MO-27779_47089_CA_IAR_20200717_Initial Abatement Report

Harmon Environmental_, PA
615 Bruce Thomas Road 704-292-4527
Monroe, North Carolina 28112 harmonenvironmental. com
July 17, 2020
Ms. Trudy Beverly, P.G.
North Carolina Department of
Environmental Quality
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Re: Transmittal of Initial Abatement Action Report
Griggs Property Residential Heating Oil Tank
18100 Statesville Road, Cornelius Road
Incident No. 47089
Project No. 848-01
Dear Ms. Beverly:
Attached please find an Initial Abatement Action Report summarizing the removal of approximately
44.98-tons of petroleum -impacted soil a former 500-gallon, non-commercial, non -regulated, heating
oil underground storage tank (UST) removed from the site on April 24, 2020 by Geo-Hydro
Engineers, Inc.
Following completion of the soil removal activities, confirmatory soil samples were collected from
the base and side walls of the excavation. The analytical results associated with the soil samples did
not indicate the presence of targeted constituents at concentrations exceeding the North Carolina
Department of Environmental Quality (DEQ) established action levels.
Based on the analytical results associated with this project, Harmon Environmental, PA respectfully
requests the DEQ consider issuing a "no further action" letter for this site.
Thank you in advance for your prompt assistance in this matter. Please call if you have any
questions or require any additional information.
Sincerely,
Har on Environmental, PA
Richard L. Harmon, P.G.
President/Principal Hydrogeologist
Attachments
cc: Mr. Jeff Bazow
Ms. Carol Van Buren - Van Buren Law, PLLC

Initial Abatement Action Report Appendix A
Report Formats
Initial Abatement Action Report
In addition to reporting initial response and abatement actions and assessment actions and presenting initial site
characterization, this newly -created Initial Abatement Action Report must fulfill the requirements, when arelease
has been discovered, for the following individual reports:
❑ Site Check Report (Section C)
❑ UST Closure Report (UST-12) with UST-2 Form (Section D)
❑ Post -Excavation Soil Contamination Assessment Report (Section H)
❑ Product Recovery Report (Section E)
Check the applicable report(s). Complete Sections A-L, as required, including the sections specifically designated
for the reports you have indicated. The Initial Abatement Action Report must be submitted to the appropriate
regional office within 90 days following discovery of release.
A. Site Information
1. Site Identification
Date of Report: July 16, 2020
'Facility LD.: Not Applicable UST Incident Number (if known): 47089
='Site Name: Griggs Property
Site Street Address: 18100 Statesville Road
City/Town: Cornelius Zip Code: 28031 County: Mecklenburg
'Description of Geographical Data Point (e.g., diesel fill port): Former UST location
"Location Method (GPS, topographical map, other): GPS
Latitude (decimal degrees):_35.460546 Longitude (decimal degrees):-80.868502
2. Information about Contacts Associated with the Leaking UST System (Addresses must include street, city,
state, zip code and inailing address, if different).
'UST Owner:
Address: Tel.:
BUST Operator
Address: Tel:
-Property Owner: Griggs Estate - Bruce F. Griggs, Executor
Address: 9522 Westmoreland Road Cornelius NC 28031 Tel.:
5-�'Property Occupant: Vacant
Address: Tel.:
-Consultant/Contractor: Harmon Environmental PA
Address: 615 Bruce Thomas Road Monroe NC 28112 Tel: [phone]
1--j Analytical Laboratory: Pace Analytical Services, LLC State Certification No.: 12
Address: 9800 Kincey Avenue, Huntersville, NC 28078 Tel: [phone]
3. Information about Release
r­—Date Discovered: April 24, 2020
^"-Estimated Quantity of Release: Unknown
''Cause of Release: pitting and holes in the tank
Source of Release (Dispenser/Piping/UST): UST -I
,='Sizes and contents of UST system(s) from which the release occurred): 500-gallon heating oil tank
4. Certification (The title page roust display the seal and signature of the certifying P.E. or L.G. and the
name and certification number of the company or corporation, if applicable (See 1 SA NCAC 2L
.0103(e)].)
I, Richard L. Harmon, a Professional Engine �rlLiccnsed Geologist (c cle one) for (firm or company of employment), do
certify that the information contained in this rcurate to the best of my knowledge.
(Please Affix Seal and Signature)�'It
Harmon Environmental PA (Name
one or both) in North Carolina The i
Initial Abatement Report
Griggs Property
18100 Statesville Road
Cornelius, North Carolina 28031
cA4onAs licensed to pra 'ce geology ngineering (circle
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Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, North Carolina 28112
harmonenvironmental. com

Initial Abatement Action Report Appendix A
Report Formats
B. Site History and Characterization
1. Provide UST owner and operator information.
® List the names, addresses, telephone numbers, and dates of ownership/operation of all previous UST
owners and operators of the UST system(s). Present in table form (Use Reporting Table B-2, Site
History, UST Owner/Operator Information, from the Guidelines, Appendix B.).
See attached Table B-2.
2. Provide UST information (inclusive of all USTs, currently and historically in place at facility). For each
UST, provide the following information in table form (Use Reporting Table 13-1, Site History, UST/AST
System Information, from the Guidelines, Appendix B.):
o Tank identification number (keyed to a site map showing the locations of all UST systems);
o Last contents of tank;
© Previous contents of tank (if any);
® Capacity of tank in gallons;
® Construction (material and structure);
o Tank dimensions;
o Installation date;
© Description of piping and pump(s) associated with each UST;
© Status of UST (in use or not in use, closed in place, closed by removal; date of last use, date of
closure); and
o Indication that a release was or was not associated with the tank or associated piping or pump(s).
Provide discussion to supplement Table B-1 and the UST location map in order to clarify the spatial and
historical relationships among tanks and between tanks and piping and dispensers. Provide information
about any historical compliance issues.
See attached Table B-1. On April 24, 2020 Geo-Hydro Engineers. Inc. removed a 500- ag llon
non-commercial, non -regulated heating oil tank from the site. In conjunction with the tank
removal approximately 19 tons of petroleum -impacted soil was excavated, and a May 19, 2020
Underground Storage Tank Closure Report was submitted to the North Carolina Department of
Environmental Quality_(DEQ). Incident No. 47089 was assigned to this release. Harmon
Environmental, PA was subsequently contracted to excavate and remove additional petroleum -
impacted soil from the site. UST-1 was a heating oil tank used to heat the building on -site.
3. Provide non -UST information.
o List, describe, and indicate location of ASTs and associated piping and pump(s) currently and
historically in place at facility) and describe historical releases. For each AST, present the information
in table form (Use Reporting Table B-1, Site History, UST/AST System Information, from the
Guidelines, Appendix B.); and
o List, describe, and indicate location and date of spills which have occurred at facility.
See attached Table B-1. This table summarizes the petroleum incidences at this site prior to April
4. Provide a comprehensive' description of the release, including date discovered, cause and source (including
tank identification number and contents), and the relationship of historical UST releases, non -UST releases,
and off -site releases (indicate incident number) to contamination from current release.
Incident Number 47089 has been assigned to the release associated with UST -I. No other
releases are documented at this site.
5. Provide a brief description of site characteristics (including status of facility (active or inactive), land use of
site and surrounding area, water supply, topography, vegetation, surface water, wells, buildings, surface
cover, soil type, depth to and nature of bedrock, depth to groundwater, direction of groundwater flow, etc.)
The site is located in a rural residential area of Cornelius, North Carolina. The topography of
this site slopes toward the southwest draining toward an unnamed tributary_of McDowell Creek.
Initial Abatement Report 2 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
The vegetation on site consists primarily of grass and ornamental shrubbery. Based on the Soil
Survey of Mecklenburg County published by the United States Department ofAgriculture, Natural
Resources Conservation Service (USDA NRCS) in 2018, the soil type associated with this region
of Mecklenburg County as Cecil sandy clay loam (CeB2). The depth to bedrock, the depth to
groundwater and the groundwater flow direction at the site have not been determined.
6. Summarize initial abatement actions, assessment activities, and corrective actions performed to date and list
all reports previously submitted.
On Ma)Z 19, 2020 Geo-Hydro Engineers. Inc, submitted a report to the DEO entitled Proposed
Leafsprings Cornelius Underground Storage Tank System Closure and Sampling Report. This
report described the removal of a 500-gallon heating oil UST from the site and the excavation of
approximately 19-tons of petroleum -impacted soil. On June 30, 2020. PGP Services. Inc. under
the oversight of Harmon Environmental, PA excavated and additional approximately 44.98-tons
of petroleum -impacted soil from the vicinity of the former UST basin. This soil was transported to
the Environmental Soil. Inc. permitted land application site in Lattimore, North Carolina for
Qppropriate disposal,
C. Site Check Report (if applicable)
Incorporate the minimum requirements of a Site Check Report, as outlined in the Guidelines, Appendix A, p.
43, if a site check revealed a release and initiated the initial response and abatement action.
l.. Present and summarize the results of tank and line tightness testing (Refer to Section L, Appendix A,
Tightness testing results and supporting documentation). If theses tightness testing results did not indicate
a release, and if, instead, environmental contamination was the basis for suspecting a release, describe the
environmental contamination.
2. Describe the site check procedure. (For guidance refer to the Guidelines; Section 4.3, Site Check
Requirements). Reference site and sample location maps provided in Section J, Figures, and summaries of
soil and groundwater analytical results provided in Section K, Tables. Explain how the selection of sample
types and locations was influenced by the nature of the stored substance, the type of initial alarm or cause
for suspicion, the type of backfill, the depth to groundwater, and other factors appropriate for identifying
the presence and source of a release. Describe the condition of the UST system (i.e., pitting, holes, etc.)
where it can be observed.
3. If a release is determined, document initial response actions (submittal of 24-14our Release and Report
Form; repair, replacement, or upgrading of system to prevent further release; mitigation of hazards) and
initial abatement actions (free product removal; submittal of 20-Day Report) performed in Section G, Initial
Response and Abatement Actions;
4. Document any soil excavation activities in Section H, Excavation of Contaminated Soil.
5. Document site investigation.
- Describe field screening, including:
`? Physical characteristics of the soil samples, as observed during collection;
Field instrumentation used to screen soils;
L;Rg Field instrument calibration procedures; and
Screening results (Refer to table provided in Section K.).
- Document soil sampling information (Refer to figures, tables, and appendices provided in Sections J,
K, and L.), including:
Lithological descriptions from logs for borings, excavations;
Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
Sample collection procedures (grab, split spoon, hand auger, etc.);
Location of soil samples;
Depth of soil samples ( feet below land surface);
Time/date collected;
Sample identification; and
Method(s) of soil sample analysis.
Document groundwater and surface water sampling information (Refer to figures, tables, and
appendices provided in Sections J, K, and L.), including:
7 Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature)
Initial Abatement Report 3 Harmon Environmental, PA
Griggs Property 05 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental com

Initial Abatement Action Report Appendix A
Report Formats
Sample collection procedures (grab, bailer, etc.);
Time/date collected.
Sample identification; and
Method(s) of water sample analysis.
Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L.), including:
-' Sample handling procedures including sample preservation techniques and sample transport
procedures;
' Decontamination procedures;
Time and date samples were submitted to lab; and
Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
Describe soil and groundwater investigation results, including:
Presentation of analytical results for soil and groundwater samples (Refer to table(s) provided in
Section K. and to appendix with laboratory analytical results provided in Section L.) and discussion of
the results in relation to the cleanup levels or action levels, as appropriate; and
Discussion pertaining to the effect of quality control sample results on the interpretation of soil,
groundwater, or surface water analytical results.
6. Present conclusions and recommendations, referencing maps and cross -sections in Section J, as follows:
Describe source and estimated extent of soil contamination (If there are multiple sources of release,
then describe the extent of contamination from each source);
Indicate if groundwater or bedrock was encountered during investigation and at what depth below land
surface;
Indicate if groundwater assessment was necessary due to the proximity of the UST system to
groundwater or bedrock (or to the presence of a slab or tank for which removal was determined to be
economically or technologically unfeasible), thereby preventing the reliable determination of a release
by soil assessment alone;
a Describe source(s) and estimated extent of any groundwater or surface water contamination;
c Describe source(s) and estimated thickness and extent of any free product;
c Indicate what initial response and abatement actions are required; and
s. 3 'Discuss the need for further investigation or remediation.
This section is not applicable. UST-lwas a non-commercial, non -regulated tank.
D. UST Closure Report following UST-12 Format) and Site Investigation Report for Permanent Closure or
Change -in -Service of UST (UST-2 Form) (if applicable).
Incorporate the minimum requirements of a UST Closure Report, as outlined in Appendix A, p.55, and
complete the UST-2 Form, found in Appendix A, p. 60 of the Guidelines), if UST closure indicated a release
and initiated the initial response and abatement action.
I. Describe preparations for closure including steps taken to notify authorities, permits obtained, and steps
taken to clean and purge the tanks.
2. Describe the closure procedure (For guidance; refer to the Guidelines, Section 5.), referencing site and
sampling location maps and cross -sections presented in Section J of this report. Clearly state how the
selection of sample types and locations was influenced by the nature of the stored substance, the type of
initial alarm or cause for suspicion; the type of backfill, the depth to groundwater, and other factors
appropriate for identifying the presence and source of a release. If presence of groundwater or bedrock
require the installation and sampling of monitoring well(s), describe the process.
3. Note the amount of residual material pumped from the tank and describe the storage, sampling and disposal
of the residual material and the disposal of the tank, pumps and piping (Refer to appendices with disposal
manifests and certificate of tank disposal in Section L.).
4. If a release is determined, document initial response actions (submittal of 24-Hour Release and Report
Form; repair, replacement, or upgrading of system to prevent further release; mitigation of hazards) and
initial abatement actions (free product removal; submittal of 20-Day Report) performed in Section G, Initial
Response and Abatement Actions.
5. Document any soil excavation activities in Section H, Excavation of Contaminated Soil;
6. Document site investigation.
1�1 Describe field screening, including:
Initial, Abatement Report 4 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
Physical characteristics of the soil samples; as observed during collection;
a Field instrumentation used to screen soils;
r-- Field instrument calibration procedures; and
Screening results (Refer to table provided in Section J.).
Document soil sampling information (Refer to figures; tables, and appendices provided in Sections J,
K and L.), including:
Lithological descriptions from logs for borings, excavations;
Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
$, Sample collection procedures (grab, split spoon, hand auger, etc.);
Location of soil samples;
m, Depth of soil samples ( feet below land surface);
Time/date collected;
Sample identification; and
Method(s) of soil sample analysis.
Document groundwater and surface water sampling information (Refer to figures, tables, and
appendices provided in Sections J, K, and L.), including:
Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
Field measurements (e.g., pH, dissolved oxygen, specific conductivity, ,temperature)
Sample collection procedures (grab, bailer, etc.);
Time/date collected.
Sample identification; and
Method(s) of water sample analysis.
Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L, including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
Decontamination procedures;
t : Time and date samples were submitted to lab; and
Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
Describe soil and groundwater investigation results, including:
1 Presentation of analytical results for soil and groundwater samples (Refer to table(s) provided in
Section K and to appendix with laboratory analytical results provided in Section L.) and discussion of
the results in relation to the cleanup levels or action levels, as appropriate; and
Discussion pertaining to the effect of quality control sample results on the interpretation of soil,
groundwater, or surface water analytical results.
Present conclusions and recommendations, referencing maps and cross -sections in Section J as follows:
Describe source and estimated extent of soil contamination, referencing maps and cross -sections in
Section J (If there are multiple sources of release, then describe the extent of contamination from each
source.);
Indicate if groundwater or bedrock was encountered during investigation and at what depth below land
surface;
Indicate if groundwater assessment was necessary due to the proximity of the UST system to
groundwater or bedrock (or to the presence of a slab or tank for which removal was determined to be
economically or technologically unfeasible), thereby preventing the reliable determination of a release
by soil assessment alone;
Describe source(s) and estimated extent of any groundwater or surface water contamination;
Describe source(s) and estimated thickness and extent of any free product;
„ffi1 Indicate what initial response and abatement actions are required; and
Discuss the need for further investigation or remediation.
This section is not anplicable. UST- 1 was a non-commercial, non -regulated tank.
E. Free Product investigation and Recovery Report (if applicable)
Discuss the status of free product at the site, as follows:
I . If free product is, or has been, present at the site, describe its current and historical status (product distribution,
thickness, recovery activities). Refer to tables in Section K: Table B-7, Monitoring and Remediation Well
Construction Information; and Table 13-8A, Free Product Recovery Information; Table 13-813, Cumulative Volume
Initial Abatement Report 5 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental. com

Initial Abatement Action Report Appendix A
Report Formats
of Free Product Recovered from Site; and Table B-9, Current and Historical Groundwater Elevations and Free
Product Thickness. Also refer to map(s) showing extent of free product in Section J;
2. Identify any on -site or off -site effluent discharges, treatment used, effluent quality, permitting actions taken, and
location of such discharges and identify the disposition of recovered free product ( refer to attached product
disposal manifests);
3. Document the performance, total cost, and cost per gallon to date of each method of free product recovery used at
site. Justify why the technology is or was used; and
4. Provide conclusions and recommendations concerning historical, current, and future recovery activities,
including:
Any proposal to change the current method of free product recovery to a better or more cost-effective
technology;
A justification for continued product recovery, if planned; and
E-, Any detennination that tree product has been eliminated from the site with a recommendation to reclassify
the risk posed by the release, if applicable.
This section is not applicable. No free -product was observed during the initial abatement process
F. Groundwater and Surface Water Investigation (if applicable)
1. If groundwater or bedrock was encountered in pits, trenches or shallow boring during site check, UST
system closure, or initial abatement investigation, if monitoring or water supply wells were found to be
contaminated, or if surface water is present nearby, then indicate actions taken to investigate suspected
contamination from a release (e.g., installation of monitoring wells, groundwater or surface sampling and
analysis).
2. Document groundwater investigation (or, if applicable, refer to groundwater investigations under Section
C, Site Check Report, or Section D, UST Closure Report), as follows:
�1 Present groundwater and surface water sampling information (Refer to tables and appendices provided
in Sections K and L.), including:
Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature)
a Sample collection procedures (grab, bailer, etc.);
Time/date collected.
Sample identification; and
Method(s) of water sample analysis.
Document quality -control measure information (Refer to tables and appendices provided in Sections K
and L), including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
r Decontamination procedures;
Time and date samples were submitted to lab; and
ca Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
Describe groundwater or surface water investigation results, including:
Presentation of analytical results (Refer to table(s) provided in Section K and to appendix with
laboratory analytical results provided in Section L.) and discussion of the results in relation to the
cleanup levels (groundwater quality or surface water quality standards); and
Discussion of the effect of quality control sample results on the interpretation of groundwater or
surface water analytical results.
This section is not applicable. Groundwater was not encountered during the initial abatement
process. _
G. Initial Response and Abatement Action
1. Describe initial response actions performed within 24 hours of discovery of the release, including:
.i Submittal of 24-Hour Release Report and UST Leak Reporting Form (UST-61);
Eenj Action to prevent further release and to determine source of the release;
Initial Abatement Report 6 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
o Identification and mitigation of hazards due to exposure to pollutants (e.g. Responsible party must
identify and sample water supply wells at risk of impact by the release and provide supply of alternate
water, if wells are impacted.); and
o Identification and mitigation of hazards due to fire, explosion, and vapor hazards.
On June 30, 2020 PGP Services. Inc. under the oversight of Harmon Environmental. PA
personnel, excavated approximately 44.98-tons of petroleum -impacted soil from the site. This soil
was transported to the Environmental Soil, Inc. permitted land application site for appropriate
disposal. Pollution hazards associated with former UST-1 were mitigated by removingpetroleum-
impacted soil associated with the former UST.
2. Describe initial abatement actions performed, including:
® Completion of investigation to confirm presence and determine source of the release;
o Investigation and recovery of free product;
© Continued mitigation and monitoring of fire, explosion, and vapor hazards;
o Remediation of hazards posed by exposed contaminated soil;
o Submittal of 20-Day Report summarizing the progress of the initial actions performed within the 20-
day period following discovery of the release; and
o Soil excavation activities (Document in Section H, Excavation of Contaminated soil.).
PGP Services. Inc. under the oversight of Harmon Environmental. PA personnel excavated
proximately 44.98-tons of petroleum -impacted soil from the site. This soil was transported to
the Environmental Soil, Inc. permitted land application site in Lattimore. North Carolina for
qppropriate disposal.
H. Excavation of Contaminated Soil
1. Describe source and estimated extent of soil contamination determined in initial investigations (e.g., site
check, UST system closure), referencing maps and cross -sections in Section J and tables presenting soil
sampling information and results in Section K (If there are multiple sources of release, then describe the
extent of contamination from each source.), including:
® Sampling location and depths; locations of tanks, piping dispensers, sumps, areas of staining (indicate
if above or below tank); utility lines; potential receptors; buildings; relationship of area(s) of
contaminated soil to groundwater and bedrock; and
o If part or all of UST system was removed, indicate dimensions of resulting pits and trenches.
This section is not applicable. UST-1 was a non-commercial, non -regulated tank.
2. Describe excavation process; referencing maps and cross -sections in Section J, tables presenting soil
sampling information and results in section K and disposal manifests and geological logs in Section J, as
follows:
Describe type of equipment used (e.g., back hoe, track hoe, dump truck);
Describe field screening, if used to determine limits of excavation, including:
® Physical characteristics of the soil samples, as observed during collection;
® Field in strum entation, used to screen soils;
© Field instrument calibration procedures;
© Screening results (Refer to table provided in Section K.);
© Indicate the final dimensions of the excavation(s);
© Indicate the volume (in cubic yards) and weight (in tons) of soil excavated from each excavation (show
calculations);
® Describe relationship of final excavation pit to former UST system, to groundwater, to bedrock, and to
structures; and
o Indicate if the excavation operation ceased on encountering clean soil, groundwater, or bedrock OR if
excavation ceased 5 feet from tank(s), dispenser(s), and/or piping and at a depth of 17 feet below land
surface.
The petroleum -impacted soil was excavated using a John Deere® 300G trackhoe operated by Mr.
Frank Gravely ofPGP Services. Inc. and loaded into tri-axle and quad -axle dump trucks operated
Initial Abatement Report 7 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
by TNT Trucking LLC for transport to the Environmental Soils, Inc. permitted land application
site in Lattimore. North Carolina for appropriate disposal. The final dimensions of the UST
excavation measured approximately 19 feet long by approximately 15 feet wide and up to 14.5 feet
deep. The excavation was terminated when clean native soil was encountered The total volume
of petroleum -impacted soil removed in conjunction with this Initial Abatement project was
approximately 44.98-tons. An additional 19-tons had reportedly been previously excavated from
the site by Geo-Hydro Engineers. Inc during the tank closure process. Based on the Soil Survey of
Mecklenburg County published by the USDA NRCS in 2018, the soil type associated with this
region of Mecklenburg County is Cecil sandy clay!oam (CeB2). The depth to bedrock, the depth
to groundwater and the groundwater flow direction at the site have not been determined
3. Describe post -excavation confirmation soil sampling , referencing maps and cross -sections in Section J,
tables presenting soil sampling information and results in Section K, and geological logs in Section L as
follows:
in Describe sample location and depth, and methods of collection and analysis for each excavation;
Note if multiple excavations were performed sequentially in an area of contaminated soil,, i.e., if
confirmatory sampling following primary excavation indicated that contaminated soil remained, so that
further excavation was performed and a second set of confirmatory samples was collected and
analyzed; and
-Ij If contaminated soil was allowed to remain after final excavation, indicate precisely the location and
depth of the residual contamination and explain why it was not removed, i.e., why it was not
economically and/or technologically feasible to excavate it
4. Document Soil Investigation.
c�D Provide soil sampling information for all samples collected following excavation and during previous
investigations. Refer to table provided in Section K: Table B-3, Summary of Soil Sampling Results; to
figures, in Section J; and to appendices, in Section L. Information should include
Lithological descriptions from logs for borings; excavations;
Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
Sample collection procedures (grab, split spoon, hand auger, etc.);
Location of soil samples;
Depth of soil samples ( feet below land surface);
Time/date collected;
Sample identification;
Indication of phase of sampling: , site check closure, IAA, etc.; and
Method(s) of soil sample analysis.
Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L.), including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
Decontamination procedures;
Time and date samples were submitted to lab; and
Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
Describe soil investigation results, including:
Presentation of analytical results for soil samples (Refer to table provided in Section K and to appendix
with laboratory analytical results provided in Section L.);
Discussion of the results inrelationto the appropriate cleanup levels, identifying the samples that
exceed the lower of:
(a) the residential'MSCCs or
(b) the soil -to -groundwater MSCCs.
Discussion of effect of quality control sample results on the interpretation of soil analytical results.
On April 24 2020 Geo-Hydro Engineers Inc removed a 500-gallon heating oil tank from the site.
In coniunction with this project approximately 19-tons of petroleum impacted soil was excavated
and transported to AES ofNorth Carolina a permitted soil treatment facility in Thomasville: North
Carolina Following- completion of the excavation activities Geo-Hydro Engineers Inc. collected
a soil sample1TP-1) from the base of the excavation and transported this sample to Pace
Anal,�tical Services LLC in Huntersville North Carolina for analysis. Upon receipt, the sample
Initial Abatement Report 8 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina28031 harmonenvironmental.com

Initial Abatement Action Report Appendix A
I.
Report Formats
was analyzed for Gasoline Range Organic (GRO) Compounds and Diesel Range Organic (DRO)
Compounds by SW-846 Method 8250C- Volatile Oceanic Compounds (VOCsLby SW-846 Method
8260D,• Volatile Petroleum Hydrocarbon (VPH) Compounds and Extractable Petroleum
Hydrocarbon (,PH Compounds by Massachusetts Methods. The analytical results associated
with this sample are summarized in the May 19, 2020 Underground Storage Tank Sxstem Closure
and Sampling Report. On June 30, 2020, PGP Services. Inc. removed an additional
approximately_44.98-tons of petroleum -impacted soil associated with a former 500-gallon heating
oil tank. In coniunction with the excavation activities eve con amatory soil samples NWO
EW(10), SW(IO),WWOO) and BOT I4.5) were collected by Harmon Environmental PA
personnel, from the base and side walls of the excavation at the locations depicted on Figure 3.
Soil sample NT IO) was collected from the north wall of the excavation at a depth of
approximately 10 feet below grade. Soil sample EWOO) was collected from the east of the
excavation at a depth of approximately 10 feet below grade. Soil sample SWOO) was collected
from the south wall of the excavation at a depth of approximately 10 het below grade. Soil
sample WWOO) was collected from the west wall o the excavation at a depth of approximately 10
feet below grade. Soil sample BOT(14.5) was collected from the base of the excavation at adept
of approximately 14.5 met below grade. These soil samples were analyzed by Pace Anal tical
Services. LLC of Huntersville, North Carolina. Soil samples NWOO), EW(10), SW(I0), WW(10)
and BOT(14.5) were analyzed for volatile organic compounds WOO) by SW-846 Method 8260D:
semi -volatile organic compounds (Semi-VOCs) in accordance with SW-846 Method 8270E BNIA
and, volatile petroleum hydrocarbon (VPU) compounds and extractable petroleum hydrocarbon
(EPH) compounds by Massachusetts Methods. A copy of the laboratory report is presented in
Appendix J and a copy of the Chain -of Custody Record is included in Appendix I. As indicated by
these results, anal sis of the base and side wall samples following completion of the excavation
activities did not indicate the presence of targeted compounds exceeding respective DEQ
established action levels.
5. Describe disposal of contaminated soil, referencing tables presenting soil sampling information and results
in Section K and disposal manifests in Section L as follows:
Indicate volume and weight of contaminated soil removed from each excavation at site;
n Describe construction of any stockpile of contaminated soil, describe collection and analysis of
stockpile samples;
Indicate if soil was treated onsite (Reference permit in Section L.);
c-:, Indicate if soil was transported offsite for disposal and, if so, by whom and to what destination; and
Confirm that excavation was back -filled with clean soil,
On June 30 2020 approximately 44.98 tons of petroleum -impacted soil was excavated from the
vicinity of former 500-gallon heating oil UST. As excavated, the impacted soil was loaded into
dump trucks and transported to the Environmental Soils Inc. Permitted land application site in
Lattimore North Carolina for appropriate disposal. A copy of the manifest is presented in
Appendix H. The excavation was backflled with clean soil from a local quarry.
6. Present conclusions, as follows;
Ei_n Briefly summarize excavation process;
Describe extent of final excavation(s) and collection of confirmatory samples;
Indicate if excavation ceased on encountering groundwater or bedrock; and
n Indicate whether soil contaminant levels in exceedance of the lowest MSCCs remain in the
excavation(s), further excavation being determined infeasible by the UST Section, or soil contaminant
levels in final excavation confirmatory soil samples were equal to below the lowest MSCCs
Conclusions
1. If soil contaminant levels in exceedance of the lowest MSCCs remain in the excavation(s) (further
excavation being determined infeasible by the UST Section), if groundwater or bedrock has been
encountered in proximity to contamination, or if free product is present, it should be concluded that a
Limited Site Assessment must be performed and a report submitted within 120 days of discovery of the
release; but
2. If soil contaminant levels in final excavation confirmatory soil samples were equal to or below the lowest
MSCCs and if groundwater, bedrock, and free product were not encountered in the excavation(s), then no
further action should be requested.
Initial Abatement Report 9 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe; North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
On April 24, 2020 Geo-H dy ro Engineers, Inc. removed a 500-gallon heating oil tank from the site.
In conjunction with this project approximately l9-tons of petroleum impacted soil was excavated
and transported to AES of North Carolina a permitted soil treatment facility in Thomasville, North
Carolina. Following completion of the excavation activities, Geo--Hydro Engineers Inc. collected
a soil sample (TP-1) from the base of the excavation and transported this sample to Pace
Analytical Services, LLC in Huntersville. North Carolina (or analysis. Upon recei t the sample
was analyzed for Gasoline Range Organic (GROI Compounds and Diesel Range Organic (DRO)
Compounds by SW-846 Method 825OC; Volatile Organic Compounds (VOCs) by SW-846 Method
826OD; Volatile Petroleum Hydrocarbon (VPH Compounds and Extractable Petroleum
Hydrocarbon (EPH) Compounds by Massachusetts Methods. The analytical results associated
with this sample are summarized in the May 19, 2020 Underground Storage Tank System Closure
and Sampling Report. On June 30, 2020, PGP Services. Inc. removed an additional
approximately 44.98-tons of petroleum -impacted soil associated with a former 500-gallon heating
oil tank. In conjunction with the excavation activities, five confirmatory soil samples NWOO),
EWOO), SWOO) WWOO) and BOT(14.5) were collected by Harmon Environmental, PA
personnel, from the base and side walls of the excavation at the locations depicted on Figure 3.
Soil sample NW(10) was collected from the north wall of the excavation at a depth of
approximately 10 feet below grade. Soil sample EWOO) was collected from the east of the
excavation at a depth of approximately IO feet below grade. Soil sample SW(10) was collected
from the south wall of the excavation at a depth of approximately 10 feet below grade. Soil
sample WWO0) was collected from the west wall of the excavation at a depth of approximately 10
feet below grade. Soil sample BOT(14.5) was collected from the base of the excavation at a depth
of approximately 14 5 feet below grade These soil samples were analyzed by Pace Anal ty ical
Services LLC of Huntersville, North Carolina. Soil samples NWOO , EW(10), SWf10), WE(10)
and BOT(14 5) were analyzed for volatile organic compounds (VOCs) by SW-846 Method 8260D;
semi -volatile organic compounds (Semi-VOCs) in accordance with SW-846 Method 8270E BNIA
and volatile petroleum hydrocarbon_(VPH) compounds and extractable petroleum hydrocarbon
(EPH) compounds by Massachusetts Methods. A copy of the laboratory report is presented in
Appendix J and a copy of the Chain -of -Custody Record is included in Appendix I As indicated by
these results analysis of the base and side wall samples following completion of the excavation
activities did not indicate the presence of targeted compounds exceeding respective DEQ
established action levels Based on the analytical data Harmon Environmental, PA recommends
the DEO Require no further assessment or remediation activities at this site.
J. Figures
Provide the following:
1, A topographic map illustrating the area within 1500-foot radius of the source of the release, showing:
Topographic contours;
Site location;
L Buildings;
Adjacent streets, roads, highways (identified by street names and numbers);
Surface water bodies;
Groundwater flow direction (if determined); and
North arrow and scale.
See Figure 1
2. A site map* and cross -sections illustrating the UST system(s)lexcavation area(s), drawn to scale, showing:
- Buildings and property boundaries;
Underground utilities, such as sewer lines and other conduits; basements; and vaults;
Water supply wells, surface water bodies
Location and orientation of current and former UST(s), pumps; product lines, sumps, etc.;
r Length, diameter and volume of current and former UST(s);
Type of material(s) stored in UST(s) (currently and formerly); and
Names or descriptions of properties adjacent to the site; and
North arrow and scale.
Initial Abatement Report 10 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental.com

Initial Abatement Action Report
Appendix A
Report Fonnats
Figure 2 presents a scaled drawing of the residence and property boundaries. Soil sample locations,
sample designations, sample depths and the final limits of the excavation are depicted on Figure 3. No
groundwater sampling activities were conducted in conjunction with this project. As a result, this
figure does not present groundwater monitoring locations or groundwater flow direction. The final
limits o the excavation, an approximate scale and a north arrow are presented on Figure 3.
Map(s)* and geological cross -sections, drawn to scale, depicting all soil analytical results obtained to date
and final confirmatory sample results, to include:
Description of soil and bedrock lithology (as determined by investigation to date);
d Location and orientation of UST(s), pumps, piping, sumps, ete.(current and former);
® Soil sample identification (unique letter and/or numerical code), location, and depth;
Soil sample analytical results;
Final limits of each stage of excavation for each excavation on site**; and
tip Two geological cross -sections, drawn across the contaminated area and intersecting at right angles,
showing the vertical distribution of the contaminants in the unsaturated zone. (Indicate vertical and
horizontal scale, orientation of each section, location of water table, soil types and lithology, all
borings and sample locations represented by the sections, and soil analytical results for each
represented sample, and show sections as labeled lines on the map.)
Figure 3 presents a scaled drawing of the area immediately surrounding the excavation. This
fore presents the locations, sample designations, depths and analytical results associated with
the soil samples collected during this excavation project. A north arrow and an approximate
scale are presented on this figure, No geologic cross -sections have been prepared in conjunction
with this protect. A description ofthe soil types encountered during this excavation is discussed in
response to Question B. S of this; form. A Geologic Log of the excavation is presented in Appendix
4. Map(s)* and geological cross -sections, drawn to scale, depicting the groundwater and surface water
analytical results,** to include;
Location and orientation ofUST(s), pumps, piping, sumps, etc.(current and former);
uE, Groundwater sample identification (unique letter and/or numerical code referencing monitoring or
water supply well)and location;
Surface water sample identification (unique letter and/or numerical code) and location; and
Groundwater and surface water sample analytical results.
No groundwater or surface water samples were collected in coniunction with this initial
abatement project.
5. A free product map* showing thickness (in feet) and extent of free product** using contour lines; and
No free product was observed during this initial abatement project.
6. A potential receptor map that clearly identifies water supply wells (municipal or public/private wells, etc.) and
other potential receptors (surface water bodies, basements, utilities, etc.) which are at risk.
*Note: If possible, use a single base map to prepare site plans using a map scale of 1 inch = 40 feet (or a
smaller scale for large sites, if necessary). Maps and figures should include conventional symbols, notations,
labeling, legends, scales, and north arrows and should conform to generally accepted practices of map
presentation such as those enumerated in the USES Geological Survey pamphlet, "Topographic Maps."
** If applicable
A receptor survey was not conducted in conjunction with this initial abatement project.
K. Tables
Provide the following:
1. Site History (Complete Tables B-1 and B-2 from Guidelines; Appendix B);
Initial Abatement Report 11 Harmon Environmental, PA
Griggs Property 615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
Tables B-1 and B-2 are attached.
2. Public and Private Water Supply Well and Other Receptor Information (Complete Table B-5 from
Guidelines, Appendix B);
A receptor survey was not conducted in conjunction with this initial abatement project.
3. Field Screening Results;
This table was not used in this project.
4. Summary of Soil Sampling Results (Complete Table B-3 from Guidelines, Appendix B);
See Table B-3 attached
5. Summary of Groundwater and Surface Water Sampling Results* ( Complete Table B-4 from Guidelines,
Appendix B)*;
This table is not applicable to this project.
6. Monitoring and Remediation Well Construction Information (Complete Table B-7 from Guidelines, Appendix
B)*;
This table is not applicable to this project.
7. Free Product Recovery Information (Complete Table B-BA from Guidelines, Appendix B)*;
This table is not applicable to this protect.
8. Cumulative Volume of Free Product Recovered from Site (Complete Table 13-813 from Guidelines, Appendix
B)*;
This table is not applicable to this project
9. Current and Historical Groundwater Elevations and Free Product Thickness (Complete Table B-9 from
Guidelines, Appendix B)*.
* If applicable
This table is not applicable to this project
L. Appendices
Provide the following:*
Appendix
Tightness testing results and supporting documentation*
Appendix B
Notification of Intent: UST Permanent Closure or Change -in -Service (UST-3 Form)
Appendix C
Site Investigation Report for Permanent Closure or Change -in -Service of UST (UST-2
Form)*
Appendix D
Site Specific Health and Safety Plan (HASP)
Appendix E
Certificate of UST disposal*
Appendix F
Groundwater field measurements (pH, dissolved oxygen, specific conductivity, temperature)*
Appendix G
Standard procedures (sampling, field equipment decontamination, field screening, etc.)
Appendix H
Soil, water, free product, and sludge disposal manifests and soil treatment permits*
Appendix I
Complete chain -of -custody records
Appendix J
Copy of all laboratory analytical records
Appendix K
Photographs of site check, closure, and excavation activities (optional)
Appendix L
Geologic logs for excavation(s)lborings (related to IAA investigation: only)
Appendix M
Monitoring Well Construction Forms (for all wells constructed to date)
* If applicable
Initial Abatement Report 12 Harmon Environmental, PA
Griggs Property
615 Bruce Thomas Road
18100 Statesville Road Monroe, North Carolina 28112
Cornelius, North Carolina 28031 harmonenvironmental.com

Figures

APPROXIMATE SCALE IN FEET
0 2000 4000
SOURCE: TOPO! 2003 NATIONAL GEOGRAPHIC
HARMON ENVIRONMENTAL, PA FIGURE 1
615 BRUCE THOMAS ROAD SITE LOCATION MAP
MONROE, NORTH CAROLINA GRIGG PROPERTY
704-292-4527 18100 STATESVILLE ROAD
HARMONENVIRONMENTAL.COM CORNELIUS, NORTH CAROLINA

i
1
V DRIVEWAY
-------------
0
GARAGE
'f
v, ` RESIDENCE
N
L
�O O
ya WATER SUPPLY WELL
` SHED
LEGEND
APPROXIMATE LOCATION OF
PROPERTY BOUNDARIES
APPROXIMATE LOCATION OF
RESIDENCES
APPROXIMATE LOCATION OF
PAVED AND GRAVEL SURFACES
9
-., APPROXIMATE LOCATION OF
`- -' FORMER UNDERGROUND
STORAGE TANK BASED ON GEO-HYDRO
ENGINEERS, INC. MAY 19. 2020 REPORT
APPROXIMATE BOUNDARY OF EXCAVATION
ACTIVITIES CONDUCTED BY GEO-HYDRO
- ENGINEERS, INC.
APPROXIMATE BOUNDARY OF JUNE 30, 2020 APPROXIMATE SCALE IN FEET
0 EXCAVATION
100 200
SOURCE: MECKLENBURG COUNTY POLARIS AND FIELD MEASUREMENTS
HARMON ENVIRONMENTAL, PA FIGURE 2
615 BRUCE THOMAS ROAD SITE LAYOUT MAP
MONROE, NORTH CAROLINA 28112 GRIGG PROPERTY
704-292-4527 18100 STATESVILLE ROAD
HARMONENVIRONMENTAL. COM CORNELIUS, NORTH CAROLINA

/ / / NW(10) BOT(14.5)
TOLUENE 0.016 MG/KG NO TARGETED COMPOUNDS
DETECTED AT CONCENTRATIONS
EXCEEDING THE RESPECTIVE
ANALYTICAL METHOD
DETECTION LIMIT
G LDRIVEWAY
GARAGE
NO TARGETED COMPOUNDS
EXCEEDING THE RESPECTIVE
DETECTION LIMIT
EW-(10)
DETECTED AT CONCENTRATIONS
ANALYTICAL METHOD
RESIDENCE
HARMON ENVIRONMENTAL, PA FIGURE 3
615 BRUCE THOMAS ROAD SITE LAYOUT MAP WITH ANALYTICAL RESULTS
MONROE, NORTH CAROLINA 28112 GRIGG PROPERTY
704-292-4527 18100 STATESVILLE ROAD
HARMON ENVIRONMENTAL.COM CORNELIUS, NORTH CAROLINA

Tables

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System Information
Revicinn T)nte• 7/16/?0?0 Tnnidnnt Nnmher and Nnme- 470RA/C7r14SXC Prnnerty
UST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank`
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
UST ***
Was release
associated
with the UST
System?
UST-1
Heating Oil
Heating
Oil
500
Gallons
Single
Wall Steel
Assumed
48 in by
65 in
Copper
Feed and
Return
Unknown
Removed
4/24/2020
Yes
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, eta, or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)

Table B-2: Site History - UST Owner and Operator Information
Kevision Uate: // 16/1UZU Incident Number and Name: 47089tGri2es Prone
UST ID Number
Facility ID Number
Name of Owner
Dates of Operation
(mm/dd/yy to mmldd/yy)
Street Address
City ,
State
Zip
Telephone Number
Name of Operator
Dates of Operation
(mm/dd/yy to mm/cid/yy)'
Unknown
Street Address
City
State
Zip
Telephone Number
Addadditional records as necessary

Table B-3: Summary of Soil Sampling Results
Revision Date: 7/16/2020 Incident Number and Name: 47089/Griggs Property
Analytical Method
8260D
8270E
VPH&EPH
VPH&EPH
Contaminant of Concern
o
E
v
v
E
O
� c
a�o�
L
c
° 0-0
L
V
v
o a
CL a, o a
Sample
Date
Source
Sample
Incident
°
v o
o
ID
Collected
Area
Depth
Phase
j
o = u
= u
�
W
NW(10)
6/30/2020
UST Basin
10 ft
Initial Abatement
0.016
No Targeted
Compounds
No Targeted
Compounds
No Targeted
Compounds
EW(10)
6/30/2020
UST Basin
10 ft
Intital Abatement
<0.0066
Detected
Above the
Detected
Above the
Detected
Above the
SW (10)
6/30/2020
UST Basin
10 ft
Initital Abatement
0.008
Respective
Method
Respective
Method
Respective
Method
VW(10)
6/30/2020
UST Basin
10 ft
Initial Abatement
0.0092
Detection
Limit
Detection
Limit
Detection
Limit
BOT(14.5)
6/30/2020
UST Basin
14.5 ft
Initial Abatement
<0.0063
Soil to Groundwater MSCC (mg/kg)
4.3
Residential MSCC (mg/kg)
1,200
Industrial/Commerical MSCC (mg/kg)
32,000
Notes: MSCC = Maximum Soil Contaminant Concentration
Sample Depth presented in feet below ground surface
Results presented in milligrams per kilogram (mg/kg)

Appendix A
Tightness Testing results and Supporting Documentation
(This Appendix is not applicable to this project)

Appendix B
Notification of Intent: UST Permanent Closure or
Change -in -Service (UST-3 Form)
(This Appendix is not applicable to this project)

Appendix C
Site Investigation Report for Permanent Closure
Or Change -in -Services of UST (UST-2 Form)
(This Appendix is not applicable to this project)

Appendix D
Site Specific Health and Safety Plan

Site Specific Health and Safety Plan
for
Soil Remediation Activities
At
18100 Statesville Road
Cornelius, North Carolina
June 23, 2020
Prepared By:
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, North Carolina 28112
704-292-4527
harmonenvironmental. com
This document is confidential and is to be used by designated project personnel. Reproduction of
this document is strictly prohibited unless approved in writing by Harmon Environmental, PA.

