10061-02-6
L2
Diisopropyl ether
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
108-20-3
L2
Ethylbenzene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
100-41-4
L2
Hexachloro-1,3-butadiene
ND
ug/kg
5.1
1
04/15/19 18:35
04/16/19 15:22
87-68-3
L2
2-Hexanone
ND
ug/kg
51.0
1
04/15/19 18:35
04/16/19 15:22
591-78-6
L2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
Sample: BOTTOM Lab ID: 92425107005 Collected: 04/11/19 11:00 Received: 04/11/19 13:58 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
98-82-8
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
99-87-6
L2
ND
ug/kg
20.4
1
04/15/1918:35
04/16/1915:22
75-09-2
L2
ND
ug/kg
51.0
1
04/15/1918:35
04/16/1915:22
108-10-1
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
1634-04-4
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
91-20-3
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
103-65-1
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
100-42-5
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
630-20-6
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
79-34-5
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
127-18-4
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
108-88-3
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
87-61-6
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
120-82-1
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
71-55-6
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
79-00-5
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
79-01-6
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
75-69-4
L2,v1
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
96-18-4
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
95-63-6
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
108-67-8
L2
ND
ug/kg
51.0
1
04/15/1918:35
04/16/1915:22
108-05-4
L2
ND
ug/kg
10.2
1
04/15/1918:35
04/16/1915:22
75-01-4
L2
ND
ug/kg
10.2
1
04/15/1918:35
04/16/1915:22
1330-20-7
LS
ND
ug/kg
10.2
1
04/15/1918:35
04/16/1915:22
179601-23-1
L2
ND
ug/kg
5.1
1
04/15/1918:35
04/16/1915:22
95-47-6
L2
103
%
70-130
1
04/15/1918:35
04/16/1915:22
2037-26-5
97
%
70-130
1
04/15/1918:35
04/16/1915:22
460-00-4
96
%
70-132
1
04/15/1918:35
04/16/1915:22
17060-07-0
Analytical Method: ASTM D2974-87
8.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
04/11/19 18:15
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
QC Batch: 468890 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Associated Lab Samples: 92425107001, 92425107002, 92425107003, 92425107004, 92425107005
METHOD BLANK: 2546694
Matrix:
Solid
Associated Lab Samples: 92425107001, 92425107002,
92425107003, 92425107004, 92425107005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-008)
mg/kg
ND
2.5
04/11/19 19:26 N2
Aliphatic (C09-C12)
mg/kg
ND
2.5
04/11/19 19:26 N2
Aromatic (C09-C10)
mg/kg
ND
2.5
04/11/19 19:26 N2
4-Bromofluorobenzene (FID) (S)
%
93
70-130
04/11/19 19:26
4-Bromofluorobenzene (PID) (S)
%
92
70-130
04/11/19 19:26
LABORATORY CONTROL SAMPLE & LCSD:
2546695
2546696
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
14.9
15.7 15.9
105
107
70-130 1 25 N2
Aliphatic (C09-C12)
mg/kg
14.9
14.3 14.6
96
98
30-130 2 25 N2
Aromatic (C09-C10)
mg/kg
5
4.7 4.8
94
97
70-130 3 25 N2
4-Bromofluorobenzene (FID) (S)
%
92
98
70-130
4-Bromofluorobenzene (PID) (S)
%
91
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC.
Page 30 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
QC Batch: 469508 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92425107001, 92425107002, 92425107003, 92425107004, 92425107005
METHOD BLANK: 2549748
Matrix:
Solid
Associated Lab Samples: 92425107001,
92425107002, 92425107003, 92425107004, 92425107005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
04/16/19 11:40
1,1,1-Trichloroethane
ug/kg
ND
5.0
04/16/19 11:40
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
04/16/19 11:40
1,1,2-Trichloroethane
ug/kg
ND
5.0
04/16/19 11:40
1,1-Dichloroethane
ug/kg
ND
5.0
04/16/19 11:40
1,1-Dichloroethene
ug/kg
ND
5.0
04/16/19 11:40
1,1-Dichloropropene
ug/kg
ND
5.0
04/16/19 11:40
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
04/16/19 11:40
1,2,3-Trichloropropane
ug/kg
ND
5.0
04/16/19 11:40
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
04/16/19 11:40
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
04/16/19 11:40
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
04/16/19 11:40
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
04/16/19 11:40
1,2-Dichlorobenzene
ug/kg
ND
5.0
04/16/19 11:40
1,2-Dichloroethane
ug/kg
ND
5.0
04/16/19 11:40
1,2-Dichloropropane
ug/kg
ND
5.0
04/16/19 11:40
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
04/16/19 11:40
1,3-Dichlorobenzene
ug/kg
ND
5.0
04/16/19 11:40
1,3-Dichloropropane
ug/kg
ND
5.0
04/16/19 11:40
1,4-Dichlorobenzene
ug/kg
ND
5.0
04/16/19 11:40
2,2-Dichloropropane
ug/kg
ND
5.0
04/16/19 11:40
2-Butanone (MEK)
ug/kg
ND
100
04/16/19 11:40
2-Chlorotoluene
ug/kg
ND
5.0
04/16/19 11:40
2-Hexanone
ug/kg
ND
50.0
04/16/19 11:40
4-Chlorotoluene
ug/kg
ND
5.0
04/16/19 11:40
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
04/16/19 11:40
Acetone
ug/kg
ND
100
04/16/19 11:40
Benzene
ug/kg
ND
5.0
04/16/19 11:40
Bromobenzene
ug/kg
ND
5.0
04/16/19 11:40
Bromochloromethane
ug/kg
ND
5.0
04/16/19 11:40
Bromodichloromethane
ug/kg
ND
5.0
04/16/19 11:40
Bromoform
ug/kg
ND
5.0
04/16/19 11:40
Bromomethane
ug/kg
ND
10.0
04/16/19 11:40
Carbon tetrachloride
ug/kg
ND
5.0
04/16/19 11:40
Chlorobenzene
ug/kg
ND
5.0
04/16/19 11:40
Chloroethane
ug/kg
ND
10.0
04/16/19 11:40 v1
Chloroform
ug/kg
ND
5.0
04/16/19 11:40
Chloromethane
ug/kg
ND
10.0
04/16/19 11:40
cis-1,2-Dichloroethene
ug/kg
ND
5.0
04/16/19 11:40
cis-1,3-Dichloropropene
ug/kg
ND
5.0
04/16/19 11:40
Dibromochloromethane
ug/kg
ND
5.0
04/16/19 11:40
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
METHOD BLANK: 2549748 Matrix: Solid
Associated Lab Samples: 92425107001, 92425107002, 92425107003, 92425107004, 92425107005
Blank Reporting
Parameter Units Result Limit Analyzed
Dibromomethane
ug/kg
ND
5.0
04/16/19 11:40
Dichlorodifluoromethane
ug/kg
ND
10.0
04/16/19 11:40
Diisopropyl ether
ug/kg
ND
5.0
04/16/19 11:40
Ethylbenzene
ug/kg
ND
5.0
04/16/19 11:40
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
04/16/19 11:40
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
04/16/19 11:40
m&p-Xylene
ug/kg
ND
10.0
04/16/19 11:40
Methyl-tert-butyl ether
ug/kg
ND
5.0
04/16/19 11:40
Methylene Chloride
ug/kg
ND
20.0
04/16/19 11:40
n-Butylbenzene
ug/kg
ND
5.0
04/16/19 11:40
n-Propylbenzene
ug/kg
ND
5.0
04/16/19 11:40
Naphthalene
ug/kg
ND
5.0
04/16/19 11:40
o-Xylene
ug/kg
ND
5.0
04/16/19 11:40
p-Isopropyltoluene
ug/kg
ND
5.0
04/16/19 11:40
sec-Butylbenzene
ug/kg
ND
5.0
04/16/19 11:40
Styrene
ug/kg
ND
5.0
04/16/19 11:40
tert-Butyl benzene
ug/kg
ND
5.0
04/16/19 11:40
Tetrachloroethene
ug/kg
ND
5.0
04/16/19 11:40
Toluene
ug/kg
ND
5.0
04/16/19 11:40
trans-1,2-Dichloroethene
ug/kg
ND
5.0
04/16/19 11:40
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
04/16/19 11:40
Trichloroethene
ug/kg
ND
5.0
04/16/19 11:40
Trichlorofluoromethane
ug/kg
ND
5.0
04/16/19 11:40
Vinyl acetate
ug/kg
ND
50.0
04/16/19 11:40
Vinyl chloride
ug/kg
ND
10.0
04/16/19 11:40
Xylene (Total)
ug/kg
ND
10.0
04/16/19 11:40
1,2-Dichloroethane-d4 (S)
%
98
70-132
04/16/19 11:40
4-Bromofluorobenzene (S)
%
100
70-130
04/16/19 11:40
Toluene-d8 (S)
%
104
70-130
04/16/19 11:40
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
2549749
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
53.3
107
70-130
1,1,1-Trichloroethane
ug/kg
50
49.9
100
70-130
1,1,2,2-Tetrachloroethane
ug/kg
50
46.6
93
55-130
1,1,2-Trichloroethane
ug/kg
50
49.3
99
70-130
1,1-Dichloroethane
ug/kg
50
49.4
99
68-130
1,1-Dichloroethene
ug/kg
50
50.2
100
70-130
1,1-Dichloropropene
ug/kg
50
48.3
97
70-130
1,2,3-Trichlorobenzene
ug/kg
50
56.1
112
70-130
1,2,3-Trichloropropane
ug/kg
50
50.9
102
70-130
1,2,4-Trichlorobenzene
ug/kg
50
54.8
110
70-130
1,2,4-Trimethylbenzene
ug/kg
50
47.8
96
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
LABORATORY CONTROL SAMPLE:
Parameter
2549749
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2-Dibromo-3-chloropropane
ug/kg
50
51.8
104
57-141
1,2-Dibromoethane (EDB)
ug/kg
50
49.6
99
70-130
1,2-Dichlorobenzene
ug/kg
50
46.8
94
70-130
1,2-Dichloroethane
ug/kg
50
47.3
95
70-130
1,2-Dichloropropane
ug/kg
50
48.0
96
70-130
1,3,5-Trimethylbenzene
ug/kg
50
47.6
95
70-130
1,3-Dichlorobenzene
ug/kg
50
47.0
94
70-130
1,3-Dichloropropane
ug/kg
50
50.0
100
70-130
1,4-Dichlorobenzene
ug/kg
50
46.1
92
70-130
2,2-Dichloropropane
ug/kg
50
51.0
102
70-130
2-Butanone (MEK)
ug/kg
100
103
103
60-130
2-Chlorotoluene
ug/kg
50
52.4
105
70-130
2-Hexanone
ug/kg
100
106
106
70-132
4-Chlorotoluene
ug/kg
50
48.3
97
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
100
106
106
69-130
Acetone
ug/kg
100
96AJ
96
49-148
Benzene
ug/kg
50
50.2
100
70-130
Bromobenzene
ug/kg
50
48.2
96
70-130
Bromochloromethane
ug/kg
50
49.7
99
70-130
Bromodichloromethane
ug/kg
50
48.6
97
70-130
Bromoform
ug/kg
50
51.1
102
68-136
Bromomethane
ug/kg
50
51.5
103
60-140
Carbon tetrachloride
ug/kg
50
55.5
111
70-130
Chlorobenzene
ug/kg
50
48.2
96
70-130
Chloroethane
ug/kg
50
56.4
113
51-147 v1
Chloroform
ug/kg
50
50.1
100
70-130
Chloromethane
ug/kg
50
54.8
110
48-130
cis-1,2-Dichloroethene
ug/kg
50
49.5
99
70-130
cis-1,3-Dichloropropene
ug/kg
50
50.2
100
70-130
Dibromochloromethane
ug/kg
50
51.3
103
70-130
Dibromomethane
ug/kg
50
47.7
95
70-130
Dichlorodifluoromethane
ug/kg
50
51.7
103
49-130
Diisopropyl ether
ug/kg
50
53.3
107
66-130
Ethylbenzene
ug/kg
50
49.6
99
70-130
Hexachloro-1,3-butadiene
ug/kg
50
47.4
95
70-130
Isopropylbenzene (Cumene)
ug/kg
50
48.9
98
70-130
m&p-Xylene
ug/kg
100
98.3
98
70-130
Methyl-tert-butyl ether
ug/kg
50
50.0
100
70-130
Methylene Chloride
ug/kg
50
47.3
95
50-137
n-Butylbenzene
ug/kg
50
47.0
94
70-130
n-Propylbenzene
ug/kg
50
50.2
100
70-130
Naphthalene
ug/kg
50
48.2
96
70-131
o-Xylene
ug/kg
50
48.6
97
70-130
p-Isopropyltoluene
ug/kg
50
48.1
96
70-130
sec-Butylbenzene
ug/kg
50
49.1
98
70-130
Styrene
ug/kg
50
47.2
94
70-130
tert-Butyl benzene
ug/kg
50
43.0
86
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
LABORATORY CONTROL SAMPLE:
Parameter
2549749
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Tetrachloroethene
ug/kg
50
48.2
96
56-130
Toluene
ug/kg
50
48.0
96
70-130
trans-1,2-Dichloroethene
ug/kg
50
48.8
98
70-130
trans- 1,3-Dichloropropene
ug/kg
50
49.7
99
70-130
Trichloroethene
ug/kg
50
48.0
96
70-141
Trichlorofluoromethane
ug/kg
50
57.6
115
67-130 v1
Vinyl acetate
ug/kg
100
104
104
10-136
Vinyl chloride
ug/kg
50
57.2
114
67-130
Xylene (Total)
ug/kg
150
147
98
70-130
1,2-Dichloroethane-d4 (S)
%
99
70-132
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2550248
MS
92424121006 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2550249
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/kg
ND
1720
1720
1460
1380
85
80
52-133
6
1,1,1-Trichloroethane
ug/kg
ND
1720
1720
1440
1370
84
80
49-137
4
1,1,2,2-Tetrachloroethane
ug/kg
ND
1720
1720
1170
1200
68
70
39-150
3
1,1,2-Trichloroethane
ug/kg
ND
1720
1720
1300
1300
76
76
48-140
0
1,1-Dichloroethane
ug/kg
ND
1720
1720
1430
1420
83
83
46-135
0
1,1-Dichloroethene
ug/kg
ND
1720
1720
1080
1030
63
60
38-149
5
1,1-Dichloropropene
ug/kg
ND
1720
1720
1320
1300
77
76
41-140
2
1,2,3-Trichlorobenzene
ug/kg
ND
1720
1720
1220
1230
71
72
10-158
1
1,2,3-Trichloropropane
ug/kg
ND
1720
1720
1200
1290
70
75
33-157
7
1,2,4-Trichlorobenzene
ug/kg
ND
1720
1720
1200
1260
70
74
10-155
5
1,2,4-Trimethylbenzene
ug/kg
ND
1720
1720
1370
1380
80
81
24-154
1
1,2-Dibromo-3-chloropropane
ug/kg
ND
1720
1720
1110
1020
64
60
33-158
8
1,2-Dibromoethane (EDB)
ug/kg
ND
1720
1720
1300
1300
76
76
40-136
0
1,2-Dichlorobenzene
ug/kg
ND
1720
1720
1350
1380
79
81
27-146
2
1,2-Dichloroethane
ug/kg
ND
1720
1720
1300
1320
76
77
49-140
1
1,2-Dichloropropane
ug/kg
ND
1720
1720
1430
1440
83
84
44-143
1
1,3,5-Trimethylbenzene
ug/kg
ND
1720
1720
1360
1370
79
80
40-144
1
1,3-Dichlorobenzene
ug/kg
ND
1720
1720
1340
1350
78
79
33-140
1
1,3-Dichloropropane
ug/kg
ND
1720
1720
1360
1330
79
78
47-147
2
1,4-Dichlorobenzene
ug/kg
ND
1720
1720
1300
1330
76
78
35-139
2
2,2-Dichloropropane
ug/kg
ND
1720
1720
1400
1370
82
80
41-140
2
2-Butanone (MEK)
ug/kg
ND
3440
3440
2360J
2220J
69
65
10-181
2-Chlorotoluene
ug/kg
ND
1720
1720
1380
1530
80
89
38-147
11
2-Hexanone
ug/kg
ND
3440
3440
2190J
1950J
64
57
18-169
4-Chlorotoluene
ug/kg
ND
1720
1720
1370
1360
80
80
36-145
1
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
3440
3440
2300J
2340J
67
68
16-175
Acetone
ug/kg
ND
3440
3440
2050J
18001
60
53
10-200
Benzene
ug/kg
ND
1720
1720
1430
1440
84
84
46-136
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 49

rr
ace Analjd al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2550248
MS
92424121006 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2550249
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Bromobenzene
ug/kg
ND
1720
1720
1430
1420
84
83
38-149
1
Bromochloromethane
ug/kg
ND
1720
1720
1350
1400
79
81
44-142
3
Bromodichloromethane
ug/kg
ND
1720
1720
1370
1270
80
74
41-140
7
Bromoform
ug/kg
ND
1720
1720
1190
988
69
58
34-145
18
Bromomethane
ug/kg
ND
1720
1720
1240
1260
72
73
14-162
2
Carbon tetrachloride
ug/kg
ND
1720
1720
1320
1250
77
73
44-141
5
Chlorobenzene
ug/kg
ND
1720
1720
1400
1420
82
83
39-141
1
Chloroethane
ug/kg
ND
1720
1720
473J
635J
28
37
10-182
v1
Chloroform
ug/kg
ND
1720
1720
1370
1390
80
81
45-140
1
Chloromethane
ug/kg
ND
1720
1720
1600
1580
93
92
19-149
1
cis-1,2-Dichloroethene
ug/kg
ND
1720
1720
1440
1380
84
80
38-150
4
cis-1,3-Dichloropropene
ug/kg
ND
1720
1720
1370
1370
80
80
30-144
0
Dibromochloromethane
ug/kg
ND
1720
1720
1300
1170
76
68
36-145
10
Dibromomethane
ug/kg
ND
1720
1720
1250
1280
73
74
41-145
2
Dichlorodifluoromethane
ug/kg
ND
1720
1720
1460
921
85
54
16-146
45
Diisopropyl ether
ug/kg
ND
1720
1720
1450
1440
84
84
41-143
1
Ethylbenzene
ug/kg
ND
1720
1720
1440
1430
84
84
35-144
0
Hexachloro-1,3-butadiene
ug/kg
ND
1720
1720
1210
1240
71
72
10-160
2
Isopropylbenzene (Cumene)
ug/kg
ND
1720
1720
1390
1410
81
82
30-152
2
m&p-Xylene
ug/kg
ND
3440
3440
2800
2810
82
82
33-145
0
Methyl-tert-butyl ether
ug/kg
ND
1720
1720
1370
1320
80
77
49-140
4
Methylene Chloride
ug/kg
399J
1720
1720
1720
1570J
77
68
10-174
n-Butylbenzene
ug/kg
ND
1720
1720
1260
1300
73
76
10-160
3
n-Propylbenzene
ug/kg
ND
1720
1720
1390
1430
81
84
24-159
3
Naphthalene
ug/kg
ND
1720
1720
1110
1150
65
67
10-171
4
o-Xylene
ug/kg
ND
1720
1720
1410
1460
82
85
31-150
4
p-Isopropyltoluene
ug/kg
209J
1720
1720
1550
1590
78
80
21-154
3
sec-Butylbenzene
ug/kg
ND
1720
1720
1390
1380
81
81
19-159
0
Styrene
ug/kg
ND
1720
1720
1350
1370
79
80
15-152
1
tert-Butyl benzene
ug/kg
ND
1720
1720
1250
1280
73
74
31-141
2
Tetrachloroethene
ug/kg
ND
1720
1720
1340
1330
78
77
19-141
1
Toluene
ug/kg
ND
1720
1720
1420
1410
83
82
31-146
1
trans-1,2-Dichloroethene
ug/kg
ND
1720
1720
1390
1400
81
82
28-157
1
trans- 1,3-Dichloropropene
ug/kg
ND
1720
1720
1290
1240
75
72
25-146
4
Trichloroethene
ug/kg
ND
1720
1720
1440
1410
84
82
34-149
2
Trichlorofluoromethane
ug/kg
ND
1720
1720
812
900
47
52
10-167
10 v1
Vinyl acetate
ug/kg
ND
3440
3440
2330J
2230J
68
65
10-200
Vinyl chloride
ug/kg
ND
1720
1720
1640
1570
96
92
36-155
4
Xylene (Total)
ug/kg
ND
5150
5150
4210
4270
82
83
29-148
1
1,2-Dichloroethane-d4 (S)
%
91
91
70-132
4-Bromofluorobenzene (S)
%
98
99
70-130
Toluene-d8(S)
%
97
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
QC Batch: 469021 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Associated Lab Samples: 92425107001, 92425107002, 92425107003, 92425107004, 92425107005
METHOD BLANK: 2547285 Matrix: Solid
Associated Lab Samples: 92425107001, 92425107002, 92425107003, 92425107004, 92425107005
Blank Reporting
Parameter Units Result Limit Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
336
04/12/19 13:47
1,2-Dichlorobenzene
ug/kg
ND
336
04/12/19 13:47
1,3-Dichlorobenzene
ug/kg
ND
336
04/12/19 13:47
1,4-Dichlorobenzene
ug/kg
ND
336
04/12/19 13:47
1-Methylnaphthalene
ug/kg
ND
336
04/12/19 13:47
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
336
04/12/19 13:47
2,4,5-Trichlorophenol
ug/kg
ND
336
04/12/19 13:47
2,4,6-Trichlorophenol
ug/kg
ND
336
04/12/19 13:47
2,4-Dichlorophenol
ug/kg
ND
336
04/12/19 13:47
2,4-Dimethylphenol
ug/kg
ND
336
04/12/19 13:47
2,4-Dinitrophenol
ug/kg
ND
1680
04/12/19 13:47
2,4-Dinitrotoluene
ug/kg
ND
336
04/12/19 13:47
2,6-Dinitrotoluene
ug/kg
ND
336
04/12/19 13:47
2-Chloronaphthalene
ug/kg
ND
336
04/12/19 13:47
2-Chlorophenol
ug/kg
ND
336
04/12/19 13:47
2-Methylnaphthalene
ug/kg
ND
336
04/12/19 13:47
2-Methylphenol(o-Cresol)
ug/kg
ND
336
04/12/19 13:47
2-Nitroaniline
ug/kg
ND
1680
04/12/19 13:47
2-Nitrophenol
ug/kg
ND
336
04/12/19 13:47
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
336
04/12/19 13:47
3,3'-Dichlorobenzidine
ug/kg
ND
1680
04/12/19 13:47
3-Nitroaniline
ug/kg
ND
1680
04/12/19 13:47
4,6-Dinitro-2-methyl phenol
ug/kg
ND
671
04/12/19 13:47
4-Bromophenylphenyl ether
ug/kg
ND
336
04/12/19 13:47
4-ChIoro-3-methyl phenol
ug/kg
ND
671
04/12/19 13:47
4-Chloroaniline
ug/kg
ND
1680
04/12/19 13:47
4-Chlorophenylphenyl ether
ug/kg
ND
336
04/12/19 13:47
4-Nitroaniline
ug/kg
ND
671
04/12/19 13:47
4-Nitrophenol
ug/kg
ND
1680
04/12/19 13:47
Acenaphthene
ug/kg
ND
336
04/12/19 13:47
Acenaphthylene
ug/kg
ND
336
04/12/19 13:47
Aniline
ug/kg
ND
336
04/12/19 13:47
Anthracene
ug/kg
ND
336
04/12/19 13:47
Benzo(a)anthracene
ug/kg
ND
336
04/12/19 13:47
Benzo(a)pyrene
ug/kg
ND
336
04/12/19 13:47
Benzo(b)fluoranthene
ug/kg
ND
336
04/12/19 13:47
Benzo(g,h,i)perylene
ug/kg
ND
336
04/12/19 13:47
Benzo(k)fluoranthene
ug/kg
ND
336
04/12/19 13:47
Benzoic Acid
ug/kg
ND
1680
04/12/19 13:47
Benzyl alcohol
ug/kg
ND
671
04/12/19 13:47
bis(2-Chloroethoxy)methane
ug/kg
ND
336
04/12/19 13:47
v1
v1
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
METHOD BLANK: 2547285 Matrix: Solid
Associated Lab Samples: 92425107001, 92425107002, 92425107003, 92425107004, 92425107005
Blank Reporting
Parameter Units Result Limit Analyzed
bis(2-Chloroethyl) ether
ug/kg
ND
336
04/12/19 13:47
bis(2-Ethylhexyl)phthalate
ug/kg
ND
336
04/12/19 13:47
Butylbenzylphthalate
ug/kg
ND
336
04/12/19 13:47
Chrysene
ug/kg
ND
336
04/12/19 13:47
Di-n-butylphthalate
ug/kg
ND
336
04/12/19 13:47
Di-n-octylphthalate
ug/kg
ND
336
04/12/19 13:47
Dibenz(a,h)anthracene
ug/kg
ND
336
04/12/19 13:47
Dibenzofuran
ug/kg
ND
336
04/12/19 13:47
Diethylphthalate
ug/kg
ND
336
04/12/19 13:47
Dimethylphthalate
ug/kg
ND
336
04/12/19 13:47
Fluoranthene
ug/kg
ND
336
04/12/19 13:47
Fluorene
ug/kg
ND
336
04/12/19 13:47
Hexachloro-1,3-butadiene
ug/kg
ND
336
04/12/19 13:47
Hexachlorobenzene
ug/kg
ND
336
04/12/19 13:47
Hexachlorocyclopentadiene
ug/kg
ND
336
04/12/19 13:47
Hexachloroethane
ug/kg
ND
336
04/12/19 13:47
Indeno(1,2,3-cd)pyrene
ug/kg
ND
336
04/12/19 13:47
Isophorone
ug/kg
ND
336
04/12/19 13:47
N-Nitroso-di-n-propylamine
ug/kg
ND
336
04/12/19 13:47
N-Nitrosodimethylamine
ug/kg
ND
336
04/12/19 13:47
N-Nitrosodiphenylamine
ug/kg
ND
336
04/12/19 13:47
Naphthalene
ug/kg
ND
336
04/12/19 13:47
Nitrobenzene
ug/kg
ND
336
04/12/19 13:47
Pentachlorophenol
ug/kg
ND
1680
04/12/19 13:47
Phenanthrene
ug/kg
ND
336
04/12/19 13:47
Phenol
ug/kg
ND
336
04/12/19 13:47
Pyrene
ug/kg
ND
336
04/12/19 13:47
2,4,6-Tribromophenol (S)
%
87
27-110
04/12/19 13:47
2-Fluorobiphenyl (S)
%
74
30-110
04/12/19 13:47
2-Fluorophenol (S)
%
74
13-110
04/12/19 13:47
Nitrobenzene-d5 (S)
%
73
23-110
04/12/19 13:47
Phenol-d6 (S)
%
76
22-110
04/12/19 13:47
Terphenyl-d14 (S)
%
83
28-110
04/12/19 13:47
v1
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
2547286
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1660
1150
70
52-130
1,2-Dichlorobenzene
ug/kg
1660
1290
78
51-130
1,3-Dichlorobenzene
ug/kg
1660
1250
76
50-130
1,4-Dichlorobenzene
ug/kg
1660
1300
79
49-130
1-Methylnaphthalene
ug/kg
1660
1390
84
55-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1660
1300
79
30-130
2,4,5-Trichlorophenol
ug/kg
1660
1270
77
55-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
LABORATORY CONTROL SAMPLE:
Parameter
2547286
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4,6-TrichIorophenol
ug/kg
1660
1280
77
57-130
2,4-DichIorophenol
ug/kg
1660
1280
77
56-130
2,4-Dimethylphenol
ug/kg
1660
1270
77
51-130
2,4-Dinitrophenol
ug/kg
8280
6380
77
27-133
2,4-Dinitrotoluene
ug/kg
1660
1340
81
61-130
2,6-Dinitrotoluene
ug/kg
1660
1370
83
60-130
2-Chloronaphthalene
ug/kg
1660
1240
75
52-130
2-Chlorophenol
ug/kg
1660
1280
78
54-130
2-Methylnaphthalene
ug/kg
1660
1400
84
54-130
2-Methylphenol(o-Cresol)
ug/kg
1660
1400
85
51-130 v1
2-Nitroaniline
ug/kg
3310
2610
79
51-130
2-Nitrophenol
ug/kg
1660
1240
75
49-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1660
1350
81
11-163
3,3'-Dichlorobenzidine
ug/kg
3310
2570
78
10-132
3-Nitroaniline
ug/kg
3310
2620
79
55-130
4,6-Dinitro-2-methyl phenol
ug/kg
3310
2950
89
47-142
4-Bromophenylphenyl ether
ug/kg
1660
1350
82
59-130
4-Chloro-3-methylphenol
ug/kg
3310
2670
81
55-130
4-Chloroaniline
ug/kg
3310
2590
78
54-130
4-Chlorophenylphenyl ether
ug/kg
1660
1320
80
58-130
4-Nitroaniline
ug/kg
3310
2760
83
54-130 v1
4-Nitrophenol
ug/kg
8280
6610
80
48-130
Acenaphthene
ug/kg
1660
1470
89
60-130
Acenaphthylene
ug/kg
1660
1580
95
60-130
Aniline
ug/kg
1660
1130
68
43-130
Anthracene
ug/kg
1660
1440
87
63-130
Benzo(a)anthracene
ug/kg
1660
1510
91
59-130
Benzo(a)pyrene
ug/kg
1660
1470
89
57-130
Benzo(b)fluoranthene
ug/kg
1660
1430
87
54-130
Benzo(g,h,i)perylene
ug/kg
1660
1540
93
59-130
Benzo(k)fluoranthene
ug/kg
1660
1480
90
54-130
Benzoic Acid
ug/kg
8280
5520
67
19-130 v1
Benzyl alcohol
ug/kg
3310
2800
84
50-130
bis(2-Chloroethoxy)methane
ug/kg
1660
1220
74
54-130
bis(2-Chloroethyl) ether
ug/kg
1660
1230
74
48-130
bis(2-Ethylhexyl)phthalate
ug/kg
1660
1450
88
45-134
Butylbenzylphthalate
ug/kg
1660
1440
87
46-138
Chrysene
ug/kg
1660
1490
90
58-130
Di-n-butylphthalate
ug/kg
1660
1420
86
60-130
Di-n-octylphthalate
ug/kg
1660
1560
94
53-130 v1
Dibenz(a,h)anthracene
ug/kg
1660
1560
94
59-130
Dibenzofuran
ug/kg
1660
1300
78
60-130
Diethylphthalate
ug/kg
1660
1340
81
60-130
Dimethylphthalate
ug/kg
1660
1370
83
60-130
Fluoranthene
ug/kg
1660
1580
95
65-130
Fluorene
ug/kg
1660
1460
88
63-130
Hexachloro-1,3-butadiene
ug/kg
1660
1140
69
46-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 49

