MO-8827_40338_CA_MRP_20200611_Monitoring Report 2020

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\I
Civil-Geotechnical-Surveying
June 11, 2020
Trudy Beverly, L.G.
Hydrogeologist
North Carolina Department of Environmental Quality
601 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Re: Transmittal of Monitoring Report
Six-O-One Stop
5661 Highway 601 South
Concord, Cabarrus County, North Carolina
Incident Number: 40338
Risk Classification: High
Dear Ms. Beverly:
On behalf of our client, Mr. Marc Glover, operator of Six-O-One Stop, Concord
Engineering and Surveying, Inc. (CESI) has prepared the attached Monitoring Report for
the facility which is located at 5661 Highway 601 South, Concord, North Carolina.
CESI apologizes for the tardiness of the report. Should you have any questions, please
do not hesitate to contact me at [phone].
Sincerely,
Az� �— e--,—
Steven E. Irminger, P.E.
Senior Engineer
45 Spring Street, SW P.O. Box 268 Concord, NC 28026-0268 704-786-5404
www.cesicgs.com NC License Number C-0263

Monitoring Report
A. Site Information
1. Site Identification
Date of Report: June 11, 2020
Facility I.D.: 4753 UST Incident Number (if known): 40338
Site Name: Six-O-One Stop
Site Street Address: 5661 Highway 601 South
City/Town: Concord Zip Code: 28025 County: Cabarrus
Description of Geographical Data Point (e.g., diesel fill port): Center of onsite building
Location Method (GPS, topographical map, other): Topographic Map
Latitude (decimal degrees): 35.339270 Longitude (decimal degrees):-80.520200
2. Information about Contacts Associated with the Leaking UST System
BUST Owner: Marc Glover
Address: 5661 Highway 601 South, Concord, North Carolina 28025 Tel.: [phone]
BUST Operator: Marc Glover
Address: 5661 Highway 601 South, Concord, North Carolina 28025 Tel: [phone]
Property Owner: Misenheimer, Sydnie, Lynne
Address: 38288A Gold Hill Road, Richfield, North Carolina 28137 Tel.:
Property Occupant: Marc Glover.
Address: 5661 Highway 601 South, Concord, North Carolina 28025 Tel: [phone]
Consultant/Contractor: CESI Land Development Services
Address: P.O. Box 268 Tel: [phone]
Analytical Laboratory: Pace Analytical, Inc. State Certification No. 37712
Address: 9800 Kincey Avenue, Huntersville, North Carolina Tel: [phone]
3. Information about Release
Date Discovered: January 17, 2014
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (Dispenser/Piping/UST): Unknown
Sizes and contents of UST system(s) from which the release occurred):
(3) 6,000 gallon gasoline USTs
(1) 2,000 gallon diesel UST
(1) 550 gallon kerosene UST
(1) 550 gallon used oil UST
4. Certification
I, Steven Irminger, a Professional Engineer for Concord Engineering and Surveying, Inc. (CESI), do certify that the
information contained in this report is correct and accurate to the best of my knowledge. CESI is licensed to practice
engineering in North Carolina. The certification number of the company or corporation is C-0263.
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Monitoring Report
Six-O-One Stop Property
June 11, 2020
Page No. 2
B. Executive Summary
No free product was observed on the on the property during the monitoring property.
During the monitoring period, groundwater samples were collected from six of the eight
monitoring wells and from three neighboring water supply wells. Monitoring well MW-4 has been
covered with gravel and could not be located on the day of the sample event. A building has been
constructed over the location of well MW-3. While the floor of the building appears to be the
former asphalt parking lot, equipment stored in the building prevented CESI personnel from
accessing the well. The owner has stated he will provide access to well MW-3 and assist in
locating well MW-4. Groundwater samples from the remaining six wells were collected on May
8, 2020, and submitted to Pace Analytical, Inc. (Pace) for analysis by EPA Method SM6200 B.
The analytical results of water samples from four monitoring wells were reported at concentrations
that exceed the 15A NCAC 2L standard. None of the water sample results were reported at
concentrations greater than the Gross Contamination Level (GCL). Analysis of groundwater
samples collected from the three water supply wells were reported to be below the sample detection
limit.
Based on isoconcentration contour diagrams prepared for dissolved hydrocarbons reported in
groundwater samples collected May 8, 2020, the horizontal and vertical extent of dissolved
petroleum hydrocarbons appear similar to the distribution of dissolved petroleum hydrocarbons
reported in groundwater samples collected January 21, 2018. The data suggests that the dissolved
hydrocarbon plume is stable. A Plume Stability Report has been prepared using the May 8, 2020
data, and is submitted under separate cover.

Monitoring Report
Six-O-One Stop Property
June 11, 2020
Page No. 3
C. Table of Contents
A.
Site Information................................................................................................................................................1
B.
Executive Summary ..........................................................................................................................................2
C.
Table of Contents.............................................................................................................................................3
D.
Site History and Characterization.....................................................................................................................5
E.
Presentation of Current Site Assessment Information......................................................................................7
F.
Free Product Removal......................................................................................................................................9
G.
Soil and Groundwater Remediation..................................................................................................................9
H.
Conclusions and Recommendations.................................................................................................................9
LIST OF FIGURES
FIGURE 1
Street Atlas
FIGURE 2
Topographic Location Map
FIGURE 3
Site Layout
FIGURE 4
Sensitive Receptor Map
FIGURE 5
Land Use Map
FIGURE 6
Soil Sample Location Map
FIGURE 7
Monitoring Well Location Map
FIGURE 8
Benzene Isoconcentration Map May 8, 2020
FIGURE 9
MTBE Isoconcentration Map May 8, 2020
FIGURE 10
Piezometric Surface Contour Diagram May 8, 2020
LIST OF TABLES
B-1
Site History — UST/AST Information
B-2
Site History — Owner/Operator Information
B-3
Soil Analytical Summary
B-4
Groundwater Analytical Summary
B-5
Receptor Information
B-6
Adjoining Parcel Ownership
B-7
Well Construction Information
B-8
NOT USED
B-9
Groundwater Elevations
B-10
Land Use

Monitoring Report
Six-O-One Stop Property
June 11, 2020
Page No. 4
LIST OF APPENDICES
APPENDIX 1 DEQ Correspondence
APPENDIX 2 Laboratory Reports and Chain -of -Custody Records

Monitoring Report
Six-O-One Stop Property
June 11, 2020
Page No. 5
D. Site History and Characterization
Since submittal of the CSA on March 4, 2016, no changes have occurred regarding the ownership
or operation of the Property. The owner and operator information is listed on the cover of this
report and in Table B-2. All of the underground storage tanks at this Property were removed in
December 2013, and no new USTs have been installed. Information regarding the former
underground storage tanks (USTs) is provided on Table B-1. A Street Atlas showing the location
of the Property is provided as Figure 1. The Property location is shown on a portion of a United
States Geological Survey Topographical Quadrangle Map as Figure 2. The location of the former
tanks is shown on a Property Layout as Figure 3.
The tanks of this report were underground. No evidence of aboveground storage tanks were
observed or reported. No spills have been reported for the facility other than the discovery January
17, 2014, of petroleum parameters in soil samples collected from beneath the gasoline USTs, diesel
and kerosene USTs, and the gasoline dispenser piping. The analytical results of soil samples
collected September 8, 2014, from beneath the dispensers were reported to the North Carolina
Department of Environmental Quality (DEQ) in a letter dated January 16, 2015.
The precise source and timing of contamination is not known. All of the USTs were observed for
evidence of corrosion or damage. No significant corrosion or damage was observed. Further
release was prevented by pump out of the USTs prior to their removal from the ground. Removal
of source material (contaminated soil) was initiated immediately following removal of tanks. Field
screening results indicated that the areas of greatest contamination were beneath the northern ends
of the gasoline USTs, the southern end of the kerosene and diesel USTs and the elbow of the
gasoline dispenser lines. No historical UST releases, non -UST releases, or off -site releases have
been reported.
Site Characteristics: The Property consists of one irregular -shaped parcel located at the northwest
quadrant of the intersection of Highway 601 south and Cold Springs Road. The area of the parcel
is approximately 2.67-acres and is improved with a gas station/convenience store/ automobile
service facility. The Property location is shown on a Street Atlas as Figure 1. According to the
Cabarrus County Tax Assessor's GIS website, the Property Parcel Number is 55486177360000.
Site Vicinity Characteristics: The Property vicinity is primarily residential and commercial use
along U.S. Highway 61, with residential and agricultural land use away from the U.S. Highway
601 corridor.
LOCATION
PROPERTY
TOPOGRAPHIC
POSITION
North adjoining
5600 Cold Springs Road, residence owned
Cross gradient.
by John Plyer (5600 Clod Springs Road,
Concord, NC 28025
Northwest
5625 Highway 601 South, vacant land owned
Down gradient.
adjoining
by Estate of Elma Saunders (140 Crescent
Street, Kanna olis, NC 28081

Monitoring Report June 11, 2020
Six-O-One Stop Property Page No. 6
East adjoining
Cold Springs Road, beyond which is 5651
Down gradient.
Cold Springs Road, residence owned by
Lanney Griffin (5651 Cold Springs Road,
Concord, NC 28025).
Southeast adjoining
Cold Springs Road, beyond which is 5807
Down gradient.
Highway 601 South, residence owned by
Robert L. Price (5807 Highway 601 South,
Concord, NC 28025).
South Adjoining
Highway 601 South, beyond which is 5770
Down gradient
Highway 601 South, residence owned by
Margie Church (2767 Dale Earnhardt Blvd.,
Kanna olis, NC 28083
Southwest
Highway 601 South, beyond which is 5664
Down gradient
Adjoining
Highway 601 South, residence owned by
Dorethea Young (4906 Fenwick Place,
Concord, NC 28025
West Adjoining
Highway 601 South, beyond which is 5727
Up gradient
Old Monroe Circle, residence owned by
Karen Sarver (5727 Old Monroe Circle,
Concord, NC 28025
Water Supply: The Property is provided water from the City of Concord. One inactive potable
well was observed on the northern portion of the Property. Adjoining properties are provided
potable water by wells and by municipal water from a main located along Highway 601. CESI
updated water supply information for properties within 1,000 feet of the Property. In April 2020,
survey questionnaires were sent certified mail to properties within 1,000 feet of the Property. For
those properties that refused delivery, CESI conducted a search for wells by reviewing aerial
photographs and by viewing from municipal streets. A summary of the mailings and field
reconnaissance for water supply wells is provided in Table B-5. The information is shown on a
map as Figure 4.
Topography. CESI obtained a copy of the USGS 7.5-minute topographic map, Concord, North
Carolina Quadrangle, dated 1991. A copy of a portion of the topographic map showing the
Property location is provided on Figure 2. The elevation of the Property is approximately 630
feet above mean sea level (msl). Based upon the topographic contours observed on the USGS
topographic contour map, the Property is located on a southwest to northeast trending ridge. The
slope is generally downward toward the east although the extreme western portion of the Property
slopes toward the northwest.
Vegetation: The Property consists of the building footprint, asphalt pavement, two canopies, a
propane AST, and grass turf.
Surface Water: No surface water was observed on the Property. The nearest surface water
indicated on the topographic map is an unnamed stream located approximately 1,000 feet
northwest of the Property.

Monitoring Report June 11, 2020
Six-O-One Stop Property Page No. 7
Wells: One inactive potable well was observed on the northern portion of the Property. The well
head is blocked and groundwater cannot be accessed.
Buildings: The Property is improved with one single -story commercial building. The building
is occupied by a convenience store and two automobile service bays. No other USTs or ASTs
(other than one propane AST) were observed onsite. In 2019, a metal storage building was erected
along the southeast side of the main building. The metal building has no floor and is used to store
automotive parts. The Property Layout is shown as Figure 3.
Surface Cover: The majority of the Property surface is covered by the building, asphalt parking
lot, and turf.
Soil Type: According to the USDA web -based soil survey of Cabarrus County, the surficial Soil
at the Property is composed of Urban Land Complex.
List of all Prior Reports Submitted:
UST Closure Report; CESI; April 4, 2014
Limited Site Assessment; CESI; May 2, 2015
Comprehensive Site Assessment; CESI; March 2, 2016
Monitoring Report; CESI; January 16, 2016
Plume Stability Report; CESI; July 10, 2017
Monitoring Report; CESI; March 20, 2018
Summarize implementation of the remedial plan proposed in the CAP.
A CAP has not been prepared for the site.
E. Presentation of Current Site Assessment Information
On May 8, 2020, CESI personnel measured the depth to water using a washed interface probe capable
of measuring phase separated liquids as thin as 0.01 feet. No free product was encountered during
the reporting period.
Groundwater samples were collected from three water supply wells on May 8, 2020. The addresses
of the water supply wells are: 5600 Cold Springs Road (Property Number 1 on Figure 5); 5677 Cold
Springs Road (Property Number 12 on Figure 5); and, 5726 Old Monroe Circle (Property Number
28 on Figure 5). The water samples were collected from a hose bib on top of the well or the nearest
hose bib available at the residence. No samples were collected through a hose. The water was allowed
to flow for five minutes prior to collection of a sample directly into the laboratory supplied sample
containers. The water samples were analyzed for volatile organic compounds using EPA Method SM
6200B. Based on the analytical report, no parameters were reported above the sample detection limit.
A copy of the laboratory report and chain of custody record is provided in Appendix 2. A summary
of water supply well analytical results is provided on Table B-8. CESI attempted to retrieve a water

Monitoring Report June 11, 2020
Six-O-One Stop Property Page No. 8
sample from the onsite water supply well (well 1) but was unable to lower a bailer because of
interference from the downhole pump cable and discharge line. This well is disconnected from the
electrical supply and has reportedly not been used for many years.
The nearest water supply well is located at 5600 Cold Springs Road (Property Number 1 on Figure
5). The owner of the well, Mr. John Plyer, stated that he was adamantly opposed to being connected
to the city water supply which is available along Highway 601. Mr. Plyer's well is approximately
310 feet north and cross -gradient of monitoring well MW-2.
On May 8, 2020, CESI personnel attempted to collect groundwater samples from wells MW-1 to
MW-8. Monitoring well MW-4 could not be located as the owner has spread gravel over this
portion of the parking lot. Monitoring well MW-3 could not be sampled because it was blocked
by automotive repair parts stored in a building constructed in 2019. The owner will contact CESI
when the wells are accessible.
The accessible monitoring wells were purged of three casing volumes using a new polyethylene
bailer. A water sample was then collected for laboratory analysis. The water samples were
collected into laboratory supplied sample bottles and immediately placed on ice. The samples
were transported to Pace using Chain -of -Custody protocol. CESI requested that Pace analyze the
water samples for VOCs using EPA Method SM6200B. The results of the groundwater analyses
are summarized on Table B-4. A copy of the laboratory report and chain -of -custody record is
provided in Appendix 3. Analysis of groundwater samples from the monitoring wells revealed
gasoline parameters greater than the North Carolina Administrative Code (NCAC) 15A 2L
standard in wells MW-I, MW-2, MW-7, MW-8. None of the tested parameters exceeded Gross
Contaminant Levels GCLs. The analytical results for benzene and Methyl-tert-butyl-ether
(MTBE) were posted on a Site Layout and contoured. The resulting isoconcentration contour
diagrams for benzene and MTBE are provided as Figure 8 and Figure 9, respectively. Based on
a comparison of prior isoconcentration contour diagrams and those prepared from the May 8, 2020,
sampling event, the dissolved hydrocarbon plume appears to be stable. However, concentrations
increased in several wells indicating that rebound from adsorbed hydrocarbons is occurring.
According to the Geologic Map of North Carolina 1985, the Property is located in the Piedmont
Physiographic Province. The dominant rocks in this region are composed mainly of
metamorphosed mudstone and argillite of the Cenozoic Era. The rocks are thin to thick bedded,
with bedding planes and angular cleavage common and occur interbedded with metasandstone,
metaconglomerate, and metavolcanic rock. This area is geologically characterized by a thin layer
of red Saprolite over fractured bedrock. Saprolite is defined as soft, earthy, clay -rich, thoroughly
decomposed rock formed in place by chemical weathering of igneous and metamorphic rocks. The
term is applied to any unconsolidated residual material underlying the soil and grading to bedrock
below. Bedrock was not observed at the surface in the vicinity of the Property. Drilling of
monitoring wells encountered a blocky, well consolidated mudstone from approximately 12-feet
below grade to the maximum depth penetrated of 50-feet below grade.
Depth to groundwater: Depth to groundwater measurements at the site revealed depth to water
approximately 18 feet below grade. No free product was encountered. A summary of the water level
data is provided on Table B-9. The water levels recorded in 2020 are several feet shallower than

Monitoring Report June 11, 2020
Six-O-One Stop Property Page No. 9
those recorded in 2018. The piezometric surface contour diagram from data recorded May 8, 2020,
is provided as Figure 10. The piezometric surface contour diagram indicates that groundwater flow
is toward the southwest.
No free product has been observed onsite. Based on the groundwater analytical results of samples
collected May 8, 2020, the areal extent of dissolved hydrocarbons appears to be defined except to the
south for benzene. The vertical extent of impact has not been defined for MTBE in the deep screen
well MW-8. However, based on the low concentrations of dissolved petroleum hydrocarbons in wells
MW-7 and MW-8, CESI does not recommend further assessment at this time.
F. Free Product Removal
No free product has been observed at the site.
G. Soil and Groundwater Remediation
No remediation has been implemented at this site.
H. Conclusions and Recommendations
None of the tested parameters were reported at concentrations exceeding GCLs. Interview with
the nearest water well owner, Mr. John Plyer of 5600 Cold Springs Road on May 8, 2020, and
interview with the second nearest water supply well owner located at 5651 Cold Springs Road on
January 21, 2018, stated that they did not want to connect to municipal water.
CESI recommends preparation of a full scale CAP designed to reduce dissolved groundwater
concentrations to below the 2L standard.

FIGURES

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FIGURE 1 STREET ATLAS MAP Not To Scale N ?
CONCORD ENGINEERING AND Site Name: Highway Six One Stop
5661 South Highway 601
SURVEYING, INC. Concord, NC 28025
Project Number: 131148

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FIGURE 2 TOPOGRAPHIC MAP Not To Scale N ?
CONCORD ENGINEERING AND Site Name: Highway Six One Stop
5661 South Highway 601
SURVEYING, INC. Concord, NC 28025
Project Number: 131148

FIGURE 3 SITE LAYOUT Not To Scale N T
Site Name: Highway Six O One Stop
Concord Engineering and 5661 South Highway 601
Surveying, Inc. Concord, NC 28025

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FIGURE 4 WATER SUPPLY WELLS Not To Scale N ?
Concord Engineering and Site Name: Highway Six O One Stop
g g 5661 South Highway 601
Surveying, Inc. Concord, NC 28025

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CONCORD ENGINEERING AND Site Name: Highway Six One Stop
5661 South Highway 601
SURVEYING, INC. Concord, NC 28025
Project Number: 131148

TABLES

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
S stem?
1
Gasoline
None
6,000
Single wall
16'L 8'D
Single wall
1961
Removed
Yes
steel
steel
2013
2
Gasoline
None
6,000
Single wall
16'L 8'D
Single wall
1961
Removed
Yes
steel
steel
2013
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
Incident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
* * * Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)
Change 2

Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: 3/2/2014 Incident Number and Name: 40338 Six O One Stop
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
S stem?
3
Gasoline
None
6,000
Single wall
16'L 8'D
Single wall
1961
Removed
Yes
steel
steel
2013
4
Kerosene
None
550
Single wall
6'L 4'D
Single wall
1978
Removed
Yes
steel
steel
2013
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
S stem?
Add additional records as necessary
Incident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)

Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: 3/2/2014 Incident Number and Name: 40338 Six O One Stop
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
S stem?
5
Diesel
None
2,000
Single wall
13.5'L 5'D
Single wall
1978
Removed
Yes
steel
steel
2013
6
Used oil
None
550
Single wall
6'L 4'D
Single wall
1985
Removed
Yes
steel
steel
2014
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
S stem?
Add additional records as necessary
Incident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
* * * Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)

Appendix B
Reporting Tables
Table B-2: Site History - UST/AST Owner/Operator and Other Responsible
Party Information
Revision Date: 01/16/2017 Incident Number and Name: 40338 Six O One Stop
UST ID Number
00-0-0000004753
Facility ID Number
4753
Name of Owner
Dates of Operation
mm/dd/ to mm/dd/
Six O One Station, LLC
Current
Street Address
304 S. Second Street
city
State
Zip
Tele hone Number
Albemarle
NC
28001
Name of Operator
Dates of Operation
mm/dd/ to mm/dd/
Marc Glover
Current
Street Address
5661 Highway 601 S.
city
State
Zip
Tele hone Number
Concord
NC
28025
704-786-0600
Incident Number
Name of Other Responsible Party
Dates of Release(s)
mm/dd/ to mm/dd/
Street Address
city
State
zip
Telephone Number
Add additional records for all owners, operators and responsible parties as necessary.

