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MO-88778_95759_CA_IAR_20200612_Initial Abatement Report
IDLD ENGINEERING, INC. June 12, 2020 Ms. Trudy Beverly NCDEQ Mooresville Regional Office 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Subject: Initial Abatement Report — Concrescere One 10900 Sudbury Road, Davidson, North Carolina Shield Project No. 4200160-01 Latitude: North 35.48560; Longitude: West-80.76190 Dear Ms. Beverly: Shield Engineering, Inc. (Shield) is, on behalf of Wayne Brothers Companies, pleased to submit this Initial Abatement Report and Request for No Further Action. On April 21, 2020, there was a release of used motor oil and hydraulic oil at the Wayne Brothers facility at 10900 Sudbury Road in Davidson, North Carolina. (Please see the site location map in Figure 1.) A construction crew was breaking rocks and a piece of rock struck a tote holding the oil. Approximately 50-100 gallons of oil was released and flowed across a soil area into a stream and through a culvert. (See photos in Appendix A.) Wayne Brothers cleaned up the soil release with backhoes and other equipment. Wayne Brothers also cleaned up the discharge to the stream with sorbent boom(s) and pads. The release was reported to the North Carolina Department of Environmental Quality (NCDEQ) by phone and a UST-61 Form dated April 22, 2020. (Form is attached as Appendix B.) On May 15, 2020, Shield Engineering, Inc. went to the site to assess and document the cleanup. Post -cleanup confirmation soil and surface water samples were collected by Shield following procedures established by the NCDEQ. All of Shield's sample results were below the most stringent NCDEQ Maximum Soil Contaminant Concentrations (MSCCs) and NC Surface Water Standards. Based on the cleanup work and sample results Shield requests a "No Further Action" determination from the NCDEQ. Soil Assessment and Excavation Following the sampling and analyses protocol established in discussions with NCDEQ, Shield collected one soil sample for every 20-foot length of soil excavation area. The soil samples were analyzed based on the NCDEQ guidelines for volatile organic compounds by EPA Method 8260B, semi -volatile organic compounds by EPA Method 8270D, Massachusetts Department of Environmental Protection volatile and extractable petroleum hydrocarbons, total chromium and lead using EPA Prep method 3050B or 3051A pesticides by EPA Method 8081B, and polychlorinated biphenyls by EPA Method 8082A. 4301 Taggart Creek Road www.shieldengineering.com Telephone 704.394.6913 Charlotte, NC 28208 Fax 704.394-6913 Initial Abatement Report — Concrescere One 10900 Sudbury Road Davidson, North Carolina Shield Project No. 4200160-01 June 12, 2020 Page 2 Shield notified the NCDEQ Water Quality Section about the release to surface water and the NCDEQ Land Quality Section about the release to the stormwater culvert. Shield proceeded with sampling based on direction from the Supervisor of the Water Quality Section. Shield contacted the Supervisor of the Land Quality Section who said the NCDEQ Underground Storage Tanks Section and the Water Quality Section would handle this incident. Post Excavation Sampling and Analyses On May 15, 2020, Shield personnel evaluated the soil excavation area. The soil excavation area was approximately 80 feet in length, requiring approximately four soil samples. Soil samples were collected approximately every 20 feet along the remediated area from a depth of 0-6 inches below the remediated area. One background soil sample was also collected from an upgradient location of the site. Samples were collected using a decontaminated stainless -steel hand auger. The samples were all placed in laboratory containers and transported on ice under Chain -of -Custody protocol to the laboratory. (See sample locations in Figure 2.) The soil samples were analyzed by Pace Analytical Services (Pace), a North Carolina certified laboratory. The samples were analyzed for volatile organic compounds by EPA Method 826013, semi - volatile organic compounds by EPA Method 8270D, Massachusetts Department of Environmental Protection volatile and extractable petroleum hydrocarbons, total chromium, and lead using EPA Prep method 3050B or 3051A pesticides by EPA Method 80816, and polychlorinated biphenyls by EPA Method 8082A. Of all the analyses conducted, only aliphatics in the C19-C36 range, chromium, and lead were detected in the soil samples. The levels detected were orders of magnitude below the most stringent of the NCDEQ MSCCs. The analytical results can be seen in Table 1 and are attached in Appendix C. The stream was evaluated, and a slight sheen was detected. (See the photos in Appendix A.) A surface -water grab sample was collected immediately downgradient of the cleanup area and the culvert from a depth of 0-6 inches. A second surface water grab sample was collected upstream of the remediated area from a depth of 0-6 inches. The surface -water samples were all placed in laboratory containers and transported on ice under Chain -of -Custody protocol to the laboratory. (See sample locations in Figure 2.) The surface water samples were also analyzed by Pace. The surface water samples were analyzed for oil and grease by EPA Method 1664B with heavy metals analyses put on hold pending the oil and grease results. The oil and grease surface water analytical results were non -detect (ND). Therefore, the sample results are below the 15A North Carolina Administrative code 2B Surface Water Standards. For this reason, the heavy metals analyses were not conducted. Initial Abatement Report—Concrescere One 10900 Sudbury Road Davidson, North Carolina Shield Project No. 4200160-01 June 12, 2020 Page 3 Disposal and Site Restoration The contaminated spill material and soil was disposed at Republic's landfill in Concord, North Carolina. The amount totaled 35.92 tons. A non -hazardous waste disposal manifest is included in Appendix D. The area was restored to its pre -spill condition. Conclusions On April 21, 2020, there was a release of used motor oil and hydraulic oil at the Wayne Brothers facility at 10900 Sudbury Road in Davidson, North Carolina. Approximately 50-100 gallons of oil was released and flowed across a soil area into a stream and through a culvert. Wayne Brothers cleaned up the soil release with backhoes and other equipment. Wayne Brothers cleaned up the discharge to water with sorbent boom(s) and pads. The release was reported to the NCDEQ. On May 15, 2020, Shield went to the site to assess and document the cleanup. Post -cleanup confirmation soil and surface water samples were collected by Shield following procedures established by the NCDEQ. All samples were below the most stringent NCDEQ MSCCs and NC Surface Water Standards. Based on the cleanup work and sample results below the NCDEQ MSCCs and NC Surface Water Standards, Shield is requesting a "No Further Action" determination from the NCDEQ. If you have any questions regarding the content of this report, please contact David Stoner, signatory below. Sincerely, aie ii�P eP SHIELD ENGINEERING,,INC. A Lw David A. Stoner, P.G.; P.E. Senior Principal/Vice President f 0ti 11 f� _y; 9 Robert L. Griffin, P.E. CEO/President Attachments: Figure 1—Site Location Map Figure 2 —Site Map Table 1— Summary of Laboratory Analytical Data Appendix A — Photo Log Appendix B — UST-61 Form Appendix C—Analytical Results Appendix D — Non -Hazardous Waste Disposal Manifest cc: Mr. Corey Basinger, NCDEQ Water Quality Section via e-mail Mr. Alan Goodman, Wayne Brothers via e-mail FIGURES DSO ' ' - 80p f SUGARHILL R� \ FgRN I JJ 1 moo tiJ—)SO „ `` �QQ`01 •r,SFy� `1�t> i. h�A4 cnp O 1 � l O 609 • 0��_ _ TFRR/LURI% DR (/1 J \ r< v VO d �. �i v �g50 = 0 1y 1 $ - -` HIDDEN F REL ST N NW �. wo 3S �j 750 Jh0 cr 700 J � �.1•TRL _ DSO �� ��� � o 50, k uj o� -u6- o�� � 1' ` rj M � � � ti it �, zl � ✓�J� a� 1 a - � L40oGf�RI f,, 10 i. F��CN E SAS AM RQ \ xf LNAPOLIS o�rf 1��/a kc 0 NGRAPHIC SCALE 4301 TAGGART CREEK ROAD 0 1,000 2,000 _,SHIELD CHARLOTTE, NC 28208 704-394-6913 704-394-6968 fax SCALE: 1 in. = 2,000 ft. ENGINEERING, INC. www. shlelaen9ineering.com SITE LOCATION MAP CONCRESCERE ONE 10900SUDBURY LANE DAVIDSON, NORTH CAROLINA SHIELD # 4200160-01 SOURCE: USGS TOPO, 7.5 MINUTE MAP, CORNELIUS QUADRANGLE, NORTH DATE : 05/21 /20 DRAWN BY: KJC CAROLINA SCALE : AS SHOWN FIGURE : 1 L L , LEGEND: APPROXIMATE SAMPLE OR TEST LOCATION HA- # INDICATES HAND AUGER LOCATION SIN- # INDICATES SURFACE WATER SAMPLE LOCATION B 9 .J ! -\ f 4• , r 1 +440 1L. N- NOTES: I .BASE MAP FROM GOOGLE MAPS. DATE 2. ALL LOCATIONS ARE APPROXIMATE. SCALE 94-6913 SHIELD704-394-696804RL0 CHARLOTTE, CREEK82 $ROAD ENGINEERING, INC. SAMPLE LOCATION MAP CONCRESCERE ONE 10900SUDBURY ROAD DAVIDSON, NORTH CAROLINA SHIELD # 4200160-01 05/21 /20 DRAWN BY: KJC N.T.S. I FIGURE : 2 TABLES Table 1 Summary of Laboratory Analytical Data Wayne Brothers - Concrescere One 10900 Sudbury Road, Davidson, NC MADEP Extractable MADEP Volatile Semi -Volatile Volatile Sample Petroleum Oil and Sample Date Media Pesticides PCBs Petroleum Chromium Organic Organic Depth Hydrocarbons Lead(mg/kg) Grease Location Sampled Sampled (ug/kg) (ug/kg) Hydrocarbons (mg/kg) Compounds Compounds (Feet) (mg/kg) Only (mg/0 (mg/kg) (ug/kg) (ug/kg) Aliphatics C19- 36 Detected Non - State Standards—> Various Various 31,000 Various 4200 Cr III 270 Various 270 injurious HA-1 5/15/2020 Soil 0-.5' ND ND ND ND 15.1 1.1 ND ND NA HA-2 5/15/2020 Soil 0-.5' ND ND 16.5 ND 120 8.2 ND ND NA HA-3 5/15/2020 Soil 0-.5' ND ND 58.3 ND 56.5 9.4 ND ND NA HA-4 5/15/2020 Soil 0-.5' ND ND ND ND 44.7 11.9 ND ND NA Background 5/15/2020 Soil 0-.5' ND ND ND ND 79.6 9.4 ND ND NA Surface SW-1 5/15/2020 Water 0-.5' NA NA NA NA NA NA NA NA ND Surface SW-2 5/15/2020 Water 0-5 NA NA NA NA NA NA NA NA ND NOTES: ND = Not detected NA = Not required to be analyzed ug/kg = micrograms per kilogram mg/kg = milligrams per kilogram mg/I = milligrams per liter PCBs = Polychlorinated biphenyls MADEP = Massachusetts Department of Environmental Protection State Standards for soil are the most stringent of the NCDEQ Maximum Soil Contaminant Concentrations; for surface water are the NCDEQ Surface Water Standards NCDEQ = North Carolina Department of Environmental Quality APPENDIX A APPENDIX B UST-61 I 24-Hour Release and UST Leak Reporting Form. For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release (DW M USE ONLY) Suspected Contamination? (YIN) Facility ID Number Incident # Risk (H,I,L,U) Confirmed GW Contamination? (YIN) Date Leak Discovered Received On Received By Confirmed Soil Contamination ?(YIN) Comm/Non-Commercial? Reported by (circle one): Phone, Fax or Report Samples Taken?(YIN) Reg/Non-regulated? Region Free Product? (YIN) If Yes, State Greatest Thickness INCIDENT DESCRIPTION Incident Name: cnJ•Crt?SCCrE 0IV i' Address: 10 9 0 0 -S Ll U i s o A County: C A 6 Fl r r u _5 City/Town: DAutd`` SaN. CSO� Zip Code: Regional Office (circle one): Asheville Mooresville Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem Latitude (decimal degrees): Longitude (decimal degrees): Obtained by: ❑GPS Briefly describe suspected or confirmed release: (including but not limited to nature of release, date of release, amount of release, amount of free product resent and recoveryefforts, responses conducted, impacts to rece tors `initial 4afe -i cr njQi V"r-,i+'c:k FIkcvT ,J-WA . TN ,dr. -j .fake QCr,j,,,l ❑Topographic map ❑GISAddressmatching ❑Other ❑ Unknown Describe location: laLJt3D S��i�ur� �c� DAe5Nr o, J\JL J itI �a. L9Fl u1A� dirJr(Jvz;e+ tl as �a �} la'I/s�l�l. A r xrn�Fel,a 5t1-IDOjovs 01 &VA5 fPIeASeC. rrfx,Ala-)e) It30 0 l�rh� lvsls ,uc4 rC1F.Ase='l. r Ic AO 1N40 ++ 1 l? 5 4� Fa y r il,fi i f{ y t 1 1 I t� Oi C!\._ lAeA IN o IDW t/CLJ 5-1r-P�il�l. c-j(fljor I)j:J blr 4 tji SCt 10,C14e. t ! -(•1Prl i rfP1,v�'Ct bL e.vd n tb)L/ 41f,���1Xtnvin(er�. )wLl: F1NL+ S�a,er} rnV 1iNed -1 CbUfrCj. Cr( i 56t1 Iu,lj be 11VoLejj 0-f i+, rOvFCI 517�. gp HOW RELEASE WAS DISCOVERED (Release Code) (Check one) ❑Release Detection Equipment or Methods >❑" VisuallOdor ❑Groundwater Contamination [:]During UST Closure/Removal ❑Water in Tank ❑Surface Water Contamination ❑Property Transfer ❑Water Supply Well Contamination ❑Other (specify) SOURCE OF CONTAMINATION Source of Release Cause of Release Type of Release Product Type Released (Check primary source) (Check primary cause) (Check one) (Check primary ry product type released) ❑ Tank ❑ Spill a> Petroleum ❑ Gasohnel Dieseil ❑ Diesel/Veg. ail Piping Kerosene Blend P g ill ❑Non -Petroleum ❑ Heating Oil ❑ Vegetable Oil 100% ❑ Dispenser ❑Corrosion ❑Bath Other Petroleum ❑ E10 — E2Q ❑ Submersible Turbine Pump ❑ Physical/Mechanicai Location Products ❑ Delivery Problem Damage ❑ E21 — E84 (Check one) El metals ❑ Install Problem El Spill Bucket ❑ E85 — E99 ❑ Other QFacility ❑Other Inorganics ❑ Ethanol 100% El Other ❑ Unknown ❑Residence ❑ Other Organics ❑ E01 — E09 El Unknown [_]Other Definition presented on reverse on reverse Ownership Ownership 1. Municipal 2. Military 3. Unknown 4. Priv a 5. Federal 6. County 7. State Operation Type 1- Public Service 2. Agricultural 3- Residential 4- EducationlRelig- 5. Industrial 6. Commercial., 7- Mining 1 ,car r "" � , .,,,,, k„) Page 1 of 2 IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1 _ Yes 2. No 3. Unknown Number of Water Supply Wells Affected Water Supply Wells Contaminated: (include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3. UST SYSTEM OWNER UST Owner/Company AU Ai 1w- ` t o ii'� Point of Contact Address -J- City { State Zip Code Telephone Number 1 - UST SYSTEM OPERATOR UST Operator/Company Address City State Zip Code Telephone Number i LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address City State Zip Code Telephone Number Draw Sketch of Area (showing two major road intersections) or Attach Map o�elf Schcsv} Ron 1 1090D 5,d.6Ur r3 v cl a o,.r Roth Person Reporting Incident rJ iA otl o'r r. Company K e i e Qa A / / Telephone Number Title ?rty e r FAr r it flc5 r �� i Address Date 35-2 C0'VCreScere. Pkw f}ur�y�rl ?80.b 5� -QO UST Form 61 (02l19) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e_g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion:use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined APPENDIX C lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 May 28, 2020 Mr. David Stoner Shield Engineering 4301 Taggart Creek Road Charlotte, NC 28208 RE: Project: Davidson NC Pace Project No.: 92477861 Dear Mr. Stoner: Enclosed are the analytical results for sample(s) received by the laboratory on May 15, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, v0 Amanda Payne Payne amanda.payne@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 72 laneAnalytical www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Davidson NC Pace Project No.: 92477861 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Mold Certification #: LAB0152 Texas Certification #: T 104704245-17-14 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: VT2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 9980939910 Wyoming UST Certification #: via A21-A 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Davidson NC 92477861 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92477861001 HA-1 EPA 8081 B BAJ 24 PASI-C EPA 8082A SEM 8 PASI-C MADEP EPH BAJ 7 PASI-C MADEP VPH JAH 5 PAN EPA 6010D RDT 2 PASI-A EPA 8270E BPJ 75 PASI-C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C SM 2540G KDW 1 PAN 92477861002 HA-2 EPA 8081 B BAJ 24 PASI-C EPA 8082A SEM 8 PASI-C MADEP EPH BAJ 7 PASI-C MADEP VPH JAH 5 PAN EPA 6010D RDT 2 PASI-A EPA 8270E BPJ 75 PASI-C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C SM 2540G KDW 1 PAN 92477861003 HA-3 EPA 8081 B BAJ 24 PASI-C EPA 8082A SEM 8 PASI-C MADEP EPH BAJ 7 PASI-C MADEP VPH JAH 5 PAN EPA 6010D RDT 2 PASI-A EPA 8270E BPJ 75 PASI-C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C SM 2540G KDW 1 PAN 92477861004 HA-4 EPA 8081 B BAJ 24 PASI-C EPA 8082A SEM 8 PASI-C MADEP EPH BAJ 7 PASI-C MADEP VPH JAH 5 PAN EPA 6010D RDT 2 PASI-A EPA 8270E BPJ 75 PASI-C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C SM 2540G KDW 1 PAN 92477861005 Background EPA 8081E BAJ 24 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Davidson NC Pace Project No.: 92477861 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8082A SEM 8 PASI-C MADEP EPH BAJ 7 PASI-C MADEP VPH JAH 5 PAN EPA 6010D RDT 2 PASI-A EPA 8270E BPJ 75 PASI-C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C SM 2540G KDW 1 PAN 92477861006 SW-1 EPA 1664E JSG 1 PASI-C 92477861007 SW-2 EPA 1664E JSG 1 PASI-C PAN = Pace National - Mt. Juliet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 1664B Description: HEM, Oil and Grease Client: Shield Date: May 28, 2020 General Information: 2 samples were analyzed for EPA 1664B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. QC Batch: 542722 A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92477498001 M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. • MS (Lab ID: 2891361) • Oil and Grease Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 8081 B Description: 8081 GCS Pesticides Client: Shield Date: May 28, 2020 General Information: 5 samples were analyzed for EPA 8081 B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3546 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. QC Batch: 542791 SO: Surrogate recovery outside laboratory control limits. • LCS (Lab ID: 2891545) • Decachlorobiphenyl (S) S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. • BLANK (Lab ID: 2891544) • Decachlorobiphenyl (S) Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 8081 B Description: 8081 GCS Pesticides Client: Shield Date: May 28, 2020 Analyte Comments QC Batch: 542791 D3: Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. • DUP (Lab ID: 2891547) • Tetrachloro-m-xylene (S) • HA-2 (Lab ID: 92477861002) • Tetrachloro-m-xylene (S) • HA-3 (Lab ID: 92477861003) • Tetrachloro-m-xylene (S) REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 8082A Description: 8082 GCS PCB Client: Shield Date: May 28, 2020 General Information: 5 samples were analyzed for EPA 8082A by Pace Analytical Services Charlotte. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3546 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: MADEP EPH Description: MADEP EPH NC Soil Client: Shield Date: May 28, 2020 General Information: 5 samples were analyzed for MADEP EPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with MADEP EPH with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: MADEP VPH Description: MADEPV Client: Shield Date: May 28, 2020 General Information: 5 samples were analyzed for MADEP VPH by Pace National Mt. Juliet. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 6010D Description: 6010 MET ICP Client: Shield Date: May 28, 2020 General Information: 5 samples were analyzed for EPA 6010D by Pace Analytical Services Asheville. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3050B with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 8270E Description: 8270E MSSV Microwave Client: Shield Date: May 28, 2020 General Information: 5 samples were analyzed for EPA 8270E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3546 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. QC Batch: 542564 v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. • BLANK (Lab ID: 2890605) • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene • Background (Lab ID:92477861005) • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene • DUP (Lab ID: 2890608) • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene • HA-1 (Lab ID: 92477861001) • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene • HA-2 (Lab ID: 92477861002) • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene • HA-3 (Lab ID: 92477861003) • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene • HA-4 (Lab ID: 92477861004) REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 8270E Description: 8270E MSSV Microwave Client: Shield Date: May 28, 2020 QC Batch: 542564 v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. • LCS (Lab ID: 2890606) • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene • MS (Lab ID: 2890607) • Benzo(g,h,i)perylene • Dibenz(a,h)anthracene • Indeno(1,2,3-cd)pyrene Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. QC Batch: 542564 S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. • BLANK (Lab ID: 2890605) • Terphenyl-d14 (S) Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 8260D Description: 8260D/5035A Volatile Organics Client: Shield Date: May 28, 2020 General Information: 5 samples were analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 5035A with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. QC Batch: 542191 v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. • BLANK (Lab ID: 2889075) • Chloroethane • Tetrachloroethene • Background (Lab ID:92477861005) • Chloroethane • Tetrachloroethene • DUP (Lab ID: 2890030) • Chloroethane • Trichlorofluoromethane • HA-1 (Lab ID: 92477861001) • Chloroethane • Tetrachloroethene • HA-2 (Lab ID: 92477861002) • Chloroethane • Tetrachloroethene • HA-3 (Lab ID: 92477861003) • Chloroethane • Tetrachloroethene • HA-4 (Lab ID: 92477861004) • Chloroethane • Tetrachloroethene • LCS (Lab ID: 2889076) • Chloroethane • Tetrachloroethene • MS (Lab ID: 2890031) REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 8260D Description: 8260D/5035A Volatile Organics Client: Shield Date: May 28, 2020 QC Batch: 542191 v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. • Chloroethane • Trichlorofluoromethane v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. • BLANK (Lab ID: 2889075) • 1,2,4-Trichlorobenzene • Vinyl acetate • n-Butylbenzene • Background (Lab ID:92477861005) • 1,2,4-Trichlorobenzene • Vinyl acetate • n-Butylbenzene • HA-1 (Lab ID: 92477861001) • 1,2,4-Trichlorobenzene • Vinyl acetate • n-Butylbenzene • HA-2 (Lab ID: 92477861002) • 1,2,4-Trichlorobenzene • Vinyl acetate • n-Butylbenzene • HA-3 (Lab ID: 92477861003) • 1,2,4-Trichlorobenzene • Vinyl acetate • n-Butylbenzene • HA-4 (Lab ID: 92477861004) • 1,2,4-Trichlorobenzene • Vinyl acetate • n-Butylbenzene v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. • LCS (Lab ID: 2889076) • 1,2,4-Trichlorobenzene • Vinyl acetate • n-Butylbenzene Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: EPA 8260D Description: 8260D/5035A Volatile Organics Client: Shield Date: May 28, 2020 Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. QC Batch: 542191 L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. • LCS (Lab ID: 2889076) • Bromomethane Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: Davidson NC Pace Project No.: 92477861 Method: SM 2540G Description: Total Solids 2540 G-2011 Client: Shield Date: May 28, 2020 General Information: 5 samples were analyzed for SM 2540G by Pace National Mt. Juliet. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-1 Lab ID: 92477861001 Collected: 05/15/20 09:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides alpha-BHC gamma-BHC (Lindane) beta-BHC Heptachlor delta-BHC Aldrin Heptachlor epoxide Endosulfan I 4,4'-DDE Dieldrin Endrin 4,4'-DDD Endosulfan 11 4,4'-DDT Endrin aldehyde Endosulfan sulfate Methoxychlor Endrin ketone Chlordane (Technical) Toxaphene Mirex Hexachlorobenzene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) JA/_1e]=1»07.[04&Yd1I Aliphatic (C09-C18) Aliphatic (C19-C36) Aromatic (C11-C22) Surrogates Nonatriacontane (S) Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 319-84-6 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 58-89-9 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 319-85-7 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 76-44-8 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 319-86-8 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 309-00-2 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 1024-57-3 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 959-98-8 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 72-55-9 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 60-57-1 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 72-20-8 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 72-54-8 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 33213-65-9 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 50-29-3 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 7421-93-4 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 1031-07-8 ND ug/kg 5.4 1 05/21/20 09:16 05/21/20 15:06 72-43-5 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 53494-70-5 ND ug/kg 7.5 1 05/21/20 09:16 05/21/20 15:06 57-74-9 ND ug/kg 7.5 1 05/21/20 09:16 05/21/20 15:06 8001-35-2 ND ug/kg 5.4 1 05/21/20 09:16 05/21/20 15:06 2385-85-5 ND ug/kg 2.1 1 05/21/20 09:16 05/21/20 15:06 118-74-1 101 % 15-130 1 05/21/20 09:16 05/21/20 15:06 877-09-8 109 % 10-130 1 05/21/20 09:16 05/21/20 15:06 2051-24-3 Analytical Method: EPA 8082A Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 35.3 1 05/18/2011:36 05/19/2015:49 12674-11-2 ND ug/kg 35.3 1 05/18/2011:36 05/19/2015:49 11104-28-2 ND ug/kg 35.3 1 05/18/2011:36 05/19/2015:49 11141-16-5 ND ug/kg 35.3 1 05/18/2011:36 05/19/2015:49 53469-21-9 ND ug/kg 35.3 1 05/18/2011:36 05/19/2015:49 12672-29-6 ND ug/kg 35.3 1 05/18/2011:36 05/19/2015:49 11097-69-1 ND ug/kg 35.3 1 05/18/2011:36 05/19/2015:49 11096-82-5 87 % 10-130 1 05/18/2011:36 05/19/2015:49 2051-24-3 Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte ND mg/kg 10.8 1 05/19/2015:18 05/21/2018:04 ND mg/kg 10.8 1 05/19/2015:18 05/21/2018:04 ND mg/kg 10.8 1 05/19/2015:18 05/21/2018:04 86 % 40-140 1 05/19/2015:18 05/21/2018:04 7194-86-7 REPORT OF LABORATORY ANALYSIS N2 N2 N2 This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-1 Lab ID: 92477861001 Collected: 05/15/20 09:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte Surrogates o-Terphenyl (S) 81 % 40-140 1 05/19/20 15:18 05/21/20 18:04 84-15-1 2-Fluorobiphenyl (S) 101 % 40-140 1 05/19/20 15:18 05/21/20 18:04 321-60-8 2-Bromonaphthalene (S) 97 % 40-140 1 05/19/20 15:18 05/21/20 18:04 580-13-2 MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV Pace National - Mt. Juliet Aliphatic (C05-008) ND mg/kg 5.35 1 05/15/20 09:20 05/22/20 16:07 Aliphatic (C09-C12) ND mg/kg 5.35 1 05/15/20 09:20 05/22/20 16:07 Aromatic (C09-C10),Unadjusted ND mg/kg 5.35 1 05/15/20 09:20 05/22/20 16:07 TPHC9C10A Surrogates 2,5-Dibromotoluene (FID) 102 % 70.0-130 1 05/15/20 09:20 05/22/20 16:07 615-59-8FID 2,5-Dibromotoluene (PID) 96.4 % 70.0-130 1 05/15/20 09:20 05/22/20 16:07 615-59-8PID 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050E Pace Analytical Services -Asheville Chromium 15.1 mg/kg 0.39 1 05/22/20 07:49 05/24/20 13:34 7440-47-3 Lead 1.1 mg/kg 0.39 1 05/22/20 07:49 05/24/20 13:34 7439-92-1 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 83-32-9 Acenaphthylene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 208-96-8 Aniline ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 62-53-3 Anthracene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 120-12-7 Benzo(a)anthracene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 56-55-3 Benzo(a)pyrene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 50-32-8 Benzo(b)fluoranthene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 205-99-2 Benzo(g,h,i)perylene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 191-24-2 v2 Benzo(k)fluoranthene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 207-08-9 Benzoic Acid ND ug/kg 1800 1 05/18/20 14:53 05/20/20 11:36 65-85-0 Benzyl alcohol ND ug/kg 721 1 05/18/20 14:53 05/20/20 11:36 100-51-6 4-Bromophenylphenyl ether ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 101-55-3 Butylbenzylphthalate ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 721 1 05/18/20 14:53 05/20/20 11:36 59-50-7 4-Chloroaniline ND ug/kg 721 1 05/18/20 14:53 05/20/20 11:36 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 111-44-4 2-Chloronaphthalene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 91-58-7 2-Chlorophenol ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 7005-72-3 Chrysene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 218-01-9 Dibenz(a,h)anthracene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 53-70-3 v2 Dibenzofuran ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 132-64-9 1,2-Dichlorobenzene ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-1 Lab ID: 92477861001 Collected: 05/15/20 09:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1,3-Dichlorobenzene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 541-73-1 1,4-Dichlorobenzene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 721 1 05/18/2014:53 05/20/2011:36 91-94-1 2,4-Dichlorophenol ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 120-83-2 Diethylphthalate ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 84-66-2 2,4-Dimethylphenol ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 105-67-9 Dimethylphthalate ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 131-11-3 Di-n-butylphthalate ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 721 1 05/18/2014:53 05/20/2011:36 534-52-1 2,4-Dinitrophenol ND ug/kg 1800 1 05/18/2014:53 05/20/2011:36 51-28-5 2,4-Dinitrotoluene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 121-14-2 2,6-Dinitrotoluene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 606-20-2 Di-n-octylphthalate ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 117-81-7 Fluoranthene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 206-44-0 Fluorene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 87-68-3 Hexachlorobenzene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 118-74-1 Hexachlorocyclopentadiene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 77-47-4 Hexachloroethane ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 193-39-5 Isophorone ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 78-59-1 1-Methylnaphthalene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 90-12-0 2-Methylnaphthalene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 360 1 05/18/20 14:53 05/20/20 11:36 15831-10-4 Naphthalene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 91-20-3 2-Nitroaniline ND ug/kg 1800 1 05/18/2014:53 05/20/2011:36 88-74-4 3-Nitroaniline ND ug/kg 1800 1 05/18/2014:53 05/20/2011:36 99-09-2 4-Nitroaniline ND ug/kg 721 1 05/18/2014:53 05/20/2011:36 100-01-6 Nitrobenzene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 98-95-3 2-Nitrophenol ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 88-75-5 4-Nitrophenol ND ug/kg 1800 1 05/18/2014:53 05/20/2011:36 100-02-7 N-Nitrosodimethylamine ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 621-64-7 N-Nitrosodiphenylamine ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 108-60-1 Pentachlorophenol ND ug/kg 721 1 05/18/2014:53 05/20/2011:36 87-86-5 Phenanthrene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 85-01-8 Phenol ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 108-95-2 Pyrene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 129-00-0 Pyridine ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 120-82-1 2,4,5-Trichlorophenol ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 95-95-4 2,4,6-Trichlorophenol ND ug/kg 360 1 05/18/2014:53 05/20/2011:36 88-06-2 REPORT OF LABORATORY ANALYSIS v2 Qual This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-1 Lab ID: 92477861001 Collected: 05/15/20 09:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Surrogates Nitrobenzene-d5 (S) 46 % 23-110 1 05/18/20 14:53 05/20/20 11:36 4165-60-0 2-Fluorobiphenyl (S) 45 % 30-110 1 05/18/20 14:53 05/20/20 11:36 321-60-8 Terphenyl-d14 (S) 97 % 28-110 1 05/18/20 14:53 05/20/20 11:36 1718-51-0 Phenol-d6 (S) 48 % 22-110 1 05/18/20 14:53 05/20/20 11:36 13127-88-3 2-Fluorophenol (S) 45 % 13-110 1 05/18/20 14:53 05/20/20 11:36 367-12-4 2,4,6-Tribromophenol (S) 65 % 27-110 1 05/18/20 14:53 05/20/20 11:36 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte Acetone ND ug/kg 80.9 1 05/18/20 17:26 05/19/20 04:53 67-64-1 Benzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 71-43-2 Bromobenzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 108-86-1 Bromochloromethane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 74-97-5 Bromodichloromethane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 75-27-4 Bromoform ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 75-25-2 Bromomethane ND ug/kg 8.1 1 05/18/20 17:26 05/19/20 04:53 74-83-9 2-Butanone (MEK) ND ug/kg 80.9 1 05/18/20 17:26 05/19/20 04:53 78-93-3 n-Butylbenzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 104-51-8 sec-Butylbenzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 135-98-8 tert-Butyl benzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 98-06-6 Carbon tetrachloride ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 56-23-5 Chlorobenzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 108-90-7 Chloroethane ND ug/kg 8.1 1 05/18/20 17:26 05/19/20 04:53 75-00-3 Chloroform ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 67-66-3 Chloromethane ND ug/kg 8.1 1 05/18/20 17:26 05/19/20 04:53 74-87-3 2-Chlorotoluene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 95-49-8 4-Chlorotoluene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 96-12-8 Dibromochloromethane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 106-93-4 Dibromomethane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 74-95-3 1,2-Dichlorobenzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 95-50-1 1,3-Dichlorobenzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 541-73-1 1,4-Dichlorobenzene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 106-46-7 Dichlorodifluoromethane ND ug/kg 8.1 1 05/18/20 17:26 05/19/20 04:53 75-71-8 1,1-Dichloroethane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 75-34-3 1,2-Dichloroethane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 107-06-2 1,1-Dichloroethene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 75-35-4 cis-1,2-Dichloroethene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 156-59-2 trans-1,2-Dichloroethene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 156-60-5 1,2-Dichloropropane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 78-87-5 1,3-Dichloropropane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 142-28-9 2,2-Dichloropropane ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 594-20-7 1,1-Dichloropropene ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 563-58-6 REPORT OF LABORATORY ANALYSIS Qual IH,L1 v2 v1 This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-1 Lab ID: 92477861001 Collected: 05/15/20 09:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters 826013/5035A Volatile Organics cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 10061-01-5 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 10061-02-6 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 108-20-3 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 100-41-4 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 87-68-3 ND ug/kg 40.4 1 05/18/20 17:26 05/19/20 04:53 591-78-6 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 98-82-8 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 99-87-6 ND ug/kg 16.2 1 05/18/20 17:26 05/19/20 04:53 75-09-2 ND ug/kg 40.4 1 05/18/20 17:26 05/19/20 04:53 108-10-1 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 1634-04-4 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 91-20-3 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 103-65-1 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 100-42-5 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 630-20-6 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 79-34-5 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 127-18-4 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 108-88-3 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 87-61-6 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 120-82-1 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 71-55-6 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 79-00-5 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 79-01-6 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 75-69-4 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 96-18-4 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 95-63-6 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 108-67-8 ND ug/kg 40.4 1 05/18/20 17:26 05/19/20 04:53 108-05-4 ND ug/kg 8.1 1 05/18/20 17:26 05/19/20 04:53 75-01-4 ND ug/kg 8.1 1 05/18/20 17:26 05/19/20 04:53 1330-20-7 ND ug/kg 8.1 1 05/18/20 17:26 05/19/20 04:53 179601-23-1 ND ug/kg 4.0 1 05/18/20 17:26 05/19/20 04:53 95-47-6 103 % 70-130 1 05/18/20 17:26 05/19/20 04:53 2037-26-5 103 % 70-130 1 05/18/20 17:26 05/19/20 04:53 460-00-4 103 % 70-132 1 05/18/20 17:26 05/19/20 04:53 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 7.2 % 0.10 1 05/18/20 14:10 Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 93.5 % 1 05/26/20 17:07 05/26/20 17:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. v1 v2 v2 Page 22 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-2 Lab ID: 92477861002 Collected: 05/15/20 09:50 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides alpha-BHC gamma-BHC (Lindane) beta-BHC Heptachlor delta-BHC Aldrin Heptachlor epoxide Endosulfan I 4,4'-DDE Dieldrin Endrin 4,4'-DDD Endosulfan 11 4,4'-DDT Endrin aldehyde Endosulfan sulfate Methoxychlor Endrin ketone Chlordane (Technical) Toxaphene Mirex Hexachlorobenzene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) JA/_1e]=1»07.