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HomeMy WebLinkAboutRA-4570_26305_CA_LAB_20200218_Laboratory Data REV1This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Case Narrative 2/18/20 13:01 Withers & Ravenel Kevin Buchanan 115 Mackenan Dr. BUILDING 117 Cary, NC 27511 Project: Sam Puckett Project No.: 02170214.22 Lab Submittal Date: 01/31/2020 Work Order: 0020001 Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL Senior Project Manager Reviewed ByAngela D. Overcash Angela D. Overcash Senior Project Manager Data Qualifiers Key Reference: A Probable lab contaminant. Method Detection LimitMDL Below Reporting LimitBRL Relative Percent DifferenceRPD *Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Sample Receipt Summary 02/18/2020 Work Order: 0020001 Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received 0020001-01 01/28/20 10:48MW-1 01/31/20 16:10Water 0020001-02 01/28/20 13:10MW-2 01/31/20 16:10Water 0020001-03 01/28/20 13:24MW-2D 01/31/20 16:10Water 0020001-04 01/28/20 14:20MW-3R 01/31/20 16:10Water 0020001-05 01/28/20 12:16MW-4 01/31/20 16:10Water 0020001-06 01/28/20 12:32MW-4D 01/31/20 16:10Water 0020001-07 01/28/20 12:00MW-5 01/31/20 16:10Water 0020001-08 01/28/20 11:48MW-6 01/31/20 16:10Water 0020001-09 01/28/20 10:40MW-7 01/31/20 16:10Water 0020001-10 01/28/20 11:10MW-8 01/31/20 16:10Water 0020001-11 01/28/20 14:35MW-9 01/31/20 16:10Water 0020001-12 01/28/20 16:06WSW-2 01/31/20 16:10Water 0020001-13 01/28/20 15:23WSW-3 Pre 01/31/20 16:10Water 0020001-14 01/28/20 15:00WSW-3 Post 01/31/20 16:10Water 0020001-15 01/28/20 15:48WSW-8 01/31/20 16:10Water Samples were received in good condition at 2.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Client ID ResultParameterMethod UnitsWaypoint ID Work Order: 0020001 02/18/2020 Summary of Detections 7.5 ug/L0020001-01 MW-1 1,2-Dibromoethane (EDB)*504.1 870 ug/L0020001-01 MW-1 1,2,4-Trimethylbenzene *SM6200 B 8.7 ug/L0020001-01 MW-1 1,2-Dibromoethane *SM6200 B 5.7 ug/L0020001-01 MW-1 1,2-Dichloropropane *SM6200 B 280 ug/L0020001-01 MW-1 1,3,5-Trimethylbenzene *SM6200 B 5.1 ug/L0020001-01 MW-1 4-Isopropyltoluene *SM6200 B 11 ug/L0020001-01 MW-1 Acetone *SM6200 B 350 ug/L0020001-01 MW-1 Benzene *SM6200 B 10 ug/L0020001-01 MW-1 Bromobenzene *SM6200 B 1300 ug/L0020001-01 MW-1 Ethylbenzene *SM6200 B 51 ug/L0020001-01 MW-1 Isopropylbenzene (Cumene)*SM6200 B 4800 ug/L0020001-01 MW-1 m,p-Xylenes *SM6200 B 5.5 ug/L0020001-01 MW-1 Methyl Butyl Ketone (2-Hexanone)*SM6200 B 4.2 ug/L0020001-01 MW-1 Methyl Isobutyl Ketone *SM6200 B 240 ug/L0020001-01 MW-1 Naphthalene *SM6200 B 7.0 ug/L0020001-01 MW-1 n-Butylbenzene *SM6200 B 110 ug/L0020001-01 MW-1 n-Propylbenzene *SM6200 B 2400 ug/L0020001-01 MW-1 o-Xylene *SM6200 B 5.7 ug/L0020001-01 MW-1 sec-Butylbenzene *SM6200 B 10 ug/L0020001-01 MW-1 Styrene *SM6200 B 0.54 ug/L0020001-01 MW-1 tert-Butylbenzene *SM6200 B 10000 ug/L0020001-01 MW-1 Toluene *SM6200 B 7200 ug/L0020001-01 MW-1 Xylenes, total *SM6200 B 55 ug/L0020001-08 MW-6 1,2-Dibromoethane (EDB)*504.1 240 ug/L0020001-08 MW-6 1,2,4-Trimethylbenzene *SM6200 B 130 ug/L0020001-08 MW-6 1,3,5-Trimethylbenzene *SM6200 B 360 ug/L0020001-08 MW-6 Benzene *SM6200 B 92 ug/L0020001-08 MW-6 Ethylbenzene *SM6200 B 800 ug/L0020001-08 MW-6 m,p-Xylenes *SM6200 B 530 ug/L0020001-08 MW-6 o-Xylene *SM6200 B 480 ug/L0020001-08 MW-6 Toluene *SM6200 B 1300 ug/L0020001-08 MW-6 Xylenes, total *SM6200 B 0.043 ug/L0020001-13 WSW-3 Pre 1,2-Dibromoethane (EDB)*504.1 0.041 ug/L0020001-14 WSW-3 Post 1,2-Dibromoethane (EDB)*504.1 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-1 Sample ID: 0020001-01 Work Order: 0020001 Time Collected: 01/28/20 10:48 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD 7.5 *504.1 P0B0033200.44 2/4/20 20:59 NMBug/L 0.0531,2-Dibromoethane (EDB) BRL *504.1 P0B003310.022 2/4/20 11:43 NMBug/L 0.00281,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.131,2,4-Trichlorobenzene 870 *SM6200 B P0B0095100502/7/20 14:58 JLBug/L 5.41,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 15:43 JLBug/L 0.171,2-Dibromo-3-chloropropane 8.7 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0661,2-Dichloroethane 5.7 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.111,2-Dichloropropane 280 *SM6200 B P0B0095100502/7/20 14:58 JLBug/L 7.61,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 15:43 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0504-Chlorotoluene 5.1 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.0894-Isopropyltoluene 11 *SM6200 B P0B00951102/6/20 15:43 JLBug/L 0.31Acetone 350 *SM6200 B P0B0095100502/7/20 14:58 JLBug/L 4.8Benzene 10 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 15:43 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.079cis-1,3-Dichloropropylene This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-1 Sample ID: 0020001-01 Work Order: 0020001 Time Collected: 01/28/20 10:48 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.081Dibromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 15:43 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 15:43 JLBug/L 27Ethanol 1300 *SM6200 B P0B0095100502/7/20 14:58 JLBug/L 6.1Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 15:43 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.050Isopropyl Ether 51 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.054Isopropylbenzene (Cumene) 4800 *SM6200 B P0B00951001002/7/20 14:58 JLBug/L 12m,p-Xylenes 5.5 *SM6200 B P0B009511.0 2/6/20 15:43 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 15:43 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) 4.2 *SM6200 B P0B009511.0 2/6/20 15:43 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 15:43 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 15:43 JLBug/L 0.042Methyl-tert-Butyl Ether 240 *SM6200 B P0B00951001002/7/20 14:58 JLBug/L 19Naphthalene 7.0 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.076n-Butylbenzene 110 *SM6200 B P0B0095100502/7/20 14:58 JLBug/L 8.7n-Propylbenzene 2400 *SM6200 B P0B0095100502/7/20 14:58 JLBug/L 4.4o-Xylene 5.7 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.076sec-Butylbenzene 10 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.047Styrene 0.54 *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.098Tetrachloroethylene 10000 *SM6200 B P0B009510005002/7/20 18:37 JLBug/L 44Toluene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 15:43 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 15:43 JLBug/L 0.097Vinyl chloride 7200 *SM6200 B P0B00951001502/7/20 14:58 JLBug/L 15Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13096 %Dibromofluoromethane 70-13070 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-2 Sample ID: 0020001-02 Work Order: 0020001 Time Collected: 01/28/20 13:10 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.021 2/4/20 12:17 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.021 2/4/20 12:17 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B011112.0 2/7/20 14:08 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B011112.0 2/7/20 14:08 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B01111102/7/20 14:08 JLBug/L 0.31Acetone BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.048Benzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.040Bromoform BRL *SM6200 B P0B011111.0 2/7/20 14:08 