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
p
Tank pit
, 20Day,
1)
LSA,
x
etc.)Tank
l
12/12/13
11
Closure
266
North
gastankBelow
Tank 1
12/12/13
11
Closure
8.9
South
gas t nkBelow
Tank 2
12/13/13
gash
11
Closure
11.7
North
Tank 2
12/13/13
Below
11
Closure
<6.1
South
gas
Minimum Reporting Limit (mg/kg)
Varies
Soil to groundwater MSCC (mg/kg)
10
Residential MSCC (mg/kg)
10
Industrial/Commercial MSCC (mg/kg)
10
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
p
Tank pit
, 20Day,
1)
LSA,
x
etc.)Tank
3
12/13/13
11
Closure
132
North
gastankBelow
Tank 3
12/13/13
11
Closure
<6.6
South
gast nkBelow
Minimum Reporting Limit (mg/kg)
Varies
Soil to groundwater MSCC (mg/kg)
10
Residential MSCC (mg/kg)
10
Industrial/Commercial MSCC (mg/kg)
10
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
0
0
0
(m/dd/yy)
(eg.
(ft BGS)
(Closure
a�
Tank pit
, 20Day,
O
O
,Z,
a00
a
°
1
LSA,
U
U
U
o
¢
O
etc.
O
U
O
O
U
O
9
N
M
East side
E1
12/13/13
gas UST
16
Closure
284
683
231
1.430
7.420
1.060
1.310
2.910
31.800
12.200
it
West side
E2
12/13/13
gas UST
16
Closure
43.2
85.9
57.6
<0.777
2.230
<0.777
<0.777
1.540
13.400
3.290
it
East
East side
12/16/13
diesel
11
Closure
241
681
397
1.360
1.460
<0.634
0.720
3.460
34.000
4.110
Wall
UST pit
South side
E3
12/13/13
gas UST
16
Closure
106
512
209
<1.290
6.110
<1.290
<1.290
3.530
28.400
10.400
it
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
4.3
4.9
1.7
0.12
0.16
8.5
8.3
Residential MSCC (mg/kg)
939
1500
469
626
1560
1564
100
313
782
782
Industrial/ Commercial MSCC (mg/kg)
24528
40000
12264
16350
40000
40880
4000
8176
20440
20440
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
10 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8260
8270
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
°
R
Tank pit
, 20Day,
i
>,
1)
LSA,
�'
¢
etc.
East side
E1
12/13/13
gas UST
16
Closure
39.700
36.900
2.850
<0.712
<0.712
it
West side
E2
12/13/13
gas UST
16
Closure
8.390
7.490
0.905
1.910
<0.790
it
East
East side
12/16/13
diesel
11
Closure
5.100
5.100
<0.634
1.920
<0.634
Wall
UST pit
South side
E3
12/13/13
gas UST
16
Closure
38.700
32.600
6.110
3.180
3.110
it
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.6
4.6
1.7
4.3
Residential MSCC (mg/kg)
3129
3129
3129
626
1200
Industrial/Commercial MSCC (mg/kg)
81760
81760
81760
16350
32000
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
11 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
0
0
0
(m/dd/yy)
(eg.
(ft BGS)
(Closure
a�
Tank pit
, 20Day,
O
O
,Z,
a
�
a
°
1
LSA,
U
U
U
o
a
o
etc.
O
O
O
U
-0
O
I
I L
I Z
N
I
M
South
South side
12/16/13
diesel
11
Closure
50.1
133
38.2
1.570
3.530
0.880
0.959
1.630
14.7
6.930
Wall
UST pit
North side
E4
12/13/13
gas UST
16
Closure
244
579
278
0.846
4.930
<0.760
<0.760
2.590
16.600
5.760
it
Bottom
E5
12/13/13
gas UST
18
Closure
147
1260
<0.251
8.910
1.260
1.760
7.380
48.500
14.600
it
North
North side
12/16/13
diesel
11
Closure
<2.5
<2.5
<2.5
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
Wall
UST pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
4.3
4.9
1.7
0.12
0.16
8.5
8.3
Residential MSCC (mg/kg)
939
1500
469
626
1560
1564
100
313
782
782
Industrial/Commercial MSCC (mg/kg)
24528
40000
12264
16350
40000
40880
4000
8176
20440
20440
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
12 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
°
R
Tank pit
, 20Day,
1)
LSA,
48
°
N
etc.)
'
South
South side
12/16/13
diesel
11
Closure
5.650
5.650
<0.822
3.600
<0.822
<0.822
Wall
UST pit
North side
E4
12/13/13
gas UST
16
Closure
29.500
22.300
7.190
2.500
<0.760
<0.760
it
North side
E5
12/13/13
gas UST
18
Closure
65.500
46.900
18.600
4.770
10.800
1.110
it
North
North side
12/16/13
diesel
11
Closure
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
Wall
UST pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.6
4.6
1.7
4.3
0.0056
Residential MSCC (mg/kg)
3129
3129
3129
626
1200
18
Industrial/Commercial MSCC (mg/kg)
81760
81760
81760
16350
32000
164
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
13 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
0
0
0
(m/dd/yy)
(eg.
(ft BGS)
(Closure
a�
Tank pit
, 20Day,
O
O
,Z,
a00
a
°
1
LSA,
U
U
U
o
a
O
etc.)
O
I U
O
I U
O
I U
O
I
I L
9
I Z
N
I
M
West
West side
12/16/13
diesel
11
Closure
<2.2
2.6
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
Wall
UST pit
Gas
L1
12/31/13
dispenser
3.5
Closure
236
764
307
3.220
10.300
1.460
1.540
9.650
53.900
16.900
line
Gas
L2
12/31/13
dispenser
3.5
Closure
<41.7
754
341
4.370
8.050
<3.340
<3.340
14.100
66.900
20.400
line
Gas
L3
12/31/13
dispenser
3.5
Closure
69.5
237
83.4
0.0136
0.0177
0.0086
0.0099
0.0235
0.192
0.0628
line
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
4.3
4.9
1.7
0.12
0.16
8.5
8.3
Residential MSCC (mg/kg)
939
1500
469
626
1560
1564
100
313
782
782
Industrial/ Commercial MSCC (mg/kg)
24528
40000
12264
16350
40000
40880
4000
8176
20440
20440
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
14 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8260
8270
8270
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
s~
R
Tank pit
, 20Day,
i
Z
w
1)
LSA,
etc.)
E
West
West side
12/16/13
diesel
11
Closure
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
0.0141
Wall
UST pit
Gas
L1
12/31/13
dispenser
3.5
Closure
47.000
44.300
2.690
7.080
<1.410
<1.410
<1.410
line
Gas
L2
12/31/13
dispenser
3.5
Closure
56.600
40.500
16.100
7.520
3.590
<3.340
<3.340
line
Gas
L3
12/31/13
dispenser
3.5
Closure
0.125
0.0791
0.0462
0.0351
<0.0054
<0.0054
<0.0054
line
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.6
4.6
1.7
4.3
0.0056
0.091
Residential MSCC (mg/kg)
3129
3129
3129
626
1200
18
350
Industrial/ Commercial MSCC (mg/kg)
81760
81760
81760
16350
32000
164
3100
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
15 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
0
0
0
(m/dd/yy)
(eg.
(ft BGS)
(Closure
a�
Tank pit
, 20Day,
O
O
,Z,
a
�
a
°
1
LSA,
U
U
U
o
a
o
etc.
O
O
O
U
-0
+�..,
O
N
H
M
H
Gas
L4
12/31/13
dispenser
12
Closure
196
451
118
2.260
10.300
1.520
<1.370
2.490
27.900
8.790
line
Gas
L5
12/31/13
dispenser
12
Closure
209
346
102
0.158
1.090
0.342
0.262
0.397
0.201
0.556
line
Gas
L6
12/31/13
dispenser
12
Closure
209
607
180
<2.810
7.770
<2.810
<2.810
3.240
23.000
8.090
line
East Wall
Bottom
12/16/13
diesel
14
Closure
<2.2
2.6
<2.2
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
(Bottom)
UST Pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
4.3
4.9
1.7
0.12
0.16
8.5
8.3
Residential MSCC (mg/kg)
939
1500
469
626
1560
1564
100
313
782
782
IndustriaUCommercial MSCC (mg/kg)
24528
40000
12264
16350
40000
40880
4000
8176
20440
20440
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
16 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8260
8270
8270
8260
Contaminant of Concern 4
r.
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
R
Tank pit
, 20Day,
i>1w
H
Gas
L4
12/31/13
dispenser
12
Closure
59.500
42.300
17.300
5.570
8.270
<1.370
<1.370
<1.370
line
Gas
L5
12/31/13
dispenser
12
Closure
1.040
0.898
0.142
0.807
0.388
0.0093
<0.0055
0.115
line
Gas
L6
12/31/13
dispenser
12
Closure
37.500
27.000
10.400
4.560
2.940
<2.810
<2.810
<2.810
line
East Wall
Bottom
12/16/13
diesel
14
Closure
<0.009
<0.009
<0.0045
<0.0045
<0.0045
<0.0045
0.0141
<0.0045
(Bottom)
UST Pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.6
4.6
1.7
4.3
0.0056
0.091
4.3
Residential MSCC (mg/kg)
3129
3129
3129
626
1200
18
350
626
IndustriaUCommercial MSCC (mg/kg)
81760
81760
81760
16350
32000
164
3100
16350
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
17 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
4
VPH x
VPHa
VPHc
EPHb
EPHy
EPHd
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
N
U
O
U
00
�O
U
N
U
U0o
U
1)
LSA,
U
i
U
0
o
0
0
0
+
^"
etc.
U
U
U
U
U
U
as
U
BUsed
1/9/14
8
Closure
<1.3
5.4
3.0
<11.7
<11.7
<11.7
16.1
14.7
0.453
0.583
Bo
O 1 UST
sed
WeOst
1/9/14
7
Closure
<2.8
<2.8
<2.8
<13.6
<13.6
<13.6
16.4
16.4
<4.470
<4.470
Oil UST
Used
WO East
1/9/14
7
Closure
<1.7
<1.7
<1.7
<13.1
<13.1
<13.1
14.8
14.8
<0.431
<0.431
Oil UST
DUST
O
1/9/14
7
Closure
<1.8
25.2
14.8
14.2
32.7
<11.5
39.4
26.3
<3.800
<3.800
N h
Oil
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
Immob
68
540
31
ile
540
31
39
290
Residential MSCC (mg/kg)
939
1500
469
31000
1500
469
88
620
Industrial/Commercial MSCC (mg/kg)
24528
40000
12264
810000
40000
12264
780
16400
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg. Groundwater MSCC. Red shading indicates exceedance of
mg/kg =milligrams per kilogram Residential MSCC.
18 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
EPH
EPH
EPH
8260
8260
8260
8260
Contaminant of Concern 4
as
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closures
Tank pit
, 20Day,
1)
LSA,
°
¢
etc.)
"
7
Used
8
Closure
3.5
0.437
<0.0029
<0.0029
Bottom1/9/14
Oil UST
Used
WeOst
1/9/14
7
Closure
66.4
<4.470
0.439
<0.0073
Oil UST
Used
WO East
1/9/14
7
Closure
10.1
<0.431
0.0662
<0.0031
Oil UST
Used
Oh
1/9/14
7
Closure
46.2
<3.800
0.077
0.0035
N
Oil UST
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
270
3.3
24
0.16
270
0.35
Residential MSCC (mg/kg)
469
626
14000
313
400
0.88
Industrial/Commercial MSCC (mg/kg)
12264
16350
360000
8176
400
8
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg. Yellow shading indicates exceedance of Soil to
mg/kg =milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
19 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
8015
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
1)
LSA,
x
x
etc.)H
H
Tank 5
12/16/13
DiesUST
8
Closure
1210
10.7
South
Tank 4
12/16/13
KeroUST
6
Closure
<5.6
<6.7
North
Tank 4
12/16/13
KeroUST
6
Closure
200
19.2
South
Tank 5
12/16/13
DiesDSTel
8
Closure
<5.9
<7.1
North
Minimum Reporting Limit (mg/kg)
10
10
Soil to groundwater MSCC (mg/kg)
10
10
Residential MSCC (mg/kg)
10
10
Industrial/Commercial MSCC (mg/kg)
10
10
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg. Groundwater MSCC. Red shading indicates exceedance of
mg/kg =milligrams per kilogram Residential MSCC.
20 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
p
Tank pit
, 20Day,
1)
LSA,
x
etc.)
p"
Displ
09/08/14
dispenser
1-2
LSA
1,510
Disp2
09/08/14
dispenser
1-2
LSA
759
Disp3
09/08/14
dispenser
1-2
LSA
6,110
Disp4
09/08/14
dispenser
1-2
LSA
909
Minimum Reporting Limit (mg/kg)
10
Soil to groundwater MSCC (mg/kg)
10
Residential MSCC (mg/kg)
10
Industrial/Commercial MSCC (mg/kg)
10
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
21 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
Contaminant of Concern 4
x
x
�
N
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
U
U
U
(m/dd/yy)
(eg.
(ft BGS)
(Closure
eke
Tank pit
, 20Day,
U
U
U
^
1)
LSA,
Z
etc.
a
a
a
Disp5
09/08/14
dispenser
1-2
LSA
172
NA
NA
NA
NA
NA
NA
NA
Diesel E
5'
09/08/14
Diesel
tank pit
3-5
Closure
NA
52.0
<23.8
50.1
458
614
Diesel E
09/08/14
Diesel
8-10
Closure
NA
25.5
<11.6
22.7
706.5
419.7
<384
<384
10,
tank pit
Diesel N
09/08/14
Diesel
tank
3-5
Closure
NA
<12.4
17.4
<12.4
<14.9
<14.9
<410
<410
5'
pit
Minimum Reporting Limit (mg/kg)
10
10
10
10
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
10
NR
lmmob
NR
540
31
4
3600
Residential MSCC (mg/kg)
1120000
10
NR
31000
NR
1500
469
63000
Industrial/Commercial MSCC (mg/kg)
320000
163500
10
NR
810000
NR
40000
12264
00
1 0
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg. Yellow shading indicates exceedance of Soil to
mg/kg =milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
22 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
N
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
U
en
e4
(m/dd/yy)
(eg.
(ft BGS)
(Closure
o,
d�
1-
eae
eae
Tank pit
, 20Day,
U
U
U
^
1)
LSA,
x
x
'W
etc.
a
W
a
W
a
W
+
e�
+
u
N
Diesel N
09/08/14
Diesel
8.10
Closure
<10.9
<10.9
<10.9
<13.4
<13.4
<361
<361
10,
tank pit
Diesel S
09/08/14
Diesel
3-5
Closure
<11.3
<11.3
<11.3
<144.3
<49.5
<372
<372
5'
tank pit
Diesel S
09/08/14
Diesel
8-10
Closure
<12.3
<12.3
<12.3
<145.3
<50.5
<405
<405
10,
tank pit
Kerosene
Diesel
indeter
indeter
W 5,
09/08/14
tank pit
3-5
Closure
<12.4
<12.4
<12.4
minate
minate
<409
<409
Minimum Reporting Limit (mg/kg)
10
10
10
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
NR
NR
540
31
4
3600
lmmob
Residential MSCC (mg/kg)
1120000
NR
31000
NR
1500
469
63000
Industrial/Commercial MSCC (mg/kg)
320000
163500
NR
810000
NR
40000
12264
00
1 0
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg. Yellow shading indicates exceedance of Soil to
mg/kg =milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
23 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
8015
Contaminant of Concern 4
N
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
U
U
U
(m/dd/yy)
(eg.
(ft BGS)
(Closure
o,
C,
,-
eae
eae
Tank pit
, 20Day,
U
U
U
^
1)
LSA,
x
d;
x
'W
etc.
a
W
a
W
a
W
+
e�
+
.�-
N
Kerosene
09/08/14
Diesel
g_10
Closure
<12.6
<12.6
<12.6
Indeter
Indeter
<414
<414
W 10,
tank pit
minate
minate
Center
09/08/14
Diesel
8_10
Closure
<11.0
<11.0
<11.0
<13.6
<13.2
<364
<363
10,
tank pit
Minimum Reporting Limit (mg/kg)
10
10
10
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
NR
NR
540
31
4
3600
lmmob
Residential MSCC (mg/kg)
1120000
NR
31000
NR
1500
469
63000
Industrial/Commercial MSCC (mg/kg)
320000
163500
NR
810000
NR
40000
12264
00
1 0
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
24 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
Ell
Sample
Date
Source
Sample
Incident
o
ID
Collected
Area
Depth
Phase
U
(m/dd/yy)
(eg.
(ft BGS)
(Closure
F-
Tank pit
, 20Day,
00
1=1
N
O
1)
LSA,
,U',
owl
off',
a
etc.)
I O
O
U
M
10/28/14
P as tank
24-26
LSA
<2.8
3.5
<2.8
6.8
<22.2
261
MW-2
Gas
18-20
10/28/14
dispenser
18-20
LSA
<3.1
3.3
<3.1
9.5
<22.7
lines
MW-3
10/28/14
Diesel
20-22
LSA
<11.5
<11.5
<11.5
<5.7
20-22
tank pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
91
0.02
Residential MSCC (mg/kg)
939
1500
12264
350000
85
Industrial/Commercial MSCC (mg/kg)
310000
24528
40000
469
763
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
25 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
c
N
Tank pit
, 20Day,
r l
rr``
o
rr``
u
1)
V
V
V
N
O
r
✓'
Y
Y
_
C�
etc.)
o
0
0
U
W
i
SB-2
10/7/15
8-10
CSA
<1.4
<1.4
<1.4
70.9
SB-7
10/7/15
8-10
CSA
<1.5
<1.5
<1.5
3.8
3.2
6.4
3.3
8.7
6.7
SB-7
10/7/15
13-15
CSA
8.1
3.3
6.2
SB-4
10/7/15
3-5
CSA
<1.3
<1.3
<1.3
<62
<3.1
<3.1
5.7
<3.1
7.4
<6.2
Minimum Reporting Limit (mg/kg) —WO—
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
24
0.0056
0.37
4.9
91
0.16
4.6
Residential MSCC (mg/kg)
939
1500
12264
14000
18
156
1560
350000
313
3129
Industrial/Commercial MSCC (mg/kg)
3310000
24528
40000
469
360000
164
4088
40000
8176
81760
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
26 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
4
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
o
(m/dd/yy)
(eg.
(ft BGS)
(Closure
N
a
a
Tank pit
, 20Day,
Oc
U
c
Z
c
1)
LSA,
N
p
etc.)
U
U
U
SB-6
10/7/15
3-5
CSA
392
1150
914
,a
5610
19,
_
SB-6
10/7/15
8-10
CSA
296
349
162ii
3430
<1620
SB-6
10/7/15
13-15
CSA
120
91.6
34.8
k,30
<709
r§
M
<709
M
E
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
0.0056
4.3
4.3
4.9
1.7
0.12
0.16
Residential MSCC (mg/kg)
939
1500
12264
18
626
626
1560
1564
100
313
Industrial/Commercial MSCC (mg/kg)
24528
40000
469
164
16350
16350
40000
40880
4000
8176
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
27 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
4
Contaminant of Concern 4
N
N
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N0
0
(m/dd/yy)
(eg.
(ft BGS)
(Closure
4
4
4
Tank pit
, 20Day,
X
a
1)
I SA,
�
E
`n
V
a
etc.)
SB-6
10/7/15
3-5
CSA
828
-
SB-6
10/7/15
8-10
CSA
<1620
_
SB-6
10/7/15
13-15
CSA
<709
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
1.7
1.5
4.3
8.5
8.3
4.6
4.6
4.6
0.37
Residential MSCC (mg/kg)
626
3128
1200
782
782
3129
3129
3129
156
Industrial/Commercial MSCC (mg/kg)
16350
81760
32000
20440
20440
81760
81760
81760
4088
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
28 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
4
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
44
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Nas
Tank pit
, 20Day,
r.
o
H
1)
LSA
N
>
;4
a�
Cd
N
N
°�
>
etc.
�,
o
SB-4
10/7/15
13-15
CSA
6.7
3.9
9.8
10.4
5.4
14.7
3.8
15.7
5.8
10
SB-5
10/7/15
13-15
CSA
13.4
9.0
12.1
<2.6
<2.6
16.9
14.0
63.6
41.2
22.4
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
0.0056
0.37
4.9
91
0.16
4.3
8.5
4.6
4.6
4.6
Residential MSCC (mg/kg)
18
156
1560
350000
313
1200
782
3129
3129
3129
Industrial/Commercial MSCC (mg/kg)
3310000
164
4088
40000
8176
32000
20440
81760
81760
81760
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
29 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
o
�,
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
;2
N
4
Tank pit
, 20Day,
o
1)
LSA,
etc.)O
CIO
w
4
ZF-
SB-7
10/7/15
8-10
CSA
6.7
14.2
5.9
37.5
14.4
12.1
52.4
47.2
7.8
350
SB-4
10/7/15
3-5
CSA
<3.1
<3.1
<3.1
5.7
<3.1
<3.1
7.4
<3.1
14.7
8.1
SB-5
10/7/15
13-15
CSA
22.4
<2.6
<2.6
12.1
<2.6
<2.6
<2.6
<2.6
16.9
14.0
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.3
4.3
4.9
1.7
0.12
0.16
1.7
4.3
8.5
Residential MSCC (mg/kg)
3129
626
626
1560
1564
100
313
626
1200
782
Industrial/Commercial MSCC (mg/kg)
81760
16350
16350
40000
40880
4000
8176
16350
32000
20440
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
30 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
4
Contaminant of Concern 4
N
N
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
r
r.
(m/dd/yy)
(eg.
(ft BGS)
(Closure
4
4
Tank pit
, 20Day,
S
X
o
1)
LSA,
etc.)
SB-7
10/7/15
8-10
CSA
67.8
135
80.1
55.1
SB-5
10/7/15
13-15
CSA
3.9
63.6
41.2
22.4
7.8
14.0
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
8.3
4.6
4.6
4.6
0.37
8.5
Residential MSCC (mg/kg)
782
3129
3129
3129
20
782
Industrial/Commercial MSCC (mg/kg)
20440
81760
81760
81760
180
20440
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
31 Change 2