[04&Yd1I Aliphatic (C09-C18) Aliphatic (C19-C36) Aromatic (C11-C22) Surrogates Nonatriacontane (S) Date: 05/28/2020 10:48 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 319-84-6 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 58-89-9 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 319-85-7 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 76-44-8 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 319-86-8 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 309-00-2 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 1024-57-3 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 959-98-8 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 72-55-9 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 60-57-1 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 72-20-8 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 72-54-8 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 33213-65-9 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 50-29-3 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 7421-93-4 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 1031-07-8 ND ug/kg 11.8 2 05/21/20 09:16 05/21/20 15:35 72-43-5 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 53494-70-5 ND ug/kg 16.6 2 05/21/20 09:16 05/21/20 15:35 57-74-9 ND ug/kg 16.6 2 05/21/20 09:16 05/21/20 15:35 8001-35-2 ND ug/kg 11.8 2 05/21/20 09:16 05/21/20 15:35 2385-85-5 ND ug/kg 4.7 2 05/21/20 09:16 05/21/20 15:35 118-74-1 97 % 15-130 2 05/21/20 09:16 05/21/20 15:35 877-09-8 D3 109 % 10-130 2 05/21/20 09:16 05/21/20 15:35 2051-24-3 Analytical Method: EPA 8082A Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 38.7 1 05/18/2011:36 05/19/2016:04 12674-11-2 ND ug/kg 38.7 1 05/18/2011:36 05/19/2016:04 11104-28-2 ND ug/kg 38.7 1 05/18/2011:36 05/19/2016:04 11141-16-5 ND ug/kg 38.7 1 05/18/2011:36 05/19/2016:04 53469-21-9 ND ug/kg 38.7 1 05/18/2011:36 05/19/2016:04 12672-29-6 ND ug/kg 38.7 1 05/18/2011:36 05/19/2016:04 11097-69-1 ND ug/kg 38.7 1 05/18/2011:36 05/19/2016:04 11096-82-5 79 % 10-130 1 05/18/2011:36 05/19/2016:04 2051-24-3 Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte ND mg/kg 11.7 1 05/19/2015:18 05/21/2018:31 N2 16.5 mg/kg 11.7 1 05/19/2015:18 05/21/2018:31 N2 ND mg/kg 11.7 1 05/19/2015:18 05/21/2018:31 N2 58 % 40-140 1 05/19/2015:18 05/21/2018:31 7194-86-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-2 Lab ID: 92477861002 Collected: 05/15/20 09:50 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte Surrogates o-Terphenyl (S) 84 % 40-140 1 05/19/20 15:18 05/21/20 18:31 84-15-1 2-Fluorobiphenyl (S) 104 % 40-140 1 05/19/20 15:18 05/21/20 18:31 321-60-8 2-Bromonaphthalene (S) 98 % 40-140 1 05/19/20 15:18 05/21/20 18:31 580-13-2 MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV Pace National - Mt. Juliet Aliphatic (C05-008) ND mg/kg 6.13 1 05/15/20 09:50 05/22/20 16:40 Aliphatic (C09-C12) ND mg/kg 6.13 1 05/15/20 09:50 05/22/20 16:40 Aromatic (C09-C10),Unadjusted ND mg/kg 6.13 1 05/15/20 09:50 05/22/20 16:40 TPHC9C10A Surrogates 2,5-Dibromotoluene (FID) 105 % 70.0-130 1 05/15/20 09:50 05/22/20 16:40 615-59-8FID 2,5-Dibromotoluene (PID) 100 % 70.0-130 1 05/15/20 09:50 05/22/20 16:40 615-59-8PID 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050E Pace Analytical Services -Asheville Chromium 120 mg/kg 0.50 1 05/22/20 07:49 05/24/20 13:48 7440-47-3 Lead 8.2 mg/kg 0.50 1 05/22/20 07:49 05/24/20 13:48 7439-92-1 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 83-32-9 Acenaphthylene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 208-96-8 Aniline ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 62-53-3 Anthracene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 120-12-7 Benzo(a)anthracene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 56-55-3 Benzo(a)pyrene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 50-32-8 Benzo(b)fluoranthene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 205-99-2 Benzo(g,h,i)perylene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 191-24-2 v2 Benzo(k)fluoranthene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 207-08-9 Benzoic Acid ND ug/kg 1950 1 05/18/20 14:53 05/20/20 12:38 65-85-0 Benzyl alcohol ND ug/kg 782 1 05/18/20 14:53 05/20/20 12:38 100-51-6 4-Bromophenylphenyl ether ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 101-55-3 Butylbenzylphthalate ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 782 1 05/18/20 14:53 05/20/20 12:38 59-50-7 4-Chloroaniline ND ug/kg 782 1 05/18/20 14:53 05/20/20 12:38 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 111-44-4 2-Chloronaphthalene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 91-58-7 2-Chlorophenol ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 7005-72-3 Chrysene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 218-01-9 Dibenz(a,h)anthracene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 53-70-3 v2 Dibenzofuran ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 132-64-9 1,2-Dichlorobenzene ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-2 Lab ID: 92477861002 Collected: 05/15/20 09:50 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1,3-Dichlorobenzene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 541-73-1 1,4-Dichlorobenzene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 782 1 05/18/2014:53 05/20/2012:38 91-94-1 2,4-Dichlorophenol ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 120-83-2 Diethylphthalate ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 84-66-2 2,4-Dimethylphenol ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 105-67-9 Dimethylphthalate ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 131-11-3 Di-n-butylphthalate ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 782 1 05/18/2014:53 05/20/2012:38 534-52-1 2,4-Dinitrophenol ND ug/kg 1950 1 05/18/2014:53 05/20/2012:38 51-28-5 2,4-Dinitrotoluene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 121-14-2 2,6-Dinitrotoluene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 606-20-2 Di-n-octylphthalate ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 117-81-7 Fluoranthene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 206-44-0 Fluorene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 87-68-3 Hexachlorobenzene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 118-74-1 Hexachlorocyclopentadiene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 77-47-4 Hexachloroethane ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 193-39-5 Isophorone ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 78-59-1 1-Methylnaphthalene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 90-12-0 2-Methylnaphthalene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 391 1 05/18/20 14:53 05/20/20 12:38 15831-10-4 Naphthalene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 91-20-3 2-Nitroaniline ND ug/kg 1950 1 05/18/2014:53 05/20/2012:38 88-74-4 3-Nitroaniline ND ug/kg 1950 1 05/18/2014:53 05/20/2012:38 99-09-2 4-Nitroaniline ND ug/kg 782 1 05/18/2014:53 05/20/2012:38 100-01-6 Nitrobenzene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 98-95-3 2-Nitrophenol ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 88-75-5 4-Nitrophenol ND ug/kg 1950 1 05/18/2014:53 05/20/2012:38 100-02-7 N-Nitrosodimethylamine ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 621-64-7 N-Nitrosodiphenylamine ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 108-60-1 Pentachlorophenol ND ug/kg 782 1 05/18/2014:53 05/20/2012:38 87-86-5 Phenanthrene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 85-01-8 Phenol ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 108-95-2 Pyrene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 129-00-0 Pyridine ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 120-82-1 2,4,5-Trichlorophenol ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 95-95-4 2,4,6-Trichlorophenol ND ug/kg 391 1 05/18/2014:53 05/20/2012:38 88-06-2 REPORT OF LABORATORY ANALYSIS v2 Qual This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-2 Lab ID: 92477861002 Collected: 05/15/20 09:50 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Surrogates Nitrobenzene-d5 (S) 61 % 23-110 1 05/18/20 14:53 05/20/20 12:38 4165-60-0 2-Fluorobiphenyl (S) 57 % 30-110 1 05/18/20 14:53 05/20/20 12:38 321-60-8 Terphenyl-d14 (S) 109 % 28-110 1 05/18/20 14:53 05/20/20 12:38 1718-51-0 Phenol-d6 (S) 62 % 22-110 1 05/18/20 14:53 05/20/20 12:38 13127-88-3 2-Fluorophenol (S) 60 % 13-110 1 05/18/20 14:53 05/20/20 12:38 367-12-4 2,4,6-Tribromophenol (S) 74 % 27-110 1 05/18/20 14:53 05/20/20 12:38 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte Acetone ND ug/kg 98.2 1 05/18/20 17:26 05/19/20 05:17 67-64-1 Benzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 71-43-2 Bromobenzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 108-86-1 Bromochloromethane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 74-97-5 Bromodichloromethane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 75-27-4 Bromoform ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 75-25-2 Bromomethane ND ug/kg 9.8 1 05/18/20 17:26 05/19/20 05:17 74-83-9 2-Butanone (MEK) ND ug/kg 98.2 1 05/18/20 17:26 05/19/20 05:17 78-93-3 n-Butylbenzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 104-51-8 sec-Butylbenzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 135-98-8 tert-Butyl benzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 98-06-6 Carbon tetrachloride ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 56-23-5 Chlorobenzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 108-90-7 Chloroethane ND ug/kg 9.8 1 05/18/20 17:26 05/19/20 05:17 75-00-3 Chloroform ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 67-66-3 Chloromethane ND ug/kg 9.8 1 05/18/20 17:26 05/19/20 05:17 74-87-3 2-Chlorotoluene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 95-49-8 4-Chlorotoluene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 96-12-8 Dibromochloromethane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 106-93-4 Dibromomethane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 74-95-3 1,2-Dichlorobenzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 95-50-1 1,3-Dichlorobenzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 541-73-1 1,4-Dichlorobenzene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 106-46-7 Dichlorodifluoromethane ND ug/kg 9.8 1 05/18/20 17:26 05/19/20 05:17 75-71-8 1,1-Dichloroethane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 75-34-3 1,2-Dichloroethane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 107-06-2 1,1-Dichloroethene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 75-35-4 cis-1,2-Dichloroethene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 156-59-2 trans-1,2-Dichloroethene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 156-60-5 1,2-Dichloropropane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 78-87-5 1,3-Dichloropropane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 142-28-9 2,2-Dichloropropane ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 594-20-7 1,1-Dichloropropene ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 563-58-6 REPORT OF LABORATORY ANALYSIS Qual IH,L1 v2 v1 This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-2 Lab ID: 92477861002 Collected: 05/15/20 09:50 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters 826013/5035A Volatile Organics cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 10061-01-5 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 10061-02-6 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 108-20-3 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 100-41-4 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 87-68-3 ND ug/kg 49.1 1 05/18/20 17:26 05/19/20 05:17 591-78-6 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 98-82-8 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 99-87-6 ND ug/kg 19.6 1 05/18/20 17:26 05/19/20 05:17 75-09-2 ND ug/kg 49.1 1 05/18/20 17:26 05/19/20 05:17 108-10-1 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 1634-04-4 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 91-20-3 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 103-65-1 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 100-42-5 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 630-20-6 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 79-34-5 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 127-18-4 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 108-88-3 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 87-61-6 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 120-82-1 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 71-55-6 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 79-00-5 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 79-01-6 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 75-69-4 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 96-18-4 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 95-63-6 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 108-67-8 ND ug/kg 49.1 1 05/18/20 17:26 05/19/20 05:17 108-05-4 ND ug/kg 9.8 1 05/18/20 17:26 05/19/20 05:17 75-01-4 ND ug/kg 9.8 1 05/18/20 17:26 05/19/20 05:17 1330-20-7 ND ug/kg 9.8 1 05/18/20 17:26 05/19/20 05:17 179601-23-1 ND ug/kg 4.9 1 05/18/20 17:26 05/19/20 05:17 95-47-6 103 % 70-130 1 05/18/20 17:26 05/19/20 05:17 2037-26-5 99 % 70-130 1 05/18/20 17:26 05/19/20 05:17 460-00-4 103 % 70-132 1 05/18/20 17:26 05/19/20 05:17 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 15.9 % 0.10 1 05/18/20 14:10 Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 81.6 % 1 05/26/20 17:07 05/26/20 17:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. v1 v2 v2 Page 27 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-3 Lab ID: 92477861003 Collected: 05/15/20 10:25 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) JA/_1e]=1»07.[04&Yd1I Aliphatic (C09-C18) Aliphatic (C19-C36) Aromatic (C11-C22) Surrogates Nonatriacontane (S) Date: 05/28/2020 10:48 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 309-00-2 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 319-84-6 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 319-85-7 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 319-86-8 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 58-89-9 ND ug/kg 21.0 2.5 05/21/20 09:16 05/21/20 16:04 57-74-9 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 72-54-8 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 72-55-9 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 50-29-3 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 60-57-1 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 959-98-8 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 33213-65-9 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 1031-07-8 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 72-20-8 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 7421-93-4 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 53494-70-5 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 76-44-8 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 1024-57-3 ND ug/kg 6.0 2.5 05/21/20 09:16 05/21/20 16:04 118-74-1 ND ug/kg 15.0 2.5 05/21/20 09:16 05/21/20 16:04 72-43-5 ND ug/kg 15.0 2.5 05/21/20 09:16 05/21/20 16:04 2385-85-5 ND ug/kg 21.0 2.5 05/21/20 09:16 05/21/20 16:04 8001-35-2 86 % 15-130 2.5 05/21/20 09:16 05/21/20 16:04 877-09-8 D3 100 % 10-130 2.5 05/21/20 09:16 05/21/20 16:04 2051-24-3 Analytical Method: EPA 8082A Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 40.5 1 05/18/2011:36 05/19/2016:18 12674-11-2 ND ug/kg 40.5 1 05/18/2011:36 05/19/2016:18 11104-28-2 ND ug/kg 40.5 1 05/18/2011:36 05/19/2016:18 11141-16-5 ND ug/kg 40.5 1 05/18/2011:36 05/19/2016:18 53469-21-9 ND ug/kg 40.5 1 05/18/2011:36 05/19/2016:18 12672-29-6 ND ug/kg 40.5 1 05/18/2011:36 05/19/2016:18 11097-69-1 ND ug/kg 40.5 1 05/18/2011:36 05/19/2016:18 11096-82-5 63 % 10-130 1 05/18/2011:36 05/19/2016:18 2051-24-3 Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte ND mg/kg 12.3 1 05/19/2015:18 05/21/2018:58 N2 58.3 mg/kg 12.3 1 05/19/2015:18 05/21/2018:58 N2 ND mg/kg 12.3 1 05/19/2015:18 05/21/2018:58 N2 72 % 40-140 1 05/19/2015:18 05/21/2018:58 7194-86-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-3 Lab ID: 92477861003 Collected: 05/15/20 10:25 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte Surrogates o-Terphenyl (S) 73 % 40-140 1 05/19/20 15:18 05/21/20 18:58 84-15-1 2-Fluorobiphenyl (S) 93 % 40-140 1 05/19/20 15:18 05/21/20 18:58 321-60-8 2-Bromonaphthalene (S) 93 % 40-140 1 05/19/20 15:18 05/21/20 18:58 580-13-2 MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV Pace National - Mt. Juliet Aliphatic (C05-008) ND mg/kg 6.06 1 05/15/20 10:25 05/22/20 17:13 Aliphatic (C09-C12) ND mg/kg 6.06 1 05/15/20 10:25 05/22/20 17:13 Aromatic (C09-C10),Unadjusted ND mg/kg 6.06 1 05/15/20 10:25 05/22/20 17:13 TPHC9C10A Surrogates 2,5-Dibromotoluene (FID) 114 % 70.0-130 1 05/15/20 10:25 05/22/20 17:13 615-59-8FID 2,5-Dibromotoluene (PID) 104 % 70.0-130 1 05/15/20 10:25 05/22/20 17:13 615-59-8PID 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050E Pace Analytical Services -Asheville Chromium 56.5 mg/kg 0.43 1 05/22/20 07:49 05/24/20 13:59 7440-47-3 Lead 9.4 mg/kg 0.43 1 05/22/20 07:49 05/24/20 13:59 7439-92-1 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 83-32-9 Acenaphthylene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 208-96-8 Aniline ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 62-53-3 Anthracene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 120-12-7 Benzo(a)anthracene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 56-55-3 Benzo(a)pyrene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 50-32-8 Benzo(b)fluoranthene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 205-99-2 Benzo(g,h,i)perylene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 191-24-2 v2 Benzo(k)fluoranthene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 207-08-9 Benzoic Acid ND ug/kg 1980 1 05/18/20 14:53 05/20/20 13:40 65-85-0 Benzyl alcohol ND ug/kg 791 