Pace Analytical Services, LLC
yical 9800 Kincey Ave. Suite 100
aceAnalJV� Huntersville, NC 28078
www.r a;awo-� UM." [phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
LABORATORY CONTROL SAMPLE:
Parameter
2547286
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachlorobenzene
ug/kg
1660
1330
80
58-130
Hexachlorocyclopentadiene
ug/kg
1660
1190
72
23-130
Hexachloroethane
ug/kg
1660
1190
72
47-130
Indeno(1,2,3-cd)pyrene
ug/kg
1660
1550
94
60-130
Isophorone
ug/kg
1660
1260
76
49-130
N-Nitroso-di-n-propylamine
ug/kg
1660
1230
74
47-130
N-Nitrosodimethylamine
ug/kg
1660
1240
75
45-130
N-Nitrosodiphenylamine
ug/kg
1660
1370
83
59-130
Naphthalene
ug/kg
1660
1430
86
55-130
Nitrobenzene
ug/kg
1660
1190
72
49-130
Pentachlorophenol
ug/kg
3310
2280
69
10-132
Phenanthrene
ug/kg
1660
1540
93
62-130
Phenol
ug/kg
1660
1430
86
46-130 v1
Pyrene
ug/kg
1660
1470
89
53-130
2,4,6-Tribromophenol (S)
%
90
27-110
2-Fluorobiphenyl (S)
%
76
30-110
2-Fluorophenol(S)
%
80
13-110
Nitrobenzene-d5 (S)
%
75
23-110
Phenol-d6 (S)
%
84
22-110
Terphenyl-d14 (S)
%
77
28-110
MATRIX SPIKE SAMPLE:
Parameter
2547287
Units
92425098001 Spike
Result Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1920
1140
59
18-130
1,2-Dichlorobenzene
ug/kg
1920
1280
67
14-130
1,3-Dichlorobenzene
ug/kg
1920
1230
64
12-130
1,4-Dichlorobenzene
ug/kg
1920
1310
68
10-130
1-Methylnaphthalene
ug/kg
ND 1920
1330
69
12-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1920
1310
69
10-130
2,4,5-Trichlorophenol
ug/kg
1920
1220
64
13-130
2,4,6-Trichlorophenol
ug/kg
1920
1250
65
17-130
2,4-Dichlorophenol
ug/kg
1920
1250
65
10-130
2,4-Dimethylphenol
ug/kg
1920
1210
63
10-130
2,4-Dinitrophenol
ug/kg
9590
4940
52
10-130
2,4-Dinitrotoluene
ug/kg
1920
1260
66
24-130
2,6-Dinitrotoluene
ug/kg
1920
1300
68
23-130
2-Chloronaphthalene
ug/kg
1920
1210
63
19-130
2-Chlorophenol
ug/kg
1920
1290
67
10-130
2-Methylnaphthalene
ug/kg
ND 1920
1340
70
18-130
2-Methylphenol(o-Cresol)
ug/kg
1920
1380
72
10-130 v1
2-Nitroaniline
ug/kg
3830
2540
66
17-130
2-Nitrophenol
ug/kg
1920
1240
65
10-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1920
1290
67
10-130
3,3'-Dichlorobenzidine
ug/kg
3830
2390
62
10-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC.
Page 39 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
MATRIX SPIKE SAMPLE:
2547287
92425098001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
3-Nitroaniline
ug/kg
3830
2620
68
24-130
4,6-Dinitro-2-methyl phenol
ug/kg
3830
2810
73
10-152
4-Bromophenylphenyl ether
ug/kg
1920
1190
62
29-130
4-Chloro-3-methylphenol
ug/kg
3830
2580
67
17-130
4-Chloroaniline
ug/kg
3830
2610
68
14-130
4-Chlorophenylphenyl ether
ug/kg
1920
1170
61
25-130
4-Nitroaniline
ug/kg
3830
2670
70
22-130 v1
4-Nitrophenol
ug/kg
9590
6250
65
10-130
Acenaphthene
ug/kg
ND
1920
1350
71
20-130
Acenaphthylene
ug/kg
ND
1920
1470
77
25-130
Aniline
ug/kg
1920
1130
59
10-130
Anthracene
ug/kg
ND
1920
1400
73
29-130
Benzo(a)anthracene
ug/kg
ND
1920
1350
71
19-130
Benzo(a)pyrene
ug/kg
ND
1920
1330
69
12-130
Benzo(b)fluoranthene
ug/kg
ND
1920
1330
69
14-130
Benzo(g,h,i)perylene
ug/kg
ND
1920
1380
72
10-130
Benzo(k)fluoranthene
ug/kg
ND
1920
1340
70
14-130
Benzoic Acid
ug/kg
9590
2250
24
10-130 v1
Benzyl alcohol
ug/kg
3830
2640
69
13-130
bis(2-Chloroethoxy)methane
ug/kg
1920
1210
63
16-130
bis(2-Chloroethyl) ether
ug/kg
1920
1240
65
11-130
bis(2-Ethylhexyl)phthalate
ug/kg
1920
1260
66
21-130
Butylbenzylphthalate
ug/kg
1920
1260
66
23-130
Chrysene
ug/kg
ND
1920
1330
69
22-130
Di-n-butylphthalate
ug/kg
1920
1270
66
30-130
Di-n-octylphthalate
ug/kg
1920
1310
69
23-142 v1
Dibenz(a,h)anthracene
ug/kg
ND
1920
1400
73
10-130
Dibenzofuran
ug/kg
1920
1220
64
24-130
Diethylphthalate
ug/kg
1920
1260
66
26-130
Dimethylphthalate
ug/kg
1920
1300
68
22-130
Fluoranthene
ug/kg
ND
1920
1410
73
33-130
Fluorene
ug/kg
ND
1920
1320
69
22-130
Hexachloro-1,3-butadiene
ug/kg
1920
1090
57
13-130
Hexachlorobenzene
ug/kg
1920
1260
66
29-130
Hexachlorocyclopentadiene
ug/kg
1920
1120
58
10-130
Hexachloroethane
ug/kg
1920
1200
62
10-130
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1920
1400
73
10-130
Isophorone
ug/kg
1920
1230
64
13-130
N-Nitroso-di-n-propylamine
ug/kg
1920
1230
64
12-130
N-Nitrosodimethylamine
ug/kg
1920
1210
63
11-130
N-Nitrosodiphenylamine
ug/kg
1920
1290
67
15-130
Naphthalene
ug/kg
ND
1920
1370
72
15-130
Nitrobenzene
ug/kg
1920
1190
62
12-130
Pentachlorophenol
ug/kg
3830
2250
59
10-130
Phenanthrene
ug/kg
ND
1920
1420
74
27-130
Phenol
ug/kg
1920
1370
72
10-130 v1
Pyrene
ug/kg
ND
1920
1350
70
19-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 49

rr
ace Analjd al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
MATRIX SPIKE SAMPLE:
2547287
92425098001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
2,4,6-Tribromophenol (S)
%
71
27-110
2-Fluorobiphenyl (S)
%
60
30-110
2-Fluorophenol(S)
%
66
13-110
Nitrobenzene-d5(S)
%
63
23-110
Phenol-d6 (S)
%
66
22-110
Terphenyl-d14 (S)
%
60
28-110
SAMPLE DUPLICATE: 2547288
Parameter
Units
92425098001
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/kg
ND
1,2-Dichlorobenzene
ug/kg
ND
1,3-Dichlorobenzene
ug/kg
ND
1,4-Dichlorobenzene
ug/kg
ND
1-Methylnaphthalene
ug/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
2,4,5-Trichlorophenol
ug/kg
ND
2,4,6-Trichlorophenol
ug/kg
ND
2,4-Dichlorophenol
ug/kg
ND
2,4-Dimethylphenol
ug/kg
ND
2,4-Dinitrophenol
ug/kg
ND
2,4-Dinitrotoluene
ug/kg
ND
2,6-Dinitrotoluene
ug/kg
ND
2-Chloronaphthalene
ug/kg
ND
2-Chlorophenol
ug/kg
ND
2-Methylnaphthalene
ug/kg
ND
ND
2-Methylphenol(o-Cresol)
ug/kg
ND
2-Nitroaniline
ug/kg
ND
2-Nitrophenol
ug/kg
ND
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
3,3'-Dichlorobenzidine
ug/kg
ND
3-Nitroaniline
ug/kg
ND
4,6-Din itro-2-methyl phenol
ug/kg
ND
4-Bromophenylphenyl ether
ug/kg
ND
4-ChIoro-3-methyl phenol
ug/kg
ND
4-Chloroaniline
ug/kg
ND
4-Chlorophenylphenyl ether
ug/kg
ND
4-Nitroaniline
ug/kg
ND
4-Nitrophenol
ug/kg
ND
Acenaphthene
ug/kg
ND
ND
Acenaphthylene
ug/kg
ND
ND
Aniline
ug/kg
ND
Anthracene
ug/kg
ND
ND
Benzo(a)anthracene
ug/kg
ND
ND
Benzo(a)pyrene
ug/kg
ND
ND
RPD Qualifiers
v1
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC.
Page 41 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
SAMPLE DUPLICATE: 2547288
Parameter
Units
92425098001
Result
Benzo(b)fluoranthene
ug/kg
ND
Benzo(g,h,i)perylene
ug/kg
ND
Benzo(k)fluoranthene
ug/kg
ND
Benzoic Acid
ug/kg
Benzyl alcohol
ug/kg
bis(2-Chloroethoxy)methane
ug/kg
bis(2-Chloroethyl) ether
ug/kg
bis(2-Ethylhexyl)phthalate
ug/kg
Butylbenzylphthalate
ug/kg
Chrysene
ug/kg
ND
Di-n-butylphthalate
ug/kg
Di-n-octylphthalate
ug/kg
Dibenz(a,h)anthracene
ug/kg
ND
Dibenzofuran
ug/kg
Diethylphthalate
ug/kg
Dimethylphthalate
ug/kg
Fluoranthene
ug/kg
ND
Fluorene
ug/kg
ND
Hexachloro-1,3-butadiene
ug/kg
Hexachlorobenzene
ug/kg
Hexachlorocyclopentadiene
ug/kg
Hexachloroethane
ug/kg
Indeno(1,2,3-cd)pyrene
ug/kg
ND
Isophorone
ug/kg
N-Nitroso-di-n-propylamine
ug/kg
N-Nitrosodimethylamine
ug/kg
N-Nitrosodiphenylamine
ug/kg
Naphthalene
ug/kg
ND
Nitrobenzene
ug/kg
Pentachlorophenol
ug/kg
Phenanthrene
ug/kg
ND
Phenol
ug/kg
Pyrene
ug/kg
ND
2,4,6-Tribromophenol (S)
%
50
2-Fluorobiphenyl (S)
%
43
2-Fluorophenol(S)
%
45
Nitrobenzene-d5 (S)
%
44
Phenol-d6 (S)
%
45
Terphenyl-d14 (S)
%
50
Dup
Result RPD Qualifiers
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
69
54
58
58
58
59
v1
v1
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC.
Page 42 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
QC Batch: 470727 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 92425107001, 92425107002, 92425107003, 92425107004, 92425107005
METHOD BLANK: 2555380
Matrix:
Solid
Associated Lab Samples:
92425107001, 92425107002,
92425107003, 92425107004, 92425107005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10.0
04/23/19 19:01 N2
Aliphatic (C19-C36)
mg/kg
ND
10.0
04/23/19 19:01 N2
Aromatic (C11-C22)
mg/kg
ND
10.0
04/23/19 19:01 N2
2-Bromonaphthalene (S)
%
83
40-140
04/23/19 19:01
2-Fluorobiphenyl (S)
%
80
40-140
04/23/19 19:01
Nonatriacontane (S)
%
41
40-140
04/23/19 19:01
o-Terphenyl (S)
%
70
40-140
04/23/19 19:01
LABORATORY CONTROL SAMPLE & LCSD:
2555381
2555382
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10
ND ND
51
46
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.3
ND ND
57
49
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.3
22.6 17.9
80
63
40-140 23 50 N2
2-Bromonaphthalene (S)
%
95
75
40-140
2-Fluorobiphenyl (S)
%
95
74
40-140
Nonatriacontane (S)
%
60
52
40-140
o-Terphenyl(S)
%
86
71
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC.
Page 43 of 49

rr
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
QC Batch: 468916 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92425107001, 92425107002, 92425107003, 92425107004, 92425107005
SAMPLE DUPLICATE: 2546867
92425077001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 30.9 30.8 0
SAMPLE DUPLICATE: 2546868
92425156006 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 3.8 3.7 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 934 W. MALLARD CREEK CH. RD
Pace Project No.: 92425107
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
LS Analyte recovery in the laboratory control sample (LCS) was outside QC limits for one or more of the constituent analytes
used in the calculated result.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
P2 Re -extraction or re -analysis could not be performed due to insufficient sample amount.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2019 11:36 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 49

t
ace Ar l tr' al
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
934 W. MALLARD CREEK CH. RD
92425107
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92425107001
WEST WALL
MADEP EPH
470727
MADEP EPH
471142
92425107002
SOUTH WALL
MADEP EPH
470727
MADEP EPH
471142
92425107003
NORTH WALL
MADEP EPH
470727
MADEP EPH
471142
92425107004
EAST WALL
MADEP EPH
470727
MADEP EPH
471142
92425107005
BOTTOM
MADEP EPH
470727
MADEP EPH
471142
92425107001
WEST WALL
MADEP VPH
468890
MADEP VPH
469430
92425107002
SOUTH WALL
MADEP VPH
468890
MADEP VPH
469430
92425107003
NORTH WALL
MADEP VPH
468890
MADEP VPH
469430
92425107004
EAST WALL
MADEP VPH
468890
MADEP VPH
469430
92425107005
BOTTOM
MADEP VPH
468890
MADEP VPH
469430
92425107001
WEST WALL
EPA 3546
469021
EPA 8270E
469087
92425107002
SOUTH WALL
EPA 3546
469021
EPA 8270E
469087
92425107003
NORTH WALL
EPA 3546
469021
EPA 8270E
469087
92425107004
EAST WALL
EPA 3546
469021
EPA 8270E
469087
92425107005
BOTTOM
EPA 3546
469021
EPA 8270E
469087
92425107001
WEST WALL
EPA 5035A
469508
EPA 8260D
469564
92425107002
SOUTH WALL
EPA 5035A
469508
EPA 8260D
469564
92425107003
NORTH WALL
EPA 5035A
469508
EPA 8260D
469564
92425107004
EAST WALL
EPA 5035A
469508
EPA 8260D
469564
92425107005
BOTTOM
EPA 5035A
469508
EPA 8260D
469564
92425107001
WEST WALL
ASTM D2974-87
468916
92425107002
SOUTH WALL
ASTM D2974-87
468916
92425107003
NORTH WALL
ASTM D2974-87
468916
92425107004
EAST WALL
ASTM D2974-87
468916
92425107005
BOTTOM
ASTM D2974-87
468916
Date: 05/02/2019 11:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 46 of 49

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Page 49 of 49

■
2ce Analyfiol
tirwrr.p�o$ab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
May 22, 2020
Mr. James Willard II
Inenco, Inc.
132 W. Statesville Ave
Mooresville, NC 28115
RE: Project: 934 W. MALLARD
Pace Project No.: 92477511
Dear Mr. II:
Enclosed are the analytical results for sample(s) received by the laboratory on May 13, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 35

■
2ce Analyfiml
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 934 W. MALLARD
Pace Project No.: 92477511
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 35