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.076Chloroform BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-2 Sample ID: 0020001-02 Work Order: 0020001 Time Collected: 01/28/20 13:10 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B011111.0 2/7/20 14:08 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B011112002/7/20 14:08 JLBug/L 27Ethanol BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B011112.0 2/7/20 14:08 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B011111.0 2/7/20 14:08 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B011111.0 2/7/20 14:08 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B011115.0 2/7/20 14:08 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B011111.0 2/7/20 14:08 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B011112.0 2/7/20 14:08 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B011111.0 2/7/20 14:08 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B011111.0 2/7/20 14:08 JLBAug/L 0.19Naphthalene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.047Styrene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.044Toluene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B011115.0 2/7/20 14:08 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B011110.50 2/7/20 14:08 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B011111.5 2/7/20 14:08 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13097 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-2D Sample ID: 0020001-03 Work Order: 0020001 Time Collected: 01/28/20 13:24 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.020 2/4/20 12:52 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.020 2/4/20 12:52 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B011112.0 2/7/20 14:33 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B011112.0 2/7/20 14:33 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B01111102/7/20 14:33 JLBug/L 0.31Acetone BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.048Benzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.040Bromoform BRL *SM6200 B P0B011111.0 2/7/20 14:33 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.076Chloroform BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-2D Sample ID: 0020001-03 Work Order: 0020001 Time Collected: 01/28/20 13:24 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B011111.0 2/7/20 14:33 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B011112002/7/20 14:33 JLBug/L 27Ethanol BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B011112.0 2/7/20 14:33 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B011111.0 2/7/20 14:33 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B011111.0 2/7/20 14:33 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B011115.0 2/7/20 14:33 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B011111.0 2/7/20 14:33 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B011112.0 2/7/20 14:33 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B011111.0 2/7/20 14:33 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B011111.0 2/7/20 14:33 JLBAug/L 0.19Naphthalene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.047Styrene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.044Toluene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B011115.0 2/7/20 14:33 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B011110.50 2/7/20 14:33 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B011111.5 2/7/20 14:33 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13096 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-3R Sample ID: 0020001-04 Work Order: 0020001 Time Collected: 01/28/20 14:20 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.021 2/4/20 13:27 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.021 2/4/20 13:27 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 16:57 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 16:57 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 16:57 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 16:57 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-3R Sample ID: 0020001-04 Work Order: 0020001 Time Collected: 01/28/20 14:20 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 16:57 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 16:57 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 16:57 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 16:57 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 16:57 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 16:57 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 16:57 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 16:57 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 16:57 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 16:57 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 16:57 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 16:57 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 16:57 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13099 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-4 Sample ID: 0020001-05 Work Order: 0020001 Time Collected: 01/28/20 12:16 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.020 2/4/20 14:01 NMBug/L 0.00241,2-Dibromoethane (EDB) BRL *504.1 P0B003310.020 2/4/20 14:01 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 17:22 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 17:22 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 17:22 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 17:22 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-4 Sample ID: 0020001-05 Work Order: 0020001 Time Collected: 01/28/20 12:16 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 17:22 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 17:22 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 17:22 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 17:22 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 17:22 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 17:22 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 17:22 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 17:22 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 17:22 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 17:22 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 17:22 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 17:22 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 17:22 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13098 %Dibromofluoromethane 70-13099 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-4D Sample ID: 0020001-06 Work Order: 0020001 Time Collected: 01/28/20 12:32 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.021 2/4/20 14:36 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.021 2/4/20 14:36 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 17:47 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 17:47 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 17:47 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 17:47 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-4D Sample ID: 0020001-06 Work Order: 0020001 Time Collected: 01/28/20 12:32 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 17:47 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 17:47 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 