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0601_Avery_MSWLF_May20GW_FID1418060_20200702
DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A DENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 213 surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Smith Gardner, Inc. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Joan A. E-mail: Joan@smithgardnerinc.com Phone: 919-828-0577 x 221 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Avery County Closed MSW Landfill Brushy Creek Road, Spruce Pine, NC 06-01 .0500 May 22, 2020 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells ❑ Leachate monitoring data El water monitoring data Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Joan A. Smyth, PG Senior Hydrogeologist 919-828-0577 x 221 od&�sR,gaesentative Name (Print) Title (Area Code) Telephone Number ^b Q. SM6 7/2/2020 J�90#4911n711 F488... Date 14 N. Boylan Ave, Raleigh, NC 27603 Facility Representative Address F-1370 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Affix NC Licensed/ Professional Geologist Seal C IJ a SEAL 712T o 1369 A. DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A This page intentionally left blank. DocuSic May 2020 Semi -Annual Groundwater Monitoring Report Avery County Closed MSW Landfill Spruce Pine, North Carolina NC Solid Waste Permit No. 06-01 Prepared for: Avery County Solid Waste 175 Linville Street Newland, North Carolina 28657 Prepared by: NCLIC.11O.E-1370 (ENGINEERING) SMITH+GARONER 14 N. Boylan Avenue, Raleigh NC 27603 1 919.B28.0577 June 2020 PRINTED ON M. RECYCLEC PAPER O 2020 Smith Gardner, Inc. This document is intended for the sole use of the client for which it was prepared and for the purpose agreed on by the client and Smith Gardner, Inc. DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A This page intentionally left blank. DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A May 2020 Semi -Annual Groundwater Monitoring Report Avery County Closed MSW Landfill NC Solid Waste Permit No. 06-01 Prepared For: Avery County Solid Waste Newland, North Carolina S+G Project No. Avery 19-2 E DocuSigned by: � can �. iZ1el�ct�5 3B8305C978EME6... Seth C. Rickerts Staff Geologist DocuSigned by: B9779EBA711F488... Joan A. Smyth, P.G. Senior Hydrogeologist June2020 CARON SEA 7/2 20 0 '�OGi A. V_.� V 6 NCLIC.NO.F-MO (ENGINEERING) SMITH GARDNER 14 N. Boylan Avenue, Raleigh NC 27603 1 919.828.0577 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A This page intentionally left blank. DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A Avery County Closed MSW Landfill NC Solid Waste Permit No. 06-01 May 2020 Semi -Annual Groundwater Monitoring Report Table of Contents Paqe 1.0 INTRODUCTION...............................................................................................................1 2.0 SITE GEOLOGY.................................................................................................................1 3.0 SAMPLING PROCEDURES...............................................................................................1 4.0 FIELD AND LABORATORY DATA......................................................................................2 4.1 Field Measurements............................................................................................... 2 4.2 Laboratory Analysis................................................................................................ 2 4.3 Laboratory Results................................................................................................. 2 5.0 GROUNDWATER CHARACTERIZATION............................................................................2 6.0 CONCLUSIONS................................................................................................................3 FIGURES Figure 1 Potentiometric Surface Map TABLES Table 1 Groundwater Elevation Data Table 2 Field Parameters Table 3 Detected Inorganic Constituents Table 4 Detected Organic Constituents APPENDICES Appendix A Laboratory Analytical Report Avery County Closed MSW Landfill May 2020 Semi -Annual Report June 202O Table of Contents Page i DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A This page intentionally left blank. DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A 1.0 INTRODUCTION Avery County is required to submit semi-annual groundwater monitoring reports for the Closed unlined MSW landfill (permit # 06-011 in accordance with Solid Waste Section Rule 15A NCAC 13B. This report, prepared by Smith Gardner, Inc (S+G), presents the semi-annual sampling for the event conducted on May 22, 2020. The groundwater monitoring network for the closed unlined MSW landfill includes three groundwater monitoring wells and two surface water monitoring locations. This report includes field procedure summaries, laboratory analyses and groundwater characterization for the closed MSW facility. 2.0 SITE GEOLOGY The Avery County Closed MSW Landfill is located in the North Carolina Blue Ridge province, along the eastern limb of the Blue Ridge anticlinorium. Published geologic mapping' places the site approximately twelve miles west of the Brevard Zone (measured perpendicular to strike), which is the boundary of the Blue Ridge Belt and the Piedmont. The principal geologic units mapped in the immediate vicinity of the site include a mix of metamorphosed sedimentary and igneous rocks - termed paragneiss and orthogneiss, respectively - interlayered with contemporaneous schist, phyllite, and marble, later injected with various granitic intrusions, including plutons, pegmatites, and hydrothermal veins. Regional metamorphic grades in the region include kyanite-grade (high grade) and retrograde chlorite-biotite metamorphism (low grade). 3.0 SAMPLING PROCEDURES S+G personnel performed this sampling event that involved collecting samples from three groundwater wells (MW-1, MW-2 and MW-3R) and two surface water locations (SW-1 and SW- 2). MW-3R is the replacement well for the previously damaged MW-3. Sampling methods followed the protocol outlined in the North Carolina Water Quality Monitoring Guidance Document for Solid Waste Facilities2. The depth to water in each well was gauged prior to purging and sampling. Samples were collected using new factory sealed Teflon bailers and placed in laboratory prepared containers for the specified analytical procedures. Groundwater samples were properly preserved, placed on ice, and transported to the laboratory facility within the specified hold times for each analysis. A map showing sampling locations is presented as Figure 1. Water table elevations and available construction details are presented in Table 1. 1 North Carolina Geologic Survey at http://www.geologV.enr.state.nc.us 2 Solid Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling, NCDENR, DWM, SWS, Rev 4-08. Avery County Closed MSW Landfill May 2020 Semi -Annual Report June 202O Pagel DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A 4.0 FIELD AND LABORATORY DATA 4.1 Field Measurements Following purging, field parameters for temperature, pH, turbidity and specific conductance were measured and recorded at each sampling location. These results are summarized in Table 2. In general these measurements were consistent with data from previous events. 4.2 Laboratory Analysis Ground and surface water samples were transported to Prism Laboratories, Inc. (Charlotte, NCI) where they were analyzed for Appendix I metals and volatile organic compounds (VOC) via the SWS approved EPA Test Method presented in the laboratory report. The additional compound, 1,4 Dioxane was analyzed via EPA Method 8260 SIM. Samples were transported under proper chain of custody. The laboratory report is included in Appendix A. 4.3 Laboratory Results Cobalt and Cadmium were the only inorganic constituents detected at concentrations above the associated standard in sample collected from MW-1. Cobalt and Vanadium were present in MW-3R sample in concentrations exceeding the associated standard. Turbidity for both of these samples was 78.8 and 34.7 NTUs, respectively. Organic constituents were not present in concentrations exceeding the associated standards. No inorganic or organic constituents were detected in surface water samples above their 2B Standard for Class C Waters in samples collected this event. Analytical results are presented in Tables 3 and 4. 5.0 GROUNDWATER CHARACTERIZATION A potentiometric surface map was prepared from groundwater data collected this sampling event. The general groundwater flow is toward the southeast across the site toward Brushy Creek. Hydraulic conductivity data was not available for these wells so groundwater velocities could not be calculated. The potentiometric surface map is included as Figure 1. 