■
2ce Analyfiol
tirwrr.p�o$ab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 934 W. MALLARD
Pace Project No.: 92477511
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92477511001 NORTH WALL 2
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
BMB
6
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KDW
1
PASI-A
92477511002 EAST WALL 2
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
BMB
6
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KDW
1
PASI-A
92477511003 SOUTH WALL 2
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
BMB
6
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KDW
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: NORTH WALL 2 Lab ID: 92477511001 Collected: 05/08/20 09:30 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
MADEPV
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10),Unadjusted
Total VPH
Surrogates
2,5-Dibromotoluene (FID)
2,5-Dibromotoluene (PID)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
ND
mg/kg
11.6
1
05/14/2015:35
05/15/2012:40
ND
mg/kg
11.6
1
05/14/2015:35
05/15/2012:40
ND
mg/kg
11.6
1
05/14/2015:35
05/15/2012:40
64
%
40-140
1
05/14/2015:35
05/15/2012:40
7194-86-7
77
%
40-140
1
05/14/2015:35
05/15/2012:40
84-15-1
107
%
40-140
1
05/14/2015:35
05/15/2012:40
321-60-8
106
%
40-140
1
05/14/2015:35
05/15/2012:40
580-13-2
Analytical Method: MADEP VPH Preparation
Method:
MADEPV
Pace Analytical
Services - Charlotte
ND
mg/kg
5.62
1
05/08/20 09:30
05/19/20 18:29
ND
mg/kg
5.62
1
05/08/20 09:30
05/19/20 18:29
ND
mg/kg
5.62
1
05/08/20 09:30
05/19/20 18:29
ND
mg/kg
5.62
1
05/08/20 09:30
05/19/20 18:29
101
%
70-130
1
05/08/20 09:30
05/19/20 18:29
93.4
%
70-130
1
05/08/20 09:30
05/19/20 18:29
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
83-32-9
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
208-96-8
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
62-53-3
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
120-12-7
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
56-55-3
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
50-32-8
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
205-99-2
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
191-24-2
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
207-08-9
ND
ug/kg
1890
1
05/14/20 15:14
05/15/20 09:45
65-85-0
ND
ug/kg
756
1
05/14/20 15:14
05/15/20 09:45
100-51-6
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
101-55-3
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
85-68-7
ND
ug/kg
756
1
05/14/20 15:14
05/15/20 09:45
59-50-7
ND
ug/kg
756
1
05/14/20 15:14
05/15/20 09:45
106-47-8
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
111-91-1
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
111-44-4
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
91-58-7
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
95-57-8
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
7005-72-3
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
218-01-9
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
53-70-3
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
132-64-9
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
95-50-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: NORTH WALL 2
Lab ID: 92477511001 Collected:
05/08/20
09:30
Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
756
1
05/14/20 15:14
05/15/20 09:45
91-94-1
2,4-Dichlorophenol
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
120-83-2
Diethylphthalate
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
84-66-2
2,4-Dimethylphenol
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
105-67-9
Dimethylphthalate
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
131-11-3
Di-n-butylphthalate
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
756
1
05/14/20 15:14
05/15/20 09:45
534-52-1
v2,v3
2,4-Dinitrophenol
ND
ug/kg
1890
1
05/14/20 15:14
05/15/20 09:45
51-28-5
v2,v3
2,4-Dinitrotoluene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
606-20-2
Di-n-octylphthalate
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
117-81-7
Fluoranthene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
206-44-0
Fluorene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
87-68-3
Hexachlorobenzene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
77-47-4
v2,v3
Hexachloroethane
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
193-39-5
Isophorone
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
78-59-1
1-Methylnaphthalene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
90-12-0
2-Methylnaphthalene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
15831-10-4
Naphthalene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
91-20-3
2-Nitroaniline
ND
ug/kg
1890
1
05/14/20 15:14
05/15/20 09:45
88-74-4
3-Nitroaniline
ND
ug/kg
1890
1
05/14/20 15:14
05/15/20 09:45
99-09-2
4-Nitroaniline
ND
ug/kg
756
1
05/14/20 15:14
05/15/20 09:45
100-01-6
Nitrobenzene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
98-95-3
2-Nitrophenol
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
88-75-5
4-Nitrophenol
ND
ug/kg
1890
1
05/14/20 15:14
05/15/20 09:45
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
108-60-1
Pentachlorophenol
ND
ug/kg
756
1
05/14/20 15:14
05/15/20 09:45
87-86-5
v1
Phenanthrene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
85-01-8
Phenol
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
108-95-2
Pyrene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
129-00-0
Pyridine
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
378
1
05/14/20 15:14
05/15/20 09:45
88-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■■
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: NORTH WALL 2
Lab ID: 92477511001 Collected:
05/08/20
09:30
Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
58
%
23-110
1
05/14/20 15:14
05/15/20 09:45
4165-60-0
2-Fluorobiphenyl (S)
55
%
30-110
1
05/14/20 15:14
05/15/20 09:45
321-60-8
Terphenyl-d14 (S)
58
%
28-110
1
05/14/20 15:14
05/15/20 09:45
1718-51-0
Phenol-d6 (S)
60
%
22-110
1
05/14/20 15:14
05/15/20 09:45
13127-88-3
2-Fluorophenol (S)
59
%
13-110
1
05/14/20 15:14
05/15/20 09:45
367-12-4
2,4,6-Tribromophenol (S)
62
%
27-110
1
05/14/20 15:14
05/15/20 09:45
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation
Method: EPA 5035A
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
156
1
05/14/20 17:52
05/14/20 20:10
67-64-1
Benzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
71-43-2
Bromobenzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
108-86-1
Bromochloromethane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
74-97-5
Bromodichloromethane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
75-27-4
Bromoform
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
75-25-2
Bromomethane
ND
ug/kg
15.6
1
05/14/20 17:52
05/14/20 20:10
74-83-9 IH
2-Butanone (MEK)
ND
ug/kg
156
1
05/14/20 17:52
05/14/20 20:10
78-93-3
n-Butylbenzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
104-51-8
sec-Butylbenzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
135-98-8
tert-Butyl benzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
98-06-6
Carbon tetrachloride
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
56-23-5
Chlorobenzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
108-90-7
Chloroethane
ND
ug/kg
15.6
1
05/14/20 17:52
05/14/20 20:10
75-00-3
Chloroform
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
67-66-3
Chloromethane
ND
ug/kg
15.6
1
05/14/20 17:52
05/14/20 20:10
74-87-3
2-Chlorotoluene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
95-49-8
4-Chlorotoluene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
96-12-8
Dibromochloromethane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
106-93-4
Dibromomethane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.6
1
05/14/20 17:52
05/14/20 20:10
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
563-58-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■■
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: NORTH WALL 2 Lab ID: 92477511001 Collected: 05/08/20 09:30 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A Volatile Organics
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
10061-01-5
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
10061-02-6
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
108-20-3
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
100-41-4
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
87-68-3
ND
ug/kg
78.0
1
05/14/20 17:52
05/14/20 20:10
591-78-6
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
98-82-8
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
99-87-6
ND
ug/kg
31.2
1
05/14/20 17:52
05/14/20 20:10
75-09-2
ND
ug/kg
78.0
1
05/14/20 17:52
05/14/20 20:10
108-10-1
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
1634-04-4
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
91-20-3
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
103-65-1
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
100-42-5
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
630-20-6
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
79-34-5
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
127-18-4
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
108-88-3
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
87-61-6
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
120-82-1
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
71-55-6
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
79-00-5
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
79-01-6
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
75-69-4
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
96-18-4
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
95-63-6
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
108-67-8
ND
ug/kg
78.0
1
05/14/20 17:52
05/14/20 20:10
108-05-4 v1
ND
ug/kg
15.6
1
05/14/20 17:52
05/14/20 20:10
75-01-4
ND
ug/kg
15.6
1
05/14/20 17:52
05/14/20 20:10
1330-20-7
ND
ug/kg
15.6
1
05/14/20 17:52
05/14/20 20:10
179601-23-1
ND
ug/kg
7.8
1
05/14/20 17:52
05/14/20 20:10
95-47-6
102
%
70-130
1
05/14/20 17:52
05/14/20 20:10
2037-26-5
103
%
70-130
1
05/14/20 17:52
05/14/20 20:10
460-00-4
106
%
70-132
1
05/14/20 17:52
05/14/20 20:10
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 13.6 % 0.10 1 05/13/20 17:43
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace Analytical Services -Asheville
Total Solids 88.9 % 1 05/21/20 14:38 05/21/20 14:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: EAST WALL 2 Lab ID: 92477511002 Collected: 05/08/20 09:50 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
MADEPV
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10),Unadjusted
Total VPH
Surrogates
2,5-Dibromotoluene (FID)
2,5-Dibromotoluene (PID)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
ND
mg/kg
11.5
1
05/14/2015:35
05/15/2013:07
ND
mg/kg
11.5
1
05/14/2015:35
05/15/2013:07
ND
mg/kg
11.5
1
05/14/2015:35
05/15/2013:07
69
%
40-140
1
05/14/2015:35
05/15/2013:07
7194-86-7
81
%
40-140
1
05/14/2015:35
05/15/2013:07
84-15-1
110
%
40-140
1
05/14/2015:35
05/15/2013:07
321-60-8
109
%
40-140
1
05/14/2015:35
05/15/2013:07
580-13-2
Analytical Method: MADEP VPH Preparation
Method:
MADEPV
Pace Analytical
Services - Charlotte
ND
mg/kg
5.68
1
05/08/20 09:50
05/19/20 19:02
ND
mg/kg
5.68
1
05/08/20 09:50
05/19/20 19:02
ND
mg/kg
5.68
1
05/08/20 09:50
05/19/20 19:02
ND
mg/kg
5.68
1
05/08/20 09:50
05/19/20 19:02
99.7
%
70-130
1
05/08/20 09:50
05/19/20 19:02
92.6
%
70-130
1
05/08/20 09:50
05/19/20 19:02
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
83-32-9
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
208-96-8
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
62-53-3
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
120-12-7
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
56-55-3
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
50-32-8
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
205-99-2
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
191-24-2
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
207-08-9
ND
ug/kg
1850
1
05/14/2015:14
05/15/2010:39
65-85-0
ND
ug/kg
742
1
05/14/2015:14
05/15/2010:39
100-51-6
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
101-55-3
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
85-68-7
ND
ug/kg
742
1
05/14/2015:14
05/15/2010:39
59-50-7
ND
ug/kg
742
1
05/14/2015:14
05/15/2010:39
106-47-8
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
111-91-1
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
111-44-4
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
91-58-7
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
95-57-8
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
7005-72-3
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
218-01-9
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
53-70-3
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
132-64-9
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
95-50-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: EAST WALL 2
Lab ID: 92477511002 Collected:
05/08/20
09:50
Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
742
1
05/14/2015:14
05/15/2010:39
91-94-1
2,4-Dichlorophenol
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
120-83-2
Diethylphthalate
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
84-66-2
2,4-Dimethylphenol
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
105-67-9
Dimethylphthalate
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
131-11-3
Di-n-butylphthalate
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
742
1
05/14/2015:14
05/15/2010:39
534-52-1
v2
2,4-Dinitrophenol
ND
ug/kg
1850
1
05/14/2015:14
05/15/2010:39
51-28-5
v2
2,4-Dinitrotoluene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
606-20-2
Di-n-octylphthalate
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
117-81-7
Fluoranthene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
206-44-0
Fluorene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
87-68-3
Hexachlorobenzene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
77-47-4
v2
Hexachloroethane
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
193-39-5
Isophorone
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
78-59-1
1-Methylnaphthalene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
90-12-0
2-Methylnaphthalene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
371
1
05/14/20 15:14
05/15/20 10:39
15831-10-4
Naphthalene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
91-20-3
2-Nitroaniline
ND
ug/kg
1850
1
05/14/2015:14
05/15/2010:39
88-74-4
3-Nitroaniline
ND
ug/kg
1850
1
05/14/2015:14
05/15/2010:39
99-09-2
4-Nitroaniline
ND
ug/kg
742
1
05/14/2015:14
05/15/2010:39
100-01-6
Nitrobenzene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
98-95-3
2-Nitrophenol
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
88-75-5
4-Nitrophenol
ND
ug/kg
1850
1
05/14/2015:14
05/15/2010:39
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
108-60-1
Pentachlorophenol
ND
ug/kg
742
1
05/14/2015:14
05/15/2010:39
87-86-5
v1
Phenanthrene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
85-01-8
Phenol
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
108-95-2
Pyrene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
129-00-0
Pyridine
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
371
1
05/14/2015:14
05/15/2010:39
88-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: EAST WALL 2 Lab ID: 92477511002 Collected: 05/08/20 09:50 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
52
%
23-110
1
05/14/20 15:14
05/15/20 10:39
4165-60-0
2-Fluorobiphenyl (S)
51
%
30-110
1
05/14/20 15:14
05/15/20 10:39
321-60-8
Terphenyl-d14 (S)
60
%
28-110
1
05/14/20 15:14
05/15/20 10:39
1718-51-0
Phenol-d6 (S)
51
%
22-110
1
05/14/20 15:14
05/15/20 10:39
13127-88-3
2-Fluorophenol (S)
53
%
13-110
1
05/14/20 15:14
05/15/20 10:39
367-12-4
2,4,6-Tribromophenol (S)
53
%
27-110
1
05/14/20 15:14
05/15/20 10:39
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
87.0
1
05/14/20 17:52
05/14/20 20:35
67-64-1
Benzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
71-43-2
Bromobenzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
108-86-1
Bromochloromethane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
74-97-5
Bromodichloromethane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
75-27-4
Bromoform
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
75-25-2
Bromomethane
ND
ug/kg
8.7
1
05/14/20 17:52
05/14/20 20:35
74-83-9
2-Butanone (MEK)
ND
ug/kg
87.0
1
05/14/20 17:52
05/14/20 20:35
78-93-3
n-Butylbenzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
104-51-8
sec-Butylbenzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
135-98-8
tert-Butyl benzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
98-06-6
Carbon tetrachloride
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
56-23-5
Chlorobenzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
108-90-7
Chloroethane
ND
ug/kg
8.7
1
05/14/20 17:52
05/14/20 20:35
75-00-3
Chloroform
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
67-66-3
Chloromethane
ND
ug/kg
8.7
1
05/14/20 17:52
05/14/20 20:35
74-87-3
2-Chlorotoluene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
95-49-8
4-Chlorotoluene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
96-12-8
Dibromochloromethane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
106-93-4
Dibromomethane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
106-46-7
Dichlorodifluoromethane
ND
ug/kg
8.7
1
05/14/20 17:52
05/14/20 20:35
75-71-8
1,1-Dichloroethane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
75-34-3
1,2-Dichloroethane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
107-06-2
1,1-Dichloroethene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
156-60-5
1,2-Dichloropropane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
78-87-5
1,3-Dichloropropane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
142-28-9
2,2-Dichloropropane
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
594-20-7
1,1-Dichloropropene
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
563-58-6
REPORT OF LABORATORY ANALYSIS
IH
Qual
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: EAST WALL 2 Lab ID: 92477511002 Collected: 05/08/20 09:50 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A Volatile Organics
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
10061-01-5
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
10061-02-6
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
108-20-3
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
100-41-4
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
87-68-3
ND
ug/kg
43.5
1
05/14/20 17:52
05/14/20 20:35
591-78-6
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
98-82-8
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
99-87-6
ND
ug/kg
17.4
1
05/14/20 17:52
05/14/20 20:35
75-09-2
ND
ug/kg
43.5
1
05/14/20 17:52
05/14/20 20:35
108-10-1
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
1634-04-4
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
91-20-3
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
103-65-1
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
100-42-5
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
630-20-6
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
79-34-5
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
127-18-4
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
108-88-3
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
87-61-6
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
120-82-1
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
71-55-6
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
79-00-5
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
79-01-6
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
75-69-4
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
96-18-4
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
95-63-6
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
108-67-8
ND
ug/kg
43.5
1
05/14/20 17:52
05/14/20 20:35
108-05-4 v1
ND
ug/kg
8.7
1
05/14/20 17:52
05/14/20 20:35
75-01-4
ND
ug/kg
8.7
1
05/14/20 17:52
05/14/20 20:35
1330-20-7
ND
ug/kg
8.7
1
05/14/20 17:52
05/14/20 20:35
179601-23-1
ND
ug/kg
4.4
1
05/14/20 17:52
05/14/20 20:35
95-47-6
102
%
70-130
1
05/14/20 17:52
05/14/20 20:35
2037-26-5
101
%
70-130
1
05/14/20 17:52
05/14/20 20:35
460-00-4
106
%
70-132
1
05/14/20 17:52
05/14/20 20:35
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 11.6 % 0.10 1 05/13/20 17:43
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace Analytical Services -Asheville
Total Solids 88.0 % 1 05/21/20 14:38 05/21/20 14:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: SOUTH WALL 2 Lab ID: 92477511003 Collected: 05/08/20 10:00 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
MADEPV
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10),Unadjusted
Total VPH
Surrogates
2,5-Dibromotoluene (FID)
2,5-Dibromotoluene (PID)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
ND
mg/kg
11.5
1
05/14/2015:35
05/15/2013:35
ND
mg/kg
11.5
1
05/14/2015:35
05/15/2013:35
ND
mg/kg
11.5
1
05/14/2015:35
05/15/2013:35
68
%
40-140
1
05/14/2015:35
05/15/2013:35
7194-86-7
73
%
40-140
1
05/14/2015:35
05/15/2013:35
84-15-1
100
%
40-140
1
05/14/2015:35
05/15/2013:35
321-60-8
99
%
40-140
1
05/14/2015:35
05/15/2013:35
580-13-2
Analytical Method: MADEP VPH Preparation
Method:
MADEPV
Pace Analytical
Services - Charlotte
ND
mg/kg
7.02
1.28
05/08/2010:00
05/19/2019:35
ND
mg/kg
7.02
1.28
05/08/2010:00
05/19/2019:35
ND
mg/kg
7.02
1.28
05/08/2010:00
05/19/2019:35
ND
mg/kg
7.02
1.28
05/08/2010:00
05/19/2019:35
106
%
70-130
1.28
05/08/2010:00
05/19/2019:35
98.1
%
70-130
1.28
05/08/2010:00
05/19/2019:35
Analytical Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
83-32-9
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
208-96-8
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
62-53-3
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
120-12-7
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
56-55-3
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
50-32-8
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
205-99-2
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
191-24-2
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
207-08-9
ND
ug/kg
1930
1
05/14/2015:14
05/15/2011:33
65-85-0
ND
ug/kg
773
1
05/14/2015:14
05/15/2011:33
100-51-6
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
101-55-3
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
85-68-7
ND
ug/kg
773
1
05/14/2015:14
05/15/2011:33
59-50-7
ND
ug/kg
773
1
05/14/2015:14
05/15/2011:33
106-47-8
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
111-91-1
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
111-44-4
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
91-58-7
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
95-57-8
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
7005-72-3
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
218-01-9
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
53-70-3
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
132-64-9
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
95-50-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: SOUTH WALL 2 Lab ID: 92477511003 Collected: 05/08/20 10:00 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
773
1
05/14/2015:14
05/15/2011:33
91-94-1
2,4-Dichlorophenol
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
120-83-2
Diethylphthalate
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
84-66-2
2,4-Dimethylphenol
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
105-67-9
Dimethylphthalate
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
131-11-3
Di-n-butylphthalate
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
773
1
05/14/2015:14
05/15/2011:33
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1930
1
05/14/2015:14
05/15/2011:33
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
606-20-2
Di-n-octylphthalate
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
117-81-7
Fluoranthene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
206-44-0
Fluorene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
87-68-3
Hexachlorobenzene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
77-47-4
Hexachloroethane
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
193-39-5
Isophorone
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
78-59-1
1-Methylnaphthalene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
90-12-0
2-Methylnaphthalene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
387
1
05/14/20 15:14
05/15/20 11:33
15831-10-4
Naphthalene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
91-20-3
2-Nitroaniline
ND
ug/kg
1930
1
05/14/2015:14
05/15/2011:33
88-74-4
3-Nitroaniline
ND
ug/kg
1930
1
05/14/2015:14
05/15/2011:33
99-09-2
4-Nitroaniline
ND
ug/kg
773
1
05/14/2015:14
05/15/2011:33
100-01-6
Nitrobenzene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
98-95-3
2-Nitrophenol
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
88-75-5
4-Nitrophenol
ND
ug/kg
1930
1
05/14/2015:14
05/15/2011:33
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
108-60-1
Pentachlorophenol
ND
ug/kg
773
1
05/14/2015:14
05/15/2011:33
87-86-5
Phenanthrene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
85-01-8
Phenol
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
108-95-2
Pyrene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
129-00-0
Pyridine
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
387
1
05/14/2015:14
05/15/2011:33
88-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v2
v1
Qual
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■■
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: SOUTH WALL 2 Lab ID: 92477511003 Collected: 05/08/20 10:00 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
55
%
23-110
1
05/14/20 15:14
05/15/20 11:33
4165-60-0
2-Fluorobiphenyl (S)
49
%
30-110
1
05/14/20 15:14
05/15/20 11:33
321-60-8
Terphenyl-d14 (S)
51
%
28-110
1
05/14/20 15:14
05/15/20 11:33
1718-51-0
Phenol-d6 (S)
53
%
22-110
1
05/14/20 15:14
05/15/20 11:33
13127-88-3
2-Fluorophenol (S)
53
%
13-110
1
05/14/20 15:14
05/15/20 11:33
367-12-4
2,4,6-Tribromophenol (S)
54
%
27-110
1
05/14/20 15:14
05/15/20 11:33
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
134
1
05/14/20 17:52
05/14/20 21:00
67-64-1
Benzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
71-43-2
Bromobenzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
108-86-1
Bromochloromethane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
74-97-5
Bromodichloromethane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
75-27-4
Bromoform
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
75-25-2
Bromomethane
ND
ug/kg
13.4
1
05/14/20 17:52
05/14/20 21:00
74-83-9
2-Butanone (MEK)
ND
ug/kg
134
1
05/14/20 17:52
05/14/20 21:00
78-93-3
n-Butylbenzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
104-51-8
sec-Butylbenzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
135-98-8
tert-Butyl benzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
98-06-6
Carbon tetrachloride
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
56-23-5
Chlorobenzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
108-90-7
Chloroethane
ND
ug/kg
13.4
1
05/14/20 17:52
05/14/20 21:00
75-00-3
Chloroform
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
67-66-3
Chloromethane
ND
ug/kg
13.4
1
05/14/20 17:52
05/14/20 21:00
74-87-3
2-Chlorotoluene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
95-49-8
4-Chlorotoluene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
96-12-8
Dibromochloromethane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
106-93-4
Dibromomethane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
106-46-7
Dichlorodifluoromethane
ND
ug/kg
13.4
1
05/14/20 17:52
05/14/20 21:00
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
563-58-6
REPORT OF LABORATORY ANALYSIS
IH
Qual
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■■
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 934 W. MALLARD
Pace Project No.: 92477511
Sample: SOUTH WALL 2 Lab ID: 92477511003 Collected: 05/08/20 10:00 Received: 05/13/20 16:46 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A Volatile Organics
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
10061-01-5
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
10061-02-6
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
108-20-3
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
100-41-4
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
87-68-3
ND
ug/kg
66.8
1
05/14/20 17:52
05/14/20 21:00
591-78-6
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
98-82-8
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
99-87-6
ND
ug/kg
26.7
1
05/14/20 17:52
05/14/20 21:00
75-09-2
ND
ug/kg
66.8
1
05/14/20 17:52
05/14/20 21:00
108-10-1
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
1634-04-4
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
91-20-3
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
103-65-1
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
100-42-5
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
630-20-6
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
79-34-5
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
127-18-4
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
108-88-3
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
87-61-6
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
120-82-1
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
71-55-6
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
79-00-5
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
79-01-6
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
75-69-4
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
96-18-4
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
95-63-6
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
108-67-8
ND
ug/kg
66.8
1
05/14/20 17:52
05/14/20 21:00
108-05-4 v1
ND
ug/kg
13.4
1
05/14/20 17:52
05/14/20 21:00
75-01-4
ND
ug/kg
13.4
1
05/14/20 17:52
05/14/20 21:00
1330-20-7
ND
ug/kg
13.4
1
05/14/20 17:52
05/14/20 21:00
179601-23-1
ND
ug/kg
6.7
1
05/14/20 17:52
05/14/20 21:00
95-47-6
103
%
70-130
1
05/14/20 17:52
05/14/20 21:00
2037-26-5
103
%
70-130
1
05/14/20 17:52
05/14/20 21:00
460-00-4
104
%
70-132
1
05/14/20 17:52
05/14/20 21:00
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 13.8 % 0.10 1 05/13/20 17:44
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace Analytical Services -Asheville
Total Solids 91.2 % 1 05/21/20 14:38 05/21/20 14:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
QC Batch: 1478960 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477511001, 92477511002, 92477511003
METHOD BLANK: R3530147-3
Matrix:
Solid
Associated Lab Samples: 92477511001, 92477511002,
92477511003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND
5.00
05/19/20 12:25
Aliphatic (C09-C12)
mg/kg
ND
5.00
05/19/20 12:25
Aromatic (C09-C10),Unadjusted
mg/kg
ND
5.00
05/19/20 12:25
Total VPH
mg/kg
ND
5.00
05/19/20 12:25
2,5-Dibromotoluene (FID)
%
100
70-130
05/19/20 12:25
2,5-Dibromotoluene (PID)
%
93.4
70-130
05/19/20 12:25
LABORATORY CONTROL SAMPLE & LCSD:
R3530147-1
R3530147-2
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg 60
63.6
64.1
106
107
70-130
0.783
25
Aliphatic (C09-C12)
mg/kg 70
82.6
83.3
118
119
70-130
0.844
25
Aromatic (C09-C10),Unadjusted
mg/kg 10
11.1
11.1
111
111
70-130
0
25
Total VPH
mg/kg 140
157
159
112
114
70-130
1.27
25
2,5-Dibromotoluene (FID)
%
107
106
70-130
2,5-Dibromotoluene (PID)
%
100
99.2
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
QC Batch: 541667 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477511001, 92477511002, 92477511003
METHOD BLANK: 2886546 Matrix:
Associated Lab Samples: 92477511001, 92477511002, 92477511003
Blank
Parameter Units Result
Solid
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
05/14/20 19:45
1,1,1-Trichloroethane
ug/kg
ND
5.0
05/14/20 19:45
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
05/14/20 19:45
1,1,2-Trichloroethane
ug/kg
ND
5.0
05/14/20 19:45
1,1-Dichloroethane
ug/kg
ND
5.0
05/14/20 19:45
1,1-Dichloroethene
ug/kg
ND
5.0
05/14/20 19:45
1,1-Dichloropropene
ug/kg
ND
5.0
05/14/20 19:45
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
05/14/20 19:45
1,2,3-Trichloropropane
ug/kg
ND
5.0
05/14/20 19:45
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
05/14/20 19:45
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
05/14/20 19:45
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
05/14/20 19:45
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
05/14/20 19:45
1,2-Dichlorobenzene
ug/kg
ND
5.0
05/14/20 19:45
1,2-Dichloroethane
ug/kg
ND
5.0
05/14/20 19:45
1,2-Dichloropropane
ug/kg
ND
5.0
05/14/20 19:45
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
05/14/20 19:45
1,3-Dichlorobenzene
ug/kg
ND
5.0
05/14/20 19:45
1,3-Dichloropropane
ug/kg
ND
5.0
05/14/20 19:45
1,4-Dichlorobenzene
ug/kg
ND
5.0
05/14/20 19:45
2,2-Dichloropropane
ug/kg
ND
5.0
05/14/20 19:45
2-Butanone (MEK)
ug/kg
ND
100
05/14/20 19:45
2-Chlorotoluene
ug/kg
ND
5.0
05/14/20 19:45
2-Hexanone
ug/kg
ND
50.0
05/14/20 19:45
4-Chlorotoluene
ug/kg
ND
5.0
05/14/20 19:45
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
05/14/20 19:45
Acetone
ug/kg
ND
100
05/14/20 19:45
Benzene
ug/kg
ND
5.0
05/14/20 19:45
Bromobenzene
ug/kg
ND
5.0
05/14/20 19:45
Bromochloromethane
ug/kg
ND
5.0
05/14/20 19:45
Bromodichloromethane
ug/kg
ND
5.0
05/14/20 19:45
Bromoform
ug/kg
ND
5.0
05/14/20 19:45
Bromomethane
ug/kg
ND
10.0
05/14/20 19:45 IH
Carbon tetrachloride
ug/kg
ND
5.0
05/14/20 19:45
Chlorobenzene
ug/kg
ND
5.0
05/14/20 19:45
Chloroethane
ug/kg
ND
10.0
05/14/20 19:45
Chloroform
ug/kg
ND
5.0
05/14/20 19:45
Chloromethane
ug/kg
ND
10.0
05/14/20 19:45
cis-1,2-Dichloroethene
ug/kg
ND
5.0
05/14/20 19:45
cis-1,3-Dichloropropene
ug/kg
ND
5.0
05/14/20 19:45
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
METHOD BLANK: 2886546
Matrix:
Solid
Associated Lab Samples: 92477511001, 92477511002, 92477511003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Dibromochloromethane
ug/kg
ND
5.0
05/14/20 19:45
Dibromomethane
ug/kg
ND
5.0
05/14/20 19:45
Dichlorodifluoromethane
ug/kg
ND
10.0
05/14/20 19:45
Diisopropyl ether
ug/kg
ND
5.0
05/14/20 19:45
Ethylbenzene
ug/kg
ND
5.0
05/14/20 19:45
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
05/14/20 19:45
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
05/14/20 19:45
m&p-Xylene
ug/kg
ND
10.0
05/14/20 19:45
Methyl-tert-butyl ether
ug/kg
ND
5.0
05/14/20 19:45
Methylene Chloride
ug/kg
ND
20.0
05/14/20 19:45
n-Butylbenzene
ug/kg
ND
5.0
05/14/20 19:45
n-Propylbenzene
ug/kg
ND
5.0
05/14/20 19:45
Naphthalene
ug/kg
ND
5.0
05/14/20 19:45
o-Xylene
ug/kg
ND
5.0
05/14/20 19:45
p-Isopropyltoluene
ug/kg
ND
5.0
05/14/20 19:45
sec-Butylbenzene
ug/kg
ND
5.0
05/14/20 19:45
Styrene
ug/kg
ND
5.0
05/14/20 19:45
tert-Butyl benzene
ug/kg
ND
5.0
05/14/20 19:45
Tetrachloroethene
ug/kg
ND
5.0
05/14/20 19:45
Toluene
ug/kg
ND
5.0
05/14/20 19:45
trans-1,2-Dichloroethene
ug/kg
ND
5.0
05/14/20 19:45
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
05/14/20 19:45
Trichloroethene
ug/kg
ND
5.0
05/14/20 19:45
Trichlorofluoromethane
ug/kg
ND
5.0
05/14/20 19:45
Vinyl acetate
ug/kg
ND
50.0
05/14/20 19:45
v1
Vinyl chloride
ug/kg
ND
10.0
05/14/20 19:45
Xylene (Total)
ug/kg
ND
10.0
05/14/20 19:45
1,2-Dichloroethane-d4 (S)
%
102
70-132
05/14/20 19:45
4-Bromofluorobenzene (S)
%
100
70-130
05/14/20 19:45
Toluene-d8 (S)
%
102
70-130
05/14/20 19:45
LABORATORY CONTROL SAMPLE & LCSD:
2886547
2886548
Spike
LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
60.8
60.7
122 121
70-130 0
30
1,1,1-Trichloroethane
ug/kg
50
53.2
54.4
106 109
70-130 2
30
1,1,2,2-Tetrachloroethane
ug/kg
50
56.0
58.9
112 118
55-130 5
30
1,1,2-Trichloroethane
ug/kg
50
57.0
58.2
114 116
70-130 2
30
1,1-Dichloroethane
ug/kg
50
53.5
56.1
107 112
68-130 5
30
1,1-Dichloroethene
ug/kg
50
57.5
58.1
115 116
70-130 1
30
1,1-Dichloropropene
ug/kg
50
57.3
57.0
115 114
70-130 0
30
1,2,3-Trichlorobenzene
ug/kg
50
59.0
56.9
118 114
70-130 4
30
1,2,3-Trichloropropane
ug/kg
50
58.2
58.5
116 117
70-130 0
30
1,2,4-Trichlorobenzene
ug/kg
50
61.7
57.6
123 115
70-130 7
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
LABORATORY CONTROL SAMPLE & LCSD:
2886547
2886548
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
1,2,4-Trimethylbenzene
ug/kg
50
60.1
58.1
120
116
69-130
3
30
1,2-Dibromo-3-chloropropane
ug/kg
50
60.7
61.5
121
123
57-141
1
30
1,2-Dibromoethane (EDB)
ug/kg
50
60.3
58.6
121
117
70-130
3
30
1,2-Dichlorobenzene
ug/kg
50
57.9
57.5
116
115
70-130
1
30
1,2-Dichloroethane
ug/kg
50
53.9
55.3
108
111
70-130
3
30
1,2-Dichloropropane
ug/kg
50
57.9
58.2
116
116
70-130
1
30
1,3,5-Trimethylbenzene
ug/kg
50
59.1
58.1
118
116
70-130
2
30
1,3-Dichlorobenzene
ug/kg
50
58.8
58.4
118
117
70-130
1
30
1,3-Dichloropropane
ug/kg
50
58.3
59.7
117
119
70-130
2
30
1,4-Dichlorobenzene
ug/kg
50
59.4
58.9
119
118
70-130
1
30
2,2-Dichloropropane
ug/kg
50
56.1
55.9
112
112
70-130
0
30
2-Butanone (MEK)
ug/kg
100
111
116
111
116
60-130
5
30
2-Chlorotoluene
ug/kg
50
58.2
57.4
116
115
70-130
2
30
2-Hexanone
ug/kg
100
115
118
115
118
70-132
2
30
4-Chlorotoluene
ug/kg
50
61.0
57.8
122
116
70-130
5
30
4-Methyl-2-pentanone (MIBK)
ug/kg
100
116
116
116
116
69-130
0
30
Acetone
ug/kg
100
108
107
108
107
49-148
2
30
Benzene
ug/kg
50
58.1
57.2
116
114
70-130
2
30
Bromobenzene
ug/kg
50
58.4
59.6
117
119
70-130
2
30
Bromochloromethane
ug/kg
50
55.7
57.4
111
115
70-130
3
30
Bromodichloromethane
ug/kg
50
59.6
58.9
119
118
70-130
1
30
Bromoform
ug/kg
50
58.7
58.9
117
118
68-136
0
30
Bromomethane
ug/kg
50
57.0
59.5
114
119
60-140
4
30 IH
Carbon tetrachloride
ug/kg
50
59.1
59.5
118
119
70-130
1
30
Chlorobenzene
ug/kg
50
58.2
58.7
116
117
70-130
1
30
Chloroethane
ug/kg
50
56.7
60.5
113
121
51-147
6
30
Chloroform
ug/kg
50
50.8
56.2
102
112
70-130
10
30
Chloromethane
ug/kg
50
43.0
42.9
86
86
48-130
0
30
cis-1,2-Dichloroethene
ug/kg
50
54.2
55.2
108
110
70-130
2
30
cis-1,3-Dichloropropene
ug/kg
50
59.5
58.8
119
118
70-130
1
30
Dibromochloromethane
ug/kg
50
59.7
59.4
119
119
70-130
1
30
Dibromomethane
ug/kg
50
58.5
58.3
117
117
70-130
0
30
Dichlorodifluoromethane
ug/kg
50
60.1
58.9
120
118
49-130
2
30
Diisopropyl ether
ug/kg
50
53.4
55.6
107
111
66-130
4
30
Ethylbenzene
ug/kg
50
55.9
55.4
112
111
70-130
1
30
Hexachloro-1,3-butadiene
ug/kg
50
60.8
57.7
122
115
70-130
5
30
Isopropylbenzene(Cumene)
ug/kg
50
57.8
58.4
116
117
70-130
1
30
m&p-Xylene
ug/kg
100
114
112
114
112
70-130
2
30
Methyl-tert-butyl ether
ug/kg
50
54.9
56.3
110
113
70-130
2
30
Methylene Chloride
ug/kg
50
55.2
57.3
110
115
50-137
4
30
n-Butylbenzene
ug/kg
50
60.6
56.9
121
114
70-130
6
30
n-Propylbenzene
ug/kg
50
56.7
54.6
113
109
70-130
4
30
Naphthalene
ug/kg
50
59.2
58.8
118
118
70-131
1
30
o-Xylene
ug/kg
50
57.9
56.2
116
112
70-130
3
30
p-Isopropyltoluene
ug/kg
50
59.0
57.2
118
114
70-130
3
30
sec-Butylbenzene
ug/kg
50
57.3
55.4
115
111
70-130
3
30
Styrene
ug/kg
50
61.0
60.8
122
122
70-130
0
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
LABORATORY CONTROL SAMPLE & LCSD:
2886547
2886548
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
tert-Butyl benzene
ug/kg
50
50.3
49.7
101
99
69-130
1
30
Tetrachloroethene
ug/kg
50
58.7
57.4
117
115
56-130
2
30
Toluene
ug/kg
50
55.6
55.9
111
112
70-130
1
30
trans-1,2-Dichloroethene
ug/kg
50
55.1
58.3
110
117
70-130
6
30
trans- 1,3-Dichloropropene
ug/kg
50
61.0
61.0
122
122
70-130
0
30
Trichloroethene
ug/kg
50
59.6
59.8
119
120
70-141
0
30
Trichlorofluoromethane
ug/kg
50
57.3
59.5
115
119
67-130
4
30
Vinyl acetate
ug/kg
100
135
135
135
135
10-136
0
30 v1
Vinyl chloride
ug/kg
50
62.7
63.6
125
127
67-130
1
30
Xylene (Total)
ug/kg
150
172
168
114
112
70-130
2
30
1,2-Dichloroethane-d4 (S)
%
97
96
70-132
4-Bromofluorobenzene (S)
%
100
99
70-130
Toluene-d8(S)
%
101
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
QC Batch: 541606 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477511001, 92477511002, 92477511003
METHOD BLANK: 2886066 Matrix:
Associated Lab Samples: 92477511001, 92477511002, 92477511003
Blank
Parameter Units Result
Solid
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
325
05/15/20 08:24
1,2-Dichlorobenzene
ug/kg
ND
325
05/15/20 08:24
1,3-Dichlorobenzene
ug/kg
ND
325
05/15/20 08:24
1,4-Dichlorobenzene
ug/kg
ND
325
05/15/20 08:24
1-Methylnaphthalene
ug/kg
ND
325
05/15/20 08:24
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
325
05/15/20 08:24
2,4,5-Trichlorophenol
ug/kg
ND
325
05/15/20 08:24
2,4,6-Trichlorophenol
ug/kg
ND
325
05/15/20 08:24
2,4-Dichlorophenol
ug/kg
ND
325
05/15/20 08:24
2,4-Dimethylphenol
ug/kg
ND
325
05/15/20 08:24
2,4-Dinitrophenol
ug/kg
ND
1620
05/15/20 08:24
2,4-Dinitrotoluene
ug/kg
ND
325
05/15/20 08:24
2,6-Dinitrotoluene
ug/kg
ND
325
05/15/20 08:24
2-Chloronaphthalene
ug/kg
ND
325
05/15/20 08:24
2-Chlorophenol
ug/kg
ND
325
05/15/20 08:24
2-Methylnaphthalene
ug/kg
ND
325
05/15/20 08:24
2-Methylphenol(o-Cresol)
ug/kg
ND
325
05/15/20 08:24
2-Nitroaniline
ug/kg
ND
1620
05/15/20 08:24
2-Nitrophenol
ug/kg
ND
325
05/15/20 08:24
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
325
05/15/20 08:24
3,3'-Dichlorobenzidine
ug/kg
ND
649
05/15/20 08:24
3-Nitroaniline
ug/kg
ND
1620
05/15/20 08:24
4,6-Dinitro-2-methyl phenol
ug/kg
ND
649
05/15/20 08:24
4-Bromophenylphenyl ether
ug/kg
ND
325
05/15/20 08:24
4-ChIoro-3-methyl phenol
ug/kg
ND
649
05/15/20 08:24
4-Chloroaniline
ug/kg
ND
649
05/15/20 08:24
4-Chlorophenylphenyl ether
ug/kg
ND
325
05/15/20 08:24
4-Nitroaniline
ug/kg
ND
649
05/15/20 08:24
4-Nitrophenol
ug/kg
ND
1620
05/15/20 08:24
Acenaphthene
ug/kg
ND
325
05/15/20 08:24
Acenaphthylene
ug/kg
ND
325
05/15/20 08:24
Aniline
ug/kg
ND
325
05/15/20 08:24
Anthracene
ug/kg
ND
325
05/15/20 08:24
Benzo(a)anthracene
ug/kg
ND
325
05/15/20 08:24
Benzo(a)pyrene
ug/kg
ND
325
05/15/20 08:24
Benzo(b)fluoranthene
ug/kg
ND
325
05/15/20 08:24
Benzo(g,h,i)perylene
ug/kg
ND
325
05/15/20 08:24
Benzo(k)fluoranthene
ug/kg
ND
325
05/15/20 08:24
Benzoic Acid
ug/kg
ND
1620
05/15/20 08:24
Benzyl alcohol
ug/kg
ND
649
05/15/20 08:24
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
METHOD BLANK: 2886066 Matrix:
Associated Lab Samples: 92477511001, 92477511002, 92477511003
Blank
Parameter Units Result
Solid
Reporting
Limit
Analyzed
bis(2-Chloroethoxy)methane
ug/kg
ND
325
05/15/20 08:24
bis(2-Chloroethyl) ether
ug/kg
ND
325
05/15/20 08:24
bis(2-Ethylhexyl)phthalate
ug/kg
ND
325
05/15/20 08:24
Butylbenzylphthalate
ug/kg
ND
325
05/15/20 08:24
Chrysene
ug/kg
ND
325
05/15/20 08:24
Di-n-butylphthalate
ug/kg
ND
325
05/15/20 08:24
Di-n-octylphthalate
ug/kg
ND
325
05/15/20 08:24
Dibenz(a,h)anthracene
ug/kg
ND
325
05/15/20 08:24
Dibenzofuran
ug/kg
ND
325
05/15/20 08:24
Diethylphthalate
ug/kg
ND
325
05/15/20 08:24
Dimethylphthalate
ug/kg
ND
325
05/15/20 08:24
Fluoranthene
ug/kg
ND
325
05/15/20 08:24
Fluorene
ug/kg
ND
325
05/15/20 08:24
Hexachloro-1,3-butadiene
ug/kg
ND
325
05/15/20 08:24
Hexachlorobenzene
ug/kg
ND
325
05/15/20 08:24
Hexachlorocyclopentadiene
ug/kg
ND
325
05/15/20 08:24
Hexachloroethane
ug/kg
ND
325
05/15/20 08:24
Indeno(1,2,3-cd)pyrene
ug/kg
ND
325
05/15/20 08:24
Isophorone
ug/kg
ND
325
05/15/20 08:24
N-Nitroso-di-n-propylamine
ug/kg
ND
325
05/15/20 08:24
N-Nitrosodimethylamine
ug/kg
ND
325
05/15/20 08:24
N-Nitrosodiphenylamine
ug/kg
ND
325
05/15/20 08:24
Naphthalene
ug/kg
ND
325
05/15/20 08:24
Nitrobenzene
ug/kg
ND
325
05/15/20 08:24
Pentachlorophenol
ug/kg
ND
649
05/15/20 08:24
Phenanthrene
ug/kg
ND
325
05/15/20 08:24
Phenol
ug/kg
ND
325
05/15/20 08:24
Pyrene
ug/kg
ND
325
05/15/20 08:24
Pyridine
ug/kg
ND
325
05/15/20 08:24
2,4,6-Tribromophenol (S)
%
76
27-110
05/15/20 08:24
2-Fluorobiphenyl (S)
%
72
30-110
05/15/20 08:24
2-Fluorophenol (S)
%
74
13-110
05/15/20 08:24
Nitrobenzene-d5 (S)
%
78
23-110
05/15/20 08:24
Phenol-d6 (S)
%
76
22-110
05/15/20 08:24
Terphenyl-d14 (S)
%
81
28-110
05/15/20 08:24
v2
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
2886067
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1690
1410
83
52-130
1,2-Dichlorobenzene
ug/kg
1690
1320
78
51-130
1,3-Dichlorobenzene
ug/kg
1690
1310
78
50-130
1,4-Dichlorobenzene
ug/kg
1690
1350
80
49-130
1-Methylnaphthalene
ug/kg
1690
1300
77
55-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
LABORATORY CONTROL SAMPLE:
Parameter
2886067
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
ug/kg
1690
1230
73
30-130
2,4,5-Trichlorophenol
ug/kg
1690
1460
87
55-130
2,4,6-Trichlorophenol
ug/kg
1690
1480
87
57-130
2,4-Dichlorophenol
ug/kg
1690
1410
84
56-130
2,4-Dimethylphenol
ug/kg
1690
1380
82
51-130
2,4-Dinitrophenol
ug/kg
8450
4670
55
27-133 v3
2,4-Dinitrotoluene
ug/kg
1690
1450
86
61-130
2,6-Dinitrotoluene
ug/kg
1690
1440
85
60-130
2-Chloronaphthalene
ug/kg
1690
1380
82
52-130
2-Chlorophenol
ug/kg
1690
1360
80
54-130
2-Methylnaphthalene
ug/kg
1690
1360
81
54-130
2-Methylphenol(o-Cresol)
ug/kg
1690
1330
79
51-130
2-Nitroaniline
ug/kg
3380
2860
85
51-130
2-Nitrophenol
ug/kg
1690
1340
80
49-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1690
1370
81
11-163
3,3'-Dichlorobenzidine
ug/kg
3380
2760
82
10-132
3-Nitroaniline
ug/kg
3380
2580
76
55-130
4,6-Dinitro-2-methyl phenol
ug/kg
3380
2060
61
47-142 v3
4-Bromophenylphenyl ether
ug/kg
1690
1520
90
59-130
4-ChIoro-3-methyl phenol
ug/kg
3380
2840
84
55-130
4-Chloroaniline
ug/kg
3380
2730
81
54-130
4-Chlorophenylphenyl ether
ug/kg
1690
1500
89
58-130
4-Nitroaniline
ug/kg
3380
2670
79
54-130
4-Nitrophenol
ug/kg
8450
7630
90
48-130
Acenaphthene
ug/kg
1690
1380
82
60-130
Acenaphthylene
ug/kg
1690
1380
82
60-130
Aniline
ug/kg
1690
1280
76
43-130
Anthracene
ug/kg
1690
1420
84
63-130
Benzo(a)anthracene
ug/kg
1690
1500
89
59-130
Benzo(a)pyrene
ug/kg
1690
1480
87
57-130
Benzo(b)fluoranthene
ug/kg
1690
1490
88
54-130
Benzo(g,h,i)perylene
ug/kg
1690
1490
88
59-130
Benzo(k)fluoranthene
ug/kg
1690
1450
86
54-130
Benzoic Acid
ug/kg
8450
5240
62
19-130
Benzyl alcohol
ug/kg
3380
2700
80
50-130
bis(2-Chloroethoxy)methane
ug/kg
1690
1280
76
54-130
bis(2-Chloroethyl) ether
ug/kg
1690
1260
75
48-130
bis(2-Ethylhexyl)phthalate
ug/kg
1690
1250
74
45-134
Butylbenzylphthalate
ug/kg
1690
1210
72
46-138
Chrysene
ug/kg
1690
1460
87
58-130
Di-n-butylphthalate
ug/kg
1690
1450
86
60-130
Di-n-octylphthalate
ug/kg
1690
1250
74
53-130
Dibenz(a,h)anthracene
ug/kg
1690
1600
95
59-130
Dibenzofuran
ug/kg
1690
1400
83
60-130
Diethylphthalate
ug/kg
1690
1470
87
60-130
Dimethylphthalate
ug/kg
1690
1470
87
60-130
Fluoranthene
ug/kg
1690
1500
89
65-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
LABORATORY CONTROL SAMPLE:
Parameter
2886067
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Fluorene
ug/kg
1690
1440
86
63-130
Hexachloro-1,3-butadiene
ug/kg
1690
1460
87
46-130
Hexachlorobenzene
ug/kg
1690
1500
89
58-130
Hexachlorocyclopentadiene
ug/kg
1690
862
51
23-130 v3
Hexachloroethane
ug/kg
1690
1290
76
47-130
Indeno(1,2,3-cd)pyrene
ug/kg
1690
1500
89
60-130
Isophorone
ug/kg
1690
1340
79
49-130
N-Nitroso-di-n-propylamine
ug/kg
1690
1310
78
47-130
N-Nitrosodimethylamine
ug/kg
1690
1270
75
45-130
N-Nitrosodiphenylamine
ug/kg
1690
1410
83
59-130
Naphthalene
ug/kg
1690
1360
80
55-130
Nitrobenzene
ug/kg
1690
1360
80
49-130
Pentachlorophenol
ug/kg
3380
3320
98
10-132 v1
Phenanthrene
ug/kg
1690
1430
85
62-130
Phenol
ug/kg
1690
1370
81
46-130
Pyrene
ug/kg
1690
1290
76
53-130
Pyridine
ug/kg
1690
1130
67
37-130
2,4,6-Tribromophenol (S)
%
91
27-110
2-Fluorobiphenyl (S)
%
78
30-110
2-Fluorophenol(S)
%
78
13-110
Nitrobenzene-d5 (S)
%
76
23-110
Phenol-d6 (S)
%
76
22-110
Terphenyl-d14 (S)
%
84
28-110
MATRIX SPIKE SAMPLE:
Parameter
2886068
Units
92477511001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
1940
1200
62
18-130
1,2-Dichlorobenzene
ug/kg
ND
1940
1190
61
14-130
1,3-Dichlorobenzene
ug/kg
ND
1940
1160
60
12-130
1,4-Dichlorobenzene
ug/kg
ND
1940
1210
62
10-130
1-Methylnaphthalene
ug/kg
ND
1940
1110
57
12-130
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
1940
1160
60
10-130
2,4,5-Trichlorophenol
ug/kg
ND
1940
1330
68
13-130
2,4,6-Trichlorophenol
ug/kg
ND
1940
1350
70
17-130
2,4-Dichlorophenol
ug/kg
ND
1940
1310
68
10-130
2,4-Dimethylphenol
ug/kg
ND
1940
1310
67
10-130
2,4-Dinitrophenol
ug/kg
ND
9710
4000
41
10-130 v3
2,4-Dinitrotoluene
ug/kg
ND
1940
1240
64
24-130
2,6-Dinitrotoluene
ug/kg
ND
1940
1230
64
23-130
2-Chloronaphthalene
ug/kg
ND
1940
1180
61
19-130
2-Chlorophenol
ug/kg
ND
1940
1320
68
10-130
2-Methylnaphthalene
ug/kg
ND
1940
1150
59
18-130
2-Methylphenol(o-Cresol)
ug/kg
ND
1940
1310
68
10-130
2-Nitroaniline
ug/kg
ND
3890
2700
70
17-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
MATRIX SPIKE SAMPLE:
2886068
92477511001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Nitrophenol
ug/kg
ND
1940
1230
64
10-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
1940
1330
69
10-130
3,3'-Dichlorobenzidine
ug/kg
ND
3890
2210
57
10-130
3-Nitroaniline
ug/kg
ND
3890
2430
62
24-130
4,6-Dinitro-2-methyl phenol
ug/kg
ND
3890
1910
49
10-152 v3
4-Bromophenylphenyl ether
ug/kg
ND
1940
1230
63
29-130
4-Chloro-3-methylphenol
ug/kg
ND
3890
2690
69
17-130
4-Chloroaniline
ug/kg
ND
3890
2490
64
14-130
4-Chlorophenylphenyl ether
ug/kg
ND
1940
1220
63
25-130
4-Nitroaniline
ug/kg
ND
3890
2550
66
22-130
4-Nitrophenol
ug/kg
ND
9710
7020
72
10-130
Acenaphthene
ug/kg
ND
1940
1170
60
20-130
Acenaphthylene
ug/kg
ND
1940
1180
61
25-130
Aniline
ug/kg
ND
1940
1190
62
10-130
Anthracene
ug/kg
ND
1940
1150
59
29-130
Benzo(a)anthracene
ug/kg
ND
1940
1180
61
19-130
Benzo(a)pyrene
ug/kg
ND
1940
1160
60
12-130
Benzo(b)fluoranthene
ug/kg
ND
1940
1170
60
14-130
Benzo(g,h,i)perylene
ug/kg
ND
1940
1170
60
10-130
Benzo(k)fluoranthene
ug/kg
ND
1940
1140
59
14-130
Benzoic Acid
ug/kg
ND
9710
3770
39
10-130
Benzyl alcohol
ug/kg
ND
3890
2620
67
13-130
bis(2-Chloroethoxy)methane
ug/kg
ND
1940
1200
62
16-130
bis(2-Chloroethyl) ether
ug/kg
ND
1940
1200
62
11-130
bis(2-Ethylhexyl)phthalate
ug/kg
ND
1940
1010
52
21-130
Butylbenzylphthalate
ug/kg
ND
1940
974
50
23-130
Chrysene
ug/kg
ND
1940
1180
61
22-130
Di-n-butylphthalate
ug/kg
ND
1940
1180
61
30-130
Di-n-octylphthalate
ug/kg
ND
1940
1020
52
23-142
Dibenz(a,h)anthracene
ug/kg
ND
1940
1070
55
10-130
Dibenzofuran
ug/kg
ND
1940
1180
61
24-130
Diethylphthalate
ug/kg
ND
1940
1210
63
26-130
Dimethylphthalate
ug/kg
ND
1940
1290
67
22-130
Fluoranthene
ug/kg
ND
1940
1210
63
33-130
Fluorene
ug/kg
ND
1940
1200
62
22-130
Hexachloro-1,3-butadiene
ug/kg
ND
1940
1200
62
13-130
Hexachlorobenzene
ug/kg
ND
1940
1200
62
29-130
Hexachlorocyclopentadiene
ug/kg
ND
1940
665
34
10-130 v3
Hexachloroethane
ug/kg
ND
1940
1110
57
10-130
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1940
1180
61
10-130
Isophorone
ug/kg
ND
1940
1250
65
13-130
N-Nitroso-di-n-propylamine
ug/kg
ND
1940
1270
65
12-130
N-Nitrosodimethylamine
ug/kg
ND
1940
1220
63
11-130
N-Nitrosodiphenylamine
ug/kg
ND
1940
1180
61
15-130
Naphthalene
ug/kg
ND
1940
1180
61
15-130
Nitrobenzene
ug/kg
ND
1940
1250
64
12-130
Pentachlorophenol
ug/kg
ND
3890
2800
72
10-130 v1
Results presented on this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
MATRIX SPIKE SAMPLE:
Parameter
2886068
Units
92477511001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Phenanthrene
ug/kg
ND
1940
1170
60
27-130
Phenol
ug/kg
ND
1940
1330
69
10-130
Pyrene
ug/kg
ND
1940
1040
54
19-130
Pyridine
ug/kg
ND
1940
957
49
10-130
2,4,6-Tribromophenol (S)
%
66
27-110
2-Fluorobiphenyl (S)
%
52
30-110
2-Fluorophenol(S)
%
64
13-110
Nitrobenzene-d5(S)
%
60
23-110
Phenol-d6 (S)
%
64
22-110
Terphenyl-d14 (S)
%
51
28-110
SAMPLE DUPLICATE: 2886069
Parameter
Units
92477511002
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
1-Methylnaphthalene
ug/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
2,4,5-Trichlorophenol
ug/kg
ND
ND
2,4,6-Trichlorophenol
ug/kg
ND
ND
2,4-Dichlorophenol
ug/kg
ND
ND
2,4-Dimethylphenol
ug/kg
ND
ND
2,4-Dinitrophenol
ug/kg
ND
ND
2,4-Dinitrotoluene
ug/kg
ND
ND
2,6-Dinitrotoluene
ug/kg
ND
ND
2-Chloronaphthalene
ug/kg
ND
ND
2-Chlorophenol
ug/kg
ND
ND
2-Methylnaphthalene
ug/kg
ND
ND
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
2-Nitroaniline
ug/kg
ND
ND
2-Nitrophenol
ug/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
3,3'-Dichlorobenzidine
ug/kg
ND
ND
3-Nitroaniline
ug/kg
ND
ND
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
4-Bromophenylphenyl ether
ug/kg
ND
ND
4-ChIoro-3-methyl phenol
ug/kg
ND
ND
4-Chloroaniline
ug/kg
ND
ND
4-Chlorophenylphenyl ether
ug/kg
ND
ND
4-Nitroaniline
ug/kg
ND
ND
4-Nitrophenol
ug/kg
ND
ND
Acenaphthene
ug/kg
ND
ND
Acenaphthylene
ug/kg
ND
ND
RPD Qualifiers
v2
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
SAMPLE DUPLICATE: 2886069
Parameter
Units
92477511002
Result
Dup
Result
Aniline
ug/kg
ND
ND
Anthracene
ug/kg
ND
ND
Benzo(a)anthracene
ug/kg
ND
ND
Benzo(a)pyrene
ug/kg
ND
ND
Benzo(b)fluoranthene
ug/kg
ND
ND
Benzo(g,h,i)perylene
ug/kg
ND
ND
Benzo(k)fluoranthene
ug/kg
ND
ND
Benzoic Acid
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
Butylbenzylphthalate
ug/kg
ND
ND
Chrysene
ug/kg
ND
ND
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Fluoranthene
ug/kg
ND
ND
Fluorene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
Isophorone
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenanthrene
ug/kg
ND
ND
Phenol
ug/kg
ND
ND
Pyrene
ug/kg
ND
ND
Pyridine
ug/kg
ND
ND
2,4,6-Tribromophenol (S)
%
53
55
2-Fluorobiphenyl (S)
%
51
54
2-Fluorophenol(S)
%
53
55
Nitrobenzene-d5 (S)
%
52
57
Phenol-d6 (S)
%
51
54
Terphenyl-d14 (S)
%
60
61
RPD Qualifiers
v2
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
QC Batch: 541610 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477511001, 92477511002, 92477511003
METHOD BLANK: 2886087
Matrix:
Solid
Associated Lab Samples:
92477511001, 92477511002,
92477511003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10.1
05/15/20 10:52 N2
Aliphatic (C19-C36)
mg/kg
ND
10.1
05/15/20 10:52 N2
Aromatic (C11-C22)
mg/kg
ND
10.1
05/15/20 10:52 N2
2-Bromonaphthalene (S)
%
93
40-140
05/15/20 10:52
2-Fluorobiphenyl (S)
%
93
40-140
05/15/20 10:52
Nonatriacontane (S)
%
67
40-140
05/15/20 10:52
o-Terphenyl (S)
%
75
40-140
05/15/20 10:52
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2886088
Units
Spike
Conc.
2886089
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec Max
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10.1
ND ND
46
42
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.5
ND ND
53
59
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.6
20.2 18.5
71
64
40-140 9 50 N2
2-Bromonaphthalene (S)
%
103
102
40-140
2-Fluorobiphenyl (S)
%
96
96
40-140
Nonatriacontane (S)
%
60
55
40-140
o-Terphenyl(S)
%
87
77
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
QC Batch: 541432 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477511001, 92477511002, 92477511003
SAMPLE DUPLICATE: 2885375
92477444009 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 21.6 23.5 8
SAMPLE DUPLICATE: 2885376
92477511003 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 13.8 12.6 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 35