17:47 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 17:47 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 17:47 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 17:47 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 17:47 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 17:47 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 17:47 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 17:47 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 17:47 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 17:47 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 17:47 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13098 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-5 Sample ID: 0020001-07 Work Order: 0020001 Time Collected: 01/28/20 12:00 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.021 2/4/20 15:11 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.021 2/4/20 15:11 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 18:12 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 18:12 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 18:12 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 18:12 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-5 Sample ID: 0020001-07 Work Order: 0020001 Time Collected: 01/28/20 12:00 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 18:12 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 18:12 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 18:12 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 18:12 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 18:12 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 18:12 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 18:12 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 18:12 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 18:12 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 18:12 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 18:12 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 18:12 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 18:12 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13096 %Dibromofluoromethane 70-13098 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-6 Sample ID: 0020001-08 Work Order: 0020001 Time Collected: 01/28/20 11:48 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD 55 *504.1 P0B00331002.1 2/4/20 21:34 NMBug/L 0.251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.021 2/4/20 15:46 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.11,1,1-Trichloroethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 3.61,1,2,2-Tetrachloroethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.61,1,2-Trichloroethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 8.31,1-Dichloroethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 8.31,1-Dichloroethylene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.11,1-Dichloropropylene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 401,2,3-Trichlorobenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 141,2,3-Trichloropropane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 131,2,4-Trichlorobenzene 240 *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.41,2,4-Trimethylbenzene BRL *SM6200 B P0B01111002002/7/20 20:46 JLBug/L 171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.11,2-Dibromoethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.61,2-Dichlorobenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.61,2-Dichloroethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 111,2-Dichloropropane 130 *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.61,3,5-Trimethylbenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.41,3-Dichlorobenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 4.31,3-Dichloropropane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.01,4-Dichlorobenzene BRL *SM6200 B P0B01111002002/7/20 20:46 JLBug/L 112,2-Dichloropropane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.62-Chlorotoluene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.04-Chlorotoluene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 8.94-Isopropyltoluene BRL *SM6200 B P0B011110010002/7/20 20:46 JLBug/L 31Acetone 360 *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 4.8Benzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.7Bromobenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 14Bromochloromethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.2Bromodichloromethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 4.0Bromoform BRL *SM6200 B P0B01111001002/7/20 20:46 JLBug/L 18Bromomethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 11Carbon Tetrachloride BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.2Chlorobenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 22Chloroethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.6Chloroform BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.9Chloromethane BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.6cis-1,2-Dichloroethylene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.9cis-1,3-Dichloropropylene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 8.1Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-6 Sample ID: 0020001-08 Work Order: 0020001 Time Collected: 01/28/20 11:48 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.5Dibromomethane BRL *SM6200 B P0B01111001002/7/20 20:46 JLBug/L 11Dichlorodifluoromethane BRL *SM6200 B P0B0111100200002/7/20 20:46 JLBug/L 2700Ethanol 92 *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.1Ethylbenzene BRL *SM6200 B P0B01111002002/7/20 20:46 JLBug/L 16Hexachlorobutadiene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.0Isopropyl Ether BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 5.4Isopropylbenzene (Cumene) 800 *SM6200 B P0B01111001002/7/20 20:46 JLBug/L 12m,p-Xylenes BRL *SM6200 B P0B01111001002/7/20 20:46 JLBug/L 6.5Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B01111005002/7/20 20:46 JLBug/L 24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B01111001002/7/20 20:46 JLBug/L 7.8Methyl Isobutyl Ketone BRL *SM6200 B P0B01111002002/7/20 20:46 JLBug/L 8.3Methylene Chloride BRL *SM6200 B P0B01111001002/7/20 20:46 JLBug/L 4.2Methyl-tert-Butyl Ether BRL *SM6200 B P0B01111001002/7/20 20:46 JLBug/L 19Naphthalene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.6n-Butylbenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 8.7n-Propylbenzene 530 *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 4.4o-Xylene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.6sec-Butylbenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 4.7Styrene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 8.8tert-Butylbenzene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 9.8Tetrachloroethylene 480 *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 4.4Toluene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.0trans-1,2-Dichloroethylene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 12trans-1,3-Dichloropropylene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 7.8Trichloroethylene BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 6.2Trichlorofluoromethane BRL *SM6200 B P0B01111005002/7/20 20:46 JLBug/L 6.0Vinyl acetate BRL *SM6200 B P0B0111100502/7/20 20:46 JLBug/L 