3449 Springbrook Road, Charlotte, NC 28224, NC DENR No.402. Avery County Closed MSW Landfill May 2020 Semi -Annual Report June 202O Page 2 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A 6.0 CONCLUSIONS Laboratory results indicate the water quality at the Avery County Closed unlined MSW Landfill is generally consistent with historically reported results. Cobalt, Vanadium and Cadmium are all naturally occurring in North Carolina soils and the exceedances can be attributed to suspended solids in the groundwater samples. S+G will continue to monitor theses parameters. The next groundwater monitoring event is scheduled for November 2020. A report summarizing that event will be submitted to NCDEQ with laboratory analyses. 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EXISTING SURFACE WATER MONITORING o o Q -___-%�-- - LOCATION SW UNIMIN C I \ \ - - -` ---� - '/ / ' "/���' /// 2970-- MOE• POTENTIOMETRIC CONTOUR a \ 'iy I 1 '------' /' '° 'i' /'� ' i /' /' �'�' �' (DASHED WHERE INFERRED) cam\ � 1 b GROUNDWATER FLOW DIRECTION zo m MW-2 TOC=26661 .8MW-1 MONITORING WELL DESIGNATION J IN i,, ,/ TOP OF CASING00� i\ / /v///= aDTW=9.11 TOC= wo �c DEPTH TO WATER I GWE=2657.70 DTW= l I I II \ �^� \ ` � - � /� //, '//ii /, / / / / l \ \ 1 1 � � /�/ � '/ /%i /• GWE= GROUNDWATER ELEVATION / I if Illf lI ' /' /' -- - - -----'i,' � , /,' / / / �j'/i IN o \ i o, //, IN 1 , 1 1 / I //, r /„ ///i /�. NOTES IN1 I l ' l l l l I l l / //'/ ` 1. DEPTH TO WATER MEASUREMENTS COLLECTED BY SMITH GARDNER IN I INC. PERSONNEL ON MAY 22, 2020. Q IN1 1 I 1 / / l l l I I // / l//l 1 /// /' LA_ \ I 1 1 1 l 1 / l r I I/II r1r/ 1lll Ill/ p I I 1 \ \ \ \ \ \\ I IIII 1/ll 1111 Z C� _ - - - -LLJ 1 I / / REFERENCES 1 111 \\ I IIII 11\I 11l l � > f `_--- \ \ r ' // I I 1 - ' /�\ / l / // / �-- I \ 1 1 \\\ \1 I IIII 1\ \1 I J Q --\ \ \\\ \\ l r 1 f 1 I� I, / // ///, / / / c \ / / / i I 1 \ \1\\ 1. ADJACENT PROPERTY BOUNDARIES FROM AVERY COUNTY GIS \ 1 / / J // / / \\ \ \ I / r, , , / / / \ I I\ \\\\ \\ \ \ MAPPING DEPARTMENT. CM I \ ` ` III 1 \1\\ \\\\ \\\\ \\\ u7 cn Cu c \-I \ / � /� / \ I , /-f-L1 / /, 2660 I I \ 1 \ f / / \\ \ I l �'�= 1 1 I. r / I �}I _ _ ''' / / f \ I I 1 1 /, 'be°r /' l \\ \\\\ \\\\\ \\; 2. MONITORING WELL LOCATIONS FROM FIELD SURVEY DATED 5/27/10, M c- Cu N \ \ ' / f I 1 I - / `-\ / / / / ' y� "' I 1 \ 1 \\ \\ \ \ BY SURVEYING SOLUTIONS, P.C. \ \ I I / _ \-�� I I /, // r ii' �/JI II 11\\ \\\\ 1 Q `\\------- I I l / / / '� i/ I / yr/ //-,; - \\ 3. PROPERTY LINE, EXISTING PROGRESS ENERGY POWER LINE AND z ... � \ l 1'lfl lff ' I I \� --- -\?s ii /i',' /i'�/" iii' o \ \ \ \\ 1 / 1 I s \ I l // /// r /- _4 �/ � , /, EASEMENT SHOWN FROM FIELD SURVEY DATED APRIL 9, 2010, BY -' `�- ; f Ifl If41/l ' \ \\\ \\ 1 I t , \\ `,. MW-1- - -\ \ l / //„ , r// /„/,���= %'' ,'' r� o - 11 jI /Ilf III / \\\\\\ \\\ \\ \ _ -_\ \ \ 1 \\ \\ /,/r APPALACHIAN PROFESSIONAL LAND SURVEYORS &CONSULTANTS. \ \ / I I I TOC=2672.60 4. LFG PROBES LOCATIONS FROM FIELD SURVEY DATED APRIL 9, 2010, /o DTW=7.59 ,'r ,' BY APPALACHIAN PROFESSIONAL LAND SURVEYORS &CONSULTANTS. ''`' w l l l III / / \ \ \ \\ \\ems \ \ \ / / I / r,/ j------- ,/^IIII III IIII / /�\� \ \ \ \\ \\o� �\ \ / , / / / / /// //// /% /%' /'//� / /// // // /'/ / /lll I /I Q G COUNTY 1 II 1 1 / / �'� /2700 `� \` ``" ` `�\ \ ' ' , / GWE=2665.01 \ / / /'/ /.� / r , rl //l/ //// / /, / l l fl 5. OVERALL SITE TOPOGRAPHY FROM AERIAL SURVEY BY NCDOT, DATE a l�O�t'Y/ / \-/ I1j1 Ifl ll\ \ / / \ \ \` \`\` `\` \\ / r / / \ /' '' /iii %% / /l l I11 //T/ /'/ / l 111 fill 1 \ \ / / / \ \ \\ \` ``\ ` \\ \ \ 1 1 1 I \`''°'i l l I I I I l 11 /'/ l l 1 OF PHOTOGRAPHY MARCH 2O05. ? AIRPORT 11\\\`;�``�;. ,// r ,,r 1 \ >`,\\\ ,`;�\\;\`;\ \\ ; / / 1I1 \ Q 11`\ 1, `\���� \\ 0 150' 300' © 2020 Smi Gardner, Inc.\ IN / I I \ I I I I1(I I 1 / , // //// DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A This Page Intentionally Left Blank DocuSic TABLES May 2020 — Semi -Annual Groundwater Report Avery County Closed MSW landfill NC Solid Waste Permit No. 06-01 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A This page intentionally left blank. DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A SMITH GARDNER .• - E • • .::- • � - to • / HIS ByaF D#eC/5I= Ground Well Well Total Well TOC Depth to Groundwater Screen Surface Screen Well Installation Latitude Longitude Diameter Depth (ft. Elevation Water (ft. Elevation (ft. Interval Elevation Geology Date ( Inches b s g) ft. amsl s b g amsl (ft. b g s (ft. amsl)( MW-1 NA 35.94624 81.99304 2 23.35 2672.60 2672.60 7.59 2665.01 10' - 20' NA MW-2 NA 35.94720 81.99173 2 19.24 2666.81 2666.81 9.11 2657.70 4' - 14' NA MW-3R NA 35.94840 81.99174 2 18.56 2696.62 2696.62 5.73 2691.72 4' - 14' NA NOTE: No boring logs or well records are available Depth to Water and Well Depth measured from the Top of Casing May 22, 2019. Screen Interval is assumed based on field measurements. K Rqects\3axdAdErKtntcnr#2Gax altitoirgRpots\Aeycar4kAeyKEN:�put\26.My=W21l3AteyK9UdJes ID: 6C72F6A6-2 E8D-4DOA-9502-51 A18FOFEA6A DocuSign Envelope S M ITH GARDNER Well Temperature (*Celsius) Turbidity (NTU) Specific Conductivity (MS/cm) pH MW-1 12.7 78.80 162.3 5.49 MW-2 12.5 3.42 33.5 5.92 MW-3R 15 34.7 1.2 5.58 SW-1 14.2 89.6 121.6 5.58 SW-2 13.1 11.6 35.3 5.37 NOTE: Data collected by S+G personnel. Bold indicates turbidity readings >10 NTUs W.3j Me US 2al MRgeds\Chi.nA&da-Nhitair#20ax altitoirgF�pt Aeycat)�AeyKEARpot\26.K4y2DMW2M3AteyfEUdJes DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A SMITHAARDNER Tade3 @#ededCT-dltL,E tS A/ry&rtyNBJLa-dll M:V2Z 2M Bf.3U [ate 6' 51 M Well ID Parameter Standard Limit Result Inorganic Constituents MW-1 Barium NC21- 700 130 Beryllium NCGWP 4 0.095 J Cadmium NC21- 2 14 Cobalt NCGWP 1 8.9 Copper NC21- 1000 4.1 Lead N C2L 15 1.8 Nickel NC21- 100 3.4 J Thallium NCGWP 0.2 0.17 J Zinc N C2L 1000 110 MW-2 Barium NC21- 700 26 Cadmium NC21- 2 0.14 J Chromium NC21- 10 2.1 Cobalt NCGWP 1 0.27 J Copper NC21- 1000 48 Lead NC21- 15 0.75 Nickel NC21- 100 0.8 J Thallium NCGWP 0.2 0.033 J Zinc NC21- 1000 5.8 J MW-3 Arsenic NC21- 10 1.6 Barium NC21- 700 130 Beryllium NCGWP 4 0.66 Chromium NC21- 10 8.2 Cobalt NCGWP 1 11 Copper NC21- 1000 21 Lead NC21- 15 11 Nickel NC21- 100 6.5 Thallium NCGWP 0.2 0.16 J Vanadium NCGWP 0.3 17 Zinc N C2L 1000 24 SW-1 Barium NC2B protect 21000 34 Beryllium NC2B 6.5 0.2 J Chromium NC2B NE 1.9 Cobalt NC2B protect 4 1.1 Copper NC2B 3.1 2.8 Lead NC2B 25 4.2 Nickel NC2B 88 1.9 J Thallium NC2B 0.47 0.038 J Zinc NC2B 81 9.11 SW-2 Barium NC2B protect 21000 16 Cobalt NC2B protect 4 0.63 J Copper NC2B 3.1 1.2 Lead NC2B 25 0.37 J Nickel NC2B 88 0.67 J Zinc NC2B 81 5.6 J :\a -:a [tT.Tti11[�'"{ yZfT,T:ililu a��C:u� �_.:� �� .. I - :i1�Fir7 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A SMITH GARDNER Tede3 138tectedanstltuErts W.ar ate 55= Well ID Parameter Standard Limit Result Organic Constituents M W--1 1,4-Dichlorobenzene NC21- 6 0.63 J Acetone N C2L 6000 4.5 J Benzene NC21- 1 0.25 J MW-2 Acetone NC21- 6000 6.8 J MW-3 1,4-Dichlorobenzene NC21- 6 0.31 J Acetone NC21- 6000 4.9 J SW-1 Acetone NC213 protect 2000 6J Tri Blank Dichloromethane NC21- 1 5 0.75 J NOTE: NC21- - North Carolina groundwater standards per 15A NCA 0 2L.0202 NC2L IMAC - 2L Interim Maximum Allowable Concentration NC2B - NCAC 2E Standard for Class C waters Bold - Concetration exceeding 2L or GWP Standard J - Aconcentration detected bythe laboratory above the method detection limit, but below the reoortina limit: therefore. result is estimated concentration. :ICI N:• :fT., --1. �" {�Gif►�fTR �11,u •i �� C:��� � .:► ��_�u- ---------- u `:C�1�i67i:1%1�1�i67f:1%1] 111a�1 iF� DocuSic AppendixA Laboratory Analytical Report May 2020 — Semi -Annual Groundwater Report Avery County Closed MSW Landfill NC Solid Waste Permit No. 06-01 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A This page intentionally left blank. DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A ,con-Ittstv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 June 4, 2020 Joan Smyth Smith & Gardner, Inc. 14 N. Boylan Avenue Raleigh, NC 27603 Project Location: Avery Co. MSW Client Job Number: Project Number: [none] Laboratory Work Order Number: 20E1082 Enclosed are results of analyses for samples received by the laboratory on May 26, 2020. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents Table of Contents Sample Summary 3 Case Narrative 4 Sample Results 5 20E1082-01 5 20E1082-02 9 20E1082-03 13 20E1082-04 17 20E1082-05 21 20E1082-06 25 Sample Preparation Information 27 QC Data 28 Volatile Organic Compounds by GC/MS 28 B258853 28 Volatile Organic Compounds by GUMS (SIM) 31 B258858 31 Metals Analyses (Total) 32 B258802 32 Flag/Qualifier Summary 34 Certifications 35 Chain of Custody/Sample Receipt 37 Page 2 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents ,con-Ittstv ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Smith & Gardner, Inc. 14 N. Boylan Avenue REPORT DATE: 6/4/2020 Raleigh, NC 27603 PURCHASE ORDER NUMBER: ATTN: Joan Smyth PROJECT NUMBER: [none] ANALYTICAL SUMMARY WORK ORDER NUMBER: 20E1082 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Avery Co. MSW FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB MW-3R 20E1082-01 Ground Water SW-846 6020B SW-846 8260D SW-1 20E1082-02 Ground Water SW-846 6020B SW-846 8260D MW-2 20E1082-03 Ground Water SW-846 6020B SW-846 8260D MW-1 20E1082-04 Ground Water SW-846 6020B SW-846 8260D SW-2 20E1082-05 Ground Water SW-846 6020B SW-846 8260D Trip Blank 20E1082-06 Trip Blank Water SW-846 8260D Page 3 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. Qualifications: V-05 SW-846 8260D Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound. Analyte & Samples(s) Qualified: 1,2-Dichloroethane 20E1082-01[MW-3R], 20E1082-02[SW-1], 20E1082-03[MW-2], 20E1082-04[MW-1], 20E1082-05[SW-2], 20E1082-06[Trip Blank], B258853-BLKI, B258853-BSI, B258853-BSDI, S048843-CCVI Bromomethane 20E1082-01[MW-3R], 20E1082-02[SW-1], 20E1082-03[MW-2], 20E1082-04[MW-1], 20El082-05[SW-2], 20ElO82-06[Trip Blank], B258853-BLKI, B258853-BS1, B258853-BSDI, S048843-CCVI Chloromethane 20E1082-01[MW-3R], 20E1082-02[SW-1], 20E1082-03[MW-2], 20E1082-04[MW-1], 20E1082-05[SW-2], 20E1082-06[Trip Blank], B258853-BLKI, B258853-BSI, B258853-BSDI, S048843-CCVI The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Technical Representative Page 4 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-3R Sampled: 5/22/2020 09:20 Sample ID: 20E1082-01 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 4.9 50 3.8 µg/L 1 J SW-846 8260D 5/28/20 5/28/20 12:31 EEH Acrylonitrile ND 5.0 0.52 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Benzene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Bromochloromethane ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Bromodichloromethane ND 0.50 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Bromoform ND 1.0 0.46 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Bromomethane ND 2.0 1.4 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 2-Butanone (MEK) ND 20 1.9 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Carbon Disulfide ND 5.0 4.4 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Carbon Tetrachloride ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Chlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Chlorodibromomethane ND 0.50 0.21 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Chloroethane ND 2.0 0.36 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Chloroform ND 2.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Chloromethane ND 2.0 0.45 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.53 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Dibromomethane ND 1.0 0.37 µg/L I SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,2-Dichlorobenzene ND 1.0 0.16 µg/L I SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,4-Dichlorobenzene 0.31 1.0 0.13 µg/L I J SW-846 8260D 5/28/20 5/28/20 12:31 EEH trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L I SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,2-Dichloroethane ND 1.0 0.41 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,1-Dichloroethylene ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH cis-1,2-Dichloroethylene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH trans-1,2-Dichloroethylene ND 1.0 0.31 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,2-Dichloropropane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Iodomethane ND 10 5.8 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Methylene Chloride ND 5.0 0.34 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 4-Methyl-2-pentanone (MIBK) ND 10 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Styrene ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1, 1, 1,2-Tetrachloroethane ND 1.0 0.27 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Tetrachloroethylene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Toluene ND 1.0 0.14 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1, 1, 1 -Trichloroethane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,1,2-Trichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Trichloroethylene ND 1.0 0.24 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Trichlorofluoromethane (Freon 11) ND 2.0 0.33 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH 1,2,3-Trichloropropane ND 2.0 0.25 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Page 5 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents ,con-Ittstv ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-3R Sampled: 5/22/2020 09:20 Sample ID: 20E1082-01 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Vinyl Acetate ND 20 10 µg/L 1 SW-8468260D 5/28/20 5/28/20 12:31 EEH Vinyl Chloride ND 2.0 0.45 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH m+p Xylene ND 2.0 0.30 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH o-Xylene ND 1.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Xylenes (total) 0.0 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:31 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 84.0 70-130 5/28/20 12:31 Toluene-d8 100 70-130 5/28/20 12:31 4-Bromofluorobenzene 107 70-130 5/28/20 12:31 Page 6 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents ,con-Ittstv ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-3R Sampled: 5/22/2020 09:20 Sample ID: 20E1082-01 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS (SIM) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst 1,4-Dioxane ND 2.0 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:20 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,4-Dioxane-d8 73.9 40-160 5/28/20 12:20 Page 7 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-3R Sampled: 5/22/2020 09:20 Samnle ID: 20E1082-01 Samnle Matrix: Ground Water Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Antimony ND 1.0 0.35 µg/L 1 Arsenic 1.6 0.80 0.64 µg/L 1 Barium 130 10 0.88 µg/L 1 Beryllium 0.66 0.40 0.091 µg/L 1 Cadmium ND 0.20 0.038 µg/L 1 Chromium 8.2 1.0 0.92 µg/L 1 Cobalt 11 1.0 0.14 µg/L 1 Copper 21 1.0 0.87 µg/L 1 Lead 11 0.50 0.085 µg/L 1 Nickel 6.5 5.0 0.62 µg/L 1 Selenium ND 5.0 1.6 µg/L 1 Silver ND 0.20 0.18 µg/L 1 Thallium 0.16 0.20 0.021 µg/L 1 Vanadium 17 5.0 3.0 µg/L 1 Zinc 24 10 2.3 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/29/20 13:34 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW J SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW SW-846 6020B 5/27/20 5/28/20 18:07 QNW Page 8 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: SW-1 Sampled: 5/22/2020 09:30 Sample ID: 20E1082-02 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 6.0 50 3.8 µg/L 1 J SW-846 8260D 5/28/20 5/28/20 12:59 EEH Acrylonitrile ND 5.0 0.52 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Benzene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Bromochloromethane ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Bromodichloromethane ND 0.50 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Bromoform ND 1.0 0.46 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Bromomethane ND 2.0 1.4 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 2-Butanone (MEK) ND 20 1.9 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Carbon Disulfide ND 5.0 4.4 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Carbon Tetrachloride ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Chlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Chlorodibromomethane ND 0.50 0.21 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Chloroethane ND 2.0 0.36 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Chloroform ND 2.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Chloromethane ND 2.0 0.45 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.53 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Dibromomethane ND 1.0 0.37 µg/L I SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,2-Dichlorobenzene ND 1.0 0.16 µg/L I SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,4-Dichlorobenzene ND 1.0 0.13 µg/L I SW-846 8260D 5/28/20 5/28/20 12:59 EEH trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L I SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,2-Dichloroethane ND 1.0 0.41 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,1-Dichloroethylene ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH cis-1,2-Dichloroethylene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH trans-1,2-Dichloroethylene ND 1.0 0.31 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,2-Dichloropropane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Iodomethane ND 10 5.8 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Methylene Chloride ND 5.0 0.34 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 4-Methyl-2-pentanone (MIBK) ND 10 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Styrene ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1, 1, 1,2-Tetrachloroethane ND 1.0 0.27 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Tetrachloroethylene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Toluene ND 1.0 0.14 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1, 1, 1 -Trichloroethane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,1,2-Trichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Trichloroethylene ND 1.0 0.24 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Trichlorofluoromethane (Freon 11) ND 2.0 0.33 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH 1,2,3-Trichloropropane ND 2.0 0.25 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Page 9 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents ,con-Ittstv ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: SW-1 Sampled: 5/22/2020 09:30 Sample ID: 20E1082-02 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Vinyl Acetate ND 20 10 µg/L 1 SW-8468260D 5/28/20 5/28/20 12:59 EEH Vinyl Chloride ND 2.0 0.45 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH m+p Xylene ND 2.0 0.30 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH o-Xylene ND 1.