Plan Acceptance
I have been permitted the opportunity to read this Health and Safety Plan for Site Assessment
Activities at 18100 Statesville Road in Cornelius, North Carolina, and have been briefed by the Site
Safety Manager or an appropriately designated alternate on its content. All questions and comments
I have asked or stated regarding this Plan have been satisfactorily addressed. I understand the
contents of this Plan and agree to abide by its requirements.
Each person entering exclusion zones defined in Section 5.4 of this Plan shall sign below.
Signature Printed Name Compa,�.-n--y Date

Table of Contents
Section
Title
Page No.
1.0
General Information
1
2.0
Project Organization
2
3.0
Site Description
2
4.0
Site Safety Control
2
5.0
Hazard Assessment/Personnel Protection
3
6.0
Decontaminating Procedures
4
7.0
Emergency Procedures
4
Figure Site Layout Map
Appendix A Exposure Limits of Chemical Hazardous
Appendix B Route to Hospital

1.0 General Information
1.1 Site Safety Plan Preparation:
Plan Prepared By: R. Harmon
Date Plan Approved: June 23, 2020
1.2 Site Information:
Site Name: Griggs Estate
Site Location: 18100 Statesville Road, Cornelius, NC
Site Contact: None
Site Status: Open (X) Closed ( )
Limited Access O Fenced( )
Existing Site Information:
Detailed O Sketch ( )
Preliminary (X) None ( )
Facility EPA I.D. No.:N/A
1.3 Hazardous Materials Information:
State/Form of Hazardous Materials:
Gas ( ) Liquid O Soil (X)
Groundwater O Sludge O Solid( )
Material Hazards:
Corrosive O Volatile (X) Ignitable ( )
Toxic ( ) Reactive ( ) Explosive ( )
Radioactive O Unknown O Flammable ( )
1.4 Scope of Work:
Excavate petroleum -impacted soil originating from a former heating oil underground
storage tank. The excavated soil will be loaded directly onto trucks for transport to a
licensed disposal facility. Following completion of the excavation, soil samples will
be collected, and the excavation will be backfilled with clean soil imported from off -
site.
Health and Safety Plan 1 Harmon Environmental, PA
18100 Statesville Road 615 Bruce Thomas Road
Cornelius, NC Monroe, NC 28112
June 23, 2020 [phone]

2.0 Project Organization
Project Manager: Richard Harmon
Corporate Health and Safety Coordinator: Richard Harmon
Site Health and Safety Manager: Richard Harmon
Technical Support: PGP Services, Inc.
Harmon Environmental Project No. 848-01
3.0 Site Description
The site consists of a commercial property with a former heating oil underground storage tank.
4.0 Site Safety Controls
4.1 Site Map:
See attached figure
4.2 Perimeter Control:
No perimeter control is in place at the site.
4.3 Command Post Area:
The command post will be established outside of the exclusion zone at the subject
site. A telephone will be available at the command post area.
4.4 Exclusion Zones:
During the excavation activities, the exclusion zone shall be defined as a 15-foot
radius around the open excavation.
4.5 Decontamination Area:
Decontamination of the excavation equipment will be performed on -site.
5.0 Hazard Assessment/Personnel Protection
5.1 General
Primary routes of potential exposure are through inhalation of dust, ingestion, and
skin contact with impacted soil and/or groundwater. Hazards include the physical
hazard associated with excavation, drilling and well advancement activities. Due to
the outdoor location of the project and expected hazards, moderate health risks are
anticipated.
Health and Safety Plan 2 Harmon Environmental, PA
18100 Statesville Road 615 Bruce Thomas Road
Cornelius, NC Monroe, NC 28112
June 23, 2020 [phone]

5.2 Health and Safety Training Requirements
All field personnel (including Subcontractors) must have appropriate hazardous
waste site health and safety training in accordance with OSHA 1910.120 regulations
prior to initiating on -site activities. The Site Safety Manager must have an additional
8 hours of specific site management training.
5.3 Personnel Protection
General Level of Protection:
A ( ) S ( ) C ( ) D modified ( ) D (X)
Level D:
For all personnel participating in the excavation and sampling activities, the
following equipment is required as a minimum:
• Chemical resistant outer gloves
• Steel toe and shank boots
• Standard work clothing (long -sleeve shirt and long pants)
• Hard hat and safety glasses.
• Ear protection (when noise levels preclude normal conversation)
5.4 Upgrading and Downgrading of Personnel Protection:
Upgrading and downgrading of personnel protection levels will be implemented if
deemed necessary by the Site Safety Manager. Any upgrades will be based on
observed site conditions. Under no circumstances will downgrading be permitted by
any field personnel without the consent of the Site Safety Manager.
6.0 Decontamination Procedures
• Boots, boot covers, and gloves will be cleaned with phosphate -free soap and tap
water.
• Disposable coverings and equipment will be cleaned with phosphate -free soap and
tap water, then disposed of as normal trash.
• Sampling equipment will be cleaned with phosphate -free soap, and tap water,
followed by a distilled water rinse.
Health and Safety Plan 3 Harmon Environmental, PA
18100 Statesville Road 615 Bruce Thomas Road
Cornelius, NC Monroe, NC 28112
June 23, 2020 [phone]

7.0 Emergency Procedure
7.1 Field Communications:
Thumbs up
Thumbs Down
Hands on wrist
Hands on Throat
Hand signals when distressed; working in noisy
environment; or wearing respirators.
OK
Not OK
Exit Exclusion Zone
Cannot Breath
7.2 In the Event of Personnel Exposure:
Skin Contact: Flush with water, remove impacted clothing. Secure Medical
Attention
Inhalation: Move person away from exclusion zone, administer first aid and CPR
as necessary. Secure medical attention.
Ingestion: Secure medical attention.
Eye Contact: Irrigate with water. Secure medical attention.
7.3 Personnel Injury:
In the event a personnel injury occurs, decontaminate individual if injury is not life
threatening. If decontamination is not feasible, wrap the victim in a blanket,
administer first aid or CPR as necessary, contact the local rescue squad, and hospital.
All injuries, exposures, or spills are to be documented by the Site Safety Manager
and reported to the Project Manager within 24 hours. Such documentation is to be
kept on file at Harmon Environmental, PA for future reference.
7.4 Heat Stress:
In the event of heat stress, move the victim out of the heat to a cool area on site.
Place the victim in shock position with their feet elevated. Cool the victim by
spraying with water or using wet towels and fanning. Secure medical attention.
Health and Safety Plan 4 Harmon Environmental, PA
18100 Statesville Road 615 Bruce Thomas Road
Cornelius, NC Monroe, NC 28112
June 23, 2020 [phone]

7.5 First Aid Equipment:
A first aid kit is located within the support vehicles on -site. Potable water is
available on -site.
7.6 Route to Hospital
See Appendix B
7.7 Emergency Information:
Service Phone
Ambulance 911
Fire Department 911
Police 911
Hospital (Lake Norman Regional Medical Center) [phone]
Charlotte Poison Control [phone]
North Carolina Department of Environment, [phone]
Health and Natural Resources
Region IV EPA [phone]
PGP Services, Inc. [phone]
Harmon Environmental, PA [phone]
848-0 I.H&S
Health and Safely Plan 5 Harmon Environmental, PA
18100 Statesville Road 615 Bruce Thomas Road
Cornelius, NC Monroe, NC28112
June 23, 2020 [phone]

Figures

6/23/2020 _ags_df24eb65de194e16adb3lfff01ecddf8.png(1520x969)
polaris3g.mecklenburgcountync.gov/polarisv/rest/directories/arcgisoutputIPrintlExportWebMap_GPServer/_ags_df24eb65de194e16adb31 fff01 ecddf8.... 1 /1

Appendix A
Exposure Limits of Chemical Hazards

*­"l 14 Ili __ lf.il 47Li.L I' U I.;,L, I N V. 4- - L1LtJ.LL
CONOCO -- DIESEL FUEL NO. 2 - DIESEL FUEL
MATERIAL SAFETY DATA SHEET
NSN: 9140002865296
Manufacturer's CAGE: 15445
Part No. Indicator: A
Part Number/Trade Name: DIESEL FUEL NO. 2
General Information
Item Name; DIESEL FUEL
Company's Name: CONOCO INC
Company's Street: 600 N DAIRY ASHFORD RD RM 3012
Company's P. O. Box: 4784
Company's City: HOUSTON
Company's State: TX
Company's Country: US
Company's Zip Code: 77210-4784
Company's Emerg Ph #: 713-293-5550/800-424-9300
Company's Info Ph #: 713-293-5550
Record No. For Safety Entry: 029
Tot Safety Entries This Stk#: 093
Status: SMU
Date MSDS Prepared: 14AUG91
Safety Data Review Date: 24JUN92
Supply Item Manager: KY
MSDS Serial Number: BMZTT
Specification Number: VV-F-800
Spec Type, Grade, Class: GRADE DF-2
Hazard Characteristic Code: F4
Ingredients/identity Information
Proprietary: NO
Ingredient: PETROLEUM MID -DISTILLATE (DIESEL MARINE FUEL)
Ingredient Sequence Number: 01
Percent: 100 %
NIOSH (RTECS) Number: 1004302PE
CAS Number: 68476-34-6
OSHA PEL: 5 MG/M3 AS OIL MIST
ACGIH TLV: 5 MG/M3 AS OIL MIST
Other Recommended Limit: NONE SPECIFIED
Physical/Chemical Characteristics
Appearance And Odor: CLEAR OR LIGHT YELLOW LIQUID, AROMATIC ODOR
Boiling Point: 350 - 68OF
Melting Point: NOT GIVEN
Vapor Pressure (MM Hg/70 F): 1 MMHG
Vapor Density (Air=l): > 1
Specific Gravity: 0.85 - 0.93
Decomposition Temperature: NOT GIVEN
Evaporation Rate And Ref: NIL
Solubility In Water: INSOLUBLE
Percent Volatiles By Volume: NIL
Corrosion Rate (IPY): UNKNOWN
Fire and Explosion Hazard Data
Flash Point: 130F,54C
Flash Point Method: TCC
http://msds.pdc.carrell.edu/msds/siri/msds/h/gI 94/q436.html 10

Lower Explosive Limit: 0.4
Upper Explosive Limit: 6 %
Extinguishing Media: WATER SPRAY, FOAM, DRY CHEMICAL CAARBON DIOXIDE
Special Fire Fighting Proc: USE WATER TO KEEP FIRE -EXPOSED CONTAINERS
COOL. IF LEAK OR SPILL HAS NOT IGNITIED, USE WATER SPRAY TO DISPERSE THE
VAPORS AND TO PROVIDE PROTECTION.
Unusual Fire And Expl Hazrds: PRODUCTS OF COMBUSTION MAY CONTAIN CARBON
MONOXIDE, CARBON DIOXIDE AND OTHER TOXIC MATERILS. DO NOT ENTER ENCLOSED OR
CONFINED SPACE WITHOUT PROPER PPE.
Reactivity Data
Stability: YES
Cond To Avoid (Stability): AVOID HEAT AND FLAME
Materials To Avoid: INCOMATIBLE WITH OXIDIZING MATERIALS.
Health Hazard Data
Precautions for Safe Handling and Use
Control Measures
Transportation Data
Disposal Data
Label Data
Label. Required: YES
Technical Review Date: 24JUN92
MFR Label Number: NONE
Label Status: G
Common Name: DIESEL FUEL NO. 2
Chronic Hazard: NO
Signal Word: CAUTION!
Acute Health Hazard -Slight: X
Contact Hazard -Slight: X
Fire Hazard -Slight: X
Reactivity Hazard -None: X
Special Hazard Precautions: STORE IN WELL VENTILATED AREEA. KEEP CONTAINER
TIGHTLY CLOSED. STORE IN ACCORDANCE WITH NATIONAL FIRE PROTECTION ASSN
REGULATIONS. FIRST AID: INHALATION: REMOVE TO FRESH AIR. IF NOT BREATHING,
GIVE ARTIFICIAL RESPIRATION. IF BREATHING IS DIFFICULT, GIVE OXYGEN. CALL A
PHYSICIAN. SKIN: FLUSH SKIN WITH WATER AFTER CONTACT. REMOVE CONTAMINATED
CLOTHING. EYES: IMMEDIATELY FLUSH WITH WATER FOR 15 MINUTES. CALL A
PHYSICIAN. INGESTION: DO NOT INDUCE VOMITING. IMMEDIATELY GIVE TWO GLASSES
OF WATER, NEVER GIVE ANYTHING TO IF UNCONCIOUS. CALL MD
Protect Eye: Y
Protect Skin: Y
Label Name: CONOCO INC
Label Street: 600 N DAIRY ASHFORD RD RM 3012
Label P.O. Box: 4784
Label City: HOUSTON
Label State: TX
Label Zip Code: 77210-4784
http://msds.pdc.comell.edu/msds/siri/msds/h/q 194/g436.html 10/14/2001

rage j of 3
Label Country: US
Label Emergency Number: 713-293-5550/800-424-9300
ip://msds.pdc.comell.edu/msds/siri/msds/h/ql94/q436.htmi 10/14/2001

Appendix B
Route to Hospital

6/23/2020 18100 Statesville Rd, Cornelius, NC 28031 to Lake Norman Regional Medical Center - Google Maps
Go gle Maps 18100 Statesville Rd, Cornelius, NC 28031 to Lake Drive 7.3 miles, 11 min
Norman Regional Medical Center
fremax
p
weN!
rs �t c
r�
- Ownnrenswe.een,w
Le Notnue Reo-,
N M<tl timer
14
CWep.
r
o
!etlen Pear, x
CewA ;r i`,J
i binooa,.h..xi.Rwa
Go gle c
18100 Statesville Rd
ornehus, NC ' 8U3
Get on 1-77 N/US-21 N in Cornelius
4 min (2 0 mi)
t 1. Head north on US-21 N/Statesville Rd toward
Westmoreland Rd
1.7 mi
2. Use the middle lane to turn left onto Catawba Ave
279 ft
3. Use the right lane to merge onto 1-77 N/US-21 N
via the ramp to Statesville
0.2 mi
Follow 1-77 N to US-21 N in Davidson. Take exit 33 from 1-77
N/US-21 N
5 min (4.7 mi)
4. Merge onto 1-77 N/US-21 N
4.5 mi
5. Take exit 33 for US-21 N toward Lake Norman
0.2 mi
r,YWF�
�.rwau �Rrver Al�^CeumryCM!
Map data 02020 1 mi
Take Fairview Rd to your destination in Mooresville
https://www.google.com/maps/dir/18100+Statesville+Rd,+Cornelius,+NC+28031 /Lake+Norman+Regional+Medical+Center,+171 +Fairview+Rd,+Moor... 1 /2

6/23/2020 18100 Statesville Rd, Cornelius, INC 28031 to Lake Norman Regional Medical Center - Google Maps
N 6. Use the right lane to turn right onto US-' i Ivin (0.7 mi)
200 ft
r' 7. Turn right onto Fairview Rd
+1 8. Turn left
r' 9. Turn right
41 10. Turn left
40 Destination will be on the left
Lake Norman Regional Medical Center
171 Fairview Rd, Mooresville, NC 28117
These directions are for planning purposes only.
You may find that construction projects, traffic,
weather, or other events may cause conditions to
differ from the map results, and you should plan
your route accordingly. You must obey all signs or
notices regarding your route.
0.5 mi
446 ft
56 ft
236 ft
https://www.google.com/maps/dir/l 8100+Statesville+Rd,+Cornelius,+NC+28031 /Lake+Norman+Regional+Medical+Center,+171 +Fairview+Rd,+Moor... 2/2

Appendix E
Certification of UST Disposal
(Tank Removed and Disposed by Geo-Hydro Engineers, Inc. See May 19, 20

Appendix F
Groundwater Field Measurements
(This Appendix is not applicable to this project)

Appendix G
Standard Procedures

Standard Procedures
Soil Sampling in Conjunction with UST Removal
For safety reasons, soil samples associated with UST closures are typically collected
using the bucket of the excavator as the sampling equipment. To accomplish this task,
Harmon Environmental, PA sampling personnel direct the excavation contractor to
extract a sample from a pre -defined location on the base or side -wall of the excavation.
This soil sample is then brought to the surface of the ground and staged at a safe location
for screening and sampling.
Typically a sample aliquot is collected from the bucket of the excavation equipment and
placed directly into a zipper seal bag for field screening with a Multi -Rae® photoionizing
organic vapor detector (PID), or equivalent, calibrated to an isobutylene standard. New
latex gloves, or equivalent, are worn throughout the collection of the screening sample.
Each zipper seal bag is labeled with a sample designation, time, date, approximate depth
and sampler's initials at the time of collected.
Based on the results of the field screening activities, Harmon Environmental, PA field
personnel may opt to collect a sample aliquot from the excavator bucket for laboratory
analyses. Prior to collecting a sample, new latex gloves, or equivalent, are donned, and
the laboratory supplied sample bottles are labeled. Each soil sample is then collected
directly from the excavator bucket and placed directly into the pre -labeled glassware
provided by the laboratory. These samples are then placed in a cooler on ice pending
delivery under chain -of -custody protocol to the analyzing laboratory.
The depth of each sample, the location of each sample, the time of sample collection, the
field screening results and any deviations from these standard protocols are documented
in the field notes prepared in conjunction with each project.

Appendix H
Soil, Water, Free -Product and Sludge Disposal Manifests
And Soil Treatment Permits

P.O. BOX 295
ENVIRONMENTAL SOILS, INC. LATTIMORE, N.C. 28089
704-434-0075
NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL
APPROVAL # MANIFEST #
LOCATION OF SOIL:
TRANSPORTER: _
TIME: _ -__ __
TRUCK #
DATE: -_ _
_ LICENSE #
DRIVER SIGNATURE
TIME: ___
TRUCK #
DATE: __
LICENSE #
DRIVER SIGNATURE
TIME:
TRUCK #. _
DATE: _ _
LICENSE # _
DRIVER SIGNATURE
TIME: _. _
_ TRUCK #
DATE:
___ _ LICENSE #
DRIVER SIGNATURE
INSPECTED & ACCEPTED BY ENVIRONMENTAL SOILS, INC.
SUPERVISOR'S SIGNATURE _
GROSS WT,
LBS
TARE WT. _
LBS
NET WT.
_ LBS
GROSS WT.
LBS.
TARE WT.._
LBS,
NET WT.
LBS.
GROSS WT.
LBS.
TARE WT.
LBS.
NET WT.
_ LBS.
_ GROSS WT.
_LBS.
TARE WT. _
_ LBS.
NET WT.
LBS.
TOTAL NET WT.
TOTAL EOUIV-TONS

So' Env' Ils Inc.
110 B%x 295 - Litt;niure, NC 28089
Fx� 704-134-9533
Non-Ha7,,,mlous Wasic N,lanlfest #
[)are Load 'Nurnber
Li'ATIRONMEATT.41, CONSULTWNT
Contact.
GEWERLITOR:
Address: e
(111.11111-)Md sequentially as trucks are dispatched)
111-ionc. ICA ?U�t 4
Count-v:
Contact: 621�-k r ---- I �L'6� I.-,--.-- Phonc:
J+WSTE OR1GLN74TJ0A`P0JA1T Complete AMress: IaLqq—�
(Zj
2-4
Class & Type of Contain',11,11c ill S011
SOURCE OFCOA7Z1J1Lv117(iN,';(ex. [IS'F oi othersOurce) 0,
GE NE, R11TOR S CERTIF M11 TION OP J,1//1STE C 0,NSTITUENTS., fit lien of si i bn i itt ing a naCytical data (in ethods
5240aced S270),,.,ei--ifj,i7ki,thtittht,,u,tiste in fj it est lon does not co n1a !it orga it ic constituents othei- than those which would
11007.1ally appear in analysis of-,-it-giiipet)-oleiioiib-t,otlttct)-ccidite, lan? submitting this Cei-tifirate offflaste
Constiments. I certify that I i(nifitinitim- with the source oft-ontumbuttion of the so;1,rrndj1trther certify the sort7*ce, to
the best of -my knowledge, ronutins no contuin ina tits other thrift thitt limed above,
TMAISPORTER: 41"
Contact: Phone.-
'
As the carrier., I describcd al ovc heing shipped under this non-ha7ardous materials
manifest are properly chissified, packaged, hibelcd. sectired. :irid are: 11) proper Condition for transport in commerce
under the applicable regulations, go-t-ci-nin, tronsportarion, <Md I hL1-ChV1VCCiVC ibis m,)terlal for delivery tee the
1,11611ty, designate.
Carrier Signature: Zi& Date:
qqq
16 1p�
TRUCK # TAG VOLUM
TRUCK DRIVER S1 GNATT TRE DATE:
DESTIMITIOX- Envlr�-roncntd Sc ll< In 910 CroOrd, Rd, Slid bv, NC 281 50 Dedicated Land Applicat' 1011
Site Pcriiii, 4SR030003S,
I certify that the carrier has ddivVI-c(l (lie nlateriall; decz�Vlbcd abovv to rhl,-z facility, and I hereby accept this materi-,d
for treitmentand/or dlsl)(,,.sal in -A MIMII-Ik!,I"
thAT left 't"C011 WM1'FWA7t:d lW111C Sale OfNorfli
Carolina.
FacilitySignature: --
Date:
-JP-20
CoTitle:
rripam ?lame I - , 1. — . 1--1---.—,,-- , - )iaz

Flnviron rilent"ll Soil,, I 11C.
PO lily l 29�� NNC 2S,089
'I -
Pholic 4._uO7? - Fxi 704-4`4-9533
Non- T-Lc/ ar, lous Waste 1\11 III fe,';T #
Date LoadNurnber— 4.,
(numbered sequentiolly as truck, are dispatched)
ENVIR ON3 IE NTYL C 0 AIS UL T111,VT 1_tt: 4
Contact: Phone, U,2, 'i
GEATEP-4TOR-
Address: vi I _,I *_4 0 )Zs'l tV- Gu
F
Ccare nw.
Contact: 13 11 ��' 1: Phone:
14,'.dSTE OR1GV\WTJ0jVPOJjVT- Complete ;kddress: /,ffi
Class &Tvpc of Conumi.nawin suii
SOURCE OFCOA'L'J,1JJjV,-1T1OX- (ex, 1,1ST 01 Othel' SOUrce)
GITIVER11TORS CF-R7'11--J(,'.IITIOA,'01,'Jf,',IS7"]: CONSTITUENTS. -In Hen of submitting analytical data (nietbods
8240 and 8270)7ierirying that the waste in ynest ion does not contain organic constit itents other than those which would
normally appear in analysis of virgin petroleum product residue, I ani snbmitting this Certiricate of ff"aste
C o nst iti i en ts. J ce a �f 3, that I uniftinifiar -with the sow -re fcontaminallon oftbesoil tmdfiirther rert�, thesource, to
the best ofin), knowledge, contains its no cantann I neints other than that listed above.
77?AtAISPORTER: TP_7
Contact:
Phone -
As the carrier, I certiT - that the roatcrials de4crlbed abovc being shipped under this non -hazardous materials
Manifest are properh" cl:issificd, packaged, labeled-suctired, mid :trey in proper condition ior transport in commerce
under the applicable rerLIlatj()j» 1'eriling trall."Tortation, and I licreby receive :his material for o'cliveryto the
facility dcsignatc.
Carrier Signature: Date:
�
TRUCK #: —I NTJ O�5 V 0 L U1\ I E
TRUCK DRIVER SJ GMATT JRE: DATE;
DESPYWITION- Envlronn,eii-tal Soils Inc, 910 Crowdy Rd, Shclb,v, NC 2SI 50 Dedicated Land Application
Sitc PCI-1111t #SRO-)000,38
I ccrti�, that the carrier has dcIlvered the materials described :trove to tl)l,- facifin% and I hereby accept this material
for treatment and/or disposal in I Inanner Ih-.11 has becil aurlionzcd by flic Satc (it -North Carolina.
Facility Signature: Date:
Si(rnature: Date:
Z'�
Company Name Title-
White/Faci)lty canary/Invoice Goldenrod/Generator Pink/Carrier

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fm 704-434-9533
Non -Hazardous Waste Manifest #
Date Load Number
(numbered sequentially as trucks are dispatched)
EAWRON,11EATT-4L CDr'VSULT�INT � ►e`a - �► cM,^tiw to `i
s
Contact: Cam* u_1 Phone: —i UtZ g57-4 _ Fay::
GEATER11TOR. _
Address: 5z-z
Count:
Contact: (3CtK (, LbOt v Phone:
MYSTE ORIGLVATIONPOINT Complete .Address: 10 gG 51476:5yit.A­155
/,fG , 2 a o3 I
n
Class cS- Tv c of Contaminate in soil
SOURCE OFCONT jW.1NWTIOX- (eat. UST or other source) Q'L- U1.1
GERTER.4TORS CERTI.I ICATION OFWASTE CONSTITUENTS: In lieu ofsubinitting analytical data (methods
8240 and 8270) verifying that the waste in question sloes not contain organic constituents other than those which would
norrnally appear in analysis of virgi?:petrolezrrnpro duct a esidice, Iani subnzitting this Ce i -tifi cate of Raste
Constituents. I certify that ant familiar with the source of contain inatio n of the soil and further certify the source, to
the Crest ofnay knowledge, contains no contaminants other than that listed above.
TRr;INSPORTER:
.�r Contact: Phone: , �,
As the carrier, I certi6r that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate. Z
Carrier Signature; _` - ' Date:
t� 61.E
r
TRUCK #: �.... f TAG #: VOLUTME: I 9b t
TRUCK DRIVER SIGNATURE DATA: c i.t''
,DESTINWTION . Environmental Soils Inc. 910 Cro-vvdy Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature: -��4 � Date: 1 t - 10
Signature: , Date: 1-f L2
Company Name, Title:
White/Facility Canary/Invoice Goldenrod/Generator Pink/Carrier

ENVIRONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE, N.C. 28089-0489
704/434-0075
[phone] FAX
Job Name:
Truck#
Gross Wgt.:
Tare Wgt:
Net Wgt.:
Tons:
ENVIRONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE, N.C. 28089-0489
704/434-0075
[phone] FAX
Job Name:
Truck#
Gross Wgt.:
Tare Wgt:
Net Wgt.:
Tons:
Weighed by: Weighed by:

ENVIRONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE, N.C. 28089-0489
704/434-0075
[phone] FAX
Job Name:
Truck#
Gross Wgt.:
Tare Wgt:
Net Wgt.:
Tons:
ENVIRONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE, N.C. 28089-0489
704/434-0075
[phone] FAX
Job Name:
Truck#
Gross Wgt.:
Tare Wgt:
Net Wgt.:
Tons:
Weighed by: Weighed by:

ENVIRONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE, N.C. 28089-0489
704/434-0075
[phone] FAX
Job Name:
Truck#
Gross Wgt.:
Tare Wgt:
Net Wgt.:
Tons:
Weighed by:

Appendix I
Completed Chain -of -Custody Records

i
PaceAnalytical
www.pacclahs.com
Section A
Required Client Information
CHAIN -OF -CUSTODY J Analytical Request Document
The Chain-of-Cuslody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Section C
Required Project Information. lnveice In I.— irlo
ompan�
Report ToW
Attenh
Addres-.
Copy To:
C any Name
Ad
C+
Email�/� t
Purchase Order No.. C•
Pace Qeow
Phppppe. �� Fax:
Project Name
r r[�}�1.✓C ^,i'J
Paco Project
Manager.
Requested Due DatefTAT:
Project Number.
Pace Profile #:
_
REGULATORY A
` NPDES
lP UST
Site Location
STATE:
Requested Analysis Filtered I
Section D Matrix Codes
s'
z
Requirod Cl "I lnl„nnnlioi� MATRIX I CODF
d
COLLECTED
Preservatives
>
Drinking Water DW
QU
Water WT
Waste Water WW
$
++
�j
m
GOSIat;�i'F
COMPOSITE
Product P
"'"i�
LNn,(:Rt 1i
W
Solusolltl SL
.N
SAMPLE ID Oil OL
_
0
w
CZ
pe
(A-Z. 0-9 Air AR
WO
w
¢
a
d
E—
Sample IDs MUST BE UNIQUE Tissue TS
O
a.
w
Q
r
m
rn
t
Other OT
U
x
w
w
Z
:
2to
a)
O
c
to
Q
o
p
=
O
cn
t
c
d
`1
~
a
O
n
r
L
\
N
DATE
TIME
DATE
TIME
N
__=
Z
Z
2
/
f
r
1
sC.,may
Y
y:
x
Y
�r
ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY / AFFILIATION DATE TI
✓ fj� t i!
SAMPLER NAME AND SIGNATURE _
PRINT Name of SAMPLER:
SIGNATURE of SAMPLDATE Signed
¢'"�;l'//'-/,-i r ^t��_ (MM/DD/YY):
'Impon:lnt Nnte. By .-gnnxj This loan you are aceophng Pace's NET 30 day paynwnt terms and ayremnq to late charges of 1.5"L per month for any mvo�ces not paid within 30 days

Appendix J
Analytical Results

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 10, 2020
Mr. Rick Harmon
Harmon Environmental
615 Bruce Thomas Road
Monroe, NC 28112
RE: Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Dear Mr. Harmon:
Enclosed are the analytical results for sample(s) received by the laboratory on July 01, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
1(704)875-9092
HORIZON Database Administrator
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 54

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A21-A 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
18100 STATESVILLE RD
92484342
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92484342001
NW (10)
MADEP EPH
BAJ
6
PASI-C
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
92484342002
EW (10)
MADEP EPH
BAJ
6
PASI-C
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
92484342003
SW (10)
MADEP EPH
BAJ
6
PASI-C
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
92484342004
WW (10)
MADEP EPH
BAJ
6
PASI-C
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
92484342005
BOT (14.5)
MADEP EPH
BAJ
6
PASI-C
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 54

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SUMMARY OF DETECTION
Project:
Pace Project No.:
18100 STATESVILLE RD
92484342
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92484342001
NW (10)
EPA 8260D
Toluene
16.0
ug/kg
7.3
07/06/20 17:28
ASTM D2974-87
Percent Moisture
20.7
%
0.10
07/01/20 17:42
SM 2540G
Total Solids
79.9
%
07/09/20 14:17
92484342002
EW (10)
ASTM D2974-87
Percent Moisture
26.3
%
0.10
07/01/20 17:42
SM 2540G
Total Solids
79.5
%
07/09/20 14:17
92484342003
SW (10)
EPA 8260D
Toluene
8.0
ug/kg
7.8
07/06/20 18:05
ASTM D2974-87
Percent Moisture
24.4
%
0.10
07/01/20 17:42
SM 2540G
Total Solids
76.7
%
07/09/20 14:17
92484342004
WW (10)
EPA 8260D
Toluene
9.2
ug/kg
6.3
07/06/20 18:23
ASTM D2974-87
Percent Moisture
22.9
%
0.10
07/01/20 17:42
SM 2540G
Total Solids
78.4
%
07/09/20 14:17
92484342005
BOT (14.5)
ASTM D2974-87
Percent Moisture
21.5
%
0.10
07/01/20 17:42
SM 2540G
Total Solids
79.4
%
07/09/20 14:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 54

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Method: MADEP EPH
Description: MADEP EPH NC Soil
Client: Harmon Environmental
Date: July 10, 2020
General Information:
5 samples were analyzed for MADEP EPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 54

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[phone]
PROJECT NARRATIVE
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Method: MADEP VPH
Description: MADEPV
Client: Harmon Environmental
Date: July 10, 2020
General Information:
5 samples were analyzed for MADEP VPH by Pace National Mt. Juliet. All samples were received in acceptable condition with any
exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this
report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Method: EPA 8270E
Description: 8270E MSSV Microwave
Client: Harmon Environmental
Date: July 10, 2020
General Information:
5 samples were analyzed for EPA 8270E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 551267
v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated
samples may have low bias.
• LCS (Lab ID: 2930329)
• 2,6-Dinitrotoluene
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 551267
L2: Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples
may be biased low.
• LCS (Lab ID: 2930329)
• 2,6-Dinitrotoluene
• Fluoranthene
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 54

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Huntersville, NC 28078
[phone]
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Method: EPA 8270E
Description: 8270E MSSV Microwave
Client: Harmon Environmental
Date: July 10, 2020
Additional Comments:
PROJECT NARRATIVE
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Method: EPA 8260D
Description: 8260D/5035A/5030B Volatiles
Client: Harmon Environmental
Date: July 10, 2020
General Information:
5 samples were analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A/5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 551292
v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated
samples and the sensitivity of the instrument was verified with a reporting limit check standard.
• BLANK (Lab ID: 2930605)
• 1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
• Bromomethane
• n-Butylbenzene
• p-Isopropyltoluene
• BOT (14.5) (Lab ID: 92484342005)
• 1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
• Bromomethane
• n-Butylbenzene
• p-Isopropyltoluene
• DUP (Lab ID: 2932154)
• 1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
• Bromomethane
• p-Isopropyltoluene
• EW (10) (Lab ID: 92484342002)
• 1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
• Bromomethane
• n-Butylbenzene
• p-Isopropyltoluene
• NW (10) (Lab ID: 92484342001)
• 1,2,3-Trichlorobenzene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Method: EPA 8260D
Description: 8260D/5035A/5030B Volatiles
Client: Harmon Environmental
Date: July 10, 2020
QC Batch: 551292
v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated
samples and the sensitivity of the instrument was verified with a reporting limit check standard.
• 1,2,4-Trichlorobenzene
• Bromomethane
• n-Butylbenzene
• p-Isopropyltoluene
• SW (10) (Lab ID: 92484342003)
• 1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
• Bromomethane
• n-Butylbenzene
• p-Isopropyltoluene
• WW (10) (Lab ID: 92484342004)
• 1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
• Bromomethane
• n-Butylbenzene
• p-Isopropyltoluene
v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated
samples may have low bias.
• LCS (Lab ID: 2930606)
• 1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
• Bromomethane
• n-Butylbenzene
• p-Isopropyltoluene
• MS (Lab ID: 2932155)
• 1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
• Bromomethane
• p-Isopropyltoluene
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Method: EPA 8260D
Description: 8260D/5035A/5030B Volatiles
Client: Harmon Environmental
Date: July 10, 2020
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 11 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Method: SM 2540G
Description: Total Solids 2540 G-2011
Client: Harmon Environmental
Date: July 10, 2020
General Information:
5 samples were analyzed for SM 2540G by Pace National Mt. Juliet. All samples were received in acceptable condition with any
exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this
report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 12 of 54

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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: NW (10) Lab ID: 92484342001 Collected: 06/30/20 08:50 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
ND
mg/kg
12.7
1
07/02/20 15:07
07/08/20 18:26
Aliphatic (C19-C36)
ND
mg/kg
12.7
1
07/02/20 15:07
07/08/20 18:26
Aromatic (C11-C22)
ND
mg/kg
12.7
1
07/02/20 15:07
07/08/20 18:26
Surrogates
o-Terphenyl (S)
71
%
40-140
1
07/02/20 15:07
07/08/20 18:26
84-15-1
2-Fluorobiphenyl (S)
86
%
40-140
1
07/02/20 15:07
07/08/20 18:26
321-60-8
2-Bromonaphthalene (S)
86
%
40-140
1
07/02/20 15:07
07/08/20 18:26
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method:
MADEPV
Pace National
- Mt. Juliet
Aliphatic (C05-008)
ND
mg/kg
7.52
1
06/30/20 08:50
07/08/20 14:25
Aliphatic (C09-C12)
ND
mg/kg
7.52
1
06/30/20 08:50
07/08/20 14:25
Aromatic (C09-C10),Unadjusted
ND
mg/kg
7.52
1
06/30/20 08:50
07/08/20 14:25
TPHC9C10A
Total VPH
ND
mg/kg
7.52
1
06/30/20 08:50
07/08/20 14:25
VPH
Surrogates
2,5-Dibromotoluene (FID)
87.5
%
70.0-130
1
06/30/20 08:50
07/08/20 14:25
615-59-8FID
2,5-Dibromotoluene (PID)
82.5
%
70.0-130
1
06/30/20 08:50
07/08/20 14:25
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
83-32-9
Acenaphthylene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
208-96-8
Aniline
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
62-53-3
Anthracene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
120-12-7
Benzo(a)anthracene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
56-55-3
Benzo(a)pyrene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
207-08-9
Benzoic Acid
ND
ug/kg
2070
1
07/06/20 11:25
07/07/20 11:30
65-85-0
Benzyl alcohol
ND
ug/kg
830
1
07/06/20 11:25
07/07/20 11:30
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
101-55-3
Butylbenzylphthalate
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
830
1
07/06/20 11:25
07/07/20 11:30
59-50-7
4-Chloroaniline
ND
ug/kg
830
1
07/06/20 11:25
07/07/20 11:30
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
111-44-4
2-Chloronaphthalene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
91-58-7
2-Chlorophenol
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
7005-72-3
Chrysene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
53-70-3
Dibenzofuran
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
541-73-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 54

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[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: NW (10) Lab ID: 92484342001 Collected: 06/30/20 08:50 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
830
1
07/06/2011:25
07/07/2011:30
91-94-1
2,4-Dichlorophenol
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
120-83-2
Diethylphthalate
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
84-66-2
2,4-Dimethylphenol
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
105-67-9
Dimethylphthalate
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
131-11-3
Di-n-butylphthalate
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
830
1
07/06/2011:25
07/07/2011:30
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2070
1
07/06/2011:25
07/07/2011:30
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
606-20-2
Di-n-octylphthalate
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
117-81-7
Fluoranthene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
206-44-0
Fluorene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
87-68-3
Hexachlorobenzene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
77-47-4
Hexachloroethane
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
193-39-5
Isophorone
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
78-59-1
1-Methylnaphthalene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
90-12-0
2-Methylnaphthalene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
415
1
07/06/20 11:25
07/07/20 11:30
15831-10-4
Naphthalene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
91-20-3
2-Nitroaniline
ND
ug/kg
2070
1
07/06/2011:25
07/07/2011:30
88-74-4
3-Nitroaniline
ND
ug/kg
2070
1
07/06/2011:25
07/07/2011:30
99-09-2
4-Nitroaniline
ND
ug/kg
830
1
07/06/2011:25
07/07/2011:30
100-01-6
Nitrobenzene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
98-95-3
2-Nitrophenol
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
88-75-5
4-Nitrophenol
ND
ug/kg
2070
1
07/06/2011:25
07/07/2011:30
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
108-60-1
Pentachlorophenol
ND
ug/kg
830
1
07/06/2011:25
07/07/2011:30
87-86-5
Phenanthrene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
85-01-8
Phenol
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
108-95-2
Pyrene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
129-00-0
Pyridine
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
415
1
07/06/2011:25
07/07/2011:30
88-06-2
REPORT OF LABORATORY ANALYSIS
L2
L2
Qual
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: NW (10) Lab ID: 92484342001 Collected: 06/30/20 08:50 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
46
%
23-110
1
07/06/20 11:25
07/07/20 11:30
4165-60-0
2-Fluorobiphenyl (S)
37
%
30-110
1
07/06/20 11:25
07/07/20 11:30
321-60-8
Terphenyl-d14 (S)
46
%
28-110
1
07/06/20 11:25
07/07/20 11:30
1718-51-0
Phenol-d6 (S)
37
%
22-110
1
07/06/20 11:25
07/07/20 11:30
13127-88-3
2-Fluorophenol (S)
38
%
13-110
1
07/06/20 11:25
07/07/20 11:30
367-12-4
2,4,6-Tribromophenol (S)
38
%
27-110
1
07/06/20 11:25
07/07/20 11:30
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
146
1
07/06/20 10:45
07/06/20 17:28
67-64-1
Benzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
71-43-2
Bromobenzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
108-86-1
Bromochloromethane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
74-97-5
Bromodichloromethane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
75-27-4
Bromoform
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
75-25-2
Bromomethane
ND
ug/kg
14.6
1
07/06/20 10:45
07/06/20 17:28
74-83-9
2-Butanone (MEK)
ND
ug/kg
146
1
07/06/20 10:45
07/06/20 17:28
78-93-3
n-Butylbenzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
104-51-8
sec-Butylbenzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
135-98-8
tert-Butyl benzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
98-06-6
Carbon tetrachloride
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
56-23-5
Chlorobenzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
108-90-7
Chloroethane
ND
ug/kg
14.6
1
07/06/20 10:45
07/06/20 17:28
75-00-3
Chloroform
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
67-66-3
Chloromethane
ND
ug/kg
14.6
1
07/06/20 10:45
07/06/20 17:28
74-87-3
2-Chlorotoluene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
95-49-8
4-Chlorotoluene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
96-12-8
Dibromochloromethane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
106-93-4
Dibromomethane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
106-46-7
Dichlorodifluoromethane
ND
ug/kg
14.6
1
07/06/20 10:45
07/06/20 17:28
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.3
1
07/06/20 10:45
07/06/20 17:28
563-58-6
REPORT OF LABORATORY ANALYSIS
v2
v2
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Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: NW (10) Lab ID: 92484342001 Collected: 06/30/20 08:50 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
10061-01-5
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
10061-02-6
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
108-20-3
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
100-41-4
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
87-68-3
ND
ug/kg
73.2
1
07/06/2010:45
07/06/2017:28
591-78-6
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
98-82-8
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
99-87-6
ND
ug/kg
29.3
1
07/06/2010:45
07/06/2017:28
75-09-2
ND
ug/kg
73.2
1
07/06/2010:45
07/06/2017:28
108-10-1
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
1634-04-4
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
91-20-3
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
103-65-1
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
100-42-5
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
630-20-6
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
79-34-5
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
127-18-4
16.0
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
108-88-3
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
87-61-6
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
120-82-1
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
71-55-6
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
79-00-5
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
79-01-6
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
75-69-4
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
96-18-4
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
95-63-6
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
108-67-8
ND
ug/kg
73.2
1
07/06/2010:45
07/06/2017:28
108-05-4
ND
ug/kg
14.6
1
07/06/2010:45
07/06/2017:28
75-01-4
ND
ug/kg
14.6
1
07/06/2010:45
07/06/2017:28
1330-20-7
ND
ug/kg
14.6
1
07/06/2010:45
07/06/2017:28
179601-23-1
ND
ug/kg
7.3
1
07/06/2010:45
07/06/2017:28
95-47-6
100
%
70-130
1
07/06/2010:45
07/06/2017:28
2037-26-5
96
%
70-130
1
07/06/2010:45
07/06/2017:28
460-00-4
116
%
70-132
1
07/06/2010:45
07/06/2017:28
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 20.7 % 0.10 1 07/01/20 17:42
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 79.9 % 1 07/09/20 13:44 07/09/20 14:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 16 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: EW (10) Lab ID: 92484342002 Collected: 06/30/20 08:53 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
ND
mg/kg
13.6
1
07/02/20 15:07
07/08/20 18:53
Aliphatic (C19-C36)
ND
mg/kg
13.6
1
07/02/20 15:07
07/08/20 18:53
Aromatic (C11-C22)
ND
mg/kg
13.6
1
07/02/20 15:07
07/08/20 18:53
Surrogates
o-Terphenyl (S)
72
%
40-140
1
07/02/20 15:07
07/08/20 18:53
84-15-1
2-Fluorobiphenyl (S)
92
%
40-140
1
07/02/20 15:07
07/08/20 18:53
321-60-8
2-Bromonaphthalene (S)
92
%
40-140
1
07/02/20 15:07
07/08/20 18:53
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method:
MADEPV
Pace National
- Mt. Juliet
Aliphatic (C05-008)
ND
mg/kg
8.02
1.07
06/30/20 08:53
07/08/20 14:58
Aliphatic (C09-C12)
ND
mg/kg
8.02
1.07
06/30/20 08:53
07/08/20 14:58
Aromatic (C09-C10),Unadjusted
ND
mg/kg
8.02
1.07
06/30/20 08:53
07/08/20 14:58
TPHC9C10A
Total VPH
ND
mg/kg
8.02
1.07
06/30/20 08:53
07/08/20 14:58
VPH
Surrogates
2,5-Dibromotoluene (FID)
90.3
%
70.0-130
1.07
06/30/20 08:53
07/08/20 14:58
615-59-8FID
2,5-Dibromotoluene (PID)
84.2
%
70.0-130
1.07
06/30/20 08:53
07/08/20 14:58
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
83-32-9
Acenaphthylene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
208-96-8
Aniline
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
62-53-3
Anthracene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
120-12-7
Benzo(a)anthracene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
56-55-3
Benzo(a)pyrene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
207-08-9
Benzoic Acid
ND
ug/kg
2250
1
07/06/20 11:25
07/07/20 11:57
65-85-0
Benzyl alcohol
ND
ug/kg
901
1
07/06/20 11:25
07/07/20 11:57
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
101-55-3
Butylbenzylphthalate
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
901
1
07/06/20 11:25
07/07/20 11:57
59-50-7
4-Chloroaniline
ND
ug/kg
901
1
07/06/20 11:25
07/07/20 11:57
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
111-44-4
2-Chloronaphthalene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
91-58-7
2-Chlorophenol
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
7005-72-3
Chrysene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
53-70-3
Dibenzofuran
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
541-73-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 54

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: EW (10) Lab ID: 92484342002 Collected: 06/30/20 08:53 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
901
1
07/06/2011:25
07/07/2011:57
91-94-1
2,4-Dichlorophenol
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
120-83-2
Diethylphthalate
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
84-66-2
2,4-Dimethylphenol
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
105-67-9
Dimethylphthalate
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
131-11-3
Di-n-butylphthalate
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
901
1
07/06/2011:25
07/07/2011:57
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2250
1
07/06/2011:25
07/07/2011:57
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
606-20-2
Di-n-octylphthalate
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
117-81-7
Fluoranthene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
206-44-0
Fluorene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
87-68-3
Hexachlorobenzene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
77-47-4
Hexachloroethane
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
193-39-5
Isophorone
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
78-59-1
1-Methylnaphthalene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
90-12-0
2-Methylnaphthalene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
451
1
07/06/20 11:25
07/07/20 11:57
15831-10-4
Naphthalene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
91-20-3
2-Nitroaniline
ND
ug/kg
2250
1
07/06/2011:25
07/07/2011:57
88-74-4
3-Nitroaniline
ND
ug/kg
2250
1
07/06/2011:25
07/07/2011:57
99-09-2
4-Nitroaniline
ND
ug/kg
901
1
07/06/2011:25
07/07/2011:57
100-01-6
Nitrobenzene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
98-95-3
2-Nitrophenol
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
88-75-5
4-Nitrophenol
ND
ug/kg
2250
1
07/06/2011:25
07/07/2011:57
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
108-60-1
Pentachlorophenol
ND
ug/kg
901
1
07/06/2011:25
07/07/2011:57
87-86-5
Phenanthrene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
85-01-8
Phenol
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
108-95-2
Pyrene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
129-00-0
Pyridine
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
451
1
07/06/2011:25
07/07/2011:57
88-06-2
REPORT OF LABORATORY ANALYSIS
L2
L2
Qual
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: EW (10) Lab ID: 92484342002 Collected: 06/30/20 08:53 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
46
%
23-110
1
07/06/20 11:25
07/07/20 11:57
4165-60-0
2-Fluorobiphenyl (S)
38
%
30-110
1
07/06/20 11:25
07/07/20 11:57
321-60-8
Terphenyl-d14 (S)
49
%
28-110
1
07/06/20 11:25
07/07/20 11:57
1718-51-0
Phenol-d6 (S)
38
%
22-110
1
07/06/20 11:25
07/07/20 11:57
13127-88-3
2-Fluorophenol (S)
41
%
13-110
1
07/06/20 11:25
07/07/20 11:57
367-12-4
2,4,6-Tribromophenol (S)
39
%
27-110
1
07/06/20 11:25
07/07/20 11:57
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
132
1
07/06/20 10:45
07/06/20 17:47
67-64-1
Benzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
71-43-2
Bromobenzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
108-86-1
Bromochloromethane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
74-97-5
Bromodichloromethane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
75-27-4
Bromoform
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
75-25-2
Bromomethane
ND
ug/kg
13.2
1
07/06/20 10:45
07/06/20 17:47
74-83-9
2-Butanone (MEK)
ND
ug/kg
132
1
07/06/20 10:45
07/06/20 17:47
78-93-3
n-Butylbenzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
104-51-8
sec-Butylbenzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
135-98-8
tert-Butyl benzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
98-06-6
Carbon tetrachloride
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
56-23-5
Chlorobenzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
108-90-7
Chloroethane
ND
ug/kg
13.2
1
07/06/20 10:45
07/06/20 17:47
75-00-3
Chloroform
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
67-66-3
Chloromethane
ND
ug/kg
13.2
1
07/06/20 10:45
07/06/20 17:47
74-87-3
2-Chlorotoluene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
95-49-8
4-Chlorotoluene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
96-12-8
Dibromochloromethane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
106-93-4
Dibromomethane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
106-46-7
Dichlorodifluoromethane
ND
ug/kg
13.2
1
07/06/20 10:45
07/06/20 17:47
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.6
1
07/06/20 10:45
07/06/20 17:47
563-58-6
REPORT OF LABORATORY ANALYSIS
v2
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Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: EW (10) Lab ID: 92484342002 Collected: 06/30/20 08:53 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
10061-01-5
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
10061-02-6
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
108-20-3
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
100-41-4
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
87-68-3
ND
ug/kg
66.1
1
07/06/2010:45
07/06/2017:47
591-78-6
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
98-82-8
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
99-87-6
ND
ug/kg
26.4
1
07/06/2010:45
07/06/2017:47
75-09-2
ND
ug/kg
66.1
1
07/06/2010:45
07/06/2017:47
108-10-1
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
1634-04-4
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
91-20-3
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
103-65-1
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
100-42-5
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
630-20-6
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
79-34-5
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
127-18-4
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
108-88-3
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
87-61-6
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
120-82-1
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
71-55-6
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
79-00-5
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
79-01-6
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
75-69-4
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
96-18-4
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
95-63-6
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
108-67-8
ND
ug/kg
66.1
1
07/06/2010:45
07/06/2017:47
108-05-4
ND
ug/kg
13.2
1
07/06/2010:45
07/06/2017:47
75-01-4
ND
ug/kg
13.2
1
07/06/2010:45
07/06/2017:47
1330-20-7
ND
ug/kg
13.2
1
07/06/2010:45
07/06/2017:47
179601-23-1
ND
ug/kg
6.6
1
07/06/2010:45
07/06/2017:47
95-47-6
100
%
70-130
1
07/06/2010:45
07/06/2017:47
2037-26-5
97
%
70-130
1
07/06/2010:45
07/06/2017:47
460-00-4
117
%
70-132
1
07/06/2010:45
07/06/2017:47
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 26.3 % 0.10 1 07/01/20 17:42
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 79.5 % 1 07/09/20 13:44 07/09/20 14:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 20 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: SW (10) Lab ID: 92484342003 Collected: 06/30/20 08:55 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
ND
mg/kg
13.4
1
07/02/20 15:07
07/08/20 19:20
Aliphatic (C19-C36)
ND
mg/kg
13.4
1
07/02/20 15:07
07/08/20 19:20
Aromatic (C11-C22)
ND
mg/kg
13.4
1
07/02/20 15:07
07/08/20 19:20
Surrogates
o-Terphenyl (S)
69
%
40-140
1
07/02/20 15:07
07/08/20 19:20
84-15-1
2-Fluorobiphenyl (S)
87
%
40-140
1
07/02/20 15:07
07/08/20 19:20
321-60-8
2-Bromonaphthalene (S)
87
%
40-140
1
07/02/20 15:07
07/08/20 19:20
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method:
MADEPV
Pace National
- Mt. Juliet
Aliphatic (C05-008)
ND
mg/kg
8.23
1.03
06/30/20 08:55
07/08/20 15:30
Aliphatic (C09-C12)
ND
mg/kg
8.23
1.03
06/30/20 08:55
07/08/20 15:30
Aromatic (C09-C10),Unadjusted
ND
mg/kg
8.23
1.03
06/30/20 08:55
07/08/20 15:30
TPHC9C10A
Total VPH
ND
mg/kg
8.23
1.03
06/30/20 08:55
07/08/20 15:30
VPH
Surrogates
2,5-Dibromotoluene (FID)
88.4
%
70.0-130
1.03
06/30/20 08:55
07/08/20 15:30
615-59-8FID
2,5-Dibromotoluene (PID)
84.2
%
70.0-130
1.03
06/30/20 08:55
07/08/20 15:30
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
83-32-9
Acenaphthylene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
208-96-8
Aniline
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
62-53-3
Anthracene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
120-12-7
Benzo(a)anthracene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
56-55-3
Benzo(a)pyrene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
207-08-9
Benzoic Acid
ND
ug/kg
2160
1
07/06/20 11:25
07/07/20 12:24
65-85-0
Benzyl alcohol
ND
ug/kg
864
1
07/06/20 11:25
07/07/20 12:24
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
101-55-3
Butylbenzylphthalate
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
864
1
07/06/20 11:25
07/07/20 12:24
59-50-7
4-Chloroaniline
ND
ug/kg
864
1
07/06/20 11:25
07/07/20 12:24
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
111-44-4
2-Chloronaphthalene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
91-58-7
2-Chlorophenol
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
7005-72-3
Chrysene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
53-70-3
Dibenzofuran
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
541-73-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: SW (10) Lab ID: 92484342003 Collected: 06/30/20 08:55 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
864
1
07/06/2011:25
07/07/2012:24
91-94-1
2,4-Dichlorophenol
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
120-83-2
Diethylphthalate
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
84-66-2
2,4-Dimethylphenol
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
105-67-9
Dimethylphthalate
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
131-11-3
Di-n-butylphthalate
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
864
1
07/06/2011:25
07/07/2012:24
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2160
1
07/06/2011:25
07/07/2012:24
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
606-20-2
Di-n-octylphthalate
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
117-81-7
Fluoranthene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
206-44-0
Fluorene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
87-68-3
Hexachlorobenzene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
77-47-4
Hexachloroethane
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
193-39-5
Isophorone
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
78-59-1
1-Methylnaphthalene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
90-12-0
2-Methylnaphthalene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
432
1
07/06/20 11:25
07/07/20 12:24
15831-10-4
Naphthalene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
91-20-3
2-Nitroaniline
ND
ug/kg
2160
1
07/06/2011:25
07/07/2012:24
88-74-4
3-Nitroaniline
ND
ug/kg
2160
1
07/06/2011:25
07/07/2012:24
99-09-2
4-Nitroaniline
ND
ug/kg
864
1
07/06/2011:25
07/07/2012:24
100-01-6
Nitrobenzene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
98-95-3
2-Nitrophenol
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
88-75-5
4-Nitrophenol
ND
ug/kg
2160
1
07/06/2011:25
07/07/2012:24
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
108-60-1
Pentachlorophenol
ND
ug/kg
864
1
07/06/2011:25
07/07/2012:24
87-86-5
Phenanthrene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
85-01-8
Phenol
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
108-95-2
Pyrene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
129-00-0
Pyridine
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
432
1
07/06/2011:25
07/07/2012:24
88-06-2
REPORT OF LABORATORY ANALYSIS
L2
L2
Qual
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: SW (10) Lab ID: 92484342003 Collected: 06/30/20 08:55 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
44
%
23-110
1
07/06/20 11:25
07/07/20 12:24
4165-60-0
2-Fluorobiphenyl (S)
43
%
30-110
1
07/06/20 11:25
07/07/20 12:24
321-60-8
Terphenyl-d14 (S)
53
%
28-110
1
07/06/20 11:25
07/07/20 12:24
1718-51-0
Phenol-d6 (S)
43
%
22-110
1
07/06/20 11:25
07/07/20 12:24
13127-88-3
2-Fluorophenol (S)
44
%
13-110
1
07/06/20 11:25
07/07/20 12:24
367-12-4
2,4,6-Tribromophenol (S)
46
%
27-110
1
07/06/20 11:25
07/07/20 12:24
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
155
1
07/06/20 10:45
07/06/20 18:05
67-64-1
Benzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
71-43-2
Bromobenzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
108-86-1
Bromochloromethane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
74-97-5
Bromodichloromethane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
75-27-4
Bromoform
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
75-25-2
Bromomethane
ND
ug/kg
15.5
1
07/06/20 10:45
07/06/20 18:05
74-83-9
2-Butanone (MEK)
ND
ug/kg
155
1
07/06/20 10:45
07/06/20 18:05
78-93-3
n-Butylbenzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
104-51-8
sec-Butylbenzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
135-98-8
tert-Butyl benzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
98-06-6
Carbon tetrachloride
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
56-23-5
Chlorobenzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
108-90-7
Chloroethane
ND
ug/kg
15.5
1
07/06/20 10:45
07/06/20 18:05
75-00-3
Chloroform
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
67-66-3
Chloromethane
ND
ug/kg
15.5
1
07/06/20 10:45
07/06/20 18:05
74-87-3
2-Chlorotoluene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
95-49-8
4-Chlorotoluene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
96-12-8
Dibromochloromethane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
106-93-4
Dibromomethane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.5
1
07/06/20 10:45
07/06/20 18:05
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.8
1
07/06/20 10:45
07/06/20 18:05
563-58-6
REPORT OF LABORATORY ANALYSIS
v2
v2
Qual
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: SW (10) Lab ID: 92484342003 Collected: 06/30/20 08:55 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
10061-01-5
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
10061-02-6
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
108-20-3
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
100-41-4
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
87-68-3
ND
ug/kg
77.6
1
07/06/2010:45
07/06/2018:05
591-78-6
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
98-82-8
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
99-87-6
ND
ug/kg
31.1
1
07/06/2010:45
07/06/2018:05
75-09-2
ND
ug/kg
77.6
1
07/06/2010:45
07/06/2018:05
108-10-1
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
1634-04-4
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
91-20-3
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
103-65-1
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
100-42-5
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
630-20-6
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
79-34-5
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
127-18-4
8.0
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
108-88-3
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
87-61-6
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
120-82-1
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
71-55-6
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
79-00-5
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
79-01-6
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
75-69-4
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
96-18-4
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
95-63-6
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
108-67-8
ND
ug/kg
77.6
1
07/06/2010:45
07/06/2018:05
108-05-4
ND
ug/kg
15.5
1
07/06/2010:45
07/06/2018:05
75-01-4
ND
ug/kg
15.5
1
07/06/2010:45
07/06/2018:05
1330-20-7
ND
ug/kg
15.5
1
07/06/2010:45
07/06/2018:05
179601-23-1
ND
ug/kg
7.8
1
07/06/2010:45
07/06/2018:05
95-47-6
99
%
70-130
1
07/06/2010:45
07/06/2018:05
2037-26-5
97
%
70-130
1
07/06/2010:45
07/06/2018:05
460-00-4
116
%
70-132
1
07/06/2010:45
07/06/2018:05
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 24.4 % 0.10 1 07/01/20 17:42
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 76.7 % 1 07/09/20 13:44 07/09/20 14:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 24 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: WW (10) Lab ID: 92484342004 Collected: 06/30/20 10:15 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
ND
mg/kg
13.0
1
07/02/20 15:07
07/08/20 19:47
Aliphatic (C19-C36)
ND
mg/kg
13.0
1
07/02/20 15:07
07/08/20 19:47
Aromatic (C11-C22)
ND
mg/kg
13.0
1
07/02/20 15:07
07/08/20 19:47
Surrogates
o-Terphenyl (S)
74
%
40-140
1
07/02/20 15:07
07/08/20 19:47
84-15-1
2-Fluorobiphenyl (S)
91
%
40-140
1
07/02/20 15:07
07/08/20 19:47
321-60-8
2-Bromonaphthalene (S)
91
%
40-140
1
07/02/20 15:07
07/08/20 19:47
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method:
MADEPV
Pace National
- Mt. Juliet
Aliphatic (C05-008)
ND
mg/kg
7.85
1
06/30/20 10:15
07/08/20 16:05
Aliphatic (C09-C12)
ND
mg/kg
7.85
1
06/30/20 10:15
07/08/20 16:05
Aromatic (C09-C10),Unadjusted
ND
mg/kg
7.85
1
06/30/20 10:15
07/08/20 16:05
TPHC9C10A
Total VPH
ND
mg/kg
7.85
1
06/30/20 10:15
07/08/20 16:05
VPH
Surrogates
2,5-Dibromotoluene (FID)
92.5
%
70.0-130
1
06/30/20 10:15
07/08/20 16:05
615-59-8FID
2,5-Dibromotoluene (PID)
86.6
%
70.0-130
1
06/30/20 10:15
07/08/20 16:05
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
83-32-9
Acenaphthylene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
208-96-8
Aniline
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
62-53-3
Anthracene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
120-12-7
Benzo(a)anthracene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
56-55-3
Benzo(a)pyrene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
207-08-9
Benzoic Acid
ND
ug/kg
2120
1
07/06/20 11:25
07/07/20 12:51
65-85-0
Benzyl alcohol
ND
ug/kg
847
1
07/06/20 11:25
07/07/20 12:51
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
101-55-3
Butylbenzylphthalate
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
847
1
07/06/20 11:25
07/07/20 12:51
59-50-7
4-Chloroaniline
ND
ug/kg
847
1
07/06/20 11:25
07/07/20 12:51
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
111-44-4
2-Chloronaphthalene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
91-58-7
2-Chlorophenol
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
7005-72-3
Chrysene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
53-70-3
Dibenzofuran
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
541-73-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: WW (10) Lab ID: 92484342004 Collected: 06/30/20 10:15 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
847
1
07/06/2011:25
07/07/2012:51
91-94-1
2,4-Dichlorophenol
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
120-83-2
Diethylphthalate
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
84-66-2
2,4-Dimethylphenol
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
105-67-9
Dimethylphthalate
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
131-11-3
Di-n-butylphthalate
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
847
1
07/06/2011:25
07/07/2012:51
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2120
1
07/06/2011:25
07/07/2012:51
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
606-20-2
Di-n-octylphthalate
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
117-81-7
Fluoranthene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
206-44-0
Fluorene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
87-68-3
Hexachlorobenzene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
77-47-4
Hexachloroethane
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
193-39-5
Isophorone
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
78-59-1
1-Methylnaphthalene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
90-12-0
2-Methylnaphthalene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
424
1
07/06/20 11:25
07/07/20 12:51
15831-10-4
Naphthalene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
91-20-3
2-Nitroaniline
ND
ug/kg
2120
1
07/06/2011:25
07/07/2012:51
88-74-4
3-Nitroaniline
ND
ug/kg
2120
1
07/06/2011:25
07/07/2012:51
99-09-2
4-Nitroaniline
ND
ug/kg
847
1
07/06/2011:25
07/07/2012:51
100-01-6
Nitrobenzene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
98-95-3
2-Nitrophenol
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
88-75-5
4-Nitrophenol
ND
ug/kg
2120
1
07/06/2011:25
07/07/2012:51
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
108-60-1
Pentachlorophenol
ND
ug/kg
847
1
07/06/2011:25
07/07/2012:51
87-86-5
Phenanthrene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
85-01-8
Phenol
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
108-95-2
Pyrene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
129-00-0
Pyridine
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
424
1
07/06/2011:25
07/07/2012:51
88-06-2
REPORT OF LABORATORY ANALYSIS
L2
L2
Qual
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: WW (10) Lab ID: 92484342004 Collected: 06/30/20 10:15 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
46
%
23-110
1
07/06/20 11:25
07/07/20 12:51
4165-60-0
2-Fluorobiphenyl (S)
41
%
30-110
1
07/06/20 11:25
07/07/20 12:51
321-60-8
Terphenyl-d14 (S)
46
%
28-110
1
07/06/20 11:25
07/07/20 12:51
1718-51-0
Phenol-d6 (S)
42
%
22-110
1
07/06/20 11:25
07/07/20 12:51
13127-88-3
2-Fluorophenol (S)
42
%
13-110
1
07/06/20 11:25
07/07/20 12:51
367-12-4
2,4,6-Tribromophenol (S)
36
%
27-110
1
07/06/20 11:25
07/07/20 12:51
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
126
1
07/06/20 10:45
07/06/20 18:23
67-64-1
Benzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
71-43-2
Bromobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
108-86-1
Bromochloromethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
74-97-5
Bromodichloromethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
75-27-4
Bromoform
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
75-25-2
Bromomethane
ND
ug/kg
12.6
1
07/06/20 10:45
07/06/20 18:23
74-83-9
2-Butanone (MEK)
ND
ug/kg
126
1
07/06/20 10:45
07/06/20 18:23
78-93-3
n-Butylbenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
104-51-8
sec-Butylbenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
135-98-8
tert-Butyl benzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
98-06-6
Carbon tetrachloride
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
56-23-5
Chlorobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
108-90-7
Chloroethane
ND
ug/kg
12.6
1
07/06/20 10:45
07/06/20 18:23
75-00-3
Chloroform
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
67-66-3
Chloromethane
ND
ug/kg
12.6
1
07/06/20 10:45
07/06/20 18:23
74-87-3
2-Chlorotoluene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
95-49-8
4-Chlorotoluene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
96-12-8
Dibromochloromethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
106-93-4
Dibromomethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.6
1
07/06/20 10:45
07/06/20 18:23
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:23
563-58-6
REPORT OF LABORATORY ANALYSIS
v2
v2
Qual
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: WW (10) Lab ID: 92484342004 Collected: 06/30/20 10:15 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
10061-01-5
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
10061-02-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
108-20-3
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
100-41-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
87-68-3
ND
ug/kg
63.1
1
07/06/2010:45
07/06/2018:23
591-78-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
98-82-8
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
99-87-6
ND
ug/kg
25.2
1
07/06/2010:45
07/06/2018:23
75-09-2
ND
ug/kg
63.1
1
07/06/2010:45
07/06/2018:23
108-10-1
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
1634-04-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
91-20-3
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
103-65-1
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
100-42-5
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
630-20-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
79-34-5
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
127-18-4
9.2
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
108-88-3
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
87-61-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
120-82-1
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
71-55-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
79-00-5
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
79-01-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
75-69-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
96-18-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
95-63-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
108-67-8
ND
ug/kg
63.1
1
07/06/2010:45
07/06/2018:23
108-05-4
ND
ug/kg
12.6
1
07/06/2010:45
07/06/2018:23
75-01-4
ND
ug/kg
12.6
1
07/06/2010:45
07/06/2018:23
1330-20-7
ND
ug/kg
12.6
1
07/06/2010:45
07/06/2018:23
179601-23-1
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:23
95-47-6
100
%
70-130
1
07/06/2010:45
07/06/2018:23
2037-26-5
97
%
70-130
1
07/06/2010:45
07/06/2018:23
460-00-4
114
%
70-132
1
07/06/2010:45
07/06/2018:23
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 22.9 % 0.10 1 07/01/20 17:42
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 78.4 % 1 07/09/20 13:44 07/09/20 14:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 28 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: BOT (14.5) Lab ID: 92484342005 Collected: 06/30/20 14:05 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Aliphatic (C09-C18)
ND
mg/kg
12.8
1
07/02/20 15:07
07/08/20 20:15
Aliphatic (C19-C36)
ND
mg/kg
12.8
1
07/02/20 15:07
07/08/20 20:15
Aromatic (C11-C22)
ND
mg/kg
12.8
1
07/02/20 15:07
07/08/20 20:15
Surrogates
o-Terphenyl (S)
60
%
40-140
1
07/02/20 15:07
07/08/20 20:15
84-15-1
2-Fluorobiphenyl (S)
92
%
40-140
1
07/02/20 15:07
07/08/20 20:15
321-60-8
2-Bromonaphthalene (S)
93
%
40-140
1
07/02/20 15:07
07/08/20 20:15
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method:
MADEPV
Pace National
- Mt. Juliet
Aliphatic (C05-CO8)
ND
mg/kg
7.89
1
06/30/20 14:05
07/08/20 16:37
Aliphatic (C09-C12)
ND
mg/kg
7.89
1
06/30/20 14:05
07/08/20 16:37
Aromatic (C09-C10),Unadjusted
ND
mg/kg
7.89
1
06/30/20 14:05
07/08/20 16:37
TPHC9C10A
Total VPH
ND
mg/kg
7.89
1
06/30/20 14:05
07/08/20 16:37
VPH
Surrogates
2,5-Dibromotoluene (FID)
89.2
%
70.0-130
1
06/30/20 14:05
07/08/20 16:37
615-59-8FID
2,5-Dibromotoluene (PID)
84.4
%
70.0-130
1
06/30/20 14:05
07/08/20 16:37
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
83-32-9
Acenaphthylene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
208-96-8
Aniline
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
62-53-3
Anthracene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
120-12-7
Benzo(a)anthracene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
56-55-3
Benzo(a)pyrene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
207-08-9
Benzoic Acid
ND
ug/kg
2070
1
07/06/20 11:25
07/07/20 13:18
65-85-0
Benzyl alcohol
ND
ug/kg
827
1
07/06/20 11:25
07/07/20 13:18
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
101-55-3
Butylbenzylphthalate
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
827
1
07/06/20 11:25
07/07/20 13:18
59-50-7
4-Chloroaniline
ND
ug/kg
827
1
07/06/20 11:25
07/07/20 13:18
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
111-44-4
2-Chloronaphthalene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
91-58-7
2-Chlorophenol
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
7005-72-3
Chrysene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
53-70-3
Dibenzofuran
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
541-73-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: BOT (14.5) Lab ID: 92484342005 Collected: 06/30/20 14:05 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
827
1
07/06/2011:25
07/07/2013:18
91-94-1
2,4-Dichlorophenol
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
120-83-2
Diethylphthalate
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
84-66-2
2,4-Dimethylphenol
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
105-67-9
Dimethylphthalate
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
131-11-3
Di-n-butylphthalate
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
827
1
07/06/2011:25
07/07/2013:18
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2070
1
07/06/2011:25
07/07/2013:18
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
606-20-2
Di-n-octylphthalate
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
117-81-7
Fluoranthene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
206-44-0
Fluorene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
87-68-3
Hexachlorobenzene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
77-47-4
Hexachloroethane
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
193-39-5
Isophorone
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
78-59-1
1-Methylnaphthalene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
90-12-0
2-Methylnaphthalene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
414
1
07/06/20 11:25
07/07/20 13:18
15831-10-4
Naphthalene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
91-20-3
2-Nitroaniline
ND
ug/kg
2070
1
07/06/2011:25
07/07/2013:18
88-74-4
3-Nitroaniline
ND
ug/kg
2070
1
07/06/2011:25
07/07/2013:18
99-09-2
4-Nitroaniline
ND
ug/kg
827
1
07/06/2011:25
07/07/2013:18
100-01-6
Nitrobenzene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
98-95-3
2-Nitrophenol
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
88-75-5
4-Nitrophenol
ND
ug/kg
2070
1
07/06/2011:25
07/07/2013:18
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
108-60-1
Pentachlorophenol
ND
ug/kg
827
1
07/06/2011:25
07/07/2013:18
87-86-5
Phenanthrene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
85-01-8
Phenol
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
108-95-2
Pyrene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
129-00-0
Pyridine
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
414
1
07/06/2011:25
07/07/2013:18
88-06-2
REPORT OF LABORATORY ANALYSIS
L2
L2
Qual
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: BOT (14.5) Lab ID: 92484342005 Collected: 06/30/20 14:05 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
42
%
23-110
1
07/06/20 11:25
07/07/20 13:18
4165-60-0
2-Fluorobiphenyl (S)
37
%
30-110
1
07/06/20 11:25
07/07/20 13:18
321-60-8
Terphenyl-d14 (S)
47
%
28-110
1
07/06/20 11:25
07/07/20 13:18
1718-51-0
Phenol-d6 (S)
37
%
22-110
1
07/06/20 11:25
07/07/20 13:18
13127-88-3
2-Fluorophenol (S)
38
%
13-110
1
07/06/20 11:25
07/07/20 13:18
367-12-4
2,4,6-Tribromophenol (S)
34
%
27-110
1
07/06/20 11:25
07/07/20 13:18
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
126
1
07/06/20 10:45
07/06/20 18:42
67-64-1
Benzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
71-43-2
Bromobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
108-86-1
Bromochloromethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
74-97-5
Bromodichloromethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
75-27-4
Bromoform
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
75-25-2
Bromomethane
ND
ug/kg
12.6
1
07/06/20 10:45
07/06/20 18:42
74-83-9
2-Butanone (MEK)
ND
ug/kg
126
1
07/06/20 10:45
07/06/20 18:42
78-93-3
n-Butylbenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
104-51-8
sec-Butylbenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
135-98-8
tert-Butyl benzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
98-06-6
Carbon tetrachloride
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
56-23-5
Chlorobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
108-90-7
Chloroethane
ND
ug/kg
12.6
1
07/06/20 10:45
07/06/20 18:42
75-00-3
Chloroform
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
67-66-3
Chloromethane
ND
ug/kg
12.6
1
07/06/20 10:45
07/06/20 18:42
74-87-3
2-Chlorotoluene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
95-49-8
4-Chlorotoluene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
96-12-8
Dibromochloromethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
106-93-4
Dibromomethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.6
1
07/06/20 10:45
07/06/20 18:42
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.3
1
07/06/20 10:45
07/06/20 18:42
563-58-6
REPORT OF LABORATORY ANALYSIS
v2
v2
Qual
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
Sample: BOT (14.5) Lab ID: 92484342005 Collected: 06/30/20 14:05 Received: 07/01/20 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
10061-01-5
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
10061-02-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
108-20-3
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
100-41-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
87-68-3
ND
ug/kg
63.1
1
07/06/2010:45
07/06/2018:42
591-78-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
98-82-8
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
99-87-6
ND
ug/kg
25.2
1
07/06/2010:45
07/06/2018:42
75-09-2
ND
ug/kg
63.1
1
07/06/2010:45
07/06/2018:42
108-10-1
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
1634-04-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
91-20-3
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
103-65-1
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
100-42-5
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
630-20-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
79-34-5
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
127-18-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
108-88-3
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
87-61-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
120-82-1
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
71-55-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
79-00-5
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
79-01-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
75-69-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
96-18-4
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
95-63-6
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
108-67-8
ND
ug/kg
63.1
1
07/06/2010:45
07/06/2018:42
108-05-4
ND
ug/kg
12.6
1
07/06/2010:45
07/06/2018:42
75-01-4
ND
ug/kg
12.6
1
07/06/2010:45
07/06/2018:42
1330-20-7
ND
ug/kg
12.6
1
07/06/2010:45
07/06/2018:42
179601-23-1
ND
ug/kg
6.3
1
07/06/2010:45
07/06/2018:42
95-47-6
100
%
70-130
1
07/06/2010:45
07/06/2018:42
2037-26-5
95
%
70-130
1
07/06/2010:45
07/06/2018:42
460-00-4
116
%
70-132
1
07/06/2010:45
07/06/2018:42
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 21.5 % 0.10 1 07/01/20 17:42
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 79.4 % 1 07/09/20 13:44 07/09/20 14:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 32 of 54

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
QC Batch: 1505748 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
METHOD BLANK: R3548284-3
Matrix:
Solid
Associated Lab Samples: 92484342001, 92484342002,
92484342003, 92484342004, 92484342005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND
5.00
07/08/20 13:16
Aliphatic (C09-C12)
mg/kg
ND
5.00
07/08/20 13:16
Aromatic (C09-C10),Unadjusted
mg/kg
ND
5.00
07/08/20 13:16
Total VPH
mg/kg
ND
5.00
07/08/20 13:16
2,5-Dibromotoluene (FID)
%
79.8
70.0-130
07/08/20 13:16
2,5-Dibromotoluene (PID)
%
75.9
70.0-130
07/08/20 13:16
LABORATORY CONTROL SAMPLE & LCSD:
R3548284-1
R3548284-2
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
60.0
56.5
57.1
94.2
95.2
70.0-130
1.06
25
Aliphatic (C09-C12)
mg/kg
70.0
60.5
60.5
86.4
86.4
70.0-130
0.00
25
Aromatic (C09-C10),Unadjusted
mg/kg
10.0
9.29
9.79
92.9
97.9
70.0-130
5.24
25
Total VPH
mg/kg
140
126
127
90.0
90.7
70.0-130
0.791
25
2,5-Dibromotoluene (FID)
%
94.7
93.1
70.0-130
2,5-Dibromotoluene (PID)
%
89.3
88.1
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
QC Batch: 551292 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
METHOD BLANK: 2930605 Matrix: Solid
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
07/06/20 12:16
1,1,1-Trichloroethane
ug/kg
ND
5.0
07/06/20 12:16
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
07/06/20 12:16
1,1,2-Trichloroethane
ug/kg
ND
5.0
07/06/20 12:16
1,1-Dichloroethane
ug/kg
ND
5.0
07/06/20 12:16
1,1-Dichloroethene
ug/kg
ND
5.0
07/06/20 12:16
1,1-Dichloropropene
ug/kg
ND
5.0
07/06/20 12:16
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
07/06/20 12:16
1,2,3-Trichloropropane
ug/kg
ND
5.0
07/06/20 12:16
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
07/06/20 12:16
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
07/06/20 12:16
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
07/06/20 12:16
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
07/06/20 12:16
1,2-Dichlorobenzene
ug/kg
ND
5.0
07/06/20 12:16
1,2-Dichloroethane
ug/kg
ND
5.0
07/06/20 12:16
1,2-Dichloropropane
ug/kg
ND
5.0
07/06/20 12:16
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
07/06/20 12:16
1,3-Dichlorobenzene
ug/kg
ND
5.0
07/06/20 12:16
1,3-Dichloropropane
ug/kg
ND
5.0
07/06/20 12:16
1,4-Dichlorobenzene
ug/kg
ND
5.0
07/06/20 12:16
2,2-Dichloropropane
ug/kg
ND
5.0
07/06/20 12:16
2-Butanone (MEK)
ug/kg
ND
100
07/06/20 12:16
2-Chlorotoluene
ug/kg
ND
5.0
07/06/20 12:16
2-Hexanone
ug/kg
ND
50.0
07/06/20 12:16
4-Chlorotoluene
ug/kg
ND
5.0
07/06/20 12:16
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
07/06/20 12:16
Acetone
ug/kg
ND
100
07/06/20 12:16
Benzene
ug/kg
ND
5.0
07/06/20 12:16
Bromobenzene
ug/kg
ND
5.0
07/06/20 12:16
Bromochloromethane
ug/kg
ND
5.0
07/06/20 12:16
Bromodichloromethane
ug/kg
ND
5.0
07/06/20 12:16
Bromoform
ug/kg
ND
5.0
07/06/20 12:16
Bromomethane
ug/kg
ND
10.0
07/06/20 12:16
Carbon tetrachloride
ug/kg
ND
5.0
07/06/20 12:16
Chlorobenzene
ug/kg
ND
5.0
07/06/20 12:16
Chloroethane
ug/kg
ND
10.0
07/06/20 12:16
Chloroform
ug/kg
ND
5.0
07/06/20 12:16
Chloromethane
ug/kg
ND
10.0
07/06/20 12:16
cis-1,2-Dichloroethene
ug/kg
ND
5.0
07/06/20 12:16
cis-1,3-Dichloropropene
ug/kg
ND
5.0
07/06/20 12:16
v2
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
METHOD BLANK: 2930605 Matrix: Solid
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
Blank Reporting
Parameter Units Result Limit Analyzed
Dibromochloromethane
ug/kg
ND
5.0
07/06/20 12:16
Dibromomethane
ug/kg
ND
5.0
07/06/20 12:16
Dichlorodifluoromethane
ug/kg
ND
10.0
07/06/20 12:16
Diisopropyl ether
ug/kg
ND
5.0
07/06/20 12:16
Ethylbenzene
ug/kg
ND
5.0
07/06/20 12:16
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
07/06/20 12:16
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
07/06/20 12:16
m&p-Xylene
ug/kg
ND
10.0
07/06/20 12:16
Methyl-tert-butyl ether
ug/kg
ND
5.0
07/06/20 12:16
Methylene Chloride
ug/kg
ND
20.0
07/06/20 12:16
n-Butylbenzene
ug/kg
ND
5.0
07/06/20 12:16
n-Propylbenzene
ug/kg
ND
5.0
07/06/20 12:16
Naphthalene
ug/kg
ND
5.0
07/06/20 12:16
o-Xylene
ug/kg
ND
5.0
07/06/20 12:16
p-Isopropyltoluene
ug/kg
ND
5.0
07/06/20 12:16
sec-Butylbenzene
ug/kg
ND
5.0
07/06/20 12:16
Styrene
ug/kg
ND
5.0
07/06/20 12:16
tert-Butyl benzene
ug/kg
ND
5.0
07/06/20 12:16
Tetrachloroethene
ug/kg
ND
5.0
07/06/20 12:16
Toluene
ug/kg
ND
5.0
07/06/20 12:16
trans-1,2-Dichloroethene
ug/kg
ND
5.0
07/06/20 12:16
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
07/06/20 12:16
Trichloroethene
ug/kg
ND
5.0
07/06/20 12:16
Trichlorofluoromethane
ug/kg
ND
5.0
07/06/20 12:16
Vinyl acetate
ug/kg
ND
50.0
07/06/20 12:16
Vinyl chloride
ug/kg
ND
10.0
07/06/20 12:16
Xylene (Total)
ug/kg
ND
10.0
07/06/20 12:16
1,2-Dichloroethane-d4 (S)
%
119
70-132
07/06/20 12:16
4-Bromofluorobenzene (S)
%
95
70-130
07/06/20 12:16
Toluene-d8 (S)
%
99
70-130
07/06/20 12:16
v2
v2
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2930606
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1250
100
70-130
1,1,1-Trichloroethane
ug/kg
1250
1150
92
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1270
102
55-130
1,1,2-Trichloroethane
ug/kg
1250
1140
91
70-130
1,1-Dichloroethane
ug/kg
1250
1180
94
68-130
1,1-Dichloroethene
ug/kg
1250
1260
101
70-130
1,1-Dichloropropene
ug/kg
1250
1150
92
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
984
79
70-130 v3
1,2,3-Trichloropropane
ug/kg
1250
1280
103
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
968
77
70-130 v3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
LABORATORY CONTROL SAMPLE:
Parameter
2930606
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
ug/kg
1250
1110
89
69-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1300
104
57-141
1,2-Dibromoethane (EDB)
ug/kg
1250
1270
101
70-130
1,2-Dichlorobenzene
ug/kg
1250
1170
93
70-130
1,2-Dichloroethane
ug/kg
1250
1060
85
70-130
1,2-Dichloropropane
ug/kg
1250
1170
94
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1160
93
70-130
1,3-Dichlorobenzene
ug/kg
1250
1150
92
70-130
1,3-Dichloropropane
ug/kg
1250
1300
104
70-130
1,4-Dichlorobenzene
ug/kg
1250
1170
93
70-130
2,2-Dichloropropane
ug/kg
1250
1140
91
70-130
2-Butanone (MEK)
ug/kg
2500
2540
101
60-130
2-Chlorotoluene
ug/kg
1250
1270
102
70-130
2-Hexanone
ug/kg
2500
2810
112
70-132
4-Chlorotoluene
ug/kg
1250
1270
102
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2520
101
69-130
Acetone
ug/kg
2500
2520
101
49-148
Benzene
ug/kg
1250
1100
88
70-130
Bromobenzene
ug/kg
1250
1310
105
70-130
Bromochloromethane
ug/kg
1250
1280
102
70-130
Bromodichloromethane
ug/kg
1250
1060
85
70-130
Bromoform
ug/kg
1250
1280
102
68-136
Bromomethane
ug/kg
1250
983
79
60-140 v3
Carbon tetrachloride
ug/kg
1250
1150
92
70-130
Chlorobenzene
ug/kg
1250
1220
97
70-130
Chloroethane
ug/kg
1250
1350
108
51-147
Chloroform
ug/kg
1250
1160
92
70-130
Chloromethane
ug/kg
1250
1010
81
48-130
cis-1,2-Dichloroethene
ug/kg
1250
1220
97
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1170
94
70-130
Dibromochloromethane
ug/kg
1250
1330
107
70-130
Dibromomethane
ug/kg
1250
1160
93
70-130
Dichlorodifluoromethane
ug/kg
1250
1190
95
49-130
Diisopropyl ether
ug/kg
1250
1210
97
66-130
Ethylbenzene
ug/kg
1250
1100
88
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1080
86
70-130
Isopropylbenzene (Cumene)
ug/kg
1250
1070
86
70-130
m&p-Xylene
ug/kg
2500
2210
88
70-130
Methyl-tert-butyl ether
ug/kg
1250
1210
96
70-130
Methylene Chloride
ug/kg
1250
1240
99
50-137
n-Butylbenzene
ug/kg
1250
1020
82
70-130 v3
n-Propylbenzene
ug/kg
1250
1200
96
70-130
Naphthalene
ug/kg
1250
1240
99
70-131
o-Xylene
ug/kg
1250
1190
95
70-130
p-Isopropyltoluene
ug/kg
1250
1020
81
70-130 v3
sec-Butylbenzene
ug/kg
1250
1050
84
70-130
Styrene
ug/kg
1250
1270
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
LABORATORY CONTROL SAMPLE:
2930606
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
tert-Butyl benzene
ug/kg
1250
1060
85
69-130
Tetrachloroethene
ug/kg
1250
1160
93
56-130
Toluene
ug/kg
1250
1150
92
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1240
99
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1140
91
70-130
Trichloroethene
ug/kg
1250
1140
91
70-141
Trichlorofluoromethane
ug/kg
1250
1210
97
67-130
Vinyl acetate
ug/kg
2500
2700
108
10-136
Vinyl chloride
ug/kg
1250
1210
97
67-130
Xylene (Total)
ug/kg
3750
3400
91
70-130
1,2-Dichloroethane-d4 (S)
%
108
70-132
4-Bromofluorobenzene (S)
%
94
70-130
Toluene-d8 (S)
%
96
70-130
MATRIX SPIKE SAMPLE:
2932155
92484232002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
565
509
90
52-133
1,1,1-Trichloroethane
ug/kg
ND
565
496
88
49-137
1,1,2,2-Tetrachloroethane
ug/kg
ND
565
518
92
39-150
1,1,2-Trichloroethane
ug/kg
ND
565
499
88
48-140
1,1-Dichloroethane
ug/kg
ND
565
503
89
46-135
1,1-Dichloroethene
ug/kg
ND
565
215
38
38-149
1,1-Dichloropropene
ug/kg
ND
565
515
91
41-140
1,2,3-Trichlorobenzene
ug/kg
ND
565
291
52
10-158 v3
1,2,3-Trichloropropane
ug/kg
ND
565
516
91
33-157
1,2,4-Trichlorobenzene
ug/kg
ND
565
404
71
10-155 v3
1,2,4-Trimethylbenzene
ug/kg
ND
565
525
92
24-154
1,2-Dibromo-3-chloropropane
ug/kg
ND
565
332
59
33-158
1,2-Dibromoethane (EDB)
ug/kg
ND
565
509
90
40-136
1,2-Dichlorobenzene
ug/kg
ND
565
511
91
27-146
1,2-Dichloroethane
ug/kg
ND
565
462
82
49-140
1,2-Dichloropropane
ug/kg
ND
565
517
91
44-143
1,3,5-Trimethylbenzene
ug/kg
ND
565
524
93
40-144
1,3-Dichlorobenzene
ug/kg
ND
565
512
91
33-140
1,3-Dichloropropane
ug/kg
ND
565
538
95
47-147
1,4-Dichlorobenzene
ug/kg
ND
565
529
94
35-139
2,2-Dichloropropane
ug/kg
ND
565
411
73
41-140
2-Butanone (MEK)
ug/kg
ND
1130
742
66
10-181
2-Chlorotoluene
ug/kg
ND
565
551
98
38-147
2-Hexanone
ug/kg
ND
1130
839
74
18-169
4-Chlorotoluene
ug/kg
ND
565
555
98
36-145
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
1130
1020
91
16-175
Acetone
ug/kg
ND
1130
1440
128
10-200
Benzene
ug/kg
ND
565
500
88
46-136
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
MATRIX SPIKE SAMPLE:
2932155
92484232002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromobenzene
ug/kg
ND
565
542
96
38-149
Bromochloromethane
ug/kg
ND
565
538
95
44-142
Bromodichloromethane
ug/kg
ND
565
433
77
41-140
Bromoform
ug/kg
ND
565
466
82
34-145
Bromomethane
ug/kg
ND
565
410
73
14-162 v3
Carbon tetrachloride
ug/kg
ND
565
566
100
44-141
Chlorobenzene
ug/kg
ND
565
527
93
39-141
Chloroethane
ug/kg
ND
565
156
28
10-182
Chloroform
ug/kg
ND
565
484
86
45-140
Chloromethane
ug/kg
ND
565
497
88
19-149
cis-1,2-Dichloroethene
ug/kg
ND
565
504
89
38-150
cis-1,3-Dichloropropene
ug/kg
ND
565
485
86
30-144
Dibromochloromethane
ug/kg
ND
565
488
86
36-145
Dibromomethane
ug/kg
ND
565
479
85
41-145
Dichlorodifluoromethane
ug/kg
ND
565
548
97
16-146
Diisopropyl ether
ug/kg
ND
565
513
91
41-143
Ethylbenzene
ug/kg
ND
565
497
88
35-144
Hexachloro-1,3-butadiene
ug/kg
ND
565
596
105
10-160
Isopropylbenzene (Cumene)
ug/kg
ND
565
501
89
30-152
m&p-Xylene
ug/kg
ND
1130
1000
89
33-145
Methyl-tert-butyl ether
ug/kg
ND
565
501
89
49-140
Methylene Chloride
ug/kg
ND
565
555
98
10-174
n-Butylbenzene
ug/kg
ND
565
499
88
10-160
n-Propylbenzene
ug/kg
ND
565
539
95
24-159
Naphthalene
ug/kg
ND
565
280
49
10-171
o-Xylene
ug/kg
ND
565
538
95
31-150
p-Isopropyltoluene
ug/kg
ND
565
484
86
21-154 v3
sec-Butylbenzene
ug/kg
ND
565
497
88
19-159
Styrene
ug/kg
ND
565
529
94
15-152
tert-Butyl benzene
ug/kg
ND
565
501
89
31-141
Tetrachloroethene
ug/kg
ND
565
524
93
19-141
Toluene
ug/kg
ND
565
522
92
31-146
trans-1,2-Dichloroethene
ug/kg
ND
565
550
97
28-157
trans- 1,3-Dichloropropene
ug/kg
ND
565
453
80
25-146
Trichloroethene
ug/kg
ND
565
523
93
34-149
Trichlorofluoromethane
ug/kg
ND
565
133
24
10-167
Vinyl acetate
ug/kg
ND
1130
942
83
10-200
Vinyl chloride
ug/kg
ND
565
563
100
36-155
Xylene (Total)
ug/kg
ND
1690
1540
91
29-148
1,2-Dichloroethane-d4 (S)
%
121
70-132
4-Bromofluorobenzene (S)
%
95
70-130
Toluene-d8 (S)
%
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
SAMPLE DUPLICATE: 2932154
Parameter
Units
92484232001
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
1,1,1-Trichloroethane
ug/kg
ND
ND
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
1,1,2-Trichloroethane
ug/kg
ND
ND
1,1-Dichloroethane
ug/kg
ND
ND
1,1-Dichloroethene
ug/kg
ND
ND
1,1-Dichloropropene
ug/kg
ND
ND
1,2,3-Trichlorobenzene
ug/kg
ND
ND
1,2,3-Trichloropropane
ug/kg
ND
ND
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2,4-Trimethylbenzene
ug/kg
ND
6.0
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,2-Dichloroethane
ug/kg
ND
ND
1,2-Dichloropropane
ug/kg
ND
ND
1,3,5-Trimethylbenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichloropropane
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
2,2-Dichloropropane
ug/kg
ND
ND
2-Butanone (MEK)
ug/kg
ND
ND
2-Chlorotoluene
ug/kg
ND
ND
2-Hexanone
ug/kg
ND
ND
4-Chlorotoluene
ug/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
Acetone
ug/kg
ND
ND
Benzene
ug/kg
ND
ND
Bromobenzene
ug/kg
ND
ND
Bromochloromethane
ug/kg
ND
ND
Bromodichloromethane
ug/kg
ND
ND
Bromoform
ug/kg
ND
ND
Bromomethane
ug/kg
ND
ND
Carbon tetrachloride
ug/kg
ND
ND
Chlorobenzene
ug/kg
ND
ND
Chloroethane
ug/kg
ND
ND
Chloroform
ug/kg
ND
ND
Chloromethane
ug/kg
ND
ND
cis-1,2-Dichloroethene
ug/kg
ND
ND
cis-1,3-Dichloropropene
ug/kg
ND
ND
Dibromochloromethane
ug/kg
ND
ND
Dibromomethane
ug/kg
ND
ND
Dichlorodifluoromethane
ug/kg
ND
ND
Diisopropyl ether
ug/kg
ND
ND
Ethylbenzene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Isopropylbenzene (Cumene)
ug/kg
ND
ND
RPD Qualifiers
v2
v2
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
SAMPLE DUPLICATE: 2932154
Parameter
Units
92484232001
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
10
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
113
107
4-Bromofluorobenzene (S)
%
97
96
Toluene-d8(S)
%
101
99
RPD Qualifiers
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
QC Batch: 551267 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
METHOD BLANK: 2930328 Matrix: Solid
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
Blank Reporting
Parameter Units Result Limit Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
330
07/07/20 10:08
1,2-Dichlorobenzene
ug/kg
ND
330
07/07/20 10:08
1,3-Dichlorobenzene
ug/kg
ND
330
07/07/20 10:08
1,4-Dichlorobenzene
ug/kg
ND
330
07/07/20 10:08
1-Methylnaphthalene
ug/kg
ND
330
07/07/20 10:08
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
330
07/07/20 10:08
2,4,5-Trichlorophenol
ug/kg
ND
330
07/07/20 10:08
2,4,6-Trichlorophenol
ug/kg
ND
330
07/07/20 10:08
2,4-Dichlorophenol
ug/kg
ND
330
07/07/20 10:08
2,4-Dimethylphenol
ug/kg
ND
330
07/07/20 10:08
2,4-Dinitrophenol
ug/kg
ND
1650
07/07/20 10:08
2,4-Dinitrotoluene
ug/kg
ND
330
07/07/20 10:08
2,6-Dinitrotoluene
ug/kg
ND
330
07/07/20 10:08
2-Chloronaphthalene
ug/kg
ND
330
07/07/20 10:08
2-Chlorophenol
ug/kg
ND
330
07/07/20 10:08
2-Methylnaphthalene
ug/kg
ND
330
07/07/20 10:08
2-Methylphenol(o-Cresol)
ug/kg
ND
330
07/07/20 10:08
2-Nitroaniline
ug/kg
ND
1650
07/07/20 10:08
2-Nitrophenol
ug/kg
ND
330
07/07/20 10:08
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
330
07/07/20 10:08
3,3'-Dichlorobenzidine
ug/kg
ND
660
07/07/20 10:08
3-Nitroaniline
ug/kg
ND
1650
07/07/20 10:08
4,6-Dinitro-2-methyl phenol
ug/kg
ND
660
07/07/20 10:08
4-Bromophenylphenyl ether
ug/kg
ND
330
07/07/20 10:08
4-ChIoro-3-methyl phenol
ug/kg
ND
660
07/07/20 10:08
4-Chloroaniline
ug/kg
ND
660
07/07/20 10:08
4-Chlorophenylphenyl ether
ug/kg
ND
330
07/07/20 10:08
4-Nitroaniline
ug/kg
ND
660
07/07/20 10:08
4-Nitrophenol
ug/kg
ND
1650
07/07/20 10:08
Acenaphthene
ug/kg
ND
330
07/07/20 10:08
Acenaphthylene
ug/kg
ND
330
07/07/20 10:08
Aniline
ug/kg
ND
330
07/07/20 10:08
Anthracene
ug/kg
ND
330
07/07/20 10:08
Benzo(a)anthracene
ug/kg
ND
330
07/07/20 10:08
Benzo(a)pyrene
ug/kg
ND
330
07/07/20 10:08
Benzo(b)fluoranthene
ug/kg
ND
330
07/07/20 10:08
Benzo(g,h,i)perylene
ug/kg
ND
330
07/07/20 10:08
Benzo(k)fluoranthene
ug/kg
ND
330
07/07/20 10:08
Benzoic Acid
ug/kg
ND
1650
07/07/20 10:08
Benzyl alcohol
ug/kg
ND
660
07/07/20 10:08
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
METHOD BLANK: 2930328 Matrix: Solid
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
Blank Reporting
Parameter Units Result Limit Analyzed
bis(2-Chloroethoxy)methane
ug/kg
ND
330
07/07/20 10:08
bis(2-Chloroethyl) ether
ug/kg
ND
330
07/07/20 10:08
bis(2-Ethylhexyl)phthalate
ug/kg
ND
330
07/07/20 10:08
Butylbenzylphthalate
ug/kg
ND
330
07/07/20 10:08
Chrysene
ug/kg
ND
330
07/07/20 10:08
Di-n-butylphthalate
ug/kg
ND
330
07/07/20 10:08
Di-n-octylphthalate
ug/kg
ND
330
07/07/20 10:08
Dibenz(a,h)anthracene
ug/kg
ND
330
07/07/20 10:08
Dibenzofuran
ug/kg
ND
330
07/07/20 10:08
Diethylphthalate
ug/kg
ND
330
07/07/20 10:08
Dimethylphthalate
ug/kg
ND
330
07/07/20 10:08
Fluoranthene
ug/kg
ND
330
07/07/20 10:08
Fluorene
ug/kg
ND
330
07/07/20 10:08
Hexachloro-1,3-butadiene
ug/kg
ND
330
07/07/20 10:08
Hexachlorobenzene
ug/kg
ND
330
07/07/20 10:08
Hexachlorocyclopentadiene
ug/kg
ND
330
07/07/20 10:08
Hexachloroethane
ug/kg
ND
330
07/07/20 10:08
Indeno(1,2,3-cd)pyrene
ug/kg
ND
330
07/07/20 10:08
Isophorone
ug/kg
ND
330
07/07/20 10:08
N-Nitroso-di-n-propylamine
ug/kg
ND
330
07/07/20 10:08
N-Nitrosodimethylamine
ug/kg
ND
330
07/07/20 10:08
N-Nitrosodiphenylamine
ug/kg
ND
330
07/07/20 10:08
Naphthalene
ug/kg
ND
330
07/07/20 10:08
Nitrobenzene
ug/kg
ND
330
07/07/20 10:08
Pentachlorophenol
ug/kg
ND
660
07/07/20 10:08
Phenanthrene
ug/kg
ND
330
07/07/20 10:08
Phenol
ug/kg
ND
330
07/07/20 10:08
Pyrene
ug/kg
ND
330
07/07/20 10:08
Pyridine
ug/kg
ND
330
07/07/20 10:08
2,4,6-Tribromophenol (S)
%
57
27-110
07/07/20 10:08
2-Fluorobiphenyl (S)
%
55
30-110
07/07/20 10:08
2-Fluorophenol(S)
%
58
13-110
07/07/20 10:08
Nitrobenzene-d5 (S)
%
66
23-110
07/07/20 10:08
Phenol-d6 (S)
%
55
22-110
07/07/20 10:08
Terphenyl-d14 (S)
%
67
28-110
07/07/20 10:08
Qualifiers
LABORATORY CONTROL SAMPLE:
2930329
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1680
953
57
52-130
1,2-Dichlorobenzene
ug/kg
1680
1090
65
51-130
1,3-Dichlorobenzene
ug/kg
1680
1080
64
50-130
1,4-Dichlorobenzene
ug/kg
1680
1140
68
49-130
1-Methylnaphthalene
ug/kg
1680
971
58
55-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
LABORATORY CONTROL SAMPLE: 2930329
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
ug/kg
1680
1300
77
30-130
2,4,5-Trichlorophenol
ug/kg
1680
1070
64
55-130
2,4,6-Trichlorophenol
ug/kg
1680
1080
64
57-130
2,4-Dichlorophenol
ug/kg
1680
1030
61
56-130
2,4-Dimethylphenol
ug/kg
1680
1020
61
51-130
2,4-Dinitrophenol
ug/kg
8390
5350
64
27-133
2,4-Dinitrotoluene
ug/kg
1680
1060
63
61-130
2,6-Dinitrotoluene
ug/kg
1680
783
47
60-130 L2,v3
2-Chloronaphthalene
ug/kg
1680
1100
65
52-130
2-Chlorophenol
ug/kg
1680
1140
68
54-130
2-Methylnaphthalene
ug/kg
1680
1010
60
54-130
2-Methylphenol(o-Cresol)
ug/kg
1680
1100
66
51-130
2-Nitroaniline
ug/kg
3360
2220
66
51-130
2-Nitrophenol
ug/kg
1680
1060
63
49-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1680
1120
67
11-163
3,3'-Dichlorobenzidine
ug/kg
3360
1980
59
10-132
3-Nitroaniline
ug/kg
3360
1960
58
55-130
4,6-Dinitro-2-methyl phenol
ug/kg
3360
2290
68
47-142
4-Bromophenylphenyl ether
ug/kg
1680
1010
60
59-130
4-ChIoro-3-methyl phenol
ug/kg
3360
2050
61
55-130
4-Chloroaniline
ug/kg
3360
2100
63
54-130
4-Chlorophenylphenyl ether
ug/kg
1680
965
58
58-130
4-Nitroaniline
ug/kg
3360
2160
64
54-130
4-Nitrophenol
ug/kg
8390
4880
58
48-130
Acenaphthene
ug/kg
1680
1100
65
60-130
Acenaphthylene
ug/kg
1680
1130
68
60-130
Aniline
ug/kg
1680
1070
64
43-130
Anthracene
ug/kg
1680
1070
64
63-130
Benzo(a)anthracene
ug/kg
1680
1100
65
59-130
Benzo(a)pyrene
ug/kg
1680
1130
67
57-130
Benzo(b)fluoranthene
ug/kg
1680
1090
65
54-130
Benzo(g,h,i)perylene
ug/kg
1680
1140
68
59-130
Benzo(k)fluoranthene
ug/kg
1680
1090
65
54-130
Benzoic Acid
ug/kg
8390
4090
49
19-130
Benzyl alcohol
ug/kg
3360
2160
65
50-130
bis(2-Chloroethoxy)methane
ug/kg
1680
1030
61
54-130
bis(2-Chloroethyl) ether
ug/kg
1680
1080
65
48-130
bis(2-Ethylhexyl)phthalate
ug/kg
1680
1190
71
45-134
Butylbenzylphthalate
ug/kg
1680
1180
70
46-138
Chrysene
ug/kg
1680
1090
65
58-130
Di-n-butylphthalate
ug/kg
1680
1100
65
60-130
Di-n-octylphthalate
ug/kg
1680
1170
70
53-130
Dibenz(a,h)anthracene
ug/kg
1680
1070
64
59-130
Dibenzofuran
ug/kg
1680
1030
62
60-130
Diethylphthalate
ug/kg
1680
1060
63
60-130
Dimethylphthalate
ug/kg
1680
1050
62
60-130
Fluoranthene
ug/kg
1680
1040
62
65-130 L2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
LABORATORY CONTROL SAMPLE:
Parameter
2930329
Units
Spike
Conc.
Fluorene
ug/kg
1680
Hexachloro-1,3-butadiene
ug/kg
1680
Hexachlorobenzene
ug/kg
1680
Hexachlorocyclopentadiene
ug/kg
1680
Hexachloroethane
ug/kg
1680
Indeno(1,2,3-cd)pyrene
ug/kg
1680
Isophorone
ug/kg
1680
N-Nitroso-di-n-propylamine
ug/kg
1680
N-Nitrosodimethylamine
ug/kg
1680
N-Nitrosodiphenylamine
ug/kg
1680
Naphthalene
ug/kg
1680
Nitrobenzene
ug/kg
1680
Pentachlorophenol
ug/kg
3360
Phenanthrene
ug/kg
1680
Phenol
ug/kg
1680
Pyrene
ug/kg
1680
Pyridine
ug/kg
1680
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1060
63
63-130
871
52
46-130
1050
62
58-130
887
53
23-130
1080
65
47-130
1150
69
60-130
1020
61
49-130
1040
62
47-130
1190
71
45-130
1160
69
59-130
1060
63
55-130
1040
62
49-130
2090
62
10-132
1090
65
62-130
1250
75
46-130
1150
68
53-130
971
58
37-130
59
27-110
58
30-110
63
13-110
56
23-110
64
22-110
66
28-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2930330
MS
92484482001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2930331
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/kg
ND
2020
2000
1050
991
52
49
18-130
6
1,2-Dichlorobenzene
ug/kg
ND
2020
2000
1090
1010
54
50
14-130
8
1,3-Dichlorobenzene
ug/kg
ND
2020
2000
1100
1050
55
52
12-130
5
1,4-Dichlorobenzene
ug/kg
ND
2020
2000
1140
1070
57
54
10-130
6
1-Methylnaphthalene
ug/kg
ND
2020
2000
1020
938
50
47
12-130
8
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
2020
2000
1080
1010
54
50
10-130
7
2,4,5-Trichlorophenol
ug/kg
ND
2020
2000
1130
1010
56
51
13-130
11
2,4,6-Trichlorophenol
ug/kg
ND
2020
2000
1060
960
53
48
17-130
10
2,4-Dichlorophenol
ug/kg
ND
2020
2000
1110
1010
55
50
10-130
10
2,4-Dimethylphenol
ug/kg
ND
2020
2000
948
862
47
43
10-130
9
2,4-Dinitrophenol
ug/kg
ND
10100
10000
3680
3680
37
37
10-130
0
2,4-Dinitrotoluene
ug/kg
ND
2020
2000
1050
955
52
48
24-130
10
2,6-Dinitrotoluene
ug/kg
ND
2020
2000
1070
983
53
49
23-130
9
2-Chloronaphthalene
ug/kg
ND
2020
2000
1010
954
50
48
19-130
5
2-Chlorophenol
ug/kg
ND
2020
2000
1160
1090
58
54
10-130
7
2-Methylnaphthalene
ug/kg
ND
2020
2000
1050
972
52
48
18-130
8
2-Methylphenol(o-Cresol)
ug/kg
ND
2020
2000
1070
976
53
49
10-130
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
Page 44 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2930330
2930331
MS
MSD
92484482001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
2-Nitroaniline
ug/kg
ND
4020
4010
2230
2040
55
51
17-130
9
2-Nitrophenol
ug/kg
ND
2020
2000
1130
1060
56
53
10-130
6
3&4-Methyl phenol (m&p
ug/kg
ND
2020
2000
1060
997
53
50
10-130
6
Cresol)
3,3'-Dichlorobenzidine
ug/kg
ND
4020
4010
1420
1470
35
37
10-130
4
3-Nitroaniline
ug/kg
ND
4020
4010
1920J
1720J
48
43
24-130
4,6-Dinitro-2-methyl phenol
ug/kg
ND
4020
4010
1780
1790
44
45
10-152
1
4-Bromophenylphenyl ether
ug/kg
ND
2020
2000
980
924
49
46
29-130
6
4-ChIoro-3-methyl phenol
ug/kg
ND
4020
4010
2250
1980
56
49
17-130
13
4-Chloroaniline
ug/kg
ND
4020
4010
1840
1940
46
48
14-130
5
4-Chlorophenylphenyl ether
ug/kg
ND
2020
2000
930
845
46
42
25-130
10
4-Nitroaniline
ug/kg
ND
4020
4010
1990
1850
49
46
22-130
7
4-Nitrophenol
ug/kg
ND
10100
10000
5120
4570
51
46
10-130
12
Acenaphthene
ug/kg
ND
2020
2000
1020
950
51
47
20-130
8
Acenaphthylene
ug/kg
ND
2020
2000
1030
946
51
47
25-130
9
Aniline
ug/kg
ND
2020
2000
646
724
32
36
10-130
11
Anthracene
ug/kg
ND
2020
2000
951
896
47
45
29-130
6
Benzo(a)anthracene
ug/kg
ND
2020
2000
930
870
46
43
19-130
7
Benzo(a)pyrene
ug/kg
ND
2020
2000
907
844
45
42
12-130
7
Benzo(b)fluoranthene
ug/kg
ND
2020
2000
866
809
43
40
14-130
7
Benzo(g,h,i)perylene
ug/kg
ND
2020
2000
947
909
47
45
10-130
4
Benzo(k)fluoranthene
ug/kg
ND
2020
2000
920
861
46
43
14-130
7
Benzoic Acid
ug/kg
ND
10100
10000
2620
2240
26
22
10-130
16
Benzyl alcohol
ug/kg
ND
4020
4010
2260
2090
56
52
13-130
8
bis(2-Chloroethoxy)methane
ug/kg
ND
2020
2000
1080
1000
54
50
16-130
7
bis(2-Chloroethyl) ether
ug/kg
ND
2020
2000
1150
1070
57
53
11-130
7
bis(2-Ethylhexyl)phthalate
ug/kg
ND
2020
2000
889
867
44
43
21-130
3
Butylbenzylphthalate
ug/kg
ND
2020
2000
848
848
42
42
23-130
0
Chrysene
ug/kg
ND
2020
2000
943
904
47
45
22-130
4
Di-n-butylphthalate
ug/kg
ND
2020
2000
868
835
43
42
30-130
4
Di-n-octylphthalate
ug/kg
ND
2020
2000
879
826
44
41
23-142
6
Dibenz(a,h)anthracene
ug/kg
ND
2020
2000
971
910
48
45
10-130
6
Dibenzofuran
ug/kg
ND
2020
2000
1030
945
51
47
24-130
9
Diethylphthalate
ug/kg
ND
2020
2000
1020
953
51
47
26-130
7
Dimethylphthalate
ug/kg
ND
2020
2000
1090
1000
54
50
22-130
8
Fluoranthene
ug/kg
ND
2020
2000
906
813
45
41
33-130
11
Fluorene
ug/kg
ND
2020
2000
974
899
48
45
22-130
8
Hexachloro-1,3-butadiene
ug/kg
ND
2020
2000
996
954
49
48
13-130
4
Hexachlorobenzene
ug/kg
ND
2020
2000
958
903
48
45
29-130
6
Hexachlorocyclopentadiene
ug/kg
ND
2020
2000
498
514
25
26
10-130
3
Hexachloroethane
ug/kg
ND
2020
2000
1070
1010
53
51
10-130
5
Indeno(1,2,3-cd)pyrene
ug/kg
ND
2020
2000
966
900
48
45
10-130
7
Isophorone
ug/kg
ND
2020
2000
1130
1040
56
52
13-130
9
N-Nitroso-di-n-propylamine
ug/kg
ND
2020
2000
1120
1020
56
51
12-130
9
N-Nitrosodimethylamine
ug/kg
ND
2020
2000
1120
1080
56
54
11-130
3
N-Nitrosodiphenylamine
ug/kg
ND
2020
2000
1020
961
51
48
15-130
6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2930330
2930331
MS
MSD
92484482001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Naphthalene
ug/kg
ND
2020
2000
1100
1020
55
51
15-130
8
Nitrobenzene
ug/kg
ND
2020
2000
1150
1060
57
53
12-130
8
Pentachlorophenol
ug/kg
ND
4020
4010
1910
1670
48
42
10-130
14
Phenanthrene
ug/kg
ND
2020
2000
985
915
49
46
27-130
7
Phenol
ug/kg
ND
2020
2000
1090
1020
54
51
10-130
7
Pyrene
ug/kg
ND
2020
2000
924
931
46
46
19-130
1
Pyridine
ug/kg
ND
2020
2000
856
992
43
49
10-130
15
2,4,6-Tribromophenol (S)
%
54
53
27-110
2-Fluorobiphenyl (S)
%
46
46
30-110
2-Fluorophenol(S)
%
54
53
13-110
Nitrobenzene-d5(S)
%
52
51
23-110
Phenol-d6 (S)
%
53
51
22-110
Terphenyl-d14(S)
%
40
43
28-110
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 54