9.7Vinyl chloride 1300 *SM6200 B P0B01111001502/7/20 20:46 JLBug/L 15Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13096 %Dibromofluoromethane 70-13096 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-7 Sample ID: 0020001-09 Work Order: 0020001 Time Collected: 01/28/20 10:40 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.021 2/4/20 16:21 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.021 2/4/20 16:21 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 18:37 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 18:37 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 18:37 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 18:37 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-7 Sample ID: 0020001-09 Work Order: 0020001 Time Collected: 01/28/20 10:40 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 18:37 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 18:37 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 18:37 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 18:37 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 18:37 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 18:37 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 18:37 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 18:37 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 18:37 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 18:37 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 18:37 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 18:37 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 18:37 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13099 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-8 Sample ID: 0020001-10 Work Order: 0020001 Time Collected: 01/28/20 11:10 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.020 2/4/20 16:56 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.020 2/4/20 16:56 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 19:02 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 19:02 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 19:02 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 19:02 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-8 Sample ID: 0020001-10 Work Order: 0020001 Time Collected: 01/28/20 11:10 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 19:02 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 19:02 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 19:02 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 19:02 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 19:02 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 19:02 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 19:02 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 19:02 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 19:02 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 19:02 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 19:02 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 19:02 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 19:02 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130102 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13098 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-9 Sample ID: 0020001-11 Work Order: 0020001 Time Collected: 01/28/20 14:35 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.020 2/4/20 18:06 NMBug/L 0.00241,2-Dibromoethane (EDB) BRL *504.1 P0B003310.020 2/4/20 18:06 NMBug/L 0.00251,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 19:27 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 19:27 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 19:27 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 19:27 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: MW-9 Sample ID: 0020001-11 Work Order: 0020001 Time Collected: 01/28/20 14:35 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 19:27 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 19:27 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 19:27 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 19:27 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 19:27 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 19:27 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 19:27 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 19:27 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 19:27 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 19:27 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 19:27 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 19:27 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 19:27 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13098 %Dibromofluoromethane 70-13098 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: WSW-2 Sample ID: 0020001-12 Work Order: 0020001 Time Collected: 01/28/20 16:06 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.020 2/4/20 18:40 NMBug/L 0.00241,2-Dibromoethane (EDB) BRL *504.1 P0B003310.020 2/4/20 18:40 NMBug/L 0.00251,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 19:52 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 19:52 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 19:52 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 19:52 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: WSW-2 Sample ID: 0020001-12 Work Order: 0020001 Time Collected: 01/28/20 16:06 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 19:52 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 19:52 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 19:52 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 19:52 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 19:52 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 19:52 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 19:52 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 19:52 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 19:52 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 19:52 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 19:52 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 19:52 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 19:52 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13097 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: WSW-3 Pre Sample ID: 0020001-13 Work Order: 0020001 Time Collected: 01/28/20 15:23 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD 0.043 *504.1 P0B003310.021 2/4/20 19:15 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.021 2/4/20 19:15 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 20:17 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 20:17 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 20:17 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 20:17 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: WSW-3 Pre Sample ID: 0020001-13 Work Order: 0020001 Time Collected: 01/28/20 15:23 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 20:17 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 20:17 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 20:17 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 20:17 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 20:17 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 20:17 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 