AS-340_5550_CA_RPTS_ 20121029_ReceptorSurveySoilAssessmentGWMonitoring

Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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TABLE OF CONTENTS
1.0 SITE IDENTIFICATION.............................................................................................................1
2.0 SITE HISTORY .............................................................................................................................2
3.0 RECEPTOR INFORMATION....................................................................................................3
3.1 WATER SUPPLY WELLS..................................................................................................................3
3.2 PUBLIC WATER SUPPLIES...............................................................................................................3
3.3 SURFACE WATER............................................................................................................................4
3.4 WELLHEAD PROTECTION AREAS ....................................................................................................4
3.5 SUBSURFACE STRUCTURES ...........................................................................................................4
3.6 PROPERTY OWNERS AND OCCUPANTS..........................................................................................4
3.7 RISK CLASSIFICATION .....................................................................................................................4
4.0 SAMPLING RESULTS................................................................................................................5
4.1 SOIL SAMPLING METHODOLOGY.....................................................................................................5
4.2 SOIL SAMPLING RESULTS...............................................................................................................5
4.3 MONITORING WELL INSTALLATION..................................................................................................6
4.4 MONITORING WELL SAMPLING .......................................................................................................6
4.5 MONITORING WELL SAMPLING RESULTS .......................................................................................7
4.6 GROUNDWATER FLOW....................................................................................................................7
4.7 ENHANCED BIOREMEDIATION..........................................................................................................8
5.0 CONCLUSIONS AND RECOMMENDATIONS..................................................................8
TABLES
Table 1 Current and Historical Groundwater Analytical Data
Table 2 Current and Historical Soil Analytical Results
Table 3 Adjacent Property Owner and Receptor Information
Table 4 Well Construction and Groundwater Level Data
FIGURES
Figure 1 Site Location Map
Figure 2 Topographic Map
Figure 3 Site Layout Map
Figure 4 Well Location Map
Figure 5 Soil Sampling Location Map
Figure 6 Groundwater Quality Map
Figure 7 Groundwater Elevations Map
APPENDICES
Appendix I Well Sampling Forms and Site Photographs
Appendix II Request for Water Supply Well Information Letter and Responses
Appendix III Laboratory Analytical Report and Chain of Custody Form
Appendix IV Monitoring Well Construction and Variance Applications and Approvals
Appendix V Monitoring Well Construction Record and Soil Boring Log
Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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2.0 SITE HISTORY
The site is located at 196 W. Palmer Street in Franklin, North Carolina, and is a former
convenience store and gasoline service station. The property is currently not being
utilized. Based on a review of the project summary provided by Ms. Sharon Ghiold with
the North Carolina Department of Environment and Natural Resources (NCDENR)
Underground Storage Tank (UST) Section via electronic mail to our Mr. Al Quarles on
June 23, 2011, and previous activities on the site, it is our understanding that:
On December 12, 1986, NCDENR staff investigated the site and found gasoline
seeping into a culvert across Maple Street from the Palmer Street Texaco.
Tank tightness tests were performed. None of the three onsite USTs tested tight.
On March 7, 1987 the three USTs were replaced with three new steel tanks.
On April 28, 1987 a monitor well was installed onsite and petroleum compounds
exceeding the North Carolina Groundwater Quality Standards (2L Standards)
were detected.
On April 12, 1990, NCDENR staff investigated the site after receiving a report of
gasoline entering a culvert ditch. Excavation of the UST product lines confirmed
a release from a loose fitting near a dispenser.
Five monitor wells (MW-1, MW-2, MW-3, MW-4, and MW-5 were installed
onsite.
The monitor wells were sampled in July 1990 and March 1991. The laboratory
analytical results were provided by Ms. Ghiold and are summarized on the
attached Table 1. Petroleum compounds were detected above the 2L Standards
in all of the onsite wells, with concentrations in monitor wells MW-1, MW-2,
and MW-3 exceeding the Gross Contamination Levels.
On April 29, 2008, Hart and Hickman (H&H) sampled the onsite monitor wells.
MW-1 was gone due to new construction, and MW-5 was filled with mud and
could not be sampled. Contaminant concentrations detected in monitor wells
MW-2, MW-3, and MW-4 had decreased significantly since the March 1991
sampling event. However, exceedances of the 2L Standards were detected in
each of the three onsite monitor wells with the greatest concentrations detected in
monitor well MW-3.
On September 25, 2008 the site was inspected by NCDENR and was reported as
being abandoned. Conversation with the property owner revealed that the USTs
had failed their Cathodic Protection test in June 2007.
Groundwater flow across the site has been determined to be toward the northeast.
Previous assessment activities do not identify water supply wells within 1,000
feet of the site. The most recent assessment activities conducted by S&ME
identified one water supply well approximately 900 feet southwest of the subject
site.
Crawford Branch (a class C stream) in the Little Tennessee River Basin is located
approximately 200 ft north of the site across West Palmer Street.
S&ME collected groundwater samples from monitoring wells MW-2, MW-3, and
MW-4 on July 26, 2011. The concentrations of several petroleum contaminants
in monitor well MW-3 exceeded the 2L Standards. Contaminant concentrations
have generally decreased compared to previous sampling events.
Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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In January 2012, NEO Corporation (NEO) removed the three onsite USTs,
dispensers, and associated piping. S&ME personnel were onsite to observe some
of the closure activities.
NEO excavated and disposed of 34.04 tons of petroleum impacted soil located
between the northern pump island and monitoring well MW-3. No confirmation
soil samples were collected from the excavation extents.
Total petroleum hydrocarbon (TPH) gasoline range organics (GRO)
concentrations exceeding the NCDENR action level of 10 mg/kg were detected
in five of the UST system closure samples with the greatest concentrations being
detected in soil samples Pump 4 (294 mg/kg) and Pump 2 (707 mg/kg). The
NEO UST closure sampling results are summarized on the attached Table 2.
The site location and vicinity are shown in Figure 1 and Figure 2.The site and pertinent
features are shown on Figure 3.
The scope of services performed for this report were performed in general accordance
with S&ME’s Proposal Number 1354-25460-12 dated June 20, 2012, and as authorized
by NCDENR’s Task Authorization No. 03 dated June 21, 2012 within NCDENR’s
Contract No. 16-1713-4C for the Western Region.
3.0 RECEPTOR INFORMATION
S&ME, Inc., (S&ME) performed a receptor study to identify the potential receptors
located within 1,500 feet of the subject site.Figure 4 shows the locations of potential
receptors located within approximately 1,500 feet and properties within 500 feet of the
source area on the subject property.
3.1 Water Supply Wells
S&ME identified one water supply well within 1,000 feet of the source area during the
receptor survey reconnaissance performed on August 15, 2012 (Figure 4, Map ID #6).
The property serviced by the well is located approximately 900 feet southwest of the
source area on the subject property. The letters requesting water supply well information
were mailed to the owners of 22 properties located within 500 feet of the subject site. To
date, responses for 16 of the properties have been received. None of the respondents
indicated that a water supply well was located on their property.
If information is received by S&ME that requires an update to the receptor survey,
S&ME will submit an addendum to this report. A copy of the Request for Water Supply
Well Information Letter and the responses to the letter received by S&ME are included in
Appendix II.Surrounding property owner information is included in Table 3.
3.2 Public Water Supplies
According to the Town of Franklin Water and Sewer Department (TFWSD), potable
water is available to properties within 1,000 feet of the site provided by the Town of
Franklin. The Town of Franklin obtains water from a surface water intake located on the
Cartoogechaye Creek. S&ME contacted Jay Gibson, TFWSD Director, by telephone on
Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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October 25, 2012 who indicated that TCWSD water lines were present throughout the
area within 1,000 feet of the subject property.
S&ME personnel also observed fire hydrants along West Palmer Street and Maple Street,
and within 1,000 feet of the subject property.
3.3 Surface Water
According to the 1987 Franklin, NC USGS Quadrangle Map, and S&ME’s site
reconnaissance, Crawford Branch (Class C stream) is located approximately 200 feet
north of the source area on the subject property (Figure 4). The Little Tennessee River is
located approximately one mile east of the source area (Figure 2).
3.4 Wellhead Protection Areas
Based on a review of the NCDENR Public Water Supply Section webpage
(http://swap.deh.enr.state.nc.us/swap_app/viewer.htm), the subject site is not designated
as a Wellhead Protection Area.
3.5 Subsurface Structures
Buried municipal water and sewer lines are located on the subject property. A basement
is not associated with the building located on the subject site.
3.6 Property Owners and Occupants
The names and addresses of the property owners and occupants within 500 feet of the
source area are summarized in Table 3. These properties are identified numerically on
the receptor survey map which is included as Figure 4. The nearest residence is located
approximately 500 feet south of the source area (Property #8,Figure 4).
According to the Town of Franklin Zoning Map, the site is zoned NMU – Neighborhood
Mixed Use. Surrounding properties are zoned NMU, C1 (Central Commercial), and R1
(Residential). Surrounding property uses include commercial and residential properties.
3.7 Risk Classification
Based on the information from the receptor survey, the site meets NCDENR’s criteria for
a classification as a High Risk site. One drinking water supply wells was identified 1,000
feet of the source area on the subject property.
None of the groundwater contaminants identified exceed the gross contamination levels
and no free product was observed at the source area. Contaminants were detected in the
groundwater at concentrations above the 2L Standards but not above the Gross
Contamination Levels (GCLs). Contaminants were detected in the soil at concentrations
above the Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs)
but not the Residential or Industrial/Commercial MSCCs.
Surface water is located within 200 feet of the release. Naphthalene (140 micrograms per
liter or µg/L) in monitor well MW-1A was detected at a concentration exceeding the
surface water standard (2B Standard) of 12 µg/L, by greater than a factor of 10.
Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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4.0 SAMPLING RESULTS
4.1 Soil Sampling Methodology
On August 15, 2012, four (4) soil borings were performed using direct push techniques
(i.e. Geoprobe). The approximate locations of the borings labeled as SB-1A, SB-2, SB-
3, and SB-4 are shown on Figure 5.
Soil boring SB-1A was performed in the approximate location of soil sample Pump 2
collected by NEO during their UST closure activities onsite. Soil boring SB-1A was
extended to 5-feet bls where the apparent water table was encountered. Soil sample SB-
1A was collected at approximately 4-feet bls, above the apparent water table.
Soil borings SB-2 and SB-3 were performed in the location of the impacted soil
excavated by NEO during their UST closure activities. Soil borings SB-2 and SB-3 were
extended to 5-feet bls where the apparent water table was encountered. Soil samples SB-
2 and SB-3 were collected from approximately 4-feet bls, above the apparent water table
and at the vertical extent of the excavation performed by NEO.
Soil boring SB-4 was performed in the approximate location of soil sample Pump 4
collected by NEO during their UST closure activities onsite. Soil boring SB-1A was
extended to 5-feet bls where the apparent water table was encountered. Soil sample SB-
1A was collected at approximately 4-feet bls, above the apparent water table.
4.2 Soil Sampling Results
In soil sample SB-1A, two carbon fractions [C5-C8 aliphatics (533 mg/kg) and C9-C22
aromatics (314 mg/kg)], were detected at concentrations exceeding their respective Soil-
to-Groundwater (STG) Maximum Soil Contaminant Concentrations (MSCCs) of 72
mg/kg and 34 mg/kg. Six (6) additional contaminants were detected in soil sample SB-
1A at concentrations less than the MSCCs.
In soil sample SB-2, benzene (1.0 mg/kg), n-butylbenzene (28 mg/kg), sec-butylbenzene
(7.2 mg/kg), ethylbenzene (130 mg/kg), p-isopropyltoluene (3.7 mg/kg), naphthalene (64
mg/kg), n-propylbenzene (77 mg/kg), toluene (23 mg/kg), 1,2,4-trimethylbenzene (410
mg/kg), 1,3,5-trimethylbenze (150 mg/kg), and xylenes (490 mg/kg) were detected at
concentrations exceeding their STG MSCCs of 0.0056 mg/kg, 4.3 mg/kg, 3.3 mg/kg, 4.9
mg/kg, 0.12 mg/kg, 0.16 mg/kg, 1.7 mg/kg, 4.3 mg/kg, 8.5 mg/kg, 8.3 mg/kg, and 4.6
mg/kg, respectively.
In soil sample SB-3, benzene was detected at a concentration of 0.110 mg/kg which
exceeds the STG MSCC for benzene of 0.0056 mg/kg. Eleven (11) additional
compounds were detected in soil sample SB-3 at concentrations less than the MSCCs.
In soil sample SB-4, benzene (0.14 mg/kg), p-isopropyltoluene (0.29 mg/kg),
naphthalene (2.6 mg/kg), n-propylbenzene (3.3 mg/kg), and two carbon fractions [C5-C8
aliphatics (132 mg/kg) and C9-C22 aromatics (45 mg/kg)] were detected at
concentrations exceeding their STG MSCCs of 0.0056 mg/kg, 0.12 mg/kg, 0.16 mg/kg,
Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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1.7 mg/kg, 72 mg/kg, and 34 mg/kg, respectively. Twelve (12) additional contaminants
were detected in soil sample SB-4 at concentrations less than their MSCCs.
A copy of the laboratory analytical report is included in Appendix III.
4.3 Monitoring Well Installation
Due to the presence of shallow groundwater on the site, prior to installation of
groundwater monitoring well MW-1A, S&ME completed and submitted an Application
for a Permit to Construct a Well Requiring a Variance to the Title 15 A NCAC 2C .0100
Well Construction Standards to the NCDENR Division of Water Quality (DWQ) dated
July 5, 2012. On July 18, 2012, S&ME submitted an Application for Permit to Construct
a Monitoring or Recovery Well System to the NCDENR DWQ. On July 25, 2012 the
NCDENR DWQ issued Well Variance Construction Permit WV0100052 and Well
Construction Permit WM0100303 for construction of monitoring well MW-1A at the
Palmer Street Texaco.
Copies of the monitoring well construction application, monitoring well construction
variance application, and well construction and variance approval letters are included in
Appendix IV.
On August 15, 2012, S&ME personnel directed the drill crew to advance soil boring SB-
1A into the groundwater table using 4 1/4” hollow stem augers. The soil boring was
converted into a groundwater monitoring well (MW-1A) by installing a 10-foot long
section of two-inch diameter polyvinyl chloride (PVC) slotted (0.010-inch) screen and
sufficient riser pipe to bring the well to ground surface. The well was completed by
placing #2 type filter sand in the boring annulus to approximately one foot above the
screen section (sand pack). Approximately 0.5 feet of hydrated bentonite was tremied
above the sand pack, and neat cement grout was then tremied from the top of the
bentonite to approximately two inches bls. The well extended to the ground surface
where it was encased with a flush mount protective steel casing with bolted manhole
cover. A four-inch thick concrete pad was used to finish the surface of the well.
Monitoring well MW-1A was installed to a depth of approximately 12 ft-bls, based on
the apparent depth to groundwater of 5 ft-bls at the time of drilling. The monitoring well
construction detail is summarized in Table 4. The location of the monitoring well is
presented on Figure 3. The monitoring well was developed by evacuating groundwater
from the well using a submersible electronic pump until the groundwater became
relatively free of visible particulates. The soil boring log and monitoring well
construction record are included in Appendix V.
4.4 Monitoring Well Sampling
On August 16, 2012, S&ME was on-site to gauge depth-to-water and collect groundwater
samples from monitor wells MW-1A, MW-2, MW-3, and MW-4. The depth-to-water
gauged onsite was approximately 4 feet below land surface (bls) in each of the monitor
wells. After measuring the depth-to-water, S&ME personnel purged each of the monitor
wells with a dedicated disposable polyethylene bailer by evacuating approximately three
well volumes from each of the wells. Well sampling forms and site photographs are
included in Appendix I.
Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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After completing the well purging and allowing groundwater to recover in the monitor
wells, S&ME personnel collected a groundwater sample from each of the wells. The
groundwater samples were placed in laboratory-supplied containers, stored in a cooler with
ice, and shipped under chain-of-custodyprocedures to ShealyEnvironmental Services, Inc.,
a North Carolina certified laboratoryfor laboratory analysis. The groundwater samples
were analyzed for volatile organic compounds (VOCs) byEPA Method 6200B. The
groundwater sample collected from monitor well MW-1A was additionallyanalyzed for
lead byEPA Method 6010 and Volatile Petroleum Hydrocarbons (VPH) by MADEP.
4.5 Monitoring Well Sampling Results
Monitor well MW-1A contained benzene (47 µg/L), chloromethane (3.3 µg/L),
naphthalene (140 µg/L), n-propylbenzene (130 µg/L), and three carbon fractions [C5-C8
aliphatics (1,710 µg/L), C9-C18 aliphatics (1,780 µg/L), and C9-C22 aromatics (1,080
µg/L)] at concentrations exceeding their 2L Standards of 1 µg/L, 3 µg/L, 6 µg/L, 70
µg/L, 400 µg/L, 700 µg/L, and 200 µg/L, respectively. The concentration of naphthalene
(140 µg/L) also exceeding the surface water standard of 12 µg/L by a factor of 11.7
(more than ten times).
Monitor well MW-2 contained benzene (54 µg/L) and naphthalene (31 µg/L) at
concentrations exceeding their 2L Standards of 1 µg/L and 6 µg/L, respectively. Thirteen
(13) additional contaminants were detected at concentrations that are less than their
respective 2L Standards.
Monitor well MW-3 contained benzene (240 µg/L), methyl tert-butyl ether or MTBE
(250 µg/L), and naphthalene (17 µg/L) at concentrations exceeding their respective 2L
Standards of 1 µg/L, 20 µg/L, and 6 µg/L. Thirteen (13) additional contaminants were
detected at concentrations that are less than their respective 2L Standards.
Monitor well MW-4 contained several petroleum contaminants at concentrations that are
less than their respective 2L Standards.
No contaminants were detected at concentrations above the Gross Contamination Levels.
Contaminant concentrations are generally decreasing with time in each of the sampled
monitor wells. A summary of current and historic groundwater analytical results and a
comparison to NCDENR’s regulatory standards is included on Table 1.A copy of the
laboratory analytical results and chain-of-custody form is included in Appendix III. The
contaminants exceeding the 2L Standards are shown on Figure 6.
4.6 Groundwater Flow
S&ME used a level and tripod to measure the relative elevations of the monitoring well
casings based on an assumed datum of 100.00 feet (top of well casing at monitor well
MW-1A).
S&ME personnel used an electronic water level indicator to measure the depth-to-
groundwater from the top of well casing for groundwater monitoring wells MW-1A,
MW-2, MW-3, and MW-4. Depth to water measurements ranged from 3.90 (MW-4) to
4.43 (MW-1A) feet below top-of-casing. The groundwater level measurements from the
Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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August 16, 2012 sampling event are summarized in Table 4. The water level
measurements collected on August 16, 2012 were used to prepare a groundwater
elevation map (Figure 7). Based on the groundwater elevations, the groundwater flow
direction onsite is generally to the north.
4.7 Enhanced Bioremediation
Following gauging the depth to groundwater and collection of groundwater samples from
monitoring wells MW-1A and MW-3, S&ME installed new 1.25-in diameter by 48-inch
long well booms (Universal Remediation Inc., Petroleum Remediation Product) in these
monitoring wells. The purpose of the well booms is to enhance the biodegradation (e.g.
natural attenuation) of petroleum constituents in the vicinity of the monitoring wells.
5.0 CONCLUSIONS AND RECOMMENDATIONS
A limited soil assessment, receptor survey, and groundwater monitoring event were
conducted at the Palmer Street Texaco located at 196 W. Palmer Street in Franklin, North
Carolina to assess potential petroleum impact to the soil and groundwater from petroleum
USTs. The findings at the site are as follows:
S&ME collected groundwater samples from monitoring wells MW-2, MW-3, and
MW-4 on July 26, 2011. The concentrations of several petroleum contaminants
in monitor wells MW-1A, MW-2, and MW-3 exceeded the 2L Standards.
Contaminant concentrations have generally decreased compared to previous
sampling events. No contaminant concentrations exceeded the Gross
Contaminant Levels. The naphthalene concentration in monitor well MW-1A
exceeded the surface water quality standard by more than 10 times.
In January 2012, NEO Corporation (NEO) removed the three onsite USTs,
dispensers, and associated piping. NEO excavated and disposed of 34.04 tons of
petroleum impacted soil located between the northern pump island and
monitoring well MW-3.
On August 15, 2012, S&ME collected soil samples from four soil borings.
Contaminant concentrations exceeding the STG MSCCs but less than the
residential and industrial/commercial MSCCs were detected in each of these soil
samples.
An unnamed tributary to the Little Tennessee River is located approximately 200
feet east of the source area on the property. Naphthalene was detected in the
groundwater sample collected from monitor well MW-1A at a concentration
greater than 10 times the surface water quality standards for Class C streams.
Groundwater flow across the site is generally to the north. The depth to
groundwater ranged from 3.90 to 4.43 feet below the flush-mount top of well
casings.
Groundwater Monitoring Report - Incident No.5550 S&ME Project No. 1354-11-130B
Palmer Street Texaco, Franklin, Macon County, NC October 29, 2012
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One drinking water supply well is located approximately 900 feet southwest of
the site.
Based on the results of this assessment, the site meets the criteria to be ranked as
a High Risk site (due to the presence of the one water supply well located ~900
feet southwest of the site). Due to the exceedance of the surface water quality
standard by more than ten times, the site also meets the criteria to be ranked as an
Intermediate Risk site.
Based on the above information, S&ME recommends the following:
Pursue a municipal water connection to the property with the active water supply
well at 145 West Dogwood Drive. The goal of this task would be to lower the
risk classification of the incident from High to Intermediate or Low.