1 05/18/20 14:53 05/20/20 13:40 100-51-6 4-Bromophenylphenyl ether ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 101-55-3 Butylbenzylphthalate ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 791 1 05/18/20 14:53 05/20/20 13:40 59-50-7 4-Chloroaniline ND ug/kg 791 1 05/18/20 14:53 05/20/20 13:40 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 111-44-4 2-Chloronaphthalene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 91-58-7 2-Chlorophenol ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 7005-72-3 Chrysene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 218-01-9 Dibenz(a,h)anthracene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 53-70-3 v2 Dibenzofuran ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 132-64-9 1,2-Dichlorobenzene ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-3 Lab ID: 92477861003 Collected: 05/15/20 10:25 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1,3-Dichlorobenzene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 541-73-1 1,4-Dichlorobenzene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 791 1 05/18/2014:53 05/20/2013:40 91-94-1 2,4-Dichlorophenol ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 120-83-2 Diethylphthalate ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 84-66-2 2,4-Dimethylphenol ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 105-67-9 Dimethylphthalate ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 131-11-3 Di-n-butylphthalate ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 791 1 05/18/2014:53 05/20/2013:40 534-52-1 2,4-Dinitrophenol ND ug/kg 1980 1 05/18/2014:53 05/20/2013:40 51-28-5 2,4-Dinitrotoluene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 121-14-2 2,6-Dinitrotoluene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 606-20-2 Di-n-octylphthalate ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 117-81-7 Fluoranthene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 206-44-0 Fluorene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 87-68-3 Hexachlorobenzene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 118-74-1 Hexachlorocyclopentadiene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 77-47-4 Hexachloroethane ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 193-39-5 Isophorone ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 78-59-1 1-Methylnaphthalene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 90-12-0 2-Methylnaphthalene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 396 1 05/18/20 14:53 05/20/20 13:40 15831-10-4 Naphthalene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 91-20-3 2-Nitroaniline ND ug/kg 1980 1 05/18/2014:53 05/20/2013:40 88-74-4 3-Nitroaniline ND ug/kg 1980 1 05/18/2014:53 05/20/2013:40 99-09-2 4-Nitroaniline ND ug/kg 791 1 05/18/2014:53 05/20/2013:40 100-01-6 Nitrobenzene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 98-95-3 2-Nitrophenol ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 88-75-5 4-Nitrophenol ND ug/kg 1980 1 05/18/2014:53 05/20/2013:40 100-02-7 N-Nitrosodimethylamine ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 621-64-7 N-Nitrosodiphenylamine ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 108-60-1 Pentachlorophenol ND ug/kg 791 1 05/18/2014:53 05/20/2013:40 87-86-5 Phenanthrene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 85-01-8 Phenol ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 108-95-2 Pyrene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 129-00-0 Pyridine ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 120-82-1 2,4,5-Trichlorophenol ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 95-95-4 2,4,6-Trichlorophenol ND ug/kg 396 1 05/18/2014:53 05/20/2013:40 88-06-2 REPORT OF LABORATORY ANALYSIS v2 Qual This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-3 Lab ID: 92477861003 Collected: 05/15/20 10:25 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Surrogates Nitrobenzene-d5 (S) 66 % 23-110 1 05/18/20 14:53 05/20/20 13:40 4165-60-0 2-Fluorobiphenyl (S) 52 % 30-110 1 05/18/20 14:53 05/20/20 13:40 321-60-8 Terphenyl-d14 (S) 99 % 28-110 1 05/18/20 14:53 05/20/20 13:40 1718-51-0 Phenol-d6 (S) 68 % 22-110 1 05/18/20 14:53 05/20/20 13:40 13127-88-3 2-Fluorophenol (S) 63 % 13-110 1 05/18/20 14:53 05/20/20 13:40 367-12-4 2,4,6-Tribromophenol (S) 75 % 27-110 1 05/18/20 14:53 05/20/20 13:40 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte Acetone ND ug/kg 106 1 05/18/20 17:26 05/19/20 05:41 67-64-1 Benzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 71-43-2 Bromobenzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 108-86-1 Bromochloromethane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 74-97-5 Bromodichloromethane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 75-27-4 Bromoform ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 75-25-2 Bromomethane ND ug/kg 10.6 1 05/18/20 17:26 05/19/20 05:41 74-83-9 2-Butanone (MEK) ND ug/kg 106 1 05/18/20 17:26 05/19/20 05:41 78-93-3 n-Butylbenzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 104-51-8 sec-Butylbenzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 135-98-8 tert-Butyl benzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 98-06-6 Carbon tetrachloride ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 56-23-5 Chlorobenzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 108-90-7 Chloroethane ND ug/kg 10.6 1 05/18/20 17:26 05/19/20 05:41 75-00-3 Chloroform ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 67-66-3 Chloromethane ND ug/kg 10.6 1 05/18/20 17:26 05/19/20 05:41 74-87-3 2-Chlorotoluene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 95-49-8 4-Chlorotoluene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 96-12-8 Dibromochloromethane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 106-93-4 Dibromomethane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 74-95-3 1,2-Dichlorobenzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 95-50-1 1,3-Dichlorobenzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 541-73-1 1,4-Dichlorobenzene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 106-46-7 Dichlorodifluoromethane ND ug/kg 10.6 1 05/18/20 17:26 05/19/20 05:41 75-71-8 1,1-Dichloroethane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 75-34-3 1,2-Dichloroethane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 107-06-2 1,1-Dichloroethene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 75-35-4 cis-1,2-Dichloroethene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 156-59-2 trans-1,2-Dichloroethene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 156-60-5 1,2-Dichloropropane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 78-87-5 1,3-Dichloropropane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 142-28-9 2,2-Dichloropropane ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 594-20-7 1,1-Dichloropropene ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 563-58-6 REPORT OF LABORATORY ANALYSIS Qual IH,L1 v2 v1 This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-3 Lab ID: 92477861003 Collected: 05/15/20 10:25 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters 826013/5035A Volatile Organics cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 10061-01-5 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 10061-02-6 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 108-20-3 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 100-41-4 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 87-68-3 ND ug/kg 53.1 1 05/18/20 17:26 05/19/20 05:41 591-78-6 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 98-82-8 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 99-87-6 ND ug/kg 21.2 1 05/18/20 17:26 05/19/20 05:41 75-09-2 ND ug/kg 53.1 1 05/18/20 17:26 05/19/20 05:41 108-10-1 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 1634-04-4 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 91-20-3 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 103-65-1 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 100-42-5 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 630-20-6 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 79-34-5 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 127-18-4 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 108-88-3 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 87-61-6 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 120-82-1 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 71-55-6 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 79-00-5 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 79-01-6 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 75-69-4 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 96-18-4 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 95-63-6 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 108-67-8 ND ug/kg 53.1 1 05/18/20 17:26 05/19/20 05:41 108-05-4 ND ug/kg 10.6 1 05/18/20 17:26 05/19/20 05:41 75-01-4 ND ug/kg 10.6 1 05/18/20 17:26 05/19/20 05:41 1330-20-7 ND ug/kg 10.6 1 05/18/20 17:26 05/19/20 05:41 179601-23-1 ND ug/kg 5.3 1 05/18/20 17:26 05/19/20 05:41 95-47-6 102 % 70-130 1 05/18/20 17:26 05/19/20 05:41 2037-26-5 100 % 70-130 1 05/18/20 17:26 05/19/20 05:41 460-00-4 104 % 70-132 1 05/18/20 17:26 05/19/20 05:41 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 17.7 % 0.10 1 05/18/20 14:10 Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 82.5 % 1 05/26/20 17:07 05/26/20 17:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. v1 v2 v2 Page 32 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-4 Lab ID: 92477861004 Collected: 05/15/20 10:55 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) JA/_1e]=1»07.[04&Yd1I Aliphatic (C09-C18) Aliphatic (C19-C36) Aromatic (C11-C22) Surrogates Nonatriacontane (S) Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 309-00-2 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 319-84-6 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 319-85-7 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 319-86-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 58-89-9 ND ug/kg 8.7 1 05/21/20 09:16 05/21/20 16:18 57-74-9 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 72-54-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 72-55-9 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 50-29-3 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 60-57-1 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 959-98-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 33213-65-9 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 1031-07-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 72-20-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 7421-93-4 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 53494-70-5 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 76-44-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 1024-57-3 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:18 118-74-1 ND ug/kg 6.2 1 05/21/20 09:16 05/21/20 16:18 72-43-5 ND ug/kg 6.2 1 05/21/20 09:16 05/21/20 16:18 2385-85-5 ND ug/kg 8.7 1 05/21/20 09:16 05/21/20 16:18 8001-35-2 103 % 15-130 1 05/21/20 09:16 05/21/20 16:18 877-09-8 109 % 10-130 1 05/21/20 09:16 05/21/20 16:18 2051-24-3 Analytical Method: EPA 8082A Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 41.8 1 05/18/2011:36 05/19/2016:32 12674-11-2 ND ug/kg 41.8 1 05/18/2011:36 05/19/2016:32 11104-28-2 ND ug/kg 41.8 1 05/18/2011:36 05/19/2016:32 11141-16-5 ND ug/kg 41.8 1 05/18/2011:36 05/19/2016:32 53469-21-9 ND ug/kg 41.8 1 05/18/2011:36 05/19/2016:32 12672-29-6 ND ug/kg 41.8 1 05/18/2011:36 05/19/2016:32 11097-69-1 ND ug/kg 41.8 1 05/18/2011:36 05/19/2016:32 11096-82-5 87 % 10-130 1 05/18/2011:36 05/19/2016:32 2051-24-3 Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte ND mg/kg 12.5 1 05/19/2015:18 05/21/2019:26 ND mg/kg 12.5 1 05/19/2015:18 05/21/2019:26 ND mg/kg 12.5 1 05/19/2015:18 05/21/2019:26 69 % 40-140 1 05/19/2015:18 05/21/2019:26 7194-86-7 REPORT OF LABORATORY ANALYSIS N2 N2 N2 This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-4 Lab ID: 92477861004 Collected: 05/15/20 10:55 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte Surrogates o-Terphenyl (S) 75 % 40-140 1 05/19/20 15:18 05/21/20 19:26 84-15-1 2-Fluorobiphenyl (S) 95 % 40-140 1 05/19/20 15:18 05/21/20 19:26 321-60-8 2-Bromonaphthalene (S) 90 % 40-140 1 05/19/20 15:18 05/21/20 19:26 580-13-2 MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV Pace National - Mt. Juliet Aliphatic (C05-008) ND mg/kg 6.27 1 05/15/20 10:55 05/22/20 17:46 Aliphatic (C09-C12) ND mg/kg 6.27 1 05/15/20 10:55 05/22/20 17:46 Aromatic (C09-C10),Unadjusted ND mg/kg 6.27 1 05/15/20 10:55 05/22/20 17:46 TPHC9C10A Surrogates 2,5-Dibromotoluene (FID) 104 % 70.0-130 1 05/15/20 10:55 05/22/20 17:46 615-59-8FID 2,5-Dibromotoluene (PID) 97.3 % 70.0-130 1 05/15/20 10:55 05/22/20 17:46 615-59-8PID 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050E Pace Analytical Services -Asheville Chromium 44.7 mg/kg 0.53 1 05/22/20 07:49 05/24/20 14:02 7440-47-3 Lead 11.9 mg/kg 0.53 1 05/22/20 07:49 05/24/20 14:02 7439-92-1 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 83-32-9 Acenaphthylene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 208-96-8 Aniline ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 62-53-3 Anthracene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 120-12-7 Benzo(a)anthracene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 56-55-3 Benzo(a)pyrene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 50-32-8 Benzo(b)fluoranthene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 205-99-2 Benzo(g,h,i)perylene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 191-24-2 v2 Benzo(k)fluoranthene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 207-08-9 Benzoic Acid ND ug/kg 2110 1 05/18/20 14:53 05/20/20 14:11 65-85-0 Benzyl alcohol ND ug/kg 844 1 05/18/20 14:53 05/20/20 14:11 100-51-6 4-Bromophenylphenyl ether ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 101-55-3 Butylbenzylphthalate ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 844 1 05/18/20 14:53 05/20/20 14:11 59-50-7 4-Chloroaniline ND ug/kg 844 1 05/18/20 14:53 05/20/20 14:11 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 111-44-4 2-Chloronaphthalene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 91-58-7 2-Chlorophenol ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 7005-72-3 Chrysene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 218-01-9 Dibenz(a,h)anthracene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 53-70-3 v2 Dibenzofuran ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 132-64-9 1,2-Dichlorobenzene ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-4 Lab ID: 92477861004 Collected: 05/15/20 10:55 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1,3-Dichlorobenzene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 541-73-1 1,4-Dichlorobenzene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 844 1 05/18/2014:53 05/20/2014:11 91-94-1 2,4-Dichlorophenol ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 120-83-2 Diethylphthalate ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 84-66-2 2,4-Dimethylphenol ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 105-67-9 Dimethylphthalate ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 131-11-3 Di-n-butylphthalate ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 844 1 05/18/2014:53 05/20/2014:11 534-52-1 2,4-Dinitrophenol ND ug/kg 2110 1 05/18/2014:53 05/20/2014:11 51-28-5 2,4-Dinitrotoluene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 121-14-2 2,6-Dinitrotoluene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 606-20-2 Di-n-octylphthalate ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 117-81-7 Fluoranthene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 206-44-0 Fluorene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 87-68-3 Hexachlorobenzene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 118-74-1 Hexachlorocyclopentadiene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 77-47-4 Hexachloroethane ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 193-39-5 Isophorone ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 78-59-1 1-Methylnaphthalene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 90-12-0 2-Methylnaphthalene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 422 1 05/18/20 14:53 05/20/20 14:11 15831-10-4 Naphthalene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 91-20-3 2-Nitroaniline ND ug/kg 2110 1 05/18/2014:53 05/20/2014:11 88-74-4 3-Nitroaniline ND ug/kg 2110 1 05/18/2014:53 05/20/2014:11 99-09-2 4-Nitroaniline ND ug/kg 844 1 05/18/2014:53 05/20/2014:11 100-01-6 Nitrobenzene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 98-95-3 2-Nitrophenol ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 88-75-5 4-Nitrophenol ND ug/kg 2110 1 05/18/2014:53 05/20/2014:11 100-02-7 N-Nitrosodimethylamine ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 621-64-7 N-Nitrosodiphenylamine ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 108-60-1 Pentachlorophenol ND ug/kg 844 1 05/18/2014:53 05/20/2014:11 87-86-5 Phenanthrene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 85-01-8 Phenol ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 108-95-2 Pyrene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 129-00-0 Pyridine ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 120-82-1 2,4,5-Trichlorophenol ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 95-95-4 2,4,6-Trichlorophenol ND ug/kg 422 1 05/18/2014:53 05/20/2014:11 88-06-2 REPORT OF LABORATORY ANALYSIS v2 Qual This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-4 Lab ID: 92477861004 Collected: 05/15/20 10:55 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Surrogates Nitrobenzene-d5 (S) 64 % 23-110 1 05/18/20 14:53 05/20/20 14:11 4165-60-0 2-Fluorobiphenyl (S) 55 % 30-110 1 05/18/20 14:53 05/20/20 14:11 321-60-8 Terphenyl-d14 (S) 99 % 28-110 1 05/18/20 14:53 05/20/20 14:11 1718-51-0 Phenol-d6 (S) 63 % 22-110 1 05/18/20 14:53 05/20/20 14:11 13127-88-3 2-Fluorophenol (S) 60 % 13-110 1 05/18/20 14:53 05/20/20 14:11 367-12-4 2,4,6-Tribromophenol (S) 67 % 27-110 1 05/18/20 14:53 05/20/20 14:11 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte Acetone ND ug/kg 102 1 05/18/20 17:26 05/19/20 06:05 67-64-1 Benzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 71-43-2 Bromobenzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 108-86-1 Bromochloromethane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 74-97-5 Bromodichloromethane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 75-27-4 Bromoform ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 75-25-2 Bromomethane ND ug/kg 10.2 1 05/18/20 17:26 05/19/20 06:05 74-83-9 2-Butanone (MEK) ND ug/kg 102 1 05/18/20 17:26 05/19/20 06:05 78-93-3 n-Butylbenzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 104-51-8 sec-Butylbenzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 135-98-8 tert-Butyl benzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 98-06-6 Carbon tetrachloride ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 56-23-5 Chlorobenzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 108-90-7 Chloroethane ND ug/kg 10.2 1 05/18/20 17:26 05/19/20 06:05 75-00-3 Chloroform ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 67-66-3 Chloromethane ND ug/kg 10.2 1 05/18/20 17:26 05/19/20 06:05 74-87-3 2-Chlorotoluene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 95-49-8 4-Chlorotoluene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 96-12-8 Dibromochloromethane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 106-93-4 Dibromomethane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 74-95-3 1,2-Dichlorobenzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 95-50-1 1,3-Dichlorobenzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 541-73-1 1,4-Dichlorobenzene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 106-46-7 Dichlorodifluoromethane ND ug/kg 10.2 1 05/18/20 17:26 05/19/20 06:05 75-71-8 1,1-Dichloroethane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 75-34-3 1,2-Dichloroethane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 107-06-2 1,1-Dichloroethene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 75-35-4 cis-1,2-Dichloroethene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 156-59-2 trans-1,2-Dichloroethene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 156-60-5 1,2-Dichloropropane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 78-87-5 1,3-Dichloropropane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 142-28-9 2,2-Dichloropropane ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 594-20-7 1,1-Dichloropropene ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 563-58-6 REPORT OF LABORATORY ANALYSIS Qual IH,L1 v2 v1 This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: HA-4 Lab ID: 92477861004 Collected: 05/15/20 10:55 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters 826013/5035A Volatile Organics cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 10061-01-5 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 10061-02-6 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 108-20-3 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 100-41-4 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 87-68-3 ND ug/kg 50.9 1 05/18/20 17:26 05/19/20 06:05 591-78-6 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 98-82-8 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 99-87-6 ND ug/kg 20.4 1 05/18/20 17:26 05/19/20 06:05 75-09-2 ND ug/kg 50.9 1 05/18/20 17:26 05/19/20 06:05 108-10-1 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 1634-04-4 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 91-20-3 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 103-65-1 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 100-42-5 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 630-20-6 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 79-34-5 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 127-18-4 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 108-88-3 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 87-61-6 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 120-82-1 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 71-55-6 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 79-00-5 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 79-01-6 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 75-69-4 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 96-18-4 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 95-63-6 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 108-67-8 ND ug/kg 50.9 1 05/18/20 17:26 05/19/20 06:05 108-05-4 ND ug/kg 10.2 1 05/18/20 17:26 05/19/20 06:05 75-01-4 ND ug/kg 10.2 1 05/18/20 17:26 05/19/20 06:05 1330-20-7 ND ug/kg 10.2 1 05/18/20 17:26 05/19/20 06:05 179601-23-1 ND ug/kg 5.1 1 05/18/20 17:26 05/19/20 06:05 95-47-6 102 % 70-130 1 05/18/20 17:26 05/19/20 06:05 2037-26-5 105 % 70-130 1 05/18/20 17:26 05/19/20 06:05 460-00-4 107 % 70-132 1 05/18/20 17:26 05/19/20 06:05 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 20.5 % 0.10 1 05/18/20 14:10 Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 79.8 % 1 05/26/20 17:07 05/26/20 17:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. v1 v2 v2 Page 37 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: Background Lab ID: 92477861005 Collected: 05/15/20 12:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides alpha-BHC gamma-BHC (Lindane) beta-BHC Heptachlor delta-BHC Aldrin Heptachlor epoxide Endosulfan I 4,4'-DDE Dieldrin Endrin 4,4'-DDD Endosulfan 11 4,4'-DDT Endrin aldehyde Endosulfan sulfate Methoxychlor Endrin ketone Chlordane (Technical) Toxaphene Mirex Hexachlorobenzene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) JA/_1e]=1»07.[04&Yd1I Aliphatic (C09-C18) Aliphatic (C19-C36) Aromatic (C11-C22) Surrogates Nonatriacontane (S) Analytical Method: EPA 8081 B Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 319-84-6 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 58-89-9 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 319-85-7 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 76-44-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 319-86-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 309-00-2 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 1024-57-3 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 959-98-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 72-55-9 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 60-57-1 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 72-20-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 72-54-8 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 33213-65-9 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 50-29-3 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 7421-93-4 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 1031-07-8 ND ug/kg 6.2 1 05/21/20 09:16 05/21/20 16:33 72-43-5 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 53494-70-5 ND ug/kg 8.6 1 05/21/20 09:16 05/21/20 16:33 57-74-9 ND ug/kg 8.6 1 05/21/20 09:16 05/21/20 16:33 8001-35-2 ND ug/kg 6.2 1 05/21/20 09:16 05/21/20 16:33 2385-85-5 ND ug/kg 2.5 1 05/21/20 09:16 05/21/20 16:33 118-74-1 106 % 15-130 1 05/21/20 09:16 05/21/20 16:33 877-09-8 ill % 10-130 1 05/21/20 09:16 05/21/20 16:33 2051-24-3 Analytical Method: EPA 8082A Preparation Method: EPA 3546 Pace Analytical Services - Charlotte ND ug/kg 39.9 1 05/18/2011:36 05/19/2016:47 12674-11-2 ND ug/kg 39.9 1 05/18/2011:36 05/19/2016:47 11104-28-2 ND ug/kg 39.9 1 05/18/2011:36 05/19/2016:47 11141-16-5 ND ug/kg 39.9 1 05/18/2011:36 05/19/2016:47 53469-21-9 ND ug/kg 39.9 1 05/18/2011:36 05/19/2016:47 12672-29-6 ND ug/kg 39.9 1 05/18/2011:36 05/19/2016:47 11097-69-1 ND ug/kg 39.9 1 05/18/2011:36 05/19/2016:47 11096-82-5 84 % 10-130 1 05/18/2011:36 05/19/2016:47 2051-24-3 Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte ND mg/kg 12.1 1 05/19/20 15:18 05/21/20 20:20 ND mg/kg 12.1 1 05/19/20 15:18 05/21/20 20:20 ND mg/kg 12.1 1 05/19/20 15:18 05/21/20 20:20 64 % 40-140 1 05/19/20 15:18 05/21/20 20:20 7194-86-7 REPORT OF LABORATORY ANALYSIS N2 N2 N2 This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: Background Lab ID: 92477861005 Collected: 05/15/20 12:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Pace Analytical Services - Charlotte Surrogates o-Terphenyl (S) 83 % 40-140 1 05/19/20 15:18 05/21/20 20:20 84-15-1 2-Fluorobiphenyl(S) ill % 40-140 1 05/19/20 15:18 05/21/20 20:20 321-60-8 2-Bromonaphthalene (S) ill % 40-140 1 05/19/20 15:18 05/21/20 20:20 580-13-2 MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV Pace National - Mt. Juliet Aliphatic (C05-008) ND mg/kg 6.00 1 05/15/20 12:20 05/22/20 18:19 Aliphatic (C09-C12) ND mg/kg 6.00 1 05/15/20 12:20 05/22/20 18:19 Aromatic (C09-C10),Unadjusted ND mg/kg 6.00 1 05/15/20 12:20 05/22/20 18:19 TPHC9C10A Surrogates 2,5-Dibromotoluene (FID) 103 % 70.0-130 1 05/15/20 12:20 05/22/20 18:19 615-59-8FID 2,5-Dibromotoluene (PID) 98.3 % 70.0-130 1 05/15/20 12:20 05/22/20 18:19 615-59-8PID 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050E Pace Analytical Services -Asheville Chromium 79.6 mg/kg 0.52 1 05/22/20 07:49 05/24/20 14:05 7440-47-3 Lead 9.4 mg/kg 0.52 1 05/22/20 07:49 05/24/20 14:05 7439-92-1 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 83-32-9 Acenaphthylene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 208-96-8 Aniline ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 62-53-3 Anthracene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 120-12-7 Benzo(a)anthracene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 56-55-3 Benzo(a)pyrene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 50-32-8 Benzo(b)fluoranthene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 205-99-2 Benzo(g,h,i)perylene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 191-24-2 v2 Benzo(k)fluoranthene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 207-08-9 Benzoic Acid ND ug/kg 2010 1 05/18/20 14:53 05/20/20 14:42 65-85-0 Benzyl alcohol ND ug/kg 805 1 05/18/20 14:53 05/20/20 14:42 100-51-6 4-Bromophenylphenyl ether ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 101-55-3 Butylbenzylphthalate ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 805 1 05/18/20 14:53 05/20/20 14:42 59-50-7 4-Chloroaniline ND ug/kg 805 1 05/18/20 14:53 05/20/20 14:42 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 111-44-4 2-Chloronaphthalene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 91-58-7 2-Chlorophenol ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 7005-72-3 Chrysene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 218-01-9 Dibenz(a,h)anthracene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 53-70-3 v2 Dibenzofuran ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 132-64-9 1,2-Dichlorobenzene ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: Background Lab ID: 92477861005 Collected: 05/15/20 12:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 1,3-Dichlorobenzene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 541-73-1 1,4-Dichlorobenzene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 805 1 05/18/2014:53 05/20/2014:42 91-94-1 2,4-Dichlorophenol ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 120-83-2 Diethylphthalate ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 84-66-2 2,4-Dimethylphenol ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 105-67-9 Dimethylphthalate ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 131-11-3 Di-n-butylphthalate ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 805 1 05/18/2014:53 05/20/2014:42 534-52-1 2,4-Dinitrophenol ND ug/kg 2010 1 05/18/2014:53 05/20/2014:42 51-28-5 2,4-Dinitrotoluene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 121-14-2 2,6-Dinitrotoluene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 606-20-2 Di-n-octylphthalate ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 117-81-7 Fluoranthene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 206-44-0 Fluorene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 87-68-3 Hexachlorobenzene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 118-74-1 Hexachlorocyclopentadiene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 77-47-4 Hexachloroethane ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 193-39-5 Isophorone ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 78-59-1 1-Methylnaphthalene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 90-12-0 2-Methylnaphthalene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 403 1 05/18/20 14:53 05/20/20 14:42 15831-10-4 Naphthalene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 91-20-3 2-Nitroaniline ND ug/kg 2010 1 05/18/2014:53 05/20/2014:42 88-74-4 3-Nitroaniline ND ug/kg 2010 1 05/18/2014:53 05/20/2014:42 99-09-2 4-Nitroaniline ND ug/kg 805 1 05/18/2014:53 05/20/2014:42 100-01-6 Nitrobenzene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 98-95-3 2-Nitrophenol ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 88-75-5 4-Nitrophenol ND ug/kg 2010 1 05/18/2014:53 05/20/2014:42 100-02-7 N-Nitrosodimethylamine ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 621-64-7 N-Nitrosodiphenylamine ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 108-60-1 Pentachlorophenol ND ug/kg 805 1 05/18/2014:53 05/20/2014:42 87-86-5 Phenanthrene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 85-01-8 Phenol ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 108-95-2 Pyrene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 129-00-0 Pyridine ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 120-82-1 2,4,5-Trichlorophenol ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 95-95-4 2,4,6-Trichlorophenol ND ug/kg 403 1 05/18/2014:53 05/20/2014:42 88-06-2 REPORT OF LABORATORY ANALYSIS v2 Qual This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: Background Lab ID: 92477861005 Collected: 05/15/20 12:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Surrogates Nitrobenzene-d5 (S) 58 % 23-110 1 05/18/20 14:53 05/20/20 14:42 4165-60-0 2-Fluorobiphenyl (S) 58 % 30-110 1 05/18/20 14:53 05/20/20 14:42 321-60-8 Terphenyl-d14 (S) 99 % 28-110 1 05/18/20 14:53 05/20/20 14:42 1718-51-0 Phenol-d6 (S) 60 % 22-110 1 05/18/20 14:53 05/20/20 14:42 13127-88-3 2-Fluorophenol (S) 58 % 13-110 1 05/18/20 14:53 05/20/20 14:42 367-12-4 2,4,6-Tribromophenol (S) 69 % 27-110 1 05/18/20 14:53 05/20/20 14:42 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte Acetone ND ug/kg 109 1 05/18/20 17:26 05/19/20 06:29 67-64-1 Benzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 71-43-2 Bromobenzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 108-86-1 Bromochloromethane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 74-97-5 Bromodichloromethane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 75-27-4 Bromoform ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 75-25-2 Bromomethane ND ug/kg 10.9 1 05/18/20 17:26 05/19/20 06:29 74-83-9 2-Butanone (MEK) ND ug/kg 109 1 05/18/20 17:26 05/19/20 06:29 78-93-3 n-Butylbenzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 104-51-8 sec-Butylbenzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 135-98-8 tert-Butyl benzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 98-06-6 Carbon tetrachloride ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 56-23-5 Chlorobenzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 108-90-7 Chloroethane ND ug/kg 10.9 1 05/18/20 17:26 05/19/20 06:29 75-00-3 Chloroform ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 67-66-3 Chloromethane ND ug/kg 10.9 1 05/18/20 17:26 05/19/20 06:29 74-87-3 2-Chlorotoluene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 95-49-8 4-Chlorotoluene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 96-12-8 Dibromochloromethane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 106-93-4 Dibromomethane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 74-95-3 1,2-Dichlorobenzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 95-50-1 1,3-Dichlorobenzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 541-73-1 1,4-Dichlorobenzene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 106-46-7 Dichlorodifluoromethane ND ug/kg 10.9 1 05/18/20 17:26 05/19/20 06:29 75-71-8 1,1-Dichloroethane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 75-34-3 1,2-Dichloroethane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 107-06-2 1,1-Dichloroethene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 75-35-4 cis-1,2-Dichloroethene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 156-59-2 trans-1,2-Dichloroethene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 156-60-5 1,2-Dichloropropane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 78-87-5 1,3-Dichloropropane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 142-28-9 2,2-Dichloropropane ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 594-20-7 1,1-Dichloropropene ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 563-58-6 REPORT OF LABORATORY ANALYSIS Qual IH,L1 v2 v1 This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 41 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: Background Lab ID: 92477861005 Collected: 05/15/20 12:20 Received: 05/15/20 14:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters 826013/5035A Volatile Organics cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260D Preparation Method: EPA 5035A Pace Analytical Services - Charlotte ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 10061-01-5 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 10061-02-6 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 108-20-3 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 100-41-4 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 87-68-3 ND ug/kg 54.6 1 05/18/20 17:26 05/19/20 06:29 591-78-6 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 98-82-8 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 99-87-6 ND ug/kg 21.9 1 05/18/20 17:26 05/19/20 06:29 75-09-2 ND ug/kg 54.6 1 05/18/20 17:26 05/19/20 06:29 108-10-1 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 1634-04-4 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 91-20-3 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 103-65-1 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 100-42-5 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 630-20-6 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 79-34-5 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 127-18-4 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 108-88-3 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 87-61-6 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 120-82-1 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 71-55-6 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 79-00-5 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 79-01-6 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 75-69-4 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 96-18-4 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 95-63-6 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 108-67-8 ND ug/kg 54.6 1 05/18/20 17:26 05/19/20 06:29 108-05-4 ND ug/kg 10.9 1 05/18/20 17:26 05/19/20 06:29 75-01-4 ND ug/kg 10.9 1 05/18/20 17:26 05/19/20 06:29 1330-20-7 ND ug/kg 10.9 1 05/18/20 17:26 05/19/20 06:29 179601-23-1 ND ug/kg 5.5 1 05/18/20 17:26 05/19/20 06:29 95-47-6 103 % 70-130 1 05/18/20 17:26 05/19/20 06:29 2037-26-5 102 % 70-130 1 05/18/20 17:26 05/19/20 06:29 460-00-4 107 % 70-132 1 05/18/20 17:26 05/19/20 06:29 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 18.6 % 0.10 1 05/18/20 14:10 Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 83.4 % 1 05/26/20 17:07 05/26/20 17:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. v1 v2 v2 Page 42 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: SW-1 Lab ID: 92477861006 Collected: 05/15/20 13:05 Received: 05/15/20 14:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 05/20/20 21:01 Date: 05/28/2020 10:48 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 43 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Davidson NC Pace Project No.: 92477861 Sample: SW-2 Lab ID: 92477861007 Collected: 05/15/20 13:20 Received: 05/15/20 14:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 05/20/20 21:01 Date: 05/28/2020 10:48 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 44 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 542722 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477861006, 92477861007 METHOD BLANK: 2891359 Matrix: Water Associated Lab Samples: 92477861006, 92477861007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 05/20/20 19:21 LABORATORY CONTROL SAMPLE: 2891360 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 35.6 89 78-114 MATRIX SPIKE SAMPLE: 2891361 92477498001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 9.1 16 78-114 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 1480781 Analysis Method: MADEP VPH QC Batch Method: MADEPV Analysis Description: MADEPV Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 METHOD BLANK: R3531482-3 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Aliphatic (C05-CO8) mg/kg ND 5.00 05/22/20 12:17 Aliphatic (C09-C12) mg/kg ND 5.00 05/22/20 12:17 Aromatic (C09-C10),Unadjusted mg/kg ND 5.00 05/22/20 12:17 2,5-Dibromotoluene (FID) % 98 70.0-130 05/22/20 12:17 2,5-Dibromotoluene (PID) % 95.1 70.0-130 05/22/20 12:17 LABORATORY CONTROL SAMPLE & LCSD: R3531482-1 R3531482-2 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Aliphatic (C05-CO8) mg/kg 60.0 50.6 50.1 84.3 83.5 70.0-130 0.993 25 Aliphatic (C09-C12) mg/kg 70.0 71.5 71.1 102 102 70.0-130 0.561 25 Aromatic (C09-C10),Unadjusted mg/kg 10.0 10.7 10.6 107 106 70.0-130 0.939 25 2,5-Dibromotoluene (FID) % 105 108 70.0-130 2,5-Dibromotoluene (PID) % 105 107 70.0-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3531482-4 Parameter Aliphatic (C05-CO8) Aliphatic (C09-C12) Aromatic (C09- C10),Unadjusted 2,5-Dibromotoluene (FID) 2,5-Dibromotoluene (PID) MS L1219595-20 Spike Units Result Conc. mg/kg 3.97 62.2 mg/kg 13.2 72.5 mg/kg 6.65 10.4 R3531482-5 MSD Spike MS MSD MS Conc. Result Result % Rec 62.2 48.2 47.5 71.1 72.5 77.2 79.5 88.3 10.4 13.8 13.9 68.7 MSD % Rec % Rec Limits RPD Qual 69.9 70.0-130 1.48 ML 91.4 70.0-130 2.85 69.9 70.0-130 0.851 ML 104 70.0-130 97.7 70.0-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 46 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 543033 Analysis Method: EPA 6010D QC Batch Method: EPA 3050E Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 METHOD BLANK: 2892753 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chromium mg/kg ND 0.50 05/24/2013:27 Lead mg/kg ND 0.50 05/24/2013:27 LABORATORY CONTROL SAMPLE: 2892754 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chromium mg/kg 50 50.5 101 80-120 Lead mg/kg 50 51.4 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2892755 2892756 MS MSD 92477861001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chromium mg/kg 15.1 40.2 44.9 46.3 54.2 78 87 75-125 16 Lead mg/kg 1.1 40.2 44.9 36.2 42.2 87 92 75-125 15 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 47 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 542191 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 METHOD BLANK: 2889075 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/19/20 02:52 1,1,1-Trichloroethane ug/kg ND 5.0 05/19/20 02:52 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/19/20 02:52 1,1,2-Trichloroethane ug/kg ND 5.0 05/19/20 02:52 1,1-Dichloroethane ug/kg ND 5.0 05/19/20 02:52 1,1-Dichloroethene ug/kg ND 5.0 05/19/20 02:52 1,1-Dichloropropene ug/kg ND 5.0 05/19/20 02:52 1,2,3-Trichlorobenzene ug/kg ND 5.0 05/19/20 02:52 1,2,3-Trichloropropane ug/kg ND 5.0 05/19/20 02:52 1,2,4-Trichlorobenzene ug/kg ND 5.0 05/19/20 02:52 1,2,4-Trimethylbenzene ug/kg ND 5.0 05/19/20 02:52 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/19/20 02:52 1,2-Dibromoethane (EDB) ug/kg ND 5.0 05/19/20 02:52 1,2-Dichlorobenzene ug/kg ND 5.0 05/19/20 02:52 1,2-Dichloroethane ug/kg ND 5.0 05/19/20 02:52 1,2-Dichloropropane ug/kg ND 5.0 05/19/20 02:52 1,3,5-Trimethylbenzene ug/kg ND 5.0 05/19/20 02:52 1,3-Dichlorobenzene ug/kg ND 5.0 05/19/20 02:52 1,3-Dichloropropane ug/kg ND 5.0 05/19/20 02:52 1,4-Dichlorobenzene ug/kg ND 5.0 05/19/20 02:52 2,2-Dichloropropane ug/kg ND 5.0 05/19/20 02:52 2-Butanone (MEK) ug/kg ND 100 05/19/20 02:52 2-Chlorotoluene ug/kg ND 5.0 05/19/20 02:52 2-Hexanone ug/kg ND 50.0 05/19/20 02:52 4-Chlorotoluene ug/kg ND 5.0 05/19/20 02:52 4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 05/19/20 02:52 Acetone ug/kg ND 100 05/19/20 02:52 Benzene ug/kg ND 5.0 05/19/20 02:52 Bromobenzene ug/kg ND 5.0 05/19/20 02:52 Bromochloromethane ug/kg ND 5.0 05/19/20 02:52 Bromodichloromethane ug/kg ND 5.0 05/19/20 02:52 Bromoform ug/kg ND 5.0 05/19/20 02:52 Bromomethane ug/kg ND 10.0 05/19/20 02:52 Carbon tetrachloride ug/kg ND 5.0 05/19/20 02:52 Chlorobenzene ug/kg ND 5.0 05/19/20 02:52 Chloroethane ug/kg ND 10.0 05/19/20 02:52 Chloroform ug/kg ND 5.0 05/19/20 02:52 Chloromethane ug/kg ND 10.0 05/19/20 02:52 cis-1,2-Dichloroethene ug/kg ND 5.0 05/19/20 02:52 cis-1,3-Dichloropropene ug/kg ND 5.0 05/19/20 02:52 v2 IH v1 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 48 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 METHOD BLANK: 2889075 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed Dibromochloromethane ug/kg ND 5.0 05/19/20 02:52 Dibromomethane ug/kg ND 5.0 05/19/20 02:52 Dichlorodifluoromethane ug/kg ND 10.0 05/19/20 02:52 Diisopropyl ether ug/kg ND 5.0 05/19/20 02:52 Ethylbenzene ug/kg ND 5.0 05/19/20 02:52 Hexachloro-1,3-butadiene ug/kg ND 5.0 05/19/20 02:52 Isopropylbenzene (Cumene) ug/kg ND 5.0 05/19/20 02:52 m&p-Xylene ug/kg ND 10.0 05/19/20 02:52 Methyl-tert-butyl ether ug/kg ND 5.0 05/19/20 02:52 Methylene Chloride ug/kg ND 20.0 05/19/20 02:52 n-Butylbenzene ug/kg ND 5.0 05/19/20 02:52 n-Propylbenzene ug/kg ND 5.0 05/19/20 02:52 Naphthalene ug/kg ND 5.0 05/19/20 02:52 o-Xylene ug/kg ND 5.0 05/19/20 02:52 p-Isopropyltoluene ug/kg ND 5.0 05/19/20 02:52 sec-Butylbenzene ug/kg ND 5.0 05/19/20 02:52 Styrene ug/kg ND 5.0 05/19/20 02:52 tert-Butyl benzene ug/kg ND 5.0 05/19/20 02:52 Tetrachloroethene ug/kg ND 5.0 05/19/20 02:52 Toluene ug/kg ND 5.0 05/19/20 02:52 trans-1,2-Dichloroethene ug/kg ND 5.0 05/19/20 02:52 trans- 1,3-Dichloropropene ug/kg ND 5.0 05/19/20 02:52 Trichloroethene ug/kg ND 5.0 05/19/20 02:52 Trichlorofluoromethane ug/kg ND 5.0 05/19/20 02:52 Vinyl acetate ug/kg ND 50.0 05/19/20 02:52 Vinyl chloride ug/kg ND 10.0 05/19/20 02:52 Xylene (Total) ug/kg ND 10.0 05/19/20 02:52 1,2-Dichloroethane-d4 (S) % 99 70-132 05/19/20 02:52 4-Bromofluorobenzene (S) % 101 70-130 05/19/20 02:52 Toluene-d8 (S) % 103 70-130 05/19/20 02:52 v2 v1 v2 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2889076 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg 50 57.7 115 70-130 1,1,1-Trichloroethane ug/kg 50 53.4 107 70-130 1,1,2,2-Tetrachloroethane ug/kg 50 52.5 105 55-130 1,1,2-Trichloroethane ug/kg 50 56.8 114 70-130 1,1-Dichloroethane ug/kg 50 53.7 107 68-130 1,1-Dichloroethene ug/kg 50 56.0 112 70-130 1,1-Dichloropropene ug/kg 50 57.2 114 70-130 1,2,3-Trichlorobenzene ug/kg 50 53.0 106 70-130 1,2,3-Trichloropropane ug/kg 50 55.7 111 70-130 1,2,4-Trichlorobenzene ug/kg 50 50.7 101 70-130 v3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Davidson NC Pace Project No.: 92477861 LABORATORY CONTROL SAMPLE: 2889076 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trimethylbenzene ug/kg 50 53.4 107 69-130 1,2-Dibromo-3-chloropropane ug/kg 50 57.2 114 57-141 1,2-Dibromoethane (EDB) ug/kg 50 60.5 121 70-130 1,2-Dichlorobenzene ug/kg 50 55.1 110 70-130 1,2-Dichloroethane ug/kg 50 57.0 114 70-130 1,2-Dichloropropane ug/kg 50 55.6 111 70-130 1,3,5-Trimethylbenzene ug/kg 50 53.6 107 70-130 1,3-Dichlorobenzene ug/kg 50 52.4 105 70-130 1,3-Dichloropropane ug/kg 50 58.5 117 70-130 1,4-Dichlorobenzene ug/kg 50 52.3 105 70-130 2,2-Dichloropropane ug/kg 50 52.4 105 70-130 2-Butanone (MEK) ug/kg 100 115 115 60-130 2-Chlorotoluene ug/kg 50 52.9 106 70-130 2-Hexanone ug/kg 100 110 110 70-132 4-Chlorotoluene ug/kg 50 53.6 107 70-130 4-Methyl-2-pentanone (MIBK) ug/kg 100 108 108 69-130 Acetone ug/kg 100 134 134 49-148 Benzene ug/kg 50 55.3 111 70-130 Bromobenzene ug/kg 50 55.3 111 70-130 Bromochloromethane ug/kg 50 57.3 115 70-130 Bromodichloromethane ug/kg 50 58.5 117 70-130 Bromoform ug/kg 50 58.2 116 68-136 Bromomethane ug/kg 50 76.8 154 60-140IH,L1 Carbon tetrachloride ug/kg 50 52.4 105 70-130 Chlorobenzene ug/kg 50 56.0 112 70-130 Chloroethane ug/kg 50 67.0 134 51-147 v1 Chloroform ug/kg 50 54.6 109 70-130 Chloromethane ug/kg 50 52.8 106 48-130 cis-1,2-Dichloroethene ug/kg 50 55.0 110 70-130 cis-1,3-Dichloropropene ug/kg 50 56.6 113 70-130 Dibromochloromethane ug/kg 50 59.1 118 70-130 Dibromomethane ug/kg 50 55.9 112 70-130 Dichlorodifluoromethane ug/kg 50 58.9 118 49-130 Diisopropyl ether ug/kg 50 57.5 115 66-130 Ethylbenzene ug/kg 50 52.6 105 70-130 Hexachloro-1,3-butadiene ug/kg 50 51.6 103 70-130 Isopropylbenzene (Cumene) ug/kg 50 54.4 109 70-130 m&p-Xylene ug/kg 100 106 106 70-130 Methyl-tert-butyl ether ug/kg 50 60.4 121 70-130 Methylene Chloride ug/kg 50 52.7 105 50-137 n-Butylbenzene ug/kg 50 49.6 99 70-130 v3 n-Propylbenzene ug/kg 50 50.6 101 70-130 Naphthalene ug/kg 50 56.4 113 70-131 o-Xylene ug/kg 50 55.7 111 70-130 p-Isopropyltoluene ug/kg 50 51.4 103 70-130 sec-Butylbenzene ug/kg 50 51.5 103 70-130 Styrene ug/kg 50 57.3 115 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 LABORATORY CONTROL SAMPLE: Parameter 2889076 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers tert-Butyl benzene ug/kg 50 46.3 93 69-130 Tetrachloroethene ug/kg 50 48.1 96 56-130 v1 Toluene ug/kg 50 53.1 106 70-130 trans-1,2-Dichloroethene ug/kg 50 54.9 110 70-130 trans- 1,3-Dichloropropene ug/kg 50 56.8 114 70-130 Trichloroethene ug/kg 50 56.5 113 70-141 Trichlorofluoromethane ug/kg 50 56.5 113 67-130 Vinyl acetate ug/kg 100 90.3 90 10-136 v3 Vinyl chloride ug/kg 50 64.3 129 67-130 Xylene (Total) ug/kg 150 162 108 70-130 1,2-Dichloroethane-d4 (S) % 99 70-132 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 2890031 Units 92477858013 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg <5.2 20.5 20.0 97 52-133 1,1,1-Trichloroethane ug/kg <5.2 20.5 21.4 104 49-137 1,1,2,2-Tetrachloroethane ug/kg <5.2 20.5 20.6 100 39-150 1,1,2-Trichloroethane ug/kg <5.2 20.5 20.0 97 48-140 1,1-Dichloroethane ug/kg <5.2 20.5 20.7 101 46-135 1,1-Dichloroethene ug/kg <5.2 20.5 22.1 107 38-149 1,1-Dichloropropene ug/kg <5.2 20.5 21.6 105 41-140 1,2,3-Trichlorobenzene ug/kg <5.2 20.5 19.6 95 10-158 1,2,3-Trichloropropane ug/kg <5.2 20.5 20.3 99 33-157 1,2,4-Trichlorobenzene ug/kg <5.2 20.5 17.6 86 10-155 1,2,4-Trimethylbenzene ug/kg <5.2 20.5 26.3 128 24-154 1,2-Dibromo-3-chloropropane ug/kg <5.2 20.5 20.7 101 33-158 1,2-Dibromoethane (EDB) ug/kg <5.2 20.5 20.0 97 40-136 1,2-Dichlorobenzene ug/kg <5.2 20.5 20.0 98 27-146 1,2-Dichloroethane ug/kg <5.2 20.5 21.4 104 49-140 1,2-Dichloropropane ug/kg <5.2 20.5 19.2 94 44-143 1,3,5-Trimethylbenzene ug/kg <5.2 20.5 22.1 108 40-144 1,3-Dichlorobenzene ug/kg <5.2 20.5 19.1 93 33-140 1,3-Dichloropropane ug/kg <5.2 20.5 19.7 96 47-147 1,4-Dichlorobenzene ug/kg <5.2 20.5 19.0 93 35-139 2,2-Dichloropropane ug/kg <5.2 20.5 20.8 101 41-140 2-Butanone (MEK) ug/kg <103 41.1 36.1J 88 10-181 2-Chlorotoluene ug/kg <5.2 20.5 19.5 95 38-147 2-Hexanone ug/kg <51.6 41.1 36.2J 88 18-169 4-Chlorotoluene ug/kg <5.2 20.5 20.0 97 36-145 4-Methyl-2-pentanone (MIBK) ug/kg <51.6 41.1 40AJ 93 16-175 Acetone ug/kg 17.5J 41.1 51AJ 83 10-200 Benzene ug/kg <5.2 20.5 19.6 96 46-136 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 MATRIX SPIKE SAMPLE: 2890031 92477858013 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromobenzene ug/kg <5.2 20.5 19.4 94 38-149 Bromochloromethane ug/kg <5.2 20.5 19.9 97 44-142 Bromodichloromethane ug/kg <5.2 20.5 20.8 101 41-140 Bromoform ug/kg <5.2 20.5 19.5 95 34-145 Bromomethane ug/kg <10.3 20.5 30.8 150 14-162 IH Carbon tetrachloride ug/kg <5.2 20.5 20.6 100 44-141 Chlorobenzene ug/kg <5.2 20.5 20.1 98 39-141 Chloroethane ug/kg <10.3 20.5 30.7 149 10-182 v1 Chloroform ug/kg <5.2 20.5 21.7 106 45-140 Chloromethane ug/kg <10.3 20.5 20.0 97 19-149 cis-1,2-Dichloroethene ug/kg <5.2 20.5 20.7 101 38-150 cis-1,3-Dichloropropene ug/kg <5.2 20.5 19.0 93 30-144 Dibromochloromethane ug/kg <5.2 20.5 19.8 96 36-145 Dibromomethane ug/kg <5.2 20.5 18.8 91 41-145 Dichlorodifluoromethane ug/kg <10.3 20.5 25.1 122 16-146 Diisopropyl ether ug/kg <5.2 20.5 19.8 96 41-143 Ethylbenzene ug/kg <5.2 20.5 19.7 96 35-144 Hexachloro-1,3-butadiene ug/kg <5.2 20.5 18.6 91 10-160 Isopropylbenzene(Cumene) ug/kg <5.2 20.5 20.9 102 30-152 m&p-Xylene ug/kg <10.3 41.1 40.6 99 33-145 Methyl-tert-butyl ether ug/kg <5.2 20.5 21.1 103 49-140 Methylene Chloride ug/kg <20.6 20.5 20AJ 100 10-174 n-Butylbenzene ug/kg <5.2 20.5 21.4 104 10-160 n-Propylbenzene ug/kg <5.2 20.5 20.6 100 24-159 Naphthalene ug/kg <5.2 20.5 21.9 106 10-171 o-Xylene ug/kg <5.2 20.5 20.3 99 31-150 p-Isopropyltoluene ug/kg <5.2 20.5 21.8 106 21-154 sec-Butylbenzene ug/kg <5.2 20.5 21.0 102 19-159 Styrene ug/kg <5.2 20.5 20.4 100 15-152 tert-Butyl benzene ug/kg <5.2 20.5 17.7 86 31-141 Tetrachloroethene ug/kg <5.2 20.5 17.4 85 19-141 Toluene ug/kg <5.2 20.5 21.0 102 31-146 trans-1,2-Dichloroethene ug/kg <5.2 20.5 21.2 103 28-157 trans- 1,3-Dichloropropene ug/kg <5.2 20.5 19.1 93 25-146 Trichloroethene ug/kg <5.2 20.5 20.0 98 34-149 Trichlorofluoromethane ug/kg <5.2 20.5 24.4 119 10-167 v1 Vinyl acetate ug/kg <51.6 41.1 36.8J 90 10-200 Vinyl chloride ug/kg <10.3 20.5 24.9 121 36-155 Xylene (Total) ug/kg <10.3 61.6 60.9 99 29-148 1,2-Dichloroethane-d4 (S) % 112 70-132 4-Bromofluorobenzene (S) % 107 70-130 Toluene-d8 (S) % 102 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 52 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 SAMPLE DUPLICATE: 2890030 Parameter Units 92477858011 Result Dup Result 1,1,1,2-Tetrachloroethane ug/kg <4.8 ND 1,1,1-Trichloroethane ug/kg <4.8 ND 1,1,2,2-Tetrachloroethane ug/kg <4.8 ND 1,1,2-Trichloroethane ug/kg <4.8 ND 1,1-Dichloroethane ug/kg <4.8 ND 1,1-Dichloroethene ug/kg <4.8 ND 1,1-Dichloropropene ug/kg <4.8 ND 1,2,3-Trichlorobenzene ug/kg <4.8 ND 1,2,3-Trichloropropane ug/kg <4.8 ND 1,2,4-Trichlorobenzene ug/kg <4.8 ND 1,2,4-Trimethylbenzene ug/kg <4.8 ND 1,2-Dibromo-3-chloropropane ug/kg <4.8 ND 1,2-Dibromoethane (EDB) ug/kg <4.8 ND 1,2-Dichlorobenzene ug/kg <4.8 ND 1,2-Dichloroethane ug/kg <4.8 ND 1,2-Dichloropropane ug/kg <4.8 ND 1,3,5-Trimethylbenzene ug/kg <4.8 ND 1,3-Dichlorobenzene ug/kg <4.8 ND 1,3-Dichloropropane ug/kg <4.8 ND 1,4-Dichlorobenzene ug/kg <4.8 ND 2,2-Dichloropropane ug/kg <4.8 ND 2-Butanone (MEK) ug/kg <95.4 ND 2-Chlorotoluene ug/kg <4.8 ND 2-Hexanone ug/kg <47.7 ND 4-Chlorotoluene ug/kg <4.8 ND 4-Methyl-2-pentanone (MIBK) ug/kg <47.7 ND Acetone ug/kg 13.9J 27.6J Benzene ug/kg <4.8 ND Bromobenzene ug/kg <4.8 ND Bromochloromethane ug/kg <4.8 ND Bromodichloromethane ug/kg <4.8 ND Bromoform ug/kg <4.8 ND Bromomethane ug/kg <9.5 ND Carbon tetrachloride ug/kg <4.8 ND Chlorobenzene ug/kg <4.8 ND Chloroethane ug/kg <9.5 ND Chloroform ug/kg <4.8 ND Chloromethane ug/kg <9.5 ND cis-1,2-Dichloroethene ug/kg <4.8 ND cis-1,3-Dichloropropene ug/kg <4.8 ND Dibromochloromethane ug/kg <4.8 ND Dibromomethane ug/kg <4.8 ND Dichlorodifluoromethane ug/kg <9.5 ND Diisopropyl ether ug/kg <4.8 ND Ethylbenzene ug/kg <4.8 ND Hexachloro-1,3-butadiene ug/kg <4.8 ND Isopropylbenzene (Cumene) ug/kg <4.8 ND RPD Qualifiers IH v1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 53 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 SAMPLE DUPLICATE: 2890030 Parameter Units 92477858011 Result Dup Result m&p-Xylene ug/kg <9.5 ND Methyl-tert-butyl ether ug/kg <4.8 ND Methylene Chloride ug/kg <19.1 ND n-Butylbenzene ug/kg <4.8 ND n-Propylbenzene ug/kg <4.8 ND Naphthalene ug/kg <4.8 ND o-Xylene ug/kg <4.8 ND p-Isopropyltoluene ug/kg <4.8 ND sec-Butylbenzene ug/kg <4.8 ND Styrene ug/kg <4.8 ND tert-Butyl benzene ug/kg <4.8 ND Tetrachloroethene ug/kg <4.8 ND Toluene ug/kg <4.8 ND trans-1,2-Dichloroethene ug/kg <4.8 ND trans- 1,3-Dichloropropene ug/kg <4.8 ND Trichloroethene ug/kg <4.8 ND Trichlorofluoromethane ug/kg <4.8 ND Vinyl acetate ug/kg <47.7 ND Vinyl chloride ug/kg <9.5 ND Xylene (Total) ug/kg <9.5 ND 1,2-Dichloroethane-d4 (S) % 102 106 4-Bromofluorobenzene (S) % 102 103 Toluene-d8 (S) % 103 105 RPD Qualifiers v1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 54 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 542791 Analysis Method: EPA 8081 B QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 METHOD BLANK: 2891544 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 4,4'-DDD ug/kg ND 2.0 05/21/20 17:02 4,4'-DDE ug/kg ND 2.0 05/21/20 17:02 4,4'-DDT ug/kg ND 2.0 05/21/20 17:02 Aldrin ug/kg ND 2.0 05/21/20 17:02 alpha-BHC ug/kg ND 2.0 05/21/20 17:02 beta-BHC ug/kg ND 2.0 05/21/20 17:02 Chlordane (Technical) ug/kg ND 7.0 05/21/20 17:02 delta-BHC ug/kg ND 2.0 05/21/20 17:02 Dieldrin ug/kg ND 2.0 05/21/20 17:02 Endosulfan I ug/kg ND 2.0 05/21/20 17:02 Endosulfan 11 ug/kg ND 2.0 05/21/20 17:02 Endosulfan sulfate ug/kg ND 2.0 05/21/20 17:02 Endrin ug/kg ND 2.0 05/21/20 17:02 Endrin aldehyde ug/kg ND 2.0 05/21/20 17:02 Endrin ketone ug/kg ND 2.0 05/21/20 17:02 gamma-BHC (Lindane) ug/kg ND 2.0 05/21/20 17:02 Heptachlor ug/kg ND 2.0 05/21/20 17:02 Heptachlor epoxide ug/kg ND 2.0 05/21/20 17:02 Hexachlorobenzene ug/kg ND 2.0 05/21/20 17:02 Methoxychlor ug/kg ND 5.0 05/21/20 17:02 Mirex ug/kg ND 5.0 05/21/20 17:02 Toxaphene ug/kg ND 7.0 05/21/20 17:02 Decachlorobiphenyl (S) % 141 10-130 05/21/20 17:02 S3 Tetrachloro-m-xylene (S) % 126 15-130 05/21/20 17:02 LABORATORY CONTROL SAMPLE: 2891545 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/kg 8.2 9.0 110 65-130 4,4'-DDE ug/kg 8.2 8.5 104 62-130 4,4'-DDT ug/kg 8.2 8.1 99 46-130 Aldrin ug/kg 8.2 7.8 96 46-130 alpha-BHC ug/kg 8.2 7.9 97 41-130 beta-BHC ug/kg 8.2 8.8 108 45-130 delta-BHC ug/kg 8.2 7.3 89 59-130 Dieldrin ug/kg 8.2 8.6 105 59-130 Endosulfan I ug/kg 8.2 8.3 102 60-130 Endosulfan II ug/kg 8.2 8.4 103 64-130 Endosulfan sulfate ug/kg 8.2 8.5 104 67-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 55 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Davidson NC Pace Project No.: 92477861 LABORATORY CONTROL SAMPLE: 2891545 Parameter Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) I•r_11IVp1=11u111WfMLb1»:i Parameter 4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC beta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg `-11-1`NE1y Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg QUALITY CONTROL DATA Spike Conc. 8.2 8.2 8.2 8.2 8.2 8.2 8.2 24.6 24.6 LCS Result 92477861001 Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9.0 7.5 9.2 8.0 7.3 7.7 7.8 23.0 23.8 Spike Conc. 