20:17 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 20:17 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 20:17 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 20:17 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 20:17 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 20:17 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 20:17 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13096 %Dibromofluoromethane 70-13098 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: WSW-3 Post Sample ID: 0020001-14 Work Order: 0020001 Time Collected: 01/28/20 15:00 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD 0.041 *504.1 P0B003310.021 2/4/20 19:50 NMBug/L 0.00251,2-Dibromoethane (EDB) BRL *504.1 P0B003310.021 2/4/20 19:50 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 20:42 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 20:42 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 20:42 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 20:42 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: WSW-3 Post Sample ID: 0020001-14 Work Order: 0020001 Time Collected: 01/28/20 15:00 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 20:42 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 20:42 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 20:42 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 20:42 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 20:42 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 20:42 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 20:42 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 20:42 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 20:42 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 20:42 JLBug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 20:42 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 20:42 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 20:42 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13098 %Dibromofluoromethane 70-13098 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: WSW-8 Sample ID: 0020001-15 Work Order: 0020001 Time Collected: 01/28/20 15:48 Time Submitted: 01/31/20 16:10 02170214.22 Volatile Organic Compounds by GC/ECD BRL *504.1 P0B003310.020 2/4/20 20:25 NMBug/L 0.00241,2-Dibromoethane (EDB) BRL *504.1 P0B003310.020 2/4/20 20:25 NMBug/L 0.00261,2-Dibromo-3-chloropropane Volatile Organic Compounds by GC/MS BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0831,1-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.131,2,4-Trichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0541,2,4-Trimethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 21:07 JLBug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0511,2-Dibromoethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0761,2-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0661,2-Dichloroethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.111,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0431,3-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P0B009512.0 2/6/20 21:07 JLBug/L 0.112,2-Dichloropropane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0662-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0504-Chlorotoluene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.0894-Isopropyltoluene BRL *SM6200 B P0B00951102/6/20 21:07 JLBug/L 0.31Acetone BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.048Benzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.057Bromobenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.14Bromochloromethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.062Bromodichloromethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.040Bromoform BRL *SM6200 B P0B009511.0 2/6/20 21:07 JLBug/L 0.18Bromomethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.11Carbon Tetrachloride BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.062Chlorobenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.22Chloroethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.076Chloroform BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.079Chloromethane BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report 02/18/2020 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Sample Matrix: Water Client Sample ID: WSW-8 Sample ID: 0020001-15 Work Order: 0020001 Time Collected: 01/28/20 15:48 Time Submitted: 01/31/20 16:10 02170214.22 BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.065Dibromomethane BRL *SM6200 B P0B009511.0 2/6/20 21:07 JLBug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P0B009512002/6/20 21:07 JLBug/L 27Ethanol BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.061Ethylbenzene BRL *SM6200 B P0B009512.0 2/6/20 21:07 JLBug/L 0.16Hexachlorobutadiene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.050Isopropyl Ether BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.054Isopropylbenzene (Cumene) BRL *SM6200 B P0B009511.0 2/6/20 21:07 JLBug/L 0.12m,p-Xylenes BRL *SM6200 B P0B009511.0 2/6/20 21:07 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P0B009515.0 2/6/20 21:07 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P0B009511.0 2/6/20 21:07 JLBug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P0B009512.0 2/6/20 21:07 JLBug/L 0.083Methylene Chloride BRL *SM6200 B P0B009511.0 2/6/20 21:07 JLBug/L 0.042Methyl-tert-Butyl Ether BRL *SM6200 B P0B009511.0 2/6/20 21:07 JLBAug/L 0.19Naphthalene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.076n-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.087n-Propylbenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.044o-Xylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.076sec-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.047Styrene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.088tert-Butylbenzene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.098Tetrachloroethylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.044Toluene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.078Trichloroethylene BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.062Trichlorofluoromethane BRL *SM6200 B P0B009515.0 2/6/20 21:07 JLBug/L 0.060Vinyl acetate BRL *SM6200 B P0B009510.50 2/6/20 21:07 JLBug/L 0.097Vinyl chloride BRL *SM6200 B P0B009511.5 2/6/20 21:07 JLBug/L 0.15Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13098 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0095 - 5030B Blank (P0B0095-BLK1)Prepared & Analyzed: 02/06/20 1,1,1,2-Tetrachloroethane ug/LBRL0.50 1,1,1-Trichloroethane ug/LBRL0.50 1,1,2,2-Tetrachloroethane ug/LBRL0.50 1,1,2-Trichloroethane ug/LBRL0.50 1,1-Dichloroethane ug/LBRL0.50 1,1-Dichloroethylene ug/LBRL0.50 1,1-Dichloropropylene ug/LBRL0.50 1,2,3-Trichlorobenzene ug/LBRL0.50 1,2,3-Trichloropropane ug/LBRL0.50 1,2,4-Trichlorobenzene ug/LBRL0.50 1,2,4-Trimethylbenzene ug/LBRL0.50 1,2-Dibromo-3-chloropropane ug/LBRL2.0 1,2-Dibromoethane ug/LBRL0.50 1,2-Dichlorobenzene ug/LBRL0.50 1,2-Dichloroethane ug/LBRL0.50 1,2-Dichloropropane ug/LBRL0.50 1,3,5-Trimethylbenzene ug/LBRL0.50 1,3-Dichlorobenzene ug/LBRL0.50 1,3-Dichloropropane ug/LBRL0.50 1,4-Dichlorobenzene ug/LBRL0.50 2,2-Dichloropropane ug/LBRL2.0 2-Chlorotoluene ug/LBRL0.50 4-Chlorotoluene ug/LBRL0.50 4-Isopropyltoluene ug/LBRL0.50 Acetone ug/LBRL10 Benzene ug/LBRL0.50 Bromobenzene