■
2ce Analyfiol
tirwrr.plo$ab�.po�
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 934 W. MALLARD
Pace Project No.: 92477511
QC Batch: 1479831 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92477511001, 92477511002, 92477511003
METHOD BLANK: R3530705-1
Matrix:
Solid
Associated Lab Samples: 92477511001, 92477511002, 92477511003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Solids
%
0.00100
05/21/20 14:47
LABORATORY CONTROL SAMPLE:
R3530705-2
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Solids
%
50
50.0
99.9 85-115
SAMPLE DUPLICATE: R3530705-3
L1218567-04 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids % 83.7 83.5 0.228
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 35

■
2ce Analyfiol
tirwrr.p�oftab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 934 W. MALLARD
Pace Project No.: 92477511
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:55 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 35

■
2ce Analyfiol
tirwrr.p�o$ab�.p■r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
934 W. MALLARD
92477511
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92477511001
NORTH WALL 2
MADEP EPH
541610
MADEP EPH
542036
92477511002
EAST WALL 2
MADEP EPH
541610
MADEP EPH
542036
92477511003
SOUTH WALL 2
MADEP EPH
541610
MADEP EPH
542036
92477511001
NORTH WALL 2
MADEPV
1478960
MADEP VPH
1478960
92477511002
EAST WALL 2
MADEPV
1478960
MADEP VPH
1478960
92477511003
SOUTH WALL 2
MADEPV
1478960
MADEP VPH
1478960
92477511001
NORTH WALL 2
EPA 3546
541606
EPA 8270E
541753
92477511002
EAST WALL 2
EPA 3546
541606
EPA 8270E
541753
92477511003
SOUTH WALL 2
EPA 3546
541606
EPA 8270E
541753
92477511001
NORTH WALL 2
EPA 5035A
541667
EPA 8260D
541845
92477511002
EAST WALL 2
EPA 5035A
541667
EPA 8260D
541845
92477511003
SOUTH WALL 2
EPA 5035A
541667
EPA 8260D
541845
92477511001
NORTH WALL 2
ASTM D2974-87
541432
92477511002
EAST WALL 2
ASTM D2974-87
541432
92477511003
SOUTH WALL 2
ASTM D2974-87
541432
92477511001
NORTH WALL 2
SM 2540 G
1479831
SM 254OG
1479831
92477511002
EAST WALL 2
SM 2540 G
1479831
SM 254OG
1479831
92477511003
SOUTH WALL 2
SM 2540 G
1479831
SM 254OG
1479831
Date: 05/22/2020 04:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 35

docurnent Name; (Mcu me -it Rowl sad: February i, PQiB
1�J71'f ■3rrY ltI COhtl Itlttn ll oM1 AaCaIpt15CUR) Pd i t}f
DocUrnent Wo.; Issuing AuUMrltV;
PaceCarullrnas OualitVOfce
LabOritOry QCeluing samples:
Asheville ❑ Eden[] Greelrvkrood ❑ iftater5vlll1e 0 Raleigh[] MechanicsWilell
Client Name:`` PraJetr ! W ' 4 511
C 1I11I1 II` I LF 1 1L I
Courier; OFeOEx OUPS LJUSPS
:1 Cnfnrvrc;al Qpace Dother- 92477511 I I
Custody Seal Pement7 Dyes C39'o Sears imatt7 ❑Yes ONG y
Oatt�'+ltrol�i}orlon EuminlnE [onmMti-,
PacWlr�g{r1�teNal'. Dubblewl-ap [ji�ubhleEYags []hfnne D Ij•ther g10101ptai7ISSURFreizoo
1;hermpRrtler; Dyes 13NO ONfA
9�Ti}� i TYrfe ai Ice: [wet [)Blue �Na nr
Gta Gun IG:
Cooler Temp ('Cj: �x �,, C'orrectlun Faller: Add Subtract S'�1 + .1 Temp snould be *oon Ireeiing Io VlG
Coal@r Tomp. Corteded J'CM' 05r+nplEF Dinar ttm4iaiteri3 S,amplrtlan lGe, caannE proem
hi: heguA
USDA Regulated SM ([] P#A. water samal9l
Did simples ali itE in i QU;PFdntfne Fane wltfun She Umred 5tate5: CA, NY, or SC "edr m,Dpsj � Old 9anon arigirkta 6v-- a+oreko sourcOInlem�IWrallY,
Yrts, Mc intludirt{l+iwill a•d PuErro elcar oyes OHc
{amr+�ntl�OltcreRa
Maln d! Cuytady W
SampteSAmlved wghln MdW Time?
Short Wei 71me Atislvshr Wl hr,f 7
Suffidenl Valuree7
Correll Cimtalners Wed?
-Parr Cantkireri Used?
COnt�hners IntaM7
0Isiolved dmaM3i5; SsrnAle.� Fiord Fllrered?
Heads ite In VOA trials 06-6mm
Tr+;r Blank "en 17
Thp Wank Ctrs o* Seals Present?
COMMENTS AMPL1EDISCREPANCY
Drys, nND ❑w �
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N A
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Tel
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Cl-IEryfiNI TIFICAUU IMFMUTMN
Pitman Cantactod
DitAfTlme;
PiviJea Meni#er 5CUAF Reultwr
Project Maimalar SU Navlew:
Field Baia7te0uired? ❑tea LJNo
Page 33 of 35