TABLE B-4
SUMMARY OF GROUNDWATER ANALYSES
SIX-O-ONE STOP
5661 HIGHWAY 601
CONCORD, NORTH CAROLINA 28025
(All units are micrograms per Liter)
Sample
Location
Sample Date
Benzene
Dilso-
propylether
Ethylbenzene
Isopropyl-
benzene
Methyl-tert-
butyl -ether
Naphthalene
N-propyl-
benzene
Toluene
1,2,4-
Trimethyl-
benzene
1,3,5-
Trimethyl-
benzene
m&p Xylenes
o-xylene
MW-1
11/12/2014
326
86.9
79.7
7
201
82
16
46.1
127
40.9
353
143
MW-1
10/12/2015
735
275
294
26.7
413
308
54.5
83.6
428
95.7
583
58.6
MW-1
11/21/2016
290
105
78.5
11.8
98.2
96.4
14.6
18.7
130
22.4
112
29.8
MW-1
5/1/2017
172
26
115
12.9
26.4
73.4
18.3
17.5
80.8
<1.0
72.9
53.6
MW-1
1/21/2018
117
33.2
65.4
10.9
37.1
63.0
11.9
11.9
76.6
<1.0
60.8
5.7
MW-1
5/8/2020
11.2
2.6
39.0
4.9
2.2
22.9
7.9
1.1
<0.50
<0.50
3.5
0.69
MW-2
11/12/2014
3810
1430
1270
70.7
66
242
169
3600
1420
365
4230
2980
MW-2
10/12/2015
3190
1800
91.5
224
397
194
2210
1460
403
3880
2220
MW-2
10/14/2016
9680
3910
2940
90.7
182
492
226
584
1810
449
6170
2160
MW-2
12/13/2016
6830
4220
1760
101
238
302
276
269
1470
424
3010
791
MW-2
5/1/2017
2250
1160
556
21.7
64.7
92.3
<0.50
706
570
<0.50
1900
1750
MW-2
1/21/2018
8570
3240
2860
84.8
132
469
241
174
1760
432
5120
148
MW-2
5/8/2020
4350
449
3490
113
<20.0
817
313
315
2650
671
5530
142
MW-3
11/12/2014
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
2.2
1.1
MW-3
10/12/2015
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<1.0
<0.5
MW-3
11/21/2016
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<1.0
<0.5
MW-3
5/1/2017
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-3
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-4
10/12/2015
<0.50
22.1
<0.50
<0.50
21.1
<2.0
<0.50
<0.50
<0.50
<0.50
<1.0
<0.5
MW-4
11/21/2016
<0.50
14
<0.50
<0.50
30
<2.0
<0.50
<0.50
<0.50
<0.50
<1.0
<0.5
MW-4
5/1/2017
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-4
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-5
10/12/2015
<0.50
<0.50
<0.50
<0.50
1.5
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-5
11/21/2016
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-5
5/1/2017
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-5
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-5
5/8/2020
<0.50
<0.50
<0.50
<0.50
0.61
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-6
10/12/2015
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-6
11/21/2016
<0.50
<0.50
<0.50
<0.50
6.2
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-6
5/1/2017
<0.50
<0.50
<0.50
<0.50
4.4
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-6
1/21/2018
<0.50
<0.50
<0.50
<0.50
4.9
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-6
5/8/2020
<0.50
<0.50
<0.50
<0.50
0.63
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-7
10/12/2015
1.3
394
4.9
2.2
235
<2.0
2.5
<0.50
4.8
7.9
4.1
<1.2
MW-7
11/21/2016
10.7
144
23.3
19.4
57.2
3.3
14.4
2.1
22.8
13.3
9.3
<0.50
MW-7
5/1/2017
4
5.1
23
13.6
1.2
3.1
15
0.92
22.4
11.9
3.5
<0.50
MW-7
1/21/2018
8.1
22.6
55.0
25.2
6.9
6.9
37.8
1.7
79.7
37.4
29.0
<0.50
MW-7
5/8/2020
2.7
1.4
25.5
8.7
<0.5
2.9
3.8
<0.5
6.8
<0.5
<1.0
<0.50
MW-8
10/12/2015
5.4
87.4
0.52
<0.50
375
<2.0
<0.50
<0.50
1.2
<0.50
1.2
<0.5
MW-8
11/21/2016
<0.50
28.5
<0.50
<0.50
98
<2.0
<0.50
<0.50
<0.50
<0.50
1.2
<0.50
MW-8
5/1/2017
<0.50
26.6
<0.50
<0.50
100
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-8
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-8
5/8/2020
<0.50
19.3
<0.50
<0.50
99.6
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
WSW-1
6/30/2015
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
WSW-1
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
W5W-1
5/8/2020
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
WSW-12
5/8/2020
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
WSW-13
6/30/2015
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
W5W-13
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
W5W-28
5/8/2020
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
NCAC 21. Standard
1
600
70
20
6
70
600
400
400
500
500
GCL
5000
84500
25000
20000
6000
30000
260000
28500
25000
85500
85500
Notes: Yellow shading indicates exceedance of 2L
Red shading indicated exccedance of Gross Contaminant levells

TABLE B-5
Water Well Supply Information Survey
Six O One Stop
5661 Highway 601
Concord, North Carolina 28025
Incident Number 40338
Map
N+A2:A22
B43A2:A2
OA2:A26A
A2:A32
Sent
Certified
Mail
Proof of
Delivery
Received?
Survey
Returned?
Survey
Indicates
Well?
Well
Observed?
Parcel Number
Parcel Address
Owners
Mailing Address
City
State
Zip
2
Yes
Yes
Yes
No
No
5548626523.00
5550 US Highway 601 South
Glenn D. Holt, Jonathan I. Webster
5550 Cold Springs Road South
Concord
NC
28025
1
Yes
Yes
Yes
Yes
No
5548627061.00
5600 Cold Springs Road South
John B. Plyler, Jr.
5600 Cold Springs Road South
Concord
NC
28025
4
Yes
RTS
No
N/A
Ind.
5548724660.00
5501 Cold Springs Road South
Matthew Daniel Pethel, Ashley Faggart Pethel
5349 Cold Springs Road South
Concord
NC
28025
5
Yes
Yes
No
N/A
Ind.
5548723427.00
5521 Cold Spring Road South
Kenneth Vance Lambert, Alison Marie Lambert
683 Elizabeth Street Southwest
Concord
NC
28025
8
Yes
RTS
No
N/A
Ind.
5548722242.00
5527 Cold Springs Road South
Kenneth Ray Lambert, Tamara Lefle Lambert
5527 Cold Springs Road South
Concord
NC
28025
6
Yes
RTS
No
N/A
No
5548822476.00
5461 Cold Springs Road South
Robert D Faggart
5449 Cold Springs Road South
Concord
NC
28025
7
Yes
RTS
No
N/A
No
5548814655.00
5551 Cold Springs Road South
Kenneth Maurice Faggart
5551 Cold Springs Road South
Concord
NC
28025
9
Yes
RTS
No
N/A
Ind.
5548722112.00
5589 Cold Springs Road South
Maurica Faggart Gaylor, John David Plyler
5589 Cold Springs Road South
Concord
NC
28025
13
Yes
RTS
No
N/A
Yes
15548710746.00
5651 Cold Springs Road South
Lanney R. Griffin, Tammy A. Griffin
5651 Cold Springs Road South
Concord
NC
28025
10
Yes
RTS
No
N/A
Ind.
5548711908.00
5651 Cold Springs Road South
Lanney R. Griffin, Tammy A. Griffin
5651 Cold Springs Road South
Concord
NC
28025
11
Yes
Yes
Yes
Yes
No
5548714746.00
5665 Cold Springs Road South
Cynthia Faggart Isenhour
5665 Cold Springs Road South
Concord
NC
28025
12
Yes
Yes
Yes
Yes
No
5548713617.00
5677 Cold Springs Road South
Matthew Dwayne Isenhour, Corissa Ashley Isenhour
5677 Cold Springs Road South
Concord
NC
28025
14
Yes
Yes
Yes
Yes
No
5548712441.00
5695 Cold Springs Road South
Kelly L. Kivett, Tyler A. Kivett
10726 NC Highway 73 East
Mt. Pleasant
NC
28124
18
Yes
Yes
Yes
No
No
5548619381.00
5807 Highway 601 South
Robert L. Rice
5807 Highway 601 South
Concord
NC
28025
17
Yes
Yes
No
N/A
No
5548619434.00
5691 Cold Springs Road South
Robert L. Rice
5807 Highway 601 South
Concord
NC
28025
19
Yes
Yes
No
N/A
No
5548710232.00
5835 Highway 601 South
Christopher L. Reed
5835 Highway 601 South
Concord
NC
28025
20
Yes
Yes
Yes
Yes
No
5548711141.00
5849 Highway 601 South
Larry Wayne Saunders
2567 Biggers Road
Concord
NC
28025
15
Yes
Yes
Yes
Yes
No
5548714221.00
5845 Highway 601 South
Sandra Faggart Furr
5851 Highway 601 South
Concord
NC
28025
16
Yes
Yes
Yes
Yes
No
5548715295.00
5851 Highway 601 South
Sandra Faggart Furr, Ricky Lynn Furr
5851 Highway 601 South
Concord
NC
28025
21
Yes
Yes
Yes
Yes
No
5548609867.00
5830 Highway 601 South
Sabre A. Foster
229 Suburban Avenue Northeast
Concord
NC
28025
22
Yes
Yes
Yes
Yes
No
5548609914.00
5824 Highway 601 South
Aubrey Haigler
10329 Flowes Store Road
Midland
NC
28107
23
Yes
Yes
Yes
Yes
No
5548618071.00
5818 Highway 601 South
Theresa Dost
5818 Highway 601 South
Concord
NC
28025
24
Yes
Yes
Yes
No
No
5548618019.00
5812 Highway 601 South
Wade Ramsey, Betty C. Ramsey
5812 Highway 601 South
Concord
NC
28025
25
Yes
Yes
Yes
No
No
5548617156.00
5806 Highway 601 South
Clyde L. Helms
5806 Highway 601 South
Concord
NC
28025
27
Yes
Yes
No
N/A
Ind.
5548603955.00
5800 Highway 601 South
Keith William Lambert, LeAnn H. Lambert
5800 Highway 601 South
Concord
NC
28025
26
Yes
Yes
No
N/A
No
5548616219.00
5770 Old Monroe Circle
Margie Church
114 Piedmont Drive
Kannapolis
NC
28081
28
Yes
Yes
Yes
Yes
No
5548612342.00
5726 Old Monroe Circle
Todd A. Feasel
5726 Old Monroe Circle
Concord
NC
28025
39
Yes
Yes
Yes
No
No
5548616509.00
5680 Highway 601 South
Annie's Cane Shop, Inc.
4906 Fenwick Place
Concord
NC
28025
36
Yes
Yes
Yes
No
No
5548614727.00
5727 Old Monroe Circle
Carlos Colon, Sr., Miriam E. Colon
5727 Old Monroe Circle
Concord
NC
28025
35
Yes
Yes
Yes
Yes
No
5548612817.00
5675 Old Monroe Circle
Frank Edward Long, Dorethea Ann Young
4906 Fenwick Place
Concord
NC
28025
30
Yes
Yes
No
N/A
Ind.
5548519598.00
5670 Old Monroe Circle
Scott F. Barbee
5670 Old Monroe Circle
Concord
NC
28025
31
Yes
Yes
Yes
Yes
No
5548518711.00
5650 Old Monroe Circle
Mitzi Troutman White
11100 Kluttz Road
Gold Hill
NC
28071
34
Yes
Yes
Yes
No
No
5548620114.00
5601 Old Monroe Circle
Howard Lane Barbee, Lorrene R. Barbee
21317 Rogers Road
Richfield
NC
28137
32
Yes
Yes
Yes
Yes
No
5548517813.00
5626 Old Monroe Circle
Randolph William Dozier, II, Jennifer Dozier
5626 Old Monroe Circle
Concord
NC
28025
33
Yes
Yes
Yes
Yes
No
5548516926.00
5600 Old Monroe Circle
Jerry Grady Love
5600 Old Monroe Circle
Concord
NC
28025
40
Yes
Yes
No
N/A
No
5548526858.00
5500 Highway 601 South
Ziff Investments, LLC
Post Office Box 6587
Concord
NC
28027
3
Yes
RTS
No
N/A
No
5548624947.00
5490 Cold Springs Road South
Thomas D. Lynch, III, Donna Griffith Lynch
5490 Cold Springs Road South
Concord
NC
28025
38
Yes
Yes
No
N/A
No
15548623341.00
5611 Highway 601 South
Carolina Oil Co of Concord, Inc
Post Office Box 5010
Concord
NC
28027
37
Yes
Yes
No
N/A
No
5548624193.00
5625 Highway 601 South
Sidney Dell Misinheimer
5661 Highway 601 South
Concord
NC
28025
Notes: Ind. = Indeterminate, N/A= Not applicable
Yellow Shading indicates known water supply well.

Appendix B
Reporting Tables
Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Date
Date
Well
Well
Screened
Depth
Top of
Depth to
Free
Groundwater
Latitude/
Well
Installed
Water
Casing
Casing
Interval
of Well
Casing
Water
Product
Elevation*
Longitude
ID
(m/dd/yy)
Level
Diameter
Depth
(x to X
(ft.
Elevation*
from Top
Thickness
(ft.)
(decimal
Measured
(in.)
(ft.
ft. BGS)
BGS)
(ft.)
of Casing
** (ft.)
degrees)***
AL
m/dd/
BGS
ft.
MW-1
10/28/2014
11/12/2014
2
20
20 to 30
30
98.92
22.87
0
76.05
35.339266/-
80.520191
MW-2
10/28/2014
11/12/2014
2
20
20 to 30
30
99.76
23.77
0
75.99
35.339206/-
80.520266
MW-3
10/28/2014
11/12/2014
2
20
20 to 30
30
100.00
24.52
0
75.48
35.339108/-
80.520021
MW-4
10/10/2015
10/12/2015
2
25
25 to 35
35
0
35.339150/-
80.520081
MW-5
10/10/2015
10/12/2015
2
25
25 to 35
35
0
35.339150/-
80.520081
MW-6
10/10/2015
10/12/2015
2
25
25 to 35
35
0
35.339150/-
80.520081
MW-7
10/10/2015
10/12/2015
2
25
25 to 35
35
0
35.339150/-
80.520081
MW-8
10/10/2015
10/12/2015
2
40
45 to 50
50
0
35.339150/-
80.520081
ft BGS = feet below ground
* Reference Point for Elevation Measurements North side casing MW-3 , Assumed Elevation: 100.00 ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
*** The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.
44 Change 2

Appendix G
Contaminant Sources Other than USTs
Table B-9: Current and Historical Groundwater Elevations and Free Product Thickness
Revision Date: 4/28/2015 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Well ID
#
Date
Screened Interval
(top of screen,
bottom of screen)
Depth to Water*
Uncorrected
(feet)
Free
Product
Thickness
feet
Depth to Water*
Corrected
for Free Product
Thickness feet)
Top of
Casing
Elevation
(MSL)
Groundwater
Surface
Elevation
(MSL
MW-1
11/12/2014
20-30
22.87
NA
22.87
98.92
76.05
MW-1
10/12/2015
20 - 30
23.04
NA
23.04
98.92
75.88
MW-1
11/21/2016
20 - 30
23.31
NA
23.31
98.92
75.88
MW-1
01/21/2018
20 - 30
21.51
NA
21.51
98.92
77.41
MW-1
5/8/2020
20 - 30
21.51
NA
18.30
98.92
80.62
MW-2
11/12/2014
20 - 30
23.77
NA
23.77
99.76
75.99
MW-2
10/12/2015
20 - 30
23.95
NA
23.95
99.76
75.81
MW-2
11/21/2016
20 - 30
24.16
NA
24.16
99.76
75.81
MW-2
1/21/2018
20 - 30
22.96
NA
22.96
99.76
76.80
MW-2
5/8/2020
20 - 30
22.96
NA
17.85
99.76
81.91
MW-3
11/12/2014
20 - 30
24.52
NA
24.52
100.00
75.48
MW-3
10/12/2015
20 - 30
25.10
NA
25.10
100.00
74.9
MW-3
11/21/2016
20 - 30
25.13
NA
25.13
100.00
74.9
46 Change 2

Appendix G
Contaminant Sources Other than USTs
MW-3
1/21/2018
20 - 30
23.58
NA
23.58
100.00
76.42
MW-4
10/12/2015
25 - 35
22.62
NA
22.62
98.75
76.13
MW-4
11/21/2016
25 - 35
22.74
NA
22.74
98.75
76.13
MW-4
1/21/2018
25 - 35
21.30
NA
21.30
98.75
77.45
MW-5
10/12/2015
25 - 35
24.53
NA
24.53
100.08
75.55
MW-5
11/21/2016
25 - 35
24.36
NA
24.36
100.08
75.55
MW-5
1/21/2018
25 - 35
23.02
NA
23.02
100.08
77.06
MW-5
5/8/2020
25 - 35
23.02
NA
15.07
100.08
85.01
MW-6
10/12/2015
25 - 35
25.81
NA
25.81
99.43
73.62
MW-6
11/21/2016
25 - 35
26.03
NA
26.03
99.43
73.62
MW-6
1/21/2018
25 - 35
24.72
NA
24.72
99.43
74.71
MW-6
5/8/2020
25 - 35
24.72
NA
18.05
99.43
81.38
MW-7
10/12/2015
25 - 35
24.40
NA
24.40
98.65
73.85
MW-7
11/21/2016
25 - 35
24.57
NA
24.57
98.65
73.85
MW-7
1/21/2018
25 - 35
22.60
NA
22.60
98.65
76.05
MW-7
5/8/2020
25 - 35
20.60
NA
20.60
98.65
78.05
MW-8
10/12/2015
45 - 50
26.38
NA
26.38
99.85
73.47
47 Change 2

Appendix G
Contaminant Sources Other than USTs
MW-8
11/21/2016
45 - 50
25.58
NA
25.58
99.85
73.47
MW-8
1/21/2018
45 - 50
24.81
NA
24.81
99.85
75.04
MW-8
5/8/2020
45 - 50
19.21
NA
19.21
99.85
80.64
*Depth to Water is measured from Top of Casing
48 Change 2

Appendix G
Contaminant Sources Other than USTs
Table B-10: Land Use
Revision Date: 4/28/2015 Incident Number and Name: 40338 Six O One Stop
Facility ID#: 4753
Map ID #
Date
Determined
Land Use Feature
(include zoning)
Location
(complete street address if applicable)
Distance and
Direction from
Source Area
1
4/27/2015
Limited
Subject Property
Subject Property
Commercial (LC)
zoning district
2
4/27/2015
Agricultural Open
All adjoining and surrounding properties within 2,000 feet
All adjoining and
(AO) Space zoning
surrounding
district
properties within
2,000 feet
49 Change 2

APPENDICES

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
SixOOneStop, Inc.
Attn: Marc Glover, Registered Agent
5661 Highway 601 S.
Concord, NC 28025
(via email)
Dear Mr. Glover:
NORTH CAROLINA
Environmental Quality
February 14, 2020
Re: Notice of Regulatory Requirements
15A NCAC 2L .0407(b)
Risk -based Assessment and Corrective Action
for Petroleum Underground Storage Tanks
Six-O-One Stop
5661 South Highway 601, Concord
Cabarrus County
Incident Number: 40338
Risk Classification: High
The UST Section, Division of Waste Management (DWM), Mooresville Regional Office
(MRO) received the March 16, 2018 Monitoring Reports on February 12, 2020. The report
recommending preparation of a full scale CAP designed to reduce dissolved groundwater
concentrations to below the 2L standard was reviewed and approved on February 12, 2020. The
paper report copies will be maintained in the MRO. The electronic copies have been loaded to the
DWM's electronic document storage system (Laserfiche).
The report states:
• On January 21, 2018, CESI collected groundwater samples from eight monitoring wells
(MW-1, MW-2, MW-3, MW-4, MW-5, MW-6, MW-7, and MW-8). Analysis of
groundwater samples from the monitoring wells revealed gasoline parameters greater than
the North Carolina Administrative Code (NCAC) 15A 2L standard in wells MW-1, MW-2,
MW-7, and MW-8. The benzene concentration in well MW-2 was reported at a
concentration greater than the GCL for benzene. None of the other tested parameters
exceeded GCL's.
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1699

• CESI also collected a groundwater sample from water supply well 2. No parameters were
reported above the sample detection limit. CESI attempted to retrieve a water sample from
the onsite water supply well (well 1) but was unable to lower a bailer because of interference
from the downhole pump cable and discharge line. This well is disconnected from the
electrical supply and has reportedly not been used for many years. The owner of water well
number 3 refused CESI access to the water well. The owner of water well number 4 stated
that the well is not used and is not accessible. Interviews with the owners of water supply
wells 2 and 3 on January 21, 2018, stated that they did not want to connect to municipal
water.
• Depth to groundwater measurements at the site revealed depth to water approximately 23 feet
below grade. Groundwater flow direction is toward the east.
• Free product has not been observed onsite. Based on the groundwater analytical results of
samples collected January 21, 2018, the areal extent of dissolved hydrocarbons appears to be
defined except to the south for benzene and MTBE and to the west for MTBE. However,
based on the low concentrations on the perimeter wells, it appears that the dissolved
hydrocarbon plume has not migrated offsite. The vertical extent of impact has been defined
in the deep screen well MW-8.
• No remediation has been implemented at this site.
Per this Notice of Regulatory Requirements:
• Continue semi-annual groundwater sampling/monitoring. Sample monitoring wells and all
water supply wells within 1,000 feet of the release.
• The next sampling event for the Monitoring Report shall be conducted in March 2020. The
next Monitoring Report is due no later than April 30, 2020.
• Please update the plume stability analysis in the next monitoring report. Include the March
2020 groundwater data in the stability analysis.
• Information was received reporting that a water line does not exist along Cold Springs Road.
The water supply source for these properties remains unclear. Please update the receptor
information to identify all water supply wells within 1,000 feet of the release and provide
clarification for water usage at each property. Include this information in the April 30, 2020
Monitoring Report.
• Connections to public water must be evaluated as a potential cost effective alternative
moving forward to help determine whether corrective action through active remediation is
necessary. The goal of public water connections is to minimize the risk to potentially
threatened water supply wells on nearby properties. You must reasonably attempt to obtain
agreements for connections to public water supply wells used for potable purposes located
within 1,000 feet downgradient of the source area. Additionally, an attempt must be made to
obtain agreements with owners to abandon all water supply wells within 250 feet of the
release.
• Obtaining public water connection agreements is the first step towards determining the
feasibility of a water line extension. Further evaluation will be requested at a later time if
water connections and/or abandonments cannot be completed and alternative active
remediation options would likely be necessary.
Please note that sampling and correction action must be conducted in accordance with the
Guidelines for Assessment and Corrective Action for UST Releases. Failure to comply in the
manner and time specified may result in the assessment of civil penalties and/or the use of the other
enforcement mechanisms.
D 1E
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1699

If you have any questions regarding trust fund eligibility or reimbursement from the
Commercial or Noncommercial Leaking Petroleum Underground Storage Tank Cleanup Funds,
please contact the UST Section Trust Fund Branch at [phone]. If you have any questions
regarding the actions that must be taken or the rules mentioned in this letter, please contact me by
email at Trudy.Beverly(?ncdenr. _gov or telephone at [phone].
Sincerely, Q,
�� Y" '6w U
Trudy Beverly, L.G.
Hydrogeologist
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ
cc: Steven Irminger, CESI Civil-Geotechnical-Surveying (via email)
Crystal Swinger, Cabarrus County Environmental Health (via email)
Mike Downs, Cabarrus County Manager (via email)
D F.
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1699

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCM
Director
SixOOneStop, Inc.
Attn: Marc Glover, Registered Agent
5661 Highway 601 S.
Concord, NC 28025
(via email)
Dear Mr. Glover:
NORTH CAROLINA
Environmental Quality
May 1, 2020
Re: Notice of Regulatory Requirements
15A NCAC 2L .0407(b) [High Risk]
Risk -based Assessment and Corrective Action
For Petroleum Underground Storage Tanks
Six-O-One Stop
5661 South Highway 601, Concord
Cabarrus County
Incident Number: 40338
Risk Classification: High
On April 30, 2020, the Mooresville Regional Office (MRO) of the Underground Storage
Tank (UST) Section of the Division of Waste Management received a request to extend the
submittal deadline for the Monitoring Report for this site from your consultant CESI Civil-
Geotechnical-Surveying. Specifically, CESI Civil-Geotechnical-Surveying requested that the
submittal deadline be extended until June 8, 2020. This request is considered reasonable and is
hereby granted.
Should you fail to submit the report by the extended deadline, the original deadline may
be used in any enforcement action. If you have any questions regarding the actions that must be
taken or the rules mentioned in this letter, please contact me by email at
Trudy.Beverlykncdenr. _ og_v or by phone at [phone].
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1699

Sincerely,
�-� I'll ;IIW -
Trudy Beverly, L.G.
Hydrogeologist
Mooresville Regional Office
UST Section, Division of Waste Management,
NCDEQ
cc: Steven Irminger, CESI Civil-Geotechnical-Surveying (via email)
Crystal Swinger, Cabarrus County Environmental Health (via email)
Mike Downs, Cabarrus County Manager (via email)
pannwY*�` n�ia.nama aal�
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115
704.663.1644

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
May 22, 2020
Mr. Steve Irminger
Irminger Consulting
7015 Erinbrook Road
Concord, NC 28025
RE: Project: 601 Stop
Pace Project No.: 92477071
Dear Mr. Irminger:
Enclosed are the analytical results for sample(s) received by the laboratory on May 08, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
CERTIFICATIONS
Project: 601 Stop
Pace Project No.: 92477071
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
601 Stop
92477071
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92477071001
5677 CSR
SM 6200B
SAS
63
PASI-C
92477071002
5600 CSR
SM 6200B
SAS
63
PASI-C
92477071003
MW-6
SM 6200B
SAS
63
PASI-C
92477071004
MW-7
SM 6200B
SAS
63
PASI-C
92477071005
MW-5
SM 6200B
SAS
63
PASI-C
92477071006
MW-1
SM 6200B
SAS
63
PASI-C
92477071007
MW-2
SM 6200B
SAS
63
PASI-C
92477071008
MW-8
SM 6200B
SAS
63
PASI-C
92477071009
5726 OMC
SM 6200B
SAS
63
PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: 5677 CSR Lab ID: 92477071001 Collected: 05/08/20 10:30 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
05/21/20 17:09
71-43-2
Bromobenzene
ND
ug/L
0.50
1
05/21/20 17:09
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
05/21/20 17:09
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
05/21/20 17:09
75-27-4
Bromoform
ND
ug/L
0.50
1
05/21/20 17:09
75-25-2
Bromomethane
ND
ug/L
5.0
1
05/21/20 17:09
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
05/21/20 17:09
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
05/21/20 17:09
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
05/21/20 17:09
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
05/21/20 17:09
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
05/21/20 17:09
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/21/20 17:09
75-00-3
Chloroform
ND
ug/L
0.50
1
05/21/20 17:09
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/21/20 17:09
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
05/21/20 17:09
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
05/21/20 17:09
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
05/21/20 17:09
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
05/21/20 17:09
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
05/21/20 17:09
106-93-4
Dibromomethane
ND
ug/L
0.50
1
05/21/20 17:09
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 17:09
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 17:09
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 17:09
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
05/21/20 17:09
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
05/21/20 17:09
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
05/21/20 17:09
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
05/21/20 17:09
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
05/21/20 17:09
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
05/21/20 17:09
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
05/21/20 17:09
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
05/21/20 17:09
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
05/21/20 17:09
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
05/21/20 17:09
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
05/21/20 17:09
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
05/21/20 17:09
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
05/21/20 17:09
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
05/21/20 17:09
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
05/21/20 17:09
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
05/21/20 17:09
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
05/21/20 17:09
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
05/21/20 17:09
1634-04-4
Naphthalene
ND
ug/L
2.0
1
05/21/20 17:09
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
05/21/20 17:09
103-65-1
Styrene
ND
ug/L
0.50
1
05/21/20 17:09
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
05/21/20 17:09
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
05/21/20 17:09
79-34-5
REPORT OF LABORATORY ANALYSIS
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Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 51

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: 5677 CSR Lab ID: 92477071001 Collected: 05/08/20 10:30 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
05/21/20 17:09
127-18-4
Toluene
ND
ug/L
0.50
1
05/21/20 17:09
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
05/21/20 17:09
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
05/21/20 17:09
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
05/21/20 17:09
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
05/21/20 17:09
79-00-5
Trichloroethene
ND
ug/L
0.50
1
05/21/20 17:09
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
05/21/20 17:09
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
05/21/20 17:09
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
05/21/20 17:09
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
05/21/20 17:09
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
05/21/20 17:09
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
05/21/20 17:09
179601-23-1
o-Xylene
ND
ug/L
0.50
1
05/21/20 17:09
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
05/21/20 17:09
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
1
05/21/20 17:09
460-00-4
Toluene-d8 (S)
100
%
70-130
1
05/21/20 17:09
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 5 of 51