Perform aquifer testing at the site (using slug testing of one of the monitor wells)
and solute transport modeling to evaluate the potential for impact to the stream
located within 200 feet of the site. The goal of this task would be to reduce the
risk classification to Low, if the municipal water connection to the above
referenced residence if conducted.
TABLES
Metals by
Method
6010C
MW-1A 8/16/2012 47 12 6.8 1.6 J 3.3 <2.0 3.5 76 <2.0 <2.0 39 0.71 J 7.3 140 130 23 56 13 109 1,710 1,780 1,080 2.8 J
7/18/1990 8,100 NA NA NA NA NA NA 1,800 5,300 NA NA NA 6,100 NA NA 9,400 NA NA 8,700 NA NA NA NA
3/7/1991 15,000 NA NA NA NA NA NA 1,700 200 NA NA NA 4,800 NA NA 18,000 NA NA 8,000 NA NA NA NA
4/29/2008
7/26/2011
8/16/2012
7/18/1990 15,000 NA NA NA NA NA NA 2,000 26 NA NA NA 31,000 NA NA 21,000 NA NA 10,000 NA NA NA NA
3/7/1991 11,000 NA NA NA NA NA NA 1,600 <50 NA NA NA 25,000 NA NA 16,000 NA NA 7,000 NA NA NA NA
4/29/2008 480 <10 <5.0 <5.0 <5.0 <5.0 <5.0 490 <5.0 <20 13 <5.0 770 110 40 20 160 <5.0 250 NA NA NA NA
7/26/2011 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.19 J <0.50 0.18 J 0.44 J 0.47 J 0.29 J NA NA NA NA
8/16/2012 54 3.6 1.3 0.37 J <0.50 <0.50 1.7 73 <0.50 <0.50 4.1 0.13 J 14 31 12 1.7 5.0 0.43 J 12.62 NA NA NA NA
7/18/1990 14,000 NA NA NA NA NA NA 1,700 49 NA NA NA 190,000 NA NA 17,000 NA NA 9,300 NA NA NA NA
3/7/1991 28,000 NA NA NA NA NA NA 2,200 150 NA NA NA 380,000 NA NA 29,000 NA NA 12,000 NA NA NA NA
4/29/2008 8,100 <100 <50 <50 <50 <50 <50 1,100 <50 <200 <50 <50 7,100 410 <50 700 480 100 4,280 NA NA NA NA
7/26/2011 200 9.2 2.8 <0.50 <0.50 4.9 13 63 <0.50 0.23 BJ 5.6 0.65 270 36 16 4.5 1.9 0.57 26 NA NA NA NA
8/16/2012 240 2.2 1.2 <1.0 1.9 <1.0 9.4 56 <1.0 <1.0 5.5 <1.0 250 17 9.9 0.77 J 1.8 <1.0 2.26 NA NA NA NA
7/18/1990 70 NA NA NA NA NA NA ND ND NA NA NA ND NA NA 16 NA NA 1.5 NA NA NA NA
3/7/19911 270 NA NA NA NA NA NA <5.0 14 NA NA NA 18,000 NA NA 8.7 NA NA 21 NA NA NA NA
4/29/2008 1.2 <1.0 0.57 <0.50 <0.50 <0.50 4.5 <0.50 <0.50 <2.0 4.6 <0.50 17 3.7 2.7 <0.50 <0.50 <0.50 <1.5 NA NA NA NA
7/26/2011 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 6.5 <0.50 <0.50 <0.50 4.6 <0.50 1.8 <0.50 7.2 <0.50 <0.50 <0.50 <1.0 NA NA NA NA
8/16/2012 <0.50 0.58 0.90 <0.50 1.8 <0.50 4.4 <0.50 <0.50 <0.50 5.2 <0.50 2.0 2.4 4.2 <0.50 <0.50 <0.50 0.17 J NA NA NA NA
7/18/1990 1.7 NA NA NA NA NA NA 0.85 1.9 NA NA NA 35 NA NA 12 NA NA 6.1 NA NA NA NA
3/7/19912 <0.5 NA NA NA NA NA NA ND <1.0 NA NA NA <1.0 NA NA ND NA NA ND NA NA NA NA
4/29/2008
7/26/2011
8/16/2012
1.0 70 70 70 3 0.4 70 600 0.02 0.4 70 25 20 6 70 600 400 400 500 400 700 200 15
5,000 6,900 8,500 70,000 3,000 400 70,000 84,500 50 400 25,000 11,700 20,000 6,000 30,000 260,000 28,500 25,000 85,500 NE NE NE 15,000
51 550 NE 170 NE 37 NE 97 NE 18 250 NE 1,500 12 3,200 11 NE 215 670 1,400 NE 4,000 25
Notes: Concentrations reported micrograms per liter (mg/L)
NA = Not analyzed
NCAC 2L Standards = NCAC 2L groundwater quality standards
2B Standard: North Carolina Surface Water Quality Standards (August 16, 2012), lower of the
Freshwater Aquatic Life or Human Health Standards
NE = No standard established
MTBE = methyl-tert-butyl ether
ND = Not detected above laboratory reporting limits
J = Estimated value. Concentration is between the method detection limit and laboratory reporting limit
B = Compound detected in the laboratory method blank
1 = Sample is actually designated as S-5 in the March 3, 1991 laboratory report prepared by GeoChem, Incorporated
2 = Sample is actually designated as S-6 in the March 3, 1991 laboratory report prepared by GeoChem, Incorporated
196 W. Palmer Street
Franklin, Macon County, North Carolina
NCDENR Incident No. 5550
S&ME Project No. 1354-11-130B
Concentrations in bold and underlined exceed the NCAC 2B Standards
MADEP VPH
Well is full of mud
Well is full of mud
Well has been covered by gravel driveway
Well has been covered by gravel driveway C9-C18 AliphaticsC9-C22 AromaticsLeadMTBE1,2,4-TrimethylbenzeneIsopropylbenzene1,3,5-TrimethylbenzeneWell ID Date
Collected
Ethylbenzene MW-1
MW-2 C5-C8 AliphaticsHexachlorobutadiene1,2-DichloroethaneDiisopropyl etherXylenes Concentrations in bold and highlighted in gray exceed the NCAC 2L Standards
NCAC 2L Standards
Gross Contamination Levels
MW-5
MW-4
Contaminant of Concern
Benzene Concentrations in bold exceed the laboratory detection limits
MW-3
NCAC 2B Standards
EPA Methods 602/6210D/6200BAnalytical Method
Table 1
Current and Historical Groundwater Analytical Data
Palmer Street Texaco
Well is full of mud
Well has been covered by gravel driveway Toluenen-PropylbenzeneNaphthalenen-Butylbenzenesec-Butylbenzenep-IsopropyltolueneChloroformChloromethaneEthylene dibromide (1,2-Dibromoethane)
TPH by
EPA
5030
AcetoneBenzene2-Butanone (MEK)n-Butylbenzenesec-ButylbenzeneChloroformEthylbenzeneIsopropylbenzenep-IsopropyltolueneMTBENaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (Total)C5-C8 AliphaticsC9-C18 AliphaticsC9-C22 AromaticsGRODate
Depth
(ft-bls)
SB-1A 8/15/2012 4 0.054 0.0016 J <0.0095 <0.0048 <0.0048 0.0013 J <0.0048 <0.0048 <0.0048 0.0015 J 0.0022 J <0.0048 <0.0048 <0.0048 <0.0048 <0.0048 533 666*314 NA
SB-2 8/15/2012 4 9.4 J 1.0 J <5.3 28 7.2 <2.6 130 <2.6 3.7 <2.6 64 77 23 410 150 490 10.4 <5.38 <5.38 NA
SB-3 8/15/2012 4 0.140 0.110 0.012 <0.0049 <0.0049 0.020 0.130 0.0064 <0.0049 0.024 0.0099 0.017 <0.0049 0.092 0.030 0.330 <5.41 <5.41 <5.41 NA
SB-4 8/15/2012 4 0.55 J 0.14 J <0.620 1.6 0.5 0.14 J 4.5 0.880 0.29 J 0.030 J 2.6 3.3 0.11 J 6.2 0.310 0.770 132 87.7 45.0 NA
Tank 1 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 2 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 3 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 4 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 5 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 6 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 7 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 8 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 9 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 10 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 11 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 12 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Tank 13 1/6/2012 8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 1 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 2 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 3 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 4 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 5 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 6 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 7 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 8 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Line 9 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 60.7
Line 10 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <10
Pump 1 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 75.9
Pump 2 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 707
Pump 3 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 180
Pump 4 1/6/2012 2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 294
24 0.0056 16 4.3 3.3 0.37 4.9 1.7 0.12 0.091 0.16 1.7 4.3 8.5 8.3 4.6 72 3,300 34 NE
14,000 18 9,385 626 626 20 1,560 1,564 100 350 313 626 1,200 782 782 3,129 939 9,386 469 NE
360,000 164 245,280 16,350 16,350 180 40,000 40,880 4,000 3,100 8,176 16,350 32,000 20,440 20,440 81,760 24,528 245,280 12,264 NE
NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE 10
Notes:
1. Analytes that are not shown were not detected.
2. All concentrations are reported in milligrams per kilogram (mg/Kg).
3. MSCC: Maximum Soil Contaminant Concentration
4. Ft-bls: Feet below land surface
5. VOCs: Volatile Organic Compounds
6. NA: Not Analyzed
7. MADEP VPH - Massachusettes Department of Environmental Protection - Volatile Petroleum Hydrocarbons
7. TPH: Total Petroleum Hydrocarbons
8. GRO: Gasoline Range Organics
10. * The concentration reported is an estimated value. The result was above the highest laboratory standard.
11. J: The concentration reported is an estimated value.
12. All samples that exceed the soil-to-groundwater MSCC are shown in Shaded and BOLD fields.
13. Concentrations exceeding the laboratory's reporting limits are shown in BOLD fields.
Table 2
Summary of Current and Historical Soil Analytical Results
Palmer Street Texaco
196 W. Palmer Street
Franklin, Macon County, North Carolina
NCDENR Incident No. 5550
Soil-to-Groundwater MSCCs
Residential MSCCs
Industrial/Commercial MSCCs
NCDENR Action Level
S&ME Project No: 1354-11-130B
MADEP VPH
Sample ID
Contaminant of
Concern
VOCs by EPA 8260B
MAP ID PROPERTY ADDRESS PROPERTY OWNER NAME OWNER ADDRESS CITY, STATE, & ZIP OCCUPANT/ USE MACON COUNTY PIN SUPPLY WELL
1 196 W PALMER ST PETERSON, SHAWN SLOAN 101 LOGG N ROAD FRANKLIN NC 28734 COMMERCIAL 6584993072 NO
2 W MAIN ST TOWN OF FRANKLIN GEN DEL FRANKLIN NC 28734 COMMERCIAL 6584899246 NO
3 244 W PALMER ST HANNAH, RICKY RAY 659 BROOKWOOD DR FRANKLIN NC 28734 COMMERCIAL 6584981912 NO
4 276 W PALMER ST TASTINGER, THOMAS J JR 198 STONE CREEK DRIVE FRANKLIN NC 28734 COMMERCIAL 6584889997 NO
5 278 W PALMER ST TASTINGER, THOMAS J JR 198 STONE CREEK DRIVE FRANKLIN NC 28734 COMMERCIAL 6584980857 NO
6 145 W DOGWOOD DR SANDERS, ANNA MARIE 5210 NW 110TH AVENUE CORAL SPRINGS FL 33076 RESIDENTIAL 6584887710 YES / 900ft SW
7 MAPLE ST ANGEL, FURMAN JR 129 GOLF VIEW DR FRANKLIN NC 28734 RESIDENTIAL 6584982760 NO
8 115 MAPLE ST REECE, FRANK W MRS 30 EVERGREEN LN BRYSON CITY NC 28713 RESIDENTIAL 6584982563 NO
9 152 W PALMER ST WALIANY, GULZAR 725 BAIRD COVE ROAD FRANKLIN NC 28734 COMMERCIAL 6584986829 NO
10 10 W PALMER ST PALMER STREET MALL LLC 81 WEST MAIN STREET FRANKLIN NC 28734 COMMERCIAL 6594080879 NO
11 106 W PALMER ST GILLESPIE, KARL E.860 CORBIN RD FRANKLIN NC 28734 COMMERCIAL 6584999110 NO
12 120 W PALMER ST GILLESPIE, KARL E.860 CORBIN RD FRANKLIN NC 28734 COMMERCIAL 6584997089 NO
13 149 W PALMER ST J H DUNCAN OIL INC P O BOX 616 FRANKLIN NC 28744 COMMERCIAL 6584995284 NO
14 109 W PALMER ST EMW PROPERTIES LLC P.O. BOX 80 ASHEVILLE NC 28802 COMMERCIAL 6584997299 NO
15 W PALMER ST EMW PROPERTIES LLC P.O. BOX 80 ASHEVILLE NC 28802 COMMERCIAL 6584997227 NO
16 W PALMER STREET EMW PROPERTIES LLC P.O. BOX 80 ASHEVILLE NC 28802 RESIDENTIAL 6584996266 NO
17 330 W MAIN ST KIDS INTERDISCIPLINARY SERVICES INC 9 WEST MAIN ST FRANKLIN NC 28734 COMMERCIAL 6584996481 NO
18 344 W MAIN ST SHULER, DEBORAH LYNN 224 CA MEADOWS RD FRANKLIN NC 28734 COMMERCIAL 6584995398 NO
19 181 W PALMER ST CONLEY MOTOR COMPANY 275 STONECREEK DRIVE FRANKLIN NC 28734 COMMERCIAL 6584994223 NO
20 368 W MAIN ST PENLAND, MELVIN R 372 WEST MAIN ST FRANKLIN NC 28734 COMMERCIAL 6584994337 NO
21 24 COMMERCE ST TALLEY, HERMAN L 211 WEST PALMER ST FRANKLIN NC 28734 COMMERCIAL 6584993215 NO
22 233 W PALMER ST NORTON, KAREN H 290 OAK HILL DR FRANKLIN NC 28734 COMMERCIAL 6584991186 NO
23 21 COMMERCE ST HAVEN, RONALD M.750 MILL CREEK RD FRANKLIN NC 28734 COMMERCIAL 6584992226 NO
24 15 COMMERCE ST HAVEN, RONALD M.750 MILL CREEK RD FRANKLIN NC 28734 COMMERCIAL 6584992333 NO
25 23 COMMERCE ST KESWICK, JOHN P TRUSTEE 625 ANDERSON CREEK RD FRANKLIN NC 28734 COMMERCIAL 6584991267 NO
26 424 W MAIN ST GOODMAN, CHLOE A.150 DEER CROSSING RD FRANKLIN NC 28734 COMMERCIAL 6584991373 NO
27 49 MAPLE ST TOWN OF FRANKLIN 70 W MAIN STREET FRANKLIN NC 28734 COMMERCIAL 6584982896 NO
28 443 W MAIN ST SILER, ROBERT & THERESA G 443 W MAIN ST FRANKLIN NC 28734 COMMERCIAL 6584899693 NO
29 407 W MAIN ST DAVIS, DOERR WENDELL 407 W MAIN FRANKLIN NC 28734 COMMERCIAL 6584991593 NO
30 391 W MAIN ST COLONIAL HOUSE OF FRANKLIN LLC 1281 GEORGIA RD FRANKLIN NC 28734 COMMERCIAL 6584992586 NO
31 373 W MAIN ST HOUSTON, MAX CARL 93 TALLENT STREET FRANKLIN NC 28734 COMMERCIAL 6584994507 NO
32 355 W MAIN ST SMART, LOU P 507 N MAIN ST WAKE FOREST NC 27587 COMMERCIAL 6584994569 NO
33 102 WEST BLVD HOLLAND, RAYMOND D.102 WEST BLVD FRANKLIN NC 28734 RESIDENTIAL 6585806340 YES / 1460ft NW
S&ME Project No. 1354-11-130B
Table 3
Adjacent Property Owner and Receptor Information
Palmer Street Texaco
196 W. Palmer Street
Franklin, Macon County, North Carolina
NCDENR Incident No. 5550
Well ID
Date
Installed
(m/dd/yy)
Date
Water
Level
Measured
(m/dd/yy)
Depth to
Water
(ft below TOC)
Groundwater
Elevation
(ft above datum.)
TOC Elevation
(ft above datum.)
Well
Casing
Diameter
(in)
Well
Casing
Depth
(ft bls)
Screen
Interval
(x to y ft. bls)
Depth
of Well
(ft bls)
MW-1A 8/15/2012 8/16/2012 4.43 95.57 100.00 2 2.00 2.00 - 12.00 12.00
MW-2 1990 8/16/2012 4.12 95.98 100.10 2 2.70 2.70 - 12.70 12.70
MW-3 1990 8/16/2012 4.13 95.46 99.59 2 2.13 2.13 - 12.13 12.13
MW-4 1990 8/16/2012 3.90 95.50 99.40 2 2.40 2.40 - 12.40 12.40
Notes:
TOC = Top of Casing
ft = feet
bls = below land surface
Elevations provided based on a 100' datum measured on top of well casing at monitor well MW-1A
Franklin, Macon County, North Carolina
NCDENR Incident No. 5550
Table 4
Well Construction and Groundwater Level Data
Palmer Street Texaco
196 W. Palmer Street
S&ME Project No. 1354-11-130B
FIGURES
SCALE:
DRAWN BY:
DATE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
ENGINEERING LICENSE NO: F-0176
1PALMER STREET TEXACO
196 W. PALMER ST., FRANKLIN, NC
INCIDENT NO. 5550
LOCATION MAP
SITEAS SHOWN
08-11-11
JDO
1354-11-130
SUBJECT PROPERTY
SCALE:
DRAWN BY:
DATE:
PRO. NO:
FIGURE NO.
WWW.SMEINC.COM
ENGINEERING LICENSE NO: F-0176
2PALMER STREET TEXACO
196 W. PALMER ST., FRANKLIN, NC
INCIDENT NO. 5550
MAP
TOPOGRAPHICAS SHOWN
10-11-12
JDO
1354-11-130B
SUBJECT PROPERTY
GRASS AREA
GRASS AREA
GRASS AREA
GRASS AREA
MW-1
MW-3
MW-6
MW-5FORMER
DISPENSER
ISLANDS
CANOPY
FORMER UST LOCATIONS
STORE
WEST PALME
R

S
T
R
E
E
T
MAPLE STREETAPPROXIMATE LOCATION
OF FORMER
UNDERGROUND
PRODUCT LINES
MW-1A
SCALE:
DRAWN BY:
DATE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
ENGINEERING LICENSE NO: F-0176
3PALMER STREET TEXACO
196 W. PALMER ST., FRANKLIN, NC
INCIDENT NO. 5550
MAP
SITE LAYOUTAS SHOWN
10-11-12
JDO
1354-11-130B
APPROXIMATE MONITORING WELL LOCATION
PREVIOUS MONITORING WELL LOCATION (NO LONGER ONSITE)
LEGEND
SITE FEATURES TRACED FROM 2010 AERIAL IMAGE PROVIDED BY MACON COUNTY MAPPING DEPARTMENT.
MW-2
MW-4
WWW.SMEINC.COM CHECKED BY:
PROJECT NO.
DATE:FIGURE NO.SCALE:
DRAWN BY:
ENGINEERING LICENSE NO:4MAP
WELL LOCATION
196 W. PALMER ST., FRANKLIN, NC
INCIDENT NO. 5550
PALMER STREET TEXACO
10-11-12AS SHOWN
1354-11-130B JDO
SAS1500' RADIUS1000' RADIUS1500' RADIUS1234567891011121314151617181920212223242526272829303132LEGENDWATER SUPPLY WELL LOCATIONMAP I.D. (SEE TABLE 3)DRAINAGE FEATUREWEST PALMER STREETMAPLE STRE
E
T 33
GRASS AREA
GRASS AREA
GRASS AREA
GRASS AREA
FORMER
DISPENSER
ISLANDS
CANOPY
FORMER UST LOCATIONS
STORE
WEST PALM
E
R

S
T
R
E
E
T
MAPLE STREETAPPROXIMATE LOCATION
OF FORMER
UNDERGROUND
PRODUCT LINES
SB-1A
SB-4
SB-2SB-3
SCALE:
DRAWN BY:
DATE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
ENGINEERING LICENSE NO: F-0176
5PALMER STREET TEXACO
196 W. PALMER ST., FRANKLIN, NC
INCIDENT NO. 5550
LOCATION MAP
SOIL SAMPLINGAS SHOWN
10-11-12
JDO
1354-11-130B
APPROXIMATE SOIL BORING LOCATION
LEGEND
SITE FEATURES TRACED FROM 2010 AERIAL IMAGE PROVIDED BY MACON COUNTY MAPPING DEPARTMENT.
GRASS AREA
GRASS AREA
GRASS AREA
GRASS AREA
MW-1
MW-3
MW-6
MW-5
MW-4
NONE >2L
FORMER
DISPENSER
ISLANDS
CANOPY
FORMER UST LOCATIONS
STORE
WEST PALME
R

S
T
R
E
E
T
MAPLE STREETAPPROXIMATE LOCATION
OF FORMER
UNDERGROUND
PRODUCT LINES
MW-1A
SCALE:
DRAWN BY:
DATE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
ENGINEERING LICENSE NO: F-0176
6PALMER STREET TEXACO
196 W. PALMER ST., FRANKLIN, NC
INCIDENT NO. 5550
MAP
GROUNDWATER QUALITYAS SHOWN
10-11-12
JDO
1354-11-130B
APPROXIMATE MONITORING WELL LOCATION
PREVIOUS MONITORING WELL LOCATION
LEGEND
SITE FEATURES TRACED FROM 2010 AERIAL IMAGE PROVIDED BY MACON COUNTY MAPPING DEPARTMENT.