Document Jlamc CMMMt PAwtied; February 7. 2419
Ginhdillar1 Upon R-me 10 �
pgi;uFn:rit NIL! I1;ltrFg Authantw,.
rx-Ai7_C5_fill-Rnr-OG PaL- Camillnis ❑Vality WNIce
*Cheek mark top half of box if p14 andlor de ch lor I n 2 l ilun IS Rroj"t ll + 511 +�
vcrMod and w�thIn the acceptance ranee far preseevadon _ '## 11``��
sampl es. PAS: F1 8 Due I] ;e : M 28 / 20
Citce tlariv VQA, Cb ldgrm: TOC. Oil and Gxeise, DROIR015 (water) 00t;, LLHg CLIEH7: 32-INENCO
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Page 34 of 35

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APPENDIX C
Soil Disposal Manifests

Environmental Soils Inc.
P0 lox 295 • Lattimore, NC 28089
Phone-4S4-0075 • Fax [phone]
on-Haous raste.11anifest # 42598
Date _ iLoad Number
EAWIRONAYEATAL CONSULT N93
Contact:
(numbcred scquentially as snicks are dispatched)
Phone:
Fax:
GENERATOR,
Address: County:
Contact:
WASTE ORI INATIONP0INTr C~omplete Address:
Class WT';rpe of Contaminate in soil
SOURCE OF OArjr EVATION.• (ex. UST or other source)
Phone:
GENERefTOR S CERTIFICATION OF WASTE CONSTITUENTS: In tieit n� f submiffing asiel tical data (methods
9240 and 82 70) verifying That the waste in question does not contain organic constituents other than? ttwse which Would
"Ormnlly appar in -analysis ofvirgin etroleuns product rtsidue, I am submitting this Cerf i rate of Waso
Canyfituents. I certify that I mitt fanriliarwith the source ofrontamination of the soil andfit rther certify the source, to
the best afros knowledge, contains no contaminants other than that listed above.
Generators ignatinc- *I.. Date: ,.
TPANSPORTER:
Contact;
Phone;
As the carrier, I certify that the materials described above being shipped under this ton -hazardous materials
manifest are properly classified, packaged,. labeled, secured, and are in proper condition for #spurt in commerce
uadcr tlic applicable regulations governing transportation, and I hereby receive this materW for delivery to the
facility designfite.
Carrier Signature:
TRUCK #: TAG #:
TRUCK DRIVER SIG XKFURE:
Date.
VOLUME:
DATE:
DESTR UTIO . Environmental Soils Inc. 910 Crowder Rd, Shelby, N C 28150 Dedicated Land Application
Site Permit #SR0300039
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has begirt authurircd by the Sate of North Cmlhia.
Facility Signature:
Signature:
Company Name
Date.
Date:
Tide:
WhiMTacility Canary/Invoice Pink/Cartier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone '704-4 4-0075 - Fax [phone]
Non -Hazart ous Waste Manifest # 42599
Date _ ,� Load Number
( numbered squcn6a,lly as trues are dispatched)
R1VV RONME T4L CONS ULT4N7.1
Contact: Phone: Fax:
GENERTGR:
Address:
on"Ct:
WASTT ORIGINATION PGLTr Complete Address:
Class &. Type of Contaminate in soil
S0URGE OF C Gl 'I, MEV.1T1ON.- (er:. U S T or other source)
County:
Phone:
GENERA TOR 9 C:ERTIF`IC TIGN OF WAST,I; GQNS'TZTUEArn In lieu of subtr it6ng anadyTical data (methods
$2,10 and S 70) vetx; ying that rbe waste in question does not contain o r amir tonsti1 izents Ober Than &om wb ch -would
Psar pally appear in analysr"s otir in pefrodianproduct residlte, I ans subm i1fing this Certificate of Mute
Constituents. I certr�y That I ain fainillar witb the source o coma tination o f't e soil and further reify the source, is
the best ofmy `my knowledge, caymai rs no cantanj marts atber Than that listed above.
Generators Signa
TRJNN PORTER:
Contact:
Phone:
Date:
s the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly cl€ssifsed, packaged, labeled, secured, .end are in proper condition for transport in commerce
ender the applicable regulations governing transportation, and I hereby receive this rnateetal for delivery to the
foiil ty designate.
Carrier Signatutc: Date:
TFRUC #:
TAG #:
VOLUME:
TRUCK DRIVER SIGNATURE: DATE.
DES'TlNA770 V.• Environmental Sails Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit *SR0300038
I certify that the carrier has delivered the materials described above to this facility, and l hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature:
Signature; _— Date:
Company Name Tine:
Date:
White/Facility ana7/Invoice Pink/Carrier oldenrodlGenerator

Environmental Soils Inc.
PCB B-ox 295 - Lattimox, NC 28089
Phone 704-434-W75 - Fax [phone]
l
l an-l-3azar&us %+ to Manifest # 0 4
_,-
s
Date '1 ! 1 Lnad Nimbeir
(numbered sequentially as trucks ark dispatched)
EN LRON1YIENT4L ONaSUL 4N '
Contact: Phone: + r Fax.
ArER,4T0R.-
Address: ,� �. ounty: 0
Contact: Phone.
NSTF. ORI I TIONPOI2V'f: Complete Address:
Class &Type of Comminatc in soil �
SOURCE OF CONTAMINATION.- (ex. UST or other source) r
ENEM MRS CERTIF'I ATIONOF WAS TE CONSTITUENTS. In lieu of`s4uhniittxn analiyticaldata (inethods
8240 and i 70) ver6ing that the suaste in question does not rontain organic constituents atber Than those whieb would
narmally appear in analysis of virgimpetruleum pro Bret residue, lam submitting this Certifieare ofWaste
Constituents, I cer-fify that I ani fayniliar with the sore rce o f eanea irratr'art ofthe e svl andfurther cert�: fy the source, to
the hest ofmy kn led e, contains no mnfaminimft other than rhaa listed above.
Generators Signature-. Dare:
Contact: Phone: ' .. ! . 2;' -
As the carrier, I certify that the materials described above being shipped u der this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in cornmerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate. f .
Carrier Signature: Date: `� f i ` J
VOLUME:
TRUCK DRIVER S)<IIATIF: i. DATE:
DLMNS4TION; Envlronmcntal Soils Inc. 910 Crmvder Rd, Shelby, NC 28150 I edicamd Land Application
Site Permit # R030.3 S
I certify that the carrier has de5vertd the inateriala described above to this facility, and I liereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Cuolina.
Facility Signature: Date;,
Signature.
Company Name
Dam
Title:
WhitdFacility anarylInvoice Pink/Cartier Golclenro&Genemtor

Environmental Soils Inc.
PO $kox 295 Lattimore, NC 28089
Phone 7p4 34-0075 • Fax [phone]
Mon -Ha rdous WLtc Manifest #46085
Date Load Number
111rTi � + 1 y �+�r +�+ (numbered sequentialiy as trucks are dispatclicd)
ENvvzo �+1 rJ[ i Y mL oN lJ�.nivr i } J t F
Contact: _ . , Phonin-1 ` • 'h 2 Fax:
OF`N ERdTOR_ T n _ , . \ � h
Address: bounty:
Contact:' _ _ ' _ . Phone: ~7 4 1
WASTE OWMATIONPOLVTr GornplL.-te Address:
Class &Tvpe of Contaminate in soil
SOURCE OF OlVMMMTION.• (ex. UST or other source) �
GENERATORS CERTIFIC TIO)V OF WASTE CONST17VFNTS In heri of submitting analytical data (Methods
8240 and827-0) -verifyiqKthat the cask in rlreestion does not ronfain argurrir constituents ather than those -which would
mormally appear in axralysas o vir in etroleurn prodrrrt residue, f am srrbmin ng this Certificate of I aste
Constituents. I certify that l urn fam liar rruifb t1m sourre o_ f rot#tr�ri� �#uxt�or� of tyre sailandfuriber cerf the source, to
fbe hest ofmy my no wled e, contains no contarra ipiants outer than that listed akow.
GeneratorsSignature: _ _ 1::�_ _ _ _ _ -- `, _ . -' ,}` ' -- � �T D ate: .
TRANSPORTEA
ontacr: Phone:
As the carriex, I certify that the matcriah described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in cc=naerce
under the applicable regulatiops governing transportation, and 1 hereby receive this material for delivery to the
facility designate. I I +
Carrier signar= Date: _
TRUCK 1 #:
TAG : ' ' r k r
Via1r ME-
TRU KDRI ER SIGNATURE: DATE:ti: - ' '
DESTI ATIO . Environmental Soils Inc, 910 Crowder Rd, Shelby, NC 29150 Dedicated Land Apphcarion
Site Permit #SR03 00038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a marina that has been authorized by the Mate of North Carolina.
Facility Signature: Date:
igliaturc: Date'
Company Name
Ti
White/Tacility anary/In voice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Sox 295 • Laniniorex, NC 28089 otl�
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 5 2 0
Date. Lead Dumber
(numbered sequentially as treks arc dispatched)
EN IR01VMENrAL OONSULT4NTr
contact: - Phonc: Fax:
GENERdTOR:
Address: County:
Comae; Phone:
WASTE ORI LVATIONPOIN?: Complete Address:
Class &Type of Comminate in soil
SOURCE OF GGA MflVATIGN.- (eat, UST or other source)
GEAEM TOR S CERTIFIC.4 TION OF WWST.+E CONSTITUENTS: In heu of .3nb mimnganalyficaldara fin ethads
8240 and8270) verifying that the •waste M questions does not contain organic constituents o1ber than those whicbwould
normally appear in analyst's a wirgia petroleum product residne, I am submratft this Certificate ofWwe
Constituents. l eertxo tbal I am famitrur with the Source of �cordaminalion of f the sod and urtber certyythe sourre, to
the fast ofmy krrmled e, contains no contam issants other than that listed above.
Generators Signature;
TRAVSIAGRT'ER:
Contact: Phone.
As the carrier, I certify that the materials described above being shipped under this rzon-hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: _ Date:
TRU K k
TRUCK DRIVER SIGNATURE:
TAG k
VOLUME;
DATE: '
DESTINr1TTON.• Environmental Soils Inc. 910 Crowder lid, Shelby, NC 28150 Dedi-cated hand Application
Site Permit # SR0500038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carchna.
Facility Signature:
Signature:
Company Dame
Date:
Title:
Matey:.
bite,,acility Canary/Invoice Pink/ mTier crlderirocil �r�eratc�r

Date
Environmental Soils Inc.
PO Box 295 * Lattimore, NC 2SO89
Phone 04- 4- 25 • Fax [phone]
Non-Hazariours waste Manifest # 4 6 C O
Load Number
(numbered sequen't4y as trucks are dispatched)
ENVLRONMEAITAL CONS LT NT.
Coma Phone, Fax:
Address: t ' 4 "' - - ~ ' County: -
�Ll�
Contact: ti Phone:
I ST*R OPWINATtONPOINT; Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONT IMINAT'IO • (ex. UST or other source)
OENERzffORS CERTIFIC-4TIONOF WASTE CON$TIT'U AIS In lieu of sr bm ittingtanalyticaldata (me-th ads
8240 and 82 70) verifying Ikt The wave in question does not contain oWnk constitarents other than r!.►use which would
normally appear in analysis oft is petroleum pradutt residue, I'afft Submitting This Cedfflcafe of paste
Constitrutits.I certify thatI am amifiar with the source of contamination o, tube soil and rtber rert the sonnv, to
Ilse best of `my knowledge, contains no contrunir ana outer than that Hsted a owe
Generators Signature:
TRANSPORTER:
Contact:
Phone:
As the carrier, I certify that the materials described above being slipped under this jaon-#rar_ardous materials
manifest are properly classified, packaged, labeled, secured, and arc in proper condition for transport in commerce
under the appliCQble tegtilations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
Date:
TRUCE #:
TRUCK DRIVERSIGNATURE:
TA #:
VOLUME:
DATE:
DESTW4TIO .• Environmental Soils Inc. 910 Crowder lid, Shelby; NC 29150 Dedicated Land Application
54-o hermit # R0300038
I tvrtity that the wrier has delivered the materials described above to this facility, and I hereby accept this material
for treatmenr and/or disposal in a manner that has been authorized by the Sam of North Carolina,
I~adlity Signature: Date:
ignaturc:
Company Dame
Date -
Title:
iitelFaciliCanary/Invoice PiOWCrrier Goldenrod/Generator

-Environmental Soils Inc.
PO B-ox 2 :• Lattimore, NC 28089
Phone 7 #-434-0075 * Fax [phone]
Non -Hazardous Waste Manifes[ # 53388
Date. _ Load dumber
(mimbered sequentially as tru ks :axc, dispatched)
EN ROB AIENTAL CONSULTANT
contact: - _� Phone:
Addre�' {3l1 r1tY: i
Coma � _ � _ � Phone:
I VASTE ORr!` IN,iTlOjVP01 T,-Coml lets Address: l-f {� . � , .. A�
d
Class &Type of Cc ntatnimite in soil _ i
SOURCE OF CONDIMEVATION. (ex. UST or other source) L 'I
GENERd1'O1RSO KI'IFIC,11'.riONOff'IVASfEOONSTlTUF 7'S:lnlrerrgfsrlhiyr;ttiti;rtirarlyriruldota(metbods
9240 wid N270) vetifting that the waste in yupstlon does not rorrtain -organir core tHisients other than Those wbieb would
normally apftear in arrrrlysis of-virginjOelro%rrin pradncr residue, I art submitting }leis Cerfifirate o f Maste
(:onstil reents. f certt, tbat } am i nj ifiar switlr [ e source of r-orrtum ination q f'the soil and furf&w cerf y the source, to
the best o gray knowledge, mnlains no other than that listed above.
Genemtnrs Sign a rtwc.-ti ._ s . ; Date:
77Rr1N S}}OE f 7*A-
ontact- Phone:
As the c:trrit!r, I certi6, drat ffie--materials described ibove heing shipped undcr rht-� n-on-hazardous mfLrerials
m��ilifc5t are Properly clagified, packaged, I.thelecl., -%T- rod, anti are in proper 4ar,djtion for tm, nsport in commerce
rend r the appucablc re rl ttions govcrnr ig rnuispomttiail, and I liere1w mc6ve rhis material for del ivi2ryr to the
f: ciliry designate,
Carrier Signature; Datte-
` RUC K #.
TRU k DRIVER SIGNATURE:
TAG #:
DATE:
DESTJ7V,ITI0,'1r, Environmental Soil; In-c. 910 Crowder Rd, Shelby, SIC 29 150 Dedicated Land Application
Site Kermit #SR0300038
I cerrifv that ncc carrier has delivered the mate f qls described =chore to this facility, -,ind I lie iuby accept this friary-E 11
for treamaent andltQr dia sal iLi a man acr tl)at leas been aurhoriced by the State of North C Vol ina.
Facility Sigrsaature-
signature. Date:.
Company Name
`title:
bate•
whitcy acility cananAnvoice Pink/Carrier GaWmind/Cittic rator

Environmental Soils Inc.
PO Box 291 • Lattimore, IBC 28089
Phone -704-434•-0075 + Pax 704-434-9533
Mon-HazarJous Waste Manifest # 4 6 14
Date Load Number '-
(numbered sequentially as trucks are "patchtd)
ENYMONMENTAL CONSULTANT -
Contact; phone: Fax
Address• L�� County:
onmet: 7 } . phone:
HNS'TE 01UGINA IONPOEV'T Complete Address:
Class $G Type of C ontamin ate in soil ti -
SOURCE OF CON AME TiO . (ex, UST or othc r bou rce)
NERrITO S CEMFICATION OF W.4STF 'ONSTI ULN'!S: In lien of subrniMn analytiraldata (methads
9240 and 92 70) verEying that the waste hs question does not contain organic ronstifrents other- than those which would
normally appear in analysis off -tor inpetroleumprodnet residne, ,dam submitting tbr'-s Certificate o Waste
'onistitzrents. I certify tbat I am fam xliar with the source of •contaminatiion a f fbe soil and u rther certify the sou rce, to
the hest o my knowledge, eontains no confaminants other than that listed above.
,i
Generators Signature: Date: + f
TI INSPORTER:
Contact: Pholic:
s the carrier, I certify that the materials described above being shipped under this nnii-ha2ardous materials
manifest are properly classified, packagcd, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hemby receive this material for delivery to the
cility designate.
Carrier Signature: Bate:
TRUCK #.
TRUCK DRIVER SIGNATURE
DATE:
DFSM.dTION., Environmental Soils Inc. 9 10 Crowder Rd, Shelby, NC 29150 Dedicated Land Application
Site Fern -it #SR030OW8
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment andfor disposal in a mariner that has been authorkmd by the State of North Carolina,
Facility signature:
Company. Maitre
Date:
Title:
Dam;
White/FacibtyCanary/Invoice Pink/Carrier �oldenrcx (cnerator

Environmental Soils Inc.
PO $gk 295 -Lattimore, NC 28089
Prone 70 4-434# -0075 • Pax 704-43 -9533
Non -Hazardous Waste Manifest # 46144
Late I.. _ Load Number
(n4rnbered sequen is ly as trucks are dispatched)
EN dRQN)VF_ TAL OONSU TANT
Contact,_ ` - 1- �� - . _ �' Y Phone, F
A,ddrew , _75 , -County..
Contact: Phonc:_
WASTE ORIG17VATIONPOLN171 Complete Address: ! - -' _ - _ - _
Class &.Type of Contaminate in soil _ 1 k , ., _ .
-
SOURCE OFONTAMLVATION.- (ex. UST or other source)
OENFl 1TORS OFRTIFI ATION OF WA S TF C ONSTI7'U NTS: In lien o, fsubmart[ing anal ticulda0 (methods
8240 and 8 70) vet yimg that the wane in piestion does not contain organic corrstawents otherthan those which would
normally appear in analysix o, f -vxr in etmiru xa product residste, I am submitting this Certificate �f Waste
Constituents. I certr; y that I ani am iliar omit$ the source o conlana inafi&n of the soil andfurther certify the source, to
the best of my knowledge, cantatas era rontam marts other than that listed above.
Generators
TRAYSPORTER:
Contact: Phone:
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
rna ffest are properly classified, packaged, labeled, secut i, and are in proper condition for transport in commerec
under the applicable regulatiom governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier ignamm: _ Date:
TRUCK #:
TRUCK DRIVER SI NATU :
TAG #:
VOLUME.
DATE:
DE T'IN TION: Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dacated Land Application
Site Permit # 1 030003g
I certify that the carrier has delivered the materials described above to this facility* and I hereby accept this material
for treatment and/or disposal in a manner that },as been authorizcd by the State of North Carohn&
Facl} tv Signatwe:
Signature-,
Company dame
Title:
Late:
Whitc/Facility anaryllnvoicc Pinwcmier Goldenro&Gencrator

Environmental Soils Inc.
PC) Box 9_ .- Lattimore, NC 28089
Phone Z04-434-0073 • Fax [phone] ^ Lc ` ,
lion-Hazaaeous wg'ste Manifest # 4 14
Load Number
(numbered sequentially as trucks are dispatched)
EN IRONI EA74L CONSULTANT: = r, I
Cornet: Phone - . • ; : ' Fax:
GENERATOR. -
Address: bounty:
onract: Phone:
MSTE 0AIGiN.4TIONPOPVT Complete Address; .j }}; . t % 5 .- i_! _ , t � •'�k
Class &.Type of Contaminate in soil �'� . _ 7-%
SOURCE OF OONT4MIN "ION., (ex. UST or other source) —
OEWE"TORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu ofsrrbmWing analytital data (metho '
8240 and 82 70) verifying that the waste in gtmstioa does Prot ronlain organ is rons#rtuents other than those sohich -would
normally appear in analyst's of T irginpetrolrrrm product residrse, Iam swhmitting this Oerfipate o `ffaste
Const`rtreenfs. I crrt6fy that I ani fam rliar wilh the source of e ont4wination of fbe soil andfurther certify the source, to
the best ofmy knowledge, cantains no rontam inants Ober Than that listed above.
Generators Signature; Dam
TWANSPORTER:
Contact: Phone:
As the carrier, / certify that the mat+erialg desaibed above being shipped under this non -hazardous materials
maRifest art properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility dcsignatc,
Carrier Signature: Efate-,
` RUCI
TAG #: VOLUME.
TRUCK DRIVER SIGNATURE: DATE,
DESTINATIO • Emironmental Soils Inc.. 91-0 Crowder lid, Shelby. NC 23150 Dedicamd Land Application
Site Permit#S1030005
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this ,material
for treatment and/or disposal in a manner that has been authorised by the State of North Carolina.
Facility Signature:
Signature:
Date:,
Company i arne Title:
Date:
him aciliry anarylInvoice Pink/Carrier Goldenro&Generator

Environmental Soils Inc,
PCB Box 255o Lattimore, NC 28089
Rhone X4-434-0075 • Fax [phone]
Noii-Hazardous Waste Manifest # 4 14
Date Load Number
(numbered sequentially as trucks are dispatched)
ENVIRONMENTAL CONSULTNW.
Contact: Phone:_ _ - - Fax:
ENEXITOR:
Contact: Y Phone:
WSTE ORI RYWTIONPOLNE Contplete Address: s
Class tic Type of Containinate in soil
SOURCE OF COAFTA PVATION.• (ex. UST or other source)
EN Rd OR S CERTIFICATION OF MSTECONSTITUENTS: In heu of su6bmitfing analytical tiara (methwh
8240 and 8270) veryying that the waste in question does not contain organic cofastftnents other than those -which would
na rmally appear its analysis of virginpetmIeum pratlsret residue, ! am submitting this Certificate of Masie
onstiMena. I certify that am familiar w tb the source ofrontarnination o the soil andfurther certify the source, to
The hest of `my knowledge, contains no cantam marts other than that listed above.
Generators Signature:
Date;
TUNSPORTER
ontact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous matcriah
manifest are properly classified., packaged, labrled, secumed, and arc in proper condition for transport in commerce
under the applicable regtiLitions gm erning transportation, and I hereby receive this material for delivery to the
fkiiry designate.
grrier Signature: Date:
'I RUC #:
TRUCK DRIVER SIGNATURE,
TAG #:
OL L ME: -
DATE:— -
DESTMATIO - Environmental Soils Inc, 910 Crowdcx Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0100038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal hi a manner that has been authorized by the State of North Caronna.
Facility Signature: - lute:
signature: Da
Company blame Tit
WhitelFadhty canaryfInvoice Pink/Carrier Goldenro&Generator

Environmental Soils Inc.
I' S�ux 2,95,, L.atrimore, NC 2808
Phone [phone] • Fax [phone]
Non -Hazardous Wgste Manifest # 4 6 14 7
Date 1 Load Number
(nurnbercd sequentially as trucks are dispatched)
EAMONMENT4L CONSULTANT
Contact: .., Phanc: '' x5 I t - ' . Fax.
U NERATOR: ti
ounty, ' � I
Contact: - -- Phone: - -
s 0)UGLm TION POLY .- Complete Address.
glass &TYF of Contarnin2te in Boil
SOURCE OF CoNT mnUTION (ex. [SST or other source)
OENER TOI S PERT}FICATION OF As ONSTMhENTS. In lieu of a bmittirl rxrralytiraldata ( lethods
8240 and S 70) vrrx:tying that the waste in qr stion does trot contain organic ronstituen a other than these wb ch would
normally appear in analy-ris o v r in etrotearnprodrrrt resldrte, lam st�bxnittin fhis Cettrf�cate o, f Ff�uste
Constituents, I certify that I am ferririltar witb the somw of contamination of the suitandf+.rrther tertxfy the source, to
Ike best of my knowledge, contains- na rontxtnsinairts -other Than that listed above,
r
Generators Sigznature:Date:
TMNSPORTER:
Contact; Phone:
s the carrier, I certify that the materials described above being shipped under this non -hazardous mamrials
nlanifegt are properly classified, packaged, labeled, secured, and are in proper condition for transport in tOMMerce
under the appScable re abort governing transportation, :Rnd I ln=by receive this material for delivery to the
facility designate.
Ler Sig nature: Date:
sri
TRUCK TAG #:
TRUCK DRIVER SIGNATURE: DATE;
DESTMITION.- Environmental Soils Inc. 910 Crcnyder lid, Shelby, NC 2 150 Dedicated Land Application
Site Permit: #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
far treatment and/or disposal in a manner that has been authorized by the State ofNorth Carolina.
Facility Signature:
Signature:
Company Name
Date:
Title:
Date
WNtelFacility anvy/Invoice Pinv arricr olds dl enerator