leAnalyiical
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ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: 5600 CSR Lab ID: 92477071002 Collected: 05/08/20 10:40 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
05/20/20 18:41
71-43-2
Bromobenzene
ND
ug/L
0.50
1
05/20/20 18:41
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
05/20/20 18:41
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
05/20/20 18:41
75-27-4
Bromoform
ND
ug/L
0.50
1
05/20/20 18:41
75-25-2
Bromomethane
ND
ug/L
5.0
1
05/20/20 18:41
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
05/20/20 18:41
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
05/20/20 18:41
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
05/20/20 18:41
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
05/20/20 18:41
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
05/20/20 18:41
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/20/20 18:41
75-00-3
Chloroform
ND
ug/L
0.50
1
05/20/20 18:41
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/20/20 18:41
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
05/20/20 18:41
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
05/20/20 18:41
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
05/20/20 18:41
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
05/20/20 18:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
05/20/20 18:41
106-93-4
Dibromomethane
ND
ug/L
0.50
1
05/20/20 18:41
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 18:41
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 18:41
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 18:41
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
05/20/20 18:41
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
05/20/20 18:41
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
05/20/20 18:41
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
05/20/20 18:41
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
05/20/20 18:41
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
05/20/20 18:41
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
05/20/20 18:41
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
05/20/20 18:41
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
05/20/20 18:41
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
05/20/20 18:41
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
05/20/20 18:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
05/20/20 18:41
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
05/20/20 18:41
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
05/20/20 18:41
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
05/20/20 18:41
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
05/20/20 18:41
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
05/20/20 18:41
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
05/20/20 18:41
1634-04-4
Naphthalene
ND
ug/L
2.0
1
05/20/20 18:41
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
05/20/20 18:41
103-65-1
Styrene
ND
ug/L
0.50
1
05/20/20 18:41
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
05/20/20 18:41
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
05/20/20 18:41
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: 5600 CSR Lab ID: 92477071002 Collected: 05/08/20 10:40 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
05/20/20 18:41
127-18-4
Toluene
ND
ug/L
0.50
1
05/20/20 18:41
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
05/20/20 18:41
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
05/20/20 18:41
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
05/20/20 18:41
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
05/20/20 18:41
79-00-5
Trichloroethene
ND
ug/L
0.50
1
05/20/20 18:41
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
05/20/20 18:41
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
05/20/20 18:41
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
05/20/20 18:41
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
05/20/20 18:41
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
05/20/20 18:41
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
05/20/20 18:41
179601-23-1
o-Xylene
ND
ug/L
0.50
1
05/20/20 18:41
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
05/20/20 18:41
17060-07-0
4-Bromofluorobenzene (S)
97
%
70-130
1
05/20/20 18:41
460-00-4
Toluene-d8 (S)
101
%
70-130
1
05/20/20 18:41
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-6 Lab ID: 92477071003 Collected: 05/08/20 11:15 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
05/20/20 18:59
71-43-2
Bromobenzene
ND
ug/L
0.50
1
05/20/20 18:59
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
05/20/20 18:59
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
05/20/20 18:59
75-27-4
Bromoform
ND
ug/L
0.50
1
05/20/20 18:59
75-25-2
Bromomethane
ND
ug/L
5.0
1
05/20/20 18:59
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
05/20/20 18:59
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
05/20/20 18:59
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
05/20/20 18:59
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
05/20/20 18:59
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
05/20/20 18:59
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/20/20 18:59
75-00-3
Chloroform
ND
ug/L
0.50
1
05/20/20 18:59
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/20/20 18:59
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
05/20/20 18:59
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
05/20/20 18:59
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
05/20/20 18:59
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
05/20/20 18:59
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
05/20/20 18:59
106-93-4
Dibromomethane
ND
ug/L
0.50
1
05/20/20 18:59
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 18:59
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 18:59
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 18:59
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
05/20/20 18:59
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
05/20/20 18:59
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
05/20/20 18:59
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
05/20/20 18:59
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
05/20/20 18:59
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
05/20/20 18:59
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
05/20/20 18:59
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
05/20/20 18:59
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
05/20/20 18:59
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
05/20/20 18:59
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
05/20/20 18:59
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
05/20/20 18:59
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
05/20/20 18:59
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
05/20/20 18:59
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
05/20/20 18:59
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
05/20/20 18:59
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
05/20/20 18:59
75-09-2
Methyl-tert-butyl ether
0.63
ug/L
0.50
1
05/20/20 18:59
1634-04-4
Naphthalene
ND
ug/L
2.0
1
05/20/20 18:59
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
05/20/20 18:59
103-65-1
Styrene
ND
ug/L
0.50
1
05/20/20 18:59
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
05/20/20 18:59
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
05/20/20 18:59
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-6 Lab ID: 92477071003 Collected: 05/08/20 11:15 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
05/20/20 18:59
127-18-4
Toluene
ND
ug/L
0.50
1
05/20/20 18:59
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
05/20/20 18:59
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
05/20/20 18:59
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
05/20/20 18:59
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
05/20/20 18:59
79-00-5
Trichloroethene
ND
ug/L
0.50
1
05/20/20 18:59
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
05/20/20 18:59
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
05/20/20 18:59
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
05/20/20 18:59
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
05/20/20 18:59
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
05/20/20 18:59
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
05/20/20 18:59
179601-23-1
o-Xylene
ND
ug/L
0.50
1
05/20/20 18:59
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
106
%
70-130
1
05/20/20 18:59
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
1
05/20/20 18:59
460-00-4
Toluene-d8(S)
103
%
70-130
1
05/20/20 18:59
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-7 Lab ID: 92477071004 Collected: 05/08/20 11:45 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
2.7
ug/L
0.50
1
05/22/20 14:18
71-43-2
Bromobenzene
ND
ug/L
0.50
1
05/22/20 14:18
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
05/22/20 14:18
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
05/22/20 14:18
75-27-4
Bromoform
ND
ug/L
0.50
1
05/22/20 14:18
75-25-2
Bromomethane
ND
ug/L
5.0
1
05/22/20 14:18
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
05/22/20 14:18
104-51-8
sec-Butylbenzene
5.9
ug/L
0.50
1
05/22/20 14:18
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
05/22/20 14:18
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
05/22/20 14:18
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
05/22/20 14:18
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/22/20 14:18
75-00-3
Chloroform
ND
ug/L
0.50
1
05/22/20 14:18
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/22/20 14:18
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
05/22/20 14:18
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
05/22/20 14:18
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
05/22/20 14:18
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
05/22/20 14:18
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
05/22/20 14:18
106-93-4
Dibromomethane
ND
ug/L
0.50
1
05/22/20 14:18
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
05/22/20 14:18
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
05/22/20 14:18
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
05/22/20 14:18
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
05/22/20 14:18
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
05/22/20 14:18
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
05/22/20 14:18
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
05/22/20 14:18
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
05/22/20 14:18
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
05/22/20 14:18
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
05/22/20 14:18
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
05/22/20 14:18
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
05/22/20 14:18
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
05/22/20 14:18
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
05/22/20 14:18
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
05/22/20 14:18
10061-02-6
Diisopropyl ether
1.4
ug/L
0.50
1
05/22/20 14:18
108-20-3
Ethylbenzene
25.5
ug/L
0.50
1
05/22/20 14:18
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
05/22/20 14:18
87-68-3
Isopropylbenzene (Cumene)
8.7
ug/L
0.50
1
05/22/20 14:18
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
05/22/20 14:18
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
05/22/20 14:18
1634-04-4
Naphthalene
2.9
ug/L
2.0
1
05/22/20 14:18
91-20-3
n-Propylbenzene
3.8
ug/L
0.50
1
05/22/20 14:18
103-65-1
Styrene
ND
ug/L
0.50
1
05/22/20 14:18
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
05/22/20 14:18
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
05/22/20 14:18
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-7 Lab ID: 92477071004 Collected: 05/08/20 11:45 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
05/22/20 14:18
127-18-4
Toluene
ND
ug/L
0.50
1
05/22/20 14:18
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
05/22/20 14:18
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
05/22/20 14:18
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
05/22/20 14:18
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
05/22/20 14:18
79-00-5
Trichloroethene
ND
ug/L
0.50
1
05/22/20 14:18
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
05/22/20 14:18
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
05/22/20 14:18
96-18-4
1,2,4-Trimethylbenzene
6.8
ug/L
0.50
1
05/22/20 14:18
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
05/22/20 14:18
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
05/22/20 14:18
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
05/22/20 14:18
179601-23-1
o-Xylene
ND
ug/L
0.50
1
05/22/20 14:18
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
05/22/20 14:18
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
1
05/22/20 14:18
460-00-4
Toluene-d8 (S)
99
%
70-130
1
05/22/20 14:18
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-5 Lab ID: 92477071005 Collected: 05/08/20 12:15 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
05/20/20 19:17
71-43-2
Bromobenzene
ND
ug/L
0.50
1
05/20/20 19:17
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
05/20/20 19:17
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
05/20/20 19:17
75-27-4
Bromoform
ND
ug/L
0.50
1
05/20/20 19:17
75-25-2
Bromomethane
ND
ug/L
5.0
1
05/20/20 19:17
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
05/20/20 19:17
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
05/20/20 19:17
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
05/20/20 19:17
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
05/20/20 19:17
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
05/20/20 19:17
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/20/20 19:17
75-00-3
Chloroform
ND
ug/L
0.50
1
05/20/20 19:17
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/20/20 19:17
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
05/20/20 19:17
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
05/20/20 19:17
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
05/20/20 19:17
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
05/20/20 19:17
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
05/20/20 19:17
106-93-4
Dibromomethane
ND
ug/L
0.50
1
05/20/20 19:17
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 19:17
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 19:17
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
05/20/20 19:17
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
05/20/20 19:17
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
05/20/20 19:17
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
05/20/20 19:17
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
05/20/20 19:17
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
05/20/20 19:17
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
05/20/20 19:17
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
05/20/20 19:17
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
05/20/20 19:17
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
05/20/20 19:17
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
05/20/20 19:17
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
05/20/20 19:17
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
05/20/20 19:17
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
05/20/20 19:17
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
05/20/20 19:17
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
05/20/20 19:17
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
05/20/20 19:17
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
05/20/20 19:17
75-09-2
Methyl-tert-butyl ether
0.61
ug/L
0.50
1
05/20/20 19:17
1634-04-4
Naphthalene
ND
ug/L
2.0
1
05/20/20 19:17
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
05/20/20 19:17
103-65-1
Styrene
ND
ug/L
0.50
1
05/20/20 19:17
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
05/20/20 19:17
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
05/20/20 19:17
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-5 Lab ID: 92477071005 Collected: 05/08/20 12:15 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
05/20/20 19:17
127-18-4
Toluene
ND
ug/L
0.50
1
05/20/20 19:17
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
05/20/20 19:17
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
05/20/20 19:17
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
05/20/20 19:17
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
05/20/20 19:17
79-00-5
Trichloroethene
ND
ug/L
0.50
1
05/20/20 19:17
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
05/20/20 19:17
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
05/20/20 19:17
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
05/20/20 19:17
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
05/20/20 19:17
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
05/20/20 19:17
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
05/20/20 19:17
179601-23-1
o-Xylene
ND
ug/L
0.50
1
05/20/20 19:17
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
05/20/20 19:17
17060-07-0
4-Bromofluorobenzene (S)
96
%
70-130
1
05/20/20 19:17
460-00-4
Toluene-d8 (S)
101
%
70-130
1
05/20/20 19:17
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-1 Lab ID: 92477071006 Collected: 05/08/20 12:45 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
11.2
ug/L
0.50
1
05/22/20 00:01
71-43-2
Bromobenzene
ND
ug/L
0.50
1
05/22/20 00:01
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
05/22/20 00:01
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
05/22/20 00:01
75-27-4
Bromoform
ND
ug/L
0.50
1
05/22/20 00:01
75-25-2
Bromomethane
ND
ug/L
5.0
1
05/22/20 00:01
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
05/22/20 00:01
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
05/22/20 00:01
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
05/22/20 00:01
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
05/22/20 00:01
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
05/22/20 00:01
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/22/20 00:01
75-00-3
Chloroform
ND
ug/L
0.50
1
05/22/20 00:01
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/22/20 00:01
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
05/22/20 00:01
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
05/22/20 00:01
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
05/22/20 00:01
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
05/22/20 00:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
05/22/20 00:01
106-93-4
Dibromomethane
ND
ug/L
0.50
1
05/22/20 00:01
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
05/22/20 00:01
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
05/22/20 00:01
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
05/22/20 00:01
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
05/22/20 00:01
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
05/22/20 00:01
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
05/22/20 00:01
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
05/22/20 00:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
05/22/20 00:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
05/22/20 00:01
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
05/22/20 00:01
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
05/22/20 00:01
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
05/22/20 00:01
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
05/22/20 00:01
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
05/22/20 00:01
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
05/22/20 00:01
10061-02-6
Diisopropyl ether
2.6
ug/L
0.50
1
05/22/20 00:01
108-20-3
Ethylbenzene
39.0
ug/L
0.50
1
05/22/20 00:01
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
05/22/20 00:01
87-68-3
Isopropylbenzene (Cumene)
4.9
ug/L
0.50
1
05/22/20 00:01
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
05/22/20 00:01
75-09-2
Methyl-tert-butyl ether
2.2
ug/L
0.50
1
05/22/20 00:01
1634-04-4
Naphthalene
22.9
ug/L
2.0
1
05/22/20 00:01
91-20-3
n-Propylbenzene
7.9
ug/L
0.50
1
05/22/20 00:01
103-65-1
Styrene
ND
ug/L
0.50
1
05/22/20 00:01
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
05/22/20 00:01
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
05/22/20 00:01
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-1 Lab ID: 92477071006 Collected: 05/08/20 12:45 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
05/22/20 00:01
127-18-4
Toluene
1.1
ug/L
0.50
1
05/22/20 00:01
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
05/22/20 00:01
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
05/22/20 00:01
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
05/22/20 00:01
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
05/22/20 00:01
79-00-5
Trichloroethene
ND
ug/L
0.50
1
05/22/20 00:01
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
05/22/20 00:01
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
05/22/20 00:01
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
05/22/20 00:01
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
05/22/20 00:01
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
05/22/20 00:01
75-01-4
m&p-Xylene
3.5
ug/L
1.0
1
05/22/20 00:01
179601-23-1
o-Xylene
0.69
ug/L
0.50
1
05/22/20 00:01
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
05/22/20 00:01
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
1
05/22/20 00:01
460-00-4
Toluene-d8 (S)
100
%
70-130
1
05/22/20 00:01
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-2 Lab ID: 92477071007 Collected: 05/08/20 13:15 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
4350
ug/L
20.0
40
05/22/20 01:13
71-43-2
Bromobenzene
ND
ug/L
20.0
40
05/22/20 01:13
108-86-1
Bromochloromethane
ND
ug/L
20.0
40
05/22/20 01:13
74-97-5
Bromodichloromethane
ND
ug/L
20.0
40
05/22/20 01:13
75-27-4
Bromoform
ND
ug/L
20.0
40
05/22/20 01:13
75-25-2
Bromomethane
ND
ug/L
200
40
05/22/20 01:13
74-83-9
n-Butylbenzene
ND
ug/L
20.0
40
05/22/20 01:13
104-51-8
sec-Butylbenzene
ND
ug/L
20.0
40
05/22/20 01:13
135-98-8
tert-Butyl benzene
ND
ug/L
20.0
40
05/22/20 01:13
98-06-6
Carbon tetrachloride
ND
ug/L
20.0
40
05/22/20 01:13
56-23-5
Chlorobenzene
ND
ug/L
20.0
40
05/22/20 01:13
108-90-7
Chloroethane
ND
ug/L
40.0
40
05/22/20 01:13
75-00-3
Chloroform
ND
ug/L
20.0
40
05/22/20 01:13
67-66-3
Chloromethane
ND
ug/L
40.0
40
05/22/20 01:13
74-87-3
2-Chlorotoluene
ND
ug/L
20.0
40
05/22/20 01:13
95-49-8
4-Chlorotoluene
ND
ug/L
20.0
40
05/22/20 01:13
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
40.0
40
05/22/20 01:13
96-12-8
Dibromochloromethane
ND
ug/L
20.0
40
05/22/20 01:13
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
20.0
40
05/22/20 01:13
106-93-4
Dibromomethane
ND
ug/L
20.0
40
05/22/20 01:13
74-95-3
1,2-Dichlorobenzene
ND
ug/L
20.0
40
05/22/20 01:13
95-50-1
1,3-Dichlorobenzene
ND
ug/L
20.0
40
05/22/20 01:13
541-73-1
1,4-Dichlorobenzene
ND
ug/L
20.0
40
05/22/20 01:13
106-46-7
Dichlorodifluoromethane
ND
ug/L
20.0
40
05/22/20 01:13
75-71-8
1,1-Dichloroethane
ND
ug/L
20.0
40
05/22/20 01:13
75-34-3
1,2-Dichloroethane
ND
ug/L
20.0
40
05/22/20 01:13
107-06-2
1,1-Dichloroethene
ND
ug/L
20.0
40
05/22/20 01:13
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
20.0
40
05/22/20 01:13
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
20.0
40
05/22/20 01:13
156-60-5
1,2-Dichloropropane
ND
ug/L
20.0
40
05/22/20 01:13
78-87-5
1,3-Dichloropropane
ND
ug/L
20.0
40
05/22/20 01:13
142-28-9
2,2-Dichloropropane
ND
ug/L
20.0
40
05/22/20 01:13
594-20-7
1,1-Dichloropropene
ND
ug/L
20.0
40
05/22/20 01:13
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
20.0
40
05/22/20 01:13
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
20.0
40
05/22/20 01:13
10061-02-6
Diisopropyl ether
449
ug/L
20.0
40
05/22/20 01:13
108-20-3
Ethylbenzene
3490
ug/L
20.0
40
05/22/20 01:13
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
80.0
40
05/22/20 01:13
87-68-3
Isopropylbenzene (Cumene)
113
ug/L
20.0
40
05/22/20 01:13
98-82-8
Methylene Chloride
ND
ug/L
80.0
40
05/22/20 01:13
75-09-2
Methyl-tert-butyl ether
ND
ug/L
20.0
40
05/22/20 01:13
1634-04-4
Naphthalene
817
ug/L
80.0
40
05/22/20 01:13
91-20-3
n-Propylbenzene
313
ug/L
20.0
40
05/22/20 01:13
103-65-1
Styrene
ND
ug/L
20.0
40
05/22/20 01:13
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
20.0
40
05/22/20 01:13
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
20.0
40
05/22/20 01:13
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-2 Lab ID: 92477071007 Collected: 05/08/20 13:15 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
20.0
40
05/22/20 01:13
127-18-4
Toluene
315
ug/L
20.0
40
05/22/20 01:13
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
80.0
40
05/22/20 01:13
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
80.0
40
05/22/20 01:13
120-82-1
1,1,1-Trichloroethane
ND
ug/L
20.0
40
05/22/20 01:13
71-55-6
1,1,2-Trichloroethane
ND
ug/L
20.0
40
05/22/20 01:13
79-00-5
Trichloroethene
ND
ug/L
20.0
40
05/22/20 01:13
79-01-6
Trichlorofluoromethane
ND
ug/L
40.0
40
05/22/20 01:13
75-69-4
1,2,3-Trichloropropane
ND
ug/L
20.0
40
05/22/20 01:13
96-18-4
1,2,4-Trimethylbenzene
2650
ug/L
20.0
40
05/22/20 01:13
95-63-6
1,3,5-Trimethylbenzene
671
ug/L
20.0
40
05/22/20 01:13
108-67-8
Vinyl chloride
ND
ug/L
40.0
40
05/22/20 01:13
75-01-4
m&p-Xylene
5530
ug/L
40.0
40
05/22/20 01:13
179601-23-1
o-Xylene
142
ug/L
20.0
40
05/22/20 01:13
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
101
%
70-130
40
05/22/20 01:13
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
40
05/22/20 01:13
460-00-4
Toluene-d8 (S)
99
%
70-130
40
05/22/20 01:13
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-8 Lab ID: 92477071008 Collected: 05/08/20 13:30 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
05/21/20 06:03
71-43-2
Bromobenzene
ND
ug/L
0.50
1
05/21/20 06:03
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
05/21/20 06:03
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
05/21/20 06:03
75-27-4
Bromoform
ND
ug/L
0.50
1
05/21/20 06:03
75-25-2
Bromomethane
ND
ug/L
5.0
1
05/21/20 06:03
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
05/21/20 06:03
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
05/21/20 06:03
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
05/21/20 06:03
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
05/21/20 06:03
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
05/21/20 06:03
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/21/20 06:03
75-00-3
Chloroform
ND
ug/L
0.50
1
05/21/20 06:03
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/21/20 06:03
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
05/21/20 06:03
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
05/21/20 06:03
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
05/21/20 06:03
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
05/21/20 06:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
05/21/20 06:03
106-93-4
Dibromomethane
ND
ug/L
0.50
1
05/21/20 06:03
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 06:03
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 06:03
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 06:03
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
05/21/20 06:03
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
05/21/20 06:03
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
05/21/20 06:03
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
05/21/20 06:03
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
05/21/20 06:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
05/21/20 06:03
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
05/21/20 06:03
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
05/21/20 06:03
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
05/21/20 06:03
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
05/21/20 06:03
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
05/21/20 06:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
05/21/20 06:03
10061-02-6
Diisopropyl ether
19.3
ug/L
0.50
1
05/21/20 06:03
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
05/21/20 06:03
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
05/21/20 06:03
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
05/21/20 06:03
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
05/21/20 06:03
75-09-2
Methyl-tert-butyl ether
99.6
ug/L
0.50
1
05/21/20 06:03
1634-04-4
Naphthalene
ND
ug/L
2.0
1
05/21/20 06:03
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
05/21/20 06:03
103-65-1
Styrene
ND
ug/L
0.50
1
05/21/20 06:03
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
05/21/20 06:03
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
05/21/20 06:03
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: MW-8 Lab ID: 92477071008 Collected: 05/08/20 13:30 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
05/21/20 06:03
127-18-4
Toluene
ND
ug/L
0.50
1
05/21/20 06:03
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
05/21/20 06:03
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
05/21/20 06:03
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
05/21/20 06:03
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
05/21/20 06:03
79-00-5
Trichloroethene
ND
ug/L
0.50
1
05/21/20 06:03
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
05/21/20 06:03
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
05/21/20 06:03
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
05/21/20 06:03
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
05/21/20 06:03
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
05/21/20 06:03
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
05/21/20 06:03
179601-23-1
o-Xylene
ND
ug/L
0.50
1
05/21/20 06:03
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
05/21/20 06:03
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
1
05/21/20 06:03
460-00-4
Toluene-d8 (S)
100
%
70-130
1
05/21/20 06:03
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: 5726 OMC Lab ID: 92477071009 Collected: 05/08/20 14:00 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
ND
ug/L
0.50
1
05/21/20 06:21
71-43-2
Bromobenzene
ND
ug/L
0.50
1
05/21/20 06:21
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
05/21/20 06:21
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
05/21/20 06:21
75-27-4
Bromoform
ND
ug/L
0.50
1
05/21/20 06:21
75-25-2
Bromomethane
ND
ug/L
5.0
1
05/21/20 06:21
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
05/21/20 06:21
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
05/21/20 06:21
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
05/21/20 06:21
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
05/21/20 06:21
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
05/21/20 06:21
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/21/20 06:21
75-00-3
Chloroform
ND
ug/L
0.50
1
05/21/20 06:21
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/21/20 06:21
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
05/21/20 06:21
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
05/21/20 06:21
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
05/21/20 06:21
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
05/21/20 06:21
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
05/21/20 06:21
106-93-4
Dibromomethane
ND
ug/L
0.50
1
05/21/20 06:21
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 06:21
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 06:21
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
05/21/20 06:21
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
05/21/20 06:21
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
05/21/20 06:21
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
05/21/20 06:21
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
05/21/20 06:21
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
05/21/20 06:21
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
05/21/20 06:21
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
05/21/20 06:21
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
05/21/20 06:21
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
05/21/20 06:21
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
05/21/20 06:21
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
05/21/20 06:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
05/21/20 06:21
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
05/21/20 06:21
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
05/21/20 06:21
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
05/21/20 06:21
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
05/21/20 06:21
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
05/21/20 06:21
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
05/21/20 06:21
1634-04-4
Naphthalene
ND
ug/L
2.0
1
05/21/20 06:21
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
05/21/20 06:21
103-65-1
Styrene
ND
ug/L
0.50
1
05/21/20 06:21
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
05/21/20 06:21
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
05/21/20 06:21
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601 Stop
Pace Project No.: 92477071
Sample: 5726 OMC Lab ID: 92477071009 Collected: 05/08/20 14:00 Received: 05/08/20 16:08 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
ug/L
0.50
1
05/21/20 06:21
127-18-4
Toluene
ND
ug/L
0.50
1
05/21/20 06:21
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
05/21/20 06:21
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
05/21/20 06:21
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
05/21/20 06:21
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
05/21/20 06:21
79-00-5
Trichloroethene
ND
ug/L
0.50
1
05/21/20 06:21
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
05/21/20 06:21
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
05/21/20 06:21
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
05/21/20 06:21
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
05/21/20 06:21
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
05/21/20 06:21
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
05/21/20 06:21
179601-23-1
o-Xylene
ND
ug/L
0.50
1
05/21/20 06:21
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
05/21/20 06:21
17060-07-0
4-Bromofluorobenzene (S)
97
%
70-130
1
05/21/20 06:21
460-00-4
Toluene-d8 (S)
102
%
70-130
1
05/21/20 06:21
2037-26-5
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
QC Batch: 542548 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477071002, 92477071003, 92477071005
METHOD BLANK: 2890510 Matrix:
Associated Lab Samples: 92477071002, 92477071003, 92477071005
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
05/20/20 11:48
1,1,1-Trichloroethane
ug/L
ND
0.50
05/20/20 11:48
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
05/20/20 11:48
1,1,2-Trichloroethane
ug/L
ND
0.50
05/20/20 11:48
1,1-Dichloroethane
ug/L
ND
0.50
05/20/20 11:48
1,1-Dichloroethene
ug/L
ND
0.50
05/20/20 11:48
1,1-Dichloropropene
ug/L
ND
0.50
05/20/20 11:48
1,2,3-Trichlorobenzene
ug/L
ND
2.0
05/20/20 11:48
1,2,3-Trichloropropane
ug/L
ND
0.50
05/20/20 11:48
1,2,4-Trichlorobenzene
ug/L
ND
2.0
05/20/20 11:48
1,2,4-Trimethylbenzene
ug/L
ND
0.50
05/20/20 11:48
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
05/20/20 11:48
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
05/20/20 11:48
1,2-Dichlorobenzene
ug/L
ND
0.50
05/20/20 11:48
1,2-Dichloroethane
ug/L
ND
0.50
05/20/20 11:48
1,2-Dichloropropane
ug/L
ND
0.50
05/20/20 11:48
1,3,5-Trimethylbenzene
ug/L
ND
0.50
05/20/20 11:48
1,3-Dichlorobenzene
ug/L
ND
0.50
05/20/20 11:48
1,3-Dichloropropane
ug/L
ND
0.50
05/20/20 11:48
1,4-Dichlorobenzene
ug/L
ND
0.50
05/20/20 11:48
2,2-Dichloropropane
ug/L
ND
0.50
05/20/20 11:48
2-Chlorotoluene
ug/L
ND
0.50
05/20/20 11:48
4-Chlorotoluene
ug/L
ND
0.50
05/20/20 11:48
Benzene
ug/L
ND
0.50
05/20/20 11:48
Bromobenzene
ug/L
ND
0.50
05/20/20 11:48
Bromochloromethane
ug/L
ND
0.50
05/20/20 11:48
Bromodichloromethane
ug/L
ND
0.50
05/20/20 11:48
Bromoform
ug/L
ND
0.50
05/20/20 11:48
Bromomethane
ug/L
ND
5.0
05/20/20 11:48
Carbon tetrachloride
ug/L
ND
0.50
05/20/20 11:48
Chlorobenzene
ug/L
ND
0.50
05/20/20 11:48
Chloroethane
ug/L
ND
1.0
05/20/20 11:48
Chloroform
ug/L
ND
0.50
05/20/20 11:48
Chloromethane
ug/L
ND
1.0
05/20/20 11:48
cis-1,2-Dichloroethene
ug/L
ND
0.50
05/20/20 11:48
cis-1,3-Dichloropropene
ug/L
ND
0.50
05/20/20 11:48
Dibromochloromethane
ug/L
ND
0.50
05/20/20 11:48
Dibromomethane
ug/L
ND
0.50
05/20/20 11:48
Dichlorodifluoromethane
ug/L
ND
0.50
05/20/20 11:48
Diisopropyl ether
ug/L
ND
0.50
05/20/20 11:48
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
METHOD BLANK: 2890510 Matrix:
Associated Lab Samples: 92477071002, 92477071003, 92477071005
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
05/20/20 11:48
Hexachloro-1,3-butadiene
ug/L
ND
2.0
05/20/20 11:48
Isopropylbenzene (Cumene)
ug/L
ND
0.50
05/20/20 11:48
m&p-Xylene
ug/L
ND
1.0
05/20/20 11:48
Methyl-tert-butyl ether
ug/L
ND
0.50
05/20/20 11:48
Methylene Chloride
ug/L
ND
2.0
05/20/20 11:48
n-Butylbenzene
ug/L
ND
0.50
05/20/20 11:48
n-Propylbenzene
ug/L
ND
0.50
05/20/20 11:48
Naphthalene
ug/L
ND
2.0
05/20/20 11:48
o-Xylene
ug/L
ND
0.50
05/20/20 11:48
sec-Butylbenzene
ug/L
ND
0.50
05/20/20 11:48
Styrene
ug/L
ND
0.50
05/20/20 11:48
tert-Butyl benzene
ug/L
ND
0.50
05/20/20 11:48
Tetrachloroethene
ug/L
ND
0.50
05/20/20 11:48
Toluene
ug/L
ND
0.50
05/20/20 11:48
trans-1,2-Dichloroethene
ug/L
ND
0.50
05/20/20 11:48
trans- 1,3-Dichloropropene
ug/L
ND
0.50
05/20/20 11:48
Trichloroethene
ug/L
ND
0.50
05/20/20 11:48
Trichlorofluoromethane
ug/L
ND
1.0
05/20/20 11:48
Vinyl chloride
ug/L
ND
1.0
05/20/20 11:48
1,2-Dichloroethane-d4 (S)
%
102
70-130
05/20/20 11:48
4-Bromofluorobenzene (S)
%
97
70-130
05/20/20 11:48
Toluene-d8 (S)
%
101
70-130
05/20/20 11:48
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2890511
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
48.8
98
60-140
1,1,1-Trichloroethane
ug/L
50
46.1
92
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
47.2
94
60-140
1,1,2-Trichloroethane
ug/L
50
46.3
93
60-140
1,1-Dichloroethane
ug/L
50
45.7
91
60-140
1,1-Dichloroethene
ug/L
50
46.5
93
60-140
1,1-Dichloropropene
ug/L
50
46.9
94
60-140
1,2,3-Trichlorobenzene
ug/L
50
46.4
93
60-140
1,2,3-Trichloropropane
ug/L
50
47.1
94
60-140
1,2,4-Trichlorobenzene
ug/L
50
47.3
95
60-140
1,2,4-Trimethylbenzene
ug/L
50
47.8
96
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
52.1
104
60-140
1,2-Dibromoethane (EDB)
ug/L
50
49.4
99
60-140
1,2-Dichlorobenzene
ug/L
50
49.5
99
60-140
1,2-Dichloroethane
ug/L
50
43.1
86
60-140
1,2-Dichloropropane
ug/L
50
46.8
94
60-140
1,3,5-Trimethylbenzene
ug/L
50
48.5
97
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
LABORATORY CONTROL SAMPLE:
Parameter
2890511
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
49.6
99
60-140
1,3-Dichloropropane
ug/L
50
48.1
96
60-140
1,4-Dichlorobenzene
ug/L
50
48.2
96
60-140
2,2-Dichloropropane
ug/L
50
47.7
95
60-140
2-Chlorotoluene
ug/L
50
47.7
95
60-140
4-Chlorotoluene
ug/L
50
48.1
96
60-140
Benzene
ug/L
50
46.4
93
60-140
Bromobenzene
ug/L
50
48.5
97
60-140
Bromochloromethane
ug/L
50
48.6
97
60-140
Bromodichloromethane
ug/L
50
49.2
98
60-140
Bromoform
ug/L
50
50.4
101
60-140
Bromomethane
ug/L
50
49.2
98
60-140
Carbon tetrachloride
ug/L
50
47.2
94
60-140
Chlorobenzene
ug/L
50
48.4
97
60-140
Chloroethane
ug/L
50
34.3
69
60-140
Chloroform
ug/L
50
44.1
88
60-140
Chloromethane
ug/L
50
40.6
81
60-140
cis-1,2-Dichloroethene
ug/L
50
45.7
91
60-140
cis-1,3-Dichloropropene
ug/L
50
48.2
96
60-140
Dibromochloromethane
ug/L
50
50.0
100
60-140
Dibromomethane
ug/L
50
47.2
94
60-140
Dichlorodifluoromethane
ug/L
50
40.6
81
60-140
Diisopropyl ether
ug/L
50
47.5
95
60-140
Ethylbenzene
ug/L
50
45.1
90
60-140
Hexachloro-1,3-butadiene
ug/L
50
48.1
96
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.0
96
60-140
m&p-Xylene
ug/L
100
90.0
90
60-140
Methyl-tert-butyl ether
ug/L
50
47.5
95
60-140
Methylene Chloride
ug/L
50
43.9
88
60-140
n-Butylbenzene
ug/L
50
48.9
98
60-140
n-Propylbenzene
ug/L
50
45.1
90
60-140
Naphthalene
ug/L
50
46.1
92
60-140
o-Xylene
ug/L
50
46.5
93
60-140
sec-Butylbenzene
ug/L
50
47.3
95
60-140
Styrene
ug/L
50
50.3
101
60-140
tert-Butyl benzene
ug/L
50
40.9
82
60-140
Tetrachloroethene
ug/L
50
47.7
95
60-140
Toluene
ug/L
50
43.8
88
60-140
trans-1,2-Dichloroethene
ug/L
50
46.1
92
60-140
trans- 1,3-Dichloropropene
ug/L
50
49.1
98
60-140
Trichloroethene
ug/L
50
48.6
97
60-140
Trichlorofluoromethane
ug/L
50
39.1
78
60-140
Vinyl chloride
ug/L
50
50.1
100
60-140
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
99
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2890512
2890513
MS
MSD
92477677001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
5000
5000
5510
5410
110
108
60-140
2
1,1,1-Trichloroethane
ug/L
ND
5000
5000
5510
5310
110
106
60-140
4
1,1,2,2-Tetrachloroethane
ug/L
ND
5000
5000
5210
5020
104
100
60-140
4
1,1,2-Trichloroethane
ug/L
ND
5000
5000
5200
5160
104
103
60-140
1
1,1-Dichloroethane
ug/L
ND
5000
5000
5330
5210
107
104
60-140
2
1,1-Dichloroethene
ug/L
ND
5000
5000
5880
5580
118
112
60-140
5
1,1-Dichloropropene
ug/L
ND
5000
5000
5600
5490
112
110
60-140
2
1,2,3-Trichlorobenzene
ug/L
ND
5000
5000
4810
5250
96
105
60-140
9
1,2,3-Trichloropropane
ug/L
ND
5000
5000
5070
5230
101
105
60-140
3
1,2,4-Trichlorobenzene
ug/L
ND
5000
5000
5100
5470
102
109
60-140
7
1,2,4-Trimethylbenzene
ug/L
2530
5000
5000
8060
8000
111
109
60-140
1
1,2-Dibromo-3-chloropropane
ug/L
ND
5000
5000
5450
5560
109
111
60-140
2
1,2-Dibromoethane (EDB)
ug/L
102J
5000
5000
5630
5530
110
109
60-140
2
1,2-Dichlorobenzene
ug/L
ND
5000
5000
5550
5410
111
108
60-140
3
1,2-Dichloroethane
ug/L
136
5000
5000
5050
4910
98
96
60-140
3
1,2-Dichloropropane
ug/L
ND
5000
5000
5380
5460
108
109
60-140
1
1,3,5-Trimethylbenzene
ug/L
ND
5000
5000
6270
6130
125
123
60-140
2
1,3-Dichlorobenzene
ug/L
ND
5000
5000
5470
5390
109
108
60-140
1
1,3-Dichloropropane
ug/L
ND
5000
5000
5380
5280
108
106
60-140
2
1,4-Dichlorobenzene
ug/L
ND
5000
5000
5440
5300
109
106
60-140
3
2,2-Dichloropropane
ug/L
ND
5000
5000
5790
5600
116
112
60-140
3
2-Chlorotoluene
ug/L
ND
5000
5000
5710
5560
114
111
60-140
3
4-Chlorotoluene
ug/L
ND
5000
5000
5500
5330
110
107
60-140
3
Benzene
ug/L
22500
5000
5000
28700
29100
125
132
60-140
1
Bromobenzene
ug/L
ND
5000
5000
5510
5290
110
106
60-140
4
Bromochloromethane
ug/L
ND
5000
5000
5460
5310
109
106
60-140
3
Bromodichloromethane
ug/L
ND
5000
5000
5530
5430
111
109
60-140
2
Bromoform
ug/L
ND
5000
5000
5390
5290
108
106
60-140
2
Bromomethane
ug/L
ND
5000
5000
6600
6500
132
130
60-140
2
Carbon tetrachloride
ug/L
ND
5000
5000
5700
5750
114
115
60-140
1
Chlorobenzene
ug/L
ND
5000
5000
5460
5420
109
108
60-140
1
Chloroethane
ug/L
ND
5000
5000
5480
4980
110
100
60-140
9
Chloroform
ug/L
ND
5000
5000
5110
4960
102
99
60-140
3
Chloromethane
ug/L
ND
5000
5000
4840
4730
97
95
60-140
2
cis-1,2-Dichloroethene
ug/L
ND
5000
5000
5300
5170
106
103
60-140
3
cis-1,3-Dichloropropene
ug/L
ND
5000
5000
5490
5440
110
109
60-140
1
Dibromochloromethane
ug/L
ND
5000
5000
5290
5360
106
107
60-140
1
Dibromomethane
ug/L
ND
5000
5000
5180
5250
104
105
60-140
1
Dichlorodifluoromethane
ug/L
ND
5000
5000
4950
4930
99
99
60-140
0
Diisopropyl ether
ug/L
973
5000
5000
6340
6290
107
106
60-140
1
Ethylbenzene
ug/L
2990
5000
5000
8330
8290
107
106
60-140
0
Hexachloro-1,3-butadiene
ug/L
ND
5000
5000
5470
5660
109
113
60-140
3
Isopropylbenzene(Cumene)
ug/L
121J
5000
5000
5640
5590
110
109
60-140
1
m&p-Xylene
ug/L
10000
10000
10000
20800
20800
108
108
60-140
0
Methyl-tert-butyl ether
ug/L
31700
5000
5000
38200
37900
129
123
60-140
1
Methylene Chloride
ug/L
ND
5000
5000
5140
5020
103
100
60-140
2
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2890512
2890513
MS
MSD
92477677001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
5000
5000
5570
5510
111
110
60-140
1
n-Propylbenzene
ug/L
ND
5000
5000
5560
5460
111
109
60-140
2
Naphthalene
ug/L
632
5000
5000
5450
5900
96
105
60-140
8
o-Xylene
ug/L
5310
5000
5000
10800
10800
110
110
60-140
0
sec-Butylbenzene
ug/L
ND
5000
5000
5530
5420
111
108
60-140
2
Styrene
ug/L
ND
5000
5000
5690
5630
114
113
60-140
1
tert-Butyl benzene
ug/L
ND
5000
5000
4700
4670
94
93
60-140
1
Tetrachloroethene
ug/L
ND
5000
5000
5460
5390
109
108
60-140
1
Toluene
ug/L
41000
5000
5000
47100
47500
123
131
60-140
1
trans-1,2-Dichloroethene
ug/L
ND
5000
5000
5490
5300
110
106
60-140
3
trans- 1,3-Dichloropropene
ug/L
ND
5000
5000
5490
5490
110
110
60-140
0
Trichloroethene
ug/L
ND
5000
5000
5700
5510
114
110
60-140
3
Trichlorofluoromethane
ug/L
ND
5000
5000
5420
5160
108
103
60-140
5
Vinyl chloride
ug/L
ND
5000
5000
6200
5960
124
119
60-140
4
1,2-Dichloroethane-d4 (S)
%
100
101
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
QC Batch: 542698 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477071008, 92477071009
METHOD BLANK: 2891207
Associated Lab Samples: 92477071008, 92477071009
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
05/20/20 23:28
1,1,1-Trichloroethane
ug/L
ND
0.50
05/20/20 23:28
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
05/20/20 23:28
1,1,2-Trichloroethane
ug/L
ND
0.50
05/20/20 23:28
1,1-Dichloroethane
ug/L
ND
0.50
05/20/20 23:28
1,1-Dichloroethene
ug/L
ND
0.50
05/20/20 23:28
1,1-Dichloropropene
ug/L
ND
0.50
05/20/20 23:28
1,2,3-Trichlorobenzene
ug/L
ND
2.0
05/20/20 23:28
1,2,3-Trichloropropane
ug/L
ND
0.50
05/20/20 23:28
1,2,4-Trichlorobenzene
ug/L
ND
2.0
05/20/20 23:28
1,2,4-Trimethylbenzene
ug/L
ND
0.50
05/20/20 23:28
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
05/20/20 23:28
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
05/20/20 23:28
1,2-Dichlorobenzene
ug/L
ND
0.50
05/20/20 23:28
1,2-Dichloroethane
ug/L
ND
0.50
05/20/20 23:28
1,2-Dichloropropane
ug/L
ND
0.50
05/20/20 23:28
1,3,5-Trimethylbenzene
ug/L
ND
0.50
05/20/20 23:28
1,3-Dichlorobenzene
ug/L
ND
0.50
05/20/20 23:28
1,3-Dichloropropane
ug/L
ND
0.50
05/20/20 23:28
1,4-Dichlorobenzene
ug/L
ND
0.50
05/20/20 23:28
2,2-Dichloropropane
ug/L
ND
0.50
05/20/20 23:28
2-Chlorotoluene
ug/L
ND
0.50
05/20/20 23:28
4-Chlorotoluene
ug/L
ND
0.50
05/20/20 23:28
Benzene
ug/L
ND
0.50
05/20/20 23:28
Bromobenzene
ug/L
ND
0.50
05/20/20 23:28
Bromochloromethane
ug/L
ND
0.50
05/20/20 23:28
Bromodichloromethane
ug/L
ND
0.50
05/20/20 23:28
Bromoform
ug/L
ND
0.50
05/20/20 23:28
Bromomethane
ug/L
ND
5.0
05/20/20 23:28
Carbon tetrachloride
ug/L
ND
0.50
05/20/20 23:28
Chlorobenzene
ug/L
ND
0.50
05/20/20 23:28
Chloroethane
ug/L
ND
1.0
05/20/20 23:28
Chloroform
ug/L
ND
0.50
05/20/20 23:28
Chloromethane
ug/L
ND
1.0
05/20/20 23:28
cis-1,2-Dichloroethene
ug/L
ND
0.50
05/20/20 23:28
cis-1,3-Dichloropropene
ug/L
ND
0.50
05/20/20 23:28
Dibromochloromethane
ug/L
ND
0.50
05/20/20 23:28
Dibromomethane
ug/L
ND
0.50
05/20/20 23:28
Dichlorodifluoromethane
ug/L
ND
0.50
05/20/20 23:28
Diisopropyl ether
ug/L
ND
0.50
05/20/20 23:28
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
METHOD BLANK: 2891207
Associated Lab Samples: 92477071008, 92477071009
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
05/20/20 23:28
Hexachloro-1,3-butadiene
ug/L
ND
2.0
05/20/20 23:28
Isopropylbenzene (Cumene)
ug/L
ND
0.50
05/20/20 23:28
m&p-Xylene
ug/L
ND
1.0
05/20/20 23:28
Methyl-tert-butyl ether
ug/L
ND
0.50
05/20/20 23:28
Methylene Chloride
ug/L
ND
2.0
05/20/20 23:28
n-Butylbenzene
ug/L
ND
0.50
05/20/20 23:28
n-Propylbenzene
ug/L
ND
0.50
05/20/20 23:28
Naphthalene
ug/L
ND
2.0
05/20/20 23:28
o-Xylene
ug/L
ND
0.50
05/20/20 23:28
sec-Butylbenzene
ug/L
ND
0.50
05/20/20 23:28
Styrene
ug/L
ND
0.50
05/20/20 23:28
tert-Butyl benzene
ug/L
ND
0.50
05/20/20 23:28
Tetrachloroethene
ug/L
ND
0.50
05/20/20 23:28
Toluene
ug/L
ND
0.50
05/20/20 23:28
trans-1,2-Dichloroethene
ug/L
ND
0.50
05/20/20 23:28
trans- 1,3-Dichloropropene
ug/L
ND
0.50
05/20/20 23:28
Trichloroethene
ug/L
ND
0.50
05/20/20 23:28
Trichlorofluoromethane
ug/L
ND
1.0
05/20/20 23:28
Vinyl chloride
ug/L
ND
1.0
05/20/20 23:28
1,2-Dichloroethane-d4 (S)
%
102
70-130
05/20/20 23:28
4-Bromofluorobenzene (S)
%
97
70-130
05/20/20 23:28
Toluene-d8 (S)
%
99
70-130
05/20/20 23:28
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2891208
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.9
100
60-140
1,1,1-Trichloroethane
ug/L
50
47.2
94
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
48.8
98
60-140
1,1,2-Trichloroethane
ug/L
50
48.8
98
60-140
1,1-Dichloroethane
ug/L
50
46.7
93
60-140
1,1-Dichloroethene
ug/L
50
47.9
96
60-140
1,1-Dichloropropene
ug/L
50
47.9
96
60-140
1,2,3-Trichlorobenzene
ug/L
50
50.8
102
60-140
1,2,3-Trichloropropane
ug/L
50
49.5
99
60-140
1,2,4-Trichlorobenzene
ug/L
50
49.8
100
60-140
1,2,4-Trimethylbenzene
ug/L
50
47.2
94
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
53.9
108
60-140
1,2-Dibromoethane (EDB)
ug/L
50
51.0
102
60-140
1,2-Dichlorobenzene
ug/L
50
49.7
99
60-140
1,2-Dichloroethane
ug/L
50
44.5
89
60-140
1,2-Dichloropropane
ug/L
50
48.8
98
60-140
1,3,5-Trimethylbenzene
ug/L
50
48.0
96
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
LABORATORY CONTROL SAMPLE:
Parameter
2891208
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
49.4
99
60-140
1,3-Dichloropropane
ug/L
50
49.4
99
60-140
1,4-Dichlorobenzene
ug/L
50
48.5
97
60-140
2,2-Dichloropropane
ug/L
50
48.7
97
60-140
2-Chlorotoluene
ug/L
50
47.1
94
60-140
4-Chlorotoluene
ug/L
50
47.7
95
60-140
Benzene
ug/L
50
46.6
93
60-140
Bromobenzene
ug/L
50
48.6
97
60-140
Bromochloromethane
ug/L
50
50.6
101
60-140
Bromodichloromethane
ug/L
50
49.7
99
60-140
Bromoform
ug/L
50
52.3
105
60-140
Bromomethane
ug/L
50
54.4
109
60-140
Carbon tetrachloride
ug/L
50
48.9
98
60-140
Chlorobenzene
ug/L
50
49.0
98
60-140
Chloroethane
ug/L
50
32.8
66
60-140
Chloroform
ug/L
50
46.9
94
60-140
Chloromethane
ug/L
50
41.5
83
60-140
cis-1,2-Dichloroethene
ug/L
50
46.7
93
60-140
cis-1,3-Dichloropropene
ug/L
50
49.7
99
60-140
Dibromochloromethane
ug/L
50
51.9
104
60-140
Dibromomethane
ug/L
50
50.4
101
60-140
Dichlorodifluoromethane
ug/L
50
39.6
79
60-140
Diisopropyl ether
ug/L
50
47.7
95
60-140
Ethylbenzene
ug/L
50
45.6
91
60-140
Hexachloro-1,3-butadiene
ug/L
50
48.1
96
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.5
97
60-140
m&p-Xylene
ug/L
100
91.5
92
60-140
Methyl-tert-butyl ether
ug/L
50
49.5
99
60-140
Methylene Chloride
ug/L
50
44.5
89
60-140
n-Butylbenzene
ug/L
50
47.8
96
60-140
n-Propylbenzene
ug/L
50
44.9
90
60-140
Naphthalene
ug/L
50
51.1
102
60-140
o-Xylene
ug/L
50
47.2
94
60-140
sec-Butylbenzene
ug/L
50
46.9
94
60-140
Styrene
ug/L
50
51.1
102
60-140
tert-Butyl benzene
ug/L
50
40.8
82
60-140
Tetrachloroethene
ug/L
50
47.6
95
60-140
Toluene
ug/L
50
44.5
89
60-140
trans-1,2-Dichloroethene
ug/L
50
47.1
94
60-140
trans- 1,3-Dichloropropene
ug/L
50
50.6
101
60-140
Trichloroethene
ug/L
50
49.5
99
60-140
Trichlorofluoromethane
ug/L
50
39.3
79
60-140
Vinyl chloride
ug/L
50
51.3
103
60-140
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2891209 2891210
MS MSD
92477766004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.1
20.5
100
102
60-140 2
1,1,1-Trichloroethane
ug/L
ND
20
20
20.5
20.5
102
102
60-140 0
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.4
19.6
97
98
60-140 1
1,1,2-Trichloroethane
ug/L
ND
20
20
20.2
19.7
101
98
60-140 3
1,1-Dichloroethane
ug/L
ND
20
20
19.8
20.3
99
101
60-140 3
1,1-Dichloroethene
ug/L
ND
20
20
21.4
21.5
107
108
60-140 0
1,1-Dichloropropene
ug/L
ND
20
20
20.4
20.9
102
104
60-140 3
1,2,3-Trichlorobenzene
ug/L
ND
20
20
20.8
20.1
104
101
60-140 3
1,2,3-Trichloropropane
ug/L
ND
20
20
19.2
19.3
96
96
60-140 0
1,2,4-Trichlorobenzene
ug/L
ND
20
20
20.3
19.7
101
99
60-140 3
1,2,4-Trimethylbenzene
ug/L
ND
20
20
18.9
19.5
93
96
60-140 3
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.1
20.6
101
103
60-140 2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
20.6
20.8
103
104
60-140 1
1,2-Dichlorobenzene
ug/L
ND
20
20
19.3
19.6
97
98
60-140 1
1,2-Dichloroethane
ug/L
ND
20
20
18.6
18.5
93
92
60-140 1
1,2-Dichloropropane
ug/L
ND
20
20
20.3
20.2
101
101
60-140 0
1,3,5-Trimethylbenzene
ug/L
ND
20
20
19.5
20.0
97
100
60-140 3
1,3-Dichlorobenzene
ug/L
ND
20
20
19.3
19.7
96
98
60-140 2
1,3-Dichloropropane
ug/L
ND
20
20
19.8
20.5
99
102
60-140 3
1,4-Dichlorobenzene
ug/L
ND
20
20
18.7
19.1
94
96
60-140 2
2,2-Dichloropropane
ug/L
ND
20
20
22.4
22.2
112
111
60-140 1
2-Chlorotoluene
ug/L
ND
20
20
18.6
19.3
93
97
60-140 4
4-Chlorotoluene
ug/L
ND
20
20
18.8
19.1
94
96
60-140 2
Benzene
ug/L
ND
20
20
20.6
20.2
103
101
60-140 2
Bromobenzene
ug/L
ND
20
20
19.5
19.8
98
99
60-140 1
Bromochloromethane
ug/L
ND
20
20
20.7
21.1
103
106
60-140 2
Bromodichloromethane
ug/L
ND
20
20
21.0
20.9
105
104
60-140 1
Bromoform
ug/L
ND
20
20
18.8
20.0
94
100
60-140 6
Bromomethane
ug/L
ND
20
20
24.4
24.0
122
120
60-140 2
Carbon tetrachloride
ug/L
ND
20
20
21.6
21.4
108
107
60-140 1
Chlorobenzene
ug/L
ND
20
20
20.0
20.3
100
102
60-140 2
Chloroethane
ug/L
ND
20
20
18.4
18.3
92
92
60-140 0
Chloroform
ug/L
ND
20
20
19.5
19.3
98
96
60-140 1
Chloromethane
ug/L
ND
20
20
19.6
18.5
98
92
60-140 6
cis-1,2-Dichloroethene
ug/L
ND
20
20
19.9
19.9
100
99
60-140 0
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.7
20.5
104
102
60-140 1
Dibromochloromethane
ug/L
ND
20
20
20.0
20.6
100
103
60-140 3
Dibromomethane
ug/L
ND
20
20
20.2
20.0
101
100
60-140 1
Dichlorodifluoromethane
ug/L
ND
20
20
18.4
18.5
92
92
60-140 1
Diisopropyl ether
ug/L
ND
20
20
20.3
20.1
101
100
60-140 1
Ethylbenzene
ug/L
ND
20
20
19.0
19.3
95
97
60-140 1
Hexachloro-1,3-butadiene
ug/L
ND
20
20
21.1
20.8
106
104
60-140 1
Isopropylbenzene (Cumene)
ug/L
ND
20
20
19.8
20.3
99
101
60-140 2
m&p-Xylene
ug/L
ND
40
40
37.5
38.3
94
96
60-140 2
Methyl-tert-butyl ether
ug/L
ND
20
20
20.2
20.4
101
102
60-140 1
Methylene Chloride
ug/L
ND
20
20
19.7
19.7
98
98
60-140 0
Results presented on this page are in the units indicated
by the "Units"
column
except where
an alternate unit
is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2891209
2891210
MS
MSD
92477766004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
19.8
20.1
99
101
60-140
2
n-Propylbenzene
ug/L
ND
20
20
18.4
18.8
92
94
60-140
2
Naphthalene
ug/L
ND
20
20
19.5
19.1
97
95
60-140
2
o-Xylene
ug/L
ND
20
20
19.2
19.6
96
98
60-140
2
sec-Butylbenzene
ug/L
ND
20
20
19.2
20.0
96
100
60-140
4
Styrene
ug/L
ND
20
20
19.8
20.0
99
100
60-140
1
tert-Butyl benzene
ug/L
ND
20
20
16.9
17.4
85
87
60-140
2
Tetrachloroethene
ug/L
ND
20
20
19.9
20.2
99
101
60-140
2
Toluene
ug/L
ND
20
20
19.4
19.0
97
95
60-140
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.7
20.7
103
104
60-140
0
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.1
20.9
101
104
60-140
3
Trichloroethene
ug/L
ND
20
20
21.4
21.3
107
106
60-140
1
Trichlorofluoromethane
ug/L
ND
20
20
19.3
19.3
96
96
60-140
0
Vinyl chloride
ug/L
ND
20
20
22.9
22.5
115
112
60-140
2
1,2-Dichloroethane-d4 (S)
%
105
104
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8(S)
%
101
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
QC Batch: 542861 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477071001
METHOD BLANK: 2891833
Associated Lab Samples: 92477071001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
05/21/20 12:22
1,1,1-Trichloroethane
ug/L
ND
0.50
05/21/20 12:22
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
05/21/20 12:22
1,1,2-Trichloroethane
ug/L
ND
0.50
05/21/20 12:22
1,1-Dichloroethane
ug/L
ND
0.50
05/21/20 12:22
1,1-Dichloroethene
ug/L
ND
0.50
05/21/20 12:22
1,1-Dichloropropene
ug/L
ND
0.50
05/21/20 12:22
1,2,3-Trichlorobenzene
ug/L
ND
2.0
05/21/20 12:22
1,2,3-Trichloropropane
ug/L
ND
0.50
05/21/20 12:22
1,2,4-Trichlorobenzene
ug/L
ND
2.0
05/21/20 12:22
1,2,4-Trimethylbenzene
ug/L
ND
0.50
05/21/20 12:22
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
05/21/20 12:22
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
05/21/20 12:22
1,2-Dichlorobenzene
ug/L
ND
0.50
05/21/20 12:22
1,2-Dichloroethane
ug/L
ND
0.50
05/21/20 12:22
1,2-Dichloropropane
ug/L
ND
0.50
05/21/20 12:22
1,3,5-Trimethylbenzene
ug/L
ND
0.50
05/21/20 12:22
1,3-Dichlorobenzene
ug/L
ND
0.50
05/21/20 12:22
1,3-Dichloropropane
ug/L
ND
0.50
05/21/20 12:22
1,4-Dichlorobenzene
ug/L
ND
0.50
05/21/20 12:22
2,2-Dichloropropane
ug/L
ND
0.50
05/21/20 12:22
2-Chlorotoluene
ug/L
ND
0.50
05/21/20 12:22
4-Chlorotoluene
ug/L
ND
0.50
05/21/20 12:22
Benzene
ug/L
ND
0.50
05/21/20 12:22
Bromobenzene
ug/L
ND
0.50
05/21/20 12:22
Bromochloromethane
ug/L
ND
0.50
05/21/20 12:22
Bromodichloromethane
ug/L
ND
0.50
05/21/20 12:22
Bromoform
ug/L
ND
0.50
05/21/20 12:22
Bromomethane
ug/L
ND
5.0
05/21/20 12:22
Carbon tetrachloride
ug/L
ND
0.50
05/21/20 12:22
Chlorobenzene
ug/L
ND
0.50
05/21/20 12:22
Chloroethane
ug/L
ND
1.0
05/21/20 12:22
Chloroform
ug/L
ND
0.50
05/21/20 12:22
Chloromethane
ug/L
ND
1.0
05/21/20 12:22
cis-1,2-Dichloroethene
ug/L
ND
0.50
05/21/20 12:22
cis-1,3-Dichloropropene
ug/L
ND
0.50
05/21/20 12:22
Dibromochloromethane
ug/L
ND
0.50
05/21/20 12:22
Dibromomethane
ug/L
ND
0.50
05/21/20 12:22
Dichlorodifluoromethane
ug/L
ND
0.50
05/21/20 12:22
Diisopropyl ether
ug/L
ND
0.50
05/21/20 12:22
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
METHOD BLANK: 2891833
Associated Lab Samples: 92477071001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
05/21/20 12:22
Hexachloro-1,3-butadiene
ug/L
ND
2.0
05/21/20 12:22
Isopropylbenzene (Cumene)
ug/L
ND
0.50
05/21/20 12:22
m&p-Xylene
ug/L
ND
1.0
05/21/20 12:22
Methyl-tert-butyl ether
ug/L
ND
0.50
05/21/20 12:22
Methylene Chloride
ug/L
ND
2.0
05/21/20 12:22
n-Butylbenzene
ug/L
ND
0.50
05/21/20 12:22
n-Propylbenzene
ug/L
ND
0.50
05/21/20 12:22
Naphthalene
ug/L
ND
2.0
05/21/20 12:22
o-Xylene
ug/L
ND
0.50
05/21/20 12:22
sec-Butylbenzene
ug/L
ND
0.50
05/21/20 12:22
Styrene
ug/L
ND
0.50
05/21/20 12:22
tert-Butyl benzene
ug/L
ND
0.50
05/21/20 12:22
Tetrachloroethene
ug/L
ND
0.50
05/21/20 12:22
Toluene
ug/L
ND
0.50
05/21/20 12:22
trans-1,2-Dichloroethene
ug/L
ND
0.50
05/21/20 12:22
trans- 1,3-Dichloropropene
ug/L
ND
0.50
05/21/20 12:22
Trichloroethene
ug/L
ND
0.50
05/21/20 12:22
Trichlorofluoromethane
ug/L
ND
1.0
05/21/20 12:22
Vinyl chloride
ug/L
ND
1.0
05/21/20 12:22
1,2-Dichloroethane-d4 (S)
%
102
70-130
05/21/20 12:22
4-Bromofluorobenzene (S)
%
100
70-130
05/21/20 12:22
Toluene-d8 (S)
%
102
70-130
05/21/20 12:22
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2891834
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.3
99
60-140
1,1,1-Trichloroethane
ug/L
50
46.8
94
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
47.2
94
60-140
1,1,2-Trichloroethane
ug/L
50
47.6
95
60-140
1,1-Dichloroethane
ug/L
50
45.6
91
60-140
1,1-Dichloroethene
ug/L
50
48.0
96
60-140
1,1-Dichloropropene
ug/L
50
47.5
95
60-140
1,2,3-Trichlorobenzene
ug/L
50
50.4
101
60-140
1,2,3-Trichloropropane
ug/L
50
46.7
93
60-140
1,2,4-Trichlorobenzene
ug/L
50
49.7
99
60-140
1,2,4-Trimethylbenzene
ug/L
50
47.2
94
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
52.4
105
60-140
1,2-Dibromoethane (EDB)
ug/L
50
50.1
100
60-140
1,2-Dichlorobenzene
ug/L
50
49.9
100
60-140
1,2-Dichloroethane
ug/L
50
43.5
87
60-140
1,2-Dichloropropane
ug/L
50
47.7
95
60-140
1,3,5-Trimethylbenzene
ug/L
50
48.4
97
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
LABORATORY CONTROL SAMPLE:
Parameter
2891834
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
49.0
98
60-140
1,3-Dichloropropane
ug/L
50
48.4
97
60-140
1,4-Dichlorobenzene
ug/L
50
48.3
97
60-140
2,2-Dichloropropane
ug/L
50
49.0
98
60-140
2-Chlorotoluene
ug/L
50
47.2
94
60-140
4-Chlorotoluene
ug/L
50
48.1
96
60-140
Benzene
ug/L
50
46.4
93
60-140
Bromobenzene
ug/L
50
48.6
97
60-140
Bromochloromethane
ug/L
50
49.0
98
60-140
Bromodichloromethane
ug/L
50
49.8
100
60-140
Bromoform
ug/L
50
50.8
102
60-140
Bromomethane
ug/L
50
47.7
95
60-140
Carbon tetrachloride
ug/L
50
49.3
99
60-140
Chlorobenzene
ug/L
50
49.3
99
60-140
Chloroethane
ug/L
50
34.6
69
60-140
Chloroform
ug/L
50
44.1
88
60-140
Chloromethane
ug/L
50
40.5
81
60-140
cis-1,2-Dichloroethene
ug/L
50
45.9
92
60-140
cis-1,3-Dichloropropene
ug/L
50
49.3
99
60-140
Dibromochloromethane
ug/L
50
50.8
102
60-140
Dibromomethane
ug/L
50
48.3
97
60-140
Dichlorodifluoromethane
ug/L
50
44.1
88
60-140
Diisopropyl ether
ug/L
50
46.4
93
60-140
Ethylbenzene
ug/L
50
45.4
91
60-140
Hexachloro-1,3-butadiene
ug/L
50
49.0
98
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.8
98
60-140
m&p-Xylene
ug/L
100
91.0
91
60-140
Methyl-tert-butyl ether
ug/L
50
47.3
95
60-140
Methylene Chloride
ug/L
50
43.6
87
60-140
n-Butylbenzene
ug/L
50
48.7
97
60-140
n-Propylbenzene
ug/L
50
45.1
90
60-140
Naphthalene
ug/L
50
48.6
97
60-140
o-Xylene
ug/L
50
47.3
95
60-140
sec-Butylbenzene
ug/L
50
47.3
95
60-140
Styrene
ug/L
50
51.0
102
60-140
tert-Butyl benzene
ug/L
50
41.2
82
60-140
Tetrachloroethene
ug/L
50
48.5
97
60-140
Toluene
ug/L
50
44.0
88
60-140
trans-1,2-Dichloroethene
ug/L
50
46.6
93
60-140
trans- 1,3-Dichloropropene
ug/L
50
49.7
99
60-140
Trichloroethene
ug/L
50
49.2
98
60-140
Trichlorofluoromethane
ug/L
50
41.3
83
60-140
Vinyl chloride
ug/L
50
50.9
102
60-140
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2891835 2891836
MS MSD
92477677005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
1000
1000
952
962
95
96
60-140 1
1,1,1-Trichloroethane
ug/L
ND
1000
1000
966
988
97
99
60-140 2
1,1,2,2-Tetrachloroethane
ug/L
ND
1000
1000
906
933
91
93
60-140 3
1,1,2-Trichloroethane
ug/L
ND
1000
1000
924
936
92
94
60-140 1
1,1-Dichloroethane
ug/L
ND
1000
1000
940
960
94
96
60-140 2
1,1-Dichloroethene
ug/L
ND
1000
1000
1010
1040
101
104
60-140 3
1,1-Dichloropropene
ug/L
ND
1000
1000
987
1020
99
102
60-140 3
1,2,3-Trichlorobenzene
ug/L
ND
1000
1000
912
943
91
94
60-140 3
1,2,3-Trichloropropane
ug/L
ND
1000
1000
903
945
90
95
60-140 5
1,2,4-Trichlorobenzene
ug/L
ND
1000
1000
913
934
91
93
60-140 2
1,2,4-Trimethylbenzene
ug/L
860
1000
1000
1730
1850
87
99
60-140 6
1,2-Dibromo-3-chloropropane
ug/L
ND
1000
1000
971
1010
97
101
60-140 4
1,2-Dibromoethane (EDB)
ug/L
ND
1000
1000
970
1000
97
100
60-140 3
1,2-Dichlorobenzene
ug/L
ND
1000
1000
924
933
92
93
60-140 1
1,2-Dichloroethane
ug/L
ND
1000
1000
865
891
86
89
60-140 3
1,2-Dichloropropane
ug/L
ND
1000
1000
954
965
95
97
60-140 1
1,3,5-Trimethylbenzene
ug/L
ND
1000
1000
1170
1230
117
123
60-140 5
1,3-Dichlorobenzene
ug/L
ND
1000
1000
912
939
91
94
60-140 3
1,3-Dichloropropane
ug/L
ND
1000
1000
922
953
92
95
60-140 3
1,4-Dichlorobenzene
ug/L
ND
1000
1000
895
929
89
93
60-140 4
2,2-Dichloropropane
ug/L
ND
1000
1000
964
980
96
98
60-140 2
2-Chlorotoluene
ug/L
ND
1000
1000
977
953
98
95
60-140 3
4-Chlorotoluene
ug/L
ND
1000
1000
905
921
90
92
60-140 2
Benzene
ug/L
3630
1000
1000
4490
4760
86
113
60-140 6
Bromobenzene
ug/L
ND
1000
1000
924
936
92
94
60-140 1
Bromochloromethane
ug/L
ND
1000
1000
961
993
96
99
60-140 3
Bromodichloromethane
ug/L
ND
1000
1000
946
972
95
97
60-140 3
Bromoform
ug/L
ND
1000
1000
908
937
91
94
60-140 3
Bromomethane
ug/L
ND
1000
1000
1110
1140
111
114
60-140 3
Carbon tetrachloride
ug/L
ND
1000
1000
985
1010
98
101
60-140 2
Chlorobenzene
ug/L
ND
1000
1000
943
962
94
96
60-140 2
Chloroethane
ug/L
ND
1000
1000
911
954
91
95
60-140 5
Chloroform
ug/L
ND
1000
1000
892
913
89
91
60-140 2
Chloromethane
ug/L
ND
1000
1000
852
871
85
87
60-140 2
cis-1,2-Dichloroethene
ug/L
ND
1000
1000
955
974
96
97
60-140 2
cis-1,3-Dichloropropene
ug/L
ND
1000
1000
941
948
94
95
60-140 1
Dibromochloromethane
ug/L
ND
1000
1000
946
961
95
96
60-140 2
Dibromomethane
ug/L
ND
1000
1000
952
964
95
96
60-140 1
Dichlorodifluoromethane
ug/L
ND
1000
1000
853
868
85
87
60-140 2
Diisopropyl ether
ug/L
ND
1000
1000
936
956
94
96
60-140 2
Ethylbenzene
ug/L
638
1000
1000
1530
1600
89
96
60-140 4
Hexachloro-1,3-butadiene
ug/L
ND
1000
1000
942
1010
94
101
60-140 7
Isopropylbenzene(Cumene)
ug/L
40.1
1000
1000
988
1020
95
98
60-140 3
m&p-Xylene
ug/L
1510
2000
2000
3300
3450
89
97
60-140 5
Methyl-tert-butyl ether
ug/L
ND
1000
1000
941
969
94
97
60-140 3
Methylene Chloride
ug/L
ND
1000
1000
905
932
91
93
60-140 3
Results presented on this page are in
the units indicated by the "Units" column
except where
an alternate unit
is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2891835
2891836
MS
MSD
92477677005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
1000
1000
971
1020
97
102
60-140
5
n-Propylbenzene
ug/L
ND
1000
1000
997
1040
100
104
60-140
4
Naphthalene
ug/L
200
1000
1000
1090
1130
89
93
60-140
3
o-Xylene
ug/L
877
1000
1000
1770
1870
89
99
60-140
6
sec-Butylbenzene
ug/L
ND
1000
1000
914
971
91
97
60-140
6
Styrene
ug/L
15.8J
1000
1000
962
986
95
97
60-140
2
tert-Butyl benzene
ug/L
ND
1000
1000
803
820
80
82
60-140
2
Tetrachloroethene
ug/L
ND
1000
1000
936
981
94
98
60-140
5
Toluene
ug/L
5790
1000
1000
6500
6890
71
110
60-140
6
trans-1,2-Dichloroethene
ug/L
ND
1000
1000
963
998
96
100
60-140
3
trans- 1,3-Dichloropropene
ug/L
ND
1000
1000
948
958
95
96
60-140
1
Trichloroethene
ug/L
ND
1000
1000
1000
1030
100
103
60-140
2
Trichlorofluoromethane
ug/L
ND
1000
1000
922
944
92
94
60-140
2
Vinyl chloride
ug/L
ND
1000
1000
1040
1070
104
107
60-140
3
1,2-Dichloroethane-d4 (S)
%
103
104
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8(S)
%
99
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
QC Batch: 542924 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477071006, 92477071007
METHOD BLANK: 2892211
Associated Lab Samples: 92477071006, 92477071007
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
05/21/20 23:26
1,1,1-Trichloroethane
ug/L
ND
0.50
05/21/20 23:26
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
05/21/20 23:26
1,1,2-Trichloroethane
ug/L
ND
0.50
05/21/20 23:26
1,1-Dichloroethane
ug/L
ND
0.50
05/21/20 23:26
1,1-Dichloroethene
ug/L
ND
0.50
05/21/20 23:26
1,1-Dichloropropene
ug/L
ND
0.50
05/21/20 23:26
1,2,3-Trichlorobenzene
ug/L
ND
2.0
05/21/20 23:26
1,2,3-Trichloropropane
ug/L
ND
0.50
05/21/20 23:26
1,2,4-Trichlorobenzene
ug/L
ND
2.0
05/21/20 23:26
1,2,4-Trimethylbenzene
ug/L
ND
0.50
05/21/20 23:26
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
05/21/20 23:26
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
05/21/20 23:26
1,2-Dichlorobenzene
ug/L
ND
0.50
05/21/20 23:26
1,2-Dichloroethane
ug/L
ND
0.50
05/21/20 23:26
1,2-Dichloropropane
ug/L
ND
0.50
05/21/20 23:26
1,3,5-Trimethylbenzene
ug/L
ND
0.50
05/21/20 23:26
1,3-Dichlorobenzene
ug/L
ND
0.50
05/21/20 23:26
1,3-Dichloropropane
ug/L
ND
0.50
05/21/20 23:26
1,4-Dichlorobenzene
ug/L
ND
0.50
05/21/20 23:26
2,2-Dichloropropane
ug/L
ND
0.50
05/21/20 23:26
2-Chlorotoluene
ug/L
ND
0.50
05/21/20 23:26
4-Chlorotoluene
ug/L
ND
0.50
05/21/20 23:26
Benzene
ug/L
ND
0.50
05/21/20 23:26
Bromobenzene
ug/L
ND
0.50
05/21/20 23:26
Bromochloromethane
ug/L
ND
0.50
05/21/20 23:26
Bromodichloromethane
ug/L
ND
0.50
05/21/20 23:26
Bromoform
ug/L
ND
0.50
05/21/20 23:26
Bromomethane
ug/L
ND
5.0
05/21/20 23:26
Carbon tetrachloride
ug/L
ND
0.50
05/21/20 23:26
Chlorobenzene
ug/L
ND
0.50
05/21/20 23:26
Chloroethane
ug/L
ND
1.0
05/21/20 23:26
Chloroform
ug/L
ND
0.50
05/21/20 23:26
Chloromethane
ug/L
ND
1.0
05/21/20 23:26
cis-1,2-Dichloroethene
ug/L
ND
0.50
05/21/20 23:26
cis-1,3-Dichloropropene
ug/L
ND
0.50
05/21/20 23:26
Dibromochloromethane
ug/L
ND
0.50
05/21/20 23:26
Dibromomethane
ug/L
ND
0.50
05/21/20 23:26
Dichlorodifluoromethane
ug/L
ND
0.50
05/21/20 23:26
Diisopropyl ether
ug/L
ND
0.50
05/21/20 23:26
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
METHOD BLANK: 2892211
Associated Lab Samples:
Parameter
92477071006, 92477071007
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
05/21/20 23:26
Hexachloro-1,3-butadiene
ug/L
ND
2.0
05/21/20 23:26
Isopropylbenzene (Cumene)
ug/L
ND
0.50
05/21/20 23:26
m&p-Xylene
ug/L
ND
1.0
05/21/20 23:26
Methyl-tert-butyl ether
ug/L
ND
0.50
05/21/20 23:26
Methylene Chloride
ug/L
ND
2.0
05/21/20 23:26
n-Butylbenzene
ug/L
ND
0.50
05/21/20 23:26
n-Propylbenzene
ug/L
ND
0.50
05/21/20 23:26
Naphthalene
ug/L
ND
2.0
05/21/20 23:26
o-Xylene
ug/L
ND
0.50
05/21/20 23:26
sec-Butylbenzene
ug/L
ND
0.50
05/21/20 23:26
Styrene
ug/L
ND
0.50
05/21/20 23:26
tert-Butyl benzene
ug/L
ND
0.50
05/21/20 23:26
Tetrachloroethene
ug/L
ND
0.50
05/21/20 23:26
Toluene
ug/L
ND
0.50
05/21/20 23:26
trans-1,2-Dichloroethene
ug/L
ND
0.50
05/21/20 23:26
trans- 1,3-Dichloropropene
ug/L
ND
0.50
05/21/20 23:26
Trichloroethene
ug/L
ND
0.50
05/21/20 23:26
Trichlorofluoromethane
ug/L
ND
1.0
05/21/20 23:26
Vinyl chloride
ug/L
ND
1.0
05/21/20 23:26
1,2-Dichloroethane-d4 (S)
%
104
70-130
05/21/20 23:26
4-Bromofluorobenzene (S)
%
98
70-130
05/21/20 23:26
Toluene-d8 (S)
%
100
70-130
05/21/20 23:26
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2892212
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.9
104
60-140
1,1,1-Trichloroethane
ug/L
50
48.5
97
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
49.6
99
60-140
1,1,2-Trichloroethane
ug/L
50
49.1
98
60-140
1,1-Dichloroethane
ug/L
50
47.6
95
60-140
1,1-Dichloroethene
ug/L
50
48.9
98
60-140
1,1-Dichloropropene
ug/L
50
49.2
98
60-140
1,2,3-Trichlorobenzene
ug/L
50
50.8
102
60-140
1,2,3-Trichloropropane
ug/L
50
48.5
97
60-140
1,2,4-Trichlorobenzene
ug/L
50
51.2
102
60-140
1,2,4-Trimethylbenzene
ug/L
50
48.9
98
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
54.2
108
60-140
1,2-Dibromoethane (EDB)
ug/L
50
52.3
105
60-140
1,2-Dichlorobenzene
ug/L
50
51.6
103
60-140
1,2-Dichloroethane
ug/L
50
45.6
91
60-140
1,2-Dichloropropane
ug/L
50
49.8
100
60-140
1,3,5-Trimethylbenzene
ug/L
50
49.9
100
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
LABORATORY CONTROL SAMPLE:
Parameter
2892212
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
51.6
103
60-140
1,3-Dichloropropane
ug/L
50
50.8
102
60-140
1,4-Dichlorobenzene
ug/L
50
50.3
101
60-140
2,2-Dichloropropane
ug/L
50
50.1
100
60-140
2-Chlorotoluene
ug/L
50
49.3
99
60-140
4-Chlorotoluene
ug/L
50
49.4
99
60-140
Benzene
ug/L
50
48.3
97
60-140
Bromobenzene
ug/L
50
50.3
101
60-140
Bromochloromethane
ug/L
50
52.4
105
60-140
Bromodichloromethane
ug/L
50
51.2
102
60-140
Bromoform
ug/L
50
54.0
108
60-140
Bromomethane
ug/L
50
49.2
98
60-140
Carbon tetrachloride
ug/L
50
48.6
97
60-140
Chlorobenzene
ug/L
50
51.4
103
60-140
Chloroethane
ug/L
50
34.4
69
60-140
Chloroform
ug/L
50
46.2
92
60-140
Chloromethane
ug/L
50
40.2
80
60-140
cis-1,2-Dichloroethene
ug/L
50
48.2
96
60-140
cis-1,3-Dichloropropene
ug/L
50
50.5
101
60-140
Dibromochloromethane
ug/L
50
53.4
107
60-140
Dibromomethane
ug/L
50
50.1
100
60-140
Dichlorodifluoromethane
ug/L
50
42.8
86
60-140
Diisopropyl ether
ug/L
50
49.8
100
60-140
Ethylbenzene
ug/L
50
47.3
95
60-140
Hexachloro-1,3-butadiene
ug/L
50
47.6
95
60-140
Isopropylbenzene(Cumene)
ug/L
50
50.5
101
60-140
m&p-Xylene
ug/L
100
95.2
95
60-140
Methyl-tert-butyl ether
ug/L
50
49.7
99
60-140
Methylene Chloride
ug/L
50
46.1
92
60-140
n-Butylbenzene
ug/L
50
49.7
99
60-140
n-Propylbenzene
ug/L
50
46.4
93
60-140
Naphthalene
ug/L
50
50.3
101
60-140
o-Xylene
ug/L
50
49.0
98
60-140
sec-Butylbenzene
ug/L
50
47.5
95
60-140
Styrene
ug/L
50
53.1
106
60-140
tert-Butyl benzene
ug/L
50
41.9
84
60-140
Tetrachloroethene
ug/L
50
50.1
100
60-140
Toluene
ug/L
50
45.7
91
60-140
trans-1,2-Dichloroethene
ug/L
50
49.4
99
60-140
trans- 1,3-Dichloropropene
ug/L
50
51.3
103
60-140
Trichloroethene
ug/L
50
50.8
102
60-140
Trichlorofluoromethane
ug/L
50
42.0
84
60-140
Vinyl chloride
ug/L
50
51.9
104
60-140
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
96
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2892933
2892934
MS
MSD
92477766003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
2500
2500
2500
2530
100
101
60-140
1
1,1,1-Trichloroethane
ug/L
ND
2500
2500
2420
2540
97
102
60-140
5
1,1,2,2-Tetrachloroethane
ug/L
ND
2500
2500
2400
2430
96
97
60-140
1
1,1,2-Trichloroethane
ug/L
ND
2500
2500
2380
2470
95
99
60-140
4
1,1-Dichloroethane
ug/L
ND
2500
2500
2410
2450
96
98
60-140
1
1,1-Dichloroethene
ug/L
ND
2500
2500
2640
2670
106
107
60-140
1
1,1-Dichloropropene
ug/L
ND
2500
2500
2540
2610
102
104
60-140
3
1,2,3-Trichlorobenzene
ug/L
ND
2500
2500
2500
2380
100
95
60-140
5
1,2,3-Trichloropropane
ug/L
ND
2500
2500
2470
2390
99
96
60-140
3
1,2,4-Trichlorobenzene
ug/L
ND
2500
2500
2500
2470
100
99
60-140
1
1,2,4-Trimethylbenzene
ug/L
2000
2500
2500
4360
4370
95
95
60-140
0
1,2-Dibromo-3-chloropropane
ug/L
ND
2500
2500
2570
2610
103
104
60-140
1
1,2-Dibromoethane (EDB)
ug/L
ND
2500
2500
2500
2550
100
102
60-140
2
1,2-Dichlorobenzene
ug/L
ND
2500
2500
2470
2500
99
100
60-140
1
1,2-Dichloroethane
ug/L
ND
2500
2500
2210
2270
88
91
60-140
3
1,2-Dichloropropane
ug/L
ND
2500
2500
2470
2520
99
101
60-140
2
1,3,5-Trimethylbenzene
ug/L
ND
2500
2500
3030
3010
121
120
60-140
1
1,3-Dichlorobenzene
ug/L
ND
2500
2500
2500
2520
100
101
60-140
1
1,3-Dichloropropane
ug/L
ND
2500
2500
2460
2520
98
101
60-140
2
1,4-Dichlorobenzene
ug/L
ND
2500
2500
2410
2460
96
98
60-140
2
2,2-Dichloropropane
ug/L
ND
2500
2500
2640
2700
106
108
60-140
2
2-Chlorotoluene
ug/L
ND
2500
2500
2520
2670
101
107
60-140
6
4-Chlorotoluene
ug/L
ND
2500
2500
2460
2490
98
100
60-140
1
Benzene
ug/L
13500
2500
2500
15700
16100
88
106
60-140
3
Bromobenzene
ug/L
ND
2500
2500
2500
2540
100
101
60-140
1
Bromochloromethane
ug/L
ND
2500
2500
2500
2590
100
104
60-140
4
Bromodichloromethane
ug/L
ND
2500
2500
2450
2570
98
103
60-140
5
Bromoform
ug/L
ND
2500
2500
2470
2460
99
98
60-140
1
Bromomethane
ug/L
ND
2500
2500
2810
2780
112
111
60-140
1
Carbon tetrachloride
ug/L
ND
2500
2500
2480
2660
99
106
60-140
7
Chlorobenzene
ug/L
ND
2500
2500
2560
2550
102
102
60-140
0
Chloroethane
ug/L
ND
2500
2500
2320
2380
93
95
60-140
2
Chloroform
ug/L
ND
2500
2500
2430
2370
97
95
60-140
3
Chloromethane
ug/L
ND
2500
2500
2200
2230
88
89
60-140
1
cis-1,2-Dichloroethene
ug/L
ND
2500
2500
2390
2520
95
101
60-140
5
cis-1,3-Dichloropropene
ug/L
ND
2500
2500
2520
2580
101
103
60-140
2
Dibromochloromethane
ug/L
ND
2500
2500
2530
2510
101
101
60-140
0
Dibromomethane
ug/L
ND
2500
2500
2430
2500
97
100
60-140
3
Dichlorodifluoromethane
ug/L
ND
2500
2500
2190
2300
88
92
60-140
5
Diisopropyl ether
ug/L
ND
2500
2500
2460
2560
96
100
60-140
4
Ethylbenzene
ug/L
2880
2500
2500
5310
5360
97
99
60-140
1
Hexachloro-1,3-butadiene
ug/L
ND
2500
2500
2510
2560
101
102
60-140
2
Isopropylbenzene (Cumene)
ug/L
112
2500
2500
2650
2680
101
103
60-140
1
m&p-Xylene
ug/L
8020
5000
5000
12800
12900
95
97
60-140
1
Methyl-tert-butyl ether
ug/L
614
2500
2500
3050
3180
97
103
60-140
4
Methylene Chloride
ug/L
ND
2500
2500
2320
2410
93
96
60-140
4
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2892933
2892934
MS
MSD
92477766003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
2500
2500
2560
2560
102
103
60-140
0
n-Propylbenzene
ug/L
ND
2500
2500
2630
2590
105
104
60-140
1
Naphthalene
ug/L
654
2500
2500
2900
2830
90
87
60-140
2
o-Xylene
ug/L
4430
2500
2500
6870
6920
98
100
60-140
1
sec-Butylbenzene
ug/L
ND
2500
2500
2510
2500
100
100
60-140
0
Styrene
ug/L
ND
2500
2500
2580
2630
103
105
60-140
2
tert-Butyl benzene
ug/L
ND
2500
2500
2150
2160
86
87
60-140
1
Tetrachloroethene
ug/L
ND
2500
2500
2520
2550
101
102
60-140
1
Toluene
ug/L
19500
2500
2500
21000
21500
59
81
60-140
3 M1
trans-1,2-Dichloroethene
ug/L
ND
2500
2500
2460
2630
98
105
60-140
7
trans- 1,3-Dichloropropene
ug/L
ND
2500
2500
2490
2570
100
103
60-140
3
Trichloroethene
ug/L
ND
2500
2500
2550
2650
102
106
60-140
4
Trichlorofluoromethane
ug/L
ND
2500
2500
2340
2440
93
98
60-140
4
Vinyl chloride
ug/L
ND
2500
2500
2710
2770
108
111
60-140
2
1,2-Dichloroethane-d4 (S)
%
102
101
70-130
4-Bromofluorobenzene (S)
%
101
101
70-130
Toluene-d8(S)
%
98
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 41 of 51