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Xylenes (total) 0.0 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:59 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 82.9 70-130 5/28/20 12:59 Toluene-d8 99.5 70-130 5/28/20 12:59 4-Bromofluorobenzene 103 70-130 5/28/20 12:59 Page 10 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents ,con-Ittstv ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: SW-1 Sampled: 5/22/2020 09:30 Sample ID: 20E1082-02 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS (SIM) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst 1,4-Dioxane ND 2.0 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 12:47 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,4-Dioxane-d8 71.9 40-160 5/28/20 12:47 Page 11 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents Project Location: Avery Co. MSW Date Received: 5/26/2020 Field Sample #: SW-1 Samnle ID: 20E1082-02 Samnle Matrix: Ground Water 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Sample Description: Sampled: 5/22/2020 09:30 Work Order: 20E1082 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Antimony ND 1.0 0.35 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Arsenic ND 0.80 0.64 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Barium 34 10 0.88 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Beryllium 0.20 0.40 0.091 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:10 QNW Cadmium ND 0.20 0.038 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Chromium 1.9 1.0 0.92 µg/L 1 SW-846 6020B 5/27/20 5/29/20 13:37 QNW Cobalt 1.1 1.0 0.14 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Copper 2.8 1.0 0.87 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Lead 4.2 0.50 0.085 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Nickel 1.9 5.0 0.62 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:10 QNW Selenium ND 5.0 1.6 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Silver ND 0.20 0.18 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Thallium 0.038 0.20 0.021 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:10 QNW Vanadium ND 5.0 3.0 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:10 QNW Zinc 9.1 10 2.3 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:10 QNW Page 12 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-2 Sampled: 5/22/2020 10:00 Sample ID: 20E1082-03 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 6.8 50 3.8 µg/L 1 J SW-846 8260D 5/28/20 5/28/20 13:26 EEH Acrylonitrile ND 5.0 0.52 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Benzene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Bromochloromethane ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Bromodichloromethane ND 0.50 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Bromoform ND 1.0 0.46 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Bromomethane ND 2.0 1.4 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 2-Butanone (MEK) ND 20 1.9 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Carbon Disulfide ND 5.0 4.4 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Carbon Tetrachloride ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Chlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Chlorodibromomethane ND 0.50 0.21 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Chloroethane ND 2.0 0.36 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Chloroform ND 2.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Chloromethane ND 2.0 0.45 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.53 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Dibromomethane ND 1.0 0.37 µg/L I SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,2-Dichlorobenzene ND 1.0 0.16 µg/L I SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,4-Dichlorobenzene ND 1.0 0.13 µg/L I SW-846 8260D 5/28/20 5/28/20 13:26 EEH trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L I SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,2-Dichloroethane ND 1.0 0.41 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,1-Dichloroethylene ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH cis-1,2-Dichloroethylene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH trans-1,2-Dichloroethylene ND 1.0 0.31 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,2-Dichloropropane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Iodomethane ND 10 5.8 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Methylene Chloride ND 5.0 0.34 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 4-Methyl-2-pentanone (MIBK) ND 10 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Styrene ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1, 1, 1,2-Tetrachloroethane ND 1.0 0.27 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Tetrachloroethylene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Toluene ND 1.0 0.14 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1, 1, 1 -Trichloroethane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,1,2-Trichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Trichloroethylene ND 1.0 0.24 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Trichlorofluoromethane (Freon 11) ND 2.0 0.33 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH 1,2,3-Trichloropropane ND 2.0 0.25 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Page 13 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents 4 ors—Ittsty ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-2 Sampled: 5/22/2020 10:00 Sample ID: 20E1082-03 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Vinyl Acetate ND 20 10 µg/L 1 SW-8468260D 5/28/20 5/28/20 13:26 EEH Vinyl Chloride ND 2.0 0.45 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH m+p Xylene ND 2.0 0.30 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH o-Xylene ND 1.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Xylenes (total) 0.0 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:26 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 84.0 70-130 5/28/20 13:26 Toluene-d8 99.6 70-130 5/28/20 13:26 4-Bromofluorobenzene 105 70-130 5/28/20 13:26 Page 14 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents 4 ors—Ittsty ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-2 Sampled: 5/22/2020 10:00 Sample ID: 20E1082-03 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS (SIM) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst 1,4-Dioxane ND 2.0 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:13 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,4-Dioxane-d8 88.1 40-160 5/28/20 13:13 Page 15 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents Project Location: Avery Co. MSW Date Received: 5/26/2020 Field Sample #: MW-2 Samnle ID: 20E1082-03 Samnle Matrix: Ground Water 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Sample Description: Sampled: 5/22/2020 10:00 Work Order: 20E1082 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Antimony ND 1.0 0.35 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Arsenic ND 0.80 0.64 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Barium 26 10 0.88 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Beryllium ND 0.40 0.091 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Cadmium 0.14 0.20 0.038 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:13 QNW Chromium 2.1 1.0 0.92 µg/L 1 SW-846 6020B 5/27/20 5/29/20 13:40 QNW Cobalt 0.27 1.0 0.14 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:13 QNW Copper 48 1.0 0.87 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Lead 0.75 0.50 0.085 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Nickel 0.80 5.0 0.62 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:13 QNW Selenium ND 5.0 1.6 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Silver ND 0.20 0.18 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Thallium 0.033 0.20 0.021 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:13 QNW Vanadium ND 5.0 3.0 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:13 QNW Zinc 5.8 10 2.3 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 18:13 QNW Page 16 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-1 Sampled: 5/22/2020 10:30 Sample ID: 20E1082-04 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 4.5 50 3.8 µg/L 1 J SW-846 8260D 5/28/20 5/28/20 13:54 EEH Acrylonitrile ND 5.0 0.52 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Benzene 0.25 1.0 0.18 µg/L 1 J SW-846 8260D 5/28/20 5/28/20 13:54 EEH Bromochloromethane ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Bromodichloromethane ND 0.50 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Bromoform ND 1.0 0.46 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Bromomethane ND 2.0 1.4 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 2-Butanone (MEK) ND 20 1.9 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Carbon Disulfide ND 5.0 4.4 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Carbon Tetrachloride ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Chlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Chlorodibromomethane ND 0.50 0.21 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Chloroethane ND 2.0 0.36 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Chloroform ND 2.