Environmental Sods Inc.
-'hone,104-414-0075 • Fax [phone]
lion-flaxar&us Waste Manifest # 46148
Date4. ' Load Number
(numbemd sequentially as trucks ire t ispatched)
WMOAME TAL CONS ULTAAT.
onftCt: `• �_ _ Phone- r ,y Fax
OLNFITOR:
Address: i I- - County:
antact: -, . Phonc-
ASTE 0MLVATIONPOIAT Complete Address: _ � � l � -�
Mass &.T}pe of Contaminate in soil
SOURCE OF CONTAMIN TIOl {cx, UST or ether source) -
GENFkdTOR S CER TIFIC4 TION OF W,4STE CONSTJTUENT'rS, In lieu Ofs11GMxtthig analyliea?duta (vietb ads
8240 and 8270) veriftimg that the waste in question does not contain a ganieromfituents other t am those which would
normally appear in analysis of `v rgjn t"lerrrrj # Vdjjct residue, I am submitttng this Certficare of f#iaste
Constit"etols. I cer-t that I am familiar with tie source of romw ;natYorj o f the soil and further rent y the sourer. tv
The crest a, ray knOwled e, rarrWins im rurrru rinants alter than that lister} abogm.
Generatars Signature: . -_ Date:
TRdNSPORT :
Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest arc properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
CartierSignature: Irate:
TRUCK #:
TRUCK DRIVER SIGNATUPE
TAG #:
VOLUME:
DATE:
DESTVV,4TtON.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Lard Application
Site Permit #S R0300038
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for tmatnient and/or disposal in :t manner that, has been authorized by the State of North Carolina.
1{`acility Signature:
Signature,
Company Nun
Date:
Tide:-
Date-,
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Etiironmcntal Sails Inc.
- - _ PO &x 295-"-Lattimore, NC 28089
Phone 'A04-434-0075 - Fax [phone]
Non -14 ag-,wdous waste Manifest #46149
Date t. _ Load Number
EP4 R ONMENT11L C O S ULTAN P
Contact
OEPIE TOK
Addre
conta
(numb'cred sequentially as trucks, = dispatched}
IC.
phone: ' J _ - Fax:
WJST`E O12TOLNATIONPOL T: Complete Address:
Class &.Type of Contaminate in soil
SOURCE: 0FC0AITA IIMMON . (tx. UST or ot� er source
County: —
Phone: -
"ENF, TORS CERTIMU TION OF W,48TE CONYTTMENTS. In hers o, sub i M ng amdytica# data (methods
9240 and 82 70) wri ing that The waste in TuesAun ryes nat rontain organic mnstituents other than those wbich would
normally appear in analysis of `iv rgin petroleum product revue, I am submitting this Certificate o Waste
Constituents. I certr that I ain amiliar with the source ofcontar motion `the sail andfieriber certify thesorrrre, to
The Best ofnib+ knowledge, ronoim no ronlarninants other than that listed above.
Generators Signature: �T � Date:
TRANSPORTER:
Contact; Phone -
As the carrier, I certify that the materials described abm a being slipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, arrd are in proper condition for transport in comrncrce
under the applicahle regulations governing transportation, and I hereby receive this material for delivery to the
Facility designate
Carrier Signature: fate:
TRUC L{ #:
TRUCK DRIVER SIGNATURE:
TAG #:
VOLUME -
DATE:
DEST)N4TION.• Environmental Soils Inc. 910 Crowder lid, Shelby, NC 29150 Dedicated Land Application
Site Permit #SR0 00038
I certify that the carrier has delivered the materials described above to this facility, and L hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature: Date:
Title:
Date:
Company Narne
White/Facility canary/111voice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Bo 95 - J attimore, NC 28089
Phonc 70 43 075 • Fax [phone] d
Dion -Ha a our Wz8fe Manifest #46150
Date , Load Number �, l
(numbered sequentially as trucks are dispatched)
NF7RONMENT L CONSULT NT
Contact:
ENERdTOR:
Address:
Phone: Fax
Counzy..
Contact; Phone
WASTE ORI EVATION POINT} Complete Address:
Clash &,Type of Contaminate. in soil
SOURCE OF CONTAMINATION: (ex. LIST or other suu rce)
EVEP.dTORS CERTIFICATION OF WASTE CONSTITUENTS: In lien a f submitting analytical data (onetbods
5240 mid $ 70) verifying that The waste its question does not contoin organic constiturnIs other than those which would
normally a ear in analysis o Vlrg,'xj etro{eism mdvcT residur, lam subnritting tbls Certificate of rite
Constituents. I certify that I utrx_famihar with the source off contain nation offofibe soil and urther cerl f jF the source, to
The best of my knowledge, contains no cantandnants other Man that listed above.
Generators Signature: __ - Date:
TRANSPORTER,
Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this [ion-hwcardous materials
rnanifc;st are properly classified, packaged, labelui, secured, and are in proper condition for transport in cok�merce
under the applicable regui2tions governing transportation, acid i hereby receive Chic material for delivery to the
facility designate.
Carrier Signature: nate.,
TRUCK #;
'I RUCK DRIVER SIGNATURE.
TAG #:
VOLUME:
DATE-
DESTEV'17HON.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #S10300038
I certify that the carrier has delivered the materials described above to this facility, astd I her6y accept this material
for treatment and/or disposal in a manner that has becn authori2ed by the Mate of North Carolina.
facility Signature:
Signature:
Company Name
Date -
Title:
Kato:
hite/F"acilstyCanary/Invoice Pink/Carrier Golden rod/Generator

P.O. BOX 295
ENVIRONMENTAL SOILS, INC. LATTIMORE, N.C. 28089
704o-n434v--0075
NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL
APPROVAL # .-.,.MANIFEST#
LOCATION OF SOIL:
TRANSPORTER:
�i e�ri����?�� � fi1a(lcirvC Lrk, ���, •�. Ch�r
CNrf 4----
IN
TIME:
DATE:
TIME10
:.
A,
DATE: � � �-40oz D
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TRUCK #
LICENSE #
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TRUCK # ,J
LICENSE #
DRIVER SIGNATURE
TIME*
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MEMO —
TRUCK # K - =2 b
�" LICENSE #
DRIVER SIGNATURE
TIME:
DRIVER SIGNATURE
TRUCK# � Sy
LICENSE # -jh
rR
INSPECTED & ACCEPTED BY ENVIRONMENTAL SOILS, INC.
SUPERVISOR'S SIGNATURE �•°�` �-'
GROSS WT. 7 _— LBS&
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TARE WT.
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GROSS WT. bLBSO-
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TOTAL NET WT.
f
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TOTAL EQUIV-TONS
I.

Phone [phone]
Environmental Soils Inc.
PO'Rox 295 Lattimore NC 28089
• Fax 704-434w­9533
Non -Hazardous Waste Manifest
Date
ENVIRONMENTAL CONSULTANT
Contact0
:
liar
GENERd4TOR.6
Address:
Contact:
# 53420
Load Number
(numbered sequentially as trucks are dispatched)
Phone: � -. � - �, �" Fax:�
} 9
�7j 7 � C...- Countv.
f-AI
W..�4STE 0JUGLVj.4T10]VP01A7T.e Complete Address:
n
t 14
Class &Type of Contaminate
in soil
n e i�45 coo Ph
_mw EP-W
F2
k
AWII f
.a A[4 '
SOURCE OF CONTAMLVATION..0 (ex. UST or other source)
4 GENEIdRd4TORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods
8240 and 8270� veriying that the waste in question does not containorganic constituents other than those 2vhich would
normally ap�iear in analysis of virgpin petroleum�iroduct residue, I am suhmitting this Certificate of Waste
Constituents. I cert. thatl am familiar �zvitb the source of contamination of the sozl and furthercerit''y thesource,,#.
o
the best o my know ledge, captains no contaminants other than that listed above.
Generators Signature:' t t v�f t � ^�r� � ��n� e � � DaDate:%%MAI1
dt—MI
TRf1NSPORTER:
Contact: Phone
s the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled,
under the applicable regulations governing trans 0
facility designate.
Carrier Signature:
secured, and are in proper condition for transport in commerce
nation, and I hereby receive this material for delivery to the
Date:
TRUCK #: TAG #: VOLUME:
TRUCK DRIVER SIGNATURE: DATE:
DESTIN�ITION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated an Application
Site Permit #SR0300038
7 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature : Da te:
Signature:
Company Name
Date6
:
Title:
IF
White/Facility
Canary/Invoice Pink/Carrier Goldenrod/Generator
40or 21. lt� tw

s Inc&
Environmental Sodi L
N9 C 28089
PO Box 295 attimore7
Phone [phone] • ]Fax [phone]
on-Hazardous Waste Manifest # 53421
D
Load Nunib
ate- z
(numbered sequentially as trucks are dispathec d)
i -4;7 ENVIRONMENT 4L CONSULTANT � J 6G Z _ /9 Fax:
Contact: -� 0s +s >'u'� Phone: % t�
GEjERfITOR: Aqw/ - '`r' 1
LTCounty:� ��
` �-aAddress:o'
Contact: � :JA)
J�✓ Phone:
W4STE ORIGLV4TIONP01AYe ComPleteAddress.
C
0
LI
Class &TYP e of Contaminate in soil �� �� �L '`J
a methods
SOURCE OF CONTAMEVATIONd• (exA%.
. UST or other source) �OPP
GENERJTORS CERTIFICATION OF WASTE CONSTITUEIVI"S: In lieu ofsUbmitting analvtical those
ta svolild
8240 and 8270� veriing that the waste in question does not contain organic constituents other
normally apj�ear in analysis o virgin1ietroleum product residue, I am submitting this Certificate 0`1 Waste
onstituents. I cert� that I am familiar with the source of contamination of the soil and further certify the source, to
the best o My nowledge, contains no con taminants other than that listed above.
Pr
ate
G: I -, ft k i%=&& --."
enerators Signature _
TR"SPORTER
Phone,.
Contact: dnNNF
that the materials described above being shipped under this non -hazardous materials
As the carrier, I certi fy .8 0
manifest are properly classified, packaged, labeled, secured, and are in proper Ceive his ition
for
for delJVe LO
commerce
under the applicable regulations governing transportation, and I hereby r
,
facility designate. Date,,
Carrier Signature: d(�6 L
TRUCK #: TAG #: VOLUME: �
TRUCKDRIVER SIGNATURE:
, DATE:
eanApplication
TLVJTIONso Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicatd Ld
DE
Site Permit 00038
I materlanereaccet this ma eri
certify that the
carrier has delivered the als described above to this facility, d I hby pal
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
ate: � �~
Facty Signature:
Date:
Signature:
Title:
Company Name
C/Invoice Pink/Carrier Goldenrod/Generator
Whereaciana Flity rY

Environmental Soils Inc. ±
PO Box 295 • Lattimore, NC 28089
Phone 704-434--oOO75 • Fax 704-434-w9533
L - Non-Hazardous Waste Manifest # Al3 4 3
-� Load Number
Date- ��►
(numbered sequentially as trucks are dispatched)
%pl
to
ENVLRONM CONSULTANT:
�—�A i . .Y. Phone@9
�.i - ���` Fax:
Contact: ._
T - F -
County:
m...
Address:
Phone:-
Contact: �1 its � Plel
WISTE ORIGINfITIONPOINT.' Complete Address: y � Z
a ,n 0.7 �
Class &Type of Contaminate in soil � � � � �
SO URCE OF CONTAMINATION.• (ex. UST or other source)
r
metho&
GEIERl4TORIY
S CERTIFICATION OF WASTE'CONSTITUENTS.*In lieu of suhmi.....Ung anafhose �w0t(111A tical data would
0
8240 and 8270� verifying that the waste in question does not contain organic constztuents
normally appear in anaivsis of virgin1ietroleumgroduct resiti'lue.) I am submItutngo11Pil andthis et� the source, to
onstituents. I ceatlamfamiliar �zvith the source ofcontamination of the,fu
the best o my knowilet'',ge, co� `ns o ontaminants other than that listed above.
,�� •� -1 Date:
Generators Signature:
0000l
T"NSPEll
ORTER:
Phone.
Contact:
As the carrier, I certify that the in aterialaterl
s described above being shipped under nation for'''ransuort in commerce
Manifest are properly classified, Packaged, labeled, secure and I erebyan aire in ro
receive this materlal for delivery tot e
under the applicable regulations governing trans ortatio
facility d'I
esignate. Date:
Carrier Signature:
TAG #: VOLUME: �3 S b c�
TRUCK #: DATE:.
TRUCK DRIVER SIGNATURE:
ntal Soils Inc. 910 Crowder Rd, Shelby, NC 28150 edic
nvironmeecl LandCation
DESTIN�ITI01V E
Site ermit #SR0300038
I certify that the carrier has elivered
the naterials described a
ove to this facility, and I hereby accept this material
norisosain mnrtt haseen autorizey te tate oortaroina.
or treatmentapc-N.,
Date: � �
Facility Signature: -Owl
Date.-
ignature: Title:
Company Name
oldenroenerator
ite/Facility anary/Invoice
Pink/Carrier GdlG

•.4
Environmental Soils Inc.
PO Box 295 •Lattimore, NC 28089
Phone 704 4 4 oo75 • Fax [phone]
533 �
'ry Non -Hazardous Waste Manifest # 53422
�Date Load NumberWOO
(numbered sequentially as trucks are dispatched)
EAWRONMEAT�iL CONSULTANT:Ar
�
CIA6,r Phone,,• 3 - 27 v � �7�Fax:
ontact: � �_� S. err
GENEJUTOR.
Address: �r
Contact:
WAIST
E 0R1GIJV..,4T10NP0VVT.1* Complete Address
Class &Type of" Contaminate in soil
SOURCE OF COAPMMLVATION: (ex. UST or other source)
s 6a
County:
Phone: ? v`i- 3 %a mow, �
oe
a
GENERJTORS CERTIFICATION OF WAST� C01STITUENTS: In Iieu of submitting analytical data (methods
8240 and 8270� ve.ifying that the waste in question does not contain organic constituents other than those whicb would
normally appear in an alysis of virgpin�ietroleum product residue, I am submitting this Certificate o Waste
Constituents. Ice rt� thatl amfamilioar with the source o contamination of the soil and further certify the source., to
the best o my kn o�zvtedge, contains no contaminants other than that listed above.
Generators Signature:
L
TRfINSPORTER
T
Phone:
Date
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
TRUCK DRIVER SIGNATURE:
}
Date:
DATE:
DESTIN�ITION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materlals described above to this facility, and I hereby accept this material
for treatment an or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Date:
Title:
Date:
rr
Goldenrod/Geneato
iite/Facility
an-ar nvoice
Pink/Carrier

APPENDIX D
Liquids Disposal Manifests

It is unknown if liquids were removed from the UST System

APPENDIX E
UST Certificate of Disposal

ED • •
CANDLINR INPIRONMENTRI 11SPON51 TINA
Emergency Response: 877-505-6799
PO Box 681016
Charlotte, NC 28216
Phone: [phone]
Fax: [phone]
www.cert-usa.com
CERTIFICATE OF DISPOSAL
Tank # 2190325-1
For: John Adams Property
934 W. Mallard Cr. Church Rd.
Charlotte, NC
Tank Size: 1 ea.- 285 gal steel tank
This is to certify that the above tank has been disposed of in accordance
with EPA regulations on Petroleum Tank Disposal.
The tank was removed to: Auto Parts U Pull and Scrap Metal of Charlotte
9820 Statesville Road
Charlotte, NC 28269
Disposal Method: emptied, cleaned, cut for scrap metal
Date: 3/13/19
Certified By: Lee S h a V1JZ Date: 3/25/19

APPENDIX F
24-Hour Release and UST Leak Reporting Report

2 Hour gm a" and 03'1' • '"`r�
,�
For Releases This form should be completed and submitted to the UST Section's regional office followinga known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
In NC suspected release
(DWM USE ONLY)
Suspected Contamination? (Y/N) ___ _?__
Facility ID Number
Incident tY Risk (H,I,L,U)
Confirmed GW Contamination? (Y/N) ��l/ _
Date L Dlsoov re _ _—_—
Received On Received By
Confirmed Soil Conlamina)ion ?(Y/N)
Com on-Commercial_;�
Reported by (cinde one): Phone, Fax or Report
Samples Taken?(YIN) �_
-Co
Reg on-regula e ---------
Region
Free Product? (Y/N) __&I_ If Yes, State Greatest
Thickness 4-1
INCIDENT DESCRIPTION
Incident Name: jam\ /y 1
�
Address: L` r�'C
County: fY\ I2iL Iy.. 1z'
City/Town: C� ����
Zip Code: �f �.
Regional Office (circle one): Asheville, ooresville Fayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Lau tude{ded"degrees): Longitude (declmWdogreim) :
Obtained by:
❑ GPS
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release amount of free product present and recovery efforts, initial responses conducted impacts to receptors)
❑ Topographic map
`'\ Z,
v�� r O Y�� O� 1
❑ GIS Address matching
` C►�\1 0-�
❑ Other
U Unknown
Dcscribe location:
�p n
HOW RELEASE WAt DISCOVERE (Release Code) 1w�t, .� ;N%'t ,
(Check one)
❑ Release Detection Equipment or Methods U Visual/Odor ❑ Groundwater Contamination
During UST Closure/Removal ❑ Water in Tank ❑ Surface Water Contamination
Property Transfer ❑ Water Supply Well Contamination ❑ Others cif
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Tme Released
(Check one to indicate primary (Check one to indicate primary (Check one) (Check one to indicate primary product type
source) cause) released)
Tank ❑ Spill petroleum ❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil
Kerosene Blend
❑ Piping ❑ Overfill U Non -Petroleum
%Hoaling Oil U Vogetablo Qil 100%
❑ Dispenser Corrosion U Both ❑ Other Petroleum ❑ E 10 - E20
❑ Submersible Turbine Pump ❑ Physical or Mechanical Products
U E21 E84
-
Damage Location ❑ Metals
❑ Delivery Problem ❑ Install Problem (Check one) ❑ Other Inorganics U E85 - E99
❑ Other ❑ Other ❑ Other Organics ❑ Ethanol 100%
❑ Facility
❑ Unknown
❑ Unknown INLResidence ❑ E01 - E09
Definitions presented on reverse Definitions presented on reverse ❑ Other
Ownershio
1. Municipal 2. Military 3. Unknown . Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. idential 4. Education/Relig. 5. industrial 6. Commercial 7. Mining
UST Form 61 (02/08) Page 1 of 2
04N-�

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1.
Yes 2. No �Ukn
Number of Water Supply Wells Affected ______________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
»>
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Point of Contact
Address
City
State
Zip Code
Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company
Address
City
State
Zip Code
Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner
Address
City
<r �`���
State
�,
Zip Code
Z�Z��,
Telephone Number
'7oq,17( L)
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident
Company
Telephone Number
Title <
1\ '� to
Address �t'J
Date
uS i rorm Cl timmu) r Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or subrrsible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser. includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during pniduct delivery to the tank. (Typical causes associated with this source are spills and overfills )
Other: serves as the option to use when the release source is known but does"not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nuzzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into nionnoring wells)
Unknown: use when the cause has not been determined

APPENDIX G
Provided Groundwater
Information

January 6, 2020
Flournoy Development Group
1100 Brookstone Centre Parkway
Columbus, Georgia, 31904
Attention: Mr. Luke Addison
[e-mail]
Reference: Limited Groundwater Assessment Letter Report
934 West Mallard Creek Church Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 4335-19-181
Dear Mr. Addison:
S&ME, Inc. (S&ME) respectfully submits this Limited Groundwater Assessment Letter Report to summarize and
document the field activities and findings of a groundwater sampling event conducted at the property at 934
West Mallard Creek Church Road in Charlotte, Mecklenburg County, North Carolina. The work of this project was
outlined in our proposal (S&ME 43-1900956) to the Flournoy Development Group dated and authorized on
December 17, 2019.
Project Background
In August 2017, S&ME completed a Phase I Environmental Site Assessment (ESA) Report on the properties located
at 900 and 934 West Mallard Creek Church Road in Charlotte, North Carolina. The target property of the August
2017 Phase I report was comprised of two Mecklenburg County tax parcels (02965101, 02965102), and the
property contained approximately 25.05 acres. S&ME's August 2017 Phase I Report identified one recognized
environmental condition (REC), which was an existing heating oil underground storage tank (UST) at the residence
at 934 West Mallard Creek Church Road.
In October 2019, the Flournoy Development Group contracted with S&ME to perform a Phase I ESA on the
properties located at 900 and 934 West Mallard Creek Church Road. During the performance of the new Phase I
assessment, it was reported that the heating oil UST at 934 Mallard Creek Church Road had been removed and
that a release from the tank was identified. Information provided by Ryan Osborne of Inenco, Inc. (Inenco) of
Mooresville, North Carolina indicated that approximately 225 tons of petroleum impacted soil was removed from
the property for disposal at Environmental Soils in Lattimore, North Carolina. The depth of the excavation in the
area of the former heating oil UST was reported to be approximately 17 to 18 feet below ground surface (BGS). A
copy of the information provided to S&ME by Inenco is included in Attachment A.
S&ME, Inc. 19751 Southern Pine Boulevard I Charlotte, NC 28273 1 p 704.523.4726 1 www.smeinc.com

Limited Groundwater Assessment Letter Report
�—� 934 West Mallard Creek Church Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No.4335-19-181
During previous geotechnical drilling activities performed by S&ME at the subject property, groundwater was
encountered in some of the geotechnical borings at depths between 15 and 20 feet BGS. As a result of the
reported heating oil UST release and the possibility of shallow groundwater in the area of the former US pit, the
Flournoy Development Group retained S&ME to conduct a limited groundwater assessment in the area of the
former heating oil UST at the subject property to assess the absence or presence of petroleum groundwater
impact.
Site and Project Description
The subject property is an approximate 3.7 acre property located at 934 West Mallard Creek Church Road in
Charlotte, Mecklenburg County, North Carolina. The subject property is identified as Mecklenburg County tax
parcel 02965101, and it is developed with a residence and a garage. The residence is currently vacant. The
subject property is located in an area characterized by a mixture of residential homes and undeveloped land.
Interstate 85 is located approximately 500 feet to the west of the subject property. A Site Vicinity map is provided
as Figure 1.
The purpose of this project was to conduct a limited groundwater assessment in the area of the former heating oil
UST at the subject property to assess the absence or presence of petroleum groundwater impact.
Limited Groundwater Assessment
Limited groundwater sampling activities were conducted on December 18 and 19, 2019.
Field Activities
One temporary groundwater monitoring well (TW-1) was installed at the subject property on December 18, 2019.
The temporary well was installed to an approximate depth of 29 feet below ground surface (BGS). The boring was
advanced to a depth of approximately 23 feet using hollow stem augers until refusal was encountered. The
boring was then advanced to an approximate depth of 29 feet using air rotary drilling. A temporary well with 20
feet of two-inch diameter PVC mill -slotted screen and nine feet of two-inch diameter PVC riser was installed in the
borehole. A sand pack was installed around to the screen section to a depth of approximately seven feet BGS, and
then bentonite was installed to approximately five feet BGS. Well drilling was conducted by Ransier Environmental
Drilling (Ransier) of West End, North Carolina. Ms. Kelsey Murphy of S&ME provided oversight of the drilling and
well installation. The approximate location of temporary well TW-1 is indicated on Figure 2. A Boring Log and a
Well Construction Record for TW-1 are included in Attachment B.
After allowing a day for groundwater to recharge into the temporary well, TW-1 was sampled on December 19,
2019 by S&ME. Depth to groundwater in TW-1 prior to purging was 17.05 feet BGS. The well was purged and
sampled by S&ME utilizing a submersible pump equipped with new tubing. The groundwater sample was
collected in laboratory supplied sample containers. A sample was collected from TW-1 for certified laboratory
analysis for benzene, toluene, ethylbenzene and xylenes (BTEX) plus naphthalene by EPA Method SM6200B, for
semi -volatile compounds (SVOCs) by EPA Method 625.1, and for volatile and extractable petroleum hydrocarbons
by MADEP VPH and EPH.
January 6, 2020

Limited Groundwater Assessment Letter Report
934 West Mallard Creek Church Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 4335-19-181
After collection, the samples were labeled as to sample identification, analysis, sample date and time and were
placed in a cooler with ice. The samples were delivered under chain of custody procedures to Waypoint Analytical
in Charlotte, North Carolina for chemical testing.
TW-1 was abandoned by Ransier on December 28, 2019. To complete well abandonment, the PVC screen and
casing were removed from the ground, and the boring was backfilled to the ground surface with bentonite pellets
and a neat cement slurry. Ransier's well abandonment record is included in Attachment B.
Analytical Testing
Analytical testing of groundwater sample TW-1 by EPA Method SM6200B indicated the presence of Benzene and
Naphthalene at concentrations in excess of their respective 15A NCAC 2L .0202 groundwater quality standards (2L
Standards). Ethylbenzene, Toluene and Total Xylenes were reported at concentrations above laboratory detection
limits but below their respective 2L Standards.
Analytical testing of groundwater sample TW-1 by EPA Method 625.1 indicated the presence of 2-
Methylnaphthalene and Naphthalene at concentrations in excess of their respective 2L Standards. 1-
Methylnaphthalene was reported at a concentration in excess its North Carolina Interim Maximum Allowable
Groundwater Concentrations (IMAC). 3/4-Methylphenol was reported above laboratory detection limits, and it
does not have a 2L Standard or an IMAC. Phenol was reported at a concentration above laboratory detection
limits but below its 2L Standard. No other EPA Method 625.1 target compounds were reported at concentrations
above laboratory detection limits.
Analytical testing of groundwater sample TW-1 by MADEP VPH/EPH indicated the presence of C9-C10 Aromatics
and C11-C22 Aromatics at concentrations equal to or above their respective 2L Standards. C5-C8 Aliphatics, C9-
C12 Aliphatics, C9-C18 Aliphatics and C19-C36 Aliphatics were reported at concentrations in excess of laboratory
detection limits but below their respective 2L Standards.
The analytical results are summarized in Table 1. A copy of the laboratory report is provided in Attachment C.
Summary and Conclusions
Summary
The following summarizes the work during this project:
One temporary monitoring well (TW-1) was installed on the subject property by S&ME on December 18,
2019.
S&ME collected a groundwater sample from TW-1 on December 19, 2019. The sample was submitted to
Waypoint Analytical in Charlotte, North Carolina for analysis for BTEX plus naphthalene by EPA Method
SM620013, for SVOCs by EPA Method 625.1, and for volatile and extractable petroleum hydrocarbons by
MADEP VPH and EPH.
January 6, 2020

s
=
Limited Groundwater Assessment Letter Report
934 West Mallard Creek Church Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 4335-19-181
Analytical testing indicated the presence of Benzene, Naphthalene, 2-Methyl naphthalene, VPH C9-C10
Aliphatics and EPH C11-C22 Aliphatics at concentrations equal to or above their corresponding 2L
Standards. 1-Methyl naphthalene was reported at a concentration in excess its IMAC. 3/4-Methyl phenol
was reported above laboratory detection limits, and it does not have a 2L Standard or an IMAC. No other
target compounds were reported at concentrations in excess of applicable North Carolina groundwater
standards.
Conclusions
Laboratory results for the chemical testing of the groundwater sample collected during this assessment indicates
that the groundwater in the area of the former heating oil UST at the subject property has been impacted by
dissolved petroleum constituents.
Recommendations
With respect to the Phase I ESA report recently conducted on the subject property by S&ME, the presence of
petroleum contaminated groundwater in the area of the former heating oil UST pit confirms that a REC remains at
the site. The petroleum release will have to be closed by the NCDEQ for the REC to be resolved.
Based on the presence of dissolved petroleum constituents in the groundwater at the subject site at
concentrations greater than 2L Standards, S&ME recommends that a copy of this report be provided to the
current property owner.
Closure
If you have any questions concerning this report, please contact us at your convenience.
Sincerely,
s&ME, Inc.
Carl Hewett
Senior Project Manager
704-351-4448
[e-mail]
Tom Raymond, P.E.
Senior Environmental Engineer
919-954-6229
[e-mail]
January 6, 2020 4

f� +
Figures
Figure 1:
Figure 2:
Tables
Table 1:
Attachments
Site Location Map
Well Location Map
Summary of Groundwater Analytical Results
Attachment A: Inenco Supplied Information
Attachment B: Temporary Monitor Well Documentation
Attachment C: Waypoint Analytical Laboratory Report
Limited Groundwater Assessment Letter Report
934 West Mallard Creek Church Road
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 4335-19-181
January 6, 2020

Figures

Tables

TABLE 1: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
934 West Mallard Creek Church Road
Charlotte, North Carolina
S&ME Project No. 4335-19-181
TW-1
NCDEQ 2L
Standards
EPA Method SM62008
Benzene
6.8
1
Ethylbenzene
0.73 J
600
Naphthalene
78
6
Toluene
0.36 J
600
Total Xylenes
1.2 J
500
EPA Method 625.7
1-Methyl naphthalene
21
1
2-Methyl naphthalene
38
30
3/4- Methyl phenol
120
INS
Naphthalene
41
6
Phenol
8.7 J
30
MADEP VPH / EPH
VPH C5-C8 Aliphatics
46 J
400
VPH C9-C12 Aliphatics
200
700
VPH C9-C10 Aromatics
200
200
EPH C9-C18 Aliphatics
520
700
EPH C19-C36 Aliphatics
500 J
10,000
EPH C11-C22 Aromatics
400
200
Notes:
• Analytical results presented in micrograms per liter (ug/L).
• J = results detected below the reporting limit, reported concentrations are estimates.
• NCDEQ 2L Standards — North Carolina Department of Environmental Quality 15A NCAC 2L
Groundwater Standards
• * - NCDEQ Interim Maximum Allowable Groundwater Concentrations
• INS — no standard established
• Results in red and bold are concentrations at or above applicable North Carolina action levels.
• Groundwater sample collected on December 19, 2019 by S&ME.
• Analytical testing by Waypoint Analytical of Charlotte, North Carolina.