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
QC Batch: 543120 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477071004
METHOD BLANK: 2893179
Associated Lab Samples: 92477071004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
05/22/20 13:24
1,1,1-Trichloroethane
ug/L
ND
0.50
05/22/20 13:24
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
05/22/20 13:24
1,1,2-Trichloroethane
ug/L
ND
0.50
05/22/20 13:24
1,1-Dichloroethane
ug/L
ND
0.50
05/22/20 13:24
1,1-Dichloroethene
ug/L
ND
0.50
05/22/20 13:24
1,1-Dichloropropene
ug/L
ND
0.50
05/22/20 13:24
1,2,3-Trichlorobenzene
ug/L
ND
2.0
05/22/20 13:24
1,2,3-Trichloropropane
ug/L
ND
0.50
05/22/20 13:24
1,2,4-Trichlorobenzene
ug/L
ND
2.0
05/22/20 13:24
1,2,4-Trimethylbenzene
ug/L
ND
0.50
05/22/20 13:24
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
05/22/20 13:24
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
05/22/20 13:24
1,2-Dichlorobenzene
ug/L
ND
0.50
05/22/20 13:24
1,2-Dichloroethane
ug/L
ND
0.50
05/22/20 13:24
1,2-Dichloropropane
ug/L
ND
0.50
05/22/20 13:24
1,3,5-Trimethylbenzene
ug/L
ND
0.50
05/22/20 13:24
1,3-Dichlorobenzene
ug/L
ND
0.50
05/22/20 13:24
1,3-Dichloropropane
ug/L
ND
0.50
05/22/20 13:24
1,4-Dichlorobenzene
ug/L
ND
0.50
05/22/20 13:24
2,2-Dichloropropane
ug/L
ND
0.50
05/22/20 13:24
2-Chlorotoluene
ug/L
ND
0.50
05/22/20 13:24
4-Chlorotoluene
ug/L
ND
0.50
05/22/20 13:24
Benzene
ug/L
ND
0.50
05/22/20 13:24
Bromobenzene
ug/L
ND
0.50
05/22/20 13:24
Bromochloromethane
ug/L
ND
0.50
05/22/20 13:24
Bromodichloromethane
ug/L
ND
0.50
05/22/20 13:24
Bromoform
ug/L
ND
0.50
05/22/20 13:24
Bromomethane
ug/L
ND
5.0
05/22/20 13:24
Carbon tetrachloride
ug/L
ND
0.50
05/22/20 13:24
Chlorobenzene
ug/L
ND
0.50
05/22/20 13:24
Chloroethane
ug/L
ND
1.0
05/22/20 13:24
Chloroform
ug/L
ND
0.50
05/22/20 13:24
Chloromethane
ug/L
ND
1.0
05/22/20 13:24
cis-1,2-Dichloroethene
ug/L
ND
0.50
05/22/20 13:24
cis-1,3-Dichloropropene
ug/L
ND
0.50
05/22/20 13:24
Dibromochloromethane
ug/L
ND
0.50
05/22/20 13:24
Dibromomethane
ug/L
ND
0.50
05/22/20 13:24
Dichlorodifluoromethane
ug/L
ND
0.50
05/22/20 13:24
Diisopropyl ether
ug/L
ND
0.50
05/22/20 13:24
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 51

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
METHOD BLANK: 2893179
Associated Lab Samples: 92477071004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Ethylbenzene
ug/L
ND
0.50
05/22/20 13:24
Hexachloro-1,3-butadiene
ug/L
ND
2.0
05/22/20 13:24
Isopropylbenzene (Cumene)
ug/L
ND
0.50
05/22/20 13:24
m&p-Xylene
ug/L
ND
1.0
05/22/20 13:24
Methyl-tert-butyl ether
ug/L
ND
0.50
05/22/20 13:24
Methylene Chloride
ug/L
ND
2.0
05/22/20 13:24
n-Butylbenzene
ug/L
ND
0.50
05/22/20 13:24
n-Propylbenzene
ug/L
ND
0.50
05/22/20 13:24
Naphthalene
ug/L
ND
2.0
05/22/20 13:24
o-Xylene
ug/L
ND
0.50
05/22/20 13:24
sec-Butylbenzene
ug/L
ND
0.50
05/22/20 13:24
Styrene
ug/L
ND
0.50
05/22/20 13:24
tert-Butyl benzene
ug/L
ND
0.50
05/22/20 13:24
Tetrachloroethene
ug/L
ND
0.50
05/22/20 13:24
Toluene
ug/L
ND
0.50
05/22/20 13:24
trans-1,2-Dichloroethene
ug/L
ND
0.50
05/22/20 13:24
trans- 1,3-Dichloropropene
ug/L
ND
0.50
05/22/20 13:24
Trichloroethene
ug/L
ND
0.50
05/22/20 13:24
Trichlorofluoromethane
ug/L
ND
1.0
05/22/20 13:24
Vinyl chloride
ug/L
ND
1.0
05/22/20 13:24
1,2-Dichloroethane-d4 (S)
%
108
70-130
05/22/20 13:24
4-Bromofluorobenzene (S)
%
98
70-130
05/22/20 13:24
Toluene-d8 (S)
%
101
70-130
05/22/20 13:24
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2893180
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.7
103
60-140
1,1,1-Trichloroethane
ug/L
50
50.7
101
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
49.3
99
60-140
1,1,2-Trichloroethane
ug/L
50
49.8
100
60-140
1,1-Dichloroethane
ug/L
50
49.4
99
60-140
1,1-Dichloroethene
ug/L
50
51.1
102
60-140
1,1-Dichloropropene
ug/L
50
51.5
103
60-140
1,2,3-Trichlorobenzene
ug/L
50
48.1
96
60-140
1,2,3-Trichloropropane
ug/L
50
47.5
95
60-140
1,2,4-Trichlorobenzene
ug/L
50
49.2
98
60-140
1,2,4-Trimethylbenzene
ug/L
50
49.3
99
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
51.7
103
60-140
1,2-Dibromoethane (EDB)
ug/L
50
51.6
103
60-140
1,2-Dichlorobenzene
ug/L
50
51.0
102
60-140
1,2-Dichloroethane
ug/L
50
46.5
93
60-140
1,2-Dichloropropane
ug/L
50
50.3
101
60-140
1,3,5-Trimethylbenzene
ug/L
50
49.7
99
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 51