ug/LBRL0.50 Bromochloromethane ug/LBRL0.50 Bromodichloromethane ug/LBRL0.50 Bromoform ug/LBRL0.50 Bromomethane ug/LBRL1.0 Carbon Tetrachloride ug/LBRL0.50 Chlorobenzene ug/LBRL0.50 Chloroethane ug/LBRL0.50 Chloroform ug/LBRL0.50 Chloromethane ug/LBRL0.50 cis-1,2-Dichloroethylene ug/LBRL0.50 cis-1,3-Dichloropropylene ug/LBRL0.50 Dibromochloromethane ug/LBRL0.50 Dibromomethane ug/LBRL0.50 Dichlorodifluoromethane ug/LBRL1.0 Ethanol ug/LBRL200 Ethylbenzene ug/LBRL0.50 Hexachlorobutadiene ug/LBRL2.0 Isopropyl Ether ug/LBRL0.50 Isopropylbenzene (Cumene)ug/LBRL0.50 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0095 - 5030B Blank (P0B0095-BLK1)Prepared & Analyzed: 02/06/20 m,p-Xylenes ug/LBRL1.0 Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0 Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0 Methyl Isobutyl Ketone ug/LBRL1.0 Methylene Chloride ug/LBRL2.0 Methyl-tert-Butyl Ether ug/LBRL1.0 Naphthalene ug/LBRL1.0 n-Butylbenzene ug/LBRL0.50 n-Propylbenzene ug/LBRL0.50 o-Xylene ug/LBRL0.50 sec-Butylbenzene ug/LBRL0.50 Styrene ug/LBRL0.50 tert-Butylbenzene ug/LBRL0.50 Tetrachloroethylene ug/LBRL0.50 Toluene ug/LBRL0.50 trans-1,2-Dichloroethylene ug/LBRL0.50 trans-1,3-Dichloropropylene ug/LBRL0.50 Trichloroethylene ug/LBRL0.50 Trichlorofluoromethane ug/LBRL0.50 Vinyl acetate ug/LBRL5.0 Vinyl chloride ug/LBRL0.50 Xylenes, total ug/LBRL1.5 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.9 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9849.0 ug/L 50.00 70-130Surrogate: Toluene-d8 9949.4 LCS (P0B0095-BS1)Prepared & Analyzed: 02/06/20 1,1,1,2-Tetrachloroethane ug/L22.8 0.50 20.00 70-130114 1,1,1-Trichloroethane ug/L20.8 0.50 20.00 70-130104 1,1,2,2-Tetrachloroethane ug/L20.7 0.50 20.00 70-130104 1,1,2-Trichloroethane ug/L20.6 0.50 20.00 70-130103 1,1-Dichloroethane ug/L20.5 0.50 20.00 70-130103 1,1-Dichloroethylene ug/L20.1 0.50 20.00 70-130100 1,1-Dichloropropylene ug/L20.2 0.50 20.00 70-130101 1,2,3-Trichlorobenzene ug/L23.0 0.50 20.00 70-130115 1,2,3-Trichloropropane ug/L21.0 0.50 20.00 70-130105 1,2,4-Trichlorobenzene ug/L21.3 0.50 20.00 70-130107 1,2,4-Trimethylbenzene ug/L19.8 0.50 20.00 70-13099 1,2-Dibromo-3-chloropropane ug/L21.9 2.0 20.00 70-130110 1,2-Dibromoethane ug/L21.2 0.50 20.00 70-130106 1,2-Dichlorobenzene ug/L19.8 0.50 20.00 70-13099 1,2-Dichloroethane ug/L19.5 0.50 20.00 70-13098 1,2-Dichloropropane ug/L20.4 0.50 20.00 70-130102 1,3,5-Trimethylbenzene ug/L19.5 0.50 20.00 70-13097 1,3-Dichlorobenzene ug/L19.6 0.50 20.00 70-13098 1,3-Dichloropropane ug/L20.6 0.50 20.00 70-130103 1,4-Dichlorobenzene ug/L19.5 0.50 20.00 70-13097 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0095 - 5030B LCS (P0B0095-BS1)Prepared & Analyzed: 02/06/20 2,2-Dichloropropane ug/L21.7 2.0 20.00 70-130108 2-Chlorotoluene ug/L19.5 0.50 20.00 70-13098 4-Chlorotoluene ug/L19.7 0.50 20.00 70-13099 4-Isopropyltoluene ug/L19.7 0.50 20.00 70-13098 Acetone ug/L28.9 10 40.00 40-16072 Benzene ug/L20.1 0.50 20.00 70-130100 Bromobenzene ug/L20.3 0.50 20.00 70-130101 Bromochloromethane ug/L21.1 0.50 20.00 70-130106 Bromodichloromethane ug/L21.1 0.50 20.00 70-130105 Bromoform ug/L20.8 0.50 20.00 70-130104 Bromomethane ug/L25.2 1.0 20.00 60-140126 Carbon Tetrachloride ug/L21.9 0.50 20.00 70-130109 Chlorobenzene ug/L19.7 0.50 20.00 70-13098 Chloroethane ug/L17.8 0.50 20.00 60-14089 Chloroform ug/L20.4 0.50 20.00 70-130102 Chloromethane ug/L18.0 0.50 20.00 60-14090 cis-1,2-Dichloroethylene ug/L19.8 0.50 20.00 70-13099 cis-1,3-Dichloropropylene ug/L20.8 0.50 20.00 70-130104 Dibromochloromethane ug/L22.4 0.50 20.00 70-130112 Dibromomethane ug/L20.8 0.50 20.00 70-130104 Dichlorodifluoromethane ug/L19.3 1.0 20.00 60-14097 Ethanol ug/L574 200 500.0 60-140115 Ethylbenzene ug/L20.0 0.50 20.00 70-130100 Hexachlorobutadiene ug/L20.6 2.0 20.00 70-130103 Isopropyl Ether ug/L20.4 0.50 20.00 70-130102 Isopropylbenzene (Cumene)ug/L20.0 0.50 20.00 70-130100 m,p-Xylenes ug/L40.8 1.0 40.00 70-130102 Methyl Butyl Ketone (2-Hexanone)ug/L20.9 1.0 20.00 60-140104 Methyl Ethyl Ketone (2-Butanone)ug/L17.7 5.0 20.00 60-14088 Methyl Isobutyl Ketone ug/L21.7 1.0 20.00 60-140108 Methylene Chloride ug/L20.5 2.0 20.00 70-130102 Methyl-tert-Butyl Ether ug/L20.1 1.0 20.00 70-130101 Naphthalene ug/L21.0 1.0 20.00 70-130105 n-Butylbenzene ug/L19.6 0.50 20.00 70-13098 n-Propylbenzene ug/L19.6 0.50 20.00 70-13098 o-Xylene ug/L20.2 0.50 20.00 70-130101 sec-Butylbenzene ug/L19.6 0.50 20.00 70-13098 Styrene ug/L20.5 0.50 20.00 70-130102 tert-Butylbenzene ug/L19.6 0.50 20.00 70-13098 Tetrachloroethylene ug/L20.2 0.50 20.00 70-130101 Toluene ug/L19.9 0.50 20.00 70-130100 trans-1,2-Dichloroethylene ug/L19.6 0.50 20.00 70-13098 trans-1,3-Dichloropropylene ug/L21.7 0.50 20.00 70-130109 Trichloroethylene ug/L19.3 0.50 20.00 70-13096 Trichlorofluoromethane ug/L22.2 0.50 20.00 60-140111 Vinyl acetate ug/L23.6 5.0 20.00 60-140118 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0095 - 5030B LCS (P0B0095-BS1)Prepared & Analyzed: 02/06/20 Vinyl chloride ug/L20.6 0.50 20.00 60-140103 Xylenes, total ug/L61.1 1.5 60.00 70-130102 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.5 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.8 ug/L 50.00 70-130Surrogate: Toluene-d8 9949.5 Matrix Spike (P0B0095-MS1)Prepared & Analyzed: 02/06/20 Source: 0020001-04 1,1,1,2-Tetrachloroethane ug/L2305.0 200.0 BRL 70-130115 1,1,1-Trichloroethane ug/L2245.0 200.0 BRL 70-130112 1,1,2,2-Tetrachloroethane ug/L2095.0 200.0 BRL 70-130105 1,1,2-Trichloroethane ug/L2155.0 200.0 BRL 70-130108 1,1-Dichloroethane ug/L2235.0 200.0 BRL 70-130112 1,1-Dichloroethylene ug/L2175.0 200.0 BRL 70-130109 1,1-Dichloropropylene ug/L2205.0 200.0 BRL 70-130110 1,2,3-Trichlorobenzene ug/L2225.0 200.0 BRL 70-130111 1,2,3-Trichloropropane ug/L2085.0 200.0 BRL 70-130104 1,2,4-Trichlorobenzene ug/L2205.0 200.0 BRL 70-130110 1,2,4-Trimethylbenzene ug/L2145.0 200.0 BRL 70-130107 1,2-Dibromo-3-chloropropane ug/L20920 200.0 BRL 70-130105 1,2-Dibromoethane ug/L2145.0 200.0 BRL 70-130107 1,2-Dichlorobenzene ug/L2115.0 200.0 BRL 70-130105 1,2-Dichloroethane ug/L2055.0 200.0 BRL 70-130103 1,2-Dichloropropane ug/L2145.0 200.0 BRL 70-130107 1,3,5-Trimethylbenzene ug/L2135.0 200.0 BRL 70-130106 1,3-Dichlorobenzene ug/L2095.0 200.0 BRL 70-130104 1,3-Dichloropropane ug/L2105.0 200.0 BRL 70-130105 1,4-Dichlorobenzene ug/L2105.0 200.0 BRL 70-130105 2,2-Dichloropropane ug/L22120 200.0 BRL 70-130110 2-Chlorotoluene ug/L2145.0 200.0 BRL 70-130107 4-Chlorotoluene ug/L2145.0 200.0 BRL 70-130107 4-Isopropyltoluene ug/L2155.0 200.0 BRL 70-130108 Acetone ug/L278 100 400.0 BRL 40-16070 Benzene ug/L2155.0 200.0 BRL 70-130108 Bromobenzene ug/L2165.0 200.0 BRL 70-130108 Bromochloromethane ug/L2305.0 200.0 BRL 70-130115 Bromodichloromethane ug/L2165.0 200.0 BRL 70-130108 Bromoform ug/L1925.0 200.0 BRL 70-13096 Bromomethane ug/L24910 200.0 BRL 60-140124 Carbon Tetrachloride ug/L2235.0 200.0 BRL 70-130111 Chlorobenzene ug/L2125.0 200.0 BRL 70-130106 Chloroethane ug/L1925.0 200.0 BRL 60-14096 Chloroform ug/L2235.0 200.0 BRL 70-130112 Chloromethane ug/L1915.0 200.0 BRL 60-14096 cis-1,2-Dichloroethylene ug/L2125.0 200.0 BRL 70-130106 cis-1,3-Dichloropropylene ug/L2115.0 200.0 BRL 70-130106 Dibromochloromethane ug/L2155.0 200.0 BRL 70-130108 Dibromomethane ug/L2165.0 200.0 BRL 70-130108 