Attachment A
Inenco Supplied Information

Carl Hewett
From:
Sent:
To:
Subject:
Attachments:
Sent from my iPhone
Begin forwarded message:
Patrick Laatsch
Wednesday, December 18, 2019 7:39 AM
Carl Hewett
Fwd: 24 HR Notice Adams Property at 934 West Mallard Creek Church Rd.
image001 jpg; ATT00001.htm; Soil Removal Summary W Mallard Creek.pdf,
ATT00002.htm
From: "[e-mail]" <[e-mail]>
Date: December 16, 2019 at 11:54:36 AM EST
To: Patrick Laatsch <[e-mail]>
Subject: RE: 24 HR Notice Adams Property at 934 West Mallard Creek Church Rd.
Reply -To: <[e-mail]>
Sorry for my delay,
I put this job on hold and hadn't made a site drawing yet.
Please let me know if I you need anything else for me.
Ryan R. Osborne, PE
INENCO, Inc.
132 W. Statesville Ave.
Mooresville, NC 28115
Office: 704-662-8192
Fax: [phone]
Mobile: [phone]
Note: Please be sure that [e-mail] is the email address you are using for me.
From: Patrick Laatsch <[e-mail]>
Sent: Tuesday, December 10, 2019 4:00 PM
To: [e-mail]
Subject: RE: 24 HR Notice Adams Property at 934 West Mallard Creek Church Rd.
Hi Ryan
Can you please provide a sample location map? As well as the dimensions of the excavation, and the
amount of soil removed from the site?
Thanks in advance
1

Patrick Laatsch
Senior Project Manager
Charlotte Environmental Dept. Group Leader
S&ME, Inc.
704.618.7147
From: [e-mail] <[e-mail]>
Sent: Tuesday, December 10, 2019 9:42 AM
To: 'Beverly, Trudy' <[e-mail]>
Cc: Patrick Laatsch <[e-mail]>
Subject: FW: 24 HR Notice Adams Property at 934 West Mallard Creek Church Rd.
Trudy,
My apologies for being slow to get back to you. This job is still on hold. I spoke to the realtor
([e-mail]) earlier this week, and he made it sound like something was going to
move soon. I'm not sure of the details, but I have been asked to provide some information to
folks doing a Phase I ESA on the property. ( I have CC'ed them on this email)
I have attached the sample results as they stand. If anyone has any questions I can answer,
will be happy to do so.
Ryan R. Osborne, PE
INENCO, Inc.
132 W. Statesville Ave.
Mooresville, NC 28115
Office: 704-662-8192
Fax: [phone]
Mobile: [phone]
Note: Please be sure that [e-mail] is the email address you are using for me.
From: Steve Hamilton <[e-mail]>
Sent: Monday, March 25, 2019 9:19 AM
To: 'Beverly, Trudy' <[e-mail]>
Cc: [e-mail]; 'Ryan Osborne' <[e-mail]>; [e-mail]
Subject: 24 HR Notice Adams Property at 934 West Mallard Creek Church Rd.
Trudy Beverly
NCDEQ
Trudy,
Attached please find the 24 HR Notice for Adams Property at 934 West Mallard Creek Church Rd.
Charlotte, NC.
Regards,
Steve

Steve Hamilton- Consultant
C.E.R.T.
Carolina Environmental Response Team
PO Box 681016
Charlotte, NC 28216
704-309-4262 cell
877-505-6799 office

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Attachment S
Temporary Monitor Well Information

LOG OF SOIL BORING TW-1 ■.w
WITH MONITOR WELL CONSTRUCTION NOTES
PROJECT NAME: West Mallard Creek Church Road
DATE DRILLED: 12/18/19 LOGGED BY: K. Murphy
DRILLING METHOD: 3 1/4 Solid Stem Auger DRILLER: Ransier Environmental
DEPTH TO WATER: 16.80 LATITUDE: N/A
TOC ELEVATION: N/M LONGITUDE: N/A
ELEVATION
(ft.)
LITHOLOGY
Description
FID (ppm)
Well
Construction
Well
Description
DEPTH (ft.)
0
0
- -
Topsoil: Organics
SILT: Brown; wet, in perch water
_-_-
. _
'
Open Hole
— . — .
8.54
-_-_
Sch. 40 PVC Casing
Bentonite
Clayey SILT: Tannish Brown; wet
—
o0 0 o c
0 0 000
85.32
-10
-10
'.T.' '.T.' ' T.
T T T T T
T.T. TT T
T.T. TT T
TTTTT11.33
T.T. TT T
T.T. TT T
T.T. TT T
T.T. TT T
T.T. TT T
T T
Silty SAND: Greyish Brown; slightly moist, strong odor
—
o0 0 o 0
.............................................:
-15
-20
-15
-20
T T T
TT T..T.T T
T T T T T
TTTTT
TTTTT
T T T T T
TT' T
T T T T
T T'Aid#2
TTTTT
'.T.
TTTTT
7..T-7
'T..T...T... T TTTTT
TTT
'T TT T.T
.T.' '-7 .T.
..........
Silty SAND: Light Brown; some rock fragments,
slightly moist, strong odor. Refusal on top of rock at
23
5.82
—
c c c o
O O 00
O
Static Water Level
Filter Sand
Sch. 40 0.010" SI. PVC
Screen
'.
4.37
vi
QNn O
O
................................
Ln
O
OO
...........
4 '
QD
Rock: White dust; in rock
-25
-25
O�
0
Q� ...
OoOQ
av, o in o
o0 0 0
O O 00
0
o�
ro o
NOTES: Auger refusal on top of rock at 23', switched to Air Rotary.

WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
For llmenlal Use ONLY,
1. Well Contractor Information:
Bryan L Vest
Well Contractor Name
3580-A
NC Well Contractor Certification Number
Ransier Environmental Drilling Inc (REDI)
Company Name
2. Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3. Well Use (check well use):
Water Supply Well:
❑Agricultural
❑Geothermal (Heating/Cooling Supply)
❑ Industrial/Commercial
❑ imgation
Non -Water Supply Well:
❑Municipal/Public
❑Residential Water Supply (single)
❑Residential Water Supply (shared)
Injection Well:
❑Aquifer Recharge
❑Groundwater Remediation
❑Aquifer Storage and Recovery
❑Salinity Barrier
❑Aquifer Test
❑Stormwater Drainage
❑Experimental Technology
❑Subsidence Control
❑Geothermal (Closed Loop)
❑Tracer
❑Geothermal (Heating/Cooling Return)
❑Other (explain under #21 Remarks)
4. Date Well(s) Completed: 12/18/2019Well ID# TW-1
5a. Well Location:
Flournoy 934 W Mallard Crk Ch Ph II
Facility/Owner Name Facility ID# (if applicable)
934 'West Mallard Creek Church Road, Charlotte, NC 28262
Physical Address, City, and Zip
Mecklenburg
County Parcel Identification No. (PIN)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
35019'55.49" N 80044'27.64" W
6. is (are) the well(s): ❑Permanent or OTemporary
7. Is this a repair to an existing well: ❑Yes or ONo
If this is a repair, Jill out known swell construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: 1
For multiple injection or non -water supply wells ONLY with the same construction, you can
submit one form.
9. Total well depth below land surface: 29 (ft.)
For multiple wells list all depths ij different (example- 3(a)200' and 2L100')
10. Static water level below top of casing: 16.8 (ft.)
Ifwater level is above casing, use "+"
11. Borehole diameter: 5 (in.)
12. Well construction method: Rotary Air Hammer
(i.e. auger, rotary, cable, direct push, etc.)
14. WATER ZONES
FROM
TO
DESCRIPTION
ft.
ft.
Pt.
ft.
15. OUTER CASING (for multi -cased wells) OR LINER (if applicable)
FROM
TO
DIAMETER
THICKNESS
MATERIAL
ft.
ft.
in.
16. INNER CASING OR TUBING eother al closed -loop)
FROM
TO
DIAMETER
THICKNESS
MATERIAL
0 et.
9 ft.
2 i"
SCH 40
PVC
ft.
ft.
in.
17. SCREEN
FROM
TO
DIAMETER
SLOT SIZE
THICKNESS
MATERIAL
9 ft
29 ft'
2 in.
0.010
SCH 40
PVC
ft.
ft,
in.
18. GROUT
FROM
TO
MATERIAL
EMPLACEMENT METHOD & AMOUNT
5 ft
7 ft
Bentonite
Pour
ft.
ft.
19. SAND/GRAVEL PACK if applicable)
FROM
TO
MATERIAL
EMPLACEMENT METHOD
7 ft.
29 ft.
#3 Gravel
Pour
ft.
ft.
20. DRILLING LOG attach additional sheets if necessary)
FROM
TO
DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
0 ft
5 ft.
Brown Silt
5 ft.
10 ft.
Tan/Brown Clayey Silt
10 ft
15 ft
Grey/Brown Silty Sand
15 ft
23 ft
Tan/Brown Weathered Rock
23 rt.
29 ft.
Grey Rock
ft.
ft.
ft.
ft.
21. REMARKS
22. Ctr(lllcutlon:
13 aC#fr tl12/30/2019
Signaj�ft of Certified Well Contractor Date
By signing this form, I hereby certify that the wells) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Iniection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636
13a. Yield m Method of test: 24c. For Water Supply & Injection Wells:
(gP ) Also submit one copy of this form within 30 days of completion of
13b. Disinfection type: Amount: well construction to the county health department of the county where
constructed.
Form GW-1 North Carolina Department of Environment and Natural Resources - Division of Water Resources Revised August 2013

WELL ABANDONMENT RECORD
1. Well Contractor Information:
Bryan L Vest
Well Contractor Name (or well owner personally abandoning well on his/her property)
3580-A
NC Well Contractor Certification Number
Ransier Environmental Drilling, Inc. (REDI)
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) ifknown
3. Well use (check well use):
Water Supply Well:
❑Agricultural
❑Geothermal (Heating/Cooling Supply)
❑ Industrial/Commercial
❑ Irrigation
Non -Water Supply Well:
❑Aquifer Recharge
❑Aquifer Storage and Recovery
❑Aquifer Test
❑Experimental Technology
❑Geothermal (Closed Loop)
❑Geothermal (Heating/Cooling
4. Date well(s) abandoned:
❑Municipal/Public
❑Residential Water Supply (single)
❑Residential Water Supply (shared)
❑Groundwater Remediation
❑ Salinity Barrier
❑Stormwater Drainage
❑Subsidence Control
[-]Tracer
❑Other (explain under
12/28/2019
5a. Well location:
Flournoy 934 W Mallard Crk Ch Ph II
For Internal Use ONLY:
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): N/A (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
111 Neat Cement Grout
IN Bentonite Chips or Pellets
❑ Sand Cement Grout
❑ Dry Clay
❑ Concrete Grout
❑ Drill Cuttings
❑ Specialty Grout
❑ Gravel
❑ Bentonite Slurry
❑ Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
Bentonite Approx. 15 Pounds
Cement Approx. 5 Gallons
7g. Provide a brief description of the abandonment procedure:
Pull out pipe.
Slow pour bentonite pellets.
Slow pour or tremie pipe neat cement slurry.
Facility/Owner Name Facility ID#(ifapplicable)
a.Certillcatlon:
934 'West Mallard Creek Church Road, Charlotte, NC 28262
5 "& 12/30/2019
Physical Address, City, and Zip
Sign re of Certified Well Contractor or Well Owner Date
Mecklenburg
By signing this form, !hereby certify that the wells) was (were) abandoned in
County Parcel Identification No. (PIN)
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
Sb. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(ifwell field, one lat/long is sufficient)
9. Site diagram or additional well details:
35019'55.49" 80°44'27.64"
You may use the back of this page to provide additional well site details or well
N W
abandonment details. You may also attach additional pages if necessary.
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
SUBMITTAL INSTRUCTIONS
Attach well construction record(s) ifavailable. For multiple injection or non -water supply wells
ONLY with the same construction/abandonment, you can submit one form.
10a. For All Wells: Submit this form within 30 days of completion of well
6a. Well ID#: TW-1
abandonment to the following:
Division of Water Resources, Information Processing Unit,
6b. Total well depth: 29 (ft.)
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Iniection Wells: In addition to sending the form to the address in 10a
6c. Borehole diameter: 5 (in)
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
6d. Water level below ground surface: 16.8 (ft.)
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
N/A
6e. Outer casing length (if known): (ft.)
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
6f. Inner casing/tubing length (if known): 9 (ft.)
abandoned.
6g. Screen length (if known): 20 (ft.)
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016

Attachment C
Waypoint Analytical Laboratory Report

Case Narrative
Way poi n
ANALYTICAL
S&ME, Inc - Charlotte
Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: W. Mallard Creek Church Rd.
Lab Submittal Date: 12/19/2019
Work Order: 9120335
12/26/19 13:52
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a,--Itl
Angela D. Overcash
Project Management Manager
Data Qualifiers Key Reference:
Reviewed By Angela D. Overcash
Project Management Manager
A Surrogate recovery is below range due to sample matrix.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 15

Sample Receipt Summary
Way iin
ANALYTICAL
12/26/2019
Work Order: 9120335
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
TW-1 9120335-01 Water 12/19/19 10:15 12/19/19 13:15
Samples were received in good condition at 3.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 15

Wayi n
AtxJALYT�A�
Summary of Detections
12/26/2019
Work Order: 9120335
Waypoint ID
Client ID
Parameter
Method
Result
Units
9120335-01
TW-1
C9-CI8 Aliphatics
MADEP EPH
520
ug/L
9120335-01
TW-1
C19-C36 Aliphatics
MADEP EPH
500 J
ug/L
9120335-01
TW-1
C1 1 -C22 Aromatics
MADEPEPH
400
ug/L
9120335-01
TW-1
1-Methylnaphthalene
625.1
21
ug/L
9120335-01
TW-1
2-Methylnaphthalene
625.1
38
ug/L
9120335-01
TW-1
3/4-Methylphenol
625.1
120
ug/L
9120335-01
TW-1
Naphthalene
625.1
41
ug/L
9120335-01
TW-1
Phenol
625.1
8.7 J
ug/L
9120335-01
TW-1
Benzene
SM6200 B
6.8
ug/L
9120335-01
TW-1
Ethylbenzene
SM6200 B
0.73 J
ug/L
9120335-01
TW-1
m,p-Xylenes
SM6200 B
0.24 J
ug/L
9120335-01
TW-1
Naphthalene
SM6200 B
78
ug/L
9120335-01
TW-1
o-Xylene
SM6200 B
1.0
ug/L
9120335-01
TW-1
Toluene
SM6200 B
0.36 J
ug/L
9120335-01
TW-1
Xylenes, total
SM6200 B
1.2 J
ug/L
9120335-01
TW-1
C5-C8 Aliphatics
MADEP VPH
46 J
ug/L
9120335-01
TW-1
C9-C12 Aliphatics
MADEP VPH
200
ug/L
9120335-01
TW-1
C9-C10 Aromatics
MADEP VPH
200
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 15

Laboratory Report
Way i �
12/26/2019
AJALYTIAL
S&ME, Inc - Charlotte
Project:
W. Mallard Creek Church Rd.
Client
Sample ID: TW-1
Attn: Carl Hewett
Sample
ID: 9120335-01
9751 Southern Pine Blvd.
Work
Order: 9120335
Charlotte, NC 28273
Sample
Matrix: Water
Time Collected:
12/19/19 10:15
Time Submitted:
12/19/19 13:15
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
520
ug/L
360
24
1
MADEP EPH 12/23/19 22:49
ZRC
P9L0367
C19-C36 Aliphatics
500 J
ug/L
520
130
1
MADEP EPH 12/23/19 22:49
ZRC
P9L0367
C11-C22 Aromatics
400
ug/L
260
84
1
MADEP EPH 12/23/19 22:49
ZRC
P9L0367
Surrogate
Recovery Control Limits
1-Chlorooctadecane
40 %
40-140
o-Terphenyl
41 %
40-140
2-Fluorobiphenyl
75 %
40-140
2-Bromonaphthalene
105 %
40-140
Semivolatile Organic Compounds by GUMS
1,2,4-Trichlorobenzene
BRL
ug/L
11
3.1
1
625.1
12/20/19 19:39
JMV
P9L0395
1,2-Dichlorobenzene
BRL
ug/L
11
2.6
1
625.1
12/20/19 19:39
JMV
P9L0395
1,3-Dichlorobenzene
BRL
ug/L
11
4.1
1
625.1
12/20/19 19:39
JMV
P9L0395
1,4-Dichlorobenzene
BRL
ug/L
11
4.3
1
625.1
12/20/19 19:39
JMV
P9L0395
1-Methyl naphthalene
21
ug/L
11
3.8
1
625.1
12/20/19 19:39
JMV
P9L0395
2,4,6-Trichlorophenol
BRL
ug/L
21
4.8
1
625.1
12/20/19 19:39
JMV
P9L0395
2,4-Dichlorophenol
BRL
ug/L
11
2.8
1
625.1
12/20/19 19:39
JMV
P9L0395
2,4-Dimethylphenol
BRL
ug/L
11
5.1
1
625.1
12/20/19 19:39
JMV
P9L0395
2,4-Dinitrophenol
BRL
ug/L
53
12
1
625.1
12/20/19 19:39
JMV
P9L0395
2,4-Dinitrotoluene
BRL
ug/L
11
4.4
1
625.1
12/20/19 19:39
JMV
P9L0395
2,6-Dinitrotoluene
BRL
ug/L
21
4.1
1
625.1
12/20/19 19:39
JMV
P9L0395
2-Chloronaphthalene
BRL
ug/L
21
4.9
1
625.1
12/20/19 19:39
JMV
P9L0395
2-Chlorophenol
BRL
ug/L
11
2.9
1
625.1
12/20/19 19:39
JMV
P9L0395
2-Methyl naphthalene
38
ug/L
11
4.4
1
625.1
12/20/19 19:39
JMV
P9L0395
2-Nitrophenol
BRL
ug/L
11
2.7
1
625.1
12/20/19 19:39
JMV
P9L0395
3,3'-Dichlorobenzidine
BRL
ug/L
11
4.1
1
625.1
12/20/19 19:39
JMV
P9L0395
3/4-Methyl phenol
120
ug/L
11
2.6
1
625.1
12/20/19 19:39
JMV
P9L0395
4,6-Dinitro-2-methylphenol
BRL
ug/L
53
12
1
625.1
12/20/19 19:39
JMV
P9L0395
4-Bromophenyl phenyl ether
BRL
ug/L
21
4.6
1
625.1
12/20/19 19:39
JMV
P9L0395
4-Chloro-3-methylphenol
BRL
ug/L
11
3.1
1
625.1
12/20/19 19:39
JMV
P9L0395
4-Chloroaniline
BRL
ug/L
11
3.7
1
625.1
12/20/19 19:39
JMV
P9L0395
4-Chlorophenyl phenyl ether
BRL
ug/L
21
4.9
1
625.1
12/20/19 19:39
JMV
P9L0395
4-Nitrophenol
BRL
ug/L
11
2.7
1
625.1
12/20/19 19:39
JMV
P9L0395
Acenaphthene
BRL
ug/L
11
4.5
1
625.1
12/20/19 19:39
JMV
P9L0395
Acenaphthylene
BRL
ug/L
21
4.6
1
625.1
12/20/19 19:39
JMV
P9L0395
Anthracene
BRL
ug/L
11
4.8
1
625.1
12/20/19 19:39
JMV
P9L0395
Benzo(a)anthracene
BRL
ug/L
11
3.4
1
625.1
12/20/19 19:39
JMV
P9L0395
Benzo(a)pyrene
BRL
ug/L
11
3.7
1
625.1
12/20/19 19:39
JMV
P9L0395
Benzo(b)fluoranthene
BRL
ug/L
11
3.6
1
625.1
12/20/19 19:39
JMV
P9L0395
Benzo(g,hJ)perylene
BRL
ug/L
11
3.8
1
625.1
12/20/19 19:39
JMV
P9L0395
Benzo(k)fluoranthene
BRL
ug/L
11
2.8
1
625.1
12/20/19 19:39
JMV
P9L0395
Benzoic Acid
BRL
ug/L
110
20
1
625.1
12/20/19 19:39
JMV
P9L0395
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 15

Laboratory Report
IL a ■ _0 12/26/2019
ANALYTICAL
S&ME, Inc - Charlotte Project: W. Mallard Creek Church Rd. Client Sample ID: TW-1
Attn: Carl Hewett Sample ID: 9120335-01
9751 Southern Pine Blvd. Work Order: 9120335
Charlotte, NC 28273 Sample Matrix: Water Time Collected: 12/19/19 10:15
Time Submitted: 12/19/19 13:15
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Benzyl alcohol
BRL
ug/L
11
2.6
1
625.1
12/20/19 19:39
JMV
P9L0395
bis(2-Chloroethoxy)methane
BRL
ug/L
11
4.0
1
625.1
12/20/19 19:39
JMV
P9L0395
Bis(2-Chloroethyl)ether
BRL
ug/L
11
2.7
1
625.1
12/20/19 19:39
JMV
P9L0395
Bis(2-chloroisopropyl)ether
BRL
ug/L
11
2.9
1
625.1
12/20/19 19:39
JMV
P9L0395
Bis(2-Ethylhexyl)phthalate
BRL
ug/L
11
3.9
1
625.1
12/20/19 19:39
JMV
P9L0395
Butyl benzyl phthalate
BRL
ug/L
11
3.1
1
625.1
12/20/19 19:39
JMV
P9L0395
Chrysene
BRL
ug/L
11
3.5
1
625.1
12/20/19 19:39
JMV
P9L0395
Dibenzo(a,h)anthracene
BRL
ug/L
21
6.0
1
625.1
12/20/19 19:39
JMV
P9L0395
Dibenzofuran
BRL
ug/L
21
4.4
1
625.1
12/20/19 19:39
JMV
P9L0395
Diethyl phthalate
BRL
ug/L
21
4.4
1
625.1
12/20/19 19:39
JMV
P9L0395
Dimethyl phthalate
BRL
ug/L
11
4.3
1
625.1
12/20/19 19:39
JMV
P9L0395
Di-n-butyl phthalate
BRL
ug/L
11
4.5
1
625.1
12/20/19 19:39
JMV
P9L0395
Di-n-octyl phthalate
BRL
ug/L
11
4.7
1
625.1
12/20/19 19:39
JMV
P9L0395
Fluoranthene
BRL
ug/L
11
4.3
1
625.1
12/20/19 19:39
JMV
P9L0395
Fluorene
BRL
ug/L
11
5.3
1
625.1
12/20/19 19:39
JMV
P9L0395
Hexachlorobenzene
BRL
ug/L
21
4.1
1
625.1
12/20/19 19:39
JMV
P9L0395
Hexachlorobutadiene
BRL
ug/L
21
4.7
1
625.1
12/20/19 19:39
JMV
P9L0395
Hexachlorocyclopentadiene
BRL
ug/L
21
7.6
1
625.1
12/20/19 19:39
JMV
P9L0395
Hexachloroethane
BRL
ug/L
11
3.9
1
625.1
12/20/19 19:39
JMV
P9L0395
Indeno(1,2,3-cd)pyrene
BRL
ug/L
11
2.8
1
625.1
12/20/19 19:39
JMV
P9L0395
Isophorone
BRL
ug/L
11
4.3
1
625.1
12/20/19 19:39
JMV
P9L0395
Naphthalene
41
ug/L
11
4.3
1
625.1
12/20/19 19:39
JMV
P9L0395
Nitrobenzene
BRL
ug/L
11
4.1
1
625.1
12/20/19 19:39
JMV
P9L0395
N-Nitroso-di-n-propylamine
BRL
ug/L
21
3.4
1
625.1
12/20/19 19:39
JMV
P9L0395
N-Nitrosodiphenylamine
BRL
ug/L
21
4.7
1
625.1
12/20/19 19:39
JMV
P9L0395
Pentachlorophenol
BRL
ug/L
53
11
1
625.1
12/20/19 19:39
JMV
P9L0395
Phenanthrene
BRL
ug/L
11
4.1
1
625.1
12/20/19 19:39
JMV
P9L0395
Phenol
8.7 J
ug/L
11
1.5
1
625.1
12/20/19 19:39
JMV
P91-0395
Pyrene
BRL
ug/L
11
3.7
1
625.1
12/20/19 19:39
JMV
P9L0395
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
25 %
31-144
A
2-Fluorobiphenyl
89 %
49-118
2-Fluorophenol
17 %
22-84
A
Nitrobenzene-d5
86 %
43-123
Phenol-d5
25 %
10-63
Terphenyl-d14
85 %
49-151
Volatile Organic 602 Compounds by GC/MS
Benzene
6.8
ug/L
0.50
0.048
1
SM6200 B
12/23/19 18:46
ANG
P91-0429
Ethylbenzene
0.73 J
ug/L
1.0
0.061
1
SM6200 B
12/23/19 18:46
ANG
P9L0429
m,p-Xylenes
0.24 J
ug/L
2.0
0.12
1
SM6200 B
12/23/19 18:46
ANG
P91-0429
Methyl-tert-Butyl Ether
BRL
ug/L
5.0
0.042
1
SM6200 B
12/23/19 18:46
ANG
P9L0429
Naphthalene
78
ug/L
5.0
0.19
1
SM6200 B
12/23/19 18:46
ANG
P9L0429
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 15