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Chloromethane ND 2.0 0.45 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.53 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Dibromomethane ND 1.0 0.37 µg/L I SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,2-Dichlorobenzene ND 1.0 0.16 µg/L I SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,4-Dichlorobenzene 0.63 1.0 0.13 µg/L I J SW-846 8260D 5/28/20 5/28/20 13:54 EEH trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L I SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,2-Dichloroethane ND 1.0 0.41 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,1-Dichloroethylene ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH cis-1,2-Dichloroethylene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH trans-1,2-Dichloroethylene ND 1.0 0.31 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,2-Dichloropropane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Iodomethane ND 10 5.8 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Methylene Chloride ND 5.0 0.34 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 4-Methyl-2-pentanone (MIBK) ND 10 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Styrene ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1, 1, 1,2-Tetrachloroethane ND 1.0 0.27 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Tetrachloroethylene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Toluene ND 1.0 0.14 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1, 1, 1 -Trichloroethane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,1,2-Trichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Trichloroethylene ND 1.0 0.24 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Trichlorofluoromethane (Freon 11) ND 2.0 0.33 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH 1,2,3-Trichloropropane ND 2.0 0.25 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Page 17 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents 4 ors—Ittsty ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-1 Sampled: 5/22/2020 10:30 Sample ID: 20E1082-04 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Vinyl Acetate ND 20 10 µg/L 1 SW-8468260D 5/28/20 5/28/20 13:54 EEH Vinyl Chloride ND 2.0 0.45 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH m+p Xylene ND 2.0 0.30 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH o-Xylene ND 1.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Xylenes (total) 0.0 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:54 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 84.2 70-130 5/28/20 13:54 Toluene-d8 99.4 70-130 5/28/20 13:54 4-Bromofluorobenzene 107 70-130 5/28/20 13:54 Page 18 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents 4 ors—Ittsty ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-1 Sampled: 5/22/2020 10:30 Sample ID: 20E1082-04 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS (SIM) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst 1,4-Dioxane ND 2.0 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 13:40 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,4-Dioxane-d8 71.1 40-160 5/28/20 13:40 Page 19 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: MW-1 Sampled: 5/22/2020 10:30 Samnle ID: 20E1082-04 Samnle Matrix: Ground Water Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Antimony ND 1.0 0.35 µg/L 1 Arsenic ND 0.80 0.64 µg/L 1 Barium 130 10 0.88 µg/L 1 Beryllium 0.095 0.40 0.091 µg/L 1 Cadmium 14 0.20 0.038 µg/L 1 Chromium ND 1.0 0.92 µg/L 1 Cobalt 8.9 1.0 0.14 µg/L 1 Copper 4.1 1.0 0.87 µg/L 1 Lead 1.8 0.50 0.085 µg/L 1 Nickel 3.4 5.0 0.62 µg/L 1 Selenium ND 5.0 1.6 µg/L 1 Silver ND 0.20 0.18 µg/L 1 Thallium 0.17 0.20 0.021 µg/L 1 Vanadium ND 5.0 3.0 µg/L 1 Zinc 110 10 2.3 µg/L 1 SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW J SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/29/20 13:42 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW J SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW J SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW SW-846 6020B 5/27/20 5/28/20 18:17 QNW Page 20 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: SW-2 Sampled: 5/22/2020 10:40 Sample ID: 20E1082-05 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Acrylonitrile ND 5.0 0.52 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Benzene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Bromochloromethane ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Bromodichloromethane ND 0.50 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Bromoform ND 1.0 0.46 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Bromomethane ND 2.0 1.4 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 2-Butanone (MEK) ND 20 1.9 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Carbon Disulfide ND 5.0 4.4 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Carbon Tetrachloride ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Chlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Chlorodibromomethane ND 0.50 0.21 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Chloroethane ND 2.0 0.36 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Chloroform ND 2.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Chloromethane ND 2.0 0.45 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.53 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Dibromomethane ND 1.0 0.37 µg/L I SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,2-Dichlorobenzene ND 1.0 0.16 µg/L I SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,4-Dichlorobenzene ND 1.0 0.13 µg/L I SW-846 8260D 5/28/20 5/28/20 14:21 EEH trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L I SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,2-Dichloroethane ND 1.0 0.41 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,1-Dichloroethylene ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH cis-1,2-Dichloroethylene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH trans-1,2-Dichloroethylene ND 1.0 0.31 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,2-Dichloropropane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Iodomethane ND 10 5.8 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Methylene Chloride ND 5.0 0.34 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 4-Methyl-2-pentanone (MIBK) ND 10 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Styrene ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1, 1, 1,2-Tetrachloroethane ND 1.0 0.27 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Tetrachloroethylene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Toluene ND 1.0 0.14 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1, 1, 1 -Trichloroethane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,1,2-Trichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Trichloroethylene ND 1.0 0.24 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Trichlorofluoromethane (Freon 11) ND 2.0 0.33 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH 1,2,3-Trichloropropane ND 2.0 0.25 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Page 21 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents ,con-Ittstv ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: SW-2 Sampled: 5/22/2020 10:40 Sample ID: 20E1082-05 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Vinyl Acetate ND 20 10 µg/L 1 SW-8468260D 5/28/20 5/28/20 14:21 EEH Vinyl Chloride ND 2.0 0.45 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH m+p Xylene ND 2.0 0.30 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH o-Xylene ND 1.