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0095 - 5030B Matrix Spike (P0B0095-MS1)Prepared & Analyzed: 02/06/20 Source: 0020001-04 Dichlorodifluoromethane ug/L20010 200.0 BRL 60-140100 Ethanol ug/L5450 2000 5000 BRL 60-140109 Ethylbenzene ug/L2165.0 200.0 BRL 70-130108 Hexachlorobutadiene ug/L22220 200.0 BRL 70-130111 Isopropyl Ether ug/L2155.0 200.0 BRL 70-130107 Isopropylbenzene (Cumene)ug/L2195.0 200.0 BRL 70-130109 m,p-Xylenes ug/L43810 400.0 BRL 70-130110 Methyl Butyl Ketone (2-Hexanone)ug/L19610 200.0 BRL 60-14098 Methyl Ethyl Ketone (2-Butanone)ug/L16650 200.0 BRL 60-14083 Methyl Isobutyl Ketone ug/L20610 200.0 BRL 60-140103 Methylene Chloride ug/L21420 200.0 BRL 70-130107 Methyl-tert-Butyl Ether ug/L20810 200.0 BRL 70-130104 Naphthalene ug/L20010 200.0 BRL 70-130100 n-Butylbenzene ug/L2125.0 200.0 BRL 70-130106 n-Propylbenzene ug/L2135.0 200.0 BRL 70-130107 o-Xylene ug/L2175.0 200.0 BRL 70-130108 sec-Butylbenzene ug/L2175.0 200.0 BRL 70-130108 Styrene ug/L2185.0 200.0 BRL 70-130109 tert-Butylbenzene ug/L2145.0 200.0 BRL 70-130107 Tetrachloroethylene ug/L2145.0 200.0 BRL 70-130107 Toluene ug/L2165.0 200.0 0.470 70-130108 trans-1,2-Dichloroethylene ug/L2145.0 200.0 BRL 70-130107 trans-1,3-Dichloropropylene ug/L2185.0 200.0 BRL 70-130109 Trichloroethylene ug/L2065.0 200.0 BRL 70-130103 Trichlorofluoromethane ug/L2295.0 200.0 BRL 60-140114 Vinyl acetate ug/L25050 200.0 BRL 60-140125 Vinyl chloride ug/L2145.0 200.0 BRL 60-140107 Xylenes, total ug/L65615 600.0 BRL 70-130109 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.3 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.4 ug/L 50.00 70-130Surrogate: Toluene-d8 9748.7 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0095 - 5030B Matrix Spike Dup (P0B0095-MSD1)Prepared & Analyzed: 02/06/20 Source: 0020001-04 1,1,1,2-Tetrachloroethane ug/L2305.0 200.0 BRL 2070-130115 0.3 1,1,1-Trichloroethane ug/L2165.0 200.0 BRL 2070-130108 4 1,1,2,2-Tetrachloroethane ug/L2135.0 200.0 BRL 2070-130107 2 1,1,2-Trichloroethane ug/L2145.0 200.0 BRL 2070-130107 0.5 1,1-Dichloroethane ug/L2175.0 200.0 BRL 2070-130109 3 1,1-Dichloroethylene ug/L2085.0 200.0 BRL 2070-130104 4 1,1-Dichloropropylene ug/L2135.0 200.0 BRL 2070-130106 4 1,2,3-Trichlorobenzene ug/L2355.0 200.0 BRL 2070-130117 6 1,2,3-Trichloropropane ug/L2135.0 200.0 BRL 2070-130106 2 1,2,4-Trichlorobenzene ug/L2235.0 200.0 BRL 2070-130112 2 1,2,4-Trimethylbenzene ug/L2095.0 200.0 BRL 2070-130104 3 1,2-Dibromo-3-chloropropane ug/L21520 200.0 BRL 2070-130108 3 1,2-Dibromoethane ug/L2125.0 200.0 BRL 2070-130106 0.8 1,2-Dichlorobenzene ug/L2085.0 200.0 BRL 2070-130104 1 1,2-Dichloroethane ug/L2025.0 200.0 BRL 2070-130101 2 1,2-Dichloropropane ug/L2135.0 200.0 BRL 2070-130106 0.6 1,3,5-Trimethylbenzene ug/L2085.0 200.0 BRL 2070-130104 2 1,3-Dichlorobenzene ug/L2065.0 200.0 BRL 2070-130103 1 1,3-Dichloropropane ug/L2135.0 200.0 BRL 2070-130106 1 1,4-Dichlorobenzene ug/L2075.0 200.0 BRL 2070-130103 1 2,2-Dichloropropane ug/L21420 200.0 BRL 2070-130107 3 2-Chlorotoluene ug/L2065.0 200.0 BRL 2070-130103 3 4-Chlorotoluene ug/L2085.0 200.0 BRL 2070-130104 3 4-Isopropyltoluene ug/L2105.0 200.0 BRL 2070-130105 2 Acetone ug/L276 100 400.0 BRL 2040-16069 1 Benzene ug/L2125.0 200.0 BRL 2070-130106 1 Bromobenzene ug/L2145.0 200.0 BRL 2070-130107 1 Bromochloromethane ug/L2225.0 200.0 BRL 2070-130111 3 Bromodichloromethane ug/L2135.0 200.0 BRL 2070-130106 1 Bromoform ug/L1965.0 200.0 BRL 2070-13098 2 Bromomethane ug/L24210 200.0 BRL 2060-140121 3 Carbon Tetrachloride ug/L2215.0 200.0 BRL 2070-130110 0.9 Chlorobenzene ug/L2085.0 200.0 BRL 2070-130104 2 Chloroethane ug/L1715.0 200.0 BRL 2060-14085 12 Chloroform ug/L2185.0 200.0 BRL 2070-130109 2 Chloromethane ug/L1815.0 200.0 BRL 2060-14090 6 cis-1,2-Dichloroethylene ug/L2055.0 200.0 BRL 2070-130103 3 cis-1,3-Dichloropropylene ug/L2115.0 200.0 BRL 2070-130105 0.05 Dibromochloromethane ug/L2235.0 200.0 BRL 2070-130111 3 Dibromomethane ug/L2185.0 200.0 BRL 2070-130109 0.9 Dichlorodifluoromethane ug/L19110 200.0 BRL 2060-14096 4 Ethanol ug/L5510 2000 5000 BRL 2060-140110 1 Ethylbenzene ug/L2105.0 200.0 BRL 2070-130105 3 Hexachlorobutadiene ug/L22020 200.0 BRL 2070-130110 1 Isopropyl Ether ug/L2135.0 200.0 BRL 2070-130106 1 Isopropylbenzene (Cumene)ug/L2115.0 200.0 BRL 2070-130106 3 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0095 - 5030B Matrix Spike Dup (P0B0095-MSD1)Prepared & Analyzed: 02/06/20 Source: 0020001-04 m,p-Xylenes ug/L42910 400.0 BRL 2070-130107 2 Methyl Butyl Ketone (2-Hexanone)ug/L20110 200.0 BRL 2060-140101 3 Methyl Ethyl Ketone (2-Butanone)ug/L17050 200.0 BRL 2060-14085 3 Methyl Isobutyl Ketone ug/L20910 200.0 BRL 2060-140105 1 Methylene Chloride ug/L211 20 200.0 BRL 2070-130105 2 Methyl-tert-Butyl Ether ug/L20910 200.0 BRL 2070-130105 0.5 Naphthalene ug/L21410 200.0 BRL 2070-130107 7 n-Butylbenzene ug/L2045.0 200.0 BRL 2170-130102 4 n-Propylbenzene ug/L2085.0 200.0 BRL 1870-130104 3 o-Xylene ug/L2145.0 200.0 BRL 2070-130107 2 sec-Butylbenzene ug/L2075.0 200.0 BRL 2070-130103 5 Styrene ug/L2155.0 200.0 BRL 2070-130108 1 tert-Butylbenzene ug/L2085.0 200.0 BRL 2070-130104 3 Tetrachloroethylene ug/L2085.0 200.0 BRL 2070-130104 3 Toluene ug/L2115.0 200.0 0.470 2070-130105 2 trans-1,2-Dichloroethylene ug/L2075.0 200.0 BRL 2070-130104 3 trans-1,3-Dichloropropylene ug/L2195.0 200.0 BRL 2070-130109 0.5 Trichloroethylene ug/L1985.0 200.0 BRL 2070-13099 4 Trichlorofluoromethane ug/L2175.0 200.0 BRL 2060-140109 5 Vinyl acetate ug/L25450 200.0 BRL 2060-140127 2 Vinyl chloride ug/L2095.0 200.0 BRL 2060-140105 2 Xylenes, total ug/L64315 600.0 BRL 2070-130107 2 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9648.1 ug/L 50.00 70-130Surrogate: Toluene-d8 9848.9 Batch P0B0111 - SM6200 B Blank (P0B0111-BLK1)Prepared & Analyzed: 02/07/20 1,1,1,2-Tetrachloroethane ug/LBRL0.50 1,1,1-Trichloroethane ug/LBRL0.50 1,1,2,2-Tetrachloroethane ug/LBRL0.50 1,1,2-Trichloroethane ug/LBRL0.50 1,1-Dichloroethane ug/LBRL0.50 1,1-Dichloroethylene ug/LBRL0.50 1,1-Dichloropropylene ug/LBRL0.50 1,2,3-Trichlorobenzene ug/LBRL0.50 1,2,3-Trichloropropane ug/LBRL0.50 1,2,4-Trichlorobenzene ug/LBRL0.50 1,2,4-Trimethylbenzene ug/LBRL0.50 1,2-Dibromo-3-chloropropane ug/LBRL2.0 1,2-Dibromoethane ug/LBRL0.50 1,2-Dichlorobenzene ug/LBRL0.50 1,2-Dichloroethane ug/LBRL0.50 1,2-Dichloropropane ug/LBRL0.50 1,3,5-Trimethylbenzene ug/LBRL0.50 1,3-Dichlorobenzene ug/LBRL0.50 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0111 - SM6200 B Blank (P0B0111-BLK1)Prepared & Analyzed: 02/07/20 1,3-Dichloropropane ug/LBRL0.50 1,4-Dichlorobenzene ug/LBRL0.50 2,2-Dichloropropane ug/LBRL2.0 2-Chlorotoluene ug/LBRL0.50 4-Chlorotoluene ug/LBRL0.50 4-Isopropyltoluene ug/LBRL0.50 Acetone ug/LBRL10 Benzene ug/LBRL0.50 Bromobenzene ug/LBRL0.50 Bromochloromethane ug/LBRL0.50 Bromodichloromethane ug/LBRL0.50 Bromoform ug/LBRL0.50 Bromomethane ug/LBRL1.0 Carbon Tetrachloride ug/LBRL0.50 Chlorobenzene ug/LBRL0.50 Chloroethane ug/LBRL0.50 Chloroform ug/LBRL0.50 Chloromethane ug/LBRL0.50 cis-1,2-Dichloroethylene ug/LBRL0.50 cis-1,3-Dichloropropylene ug/LBRL0.50 Dibromochloromethane ug/LBRL0.50 Dibromomethane ug/LBRL0.50 Dichlorodifluoromethane ug/LBRL1.0 Ethanol ug/LBRL200 Ethylbenzene ug/LBRL0.50 Hexachlorobutadiene ug/LBRL2.0 Isopropyl Ether ug/LBRL0.50 Isopropylbenzene (Cumene)ug/LBRL0.50 