WayRo i!
ALYTII`AL
S&ME, Inc - Charlotte
Attn: Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
Parameter
Laboratory Report
12/26/2019
Project: W. Mallard Creek Church Rd. Client Sample ID: TW-1
Sample ID: 9120335-01
Work Order: 9120335
Sample Matrix: Water Time Collected: 12/19/19 10:15
Time Submitted: 12/19/19 13:15
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
o-Xylene
1.0
ug/L
1.0
0.044
1
SM6200 B
12/23/19 18:46
ANG
P91-0429
Toluene
0.36 J
ug/L
1.0
0.044
1
SM6200 B
12/23/19 18:46
ANG
P91-0429
Xylenes, total
1.2 J
ug/L
3.0
0.15
1
SM6200 B
12/23/19 18:46
ANG
P91-0429
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
46 J
C9-C12 Aliphatics
200
C9-C10 Aromatics
200
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
101 %
70-130
Dibromofluoromethane
98 %
70-130
Toluene-d8
100 %
70-130
ug/L
50
4.0 1
MADEP VPH
12/20/19 12:29
TBL
P91-0374
ug/L
50
3.9 1
MADEP VPH
12/20/19 12:29
TBL
P91-0374
ug/L
50
4.2 1
MADEP VPH
12/20/19 12:29
TBL
P91-0374
Surrogate
Recovery Control Limits
25-Dibromotoluene (PID) 100 % 70-130
25-Dibromotoluene (FID) 112 % 70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 15

WI n
A.NALY T ICAL
S&ME, Inc - Charlotte
Attn: Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
Project: W. Mallard Creek Church Rd
Volatile Organic 602 Compounds by GC/MS - Quality Control
Analyte
Batch P911-0429 - SM6200 B
Level II QC Report
12/26/19
Work Order: 9120335
Time Submitted: 12/19/2019 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9L0429-BLK1)
Prepared &Analyzed: 12/23/19
Benzene
BRL
0.50
ug/L
Ethylbenzene
BRL
1.0
ug/L
m,p-Xylenes
BRL
2.0
ug/L
Methyl-tert-Butyl Ether
BRL
5.0
ug/L
Naphthalene
0.320
5.0
ug/L
J
o-Xylene
BRL
1.0
ug/L
Toluene
BRL
1.0
ug/L
Xylenes, total
BRL
3.0
ug/L
Surrogate:4-Bromofluorobenzene
50.5
ug/L
50.00 101
70-130
Surrogate: Dibromofluoromethane
48.3
ug/L
50.00 97
70-130
Surrogate: Toluene-d8
50.0
ug/L
50.00 100
70-130
LCS (P9L0429-BS1)
Prepared &Analyzed: 12/23/19
Benzene
22.7
0.50
ug/L
20.00 113
70-130
Ethylbenzene
22.7
1.0
ug/L
20.00 113
70-130
m,p-Xylenes
46.6
2.0
ug/L
40.00 117
70-130
Methyl-tert-Butyl Ether
22.9
5.0
ug/L
20.00 115
70-130
Naphthalene
23.4
5.0
ug/L
20.00 117
70-130
o-Xylene
23.1
1.0
ug/L
20.00 116
70-130
Toluene
23.0
1.0
ug/L
20.00 115
70-130
Xylenes, total
69.8
3.0
ug/L
60.00 116
70-130
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00 100
70-130
Surrogate: Dibromofluoromethane
48.2
ug/L
50.00 96
70-130
Surrogate: Toluene-d8
50.2
ug/L
50.00 100
70-130
LCS Dup (P9L0429-BSD1)
Prepared &Analyzed: 12/23/19
Benzene
21.5
0.50
ug/L
20.00 108
70-130
5
20
Ethylbenzene
21.5
1.0
ug/L
20.00 108
70-130
5
20
m,p-Xylenes
44.3
2.0
ug/L
40.00 ill
70-130
5
20
Methyl-tert-Butyl Ether
21.9
5.0
ug/L
20.00 109
70-130
5
20
Naphthalene
22.3
5.0
ug/L
20.00 111
70-130
5
20
o-Xylene
22.1
1.0
ug/L
20.00 110
70-130
5
20
Toluene
21.7
1.0
ug/L
20.00 109
70-130
6
20
Xylenes, total
66.4
3.0
ug/L
60.00 ill
70-130
5
20
Surrogate:4-Bromofluorobenzene
50.4
ug/L
50.00 101
70-130
Surrogate: Dibromofluoromethane
48.3
ug/L
50.00 97
70-130
Surrogate: Toluene-d8
50.1
ug/L
50.00 100
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 15

Way 1rn
ANALYTICAL
S&ME, Inc - Charlotte Project: W. Mallard Creek Church Rd
Attn: Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
12/26/19
Work Order: 9120335
Time Submitted: 12/19/2019 1:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9LO395 - 3510C MS
Blank (P911-0395-113LK1)
1,2,4-Trichlorobenzene
BRL
10
ug/L
1,2-Dichlorobenzene
BRL
10
ug/L
1,3-Dichlorobenzene
BRL
10
ug/L
1,4-Dichlorobenzene
BRL
10
ug/L
1-Methyl naphthalene
BRL
10
ug/L
2,4,6-Trichlorophenol
BRL
20
ug/L
2,4-Dichlorophenol
BRL
10
ug/L
2,4-Dimethyl phenol
BRL
10
ug/L
2,4-Dinitrophenol
BRL
50
ug/L
2,4-Dinitrotoluene
BRL
10
ug/L
2,6-Dinitrotoluene
BRL
20
ug/L
2-Chloronaphthalene
BRL
20
ug/L
2-Chlorophenol
BRL
10
ug/L
2-Methyl naphthalene
BRL
10
ug/L
2-Nitrophenol
BRL
10
ug/L
3,3'-Dichlorobenzidine
BRL
10
ug/L
3/4-Methyl phenol
BRL
10
ug/L
4,6-Dinitro-2-methylphenol
BRL
50
ug/L
4-Bromophenyl phenyl ether
BRL
20
ug/L
4-Chloro-3-methylphenol
BRL
10
ug/L
4-Chloroaniline
BRL
10
ug/L
4-Chlorophenyl phenyl ether
BRL
20
ug/L
4-Nitrophenol
BRL
10
ug/L
Acenaphthene
BRL
10
ug/L
Acenaphthylene
BRL
20
ug/L
Anthracene
BRL
10
ug/L
Benzo(a)anthracene
BRL
10
ug/L
Benzo(a)pyrene
BRL
10
ug/L
Benzo(b)fluoranthene
BRL
10
ug/L
Benzo(g,h,i)perylene
BRL
10
ug/L
Benzo(k)fluoranthene
BRL
10
ug/L
Benzoic Acid
BRL
100
ug/L
Benzyl alcohol
BRL
10
ug/L
bis(2-Chloroethoxy)methane
BRL
10
ug/L
Bis(2-Chloroethyl)ether
BRL
10
ug/L
Bis(2-chloroisopropyl)ether
BRL
10
ug/L
Bis(2-Ethylhexyl)phthalate
BRL
10
ug/L
Butyl benzyl phthalate
BRL
10
ug/L
Chrysene
BRL
10
ug/L
Dibenzo(a,h)anthracene
BRL
20
ug/L
Dibenzofuran
BRL
20
ug/L
Diethyl phthalate
BRL
20
ug/L
Dimethyl phthalate
BRL
10
ug/L
Di-n-butyl phthalate
BRL
10
ug/L
Di-n-octyl phthalate
BRL
10
ug/L
Fluoranthene
BRL
10
ug/L
Prepared & Analyzed: 12/20/19
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 15

W� in
4.txJ ALY T I C AL
S&ME, Inc - Charlotte
Attn: Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
Project: W. Mallard Creek Church Rd
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P911-0395 - 3510C MS
Level II QC Report
12/26/19
Work Order: 9120335
Time Submitted: 12/19/2019 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9L0395-BLK1)
Prepared & Analyzed: 12/20/19
Fluorene
BRL
10
ug/L
Hexachlorobenzene
BRL
20
ug/L
Hexachlorobutadiene
BRL
20
ug/L
Hexachlorocyclopentadiene
BRL
20
ug/L
Hexachloroethane
BRL
10
ug/L
Indeno(1,2,3-cd)pyrene
BRL
10
ug/L
Isophorone
BRL
10
ug/L
Naphthalene
BRL
10
ug/L
Nitrobenzene
BRL
10
ug/L
N-Nitroso-di-n-propylamine
BRL
20
ug/L
N-Nitrosodiphenylamine
BRL
20
ug/L
Pentachlorophenol
BRL
50
ug/L
Phenanthrene
BRL
10
ug/L
Phenol
BRL
10
ug/L
Pyrene
BRL
10
ug/L
Surrogate: 2,4,6-Tiibromophenol
110
ug/L
100.0
110
31-144
Surrogate:2-Fluorobiphenyl
50.5
ug/L
50.00
101
49-118
Surrogate:2-Fluorophenol
66.7
ug/L
100.0
67
22-84
Surrogate: Nitrobenzene-d5
48.2
ug/L
50.00
96
43-123
Surrogate: Phenol-d5
40.2
ug/L
100.0
40
10-63
Surrogate: Terphenyl-d14
47.1
ug/L
50.00
94
49-151
LCS (1391-0395-113SI)
Prepared & Analyzed: 12/20/19
1,2,4-Trichlorobenzene
48.1
10
ug/L
50.00
96
44-142
1,2-Dichlorobenzene
54.3
10
ug/L
50.00
109
32-129
1,3-Dichlorobenzene
53.1
10
ug/L
50.00
106
20-124
1,4-Dichlorobenzene
52.2
10
ug/L
50.00
104
20-124
1-Methyl naphthalene
50.7
10
ug/L
50.00
101
40-135
2,4,6-Trichlorophenol
56.8
20
ug/L
50.00
114
37-144
2,4-Dichlorophenol
47.6
10
ug/L
50.00
95
39-135
2,4-Dimethylphenol
54.1
10
ug/L
50.00
108
32-119
2,4-Dinitrophenol
27.1
50
ug/L
50.00
54
10-191 J
2,4-Dinitrotoluene
57.3
10
ug/L
50.00
115
39-139
2,6-Dinitrotoluene
60.7
20
ug/L
50.00
121
50-158
2-Chloronaphthalene
55.7
20
ug/L
50.00
ill
60-118
2-Chorophenol
54.1
10
ug/L
50.00
108
23-134
2-Methyl naphthalene
49.4
10
ug/L
50.00
99
18-121
2-Nitrophenol
49.8
10
ug/L
50.00
100
29-182
3,3'-Dichlorobenzidine
62.6
10
ug/L
50.00
125
10-262
3/4-Methyl phenol
40.6
10
ug/L
50.00
81
76-107
4,6-Dinitro-2-methylphenol
46.1
50
ug/L
50.00
92
10-181 J
4-Bromophenyl phenyl ether
55.9
20
ug/L
50.00
112
53-127
4-Chloro-3-methylphenol
48.6
10
ug/L
50.00
97
22-147
4-Chloroaniline
46.2
10
ug/L
50.00
92
44-163
4-Chlorophenyl phenyl ether
55.1
20
ug/L
50.00
110
25-158
4-Nitrophenol
20.1
10
ug/L
50.00
40
10-132
Acenaphthene
57.0
10
ug/L
50.00
114
47-145
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 15

W� in
4.txJ ALY T I C AL
S&ME, Inc - Charlotte Project: W. Mallard Creek Church Rd
Attn: Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
12/26/19
Work Order: 9120335
Time Submitted: 12/19/2019 1:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P911-0395 - 3510C MS
LCS (P9L0395-BS1)
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
Bis(2-Chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Di benzo(a, h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-Nitrosod imethylam ine
N-Nitroso-di-n-propylami ne
N-Nitrosod iphenylam ine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Surrogate: 2,4, 6-Tiibromophenol
Surrogate: 2-Fluorobiphen yl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: Phenol-d5
Surrogate: Terphenyl-d14
Prepared & Analyzed: 12/20/19
60.0
20
ug/L
50.00
120
33-145
55.8
10
ug/L
50.00
112
27-133
51.4
10
ug/L
50.00
103
15-150
53.0
10
ug/L
50.00
106
33-143
56.7
10
ug/L
50.00
113
17-163
55.7
10
ug/L
50.00
111
24-159
50.8
10
ug/L
50.00
102
10-219
53.0
10
ug/L
50.00
106
11-162
BRL
100
ug/L
50.00
10-125
45.6
10
ug/L
50.00
91
16-107
46.4
10
ug/L
50.00
93
33-184
53.5
10
ug/L
50.00
107
12-158
53.5
10
ug/L
50.00
107
36-166
56.9
10
ug/L
50.00
114
10-158
55.3
10
ug/L
50.00
111
10-152
49.1
10
ug/L
50.00
98
17-168
44.6
20
ug/L
50.00
89
10-227
56.0
20
ug/L
50.00
112
39-114
55.0
20
ug/L
50.00
110
10-114
55.6
10
ug/L
50.00
ill
10-112
57.4
10
ug/L
50.00
115
10-118
59.5
10
ug/L
50.00
119
10-146
57.5
10
ug/L
50.00
115
26-137
57.7
10
ug/L
50.00
115
59-121
51.1
20
ug/L
50.00
102
10-152
49.5
20
ug/L
50.00
99
24-116
49.5
20
ug/L
50.00
99
32-117
51.6
10
ug/L
50.00
103
40-113
52.8
10
ug/L
50.00
106
10-171
42.3
10
ug/L
50.00
85
21-196
46.8
10
ug/L
50.00
94
21-133
45.2
10
ug/L
50.00
90
35-180
28.4
10
ug/L
50.00
57
10-119
57.0
20
ug/L
50.00
114
10-230
70.4
20
ug/L
50.00
141
69-152
43.2
50
ug/L
50.00
86
14-176
57.0
10
ug/L
50.00
114
54-120
26.2
10
ug/L
50.00
52
10-112
57.6
10
ug/L
50.00
115
52-115
105
ug/L
100.0
105
31-144
48.1
ug/L
50.00
96
49-118
63.4
ug/L
100.0
63
22-84
40.1
ug/L
50.00
80
43-123
39.7
ug/L
100.0
40
10-63
47.7
ug/L
50.00
95
49-151
L
J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 10 of 15

W� in
4.txJ ALY T I C AL
S&ME, Inc - Charlotte Project: W. Mallard Creek Church Rd
Attn: Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P911-0395 - 3510C MS
Level II QC Report
12/26/19
Work Order: 9120335
Time Submitted: 12/19/2019 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS Dup (P9L0395-BSD1)
Prepared & Analyzed: 12/20/19
1,2,4-Trichlorobenzene
46.4
10
ug/L
50.00
93
44-142
4
20
1,2-Dichlorobenzene
50.8
10
ug/L
50.00
102
32-129
7
20
1,3-Dichlorobenzene
49.1
10
ug/L
50.00
98
20-124
8
20
1,4-Dichlorobenzene
49.4
10
ug/L
50.00
99
20-124
6
20
1-Methyl naphthalene
50.2
10
ug/L
50.00
100
40-135
1
20
2,4,6-Trichlorophenol
56.8
20
ug/L
50.00
114
37-144
0.1
20
2,4-Dichlorophenol
48.5
10
ug/L
50.00
97
39-135
2
20
2,4-Dimethylphenol
54.7
10
ug/L
50.00
109
32-119
1
20
2,4-Dinitrophenol
31.7
50
ug/L
50.00
63
10-191
16
20
2,4-Dinitrotoluene
57.0
10
ug/L
50.00
114
39-139
0.6
20
2,6-Dinitrotoluene
59.4
20
ug/L
50.00
119
50-158
2
20
2-Chloronaphthalene
54.6
20
ug/L
50.00
109
60-118
2
20
2-Chlorophenol
52.1
10
ug/L
50.00
104
23-134
4
20
2-Methyl naphthalene
47.4
10
ug/L
50.00
95
18-121
4
20
2-Nitrophenol
50.4
10
ug/L
50.00
101
29-182
1
20
3,3'-Dichlorobenzidine
62.0
10
ug/L
50.00
124
10-262
1
20
3/4-Methyl phenol
38.8
10
ug/L
50.00
78
76-107
5
20
4,6-Dinitro-2-methylphenol
52.3
50
ug/L
50.00
105
10-181
13
20
4-Bromophenyl phenyl ether
54.2
20
ug/L
50.00
108
53-127
3
20
4-Chloro-3-methylphenol
48.0
10
ug/L
50.00
96
22-147
1
20
4-Chloroaniline
43.9
10
ug/L
50.00
88
44-163
5
20
4-Chlorophenyl phenyl ether
54.5
20
ug/L
50.00
109
25-158
1
20
4-Nitrophenol
21.1
10
ug/L
50.00
42
10-132
5
20
Acenaphthene
56.7
10
ug/L
50.00
113
47-145
0.6
20
Acenaphthylene
59.6
20
ug/L
50.00
119
33-145
0.7
20
Anthracene
57.0
10
ug/L
50.00
114
27-133
2
20
Benzidine
34.9
10
ug/L
50.00
70
15-150
38
20
Benzo(a)anthracene
52.8
10
ug/L
50.00
106
33-143
0.4
20
Benzo(a)pyrene
55.6
10
ug/L
50.00
111
17-163
2
20
Benzo(b)fluoranthene
55.6
10
ug/L
50.00
111
24-159
0.2
20
Benzo(g,h,i)perylene
50.2
10
ug/L
50.00
100
10-219
1
20
Benzo(k)fluoranthene
52.5
10
ug/L
50.00
105
11-162
0.9
20
Benzoic Acid
BRL
100
ug/L
50.00
10-125
20
Benzyl alcohol
42.9
10
ug/L
50.00
86
16-107
6
20
bis(2-Chloroethoxy)methane
45.5
10
ug/L
50.00
91
33-184
2
20
Bis(2-Chloroethyl)ether
51.4
10
ug/L
50.00
103
12-158
4
20
Bis(2-chloroisopropyl)ether
51.2
10
ug/L
50.00
102
36-166
4
20
Bis(2-Ethylhexyl)phthalate
56.4
10
ug/L
50.00
113
10-158
0.8
20
Butyl benzyl phthalate
54.2
10
ug/L
50.00
108
10-152
2
20
Chrysene
49.1
10
ug/L
50.00
98
17-168
0.04
20
Dibenzo(a,h)anthracene
47.3
20
ug/L
50.00
95
10-227
6
20
Dibenzofuran
54.9
20
ug/L
50.00
110
39-114
2
20
Diethyl phthalate
54.8
20
ug/L
50.00
110
10-114
0.3
20
Dimethyl phthalate
54.7
10
ug/L
50.00
109
10-112
2
20
Di-n-butyl phthalate
57.7
10
ug/L
50.00
115
10-118
0.6
20
Di-n-octyl phthalate
58.9
10
ug/L
50.00
118
10-146
1
20
J
7
L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 11 of 15

Way 1rn
ANALYTICAL
S&ME, Inc - Charlotte Project: W. Mallard Creek Church Rd
Attn: Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting
Analyte Result Limit Units
Batch P9LO395 - 3510C MS
Level II QC Report
12/26/19
Work Order: 9120335
Time Submitted: 12/19/2019 1:15:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P911-0395-113SD1)
Prepared &Analyzed: 12/20/19
Fluoranthene
58.2
10
ug/L
50.00
116
26-137
Fluorene
56.9
10
ug/L
50.00
114
59-121
Hexachlorobenzene
50.2
20
ug/L
50.00
100
10-152
Hexachlorobutadiene
47.5
20
ug/L
50.00
95
24-116
Hexachlorocyclopentadiene
47.4
20
ug/L
50.00
95
32-117
Hexachloroethane
48.5
10
ug/L
50.00
97
40-113
Indeno(1,2,3-cd)pyrene
53.1
10
ug/L
50.00
106
10-171
Isophorone
42.1
10
ug/L
50.00
84
21-196
Naphthalene
45.0
10
ug/L
50.00
90
21-133
Nitrobenzene
44.9
10
ug/L
50.00
90
35-180
N-Nitrosodimethyl amine
23.1
10
ug/L
50.00
46
10-119
WIN itroso-di-n-propylamine
54.8
20
ug/L
50.00
110
10-230
WNitrosodiphenylamine
70.0
20
ug/L
50.00
140
69-152
Pentachlorophenol
46.4
50
ug/L
50.00
93
14-176
Phenanthrene
57.9
10
ug/L
50.00
116
54-120
Phenol
24.9
10
ug/L
50.00
50
10-112
Pyrene
57.0
10
ug/L
50.00
114
52-115
Surrogate: 2,4,6-Tribromophenol
108
ug/L
100.0
108
31-144
Surrogate:2-Fluorobiphenyl
45.6
ug/L
50.00
91
49-118
Surrogate:2-Fluorophenol
59.4
ug/L
100.0
59
22-84
Surrogate: Nitrobenzene-d5
39.3
ug/L
50.00
79
43-123
Surrogate: Phenol-d5
36.6
ug/L
100.0
37
10-63
Surrogate: Terphenyl-d14
43.7
ug/L
50.00
87
49-151
1 20
1 20
2 20
4 20
4 20
6 20
0.5 20
0.5 20
4 20
0.5 20
21 20
4 20
0.5 20
7 20
2 20
5 20
1 20
7
J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 12 of 15

Way 1rn
ANALYTICAL
S&ME, Inc - Charlotte Project: W. Mallard Creek Church Rd
Attn: Carl Hewett
9751 Southern Pine Blvd.
Charlotte, NC 28273
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Level II QC Report
12/26/19
Work Order: 9120335
Time Submitted: 12/19/2019 1:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9LO374 - MADEP VPH (W)
Blank (P911-0374-113LK1)
Prepared & Analyzed: 12/20/19
C5-C8 Aliphatics
BRL
50
ug/L
C9-C12 Aliphatics
BRL
50
ug/L
C9-Cl0 Aromatics
BRL
50
ug/L
Surrogate: 2,5-Dibromotoluene (PID)
103
ug/L
100.0 103
70-130
Surrogate: 2,5-Dibromotoluene (FID)
117
ug/L
100.0 117
70-130
LCS (P91-0374-BS1)
Prepared &Analyzed: 12/20/19
C5-C8 Aliphatics
344
50
ug/L
300.0 115
70-130
C9-Cl0 Aromatics
88.7
50
ug/L
100.0 89
70-130
C9-C12 Aliphatic
307
50
ug/L
300.0 102
70-130
Surrogate: 2,5-Dibromotoluene (PID)
101
ug/L
100.0 101
70-130
Surrogate: 2,5-Dibromotoluene (FID)
115
ug/L
100.0 115
70-130
LCS Dup (P91-0374-113SD1)
Prepared &Analyzed: 12/20/19
C5-C8 Aliphatics
322
50
ug/L
300.0 107
70-130 7 50
C9-Cl0 Aromatics
93.2
50
ug/L
100.0 93
70-130 5 50
C9-C12 Aliphatic
308
50
ug/L
300.0 103
70-130 0.1 50
Surrogate: 2,5-Dibromotoluene (PID)
99.1
ug/L
100.0 99
70-130
Surrogate: 2,5-Dibromotoluene (FID)
115
ug/L
100.0 115
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 13 of 15

Level II QC Report
� G 12/26/19
W1in
ANALYTICAL
S&ME, Inc - Charlotte Project: W. Mallard Creek Church Rd. Work Order: 9120335
Attn: Carl Hewett Time Submitted: 12/19/2019 1:15:OOPM
9751 Southern Pine Blvd.
Charlotte, NC 28273
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9L0367 - 3510C GC
Blank (P91-0367-113LKI)
Prepared: 12/19/19 Analyzed: 12/23/19
C9-C18 Aliphatics
BRL
350
ug/L
C19-C36 Aliphatics
BRL
500
ug/L
C1 1 -C22 Aromatics
BRL
250
ug/L
Surrogate:1-Chlorooctadecane
15.7
ug/L
20.00
79
40-140
Surrogate: o-Terphenyl
15.0
ug/L
20.00
75
40-140
Surrogate:2-Fluorobiphenyl
32.1
ug/L
40.00
80
40-140
Surrogate:2-Bromonaphthalene
34.6
ug/L
40.00
86
40-140
LCS (P91-0367-BSI)
Prepared: 12/19/19 Analyzed:
12/23/19
C9-C18 Aliphatics
349
350
ug/L
600.0
58
40-140 J
C19-C36 Aliphatics
735
500
ug/L
800.0
92
40-140
C11-C22 Aromatics
1410
250
ug/L
1700
83
40-140
Surrogate:1-Chlorooctadecane
14.8
ug/L
20.00
74
40-140
Surrogate: o-Terphenyl
16.6
ug/L
20.00
83
40-140
Surrogate:2-Fluorobiphenyl
28.3
ug/L
40.00
71
40-140
Surrogate:2-Bromonaphthalene
39.3
ug/L
40.00
98
40-140
LCS Dup (P9L0367-BSD1)
Prepared: 12/19/19 Analyzed: 12/23/19
C9-Cl8 Aliphatics
407
350
ug/L
600.0
68
40-140 15 50
C19-C36 Aliphatics
873
500
ug/L
800.0
109
40-140 17 50
C11-C22 Aromatics
1520
250
ug/L
1700
90
40-140 8 50
Surrogate:1-Chlorooctadecane
16.0
ug/L
20.00
80
40-140
Surrogate: o-Terphenyl
17.3
ug/L
20.00
87
40-140
Surrogate:2-Fluorobiphenyl
29.4
ug/L
40.00
74
40-140
Surrogate:2-Bromonaphthalene
42.7
ug/L
40.00
107
40-140
Sample
Extraction
Data
Prep Method: 3510C GC
Lab Number Batch
Initial
Final
Daterrime
9120335-01 P91-0367
960 mL
2 mL
12/19/19 15:00
Prep Method: 3510C MS
Lab Number Batch
Initial
Final
Date/Time
9120335-01 P91-0395
950 mL
1 mL
12/20/19 10:00
Prep Method: SM6200 B
Lab Number Batch
Initial
Final
Date/Time
9120335-01 P91-0429
10 mL
10 mL
12/23/19 9:28
Prep Method: MADEP VPH (W)
Lab Number Batch
Initial
Final
Date/Time
9120335-01 P91-0374
44 mL
44 mL
12/20/19 8:00
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 0f 15

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Page 15 of 15

Beverly, Trudy
From: Beverly, Trudy
Sent: Friday, July 10, 2020 5:18 PM
To: [e-mail]
Cc: 'Dwaine Holden'; 'Addison, Luke'
Subject: RE: [External] Incident #40967, Adams Property at 934 W. Mallard Cr. Ch. Rd.
Received.
Trudy
OX 5QiK-M Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httos://dea.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-mans
File Review Procedures:
hitps://deq.ne. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
bit.ps://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htti)s:Hfiles.ne.izov/ncdea[Waste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.l)df
https:Hfiles.nc.gov/ncdeq/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: [e-mail] [mailto:[e-mail]]
Sent: Friday, July 10, 2020 3:10 PM
To: Beverly, Trudy <[e-mail]>
Cc: 'Dwaine Holden' <dholden @carol ina. rr.com>; 'Addison, Luke' <[e-mail]>
Subject: [External] Incident #40967, Adams Property at 934 W. Mallard Cr. Ch. Rd.
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
K0rt.sDam(d)nc.gov
Ms. Beverly,
I hope you are doing well.
Please find attached the IAA report for the subject site.
Thanks!
Ryan R. Osborne, PE
INENCO, Inc.

132 W. Statesville Ave.
Mooresville, NC 28115
Office: 704-662-8192
Fax: [phone]
Mobile: [phone]