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
QC Batch: 551093 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
METHOD BLANK: 2929351
Matrix:
Solid
Associated Lab Samples:
92484342001, 92484342002,
92484342003, 92484342004, 92484342005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10
07/08/20 16:37 N2
Aliphatic (C19-C36)
mg/kg
ND
10
07/08/20 16:37 N2
Aromatic (C11-C22)
mg/kg
ND
10
07/08/20 16:37 N2
2-Bromonaphthalene (S)
%
85
40-140
07/08/20 16:37
2-Fluorobiphenyl (S)
%
85
40-140
07/08/20 16:37
o-Terphenyl (S)
%
73
40-140
07/08/20 16:37
LABORATORY CONTROL SAMPLE & LCSD:
2929352
2929353
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
9.9
ND ND
53
53
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.2
ND ND
63
65
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.1
18.0 18.9
64
66
40-140 5 50 N2
2-Bromonaphthalene (S)
%
87
82
40-140
2-Fluorobiphenyl (S)
%
84
79
40-140
o-Terphenyl(S)
%
73
73
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
Page 47 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
QC Batch: 550882 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
SAMPLE DUPLICATE: 2928437
92484342001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 20.7 21.1 2
SAMPLE DUPLICATE: 2928438
92484306009 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 20.7 20.5 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
QC Batch: 1506139 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92484342001, 92484342002, 92484342003, 92484342004, 92484342005
METHOD BLANK: R3548101-1
Matrix:
Solid
Associated Lab Samples: 92484342001, 92484342002,
92484342003, 92484342004,
92484342005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Solids
%
0.00100
07/09/20 14:17
LABORATORY CONTROL SAMPLE:
R3548101-2
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Solids
%
50.0
50.0
99.9 85.0-115
SAMPLE DUPLICATE: R3548101-3
L1236263-09 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids % 86.2 84.8 1.58
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 54

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 18100 STATESVILLE RD
Pace Project No.: 92484342
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2020 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 54

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
18100 STATESVILLE RD
92484342
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92484342001
NW (10)
MADEP EPH
551093
MADEP EPH
552081
92484342002
EW (10)
MADEP EPH
551093
MADEP EPH
552081
92484342003
SW (10)
MADEP EPH
551093
MADEP EPH
552081
92484342004
WW (10)
MADEP EPH
551093
MADEP EPH
552081
92484342005
BOT (14.5)
MADEP EPH
551093
MADEP EPH
552081
92484342001
NW (10)
MADEPV
1505748
MADEP VPH
1505748
92484342002
EW (10)
MADEPV
1505748
MADEP VPH
1505748
92484342003
SW (10)
MADEPV
1505748
MADEP VPH
1505748
92484342004
WW (10)
MADEPV
1505748
MADEP VPH
1505748
92484342005
BOT (14.5)
MADEPV
1505748
MADEP VPH
1505748
92484342001
NW (10)
EPA 3546
551267
EPA 8270E
551511
92484342002
EW (10)
EPA 3546
551267
EPA 8270E
551511
92484342003
SW (10)
EPA 3546
551267
EPA 8270E
551511
92484342004
WW (10)
EPA 3546
551267
EPA 8270E
551511
92484342005
BOT (14.5)
EPA 3546
551267
EPA 8270E
551511
92484342001
NW (10)
EPA 5035A/5030B
551292
EPA 8260D
551308
92484342002
EW (10)
EPA 5035A/5030B
551292
EPA 8260D
551308
92484342003
SW (10)
EPA 5035A/5030B
551292
EPA 8260D
551308
92484342004
WW (10)
EPA 5035A/5030B
551292
EPA 8260D
551308
92484342005
BOT (14.5)
EPA 5035A/5030B
551292
EPA 8260D
551308
92484342001
NW (10)
ASTM D2974-87
550882
92484342002
EW (10)
ASTM D2974-87
550882
92484342003
SW (10)
ASTM D2974-87
550882
92484342004
WW (10)
ASTM D2974-87
550882
92484342005
BOT (14.5)
ASTM D2974-87
550882
92484342001
NW (10)
SM 2540 G
1506139
SM 2540G
1506139
92484342002
EW (10)
SM 2540 G
1506139
SM 2540G
1506139
92484342003
SW (10)
SM 2540 G
1506139
SM 2540G
1506139
92484342004
WW (10)
SM 2540 G
1506139
SM 2540G
1506139
92484342005
BOT (14.5)
SM 2540 G
1506139
SM 2540G
1506139
Date: 07/10/2020 05:12 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 51 of 54

Document Name:
Document Revised: February 7, 2018
a
_ aeeAnalXieal
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
I Issuing Authority:
F-CAR-CS-033-Rev.06
I Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑
i Sample Condition Client Name
Upon Receipt: / Wp# : 92484342
��G`/t:/1 ✓ 1 Project#:
Courier:
❑Dun U5p5 ❑CRent
commercial
❑ ❑Pa e❑Other 92484342
I
Custody Seal Present? Des ❑No Seals Intact? []Yes ❑No
f , J
Hatellnitlals Person Examining Contents:
Packing Material: ❑Isubble Wrap ❑Subbie Sags []None ❑ other Biological Tissue Frozen?
Thermometer: []Yes [:]No ❑N/A
❑ fB Gun ID: 92TO6 t Type of Ice: ❑Wet []Blue [:]None
Cooler Temp (°C): } Correction Factor: Add/Subtract ("C) +Q 1
Temp should be above freezing to VC
Cooler Temp Corrected ('C): ❑Samples out of temp criteria. samples on ice, cooling process
has begun
USDA Regulated $oil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samsesonginate from a foreign source {internationally,
IlYes n, Na indudineHawaii and Puerto Ricol? MYes -FlNo
Comments/Dlscre ancy:
Chain of Custody Present?
0 Yes
[:]No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
ELN.
❑N/A
2.
Short Hold Time Analysis (e72 hr.)?
DYes
❑No
❑N/A
3,
Rush Turn Around Time Requested?
Dyes
❑No
❑N/A
4.
Sufficient Volume?
❑Yes
❑No
[]N/A
S.
Correct Containers Used?
-Pace Containers Used?
OYU
Dies
❑No
❑No
❑N/A
❑N/A
5.
Containers Intact?
©Ves�
❑Na
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[:]No
❑N/A
8.
�e s
rINo
N A
9.
Includes Date/Time/ID/Analysis Matrix:
Heads ace in VOA Vials (>5-Gmm)?
❑Yes
[]No
j /A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]Yes❑No
❑No
❑O1(/A
IJN/A
11.
COMMENTS/SAMPLE DISCREPANCY
NT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Lot ID of spit containers:
Date:
Date:
field Data Required? ❑Yes [—]No
Page 52 of 54

Document Name:
document Revised: February 7, 2018
ceAr7$fytrca!
Sample Condition Upon Recef t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F•CAR-CS-033-Rev.05
Pace Carol Inas Quality Office
*Check mark top half of box if pH and/or dethlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: v0A, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, U.Hg
"Bottom half of box is to list number of bottle
Project t WO# : 92484342
PM: KLH1 Due Date: 07/09/20
CLIENT: 92—Harmon En
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PH Adjustment log for Preserved Samples
Sample 10
Type of Preservative
PH upon receipt
- -
Date preservation adjusted
Time prose rvcon
adjusted
Amount of Preservative
added
Lot #
-
Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy or this form will be sent to the North Carolina DEHNR Certification Office (Le.
out of hold, Incorrect preservative, out of temp, incorrect containers.
Page 53 of 54

Appendix K
Photographs of Site Check, Closure and Excavation

t
Z �. 3
-
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r N 20
ZOO -^
4 r- 7o m
_.
ti
n >�Zi
0D
.,
N
PHOTOGRAPH 2
PHOTOGRAPH 1
VIEW OF THE GEO HYDRO ENGINEERS, INC. BACKFILLED SITE PRIOR TO
VIEW OF ON -SITE WATER SUPPLY WELL.
INITIATING ADDITIONAL EXCAVATION.
.r
-
(1i..
�_ _Ab
rn 0
m p p
-
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Q r
- RMER CAVR
t 8 jj FIL
.'�� _ ter• __
r
.�i.•
(l A
ram, its �`2,^
iy4
PHOTOGRAPH 3
PHOTOGRAPH 4
VIEW OF SOUTH WALL OF JUNE 30, 2020 EXCAVATION WITH APPARENT
VIEW OF THE FINAL EXCAVATION. NOTE THE CONCRETE FOOTING EXPOSED
BACKFILL LINE FROM PREVIOUS EXCAVATION.
NEAR THE NORTHEAST CORNER OF THE EXCAVATION.
D/A(1' 1010Hd 10-848

Appendix L
Geologic Log of the Excavation

BORING/WELL NO.: UST EXCAVATION
EXCAVATION LOG
PROJECT NAME: GRIGG PROPERTY
PROJECT NO.: 848-01
HARMON ENVIRONMENTAL, PA
CONTRACTOR: PGP SERVICE INC.
OPERATOR: FRANK GRAVELLY
615 BRUCE THOMAS ROAD
METHOD: TRACKHOE
MONROE, NORTH CAROLINA 28112
DATE: JUNE 30, 2020
704-292-4527
ELEVATION: NO MEASURED
HARMONENVIRONMENTAL.COM
DEPTH
SAMPLING
SAMPLE
REMARKS/
(FEET)
METHOD
DESCRIPTION
COMMENTS
BACKHOE
FILL SOIL INSTALLED BY HYDRO-GEO
ENGINEERS, INC.
10.0
TAN, RED AND BLACK MOTTLED MICACEOUS
SILTY SAND (RESIDUAL SOIL)
14.5
EXCAVATION TERMINATED AT 14.5 FEET

Appendix M
Monitor Well Construction Forms
(This Appendix is not applicable to this project)

Beverly, Trudy
From: Beverly, Trudy
Sent: Friday, July 17, 2020 8:22 AM
To: Rick Harmon
Cc: Jeff Bazow; Carol Jones Van Buren
Subject: RE: [External] Griggs Property Initial Abatement Report (Incident No. 47089)
Received.
Good Morning Rick — The UST Section transitioned to electronic report submittals at the end of March. We no longer
require paper copies of reports. You are welcome to mail a physical copy, but are no longer required to do so.
Have a great day,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
QQ J) UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://dea.ne. eov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaeement-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
htt2s://deg.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.eov/nedea/Waste%2OManaeement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.])df
https:Hfiles.nc.gov/ncdeq/Waste%20Management/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Rick Harmon [maiIto: [e-mail]]
Sent: Friday, July 17, 2020 8:15 AM
To: Beverly, Trudy <[e-mail]>
Cc: Jeff Bazow <[e-mail]>; Carol Jones Van Buren <[e-mail]>
Subject: [External] Griggs Property Initial Abatement Report (Incident No. 47089)
��n
rnal email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
c. ov
Ms. Beverly:
Attached please find a digital copy of an Initial Abatement Action Report for the Griggs Property non-
commercial, non -regulated, heating oil underground storage tank (UST) former located at 18100 Statesville
Road, in Cornelius, North Carolina. As indicated in this report, analytical data associated with the confirmatory
samples did not indicate the presence of petroleum -constituents remaining at concentrations exceeding the

North Carolina Department of Environmental Quality (DEQ) action levels. As a result, Harmon
Environmental, PA respectfully requests the DEQ consider issuing a "no further action" letter for this incident.
A digital copy of this report and the transmittal letter are also being sent to your office by US Mail. Please call
or email if you have any questions or require any additional information.
Richard Harmon, P.G.
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
harmonenvironmental.com