m,p-Xylenes ug/LBRL1.0 Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0 Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0 Methyl Isobutyl Ketone ug/LBRL1.0 Methylene Chloride ug/LBRL2.0 Methyl-tert-Butyl Ether ug/LBRL1.0 Naphthalene ug/LBRL1.0 n-Butylbenzene ug/LBRL0.50 n-Propylbenzene ug/LBRL0.50 o-Xylene ug/LBRL0.50 sec-Butylbenzene ug/LBRL0.50 Styrene ug/LBRL0.50 tert-Butylbenzene ug/LBRL0.50 Tetrachloroethylene ug/LBRL0.50 Toluene ug/LBRL0.50 trans-1,2-Dichloroethylene ug/LBRL0.50 trans-1,3-Dichloropropylene ug/LBRL0.50 Trichloroethylene ug/LBRL0.50 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0111 - SM6200 B Blank (P0B0111-BLK1)Prepared & Analyzed: 02/07/20 Trichlorofluoromethane ug/LBRL0.50 Vinyl acetate ug/LBRL5.0 Vinyl chloride ug/LBRL0.50 Xylenes, total ug/LBRL1.5 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.7 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.4 ug/L 50.00 70-130Surrogate: Toluene-d8 9648.2 LCS (P0B0111-BS1)Prepared & Analyzed: 02/07/20 1,1,1,2-Tetrachloroethane ug/L23.9 0.50 20.00 70-130120 1,1,1-Trichloroethane ug/L22.3 0.50 20.00 70-130112 1,1,2,2-Tetrachloroethane ug/L21.6 0.50 20.00 70-130108 1,1,2-Trichloroethane ug/L21.8 0.50 20.00 70-130109 1,1-Dichloroethane ug/L22.4 0.50 20.00 70-130112 1,1-Dichloroethylene ug/L21.7 0.50 20.00 70-130108 1,1-Dichloropropylene ug/L21.9 0.50 20.00 70-130110 1,2,3-Trichlorobenzene ug/L24.5 0.50 20.00 70-130122 1,2,3-Trichloropropane ug/L21.6 0.50 20.00 70-130108 1,2,4-Trichlorobenzene ug/L22.9 0.50 20.00 70-130114 1,2,4-Trimethylbenzene ug/L21.0 0.50 20.00 70-130105 1,2-Dibromo-3-chloropropane ug/L24.0 2.0 20.00 70-130120 1,2-Dibromoethane ug/L22.0 0.50 20.00 70-130110 1,2-Dichlorobenzene ug/L21.2 0.50 20.00 70-130106 1,2-Dichloroethane ug/L20.6 0.50 20.00 70-130103 1,2-Dichloropropane ug/L21.6 0.50 20.00 70-130108 1,3,5-Trimethylbenzene ug/L21.0 0.50 20.00 70-130105 1,3-Dichlorobenzene ug/L21.0 0.50 20.00 70-130105 1,3-Dichloropropane ug/L21.6 0.50 20.00 70-130108 1,4-Dichlorobenzene ug/L20.8 0.50 20.00 70-130104 2,2-Dichloropropane ug/L23.8 2.0 20.00 70-130119 2-Chlorotoluene ug/L20.8 0.50 20.00 70-130104 4-Chlorotoluene ug/L21.2 0.50 20.00 70-130106 4-Isopropyltoluene ug/L21.3 0.50 20.00 70-130107 Acetone ug/L30.9 10 40.00 40-16077 Benzene ug/L21.7 0.50 20.00 70-130108 Bromobenzene ug/L21.6 0.50 20.00 70-130108 Bromochloromethane ug/L23.2 0.50 20.00 70-130116 Bromodichloromethane ug/L22.2 0.50 20.00 70-130111 Bromoform ug/L21.1 0.50 20.00 70-130105 Bromomethane ug/L23.2 1.0 20.00 60-140116 Carbon Tetrachloride ug/L23.6 0.50 20.00 70-130118 Chlorobenzene ug/L21.1 0.50 20.00 70-130106 Chloroethane ug/L16.3 0.50 20.00 60-14081 Chloroform ug/L22.1 0.50 20.00 70-130110 Chloromethane ug/L18.6 0.50 20.00 60-14093 cis-1,2-Dichloroethylene ug/L21.0 0.50 20.00 70-130105 cis-1,3-Dichloropropylene ug/L21.9 0.50 20.00 70-130110 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P0B0111 - SM6200 B LCS (P0B0111-BS1)Prepared & Analyzed: 02/07/20 Dibromochloromethane ug/L23.0 0.50 20.00 70-130115 Dibromomethane ug/L22.0 0.50 20.00 70-130110 Dichlorodifluoromethane ug/L18.8 1.0 20.00 60-14094 Ethanol ug/L639 200 500.0 60-140128 Ethylbenzene ug/L21.5 0.50 20.00 70-130107 Hexachlorobutadiene ug/L23.1 2.0 20.00 70-130116 Isopropyl Ether ug/L21.8 0.50 20.00 70-130109 Isopropylbenzene (Cumene)ug/L21.3 0.50 20.00 70-130106 m,p-Xylenes ug/L43.8 1.0 40.00 70-130109 Methyl Butyl Ketone (2-Hexanone)ug/L22.2 1.0 20.00 60-140111 Methyl Ethyl Ketone (2-Butanone)ug/L18.6 5.0 20.00 60-14093 Methyl Isobutyl Ketone ug/L23.1 1.0 20.00 60-140115 Methylene Chloride ug/L21.6 2.0 20.00 70-130108 Methyl-tert-Butyl Ether ug/L21.3 1.0 20.00 70-130107 Naphthalene ug/L22.0 1.0 20.00 70-130110 n-Butylbenzene ug/L21.0 0.50 20.00 70-130105 n-Propylbenzene ug/L21.1 0.50 20.00 70-130106 o-Xylene ug/L21.4 0.50 20.00 70-130107 sec-Butylbenzene ug/L21.3 0.50 20.00 70-130107 Styrene ug/L21.7 0.50 20.00 70-130109 tert-Butylbenzene ug/L21.2 0.50 20.00 70-130106 Tetrachloroethylene ug/L21.8 0.50 20.00 70-130109 Toluene ug/L21.6 0.50 20.00 70-130108 trans-1,2-Dichloroethylene ug/L21.3 0.50 20.00 70-130106 trans-1,3-Dichloropropylene ug/L22.6 0.50 20.00 70-130113 Trichloroethylene ug/L21.0 0.50 20.00 70-130105 Trichlorofluoromethane ug/L22.6 0.50 20.00 60-140113 Vinyl acetate ug/L24.5 5.0 20.00 60-140123 Vinyl chloride ug/L21.2 0.50 20.00 60-140106 Xylenes, total ug/L65.2 1.5 60.00 70-130109 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.5 ug/L 50.00 70-130Surrogate: Toluene-d8 9748.6 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 2/18/20 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.22 Project: Sam PuckettWithers & Ravenel Cary, NC 27511 Attn: Kevin Buchanan Work Order: 0020001 Time Submitted: 1/31/2020 4:10:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/ECD - Quality Control Batch P0B0033 - 504.1 Blank (P0B0033-BLK1)Prepared & Analyzed: 02/04/20 1,2-Dibromoethane (EDB)ug/LBRL0.020 1,2-Dibromo-3-chloropropane ug/LBRL0.020 LCS (P0B0033-BS1)Prepared & Analyzed: 02/04/20 1,2-Dibromoethane (EDB)ug/L0.229 0.020 0.2500 70-13092 1,2-Dibromo-3-chloropropane ug/L0.247 0.020 0.2500 70-13099 Duplicate (P0B0033-DUP1)Prepared & Analyzed: 02/04/20 Source: 0020001-14 1,2-Dibromoethane (EDB)ug/L0.0409 0.020 0.0411 2000.3 1,2-Dibromo-3-chloropropane ug/LBRL0.020 BRL 200 Matrix Spike (P0B0033-MS1)Prepared & Analyzed: 02/04/20 Source: 0020001-15 1,2-Dibromoethane (EDB)ug/L0.198 0.021 0.2589 BRL 70-13076 1,2-Dibromo-3-chloropropane ug/L0.212 0.021 0.2589 BRL 70-13082 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Sample Extraction Data Prep Method: 504.1 Lab Number Batch Date/TimeInitialFinal P0B00330020001-01 02/04/20 10:0031.8 35mL mL P0B00330020001-01 02/04/20 10:0031.8 35mL mL P0B00330020001-02 02/04/20 10:0034.1 35mL mL P0B00330020001-03 02/04/20 10:0034.2 35mL mL P0B00330020001-04 02/04/20 10:0033.3 35mL mL P0B00330020001-05 02/04/20 10:0034.3 35mL mL P0B00330020001-06 02/04/20 10:0033.9 35mL mL P0B00330020001-07 02/04/20 10:0033.7 35mL mL P0B00330020001-08 02/04/20 10:0033.8 35mL mL P0B00330020001-08 02/04/20 10:0033.8 35mL mL P0B00330020001-09 02/04/20 10:0033.7 35mL mL P0B00330020001-10 02/04/20 10:0034.2 35mL mL P0B00330020001-11 02/04/20 10:0034.5 35mL mL P0B00330020001-12 02/04/20 10:0034.4 35mL mL P0B00330020001-13 02/04/20 10:0033.7 35mL mL P0B00330020001-14 02/04/20 10:0034.1 35mL mL P0B00330020001-15 02/04/20 10:0034.3 35mL mL Prep Method: 5030B Lab Number Batch Date/TimeInitialFinal P0B00950020001-01 02/06/20 8:0010 10mL mL P0B00950020001-01 02/06/20 8:0010 10mL mL P0B00950020001-01 02/06/20 8:0010 10mL mL P0B00950020001-04 02/06/20 8:0010 10mL mL P0B00950020001-05 02/06/20 8:0010 10mL mL P0B00950020001-06 02/06/20 8:0010 10mL mL P0B00950020001-07 02/06/20 8:0010 10mL mL P0B00950020001-09 02/06/20 8:0010 10mL mL P0B00950020001-10 02/06/20 8:0010 10mL mL P0B00950020001-11 02/06/20 8:0010 10mL mL P0B00950020001-12 02/06/20 8:0010 10mL mL P0B00950020001-13 02/06/20 8:0010 10mL mL P0B00950020001-14 02/06/20 8:0010 10mL mL P0B00950020001-15 02/06/20 8:0010 10mL mL Prep Method: SM6200 B Lab Number Batch Date/TimeInitialFinal P0B01110020001-02 02/07/20 9:2310 10mL mL P0B01110020001-03 02/07/20 9:2310 10mL mL P0B01110020001-08 02/07/20 9:2310 10mL mL This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409