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 8.9 26.7 26.7 LCS % Rec 109 92 112 97 89 93 95 94 97 133 127 MS Result 9.8 9.0 8.8 9.2 8.3 9.3 7.7 9.3 8.8 9.1 9.2 10 8.1 10.4 8.4 7.8 7.9 7.9 25.4 24.8 % Rec Limits Qualifiers 62-130 52-130 57-130 47-130 48-130 56-130 40-130 62-130 70-130 10-130 SO 15-130 MS % Rec % Rec Limits 110 36-130 101 26-131 99 32-131 103 28-130 93 10-123 105 25-130 86 28-130 104 29-130 99 31-130 102 18-141 103 40-130 112 19-147 91 25-130 117 27-134 94 30-130 87 33-130 89 33-130 89 10-147 95 26-133 93 26-125 122 10-130 112 15-130 SAMPLE DUPLICATE: 2891547 92477861002 Dup Parameter Units Result Result RPD Qualifiers 4,4'-DDD ug/kg ND ND 4,4'-DDE ug/kg ND ND 4,4'-DDT ug/kg ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Qualifiers Page 56 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 SAMPLE DUPLICATE: 2891547 Parameter Units 92477861002 Result Dup Result Aldrin ug/kg ND ND alpha-BHC ug/kg ND ND beta-BHC ug/kg ND ND Chlordane (Technical) ug/kg ND ND delta-BHC ug/kg ND ND Dieldrin ug/kg ND ND Endosulfan I ug/kg ND ND Endosulfan II ug/kg ND ND Endosulfan sulfate ug/kg ND ND Endrin ug/kg ND ND Endrin aldehyde ug/kg ND ND Endrin ketone ug/kg ND ND gamma-BHC (Lindane) ug/kg ND ND Heptachlor ug/kg ND ND Heptachlor epoxide ug/kg ND ND Hexachlorobenzene ug/kg ND ND Methoxychlor ug/kg ND ND Mirex ug/kg ND ND Toxaphene ug/kg ND ND Decachlorobiphenyl (S) % 109 106 Tetrachloro-m-xylene (S) % 97 93 RPD Qualifiers D3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 57 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 542064 Analysis Method: EPA 8082A QC Batch Method: EPA 3546 Analysis Description: 8082 GCS PCB Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 METHOD BLANK: 2888357 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/kg ND 32.7 05/19/20 17:15 PCB-1221 (Aroclor 1221) ug/kg ND 32.7 05/19/20 17:15 PCB-1232 (Aroclor 1232) ug/kg ND 32.7 05/19/20 17:15 PCB-1242 (Aroclor 1242) ug/kg ND 32.7 05/19/20 17:15 PCB-1248 (Aroclor 1248) ug/kg ND 32.7 05/19/20 17:15 PCB-1254 (Aroclor 1254) ug/kg ND 32.7 05/19/20 17:15 PCB-1260 (Aroclor 1260) ug/kg ND 32.7 05/19/20 17:15 Decachlorobiphenyl (S) % 107 10-130 05/19/20 17:15 LABORATORY CONTROL SAMPLE: 2888358 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/kg 167 119 72 35-130 PCB-1260 (Aroclor 1260) ug/kg 167 123 74 46-130 Decachlorobiphenyl (S) % 100 10-130 MATRIX SPIKE SAMPLE: Parameter 2888359 Units 92477610001 Result Spike MS Conc. Result MS % Rec % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/kg ND 175 87.5 50 10-130 PCB-1260 (Aroclor 1260) ug/kg ND 175 91.1 52 10-130 Decachlorobiphenyl (S) % 80 10-130 SAMPLE DUPLICATE: 2888360 92477610002 Dup Parameter Units Result Result RPD Qualifiers PCB-1016 (Aroclor 1016) ug/kg ND ND PCB-1221 (Aroclor 1221) ug/kg ND ND PCB-1232 (Aroclor 1232) ug/kg ND ND PCB-1242 (Aroclor 1242) ug/kg ND ND PCB-1248 (Aroclor 1248) ug/kg ND ND PCB-1254 (Aroclor 1254) ug/kg ND ND PCB-1260 (Aroclor 1260) ug/kg ND ND Decachlorobiphenyl (S) % 79 69 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 58 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 542564 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 METHOD BLANK: 2890605 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed 1,2,4-Trichlorobenzene ug/kg ND 325 05/20/20 10:34 1,2-Dichlorobenzene ug/kg ND 325 05/20/20 10:34 1,3-Dichlorobenzene ug/kg ND 325 05/20/20 10:34 1,4-Dichlorobenzene ug/kg ND 325 05/20/20 10:34 1-Methylnaphthalene ug/kg ND 325 05/20/20 10:34 2,2'-Oxybis(1-chloropropane) ug/kg ND 325 05/20/20 10:34 2,4,5-Trichlorophenol ug/kg ND 325 05/20/20 10:34 2,4,6-Trichlorophenol ug/kg ND 325 05/20/20 10:34 2,4-Dichlorophenol ug/kg ND 325 05/20/20 10:34 2,4-Dimethylphenol ug/kg ND 325 05/20/20 10:34 2,4-Dinitrophenol ug/kg ND 1620 05/20/20 10:34 2,4-Dinitrotoluene ug/kg ND 325 05/20/20 10:34 2,6-Dinitrotoluene ug/kg ND 325 05/20/20 10:34 2-Chloronaphthalene ug/kg ND 325 05/20/20 10:34 2-Chlorophenol ug/kg ND 325 05/20/20 10:34 2-Methylnaphthalene ug/kg ND 325 05/20/20 10:34 2-Methylphenol(o-Cresol) ug/kg ND 325 05/20/20 10:34 2-Nitroaniline ug/kg ND 1620 05/20/20 10:34 2-Nitrophenol ug/kg ND 325 05/20/20 10:34 3&4-Methyl phenol (m&p Cresol) ug/kg ND 325 05/20/20 10:34 3,3'-Dichlorobenzidine ug/kg ND 649 05/20/20 10:34 3-Nitroaniline ug/kg ND 1620 05/20/20 10:34 4,6-Dinitro-2-methyl phenol ug/kg ND 649 05/20/20 10:34 4-Bromophenylphenyl ether ug/kg ND 325 05/20/20 10:34 4-ChIoro-3-methyl phenol ug/kg ND 649 05/20/20 10:34 4-Chloroaniline ug/kg ND 649 05/20/20 10:34 4-Chlorophenylphenyl ether ug/kg ND 325 05/20/20 10:34 4-Nitroaniline ug/kg ND 649 05/20/20 10:34 4-Nitrophenol ug/kg ND 1620 05/20/20 10:34 Acenaphthene ug/kg ND 325 05/20/20 10:34 Acenaphthylene ug/kg ND 325 05/20/20 10:34 Aniline ug/kg ND 325 05/20/20 10:34 Anthracene ug/kg ND 325 05/20/20 10:34 Benzo(a)anthracene ug/kg ND 325 05/20/20 10:34 Benzo(a)pyrene ug/kg ND 325 05/20/20 10:34 Benzo(b)fluoranthene ug/kg ND 325 05/20/20 10:34 Benzo(g,h,i)perylene ug/kg ND 325 05/20/20 10:34 v2 Benzo(k)fluoranthene ug/kg ND 325 05/20/20 10:34 Benzoic Acid ug/kg ND 1620 05/20/20 10:34 Benzyl alcohol ug/kg ND 649 05/20/20 10:34 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 59 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 METHOD BLANK: 2890605 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed bis(2-Chloroethoxy)methane ug/kg ND 325 05/20/20 10:34 bis(2-Chloroethyl) ether ug/kg ND 325 05/20/20 10:34 bis(2-Ethylhexyl)phthalate ug/kg ND 325 05/20/20 10:34 Butylbenzylphthalate ug/kg ND 325 05/20/20 10:34 Chrysene ug/kg ND 325 05/20/20 10:34 Di-n-butylphthalate ug/kg ND 325 05/20/20 10:34 Di-n-octylphthalate ug/kg ND 325 05/20/20 10:34 Dibenz(a,h)anthracene ug/kg ND 325 05/20/20 10:34 v2 Dibenzofuran ug/kg ND 325 05/20/20 10:34 Diethylphthalate ug/kg ND 325 05/20/20 10:34 Dimethylphthalate ug/kg ND 325 05/20/20 10:34 Fluoranthene ug/kg ND 325 05/20/20 10:34 Fluorene ug/kg ND 325 05/20/20 10:34 Hexachloro-1,3-butadiene ug/kg ND 325 05/20/20 10:34 Hexachlorobenzene ug/kg ND 325 05/20/20 10:34 Hexachlorocyclopentadiene ug/kg ND 325 05/20/20 10:34 Hexachloroethane ug/kg ND 325 05/20/20 10:34 Indeno(1,2,3-cd)pyrene ug/kg ND 325 05/20/20 10:34 v2 Isophorone ug/kg ND 325 05/20/20 10:34 N-Nitroso-di-n-propylamine ug/kg ND 325 05/20/20 10:34 N-Nitrosodimethylamine ug/kg ND 325 05/20/20 10:34 N-Nitrosodiphenylamine ug/kg ND 325 05/20/20 10:34 Naphthalene ug/kg ND 325 05/20/20 10:34 Nitrobenzene ug/kg ND 325 05/20/20 10:34 Pentachlorophenol ug/kg ND 649 05/20/20 10:34 Phenanthrene ug/kg ND 325 05/20/20 10:34 Phenol ug/kg ND 325 05/20/20 10:34 Pyrene ug/kg ND 325 05/20/20 10:34 Pyridine ug/kg ND 325 05/20/20 10:34 2,4,6-Tribromophenol (S) % 75 27-110 05/20/20 10:34 2-Fluorobiphenyl (S) % 75 30-110 05/20/20 10:34 2-Fluorophenol(S) % 71 13-110 05/20/20 10:34 Nitrobenzene-d5 (S) % 71 23-110 05/20/20 10:34 Phenol-d6 (S) % 75 22-110 05/20/20 10:34 Terphenyl-d14 (S) % 115 28-110 05/20/20 10:34 S3 Qualifiers LABORATORY CONTROL SAMPLE: 2890606 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg 1690 1520 90 52-130 1,2-Dichlorobenzene ug/kg 1690 1590 94 51-130 1,3-Dichlorobenzene ug/kg 1690 1550 91 50-130 1,4-Dichlorobenzene ug/kg 1690 1640 97 49-130 1-Methylnaphthalene ug/kg 1690 1450 86 55-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 60 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 LABORATORY CONTROL SAMPLE: Parameter 2890606 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,2'-Oxybis(1-chloropropane) ug/kg 1690 1630 96 30-130 2,4,5-Trichlorophenol ug/kg 1690 1730 102 55-130 2,4,6-Trichlorophenol ug/kg 1690 1690 100 57-130 2,4-Dichlorophenol ug/kg 1690 1630 96 56-130 2,4-Dimethylphenol ug/kg 1690 1600 94 51-130 2,4-Dinitrophenol ug/kg 8470 8250 97 27-133 2,4-Dinitrotoluene ug/kg 1690 1760 104 61-130 2,6-Dinitrotoluene ug/kg 1690 1260 74 60-130 2-Chloronaphthalene ug/kg 1690 1680 99 52-130 2-Chlorophenol ug/kg 1690 1690 100 54-130 2-Methylnaphthalene ug/kg 1690 1510 89 54-130 2-Methylphenol(o-Cresol) ug/kg 1690 1650 97 51-130 2-Nitroaniline ug/kg 3390 3270 96 51-130 2-Nitrophenol ug/kg 1690 1670 99 49-130 3&4-Methyl phenol (m&p Cresol) ug/kg 1690 1640 97 11-163 3,3'-Dichlorobenzidine ug/kg 3390 3500 103 10-132 3-Nitroaniline ug/kg 3390 3360 99 55-130 4,6-Dinitro-2-methyl phenol ug/kg 3390 3400 100 47-142 4-Bromophenylphenyl ether ug/kg 1690 1540 91 59-130 4-ChIoro-3-methyl phenol ug/kg 3390 3140 92 55-130 4-Chloroaniline ug/kg 3390 3340 99 54-130 4-Chlorophenylphenyl ether ug/kg 1690 1580 93 58-130 4-Nitroaniline ug/kg 3390 3600 106 54-130 4-Nitrophenol ug/kg 8470 8250 97 48-130 Acenaphthene ug/kg 1690 1680 99 60-130 Acenaphthylene ug/kg 1690 1710 101 60-130 Aniline ug/kg 1690 1580 93 43-130 Anthracene ug/kg 1690 1670 99 63-130 Benzo(a)anthracene ug/kg 1690 1710 101 59-130 Benzo(a)pyrene ug/kg 1690 1730 102 57-130 Benzo(b)fluoranthene ug/kg 1690 1980 117 54-130 Benzo(g,h,i)perylene ug/kg 1690 1390 82 59-130 v3 Benzo(k)fluoranthene ug/kg 1690 1850 109 54-130 Benzoic Acid ug/kg 8470 5290 62 19-130 Benzyl alcohol ug/kg 3390 3180 94 50-130 bis(2-Chloroethoxy)methane ug/kg 1690 1470 87 54-130 bis(2-Chloroethyl) ether ug/kg 1690 1550 92 48-130 bis(2-Ethylhexyl)phthalate ug/kg 1690 1620 95 45-134 Butylbenzylphthalate ug/kg 1690 1790 106 46-138 Chrysene ug/kg 1690 1650 98 58-130 Di-n-butylphthalate ug/kg 1690 1590 94 60-130 Di-n-octylphthalate ug/kg 1690 1820 107 53-130 Dibenz(a,h)anthracene ug/kg 1690 1260 74 59-130 v3 Dibenzofuran ug/kg 1690 1670 99 60-130 Diethylphthalate ug/kg 1690 1570 93 60-130 Dimethylphthalate ug/kg 1690 1610 95 60-130 Fluoranthene ug/kg 1690 1750 103 65-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 61 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 LABORATORY CONTROL SAMPLE: Parameter 2890606 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Fluorene ug/kg 1690 1650 97 63-130 Hexachloro-1,3-butadiene ug/kg 1690 1370 81 46-130 Hexachlorobenzene ug/kg 1690 1600 94 58-130 Hexachlorocyclopentadiene ug/kg 1690 1350 80 23-130 Hexachloroethane ug/kg 1690 1540 91 47-130 Indeno(1,2,3-cd)pyrene ug/kg 1690 1400 83 60-130 v3 Isophorone ug/kg 1690 1480 87 49-130 N-Nitroso-di-n-propylamine ug/kg 1690 1550 91 47-130 N-Nitrosodimethylamine ug/kg 1690 1630 96 45-130 N-Nitrosodiphenylamine ug/kg 1690 1650 98 59-130 Naphthalene ug/kg 1690 1570 93 55-130 Nitrobenzene ug/kg 1690 1510 89 49-130 Pentachlorophenol ug/kg 3390 3580 106 10-132 Phenanthrene ug/kg 1690 1640 97 62-130 Phenol ug/kg 1690 1820 107 46-130 Pyrene ug/kg 1690 1790 106 53-130 Pyridine ug/kg 1690 1330 79 37-130 2,4,6-Tribromophenol (S) % 91 27-110 2-Fluorobiphenyl (S) % 83 30-110 2-Fluorophenol(S) % 92 13-110 Nitrobenzene-d5 (S) % 81 23-110 Phenol-d6 (S) % 93 22-110 Terphenyl-d14 (S) % 103 28-110 MATRIX SPIKE SAMPLE: Parameter 2890607 Units 92477861001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg ND 1770 1280 72 18-130 1,2-Dichlorobenzene ug/kg ND 1770 1310 74 14-130 1,3-Dichlorobenzene ug/kg ND 1770 1260 71 12-130 1,4-Dichlorobenzene ug/kg ND 1770 1360 77 10-130 1-Methylnaphthalene ug/kg ND 1770 1190 67 12-130 2,2'-Oxybis(1-chloropropane) ug/kg ND 1770 1390 79 10-130 2,4,5-Trichlorophenol ug/kg ND 1770 1480 84 13-130 2,4,6-Trichlorophenol ug/kg ND 1770 1420 80 17-130 2,4-Dichlorophenol ug/kg ND 1770 1360 77 10-130 2,4-Dimethylphenol ug/kg ND 1770 1310 74 10-130 2,4-Dinitrophenol ug/kg ND 8830 4330 49 10-130 2,4-Dinitrotoluene ug/kg ND 1770 1550 88 24-130 2,6-Dinitrotoluene ug/kg ND 1770 1100 62 23-130 2-Chloronaphthalene ug/kg ND 1770 1380 78 19-130 2-Chlorophenol ug/kg ND 1770 1400 79 10-130 2-Methylnaphthalene ug/kg ND 1770 1250 71 18-130 2-Methylphenol(o-Cresol) ug/kg ND 1770 1340 76 10-130 2-Nitroaniline ug/kg ND 3530 2910 82 17-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 62 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 MATRIX SPIKE SAMPLE: 2890607 92477861001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Nitrophenol ug/kg ND 1770 1410 80 10-130 3&4-Methyl phenol (m&p Cresol) ug/kg ND 1770 1310 74 10-130 3,3'-Dichlorobenzidine ug/kg ND 3530 3030 86 10-130 3-Nitroaniline ug/kg ND 3530 3020 85 24-130 4,6-Dinitro-2-methyl phenol ug/kg ND 3530 2940 83 10-152 4-Bromophenylphenyl ether ug/kg ND 1770 1400 79 29-130 4-Chloro-3-methylphenol ug/kg ND 3530 2650 75 17-130 4-Chloroaniline ug/kg ND 3530 2800 79 14-130 4-Chlorophenylphenyl ether ug/kg ND 1770 1330 75 25-130 4-Nitroaniline ug/kg ND 3530 3290 93 22-130 4-Nitrophenol ug/kg ND 8830 7200 81 10-130 Acenaphthene ug/kg ND 1770 1410 80 20-130 Acenaphthylene ug/kg ND 1770 1440 82 25-130 Aniline ug/kg ND 1770 1260 72 10-130 Anthracene ug/kg ND 1770 1500 85 29-130 Benzo(a)anthracene ug/kg ND 1770 1500 85 19-130 Benzo(a)pyrene ug/kg ND 1770 1540 87 12-130 Benzo(b)fluoranthene ug/kg ND 1770 1660 94 14-130 Benzo(g,h,i)perylene ug/kg ND 1770 1270 72 10-130 v3 Benzo(k)fluoranthene ug/kg ND 1770 1580 89 14-130 Benzoic Acid ug/kg ND 8830 1590J 18 10-130 Benzyl alcohol ug/kg ND 3530 2550 72 13-130 bis(2-Chloroethoxy)methane ug/kg ND 1770 1250 71 16-130 bis(2-Chloroethyl) ether ug/kg ND 1770 1300 74 11-130 bis(2-Ethylhexyl)phthalate ug/kg ND 1770 1450 82 21-130 Butylbenzylphthalate ug/kg ND 1770 1520 86 23-130 Chrysene ug/kg ND 1770 1460 83 22-130 Di-n-butylphthalate ug/kg ND 1770 1420 81 30-130 Di-n-octylphthalate ug/kg ND 1770 1520 86 23-142 Dibenz(a,h)anthracene ug/kg ND 1770 1140 65 10-130 v3 Dibenzofuran ug/kg ND 1770 1400 79 24-130 Diethylphthalate ug/kg ND 1770 1390 79 26-130 Dimethylphthalate ug/kg ND 1770 1400 79 22-130 Fluoranthene ug/kg ND 1770 1510 86 33-130 Fluorene ug/kg ND 1770 1410 80 22-130 Hexachloro-1,3-butadiene ug/kg ND 1770 1140 64 13-130 Hexachlorobenzene ug/kg ND 1770 1460 83 29-130 Hexachlorocyclopentadiene ug/kg ND 1770 994 56 10-130 Hexachloroethane ug/kg ND 1770 1280 73 10-130 Indeno(1,2,3-cd)pyrene ug/kg ND 1770 1240 70 10-130 v3 Isophorone ug/kg ND 1770 1250 71 13-130 N-Nitroso-di-n-propylamine ug/kg ND 1770 1300 74 12-130 N-Nitrosodimethylamine ug/kg ND 1770 1250 71 11-130 N-Nitrosodiphenylamine ug/kg ND 1770 1500 85 15-130 Naphthalene ug/kg ND 1770 1310 74 15-130 Nitrobenzene ug/kg ND 1770 1290 73 12-130 Pentachlorophenol ug/kg ND 3530 3220 91 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 63 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 MATRIX SPIKE SAMPLE: Parameter 2890607 Units 92477861001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Phenanthrene ug/kg ND 1770 1480 84 27-130 Phenol ug/kg ND 1770 1460 82 10-130 Pyrene ug/kg ND 1770 1630 92 19-130 Pyridine ug/kg ND 1770 1080 61 10-130 2,4,6-Tribromophenol (S) % 82 27-110 2-Fluorobiphenyl (S) % 69 30-110 2-Fluorophenol(S) % 75 13-110 Nitrobenzene-d5 (S) % 69 23-110 Phenol-d6 (S) % 75 22-110 Terphenyl-d14 (S) % 93 28-110 SAMPLE DUPLICATE: 2890608 Parameter Units 92477861001 Result Dup Result 1,2,4-Trichlorobenzene ug/kg ND ND 1,2-Dichlorobenzene ug/kg ND ND 1,3-Dichlorobenzene ug/kg ND ND 1,4-Dichlorobenzene ug/kg ND ND 1-Methylnaphthalene ug/kg ND ND 2,2'-Oxybis(1-chloropropane) ug/kg ND ND 2,4,5-Trichlorophenol ug/kg ND ND 2,4,6-Trichlorophenol ug/kg ND ND 2,4-Dichlorophenol ug/kg ND ND 2,4-Dimethylphenol ug/kg ND ND 2,4-Dinitrophenol ug/kg ND ND 2,4-Dinitrotoluene ug/kg ND ND 2,6-Dinitrotoluene ug/kg ND ND 2-Chloronaphthalene ug/kg ND ND 2-Chlorophenol ug/kg ND ND 2-Methylnaphthalene ug/kg ND ND 2-Methylphenol(o-Cresol) ug/kg ND ND 2-Nitroaniline ug/kg ND ND 2-Nitrophenol ug/kg ND ND 3&4-Methyl phenol (m&p Cresol) ug/kg ND ND 3,3'-Dichlorobenzidine ug/kg ND ND 3-Nitroaniline ug/kg ND ND 4,6-Dinitro-2-methyl phenol ug/kg ND ND 4-Bromophenylphenyl ether ug/kg ND ND 4-ChIoro-3-methyl phenol ug/kg ND ND 4-Chloroaniline ug/kg ND ND 4-Chlorophenylphenyl ether ug/kg ND ND 4-Nitroaniline ug/kg ND ND 4-Nitrophenol ug/kg ND ND Acenaphthene ug/kg ND ND Acenaphthylene ug/kg ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 64 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 SAMPLE DUPLICATE: 2890608 Parameter Units 92477861001 Result Dup Result Aniline ug/kg ND ND Anthracene ug/kg ND ND Benzo(a)anthracene ug/kg ND ND Benzo(a)pyrene ug/kg ND ND Benzo(b)fluoranthene ug/kg ND ND Benzo(g,h,i)perylene ug/kg ND ND Benzo(k)fluoranthene ug/kg ND ND Benzoic Acid ug/kg ND ND Benzyl alcohol ug/kg ND ND bis(2-Chloroethoxy)methane ug/kg ND ND bis(2-Chloroethyl) ether ug/kg ND ND bis(2-Ethylhexyl)phthalate ug/kg ND ND Butylbenzylphthalate ug/kg ND ND Chrysene ug/kg ND ND Di-n-butylphthalate ug/kg ND ND Di-n-octylphthalate ug/kg ND ND Dibenz(a,h)anthracene ug/kg ND ND Dibenzofuran ug/kg ND ND Diethylphthalate ug/kg ND ND Dimethylphthalate ug/kg ND ND Fluoranthene ug/kg ND ND Fluorene ug/kg ND ND Hexachloro-1,3-butadiene ug/kg ND ND Hexachlorobenzene ug/kg ND ND Hexachlorocyclopentadiene ug/kg ND ND Hexachloroethane ug/kg ND ND Indeno(1,2,3-cd)pyrene ug/kg ND ND Isophorone ug/kg ND ND N-Nitroso-di-n-propylamine ug/kg ND ND N-Nitrosodimethylamine ug/kg ND ND N-Nitrosodiphenylamine ug/kg ND ND Naphthalene ug/kg ND ND Nitrobenzene ug/kg ND ND Pentachlorophenol ug/kg ND ND Phenanthrene ug/kg ND ND Phenol ug/kg ND ND Pyrene ug/kg ND ND Pyridine ug/kg ND ND 2,4,6-Tribromophenol (S) % 65 68 2-Fluorobiphenyl (S) % 45 49 2-Fluorophenol(S) % 45 55 Nitrobenzene-d5 (S) % 46 55 Phenol-d6 (S) % 48 58 Terphenyl-d14 (S) % 97 98 RPD Qualifiers v2 v2 v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 65 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 542365 Analysis Method: MADEP EPH QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 METHOD BLANK: 2889774 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Aliphatic (C09-C18) mg/kg ND 9.8 05/20/20 16:31 N2 Aliphatic (C19-C36) mg/kg ND 9.8 05/20/20 16:31 N2 Aromatic (C11-C22) mg/kg ND 9.8 05/20/20 16:58 N2 2-Bromonaphthalene (S) % 124 40-140 05/20/20 16:58 2-Fluorobiphenyl (S) % 124 40-140 05/20/20 16:58 Nonatriacontane (S) % 74 40-140 05/20/20 16:31 o-Terphenyl (S) % 99 40-140 05/20/20 16:58 LABORATORY CONTROL SAMPLE & LCSD: Parameter 2889775 Units Spike Conc. 2889776 LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Max Limits RPD RPD Qualifiers Aliphatic (C09-C18) mg/kg 9.8 ND ND 52 51 40-140 50 N2 Aliphatic (C19-C36) mg/kg 13.1 ND ND 57 61 40-140 50 N2 Aromatic (C11-C22) mg/kg 27.9 21.1 23.4 76 81 40-140 10 50 N2 2-Bromonaphthalene (S) % 114 118 40-140 2-Fluorobiphenyl (S) % 114 119 40-140 Nonatriacontane (S) % 63 69 40-140 o-Terphenyl(S) % 84 91 40-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 66 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 542121 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 SAMPLE DUPLICATE: 2888728 92477783002 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 19.3 19.7 2 SAMPLE DUPLICATE: 2888729 92477861005 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 18.6 16.9 9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 67 of 72 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Davidson NC Pace Project No.: 92477861 QC Batch: 1481811 Analysis Method: SM 2540G QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 METHOD BLANK: R3532019-1 Matrix: Solid Associated Lab Samples: 92477861001, 92477861002, 92477861003, 92477861004, 92477861005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Solids % ND 05/26/20 17:21 LABORATORY CONTROL SAMPLE: R3532019-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Solids % 50.0 50.0 100 85.0-115 SAMPLE DUPLICATE: R3532019-3 L1219931-02 Dup Parameter Units Result Result RPD Qualifiers Total Solids % 82.2 82.6 0.496 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 68 of 72 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Davidson NC Pace Project No.: 92477861 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased low. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. SO Surrogate recovery outside laboratory control limits. S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 69 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Davidson NC 92477861 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92477861006 SW-1 EPA1664B 542722 92477861007 SW-2 EPA1664B 542722 92477861001 HA-1 EPA 3546 542791 EPA 8081 B 542877 92477861002 HA-2 EPA 3546 542791 EPA 8081 B 542877 92477861003 HA-3 EPA 3546 542791 EPA 8081 B 542877 92477861004 HA-4 EPA 3546 542791 EPA 8081 B 542877 92477861005 Background EPA 3546 542791 EPA 8081 B 542877 92477861001 HA-1 EPA 3546 542064 EPA 8082A 542265 92477861002 HA-2 EPA 3546 542064 EPA 8082A 542265 92477861003 HA-3 EPA 3546 542064 EPA 8082A 542265 92477861004 HA-4 EPA 3546 542064 EPA 8082A 542265 92477861005 Background EPA 3546 542064 EPA 8082A 542265 92477861001 HA-1 MADEP EPH 542365 MADEP EPH 542915 92477861002 HA-2 MADEP EPH 542365 MADEP EPH 542915 92477861003 HA-3 MADEP EPH 542365 MADEP EPH 542915 92477861004 HA-4 MADEP EPH 542365 MADEP EPH 542915 92477861005 Background MADEP EPH 542365 MADEP EPH 542915 92477861001 HA-1 MADEPV 1480781 MADEP VPH 1480781 92477861002 HA-2 MADEPV 1480781 MADEP VPH 1480781 92477861003 HA-3 MADEPV 1480781 MADEP VPH 1480781 92477861004 HA-4 MADEPV 1480781 MADEP VPH 1480781 92477861005 Background MADEPV 1480781 MADEP VPH 1480781 92477861001 HA-1 EPA 3050B 543033 EPA 6010D 543154 92477861002 HA-2 EPA 3050B 543033 EPA 6010D 543154 92477861003 HA-3 EPA 3050B 543033 EPA 6010D 543154 92477861004 HA-4 EPA 3050B 543033 EPA 6010D 543154 92477861005 Background EPA 3050B 543033 EPA 6010D 543154 92477861001 HA-1 EPA 3546 542564 EPA 8270E 542582 92477861002 HA-2 EPA 3546 542564 EPA 8270E 542582 92477861003 HA-3 EPA 3546 542564 EPA 8270E 542582 92477861004 HA-4 EPA 3546 542564 EPA 8270E 542582 92477861005 Background EPA 3546 542564 EPA 8270E 542582 92477861001 HA-1 EPA 5035A 542191 EPA 8260D 542212 92477861002 HA-2 EPA 5035A 542191 EPA 8260D 542212 92477861003 HA-3 EPA 5035A 542191 EPA 8260D 542212 92477861004 HA-4 EPA 5035A 542191 EPA 8260D 542212 92477861005 Background EPA 5035A 542191 EPA 8260D 542212 92477861001 HA-1 ASTM D2974-87 542121 92477861002 HA-2 ASTM D2974-87 542121 92477861003 HA-3 ASTM D2974-87 542121 92477861004 HA-4 ASTM D2974-87 542121 92477861005 Background ASTM D2974-87 542121 92477861001 HA-1 SM 2540 G 1481811 SM 2540G 1481811 92477861002 HA-2 SM 2540 G 1481811 SM 2540G 1481811 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2020 10:48 AM without the written consent of Pace Analytical Services, LLC. Page 70 of 72 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Davidson NC Pace Project No.: 92477861 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92477861003 HA-3 SM 2540 G 1481811 SM 2540G 1481811 92477861004 HA-4 SM 2540 G 1481811 SM 2540G 1481811 92477861005 Background SM 2540 G 1481811 SM 2540G 1481811 Date: 05/28/2020 10:48 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 71 of 72 ;Weanaryrr�t' CHAIN -OF -CUSTODY 1 Analytical Request Document wwwhi The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client information: Required Project Information: Invoice Information: Page ; 1 Of 1 Company Shield Report To. Stoner, David Attention Address 4301 Taggart Creek Road Copy To. Company Name Charlotte, INC 28206 Address Re ulato A enc Email dsloner@shieldengmeenng com Pwchase Order 4 4200160-01 Pace Quote NC UST Phone (704)604-5202 JFaX Project Name Davidson NC Pace Project Manager areal payne@pacelabs.com. State! Location Requested Due Oats Standard Project # 4200160-01 Pace Profile # 754-2a/2g NC Requested Analysis Filtered YfN a' 2 MATRIX copE U COLLECTED z Preservatives >- U D-Wing wntnr Dw V a — wmm wT m w worm wntor ww _ a Proe��e v SAMPLE ID sa"fso''c 5L 7 O a) Oilo� _ '�' -- START END N One Character per box. w.po wa w w a In "' c to-2, 0-9 1. -j alrw. AIR n w z x = �- Sample Ids must be unique Tl, a TS U % T,.T,T,., Z Q Z N C i7 — N ca _ lL R a V ~ a ¢ en DATE TIME ¢ en O n rOii tV x O 2 z U = O m z m z d O Q m G Q o m o m m tr of. fit! ✓� �� i l 1 HA-1 SL G 5115120 5115120 X X X X X X 2 HA-2 SL G 5115120 1 5115120 X X X X X X /1� 3 HA-3 SL G 51 1 5M5120 — X X X X X X 4 HA -4 SL G 5115120 1 5115120- .- - X X X X X X r, V $ Qackground SL G 5115120 5115120 - X X X X X X `—y 7 — 00, 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY f AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS fir SAMPLER NAME AND SIGNATURE c U c y PRINT Name of SAMPLER: Danny Hefner SIGNATURE of SAMPLER: DATE Signed: �, z a m o? m z A c ? 111 of 72 APPENDIX D °a REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste is asbestos waste, complete Sections I, II,111 and IV If waste is NOT asbestos waste, complete Sections I, II and III I. GENERATOR (Generator completes la r) qCNI a. Generator's US EPA ID Number b. Manifest Document Number c. Page 1 of d. Generator's Name and Location: e. Generator's Mailing Address: Wayne Brothersl 10900Subury Rd Davidson, NC 28036 g. Phone: f. Phone: If owner of the generating facility differs from the generator, provide: h. Owner's Name: i. Owner's Phone No.: j. Waste Profile # k. Exp. Date I. Wastg'Shipping Name'and Description m. Containers n. Total Quantity o. Unit. WWaI No. Type 5010 20 7231 I ' soil U11- bill to17700 4 GENERATOR'S CERTIFICATION: I,hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or.any applicable nsportation according to applicable regulations: AND, if this state law, has bean properly described, classified and packaged, and is in proper conditroulsspwaste waste is a treatment residue of a previously restricted hazardous waste subject to thesal'Restrictions. I certify and warrant that the waste has been -treated in accordance with the requirements of.40 CFR 2fi and is no longer a as defined by 40 CFR 261. Ge-nerator#uQiorized A ent Name Print . Signature r..Date It. I KAIVSYUKI tK (Generator completes na-D ana i ransparzer campieres uc-e) a. Transporter's Name and Address: Wayne Brothers b. Phone: c. Driver Nan( Print . Si nature e. Date III nFSTINAT1r1N 1(-,anarafnr rmmnlPfa I]la-r. an esfinatinn Site comnletes llld-o) a. Disposal Facility and Site Address: c. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105,Morehead Rd Concord, NC 28027 b. Phone' 704=782-2004 1 herby c*tIfV that the above named material has been acce a nd to the best of my kna led a the fore pin is true and accur teU" 1 0 e- 4 e. Name bf Aulhoriz A ent not f. toe Date IV_ ASBESTOS (Generator comnletes Na-f sand Operator cornplete IVcH) a. Operatofs Name and Address: c. Responsible Agency Name and Address: b. Phone: d. Phone: e. Special Handling Instructions.and Additional Information: f. ❑ Friable ❑ Non -Friable ❑ Both % Friable % Non -Friable OPERATOR'S CERTIFICATION. I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are'classifred, packed, marked and labeled and are in all respects in proper condition for transport by highway according td'applicable international and national governmental regulations. q. Operator's Name and Title Print h. Signature 'Operator refers to the company which owns, leases, operates,.controls, or supervises the facility being demolished or renovated, or the demolition or renovation operation or both SITE BFI/CMS LANDFILL 704-782- 004 510 5 MORE HEAD RD CONCORD, NC 28025 CUSTOMER 011700 WA NE BROTHERS INC. 57 CONCRESCERE PARKWAY DAVIDSON, N "78036 Cntrat:010,2)07-)31_ C,enerator:WaNine Brothers, In SITE TICKET # CELL IfsEIGHMASTER DATEMME IN DATEMME OUT VEHICLE CONTAINER REFERENCE BILL OF LADING S AIjE Ill CROSS WEIGHT NET TONS IIj , �. BJA-D TARE OUT 'BARE WEIGHS �� 1 7 0 SET EIC�I�I' 4 8 f 0 TNVnTCE QTY. UNIT DES RiPTI N RATE EXTENSION TAX TOTAL 0, 00 YD Tracking QTY 24 .()t to -ONT SOIL --,-Ln,.ALAMANCE ID HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE WHILE IN THE LANDFILL, 1F YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW SET FROM THE SCALE HORSE. THANK YOU - The undersigned individual signing this document on behalf of Ctjstc�rner acknowledges that he or she has read and understands the terms and conditions on the reverse side and that he or she has the authority to sign this document on behalf of the custorner, TENDERED CHANGE CHECK# R-F042UPR (07112) SIGNATURE c-O PREPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste is asbestos waste, complete Sections I, II, III and IV If waste is NOT asbestos waste, complete Sections I, 11 and III GENERATOR (Generator completes la-r) a. Generator's US EPA ID Number b. Manifest Document Number c. Page 1 of d. Generator's Name and Location: e. Generator's Mailing Address: Wayne Brotherst 10900Subury Rd Davidson, NC 28036 g. Phone: f. Phone: If owner of the generating facility differs from the generator, provide: h. Owner's Name: 1. Owner's Phone No.: J. Waste Profile # k. Exp, Date I. Waste Shipping Name and m. Containers n. Total o. Unit No. I Type Description Quantity WWol. 5010 20 7231 I soil bill toll 1700 GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been property described,'classified and packaged, and is in proper coati for transportation according to applicable regulations; AND, If this waste is a treatment. residue of a previously restricted hazardous waste subject to i5e L � Disposal Restrictions. I certify and warrant that the waste has been treated in aocordance,with the requirements of 40 CFR 258 and is no long0a Wardous waste as defined b 40 CFR 261. 'Generato _kthorizedA ent:Name Print:. _. _ ., - `Si nature _ :.:- II. TRANSPORTER (Generator completes Ila-b ana I ransporter compietes iic-e) a. Transportees Name and Address: Wayne Brothers 'b. Phone: j /) -f9-6 c. Driver N e Print 'C• III. DESTINATION (Generator complet Site completes Illd-o) ASBESTOS (Generator completes IVa-f and Operator complete SITE DFI/CMS LANDFILL 70-78-004 5 10 MORE HEAD RD CC CC RIB , NC 28025 CUSTOMER 1AYNE BROTHERS INC. DAVIDSONr NC 28036 Contract: 5010-20 7)31-,� Generator: Wayne Brothers, IrL SCALE IN GROSS WEIGHT TARE OUT 'TARE WEIGHT OTY, UNIT 1 . to SST-ONT SOIL HARn HATS AND SAFETY HEST ARE RE NET TONS 7 60 NET WEIGHT DESCRIPTION Origin: ALAMAi CE 100% I ED WHEN EXITING YOUR VEHt 11.0 21r800 WHILE IN THE LANDFILL IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YU. s�T TICKET # 1744477 DELL 4 J1664 v WEIoiHMASTER DATEMME IN 10. 0 10 : , aa<< D TEITIME�V T6 r ' 0 10 : ? al VEHICLE WB,I REFERENCE BILL OF LADING RATE CONTAINER INBOUND INVOICE EXTENSION I TAX The undersigned individual signing this document on behalf of Custer acknowledges that he or she has read and understands the terms and conditions on the reverse side and that he or she has the authority to sign this document on behalf of ttre customer. TOTAL TENDERED CHANGE R -F04 U PR �07112) SIGNATURE Beverly, Trudy From: Basinger, Corey Sent: Monday, June 15, 2020 7:08 AM To: David Stoner; Beverly, Trudy Cc: Alan Goodman; Bob Griffin Subject: RE: [External] Concrescere One Initial Abatement Report Electronic copy will suffice. Thanks, Corey From: David Stoner [mailto:dstoner@shieldengineering.com] Sent: Friday, June 12, 2020 4:24 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov>; Basinger, Corey <corey.basinger@ncdenr.gov> Cc: Alan Goodman <alan.goodman@preferredconstructionsupply.com>; Bob Griffin<bgriffin@shieldengineering.com> Subject: RE: [External] Concrescere One Initial Abatement Report External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to report.spam@nc.gov Thank you Trudy. Corey, would you like a hard copy? Regards, David David A. Stoner, P.G., P.E. Sr. Principal/Vice President Shield Engineering, Inc.'s Risk Management Group 4301Taggart Creek Rd. Charlotte, NC 28208 ph. (704) 394-6913 fax (704) 394-6968 e-mail DStoner(a)ShieldEn in_ e�erin .cgom Shield Engineering's Action Environmental Group is now Shield Engineering's Risk Management Group with additional expertise and service lines! k�ii IJ www.ShieldEngineering.com [shieldene ineering coml This message is intended only for the use of the addressee and may contain information that is PRIVILEGED and CONFIDENTIAL, and/or may contain ATTORNEY WORK PRODUCT. If you are not the intended recipient, you are hereby notified that any dissemination of this communication is strictly prohibited. If you have received this communication in error, please erase all copies of the message and its attachments and notify us immediately. Thank you. From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Friday, June 12, 2020 3:06 PM To: David Stoner<dstoner@shieldengineering.com>; Basinger, Corey <corey.basinger@ncdenr.gov> Cc: Alan Goodman <alan.goodman@preferredconstructionsupply.com>; Bob Griffin<bgriffin@shieldengineering.com> Subject: RE: [External] Concrescere One Initial Abatement Report Received. No need to mail a hard copy for the UST Section. Thanks, Trudy D�EQ7�� RM rH 'fi;pn�lWd.vonRWt740u�Y1� Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy. B everly(a),ncdenr. gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: hitps://deq.nc.gov/about/divisions/waste-management/ust Inaml2.safelinks.protection.outlook.coml Branch's Above Ground Storage Tanks Website Address: ht!ps:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program Inaml2.safelinks.protection.outlook.coml INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: https://deq.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-macs Inaml2.safelinks.protection.outlook.coml File Review Procedures: https://deg.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office fnaml2.safelinks.protection.outlook.coml ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): https://deq.nc.gov/about/divisions/waste-management/laserfiche [naml2.safelinks.protection.outlook.com] Document Submittal & UST File Names for Laserfiche Policies: https://files.ne.eov/nedecl/W aste%20Management/D WM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policy.pdf Inaml2.safelinks.protection.outlook.coml https://files.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx [nam l 2. safelinks.protection. outlook. com] From: David Stoner[maiIto:dstoner@shieldengineering.com] Sent: Friday, June 12, 2020 1:33 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov>; Basinger, Corey <corey.basinger@ncdenr.gov> Cc: Alan Goodman <alan.goodman@preferredconstructionsupply.com>; Bob Griffin<bgriffin@shieldengineering.com> Subject: [External] Concrescere One Initial Abatement Report ��n rnal email. Do not click links or open attachments unless you verify. Send all suspl C. ov Good afternoon Trudy and Corey, Attached please find the Initial Abatement Report for the spill incident at Wayne Brothers Concrescere One facility. Wayne Brothers conducted the initial cleanup of the spilled oil. Shield Engineering, Inc. went to the site to assess and document the cleanup. Shield conducted sampling and analyses as specified by the NCDEQ. All of Shield's post -cleanup sample results were below the most stringent NCDEQ Maximum Soil Contaminant Concentrations (MSCCs) and NC Surface Water Standards. Based on the cleanup work and sample results Shield requests a "No Further Action" determination from the NCDEQ for this incident. A hard copy of the report is being sent to Trudy by regular mail. Thank you, David David A. Stoner, P.G., P.E. Sr. Principal/Vice President Shield Engineering, Inc.'s Risk Management Group 4301Taggart Creek Rd. Charlotte, NC 28208 ph. (704) 394-6913 fax (704) 394-6968 e-mail DStonerg_ShieldEn.ing eerin. com Shield Engineering's Action Environmental Group is now Shield Engineering's Risk Management Group with additional expertise and service lines! * 0 www.ShieldEngineering.com [shieldene ineerine .c9 om7 fnam 72.safelinks.protection.outlook. coml This message is intended only for the use of the addressee and may contain information that is PRIVILEGED and CONFIDENTIAL, and/or may contain ATTORNEY WORK PRODUCT. If you are not the intended recipient, you are hereby notified that any dissemination of this communication is strictly prohibited. If you have received this communication in error, please erase all copies of the message and its attachments and notify us immediately. Thank you.