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Xylenes (total) 0.0 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:21 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 84.2 70-130 5/28/20 14:21 Toluene-d8 98.1 70-130 5/28/20 14:21 4-Bromofluorobenzene 107 70-130 5/28/20 14:21 Page 22 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents ,con-Ittstv ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: SW-2 Sampled: 5/22/2020 10:40 Sample ID: 20E1082-05 Samnle Matrix: Ground Water Volatile Organic Compounds by GC/MS (SIM) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst 1,4-Dioxane ND 2.0 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 14:07 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,4-Dioxane-d8 79.5 40-160 5/28/20 14:07 Page 23 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents Project Location: Avery Co. MSW Date Received: 5/26/2020 Field Sample #: SW-2 Samnle ID: 20E1082-05 Samnle Matrix: Ground Water 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Sample Description: Sampled: 5/22/2020 10:40 Work Order: 20E1082 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Antimony ND 1.0 0.35 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Arsenic ND 0.80 0.64 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Barium 16 10 0.88 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Beryllium ND 0.40 0.091 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Cadmium ND 0.20 0.038 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Chromium ND 1.0 0.92 µg/L 1 SW-846 6020B 5/27/20 5/29/20 13:31 QNW Cobalt 0.63 1.0 0.14 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 17:17 QNW Copper 1.2 1.0 0.87 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Lead 0.37 0.50 0.085 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 17:17 QNW Nickel 0.67 5.0 0.62 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 17:17 QNW Selenium ND 5.0 1.6 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Silver ND 0.20 0.18 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Thallium ND 0.20 0.021 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Vanadium ND 5.0 3.0 µg/L 1 SW-846 6020B 5/27/20 5/28/20 17:17 QNW Zinc 5.6 10 2.3 µg/L 1 J SW-846 6020B 5/27/20 5/28/20 17:17 QNW Page 24 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: Trip Blank Sampled: 5/22/2020 00:00 Sample ID: 20E1082-06 Samnle Matrix: Trin Blank Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Acrylonitrile ND 5.0 0.52 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Benzene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Bromochloromethane ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Bromodichloromethane ND 0.50 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Bromoform ND 1.0 0.46 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Bromomethane ND 2.0 1.4 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 2-Butanone (MEK) ND 20 1.9 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Carbon Disulfide ND 5.0 4.4 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Carbon Tetrachloride ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Chlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Chlorodibromomethane ND 0.50 0.21 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Chloroethane ND 2.0 0.36 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Chloroform ND 2.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Chloromethane ND 2.0 0.45 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.53 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Dibromomethane ND 1.0 0.37 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,2-Dichlorobenzene ND 1.0 0.16 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,4-Dichlorobenzene ND 1.0 0.13 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,2-Dichloroethane ND 1.0 0.41 µg/L 1 V-05 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,1-Dichloroethylene ND 1.0 0.32 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH cis-1,2-Dichloroethylene ND 1.0 0.13 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH trans-1,2-Dichloroethylene ND 1.0 0.31 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,2-Dichloropropane ND 1.0 0.20 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH cis-1,3-Dichloropropene ND 0.50 0.13 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Iodomethane ND 10 5.8 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Methylene Chloride 0.75 5.0 0.34 µg/L 1 J SW-846 8260D 5/28/20 5/28/20 11:36 EEH 4-Methyl-2-pentanone (M1BK) ND 10 1.7 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Styrene ND 1.0 0.11 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1, 1, 1,2-Tetrachloroethane ND 1.0 0.27 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Tetrachloroethylene ND 1.0 0.18 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Toluene ND 1.0 0.14 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1, 1, 1 -Trichloroethane ND 1.0 0.20 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,1,2-Trichloroethane ND 1.0 0.16 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH Trichloroethylene ND 1.0 0.24 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH Trichlorofluoromethane (Freon 11) ND 2.0 0.33 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH 1,2,3-Trichloropropane ND 2.0 0.25 µg/L I SW-846 8260D 5/28/20 5/28/20 11:36 EEH Page 25 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A Table of Contents 4 ors—Ittsty ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Avery Co. MSW Sample Description: Work Order: 20E1082 Date Received: 5/26/2020 Field Sample #: Trip Blank Sampled: 5/22/2020 00:00 Sample ID: 20E1082-06 Samnle Matrix: Trin Blank Water Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Vinyl Acetate ND 20 10 µg/L 1 SW-8468260D 5/28/20 5/28/20 11:36 EEH Vinyl Chloride ND 2.0 0.45 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH m+p Xylene ND 2.0 0.30 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH o-Xylene ND 1.0 0.17 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Xylenes (total) 0.0 µg/L 1 SW-846 8260D 5/28/20 5/28/20 11:36 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 85.0 70-130 5/28/20 11:36 Toluene-d8 98.0 70-130 5/28/20 11:36 4-Bromofluorobenzene 105 70-130 5/28/20 11:36 Page 26 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A ,con-Ittstv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 3005A Analytical Method: SW-846 6020B Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 20E1082-01 [MW-3R] B258802 50.0 50.0 05/27/20 20E1082-02 [SW-1] B258802 50.0 50.0 05/27/20 20E1082-03 [MW-2] B258802 50.0 50.0 05/27/20 20E1082-04 [MW-1] B258802 50.0 50.0 05/27/20 20E1082-05 [SW-2] B258802 50.0 50.0 05/27/20 Prep Method: SW-846 5030B Analytical Method: SW-846 8260D Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 20E1082-01 [MW-3R] B258853 5 5.00 05/28/20 20E1082-02 [SW-1] B258853 5 5.00 05/28/20 20E1082-03 [MW-2] B258853 5 5.00 05/28/20 20E1082-04 [MW-1] B258853 5 5.00 05/28/20 20E1082-05 [SW-2] B258853 5 5.00 05/28/20 20E1082-06 [Trip Blank] B258853 5 5.00 05/28/20 Prep Method: SW-846 5035 Analytical Method: SW-846 8260D Lab Number [Field ID] Batch Initial ImLI Final [mL] Date 20E1082-01 [MW-3R] B258858 5 5.00 05/28/20 20E1082-02 [SW-1] B258858 5 5.00 05/28/20 20E1082-03 [MW-2] B258858 5 5.00 05/28/20 20E1082-04 [MW-1] B258858 5 5.00 05/28/20 20E1082-05 [SW-2] B258858 5 5.00 05/28/20 Page 27 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B258853 - SW-846 5030B Blank (B258853-BLK1) Prepared & Analyzed: 05/28/20 Acetone ND 50 µg/L Acrylonitrile ND 5.0 µg/L Benzene ND 1.0 µg/L Bromochloromethane ND 1.0 µg/L Bromodichloromethane ND 0.50 µg/L Bromoform ND 1.0 µg/L Bromomethane ND 2.0 µg/L V-05 2-Butanone (MEK) ND 20 µg/L Carbon Disulfide ND 5.0 µg/L Carbon Tetrachloride ND 1.0 µg/L Chlorobenzene ND 1.0 µg/L Chlorodibromomethane ND 0.50 µg/L Chloroethane ND 2.0 µg/L Chloroform ND 2.0 µg/L Chloromethane ND 2.0 µg/L V-05 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 µg/L 1,2-Dibromoethane (EDB) ND 0.50 µg/L Dibromomethane ND 1.0 µg/L 1,2-Dichlorobenzene ND 1.0 µg/L 1,4-Dichlorobenzene ND 1.0 µg/L trans-1,4-Dichloro-2-butene ND 2.0 µg/L 1,1-Dichloroethane ND 1.0 µg/L 1,2-Dichloroethane ND 1.0 µg/L V-05 1,1-Dichloroethylene ND 1.0 µg/L cis-1,2-Dichloroethylene ND 1.0 µg/L trans-1,2-Dichloroethylene ND 1.0 µg/L 1,2-Dichloropropane ND 1.0 µg/L cis- 1,3 -Dichloropropene ND 0.50 µg/L trans- 1, 3 -Dichloropropene ND 0.50 µg/L Ethylbenzene ND 1.0 µg/L 2-Hexanone (MBK) ND 10 µg/L Iodomethane ND 10 µg/L Methylene Chloride ND 5.0 µg/L 4-Methyl-2-pentanone (MIBK) ND 10 µg/L Styrene ND 1.0 µg/L 1, 1, 1,2-Tetrachloroethane ND 1.0 µg/L 1,1,2,2-Tetrachloroethane ND 0.50 µg/L Tetrachloroethylene ND 1.0 µg/L Toluene ND 1.0 µg/L 1, 1, 1 -Trichloroethane ND 1.0 µg/L 1,1,2-Trichloroethane ND 1.0 µg/L Trichloroethylene ND 1.0 µg/L Trichlorofluoromethane (Freon 11) ND 2.0 µg/L 1,2,3-Trichloropropane ND 2.0 µg/L Vinyl