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
LABORATORY CONTROL SAMPLE:
Parameter
2893180
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichlorobenzene
ug/L
50
49.8
100
60-140
1,3-Dichloropropane
ug/L
50
50.3
101
60-140
1,4-Dichlorobenzene
ug/L
50
49.1
98
60-140
2,2-Dichloropropane
ug/L
50
51.5
103
60-140
2-Chlorotoluene
ug/L
50
49.0
98
60-140
4-Chlorotoluene
ug/L
50
49.1
98
60-140
Benzene
ug/L
50
48.9
98
60-140
Bromobenzene
ug/L
50
49.8
100
60-140
Bromochloromethane
ug/L
50
54.1
108
60-140
Bromodichloromethane
ug/L
50
52.1
104
60-140
Bromoform
ug/L
50
52.5
105
60-140
Bromomethane
ug/L
50
52.5
105
60-140
Carbon tetrachloride
ug/L
50
51.5
103
60-140
Chlorobenzene
ug/L
50
50.7
101
60-140
Chloroethane
ug/L
50
36.4
73
60-140
Chloroform
ug/L
50
49.4
99
60-140
Chloromethane
ug/L
50
44.0
88
60-140
cis-1,2-Dichloroethene
ug/L
50
49.8
100
60-140
cis-1,3-Dichloropropene
ug/L
50
52.1
104
60-140
Dibromochloromethane
ug/L
50
52.5
105
60-140
Dibromomethane
ug/L
50
51.5
103
60-140
Dichlorodifluoromethane
ug/L
50
43.6
87
60-140
Diisopropyl ether
ug/L
50
51.4
103
60-140
Ethylbenzene
ug/L
50
47.4
95
60-140
Hexachloro-1,3-butadiene
ug/L
50
49.7
99
60-140
Isopropylbenzene (Cumene)
ug/L
50
50.7
101
60-140
m&p-Xylene
ug/L
100
95.6
96
60-140
Methyl-tert-butyl ether
ug/L
50
51.2
102
60-140
Methylene Chloride
ug/L
50
47.6
95
60-140
n-Butylbenzene
ug/L
50
50.0
100
60-140
n-Propylbenzene
ug/L
50
46.5
93
60-140
Naphthalene
ug/L
50
47.2
94
60-140
o-Xylene
ug/L
50
49.0
98
60-140
sec-Butylbenzene
ug/L
50
48.9
98
60-140
Styrene
ug/L
50
53.0
106
60-140
tert-Butyl benzene
ug/L
50
42.5
85
60-140
Tetrachloroethene
ug/L
50
49.1
98
60-140
Toluene
ug/L
50
47.2
94
60-140
trans-1,2-Dichloroethene
ug/L
50
50.6
101
60-140
trans- 1,3-Dichloropropene
ug/L
50
52.1
104
60-140
Trichloroethene
ug/L
50
52.2
104
60-140
Trichlorofluoromethane
ug/L
50
43.1
86
60-140
Vinyl chloride
ug/L
50
54.8
110
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
99
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 51

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2893181 2893182
MS MSD
92477807009 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
<2.1
100
100
104
104
104
104
60-140 0
1,1,1-Trichloroethane
ug/L
<1.4
100
100
100
101
100
101
60-140 0
1,1,2,2-Tetrachloroethane
ug/L
<0.96
100
100
100
101
100
101
60-140 1
1,1,2-Trichloroethane
ug/L
<1.2
100
100
99.2
100
99
100
60-140 1
1,1-Dichloroethane
ug/L
<1.2
100
100
101
100
101
100
60-140 0
1,1-Dichloroethene
ug/L
<1.1
100
100
108
108
108
108
60-140 0
1,1-Dichloropropene
ug/L
<1.7
100
100
105
107
105
107
60-140 1
1,2,3-Trichlorobenzene
ug/L
<3.9
100
100
98.4
98.4
98
98
60-140 0
1,2,3-Trichloropropane
ug/L
<1.4
100
100
97.8
100
98
100
60-140 3
1,2,4-Trichlorobenzene
ug/L
<2.2
100
100
99.9
98.3
100
98
60-140 2
1,2,4-Trimethylbenzene
ug/L
222
100
100
301
306
79
85
60-140 2
1,2-Dibromo-3-chloropropane
ug/L
<1.9
100
100
109
110
109
110
60-140 0
1,2-Dibromoethane (EDB)
ug/L
<1.2
100
100
105
105
105
105
60-140 1
1,2-Dichlorobenzene
ug/L
<1.2
100
100
99.1
102
99
102
60-140 3
1,2-Dichloroethane
ug/L
<1.3
100
100
92.2
93.7
92
94
60-140 2
1,2-Dichloropropane
ug/L
<0.92
100
100
103
103
103
103
60-140 0
1,3,5-Trimethylbenzene
ug/L
<1.1
100
100
112
116
112
116
60-140 3
1,3-Dichlorobenzene
ug/L
<1.2
100
100
99.5
102
99
102
60-140 2
1,3-Dichloropropane
ug/L
<1.7
100
100
102
103
102
103
60-140 1
1,4-Dichlorobenzene
ug/L
<1.2
100
100
97.7
100
98
100
60-140 2
2,2-Dichloropropane
ug/L
<1.4
100
100
111
114
111
114
60-140 3
2-Chlorotoluene
ug/L
<1.0
100
100
103
106
103
106
60-140 3
4-Chlorotoluene
ug/L
<1.0
100
100
98.4
102
98
102
60-140 3
Benzene
ug/L
378
100
100
446
454
68
76
60-140 2
Bromobenzene
ug/L
<1.1
100
100
101
103
101
103
60-140 3
Bromochloromethane
ug/L
<1.3
100
100
103
102
103
102
60-140 1
Bromodichloromethane
ug/L
<0.92
100
100
105
104
105
104
60-140 1
Bromoform
ug/L
<2.0
100
100
101
103
101
103
60-140 1
Bromomethane
ug/L
<8.6
100
100
102
101
102
101
60-140 1
Carbon tetrachloride
ug/L
<1.2
100
100
109
111
109
111
60-140 2
Chlorobenzene
ug/L
<1.1
100
100
103
103
103
103
60-140 0
Chloroethane
ug/L
<2.9
100
100
94.6
96.4
95
96
60-140 2
Chloroform
ug/L
<1.8
100
100
98.4
97.5
98
98
60-140 1
Chloromethane
ug/L
<2.1
100
100
86.7
86.5
87
86
60-140 0
cis-1,2-Dichloroethene
ug/L
<1.0
100
100
100
100
100
100
60-140 0
cis-1,3-Dichloropropene
ug/L
<1.8
100
100
105
104
105
104
60-140 1
Dibromochloromethane
ug/L
<2.0
100
100
105
106
105
106
60-140 1
Dibromomethane
ug/L
<1.6
100
100
102
105
102
105
60-140 3
Dichlorodifluoromethane
ug/L
<1.4
100
100
90.0
93.1
90
93
60-140 3
Diisopropyl ether
ug/L
6.2
100
100
107
109
101
102
60-140 2
Ethylbenzene
ug/L
411
100
100
475
482
64
71
60-140 2
Hexachloro-1,3-butadiene
ug/L
<6.0
100
100
106
107
106
107
60-140 2
Isopropylbenzene(Cumene)
ug/L
17.3
100
100
118
120
101
102
60-140 1
m&p-Xylene
ug/L
193
200
200
373
377
90
92
60-140 1
Methyl-tert-butyl ether
ug/L
640
100
100
729
725
88
84
60-140 1
Methylene Chloride
ug/L
<7.5
100
100
99.4
98.8
99
99
60-140 1
Results presented on this page are
in the units indicated by the "Units"
column
except where
an alternate unit
is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 51

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601 Stop
Pace Project No.: 92477071
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2893181
2893182
MS
MSD
92477807009
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
<1.8
100
100
103
105
103
105
60-140
1
n-Propylbenzene
ug/L
39.8
100
100
131
134
91
94
60-140
2
Naphthalene
ug/L
77.0
100
100
172
176
95
99
60-140
3
o-Xylene
ug/L
79.7
100
100
175
173
95
94
60-140
1
sec-Butylbenzene
ug/L
<1.2
100
100
102
104
102
104
60-140
2
Styrene
ug/L
<1.3
100
100
103
103
103
103
60-140
0
tert-Butyl benzene
ug/L
<1.2
100
100
87.8
88.8
88
89
60-140
1
Tetrachloroethene
ug/L
<1.2
100
100
102
105
102
105
60-140
3
Toluene
ug/L
64.1
100
100
153
152
89
88
60-140
1
trans-1,2-Dichloroethene
ug/L
<1.3
100
100
104
105
104
105
60-140
0
trans- 1,3-Dichloropropene
ug/L
<2.0
100
100
104
105
104
105
60-140
0
Trichloroethene
ug/L
<1.2
100
100
105
106
105
106
60-140
1
Trichlorofluoromethane
ug/L
<1.7
100
100
97.2
97.9
97
98
60-140
1
Vinyl chloride
ug/L
<2.0
100
100
113
112
113
112
60-140
1
1,2-Dichloroethane-d4 (S)
%
102
104
70-130
4-Bromofluorobenzene (S)
%
100
99
70-130
Toluene-d8(S)
%
100
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 51

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 601 Stop
Pace Project No.: 92477071
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 05/22/2020 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 51

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 601 Stop
Pace Project No.: 92477071
Lab ID
Sample ID
QC
Batch Method
QC Batch
92477071001
5677 CSR
SM
6200B
542861
92477071002
5600 CSR
SM
6200B
542548
92477071003
MW-6
SM
6200B
542548
92477071004
MW-7
SM
6200B
543120
92477071005
MW-5
SM
6200B
542548
92477071006
MW-1
SM
6200B
542924
92477071007
MW-2
SM
6200B
542924
92477071008
MW-8
SM
6200B
542698
92477071009
5726 OMC
SM
6200B
542698
Date: 05/22/2020 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 48 of 51

Document Name:
Document Revised: February 7, 2018
52WWIACal'
Sample Condition Upon Recelpt{SOUR}
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[:] Greenwood ❑ Huntersville a Raleigh[] Mechanicsville❑
Sample Condition Client Name: Wo# : 92477071
Upon Receipt Project #:
Courier: ❑Fed Ex ❑UPS EIUSPS Tint
❑ Commercial ❑Pace ❑other: 92477071
Custody Seal Present? ❑Yes [ fq" Seals Intact? []Yes No
pate/lnitlals Person Examining Contents'
Packing Material: ❑bubble Wrap Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes -oho ❑N/A
-QA Gun ID: 92
`T461 Type of Ice: $wet ❑Blue []mane
Cooler Temp (°C): ) Correction Factor: Add/Subtract (+C► +_ 00..1 —
Gj Temp should be above freezing to VC
Cooler Temp Corrected ("Cj: ❑Samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil (2 N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
I —Iva. r-1w..- inrludine Hawall and Puertn Ricol? 7IYes MNo
Comments/Dlscre ancy:
Chain of Custody Present?
es
❑No
❑N/A
1.
Samples Arrived within Hold Time?
MNo
❑N/A
2,
Short Hold Time Analysis (<72 hr.)?
[]Yes
E�—No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
-j]Na
❑N/A
4.
Sufficient Volume?
es
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
les
Yes
❑No
ONO
❑NIA
❑N/A
6,
Containers Intact?
es ❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
❑o/A
8.
Samule Labels Match COO
es
oNo
N A
9.
-Includes Date/Time/ID/Analysis Matrix:
/ r
Heads ace in VOA Vials (>5-6mm)?
I❑Yes
]�lo
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
oilo
❑No
❑N/A
aN/A
11.
COMMENTSISAMPLE DISCREPANCY field Data Required? []Yes ❑No
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Lot ID of Wit containers:
Date:
Date:
Page 49 of 51

Document Name:
Document Revised: February 7, 2018
aceArtalyfleal
/�7L!j-CAR-CS-033-Rev.06
Condition Upon Recel t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechiorination is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of battle
V#:92477071
PSI: TIH Due Dale: 05/22/20
CLIENT: 92-Irminger
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pH Adjustment Log for Preserved Samples
Sample ID
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pH upon receipt
Date preservation adjusted
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adjusted
Amount of Preservative
added
Lot M
Note: Whenever therels a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNS Certification Office (i e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 50 of 51

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Page 51 of 51

Beverly, Trudy
From: Beverly, Trudy
Sent: Friday, June 12, 2020 6:59 AM
To: Steven Irminger
Subject: RE: [External] 40338 Monitoring Report Highway Six O One Stop
Received. Thank you Steve.
Have a great weekend,
Trudy
�IEQTrudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
rL�n[O ��" UST Section, Mooresville Regional Office
LMW704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: htips://deq.nc.gov/about/divisions/waste-manaaement/ust
Branch's Above Ground Storage Tanks Website Address: ht!ps:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hit 2s: //deg.nc. gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.eov/nedeci/Waste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
htips:Hfiles.nc. gov/ncdeq/\Vaste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Steven Irminger [mailto:[e-mail]]
Sent: Thursday, June 11, 2020 4:51 PM
To: Beverly, Trudy <[e-mail]>
Subject: [External] 40338 Monitoring Report Highway Six O One Stop
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
[e-mail]
Dear Ms. Beverly,
The 2020 Monitoring Report for Incident Number 40338 is attached to this email. Should you have any
questions regarding this transmission, please do not hesitate to contact me.
Steve Irminger
704-701-9099