COMPOUNDS LISTED EXCEED THEIR RESPECTIVE NORTH CAROLINA GROUNDWATER QUALITY STANDARDS (2L STANDARDS)
BENZENE 240 ȝJO
MTBE 250 ȝJO
NAPHTHALENE 17 ȝJO
BENZENE 47 ȝJO
CHLOROMETHANE 3.3 ȝJO
NAPHTHALENE 140 ȝJO
n-PROPYLBENZENE 130 ȝJO
C5-C8 ALIPHATICS 1710 ȝJO
C9-C18 ALIPHATICS 1780 ȝJO
C9-C22 AROMATICS 1080 ȝJO
BENZENE 54 ȝJO
NAPHTHALENE 31 ȝJO
MW-2
GRASS AREA
GRASS AREA
GRASS AREA
GRASS AREA
MW-1
MW-2
MW-3
MW-6
MW-5
MW-4
8000 GAL. UST
6000 GAL. UST
STORE
WEST PALM
E
R

S
T
R
E
E
T
MAPLE STREETMW-1A
SCALE:
DRAWN BY:
DATE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM
ENGINEERING LICENSE NO: F-0176
7PALMER STREET TEXACO
196 W. PALMER ST., FRANKLIN, NC
INCIDENT NO. 5550
ELEVATIONS MAP
GROUNDWATERAS SHOWN
10-11-12
JDO
1354-11-130B
APPROXIMATE MONITORING WELL LOCATION
PREVIOUS MONITORING WELL LOCATION (NO LONGER ONSITE)
LEGEND
SITE FEATURES TRACED FROM 2010 AERIAL IMAGE PROVIDED BY MACON COUNTY MAPPING DEPARTMENT.
(95.57)
(95.98)
(95.46)
(95.50)
(95.57)GROUNDWATER ELEVATION (FEET,RELATIVE) ON 8-16-12
APPENDIX I
Well Sampling Forms and Site Photographs
Palmer Street Texaco
196 W. Palmer Street, Franklin, NC
S&ME Project # 1354-11-130B
Taken by: SAS Date Taken: 8/15/2012
1 Installation of boring MW-1A prior to monitoring well installation.2 Monitoring well MW-1A prior to pouring the concrete pad and
installing the steel well cover.
3 Development of monitoring well MW-1A.4 View of completed monitoring well MW-1A.
APPENDIX II
Request for Water Supply Well Information Letter and Responses
APPENDIX III
Laboratory Report and Chain-of-Custody Form
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
NCDENR-DWM-UST Section
1637 Mail Service Ctr.
Raleigh, NC 27699
Attention: Linda Blalock
NH17015Lot Number:
5550Project Number:
Palmer Street TexacoProject Name:
08/31/2012Date Completed:
Lucas Odom
Project Manager
*NH17015*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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Shealy Environmental Services, Inc.
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
NCDENR-DWM-UST Section
Lot Number: NH17015
SC DHEC No: 32010 NC DENR No: 329 NELAC No: E87653
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
GC/MS VOC
Due to large detections of target compounds, sample -001 was analyzed at a 500X and 2000X dilution causing surrogates to recover outside of
method criteria. No corrective action was required as it is known that dilutions of 5X and greater may impact surrogate recoveries.
The LCS associated with batch 92388 recovered two compounds marginally outside of method criteria. No corrective action was required as all
associated samples were non-detect for these compounds.
Page: 2 of 50
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
NCDENR-DWM-UST Section
Lot Number: NH17015

Sample Number Sample ID Matrix Date Sampled Date Received
001 08/15/2012 0900SB-2 Solid 08/17/2012
002 08/15/2012 0910SB-3 Solid 08/17/2012
003 08/15/2012 0920SB-1A Solid 08/17/2012
004 08/15/2012 0930SB-4 Solid 08/17/2012
005 08/16/2012 1015MW-2 Aqueous 08/17/2012
006 08/16/2012 1040MW-4 Aqueous 08/17/2012
007 08/16/2012 1110MW-3 Aqueous 08/17/2012
008 08/16/2012 1145MW-1A Aqueous 08/17/2012
(8 samples)
Page: 3 of 50
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
NCDENR-DWM-UST Section
Lot Number: NH17015

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SB-2 Solid Acetone 8260B 9400 J ug/kg 7
001 SB-2 Solid Benzene 8260B 1000 J ug/kg 7
001 SB-2 Solid n-Butylbenzene 8260B 28000 ug/kg 7
001 SB-2 Solid sec-Butylbenzene 8260B 7200 ug/kg 7
001 SB-2 Solid Ethylbenzene 8260B 130000 ug/kg 7
001 SB-2 Solid p-Isopropyltoluene 8260B 3700 ug/kg 8
001 SB-2 Solid Naphthalene 8260B 64000 ug/kg 8
001 SB-2 Solid n-Propylbenzene 8260B 77000 ug/kg 8
001 SB-2 Solid Toluene 8260B 23000 ug/kg 8
001 SB-2 Solid 1,2,4-Trimethylbenzene 8260B 410000 ug/kg 8
001 SB-2 Solid 1,3,5-Trimethylbenzene 8260B 150000 ug/kg 8
001 SB-2 Solid Xylenes (total)8260B 490000 ug/kg 8
002 SB-3 Solid Acetone 8260B 140 ug/kg 9
002 SB-3 Solid Benzene 8260B 110 ug/kg 9
002 SB-3 Solid 2-Butanone (MEK)8260B 12 ug/kg 9
002 SB-3 Solid Chloroform 8260B 20 ug/kg 9
002 SB-3 Solid Ethylbenzene 8260B 130 ug/kg 9
002 SB-3 Solid Isopropylbenzene 8260B 6.4 ug/kg 9
002 SB-3 Solid Methyl tertiary butyl ether (MTBE)8260B 24 ug/kg 10
002 SB-3 Solid Naphthalene 8260B 9.9 ug/kg 10
002 SB-3 Solid n-Propylbenzene 8260B 17 ug/kg 10
002 SB-3 Solid 1,2,4-Trimethylbenzene 8260B 92 ug/kg 10
002 SB-3 Solid 1,3,5-Trimethylbenzene 8260B 30 ug/kg 10
002 SB-3 Solid Xylenes (total)8260B 330 ug/kg 10
003 SB-1A Solid Acetone 8260B 54 ug/kg 11
003 SB-1A Solid Benzene 8260B 1.6 J ug/kg 11
003 SB-1A Solid Chloroform 8260B 1.3 J ug/kg 11
003 SB-1A Solid Methyl tertiary butyl ether (MTBE)8260B 1.5 J ug/kg 12
003 SB-1A Solid Naphthalene 8260B 2.2 J ug/kg 12
004 SB-4 Solid Acetone 8260B 550 J ug/kg 13
004 SB-4 Solid Benzene 8260B 140 J ug/kg 13
004 SB-4 Solid n-Butylbenzene 8260B 1600 ug/kg 13
004 SB-4 Solid sec-Butylbenzene 8260B 500 ug/kg 13
004 SB-4 Solid Chloroform 8260B 140 J ug/kg 13
004 SB-4 Solid Ethylbenzene 8260B 4500 ug/kg 13
004 SB-4 Solid Isopropylbenzene 8260B 880 ug/kg 13
004 SB-4 Solid p-Isopropyltoluene 8260B 290 J ug/kg 13
004 SB-4 Solid Methyl tertiary butyl ether (MTBE)8260B 30 J ug/kg 14
004 SB-4 Solid Naphthalene 8260B 2600 ug/kg 14
004 SB-4 Solid n-Propylbenzene 8260B 3300 ug/kg 14
004 SB-4 Solid Toluene 8260B 110 J ug/kg 14
004 SB-4 Solid 1,2,4-Trimethylbenzene 8260B 6200 ug/kg 14
004 SB-4 Solid 1,3,5-Trimethylbenzene 8260B 310 ug/kg 14
004 SB-4 Solid Xylenes (total)8260B 770 ug/kg 14
005 MW-2 Aqueous Benzene SM 6200B 54 ug/L 15
Page: 4 of 50
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Executive Summary (Continued)
Lot Number: NH17015
Sample Sample ID Matrix Parameter Method Result Q Units Page
005 MW-2 Aqueous n-Butylbenzene SM 6200B 3.6 ug/L 15
005 MW-2 Aqueous sec-Butylbenzene SM 6200B 1.3 ug/L 15
005 MW-2 Aqueous Chloroform SM 6200B 0.37 J ug/L 15
005 MW-2 Aqueous Diisopropyl ether (IPE)SM 6200B 1.7 ug/L 15
005 MW-2 Aqueous Ethylbenzene SM 6200B 73 ug/L 15
005 MW-2 Aqueous Isopropylbenzene (Cumene)SM 6200B 4.1 ug/L 15
005 MW-2 Aqueous p-Isopropyltoluene (p-Cymene)SM 6200B 0.13 J ug/L 15
005 MW-2 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B 14 ug/L 16
005 MW-2 Aqueous Naphthalene SM 6200B 31 ug/L 16
005 MW-2 Aqueous n-Propylbenzene SM 6200B 12 ug/L 16
005 MW-2 Aqueous Toluene SM 6200B 1.7 ug/L 16
005 MW-2 Aqueous 1,3,5-Trimethylbenzene (Mesitylene)SM 6200B 0.43 J ug/L 16
005 MW-2 Aqueous 1,2,4-Trimethylbenzene SM 6200B 5.0 ug/L 16
005 MW-2 Aqueous m+p - Xylenes SM 6200B 12 ug/L 16
005 MW-2 Aqueous o - Xylenes SM 6200B 0.62 ug/L 16
006 MW-4 Aqueous n-Butylbenzene SM 6200B 0.58 ug/L 17
006 MW-4 Aqueous sec-Butylbenzene SM 6200B 0.90 ug/L 17
006 MW-4 Aqueous Chloromethane (Methyl chloride)SM 6200B 1.8 ug/L 17
006 MW-4 Aqueous Diisopropyl ether (IPE)SM 6200B 4.4 ug/L 17
006 MW-4 Aqueous Isopropylbenzene (Cumene)SM 6200B 5.2 ug/L 17
006 MW-4 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B 2.0 ug/L 18
006 MW-4 Aqueous Naphthalene SM 6200B 2.4 ug/L 18
006 MW-4 Aqueous n-Propylbenzene SM 6200B 4.2 ug/L 18
006 MW-4 Aqueous m+p - Xylenes SM 6200B 0.17 J ug/L 18
007 MW-3 Aqueous Benzene SM 6200B 240 ug/L 19
007 MW-3 Aqueous n-Butylbenzene SM 6200B 2.2 ug/L 19
007 MW-3 Aqueous sec-Butylbenzene SM 6200B 1.2 ug/L 19
007 MW-3 Aqueous Chloromethane (Methyl chloride)SM 6200B 1.9 ug/L 19
007 MW-3 Aqueous Diisopropyl ether (IPE)SM 6200B 9.4 ug/L 19
007 MW-3 Aqueous Ethylbenzene SM 6200B 56 ug/L 19
007 MW-3 Aqueous Isopropylbenzene (Cumene)SM 6200B 5.5 ug/L 19
007 MW-3 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B 250 ug/L 20
007 MW-3 Aqueous Naphthalene SM 6200B 17 ug/L 20
007 MW-3 Aqueous n-Propylbenzene SM 6200B 9.9 ug/L 20
007 MW-3 Aqueous Toluene SM 6200B 0.77 J ug/L 20
007 MW-3 Aqueous 1,2,4-Trimethylbenzene SM 6200B 1.8 ug/L 20
007 MW-3 Aqueous m+p - Xylenes SM 6200B 0.96 J ug/L 20
007 MW-3 Aqueous o - Xylenes SM 6200B 1.3 ug/L 20
008 MW-1A Aqueous Benzene SM 6200B 47 ug/L 21
008 MW-1A Aqueous n-Butylbenzene SM 6200B 12 ug/L 21
008 MW-1A Aqueous sec-Butylbenzene SM 6200B 6.8 ug/L 21
008 MW-1A Aqueous Chloroform SM 6200B 1.6 J ug/L 21
008 MW-1A Aqueous Chloromethane (Methyl chloride)SM 6200B 3.3 ug/L 21
008 MW-1A Aqueous Diisopropyl ether (IPE)SM 6200B 3.5 ug/L 21
008 MW-1A Aqueous Ethylbenzene SM 6200B 76 ug/L 21
008 MW-1A Aqueous Isopropylbenzene (Cumene)SM 6200B 39 ug/L 21
008 MW-1A Aqueous p-Isopropyltoluene (p-Cymene)SM 6200B 0.71 J ug/L 21
008 MW-1A Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B 7.3 ug/L 22
Page: 5 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Executive Summary (Continued)
Lot Number: NH17015
Sample Sample ID Matrix Parameter Method Result Q Units Page
008 MW-1A Aqueous Naphthalene SM 6200B 140 ug/L 22
008 MW-1A Aqueous n-Propylbenzene SM 6200B 130 ug/L 22
008 MW-1A Aqueous Toluene SM 6200B 23 ug/L 22
008 MW-1A Aqueous 1,3,5-Trimethylbenzene (Mesitylene)SM 6200B 13 ug/L 22
008 MW-1A Aqueous 1,2,4-Trimethylbenzene SM 6200B 56 ug/L 22
008 MW-1A Aqueous m+p - Xylenes SM 6200B 96 ug/L 22
008 MW-1A Aqueous o - Xylenes SM 6200B 13 ug/L 22
008 MW-1A Aqueous Lead 6010C 0.0028 J mg/L 22
(101 detections)
Page: 6 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
SB-2
NH17015-001
08/15/2012 0900
08/17/2012
Solid
% Solids:82.8 08/17/2012 1731
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 500 08/24/2012 0039 DD 92054 5.73
2 5035 8260B 2000 08/27/2012 1515 AAC 92260 5.73
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 9400 J 1ug/kg350011000
Benzene 71-43-2 8260B 1000 J 1ug/kg5802600
Bromobenzene 108-86-1 8260B ND 1ug/kg3702600
Bromochloromethane 74-97-5 8260B ND 1ug/kg5302600
Bromodichloromethane 75-27-4 8260B ND 1ug/kg9002600
Bromoform 75-25-2 8260B ND 1ug/kg3702600
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg9502600
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg13005300
n-Butylbenzene 104-51-8 8260B 28000 1ug/kg5302600
sec-Butylbenzene 135-98-8 8260B 7200 1ug/kg5302600
tert-Butylbenzene 98-06-6 8260B ND 1ug/kg5302600
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg9502600
Chlorobenzene 108-90-7 8260B ND 1ug/kg9002600
Chloroethane 75-00-3 8260B ND 1ug/kg6902600
Chloroform 67-66-3 8260B ND 1ug/kg4402600
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5302600
2-Chlorotoluene 95-49-8 8260B ND 1ug/kg14002600
4-Chlorotoluene 106-43-4 8260B ND 1ug/kg10002600
Dibromochloromethane 124-48-1 8260B ND 1ug/kg9002600
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4502600
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg9002600
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg9002600
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg9002600
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg8402600
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg3802600
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5302600
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg9002600
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4002600
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg7902600
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4802600
1,3-Dichloropropane 142-28-9 8260B ND 1ug/kg5302600
2,2-Dichloropropane 594-20-7 8260B ND 1ug/kg5802600
1,1-Dichloropropene 563-58-6 8260B ND 1ug/kg7902600
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg3602600
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4302600
Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/kg1602600
Ethylbenzene 100-41-4 8260B 130000 1ug/kg9002600
2-Hexanone 591-78-6 8260B ND 1ug/kg6905300
Isopropylbenzene 98-82-8 8260B ND 1ug/kg1202600
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 7 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
SB-2
NH17015-001
08/15/2012 0900
08/17/2012
Solid
% Solids:82.8 08/17/2012 1731
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 500 08/24/2012 0039 DD 92054 5.73
2 5035 8260B 2000 08/27/2012 1515 AAC 92260 5.73
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
p-Isopropyltoluene 99-87-6 8260B 3700 1ug/kg7402600
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2102600
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg7905300
Methylene chloride 75-09-2 8260B ND 1ug/kg14002600
Naphthalene 91-20-3 8260B 64000 1ug/kg9002600
n-Propylbenzene 103-65-1 8260B 77000 1ug/kg5302600
Styrene 100-42-5 8260B ND 1ug/kg5802600
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2502600
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2602600
Toluene 108-88-3 8260B 23000 1ug/kg9002600
1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/kg9002600
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg9002600
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4502600
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4202600
Trichloroethene 79-01-6 8260B ND 1ug/kg10002600
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg7902600
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/kg4502600
1,2,4-Trimethylbenzene 95-63-6 8260B 410000 1ug/kg9002600
1,3,5-Trimethylbenzene 108-67-8 8260B 150000 1ug/kg9002600
Vinyl acetate 108-05-4 8260B ND 1ug/kg4702600
Vinyl chloride 75-01-4 8260B ND 1ug/kg4502600
Xylenes (total)1330-20-7 8260B 490000 2ug/kg610011000
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
1,2-Dichloroethane-d4 N 0.00 53-142 N 0.00 53-142
Bromofluorobenzene N 0.00 47-138 N 0.00 47-138
Toluene-d8 N 0.00 68-124 N 0.00 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 8 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
SB-3
NH17015-002
08/15/2012 0910
08/17/2012
Solid
% Solids:88.1 08/17/2012 1731
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/22/2012 1328 AAC 91951 5.85
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 140 1ug/kg6.519
Benzene 71-43-2 8260B 110 1ug/kg1.14.9
Bromobenzene 108-86-1 8260B ND 1ug/kg0.684.9
Bromochloromethane 74-97-5 8260B ND 1ug/kg0.974.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.74.9
Bromoform 75-25-2 8260B ND 1ug/kg0.684.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.74.9
2-Butanone (MEK)78-93-3 8260B 12 1ug/kg2.39.7
n-Butylbenzene 104-51-8 8260B ND 1ug/kg0.974.9
sec-Butylbenzene 135-98-8 8260B ND 1ug/kg0.974.9
tert-Butylbenzene 98-06-6 8260B ND 1ug/kg0.974.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.74.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.74.9
Chloroethane 75-00-3 8260B ND 1ug/kg1.34.9
Chloroform 67-66-3 8260B 20 1ug/kg0.814.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg0.974.9
2-Chlorotoluene 95-49-8 8260B ND 1ug/kg2.64.9
4-Chlorotoluene 106-43-4 8260B ND 1ug/kg1.84.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.74.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.834.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.74.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.74.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.74.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.64.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.714.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg0.974.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.74.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.744.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.54.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.884.9
1,3-Dichloropropane 142-28-9 8260B ND 1ug/kg0.974.9
2,2-Dichloropropane 594-20-7 8260B ND 1ug/kg1.14.9
1,1-Dichloropropene 563-58-6 8260B ND 1ug/kg1.54.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.664.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.804.9
Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/kg0.304.9
Ethylbenzene 100-41-4 8260B 130 1ug/kg1.74.9
2-Hexanone 591-78-6 8260B ND 1ug/kg1.39.7
Isopropylbenzene 98-82-8 8260B 6.4 1ug/kg0.224.9
p-Isopropyltoluene 99-87-6 8260B ND 1ug/kg1.44.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 9 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
SB-3
NH17015-002
08/15/2012 0910
08/17/2012
Solid
% Solids:88.1 08/17/2012 1731
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/22/2012 1328 AAC 91951 5.85
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 24 1ug/kg0.394.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.59.7
Methylene chloride 75-09-2 8260B ND 1ug/kg2.54.9
Naphthalene 91-20-3 8260B 9.9 1ug/kg1.74.9
n-Propylbenzene 103-65-1 8260B 17 1ug/kg0.974.9
Styrene 100-42-5 8260B ND 1ug/kg1.14.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.464.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.494.9
Toluene 108-88-3 8260B ND 1ug/kg1.74.9
1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/kg1.74.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.74.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.834.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.774.9
Trichloroethene 79-01-6 8260B ND 1ug/kg1.84.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.54.9
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/kg0.834.9
1,2,4-Trimethylbenzene 95-63-6 8260B 92 1ug/kg1.74.9
1,3,5-Trimethylbenzene 108-67-8 8260B 30 1ug/kg1.74.9
Vinyl acetate 108-05-4 8260B ND 1ug/kg0.874.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.834.9
Xylenes (total)1330-20-7 8260B 330 1ug/kg2.84.9
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 53-142
Bromofluorobenzene 92 47-138
Toluene-d8 91 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 10 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
SB-1A
NH17015-003
08/15/2012 0920
08/17/2012
Solid
% Solids:73.2 08/17/2012 1731
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/22/2012 1351 AAC 91951 7.16
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 54 1ug/kg6.419
Benzene 71-43-2 8260B 1.6 J 1ug/kg1.04.8
Bromobenzene 108-86-1 8260B ND 1ug/kg0.674.8
Bromochloromethane 74-97-5 8260B ND 1ug/kg0.954.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg1.64.8
Bromoform 75-25-2 8260B ND 1ug/kg0.674.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg1.74.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg2.39.5
n-Butylbenzene 104-51-8 8260B ND 1ug/kg0.954.8
sec-Butylbenzene 135-98-8 8260B ND 1ug/kg0.954.8
tert-Butylbenzene 98-06-6 8260B ND 1ug/kg0.954.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg1.74.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg1.64.8
Chloroethane 75-00-3 8260B ND 1ug/kg1.24.8
Chloroform 67-66-3 8260B 1.3 J 1ug/kg0.794.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg0.954.8
2-Chlorotoluene 95-49-8 8260B ND 1ug/kg2.64.8
4-Chlorotoluene 106-43-4 8260B ND 1ug/kg1.84.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg1.64.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg0.814.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg1.64.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg1.64.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg1.64.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg1.54.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg0.704.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg0.954.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg1.64.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg0.734.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg1.44.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg0.874.8
1,3-Dichloropropane 142-28-9 8260B ND 1ug/kg0.954.8
2,2-Dichloropropane 594-20-7 8260B ND 1ug/kg1.04.8
1,1-Dichloropropene 563-58-6 8260B ND 1ug/kg1.44.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg0.654.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg0.784.8
Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/kg0.304.8
Ethylbenzene 100-41-4 8260B ND 1ug/kg1.64.8
2-Hexanone 591-78-6 8260B ND 1ug/kg1.29.5
Isopropylbenzene 98-82-8 8260B ND 1ug/kg0.224.8
p-Isopropyltoluene 99-87-6 8260B ND 1ug/kg1.34.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 11 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
SB-1A
NH17015-003
08/15/2012 0920
08/17/2012
Solid
% Solids:73.2 08/17/2012 1731
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 08/22/2012 1351 AAC 91951 7.16
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 1.5 J 1ug/kg0.384.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg1.49.5
Methylene chloride 75-09-2 8260B ND 1ug/kg2.54.8
Naphthalene 91-20-3 8260B 2.2 J 1ug/kg1.64.8
n-Propylbenzene 103-65-1 8260B ND 1ug/kg0.954.8
Styrene 100-42-5 8260B ND 1ug/kg1.04.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg0.454.8
Tetrachloroethene 127-18-4 8260B ND 1ug/kg0.484.8
Toluene 108-88-3 8260B ND 1ug/kg1.64.8
1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/kg1.64.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg1.64.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg0.814.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg0.754.8
Trichloroethene 79-01-6 8260B ND 1ug/kg1.84.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg1.44.8
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/kg0.814.8
1,2,4-Trimethylbenzene 95-63-6 8260B ND 1ug/kg1.64.8
1,3,5-Trimethylbenzene 108-67-8 8260B ND 1ug/kg1.64.8
Vinyl acetate 108-05-4 8260B ND 1ug/kg0.864.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg0.824.8
Xylenes (total)1330-20-7 8260B ND 1ug/kg2.84.8
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 109 53-142
Bromofluorobenzene 105 47-138
Toluene-d8 94 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 12 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
SB-4
NH17015-004
08/15/2012 0930
08/17/2012
Solid
% Solids:69.0 08/17/2012 1731
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 50 08/27/2012 1340 AAC 92260 5.82
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 550 J 2ug/kg4201200
Benzene 71-43-2 8260B 140 J 2ug/kg68310
Bromobenzene 108-86-1 8260B ND 2ug/kg44310
Bromochloromethane 74-97-5 8260B ND 2ug/kg62310
Bromodichloromethane 75-27-4 8260B ND 2ug/kg110310
Bromoform 75-25-2 8260B ND 2ug/kg44310
Bromomethane (Methyl bromide)74-83-9 8260B ND 2ug/kg110310
2-Butanone (MEK)78-93-3 8260B ND 2ug/kg150620
n-Butylbenzene 104-51-8 8260B 1600 2ug/kg62310
sec-Butylbenzene 135-98-8 8260B 500 2ug/kg62310
tert-Butylbenzene 98-06-6 8260B ND 2ug/kg62310
Carbon tetrachloride 56-23-5 8260B ND 2ug/kg110310
Chlorobenzene 108-90-7 8260B ND 2ug/kg110310
Chloroethane 75-00-3 8260B ND 2ug/kg81310
Chloroform 67-66-3 8260B 140 J 2ug/kg52310
Chloromethane (Methyl chloride)74-87-3 8260B ND 2ug/kg62310
2-Chlorotoluene 95-49-8 8260B ND 2ug/kg170310
4-Chlorotoluene 106-43-4 8260B ND 2ug/kg120310
Dibromochloromethane 124-48-1 8260B ND 2ug/kg110310
1,2-Dibromoethane (EDB)106-93-4 8260B ND 2ug/kg53310
1,2-Dichlorobenzene 95-50-1 8260B ND 2ug/kg110310
1,3-Dichlorobenzene 541-73-1 8260B ND 2ug/kg110310
1,4-Dichlorobenzene 106-46-7 8260B ND 2ug/kg110310
Dichlorodifluoromethane 75-71-8 8260B ND 2ug/kg100310
1,1-Dichloroethane 75-34-3 8260B ND 2ug/kg45310
1,2-Dichloroethane 107-06-2 8260B ND 2ug/kg62310
1,1-Dichloroethene 75-35-4 8260B ND 2ug/kg110310
cis-1,2-Dichloroethene 156-59-2 8260B ND 2ug/kg47310
trans-1,2-Dichloroethene 156-60-5 8260B ND 2ug/kg93310
1,2-Dichloropropane 78-87-5 8260B ND 2ug/kg57310
1,3-Dichloropropane 142-28-9 8260B ND 2ug/kg62310
2,2-Dichloropropane 594-20-7 8260B ND 2ug/kg68310
1,1-Dichloropropene 563-58-6 8260B ND 2ug/kg93310
cis-1,3-Dichloropropene 10061-01-5 8260B ND 2ug/kg42310
trans-1,3-Dichloropropene 10061-02-6 8260B ND 2ug/kg51310
Diisopropyl ether (IPE)108-20-3 8260B ND 2ug/kg19310
Ethylbenzene 100-41-4 8260B 4500 2ug/kg110310
2-Hexanone 591-78-6 8260B ND 2ug/kg81620
Isopropylbenzene 98-82-8 8260B 880 2ug/kg14310
p-Isopropyltoluene 99-87-6 8260B 290 J 2ug/kg87310
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 13 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
SB-4
NH17015-004
08/15/2012 0930
08/17/2012
Solid
% Solids:69.0 08/17/2012 1731
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 8260B 50 08/27/2012 1340 AAC 92260 5.82
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 30 J 2ug/kg25310
4-Methyl-2-pentanone 108-10-1 8260B ND 2ug/kg93620
Methylene chloride 75-09-2 8260B ND 2ug/kg160310
Naphthalene 91-20-3 8260B 2600 2ug/kg110310
n-Propylbenzene 103-65-1 8260B 3300 2ug/kg62310
Styrene 100-42-5 8260B ND 2ug/kg68310
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 2ug/kg29310
Tetrachloroethene 127-18-4 8260B ND 2ug/kg31310
Toluene 108-88-3 8260B 110 J 2ug/kg110310
1,2,3-Trichlorobenzene 87-61-6 8260B ND 2ug/kg110310
1,2,4-Trichlorobenzene 120-82-1 8260B ND 2ug/kg110310
1,1,1-Trichloroethane 71-55-6 8260B ND 2ug/kg53310
1,1,2-Trichloroethane 79-00-5 8260B ND 2ug/kg49310
Trichloroethene 79-01-6 8260B ND 2ug/kg120310
Trichlorofluoromethane 75-69-4 8260B ND 2ug/kg93310
1,2,3-Trichloropropane 96-18-4 8260B ND 2ug/kg53310
1,2,4-Trimethylbenzene 95-63-6 8260B 6200 2ug/kg110310
1,3,5-Trimethylbenzene 108-67-8 8260B 310 2ug/kg110310
Vinyl acetate 108-05-4 8260B ND 2ug/kg56310
Vinyl chloride 75-01-4 8260B ND 2ug/kg54310
Xylenes (total)1330-20-7 8260B 770 2ug/kg180310
AcceptanceRun 2
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 87 53-142
Bromofluorobenzene 63 47-138
Toluene-d8 68 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 14 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
MW-2
NH17015-005
08/16/2012 1015
08/17/2012
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 6200B SM 6200B 1 08/29/2012 1124 BDC 92388
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B 54 1ug/L0.0270.50
Bromobenzene 108-86-1 SM 6200B ND 1ug/L0.0270.50
Bromochloromethane 74-97-5 SM 6200B ND 1ug/L0.0550.50
Bromodichloromethane 75-27-4 SM 6200B ND 1ug/L0.170.50
Bromoform 75-25-2 SM 6200B ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B ND 1ug/L0.200.50
n-Butylbenzene 104-51-8 SM 6200B 3.6 1ug/L0.0170.50
sec-Butylbenzene 135-98-8 SM 6200B 1.3 1ug/L0.0100.50
tert-Butylbenzene 98-06-6 SM 6200B ND 1ug/L0.0370.50
Carbon tetrachloride 56-23-5 SM 6200B ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 SM 6200B ND 1ug/L0.170.50
Chloroethane 75-00-3 SM 6200B ND 1ug/L0.170.50
Chloroform 67-66-3 SM 6200B 0.37 J 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B ND 1ug/L0.170.50
2-Chlorotoluene 95-49-8 SM 6200B ND 1ug/L0.0590.50
4-Chlorotoluene 106-43-4 SM 6200B ND 1ug/L0.0190.50
Dibromochloromethane 124-48-1 SM 6200B ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B ND 1ug/L0.0610.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B ND 1ug/L0.0940.50
1,2-Dichlorobenzene 95-50-1 SM 6200B ND 1ug/L0.170.50
1,3-Dichlorobenzene 541-73-1 SM 6200B ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 SM 6200B ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 SM 6200B ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 SM 6200B ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 SM 6200B ND 1ug/L0.0230.50
1,1-Dichloroethene 75-35-4 SM 6200B ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B ND 1ug/L0.0870.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B ND 1ug/L0.0790.50
1,2-Dichloropropane 78-87-5 SM 6200B ND 1ug/L0.0810.50
1,3-Dichloropropane 142-28-9 SM 6200B ND 1ug/L0.0190.50
2,2-Dichloropropane 594-20-7 SM 6200B ND 1ug/L0.0600.50
1,1-Dichloropropene 563-58-6 SM 6200B ND 1ug/L0.0740.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B ND 1ug/L0.0900.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B ND 1ug/L0.180.50
Diisopropyl ether (IPE)108-20-3 SM 6200B 1.7 1ug/L0.0520.50
Ethanol 64-17-5 SM 6200B ND 1ug/L33100
Ethylbenzene 100-41-4 SM 6200B 73 1ug/L0.170.50
Hexachlorobutadiene 87-68-3 SM 6200B ND 1ug/L0.170.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B 4.1 1ug/L0.0290.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B 0.13 J 1ug/L0.0180.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 15 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
MW-2
NH17015-005
08/16/2012 1015
08/17/2012
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 6200B SM 6200B 1 08/29/2012 1124 BDC 92388
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B 14 1ug/L0.0190.50
Methylene chloride 75-09-2 SM 6200B ND 1ug/L0.170.50
Naphthalene 91-20-3 SM 6200B 31 1ug/L0.170.50
n-Propylbenzene 103-65-1 SM 6200B 12 1ug/L0.0240.50
Styrene 100-42-5 SM 6200B ND 1ug/L0.0150.50
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B ND 1ug/L0.0570.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 SM 6200B ND 1ug/L0.0140.50
Toluene 108-88-3 SM 6200B 1.7 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B ND 1ug/L0.300.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B ND 1ug/L0.170.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 SM 6200B ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 SM 6200B ND 1ug/L0.0310.50
Trichloroethene 79-01-6 SM 6200B ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 SM 6200B ND 1ug/L0.0510.50
1,2,3-Trichloropropane 96-18-4 SM 6200B ND 1ug/L0.330.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B 0.43 J 1ug/L0.170.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B 5.0 1ug/L0.170.50
Vinyl chloride 75-01-4 SM 6200B ND 1ug/L0.0650.50
m+p - Xylenes 179601-23-1 SM 6200B 12 1ug/L0.170.50
o - Xylenes 95-47-6 SM 6200B 0.62 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 94 52-138
Bromofluorobenzene 99 70-147
Toluene-d8 99 76-125
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 16 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
MW-4
NH17015-006
08/16/2012 1040
08/17/2012
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 6200B SM 6200B 1 08/29/2012 1145 BDC 92388
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B ND 1ug/L0.0270.50
Bromobenzene 108-86-1 SM 6200B ND 1ug/L0.0270.50
Bromochloromethane 74-97-5 SM 6200B ND 1ug/L0.0550.50
Bromodichloromethane 75-27-4 SM 6200B ND 1ug/L0.170.50
Bromoform 75-25-2 SM 6200B ND 1ug/L0.0100.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B ND 1ug/L0.200.50
n-Butylbenzene 104-51-8 SM 6200B 0.58 1ug/L0.0170.50
sec-Butylbenzene 135-98-8 SM 6200B 0.90 1ug/L0.0100.50
tert-Butylbenzene 98-06-6 SM 6200B ND 1ug/L0.0370.50
Carbon tetrachloride 56-23-5 SM 6200B ND 1ug/L0.0850.50
Chlorobenzene 108-90-7 SM 6200B ND 1ug/L0.170.50
Chloroethane 75-00-3 SM 6200B ND 1ug/L0.170.50
Chloroform 67-66-3 SM 6200B ND 1ug/L0.170.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B 1.8 1ug/L0.170.50
2-Chlorotoluene 95-49-8 SM 6200B ND 1ug/L0.0590.50
4-Chlorotoluene 106-43-4 SM 6200B ND 1ug/L0.0190.50
Dibromochloromethane 124-48-1 SM 6200B ND 1ug/L0.170.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B ND 1ug/L0.0610.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B ND 1ug/L0.0940.50
1,2-Dichlorobenzene 95-50-1 SM 6200B ND 1ug/L0.170.50
1,3-Dichlorobenzene 541-73-1 SM 6200B ND 1ug/L0.170.50
1,4-Dichlorobenzene 106-46-7 SM 6200B ND 1ug/L0.170.50
Dichlorodifluoromethane 75-71-8 SM 6200B ND 1ug/L0.0710.50
1,1-Dichloroethane 75-34-3 SM 6200B ND 1ug/L0.0540.50
1,2-Dichloroethane 107-06-2 SM 6200B ND 1ug/L0.0230.50
1,1-Dichloroethene 75-35-4 SM 6200B ND 1ug/L0.0940.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B ND 1ug/L0.0870.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B ND 1ug/L0.0790.50
1,2-Dichloropropane 78-87-5 SM 6200B ND 1ug/L0.0810.50
1,3-Dichloropropane 142-28-9 SM 6200B ND 1ug/L0.0190.50
2,2-Dichloropropane 594-20-7 SM 6200B ND 1ug/L0.0600.50
1,1-Dichloropropene 563-58-6 SM 6200B ND 1ug/L0.0740.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B ND 1ug/L0.0900.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B ND 1ug/L0.180.50
Diisopropyl ether (IPE)108-20-3 SM 6200B 4.4 1ug/L0.0520.50
Ethanol 64-17-5 SM 6200B ND 1ug/L33100
Ethylbenzene 100-41-4 SM 6200B ND 1ug/L0.170.50
Hexachlorobutadiene 87-68-3 SM 6200B ND 1ug/L0.170.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B 5.2 1ug/L0.0290.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B ND 1ug/L0.0180.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 17 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
MW-4
NH17015-006
08/16/2012 1040
08/17/2012
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 6200B SM 6200B 1 08/29/2012 1145 BDC 92388
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B 2.0 1ug/L0.0190.50
Methylene chloride 75-09-2 SM 6200B ND 1ug/L0.170.50
Naphthalene 91-20-3 SM 6200B 2.4 1ug/L0.170.50
n-Propylbenzene 103-65-1 SM 6200B 4.2 1ug/L0.0240.50
Styrene 100-42-5 SM 6200B ND 1ug/L0.0150.50
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B ND 1ug/L0.0570.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B ND 1ug/L0.0130.50
Tetrachloroethene 127-18-4 SM 6200B ND 1ug/L0.0140.50
Toluene 108-88-3 SM 6200B ND 1ug/L0.170.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B ND 1ug/L0.300.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B ND 1ug/L0.170.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B ND 1ug/L0.170.50
1,1,1-Trichloroethane 71-55-6 SM 6200B ND 1ug/L0.0290.50
1,1,2-Trichloroethane 79-00-5 SM 6200B ND 1ug/L0.0310.50
Trichloroethene 79-01-6 SM 6200B ND 1ug/L0.0240.50
Trichlorofluoromethane 75-69-4 SM 6200B ND 1ug/L0.0510.50
1,2,3-Trichloropropane 96-18-4 SM 6200B ND 1ug/L0.330.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B ND 1ug/L0.170.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B ND 1ug/L0.170.50
Vinyl chloride 75-01-4 SM 6200B ND 1ug/L0.0650.50
m+p - Xylenes 179601-23-1 SM 6200B 0.17 J 1ug/L0.170.50
o - Xylenes 95-47-6 SM 6200B ND 1ug/L0.170.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 94 52-138
Bromofluorobenzene 100 70-147
Toluene-d8 99 76-125
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 18 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
MW-3
NH17015-007
08/16/2012 1110
08/17/2012
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 6200B SM 6200B 2 08/29/2012 1522 BDC 92388
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B 240 1ug/L0.0541.0
Bromobenzene 108-86-1 SM 6200B ND 1ug/L0.0541.0
Bromochloromethane 74-97-5 SM 6200B ND 1ug/L0.111.0
Bromodichloromethane 75-27-4 SM 6200B ND 1ug/L0.341.0
Bromoform 75-25-2 SM 6200B ND 1ug/L0.0201.0
Bromomethane (Methyl bromide)74-83-9 SM 6200B ND 1ug/L0.411.0
n-Butylbenzene 104-51-8 SM 6200B 2.2 1ug/L0.0331.0
sec-Butylbenzene 135-98-8 SM 6200B 1.2 1ug/L0.0211.0
tert-Butylbenzene 98-06-6 SM 6200B ND 1ug/L0.0741.0
Carbon tetrachloride 56-23-5 SM 6200B ND 1ug/L0.171.0
Chlorobenzene 108-90-7 SM 6200B ND 1ug/L0.341.0
Chloroethane 75-00-3 SM 6200B ND 1ug/L0.341.0
Chloroform 67-66-3 SM 6200B ND 1ug/L0.341.0
Chloromethane (Methyl chloride)74-87-3 SM 6200B 1.9 1ug/L0.351.0
2-Chlorotoluene 95-49-8 SM 6200B ND 1ug/L0.121.0
4-Chlorotoluene 106-43-4 SM 6200B ND 1ug/L0.0381.0
Dibromochloromethane 124-48-1 SM 6200B ND 1ug/L0.341.0
1,2-Dibromoethane (EDB)106-93-4 SM 6200B ND 1ug/L0.121.0
Dibromomethane (Methylene bromide)74-95-3 SM 6200B ND 1ug/L0.191.0
1,2-Dichlorobenzene 95-50-1 SM 6200B ND 1ug/L0.341.0
1,3-Dichlorobenzene 541-73-1 SM 6200B ND 1ug/L0.341.0
1,4-Dichlorobenzene 106-46-7 SM 6200B ND 1ug/L0.341.0
Dichlorodifluoromethane 75-71-8 SM 6200B ND 1ug/L0.141.0
1,1-Dichloroethane 75-34-3 SM 6200B ND 1ug/L0.111.0
1,2-Dichloroethane 107-06-2 SM 6200B ND 1ug/L0.0471.0
1,1-Dichloroethene 75-35-4 SM 6200B ND 1ug/L0.191.0
cis-1,2-Dichloroethene 156-59-2 SM 6200B ND 1ug/L0.171.0
trans-1,2-Dichloroethene 156-60-5 SM 6200B ND 1ug/L0.161.0
1,2-Dichloropropane 78-87-5 SM 6200B ND 1ug/L0.161.0
1,3-Dichloropropane 142-28-9 SM 6200B ND 1ug/L0.0381.0
2,2-Dichloropropane 594-20-7 SM 6200B ND 1ug/L0.121.0
1,1-Dichloropropene 563-58-6 SM 6200B ND 1ug/L0.151.0
cis-1,3-Dichloropropene 10061-01-5 SM 6200B ND 1ug/L0.181.0
trans-1,3-Dichloropropene 10061-02-6 SM 6200B ND 1ug/L0.361.0
Diisopropyl ether (IPE)108-20-3 SM 6200B 9.4 1ug/L0.101.0
Ethanol 64-17-5 SM 6200B ND 1ug/L66200
Ethylbenzene 100-41-4 SM 6200B 56 1ug/L0.341.0
Hexachlorobutadiene 87-68-3 SM 6200B ND 1ug/L0.341.0
Isopropylbenzene (Cumene)98-82-8 SM 6200B 5.5 1ug/L0.0581.0
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B ND 1ug/L0.0351.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 19 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
MW-3
NH17015-007
08/16/2012 1110
08/17/2012
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 6200B SM 6200B 2 08/29/2012 1522 BDC 92388
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B 250 1ug/L0.0381.0
Methylene chloride 75-09-2 SM 6200B ND 1ug/L0.341.0
Naphthalene 91-20-3 SM 6200B 17 1ug/L0.341.0
n-Propylbenzene 103-65-1 SM 6200B 9.9 1ug/L0.0471.0
Styrene 100-42-5 SM 6200B ND 1ug/L0.0301.0
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B ND 1ug/L0.111.0
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B ND 1ug/L0.0261.0
Tetrachloroethene 127-18-4 SM 6200B ND 1ug/L0.0291.0
Toluene 108-88-3 SM 6200B 0.77 J 1ug/L0.341.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B ND 1ug/L0.601.0
1,2,3-Trichlorobenzene 87-61-6 SM 6200B ND 1ug/L0.341.0
1,2,4-Trichlorobenzene 120-82-1 SM 6200B ND 1ug/L0.341.0
1,1,1-Trichloroethane 71-55-6 SM 6200B ND 1ug/L0.0581.0
1,1,2-Trichloroethane 79-00-5 SM 6200B ND 1ug/L0.0621.0
Trichloroethene 79-01-6 SM 6200B ND 1ug/L0.0491.0
Trichlorofluoromethane 75-69-4 SM 6200B ND 1ug/L0.101.0
1,2,3-Trichloropropane 96-18-4 SM 6200B ND 1ug/L0.661.0
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B ND 1ug/L0.341.0
1,2,4-Trimethylbenzene 95-63-6 SM 6200B 1.8 1ug/L0.341.0
Vinyl chloride 75-01-4 SM 6200B ND 1ug/L0.131.0
m+p - Xylenes 179601-23-1 SM 6200B 0.96 J 1ug/L0.341.0
o - Xylenes 95-47-6 SM 6200B 1.3 1ug/L0.341.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 91 52-138
Bromofluorobenzene 98 70-147
Toluene-d8 100 76-125
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 20 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
MW-1A
NH17015-008
08/16/2012 1145
08/17/2012
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 6200B SM 6200B 4 08/29/2012 1543 BDC 92388
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzene 71-43-2 SM 6200B 47 1ug/L0.112.0
Bromobenzene 108-86-1 SM 6200B ND 1ug/L0.112.0
Bromochloromethane 74-97-5 SM 6200B ND 1ug/L0.222.0
Bromodichloromethane 75-27-4 SM 6200B ND 1ug/L0.682.0
Bromoform 75-25-2 SM 6200B ND 1ug/L0.0412.0
Bromomethane (Methyl bromide)74-83-9 SM 6200B ND 1ug/L0.812.0
n-Butylbenzene 104-51-8 SM 6200B 12 1ug/L0.0672.0
sec-Butylbenzene 135-98-8 SM 6200B 6.8 1ug/L0.0422.0
tert-Butylbenzene 98-06-6 SM 6200B ND 1ug/L0.152.0
Carbon tetrachloride 56-23-5 SM 6200B ND 1ug/L0.342.0
Chlorobenzene 108-90-7 SM 6200B ND 1ug/L0.682.0
Chloroethane 75-00-3 SM 6200B ND 1ug/L0.682.0
Chloroform 67-66-3 SM 6200B 1.6 J 1ug/L0.682.0
Chloromethane (Methyl chloride)74-87-3 SM 6200B 3.3 1ug/L0.702.0
2-Chlorotoluene 95-49-8 SM 6200B ND 1ug/L0.242.0
4-Chlorotoluene 106-43-4 SM 6200B ND 1ug/L0.0762.0
Dibromochloromethane 124-48-1 SM 6200B ND 1ug/L0.682.0
1,2-Dibromoethane (EDB)106-93-4 SM 6200B ND 1ug/L0.242.0
Dibromomethane (Methylene bromide)74-95-3 SM 6200B ND 1ug/L0.382.0
1,2-Dichlorobenzene 95-50-1 SM 6200B ND 1ug/L0.682.0
1,3-Dichlorobenzene 541-73-1 SM 6200B ND 1ug/L0.682.0
1,4-Dichlorobenzene 106-46-7 SM 6200B ND 1ug/L0.682.0
Dichlorodifluoromethane 75-71-8 SM 6200B ND 1ug/L0.282.0
1,1-Dichloroethane 75-34-3 SM 6200B ND 1ug/L0.212.0
1,2-Dichloroethane 107-06-2 SM 6200B ND 1ug/L0.0932.0
1,1-Dichloroethene 75-35-4 SM 6200B ND 1ug/L0.382.0
cis-1,2-Dichloroethene 156-59-2 SM 6200B ND 1ug/L0.352.0
trans-1,2-Dichloroethene 156-60-5 SM 6200B ND 1ug/L0.322.0
1,2-Dichloropropane 78-87-5 SM 6200B ND 1ug/L0.322.0
1,3-Dichloropropane 142-28-9 SM 6200B ND 1ug/L0.0762.0
2,2-Dichloropropane 594-20-7 SM 6200B ND 1ug/L0.242.0
1,1-Dichloropropene 563-58-6 SM 6200B ND 1ug/L0.302.0
cis-1,3-Dichloropropene 10061-01-5 SM 6200B ND 1ug/L0.362.0
trans-1,3-Dichloropropene 10061-02-6 SM 6200B ND 1ug/L0.722.0
Diisopropyl ether (IPE)108-20-3 SM 6200B 3.5 1ug/L0.212.0
Ethanol 64-17-5 SM 6200B ND 1ug/L130400
Ethylbenzene 100-41-4 SM 6200B 76 1ug/L0.682.0
Hexachlorobutadiene 87-68-3 SM 6200B ND 1ug/L0.682.0
Isopropylbenzene (Cumene)98-82-8 SM 6200B 39 1ug/L0.122.0
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B 0.71 J 1ug/L0.0712.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 21 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDENR-DWM-UST Section
MW-1A
NH17015-008
08/16/2012 1145
08/17/2012
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 6200B SM 6200B 4 08/29/2012 1543 BDC 92388
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B 7.3 1ug/L0.0762.0
Methylene chloride 75-09-2 SM 6200B ND 1ug/L0.682.0
Naphthalene 91-20-3 SM 6200B 140 1ug/L0.682.0
n-Propylbenzene 103-65-1 SM 6200B 130 1ug/L0.0952.0
Styrene 100-42-5 SM 6200B ND 1ug/L0.0602.0
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B ND 1ug/L0.232.0
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B ND 1ug/L0.0522.0
Tetrachloroethene 127-18-4 SM 6200B ND 1ug/L0.0572.0
Toluene 108-88-3 SM 6200B 23 1ug/L0.682.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B ND 1ug/L1.22.0
1,2,3-Trichlorobenzene 87-61-6 SM 6200B ND 1ug/L0.682.0
1,2,4-Trichlorobenzene 120-82-1 SM 6200B ND 1ug/L0.682.0
1,1,1-Trichloroethane 71-55-6 SM 6200B ND 1ug/L0.122.0
1,1,2-Trichloroethane 79-00-5 SM 6200B ND 1ug/L0.122.0
Trichloroethene 79-01-6 SM 6200B ND 1ug/L0.0982.0
Trichlorofluoromethane 75-69-4 SM 6200B ND 1ug/L0.202.0
1,2,3-Trichloropropane 96-18-4 SM 6200B ND 1ug/L1.32.0
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B 13 1ug/L0.682.0
1,2,4-Trimethylbenzene 95-63-6 SM 6200B 56 1ug/L0.682.0
Vinyl chloride 75-01-4 SM 6200B ND 1ug/L0.262.0
m+p - Xylenes 179601-23-1 SM 6200B 96 1ug/L0.682.0
o - Xylenes 95-47-6 SM 6200B 13 1ug/L0.682.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 90 52-138
Bromofluorobenzene 99 70-147
Toluene-d8 100 76-125
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3030 C 6010C 1 08/20/2012 2126 CDF 08/17/2012 1526 91592
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Lead 7439-92-1 6010C 0.0028 J 1mg/L0.00200.010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
* = Reportable result (only when report all runs)
Page: 22 of 50
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 23 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:NQ91951-001
91951 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 08/22/2012 0810206.7 ug/kg1
Benzene ND 08/22/2012 08105.0 1.1 ug/kg1
Bromobenzene ND 08/22/2012 08105.0 0.70 ug/kg1
Bromochloromethane ND 08/22/2012 08105.0 1.0 ug/kg1
Bromodichloromethane ND 08/22/2012 08105.0 1.7 ug/kg1
Bromoform ND 08/22/2012 08105.0 0.70 ug/kg1
Bromomethane (Methyl bromide)ND 08/22/2012 08105.0 1.8 ug/kg1
2-Butanone (MEK)ND 08/22/2012 0810102.4 ug/kg1
n-Butylbenzene ND 08/22/2012 08105.0 1.0 ug/kg1
tert-Butylbenzene ND 08/22/2012 08105.0 1.0 ug/kg1
sec-Butylbenzene ND 08/22/2012 08105.0 1.0 ug/kg1
Carbon tetrachloride ND 08/22/2012 08105.0 1.8 ug/kg1
Chlorobenzene ND 08/22/2012 08105.0 1.7 ug/kg1
Chloroethane ND 08/22/2012 08105.0 1.3 ug/kg1
Chloroform ND 08/22/2012 08105.0 0.83 ug/kg1
Chloromethane (Methyl chloride)ND 08/22/2012 08105.0 1.0 ug/kg1
4-Chlorotoluene ND 08/22/2012 08105.0 1.9 ug/kg1
2-Chlorotoluene ND 08/22/2012 08105.0 2.7 ug/kg1
Dibromochloromethane ND 08/22/2012 08105.0 1.7 ug/kg1
1,2-Dibromoethane (EDB)ND 08/22/2012 08105.0 0.85 ug/kg1
1,4-Dichlorobenzene ND 08/22/2012 08105.0 1.7 ug/kg1
1,3-Dichlorobenzene ND 08/22/2012 08105.0 1.7 ug/kg1
1,2-Dichlorobenzene ND 08/22/2012 08105.0 1.7 ug/kg1
Dichlorodifluoromethane ND 08/22/2012 08105.0 1.6 ug/kg1
1,2-Dichloroethane ND 08/22/2012 08105.0 1.0 ug/kg1
1,1-Dichloroethane ND 08/22/2012 08105.0 0.73 ug/kg1
cis-1,2-Dichloroethene ND 08/22/2012 08105.0 0.76 ug/kg1
1,1-Dichloroethene ND 08/22/2012 08105.0 1.7 ug/kg1
trans-1,2-Dichloroethene ND 08/22/2012 08105.0 1.5 ug/kg1
1,2-Dichloropropane ND 08/22/2012 08105.0 0.91 ug/kg1
2,2-Dichloropropane ND 08/22/2012 08105.0 1.1 ug/kg1
1,3-Dichloropropane ND 08/22/2012 08105.0 1.0 ug/kg1
trans-1,3-Dichloropropene ND 08/22/2012 08105.0 0.82 ug/kg1
cis-1,3-Dichloropropene ND 08/22/2012 08105.0 0.68 ug/kg1
1,1-Dichloropropene ND 08/22/2012 08105.0 1.5 ug/kg1
Diisopropyl ether (IPE)ND 08/22/2012 08105.0 0.31 ug/kg1
Ethylbenzene ND 08/22/2012 08105.0 1.7 ug/kg1
2-Hexanone ND 08/22/2012 0810101.3 ug/kg1
Isopropylbenzene ND 08/22/2012 08105.0 0.23 ug/kg1
p-Isopropyltoluene ND 08/22/2012 08105.0 1.4 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 08/22/2012 08105.0 0.40 ug/kg1
4-Methyl-2-pentanone ND 08/22/2012 0810101.5 ug/kg1
Methylene chloride ND 08/22/2012 08105.0 2.6 ug/kg1
Naphthalene ND 08/22/2012 08105.0 1.7 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 24 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:NQ91951-001
91951 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
n-Propylbenzene ND 08/22/2012 08105.0 1.0 ug/kg1
Styrene ND 08/22/2012 08105.0 1.1 ug/kg1
1,1,2,2-Tetrachloroethane ND 08/22/2012 08105.0 0.47 ug/kg1
Tetrachloroethene ND 08/22/2012 08105.0 0.50 ug/kg1
Toluene ND 08/22/2012 08105.0 1.7 ug/kg1
1,2,3-Trichlorobenzene ND 08/22/2012 08105.0 1.7 ug/kg1
1,2,4-Trichlorobenzene ND 08/22/2012 08105.0 1.7 ug/kg1
1,1,2-Trichloroethane ND 08/22/2012 08105.0 0.79 ug/kg1
1,1,1-Trichloroethane ND 08/22/2012 08105.0 0.85 ug/kg1
Trichloroethene ND 08/22/2012 08105.0 1.9 ug/kg1
Trichlorofluoromethane ND 08/22/2012 08105.0 1.5 ug/kg1
1,2,3-Trichloropropane ND 08/22/2012 08105.0 0.85 ug/kg1
1,2,4-Trimethylbenzene ND 08/22/2012 08105.0 1.7 ug/kg1
1,3,5-Trimethylbenzene ND 08/22/2012 08105.0 1.7 ug/kg1
Vinyl acetate ND 08/22/2012 08105.0 0.90 ug/kg1
Vinyl chloride ND 08/22/2012 08105.0 0.86 ug/kg1
Xylenes (total)ND 08/22/2012 08105.0 2.9 ug/kg1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 112 47-138
1,2-Dichloroethane-d4 117 53-142
Toluene-d8 90 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 25 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:NQ91951-002
91951 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 86 08/22/2012 08548610042-1491
Benzene 49 08/22/2012 0854985069-1231
Bromobenzene 48 08/22/2012 0854955053-1371
Bromochloromethane 48 08/22/2012 0854975070-1211
Bromodichloromethane 46 08/22/2012 0854925069-1211
Bromoform 46 08/22/2012 0854925061-1191
Bromomethane (Methyl bromide)42 08/22/2012 0854855010-1681
2-Butanone (MEK)87 08/22/2012 08548710057-1481
n-Butylbenzene 51 08/22/2012 08541025029-1521
tert-Butylbenzene 49 08/22/2012 0854985038-1491
sec-Butylbenzene 50 08/22/2012 0854995037-1471
Carbon tetrachloride 50 08/22/2012 08541005058-1361
Chlorobenzene 47 08/22/2012 0854935059-1291
Chloroethane 50 08/22/2012 08541005042-1631
Chloroform 48 08/22/2012 0854975071-1251
Chloromethane (Methyl chloride)52 08/22/2012 08541055034-1341
4-Chlorotoluene 48 08/22/2012 0854965053-1351
2-Chlorotoluene 48 08/22/2012 0854965053-1331
Dibromochloromethane 45 08/22/2012 0854895066-1191
1,2-Dibromoethane (EDB)45 08/22/2012 0854905074-1241
1,4-Dichlorobenzene 48 08/22/2012 0854965052-1331
1,3-Dichlorobenzene 50 08/22/2012 0854995051-1341
1,2-Dichlorobenzene 47 08/22/2012 0854955057-1311
Dichlorodifluoromethane 52 08/22/2012 08541055010-1571
1,2-Dichloroethane 46 08/22/2012 0854915067-1291
1,1-Dichloroethane 48 08/22/2012 0854975071-1271
cis-1,2-Dichloroethene 49 08/22/2012 0854985070-1221
1,1-Dichloroethene 50 08/22/2012 0854995069-1381
trans-1,2-Dichloroethene 49 08/22/2012 0854985068-1311
1,2-Dichloropropane 46 08/22/2012 0854935072-1241
2,2-Dichloropropane 52 08/22/2012 08541045059-1291
1,3-Dichloropropane 42 08/22/2012 0854845070-1301
trans-1,3-Dichloropropene 41 08/22/2012 0854825070-1241
cis-1,3-Dichloropropene 42 08/22/2012 0854835070-1261
1,1-Dichloropropene 49 08/22/2012 0854995060-1331
Diisopropyl ether (IPE)49 08/22/2012 0854985026-1431
Ethylbenzene 48 08/22/2012 0854975059-1281
2-Hexanone 83 08/22/2012 08548310054-1371
Isopropylbenzene 47 08/22/2012 0854955050-1361
p-Isopropyltoluene 50 08/22/2012 08541015036-1461
Methyl tertiary butyl ether (MTBE)50 08/22/2012 0854995070-1301
4-Methyl-2-pentanone 90 08/22/2012 08549010060-1341
Methylene chloride 45 08/22/2012 0854915070-1301
Naphthalene 44 08/22/2012 0854895054-1311
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 26 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:NQ91951-002
91951 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
n-Propylbenzene 49 08/22/2012 0854985041-1441
Styrene 51 08/22/2012 08541025054-1361
1,1,2,2-Tetrachloroethane 48 08/22/2012 0854955069-1321
Tetrachloroethene 47 08/22/2012 0854935045-1501
Toluene 36 08/22/2012 0854725061-1291
1,2,3-Trichlorobenzene 42 08/22/2012 0854855040-1431
1,2,4-Trichlorobenzene 47 08/22/2012 0854955034-1451
1,1,2-Trichloroethane 42 08/22/2012 0854845055-1281
1,1,1-Trichloroethane 50 08/22/2012 08541005063-1281
Trichloroethene 49 08/22/2012 0854985062-1261
Trichlorofluoromethane 50 08/22/2012 08541005045-1381
1,2,3-Trichloropropane 48 08/22/2012 0854955067-1261
1,2,4-Trimethylbenzene 49 08/22/2012 0854975047-1381
1,3,5-Trimethylbenzene 49 08/22/2012 0854995046-1391
Vinyl acetate 57 08/22/2012 08541135055-1281
Vinyl chloride 55 08/22/2012 08541095042-1321
Xylenes (total)99 08/22/2012 08549910058-1281
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 103 47-138
1,2-Dichloroethane-d4 101 53-142
Toluene-d8 90 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 27 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:NQ91951-003
91951 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 80 08/22/2012 07238010042-1496.9 201
Benzene 44 08/22/2012 0723875069-12312 201
Bromobenzene 43 08/22/2012 0723855053-13711 201
Bromochloromethane 43 08/22/2012 0723855070-12112 201
Bromodichloromethane 41 08/22/2012 0723825069-12111 201
Bromoform 40 08/22/2012 0723805061-11913 201
Bromomethane (Methyl bromide)36 08/22/2012 0723735010-16815 201
2-Butanone (MEK)85 08/22/2012 07238510057-1482.3 201
n-Butylbenzene 45 08/22/2012 0723895029-15213 201
tert-Butylbenzene 43 08/22/2012 0723855038-14914 201
sec-Butylbenzene 43 08/22/2012 0723875037-14714 201
Carbon tetrachloride 43 08/22/2012 0723875058-13614 201
Chlorobenzene 42 08/22/2012 0723835059-12911 201
Chloroethane 44 08/22/2012 0723875042-16314 201
Chloroform 42 08/22/2012 0723845071-12514 201
Chloromethane (Methyl chloride)46 08/22/2012 0723925034-13413 201
4-Chlorotoluene 43 08/22/2012 0723855053-13512 201
2-Chlorotoluene 43 08/22/2012 0723855053-13312 201
Dibromochloromethane 39 08/22/2012 0723795066-11912 201
1,2-Dibromoethane (EDB)41 08/22/2012 0723835074-1248.3 201
1,4-Dichlorobenzene 43 08/22/2012 0723865052-13311 201
1,3-Dichlorobenzene 43 08/22/2012 0723865051-13414 201
1,2-Dichlorobenzene 41 08/22/2012 0723835057-13114 201
Dichlorodifluoromethane 45 08/22/2012 0723915010-15715 201
1,2-Dichloroethane 41 08/22/2012 0723815067-12912 201
1,1-Dichloroethane 42 08/22/2012 0723855071-12713 201
cis-1,2-Dichloroethene 43 08/22/2012 0723855070-12214 201
1,1-Dichloroethene 43 08/22/2012 0723865069-13814 201
trans-1,2-Dichloroethene 43 08/22/2012 0723855068-13114 201
1,2-Dichloropropane 41 08/22/2012 0723825072-12412 201
2,2-Dichloropropane 47 08/22/2012 0723945059-1299.6 201
1,3-Dichloropropane 38 08/22/2012 0723775070-1308.9 201
trans-1,3-Dichloropropene 38 08/22/2012 0723765070-1247.5 201
cis-1,3-Dichloropropene 39 08/22/2012 0723775070-1267.3 201
1,1-Dichloropropene 43 08/22/2012 0723875060-13313 201
Diisopropyl ether (IPE)42 08/22/2012 0723855026-14315 201
Ethylbenzene 42 08/22/2012 0723835059-12815 201
2-Hexanone 80 08/22/2012 07238010054-1373.8 201
Isopropylbenzene 42 08/22/2012 0723845050-13612 201
p-Isopropyltoluene 44 08/22/2012 0723895036-14613 201
Methyl tertiary butyl ether (MTBE)44 08/22/2012 0723875070-13013 201
4-Methyl-2-pentanone 84 08/22/2012 07238410060-1347.8 201
Methylene chloride 40 08/22/2012 0723805070-13013 201
Naphthalene 44 08/22/2012 0723885054-1311.4 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 28 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:NQ91951-003
91951 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
n-Propylbenzene 43 08/22/2012 0723875041-14412 201
Styrene 45 08/22/2012 0723905054-13612 201
1,1,2,2-Tetrachloroethane 43 08/22/2012 0723875069-1329.4 201
Tetrachloroethene 41 08/22/2012 0723825045-15012 201
Toluene 31 08/22/2012 0723625061-12916 201
1,2,3-Trichlorobenzene 42 08/22/2012 0723845040-1431.0 201
1,2,4-Trichlorobenzene 43 08/22/2012 0723875034-1458.5 201
1,1,2-Trichloroethane 39 08/22/2012 0723775055-1289.0 201
1,1,1-Trichloroethane 43 08/22/2012 0723865063-12815 201
Trichloroethene 43 08/22/2012 0723855062-12614 201
Trichlorofluoromethane 43 08/22/2012 0723865045-13815 201
1,2,3-Trichloropropane 44 08/22/2012 0723875067-1268.6 201
1,2,4-Trimethylbenzene 43 08/22/2012 0723865047-13813 201
1,3,5-Trimethylbenzene 43 08/22/2012 0723875046-13913 201
Vinyl acetate 54 08/22/2012 07231085055-1285.1 201
Vinyl chloride 47 08/22/2012 0723945042-13215 201
Xylenes (total)87 08/22/2012 07238710058-12814 201
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 107 47-138
1,2-Dichloroethane-d4 106 53-142
Toluene-d8 95 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 29 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:NQ92054-001
92054 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 08/24/2012 03491000340ug/kg50
Benzene ND 08/24/2012 034925055ug/kg50
Bromobenzene ND 08/24/2012 034925035ug/kg50
Bromochloromethane ND 08/24/2012 034925050ug/kg50
Bromodichloromethane ND 08/24/2012 034925085ug/kg50
Bromoform ND 08/24/2012 034925035ug/kg50
Bromomethane (Methyl bromide)ND 08/24/2012 034925090ug/kg50
2-Butanone (MEK)ND 08/24/2012 0349500120ug/kg50
tert-Butylbenzene ND 08/24/2012 034925050ug/kg50
sec-Butylbenzene ND 08/24/2012 034925050ug/kg50
n-Butylbenzene ND 08/24/2012 034925050ug/kg50
Carbon tetrachloride ND 08/24/2012 034925090ug/kg50
Chlorobenzene ND 08/24/2012 034925085ug/kg50
Chloroethane ND 08/24/2012 034925065ug/kg50
Chloroform ND 08/24/2012 034925042ug/kg50
Chloromethane (Methyl chloride)ND 08/24/2012 034925050ug/kg50
2-Chlorotoluene ND 08/24/2012 0349250140ug/kg50
4-Chlorotoluene ND 08/24/2012 034925095ug/kg50
Dibromochloromethane ND 08/24/2012 034925085ug/kg50
1,2-Dibromoethane (EDB)ND 08/24/2012 034925043ug/kg50
1,3-Dichlorobenzene ND 08/24/2012 034925085ug/kg50
1,2-Dichlorobenzene ND 08/24/2012 034925085ug/kg50
1,4-Dichlorobenzene ND 08/24/2012 034925085ug/kg50
Dichlorodifluoromethane ND 08/24/2012 034925080ug/kg50
1,2-Dichloroethane ND 08/24/2012 034925050ug/kg50
1,1-Dichloroethane ND 08/24/2012 034925037ug/kg50
trans-1,2-Dichloroethene ND 08/24/2012 034925075ug/kg50
cis-1,2-Dichloroethene ND 08/24/2012 034925038ug/kg50
1,1-Dichloroethene ND 08/24/2012 034925085ug/kg50
1,2-Dichloropropane ND 08/24/2012 034925046ug/kg50
2,2-Dichloropropane ND 08/24/2012 034925055ug/kg50
1,3-Dichloropropane ND 08/24/2012 034925050ug/kg50
trans-1,3-Dichloropropene ND 08/24/2012 034925041ug/kg50
cis-1,3-Dichloropropene ND 08/24/2012 034925034ug/kg50
1,1-Dichloropropene ND 08/24/2012 034925075ug/kg50
Diisopropyl ether (IPE)ND 08/24/2012 034925016ug/kg50
Ethylbenzene ND 08/24/2012 034925085ug/kg50
2-Hexanone ND 08/24/2012 034950065ug/kg50
Isopropylbenzene ND 08/24/2012 034925012ug/kg50
p-Isopropyltoluene ND 08/24/2012 034925070ug/kg50
Methyl tertiary butyl ether (MTBE)ND 08/24/2012 034925020ug/kg50
4-Methyl-2-pentanone ND 08/24/2012 034950075ug/kg50
Methylene chloride ND 08/24/2012 0349250130ug/kg50
Naphthalene ND 08/24/2012 034925085ug/kg50
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 30 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:NQ92054-001
92054 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
n-Propylbenzene ND 08/24/2012 034925050ug/kg50
Styrene ND 08/24/2012 034925055ug/kg50
1,1,2,2-Tetrachloroethane ND 08/24/2012 034925024ug/kg50
Tetrachloroethene ND 08/24/2012 034925025ug/kg50
Toluene ND 08/24/2012 034925085ug/kg50
1,2,4-Trichlorobenzene ND 08/24/2012 034925085ug/kg50
1,2,3-Trichlorobenzene ND 08/24/2012 034925085ug/kg50
1,1,1-Trichloroethane ND 08/24/2012 034925043ug/kg50
1,1,2-Trichloroethane ND 08/24/2012 034925040ug/kg50
Trichloroethene ND 08/24/2012 034925095ug/kg50
Trichlorofluoromethane ND 08/24/2012 034925075ug/kg50
1,2,3-Trichloropropane ND 08/24/2012 034925043ug/kg50
1,3,5-Trimethylbenzene ND 08/24/2012 034925085ug/kg50
1,2,4-Trimethylbenzene ND 08/24/2012 034925085ug/kg50
Vinyl acetate ND 08/24/2012 034925045ug/kg50
Vinyl chloride ND 08/24/2012 034925043ug/kg50
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 94 47-138
1,2-Dichloroethane-d4 122 53-142
Toluene-d8 92 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 31 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:NQ92054-002
92054 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 4900 08/24/2012 023899500042-14950
Benzene 2600 08/24/2012 0238106250069-12350
Bromobenzene 2300 08/24/2012 023891250053-13750
Bromochloromethane 2700 08/24/2012 0238107250070-12150
Bromodichloromethane 2300 08/24/2012 023893250069-12150
Bromoform 2100 08/24/2012 023882250061-11950
Bromomethane (Methyl bromide)1100 08/24/2012 023843250010-16850
2-Butanone (MEK)4600 08/24/2012 023892500057-14850
tert-Butylbenzene 2400 08/24/2012 023894250038-14950
sec-Butylbenzene 2400 08/24/2012 023896250037-14750
n-Butylbenzene 2400 08/24/2012 023895250029-15250
Carbon tetrachloride 2600 08/24/2012 0238103250058-13650
Chlorobenzene 2400 08/24/2012 023894250059-12950
Chloroethane 1700 08/24/2012 023867250042-16350
Chloroform 2600 08/24/2012 0238105250071-12550
Chloromethane (Methyl chloride)2700 08/24/2012 0238106250034-13450
2-Chlorotoluene 2300 08/24/2012 023892250053-13350
4-Chlorotoluene 2300 08/24/2012 023891250053-13550
Dibromochloromethane 2100 08/24/2012 023884250066-11950
1,2-Dibromoethane (EDB)2200 08/24/2012 023888250074-12450
1,3-Dichlorobenzene 2300 08/24/2012 023893250051-13450
1,2-Dichlorobenzene 2300 08/24/2012 023890250057-13150
1,4-Dichlorobenzene 2300 08/24/2012 023891250052-13350
Dichlorodifluoromethane 2100 08/24/2012 023884250010-15750
1,2-Dichloroethane 2300 08/24/2012 023893250067-12950
1,1-Dichloroethane 2700 08/24/2012 0238109250071-12750
trans-1,2-Dichloroethene 2700 08/24/2012 0238110250068-13150
cis-1,2-Dichloroethene 2700 08/24/2012 0238110250070-12250
1,1-Dichloroethene 2800 08/24/2012 0238112250069-13850
1,2-Dichloropropane 2400 08/24/2012 023897250072-12450
2,2-Dichloropropane 2700 08/24/2012 0238110250059-12950
1,3-Dichloropropane 2100 08/24/2012 023886250070-13050
trans-1,3-Dichloropropene 2100 08/24/2012 023883250070-12450
cis-1,3-Dichloropropene 2200 08/24/2012 023888250070-12650
1,1-Dichloropropene 2700 08/24/2012 0238106250060-13350
Diisopropyl ether (IPE)2700 08/24/2012 0238109250026-14350
Ethylbenzene 2400 08/24/2012 023894250059-12850
2-Hexanone 3800 08/24/2012 023876500054-13750
Isopropylbenzene 2300 08/24/2012 023892250050-13650
p-Isopropyltoluene 2400 08/24/2012 023894250036-14650
Methyl tertiary butyl ether (MTBE)2700 08/24/2012 0238110250070-13050
4-Methyl-2-pentanone 4200 08/24/2012 023884500060-13450
Methylene chloride 2600 08/24/2012 0238106250070-13050
Naphthalene 1800 08/24/2012 023870250054-13150
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 32 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:NQ92054-002
92054 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
n-Propylbenzene 2300 08/24/2012 023892250041-14450
Styrene 2500 08/24/2012 0238101250054-13650
1,1,2,2-Tetrachloroethane 2200 08/24/2012 023888250069-13250
Tetrachloroethene 2300 08/24/2012 023892250045-15050
Toluene 2000 08/24/2012 023879250061-12950
1,2,4-Trichlorobenzene 1900 08/24/2012 023877250034-14550
1,2,3-Trichlorobenzene 1700 08/24/2012 023867250040-14350
1,1,1-Trichloroethane 2600 08/24/2012 0238105250063-12850
1,1,2-Trichloroethane 2100 08/24/2012 023884250055-12850
Trichloroethene 2600 08/24/2012 0238102250062-12650
Trichlorofluoromethane 2600 08/24/2012 0238103250045-13850
1,2,3-Trichloropropane 2200 08/24/2012 023888250067-12650
1,3,5-Trimethylbenzene 2300 08/24/2012 023894250046-13950
1,2,4-Trimethylbenzene 2300 08/24/2012 023893250047-13850
Vinyl acetate 2700 08/24/2012 0238109250055-12850
Vinyl chloride 2700 08/24/2012 0238108250042-13250
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 91 47-138
1,2-Dichloroethane-d4 113 53-142
Toluene-d8 91 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 33 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:NQ92054-003
92054 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 4600 08/24/2012 030291500042-1497.7 2050
Benzene 2600 08/24/2012 0302104250069-1231.7 2050
Bromobenzene 2200 08/24/2012 030289250053-1372.0 2050
Bromochloromethane 2500 08/24/2012 0302101250070-1215.9 2050
Bromodichloromethane 2300 08/24/2012 030291250069-1212.5 2050
Bromoform 1900 08/24/2012 030277250061-1196.0 2050
Bromomethane (Methyl bromide)1100 08/24/2012 030243250010-1680.75 2050
2-Butanone (MEK)4300 08/24/2012 030287500057-1485.6 2050
tert-Butylbenzene 2400 08/24/2012 030294250038-1490.25 2050
sec-Butylbenzene 2300 08/24/2012 030294250037-1472.3 2050
n-Butylbenzene 2300 08/24/2012 030293250029-1522.4 2050
Carbon tetrachloride 2500 08/24/2012 0302100250058-1363.2 2050
Chlorobenzene 2300 08/24/2012 030293250059-1291.5 2050
Chloroethane 1500 08/24/2012 030259250042-16312 2050
Chloroform 2600 08/24/2012 0302102250071-1252.9 2050
Chloromethane (Methyl chloride)2600 08/24/2012 0302105250034-1341.8 2050
2-Chlorotoluene 2300 08/24/2012 030291250053-1331.4 2050
4-Chlorotoluene 2200 08/24/2012 030289250053-1351.4 2050
Dibromochloromethane 2000 08/24/2012 030281250066-1193.7 2050
1,2-Dibromoethane (EDB)2100 08/24/2012 030286250074-1242.2 2050
1,3-Dichlorobenzene 2300 08/24/2012 030293250051-1340.95 2050
1,2-Dichlorobenzene 2200 08/24/2012 030288250057-1312.6 2050
1,4-Dichlorobenzene 2300 08/24/2012 030291250052-1330.54 2050
Dichlorodifluoromethane 1900 08/24/2012 030277250010-1578.0 2050
1,2-Dichloroethane 2200 08/24/2012 030289250067-1295.0 2050
1,1-Dichloroethane 2600 08/24/2012 0302105250071-1274.2 2050
trans-1,2-Dichloroethene 2600 08/24/2012 0302105250068-1314.2 2050
cis-1,2-Dichloroethene 2700 08/24/2012 0302107250070-1222.9 2050
1,1-Dichloroethene 2700 08/24/2012 0302108250069-1384.4 2050
1,2-Dichloropropane 2400 08/24/2012 030295250072-1242.3 2050
2,2-Dichloropropane 2700 08/24/2012 0302107250059-1292.6 2050
1,3-Dichloropropane 2000 08/24/2012 030282250070-1304.7 2050
trans-1,3-Dichloropropene 2000 08/24/2012 030281250070-1243.0 2050
cis-1,3-Dichloropropene 2100 08/24/2012 030286250070-1262.3 2050
1,1-Dichloropropene 2600 08/24/2012 0302103250060-1332.9 2050
Diisopropyl ether (IPE)2600 08/24/2012 0302104250026-1433.8 2050
Ethylbenzene 2300 08/24/2012 030293250059-1280.99 2050
2-Hexanone 3600 08/24/2012 030272500054-1375.7 2050
Isopropylbenzene 2300 08/24/2012 030291250050-1360.90 2050
p-Isopropyltoluene 2400 08/24/2012 030294250036-1460.31 2050
Methyl tertiary butyl ether (MTBE)2500 08/24/2012 0302101250070-1308.3 2050
4-Methyl-2-pentanone 3800 08/24/2012 030277500060-1349.5 2050
Methylene chloride 2500 08/24/2012 0302100250070-1304.9 2050
Naphthalene 1700 08/24/2012 030270250054-1311.1 2050
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 34 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:NQ92054-003
92054 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
n-Propylbenzene 2300 08/24/2012 030291250041-1441.2 2050
Styrene 2500 08/24/2012 030299250054-1361.7 2050
1,1,2,2-Tetrachloroethane 2100 08/24/2012 030282250069-1326.3 2050
Tetrachloroethene 2300 08/24/2012 030290250045-1502.5 2050
Toluene 1900 08/24/2012 030278250061-1291.7 2050
1,2,4-Trichlorobenzene 1800 08/24/2012 030274250034-1454.7 2050
1,2,3-Trichlorobenzene 1700 08/24/2012 030269250040-1432.3 2050
1,1,1-Trichloroethane 2500 08/24/2012 0302102250063-1282.7 2050
1,1,2-Trichloroethane 2000 08/24/2012 030281250055-1283.4 2050
Trichloroethene 2500 08/24/2012 0302100250062-1262.6 2050
Trichlorofluoromethane 2400 08/24/2012 030297250045-1385.6 2050
1,2,3-Trichloropropane 2000 08/24/2012 030282250067-1267.8 2050
1,3,5-Trimethylbenzene 2300 08/24/2012 030292250046-1391.8 2050
1,2,4-Trimethylbenzene 2300 08/24/2012 030292250047-1381.1 2050
Vinyl acetate 2400 08/24/2012 030297250055-12811 2050
Vinyl chloride 2700 08/24/2012 0302106250042-1322.1 2050
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 93 47-138
1,2-Dichloroethane-d4 112 53-142
Toluene-d8 92 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 35 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:NQ92260-001
92260 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 08/24/2012 03491000340ug/kg50
Benzene ND 08/24/2012 034925055ug/kg50
Bromobenzene ND 08/24/2012 034925035ug/kg50
Bromochloromethane ND 08/24/2012 034925050ug/kg50
Bromodichloromethane ND 08/24/2012 034925085ug/kg50
Bromoform ND 08/24/2012 034925035ug/kg50
Bromomethane (Methyl bromide)ND 08/24/2012 034925090ug/kg50
2-Butanone (MEK)ND 08/24/2012 0349500120ug/kg50
tert-Butylbenzene ND 08/24/2012 034925050ug/kg50
sec-Butylbenzene ND 08/24/2012 034925050ug/kg50
n-Butylbenzene ND 08/24/2012 034925050ug/kg50
Carbon tetrachloride ND 08/24/2012 034925090ug/kg50
Chlorobenzene ND 08/24/2012 034925085ug/kg50
Chloroethane ND 08/24/2012 034925065ug/kg50
Chloroform ND 08/24/2012 034925042ug/kg50
Chloromethane (Methyl chloride)ND 08/24/2012 034925050ug/kg50
4-Chlorotoluene ND 08/24/2012 034925095ug/kg50
2-Chlorotoluene ND 08/24/2012 0349250140ug/kg50
Dibromochloromethane ND 08/24/2012 034925085ug/kg50
1,2-Dibromoethane (EDB)ND 08/24/2012 034925043ug/kg50
1,4-Dichlorobenzene ND 08/24/2012 034925085ug/kg50
1,3-Dichlorobenzene ND 08/24/2012 034925085ug/kg50
1,2-Dichlorobenzene ND 08/24/2012 034925085ug/kg50
Dichlorodifluoromethane ND 08/24/2012 034925080ug/kg50
1,2-Dichloroethane ND 08/24/2012 034925050ug/kg50
1,1-Dichloroethane ND 08/24/2012 034925037ug/kg50
trans-1,2-Dichloroethene ND 08/24/2012 034925075ug/kg50
cis-1,2-Dichloroethene ND 08/24/2012 034925038ug/kg50
1,1-Dichloroethene ND 08/24/2012 034925085ug/kg50
2,2-Dichloropropane ND 08/24/2012 034925055ug/kg50
1,3-Dichloropropane ND 08/24/2012 034925050ug/kg50
1,2-Dichloropropane ND 08/24/2012 034925046ug/kg50
trans-1,3-Dichloropropene ND 08/24/2012 034925041ug/kg50
cis-1,3-Dichloropropene ND 08/24/2012 034925034ug/kg50
1,1-Dichloropropene ND 08/24/2012 034925075ug/kg50
Diisopropyl ether (IPE)ND 08/24/2012 034925016ug/kg50
Ethylbenzene ND 08/24/2012 034925085ug/kg50
2-Hexanone ND 08/24/2012 034950065ug/kg50
Isopropylbenzene ND 08/24/2012 034925012ug/kg50
p-Isopropyltoluene ND 08/24/2012 034925070ug/kg50
Methyl tertiary butyl ether (MTBE)ND 08/24/2012 034925020ug/kg50
4-Methyl-2-pentanone ND 08/24/2012 034950075ug/kg50
Methylene chloride ND 08/24/2012 0349250130ug/kg50
Naphthalene ND 08/24/2012 034925085ug/kg50
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 36 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:NQ92260-001
92260 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
n-Propylbenzene ND 08/24/2012 034925050ug/kg50
Styrene ND 08/24/2012 034925055ug/kg50
1,1,2,2-Tetrachloroethane ND 08/24/2012 034925024ug/kg50
Tetrachloroethene ND 08/24/2012 034925025ug/kg50
Toluene ND 08/24/2012 034925085ug/kg50
1,2,4-Trichlorobenzene ND 08/24/2012 034925085ug/kg50
1,2,3-Trichlorobenzene ND 08/24/2012 034925085ug/kg50
1,1,2-Trichloroethane ND 08/24/2012 034925040ug/kg50
1,1,1-Trichloroethane ND 08/24/2012 034925043ug/kg50
Trichloroethene ND 08/24/2012 034925095ug/kg50
Trichlorofluoromethane ND 08/24/2012 034925075ug/kg50
1,2,3-Trichloropropane ND 08/24/2012 034925043ug/kg50
1,3,5-Trimethylbenzene ND 08/24/2012 034925085ug/kg50
1,2,4-Trimethylbenzene ND 08/24/2012 034925085ug/kg50
Vinyl acetate ND 08/24/2012 034925045ug/kg50
Vinyl chloride ND 08/24/2012 034925043ug/kg50
Xylenes (total)ND 08/24/2012 0349250150ug/kg50
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 94 47-138
1,2-Dichloroethane-d4 122 53-142
Toluene-d8 92 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 37 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:NQ92260-002
92260 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 4900 08/24/2012 023899500042-14950
Benzene 2600 08/24/2012 0238106250069-12350
Bromobenzene 2300 08/24/2012 023891250053-13750
Bromochloromethane 2700 08/24/2012 0238107250070-12150
Bromodichloromethane 2300 08/24/2012 023893250069-12150
Bromoform 2100 08/24/2012 023882250061-11950
Bromomethane (Methyl bromide)1100 08/24/2012 023843250010-16850
2-Butanone (MEK)4600 08/24/2012 023892500057-14850
tert-Butylbenzene 2400 08/24/2012 023894250038-14950
sec-Butylbenzene 2400 08/24/2012 023896250037-14750
n-Butylbenzene 2400 08/24/2012 023895250029-15250
Carbon tetrachloride 2600 08/24/2012 0238103250058-13650
Chlorobenzene 2400 08/24/2012 023894250059-12950
Chloroethane 1700 08/24/2012 023867250042-16350
Chloroform 2600 08/24/2012 0238105250071-12550
Chloromethane (Methyl chloride)2700 08/24/2012 0238106250034-13450
4-Chlorotoluene 2300 08/24/2012 023891250053-13550
2-Chlorotoluene 2300 08/24/2012 023892250053-13350
Dibromochloromethane 2100 08/24/2012 023884250066-11950
1,2-Dibromoethane (EDB)2200 08/24/2012 023888250074-12450
1,4-Dichlorobenzene 2300 08/24/2012 023891250052-13350
1,3-Dichlorobenzene 2300 08/24/2012 023893250051-13450
1,2-Dichlorobenzene 2300 08/24/2012 023890250057-13150
Dichlorodifluoromethane 2100 08/24/2012 023884250010-15750
1,2-Dichloroethane 2300 08/24/2012 023893250067-12950
1,1-Dichloroethane 2700 08/24/2012 0238109250071-12750
trans-1,2-Dichloroethene 2700 08/24/2012 0238110250068-13150
cis-1,2-Dichloroethene 2700 08/24/2012 0238110250070-12250
1,1-Dichloroethene 2800 08/24/2012 0238112250069-13850
2,2-Dichloropropane 2700 08/24/2012 0238110250059-12950
1,3-Dichloropropane 2100 08/24/2012 023886250070-13050
1,2-Dichloropropane 2400 08/24/2012 023897250072-12450
trans-1,3-Dichloropropene 2100 08/24/2012 023883250070-12450
cis-1,3-Dichloropropene 2200 08/24/2012 023888250070-12650
1,1-Dichloropropene 2700 08/24/2012 0238106250060-13350
Diisopropyl ether (IPE)2700 08/24/2012 0238109250026-14350
Ethylbenzene 2400 08/24/2012 023894250059-12850
2-Hexanone 3800 08/24/2012 023876500054-13750
Isopropylbenzene 2300 08/24/2012 023892250050-13650
p-Isopropyltoluene 2400 08/24/2012 023894250036-14650
Methyl tertiary butyl ether (MTBE)2700 08/24/2012 0238110250070-13050
4-Methyl-2-pentanone 4200 08/24/2012 023884500060-13450
Methylene chloride 2600 08/24/2012 0238106250070-13050
Naphthalene 1800 08/24/2012 023870250054-13150
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 38 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:NQ92260-002
92260 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
n-Propylbenzene 2300 08/24/2012 023892250041-14450
Styrene 2500 08/24/2012 0238101250054-13650
1,1,2,2-Tetrachloroethane 2200 08/24/2012 023888250069-13250
Tetrachloroethene 2300 08/24/2012 023892250045-15050
Toluene 2000 08/24/2012 023879250061-12950
1,2,4-Trichlorobenzene 1900 08/24/2012 023877250034-14550
1,2,3-Trichlorobenzene 1700 08/24/2012 023867250040-14350
1,1,2-Trichloroethane 2100 08/24/2012 023884250055-12850
1,1,1-Trichloroethane 2600 08/24/2012 0238105250063-12850
Trichloroethene 2600 08/24/2012 0238102250062-12650
Trichlorofluoromethane 2600 08/24/2012 0238103250045-13850
1,2,3-Trichloropropane 2200 08/24/2012 023888250067-12650
1,3,5-Trimethylbenzene 2300 08/24/2012 023894250046-13950
1,2,4-Trimethylbenzene 2300 08/24/2012 023893250047-13850
Vinyl acetate 2700 08/24/2012 0238109250055-12850
Vinyl chloride 2700 08/24/2012 0238108250042-13250
Xylenes (total)4800 08/24/2012 023897500058-12850
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 91 47-138
1,2-Dichloroethane-d4 113 53-142
Toluene-d8 91 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 39 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:NQ92260-003
92260 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 4600 08/24/2012 030291500042-1497.7 2050
Benzene 2600 08/24/2012 0302104250069-1231.7 2050
Bromobenzene 2200 08/24/2012 030289250053-1372.0 2050
Bromochloromethane 2500 08/24/2012 0302101250070-1215.9 2050
Bromodichloromethane 2300 08/24/2012 030291250069-1212.5 2050
Bromoform 1900 08/24/2012 030277250061-1196.0 2050
Bromomethane (Methyl bromide)1100 08/24/2012 030243250010-1680.75 2050
2-Butanone (MEK)4300 08/24/2012 030287500057-1485.6 2050
tert-Butylbenzene 2400 08/24/2012 030294250038-1490.25 2050
sec-Butylbenzene 2300 08/24/2012 030294250037-1472.3 2050
n-Butylbenzene 2300 08/24/2012 030293250029-1522.4 2050
Carbon tetrachloride 2500 08/24/2012 0302100250058-1363.2 2050
Chlorobenzene 2300 08/24/2012 030293250059-1291.5 2050
Chloroethane 1500 08/24/2012 030259250042-16312 2050
Chloroform 2600 08/24/2012 0302102250071-1252.9 2050
Chloromethane (Methyl chloride)2600 08/24/2012 0302105250034-1341.8 2050
4-Chlorotoluene 2200 08/24/2012 030289250053-1351.4 2050
2-Chlorotoluene 2300 08/24/2012 030291250053-1331.4 2050
Dibromochloromethane 2000 08/24/2012 030281250066-1193.7 2050
1,2-Dibromoethane (EDB)2100 08/24/2012 030286250074-1242.2 2050
1,4-Dichlorobenzene 2300 08/24/2012 030291250052-1330.54 2050
1,3-Dichlorobenzene 2300 08/24/2012 030293250051-1340.95 2050
1,2-Dichlorobenzene 2200 08/24/2012 030288250057-1312.6 2050
Dichlorodifluoromethane 1900 08/24/2012 030277250010-1578.0 2050
1,2-Dichloroethane 2200 08/24/2012 030289250067-1295.0 2050
1,1-Dichloroethane 2600 08/24/2012 0302105250071-1274.2 2050
trans-1,2-Dichloroethene 2600 08/24/2012 0302105250068-1314.2 2050
cis-1,2-Dichloroethene 2700 08/24/2012 0302107250070-1222.9 2050
1,1-Dichloroethene 2700 08/24/2012 0302108250069-1384.4 2050
2,2-Dichloropropane 2700 08/24/2012 0302107250059-1292.6 2050
1,3-Dichloropropane 2000 08/24/2012 030282250070-1304.7 2050
1,2-Dichloropropane 2400 08/24/2012 030295250072-1242.3 2050
trans-1,3-Dichloropropene 2000 08/24/2012 030281250070-1243.0 2050
cis-1,3-Dichloropropene 2100 08/24/2012 030286250070-1262.3 2050
1,1-Dichloropropene 2600 08/24/2012 0302103250060-1332.9 2050
Diisopropyl ether (IPE)2600 08/24/2012 0302104250026-1433.8 2050
Ethylbenzene 2300 08/24/2012 030293250059-1280.99 2050
2-Hexanone 3600 08/24/2012 030272500054-1375.7 2050
Isopropylbenzene 2300 08/24/2012 030291250050-1360.90 2050
p-Isopropyltoluene 2400 08/24/2012 030294250036-1460.31 2050
Methyl tertiary butyl ether (MTBE)2500 08/24/2012 0302101250070-1308.3 2050
4-Methyl-2-pentanone 3800 08/24/2012 030277500060-1349.5 2050
Methylene chloride 2500 08/24/2012 0302100250070-1304.9 2050
Naphthalene 1700 08/24/2012 030270250054-1311.1 2050
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 40 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:NQ92260-003
92260 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
n-Propylbenzene 2300 08/24/2012 030291250041-1441.2 2050
Styrene 2500 08/24/2012 030299250054-1361.7 2050
1,1,2,2-Tetrachloroethane 2100 08/24/2012 030282250069-1326.3 2050
Tetrachloroethene 2300 08/24/2012 030290250045-1502.5 2050
Toluene 1900 08/24/2012 030278250061-1291.7 2050
1,2,4-Trichlorobenzene 1800 08/24/2012 030274250034-1454.7 2050
1,2,3-Trichlorobenzene 1700 08/24/2012 030269250040-1432.3 2050
1,1,2-Trichloroethane 2000 08/24/2012 030281250055-1283.4 2050
1,1,1-Trichloroethane 2500 08/24/2012 0302102250063-1282.7 2050
Trichloroethene 2500 08/24/2012 0302100250062-1262.6 2050
Trichlorofluoromethane 2400 08/24/2012 030297250045-1385.6 2050
1,2,3-Trichloropropane 2000 08/24/2012 030282250067-1267.8 2050
1,3,5-Trimethylbenzene 2300 08/24/2012 030292250046-1391.8 2050
1,2,4-Trimethylbenzene 2300 08/24/2012 030292250047-1381.1 2050
Vinyl acetate 2400 08/24/2012 030297250055-12811 2050
Vinyl chloride 2700 08/24/2012 0302106250042-1322.1 2050
Xylenes (total)4700 08/24/2012 030295500058-1281.9 2050
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 93 47-138
1,2-Dichloroethane-d4 112 53-142
Toluene-d8 92 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 41 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:NQ92388-001
92388 6200B
Analytical Method:SM 6200B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Benzene ND 08/29/2012 08330.50 0.027 ug/L1
Bromobenzene ND 08/29/2012 08330.50 0.027 ug/L1
Bromochloromethane ND 08/29/2012 08330.50 0.055 ug/L1
Bromodichloromethane ND 08/29/2012 08330.50 0.17 ug/L1
Bromoform ND 08/29/2012 08330.50 0.010 ug/L1
Bromomethane (Methyl bromide)ND 08/29/2012 08330.50 0.20 ug/L1
tert-Butylbenzene ND 08/29/2012 08330.50 0.037 ug/L1
sec-Butylbenzene ND 08/29/2012 08330.50 0.010 ug/L1
n-Butylbenzene ND 08/29/2012 08330.50 0.017 ug/L1
Carbon tetrachloride ND 08/29/2012 08330.50 0.085 ug/L1
Chlorobenzene ND 08/29/2012 08330.50 0.17 ug/L1
Chloroethane ND 08/29/2012 08330.50 0.17 ug/L1
Chloroform ND 08/29/2012 08330.50 0.17 ug/L1
Chloromethane (Methyl chloride)ND 08/29/2012 08330.50 0.17 ug/L1
4-Chlorotoluene ND 08/29/2012 08330.50 0.019 ug/L1
2-Chlorotoluene ND 08/29/2012 08330.50 0.059 ug/L1
Dibromochloromethane ND 08/29/2012 08330.50 0.17 ug/L1
1,2-Dibromoethane (EDB)ND 08/29/2012 08330.50 0.061 ug/L1
Dibromomethane (Methylene bromide)ND 08/29/2012 08330.50 0.094 ug/L1
1,4-Dichlorobenzene ND 08/29/2012 08330.50 0.17 ug/L1
1,3-Dichlorobenzene ND 08/29/2012 08330.50 0.17 ug/L1
1,2-Dichlorobenzene ND 08/29/2012 08330.50 0.17 ug/L1
Dichlorodifluoromethane ND 08/29/2012 08330.50 0.071 ug/L1
1,2-Dichloroethane ND 08/29/2012 08330.50 0.023 ug/L1
1,1-Dichloroethane ND 08/29/2012 08330.50 0.054 ug/L1
trans-1,2-Dichloroethene ND 08/29/2012 08330.50 0.079 ug/L1
cis-1,2-Dichloroethene ND 08/29/2012 08330.50 0.087 ug/L1
1,1-Dichloroethene ND 08/29/2012 08330.50 0.094 ug/L1
2,2-Dichloropropane ND 08/29/2012 08330.50 0.060 ug/L1
1,3-Dichloropropane ND 08/29/2012 08330.50 0.019 ug/L1
1,2-Dichloropropane ND 08/29/2012 08330.50 0.081 ug/L1
trans-1,3-Dichloropropene ND 08/29/2012 08330.50 0.18 ug/L1
cis-1,3-Dichloropropene ND 08/29/2012 08330.50 0.090 ug/L1
1,1-Dichloropropene ND 08/29/2012 08330.50 0.074 ug/L1
Diisopropyl ether (IPE)ND 08/29/2012 08330.50 0.052 ug/L1
Ethanol ND 08/29/2012 083310033ug/L1
Ethylbenzene ND 08/29/2012 08330.50 0.17 ug/L1
Hexachlorobutadiene ND 08/29/2012 08330.50 0.17 ug/L1
Isopropylbenzene (Cumene)ND 08/29/2012 08330.50 0.029 ug/L1
p-Isopropyltoluene (p-Cymene)ND 08/29/2012 08330.50 0.018 ug/L1
Methyl tertiary butyl ether (MTBE)ND 08/29/2012 08330.50 0.019 ug/L1
Methylene chloride ND 08/29/2012 08330.50 0.17 ug/L1
Naphthalene ND 08/29/2012 08330.50 0.17 ug/L1
n-Propylbenzene ND 08/29/2012 08330.50 0.024 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 42 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:NQ92388-001
92388 6200B
Analytical Method:SM 6200B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Styrene ND 08/29/2012 08330.50 0.015 ug/L1
1,1,2,2-Tetrachloroethane ND 08/29/2012 08330.50 0.013 ug/L1
1,1,1,2-Tetrachloroethane ND 08/29/2012 08330.50 0.057 ug/L1
Tetrachloroethene ND 08/29/2012 08330.50 0.014 ug/L1
Toluene ND 08/29/2012 08330.50 0.17 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 08/29/2012 08330.50 0.30 ug/L1
1,2,4-Trichlorobenzene ND 08/29/2012 08330.50 0.17 ug/L1
1,2,3-Trichlorobenzene ND 08/29/2012 08330.50 0.17 ug/L1
1,1,2-Trichloroethane ND 08/29/2012 08330.50 0.031 ug/L1
1,1,1-Trichloroethane ND 08/29/2012 08330.50 0.029 ug/L1
Trichloroethene ND 08/29/2012 08330.50 0.024 ug/L1
Trichlorofluoromethane ND 08/29/2012 08330.50 0.051 ug/L1
1,2,3-Trichloropropane ND 08/29/2012 08330.50 0.33 ug/L1
1,2,4-Trimethylbenzene ND 08/29/2012 08330.50 0.17 ug/L1
1,3,5-Trimethylbenzene (Mesitylene)ND 08/29/2012 08330.50 0.17 ug/L1
Vinyl chloride ND 08/29/2012 08330.50 0.065 ug/L1
o - Xylenes ND 08/29/2012 08330.50 0.17 ug/L1
m+p - Xylenes ND 08/29/2012 08330.50 0.17 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 98 70-147
1,2-Dichloroethane-d4 93 52-138
Toluene-d8 100 76-125
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 43 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:NQ92388-002
92388 6200B
Analytical Method:SM 6200B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 49 08/29/2012 0707985070-1301
Bromobenzene 47 08/29/2012 0707935070-1301
Bromochloromethane 49 08/29/2012 0707985070-1301
Bromodichloromethane 48 08/29/2012 0707955070-1301
Bromoform 40 08/29/2012 0707805070-1301
Bromomethane (Methyl bromide)25 08/29/2012 0707N505060-1401
tert-Butylbenzene 44 08/29/2012 0707885070-1301
sec-Butylbenzene 48 08/29/2012 0707975070-1301
n-Butylbenzene 50 08/29/2012 0707995070-1301
Carbon tetrachloride 48 08/29/2012 0707965070-1301
Chlorobenzene 47 08/29/2012 0707955070-1301
Chloroethane 51 08/29/2012 07071025042-1631
Chloroform 46 08/29/2012 0707925070-1301
Chloromethane (Methyl chloride)54 08/29/2012 07071075020-1581
4-Chlorotoluene 47 08/29/2012 0707955070-1301
2-Chlorotoluene 47 08/29/2012 0707955070-1301
Dibromochloromethane 43 08/29/2012 0707875070-1301
1,2-Dibromoethane (EDB)49 08/29/2012 0707985070-1301
Dibromomethane (Methylene bromide)47 08/29/2012 0707935070-1301
1,4-Dichlorobenzene 45 08/29/2012 0707915070-1301
1,3-Dichlorobenzene 47 08/29/2012 0707945070-1301
1,2-Dichlorobenzene 46 08/29/2012 0707925070-1301
Dichlorodifluoromethane 59 08/29/2012 07071185060-1401
1,2-Dichloroethane 44 08/29/2012 0707885070-1301
1,1-Dichloroethane 48 08/29/2012 0707965070-1301
trans-1,2-Dichloroethene 50 08/29/2012 0707995070-1301
cis-1,2-Dichloroethene 49 08/29/2012 0707985070-1301
1,1-Dichloroethene 50 08/29/2012 0707995070-1301
2,2-Dichloropropane 59 08/29/2012 07071195070-1301
1,3-Dichloropropane 48 08/29/2012 0707955070-1301
1,2-Dichloropropane 48 08/29/2012 0707975070-1301
trans-1,3-Dichloropropene 50 08/29/2012 0707995070-1301
cis-1,3-Dichloropropene 51 08/29/2012 07071025070-1301
1,1-Dichloropropene 48 08/29/2012 0707975070-1301
Diisopropyl ether (IPE)50 08/29/2012 07071005070-1301
Ethanol 6600 08/29/2012 0707N131500040-1301
Ethylbenzene 49 08/29/2012 0707995070-1301
Hexachlorobutadiene 44 08/29/2012 0707875070-1301
Isopropylbenzene (Cumene)51 08/29/2012 07071015070-1301
p-Isopropyltoluene (p-Cymene)51 08/29/2012 07071025070-1301
Methyl tertiary butyl ether (MTBE)48 08/29/2012 0707975070-1301
Methylene chloride 49 08/29/2012 0707985070-1301
Naphthalene 51 08/29/2012 07071025050-1401
n-Propylbenzene 48 08/29/2012 0707965070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 44 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:NQ92388-002
92388 6200B
Analytical Method:SM 6200B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Styrene 52 08/29/2012 07071045070-1301
1,1,2,2-Tetrachloroethane 49 08/29/2012 0707985070-1301
1,1,1,2-Tetrachloroethane 49 08/29/2012 0707985070-1301
Tetrachloroethene 48 08/29/2012 0707965070-1301
Toluene 48 08/29/2012 0707965070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 59 08/29/2012 07071195070-1301
1,2,4-Trichlorobenzene 47 08/29/2012 0707945070-1301
1,2,3-Trichlorobenzene 47 08/29/2012 0707945070-1301
1,1,2-Trichloroethane 47 08/29/2012 0707945070-1301
1,1,1-Trichloroethane 47 08/29/2012 0707955070-1301
Trichloroethene 49 08/29/2012 0707975070-1301
Trichlorofluoromethane 51 08/29/2012 07071025060-1401
1,2,3-Trichloropropane 45 08/29/2012 0707915070-1301
1,2,4-Trimethylbenzene 50 08/29/2012 07071015070-1301
1,3,5-Trimethylbenzene (Mesitylene)51 08/29/2012 07071015070-1301
Vinyl chloride 58 08/29/2012 07071165060-1401
o - Xylenes 49 08/29/2012 0707995070-1301
m+p - Xylenes 50 08/29/2012 07071015070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 100 70-147
1,2-Dichloroethane-d4 96 52-138
Toluene-d8 101 76-125
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 45 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:NQ92388-003
92388 6200B
Analytical Method:SM 6200B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Benzene 45 08/29/2012 0729915070-1308.0 201
Bromobenzene 43 08/29/2012 0729875070-1306.9 201
Bromochloromethane 46 08/29/2012 0729915070-1307.0 201
Bromodichloromethane 44 08/29/2012 0729885070-1307.5 201
Bromoform 37 08/29/2012 0729745070-1306.8 201
Bromomethane (Methyl bromide)48 08/29/2012 0729+9650 60-14063 201
tert-Butylbenzene 42 08/29/2012 0729835070-1305.6 201
sec-Butylbenzene 45 08/29/2012 0729895070-1308.0 201
n-Butylbenzene 47 08/29/2012 0729955070-1304.7 201
Carbon tetrachloride 43 08/29/2012 0729865070-13011 201
Chlorobenzene 44 08/29/2012 0729875070-1307.9 201
Chloroethane 48 08/29/2012 0729975042-1635.6 201
Chloroform 43 08/29/2012 0729855070-1307.8 201
Chloromethane (Methyl chloride)50 08/29/2012 07291005020-1587.6 201
4-Chlorotoluene 44 08/29/2012 0729895070-1306.7 201
2-Chlorotoluene 44 08/29/2012 0729885070-1307.3 201
Dibromochloromethane 39 08/29/2012 0729795070-1309.4 201
1,2-Dibromoethane (EDB)45 08/29/2012 0729905070-1308.5 201
Dibromomethane (Methylene bromide)43 08/29/2012 0729875070-1307.4 201
1,4-Dichlorobenzene 43 08/29/2012 0729855070-1306.6 201
1,3-Dichlorobenzene 44 08/29/2012 0729885070-1307.2 201
1,2-Dichlorobenzene 44 08/29/2012 0729885070-1304.3 201
Dichlorodifluoromethane 53 08/29/2012 07291065060-1409.9 201
1,2-Dichloroethane 41 08/29/2012 0729825070-1307.4 201
1,1-Dichloroethane 44 08/29/2012 0729885070-1308.6 201
trans-1,2-Dichloroethene 46 08/29/2012 0729925070-1307.7 201
cis-1,2-Dichloroethene 46 08/29/2012 0729915070-1307.4 201
1,1-Dichloroethene 45 08/29/2012 0729915070-1309.0 201
2,2-Dichloropropane 56 08/29/2012 07291125070-1305.6 201
1,3-Dichloropropane 44 08/29/2012 0729875070-1308.4 201
1,2-Dichloropropane 45 08/29/2012 0729895070-1307.8 201
trans-1,3-Dichloropropene 46 08/29/2012 0729925070-1307.8 201
cis-1,3-Dichloropropene 47 08/29/2012 0729945070-1308.1 201
1,1-Dichloropropene 44 08/29/2012 0729895070-1309.0 201
Diisopropyl ether (IPE)47 08/29/2012 0729935070-1306.9 201
Ethanol 5900 08/29/2012 0729118500040-13010 201
Ethylbenzene 45 08/29/2012 0729905070-1309.4 201
Hexachlorobutadiene 42 08/29/2012 0729845070-1304.4 201
Isopropylbenzene (Cumene)47 08/29/2012 0729955070-1306.6 201
p-Isopropyltoluene (p-Cymene)48 08/29/2012 0729955070-1306.9 201
Methyl tertiary butyl ether (MTBE)45 08/29/2012 0729905070-1307.2 201
Methylene chloride 46 08/29/2012 0729925070-1307.0 201
Naphthalene 48 08/29/2012 0729975050-1405.6 201
n-Propylbenzene 46 08/29/2012 0729915070-1305.3 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 46 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:NQ92388-003
92388 6200B
Analytical Method:SM 6200B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Styrene 48 08/29/2012 0729955070-1308.4 201
1,1,2,2-Tetrachloroethane 47 08/29/2012 0729945070-1304.5 201
1,1,1,2-Tetrachloroethane 45 08/29/2012 0729895070-1308.7 201
Tetrachloroethene 44 08/29/2012 0729885070-1309.4 201
Toluene 44 08/29/2012 0729885070-1308.3 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 52 08/29/2012 07291045070-13013 201
1,2,4-Trichlorobenzene 45 08/29/2012 0729895070-1305.4 201
1,2,3-Trichlorobenzene 45 08/29/2012 0729905070-1304.4 201
1,1,2-Trichloroethane 44 08/29/2012 0729875070-1307.9 201
1,1,1-Trichloroethane 43 08/29/2012 0729875070-1308.8 201
Trichloroethene 45 08/29/2012 0729895070-1308.9 201
Trichlorofluoromethane 45 08/29/2012 0729905060-14012 201
1,2,3-Trichloropropane 42 08/29/2012 0729855070-1306.9 201
1,2,4-Trimethylbenzene 47 08/29/2012 0729945070-1307.3 201
1,3,5-Trimethylbenzene (Mesitylene)48 08/29/2012 0729955070-1306.1 201
Vinyl chloride 53 08/29/2012 07291065060-1409.3 201
o - Xylenes 45 08/29/2012 0729915070-1308.7 201
m+p - Xylenes 46 08/29/2012 0729925070-1308.3 201
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 99 70-147
1,2-Dichloroethane-d4 96 52-138
Toluene-d8 101 76-125
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 47 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
ICP-AES - MB
Batch:Prep Method:
Prep Date:
Sample ID:NQ91592-001
91592 3030 C
08/17/2012 1526Analytical Method:6010C
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Lead ND 08/20/2012 20400.010 0.0020 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 48 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
ICP-AES - LCS
Batch:Prep Method:
Prep Date:
Sample ID:NQ91592-002
91592 3030 C
08/17/2012 1526Analytical Method:6010C
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Lead 0.45 08/20/2012 20441120.40 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 49 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
ICP-AES - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:NQ91592-003
91592 3030 C
08/17/2012 1526Analytical Method:6010C
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(mg/L)(mg/L)
Lead 0.44 08/20/2012 20481110.40 80-1200.79 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N - Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ - RPD is out of criteria_
Page: 50 of 50
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-4620-1
Client Project/Site: NH17015
For:
Shealy Environmental Services, Inc.
106 Vantage Point Drive
West Columbia, South Carolina 29172
Attn: Mr. Lucas Odom
Authorized for release by:
9/6/2012 5:27:47 PM
Ken Hayes
Project Manager I
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
TestAmerica Job ID: 490-4620-1
Page 2 of 21 TestAmerica Nashville9/6/2012
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
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Sample Summary
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-4620-1 SB-2 Solid 08/15/12 09:00 08/21/12 08:15
490-4620-2 SB-3 Solid 08/15/12 09:10 08/21/12 08:15
490-4620-3 SB-1A Solid 08/15/12 09:20 08/21/12 08:15
490-4620-4 SB-4 Solid 08/15/12 09:30 08/21/12 08:15
490-4620-5 MW-1A Ground Water 08/16/12 11:45 08/21/12 08:15
TestAmerica NashvillePage 3 of 21 9/6/2012
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Case Narrative
Client: Shealy Environmental Services, Inc.TestAmerica Job ID: 490-4620-1
Project/Site: NH17015
Job ID: 490-4620-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-4620-1
Comments
No additional comments.
Receipt
The samples were received on 8/21/2012 8:15 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 3.7º C.
GC VOA
Method(s) MA VPH, MAVPH: pH is <2 for all selected samples.
No other analytical or quality issues were noted.
Organic Prep
No analytical or quality issues were noted.
VOA Prep
No analytical or quality issues were noted.
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Definitions/Glossary
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Qualifiers
GC VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
E Result exceeded calibration range.
Glossary
These commonly used abbreviations may or may not be present in this report.
☼Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RL Reporting Limit
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Lab Sample ID: 490-4620-1Client Sample ID: SB-2
Matrix: SolidDate Collected: 08/15/12 09:00
Percent Solids: 82.8Date Received: 08/21/12 08:15
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (adjusted)ND 0.121 mg/Kg ☼09/06/12 15:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.121 mg/Kg 09/06/12 15:25 1☼C5-C8 Aliphatics (adjusted)10.4
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 10.4 5.38 mg/Kg ☼08/22/12 10:17 08/24/12 18:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.38 mg/Kg 08/22/12 10:17 08/24/12 18:44 1☼C9-C10 Aromatics ND
5.38 mg/Kg 08/22/12 10:17 08/24/12 18:44 1☼C9-C12 Aliphatics ND
2,5-Dibromotoluene (fid)105 70-130 08/22/12 10:17 08/24/12 18:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)93 08/22/12 10:17 08/24/12 18:44 170-130
General Chemistry
RL RL
Percent Solids 83 0.10 %08/28/12 12:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Lab Sample ID: 490-4620-2Client Sample ID: SB-3
Matrix: SolidDate Collected: 08/15/12 09:10
Percent Solids: 88.1Date Received: 08/21/12 08:15
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (adjusted)ND 0.114 mg/Kg ☼09/06/12 15:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.114 mg/Kg 09/06/12 15:25 1☼C5-C8 Aliphatics (adjusted)ND
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics ND 5.41 mg/Kg ☼08/22/12 10:17 08/24/12 19:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.41 mg/Kg 08/22/12 10:17 08/24/12 19:15 1☼C9-C10 Aromatics ND
5.41 mg/Kg 08/22/12 10:17 08/24/12 19:15 1☼C9-C12 Aliphatics ND
2,5-Dibromotoluene (fid)101 70-130 08/22/12 10:17 08/24/12 19:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)97 08/22/12 10:17 08/24/12 19:15 170-130
General Chemistry
RL RL
Percent Solids 88 0.10 %08/28/12 12:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Lab Sample ID: 490-4620-3Client Sample ID: SB-1A
Matrix: SolidDate Collected: 08/15/12 09:20
Percent Solids: 73.2Date Received: 08/21/12 08:15
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (adjusted)266 0.137 mg/Kg ☼09/06/12 15:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.137 mg/Kg 09/06/12 15:25 1☼C5-C8 Aliphatics (adjusted)522
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 533 7.15 mg/Kg ☼08/22/12 10:17 08/24/12 19:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
143 mg/Kg 08/22/12 10:17 08/30/12 02:27 20☼C9-C10 Aromatics 314
7.15 mg/Kg 08/22/12 10:17 08/24/12 19:45 1☼C9-C12 Aliphatics 666 E
2,5-Dibromotoluene (fid)183 X 70-130 08/22/12 10:17 08/24/12 19:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)96 08/22/12 10:17 08/30/12 02:27 2070-130
General Chemistry
RL RL
Percent Solids 73 0.10 %08/28/12 12:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Lab Sample ID: 490-4620-4Client Sample ID: SB-4
Matrix: SolidDate Collected: 08/15/12 09:30
Percent Solids: 69.0Date Received: 08/21/12 08:15
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (adjusted)36.1 0.145 mg/Kg ☼09/06/12 15:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.145 mg/Kg 09/06/12 15:25 1☼C5-C8 Aliphatics (adjusted)131
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 132 7.96 mg/Kg ☼08/22/12 10:17 08/24/12 20:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15.9 mg/Kg 08/22/12 10:17 08/30/12 01:57 2☼C9-C10 Aromatics 45.0
7.96 mg/Kg 08/22/12 10:17 08/24/12 20:46 1☼C9-C12 Aliphatics 87.7
2,5-Dibromotoluene (fid)99 70-130 08/22/12 10:17 08/24/12 20:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)95 08/22/12 10:17 08/30/12 01:57 270-130
General Chemistry
RL RL
Percent Solids 69 0.10 %08/28/12 12:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Lab Sample ID: 490-4620-5Client Sample ID: MW-1A
Matrix: Ground WaterDate Collected: 08/16/12 11:45
Date Received: 08/21/12 08:15
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (adjusted)442 100 ug/L 09/06/12 15:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
100 ug/L 09/06/12 15:35 1C5-C8 Aliphatics (adjusted)1660
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics 1710 1000 ug/L 08/23/12 14:56 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1000 ug/L 08/23/12 14:56 10C9-C10 Aromatics 1080
1000 ug/L 08/23/12 14:56 10C9-C12 Aliphatics 1780
2,5-Dibromotoluene (fid)105 70-130 08/23/12 14:56 10
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)96 08/23/12 14:56 1070-130
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QC Sample Results
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 490-14662/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 14662
RL MDL
C5-C8 Aliphatics ND 5000 ug/L 08/23/12 12:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 5000 ug/L 08/23/12 12:54 1C9-C10 Aromatics
ND 5000 ug/L 08/23/12 12:54 1C9-C12 Aliphatics
2,5-Dibromotoluene (fid)95 70-130 08/23/12 12:54 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
91 08/23/12 12:54 12,5-Dibromotoluene (pid)70-130
Client Sample ID: Method BlankLab Sample ID: MB 490-14662/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 14662
RL MDL
C5-C8 Aliphatics ND 100 ug/L 08/23/12 13:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 100 ug/L 08/23/12 13:25 1C9-C10 Aromatics
ND 100 ug/L 08/23/12 13:25 1C9-C12 Aliphatics
2,5-Dibromotoluene (fid)102 70-130 08/23/12 13:25 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
92 08/23/12 13:25 12,5-Dibromotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-14662/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 14662
C5-C8 Aliphatics 300 261.1 ug/L 87 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C10 Aromatics 100 ND ug/L 99 70 -130
C9-C12 Aliphatics 200 179.2 ug/L 90 70 -130
2,5-Dibromotoluene (fid)70 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
962,5-Dibromotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-14662/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 14662
C5-C8 Aliphatics 300 322.7 ug/L 108 70 -130 21 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C10 Aromatics 100 115.3 ug/L 115 70 -130 15 50
C9-C12 Aliphatics 200 225.3 ug/L 113 70 -130 23 50
2,5-Dibromotoluene (fid)70 -130
Surrogate
95
LCSD LCSD
Qualifier Limits%Recovery
862,5-Dibromotoluene (pid)70 -130
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QC Sample Results
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-15072/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 15072
RL MDL
C5-C8 Aliphatics ND 5.00 mg/Kg 08/24/12 12:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 5.00 mg/Kg 08/24/12 12:53 1C9-C10 Aromatics
ND 5.00 mg/Kg 08/24/12 12:53 1C9-C12 Aliphatics
2,5-Dibromotoluene (fid)99 70-130 08/24/12 12:53 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
92 08/24/12 12:53 12,5-Dibromotoluene (pid)70-130
Client Sample ID: Method BlankLab Sample ID: MB 490-15072/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 15072
RL MDL
C5-C8 Aliphatics ND 0.100 mg/Kg 08/24/12 13:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.100 mg/Kg 08/24/12 13:24 1C9-C10 Aromatics
ND 0.100 mg/Kg 08/24/12 13:24 1C9-C12 Aliphatics
2,5-Dibromotoluene (fid)99 70-130 08/24/12 13:24 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
92 08/24/12 13:24 12,5-Dibromotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-15072/2
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 15072
C5-C8 Aliphatics 0.300 0.3006 mg/Kg 100 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C10 Aromatics 0.100 0.1089 mg/Kg 109 70 -130
C9-C12 Aliphatics 0.200 0.1984 mg/Kg 99 70 -130
2,5-Dibromotoluene (fid)70 -130
Surrogate
111
LCS LCS
Qualifier Limits%Recovery
1002,5-Dibromotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-15072/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 15072
C5-C8 Aliphatics 0.300 0.3008 mg/Kg 100 70 -130 0 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C10 Aromatics 0.100 0.1066 mg/Kg 107 70 -130 2 50
C9-C12 Aliphatics 0.200 0.2074 mg/Kg 104 70 -130 4 50
2,5-Dibromotoluene (fid)70 -130
Surrogate
104
LCSD LCSD
Qualifier Limits%Recovery
962,5-Dibromotoluene (pid)70 -130
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QC Sample Results
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-16210/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 16210
RL MDL
C9-C10 Aromatics ND 5.00 mg/Kg 08/29/12 13:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
2,5-Dibromotoluene (pid)94 70-130 08/29/12 13:17 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-16210/2
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 16210
C9-C10 Aromatics 0.100 0.1132 mg/Kg 113 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
2,5-Dibromotoluene (pid)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-16210/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 16210
C9-C10 Aromatics 0.100 0.1073 mg/Kg 107 70 -130 5 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2,5-Dibromotoluene (pid)70 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
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QC Association Summary
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
GC VOA
Prep Batch: 14294
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035490-4620-1 SB-2 Total/NA
Solid 5035490-4620-2 SB-3 Total/NA
Solid 5035490-4620-3 SB-1A Total/NA
Solid 5035490-4620-4 SB-4 Total/NA
Analysis Batch: 14662
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water MAVPH490-4620-5 MW-1A Total/NA
Water MAVPHLCS 490-14662/2 Lab Control Sample Total/NA
Water MAVPHLCSD 490-14662/3 Lab Control Sample Dup Total/NA
Water MAVPHMB 490-14662/4 Method Blank Total/NA
Water MAVPHMB 490-14662/5 Method Blank Total/NA
Analysis Batch: 15072
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 14294490-4620-1 SB-2 Total/NA
Solid MAVPH 14294490-4620-2 SB-3 Total/NA
Solid MAVPH 14294490-4620-3 SB-1A Total/NA
Solid MAVPH 14294490-4620-4 SB-4 Total/NA
Solid MAVPHLCS 490-15072/2 Lab Control Sample Total/NA
Solid MAVPHLCSD 490-15072/3 Lab Control Sample Dup Total/NA
Solid MAVPHMB 490-15072/4 Method Blank Total/NA
Solid MAVPHMB 490-15072/5 Method Blank Total/NA
Analysis Batch: 16210
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 14294490-4620-3 SB-1A Total/NA
Solid MAVPH 14294490-4620-4 SB-4 Total/NA
Solid MAVPHLCS 490-16210/2 Lab Control Sample Total/NA
Solid MAVPHLCSD 490-16210/3 Lab Control Sample Dup Total/NA
Solid MAVPHMB 490-16210/4 Method Blank Total/NA
Analysis Batch: 18079
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA VPH490-4620-1 SB-2 Total/NA
Solid MA VPH490-4620-2 SB-3 Total/NA
Solid MA VPH490-4620-3 SB-1A Total/NA
Solid MA VPH490-4620-4 SB-4 Total/NA
Analysis Batch: 18082
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Ground Water MA VPH490-4620-5 MW-1A Total/NA
General Chemistry
Analysis Batch: 15939
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-4620-1 SB-2 Total/NA
Solid Moisture490-4620-2 SB-3 Total/NA
Solid Moisture490-4620-3 SB-1A Total/NA
Solid Moisture490-4620-4 SB-4 Total/NA
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Lab Chronicle
Client: Shealy Environmental Services, Inc.TestAmerica Job ID: 490-4620-1
Project/Site: NH17015
Client Sample ID: SB-2 Lab Sample ID: 490-4620-1
Matrix: SolidDate Collected: 08/15/12 09:00
Percent Solids: 82.8Date Received: 08/21/12 08:15
Prep 5035 08/22/12 10:17 TP14294 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis MAVPH 1 15072 08/24/12 18:44 FG TAL NSHTotal/NA
Analysis MA VPH 1 18079 09/06/12 15:25 OD TAL NSHTotal/NA
Analysis Moisture 1 15939 08/28/12 12:34 RC TAL NSHTotal/NA
Client Sample ID: SB-3 Lab Sample ID: 490-4620-2
Matrix: SolidDate Collected: 08/15/12 09:10
Percent Solids: 88.1Date Received: 08/21/12 08:15
Prep 5035 08/22/12 10:17 TP14294 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis MAVPH 1 15072 08/24/12 19:15 FG TAL NSHTotal/NA
Analysis MA VPH 1 18079 09/06/12 15:25 OD TAL NSHTotal/NA
Analysis Moisture 1 15939 08/28/12 12:34 RC TAL NSHTotal/NA
Client Sample ID: SB-1A Lab Sample ID: 490-4620-3
Matrix: SolidDate Collected: 08/15/12 09:20
Percent Solids: 73.2Date Received: 08/21/12 08:15
Prep 5035 08/22/12 10:17 TP14294 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis MAVPH 1 15072 08/24/12 19:45 FG TAL NSHTotal/NA
Analysis MAVPH 20 16210 08/30/12 02:27 FG TAL NSHTotal/NA
Analysis MA VPH 1 18079 09/06/12 15:25 OD TAL NSHTotal/NA
Analysis Moisture 1 15939 08/28/12 12:34 RC TAL NSHTotal/NA
Client Sample ID: SB-4 Lab Sample ID: 490-4620-4
Matrix: SolidDate Collected: 08/15/12 09:30
Percent Solids: 69.0Date Received: 08/21/12 08:15
Prep 5035 08/22/12 10:17 TP14294 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis MAVPH 1 15072 08/24/12 20:46 FG TAL NSHTotal/NA
Analysis MAVPH 2 16210 08/30/12 01:57 FG TAL NSHTotal/NA
Analysis MA VPH 1 18079 09/06/12 15:25 OD TAL NSHTotal/NA
Analysis Moisture 1 15939 08/28/12 12:34 RC TAL NSHTotal/NA
Client Sample ID: MW-1A Lab Sample ID: 490-4620-5
Matrix: Ground WaterDate Collected: 08/16/12 11:45
Date Received: 08/21/12 08:15
Analysis MAVPH 08/23/12 14:56 FG1014662 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
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Lab Chronicle
Client: Shealy Environmental Services, Inc.TestAmerica Job ID: 490-4620-1
Project/Site: NH17015
Client Sample ID: MW-1A Lab Sample ID: 490-4620-5
Matrix: Ground WaterDate Collected: 08/16/12 11:45
Date Received: 08/21/12 08:15
Analysis MA VPH 09/06/12 15:35 OD118082 TAL NSH
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-4620-1Client: Shealy Environmental Services, Inc.
Project/Site: NH17015
Method Method Description LaboratoryProtocol
MA DEPMA VPH Massachusetts - Volatile Petroleum Hydrocarbons (GC)TAL NSH
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Certification Summary
Client: Shealy Environmental Services, Inc.TestAmerica Job ID: 490-4620-1
Project/Site: NH17015
Laboratory: TestAmerica Nashville
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
10-30-12393ACIL
A2LA ISO/IEC 17025 0453.07 12-31-13
Alabama State Program 4 41150 05-31-13
Alaska (UST)State Program 10 UST-087 07-24-13
Arizona State Program 9 AZ0473 05-05-13
Arkansas DEQ State Program 6 88-0737 04-25-13
California NELAC 9 1168CA 10-31-12
Canadian Assoc Lab Accred (CALA)Canada 3744 03-08-14
Colorado State Program 8 N/A 02-28-13
Connecticut State Program 1 PH-0220 12-31-13
Florida NELAC 4 E87358 06-30-13
Illinois NELAC 5 200010 12-09-12
Iowa State Program 7 131 05-01-14
Kansas NELAC 7 E-10229 10-31-12
Kentucky State Program 4 90038 12-31-12
Kentucky (UST)State Program 4 19 09-15-13
Louisiana NELAC 6 LA110014 12-31-12
Louisiana NELAC 6 30613 06-30-13
Maryland State Program 3 316 03-31-13
Massachusetts State Program 1 M-TN032 06-30-13
Minnesota NELAC 5 047-999-345 12-31-12
Mississippi State Program 4 N/A 06-30-13
Montana (UST)State Program 8 NA 01-01-15
Nevada State Program 9 TN00032 09-30-12
New Hampshire NELAC 1 2963 10-09-12
New Jersey NELAC 2 TN965 06-30-13
New York NELAC 2 11342 04-01-13
North Carolina DENR State Program 4 387 12-31-12
North Dakota State Program 8 R-146 06-30-13
Ohio VAP State Program 5 CL0033 01-19-14
Oregon NELAC 10 TN200001 04-30-13
Pennsylvania NELAC 3 68-00585 06-30-13
Rhode Island State Program 1 LAO00268 12-30-12
South Carolina State Program 4 84009 [phone]
South Carolina State Program 4 84009 [phone]
Tennessee State Program 4 2008 02-23-14
Texas NELAC 6 T104704077-09-TX 08-31-13
USDA Federal S-48469 11-02-13
Utah NELAC 8 TAN 06-30-13
Virginia NELAC 3 460152 06-14-13
Washington State Program 10 C789 07-19-13
West Virginia DEP State Program 3 219 02-28-13
Wisconsin State Program 5 998020430 08-31-13
Wyoming (UST)A2LA 8 453.07 12-31-13
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Login Sample Receipt Checklist
Client: Shealy Environmental Services, Inc.Job Number: 490-4620-1
Login Number: 4620
Question Answer Comment
Creator: Gambill, Shane
List Source: TestAmerica Nashville
List Number: 1
N/ARadioactivity either was not measured or, if measured, is at or below
background
N/AThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.3.7
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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APPENDIX IV
Monitoring Well Construction and Variance Applications and Approvals

APPENDIX V

Monitoring Well Construction Record and Soil Boring Log