Acetate ND 20 µg/L Vmyl Chloride ND 2.0 µg/L m+p Xylene ND 2.0 µg/L o-Xylene ND 1.0 µg/L Xylenes (total) 0.0 µg/L Surrogate:l,2-Dichloroethane-d4 20.6 µg/L 25.0 82.4 70-130 Surrogate: Toluene-d8 24.8 µg/L 25.0 99.0 70-130 Surrogate:4-Bromofluorobenzene 26.2 µg/L 25.0 105 70-130 Page 28 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B258853 - SW-846 5030B LCS (B258853-BSI) Prepared & Analyzed: 05/28/20 Acetone 110 50 µg/L 100 110 70-160 t Acrylonitrile 11.6 5.0 µg/L 10.0 116 70-130 Benzene 9.49 1.0 µg/L 10.0 94.9 70-130 Bromochloromethane 9.25 1.0 µg/L 10.0 92.5 70-130 Bromodichloromethane 9.44 0.50 µg/L 10.0 94.4 70-130 Bromoform 11.1 1.0 µg/L 10.0 ill 70-130 Bromomethane 7.39 2.0 µg/L 10.0 73.9 40-160 V-05 t 2-Butanone(MEK) 123 20 µg/L 100 123 40-160 t Carbon Disulfide 107 5.0 µg/L 100 107 70-130 Carbon Tetrachloride 9.62 1.0 µg/L 10.0 96.2 70-130 Chlorobenzene 9.98 1.0 µg/L 10.0 99.8 70-130 Chlorodibromomethane 10.0 0.50 µg/L 10.0 100 70-130 Chloroethane 10.1 2.0 µg/L 10.0 101 70-130 Chloroform 8.96 2.0 µg/L 10.0 89.6 70-130 Chloromethane 8.21 2.0 µg/L 10.0 82.1 40-160 V-05 t 1,2-Dibromo-3-chloropropane (DBCP) 9.47 5.0 µg/L 10.0 95.7 70-130 1,2-Dibromoethane (EDB) 10.2 0.50 µg/L 10.0 102 70-130 Dibromomethane 10.0 1.0 µg/L 10.0 100 70-130 1,2-Dichlorobenzene 9.09 1.0 µg/L 10.0 90.9 70-130 1,4-Dichlorobenzene 8.83 1.0 µg/L 10.0 88.3 70-130 trans-1,4-Dichloro-2-butene 10.3 2.0 µg/L 10.0 103 70-130 1,1-Dichloroethane 9.29 1.0 µg/L 10.0 92.9 70-130 1,2-Dichloroethane 7.94 1.0 µg/L 10.0 79.4 70-130 V-05 1,1-Dichloroethylene 9.51 1.0 µg/L 10.0 95.1 70-130 cis-1,2-Dichloroethylene 9.21 1.0 µg/L 10.0 92.1 70-130 trans-1,2-Dichloroethylene 8.96 1.0 µg/L 10.0 85.6 70-130 1,2-Dichloropropane 9.35 1.0 µg/L 10.0 93.5 70-130 cis- 1,3 -Dichloropropene 9.46 0.50 µg/L 10.0 94.6 70-130 trans- 1, 3 -Dichloropropene 9.98 0.50 µg/L 10.0 95.8 70-130 Ethylbenzene 9.68 1.0 µg/L 10.0 96.8 70-130 2-Hexanone (MBK) 122 10 µg/L 100 122 70-160 f Iodomethane 104 10 µg/L 100 104 70-130 Methylene Chloride 9.78 5.0 µg/L 10.0 97.8 70-130 4-Methyl-2-pentanone (MIBK) 116 10 µg/L 100 116 70-160 f Styrene 9.79 1.0 µg/L 10.0 97.9 70-130 1, 1, 1,2-Tetrachloroethane 10.1 1.0 µg/L 10.0 101 70-130 1,1,2,2-Tetrachloroethane 10.6 0.50 µg/L 10.0 106 70-130 Tetrachloroethylene 10.3 1.0 µg/L 10.0 103 70-130 Toluene 9.53 1.0 µg/L 10.0 95.3 70-130 1, 1, 1 -Trichloroethane 9.63 1.0 µg/L 10.0 96.3 70-130 1,1,2-Trichloroethane 10.1 1.0 µg/L 10.0 101 70-130 Trichloroethylene 9.90 1.0 µg/L 10.0 99.0 70-130 Trichlorofluoromethane (Freon 11) 9.33 2.0 µg/L 10.0 93.3 70-130 1,2,3-Trichloropropane 10.6 2.0 µg/L 10.0 106 70-130 Vinyl Acetate 104 20 µg/L 100 104 70-130 Vmyl Chloride 10.3 2.0 µg/L 10.0 103 40-160 m+p Xylene 19.4 2.0 µg/L 20.0 97.2 70-130 o-Xylene 9.81 1.0 µg/L 10.0 98.1 70-130 Surrogate:l,2-Dichloroethane-d4 20.4 µg/L 25.0 81.5 70-130 Surrogate: Toluene-d8 24.6 µg/L 25.0 98.2 70-130 Surrogate:4-Bromofluorobenzene 26.7 µg/L 25.0 107 70-130 Page 29 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B258853 - SW-846 5030B LCS Dup (B258853-BSD1) Prepared & Analyzed: 05/28/20 Acetone 114 50 µg/L 100 114 70-160 2.93 25 f Acrylonitrile 11.3 5.0 µg/L 10.0 113 70-130 2.35 25 Benzene 9.20 1.0 µg/L 10.0 92.0 70-130 3.10 25 Bromochloromethane 8.89 1.0 µg/L 10.0 88.9 70-130 3.97 25 Bromodichloromethane 9.44 0.50 µg/L 10.0 94.4 70-130 0.00 25 Bromoform 10.9 1.0 µg/L 10.0 109 70-130 1.27 25 Bromomethane 8.07 2.0 µg/L 10.0 80.7 40-160 8.80 25 V-05 f 2-Butanone(MEK) 129 20 µg/L 100 129 40-160 4.85 25 t Carbon Disulfide 107 5.0 µg/L 100 107 70-130 0.599 25 Carbon Tetrachloride 9.42 1.0 µg/L 10.0 95.2 70-130 1.04 25 Chlorobenzene 9.80 1.0 µg/L 10.0 98.0 70-130 1.82 25 Chlorodibromomethane 10.0 0.50 µg/L 10.0 100 70-130 0.0997 25 Chloroethane 10.3 2.0 µg/L 10.0 103 70-130 2.65 25 Chloroform 8.90 2.0 µg/L 10.0 89.0 70-130 0.672 25 Chloromethane 8.47 2.0 µg/L 10.0 84.7 40-160 3.12 25 V-05 t 1,2-Dibromo-3-chloropropane (DBCP) 9.96 5.0 µg/L 10.0 99.6 70-130 3.99 25 1,2-Dibromoethane (EDB) 10.3 0.50 µg/L 10.0 103 70-130 0.878 25 Dibromomethane 10.0 1.0 µg/L 10.0 100 70-130 0.0996 25 1,2-Dichlorobenzene 8.91 1.0 µg/L 10.0 89.1 70-130 2.00 25 1,4-Dichlorobenzene 8.85 1.0 µg/L 10.0 88.5 70-130 0.226 25 trans-1,4-Dichloro-2-butene 10.1 2.0 µg/L 10.0 101 70-130 1.86 25 1,1-Dichloroethane 9.47 1.0 µg/L 10.0 94.7 70-130 1.92 25 1,2-Dichloroethane 7.92 1.0 µg/L 10.0 79.2 70-130 0.252 25 V-05 1,1-Dichloroethylene 9.63 1.0 µg/L 10.0 96.3 70-130 1.25 25 cis-1,2-Dichloroethylene 8.96 1.0 µg/L 10.0 89.6 70-130 2.75 25 trans-1,2-Dichloroethylene 8.60 1.0 µg/L 10.0 86.0 70-130 0.466 25 1,2-Dichloropropane 9.39 1.0 µg/L 10.0 93.9 70-130 0.427 25 cis- 1,3 -Dichloropropene 9.61 0.50 µg/L 10.0 96.1 70-130 1.57 25 trans- 1, 3 -Dichloropropene 9.39 0.50 µg/L 10.0 93.9 70-130 2.00 25 Ethylbenzene 9.67 1.0 µg/L 10.0 96.7 70-130 0.103 25 2-Hexanone (MBK) 123 10 µg/L 100 123 70-160 1.18 25 f Iodomethane 104 10 µg/L 100 104 70-130 0.0384 25 Methylene Chloride 9.56 5.0 µg/L 10.0 95.6 70-130 2.28 25 4-Methyl-2-pentanone (MIBK) 120 10 µg/L 100 120 70-160 3.53 25 f Styrene 9.66 1.0 µg/L 10.0 96.6 70-130 1.34 25 1, 1, 1,2-Tetrachloroethane 9.92 1.0 µg/L 10.0 99.2 70-130 1.90 25 1,1,2,2-Tetrachloroethane 10.4 0.50 µg/L 10.0 104 70-130 1.72 25 Tetrachloroethylene 10.2 1.0 µg/L 10.0 102 70-130 0.292 25 Toluene 9.62 1.0 µg/L 10.0 96.2 70-130 0.940 25 1, 1, 1 -Trichloroethane 9.53 1.0 µg/L 10.0 95.3 70-130 1.04 25 1,1,2-Trichloroethane 9.87 1.0 µg/L 10.0 98.7 70-130 2.01 25 Trichloroethylene 9.65 1.0 µg/L 10.0 96.5 70-130 2.56 25 Trichlorofluoromethane (Freon 11) 9.21 2.0 µg/L 10.0 92.1 70-130 1.29 25 1,2,3-Trichloropropane 10.8 2.0 µg/L 10.0 108 70-130 1.78 25 Vinyl Acetate 106 20 µg/L 100 106 70-130 2.09 25 Vmyl Chloride 10.5 2.0 µg/L 10.0 105 40-160 1.73 25 m+p Xylene 19.4 2.0 µg/L 20.0 96.8 70-130 0.464 25 o-Xylene 9.63 1.0 µg/L 10.0 96.3 70-130 1.85 25 Surrogate:l,2-Dichloroethane-d4 20.6 µg/L 25.0 82.4 70-130 Surrogate: Toluene-d8 24.9 µg/L 25.0 99.7 70-130 Surrogate:4-Bromofluorobenzene 26.6 µg/L 25.0 107 70-130 Page 30 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS (SIM) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B258858 - SW-846 5035 Blank (B258858-BLK1) Prepared & Analyzed: 05/28/20 1,4-Dioxane ND 2.0 µg/L Surrogate: 1,4-Dioxane-d8 LCS (B258858-BS1) 7.27 µg/L 10.0 72.7 Prepared & Analyzed: 05/28/20 40-160 1,4-Dioxane 7.80 2.0 µg/L 10.0 78.0 60-140 Surrogate:l,4-Dioxane-d8 LCS Dup (B258858-BSD1) 8.09 µg/L 10.0 80.9 Prepared & Analyzed: 05/28/20 40-160 1,4-Dioxane 7.12 2.0 µg/L 10.0 71.2 60-140 9.12 20 Surrogate:l,4-Dioxane-d8 7.69 µg/L 10.0 76.9 40-160 Page 31 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B258802 - SW-846 3005A Blank (B258802-BLK1) Prepared: 05/27/20 Analyzed: 05/28/20 Antimony ND 1.0 µg/L Arsenic ND 0.80 µg/L Barium ND 10 µg/L Beryllium ND 0.40 µg/L Cadmium ND 0.20 µg/L Chromium ND 1.0 µg/L Cobalt ND 1.0 µg/L Copper ND 1.0 µg/L Lead ND 0.50 µg/L Nickel ND 5.0 µg/L Selenium ND 5.0 µg/L Silver ND 0.20 µg/L Thallium ND 0.20 µg/L Vanadium ND 5.0 µg/L Zinc ND 10 µg/L LCS (B258802-BS1) Prepared: 05/27/20 Analyzed: 05/28/20 Antimony 490 10 µg/L 500 98.0 80-120 Arsenic 512 8.0 µg/L 500 102 80-120 Barium 472 100 µg/L 500 94.3 80-120 Beryllium 504 4.0 µg/L 500 101 80-120 Cadmium 496 2.0 µg/L 500 99.2 80-120 Chromium 513 10 µg/L 500 103 80-120 Cobalt 511 10 µg/L 500 102 80-120 Copper 991 10 µg/L 1000 99.1 80-120 Lead 516 5.0 µg/L 500 103 80-120 Nickel 501 50 µg/L 500 100 80-120 Selenium 300 50 µg/L 500 100 80-120 Silver 493 2.0 µg/L 500 98.7 80-120 Thallium 484 2.0 µg/L 500 96.8 80-120 Vanadium 483 50 µg/L 500 96.5 80-120 Zinc 1020 100 µg/L 1000 102 80-120 LCS Dup (B258802-BSD1) Prepared: 05/27/20 Analyzed: 05/28/20 Antimony 479 10 µg/L 500 95.8 80-120 2.20 20 Arsenic 503 8.0 µg/L 500 101 80-120 1.79 20 Barium 462 100 µg/L 500 92.4 80-120 2.06 20 Beryllium 498 4.0 µg/L 500 99.5 80-120 1.20 20 Cadmium 484 2.0 µg/L 500 96.9 80-120 2.37 20 Chromium 492 10 µg/L 500 98.5 80-120 4.11 20 Cobalt 501 10 µg/L 500 100 80-120 1.84 20 Copper 964 10 µg/L 1000 96.4 80-120 2.80 20 Lead 499 5.0 µg/L 500 99.7 80-120 3.42 20 Nickel 490 50 µg/L 500 98.0 80-120 2.28 20 Selenium 493 50 µg/L 500 98.6 80-120 1.46 20 Silver 484 2.0 µg/L 500 96.8 80-120 1.93 20 Thallium 476 2.0 µg/L 500 95.1 80-120 1.77 20 Vanadium 470 50 µg/L 500 94.0 80-120 2.63 20 Zinc 979 100 µg/L 1000 97.9 80-120 4.09 20 Page 32 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B258802 - SW-846 3005A Duplicate (B258802-DUPl) Source: 20E1082-05 Prepared: 05/27/20 Analyzed: 05/28/20 Antimony ND 1.0 µg/L ND NC 20 Arsenic ND 0.80 µg/L ND NC 20 Barium 15.6 10 µg/L 15.8 1.24 20 Beryllium ND 0.40 µg/L ND NC 20 Cadmium ND 0.20 µg/L ND NC 20 Chromium ND 1.0 µg/L ND NC 20 Cobalt 0.617 1.0 µg/L 0.634 2.70 20 J Copper 1.15 1.0 µg/L 1.17 2.29 20 Lead 0.360 0.50 µg/L 0.368 2.18 20 1 Nickel 0.642 5.0 µg/L 0.670 4.26 20 J Selenium ND 5.0 µg/L ND NC 20 Silver ND 0.20 µg/L ND NC 20 Thallium ND 0.20 µg/L ND NC 20 Vanadium ND 5.0 µg/L ND NC 20 Zinc 5.10 10 µg/L 5.61 9.40 20 1 Matrix Spike (B258802-MS1) Source: 20E1082-05 Prepared: 05/27/20 Analyzed: 05/28/20 Antimony 488 10 µg/L 500 ND 97.5 75-125 Arsenic 510 8•0 µg/L 500 ND 102 75-125 Barium 489 100 µg/L 500 15.8 94.6 75-125 Beryllium 907 4.0 µg/L 500 ND 101 75-125 Cadmium 495 2•0 µg/L 500 ND 99.0 75-125 Chromium 509 10 µg/L 500 ND 102 75-125 Cobalt 910 10 µg/L 500 ND 102 75-125 Copper 976 10 µg/L 1000 ND 97.6 75-125 Lead 517 5.0 µg/L 500 ND 103 75-125 Nickel 499 50 µg/L 500 ND 99.8 75-125 Selenium 301 50 µg/L 500 ND 100 75-125 Silver 454 2.0 µg/L 500 ND 90.8 75-125 Thallium 485 2.0 µg/L 500 ND 97.1 75-125 Vanadium 481 50 µg/L 500 ND 96.2 75-125 Zinc 1010 100 µg/L, 1000 ND 101 75-125 Page 33 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LOQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). V-05 Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound. Page 34 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 6020B in Water Antimony CT,NH,NY,ME,VA,NC Arsenic CT,NH,NY,ME,VA,NC Barium CT,NH,NY,ME,VA,NC Beryllium CT,NH,NY,ME,VA,NC Cadmium CT,NH,NY,RI,ME,VA,NC Chromium CT,NH,NY,ME,VA,NC Cobalt CT,NH,NY,ME,VA,NC Copper CT,NH,NY,ME,VA,NC Lead CT,NH,NY,ME,VA,NC Nickel CT,NH,NY,ME,VA,NC Selenium CT,NH,NY,ME,VA,NC Silver CT,NH,NY,ME,VA,NC Thallium CT,NH,NY,ME,VA,NC Vanadium CT,NH,NY,ME,VA,NC Zinc CT,NH,NY,ME,VA,NC SW-846 8260D in Water Acetone NC Acrylonitrile NC Benzene NC Bromochloromethane NC Bromodichloromethane NC Bromoform NC Bromomethane NC 2-Butanone (MEK) NC Carbon Disulfide NC Carbon Tetrachloride NC Chlorobenzene NC Chlorodibromomethane NC Chloroethane NC Chloroform NC Chloromethane NC 1,2-Dibromo-3-chloropropane (DBCP) NC 1,2-Dibromoethane (EDB) NC Dibromomethane NC 1,2-Dichlorobenzene NC 1,4-Dichlorobenzene NC trans-1,4-Dichloro-2-butene NC 1,1-Dichloroethane NC 1,2-Dichloroethane NC 1,1-Dichloroethylene NC cis-1,2-Dichloroethylene NC trans-1,2-Dichloroethylene NC 1,2-Dichloropropane NC cis- 1,3 -Dichloropropene NC trans- l,3-Dichloropropene NC 1,4-Dioxane NC Page 35 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A icon-ttstkv ANALYTICAL LABORATORY Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8260D in Water Ethylbenzene NC 2-Hexanone (MBK) NC Iodomethane NC Methylene Chloride NC 4-Methyl-2-pentanone (MIBK) NC Styrene NC 1, 1, 1,2-Tetrachloroethane NC 1,1,2,2-Tetrachloroethane NC Tetrachloroethylene NC Toluene NC 1, 1, 1 -Trichloroethane NC 1,1,2-Trichloroethane NC Trichloroethylene NC Trichlorofluoromethane (Freon 11) NC 1,2,3-Trichloropropane NC Vinyl Acetate NC Vinyl Chloride NC m+p Xylene NC o-Xylene NC The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2017 100033 03/1/2022 MA Massachusetts DEP M-MA100 06/30/2020 CT Connecticut Department of Publilc Health PH-0567 09/30/2021 NY New York State Department of Health 10899 NELAP 04/1/2021 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2021 RI Rhode Island Department of Health LA000112 12/30/2020 NC North Carolina Div. of Water Quality 652 12/31/2020 NJ New Jersey DEP MA007 NELAP 06/30/2020 FL Florida Department of Health E871027 NELAP 06/30/2020 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2021 ME State of Maine 2011028 06/9/2021 VA Commonwealth of Virginia 460217 12/14/2020 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2020 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2020 NC-DW North Carolina Department of Health 25703 07/31/2020 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2020 Page 36 of 39 hWj Ivvwvv....com Doc 4 379 Rev 1 03242017 ........ DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A ltvftf 11 — M-A! _V_ Phone: 413-525-2332 CMAM OF CUSTODY RECORD Mortli Carolina) 39 Spruce Street Page. of ANAkYTICAI. of ORAT—Y Fax: 413-525-6405 East Longmeadow, MA 01028 . . .. . ..... CLI C7� Email: info@contestiabs.com 7-Day ❑ 10-Day I # of Containers Due Date: 2 Preservation Code Address: Container Code Ph. ne I -Day 3-Day ANALYSIS REQUESTED 2-Day 4-Day ❑ Field Filtered Pro J, E] Lab to Filter Project Number: Format: PDF 0 EXCEL E] Project Manager-.WT" Other. . . . . . . . . . . . . ..... Con -Test Quote Name/Number: CLP Like Data Pkg Required: Field Filtered Invoice Recipient: 0t e12 SM C1A9_brJeV4 ,(OKA Email To: Mt 0 � ❑Lab to Filter Sampled By: Fax To Con -Test Work Order# Matrix CGdes- GW = Ground Water Ww = Waste water DW = Drinking Water A - = Air cf30 S = Soil -SL = Sludge 7 SOL = Solid D' 31D 0 = Other (please define) 0, 10 2 Preservation Codes: I = Iced H = HCL M = Methanol N = Nitric Acid S = Sulfuric Acid B = Sodium Bisulfate X = Sodium Hydroxide T = Sodium commen Thiosulfate Run trip blank for 8260 Standard 0 = Other (please per Joan S. Please use the following codes to indicate possible sample concentration define) within the Conc Code column above: -KKM 5/28/2020 H - High; M - Medium; L - Low; C - Clean; U - Unknown Container Codes: Re Aquished by: (Sig a 4re) Date/Time: I -1q 7 7A � Amber Glass : wn Infomution G = Glass U 2L DSCA UST/Trust Fund P = Plastic ReC (signatu ST = Sterile D t /Ti GwPc SWS Landfill E] REC V = Vial SWSL IHSB Orphaned Landfill S Summa Canister (sig—natur Date/Time: IHSB State Lead T g MSCC Other; 0 = Other (please define) led by: Ignature) Date/T(me: 7 07, R CD uished by: (signature) Date/Time: Project Entity Other PCB ONLY W 4 ❑ Government ❑ Municipality ❑ Chromatogram ❑ Soxhlet R 0, IF red by: Federal ❑E] ❑Brownfield A1HA-LAPLLC ❑ Non Soxhlet (signature) Date/Time: I C.0 ❑ El city E] School .. .......... . . . . .. .......... . ...... ... . . ........ ...... ......... ..... . DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-5lA18FOFEA6A b1ztIZUZU , it L K yuui package or shipment with FedEx Tracking Table of Contents IMPORTANT! Flooding is causing hazardous conditions in parts of Mid -Michigan. Learn More N&x Cff) 149454202172 Delivered Wednesday 5/27/2020 at 1 A 4 am Shipment Facts TRACKING NUMBER 4�,4 r41 202172 TOTAL PIECES 1 STANDARD TRANSIT 5/`l_i12020 by 10:30 a Travel History Wednesday,5/271202© 1114am 811am 7,52 any 5.19 am 4:38 wn Tuesday,5126/2020 11.56 pm 5.18 prn DELIVERED Signed for by: [.CON TES-1 GET STATUS UPDATES OBTAIN PROOF OF DELIVERY SERVICE DELIVERED To FedEx Priority Ovcrnlglll Sig= >I�ing/f eceivir�g PACKAGING SPECIAL, HANDLING SECTION Your Packaging Delivet INpekday SHIP DATE ACTUAL. DELIVERY V',�ed ' /27/2C2011 14 um TLie 5,/26i20201 WINDSOR LOCKS, CT WINDSOR LOCKS, CT EAST GRANBY, CT INDIANAPOLIS, IN I NO IANAPO L IS, iN RALEIGH, NO Delivereri On FedEx vehicle for delivery At local FedEx facility Al destination sort facility Departed FedEx location Arrived at FedEx location Picked up Local Scan Time \/' ID hUps:llwww.fedex.com/apps/fedextracklindex.htmi?action=track&tracknurnbers=149454202172&locale=en_US&cntr-y_code=en Page 38 of 39 DocuSign Envelope ID: 6C72F6A6-2E8D-4DOA-9502-51A18FOFEA6A Table of Contents do" MEMO I Have Not Confirmed Sample Container All via c C 3 0 n own - t Numbers With Lab Staff Before Relinquishing QNALY i"'ICQ1,.._ LAE30RA`i'01=iY Over Samples Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client -9_ Received By Date S 1 - zo_2n-_ Time How were the samples In Cooler _ r No Cooler On Ice ; No Ice received? Direct from Sampling Ambient Melted Ice Were samples within By Gun # Actual Temp - 2 .y Temperature? 2-6°C _ —r By Blank # Actual Temp - Was Custody Seal Intact? 13,N Were Samples Tampered with? AJA Was COC Relinquished ? T Does Chain Agree With Samples? Are there broke nlleaking/loose caps on any samples? i Is COC in ink/ Legible? ' F Were samples received within holding time? ; Did COC include all Client i Analysis ; Sampler Name i pertinent Information? Project t Are Sample labels filled out and legible? e Are there Lab to Filters? r Are there Rushes? f= Are there Short Holds? �= Is there enough Volume? T Is there Head space where applicable? t- Proper Media/Containers Used? -F Were trip blanks received? Do all samples have the proper pH? ID's Collection Dates/Times Who was notified? Who was notified? Who was notified? MS/MSD? i= Is splitting samples required? F On COC? f Acid -T- Base 1 Liter Plastic 7 16 oz Amb. Unp- 1 Liter Amb. HCL- 3a, 500 mL Amb. 7Bisulfate- 500 mL Plastic 8oz AmblClear Meoh- 250 mL Amb. 2 00 mL Plastic 4oz AmblClear Flashpoint Col./Bacteria 2oz AmblClear DI- Other Glass Other Plastic Encore Thiosulfate- SOC Kit Plastic Bag Frozen: Sulfuric- Perchlorate Zi lock . 5..� �',. o.� � - r r ..3/�E'.-f.' <.✓ ' r 4"y„ - k✓' s r r'". r,,k n"�a.? .•s' �T'�Y,.-%, Y'C `.:, ; `y- '" -yam," L �,wii� �.�!A!)Fb;� s� -�- - :..-- �; 'r^:.::, � �- ;� � � f Unp- 1 Liter Amb. 1 Liter Plastic 16 oz Amb. HCL- 500 mL Amb. 500 mL Plastic 8oz AmblClear Meoh- 250 mL Amb. 250 mL Plastic 4oz Amb/Clear Bisulfate- Col./Bacteria Flashpoint 2oz AmblClear DI- Other Plastic Other Glass Encore Thiosulfate- SOC Kit Plastic Bag Frozen: Sulfuric- Perchlorate Ziplock Comments: